25035_National Welders Supply Soil Exc Rpt_20230607

Via Email
June 7, 2023
NCDEQ – Division of Waste Management Brownfields Redevelopment Section
1646 Mail Service Center Raleigh, North Carolina 27699-1646 Attn: Mr. Bill Schmithorst

Re: Soil Excavation Report National Welders Supply Gesco Street and State Street
Charlotte, North Carolina Brownfields Project No. 25035-21-060 H&H Project No. RMR-013
Dear Bill On behalf of RRPVI Gesco Charlotte LP, please find the enclosed Soil Excavation Report prepared for the above-referenced Brownfields property located in Charlotte, Mecklenburg County. Should
you have questions or need additional information, please do not hesitate to contact us. Sincerely,
Hart & Hickman, PC
Alexis McKenzie, PE Ralph McGee, PG Senior Project Engineer Senior Project Manager
Enclosures
cc: Ms. Rachel Russel Krenz, Ram Realty Advisors (via email) Mr. Quinn Augustine, Ram Realty Advisors (via email) Ms. Karen Geller, Ram Realty Advisors (via email) Ms. Amanda Short, Parker Poe (via email)
Attachment:
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Soil Excavation Report National Welders Supply Gesco Street and State Street Charlotte, North Carolina H&H Job No. RMR-013 Table of Contents
1.0 Introduction .............................................................................................................................1
1.1 Site History ............................................................................................................................1
1.2 Previous Assessment Activities .............................................................................................2
2.0 Soil Excavation Activities .......................................................................................................6
2.1 Soil Screening Activities .......................................................................................................6
2.2 Confirmation Soil Sampling Activities .................................................................................7
2.3 Post-Excavation Confirmation Soil Sample Results .............................................................9
2.4 Direct Contact Risk Evaluation ...........................................................................................10
3.0 Post-Excavation Soil Gas Sampling Activities ...................................................................11
3.1 Soil Gas Sampling Methodology ..........................................................................................11
3.2 Soil Gas Sample Analytical Results .....................................................................................13
3.3 Vapor Intrusion Risk Evaluation .........................................................................................14
4.0 Quality Assurance – Quality Control ..................................................................................16
5.0 Summary and Conclusions ..................................................................................................17

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List of Tables

Table 1 Summary of Post-Excavation Confirmation Soil Sample Analytical Data
Table 2 Summary of Post-Excavation Soil Gas Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Previous Sample Location Map
Figure 3 Source Area Sample Location Map
Figure 4 Post-Excavation Sample Location Map

List of Appendices
Appendix A Waste Manifests
Appendix B Summary of Excavation Field Screening Results
Appendix C Laboratory Analytical Reports
Appendix D DEQ Risk Calculators
Appendix E Boring Logs
Appendix F Field Forms

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Soil Excavation Report National Welders Supply Gesco Street and State Street Charlotte, North Carolina H&H Job No. RMR-013 1.0 Introduction
On behalf of RRPVI Gesco Charlotte LP (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this report to document removal of impacted soil discovered at the National
Welders Supply Brownfields property (Brownfields Project No. 25035-21-060) located at Gesco
Street and State Street in Charlotte, Mecklenburg County, North Carolina (Site or subject Site).
The Site consists of two adjacent parcels bisected by Gesco Street in a rapidly densifying mixed-
use area approximately one mile northwest of uptown Charlotte. A Site location map is provided
as Figure 1.

The parcel to the west of Gesco Street (Mecklenburg County Parcel ID No. {PIN} 07108103) is
approximately 2.98-acres and is currently being developed with multi-family residential
apartment buildings identified as Building A (Left) and Building A (Right), plus surface parking
and a pool and amenity area. The parcel to the east of Gesco Street (PIN 07107806) is
approximately 0.89-acre and is being developed with a multi-family residential apartment
building identified as Building B with associated surface parking. An overlay of the proposed
redevelopment plan is included in Figure 2.

1.1 Site History
The Site historically consisted of undeveloped agricultural land and a rail spur located in the
western portion of the Site prior to the construction of an industrial warehouse building in the
northern portion of the Site west of Gesco Street in the 1940s. The southwestern portion of the
Site (west of Gesco Street) was developed with an industrial facility in the late 1950s or early
1960s. Portions of the Site located east of Gesco Street were utilized for parking but have
otherwise remained undeveloped. The Site buildings were occupied by National Welders Supply
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and utilized for sale and distribution of compressed welding gasses. The southwestern Site
building was also utilized for wholesale storage and distribution of steel.

The northernmost portion of the National Welders Supply facility was removed in the 1980s and
remaining portions of the northern Site buildings were razed in the mid-2010s. The
southwestern Site building was razed in 2017, and the Site has remained undeveloped vacant
land since that time.

1.2 Previous Assessment Activities

As part of initial property transaction due diligence activities, H&H completed a Phase I ESA at
the Site and identified environmental concerns associated with historical on-Site and nearby off-
Site operations. To address environmental concerns and the potential for persistent impacts
associated with historical on-Site and nearby off-Site operations, a Brownfields Property
Application for the Site was submitted to the North Carolina Department of Environmental
Quality (DEQ) on May 3, 2021. The Site received eligibility into the DEQ Brownfields
Redevelopment Section in a letter dated October 18, 2021.

Based on results of the Phase I ESA, H&H performed Phase II ESA activities at the Site in
August 2021 which included the collection of soil, groundwater, and soil gas samples for
laboratory analysis. The locations of the Phase II ESA soil, groundwater, and soil gas samples
are shown in Figure 2.

Results of groundwater assessment activities identified concentrations of chloroform, carbon
tetrachloride, and trichloroethene (TCE) at concentrations above the DEQ 2L Groundwater
Quality Standards (2L Standards) and/or the DEQ Vapor Intrusion Groundwater Screening
Levels (GWSLs) in samples collected in the northern and western portions of the Site. Results
of soil gas sampling identified multiple petroleum-related compounds and chlorinated solvents at
concentrations exceeding the DEQ Vapor Intrusion Sub-slab and Exterior Soil Gas Screening
Levels (SGSLs). Most notably, soil gas sample SG-2, collected from the northern portion of the
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Site in the area of the former National Welders Supply facility indicated the presence of TCE at a
concentration of 290,000 micrograms per cubic meter (µg/m3) as compared to the DEQ
Residential Vapor Intrusion SGSL of 14 µg/m3.

Based on the results of the Phase II ESA sampling activities, it was determined that the lower
levels of TCE in groundwater were unlikely to be the source of TCE concentrations detected in
the SG-2 soil gas sample and that additional assessment was needed to evaluate the potential for
a soil source in the northern portion of the Site. In May 2022, H&H completed Brownfields
assessment activities at the National Welders Supply property in accordance with a DEQ-
approved Brownfields Assessment Work Plan dated May 9, 2022.

Brownfields assessment activities included the advancement and sampling of nine soil borings,
the installation and sampling of one temporary groundwater monitoring well, and the installation
and sampling of one soil gas point to evaluate the potential of an undocumented release to soil in
the area of Phase II ESA soil gas sample SG-2 collected within the footprint of the northern
former National Welders Supply facility. The locations of the May 2022 Brownfields
assessment sample locations are shown in Figure 3.

Results of soil sample analytical data indicated that TCE was detected at concentrations above
the laboratory method detection limit in eight of the nine soil samples. TCE concentrations were
detected at concentrations above the DEQ Protection of Groundwater Preliminary Soil
Remediation Goal (PSRG) in six of the nine soil samples. Based on results of the soil
assessment activities, it was determined that TCE impacted soil was limited to an isolated area
within the building footprint of the former National Welders Supply facility in the northern
portion of the Site nearest State Street and west of Gesco Street (Figure 3).

Temporary groundwater monitoring well TMW-8 was installed and sampled immediately east
and hydraulically downgradient of the area of TCE soil impacts. Results of groundwater sample
analytical data indicated that TCE (up to 32.4 µg/L) was detected in the TMW-8 groundwater
sample and its duplicate groundwater sample GW-DUP at concentrations above the DEQ 2L
Standard and the DEQ Residential and Non-Residential Vapor Intrusion GWSLs. TCE
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concentrations detected in the TMW-8 groundwater sample collected downgradient of the TCE
soil impacts are higher than the TCE concentrations detected in the Phase II ESA TMW-1 and
TMW-2 groundwater samples collected upgradient of the TCE soil impacts. The higher TCE
concentration in groundwater downgradient of the impacted soil is consistent with the soil
sample analytical results indicating the potential for impacts to groundwater from the soil source
discovered in the footprint of the former National Welders supply building.

H&H installed and sampled a temporary soil gas sampling point in the location of the Phase II
ESA SG-2 soil gas sample to confirm the results of the initial sample. The soil gas analytical
results from the confirmation SG-2 soil gas sample indicated that TCE was detected at a
concentration of 102,000 µg/m3 which was considered to generally be consistent with the initial
SG-2 soil gas sample results.

Similar to the original SG-2 soil gas sample collected during the Phase II ESA, the TCE
concentrations in the SG-2 confirmation soil gas sample are not indicative of predicted soil gas
concentrations from a groundwater source. A soil gas concentration assuming a worst-case
groundwater concentration of 32.4 µg/L (TMW-8) using Henry’s Law calculations is 12,960
µg/m3. The calculated soil gas concentration is an order of magnitude below the actual detected
values at the Site. This further confirms the soil sample results and indicates soil impacts are the
primary contribution of TCE detected in the SG-2 soil gas samples.

Based on 1) soil samples with TCE exceedances of the DEQ Protection of Groundwater PSRG,
2) elevated TCE concentrations in groundwater downgradient of the TCE soil source area
compared to samples collected upgradient of the soil impacts, and 3) detected soil gas
concentrations an order of magnitude above the calculated value assuming a groundwater source,
H&H concluded that a TCE soil source was present in an isolated area within the footprint of the
former northern National Welders Supply facility. Based on results of the assessment activities
completed at the Site, DEQ Brownfields requested removal of the impacted soil prior to
approving residential use for this portion of the Site.

To reduce soil gas concentrations and the risk of potential structural vapor intrusion into the
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proposed residential building in the northwestern portion of the Brownfields property, H&H
prepared a Soil Excavation Work Plan (Work Plan) dated August 11, 2022, which received DEQ
approval on August 26, 2022. In addition, H&H prepared an Environmental Management Plan
for the proposed redevelopment dated June 21, 2022, which received DEQ approval on August
8, 2022. Following approval of the Work Plan, DEQ requested additional confirmation sampling
following removal of impacted soil including the installation and sampling of two temporary soil
gas monitoring points within the backfilled excavation area.

Soil excavation activities, and the post-excavation confirmation soil and soil gas sampling
activities and results are summarized in the following sections.
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2.0 Soil Excavation Activities

Between October 24 and November 9, 2022, H&H provided oversight during the removal of
TCE-impacted soil discovered in the northwestern portion of the Site and delineated to be within
the footprint of the former National Welders Supply facility. The soil removal activities were
completed pursuant to the DEQ-approved Work Plan and DEQ-approved EMP. Prior to
completing the excavation activities, H&H teamed with the general contractor to mark utilities in
the area planned for excavations.

Soil was excavated to approximately 9 feet below ground surface (ft bgs), which is the
approximate depth to groundwater in the northwestern portion of the Site. Approximately 2,600
cubic yards of soil was excavated using a track-mounted backhoe excavator, direct loaded onto
trucks, and transported off-Site for disposal at the Republic Services municipal solid waste
landfill located in Concord, North Carolina. Waste manifests documenting the transport and off-
Site disposal of impacted soil are included in Appendix A.

2.1 Soil Screening Activities
H&H collected soil samples from the excavation for field screening using a calibrated
photoionization detector (PID) and a hand-held gas chromatograph calibrated to measure TCE
concentrations. The field screening was completed as an additional tool during excavation
activities to assist with the removal of impacted soil. The excavation was initially advanced to
the approximate extents outlined in Figure 3, as determined by the results of the Brownfields soil
assessment completed in May 2022. H&H used the calibrated PID and handheld gas
chromatograph to screen soil at various locations and depths along the initial excavation extents.
Following removal of soil to the initial estimated extents (Figure 3), post-excavation field
screening results indicated that TCE concentrations remained in soil at measurable levels and the
excavation was expanded to the final excavation extents as shown in Figure 4.

Upon expansion of the excavation, soil sample aliquots were collected from shallow (0-3 ft bgs),
middle (3-6 ft bgs), and deeper (6-9 ft bgs) depth intervals at locations every approximate 10
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linear feet of the excavation sidewalls. The shallow, middle, and deep aliquot samples were field
screened for the presence of volatile organic vapors using a calibrated PID. The depth interval
exhibiting the highest PID reading was then screened for the presence of TCE using a hand-held
gas chromatograph. Based on results of field screening, post-excavation soil samples were
collected for laboratory analysis to confirm that soil impacts were adequately removed. The
post-excavation confirmation soil sample locations (denoted by EX-SB nomenclature) are shown
in Figure 4.

Field screening results indicated that TCE was not present at measurable levels in the screened
samples with the exception of low levels detected in soil samples EX-SB-3, EX-SB-9, EX-
SB-15, and EX-SB-23. Although field screening results indicated the presence of TCE at
measurable levels, H&H collected the soil samples for laboratory analysis at these locations due
to spatial constraints associated with utility corridors near State Street and Gesco Street on the
northern and eastern Site boundaries (EX-SB-3 and EX-SB-9) and based on the PID readings
consistent with other locations at which TCE was not present based on gas chromatograph
measurements (EX-SB-15). In addition, to avoid leaving the excavation open over the weekend
when precipitation was expected, soil sample EX-SB-23 was collected for laboratory analysis. A
tabular summary of PID readings and hand-held gas chromatograph measurements is included in
Appendix B.

On the afternoon of October 28, 2022, the last day of the excavation, the generator for the gas
chromatograph ran out of fuel and the instrument could not be operated. Therefore, aliquots
exhibiting the highest PID readings from EX-SB-18 through EX-SB-22, and EX-SB-24 through
EX-SB-26 were collected for laboratory analysis without screening with the gas chromatograph.

A brief summary of the post-excavation confirmation soil sampling activities is provided below.

2.2 Confirmation Soil Sampling Activities
Once the field screening results indicated that impacted soil had been adequately removed, H&H
collected post-excavation confirmation samples for laboratory analysis from the sidewalls of the
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excavation. The soil samples were collected from the soil sample aliquot (shallow, middle, or
deeper) exhibiting the highest potential for impacts based on the field screening results. Because
the excavation depths were consistent with measured depths to groundwater, soil samples were
not collected for laboratory analysis from the saturated zone at the base of the excavation.

Soil samples selected for laboratory analysis were placed in dedicated laboratory-supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory-supplied cooler with ice. The samples were submitted to Waypoint
Analytical under standard chain of custody protocols for laboratory analysis of volatile organic
compounds (VOCs) by EPA Method 8260.

Post-excavation confirmation soil sample laboratory analytical results indicated that TCE
remained in the sidewall of the excavation at concentrations above the DEQ Protection of
Groundwater PSRG in soil samples EX-SB-20, EX-SB-23, and EX-SB-25 collected along the
southwestern portion of the excavation. Based on laboratory analytical results, H&H directed
the contractor to remove additional soil in these areas. Following over-excavation activities at
the EX-SB-20, EX-SB-23, and EX-SB-25 sample locations, additional post-excavation
confirmation soil samples (EX-SB-20A, EX-SB-23A, and EX-SB-25A) were collected using the
same methodologies described above.

Prior to completion of screening activities at location EX-SB-20A, the top approximately six (6)
feet of soil was graded to reach final grade elevations for the proposed development. Soil
generated in this area during grading was loaded onto trucks and transported off-Site for disposal
at the Republic Services landfill facility with soil generated during the impacted soil removal
activities. Therefore, soil sample EX-SB-20A was collected from the sidewall at a depth interval
of 6-9 ft bgs. Note that the gas chromatograph was returned to the manufacturer and was not
used to screen post-excavation soil samples collected following removal of additional soil in
these select areas.
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2.3 Post-Excavation Confirmation Soil Sample Results
Tabular summaries of the final post-excavation soil sample analytical results are included in
Table 1. Soil sample laboratory analytical results are compared to the DEQ Protection of
Groundwater, Residential, and Industrial/Commercial PSRGs dated January 2023. A copy of the
laboratory analytical reports and chain of custody records are included in Appendix C.

As shown in Table 1, laboratory analytical results indicate that select VOCs were detected at
concentrations above the laboratory method detection limits in each sample with the exception of
EX-SB-10 at which no compounds were detected above the laboratory method detection limits.
TCE was detected above the DEQ Protection of Groundwater PSRG of 0.021 mg/kg in initial
post-excavation confirmation soil samples EX-SB-20 (0.060 mg/kg), EX-SB-23 (0.503 mg/kg),
and EX-SB-25 (0.082 mg/kg). TCE was not detected at concentrations above the DEQ
Protection of Groundwater PSRG in the remaining post-excavation confirmation soil samples
collected at the Site.

As discussed above, over-excavation activities were completed in select locations where TCE
remained at concentrations above the DEQ Protection of Groundwater PSRGs, and confirmation
samples EX-SB-20A, EX-SB-23A, and EX-SB-25A were collected for laboratory analysis
following removal of the additional soil. Laboratory analytical results indicated TCE was not
detected at concentrations above the laboratory method detection limit in soil sample EX-SB-
20A. Trace levels of TCE were detected at concentrations below the DEQ Protection of
Groundwater PSRG in the EX-SB-23A and EX-SB-25A soil samples.

Laboratory analytical results also identified 1,1,1-trichloroethane (4.58 mg/kg) at a concentration
above the DEQ Protection of Groundwater PSRG (1.4 mg/kg) in initial post-excavation
confirmation soil sample EX-SB-20. Similar to the TCE concentration, confirmation sample
EX-SB-20A indicated that 1,1,1-trichloroethane was not detected above the laboratory method
detection following over-excavation activities. No other VOCs were detected at concentrations
above the DEQ PSRGs in the confirmation soil samples collected from the excavation.
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Following completion of the excavation activities, the excavated area was backfilled using soil
generated during grading activities in the southern and eastern portions of the Site (east of Gesco
Street) where no Site operations have historically been conducted aside from surface parking
lots. In total, approximately 2,600 cubic yards of soil was removed from the on-Site borrow area
and was used to replace the soil in the TCE excavation area in accordance with the DEQ-
approved EMP and DEQ-approved Work Plan.

2.4 Direct Contact Risk Evaluation
The DEQ PSRGs used for comparison to the laboratory analytical results are conservative and
based upon a Target Cancer Risk (TCR) of 1 x 10-6 for potential carcinogenic effects and a
Target Hazard Quotient (THQ) of 0.2 for potential non-carcinogenic effects. The DEQ and EPA
acceptable level for potential carcinogenic risks is a cumulative LICR of 1 x 10-4 or less, and the
acceptable level for non-carcinogenic risks is a cumulative HI of 1.0 or less.

To further evaluate potential risks, H&H used the DEQ Risk Calculator (January 2023) and the
highest concentration of each compound detected in any post-excavation confirmation soil
sample to model a hypothetical “worst-case” risk scenario for the residential, non-residential
worker, and construction worker direct exposure pathways. A copy of the completed DEQ Risk
Calculator is provided in Appendix D, and the risk calculator results are summarized in the table
below.

As shown in the table above, the residual concentrations of organic compounds detected in the
post-excavation confirmation soil samples do not exceed unacceptable risk levels for the
residential, non-residential worker, or construction worker direct exposure pathways.
Use Scenario
Calculated
Cumulative
LICR
Calculated Cumulative HI Exceedance of Acceptable Levels?
Residential 2.0 x 10-8 0.0041 No
Non-Residential 3.5 x 10-9 0.00084 No
Construction Worker 8.1 x 10-10 0.0093 No
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3.0 Post-Excavation Soil Gas Sampling Activities

At the request of DEQ Brownfields, H&H installed and sampled two temporary soil gas
sampling points (SG-12 and SG-13) for laboratory analysis in November 2022. The additional
soil gas samples were collected to confirm TCE concentrations in soil gas within the excavation
boundaries were lower than pre-excavation concentrations following the removal of impacted
soil.

The assessment activities were completed in general accordance with DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites dated
September 2022, the DEQ Division of Waste Management (DWM) Vapor Intrusion Guidance
dated March 2018, the most recent versions of the U.S. EPA Region IV Laboratory Services and
Applied Science Division (LSASD) Field Branches Quality System and Technical Procedures
guidance, and the DEQ Brownfields Site Assessment Minimum Requirements Checklist.

3.1 Soil Gas Sampling Methodology
H&H collected two (2) soil gas samples within the extents of the excavation area. The soil gas
monitoring point borings were advanced to approximately 5.5 ft bgs utilizing a decontaminated
stainless steel hand auger on November 22, 2022. Continuous soil samples were collected in
each boring and logged for lithologic description and field screened for indication of potential
impacts by observation for staining, odors, and the presence of organic vapors using a calibrated
PID. No obvious evidence of potential impacts was observed in the soil borings based on field
screening results. Boring logs documenting lithology and field screening results are are included
in Appendix E.

The soil gas monitoring points were installed by placing an approximate 6-inch long stainless
steel vapor implant screen attached to Teflon tubing at the base of each borehole. Annular space
around the vapor implant screen was filled with a sand filter pack to a depth approximately 6
inches above the top of the screened interval. Following installation of the sand, a hydrated
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bentonite seal was placed from the top of the sand to the ground surface. The soil gas points
were allowed to equilibrate for approximately 24 hours prior to sampling.

Each soil gas sample was collected using a laboratory supplied batch certified 1-liter stainless
steel Summa sample canister connected to an in-line flow controller with a vacuum gauge using
a brass nut and ferrule assembly to form an air-tight seal. The flow regulator was pre-set by the
laboratory to regulate the vapor intake rate to approximately 100 milliliters per minute. Prior to
the collection of the soil gas samples, “shut-in” tests were conducted on the sampling train and
helium leak checks were conducted at each sampling point. A description of the shut-in test and
helium leak testing procedures is provided below.

The shut-in test was conducted by connecting the flow regulator and vacuum gauge to the
Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once
the sampling train was “closed”, the sample valve on the Summa® canister was opened and the
reading on the vacuum gauge was recorded. The Summa® canister sample valve was then
closed, and the vacuum gauge was observed to ensure no vacuum loss occurred. If the vacuum
reading remained the same, the shut-in test was considered successful. If vacuum loss occurred,
the flow regulator and/or brass cap was reseated, and the shut-in test was repeated until the
vacuum reading remained stable. Each Summa® canister passed the shut-in test.

Following a successful shut-in test, the Summa® canister was connected to the Teflon® sample
tubing using a brass nut and ferrule assembly to create an airtight seal and a leak check was
performed on each sampling point. The leak checks were conducted by constructing a shroud
around the sampling point, sample train, and Summa canister and flooding the air within the
shroud with helium gas. Helium within the shroud was monitored using a calibrated helium gas
detector and was measured between 5% and 10%. Once helium concentrations within the shroud
stabilized, a syringe and three-way valve was used to purge a minimum of three sample volumes
from the vapor implant screen, sand filter pack, and sample tubing.

Vapor from the sample tubing was collected outside of the shroud into a Tedlar bag and analyzed
using the helium gas detector to ensure that helium concentrations were less than 10% of the
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concentration measured within the shroud. Field forms documenting the successful leak checks
are included in Appendix F.

Following successful leak checks, the intake valve on the Summa canister was fully opened to
begin collection of the soil gas sample. Vacuum readings on the Summa® canister were recorded
prior to and following the sampling period to ensure adequate sample volume was collected. A
vacuum was maintained within the canister at the conclusion of the sampling event as
documented in the field form included in Appendix F.

After sample collection, the intake valve was closed, and the regulator was disconnected from
the canister. The starting and ending vacuum in the canister was recorded on the chain-of-custody
and submitted to the laboratory along with the sample. The canister was placed in laboratory
supplied shipping containers, properly labeled, and shipped under standard chain of custody
protocols to a Waypoint Analytical laboratory for analysis of VOCs by EPA Method TO-15.
3.2 Soil Gas Sample Analytical Results
A tabular summary of the soil gas sample laboratory analytical results is provided as Table 2.
Previous soil gas sample results from pre-excavation soil gas sample SG-2, collected within the
delineated TCE impacted soil area during the 2021 Phase II ESA and 2022 Brownfields
assessment, are also included in Table 2 for comparison of pre-excavation and post-excavation
compound concentrations. The analytical results were also compared to the DEQ Residential
and Non-Residential Vapor Intrusion SGSLs dated January 2023. The laboratory analytical
report and chain of custody records are provided in Appendix C.
Analytical results for soil gas samples SG-12 and SG-13 indicate that multiple VOCs were
detected at concentrations above the laboratory method detection limits in each sample.
Chloroform was detected in SG-12 up to 9.30 µg/m3 which slightly exceeds the Residential
SGSL of 4.1. Note, the chloroform concentration detected at SG-13 (3.00 µg/m3) was below the
Residential SGSL. TCE was also detected in soil gas sample SG-12 at a concentration up to 114
µg/m3, which exceeds the Residential SGSL of 14 µg/m3, and TCE was detected at SG-13 at a
concentration of 500 µg/m3 which exceeds the Residential and Non-Residential (180 µg/m3)
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SGSLs. Except for chloroform in SG-12 and TCE in both SG-12 and SG-13, no other
compounds were detected at concentrations above the DEQ Residential or Non-Residential
Vapor Intrusion SGSLs in the post-excavation soil gas samples.

In comparison to the pre-excavation compound concentrations detected in the SG-2 soil gas
samples collected in August 2021 and May 2022, the compound concentrations in the post-
excavation soil gas samples have significantly decreased. Prior to excavation activities, SG-2
soil gas sample results identified the presence of benzene, carbon tetrachloride, 1,4-
dichlorobenzene, trans-1,2-dichloroethylene, and ethylbenzene at concentrations above the
Residential SGSLs, and 1,3-butadiene, chloromethane, chloroform 1,1-dichloroethane, 1,1-
dichloroethylene, cis-1,2-dichloroethylene, hexachlorobutadiene, naphthalene, TCE, and vinyl
chloride at concentrations above Residential and Non-Residential SGSLs. Following excavation
activities, as noted above, chloroform and TCE are the only compounds detected at
concentrations above the Residential SGSLs in soil gas. The chloroform concentration
decreased from 1,200 µg/m3 to 9.30 µg/m3 and the TCE concentration decreased from 290,000
µg/m3 to 500 µg/m3, both of which indicate an approximate 99% concentration reduction.

Based on the soil gas analytical results indicating a 99% reduction in the detected TCE
concentration in soil gas following the soil excavation activities, the remaining TCE in soil gas
can be attributed to the existing groundwater impacts and will be managed through DEQ-
approved vapor intrusion mitigation measures being installed at the Site.

3.3 Vapor Intrusion Risk Evaluation

Similar to the DEQ PSRGs for comparison to compound concentrations detected in soil, the
DEQ Vapor Intrusion SGSLs used for comparison to the soil gas laboratory analytical results are
conservative and based upon a TCR of 1 x 10-6 for potential carcinogenic effects and a THQ of
0.2 for potential non-carcinogenic effects. The DEQ and EPA acceptable level for potential
carcinogenic risks is a cumulative LICR of 1 x 10-4 or less, and the acceptable level for non-
carcinogenic risks is a cumulative HI of 1.0 or less.
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To further evaluate potential vapor intrusion risks, H&H used the DEQ Risk Calculator (January
2023) and the highest concentration of each compound detected in the post-excavation soil gas
samples to model a hypothetical “worst-case” risk for the soil gas to indoor air vapor intrusion
pathway under a residential use scenario. Results of the residential risk calculator are included
below. For comparison, the table below also includes the pre-excavation residential risk
calculator results. A copy of the completed DEQ Risk Calculator is provided in Appendix D.

The results of pre- and post-excavation risk evaluations indicate the calculated cumulative risk
levels decreased by approximately 99% which is consistent with the percentage decrease in
compound concentrations detected in the post-excavation soil gas samples.

Excavation Status Calculated Cumulative LICR Calculated Cumulative HI
Pre-Excavation 1.9 x 10-2 4,200
Post-Excavation 3.5 x 10-5 7.4
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4.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated sampling equipment
was decontaminated prior to use and between each sample location or exposure to soil. H&H
also collected duplicate soil and soil gas samples for laboratory analysis. The duplicate soil
sample (EX-SB-DUP) was collected from the EX-SB-9 post-excavation confirmation soil
sample location and was collected directly into individual laboratory supplied sample containers
using sampling methodologies described in Section 2.0. The duplicate soil gas sample (SG-
DUP-112322) was collected concurrently with the parent sample at SG-12 using a laboratory
supplied T-fitting which allows for simultaneous collection of two soil gas samples from one soil
gas sampling point. The samples were analyzed for the same parameters as the parent samples,
and the analytical results were compared to those of the parent sample. The analytical results of
the parent sample and the duplicate sample were used to evaluate the cumulative precision of the
analytical method, sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1 and Table 2). Review of the duplicate sample results in comparison to
the parent sample results for the soil and soil gas samples indicates that there was no significant
variability and confirms adequate sampling and laboratory reproducibility.

Laboratory QA/QC procedures were employed to ensure appropriate sample handling and
analysis and to aid in the review and validation of the analytical data. QA/QC procedures were
conducted in accordance with the method protocols and included regular equipment
maintenance, equipment calibrations, and adherence to specific sample custody and data
management procedures. Samples were analyzed in conjunction with appropriate blanks,
laboratory duplicates, continuing calibration standards, surrogate standards, and matrix spiking
standards in accordance with approved methodologies to monitor both instrument and analyst
performance. The laboratory analytical data report and QA package for each group of samples
submitted to and analyzed by the subcontracted laboratory are provided in Appendix C. A copy
of the completed chain of custody record and shipping receipt are included in the laboratory
analytical report.
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5.0 Summary and Conclusions
Soil excavation activities have been completed at the National Welders Supply Brownfields
property located at Gesco Street and State Street in Charlotte, Mecklenburg County, North
Carolina. The remedial activities included excavation of TCE impacted soil in the former
National Welders Supply building footprint to reduce risks of potential vapor intrusion into the
proposed building. The soil excavation activities were completed in accordance with the DEQ-
approved EMP dated June 21, 2022, and the DEQ-approved Work Plan dated August 11, 2022.
A summary of the excavation activities and results of post-excavation confirmation sampling is
provided below.

During excavation activities, approximately 2,600 cubic yards of impacted soil were excavated,
loaded onto trucks, and transported off-Site for disposal at the Republic Services landfill located
in Concord, North Carolina. The results of analysis of the post-excavation confirmation soil
samples indicate that TCE impacted soil was adequately removed to unrestricted use levels that
are protective of human health. Based upon the results of health-based risk evaluations, the
residual concentrations of organic compounds detected in the post-excavation confirmation soil
samples do not exceed acceptable risk levels for the residential, non-residential, or construction
worker direct exposure pathways.

Following completion of excavation activities, two post-excavation temporary soil gas
monitoring points were installed for collection of soil gas samples within the backfilled
excavation area. Soil gas sample analytical results indicated TCE was detected at concentrations
up to 500 µg/m3, which exceeds the Residential and Non-Residential SGSLs. However, the
detected TCE concentrations indicate an approximately 99% reduction in soil gas concentrations
compared to pre-excavation soil gas sample results which identified TCE at concentrations up to
290,000 µg/m3. Therefore, the residual soil gas concentrations are attributed to lower levels of
TCE detected in groundwater which are expected to attenuate overtime following removal of the
soil source. Potential vapor intrusion risks for the proposed building in the northwestern portion
of the Site will be managed through the DEQ-approved Vapor Intrusion Mitigation Plan.
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In summary, results of soil excavation activities and post-excavation confirmation soil sampling
indicate that soil impacts above the DEQ PSRGs were successfully removed from the area in the
vicinity of the former Site building. Post-excavation soil gas samples indicate a significant
decrease in soil gas concentrations to levels likely attributable to existing groundwater impacts.
Remaining soil gas concentrations will be managed through vapor mitigation measures installed
in the new Site buildings.

Table 1Summary of Post-Excavation Confirmation Soil Sample Analytical DataNational Welders SupplyGesco Street & State StreetCharlotte, North CarolinaH&H Job No. RMR-013Sample IDEX-SB-1 EX-SB-2 EX-SB-3 EX-SB-4 EX-SB-5 EX-SB-6 EX-SB-7 EX-SB-8Depth (ft bgs)3-6 3-6 3-6 3-6 3-6 3-6 6-9 3-6Date10/26/22 10/27/22 10/27/22 10/27/22 10/27/22 10/27/22 10/27/22 10/27/22 10/28/22 10/28/2022UnitsVOCs (8260D)Acetone 0.008 J 0.005 J 0.009 J 0.007 J 0.006 J 0.007 J 0.010 J 0.009 J<0.002 <0.00225 14,000 210,000Benzene<0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.00070.01 1.2 5.4Carbon Disulfide<0.0007 <0.0007 <0.0008 <0.0007 <0.0008 <0.0008 <0.0008 <0.0007 <0.0008 <0.00084.1 160 740Chloroform<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0010.39 0.34 1.51,1-Dichloroethane<0.0009 <0.0010 <0.0010 <0.0009 <0.0010 <0.0010 <0.001 <0.0010 <0.001 <0.0010.034 3.8 171,1-Dichloroethene<0.0008 <0.0008 <0.0009 <0.00080.001 J<0.0009 <0.0009 <0.0008 <0.0009 <0.00092.5 48 210cis-1,2-Dichloroethene 0.0010 J<0.00090.004 J<0.0009 <0.0009 <0.0010 <0.0010 <0.0009 <0.0010 <0.00100.41 13 78Ethyl Tertiary Butyl Ether (ETBE) 0.003 J 0.002 J 0.008 J 0.003 J 0.006 J 0.004 J 0.008 J 0.006 J<0.001 <0.0010.23 140 600Methyl tert-butyl ether (MTBE) 0.001 J<0.00070.002 J 0.001 J 0.001 J 0.001 J 0.001 J 0.001 J<0.0008 <0.00080.09 49 220Methylene Chloride 0.002 J<0.0010.002 J 0.001 J<0.0010.001 J 0.002 J 0.002 J<0.001 <0.0010.025 58 650Toluene<0.0007 <0.0008 <0.0008 <0.0008 <0.0008 <0.0008 <0.0008 <0.0008 <0.0008 <0.00088.3 990 9,7001,1,1-Trichloroethane<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0011.4 1,700 7,600Trichloroethene 0.001 J<0.0010.001 J<0.0010.004 J<0.0010.002 J<0.0010.002 J 0.001 J 0.021 0.87 4.01,2,4-Trimethylbenzene<0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.000612 63 370Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only constituents detected in at least one sample are shown in the table above.Bold values exceed the Protection of Groundwater PSRGs.VOCs = volatile organic compounds; ft bgs = feet below ground surfaceJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kg3-6Residential PSRGs (1)Protection of Groundwater PSRGs (1)Industrial/ Commercial PSRGs (1)EX-SB-9/EX-SB-DUPhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/Soil Removal/Report/Tables/Data Tables_excavationTable 1 (Page 1 of 3)Hart & Hickman, PC
Table 1Summary of Post-Excavation Confirmation Soil Sample Analytical DataNational Welders SupplyGesco Street & State StreetCharlotte, North CarolinaH&H Job No. RMR-013Sample IDEX-SB-10 EX-SB-11 EX-SB-12 EX-SB-13 EX-SB-14 EX-SB-15 EX-SB-16 EX-SB-17 EX-SB-18 EX-SB-19Depth (ft bgs)6-9 6-9 3-6 6-9 3-6 0-3 3-6 6-9 3-6 3-6Date10/28/22 10/28/22 10/28/22 10/28/22 10/28/2022 10/28/2022 10/28/2022 10/28/2022 10/28/2022 10/28/2022UnitsVOCs (8260D)Acetone<0.002 <0.003 <0.0020.011 J 0.009 J 0.011 J 0.025 0.012 J 0.015 J 0.009 J 25 14,000 210,000Benzene<0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.00070.001 J<0.00080.001 J<0.00070.01 1.2 5.4Carbon Disulfide<0.0008 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007 <0.0008 <0.0009 <0.0008 <0.00074.1 160 740Chloroform<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0010.39 0.34 1.51,1-Dichloroethane<0.001 <0.001 <0.0009 <0.0010 <0.0009 <0.0009 <0.001 <0.001 <0.001 <0.00100.034 3.8 171,1-Dichloroethene<0.0009 <0.0009 <0.00080.005 J<0.0008 <0.0008 <0.00090.002 J<0.0010 <0.00092.5 48 210cis-1,2-Dichloroethene<0.00100.003 J 0.002 J 0.001 J<0.0009 <0.0009 <0.0010 <0.001 <0.001 <0.00090.41 13 78Ethyl Tertiary Butyl Ether (ETBE)<0.001 <0.001 <0.0009 <0.0010 <0.0010 <0.0010 <0.001 <0.001 <0.001 <0.00100.23 140 600Methyl tert-butyl ether (MTBE)<0.0008 <0.0008 <0.0007 <0.0007 <0.0007 <0.0007 <0.0008 <0.0008 <0.0008 <0.00070.09 49 220Methylene Chloride<0.0010.002 J<0.0010.002 J<0.001 <0.0010.002 J 0.002 J<0.001 <0.0010.025 58 650Toluene<0.0008 <0.0008 <0.0008 <0.0008 <0.0008 <0.00080.002 J<0.00090.002 J<0.00088.3 990 9,7001,1,1-Trichloroethane<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0011.4 1,700 7,600Trichloroethene<0.001 <0.0010.007 0.019<0.0010.015 0.008 0.014 0.001 J<0.0010.021 0.87 4.01,2,4-Trimethylbenzene<0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0007 <0.0006 <0.000612 63 370Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only constituents detected in at least one sample are shown in the table above.Bold values exceed the Protection of Groundwater PSRGs.VOCs = volatile organic compounds; ft bgs = feet below ground surfaceJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgIndustrial/ Commercial PSRGs (1)Protection of Groundwater PSRGs (1)Residential PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/Soil Removal/Report/Tables/Data Tables_excavationTable 1 (Page 2 of 3)Hart & Hickman, PC
Table 1Summary of Post-Excavation Confirmation Soil Sample Analytical DataNational Welders SupplyGesco Street & State StreetCharlotte, North CarolinaH&H Job No. RMR-013Sample IDEX-SB-20 EX-SB-20a EX-SB-21 EX-SB-22 EX-SB-23 EX-SB-23a EX-SB-24 EX-SB-25 EX-SB-25a EX-SB-26Depth (ft bgs)0-3 6-9 3-6 3-6 0-3 6-9 3-6 3-6 3-6 6-9Date10/28/2022 11/9/2022 10/28/2022 10/28/2022 10/28/2022 11/9/2022 10/28/2022 10/28/2022 11/9/2022 10/28/2022UnitsVOCs (8260D)Acetone 0.024 0.013 J 0.012 J 0.008 J 0.016 J 0.014 J 0.007 J 0.006 J 0.014 J 0.015 J 25 14,000 210,000Benzene 0.002 J<0.00070.001 J<0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.0007 <0.00070.01 1.2 5.4Carbon Disulfide<0.0007 <0.0008 <0.0008 <0.0008 <0.0007 <0.0008 <0.0007 <0.0008 <0.00070.001 J 4.1 160 740Chloroform<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0010.001 J<0.001 <0.0010.39 0.34 1.51,1-Dichloroethane 0.005 J<0.001 <0.0010 <0.0010 <0.0009 <0.001 <0.00100.001 J<0.0009 <0.0010.034 3.8 171,1-Dichloroethene 0.021<0.0009 <0.0009 <0.00090.001 J<0.0009 <0.00080.003 J<0.00080.001 J 2.5 48 210cis-1,2-Dichloroethene<0.0009 <0.0010 <0.0009 <0.00090.023 0.001 J 0.003 J 0.043 0.002 J 0.014 0.41 13 78Ethyl Tertiary Butyl Ether (ETBE)<0.0009 <0.001 <0.0010 <0.0010 <0.0010 <0.001 <0.0010 <0.001 <0.0009 <0.0010.23 140 600Methyl tert-butyl ether (MTBE)<0.0007 <0.0008 <0.0007 <0.0007 <0.0007 <0.0008 <0.0007 <0.0008 <0.0007 <0.00080.09 49 220Methylene Chloride<0.0010.007 J<0.001 <0.001 <0.0010.007 J<0.001 <0.0010.004 J<0.0010.025 58 650Toluene 0.003 J<0.00080.002 J 0.001 J<0.0008 <0.0008 <0.0008 <0.0008 <0.0007 <0.00098.3 990 9,7001,1,1-Trichloroethane4.58<0.0010.002 J<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0011.4 1,700 7,600Trichloroethene0.060<0.0010.002 J<0.0010.5030.010 0.004 J0.0820.009 0.005 J 0.021 0.87 4.01,2,4-Trimethylbenzene0.0006 J<0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.000612 63 370Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only constituents detected in at least one sample are shown in the table above.Bold values exceed the Protection of Groundwater PSRGs.VOCs = volatile organic compounds; ft bgs = feet below ground surfaceJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgIndustrial/ Commercial PSRGs (1)Protection of Groundwater PSRGs (1)Residential PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/Soil Removal/Report/Tables/Data Tables_excavationTable 1 (Page 3 of 3)Hart & Hickman, PC
Table 2Summary of Post-Excavation Soil Gas Analytical DataNational Welders SupplyGesco Street & State StreetCharlotte, North CarolinaH&H Job No. RMR-013Excavation StatusSample IDSG-13Depth (ft bgs)5.565.5Date8/11/20215/11/202211/23/2022UnitsVOCs (TO-15)Acetone<8601345.43 6.0017.5NE NEBenzene12057.10.610 J0.601 J3.26121602-Butanone (MEK)<15028.8 J0.784 J0.702 J2.8235,000440,0001,3-Butadiene<2483.5<0.328<0.328<0.3283.141Carbon Disulfide300 J65.3 J1.33 J, B1.65 J, B8.69 B4,90061,000Carbon Tetrachloride32 J<3.104.214.12<0.15516200Chlorobenzene<17<2.14<0.107<0.1072.343504,400Chloroform1,2003389.239.303.004.153Chloromethane<2412.8 J<0.067<0.0670.167 J6307,900Cyclohexane<2534.6 J7.186.788.8842,000530,0001,4-Dichlorobenzene23 J<3.72<0.186<0.186<0.1868.5110Dichlorodifluoromethane<23<2.683.143.233.137008,8001,1-Dichloroethane16,0002,8001.28 J1.19 J8.61587701,2-Dichloroethane52 J<2.58<0.129<0.129<0.1293.6471,1-Dichloroethylene330,00028,20010.710.51,1001,40018,000cis-1,2-Dichloroethylene27,00019,5005.975.8516.72803,500trans-1,2-Dichloroethylene1,2002392.101.95 J2.682803,500Ethylbenzene11042.5 J<0.106<0.1064.94374904-Ethyltoluene29 J37.0 J<0.128<0.1281.97 JNENEHeptane8572.5<0.143<0.1435.552,80035,000Hexachlorobutadiene86 J<6.62<0.330 <0.330<0.3304.356Hexane180 J2,1900.892 J0.758 J24.74,90061,000Isopropanol<3407.42 J2.38 J, B3.08 J, B2.19 J, B1,40018,000Methylene Chloride6901461.18 J1.863.343,40053,0004-Methyl-2-Pentanone (MIBK)<3221.5 J<0.121<0.121<0.12121,000260,000Naphthalene46 J<3.66<0.183 <0.183<0.1832.836Propene1,400521<0.2421.5632321,000260,000Styrene<18<2.48<0.124<0.1240.660 J7,00088,000Tetrachloroethylene15028.6 J10.79.572.97 J2803,500Tetrahydrofuran<110<2.14<0.107<0.1071.19 J14,000180,000Toluene5702531.35 J1.38 J26.635,000440,0001,1,1-Trichloroethane9274.41.85 J1.84 J9.8035,000440,000Trichloroethylene290,000102,000 E11311450014180Trichlorofluoromethane<649.33 J9.259.207.80NENE1,1,2-Trichloro-1,2,2-trifluoroethane<87<11.20.697 J0.690 J0.659 J35,000440,0001,2,4-Trimethylbenzene751280.590 J0.944 J7.354205,3001,3,5-Trimethylbenzene53 J37.6 J0.782 J0.703 J2.464205,300Vinyl Acetate<150<4.48<0.224 0.669 J<0.2241,40018,000Vinyl Chloride1,40031.1<0.127 <0.1273.785.6 280m&p-Xylene2901462.59 J3.07 J17.27008,800o-Xylene12052.01.27 J1.38 J6.257008,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) dated January 2023.SG-2 re-installed and sampled on 5/11/22.Compound concentrations are reported in micrograms per cubic meter (μg/m3)Compound concentrations are reported to the laboratory method detection limits.Bold indicates concentration exceeds Residential SGSL.Underline indicates compound exceeds the Non-Residential SGSL.Only those compounds detected in at least one sample are shown in the table above.Laboratory analytical method shown in parentheses.VOCs = volatile organic compounds; ft bgs= feet below ground surface; NE = not established; NA = not analyzedJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.B = Analyte detected in laboratory blankE = Result above calibration rangePre-ExcavationSG-2Post-ExcavationResidentialSGSLs (1)Non-Residential SGSLs(1)SG-12/SG-DUP-11232211/23/20225.5µg/m3https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/Soil Removal/Report/Tables/Data Tables_excavation5/25/2023Table 2 (Page 1 of 1)Hart & Hickman, PC
Copyright:© 2013 National Geographic Society, i-cubed
SITE LOCATION MAP
NATIONAL WELDERS SUPPLY GESCO STREET & STATE STREET CHARLOTTE, NORTH CAROLINA
DATE: 4-28-23
JOB NO: RMR-013
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2013DERITA, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
ACCESS ROAD
(RESIDENTIALBRIDGE ABOVE)
ACCESS
R
O
A
DPOOL
SG-1
SG-3
REVISION NO. 0
JOB NO. RMR-013
DATE: 4-26-23
FIGURE NO. 2
NATIONAL WELDERS SUPPLY
GESCO STREET & STATE STREET
CHARLOTTE, NORTH CAROLINA
PREVIOUS SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
SURFACE WATER FEATURE
FORMER RAILROAD
FORMER UST
PROPOSED BUILDING FOOTPRINT
WORTH CHEMICAL MONITORING WELL
LOCATIONS
SOIL BORING LOCATION
TEMPORARY MONITORING WELL
LOCATION
SOIL GAS MONITORING POINT LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
SOUTHERN CONCRETE
MATERIALS
(715 STATE STREET)
FORSHAW
(650 STATE STREET)
INDUSTRIAL BUILDING
(FORMER PLYLER PAPER STOCK CO.)
(800 GESCO STREET)STEWART CREEKSEVERSVILLE PARK
(830 S. BRUNS AVENUE)
NOTES:
1. PARCEL DATA OBTAINED FROM MECKLENBURG COUNTY
GIS (2020).
2. UST = UNDERGROUND STORAGE TANK
3. MONITORING WELL LOCATIONS OVERLAIN FROM
MONITOR WELL LOCATION MAP IN THE GROUNDWATER
MONITORING REPORT PREPARED FOR THE WORTH
CHEMICAL FACILITY BY ARCADIS DATED JULY 2019.
4. REDEVELOPMENT PLAN OVERLAIN FROM SITE PLAN
PROVIDED BY BB+M ARCHITECTURE.
5. PHASE II ESA SOIL, GROUNDWATER, AND SOIL GAS
SAMPLES COLLECTED BY H&H IN AUGUST 2021.
DUKE ENERGY
RIGHT-OF-WAY
GESCO STREET
STATE STREET
MW-9 I/S
MW-14 I/S
TMW-1
TMW-2
TMW-3
TMW-6
TMW-4
TMW-7
TMW-5
SG-7
SG-6
SG-5
SG-4
SG-3
SG-2SG-1
SG-8
COMP-1
COMP-2
BKG-1
BKG-2
SG-9 SG-10
SG-11
SB-1
PIPED STORMWATER
DRAINAGE
BUILDING A (LEFT)
BUILDING A (RIGHT)
BUILDING B
S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\Site Map.dwg, Phase II ESA, 5/25/2023 9:09:02 AM, amckenzie
REVISION NO. 0
JOB NO. RMR-013
DATE: 5-25-23
FIGURE NO. 3
NATIONAL WELDERS SUPPLY
GESCO STREET & STATE STREET
CHARLOTTE, NORTH CAROLINA
SOURCE AREA SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
FORMER RAILROAD
APPROXIMATE HISTORICAL BUILDING
FOOTPRINT
PREVIOUS ASSESSMENT SOIL BORING
LOCATION
PREVIOUS ASSESSMENT TEMPORARY
MONITORING WELL LOCATION
PREVIOUS ASSESSMENT SOIL GAS
MONITORING POINT LOCATION
TRICHLOROETHENE CONCENTRATION
APPROXIMATE EXTENTS OF SOIL
IMPACTS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FORSHAW
(650 STATE STREET)
NOTES:
1.PARCEL DATA OBTAINED FROM MECKLENBURG COUNTY GIS
(2020).
2.TRICHLOROETHENE CONCENTRATIONS FOR EACH MEDIA
SHOWN IN THE FOLLOWING UNITS:
2.1.SOIL CONCENTRATIONS SHOWN IN MILLIGRAMS PER
KILOGRAM (mg/kg)
2.2.GROUNDWATER CONCENTRATIONS SHOWN IN
MICROGRAMS PER LITER (µg/L)
2.3.SOIL GAS CONCENTRATION SHOWN IN MICROGRAMS
PER CUBIC METER (µg/m3)
3.BOLD INDICATES AN EXCEEDANCE OF THE PROTECTION OF
GROUNDWATER PRELIMINARY SOIL REMEDIATION GOALS.
4.UNDERLINE INDICATES GROUNDWATER OR SOIL GAS
CONCENTRATIONS EXCEED THE RESIDENTIAL AND
NON-RESIDENTIAL VAPOR INTRUSION SCREENING LEVELS.
5.BDL = BELOW LABORATORY METHOD DETECTION LIMITS
6.SOIL, GROUNDWATER, AND SOIL GAS SAMPLES COLLECTED
BY H&H IN AUGUST 2021 AND MAY 2022.
STATE STREET
TMW-1
SG-1
SG-3 GESCO STREETTMW-2
SS-2SS-1
SS-8
SS-9
SS-5
SS-7
SS-4
SS-3
(BDL)
(0.0150)(0.0342)
(0.0035 J)
(0.787)
(0.284)
(0.0323)
(0.0276)
TMW-8
SG-2
(17)
(32.4)
(2,300)
(770)
(0.81 J)
SS-6(0.186)
SG-2
8/11/21 290,000
5/11/22 102,000
(0.186)S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\TCE Delineation Map.dwg, tce delineation map, 5/25/2023 9:38:46 AM, amckenzie
REVISION NO. 0
JOB NO. RMR-013
DATE: 4-27-23
FIGURE NO. 4
NATIONAL WELDERS SUPPLY
GESCO STREET & STATE STREET
CHARLOTTE, NORTH CAROLINA
POST-EXCAVATION SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
FORMER RAILROAD
APPROXIMATE HISTORICAL BUILDING
FOOTPRINT
EXCAVATION EXTENTS (DASHED WHERE
OVER-EXCAVATION OCCURRED)
EXCAVATION SOIL SAMPLE LOCATION
(TCE BELOW SCREENING LEVELS)
EXCAVATION SOIL SAMPLE LOCATION
(TCE ABOVE SCREENING LEVELS)
POST-EXCAVATION SOIL GAS SAMPLE
LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FORSHAW
(650 STATE STREET)
NOTES:
1.PARCEL DATA OBTAINED FROM MECKLENBURG COUNTY GIS
(2020).
2.POST-EXCAVATION SOIL SAMPLES COLLECTED BETWEEN
OCTOBER 26, 2022 AND NOVEMBER 8, 2022.
3.POST-EXCAVATION SOIL GAS SAMPLES COLLECTED ON
NOVEMBER 23, 2022.
STATE STREET
GESCO STREETEX-SB-1
EX-SB-2 EX-SB-3
EX-SB-4 EX-SB-5
EX-SB-6
EX-SB-7
EX-SB-8
EX-SB-9
EX-SB-10
EX-SB-11
EX-SB-26
EX-SB-25
EX-SB-24
EX-SB-23
EX-SB-22EX-SB-21
EX-SB-20EX-SB-19
EX-SB-18
EX-SB-17
EX-SB-16
EX-SB-15
EX-SB-14
EX-SB-12
EX-SB-13
EX-SB-20A
EX-SB-23A EX-SB-25A
SG-13
SG-12
S:\AAA-Master Projects\Ram Realty - RMR\RMR-013 Gesco Street\Figures\TCE Delineation Map_4.26.23.dwg, tce delineation map, 5/25/2023 9:12:23 AM, amckenzie

Appendix A Waste Manifests

Appendix B Summary of Excavation Field Screening Results
Appendix B
Summary of Excavation Field Screening Results
National Welders Supply
Gesco Street & State Street
Charlotte, North Carolina
H&H Job No. RMR-013
PID
Reading VOCAM Results
(ppm) TCE
0-3 NM --
3-6 41.1 Not Present
6-9 8.2 --
0-3 0.7 --
3-6 13.1 Not Present
6-9 11.1 --
0-3 0.6 --
3-6 32.7 Present
6-9 28.5 --
0-3 0.8 --
3-6 23.1 Not Present
6-9 11.1 --
0-3 6.9 --
3-6 32.8 Not Present
6-9 22.0 --
0-3 3.1 --
3-6 24.0 Not Present
6-9 9.9 --
0-3 0.4 --
3-6 15.5 --
6-9 22.0 Not Present
0-3 1.2 --
3-6 15.2 Not Present
6-9 11.2 --
0-3 1.8 --
3-6 3.6 Present
6-9 1.9 --
0-3 2.3 --
3-6 0.6 --
6-9 11.0 Not Present
0-3 0.6 --
3-6 1.3 --
6-9 5.6 Not Present
Notes:
NM= Not Measured
-- = Not Analyzed
* = Generator down so VOCAM readings not collected
** = Existing grade was cut down and exported prior to H&H on-Site.
EX-SB-7 10/27/2022
EX-SB-8 10/27/2022
EX-SB-11 10/28/2022
EX-SB-5 10/27/2022
EX-SB-6 10/27/2022
EX-SB-9 10/28/2022
EX-SB-10 10/28/2022
Sample ID Screening
Date
Depth (ft
bgs)
EX-SB-4 10/27/2022
EX-SB-1 10/26/2022
EX-SB-2 10/27/2022
EX-SB-3 10/27/2022
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/
Soil Removal Work Plan/Report/Data Tables_excavation
Appendix B (Page 1 of 3)
Hart & Hickman, PC
Appendix B
Summary of Excavation Field Screening Results
National Welders Supply
Gesco Street & State Street
Charlotte, North Carolina
H&H Job No. RMR-013
PID
Reading VOCAM Results
(ppm) TCE
0-3 0.4 --
3-6 1.5 Not Present
6-9 0.9 --
0-3 0.7 --
3-6 1.2 --
6-9 2.1 Not Present
0-3 0.5 --
3-6 1.0 Not Present
6-9 0.9 --
0-3 5.2 Present
3-6 2.1 --
6-9 1.4 --
0-3 1.0 --
3-6 3.2 Not Present
6-9 1.0 --
0-3 0.6 --
3-6 0.7 --
6-9 0.9 Not Present
0-3 0.6 --
3-6 0.8 --*
6-9 0.7 --
0-3 0.5 --
3-6 0.9 --*
6-9 0.9 --
0-3 4.4 --*
3-6 2.1 --
6-9 1.3 --
0-3 NM**--
3-6 NM** --
6-9 0.3 --
0-3 0.6 --
3-6 0.6 --*
6-9 0.6 --
Notes:
NM= Not Measured
-- = Not Analyzed
* = Generator down so VOCAM readings not collected
** = Existing grade was cut down and exported prior to H&H on-Site.
EX-SB-13 10/28/2022
10/28/2022
EX-SB-20A 11/9/2022
EX-SB-17
EX-SB-20 10/28/2022
EX-SB-21 10/28/2022
EX-SB-12 10/28/2022
EX-SB-14 10/28/2022
Sample ID Screening
Date
Depth (ft
bgs)
EX-SB-19 10/28/2022
EX-SB-18 10/28/2022
EX-SB-15 10/28/2022
EX-SB-16 10/28/2022
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/
Soil Removal Work Plan/Report/Data Tables_excavation
Appendix B (Page 2 of 3)
Hart & Hickman, PC
Appendix B
Summary of Excavation Field Screening Results
National Welders Supply
Gesco Street & State Street
Charlotte, North Carolina
H&H Job No. RMR-013
PID
Reading VOCAM Results
(ppm) TCE
0-3 0.3 --*
3-6 0.2 --
6-9 0.2 --
0-3 20.3 Present
3-6 2.2 --
6-9 0.3 --
0-3 0.3 --
3-6 0.3 --
6-9 1.6 --
0-3 1.6 --
3-6 4.0 --*
6-9 3.2 --
0-3 0.8 --
3-6 4.6 --*
6-9 3.5 --
0-3 0.3 --
3-6 1.4 --
6-9 1.0 --
0-3 0.2 --
3-6 0.4 --
6-9 1.1 --*
Notes:
NM= Not Measured
-- = Not Analyzed
* = Generator down so VOCAM readings not collected
** = Existing grade was cut down and exported prior to H&H on-Site.
EX-SB-24
EX-SB-25
EX-SB-26 10/28/2022
10/28/2022
EX-SB-23A 11/9/2022
EX-SB-25A 11/9/2022
EX-SB-22 10/28/2022
EX-SB-23 10/28/2022
10/28/2022
Sample ID Screening
Date
Depth (ft
bgs)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Ram Realty - RMR/RMR-013 Gesco Street/
Soil Removal Work Plan/Report/Data Tables_excavation
Appendix B (Page 3 of 3)
Hart & Hickman, PC

Appendix C Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/2/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-300-0011 Client Project Description: RMR-013
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/27/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 18
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-300-0011
Page 2 of 18
Report Number:
Sample Summary Table
Client Project Description:
22-300-0011
RMR-013
Lab No Client Sample ID Matrix Date Collected Date Received
10/26/2022 15:00Solids 91637 EX-SB-1 10/27/2022 11:00
Page 3 of 18
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-300-0011
Report Limit
Project:RMR-013
V 91637EX-SB-1
J0.008 10/31/2022 17:568260DAcetonemg/Kg - dry 0.002
J0.0010 10/31/2022 17:568260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
J0.003 10/31/2022 17:568260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.0009
J0.001 10/31/2022 17:568260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.002 10/31/2022 17:568260DMethylene Chloride mg/Kg - dry 0.001
J0.001 10/31/2022 17:568260DTrichloroethenemg/Kg - dry 0.001
11.9 11/02/2022 10:30SW-DRYWT Moisture %
Page 4 of 18
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-300-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/27/2022
RMR-013
Report Date : 11/02/2022
Sample ID :
Lab No :
Sampled:EX-SB-1
91637 Matrix:
10/26/2022 15:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.9 %Moisture 1 11/02/22 10:30 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 18
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-300-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/27/2022
RMR-013
Report Date : 11/02/2022
Sample ID :
Lab No :
Sampled:EX-SB-1
91637 Matrix:
10/26/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.008 J mg/Kg - dry 0.002 0.022Acetone 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 17:56 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 17:56 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 17:56 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 10/31/22 17:56 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 17:56 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 18
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-300-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/27/2022
RMR-013
Report Date : 11/02/2022
Sample ID :
Lab No :
Sampled:EX-SB-1
91637 Matrix:
10/26/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 10/31/22 17:56 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 17:56 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 17:56 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/31/22 17:56 V25732TBL
0.0010 J mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 17:56 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 17:56 V25732TBL
<0.015 mg/Kg - dry 0.015 0.283Ethanol 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 17:56 V25732TBL
0.003 J mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 17:56 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 17:56 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 18
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-300-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/27/2022
RMR-013
Report Date : 11/02/2022
Sample ID :
Lab No :
Sampled:EX-SB-1
91637 Matrix:
10/26/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 10/31/22 17:56 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 10/31/22 17:56 V25732TBL
0.001 J mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 17:56 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 10/31/22 17:56 V25732TBL
0.002 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 17:56 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/31/22 17:56 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 17:56 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/31/22 17:56 V25732TBL
0.001 J mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 17:56 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 17:56 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/31/22 17:56 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 18
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-300-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/27/2022
RMR-013
Report Date : 11/02/2022
Sample ID :
Lab No :
Sampled:EX-SB-1
91637 Matrix:
10/26/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 10/31/22 17:56 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 17:56 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 17:56 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 17:56 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 17:56 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 17:561 TBL V25732
Surrogate: Dibromofluoromethane 103 Limits: 84-123%10/31/22 17:561 TBL V25732
Surrogate: Toluene-d8 92.0 Limits: 76-129%10/31/22 17:561 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91637
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0200.002<0.002mg/KgAcetone
10/31/22 12:570.0200.001<0.001mg/KgAcrolein
10/31/22 12:570.0200.0008<0.0008mg/KgAcrylonitrile
10/31/22 12:570.0050.0006<0.0006mg/KgBenzene
10/31/22 12:570.0050.0005<0.0005mg/KgBromobenzene
10/31/22 12:570.0050.0008<0.0008mg/KgBromochloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromodichloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromoform
10/31/22 12:570.0100.001<0.001mg/KgBromomethane
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Butylbenzene
10/31/22 12:570.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/31/22 12:570.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/31/22 12:570.0050.0006<0.0006mg/KgCarbon Disulfide
10/31/22 12:570.0050.001<0.001mg/KgCarbon Tetrachloride
10/31/22 12:570.0050.0007<0.0007mg/KgChlorobenzene
10/31/22 12:570.0050.0009<0.0009mg/KgChlorodibromomethane
10/31/22 12:570.0100.0009<0.0009mg/KgChloroethane
10/31/22 12:570.0050.001<0.001mg/KgChloroform
10/31/22 12:570.0100.0006<0.0006mg/KgChloromethane
10/31/22 12:570.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/31/22 12:570.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/31/22 12:570.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/31/22 12:570.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/31/22 12:570.0050.0006<0.0006mg/KgDibromomethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 7Date:11/02/2022 04:16 PM
Page 10 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91637
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/31/22 12:570.0100.001<0.001mg/KgDichlorodifluoromethane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/31/22 12:570.0050.001<0.001mg/Kg1,2-Dichloroethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/31/22 12:570.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/31/22 12:570.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/31/22 12:570.0050.001<0.001mg/Kg2,2-Dichloropropane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/31/22 12:570.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/31/22 12:570.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/31/22 12:570.2500.014<0.014mg/KgEthanol
10/31/22 12:570.0050.0006<0.0006mg/KgEthylbenzene
10/31/22 12:570.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/31/22 12:570.0100.0008<0.0008mg/KgHexachlorobutadiene
10/31/22 12:570.0100.0007<0.0007mg/Kgn-Hexane
10/31/22 12:570.0200.0006<0.0006mg/Kg2-Hexanone
10/31/22 12:570.0050.0005<0.0005mg/KgIsopropylbenzene
10/31/22 12:570.0050.001<0.001mg/Kg4-Isopropyl toluene
10/31/22 12:570.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/31/22 12:570.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/31/22 12:570.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/31/22 12:570.0100.001<0.001mg/KgMethylene Chloride
10/31/22 12:570.0100.0010<0.0010mg/KgNaphthalene
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 2 of 7Date:11/02/2022 04:16 PM
Page 11 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91637
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.001<0.001mg/KgStyrene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTetrachloroethene
10/31/22 12:570.0050.0007<0.0007mg/KgToluene
10/31/22 12:570.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/31/22 12:570.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTrichloroethene
10/31/22 12:570.0100.002<0.002mg/KgTrichlorofluoromethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/31/22 12:570.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Acetate
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Chloride
10/31/22 12:570.0050.0005<0.0005mg/Kgo-Xylene
10/31/22 12:570.0100.001<0.001mg/Kgm,p-Xylene
10/31/22 12:574-Bromofluorobenzene (S)101 70-130
10/31/22 12:57Dibromofluoromethane (S)97.6 84-123
10/31/22 12:57Toluene-d8 (S)93.6 76-129
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.095 95.389.60.0890.100mg/KgAcetone 29-198 6.1 20
Page 3 of 7Date:11/02/2022 04:16 PM
Page 12 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031040.1040.100mg/KgAcrolein 70-130 0.9 20
0.115 1151100.1100.100mg/KgAcrylonitrile 65-134 4.4 20
0.048 97.61000.0500.050mg/KgBenzene 74-127 2.4 20
0.043 86.091.40.0450.050mg/KgBromobenzene 73-125 6.0 20
0.054 1081070.0530.050mg/KgBromochloromethane 72-134 1.2 20
0.055 1101120.0550.050mg/KgBromodichloromethane 75-122 1.0 20
0.055 1101090.0540.050mg/KgBromoform 66-135 1.2 20
0.059 1201250.0620.050mg/KgBromomethane 20-180 4.5 20
0.040 81.089.20.0440.050mg/Kgn-Butylbenzene 65-135 9.6 20
0.041 82.290.20.0450.050mg/Kgsec-Butyl benzene 66-131 9.2 20
0.040 81.287.00.0430.050mg/Kgtert-Butyl benzene 67-132 6.8 20
0.045 91.495.60.0470.050mg/KgCarbon Disulfide 61-129 4.4 20
0.045 91.295.00.0470.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.044 88.291.80.0450.050mg/KgChlorobenzene 74-118 4.0 20
0.051 1031030.0510.050mg/KgChlorodibromomethane 73-122 0.0 20
0.049 99.41040.0510.050mg/KgChloroethane 33-149 4.3 20
0.049 98.01000.0500.050mg/KgChloroform 73-127 2.0 20
0.055 1101110.0550.050mg/KgChloromethane 45-143 0.7 20
0.040 81.886.60.0430.050mg/Kg2-Chlorotoluene 67-124 5.7 20
0.040 81.886.60.0430.050mg/Kg4-Chlorotoluene 71-126 5.7 20
0.055 1111130.0560.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.2 20
0.061 1241280.0640.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.4 20
0.055 1111130.0560.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.054 1091150.0570.050mg/KgDibromomethane 74-133 5.1 20
0.044 89.290.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.041 83.686.40.0430.050mg/Kg1,3-Dichlorobenzene 71-120 3.2 20
Page 4 of 7Date:11/02/2022 04:16 PM
Page 13 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.045 91.21010.0500.050mg/KgDichlorodifluoromethane 26-146 9.8 20
0.048 96.81020.0510.050mg/Kg1,1-Dichloroethane 74-127 5.2 20
0.051 1031030.0510.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.898.60.0490.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.050 1021070.0530.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.048 96.81010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.053 1061090.0540.050mg/Kg1,2-Dichloropropane 73-130 2.4 20
0.052 1051070.0530.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.045 91.294.40.0470.050mg/Kg2,2-Dichloropropane 50-142 3.4 20
0.043 86.894.80.0470.050mg/Kg1,1-Dichloropropene 71-130 8.8 20
0.055 1111130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.056 1131120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.984 78.792.01.151.25mg/KgEthanol 70-130 15.5 20
0.044 88.490.40.0450.050mg/KgEthylbenzene 74-128 2.2 20
0.109 1091090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.039 79.887.40.0430.050mg/KgHexachlorobutadiene 64-125 9.0 20
0.048 96.81010.0500.050mg/Kgn-Hexane 70-130 3.8 20
0.054 1091070.0530.050mg/Kg2-Hexanone 61-157 2.2 20
0.039 79.487.00.0430.050mg/KgIsopropylbenzene 68-126 9.1 20
0.039 79.885.80.0420.050mg/Kg4-Isopropyl toluene 68-129 7.2 20
0.052 1051190.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 12.8 20
0.057 1141170.0580.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.7 20
0.052 10491.40.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 13.2 20
0.052 1051090.0540.050mg/KgMethylene Chloride 74-129 3.9 20
0.050 1021080.0530.050mg/KgNaphthalene 57-157 5.7 20
Page 5 of 7Date:11/02/2022 04:16 PM
Page 14 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.889.60.0440.050mg/Kgn-Propylbenzene 67-130 6.6 20
0.047 94.097.60.0480.050mg/KgStyrene 77-121 3.7 20
0.045 90.691.60.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.055 1101140.0570.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.046 92.696.20.0480.050mg/KgTetrachloroethene 68-130 3.8 20
0.047 94.298.20.0490.050mg/KgToluene 71-129 4.1 20
0.045 91.096.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.7 20
0.046 92.897.80.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.2 20
0.044 88.092.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.3 20
0.053 1081080.0540.050mg/Kg1,1,2-Trichloroethane 70-133 0.3 20
0.049 98.21050.0520.050mg/KgTrichloroethene 75-133 6.5 20
0.045 90.096.60.0480.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.056 1141150.0570.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.041 83.887.20.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.9 20
0.040 81.687.40.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.8 20
0.058 1171200.0590.050mg/KgVinyl Acetate 60-140 1.8 20
0.050 1011040.0520.050mg/KgVinyl Chloride 48-147 2.9 20
0.045 90.894.60.0470.050mg/Kgo-Xylene 74-126 4.0 20
0.087 87.490.90.0900.100mg/Kgm,p-Xylene 75-124 3.9 20
97.099.44-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)84-123
93.693.0Toluene-d8 (S)76-129
Page 6 of 7Date:11/02/2022 04:16 PM
Page 15 of 18
Quality Control Data
22-300-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V25801QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91503-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/02/22 10:3015.57.819.13%Moisture
V 91505-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/02/22 10:3018.35.484.56%Moisture
Page 7 of 7Date:11/02/2022 04:16 PM
Page 16 of 18
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-300-0011
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.9C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/27/2022 13:13:23
Special precautions or instructions included?
Comments:
Page 17 of 18
Page 18 of 18

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/4/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-301-0007 Client Project Description: RMR-013
Gesco Strreet
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/28/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 50
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-301-0007
Page 2 of 50
Report Number:
Sample Summary Table
Client Project Description:
22-301-0007
RMR-013
Gesco Strreet
Lab No Client Sample ID Matrix Date Collected Date Received
10/27/2022Solids 91714 EX-SB-2 10/28/2022 12:45
10/27/2022Solids 91715 EX-SB-3 10/28/2022 12:45
10/27/2022Solids 91716 EX-SB-4 10/28/2022 12:45
10/27/2022Solids 91717 EX-SB-5 10/28/2022 12:45
10/27/2022Solids 91718 EX-SB-6 10/28/2022 12:45
10/27/2022Solids 91719 EX-SB-7 10/28/2022 12:45
10/27/2022Solids 91720 EX-SB-8 10/28/2022 12:45
Page 3 of 50
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0007
Report Limit
Project:RMR-013
V 91714EX-SB-2
J0.005 10/31/2022 14:468260DAcetonemg/Kg - dry 0.002
J0.002 10/31/2022 14:468260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
13.8 11/04/2022 11:19SW-DRYWT Moisture %
V 91715EX-SB-3
J0.009 10/31/2022 15:138260DAcetonemg/Kg - dry 0.002
J0.004 10/31/2022 15:138260Dcis-1,2-Dichloroethene mg/Kg - dry 0.001
J0.008 10/31/2022 15:138260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.002 10/31/2022 15:138260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.002 10/31/2022 15:138260DMethylene Chloride mg/Kg - dry 0.001
J0.001 10/31/2022 15:138260DTrichloroethenemg/Kg - dry 0.001
17.5 11/04/2022 11:19SW-DRYWT Moisture %
V 91716EX-SB-4
J0.007 10/31/2022 15:408260DAcetonemg/Kg - dry 0.002
J0.003 10/31/2022 15:408260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.001 10/31/2022 15:408260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.001 10/31/2022 15:408260DMethylene Chloride mg/Kg - dry 0.001
12.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91717EX-SB-5
J0.006 10/31/2022 16:078260DAcetonemg/Kg - dry 0.002
J0.001 10/31/2022 16:078260D1,1-Dichloroethene mg/Kg - dry 0.0009
J0.006 10/31/2022 16:078260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.001 10/31/2022 16:078260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.004 10/31/2022 16:078260DTrichloroethenemg/Kg - dry 0.001
16.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91718EX-SB-6
J0.007 10/31/2022 16:358260DAcetonemg/Kg - dry 0.002
J0.004 10/31/2022 16:358260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.001 10/31/2022 16:358260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.001 10/31/2022 16:358260DMethylene Chloride mg/Kg - dry 0.001
16.9 11/04/2022 11:19SW-DRYWT Moisture %
V 91719EX-SB-7
J0.010 10/31/2022 17:028260DAcetonemg/Kg - dry 0.002
J0.008 10/31/2022 17:028260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.001 10/31/2022 17:028260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
Page 4 of 50
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0007
Report Limit
Project:RMR-013
V 91719EX-SB-7
J0.002 10/31/2022 17:028260DMethylene Chloride mg/Kg - dry 0.001
J0.002 10/31/2022 17:028260DTrichloroethenemg/Kg - dry 0.001
18.8 11/04/2022 11:19SW-DRYWT Moisture %
V 91720EX-SB-8
J0.009 10/31/2022 17:298260DAcetonemg/Kg - dry 0.002
J0.006 10/31/2022 17:298260DEthyl Tertiary Butyl Ether (ETBE)mg/Kg - dry 0.001
J0.001 10/31/2022 17:298260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.002 10/31/2022 17:298260DMethylene Chloride mg/Kg - dry 0.001
14.1 11/04/2022 11:19SW-DRYWT Moisture %
Page 5 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-2
91714 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.8 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-2
91714 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.005 J mg/Kg - dry 0.002 0.023Acetone 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 14:46 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 14:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 14:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-2
91714 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 10/31/22 14:46 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 14:46 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 14:46 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 14:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 14:46 V25732TBL
<0.016 mg/Kg - dry 0.016 0.290Ethanol 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 14:46 V25732TBL
0.002 J mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 14:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 14:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-2
91714 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 10/31/22 14:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 14:46 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 14:46 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/31/22 14:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 14:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 14:46 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 14:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/31/22 14:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-2
91714 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 10/31/22 14:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 14:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 14:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 14:46 V25732
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%10/31/22 14:461 TBL V25732
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/31/22 14:461 TBL V25732
Surrogate: Toluene-d8 92.4 Limits: 76-129%10/31/22 14:461 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-3
91715 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.5 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-3
91715 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.009 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 10/31/22 15:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 15:13 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 15:13 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 15:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 15:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 15:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-3
91715 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 15:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 15:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 15:13 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 15:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 15:13 V25732TBL
0.004 J mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 15:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 15:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 15:13 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 15:13 V25732TBL
<0.016 mg/Kg - dry 0.016 0.303Ethanol 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 15:13 V25732TBL
0.008 J mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 15:13 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 15:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-3
91715 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 15:13 V25732TBL
0.002 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 15:13 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 15:13 V25732TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 15:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/31/22 15:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 15:13 V25732TBL
0.001 J mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 15:13 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 15:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 15:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-3
91715 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 15:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 15:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 15:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 15:13 V25732
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%10/31/22 15:131 TBL V25732
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/31/22 15:131 TBL V25732
Surrogate: Toluene-d8 91.0 Limits: 76-129%10/31/22 15:131 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-4
91716 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-4
91716 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.007 J mg/Kg - dry 0.002 0.022Acetone 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 15:40 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 15:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 15:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 10/31/22 15:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 15:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-4
91716 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 10/31/22 15:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 15:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 15:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 15:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 15:40 V25732TBL
<0.016 mg/Kg - dry 0.016 0.286Ethanol 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 15:40 V25732TBL
0.003 J mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 15:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 15:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-4
91716 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 10/31/22 15:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 10/31/22 15:40 V25732TBL
0.001 J mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 15:40 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 10/31/22 15:40 V25732TBL
0.001 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 15:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 15:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/31/22 15:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 15:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 15:40 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 15:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/31/22 15:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-4
91716 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 10/31/22 15:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 15:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 15:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 15:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 15:40 V25732
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%10/31/22 15:401 TBL V25732
Surrogate: Dibromofluoromethane 103 Limits: 84-123%10/31/22 15:401 TBL V25732
Surrogate: Toluene-d8 92.6 Limits: 76-129%10/31/22 15:401 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-5
91717 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-5
91717 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 16:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 16:07 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 16:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 16:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-5
91717 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 16:07 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 16:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 16:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 16:07 V25732TBL
0.001 J mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006cis-1,2-Dichloroethene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 16:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 10/31/22 16:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 16:07 V25732TBL
<0.016 mg/Kg - dry 0.016 0.300Ethanol 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 16:07 V25732TBL
0.006 J mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.012Hexachlorobutadiene 1 10/31/22 16:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-5
91717 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 16:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.024
2-Hexanone 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 16:07 V25732TBL
0.001 J mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 16:07 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 16:07 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 10/31/22 16:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 16:07 V25732TBL
0.004 J mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 16:07 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 16:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 16:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-5
91717 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,3,5-Trimethylbenzene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 16:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 16:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 16:07 V25732
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%10/31/22 16:071 TBL V25732
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/31/22 16:071 TBL V25732
Surrogate: Toluene-d8 91.4 Limits: 76-129%10/31/22 16:071 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-6
91718 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.9 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-6
91718 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.007 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 10/31/22 16:35 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 16:35 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 16:35 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 16:35 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 16:35 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 16:35 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-6
91718 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 16:35 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 16:35 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 16:35 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 16:35 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 16:35 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 16:35 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 16:35 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 10/31/22 16:35 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 16:35 V25732TBL
<0.016 mg/Kg - dry 0.016 0.300Ethanol 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 16:35 V25732TBL
0.004 J mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 16:35 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 16:35 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-6
91718 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 16:35 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.024
2-Hexanone 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 16:35 V25732TBL
0.001 J mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 16:35 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 16:35 V25732TBL
0.001 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 16:35 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 10/31/22 16:35 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 16:35 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 16:35 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 16:35 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-6
91718 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,3,5-Trimethylbenzene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 16:35 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 16:35 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 16:35 V25732
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%10/31/22 16:351 TBL V25732
Surrogate: Dibromofluoromethane 98.8 Limits: 84-123%10/31/22 16:351 TBL V25732
Surrogate: Toluene-d8 92.4 Limits: 76-129%10/31/22 16:351 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-7
91719 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.8 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-7
91719 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.010 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 10/31/22 17:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 17:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 17:02 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 17:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 17:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 17:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-7
91719 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 17:02 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 17:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 17:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 17:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 17:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 17:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 17:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 17:02 V25732TBL
<0.017 mg/Kg - dry 0.017 0.307Ethanol 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 17:02 V25732TBL
0.008 J mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 17:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 17:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-7
91719 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 17:02 V25732TBL
0.001 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 17:02 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 17:02 V25732TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 17:02 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/31/22 17:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 17:02 V25732TBL
0.002 J mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 17:02 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 17:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 17:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-7
91719 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 17:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 17:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 17:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 17:02 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 17:021 TBL V25732
Surrogate: Dibromofluoromethane 101 Limits: 84-123%10/31/22 17:021 TBL V25732
Surrogate: Toluene-d8 92.8 Limits: 76-129%10/31/22 17:021 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-8
91720 Matrix:
10/27/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.1 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-8
91720 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.009 J mg/Kg - dry 0.002 0.023Acetone 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 17:29 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 17:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 17:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-8
91720 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/31/22 17:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 17:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 17:29 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 17:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 17:29 V25732TBL
<0.016 mg/Kg - dry 0.016 0.291Ethanol 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 17:29 V25732TBL
0.006 J mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 17:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 17:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-8
91720 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 10/31/22 17:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/31/22 17:29 V25732TBL
0.001 J mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 17:29 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/31/22 17:29 V25732TBL
0.002 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 17:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 10/31/22 17:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 17:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 17:29 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 17:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/31/22 17:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0007
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Gesco Strreet Received : 10/28/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-8
91720 Matrix:
10/27/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 10/31/22 17:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 17:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 17:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 17:29 V25732
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%10/31/22 17:291 TBL V25732
Surrogate: Dibromofluoromethane 106 Limits: 84-123%10/31/22 17:291 TBL V25732
Surrogate: Toluene-d8 94.2 Limits: 76-129%10/31/22 17:291 TBL V25732
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91714, 91715, 91716, 91717, 91718, 91719, 91720
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0200.002<0.002mg/KgAcetone
10/31/22 12:570.0200.001<0.001mg/KgAcrolein
10/31/22 12:570.0200.0008<0.0008mg/KgAcrylonitrile
10/31/22 12:570.0050.0006<0.0006mg/KgBenzene
10/31/22 12:570.0050.0005<0.0005mg/KgBromobenzene
10/31/22 12:570.0050.0008<0.0008mg/KgBromochloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromodichloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromoform
10/31/22 12:570.0100.001<0.001mg/KgBromomethane
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Butylbenzene
10/31/22 12:570.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/31/22 12:570.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/31/22 12:570.0050.0006<0.0006mg/KgCarbon Disulfide
10/31/22 12:570.0050.001<0.001mg/KgCarbon Tetrachloride
10/31/22 12:570.0050.0007<0.0007mg/KgChlorobenzene
10/31/22 12:570.0050.0009<0.0009mg/KgChlorodibromomethane
10/31/22 12:570.0100.0009<0.0009mg/KgChloroethane
10/31/22 12:570.0050.001<0.001mg/KgChloroform
10/31/22 12:570.0100.0006<0.0006mg/KgChloromethane
10/31/22 12:570.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/31/22 12:570.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/31/22 12:570.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/31/22 12:570.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/31/22 12:570.0050.0006<0.0006mg/KgDibromomethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 8Date:11/04/2022 04:21 PM
Page 41 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91714, 91715, 91716, 91717, 91718, 91719, 91720
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/31/22 12:570.0100.001<0.001mg/KgDichlorodifluoromethane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/31/22 12:570.0050.001<0.001mg/Kg1,2-Dichloroethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/31/22 12:570.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/31/22 12:570.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/31/22 12:570.0050.001<0.001mg/Kg2,2-Dichloropropane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/31/22 12:570.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/31/22 12:570.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/31/22 12:570.2500.014<0.014mg/KgEthanol
10/31/22 12:570.0050.0006<0.0006mg/KgEthylbenzene
10/31/22 12:570.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/31/22 12:570.0100.0008<0.0008mg/KgHexachlorobutadiene
10/31/22 12:570.0100.0007<0.0007mg/Kgn-Hexane
10/31/22 12:570.0200.0006<0.0006mg/Kg2-Hexanone
10/31/22 12:570.0050.0005<0.0005mg/KgIsopropylbenzene
10/31/22 12:570.0050.001<0.001mg/Kg4-Isopropyl toluene
10/31/22 12:570.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/31/22 12:570.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/31/22 12:570.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/31/22 12:570.0100.001<0.001mg/KgMethylene Chloride
10/31/22 12:570.0100.0010<0.0010mg/KgNaphthalene
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 2 of 8Date:11/04/2022 04:21 PM
Page 42 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91714, 91715, 91716, 91717, 91718, 91719, 91720
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.001<0.001mg/KgStyrene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTetrachloroethene
10/31/22 12:570.0050.0007<0.0007mg/KgToluene
10/31/22 12:570.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/31/22 12:570.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTrichloroethene
10/31/22 12:570.0100.002<0.002mg/KgTrichlorofluoromethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/31/22 12:570.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Acetate
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Chloride
10/31/22 12:570.0050.0005<0.0005mg/Kgo-Xylene
10/31/22 12:570.0100.001<0.001mg/Kgm,p-Xylene
10/31/22 12:574-Bromofluorobenzene (S)101 70-130
10/31/22 12:57Dibromofluoromethane (S)97.6 84-123
10/31/22 12:57Toluene-d8 (S)93.6 76-129
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.095 95.389.60.0890.100mg/KgAcetone 29-198 6.1 20
Page 3 of 8Date:11/04/2022 04:21 PM
Page 43 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031040.1040.100mg/KgAcrolein 70-130 0.9 20
0.115 1151100.1100.100mg/KgAcrylonitrile 65-134 4.4 20
0.048 97.61000.0500.050mg/KgBenzene 74-127 2.4 20
0.043 86.091.40.0450.050mg/KgBromobenzene 73-125 6.0 20
0.054 1081070.0530.050mg/KgBromochloromethane 72-134 1.2 20
0.055 1101120.0550.050mg/KgBromodichloromethane 75-122 1.0 20
0.055 1101090.0540.050mg/KgBromoform 66-135 1.2 20
0.059 1201250.0620.050mg/KgBromomethane 20-180 4.5 20
0.040 81.089.20.0440.050mg/Kgn-Butylbenzene 65-135 9.6 20
0.041 82.290.20.0450.050mg/Kgsec-Butyl benzene 66-131 9.2 20
0.040 81.287.00.0430.050mg/Kgtert-Butyl benzene 67-132 6.8 20
0.045 91.495.60.0470.050mg/KgCarbon Disulfide 61-129 4.4 20
0.045 91.295.00.0470.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.044 88.291.80.0450.050mg/KgChlorobenzene 74-118 4.0 20
0.051 1031030.0510.050mg/KgChlorodibromomethane 73-122 0.0 20
0.049 99.41040.0510.050mg/KgChloroethane 33-149 4.3 20
0.049 98.01000.0500.050mg/KgChloroform 73-127 2.0 20
0.055 1101110.0550.050mg/KgChloromethane 45-143 0.7 20
0.040 81.886.60.0430.050mg/Kg2-Chlorotoluene 67-124 5.7 20
0.040 81.886.60.0430.050mg/Kg4-Chlorotoluene 71-126 5.7 20
0.055 1111130.0560.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.2 20
0.061 1241280.0640.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.4 20
0.055 1111130.0560.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.054 1091150.0570.050mg/KgDibromomethane 74-133 5.1 20
0.044 89.290.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.041 83.686.40.0430.050mg/Kg1,3-Dichlorobenzene 71-120 3.2 20
Page 4 of 8Date:11/04/2022 04:21 PM
Page 44 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.045 91.21010.0500.050mg/KgDichlorodifluoromethane 26-146 9.8 20
0.048 96.81020.0510.050mg/Kg1,1-Dichloroethane 74-127 5.2 20
0.051 1031030.0510.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.898.60.0490.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.050 1021070.0530.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.048 96.81010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.053 1061090.0540.050mg/Kg1,2-Dichloropropane 73-130 2.4 20
0.052 1051070.0530.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.045 91.294.40.0470.050mg/Kg2,2-Dichloropropane 50-142 3.4 20
0.043 86.894.80.0470.050mg/Kg1,1-Dichloropropene 71-130 8.8 20
0.055 1111130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.056 1131120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.984 78.792.01.151.25mg/KgEthanol 70-130 15.5 20
0.044 88.490.40.0450.050mg/KgEthylbenzene 74-128 2.2 20
0.109 1091090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.039 79.887.40.0430.050mg/KgHexachlorobutadiene 64-125 9.0 20
0.048 96.81010.0500.050mg/Kgn-Hexane 70-130 3.8 20
0.054 1091070.0530.050mg/Kg2-Hexanone 61-157 2.2 20
0.039 79.487.00.0430.050mg/KgIsopropylbenzene 68-126 9.1 20
0.039 79.885.80.0420.050mg/Kg4-Isopropyl toluene 68-129 7.2 20
0.052 1051190.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 12.8 20
0.057 1141170.0580.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.7 20
0.052 10491.40.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 13.2 20
0.052 1051090.0540.050mg/KgMethylene Chloride 74-129 3.9 20
0.050 1021080.0530.050mg/KgNaphthalene 57-157 5.7 20
Page 5 of 8Date:11/04/2022 04:21 PM
Page 45 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.889.60.0440.050mg/Kgn-Propylbenzene 67-130 6.6 20
0.047 94.097.60.0480.050mg/KgStyrene 77-121 3.7 20
0.045 90.691.60.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.055 1101140.0570.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.046 92.696.20.0480.050mg/KgTetrachloroethene 68-130 3.8 20
0.047 94.298.20.0490.050mg/KgToluene 71-129 4.1 20
0.045 91.096.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.7 20
0.046 92.897.80.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.2 20
0.044 88.092.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.3 20
0.053 1081080.0540.050mg/Kg1,1,2-Trichloroethane 70-133 0.3 20
0.049 98.21050.0520.050mg/KgTrichloroethene 75-133 6.5 20
0.045 90.096.60.0480.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.056 1141150.0570.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.041 83.887.20.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.9 20
0.040 81.687.40.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.8 20
0.058 1171200.0590.050mg/KgVinyl Acetate 60-140 1.8 20
0.050 1011040.0520.050mg/KgVinyl Chloride 48-147 2.9 20
0.045 90.894.60.0470.050mg/Kgo-Xylene 74-126 4.0 20
0.087 87.490.90.0900.100mg/Kgm,p-Xylene 75-124 3.9 20
97.099.44-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)84-123
93.693.0Toluene-d8 (S)76-129
Page 6 of 8Date:11/04/2022 04:21 PM
Page 46 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V25891QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91551-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:193.519.420.1%Moisture
V 92190-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:190.036.236.2%Moisture
Page 7 of 8Date:11/04/2022 04:21 PM
Page 47 of 50
Quality Control Data
22-301-0007Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V25892QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91770-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:195.716.215.3%Moisture
V 91773-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:190.519.819.7%Moisture
Page 8 of 8Date:11/04/2022 04:21 PM
Page 48 of 50
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-301-0007
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/28/2022 14:41:17
Special precautions or instructions included?
Comments:
Page 49 of 50
Page 50 of 50

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/4/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-301-0020 Client Project Description: RMR-013
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/29/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 122
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-301-0020
Page 2 of 122
Report Number:
Sample Summary Table
Client Project Description:
22-301-0020
RMR-013
Lab No Client Sample ID Matrix Date Collected Date Received
10/28/2022 10:00Solids 91773 EX-SB-9 10/29/2022 15:44
10/28/2022 10:30Solids 91774 EX-SB-10 10/29/2022 15:44
10/28/2022 11:20Solids 91775 EX-SB-11 10/29/2022 15:44
10/28/2022 11:10Solids 91776 EX-SB-12 10/29/2022 15:44
10/28/2022 11:35Solids 91777 EX-SB-13 10/29/2022 15:44
10/28/2022 12:40Solids 91778 EX-SB-14 10/29/2022 15:44
10/28/2022 12:50Solids 91779 EX-SB-15 10/29/2022 15:44
10/28/2022 13:00Solids 91780 EX-SB-16 10/29/2022 15:44
10/28/2022 13:05Solids 91781 EX-SB-17 10/29/2022 15:44
10/28/2022 13:30Solids 91782 EX-SB-18 10/29/2022 15:44
10/28/2022 13:35Solids 91783 EX-SB-19 10/29/2022 15:44
10/28/2022 13:45Solids 91784 EX-SB-20 10/29/2022 15:44
10/28/2022 13:55Solids 91785 EX-SB-21 10/29/2022 15:44
10/28/2022 14:00Solids 91786 EX-SB-22 10/29/2022 15:44
10/28/2022 14:10Solids 91787 EX-SB-23 10/29/2022 15:44
10/28/2022 14:15Solids 91788 EX-SB-24 10/29/2022 15:44
10/28/2022 14:20Solids 91789 EX-SB-25 10/29/2022 15:44
10/28/2022 14:20Solids 91790 EX-SB-26 10/29/2022 15:44
10/28/2022Solids 91791 EX-SB-DUP 10/29/2022 15:44
Page 3 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0020
Report Limit
Project:RMR-013
V 91773EX-SB-9
J0.002 11/01/2022 14:038260DTrichloroethenemg/Kg - dry 0.001
19.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91774EX-SB-10
19.6 11/04/2022 11:19SW-DRYWT Moisture %
V 91775EX-SB-11
J0.003 11/01/2022 14:588260Dcis-1,2-Dichloroethene mg/Kg - dry 0.001
J0.002 11/01/2022 14:588260DMethylene Chloride mg/Kg - dry 0.001
21.8 11/04/2022 11:19SW-DRYWT Moisture %
V 91776EX-SB-12
J0.002 11/01/2022 15:258260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
0.007 11/01/2022 15:258260DTrichloroethenemg/Kg - dry 0.001
12.3 11/04/2022 11:19SW-DRYWT Moisture %
V 91777EX-SB-13
J0.011 11/01/2022 15:528260DAcetonemg/Kg - dry 0.002
J0.005 11/01/2022 15:528260D1,1-Dichloroethene mg/Kg - dry 0.0008
J0.001 11/01/2022 15:528260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
J0.002 11/01/2022 15:528260DMethylene Chloride mg/Kg - dry 0.001
0.019 11/01/2022 15:528260DTrichloroethenemg/Kg - dry 0.001
13.9 11/04/2022 11:19SW-DRYWT Moisture %
V 91778EX-SB-14
J0.009 11/01/2022 16:208260DAcetonemg/Kg - dry 0.002
13.1 11/04/2022 11:19SW-DRYWT Moisture %
V 91779EX-SB-15
J0.011 11/03/2022 16:138260DAcetonemg/Kg - dry 0.002
0.015 11/03/2022 16:138260DTrichloroethenemg/Kg - dry 0.001
12.9 11/04/2022 11:19SW-DRYWT Moisture %
V 91780EX-SB-16
0.025 11/01/2022 17:148260DAcetonemg/Kg - dry 0.003
J0.001 11/01/2022 17:148260DBenzenemg/Kg - dry 0.0007
J0.002 11/01/2022 17:148260DMethylene Chloride mg/Kg - dry 0.001
J0.002 11/01/2022 17:148260DToluenemg/Kg - dry 0.0008
0.008 11/01/2022 17:148260DTrichloroethenemg/Kg - dry 0.001
Page 4 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0020
Report Limit
Project:RMR-013
V 91780EX-SB-16
20.6 11/04/2022 11:19SW-DRYWT Moisture %
V 91781EX-SB-17
J0.012 11/01/2022 17:418260DAcetonemg/Kg - dry 0.003
J0.002 11/01/2022 17:418260D1,1-Dichloroethene mg/Kg - dry 0.001
J0.002 11/01/2022 17:418260DMethylene Chloride mg/Kg - dry 0.001
0.014 11/01/2022 17:418260DTrichloroethenemg/Kg - dry 0.001
25.2 11/04/2022 11:19SW-DRYWT Moisture %
V 91782EX-SB-18
J0.015 11/01/2022 18:098260DAcetonemg/Kg - dry 0.003
J0.001 11/01/2022 18:098260DBenzenemg/Kg - dry 0.0008
J0.002 11/01/2022 18:098260DToluenemg/Kg - dry 0.0009
J0.001 11/01/2022 18:098260DTrichloroethenemg/Kg - dry 0.001
23.9 11/04/2022 11:19SW-DRYWT Moisture %
V 91783EX-SB-19
J0.009 11/01/2022 18:368260DAcetonemg/Kg - dry 0.002
14.5 11/04/2022 11:19SW-DRYWT Moisture %
V 91784EX-SB-20
0.024 11/01/2022 19:038260DAcetonemg/Kg - dry 0.002
J0.002 11/01/2022 19:038260DBenzenemg/Kg - dry 0.0007
J0.005 11/01/2022 19:038260D1,1-Dichloroethane mg/Kg - dry 0.0009
0.021 11/01/2022 19:038260D1,1-Dichloroethene mg/Kg - dry 0.0008
J0.003 11/01/2022 19:038260DToluenemg/Kg - dry 0.0007
4.58 11/03/2022 22:358260D1,1,1-Trichloroethane mg/Kg - dry 0.040
0.060 11/01/2022 19:038260DTrichloroethenemg/Kg - dry 0.001
J0.0006 11/01/2022 19:038260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
11.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91785EX-SB-21
J0.012 11/01/2022 19:308260DAcetonemg/Kg - dry 0.002
J0.001 11/01/2022 19:308260DBenzenemg/Kg - dry 0.0007
J0.002 11/01/2022 19:308260DToluenemg/Kg - dry 0.0008
J0.002 11/01/2022 19:308260D1,1,1-Trichloroethane mg/Kg - dry 0.001
J0.002 11/01/2022 19:308260DTrichloroethenemg/Kg - dry 0.001
15.8 11/04/2022 11:19SW-DRYWT Moisture %
Page 5 of 122
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0020
Report Limit
Project:RMR-013
V 91786EX-SB-22
J0.008 11/03/2022 16:418260DAcetonemg/Kg - dry 0.002
J0.001 11/03/2022 16:418260DToluenemg/Kg - dry 0.0008
16.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91787EX-SB-23
J0.016 11/03/2022 17:088260DAcetonemg/Kg - dry 0.002
J0.001 11/03/2022 17:088260D1,1-Dichloroethene mg/Kg - dry 0.0008
0.023 11/03/2022 17:088260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
0.503 11/04/2022 12:588260DTrichloroethenemg/Kg - dry 0.026
13.6 11/04/2022 11:19SW-DRYWT Moisture %
V 91788EX-SB-24
J0.007 11/03/2022 17:358260DAcetonemg/Kg - dry 0.002
J0.003 11/03/2022 17:358260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
J0.004 11/03/2022 17:358260DTrichloroethenemg/Kg - dry 0.001
13.7 11/04/2022 11:19SW-DRYWT Moisture %
V 91789EX-SB-25
J0.006 11/03/2022 18:028260DAcetonemg/Kg - dry 0.002
J0.001 11/03/2022 18:028260DChloroformmg/Kg - dry 0.001
J0.001 11/03/2022 18:028260D1,1-Dichloroethane mg/Kg - dry 0.001
J0.003 11/03/2022 18:028260D1,1-Dichloroethene mg/Kg - dry 0.0009
0.043 11/03/2022 18:028260Dcis-1,2-Dichloroethene mg/Kg - dry 0.001
0.082 11/03/2022 18:028260DTrichloroethenemg/Kg - dry 0.001
18.2 11/04/2022 11:19SW-DRYWT Moisture %
V 91790EX-SB-26
J0.015 11/03/2022 18:308260DAcetonemg/Kg - dry 0.003
J0.001 11/03/2022 18:308260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 11/03/2022 18:308260D1,1-Dichloroethene mg/Kg - dry 0.0009
0.014 11/03/2022 18:308260Dcis-1,2-Dichloroethene mg/Kg - dry 0.001
J0.005 11/03/2022 18:308260DTrichloroethenemg/Kg - dry 0.001
22.6 11/04/2022 11:19SW-DRYWT Moisture %
V 91791EX-SB-DUP
J0.001 11/03/2022 18:578260DTrichloroethenemg/Kg - dry 0.001
19.1 11/04/2022 11:19SW-DRYWT Moisture %
Page 6 of 122

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: RMR-013 Lab Report Number: 22-301-0020
Date: 11/4/2022
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 4-Methyl-2-pentanone QC Batch No: V25789/V25787
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Acrylonitrile QC Batch No: V25789/V25787
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 7 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-9
91773 Matrix:
10/28/2022 10:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-9
91773 Matrix:
10/28/2022 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.002 mg/Kg - dry 0.002 0.024Acetone 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/01/22 14:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/01/22 14:03 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 14:03 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/01/22 14:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 14:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 14:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-9
91773 Matrix:
10/28/2022 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 14:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 14:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 14:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/01/22 14:03 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 14:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 14:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 14:03 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/01/22 14:03 V25789TBL
<0.017 mg/Kg - dry 0.017 0.311Ethanol 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 14:03 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/01/22 14:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-9
91773 Matrix:
10/28/2022 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 14:03 V25789TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 14:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/01/22 14:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 14:03 V25789TBL
0.002 J mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 14:03 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/01/22 14:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/01/22 14:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-9
91773 Matrix:
10/28/2022 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/01/22 14:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/01/22 14:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/01/22 14:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/01/22 14:03 V25789
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/01/22 14:031 TBL V25789
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/01/22 14:031 TBL V25789
Surrogate: Toluene-d8 89.6 Limits: 76-129%11/01/22 14:031 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-10
91774 Matrix:
10/28/2022 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-10
91774 Matrix:
10/28/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.002 mg/Kg - dry 0.002 0.024Acetone 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/01/22 14:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/01/22 14:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 14:30 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/01/22 14:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 14:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 14:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-10
91774 Matrix:
10/28/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 14:30 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 14:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 14:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/01/22 14:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 14:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 14:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 14:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/01/22 14:30 V25789TBL
<0.017 mg/Kg - dry 0.017 0.310Ethanol 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 14:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/01/22 14:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-10
91774 Matrix:
10/28/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 14:30 V25789TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 14:30 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/01/22 14:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 14:30 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/01/22 14:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/01/22 14:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-10
91774 Matrix:
10/28/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/01/22 14:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/01/22 14:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/01/22 14:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/01/22 14:30 V25789
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/01/22 14:301 TBL V25789
Surrogate: Dibromofluoromethane 101 Limits: 84-123%11/01/22 14:301 TBL V25789
Surrogate: Toluene-d8 90.6 Limits: 76-129%11/01/22 14:301 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-11
91775 Matrix:
10/28/2022 11:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.8 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-11
91775 Matrix:
10/28/2022 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.025Acetone 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 11/01/22 14:58 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 14:58 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/01/22 14:58 V25789TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/01/22 14:58 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/01/22 14:58 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 14:58 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 14:58 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-11
91775 Matrix:
10/28/2022 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 14:58 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 14:58 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 14:58 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/01/22 14:58 V25789TBL
0.003 J mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 14:58 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/01/22 14:58 V25789TBL
<0.017 mg/Kg - dry 0.017 0.319Ethanol 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/01/22 14:58 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-11
91775 Matrix:
10/28/2022 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 14:58 V25789TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/01/22 14:58 V25789TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 14:58 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/01/22 14:58 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 14:58 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/01/22 14:58 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/01/22 14:58 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-11
91775 Matrix:
10/28/2022 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/01/22 14:58 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/01/22 14:58 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/01/22 14:58 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/01/22 14:58 V25789
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/01/22 14:581 TBL V25789
Surrogate: Dibromofluoromethane 100 Limits: 84-123%11/01/22 14:581 TBL V25789
Surrogate: Toluene-d8 93.0 Limits: 76-129%11/01/22 14:581 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-12
91776 Matrix:
10/28/2022 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.3 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-12
91776 Matrix:
10/28/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.002 mg/Kg - dry 0.002 0.022Acetone 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 15:25 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 15:25 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 15:25 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/01/22 15:25 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 15:25 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-12
91776 Matrix:
10/28/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/01/22 15:25 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 15:25 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 15:25 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/01/22 15:25 V25789TBL
0.002 J mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 15:25 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/01/22 15:25 V25789TBL
<0.015 mg/Kg - dry 0.015 0.285Ethanol 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 15:25 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 15:25 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-12
91776 Matrix:
10/28/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 11/01/22 15:25 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 15:25 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 15:25 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 15:25 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 15:25 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 15:25 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/01/22 15:25 V25789TBL
0.007 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 15:25 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 15:25 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/01/22 15:25 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-12
91776 Matrix:
10/28/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 15:25 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 15:25 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 15:25 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 15:25 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 15:25 V25789
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/01/22 15:251 TBL V25789
Surrogate: Dibromofluoromethane 102 Limits: 84-123%11/01/22 15:251 TBL V25789
Surrogate: Toluene-d8 91.4 Limits: 76-129%11/01/22 15:251 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-13
91777 Matrix:
10/28/2022 11:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.9 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-13
91777 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.011 J mg/Kg - dry 0.002 0.023Acetone 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/01/22 15:52 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 15:52 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 15:52 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 15:52 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 15:52 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/01/22 15:52 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 15:52 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-13
91777 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/01/22 15:52 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 15:52 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 15:52 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 15:52 V25789TBL
0.005 J mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/01/22 15:52 V25789TBL
0.001 J mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 15:52 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 15:52 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 15:52 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/01/22 15:52 V25789TBL
<0.016 mg/Kg - dry 0.016 0.290Ethanol 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 15:52 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 15:52 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 15:52 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-13
91777 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/01/22 15:52 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 15:52 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 15:52 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/01/22 15:52 V25789TBL
0.002 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 15:52 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 15:52 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 15:52 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 15:52 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/01/22 15:52 V25789TBL
0.019 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 15:52 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 15:52 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/01/22 15:52 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-13
91777 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 15:52 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 15:52 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 15:52 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 15:52 V25789
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%11/01/22 15:521 TBL V25789
Surrogate: Dibromofluoromethane 106 Limits: 84-123%11/01/22 15:521 TBL V25789
Surrogate: Toluene-d8 90.8 Limits: 76-129%11/01/22 15:521 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-14
91778 Matrix:
10/28/2022 12:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-14
91778 Matrix:
10/28/2022 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.009 J mg/Kg - dry 0.002 0.023Acetone 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 16:20 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 16:20 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 16:20 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/01/22 16:20 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 16:20 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-14
91778 Matrix:
10/28/2022 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/01/22 16:20 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 16:20 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 16:20 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 16:20 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/01/22 16:20 V25789TBL
<0.016 mg/Kg - dry 0.016 0.287Ethanol 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 16:20 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 16:20 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 16:20 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-14
91778 Matrix:
10/28/2022 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/01/22 16:20 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.023Methyl Ethyl Ketone (MEK)1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 16:20 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 16:20 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 16:20 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 16:20 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 16:20 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 16:20 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 16:20 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/01/22 16:20 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-14
91778 Matrix:
10/28/2022 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 16:20 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 16:20 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 16:20 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 16:20 V25789
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/01/22 16:201 TBL V25789
Surrogate: Dibromofluoromethane 109 Limits: 84-123%11/01/22 16:201 TBL V25789
Surrogate: Toluene-d8 89.2 Limits: 76-129%11/01/22 16:201 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-15
91779 Matrix:
10/28/2022 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.9 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-15
91779 Matrix:
10/28/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
0.011 J mg/Kg - dry 0.002 0.022Acetone 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/03/22 16:13 V25896TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/03/22 16:13 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/03/22 16:13 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/03/22 16:13 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/03/22 16:13 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-15
91779 Matrix:
10/28/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/03/22 16:13 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/03/22 16:13 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/03/22 16:13 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/03/22 16:13 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/03/22 16:13 V25896TBL
<0.016 mg/Kg - dry 0.016 0.287Ethanol 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/03/22 16:13 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 16:13 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/03/22 16:13 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-15
91779 Matrix:
10/28/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 11/03/22 16:13 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/03/22 16:13 V25896TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/03/22 16:13 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/03/22 16:13 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/03/22 16:13 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/03/22 16:13 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/03/22 16:13 V25896TBL
0.015 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/03/22 16:13 V25896TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/03/22 16:13 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/03/22 16:13 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-15
91779 Matrix:
10/28/2022 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/03/22 16:13 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/03/22 16:13 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/03/22 16:13 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/03/22 16:13 V25896
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%11/03/22 16:131 TBL V25896
Surrogate: Dibromofluoromethane 102 Limits: 84-123%11/03/22 16:131 TBL V25896
Surrogate: Toluene-d8 99.1 Limits: 76-129%11/03/22 16:131 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-16
91780 Matrix:
10/28/2022 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-16
91780 Matrix:
10/28/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.025 mg/Kg - dry 0.003 0.025Acetone 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 11/01/22 17:14 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 11/01/22 17:14 V25789TBL
0.001 J mg/Kg - dry 0.0007 0.006Benzene 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 17:14 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/01/22 17:14 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 17:14 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 17:14 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-16
91780 Matrix:
10/28/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 17:14 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 17:14 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 17:14 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/01/22 17:14 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 17:14 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/01/22 17:14 V25789TBL
<0.017 mg/Kg - dry 0.017 0.314Ethanol 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 17:14 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/01/22 17:14 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-16
91780 Matrix:
10/28/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 17:14 V25789TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 11/01/22 17:14 V25789TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 17:14 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 17:14 V25789TBL
0.002 J mg/Kg - dry 0.0008 0.006Toluene 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/01/22 17:14 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 17:14 V25789TBL
0.008 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 17:14 V25789TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/01/22 17:14 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/01/22 17:14 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-16
91780 Matrix:
10/28/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/01/22 17:14 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/01/22 17:14 V25789TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/01/22 17:14 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/01/22 17:14 V25789
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/01/22 17:141 TBL V25789
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/01/22 17:141 TBL V25789
Surrogate: Toluene-d8 90.0 Limits: 76-129%11/01/22 17:141 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-17
91781 Matrix:
10/28/2022 13:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.2 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-17
91781 Matrix:
10/28/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.012 J mg/Kg - dry 0.003 0.026Acetone 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 17:41 V25789TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/01/22 17:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 11/01/22 17:41 V25789TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/01/22 17:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/01/22 17:41 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 17:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 17:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-17
91781 Matrix:
10/28/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 17:41 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 17:41 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 17:41 V25789TBL
0.002 J mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 17:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/01/22 17:41 V25789TBL
<0.018 mg/Kg - dry 0.018 0.334Ethanol 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/01/22 17:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-17
91781 Matrix:
10/28/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 11/01/22 17:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 17:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/01/22 17:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 17:41 V25789TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 11/01/22 17:41 V25789TBL
0.002 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 17:41 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 17:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 11/01/22 17:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 17:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 17:41 V25789TBL
0.014 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 17:41 V25789TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/01/22 17:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 11/01/22 17:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-17
91781 Matrix:
10/28/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 17:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/01/22 17:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/01/22 17:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/01/22 17:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/01/22 17:41 V25789
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%11/01/22 17:411 TBL V25789
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/01/22 17:411 TBL V25789
Surrogate: Toluene-d8 88.4 Limits: 76-129%11/01/22 17:411 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-18
91782 Matrix:
10/28/2022 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.9 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-18
91782 Matrix:
10/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.015 J mg/Kg - dry 0.003 0.026Acetone 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 11/01/22 18:09 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 11/01/22 18:09 V25789TBL
0.001 J mg/Kg - dry 0.0008 0.006Benzene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/01/22 18:09 V25789TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/01/22 18:09 V25789TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/01/22 18:09 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/01/22 18:09 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/01/22 18:09 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 11/01/22 18:09 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-18
91782 Matrix:
10/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/01/22 18:09 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/01/22 18:09 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/01/22 18:09 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/01/22 18:09 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/01/22 18:09 V25789TBL
<0.018 mg/Kg - dry 0.018 0.328Ethanol 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 11/01/22 18:09 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-18
91782 Matrix:
10/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/01/22 18:09 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/01/22 18:09 V25789TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/01/22 18:09 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/01/22 18:09 V25789TBL
0.002 J mg/Kg - dry 0.0009 0.006Toluene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 11/01/22 18:09 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/01/22 18:09 V25789TBL
0.001 J mg/Kg - dry 0.001 0.006Trichloroethene 1 11/01/22 18:09 V25789TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 11/01/22 18:09 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/01/22 18:09 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-18
91782 Matrix:
10/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 11/01/22 18:09 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 11/01/22 18:09 V25789TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 11/01/22 18:09 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 11/01/22 18:09 V25789
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/01/22 18:091 TBL V25789
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/01/22 18:091 TBL V25789
Surrogate: Toluene-d8 89.4 Limits: 76-129%11/01/22 18:091 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-19
91783 Matrix:
10/28/2022 13:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.5 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-19
91783 Matrix:
10/28/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.009 J mg/Kg - dry 0.002 0.023Acetone 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 18:36 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 18:36 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 18:36 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 18:36 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-19
91783 Matrix:
10/28/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/01/22 18:36 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 18:36 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 18:36 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 18:36 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/01/22 18:36 V25789TBL
<0.016 mg/Kg - dry 0.016 0.292Ethanol 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 18:36 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 18:36 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 18:36 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-19
91783 Matrix:
10/28/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/01/22 18:36 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 18:36 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 18:36 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 18:36 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 18:36 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 18:36 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 18:36 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 18:36 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 18:36 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/01/22 18:36 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-19
91783 Matrix:
10/28/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 18:36 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 18:36 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 18:36 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 18:36 V25789
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%11/01/22 18:361 TBL V25789
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/01/22 18:361 TBL V25789
Surrogate: Toluene-d8 88.4 Limits: 76-129%11/01/22 18:361 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-20
91784 Matrix:
10/28/2022 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-20
91784 Matrix:
10/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00 V25897 11/03/22 08:00
0.024 mg/Kg - dry 0.002 0.022Acetone 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 11/01/22 19:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/01/22 19:03 V25789TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 19:03 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 19:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 19:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/01/22 19:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 19:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-20
91784 Matrix:
10/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00 V25897 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/01/22 19:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 19:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 19:03 V25789TBL
0.005 J mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 19:03 V25789TBL
0.021 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 19:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/01/22 19:03 V25789TBL
<0.015 mg/Kg - dry 0.015 0.283Ethanol 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 19:03 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 19:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-20
91784 Matrix:
10/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00 V25897 11/03/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 11/01/22 19:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 19:03 V25789TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 19:03 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 19:03 V25789TBL
0.003 J mg/Kg - dry 0.0007 0.005Toluene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 19:03 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/01/22 19:03 V25789TBL
4.58 mg/Kg - dry 0.040 0.1411,1,1-Trichloroethane 50 11/03/22 22:35 V25898TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/01/22 19:03 V25789TBL
0.060 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 19:03 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 19:03 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/01/22 19:03 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-20
91784 Matrix:
10/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00 V25897 11/03/22 08:00
0.0006 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 19:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 19:03 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 19:03 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 19:03 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 19:03 V25789
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%11/01/22 19:031 TBL V25789
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/01/22 19:031 TBL V25789
Surrogate: Toluene-d8 89.4 Limits: 76-129%11/01/22 19:031 TBL V25789
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/03/22 22:3550 TBL V25898
Surrogate: Dibromofluoromethane 109 Limits: 70-130%11/03/22 22:3550 TBL V25898
Surrogate: Toluene-d8 105 Limits: 76-129%11/03/22 22:3550 TBL V25898
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-21
91785 Matrix:
10/28/2022 13:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.8 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-21
91785 Matrix:
10/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.012 J mg/Kg - dry 0.002 0.023Acetone 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/01/22 19:30 V25789TBL
0.001 J mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 19:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 19:30 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 19:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 19:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 19:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 19:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-21
91785 Matrix:
10/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/01/22 19:30 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 19:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 19:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 19:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 19:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 11/01/22 19:30 V25789TBL
<0.016 mg/Kg - dry 0.016 0.296Ethanol 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 19:30 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 19:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-21
91785 Matrix:
10/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/01/22 19:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 19:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/01/22 19:30 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 19:30 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 19:30 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 19:30 V25789TBL
0.002 J mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/01/22 19:30 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 11/01/22 19:30 V25789TBL
0.002 J mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 11/01/22 19:30 V25789TBL
0.002 J mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 19:30 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 19:30 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 11/01/22 19:30 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-21
91785 Matrix:
10/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/01/22 19:30 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 19:30 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 19:30 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 19:30 V25789
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%11/01/22 19:301 TBL V25789
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/01/22 19:301 TBL V25789
Surrogate: Toluene-d8 88.8 Limits: 76-129%11/01/22 19:301 TBL V25789
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-22
91786 Matrix:
10/28/2022 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-22
91786 Matrix:
10/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
0.008 J mg/Kg - dry 0.002 0.024Acetone 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/03/22 16:41 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/03/22 16:41 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/03/22 16:41 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/03/22 16:41 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/03/22 16:41 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/03/22 16:41 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/03/22 16:41 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-22
91786 Matrix:
10/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/03/22 16:41 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/03/22 16:41 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/03/22 16:41 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006cis-1,2-Dichloroethene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/03/22 16:41 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 11/03/22 16:41 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/03/22 16:41 V25896TBL
<0.016 mg/Kg - dry 0.016 0.300Ethanol 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/03/22 16:41 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.012Hexachlorobutadiene 1 11/03/22 16:41 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-22
91786 Matrix:
10/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.024
2-Hexanone 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/03/22 16:41 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/03/22 16:41 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 11/03/22 16:41 V25896TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/03/22 16:41 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/03/22 16:41 V25896TBL
0.001 J mg/Kg - dry 0.0008 0.006Toluene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 11/03/22 16:41 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/03/22 16:41 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/03/22 16:41 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/03/22 16:41 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-22
91786 Matrix:
10/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,3,5-Trimethylbenzene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/03/22 16:41 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/03/22 16:41 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/03/22 16:41 V25896
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%11/03/22 16:411 TBL V25896
Surrogate: Dibromofluoromethane 106 Limits: 84-123%11/03/22 16:411 TBL V25896
Surrogate: Toluene-d8 96.5 Limits: 76-129%11/03/22 16:411 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-23
91787 Matrix:
10/28/2022 14:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-23
91787 Matrix:
10/28/2022 14:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00 V25946 11/04/22 08:00
0.016 J mg/Kg - dry 0.002 0.023Acetone 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/03/22 17:08 V25896TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/03/22 17:08 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/03/22 17:08 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/03/22 17:08 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/03/22 17:08 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-23
91787 Matrix:
10/28/2022 14:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00 V25946 11/04/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/03/22 17:08 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/03/22 17:08 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/03/22 17:08 V25896TBL
0.001 J mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/03/22 17:08 V25896TBL
0.023 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/03/22 17:08 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/03/22 17:08 V25896TBL
<0.016 mg/Kg - dry 0.016 0.289Ethanol 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/03/22 17:08 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 17:08 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/03/22 17:08 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-23
91787 Matrix:
10/28/2022 14:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00 V25946 11/04/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/03/22 17:08 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/03/22 17:08 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/03/22 17:08 V25896TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/03/22 17:08 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/03/22 17:08 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/03/22 17:08 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/03/22 17:08 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/03/22 17:08 V25896TBL
0.503 mg/Kg - dry 0.026 0.144Trichloroethene 50 11/04/22 12:58 V25948TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/03/22 17:08 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/03/22 17:08 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-23
91787 Matrix:
10/28/2022 14:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00 V25946 11/04/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/03/22 17:08 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/03/22 17:08 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/03/22 17:08 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/03/22 17:08 V25896
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%11/03/22 17:081 TBL V25896
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/03/22 17:081 TBL V25896
Surrogate: Toluene-d8 97.8 Limits: 76-129%11/03/22 17:081 TBL V25896
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%11/04/22 12:5850 TBL V25948
Surrogate: Dibromofluoromethane 107 Limits: 70-130%11/04/22 12:5850 TBL V25948
Surrogate: Toluene-d8 115 Limits: 76-129%11/04/22 12:5850 TBL V25948
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 82 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-24
91788 Matrix:
10/28/2022 14:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.7 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-24
91788 Matrix:
10/28/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
0.007 J mg/Kg - dry 0.002 0.023Acetone 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 11/03/22 17:35 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/03/22 17:35 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/03/22 17:35 V25896TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/03/22 17:35 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/03/22 17:35 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-24
91788 Matrix:
10/28/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/03/22 17:35 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/03/22 17:35 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/03/22 17:35 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/03/22 17:35 V25896TBL
0.003 J mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/03/22 17:35 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/03/22 17:35 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/03/22 17:35 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/03/22 17:35 V25896TBL
<0.016 mg/Kg - dry 0.016 0.289Ethanol 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/03/22 17:35 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 17:35 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/03/22 17:35 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-24
91788 Matrix:
10/28/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 11/03/22 17:35 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/03/22 17:35 V25896TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/03/22 17:35 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/03/22 17:35 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/03/22 17:35 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/03/22 17:35 V25896TBL
0.004 J mg/Kg - dry 0.001 0.005Trichloroethene 1 11/03/22 17:35 V25896TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/03/22 17:35 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/03/22 17:35 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-24
91788 Matrix:
10/28/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/03/22 17:35 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/03/22 17:35 V25896TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/03/22 17:35 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/03/22 17:35 V25896
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%11/03/22 17:351 TBL V25896
Surrogate: Dibromofluoromethane 108 Limits: 84-123%11/03/22 17:351 TBL V25896
Surrogate: Toluene-d8 95.4 Limits: 76-129%11/03/22 17:351 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-25
91789 Matrix:
10/28/2022 14:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.2 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-25
91789 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/03/22 18:02 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/03/22 18:02 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/03/22 18:02 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/03/22 18:02 V25896TBL
0.001 J mg/Kg - dry 0.001 0.006Chloroform 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/03/22 18:02 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/03/22 18:02 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/03/22 18:02 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 89 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-25
91789 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/03/22 18:02 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/03/22 18:02 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/03/22 18:02 V25896TBL
0.001 J mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/03/22 18:02 V25896TBL
0.003 J mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/03/22 18:02 V25896TBL
0.043 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/03/22 18:02 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/03/22 18:02 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/03/22 18:02 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/03/22 18:02 V25896TBL
<0.017 mg/Kg - dry 0.017 0.305Ethanol 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 18:02 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/03/22 18:02 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 90 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-25
91789 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/03/22 18:02 V25896TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/03/22 18:02 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/03/22 18:02 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/03/22 18:02 V25896TBL
0.082 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/03/22 18:02 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/03/22 18:02 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/03/22 18:02 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 91 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-25
91789 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/03/22 18:02 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/03/22 18:02 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/03/22 18:02 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/03/22 18:02 V25896
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/03/22 18:021 TBL V25896
Surrogate: Dibromofluoromethane 110 Limits: 84-123%11/03/22 18:021 TBL V25896
Surrogate: Toluene-d8 95.8 Limits: 76-129%11/03/22 18:021 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 92 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-26
91790 Matrix:
10/28/2022 14:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 93 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-26
91790 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
0.015 J mg/Kg - dry 0.003 0.025Acetone 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 11/03/22 18:30 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/03/22 18:30 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/03/22 18:30 V25896TBL
0.001 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/03/22 18:30 V25896TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/03/22 18:30 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/03/22 18:30 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/03/22 18:30 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/03/22 18:30 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 94 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-26
91790 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/03/22 18:30 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/03/22 18:30 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/03/22 18:30 V25896TBL
0.001 J mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/03/22 18:30 V25896TBL
0.014 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/03/22 18:30 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/03/22 18:30 V25896TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/03/22 18:30 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 95 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-26
91790 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/03/22 18:30 V25896TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/03/22 18:30 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/03/22 18:30 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/03/22 18:30 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/03/22 18:30 V25896TBL
0.005 J mg/Kg - dry 0.001 0.006Trichloroethene 1 11/03/22 18:30 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/03/22 18:30 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/03/22 18:30 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 96 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-26
91790 Matrix:
10/28/2022 14:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/03/22 18:30 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/03/22 18:30 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/03/22 18:30 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/03/22 18:30 V25896
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/03/22 18:301 TBL V25896
Surrogate: Dibromofluoromethane 110 Limits: 84-123%11/03/22 18:301 TBL V25896
Surrogate: Toluene-d8 99.6 Limits: 76-129%11/03/22 18:301 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 97 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-DUP
91791 Matrix:
10/28/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.1 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 98 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-DUP
91791 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.002 mg/Kg - dry 0.002 0.024Acetone 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/03/22 18:57 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/03/22 18:57 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/03/22 18:57 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/03/22 18:57 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/03/22 18:57 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/03/22 18:57 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 99 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-DUP
91791 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/03/22 18:57 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/03/22 18:57 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/03/22 18:57 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/03/22 18:57 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/03/22 18:57 V25896TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/03/22 18:57 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/03/22 18:57 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/03/22 18:57 V25896TBL
<0.017 mg/Kg - dry 0.017 0.309Ethanol 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 11/03/22 18:57 V25896TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/03/22 18:57 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 100 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-DUP
91791 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/03/22 18:57 V25896TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/03/22 18:57 V25896TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/03/22 18:57 V25896TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/03/22 18:57 V25896TBL
0.001 J mg/Kg - dry 0.001 0.006Trichloroethene 1 11/03/22 18:57 V25896TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/03/22 18:57 V25896TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/03/22 18:57 V25896TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 101 of 122
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0020
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 10/29/2022
RMR-013
Report Date : 11/04/2022
Sample ID :
Lab No :
Sampled:EX-SB-DUP
91791 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25895 11/03/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/03/22 18:57 V25896TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/03/22 18:57 V25896TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/03/22 18:57 V25896TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/03/22 18:57 V25896
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/03/22 18:571 TBL V25896
Surrogate: Dibromofluoromethane 107 Limits: 84-123%11/03/22 18:571 TBL V25896
Surrogate: Toluene-d8 98.2 Limits: 76-129%11/03/22 18:571 TBL V25896
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 102 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778, 91780, 91781, 91782, 91783, 91784, 91785
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0200.002<0.002mg/KgAcetone
11/01/22 12:140.0200.001<0.001mg/KgAcrolein
11/01/22 12:140.0200.0008<0.0008mg/KgAcrylonitrile
11/01/22 12:140.0050.0006<0.0006mg/KgBenzene
11/01/22 12:140.0050.0005<0.0005mg/KgBromobenzene
11/01/22 12:140.0050.0008<0.0008mg/KgBromochloromethane
11/01/22 12:140.0050.001<0.001mg/KgBromodichloromethane
11/01/22 12:140.0050.001<0.001mg/KgBromoform
11/01/22 12:140.0100.001<0.001mg/KgBromomethane
11/01/22 12:140.0050.0005<0.0005mg/Kgn-Butylbenzene
11/01/22 12:140.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/01/22 12:140.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/01/22 12:140.0050.0006<0.0006mg/KgCarbon Disulfide
11/01/22 12:140.0050.001<0.001mg/KgCarbon Tetrachloride
11/01/22 12:140.0050.0007<0.0007mg/KgChlorobenzene
11/01/22 12:140.0050.0009<0.0009mg/KgChlorodibromomethane
11/01/22 12:140.0100.0009<0.0009mg/KgChloroethane
11/01/22 12:140.0050.001<0.001mg/KgChloroform
11/01/22 12:140.0100.0006<0.0006mg/KgChloromethane
11/01/22 12:140.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/01/22 12:140.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/01/22 12:140.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/01/22 12:140.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/01/22 12:140.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/01/22 12:140.0050.0006<0.0006mg/KgDibromomethane
11/01/22 12:140.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/01/22 12:140.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 16Date:11/04/2022 04:21 PM
Page 103 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778, 91780, 91781, 91782, 91783, 91784, 91785
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/01/22 12:140.0100.001<0.001mg/KgDichlorodifluoromethane
11/01/22 12:140.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/01/22 12:140.0050.001<0.001mg/Kg1,2-Dichloroethane
11/01/22 12:140.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/01/22 12:140.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/01/22 12:140.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/01/22 12:140.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/01/22 12:140.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/01/22 12:140.0050.001<0.001mg/Kg2,2-Dichloropropane
11/01/22 12:140.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/01/22 12:140.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/01/22 12:140.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/01/22 12:140.2500.014<0.014mg/KgEthanol
11/01/22 12:140.0050.0006<0.0006mg/KgEthylbenzene
11/01/22 12:140.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/01/22 12:140.0100.0008<0.0008mg/KgHexachlorobutadiene
11/01/22 12:140.0100.0007<0.0007mg/Kgn-Hexane
11/01/22 12:140.0200.0006<0.0006mg/Kg2-Hexanone
11/01/22 12:140.0050.0005<0.0005mg/KgIsopropylbenzene
11/01/22 12:140.0050.001<0.001mg/Kg4-Isopropyl toluene
11/01/22 12:140.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/01/22 12:140.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/01/22 12:140.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/01/22 12:140.0100.001<0.001mg/KgMethylene Chloride
11/01/22 12:140.0100.0010<0.0010mg/KgNaphthalene
11/01/22 12:140.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 2 of 16Date:11/04/2022 04:21 PM
Page 104 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778, 91780, 91781, 91782, 91783, 91784, 91785
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0050.001<0.001mg/KgStyrene
11/01/22 12:140.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/01/22 12:140.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/01/22 12:140.0050.0009<0.0009mg/KgTetrachloroethene
11/01/22 12:140.0050.0007<0.0007mg/KgToluene
11/01/22 12:140.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/01/22 12:140.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/01/22 12:140.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/01/22 12:140.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/01/22 12:140.0050.0009<0.0009mg/KgTrichloroethene
11/01/22 12:140.0100.002<0.002mg/KgTrichlorofluoromethane
11/01/22 12:140.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/01/22 12:140.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/01/22 12:140.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/01/22 12:140.0100.0005<0.0005mg/KgVinyl Acetate
11/01/22 12:140.0100.0005<0.0005mg/KgVinyl Chloride
11/01/22 12:140.0050.0005<0.0005mg/Kgo-Xylene
11/01/22 12:140.0100.001<0.001mg/Kgm,p-Xylene
11/01/22 12:144-Bromofluorobenzene (S)103 70-130
11/01/22 12:14Dibromofluoromethane (S)98.8 84-123
11/01/22 12:14Toluene-d8 (S)91.0 76-129
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091050.1050.100mg/KgAcetone 29-198 3.7 20
Page 3 of 16Date:11/04/2022 04:21 PM
Page 105 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.120 1201190.1190.100mg/KgAcrolein 70-130 0.8 20
0.097 97.01220.1220.100mg/KgAcrylonitrile 65-134 22.8*20
0.050 1021070.0530.050mg/KgBenzene 74-127 4.8 20
0.044 89.687.80.0430.050mg/KgBromobenzene 73-125 2.0 20
0.053 1071070.0530.050mg/KgBromochloromethane 72-134 0.3 20
0.056 1121130.0560.050mg/KgBromodichloromethane 75-122 0.5 20
0.052 10495.00.0470.050mg/KgBromoform 66-135 9.2 20
0.062 1251250.0620.050mg/KgBromomethane 20-180 0.4 20
0.043 87.890.20.0450.050mg/Kgn-Butylbenzene 65-135 2.6 20
0.044 89.091.00.0450.050mg/Kgsec-Butyl benzene 66-131 2.2 20
0.044 88.688.00.0440.050mg/Kgtert-Butyl benzene 67-132 0.6 20
0.048 96.699.20.0490.050mg/KgCarbon Disulfide 61-129 2.6 20
0.048 97.01020.0510.050mg/KgCarbon Tetrachloride 64-143 5.4 20
0.047 95.692.60.0460.050mg/KgChlorobenzene 74-118 3.1 20
0.051 10396.80.0480.050mg/KgChlorodibromomethane 73-122 6.4 20
0.051 1021010.0500.050mg/KgChloroethane 33-149 1.1 20
0.051 1031010.0500.050mg/KgChloroform 73-127 1.3 20
0.056 1141150.0570.050mg/KgChloromethane 45-143 1.0 20
0.043 86.087.80.0430.050mg/Kg2-Chlorotoluene 67-124 2.0 20
0.043 86.087.80.0430.050mg/Kg4-Chlorotoluene 71-126 2.0 20
0.057 1151160.0570.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.6 20
0.053 10898.80.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 8.5 20
0.054 1101020.0510.050mg/Kg1,2-Dibromoethane 70-132 7.1 20
0.054 1101080.0540.050mg/KgDibromomethane 74-133 1.1 20
0.045 90.089.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.044 88.687.60.0430.050mg/Kg1,3-Dichlorobenzene 71-120 1.1 20
Page 4 of 16* QC Fail Date:11/04/2022 04:21 PM
Page 106 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.288.40.0440.050mg/Kg1,4-Dichlorobenzene 71-123 0.9 20
0.045 91.497.40.0480.050mg/KgDichlorodifluoromethane 26-146 6.3 20
0.052 1041080.0530.050mg/Kg1,1-Dichloroethane 74-127 3.5 20
0.051 1031010.0500.050mg/Kg1,2-Dichloroethane 68-128 2.1 20
0.050 1001020.0500.050mg/Kg1,1-Dichloroethene 67-149 1.7 20
0.054 1091090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.1 20
0.050 1021060.0530.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.056 1131120.0550.050mg/Kg1,2-Dichloropropane 73-130 0.8 20
0.052 10496.20.0480.050mg/Kg1,3-Dichloropropane 75-124 8.1 20
0.049 98.01020.0500.050mg/Kg2,2-Dichloropropane 50-142 3.8 20
0.046 92.698.20.0490.050mg/Kg1,1-Dichloropropene 71-130 5.8 20
0.058 1171130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 3.6 20
0.055 1101080.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.0 20
1.28 1021031.291.25mg/KgEthanol 70-130 0.7 20
0.047 94.093.00.0460.050mg/KgEthylbenzene 74-128 1.0 20
0.112 1121090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.043 87.088.20.0440.050mg/KgHexachlorobutadiene 64-125 1.3 20
0.050 1021130.0560.050mg/Kgn-Hexane 70-130 10.7 20
0.058 1161080.0530.050mg/Kg2-Hexanone 61-157 7.6 20
0.043 86.688.00.0440.050mg/KgIsopropylbenzene 68-126 1.6 20
0.042 85.287.20.0430.050mg/Kg4-Isopropyl toluene 68-129 2.3 20
0.059 1191150.0570.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.5 20
0.055 1111050.0520.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.7 20
0.071 1421130.0560.050mg/Kg4-Methyl-2-Pentanone 57-162 23.3*20
0.055 1101080.0540.050mg/KgMethylene Chloride 74-129 1.8 20
0.047 94.686.60.0430.050mg/KgNaphthalene 57-157 8.8 20
Page 5 of 16* QC Fail Date:11/04/2022 04:21 PM
Page 107 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.892.80.0460.050mg/Kgn-Propylbenzene 67-130 3.2 20
0.049 99.096.80.0480.050mg/KgStyrene 77-121 2.2 20
0.046 93.289.20.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.3 20
0.050 10294.60.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 7.1 20
0.049 99.21020.0500.050mg/KgTetrachloroethene 68-130 2.3 20
0.050 1011020.0510.050mg/KgToluene 71-129 1.1 20
0.046 92.889.00.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 4.1 20
0.048 96.492.40.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.2 20
0.047 95.61000.0500.050mg/Kg1,1,1-Trichloroethane 67-131 4.8 20
0.053 10798.60.0490.050mg/Kg1,1,2-Trichloroethane 70-133 8.1 20
0.052 1051050.0520.050mg/KgTrichloroethene 75-133 0.0 20
0.049 98.41050.0520.050mg/KgTrichlorofluoromethane 44-146 6.1 20
0.051 10395.60.0470.050mg/Kg1,2,3-Trichloropropane 60-137 7.2 20
0.043 87.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.9 20
0.044 88.689.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.6 20
0.058 1161190.0590.050mg/KgVinyl Acetate 60-140 2.8 20
0.051 1031090.0540.050mg/KgVinyl Chloride 48-147 5.8 20
0.048 97.094.80.0470.050mg/Kgo-Xylene 74-126 2.2 20
0.093 93.192.60.0920.100mg/Kgm,p-Xylene 75-124 0.5 20
1011004-Bromofluorobenzene (S)70-130
99.2101Dibromofluoromethane (S)84-123
93.892.6Toluene-d8 (S)76-129
Page 6 of 16Date:11/04/2022 04:21 PM
Page 108 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
Associated Lab Samples: 91779, 91786, 91787, 91788, 91789, 91790, 91791
LRB-V25895 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/22 15:460.0200.002<0.002mg/KgAcetone
11/03/22 15:460.0200.001<0.001mg/KgAcrolein
11/03/22 15:460.0200.0008<0.0008mg/KgAcrylonitrile
11/03/22 15:460.0050.0006<0.0006mg/KgBenzene
11/03/22 15:460.0050.0005<0.0005mg/KgBromobenzene
11/03/22 15:460.0050.0008<0.0008mg/KgBromochloromethane
11/03/22 15:460.0050.001<0.001mg/KgBromodichloromethane
11/03/22 15:460.0050.001<0.001mg/KgBromoform
11/03/22 15:460.0100.001<0.001mg/KgBromomethane
11/03/22 15:460.0050.0005<0.0005mg/Kgn-Butylbenzene
11/03/22 15:460.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/03/22 15:460.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/03/22 15:460.0050.0006<0.0006mg/KgCarbon Disulfide
11/03/22 15:460.0050.001<0.001mg/KgCarbon Tetrachloride
11/03/22 15:460.0050.0007<0.0007mg/KgChlorobenzene
11/03/22 15:460.0050.0009<0.0009mg/KgChlorodibromomethane
11/03/22 15:460.0100.0009<0.0009mg/KgChloroethane
11/03/22 15:460.0050.001<0.001mg/KgChloroform
11/03/22 15:460.0100.0006<0.0006mg/KgChloromethane
11/03/22 15:460.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/03/22 15:460.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/03/22 15:460.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/03/22 15:460.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/03/22 15:460.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/03/22 15:460.0050.0006<0.0006mg/KgDibromomethane
11/03/22 15:460.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/03/22 15:460.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 7 of 16Date:11/04/2022 04:21 PM
Page 109 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
Associated Lab Samples: 91779, 91786, 91787, 91788, 91789, 91790, 91791
LRB-V25895 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/22 15:460.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/03/22 15:460.0100.001<0.001mg/KgDichlorodifluoromethane
11/03/22 15:460.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/03/22 15:460.0050.001<0.001mg/Kg1,2-Dichloroethane
11/03/22 15:460.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/03/22 15:460.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/03/22 15:460.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/03/22 15:460.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/03/22 15:460.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/03/22 15:460.0050.001<0.001mg/Kg2,2-Dichloropropane
11/03/22 15:460.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/03/22 15:460.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/03/22 15:460.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/03/22 15:460.2500.014<0.014mg/KgEthanol
11/03/22 15:460.0050.0006<0.0006mg/KgEthylbenzene
11/03/22 15:460.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/03/22 15:460.0100.0008<0.0008mg/KgHexachlorobutadiene
11/03/22 15:460.0100.0007<0.0007mg/Kgn-Hexane
11/03/22 15:460.0200.0006<0.0006mg/Kg2-Hexanone
11/03/22 15:460.0050.0005<0.0005mg/KgIsopropylbenzene
11/03/22 15:460.0050.001<0.001mg/Kg4-Isopropyl toluene
11/03/22 15:460.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/03/22 15:460.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/03/22 15:460.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/03/22 15:460.0100.001<0.001mg/KgMethylene Chloride
11/03/22 15:460.0100.0010<0.0010mg/KgNaphthalene
11/03/22 15:460.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 8 of 16Date:11/04/2022 04:21 PM
Page 110 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
Associated Lab Samples: 91779, 91786, 91787, 91788, 91789, 91790, 91791
LRB-V25895 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/22 15:460.0050.001<0.001mg/KgStyrene
11/03/22 15:460.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/03/22 15:460.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/03/22 15:460.0050.0009<0.0009mg/KgTetrachloroethene
11/03/22 15:460.0050.0007<0.0007mg/KgToluene
11/03/22 15:460.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/03/22 15:460.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/03/22 15:460.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/03/22 15:460.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/03/22 15:460.0050.0009<0.0009mg/KgTrichloroethene
11/03/22 15:460.0100.002<0.002mg/KgTrichlorofluoromethane
11/03/22 15:460.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/03/22 15:460.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/03/22 15:460.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/03/22 15:460.0100.0005<0.0005mg/KgVinyl Acetate
11/03/22 15:460.0100.0005<0.0005mg/KgVinyl Chloride
11/03/22 15:460.0050.0005<0.0005mg/Kgo-Xylene
11/03/22 15:460.0100.001<0.001mg/Kgm,p-Xylene
11/03/22 15:464-Bromofluorobenzene (S)104 70-130
11/03/22 15:46Dibromofluoromethane (S)102 84-123
11/03/22 15:46Toluene-d8 (S)95.4 76-129
LCS-V25895 LCSD-V25895Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.113 1131150.1150.100mg/KgAcetone 29-198 1.7 20
Page 9 of 16Date:11/04/2022 04:21 PM
Page 111 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
LCS-V25895 LCSD-V25895Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.287.90.0870.100mg/KgAcrolein 70-130 5.8 20
0.109 1091010.1010.100mg/KgAcrylonitrile 65-134 7.6 20
0.049 98.698.00.0490.050mg/KgBenzene 74-127 0.6 20
0.043 87.889.40.0440.050mg/KgBromobenzene 73-125 1.8 20
0.051 1031010.0500.050mg/KgBromochloromethane 72-134 2.1 20
0.060 1211200.0600.050mg/KgBromodichloromethane 75-122 0.3 20
0.052 10599.60.0490.050mg/KgBromoform 66-135 5.2 20
0.055 1121180.0580.050mg/KgBromomethane 20-180 5.2 20
0.046 93.495.60.0470.050mg/Kgn-Butylbenzene 65-135 2.3 20
0.044 89.893.00.0460.050mg/Kgsec-Butyl benzene 66-131 3.5 20
0.045 90.292.40.0460.050mg/Kgtert-Butyl benzene 67-132 2.4 20
0.044 88.691.80.0450.050mg/KgCarbon Disulfide 61-129 3.5 20
0.058 1171210.0600.050mg/KgCarbon Tetrachloride 64-143 2.6 20
0.046 92.290.80.0450.050mg/KgChlorobenzene 74-118 1.5 20
0.052 10699.60.0490.050mg/KgChlorodibromomethane 73-122 6.0 20
0.043 87.087.20.0430.050mg/KgChloroethane 33-149 0.2 20
0.054 1091050.0520.050mg/KgChloroform 73-127 3.7 20
0.052 1051030.0510.050mg/KgChloromethane 45-143 1.9 20
0.043 87.288.80.0440.050mg/Kg2-Chlorotoluene 67-124 1.8 20
0.043 87.288.80.0440.050mg/Kg4-Chlorotoluene 71-126 1.8 20
0.056 1131100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.0 20
0.045 90.087.60.0430.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.7 20
0.048 96.897.60.0480.050mg/Kg1,2-Dibromoethane 70-132 0.8 20
0.053 1071020.0510.050mg/KgDibromomethane 74-133 4.5 20
0.043 87.489.20.0440.050mg/Kg1,2-Dichlorobenzene 72-123 2.0 20
0.043 86.686.60.0430.050mg/Kg1,3-Dichlorobenzene 71-120 0.0 20
Page 10 of 16Date:11/04/2022 04:21 PM
Page 112 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
LCS-V25895 LCSD-V25895Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.288.20.0440.050mg/Kg1,4-Dichlorobenzene 71-123 1.1 20
0.046 92.695.20.0470.050mg/KgDichlorodifluoromethane 26-146 2.7 20
0.051 1041020.0500.050mg/Kg1,1-Dichloroethane 74-127 1.9 20
0.059 1191180.0590.050mg/Kg1,2-Dichloroethane 68-128 0.5 20
0.053 1061100.0550.050mg/Kg1,1-Dichloroethene 67-149 3.3 20
0.053 1081100.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 1.6 20
0.053 1081060.0530.050mg/Kgtrans-1,2-Dichloroethene 73-132 1.4 20
0.051 10297.20.0480.050mg/Kg1,2-Dichloropropane 73-130 4.8 20
0.047 95.893.80.0460.050mg/Kg1,3-Dichloropropane 75-124 2.1 20
0.056 1121110.0550.050mg/Kg2,2-Dichloropropane 50-142 0.7 20
0.050 1011020.0510.050mg/Kg1,1-Dichloropropene 71-130 0.9 20
0.055 1121080.0540.050mg/Kgcis-1,3-Dichloropropene 71-125 3.2 20
0.056 1131120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.2 20
1.35 10892.81.161.25mg/KgEthanol 70-130 15.1 20
0.048 96.296.40.0480.050mg/KgEthylbenzene 74-128 0.2 20
0.109 1091060.1060.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.045 91.895.20.0470.050mg/KgHexachlorobutadiene 64-125 3.6 20
0.051 1041060.0530.050mg/Kgn-Hexane 70-130 2.2 20
0.055 1111100.0550.050mg/Kg2-Hexanone 61-157 0.1 20
0.043 87.490.20.0450.050mg/KgIsopropylbenzene 68-126 3.1 20
0.045 90.492.40.0460.050mg/Kg4-Isopropyl toluene 68-129 2.1 20
0.061 1221110.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 9.2 20
0.053 1071070.0530.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.067 1361280.0630.050mg/Kg4-Methyl-2-Pentanone 57-162 6.0 20
0.054 1091080.0540.050mg/KgMethylene Chloride 74-129 1.1 20
0.042 84.884.20.0420.050mg/KgNaphthalene 57-157 0.7 20
Page 11 of 16Date:11/04/2022 04:21 PM
Page 113 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25896QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25895
LCS-V25895 LCSD-V25895Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.893.00.0460.050mg/Kgn-Propylbenzene 67-130 2.3 20
0.050 10096.60.0480.050mg/KgStyrene 77-121 3.6 20
0.048 96.296.00.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.2 20
0.042 85.482.60.0410.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.053 1071060.0530.050mg/KgTetrachloroethene 68-130 0.9 20
0.049 98.099.00.0490.050mg/KgToluene 71-129 1.0 20
0.043 87.289.60.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.7 20
0.045 90.693.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.6 20
0.058 1171210.0600.050mg/Kg1,1,1-Trichloroethane 67-131 3.0 20
0.047 94.691.60.0450.050mg/Kg1,1,2-Trichloroethane 70-133 3.2 20
0.051 10399.80.0490.050mg/KgTrichloroethene 75-133 3.3 20
0.055 1111110.0550.050mg/KgTrichlorofluoromethane 44-146 0.5 20
0.048 96.097.60.0480.050mg/Kg1,2,3-Trichloropropane 60-137 1.6 20
0.044 88.493.00.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 5.0 20
0.045 91.091.40.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.4 20
0.049 98.486.80.0430.050mg/KgVinyl Acetate 60-140 12.5 20
0.044 89.291.60.0450.050mg/KgVinyl Chloride 48-147 2.6 20
0.050 1011010.0500.050mg/Kgo-Xylene 74-126 0.5 20
0.098 98.797.40.0970.100mg/Kgm,p-Xylene 75-124 1.3 20
98.21014-Bromofluorobenzene (S)70-130
10398.2Dibromofluoromethane (S)84-123
93.892.4Toluene-d8 (S)76-129
Page 12 of 16Date:11/04/2022 04:21 PM
Page 114 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25898QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V25897
Associated Lab Samples: 91784
LRB-V25897 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/22 15:460.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/03/22 15:464-Bromofluorobenzene (S)104 70-130
11/03/22 15:46Dibromofluoromethane (S)102 70-130
11/03/22 15:46Toluene-d8 (S)95.4 76-129
LCS-V25897 LCSD-V25897Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.058 1171210.0600.050mg/Kg1,1,1-Trichloroethane 67-131 3.0 20
98.21014-Bromofluorobenzene (S)70-130
10398.2Dibromofluoromethane (S)70-130
93.892.4Toluene-d8 (S)76-129
Page 13 of 16Date:11/04/2022 04:21 PM
Page 115 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25948QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V25946
Associated Lab Samples: 91787
LRB-V25946 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 10:410.0050.0009<0.0009mg/KgTrichloroethene
11/04/22 10:414-Bromofluorobenzene (S)106 70-130
11/04/22 10:41Dibromofluoromethane (S)107 70-130
11/04/22 10:41Toluene-d8 (S)115 76-129
LCS-V25946 LCSD-V25946Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 76.078.00.0390.050mg/KgTrichloroethene 75-133 2.5 20
1041044-Bromofluorobenzene (S)70-130
105108Dibromofluoromethane (S)70-130
113112Toluene-d8 (S)76-129
Page 14 of 16Date:11/04/2022 04:21 PM
Page 116 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V25892QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91770-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:195.716.215.3%Moisture
V 91773-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:190.519.819.7%Moisture
Page 15 of 16Date:11/04/2022 04:21 PM
Page 117 of 122
Quality Control Data
22-301-0020Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V25893QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91791-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:194.119.919.1%Moisture
V 91812-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:194.627.228.5%Moisture
Page 16 of 16Date:11/04/2022 04:21 PM
Page 118 of 122
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-301-0020
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/29/2022 11:22:29
Special precautions or instructions included?
Comments:
Page 119 of 122
Page 120 of 122
Page 121 of 122
Page 122 of 122

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/10/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-313-0005 Client Project Description: RMR-013
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/9/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 29
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-313-0005
Page 2 of 29
Report Number:
Sample Summary Table
Client Project Description:
22-313-0005
RMR-013
Lab No Client Sample ID Matrix Date Collected Date Received
11/09/2022 07:55Solids 92709 EX-SB-20a 11/09/2022 09:52
11/09/2022 08:00Solids 92710 EX-SB-23a 11/09/2022 09:52
11/09/2022 08:05Solids 92711 EX-SB-25a 11/09/2022 09:52
Page 3 of 29
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-313-0005
Report Limit
Project:RMR-013
V 92709EX-SB-20a
J0.013 11/09/2022 14:348260DAcetonemg/Kg - dry 0.002
J0.007 11/09/2022 14:348260DMethylene Chloride mg/Kg - dry 0.001
18.4 11/10/2022 10:23SW-DRYWT Moisture %
V 92710EX-SB-23a
J0.014 11/09/2022 15:028260DAcetonemg/Kg - dry 0.002
J0.001 11/09/2022 15:028260Dcis-1,2-Dichloroethene mg/Kg - dry 0.001
J0.007 11/09/2022 15:028260DMethylene Chloride mg/Kg - dry 0.001
0.010 11/09/2022 15:028260DTrichloroethenemg/Kg - dry 0.001
18.9 11/10/2022 10:23SW-DRYWT Moisture %
V 92711EX-SB-25a
J0.014 11/09/2022 15:298260DAcetonemg/Kg - dry 0.002
J0.002 11/09/2022 15:298260Dcis-1,2-Dichloroethene mg/Kg - dry 0.0009
J0.004 11/09/2022 15:298260DMethylene Chloride mg/Kg - dry 0.001
0.009 11/09/2022 15:298260DTrichloroethenemg/Kg - dry 0.001
11.6 11/10/2022 10:23SW-DRYWT Moisture %
Page 4 of 29

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: RMR-013 Lab Report Number: 22-313-0005
Date: 11/10/2022
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Hexane QC Batch No: V26222/V26221
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 5 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-20a
92709 Matrix:
11/9/2022 7:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.4 %Moisture 1 11/10/22 10:23 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-20a
92709 Matrix:
11/9/2022 7:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
0.013 J mg/Kg - dry 0.002 0.024Acetone 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/09/22 14:34 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/09/22 14:34 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/09/22 14:34 V26222MSA
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/09/22 14:34 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/09/22 14:34 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/09/22 14:34 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-20a
92709 Matrix:
11/9/2022 7:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/09/22 14:34 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/09/22 14:34 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/09/22 14:34 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/09/22 14:34 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/09/22 14:34 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/09/22 14:34 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/09/22 14:34 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/09/22 14:34 V26222MSA
<0.017 mg/Kg - dry 0.017 0.306Ethanol 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 11/09/22 14:34 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/09/22 14:34 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-20a
92709 Matrix:
11/9/2022 7:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/09/22 14:34 V26222MSA
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/09/22 14:34 V26222MSA
0.007 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/09/22 14:34 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/09/22 14:34 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/09/22 14:34 V26222MSA
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/09/22 14:34 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/09/22 14:34 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-20a
92709 Matrix:
11/9/2022 7:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/09/22 14:34 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/09/22 14:34 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/09/22 14:34 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/09/22 14:34 V26222
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%11/09/22 14:341 MSA V26222
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/09/22 14:341 MSA V26222
Surrogate: Toluene-d8 101 Limits: 76-129%11/09/22 14:341 MSA V26222
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-23a
92710 Matrix:
11/9/2022 8:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.9 %Moisture 1 11/10/22 10:23 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-23a
92710 Matrix:
11/9/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
0.014 J mg/Kg - dry 0.002 0.024Acetone 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 11/09/22 15:02 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/09/22 15:02 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/09/22 15:02 V26222MSA
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 11/09/22 15:02 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/09/22 15:02 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/09/22 15:02 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-23a
92710 Matrix:
11/9/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/09/22 15:02 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/09/22 15:02 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/09/22 15:02 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/09/22 15:02 V26222MSA
0.001 J mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/09/22 15:02 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/09/22 15:02 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/09/22 15:02 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 11/09/22 15:02 V26222MSA
<0.017 mg/Kg - dry 0.017 0.308Ethanol 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 11/09/22 15:02 V26222MSA
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 11/09/22 15:02 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-23a
92710 Matrix:
11/9/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/09/22 15:02 V26222MSA
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 11/09/22 15:02 V26222MSA
0.007 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/09/22 15:02 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 11/09/22 15:02 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/09/22 15:02 V26222MSA
0.010 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/09/22 15:02 V26222MSA
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/09/22 15:02 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/09/22 15:02 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-23a
92710 Matrix:
11/9/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/09/22 15:02 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/09/22 15:02 V26222MSA
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/09/22 15:02 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/09/22 15:02 V26222
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%11/09/22 15:021 MSA V26222
Surrogate: Dibromofluoromethane 103 Limits: 84-123%11/09/22 15:021 MSA V26222
Surrogate: Toluene-d8 98.5 Limits: 76-129%11/09/22 15:021 MSA V26222
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-25a
92711 Matrix:
11/9/2022 8:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.6 %Moisture 1 11/10/22 10:23 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-25a
92711 Matrix:
11/9/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
0.014 J mg/Kg - dry 0.002 0.022Acetone 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 11/09/22 15:29 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/09/22 15:29 V26222MSA
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/09/22 15:29 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/09/22 15:29 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 11/09/22 15:29 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 11/09/22 15:29 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-25a
92711 Matrix:
11/9/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 11/09/22 15:29 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/09/22 15:29 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/09/22 15:29 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 11/09/22 15:29 V26222MSA
0.002 J mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/09/22 15:29 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 11/09/22 15:29 V26222MSA
<0.015 mg/Kg - dry 0.015 0.282Ethanol 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 11/09/22 15:29 V26222MSA
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/09/22 15:29 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-25a
92711 Matrix:
11/9/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 11/09/22 15:29 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/09/22 15:29 V26222MSA
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 11/09/22 15:29 V26222MSA
0.004 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/09/22 15:29 V26222MSA
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 11/09/22 15:29 V26222MSA
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/09/22 15:29 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 11/09/22 15:29 V26222MSA
0.009 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/09/22 15:29 V26222MSA
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/09/22 15:29 V26222MSA
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 11/09/22 15:29 V26222MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 29
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-313-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/09/2022
RMR-013
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:EX-SB-25a
92711 Matrix:
11/9/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V26221 11/09/22 06:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 11/09/22 15:29 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 11/09/22 15:29 V26222MSA
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/09/22 15:29 V26222MSA
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/09/22 15:29 V26222MSA
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/09/22 15:29 V26222
Surrogate: 4-Bromofluorobenzene 97.5 Limits: 70-130%11/09/22 15:291 MSA V26222
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/09/22 15:291 MSA V26222
Surrogate: Toluene-d8 100 Limits: 76-129%11/09/22 15:291 MSA V26222
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
Associated Lab Samples: 92709, 92710, 92711
LRB-V26221 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/09/22 14:070.0200.002<0.002mg/KgAcetone
11/09/22 14:070.0200.001<0.001mg/KgAcrolein
11/09/22 14:070.0200.0008<0.0008mg/KgAcrylonitrile
11/09/22 14:070.0050.0006<0.0006mg/KgBenzene
11/09/22 14:070.0050.0005<0.0005mg/KgBromobenzene
11/09/22 14:070.0050.0008<0.0008mg/KgBromochloromethane
11/09/22 14:070.0050.001<0.001mg/KgBromodichloromethane
11/09/22 14:070.0050.001<0.001mg/KgBromoform
11/09/22 14:070.0100.001<0.001mg/KgBromomethane
11/09/22 14:070.0050.0005<0.0005mg/Kgn-Butylbenzene
11/09/22 14:070.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/09/22 14:070.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/09/22 14:070.0050.0006<0.0006mg/KgCarbon Disulfide
11/09/22 14:070.0050.001<0.001mg/KgCarbon Tetrachloride
11/09/22 14:070.0050.0007<0.0007mg/KgChlorobenzene
11/09/22 14:070.0050.0009<0.0009mg/KgChlorodibromomethane
11/09/22 14:070.0100.0009<0.0009mg/KgChloroethane
11/09/22 14:070.0050.001<0.001mg/KgChloroform
11/09/22 14:070.0100.0006<0.0006mg/KgChloromethane
11/09/22 14:070.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/09/22 14:070.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/09/22 14:070.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/09/22 14:070.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/09/22 14:070.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/09/22 14:070.0050.0006<0.0006mg/KgDibromomethane
11/09/22 14:070.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/09/22 14:070.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 7Date:11/10/2022 03:06 PM
Page 21 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
Associated Lab Samples: 92709, 92710, 92711
LRB-V26221 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/09/22 14:070.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/09/22 14:070.0100.001<0.001mg/KgDichlorodifluoromethane
11/09/22 14:070.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/09/22 14:070.0050.001<0.001mg/Kg1,2-Dichloroethane
11/09/22 14:070.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/09/22 14:070.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/09/22 14:070.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/09/22 14:070.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/09/22 14:070.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/09/22 14:070.0050.001<0.001mg/Kg2,2-Dichloropropane
11/09/22 14:070.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/09/22 14:070.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/09/22 14:070.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/09/22 14:070.2500.014<0.014mg/KgEthanol
11/09/22 14:070.0050.0006<0.0006mg/KgEthylbenzene
11/09/22 14:070.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/09/22 14:070.0100.0008<0.0008mg/KgHexachlorobutadiene
11/09/22 14:070.0100.0007<0.0007mg/Kgn-Hexane
11/09/22 14:070.0200.0006<0.0006mg/Kg2-Hexanone
11/09/22 14:070.0050.0005<0.0005mg/KgIsopropylbenzene
11/09/22 14:070.0050.001<0.001mg/Kg4-Isopropyl toluene
11/09/22 14:070.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/09/22 14:070.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/09/22 14:070.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/09/22 14:070.0100.001<0.001mg/KgMethylene Chloride
11/09/22 14:070.0100.0010<0.0010mg/KgNaphthalene
11/09/22 14:070.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 2 of 7Date:11/10/2022 03:06 PM
Page 22 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
Associated Lab Samples: 92709, 92710, 92711
LRB-V26221 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/09/22 14:070.0050.001<0.001mg/KgStyrene
11/09/22 14:070.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/09/22 14:070.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/09/22 14:070.0050.0009<0.0009mg/KgTetrachloroethene
11/09/22 14:070.0050.0007<0.0007mg/KgToluene
11/09/22 14:070.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/09/22 14:070.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/09/22 14:070.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/09/22 14:070.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/09/22 14:070.0050.0009<0.0009mg/KgTrichloroethene
11/09/22 14:070.0100.002<0.002mg/KgTrichlorofluoromethane
11/09/22 14:070.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/09/22 14:070.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/09/22 14:070.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/09/22 14:070.0100.0005<0.0005mg/KgVinyl Acetate
11/09/22 14:070.0100.0005<0.0005mg/KgVinyl Chloride
11/09/22 14:070.0050.0005<0.0005mg/Kgo-Xylene
11/09/22 14:070.0100.001<0.001mg/Kgm,p-Xylene
11/09/22 14:074-Bromofluorobenzene (S)95.4 70-130
11/09/22 14:07Dibromofluoromethane (S)103 84-123
11/09/22 14:07Toluene-d8 (S)102 76-129
LCS-V26221 LCSD-V26221Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.41000.1000.100mg/KgAcetone 29-198 2.6 20
Page 3 of 7Date:11/10/2022 03:06 PM
Page 23 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
LCS-V26221 LCSD-V26221Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091180.1180.100mg/KgAcrolein 70-130 7.9 20
0.110 1101120.1120.100mg/KgAcrylonitrile 65-134 1.8 20
0.047 94.497.40.0480.050mg/KgBenzene 74-127 3.1 20
0.046 93.090.80.0450.050mg/KgBromobenzene 73-125 2.3 20
0.048 97.293.20.0460.050mg/KgBromochloromethane 72-134 4.2 20
0.046 93.292.40.0460.050mg/KgBromodichloromethane 75-122 0.8 20
0.046 93.091.20.0450.050mg/KgBromoform 66-135 1.9 20
0.050 10098.80.0490.050mg/KgBromomethane 20-180 1.2 20
0.046 93.496.00.0480.050mg/Kgn-Butylbenzene 65-135 2.7 20
0.045 91.291.60.0450.050mg/Kgsec-Butyl benzene 66-131 0.4 20
0.043 87.289.20.0440.050mg/Kgtert-Butyl benzene 67-132 2.2 20
0.044 88.291.40.0450.050mg/KgCarbon Disulfide 61-129 3.5 20
0.041 83.891.80.0450.050mg/KgCarbon Tetrachloride 64-143 9.1 20
0.046 92.291.40.0450.050mg/KgChlorobenzene 74-118 0.8 20
0.044 88.885.60.0420.050mg/KgChlorodibromomethane 73-122 3.6 20
0.044 89.291.80.0450.050mg/KgChloroethane 33-149 2.8 20
0.046 92.295.40.0470.050mg/KgChloroform 73-127 3.4 20
0.036 73.478.80.0390.050mg/KgChloromethane 45-143 7.0 20
0.046 93.892.40.0460.050mg/Kg2-Chlorotoluene 67-124 1.5 20
0.047 94.092.40.0460.050mg/Kg4-Chlorotoluene 71-126 1.7 20
0.052 1051030.0510.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.5 20
0.044 88.890.60.0450.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.0 20
0.049 98.895.60.0470.050mg/Kg1,2-Dibromoethane 70-132 3.2 20
0.048 97.497.40.0480.050mg/KgDibromomethane 74-133 0.0 20
0.046 93.493.20.0460.050mg/Kg1,2-Dichlorobenzene 72-123 0.2 20
0.047 94.493.00.0460.050mg/Kg1,3-Dichlorobenzene 71-120 1.4 20
Page 4 of 7Date:11/10/2022 03:06 PM
Page 24 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
LCS-V26221 LCSD-V26221Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.688.00.0440.050mg/Kg1,4-Dichlorobenzene 71-123 4.0 20
0.043 86.092.00.0460.050mg/KgDichlorodifluoromethane 26-146 6.7 20
0.047 94.296.00.0480.050mg/Kg1,1-Dichloroethane 74-127 1.8 20
0.052 1041020.0510.050mg/Kg1,2-Dichloroethane 68-128 1.9 20
0.044 89.094.20.0470.050mg/Kg1,1-Dichloroethene 67-149 5.6 20
0.045 91.095.00.0470.050mg/Kgcis-1,2-Dichloroethene 76-134 4.3 20
0.046 92.492.60.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 0.2 20
0.049 99.81030.0510.050mg/Kg1,2-Dichloropropane 73-130 2.7 20
0.048 97.096.40.0480.050mg/Kg1,3-Dichloropropane 75-124 0.6 20
0.047 95.695.20.0470.050mg/Kg2,2-Dichloropropane 50-142 0.4 20
0.046 93.093.80.0460.050mg/Kg1,1-Dichloropropene 71-130 0.8 20
0.048 97.297.00.0480.050mg/Kgcis-1,3-Dichloropropene 71-125 0.2 20
0.050 1001030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.9 20
1.32 1061051.311.25mg/KgEthanol 70-130 0.7 20
0.044 89.091.20.0450.050mg/KgEthylbenzene 74-128 2.4 20
0.103 1031040.1040.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.044 88.888.20.0440.050mg/KgHexachlorobutadiene 64-125 0.6 20
0.041 82.01050.0520.050mg/Kgn-Hexane 70-130 24.4*20
0.054 1081130.0560.050mg/Kg2-Hexanone 61-157 4.8 20
0.043 87.289.00.0440.050mg/KgIsopropylbenzene 68-126 2.0 20
0.045 91.092.80.0460.050mg/Kg4-Isopropyl toluene 68-129 1.9 20
0.054 1081150.0570.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.7 20
0.048 96.696.60.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.0 20
0.054 1091100.0550.050mg/Kg4-Methyl-2-Pentanone 57-162 1.2 20
0.047 95.297.20.0480.050mg/KgMethylene Chloride 74-129 2.0 20
0.048 97.295.60.0470.050mg/KgNaphthalene 57-157 1.6 20
Page 5 of 7* QC Fail Date:11/10/2022 03:06 PM
Page 25 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V26222QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V26221
LCS-V26221 LCSD-V26221Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.491.40.0450.050mg/Kgn-Propylbenzene 67-130 0.0 20
0.046 93.493.40.0460.050mg/KgStyrene 77-121 0.0 20
0.044 89.688.20.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.5 20
0.047 94.690.00.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 4.9 20
0.044 88.092.40.0460.050mg/KgTetrachloroethene 68-130 4.8 20
0.045 91.094.80.0470.050mg/KgToluene 71-129 4.0 20
0.049 98.895.20.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.7 20
0.047 94.495.20.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.8 20
0.045 91.495.80.0470.050mg/Kg1,1,1-Trichloroethane 67-131 4.7 20
0.046 92.493.20.0460.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.043 87.891.60.0450.050mg/KgTrichloroethene 75-133 4.2 20
0.043 86.091.80.0450.050mg/KgTrichlorofluoromethane 44-146 6.5 20
0.044 88.688.60.0440.050mg/Kg1,2,3-Trichloropropane 60-137 0.0 20
0.044 88.690.00.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.5 20
0.044 89.289.40.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.2 20
0.048 96.293.00.0460.050mg/KgVinyl Acetate 60-140 3.3 20
0.044 88.296.40.0480.050mg/KgVinyl Chloride 48-147 8.8 20
0.047 95.691.40.0450.050mg/Kgo-Xylene 74-126 4.4 20
0.090 90.692.40.0920.100mg/Kgm,p-Xylene 75-124 1.9 20
97.895.04-Bromofluorobenzene (S)70-130
101102Dibromofluoromethane (S)84-123
103101Toluene-d8 (S)76-129
Page 6 of 7Date:11/10/2022 03:06 PM
Page 26 of 29
Quality Control Data
22-313-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR-013
Dry Weight Determination
SW-DRYWT
V26196QC Analytical Batch:
Analysis Method:
Analysis Description:
V 92188-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/10/22 10:234.413.813.2%Moisture
V 92569-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/10/22 10:232.619.118.6%Moisture
Page 7 of 7Date:11/10/2022 03:06 PM
Page 27 of 29
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-313-0005
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/09/2022 11:04:43
Special precautions or instructions included?
Comments:
Page 28 of 29
Page 29 of 29

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/5/2022
Hart & Hickman (Charlotte) Alexis McKenzie
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-327-0028 Client Project Description: RMR.013
Dear Alexis McKenzie:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/23/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 23
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-327-0028
Page 2 of 23
Report Number:
Sample Summary Table
Client Project Description:
22-327-0028
RMR.013
Lab No Client Sample ID Matrix Date Collected Date Received
11/23/2022Air 94145 SG-DUP-112322 11/23/2022 12:40
11/23/2022 08:39Air 94146 SG-12 11/23/2022 12:40
11/23/2022 09:05Air 94147 SG-13 11/23/2022 12:40
Page 3 of 23
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-327-0028
Report Limit
Project:RMR.013
V 94145SG-DUP-112322
6.00 12/01/2022 16:08TO-15 Acetone µg/m3 0.202
J0.601 12/01/2022 16:08TO-15 Benzene µg/m3 0.073
JB1.65 12/01/2022 16:08TO-15 Carbon Disulfide µg/m3 0.060
4.12 12/01/2022 16:08TO-15 Carbon Tetrachloride µg/m3 0.155
9.30 12/01/2022 16:08TO-15 Chloroform µg/m3 0.086
6.78 12/01/2022 16:08TO-15 Cyclohexane µg/m3 0.161
3.23 12/01/2022 16:08TO-15 Dichlorodifluoromethane µg/m3 0.134
J1.19 12/01/2022 16:08TO-15 1,1-Dichloroethane µg/m3 0.101
10.5 12/01/2022 16:08TO-15 1,1-Dichloroethene µg/m3 0.107
5.85 12/01/2022 16:08TO-15 cis-1,2-Dichloroethene µg/m3 0.095
J1.95 12/01/2022 16:08TO-15 trans-1,2-Dichloroethene µg/m3 0.108
J0.690 12/01/2022 16:08TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
J0.758 12/01/2022 16:08TO-15 n-Hexane µg/m3 0.047
JB3.08 12/01/2022 16:08TO-15 Isopropyl Alchohol µg/m3 0.139
J0.702 12/01/2022 16:08TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
1.86 12/01/2022 16:08TO-15 Methylene Chloride µg/m3 0.489
1.56 12/01/2022 16:08TO-15 Propene µg/m3 0.242
9.57 12/01/2022 16:08TO-15 Tetrachloroethene µg/m3 0.181
J1.38 12/01/2022 16:08TO-15 Toluene µg/m3 0.090
J1.84 12/01/2022 16:08TO-15 1,1,1-Trichloroethane µg/m3 0.144
114 12/01/2022 16:08TO-15 Trichloroethene µg/m3 0.199
9.20 12/01/2022 16:08TO-15 Trichlorofluoromethane µg/m3 0.130
J0.944 12/01/2022 16:08TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.703 12/01/2022 16:08TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
J0.669 12/01/2022 16:08TO-15 Vinyl Acetate µg/m3 0.224
J1.38 12/01/2022 16:08TO-15 o-Xylene µg/m3 0.157
J3.07 12/01/2022 16:08TO-15 m,p-Xylene µg/m3 0.217
J4.45 12/01/2022 16:08TO-15 Xylene (Total)µg/m3 0.157
V 94146SG-12
5.43 12/01/2022 16:59TO-15 Acetone µg/m3 0.202
J0.610 12/01/2022 16:59TO-15 Benzene µg/m3 0.073
JB1.33 12/01/2022 16:59TO-15 Carbon Disulfide µg/m3 0.060
4.21 12/01/2022 16:59TO-15 Carbon Tetrachloride µg/m3 0.155
9.23 12/01/2022 16:59TO-15 Chloroform µg/m3 0.086
7.18 12/01/2022 16:59TO-15 Cyclohexane µg/m3 0.161
3.14 12/01/2022 16:59TO-15 Dichlorodifluoromethane µg/m3 0.134
Page 4 of 23
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-327-0028
Report Limit
Project:RMR.013
V 94146SG-12
J1.28 12/01/2022 16:59TO-15 1,1-Dichloroethane µg/m3 0.101
10.7 12/01/2022 16:59TO-15 1,1-Dichloroethene µg/m3 0.107
5.97 12/01/2022 16:59TO-15 cis-1,2-Dichloroethene µg/m3 0.095
2.10 12/01/2022 16:59TO-15 trans-1,2-Dichloroethene µg/m3 0.108
J0.697 12/01/2022 16:59TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
J0.892 12/01/2022 16:59TO-15 n-Hexane µg/m3 0.047
JB2.38 12/01/2022 16:59TO-15 Isopropyl Alchohol µg/m3 0.139
J0.784 12/01/2022 16:59TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.18 12/01/2022 16:59TO-15 Methylene Chloride µg/m3 0.489
10.7 12/01/2022 16:59TO-15 Tetrachloroethene µg/m3 0.181
J1.35 12/01/2022 16:59TO-15 Toluene µg/m3 0.090
J1.85 12/01/2022 16:59TO-15 1,1,1-Trichloroethane µg/m3 0.144
113 12/01/2022 16:59TO-15 Trichloroethene µg/m3 0.199
9.25 12/01/2022 16:59TO-15 Trichlorofluoromethane µg/m3 0.130
J0.590 12/01/2022 16:59TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.782 12/01/2022 16:59TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
J1.27 12/01/2022 16:59TO-15 o-Xylene µg/m3 0.157
J2.59 12/01/2022 16:59TO-15 m,p-Xylene µg/m3 0.217
J3.86 12/01/2022 16:59TO-15 Xylene (Total)µg/m3 0.157
V 94147SG-13
17.5 12/01/2022 17:49TO-15 Acetone µg/m3 0.202
3.26 12/01/2022 17:49TO-15 Benzene µg/m3 0.073
B8.69 12/01/2022 17:49TO-15 Carbon Disulfide µg/m3 0.060
2.34 12/01/2022 17:49TO-15 Chlorobenzene µg/m3 0.107
3.00 12/01/2022 17:49TO-15 Chloroform µg/m3 0.086
J0.167 12/01/2022 17:49TO-15 Chloromethane µg/m3 0.067
8.88 12/01/2022 17:49TO-15 Cyclohexane µg/m3 0.161
3.13 12/01/2022 17:49TO-15 Dichlorodifluoromethane µg/m3 0.134
8.61 12/01/2022 17:49TO-15 1,1-Dichloroethane µg/m3 0.101
1100 12/05/2022 11:53TO-15 1,1-Dichloroethene µg/m3 2.14
16.7 12/01/2022 17:49TO-15 cis-1,2-Dichloroethene µg/m3 0.095
2.68 12/01/2022 17:49TO-15 trans-1,2-Dichloroethene µg/m3 0.108
4.94 12/01/2022 17:49TO-15 Ethylbenzene µg/m3 0.106
J1.97 12/01/2022 17:49TO-15 4-Ethyltoluene µg/m3 0.128
J0.659 12/01/2022 17:49TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
5.55 12/01/2022 17:49TO-15 Heptane µg/m3 0.143
Page 5 of 23
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-327-0028
Report Limit
Project:RMR.013
V 94147SG-13
24.7 12/01/2022 17:49TO-15 n-Hexane µg/m3 0.047
JB2.19 12/01/2022 17:49TO-15 Isopropyl Alchohol µg/m3 0.139
2.82 12/01/2022 17:49TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
3.34 12/01/2022 17:49TO-15 Methylene Chloride µg/m3 0.489
323 12/05/2022 11:53TO-15 Propene µg/m3 4.84
J0.660 12/01/2022 17:49TO-15 Styrene µg/m3 0.124
J2.97 12/01/2022 17:49TO-15 Tetrachloroethene µg/m3 0.181
J1.19 12/01/2022 17:49TO-15 Tetrahydrofuran µg/m3 0.107
26.6 12/01/2022 17:49TO-15 Toluene µg/m3 0.090
9.80 12/01/2022 17:49TO-15 1,1,1-Trichloroethane µg/m3 0.144
500 12/05/2022 11:53TO-15 Trichloroethene µg/m3 3.98
7.80 12/01/2022 17:49TO-15 Trichlorofluoromethane µg/m3 0.130
7.35 12/01/2022 17:49TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
2.46 12/01/2022 17:49TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
3.78 12/01/2022 17:49TO-15 Vinyl Chloride µg/m3 0.127
6.25 12/01/2022 17:49TO-15 o-Xylene µg/m3 0.157
17.2 12/01/2022 17:49TO-15 m,p-Xylene µg/m3 0.217
23.5 12/01/2022 17:49TO-15 Xylene (Total)µg/m3 0.157
Page 6 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-DUP-112322
94145 Matrix:
11/23/2022 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
6.00 µg/m3 0.202 4.75Acetone 1 12/01/22 16:08 V27231ENM
0.601 J µg/m3 0.073 1.60Benzene 1 12/01/22 16:08 V27231ENM
<0.148 µg/m3 0.148 10.4Benzyl Chloride 1 12/01/22 16:08 V27231ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 12/01/22 16:08 V27231ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 12/01/22 16:08 V27231ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 12/01/22 16:08 V27231ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 12/01/22 16:08 V27231ENM
1.65 JB µg/m3 0.060 6.23Carbon Disulfide 1 12/01/22 16:08 V27231ENM
4.12 µg/m3 0.155 3.15
Carbon Tetrachloride 1 12/01/22 16:08 V27231ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 12/01/22 16:08 V27231ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 12/01/22 16:08 V27231ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 12/01/22 16:08 V27231ENM
9.30 µg/m3 0.086 2.44Chloroform 1 12/01/22 16:08 V27231ENM
<0.0673 µg/m3 0.067 1.03Chloromethane 1 12/01/22 16:08 V27231ENM
6.78 µg/m3 0.161 3.44Cyclohexane 1 12/01/22 16:08 V27231ENM
<0.151 µg/m3 0.151 3.84
1,2-Dibromoethane 1 12/01/22 16:08 V27231ENM
<0.0963 µg/m3 0.096 3.011,2-Dichlorobenzene 1 12/01/22 16:08 V27231ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 12/01/22 16:08 V27231ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 12/01/22 16:08 V27231ENM
3.23 µg/m3 0.134 2.47Dichlorodifluoromethane 1 12/01/22 16:08 V27231ENM
1.19 J µg/m3 0.101 2.021,1-Dichloroethane 1 12/01/22 16:08 V27231ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 12/01/22 16:08 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-DUP-112322
94145 Matrix:
11/23/2022 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
10.5 µg/m3 0.107 1.981,1-Dichloroethene 1 12/01/22 16:08 V27231ENM
5.85 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 12/01/22 16:08 V27231ENM
1.95 J µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 12/01/22 16:08 V27231ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 12/01/22 16:08 V27231ENM
<0.623 µg/m3 0.623 3.501,2-Dichlorotetrafluoroethane 1 12/01/22 16:08 V27231ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 12/01/22 16:08 V27231ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 12/01/22 16:08 V27231ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 12/01/22 16:08 V27231ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 12/01/22 16:08 V27231ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 12/01/22 16:08 V27231ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 12/01/22 16:08 V27231ENM
0.690 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 12/01/22 16:08 V27231ENM
<0.143 µg/m3 0.143 2.05Heptane 1 12/01/22 16:08 V27231ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 12/01/22 16:08 V27231ENM
0.758 J µg/m3 0.047 1.76n-Hexane 1 12/01/22 16:08 V27231ENM
<0.285 µg/m3 0.285 2.05
2-Hexanone 1 12/01/22 16:08 V27231ENM
3.08 JB µg/m3 0.139 4.92Isopropyl Alchohol 1 12/01/22 16:08 V27231ENM
0.702 J µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 12/01/22 16:08 V27231ENM
<0.0336 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 12/01/22 16:08 V27231ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 12/01/22 16:08 V27231ENM
1.86 µg/m3 0.489 1.74Methylene Chloride 1 12/01/22 16:08 V27231ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 12/01/22 16:08 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-DUP-112322
94145 Matrix:
11/23/2022 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
1.56 µg/m3 0.242 0.861Propene 1 12/01/22 16:08 V27231ENM
<0.124 µg/m3 0.124 2.13Styrene 1 12/01/22 16:08 V27231ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 12/01/22 16:08 V27231ENM
9.57 µg/m3 0.181 3.39Tetrachloroethene 1 12/01/22 16:08 V27231ENM
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 12/01/22 16:08 V27231ENM
1.38 J µg/m3 0.090 1.88Toluene 1 12/01/22 16:08 V27231ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 12/01/22 16:08 V27231ENM
1.84 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 12/01/22 16:08 V27231ENM
<0.0877 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 12/01/22 16:08 V27231ENM
114 µg/m3 0.199 2.15Trichloroethene 1 12/01/22 16:08 V27231ENM
9.20 µg/m3 0.130 2.81Trichlorofluoromethane 1 12/01/22 16:08 V27231ENM
0.944 J µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 12/01/22 16:08 V27231ENM
0.703 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 12/01/22 16:08 V27231ENM
0.669 J µg/m3 0.224 1.76Vinyl Acetate 1 12/01/22 16:08 V27231ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 12/01/22 16:08 V27231ENM
1.38 J
µg/m3 0.157 2.17
o-Xylene 1 12/01/22 16:08 V27231ENM
3.07 J µg/m3 0.217 5.65m,p-Xylene 1 12/01/22 16:08 V27231ENM
4.45 J µg/m3 0.157 2.17Xylene (Total)1 12/01/22 16:08 V27231
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%12/01/22 16:081 ENM V27231
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-12
94146 Matrix:
11/23/2022 8:39
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
5.43 µg/m3 0.202 4.75Acetone 1 12/01/22 16:59 V27231ENM
0.610 J µg/m3 0.073 1.60Benzene 1 12/01/22 16:59 V27231ENM
<0.148 µg/m3 0.148 10.4Benzyl Chloride 1 12/01/22 16:59 V27231ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 12/01/22 16:59 V27231ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 12/01/22 16:59 V27231ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 12/01/22 16:59 V27231ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 12/01/22 16:59 V27231ENM
1.33 JB µg/m3 0.060 6.23Carbon Disulfide 1 12/01/22 16:59 V27231ENM
4.21 µg/m3 0.155 3.15
Carbon Tetrachloride 1 12/01/22 16:59 V27231ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 12/01/22 16:59 V27231ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 12/01/22 16:59 V27231ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 12/01/22 16:59 V27231ENM
9.23 µg/m3 0.086 2.44Chloroform 1 12/01/22 16:59 V27231ENM
<0.0673 µg/m3 0.067 1.03Chloromethane 1 12/01/22 16:59 V27231ENM
7.18 µg/m3 0.161 3.44Cyclohexane 1 12/01/22 16:59 V27231ENM
<0.151 µg/m3 0.151 3.84
1,2-Dibromoethane 1 12/01/22 16:59 V27231ENM
<0.0963 µg/m3 0.096 3.011,2-Dichlorobenzene 1 12/01/22 16:59 V27231ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 12/01/22 16:59 V27231ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 12/01/22 16:59 V27231ENM
3.14 µg/m3 0.134 2.47Dichlorodifluoromethane 1 12/01/22 16:59 V27231ENM
1.28 J µg/m3 0.101 2.021,1-Dichloroethane 1 12/01/22 16:59 V27231ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 12/01/22 16:59 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-12
94146 Matrix:
11/23/2022 8:39
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
10.7 µg/m3 0.107 1.981,1-Dichloroethene 1 12/01/22 16:59 V27231ENM
5.97 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 12/01/22 16:59 V27231ENM
2.10 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 12/01/22 16:59 V27231ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 12/01/22 16:59 V27231ENM
<0.623 µg/m3 0.623 3.501,2-Dichlorotetrafluoroethane 1 12/01/22 16:59 V27231ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 12/01/22 16:59 V27231ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 12/01/22 16:59 V27231ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 12/01/22 16:59 V27231ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 12/01/22 16:59 V27231ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 12/01/22 16:59 V27231ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 12/01/22 16:59 V27231ENM
0.697 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 12/01/22 16:59 V27231ENM
<0.143 µg/m3 0.143 2.05Heptane 1 12/01/22 16:59 V27231ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 12/01/22 16:59 V27231ENM
0.892 J µg/m3 0.047 1.76n-Hexane 1 12/01/22 16:59 V27231ENM
<0.285 µg/m3 0.285 2.05
2-Hexanone 1 12/01/22 16:59 V27231ENM
2.38 JB µg/m3 0.139 4.92Isopropyl Alchohol 1 12/01/22 16:59 V27231ENM
0.784 J µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 12/01/22 16:59 V27231ENM
<0.0336 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 12/01/22 16:59 V27231ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 12/01/22 16:59 V27231ENM
1.18 J µg/m3 0.489 1.74Methylene Chloride 1 12/01/22 16:59 V27231ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 12/01/22 16:59 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-12
94146 Matrix:
11/23/2022 8:39
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00
<0.242 µg/m3 0.242 0.861Propene 1 12/01/22 16:59 V27231ENM
<0.124 µg/m3 0.124 2.13Styrene 1 12/01/22 16:59 V27231ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 12/01/22 16:59 V27231ENM
10.7 µg/m3 0.181 3.39Tetrachloroethene 1 12/01/22 16:59 V27231ENM
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 12/01/22 16:59 V27231ENM
1.35 J µg/m3 0.090 1.88Toluene 1 12/01/22 16:59 V27231ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 12/01/22 16:59 V27231ENM
1.85 J µg/m3 0.144 2.731,1,1-Trichloroethane 1 12/01/22 16:59 V27231ENM
<0.0877 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 12/01/22 16:59 V27231ENM
113 µg/m3 0.199 2.15Trichloroethene 1 12/01/22 16:59 V27231ENM
9.25 µg/m3 0.130 2.81Trichlorofluoromethane 1 12/01/22 16:59 V27231ENM
0.590 J µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 12/01/22 16:59 V27231ENM
0.782 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 12/01/22 16:59 V27231ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 12/01/22 16:59 V27231ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 12/01/22 16:59 V27231ENM
1.27 J
µg/m3 0.157 2.17
o-Xylene 1 12/01/22 16:59 V27231ENM
2.59 J µg/m3 0.217 5.65m,p-Xylene 1 12/01/22 16:59 V27231ENM
3.86 J µg/m3 0.157 2.17Xylene (Total)1 12/01/22 16:59 V27231
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%12/01/22 16:591 ENM V27231
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-13
94147 Matrix:
11/23/2022 9:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00 V27254 12/05/22 09:00
17.5 µg/m3 0.202 4.75Acetone 1 12/01/22 17:49 V27231ENM
3.26 µg/m3 0.073 1.60Benzene 1 12/01/22 17:49 V27231ENM
<0.148 µg/m3 0.148 10.4Benzyl Chloride 1 12/01/22 17:49 V27231ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 12/01/22 17:49 V27231ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 12/01/22 17:49 V27231ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 12/01/22 17:49 V27231ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 12/01/22 17:49 V27231ENM
8.69 B µg/m3 0.060 6.23Carbon Disulfide 1 12/01/22 17:49 V27231ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 12/01/22 17:49 V27231ENM
2.34 µg/m3 0.107 2.30Chlorobenzene 1 12/01/22 17:49 V27231ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 12/01/22 17:49 V27231ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 12/01/22 17:49 V27231ENM
3.00 µg/m3 0.086 2.44Chloroform 1 12/01/22 17:49 V27231ENM
0.167 J µg/m3 0.067 1.03Chloromethane 1 12/01/22 17:49 V27231ENM
8.88 µg/m3 0.161 3.44Cyclohexane 1 12/01/22 17:49 V27231ENM
<0.151 µg/m3 0.151 3.84
1,2-Dibromoethane 1 12/01/22 17:49 V27231ENM
<0.0963 µg/m3 0.096 3.011,2-Dichlorobenzene 1 12/01/22 17:49 V27231ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 12/01/22 17:49 V27231ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 12/01/22 17:49 V27231ENM
3.13 µg/m3 0.134 2.47Dichlorodifluoromethane 1 12/01/22 17:49 V27231ENM
8.61 µg/m3 0.101 2.021,1-Dichloroethane 1 12/01/22 17:49 V27231ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 12/01/22 17:49 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-13
94147 Matrix:
11/23/2022 9:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00 V27254 12/05/22 09:00
1100 µg/m3 2.14 39.61,1-Dichloroethene 20 12/05/22 11:53 V27256ENM
16.7 µg/m3 0.095 1.98cis-1,2-Dichloroethene 1 12/01/22 17:49 V27231ENM
2.68 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 12/01/22 17:49 V27231ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 12/01/22 17:49 V27231ENM
<0.623 µg/m3 0.623 3.501,2-Dichlorotetrafluoroethane 1 12/01/22 17:49 V27231ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 12/01/22 17:49 V27231ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 12/01/22 17:49 V27231ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 12/01/22 17:49 V27231ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 12/01/22 17:49 V27231ENM
4.94 µg/m3 0.106 2.17Ethylbenzene 1 12/01/22 17:49 V27231ENM
1.97 J µg/m3 0.128 2.464-Ethyltoluene 1 12/01/22 17:49 V27231ENM
0.659 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 12/01/22 17:49 V27231ENM
5.55 µg/m3 0.143 2.05Heptane 1 12/01/22 17:49 V27231ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 12/01/22 17:49 V27231ENM
24.7 µg/m3 0.047 1.76n-Hexane 1 12/01/22 17:49 V27231ENM
<0.285 µg/m3 0.285 2.05
2-Hexanone 1 12/01/22 17:49 V27231ENM
2.19 JB µg/m3 0.139 4.92Isopropyl Alchohol 1 12/01/22 17:49 V27231ENM
2.82 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 12/01/22 17:49 V27231ENM
<0.0336 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 12/01/22 17:49 V27231ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 12/01/22 17:49 V27231ENM
3.34 µg/m3 0.489 1.74Methylene Chloride 1 12/01/22 17:49 V27231ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 12/01/22 17:49 V27231ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 23
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-327-0028
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Alexis McKenzie
Charlotte
Received : 11/23/2022
RMR.013
Report Date : 12/05/2022
Sample ID :
Lab No :
Sampled:SG-13
94147 Matrix:
11/23/2022 9:05
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V27226 12/01/22 09:00 V27254 12/05/22 09:00
323 µg/m3 4.84 17.2Propene 20 12/05/22 11:53 V27256ENM
0.660 J µg/m3 0.124 2.13Styrene 1 12/01/22 17:49 V27231ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 12/01/22 17:49 V27231ENM
2.97 J µg/m3 0.181 3.39Tetrachloroethene 1 12/01/22 17:49 V27231ENM
1.19 J µg/m3 0.107 1.47Tetrahydrofuran 1 12/01/22 17:49 V27231ENM
26.6 µg/m3 0.090 1.88Toluene 1 12/01/22 17:49 V27231ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 12/01/22 17:49 V27231ENM
9.80 µg/m3 0.144 2.731,1,1-Trichloroethane 1 12/01/22 17:49 V27231ENM
<0.0877 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 12/01/22 17:49 V27231ENM
500 µg/m3 3.98 43.0Trichloroethene 20 12/05/22 11:53 V27256ENM
7.80 µg/m3 0.130 2.81Trichlorofluoromethane 1 12/01/22 17:49 V27231ENM
7.35 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 12/01/22 17:49 V27231ENM
2.46 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 12/01/22 17:49 V27231ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 12/01/22 17:49 V27231ENM
3.78 µg/m3 0.127 1.28Vinyl Chloride 1 12/01/22 17:49 V27231ENM
6.25 µg/m3 0.157 2.17
o-Xylene 1 12/01/22 17:49 V27231ENM
17.2 µg/m3 0.217 5.65m,p-Xylene 1 12/01/22 17:49 V27231ENM
23.5 µg/m3 0.157 2.17Xylene (Total)1 12/01/22 17:49 V27231
Surrogate: 4-Bromofluorobenzene 108 Limits: 70-130%12/01/22 17:491 ENM V27231
Surrogate: 4-Bromofluorobenzene 92.2 Limits: 70-130%12/05/22 11:5320 ENM V27256
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27226
Associated Lab Samples: 94145, 94146, 94147
LRB-V27226 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 11:064.750.2020.290µg/m3Acetone
12/01/22 11:061.600.0733<0.0733µg/m3Benzene
12/01/22 11:0610.40.148<0.148µg/m3Benzyl Chloride
12/01/22 11:063.350.150<0.150µg/m3Bromodichloromethane
12/01/22 11:065.170.153<0.153µg/m3Bromoform
12/01/22 11:061.940.115<0.115µg/m3Bromomethane
12/01/22 11:061.110.328<0.328µg/m31,3-Butadiene
12/01/22 11:066.230.06081.10µg/m3Carbon Disulfide
12/01/22 11:063.150.155<0.155µg/m3Carbon Tetrachloride
12/01/22 11:062.300.107<0.107µg/m3Chlorobenzene
12/01/22 11:064.260.208<0.208µg/m3Chlorodibromomethane
12/01/22 11:061.320.164<0.164µg/m3Chloroethane
12/01/22 11:062.440.0864<0.0864µg/m3Chloroform
12/01/22 11:061.030.0673<0.0673µg/m3Chloromethane
12/01/22 11:063.440.161<0.161µg/m3Cyclohexane
12/01/22 11:063.840.151<0.151µg/m31,2-Dibromoethane
12/01/22 11:063.010.0963<0.0963µg/m31,2-Dichlorobenzene
12/01/22 11:0612.00.174<0.174µg/m31,3-Dichlorobenzene
12/01/22 11:063.010.186<0.186µg/m31,4-Dichlorobenzene
12/01/22 11:062.470.134<0.134µg/m3Dichlorodifluoromethane
12/01/22 11:062.020.101<0.101µg/m31,1-Dichloroethane
12/01/22 11:062.020.129<0.129µg/m31,2-Dichloroethane
12/01/22 11:061.980.107<0.107µg/m31,1-Dichloroethene
12/01/22 11:061.980.0955<0.0955µg/m3cis-1,2-Dichloroethene
12/01/22 11:061.980.108<0.108µg/m3trans-1,2-Dichloroethene
12/01/22 11:062.310.205<0.205µg/m31,2-Dichloropropane
12/01/22 11:063.500.623<0.623µg/m31,2-Dichlorotetrafluoroethane
Page 1 of 6Date:12/05/2022 03:13 PM
Page 16 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27226
Associated Lab Samples: 94145, 94146, 94147
LRB-V27226 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 11:062.270.178<0.178µg/m3cis-1,3-Dichloropropene
12/01/22 11:062.270.178<0.178µg/m3trans-1,3-Dichloropropene
12/01/22 11:061.800.435<0.435µg/m31,4-Dioxane
12/01/22 11:061.800.136<0.136µg/m3Ethyl Acetate
12/01/22 11:062.170.106<0.106µg/m3Ethylbenzene
12/01/22 11:062.460.128<0.128µg/m34-Ethyltoluene
12/01/22 11:063.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
12/01/22 11:062.050.143<0.143µg/m3Heptane
12/01/22 11:065.330.330<0.330µg/m3Hexachlorobutadiene
12/01/22 11:061.760.0472<0.0472µg/m3n-Hexane
12/01/22 11:062.050.285<0.285µg/m32-Hexanone
12/01/22 11:064.920.1391.29µg/m3Isopropyl Alchohol
12/01/22 11:061.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
12/01/22 11:061.800.0336<0.0336µg/m3Methyl tert-butyl ether (MTBE)
12/01/22 11:062.050.121<0.121µg/m34-Methyl-2-Pentanone
12/01/22 11:061.740.489<0.489µg/m3Methylene Chloride
12/01/22 11:062.620.183<0.183µg/m3Naphthalene
12/01/22 11:060.8610.242<0.242µg/m3Propene
12/01/22 11:062.130.124<0.124µg/m3Styrene
12/01/22 11:063.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
12/01/22 11:063.390.181<0.181µg/m3Tetrachloroethene
12/01/22 11:061.470.107<0.107µg/m3Tetrahydrofuran
12/01/22 11:061.880.0901<0.0901µg/m3Toluene
12/01/22 11:063.710.209<0.209µg/m31,2,4-Trichlorobenzene
12/01/22 11:062.730.144<0.144µg/m31,1,1-Trichloroethane
12/01/22 11:062.730.0877<0.0877µg/m31,1,2-Trichloroethane
12/01/22 11:062.150.199<0.199µg/m3Trichloroethene
Page 2 of 6Date:12/05/2022 03:13 PM
Page 17 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27226
Associated Lab Samples: 94145, 94146, 94147
LRB-V27226 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 11:062.810.130<0.130µg/m3Trichlorofluoromethane
12/01/22 11:062.460.110<0.110µg/m31,2,4-Trimethylbenzene
12/01/22 11:062.460.236<0.236µg/m31,3,5-Trimethylbenzene
12/01/22 11:061.760.224<0.224µg/m3Vinyl Acetate
12/01/22 11:061.280.127<0.127µg/m3Vinyl Chloride
12/01/22 11:062.170.157<0.157µg/m3o-Xylene
12/01/22 11:065.650.217<0.217µg/m3m,p-Xylene
12/01/22 11:064-Bromofluorobenzene (S)103 70-130
LCS-V27226Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
73.88.7911.9µg/m3Acetone 70-130
94.315.116.0µg/m3Benzene 70-130
10727.825.9µg/m3Benzyl Chloride 70-130
88.929.833.5µg/m3Bromodichloromethane 70-130
95.349.351.7µg/m3Bromoform 70-130
95.818.619.4µg/m3Bromomethane 70-130
90.910.111.1µg/m31,3-Butadiene 70-130
98.015.315.6µg/m3Carbon Disulfide 70-130
89.228.131.5µg/m3Carbon Tetrachloride 70-130
10023.123.0µg/m3Chlorobenzene 70-130
98.141.842.6µg/m3Chlorodibromomethane 70-130
94.612.513.2µg/m3Chloroethane 70-130
92.622.624.4µg/m3Chloroform 70-130
94.29.7110.3µg/m3Chloromethane 70-130
91.215.717.2µg/m3Cyclohexane 70-130
Page 3 of 6Date:12/05/2022 03:13 PM
Page 18 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27226
LCS-V27226Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.637.938.4µg/m31,2-Dibromoethane 70-130
10932.730.1µg/m31,2-Dichlorobenzene 70-130
10230.730.1µg/m31,3-Dichlorobenzene 70-130
10431.330.1µg/m31,4-Dichlorobenzene 70-130
86.621.424.7µg/m3Dichlorodifluoromethane 70-130
95.519.320.2µg/m31,1-Dichloroethane 70-130
87.117.620.2µg/m31,2-Dichloroethane 70-130
92.418.319.8µg/m31,1-Dichloroethene 70-130
94.418.719.8µg/m3cis-1,2-Dichloroethene 70-130
93.918.619.8µg/m3trans-1,2-Dichloroethene 70-130
93.921.723.1µg/m31,2-Dichloropropane 70-130
92.532.435.0µg/m31,2-Dichlorotetrafluoroethane 70-130
92.921.122.7µg/m3cis-1,3-Dichloropropene 70-130
92.921.122.7µg/m3trans-1,3-Dichloropropene 70-130
94.417.018.0µg/m31,4-Dioxane 70-130
90.016.218.0µg/m3Ethyl Acetate 70-130
10021.821.7µg/m3Ethylbenzene 70-130
10124.924.6µg/m34-Ethyltoluene 70-130
97.137.238.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
92.619.020.5µg/m3Heptane 70-130
99.252.953.3µg/m3Hexachlorobutadiene 70-130
90.916.017.6µg/m3n-Hexane 70-130
94.119.320.5µg/m32-Hexanone 70-130
88.610.912.3µg/m3Isopropyl Alchohol 70-130
85.812.714.8µg/m3Methyl Ethyl Ketone (MEK)70-130
91.616.518.0µg/m3Methyl tert-butyl ether (MTBE)70-130
89.718.420.5µg/m34-Methyl-2-Pentanone 70-130
Page 4 of 6Date:12/05/2022 03:13 PM
Page 19 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27226
LCS-V27226Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.014.817.4µg/m3Methylene Chloride 70-130
99.626.126.2µg/m3Naphthalene 70-130
85.97.408.61µg/m3Propene 70-130
99.021.121.3µg/m3Styrene 70-130
10335.434.3µg/m31,1,2,2-Tetrachloroethane 70-130
92.631.433.9µg/m3Tetrachloroethene 70-130
89.713.214.7µg/m3Tetrahydrofuran 70-130
95.217.918.8µg/m3Toluene 70-130
94.335.037.1µg/m31,2,4-Trichlorobenzene 70-130
88.624.227.3µg/m31,1,1-Trichloroethane 70-130
10027.427.3µg/m31,1,2-Trichloroethane 70-130
91.424.626.9µg/m3Trichloroethene 70-130
90.025.328.1µg/m3Trichlorofluoromethane 70-130
10525.924.6µg/m31,2,4-Trimethylbenzene 70-130
10325.424.6µg/m31,3,5-Trimethylbenzene 70-130
99.417.517.6µg/m3Vinyl Acetate 70-130
94.512.112.8µg/m3Vinyl Chloride 70-130
10122.021.7µg/m3o-Xylene 70-130
92.840.343.4µg/m3m,p-Xylene 70-130
1064-Bromofluorobenzene (S)70-130
Page 5 of 6Date:12/05/2022 03:13 PM
Page 20 of 23
Quality Control Data
22-327-0028Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
RMR.013
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V27256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V27254
Associated Lab Samples: 94147
LRB-V27254 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/05/22 11:111.980.107<0.107µg/m31,1-Dichloroethene
12/05/22 11:110.8600.242<0.242µg/m3Propene
12/05/22 11:112.150.199<0.199µg/m3Trichloroethene
12/05/22 11:114-Bromofluorobenzene (S)94.6 70-130
LCS-V27254Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10120.019.8µg/m31,1-Dichloroethene 70-130
94.08.108.61µg/m3Propene 70-130
89.524.126.9µg/m3Trichloroethene 70-130
1004-Bromofluorobenzene (S)70-130
Page 6 of 6Date:12/05/2022 03:13 PM
Page 21 of 23
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-327-0028
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:N/A
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/23/2022 14:54:43
Special precautions or instructions included?
Comments:
Page 22 of 23
Page 23 of 23

Appendix D DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Worst-Case Post Excavation
North Carolina Department of Environmental Quality
Risk Calculator
National Welders Supply
Gesco Street & State Street
Brownfields Redevelopment Section
25035-21-060
January 2023
November 2022 EPA RSL Table
4/13/2023
Prepared By:H&H
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.025 67-64-1 Acetone mg/kg
0.002 71-43-2 Benzene mg/kg
0.001 75-15-0 Carbon Disulfide mg/kg
0.001 67-66-3 Chloroform mg/kg
0.005 75-34-3 Dichloroethane, 1,1-mg/kg
0.021 75-35-4 Dichloroethylene, 1,1-mg/kg
0.043 156-59-2 Dichloroethylene, cis-1,2-mg/kg
0.008 637-92-3 Ethyl Tertiary Butyl Ether (ETBE)mg/kg
0.002 1634-04-4 Methyl tert-Butyl Ether (MTBE)mg/kg
0.007 75-09-2 Methylene Chloride mg/kg
0.003 108-88-3 Toluene mg/kg
0.002 71-55-6 Trichloroethane, 1,1,1-mg/kg
0.019 79-01-6 Trichloroethylene mg/kg
0.0006 95-63-6 Trimethylbenzene, 1,2,4-mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/m3)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC Flag
(Y/N)
Rationale for
Selection or
Deletion
17.5 67-64-1 Acetone ug/m3
3.26 71-43-2 Benzene ug/m3
8.96 75-15-0 Carbon Disulfide ug/m3
4.21 56-23-5 Carbon Tetrachloride ug/m3
2.34 108-90-7 Chlorobenzene ug/m3
9.3 67-66-3 Chloroform ug/m3
0.167 74-87-3 Chloromethane ug/m3
8.88 110-82-7 Cyclohexane ug/m3
3.23 75-71-8 Dichlorodifluoromethane ug/m3
8.61 75-34-3 Dichloroethane, 1,1-ug/m3
1100 75-35-4 Dichloroethylene, 1,1-ug/m3
16.7 156-59-2 Dichloroethylene, cis-1,2-ug/m3
2.68 156-60-5 Dichloroethylene, trans-1,2-ug/m3
4.94 100-41-4 Ethylbenzene ug/m3
1.19 109-99-9 ~Tetrahydrofuran ug/m3
5.55 142-82-5 Heptane, N-ug/m3
24.7 110-54-3 Hexane, N-ug/m3
3.08 67-63-0 Isopropanol ug/m3
2.82 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
3.34 75-09-2 Methylene Chloride ug/m3
323 115-07-1 Propylene ug/m3
0.66 100-42-5 Styrene ug/m3
10.7 127-18-4 Tetrachloroethylene ug/m3
26.6 108-88-3 Toluene ug/m3
0.697 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3
9.8 71-55-6 Trichloroethane, 1,1,1-ug/m3
500 79-01-6 Trichloroethylene ug/m3
9.25 75-69-4 Trichlorofluoromethane ug/m3
7.35 95-63-6 Trimethylbenzene, 1,2,4-ug/m3
2.46 108-67-8 Trimethylbenzene, 1,3,5-ug/m3
0.669 108-05-4 Vinyl Acetate ug/m3
3.78 75-01-4 Vinyl Chloride ug/m3
17.2 108-38-3 Xylene, m-ug/m3
6.25 95-47-6 Xylene, o-ug/m3
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 2.0E-08 4.1E-03 NO
Groundwater Use*NC NC NC
Soil 3.5E-09 8.4E-04 NO
Groundwater Use*NC NC NC
Construction Worker Soil 8.1E-10 9.3E-03 NO
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.5E-05 7.4E+00 YES
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentratio
n (mg/kg)
Dermal
Concentratio
n (mg/kg)
Inhalation
Concentratio
n (mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.025 0.025 0.025 3.6E-07 3.6E-07
71-43-2 Benzene 0.002 0.002 0.002 1.6E-10 1.5E-09 1.6E-09 6.4E-06 1.7E-05 2.3E-05
75-15-0 Carbon Disulfide 0.001 0.001 0.001 1.3E-07 4.4E-07 5.6E-07
67-66-3 Chloroform 0.001 0.001 0.001 4.5E-11 2.6E-09 2.7E-09 1.3E-06 3.1E-06 4.4E-06
75-34-3 Dichloroethane, 1,1-0.005 0.005 0.005 4.1E-11 9.1E-10 9.5E-10 3.2E-07 3.2E-07
75-35-4 Dichloroethylene, 1,1-0.021 0.021 0.021 5.4E-06 3.2E-05 3.7E-05
156-59-2 Dichloroethylene, cis-1,2-0.043 0.043 0.043 2.7E-04 3.3E-04 6.0E-04
637-92-3 Ethyl Tertiary Butyl Ether (ETBE)0.008 0.008 0.008 5.8E-11 5.8E-11 1.0E-07 4.9E-08 1.5E-07
1634-04-4 Methyl tert-Butyl Ether (MTBE)0.002 0.002 0.002 5.2E-12 3.5E-11 4.1E-11 1.2E-07 1.2E-07
75-09-2 Methylene Chloride 0.007 0.007 0.007 9.1E-11 2.2E-11 1.1E-10 1.5E-05 3.6E-06 1.8E-05
108-88-3 Toluene 0.003 0.003 0.003 4.8E-07 1.3E-07 6.1E-07
71-55-6 Trichloroethane, 1,1,1-0.002 0.002 0.002 1.3E-08 1.2E-07 1.3E-07
79-01-6 Trichloroethylene 0.019 0.019 0.019 2.2E-09 1.3E-08 1.5E-08 4.9E-04 2.9E-03 3.4E-03
95-63-6 Trimethylbenzene, 1,2,4-0.0006 0.0006 0.0006 7.7E-07 1.1E-06 1.9E-06
Cumulative:2.0E-08 4.1E-03
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening
level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentratio
n (mg/kg)
Dermal
Concentratio
n (mg/kg)
Inhalation
Concentratio
n (mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.025 0.025 0.025 2.4E-08 2.4E-08
71-43-2 Benzene 0.002 0.002 0.002 3.4E-11 3.4E-10 3.7E-10 4.3E-07 4.0E-06 4.5E-06
75-15-0 Carbon Disulfide 0.001 0.001 0.001 8.6E-09 1.0E-07 1.1E-07
67-66-3 Chloroform 0.001 0.001 0.001 9.5E-12 6.0E-10 6.1E-10 8.6E-08 7.4E-07 8.3E-07
75-34-3 Dichloroethane, 1,1-0.005 0.005 0.005 8.7E-12 2.1E-10 2.2E-10 2.1E-08 2.1E-08
75-35-4 Dichloroethylene, 1,1-0.021 0.021 0.021 3.6E-07 7.6E-06 8.0E-06
156-59-2 Dichloroethylene, cis-1,2-0.043 0.043 0.043 1.8E-05 7.8E-05 9.7E-05
637-92-3 Ethyl Tertiary Butyl Ether (ETBE)0.008 0.008 0.008 1.3E-11 1.3E-11 6.8E-09 1.2E-08 1.9E-08
1634-04-4 Methyl tert-Butyl Ether (MTBE)0.002 0.002 0.002 1.1E-12 8.1E-12 9.2E-12 2.9E-08 2.9E-08
75-09-2 Methylene Chloride 0.007 0.007 0.007 4.3E-12 1.8E-12 6.1E-12 1.0E-06 8.5E-07 1.8E-06
108-88-3 Toluene 0.003 0.003 0.003 3.2E-08 3.0E-08 6.2E-08
71-55-6 Trichloroethane, 1,1,1-0.002 0.002 0.002 8.6E-10 2.9E-08 3.0E-08
79-01-6 Trichloroethylene 0.019 0.019 0.019 2.7E-10 2.0E-09 2.3E-09 3.3E-05 6.9E-04 7.2E-04
95-63-6 Trimethylbenzene, 1,2,4-0.0006 0.0006 0.0006 5.1E-08 2.7E-07 3.2E-07
Cumulative:3.5E-09 8.4E-04
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of
800 mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentratio
n (mg/kg)
Dermal
Concentratio
n (mg/kg)
Inhalation
Concentratio
n (mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.025 0.025 0.025 1.2E-07 1.2E-07
71-43-2 Benzene 0.002 0.002 0.002 4.4E-12 6.4E-11 6.9E-11 5.9E-07 7.5E-06 8.1E-06
75-15-0 Carbon Disulfide 0.001 0.001 0.001 2.9E-08 1.3E-06 1.3E-06
67-66-3 Chloroform 0.001 0.001 0.001 1.3E-12 1.3E-10 1.3E-10 2.9E-08 1.7E-06 1.7E-06
75-34-3 Dichloroethane, 1,1-0.005 0.005 0.005 1.2E-12 5.6E-11 5.7E-11 7.4E-09 7.4E-09
75-35-4 Dichloroethylene, 1,1-0.021 0.021 0.021 6.9E-06 4.9E-03 4.9E-03
156-59-2 Dichloroethylene, cis-1,2-0.043 0.043 0.043 6.3E-06 4.6E-05 5.2E-05
637-92-3 Ethyl Tertiary Butyl Ether (ETBE)0.008 0.008 0.008 2.5E-12 2.5E-12 2.4E-08 5.8E-08 8.1E-08
1634-04-4 Methyl tert-Butyl Ether (MTBE)0.002 0.002 0.002 1.5E-13 1.5E-12 1.7E-12 1.4E-07 1.4E-07
75-09-2 Methylene Chloride 0.007 0.007 0.007 5.7E-13 4.6E-13 1.0E-12 3.4E-07 3.3E-06 3.6E-06
108-88-3 Toluene 0.003 0.003 0.003 1.1E-08 1.5E-07 1.6E-07
71-55-6 Trichloroethane, 1,1,1-0.002 0.002 0.002 8.4E-10 2.6E-07 2.6E-07
79-01-6 Trichloroethylene 0.019 0.019 0.019 3.5E-11 5.1E-10 5.5E-10 1.1E-04 4.2E-03 4.4E-03
95-63-6 Trimethylbenzene, 1,2,4-0.0006 0.0006 0.0006 4.4E-08 4.0E-07 4.5E-07
Cumulative:8.1E-10 9.3E-03
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 25035-21-060
Exposure Unit ID: Worst-Case Post Excavation
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 17.5 0.525 --
71-43-2 Benzene 3.26 0.0978 3.6E-01 6.3E+00 2.7E-07 3.1E-03
75-15-0 Carbon Disulfide 8.96 0.2688 -1.5E+02 3.7E-04
56-23-5 Carbon Tetrachloride 4.21 0.1263 4.7E-01 2.1E+01 2.7E-07 1.2E-03
108-90-7 Chlorobenzene 2.34 0.0702 -1.0E+01 1.3E-03
67-66-3 Chloroform 9.3 0.279 1.2E-01 2.0E+01 2.3E-06 2.7E-03
74-87-3 Chloromethane 0.167 0.00501 -1.9E+01 5.3E-05
110-82-7 Cyclohexane 8.88 0.2664 -1.3E+03 4.3E-05
75-71-8 Dichlorodifluoromethane 3.23 0.0969 -2.1E+01 9.3E-04
75-34-3 Dichloroethane, 1,1-8.61 0.2583 1.8E+00 -1.5E-07
75-35-4 Dichloroethylene, 1,1-1100 33 -4.2E+01 1.6E-01
156-59-2 Dichloroethylene, cis-1,2-16.7 0.501 -8.3E+00 1.2E-02
156-60-5 Dichloroethylene, trans-1,2-2.68 0.0804 -8.3E+00 1.9E-03
100-41-4 Ethylbenzene 4.94 0.1482 1.1E+00 2.1E+02 1.3E-07 1.4E-04
109-99-9 ~Tetrahydrofuran 1.19 0.0357 -4.2E+02 1.7E-05
142-82-5 Heptane, N-5.55 0.1665 -8.3E+01 4.0E-04
110-54-3 Hexane, N-24.7 0.741 -1.5E+02 1.0E-03
67-63-0 Isopropanol 3.08 0.0924 -4.2E+01 4.4E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.82 0.0846 -1.0E+03 1.6E-05
75-09-2 Methylene Chloride 3.34 0.1002 1.0E+02 1.3E+02 9.9E-10 1.6E-04
115-07-1 Propylene 323 9.69 -6.3E+02 3.1E-03
100-42-5 Styrene 0.66 0.0198 -2.1E+02 1.9E-05
127-18-4 Tetrachloroethylene 10.7 0.321 1.1E+01 8.3E+00 3.0E-08 7.7E-03
108-88-3 Toluene 26.6 0.798 -1.0E+03 1.5E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.697 0.02091 -1.0E+03 4.0E-06
71-55-6 Trichloroethane, 1,1,1-9.8 0.294 -1.0E+03 5.6E-05
79-01-6 Trichloroethylene 500 15 4.8E-01 4.2E-01 3.1E-05 7.2E+00
75-69-4 Trichlorofluoromethane 9.25 0.2775 --
95-63-6 Trimethylbenzene, 1,2,4-7.35 0.2205 -1.3E+01 3.5E-03
108-67-8 Trimethylbenzene, 1,3,5-2.46 0.0738 -1.3E+01 1.2E-03
108-05-4 Vinyl Acetate 0.669 0.02007 -4.2E+01 9.6E-05
75-01-4 Vinyl Chloride 3.78 0.1134 1.7E-01 1.7E+01 6.8E-07 1.4E-03
108-38-3 Xylene, m-17.2 0.516 -2.1E+01 4.9E-03
95-47-6 Xylene, o-6.25 0.1875 -2.1E+01 1.8E-03
Cumulative:3.5E-05 7.4E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator

Appendix E Boring Logs
NOTES: Hole precleared by H&H using hand auger. Hand Auger all 6' bgs. Install SG-12 at 6' bgs. Sand 6" above top of screen.
generated using GroundLogs.online
Client:
Project:
Address:
RMR
RMR-013
Gesco Street & State Street,Charlotte, NC
BORING LOG
Boring No.
Page:
SG-12
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/22/22
11/22/22
H&H
Other
CMB
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') SILT (ML); few medium sand, some clay, medium stiff, moist, red-brown w/ some
green brown
(2.5') SILT (ML); few medium sand, some clay, medium stiff, moist, red-brown
(6') Boring terminated
0.8
1.2
1.5
0.9
0.7
0.5
0
5
10
Hand Auger
CMB
NOTES: Hole precleared by H&H using hand auger. Hand Auger all 6' bgs. Install SG-13 at 6' bgs. Sand 6" above top of screen.
generated using GroundLogs.online
Client:
Project:
Address:
RMR
RMR-013
Gesco Street & State Street,Charlotte, NC
BORING LOG
Boring No.
Page:
SG-13
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/22/22
11/22/22
H&H
Other
CMB
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') SILT (ML); few medium sand, some clay, medium stiff, moist, red-brown w/ some
green brown
(2.5') SILT (ML); few medium sand, some clay, medium stiff, moist, red-brown
(6') Boring terminated
0.8
1.2
1.5
0.9
0.7
0.5
0
5
10
Hand Auger
CMB

Appendix F Field Forms
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