27027_Ables Auto_Limited Phase I ESA_20220606

Limited Groundwater Sampling SUMMIT Project No. 9408.E0001
2501 Wilkinson Blvd, Charlotte, North Carolina June 6, 2022
SUMMIT Engineering, Laboratory & Testing, Inc. (SUMMIT)
3575 Centre Circle
Fort Mill, South Carolina 29715
Phone: [phone]
Fax: [phone]
www.summit-companies.com
June 6, 2022
Scott C. Bortz
Sbbh, llc.
101 S. Kings Drive, Suite 200
Charlotte, NC 28204
Subject:Limited Phase I Environmental Site Assessment
Mecklenburg County Parcel: 11701109
2501 Wilkinson Blvd, Charlotte, North Carolina
SUMMIT Project No. 9408.E0001
SUMMIT ENGINEERING,LABORATORY &TESTING,INC.(SUMMIT) is pleased to submit the
following report of our Limited Groundwater Sampling of the property at 2501 Wilkinson Blvd,
Charlotte, Mecklenburg County, North Carolina.
The following environmental concerns have been identified during the due diligence process and
will be addressed with this Limited Phase II ESA:
The subject property was used as an automobile repair facility since the 1940’s until
approximately 2012.
SUMMIT collected three (3) groundwater samples from temporary monitoring wells. The
temporary monitoring wells were installed on June 2, 2022. The samples were analyzed for the
following constituents: EPA Method 8260 (Volatile Organics) and EPA Method 8270 (Semi-Volatile
Organics). Groundwater could not be obtained from TMW-3 due to refusal on rock.
Standard decontamination performed by field personnel on coring and sampling equipment in the
field included rinsing and scrubbing using water and soap, organic/analyte free water and solvent.
Decontamination was conducted prior to sampling operations at each location and upon completion
of the project. All environmental samples were packed, placed in coolers and shipped to North
Carolina approved laboratory for the above-mentioned parameters. Chain-of-Custody records were
maintained and presented as attachments. The location of the samples collected are presented in
Figure 4.
A review of the analysis indicates groundwater contamination. TMW-1 had concentrations of
9.6 ug/L for cis-1,2-Dichloroethene and 35.8 ug/L of Trichloroethene (TCE). TMW-2 had
concentrations of 2.0 ug/L for 1,1-Dichlorethane and 5.3 ug/L of 1,1-Dichlorethene.The
NCDEQ regulatory limit for TCE in groundwater is 3.0 ug/L.
If you have any questions, please do not hesitate to call us at [phone].
Sincerely,
SUMMIT
Limited Groundwater Sampling SUMMIT Project No. 9408.E0001
2501 Wilkinson Blvd, Charlotte, North Carolina June 6, 2022
Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE
Environmental Department Manager
Attachments:Figures and Analytical Results
D:\!Michael!\!SUMMIT!\9408 - sbbh, llc\9408.E0001 - 2501 Wilkinson Blvd\Phase II ESA\Report Files\Ph I - Figure 1 - Topo.doc
SUMMIT ELT, Inc.
Project: 9408.E0001
Figure 1
USGS Topographic Map
2501 Wilkinson Blvd
Charlotte, NC
Subject Property N
D:\!Michael!\!SUMMIT!\9408 - sbbh, llc\9408.E0001 - 2501 Wilkinson Blvd\Phase II ESA\Report Files\Ph I - Figure 2 - Aerial Map.doc
SUMMIT ELT, Inc.
Project: 9408.E0001
Figure 2
Sampling Map
2501 Wilkinson Blvd
Charlotte, NC
N
TMW-1
TMW-2
TMW-3
#=CL#
June 06, 2022
LIMS USE: FR - BRYAN LUCAS
LIMS OBJECT ID: 92607644
92607644
Project:
Pace Project No.:
RE:
BRYAN M. LUCAS
Summit Engineering
2520 WHitehall Park Dr
#250
Charlotte, NC 28273
2501 WILKINSON BLVD
Dear BRYAN LUCAS:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 26
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 26
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92607644001 TMW-1 EPA 8270E 74 PASI-CPKS
EPA 8260D 62 PASI-CSAS
92607644002 TMW-2 EPA 8270E 74 PASI-CPKS
EPA 8260D 62 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-1 Lab ID:92607644001 Collected:06/02/22 14:00 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/03/22 13:59 83-32-906/03/22 05:1310.0 1
Acenaphthylene ND ug/L 06/03/22 13:59 208-96-806/03/22 05:1310.0 1
Aniline ND ug/L 06/03/22 13:59 62-53-306/03/22 05:1310.0 1
Anthracene ND ug/L 06/03/22 13:59 120-12-706/03/22 05:1310.0 1
Benzo(a)anthracene ND ug/L 06/03/22 13:59 56-55-306/03/22 05:1310.0 1
Benzo(a)pyrene ND ug/L 06/03/22 13:59 50-32-806/03/22 05:1310.0 1
Benzo(b)fluoranthene ND ug/L 06/03/22 13:59 205-99-206/03/22 05:1310.0 1
Benzo(g,h,i)perylene ND ug/L 06/03/22 13:59 191-24-206/03/22 05:1310.0 1
Benzo(k)fluoranthene ND ug/L 06/03/22 13:59 207-08-906/03/22 05:1310.0 1
Benzoic Acid ND ug/L 06/03/22 13:59 65-85-0 M106/03/22 05:1350.0 1
Benzyl alcohol ND ug/L 06/03/22 13:59 100-51-606/03/22 05:1320.0 1
4-Bromophenylphenyl ether ND ug/L 06/03/22 13:59 101-55-306/03/22 05:1310.0 1
Butylbenzylphthalate ND ug/L 06/03/22 13:59 85-68-706/03/22 05:1310.0 1
4-Chloro-3-methylphenol ND ug/L 06/03/22 13:59 59-50-706/03/22 05:1310.0 1
4-Chloroaniline ND ug/L 06/03/22 13:59 106-47-806/03/22 05:1320.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/03/22 13:59 111-91-106/03/22 05:1310.0 1
bis(2-Chloroethyl) ether ND ug/L 06/03/22 13:59 111-44-406/03/22 05:1310.0 1
2-Chloronaphthalene ND ug/L 06/03/22 13:59 91-58-706/03/22 05:1310.0 1
2-Chlorophenol ND ug/L 06/03/22 13:59 95-57-8 R106/03/22 05:1310.0 1
4-Chlorophenylphenyl ether ND ug/L 06/03/22 13:59 7005-72-306/03/22 05:1310.0 1
Chrysene ND ug/L 06/03/22 13:59 218-01-906/03/22 05:1310.0 1
Dibenz(a,h)anthracene ND ug/L 06/03/22 13:59 53-70-306/03/22 05:1310.0 1
Dibenzofuran ND ug/L 06/03/22 13:59 132-64-906/03/22 05:1310.0 1
1,2-Dichlorobenzene ND ug/L 06/03/22 13:59 95-50-106/03/22 05:1310.0 1
1,3-Dichlorobenzene ND ug/L 06/03/22 13:59 541-73-106/03/22 05:1310.0 1
1,4-Dichlorobenzene ND ug/L 06/03/22 13:59 106-46-706/03/22 05:1310.0 1
3,3'-Dichlorobenzidine ND ug/L 06/03/22 13:59 91-94-106/03/22 05:1320.0 1
2,4-Dichlorophenol ND ug/L 06/03/22 13:59 120-83-2 R106/03/22 05:1310.0 1
Diethylphthalate ND ug/L 06/03/22 13:59 84-66-206/03/22 05:1310.0 1
2,4-Dimethylphenol ND ug/L 06/03/22 13:59 105-67-906/03/22 05:1310.0 1
Dimethylphthalate ND ug/L 06/03/22 13:59 131-11-306/03/22 05:1310.0 1
Di-n-butylphthalate ND ug/L 06/03/22 13:59 84-74-206/03/22 05:1310.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/03/22 13:59 534-52-106/03/22 05:1320.0 1
2,4-Dinitrophenol ND ug/L 06/03/22 13:59 51-28-506/03/22 05:1350.0 1
2,4-Dinitrotoluene ND ug/L 06/03/22 13:59 121-14-206/03/22 05:1310.0 1
2,6-Dinitrotoluene ND ug/L 06/03/22 13:59 606-20-206/03/22 05:1310.0 1
Di-n-octylphthalate ND ug/L 06/03/22 13:59 117-84-006/03/22 05:1310.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/03/22 13:59 117-81-706/03/22 05:136.0 1
Fluoranthene ND ug/L 06/03/22 13:59 206-44-006/03/22 05:1310.0 1
Fluorene ND ug/L 06/03/22 13:59 86-73-706/03/22 05:1310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/03/22 13:59 87-68-306/03/22 05:1310.0 1
Hexachlorobenzene ND ug/L 06/03/22 13:59 118-74-106/03/22 05:1310.0 1
Hexachlorocyclopentadiene ND ug/L 06/03/22 13:59 77-47-406/03/22 05:1310.0 1
Hexachloroethane ND ug/L 06/03/22 13:59 67-72-106/03/22 05:1310.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/03/22 13:59 193-39-5 L106/03/22 05:1310.0 1
Isophorone ND ug/L 06/03/22 13:59 78-59-106/03/22 05:1310.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-1 Lab ID:92607644001 Collected:06/02/22 14:00 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
1-Methylnaphthalene ND ug/L 06/03/22 13:59 90-12-006/03/22 05:1310.0 1
2-Methylnaphthalene ND ug/L 06/03/22 13:59 91-57-606/03/22 05:1310.0 1
2-Methylphenol(o-Cresol)ND ug/L 06/03/22 13:59 95-48-706/03/22 05:1310.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/03/22 13:59 15831-10-406/03/22 05:1310.0 1
Naphthalene ND ug/L 06/03/22 13:59 91-20-306/03/22 05:1310.0 1
2-Nitroaniline ND ug/L 06/03/22 13:59 88-74-406/03/22 05:1320.0 1
3-Nitroaniline ND ug/L 06/03/22 13:59 99-09-206/03/22 05:1320.0 1
4-Nitroaniline ND ug/L 06/03/22 13:59 100-01-606/03/22 05:1320.0 1
Nitrobenzene ND ug/L 06/03/22 13:59 98-95-306/03/22 05:1310.0 1
2-Nitrophenol ND ug/L 06/03/22 13:59 88-75-5 R1,v106/03/22 05:1310.0 1
4-Nitrophenol ND ug/L 06/03/22 13:59 100-02-7 M106/03/22 05:1350.0 1
N-Nitrosodimethylamine ND ug/L 06/03/22 13:59 62-75-906/03/22 05:1310.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/03/22 13:59 621-64-706/03/22 05:1310.0 1
N-Nitrosodiphenylamine ND ug/L 06/03/22 13:59 86-30-606/03/22 05:1310.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/03/22 13:59 108-60-106/03/22 05:1310.0 1
Pentachlorophenol ND ug/L 06/03/22 13:59 87-86-506/03/22 05:1320.0 1
Phenanthrene ND ug/L 06/03/22 13:59 85-01-806/03/22 05:1310.0 1
Phenol ND ug/L 06/03/22 13:59 108-95-2 R106/03/22 05:1310.0 1
Pyrene ND ug/L 06/03/22 13:59 129-00-006/03/22 05:1310.0 1
1,2,4-Trichlorobenzene ND ug/L 06/03/22 13:59 120-82-106/03/22 05:1310.0 1
2,4,5-Trichlorophenol ND ug/L 06/03/22 13:59 95-95-4 R106/03/22 05:1310.0 1
2,4,6-Trichlorophenol ND ug/L 06/03/22 13:59 88-06-2 R106/03/22 05:1310.0 1
Surrogates
Nitrobenzene-d5 (S)112 %06/03/22 13:59 4165-60-006/03/22 05:1310-144 1
2-Fluorobiphenyl (S)87 %06/03/22 13:59 321-60-806/03/22 05:1310-130 1
Terphenyl-d14 (S)132 %06/03/22 13:59 1718-51-006/03/22 05:1334-163 1
Phenol-d6 (S)66 %06/03/22 13:59 13127-88-306/03/22 05:1310-130 1
2-Fluorophenol (S)80 %06/03/22 13:59 367-12-406/03/22 05:1310-130 1
2,4,6-Tribromophenol (S)103 %06/03/22 13:59 118-79-606/03/22 05:1310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
Acetone ND ug/L 06/06/22 13:20 67-64-125.0 1
Benzene ND ug/L 06/06/22 13:20 71-43-21.0 1
Bromobenzene ND ug/L 06/06/22 13:20 108-86-11.0 1
Bromochloromethane ND ug/L 06/06/22 13:20 74-97-51.0 1
Bromodichloromethane ND ug/L 06/06/22 13:20 75-27-41.0 1
Bromoform ND ug/L 06/06/22 13:20 75-25-21.0 1
Bromomethane ND ug/L 06/06/22 13:20 74-83-9 v12.0 1
2-Butanone (MEK)ND ug/L 06/06/22 13:20 78-93-35.0 1
Carbon tetrachloride ND ug/L 06/06/22 13:20 56-23-51.0 1
Chlorobenzene ND ug/L 06/06/22 13:20 108-90-71.0 1
Chloroethane ND ug/L 06/06/22 13:20 75-00-3 v11.0 1
Chloroform ND ug/L 06/06/22 13:20 67-66-31.0 1
Chloromethane ND ug/L 06/06/22 13:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/06/22 13:20 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-1 Lab ID:92607644001 Collected:06/02/22 14:00 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
4-Chlorotoluene ND ug/L 06/06/22 13:20 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/06/22 13:20 96-12-82.0 1
Dibromochloromethane ND ug/L 06/06/22 13:20 124-48-11.0 1
Dibromomethane ND ug/L 06/06/22 13:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/06/22 13:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 06/06/22 13:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 06/06/22 13:20 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 06/06/22 13:20 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 06/06/22 13:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/06/22 13:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 06/06/22 13:20 75-35-41.0 1
cis-1,2-Dichloroethene 9.6 ug/L 06/06/22 13:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/06/22 13:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/06/22 13:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 06/06/22 13:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 06/06/22 13:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 06/06/22 13:20 563-58-6 IK1.0 1
cis-1,3-Dichloropropene ND ug/L 06/06/22 13:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/06/22 13:20 10061-02-61.0 1
Diisopropyl ether ND ug/L 06/06/22 13:20 108-20-31.0 1
Ethylbenzene ND ug/L 06/06/22 13:20 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 06/06/22 13:20 87-68-32.0 1
2-Hexanone ND ug/L 06/06/22 13:20 591-78-65.0 1
p-Isopropyltoluene ND ug/L 06/06/22 13:20 99-87-61.0 1
Methylene Chloride ND ug/L 06/06/22 13:20 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/06/22 13:20 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 06/06/22 13:20 1634-04-41.0 1
Naphthalene ND ug/L 06/06/22 13:20 91-20-31.0 1
Styrene ND ug/L 06/06/22 13:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/06/22 13:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/06/22 13:20 79-34-51.0 1
Tetrachloroethene ND ug/L 06/06/22 13:20 127-18-41.0 1
Toluene ND ug/L 06/06/22 13:20 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 06/06/22 13:20 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 06/06/22 13:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 06/06/22 13:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/06/22 13:20 79-00-51.0 1
Trichloroethene 35.8 ug/L 06/06/22 13:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/06/22 13:20 75-69-4 v11.0 1
1,2,3-Trichloropropane ND ug/L 06/06/22 13:20 96-18-41.0 1
Vinyl acetate ND ug/L 06/06/22 13:20 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 06/06/22 13:20 75-01-41.0 1
Xylene (Total)ND ug/L 06/06/22 13:20 1330-20-71.0 1
m&p-Xylene ND ug/L 06/06/22 13:20 179601-23-12.0 1
o-Xylene ND ug/L 06/06/22 13:20 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-1 Lab ID:92607644001 Collected:06/02/22 14:00 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
Surrogates
4-Bromofluorobenzene (S)99 %06/06/22 13:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %06/06/22 13:20 17060-07-070-130 1
Toluene-d8 (S)108 %06/06/22 13:20 2037-26-570-130 1
Sample:TMW-2 Lab ID:92607644002 Collected:06/02/22 14:40 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/03/22 14:29 83-32-906/03/22 05:1310.0 1
Acenaphthylene ND ug/L 06/03/22 14:29 208-96-806/03/22 05:1310.0 1
Aniline ND ug/L 06/03/22 14:29 62-53-306/03/22 05:1310.0 1
Anthracene ND ug/L 06/03/22 14:29 120-12-706/03/22 05:1310.0 1
Benzo(a)anthracene ND ug/L 06/03/22 14:29 56-55-306/03/22 05:1310.0 1
Benzo(a)pyrene ND ug/L 06/03/22 14:29 50-32-806/03/22 05:1310.0 1
Benzo(b)fluoranthene ND ug/L 06/03/22 14:29 205-99-206/03/22 05:1310.0 1
Benzo(g,h,i)perylene ND ug/L 06/03/22 14:29 191-24-206/03/22 05:1310.0 1
Benzo(k)fluoranthene ND ug/L 06/03/22 14:29 207-08-906/03/22 05:1310.0 1
Benzoic Acid ND ug/L 06/03/22 14:29 65-85-006/03/22 05:1350.0 1
Benzyl alcohol ND ug/L 06/03/22 14:29 100-51-606/03/22 05:1320.0 1
4-Bromophenylphenyl ether ND ug/L 06/03/22 14:29 101-55-306/03/22 05:1310.0 1
Butylbenzylphthalate ND ug/L 06/03/22 14:29 85-68-706/03/22 05:1310.0 1
4-Chloro-3-methylphenol ND ug/L 06/03/22 14:29 59-50-706/03/22 05:1310.0 1
4-Chloroaniline ND ug/L 06/03/22 14:29 106-47-806/03/22 05:1320.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/03/22 14:29 111-91-106/03/22 05:1310.0 1
bis(2-Chloroethyl) ether ND ug/L 06/03/22 14:29 111-44-406/03/22 05:1310.0 1
2-Chloronaphthalene ND ug/L 06/03/22 14:29 91-58-706/03/22 05:1310.0 1
2-Chlorophenol ND ug/L 06/03/22 14:29 95-57-806/03/22 05:1310.0 1
4-Chlorophenylphenyl ether ND ug/L 06/03/22 14:29 7005-72-306/03/22 05:1310.0 1
Chrysene ND ug/L 06/03/22 14:29 218-01-906/03/22 05:1310.0 1
Dibenz(a,h)anthracene ND ug/L 06/03/22 14:29 53-70-306/03/22 05:1310.0 1
Dibenzofuran ND ug/L 06/03/22 14:29 132-64-906/03/22 05:1310.0 1
1,2-Dichlorobenzene ND ug/L 06/03/22 14:29 95-50-106/03/22 05:1310.0 1
1,3-Dichlorobenzene ND ug/L 06/03/22 14:29 541-73-106/03/22 05:1310.0 1
1,4-Dichlorobenzene ND ug/L 06/03/22 14:29 106-46-706/03/22 05:1310.0 1
3,3'-Dichlorobenzidine ND ug/L 06/03/22 14:29 91-94-106/03/22 05:1320.0 1
2,4-Dichlorophenol ND ug/L 06/03/22 14:29 120-83-206/03/22 05:1310.0 1
Diethylphthalate ND ug/L 06/03/22 14:29 84-66-206/03/22 05:1310.0 1
2,4-Dimethylphenol ND ug/L 06/03/22 14:29 105-67-906/03/22 05:1310.0 1
Dimethylphthalate ND ug/L 06/03/22 14:29 131-11-306/03/22 05:1310.0 1
Di-n-butylphthalate ND ug/L 06/03/22 14:29 84-74-206/03/22 05:1310.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/03/22 14:29 534-52-106/03/22 05:1320.0 1
2,4-Dinitrophenol ND ug/L 06/03/22 14:29 51-28-506/03/22 05:1350.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-2 Lab ID:92607644002 Collected:06/02/22 14:40 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dinitrotoluene ND ug/L 06/03/22 14:29 121-14-206/03/22 05:1310.0 1
2,6-Dinitrotoluene ND ug/L 06/03/22 14:29 606-20-206/03/22 05:1310.0 1
Di-n-octylphthalate ND ug/L 06/03/22 14:29 117-84-006/03/22 05:1310.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/03/22 14:29 117-81-706/03/22 05:136.0 1
Fluoranthene ND ug/L 06/03/22 14:29 206-44-006/03/22 05:1310.0 1
Fluorene ND ug/L 06/03/22 14:29 86-73-706/03/22 05:1310.0 1
Hexachloro-1,3-butadiene ND ug/L 06/03/22 14:29 87-68-306/03/22 05:1310.0 1
Hexachlorobenzene ND ug/L 06/03/22 14:29 118-74-106/03/22 05:1310.0 1
Hexachlorocyclopentadiene ND ug/L 06/03/22 14:29 77-47-406/03/22 05:1310.0 1
Hexachloroethane ND ug/L 06/03/22 14:29 67-72-106/03/22 05:1310.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/03/22 14:29 193-39-5 L106/03/22 05:1310.0 1
Isophorone ND ug/L 06/03/22 14:29 78-59-106/03/22 05:1310.0 1
1-Methylnaphthalene ND ug/L 06/03/22 14:29 90-12-006/03/22 05:1310.0 1
2-Methylnaphthalene ND ug/L 06/03/22 14:29 91-57-606/03/22 05:1310.0 1
2-Methylphenol(o-Cresol)ND ug/L 06/03/22 14:29 95-48-706/03/22 05:1310.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/03/22 14:29 15831-10-406/03/22 05:1310.0 1
Naphthalene ND ug/L 06/03/22 14:29 91-20-306/03/22 05:1310.0 1
2-Nitroaniline ND ug/L 06/03/22 14:29 88-74-406/03/22 05:1320.0 1
3-Nitroaniline ND ug/L 06/03/22 14:29 99-09-206/03/22 05:1320.0 1
4-Nitroaniline ND ug/L 06/03/22 14:29 100-01-606/03/22 05:1320.0 1
Nitrobenzene ND ug/L 06/03/22 14:29 98-95-306/03/22 05:1310.0 1
2-Nitrophenol ND ug/L 06/03/22 14:29 88-75-5 v106/03/22 05:1310.0 1
4-Nitrophenol ND ug/L 06/03/22 14:29 100-02-706/03/22 05:1350.0 1
N-Nitrosodimethylamine ND ug/L 06/03/22 14:29 62-75-906/03/22 05:1310.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/03/22 14:29 621-64-706/03/22 05:1310.0 1
N-Nitrosodiphenylamine ND ug/L 06/03/22 14:29 86-30-606/03/22 05:1310.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/03/22 14:29 108-60-106/03/22 05:1310.0 1
Pentachlorophenol ND ug/L 06/03/22 14:29 87-86-506/03/22 05:1320.0 1
Phenanthrene ND ug/L 06/03/22 14:29 85-01-806/03/22 05:1310.0 1
Phenol ND ug/L 06/03/22 14:29 108-95-206/03/22 05:1310.0 1
Pyrene ND ug/L 06/03/22 14:29 129-00-006/03/22 05:1310.0 1
1,2,4-Trichlorobenzene ND ug/L 06/03/22 14:29 120-82-106/03/22 05:1310.0 1
2,4,5-Trichlorophenol ND ug/L 06/03/22 14:29 95-95-406/03/22 05:1310.0 1
2,4,6-Trichlorophenol ND ug/L 06/03/22 14:29 88-06-206/03/22 05:1310.0 1
Surrogates
Nitrobenzene-d5 (S)109 %06/03/22 14:29 4165-60-006/03/22 05:1310-144 1
2-Fluorobiphenyl (S)87 %06/03/22 14:29 321-60-806/03/22 05:1310-130 1
Terphenyl-d14 (S)130 %06/03/22 14:29 1718-51-006/03/22 05:1334-163 1
Phenol-d6 (S)57 %06/03/22 14:29 13127-88-306/03/22 05:1310-130 1
2-Fluorophenol (S)74 %06/03/22 14:29 367-12-406/03/22 05:1310-130 1
2,4,6-Tribromophenol (S)96 %06/03/22 14:29 118-79-606/03/22 05:1310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
Acetone ND ug/L 06/06/22 13:38 67-64-125.0 1
Benzene ND ug/L 06/06/22 13:38 71-43-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-2 Lab ID:92607644002 Collected:06/02/22 14:40 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
Bromobenzene ND ug/L 06/06/22 13:38 108-86-11.0 1
Bromochloromethane ND ug/L 06/06/22 13:38 74-97-51.0 1
Bromodichloromethane ND ug/L 06/06/22 13:38 75-27-41.0 1
Bromoform ND ug/L 06/06/22 13:38 75-25-21.0 1
Bromomethane ND ug/L 06/06/22 13:38 74-83-9 v12.0 1
2-Butanone (MEK)ND ug/L 06/06/22 13:38 78-93-35.0 1
Carbon tetrachloride ND ug/L 06/06/22 13:38 56-23-51.0 1
Chlorobenzene ND ug/L 06/06/22 13:38 108-90-71.0 1
Chloroethane ND ug/L 06/06/22 13:38 75-00-3 v11.0 1
Chloroform ND ug/L 06/06/22 13:38 67-66-31.0 1
Chloromethane ND ug/L 06/06/22 13:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/06/22 13:38 95-49-81.0 1
4-Chlorotoluene ND ug/L 06/06/22 13:38 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 06/06/22 13:38 96-12-82.0 1
Dibromochloromethane ND ug/L 06/06/22 13:38 124-48-11.0 1
Dibromomethane ND ug/L 06/06/22 13:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 06/06/22 13:38 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 06/06/22 13:38 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 06/06/22 13:38 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 06/06/22 13:38 75-71-8 v11.0 1
1,1-Dichloroethane 2.0 ug/L 06/06/22 13:38 75-34-31.0 1
1,2-Dichloroethane ND ug/L 06/06/22 13:38 107-06-21.0 1
1,1-Dichloroethene 5.3 ug/L 06/06/22 13:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 06/06/22 13:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 06/06/22 13:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 06/06/22 13:38 78-87-51.0 1
1,3-Dichloropropane ND ug/L 06/06/22 13:38 142-28-91.0 1
2,2-Dichloropropane ND ug/L 06/06/22 13:38 594-20-71.0 1
1,1-Dichloropropene ND ug/L 06/06/22 13:38 563-58-6 IK1.0 1
cis-1,3-Dichloropropene ND ug/L 06/06/22 13:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 06/06/22 13:38 10061-02-61.0 1
Diisopropyl ether ND ug/L 06/06/22 13:38 108-20-31.0 1
Ethylbenzene ND ug/L 06/06/22 13:38 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 06/06/22 13:38 87-68-32.0 1
2-Hexanone ND ug/L 06/06/22 13:38 591-78-65.0 1
p-Isopropyltoluene ND ug/L 06/06/22 13:38 99-87-61.0 1
Methylene Chloride ND ug/L 06/06/22 13:38 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/06/22 13:38 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 06/06/22 13:38 1634-04-41.0 1
Naphthalene ND ug/L 06/06/22 13:38 91-20-31.0 1
Styrene ND ug/L 06/06/22 13:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 06/06/22 13:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 06/06/22 13:38 79-34-51.0 1
Tetrachloroethene ND ug/L 06/06/22 13:38 127-18-41.0 1
Toluene ND ug/L 06/06/22 13:38 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 06/06/22 13:38 87-61-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Sample:TMW-2 Lab ID:92607644002 Collected:06/02/22 14:40 Received:06/02/22 15:46 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
1,2,4-Trichlorobenzene ND ug/L 06/06/22 13:38 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 06/06/22 13:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 06/06/22 13:38 79-00-51.0 1
Trichloroethene ND ug/L 06/06/22 13:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 06/06/22 13:38 75-69-4 v11.0 1
1,2,3-Trichloropropane ND ug/L 06/06/22 13:38 96-18-41.0 1
Vinyl acetate ND ug/L 06/06/22 13:38 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 06/06/22 13:38 75-01-41.0 1
Xylene (Total)ND ug/L 06/06/22 13:38 1330-20-71.0 1
m&p-Xylene ND ug/L 06/06/22 13:38 179601-23-12.0 1
o-Xylene ND ug/L 06/06/22 13:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %06/06/22 13:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %06/06/22 13:38 17060-07-070-130 1
Toluene-d8 (S)107 %06/06/22 13:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702473
EPA 8260D
EPA 8260D
8260 MSV Low Level SC
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607644001, 92607644002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3666018
Associated Lab Samples:92607644001, 92607644002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/06/22 12:27
1,1,1-Trichloroethane ug/L ND 1.0 06/06/22 12:27
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/06/22 12:27
1,1,2-Trichloroethane ug/L ND 1.0 06/06/22 12:27
1,1-Dichloroethane ug/L ND 1.0 06/06/22 12:27
1,1-Dichloroethene ug/L ND 1.0 06/06/22 12:27
1,1-Dichloropropene ug/L ND 1.0 IK06/06/22 12:27
1,2,3-Trichlorobenzene ug/L ND 1.0 06/06/22 12:27
1,2,3-Trichloropropane ug/L ND 1.0 06/06/22 12:27
1,2,4-Trichlorobenzene ug/L ND 1.0 06/06/22 12:27
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/06/22 12:27
1,2-Dichlorobenzene ug/L ND 1.0 06/06/22 12:27
1,2-Dichloroethane ug/L ND 1.0 06/06/22 12:27
1,2-Dichloropropane ug/L ND 1.0 06/06/22 12:27
1,3-Dichlorobenzene ug/L ND 1.0 06/06/22 12:27
1,3-Dichloropropane ug/L ND 1.0 06/06/22 12:27
1,4-Dichlorobenzene ug/L ND 1.0 06/06/22 12:27
2,2-Dichloropropane ug/L ND 1.0 06/06/22 12:27
2-Butanone (MEK)ug/L ND 5.0 06/06/22 12:27
2-Chlorotoluene ug/L ND 1.0 06/06/22 12:27
2-Hexanone ug/L ND 5.0 06/06/22 12:27
4-Chlorotoluene ug/L ND 1.0 06/06/22 12:27
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/06/22 12:27
Acetone ug/L ND 25.0 06/06/22 12:27
Benzene ug/L ND 1.0 06/06/22 12:27
Bromobenzene ug/L ND 1.0 06/06/22 12:27
Bromochloromethane ug/L ND 1.0 06/06/22 12:27
Bromodichloromethane ug/L ND 1.0 06/06/22 12:27
Bromoform ug/L ND 1.0 06/06/22 12:27
Bromomethane ug/L ND 2.0 v106/06/22 12:27
Carbon tetrachloride ug/L ND 1.0 06/06/22 12:27
Chlorobenzene ug/L ND 1.0 06/06/22 12:27
Chloroethane ug/L ND 1.0 v106/06/22 12:27
Chloroform ug/L ND 1.0 06/06/22 12:27
Chloromethane ug/L ND 1.0 06/06/22 12:27
cis-1,2-Dichloroethene ug/L ND 1.0 06/06/22 12:27
cis-1,3-Dichloropropene ug/L ND 1.0 06/06/22 12:27
Dibromochloromethane ug/L ND 1.0 06/06/22 12:27
Dibromomethane ug/L ND 1.0 06/06/22 12:27
Dichlorodifluoromethane ug/L ND 1.0 v106/06/22 12:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3666018
Associated Lab Samples:92607644001, 92607644002
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 06/06/22 12:27
Ethylbenzene ug/L ND 1.0 06/06/22 12:27
Hexachloro-1,3-butadiene ug/L ND 2.0 06/06/22 12:27
m&p-Xylene ug/L ND 2.0 06/06/22 12:27
Methyl-tert-butyl ether ug/L ND 1.0 06/06/22 12:27
Methylene Chloride ug/L ND 5.0 06/06/22 12:27
Naphthalene ug/L ND 1.0 06/06/22 12:27
o-Xylene ug/L ND 1.0 06/06/22 12:27
p-Isopropyltoluene ug/L ND 1.0 06/06/22 12:27
Styrene ug/L ND 1.0 06/06/22 12:27
Tetrachloroethene ug/L ND 1.0 06/06/22 12:27
Toluene ug/L ND 1.0 06/06/22 12:27
trans-1,2-Dichloroethene ug/L ND 1.0 06/06/22 12:27
trans-1,3-Dichloropropene ug/L ND 1.0 06/06/22 12:27
Trichloroethene ug/L ND 1.0 06/06/22 12:27
Trichlorofluoromethane ug/L ND 1.0 v106/06/22 12:27
Vinyl acetate ug/L ND 2.0 IK06/06/22 12:27
Vinyl chloride ug/L ND 1.0 06/06/22 12:27
Xylene (Total)ug/L ND 1.0 06/06/22 12:27
1,2-Dichloroethane-d4 (S)%93 70-130 06/06/22 12:27
4-Bromofluorobenzene (S)%99 70-130 06/06/22 12:27
Toluene-d8 (S)%108 70-130 06/06/22 12:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3666019LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 39.350 79 70-130
1,1,1-Trichloroethane ug/L 40.950 82 70-130
1,1,2,2-Tetrachloroethane ug/L 37.450 75 70-130
1,1,2-Trichloroethane ug/L 40.150 80 70-130
1,1-Dichloroethane ug/L 38.150 76 70-130
1,1-Dichloroethene ug/L 42.550 85 70-130
1,1-Dichloropropene ug/L 39.6 IK507970-130
1,2,3-Trichlorobenzene ug/L 42.450 85 70-130
1,2,3-Trichloropropane ug/L 37.350 75 70-130
1,2,4-Trichlorobenzene ug/L 40.950 82 70-130
1,2-Dibromo-3-chloropropane ug/L 35.850 72 70-130
1,2-Dichlorobenzene ug/L 38.550 77 70-130
1,2-Dichloroethane ug/L 39.950 80 70-130
1,2-Dichloropropane ug/L 42.750 85 70-130
1,3-Dichlorobenzene ug/L 38.750 77 70-130
1,3-Dichloropropane ug/L 39.450 79 70-130
1,4-Dichlorobenzene ug/L 38.550 77 70-130
2,2-Dichloropropane ug/L 39.350 79 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3666019LABORATORY CONTROL SAMPLE:
LCSSpike
2-Butanone (MEK)ug/L 71.4100 71 70-130
2-Chlorotoluene ug/L 37.150 74 70-130
2-Hexanone ug/L 79.8100 80 70-130
4-Chlorotoluene ug/L 37.450 75 70-130
4-Methyl-2-pentanone (MIBK)ug/L 82.1100 82 70-130
Acetone ug/L 76.3100 76 70-130
Benzene ug/L 39.150 78 70-130
Bromobenzene ug/L 37.650 75 70-130
Bromochloromethane ug/L 37.750 75 70-130
Bromodichloromethane ug/L 39.050 78 70-130
Bromoform ug/L 38.350 77 70-130
Bromomethane ug/L 48.8 v1509870-130
Carbon tetrachloride ug/L 43.850 88 70-130
Chlorobenzene ug/L 38.950 78 70-130
Chloroethane ug/L 59.7 v15011970-130
Chloroform ug/L 37.150 74 70-130
Chloromethane ug/L 47.750 95 70-130
cis-1,2-Dichloroethene ug/L 39.350 79 70-130
cis-1,3-Dichloropropene ug/L 40.750 81 70-130
Dibromochloromethane ug/L 38.250 76 70-130
Dibromomethane ug/L 39.750 79 70-130
Dichlorodifluoromethane ug/L 56.7 v15011370-130
Diisopropyl ether ug/L 40.750 81 70-130
Ethylbenzene ug/L 38.650 77 70-130
Hexachloro-1,3-butadiene ug/L 46.150 92 70-130
m&p-Xylene ug/L 78.3100 78 70-130
Methyl-tert-butyl ether ug/L 39.050 78 70-130
Methylene Chloride ug/L 36.150 72 70-130
Naphthalene ug/L 40.050 80 70-130
o-Xylene ug/L 38.750 77 70-130
p-Isopropyltoluene ug/L 42.150 84 70-130
Styrene ug/L 38.750 77 70-130
Tetrachloroethene ug/L 41.450 83 70-130
Toluene ug/L 38.450 77 70-130
trans-1,2-Dichloroethene ug/L 41.150 82 70-130
trans-1,3-Dichloropropene ug/L 40.150 80 70-130
Trichloroethene ug/L 44.350 89 70-130
Trichlorofluoromethane ug/L 52.1 v15010470-130
Vinyl acetate ug/L 74.4 IK1007470-130
Vinyl chloride ug/L 49.050 98 70-130
Xylene (Total)ug/L 117150 78 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607505001
3666021
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 112 73-13493 1820ND22.4 18.6
1,1,1-Trichloroethane ug/L 20 131 82-143111 1620ND26.2 22.2
1,1,2,2-Tetrachloroethane ug/L 20 110 70-13691 1920ND22.0 18.2
1,1,2-Trichloroethane ug/L 20 118 70-135101 1620ND23.5 20.1
1,1-Dichloroethane ug/L 20 127 70-139107 1720ND25.3 21.5
1,1-Dichloroethene ug/L 20 143 70-154123 1520ND28.6 24.5
1,1-Dichloropropene ug/L IK2012570-149106 1620ND25.0 21.3
1,2,3-Trichlorobenzene ug/L 20 105 70-13598 720ND21.0 19.6
1,2,3-Trichloropropane ug/L 20 109 71-13792 1620ND21.8 18.5
1,2,4-Trichlorobenzene ug/L 20 106 73-14098 720ND21.1 19.7
1,2-Dibromo-3-chloropropane ug/L 20 97 65-13480 1920ND19.4 16.0
1,2-Dichlorobenzene ug/L 20 107 70-13393 1320ND21.3 18.7
1,2-Dichloroethane ug/L 20 127 70-137106 1820ND25.4 21.2
1,2-Dichloropropane ug/L 20 131 70-140111 1620ND26.1 22.1
1,3-Dichlorobenzene ug/L 20 109 70-13594 1420ND21.7 18.8
1,3-Dichloropropane ug/L 20 115 70-14395 1920ND23.0 18.9
1,4-Dichlorobenzene ug/L 20 106 70-13394 1220ND21.2 18.8
2,2-Dichloropropane ug/L 20 127 61-148107 1820ND25.4 21.3
2-Butanone (MEK)ug/L 40 107 60-13987 2040ND42.9 34.9
2-Chlorotoluene ug/L 20 107 70-14494 1320ND21.5 18.8
2-Hexanone ug/L 40 119 65-138100 1840ND47.7 39.8
4-Chlorotoluene ug/L 20 104 70-13792 1220ND20.9 18.5
4-Methyl-2-pentanone (MIBK)ug/L 40 123 65-135102 1940ND49.2 40.6
Acetone ug/L 40 131 60-148103 2440ND52.4 41.3
Benzene ug/L 20 121 70-151104 1520ND24.2 20.8
Bromobenzene ug/L 20 109 70-13691 1920ND21.8 18.1
Bromochloromethane ug/L 20 121 70-141100 1920ND24.2 20.1
Bromodichloromethane ug/L 20 114 70-13899 1420ND22.7 19.9
Bromoform ug/L 20 101 63-13086 1620ND20.2 17.1
Bromomethane ug/L v12014315-152134 720ND28.5 26.7
Carbon tetrachloride ug/L 20 132 70-143115 1420ND26.5 23.0
Chlorobenzene ug/L 20 116 70-138100 1520ND23.2 20.0
Chloroethane ug/L M1,v12019452-163162 1820ND38.8 32.5
Chloroform ug/L 20 114 70-13995 1820ND22.7 19.0
Chloromethane ug/L M12015841-139138 1420ND31.7 27.6
cis-1,2-Dichloroethene ug/L 20 128 70-141108 1720ND25.6 21.6
cis-1,3-Dichloropropene ug/L 20 116 70-13798 1720ND23.1 19.6
Dibromochloromethane ug/L 20 104 70-13489 1520ND20.8 17.8
Dibromomethane ug/L 20 123 70-138105 1620ND24.7 21.0
Dichlorodifluoromethane ug/L M1,v12017847-155150 1720ND35.6 30.0
Diisopropyl ether ug/L 20 122 63-144103 1720ND24.5 20.6
Ethylbenzene ug/L 20 116 66-153101 1420ND23.2 20.2
Hexachloro-1,3-butadiene ug/L 20 124 65-149114 820ND24.9 22.9
m&p-Xylene ug/L 40 116 69-152102 1340ND46.4 40.7
Methyl-tert-butyl ether ug/L 20 114 54-15695 1820ND22.8 19.1
Methylene Chloride ug/L 20 108 42-15991 1720ND21.6 18.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607505001
3666021
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Naphthalene ug/L 20 100 61-14891 920ND20.0 18.2
o-Xylene ug/L 20 114 70-14899 1420ND22.9 19.8
p-Isopropyltoluene ug/L 20 118 70-146107 1020ND23.7 21.5
Styrene ug/L 20 112 70-13597 1420ND22.4 19.4
Tetrachloroethene ug/L 20 120 59-143106 1220ND23.9 21.2
Toluene ug/L 20 121 59-148105 1420ND24.1 21.0
trans-1,2-Dichloroethene ug/L 20 135 70-146116 1520ND27.1 23.3
trans-1,3-Dichloropropene ug/L 20 114 70-13599 1420ND22.8 19.7
Trichloroethene ug/L 20 134 70-147114 1720ND26.8 22.7
Trichlorofluoromethane ug/L M1,v12017470-148146 1820ND34.7 29.1
Vinyl acetate ug/L IK4011149-15190 2140ND44.3 35.8
Vinyl chloride ug/L M12016470-156142 1420ND32.8 28.4
Xylene (Total)ug/L 60 115 63-158101 1360ND69.3 60.5
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702093
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607644001, 92607644002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664254
Associated Lab Samples:92607644001, 92607644002
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 06/03/22 11:32
1,2-Dichlorobenzene ug/L ND 10.0 06/03/22 11:32
1,3-Dichlorobenzene ug/L ND 10.0 06/03/22 11:32
1,4-Dichlorobenzene ug/L ND 10.0 06/03/22 11:32
1-Methylnaphthalene ug/L ND 10.0 06/03/22 11:32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/03/22 11:32
2,4,5-Trichlorophenol ug/L ND 10.0 06/03/22 11:32
2,4,6-Trichlorophenol ug/L ND 10.0 06/03/22 11:32
2,4-Dichlorophenol ug/L ND 10.0 06/03/22 11:32
2,4-Dimethylphenol ug/L ND 10.0 06/03/22 11:32
2,4-Dinitrophenol ug/L ND 50.0 06/03/22 11:32
2,4-Dinitrotoluene ug/L ND 10.0 06/03/22 11:32
2,6-Dinitrotoluene ug/L ND 10.0 06/03/22 11:32
2-Chloronaphthalene ug/L ND 10.0 06/03/22 11:32
2-Chlorophenol ug/L ND 10.0 06/03/22 11:32
2-Methylnaphthalene ug/L ND 10.0 06/03/22 11:32
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/03/22 11:32
2-Nitroaniline ug/L ND 20.0 06/03/22 11:32
2-Nitrophenol ug/L ND 10.0 v106/03/22 11:32
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/03/22 11:32
3,3'-Dichlorobenzidine ug/L ND 20.0 06/03/22 11:32
3-Nitroaniline ug/L ND 20.0 06/03/22 11:32
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/03/22 11:32
4-Bromophenylphenyl ether ug/L ND 10.0 06/03/22 11:32
4-Chloro-3-methylphenol ug/L ND 10.0 06/03/22 11:32
4-Chloroaniline ug/L ND 20.0 06/03/22 11:32
4-Chlorophenylphenyl ether ug/L ND 10.0 06/03/22 11:32
4-Nitroaniline ug/L ND 20.0 06/03/22 11:32
4-Nitrophenol ug/L ND 50.0 06/03/22 11:32
Acenaphthene ug/L ND 10.0 06/03/22 11:32
Acenaphthylene ug/L ND 10.0 06/03/22 11:32
Aniline ug/L ND 10.0 06/03/22 11:32
Anthracene ug/L ND 10.0 06/03/22 11:32
Benzo(a)anthracene ug/L ND 10.0 06/03/22 11:32
Benzo(a)pyrene ug/L ND 10.0 06/03/22 11:32
Benzo(b)fluoranthene ug/L ND 10.0 06/03/22 11:32
Benzo(g,h,i)perylene ug/L ND 10.0 06/03/22 11:32
Benzo(k)fluoranthene ug/L ND 10.0 06/03/22 11:32
Benzoic Acid ug/L ND 50.0 06/03/22 11:32
Benzyl alcohol ug/L ND 20.0 06/03/22 11:32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664254
Associated Lab Samples:92607644001, 92607644002
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/03/22 11:32
bis(2-Chloroethyl) ether ug/L ND 10.0 06/03/22 11:32
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/03/22 11:32
Butylbenzylphthalate ug/L ND 10.0 06/03/22 11:32
Chrysene ug/L ND 10.0 06/03/22 11:32
Di-n-butylphthalate ug/L ND 10.0 06/03/22 11:32
Di-n-octylphthalate ug/L ND 10.0 06/03/22 11:32
Dibenz(a,h)anthracene ug/L ND 10.0 06/03/22 11:32
Dibenzofuran ug/L ND 10.0 06/03/22 11:32
Diethylphthalate ug/L ND 10.0 06/03/22 11:32
Dimethylphthalate ug/L ND 10.0 06/03/22 11:32
Fluoranthene ug/L ND 10.0 06/03/22 11:32
Fluorene ug/L ND 10.0 06/03/22 11:32
Hexachloro-1,3-butadiene ug/L ND 10.0 06/03/22 11:32
Hexachlorobenzene ug/L ND 10.0 06/03/22 11:32
Hexachlorocyclopentadiene ug/L ND 10.0 06/03/22 11:32
Hexachloroethane ug/L ND 10.0 06/03/22 11:32
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/03/22 11:32
Isophorone ug/L ND 10.0 06/03/22 11:32
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/03/22 11:32
N-Nitrosodimethylamine ug/L ND 10.0 06/03/22 11:32
N-Nitrosodiphenylamine ug/L ND 10.0 06/03/22 11:32
Naphthalene ug/L ND 10.0 06/03/22 11:32
Nitrobenzene ug/L ND 10.0 06/03/22 11:32
Pentachlorophenol ug/L ND 20.0 06/03/22 11:32
Phenanthrene ug/L ND 10.0 06/03/22 11:32
Phenol ug/L ND 10.0 06/03/22 11:32
Pyrene ug/L ND 10.0 06/03/22 11:32
2,4,6-Tribromophenol (S)%94 10-144 06/03/22 11:32
2-Fluorobiphenyl (S)%93 10-130 06/03/22 11:32
2-Fluorophenol (S)%80 10-130 06/03/22 11:32
Nitrobenzene-d5 (S)%118 10-144 06/03/22 11:32
Phenol-d6 (S)%61 10-130 06/03/22 11:32
Terphenyl-d14 (S)%133 34-163 06/03/22 11:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664255LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 26.950 54 18-130
1,2-Dichlorobenzene ug/L 27.550 55 20-130
1,3-Dichlorobenzene ug/L 27.250 54 18-130
1,4-Dichlorobenzene ug/L 26.950 54 18-130
1-Methylnaphthalene ug/L 27.550 55 29-130
2,2'-Oxybis(1-chloropropane)ug/L 33.050 66 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664255LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 38.150 76 35-130
2,4,6-Trichlorophenol ug/L 38.950 78 31-130
2,4-Dichlorophenol ug/L 35.450 71 35-130
2,4-Dimethylphenol ug/L 36.050 72 34-130
2,4-Dinitrophenol ug/L 244250 97 10-153
2,4-Dinitrotoluene ug/L 54.650 109 37-136
2,6-Dinitrotoluene ug/L 45.450 91 33-136
2-Chloronaphthalene ug/L 29.050 58 26-130
2-Chlorophenol ug/L 34.150 68 37-130
2-Methylnaphthalene ug/L 27.450 55 29-130
2-Methylphenol(o-Cresol)ug/L 30.950 62 35-130
2-Nitroaniline ug/L 83.4100 83 37-130
2-Nitrophenol ug/L 41.7 v1508332-130
3&4-Methylphenol(m&p Cresol)ug/L 29.550 59 34-130
3,3'-Dichlorobenzidine ug/L 113100 113 34-136
3-Nitroaniline ug/L 87.3100 87 37-138
4,6-Dinitro-2-methylphenol ug/L 113100 113 21-157
4-Bromophenylphenyl ether ug/L 38.650 77 38-130
4-Chloro-3-methylphenol ug/L 72.0100 72 37-130
4-Chloroaniline ug/L 67.6100 68 38-130
4-Chlorophenylphenyl ether ug/L 33.250 66 33-130
4-Nitroaniline ug/L 106100 106 42-137
4-Nitrophenol ug/L 163250 65 10-130
Acenaphthene ug/L 31.450 63 33-130
Acenaphthylene ug/L 32.250 64 35-130
Aniline ug/L 30.850 62 22-130
Anthracene ug/L 43.750 87 48-130
Benzo(a)anthracene ug/L 55.250 110 48-137
Benzo(a)pyrene ug/L 64.250 128 49-138
Benzo(b)fluoranthene ug/L 61.050 122 52-138
Benzo(g,h,i)perylene ug/L 65.550 131 48-140
Benzo(k)fluoranthene ug/L 64.350 129 48-139
Benzoic Acid ug/L 77.6250 31 10-130
Benzyl alcohol ug/L 63.5100 63 35-130
bis(2-Chloroethoxy)methane ug/L 36.450 73 34-130
bis(2-Chloroethyl) ether ug/L 35.750 71 36-130
bis(2-Ethylhexyl)phthalate ug/L 65.650 131 32-165
Butylbenzylphthalate ug/L 65.550 131 34-161
Chrysene ug/L 56.150 112 47-131
Di-n-butylphthalate ug/L 59.650 119 39-144
Di-n-octylphthalate ug/L 59.050 118 30-170
Dibenz(a,h)anthracene ug/L 65.750 131 49-138
Dibenzofuran ug/L 33.350 67 33-130
Diethylphthalate ug/L 47.150 94 38-131
Dimethylphthalate ug/L 40.550 81 37-130
Fluoranthene ug/L 55.450 111 46-137
Fluorene ug/L 35.650 71 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664255LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 24.950 50 11-130
Hexachlorobenzene ug/L 41.850 84 38-130
Hexachlorocyclopentadiene ug/L 25.150 50 10-130
Hexachloroethane ug/L 26.550 53 14-130
Indeno(1,2,3-cd)pyrene ug/L 65.9 L15013241-130
Isophorone ug/L 35.350 71 33-130
N-Nitroso-di-n-propylamine ug/L 35.750 71 36-130
N-Nitrosodimethylamine ug/L 33.450 67 34-130
N-Nitrosodiphenylamine ug/L 43.650 87 37-130
Naphthalene ug/L 28.750 57 30-130
Nitrobenzene ug/L 40.750 81 36-130
Pentachlorophenol ug/L 97.1100 97 23-149
Phenanthrene ug/L 47.850 96 44-130
Phenol ug/L 23.750 47 18-130
Pyrene ug/L 54.350 109 47-134
2,4,6-Tribromophenol (S)%99 10-144
2-Fluorobiphenyl (S)%71 10-130
2-Fluorophenol (S)%62 10-130
Nitrobenzene-d5 (S)%91 10-144
Phenol-d6 (S)%46 10-130
Terphenyl-d14 (S)%124 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3664256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607644001
3664257
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 53 10-13056 650ND26.3 27.9
1,2-Dichlorobenzene ug/L 50 33 10-13035 550ND16.6 17.5
1,3-Dichlorobenzene ug/L 50 27 10-13029 750ND13.5 14.4
1,4-Dichlorobenzene ug/L 50 29 10-13030 450ND14.6 15.1
1-Methylnaphthalene ug/L 50 77 10-13084 850ND38.7 41.8
2,2'-Oxybis(1-chloropropane)ug/L 50 78 12-14286 1050ND38.8 42.9
2,4,5-Trichlorophenol ug/L R1504210-143118 9550ND21.0 59.1
2,4,6-Trichlorophenol ug/L R1502110-147116 13950ND10.5 58.0
2,4-Dichlorophenol ug/L R1505110-138103 6750ND25.7 51.5
2,4-Dimethylphenol ug/L 50 92 25-130104 1350ND45.9 52.1
2,4-Dinitrophenol ug/L 250 15 10-165123250ND36.7J 306
2,4-Dinitrotoluene ug/L 50 112 29-148132 1650ND56.0 66.0
2,6-Dinitrotoluene ug/L 50 117 26-146131 1150ND58.4 65.3
2-Chloronaphthalene ug/L 50 85 11-13097 1250ND42.7 48.4
2-Chlorophenol ug/L R1504510-13393 6950ND22.5 46.3
2-Methylnaphthalene ug/L 50 75 13-13082 850ND37.6 40.8
2-Methylphenol(o-Cresol)ug/L 50 77 20-13094 1950ND38.5 46.8
2-Nitroaniline ug/L 100 111 24-136123 10100ND111123
2-Nitrophenol ug/L R1,v1504210-153116 9350ND21.0 57.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3664256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607644001
3664257
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 74 16-13095 2450ND37.1 47.4
3,3'-Dichlorobenzidine ug/L 100 114 10-153107 6100ND114107
3-Nitroaniline ug/L 100 116 22-151130 11100ND116130
4,6-Dinitro-2-methylphenol ug/L 100 20 10-180127100ND19.7J 127
4-Bromophenylphenyl ether ug/L 50 103 25-130113 1050ND51.4 56.6
4-Chloro-3-methylphenol ug/L 100 96 25-133116 19100ND96.5 116
4-Chloroaniline ug/L 100 81 14-13287 7100ND81.0 87.2
4-Chlorophenylphenyl ether ug/L 50 97 19-130105 850ND48.6 52.7
4-Nitroaniline ug/L 100 110 29-150123 10100ND110123
4-Nitrophenol ug/L M1250010-13084250NDND210
Acenaphthene ug/L 50 93 16-130103 1150ND46.3 51.6
Acenaphthylene ug/L 50 94 15-137105 1150ND46.9 52.6
Aniline ug/L 50 70 10-13058 2050ND35.2 28.8
Anthracene ug/L 50 100 37-136110 950ND50.0 55.0
Benzo(a)anthracene ug/L 50 111 40-145119 750ND55.6 59.7
Benzo(a)pyrene ug/L 50 129 41-146138 750ND64.6 68.9
Benzo(b)fluoranthene ug/L 50 123 39-151129 550ND61.3 64.6
Benzo(g,h,i)perylene ug/L 50 128 40-147143 1150ND64.2 71.4
Benzo(k)fluoranthene ug/L 50 129 40-146139 750ND64.7 69.3
Benzoic Acid ug/L M1250010-13073250NDND182
Benzyl alcohol ug/L 100 83 25-13095 14100ND82.9 95.0
bis(2-Chloroethoxy)methane ug/L 50 93 23-130105 1150ND46.6 52.3
bis(2-Chloroethyl) ether ug/L 50 87 25-13098 1250ND43.4 49.1
bis(2-Ethylhexyl)phthalate ug/L 50 136 28-166144 650ND68.0 71.9
Butylbenzylphthalate ug/L 50 138 33-165147 650ND68.9 73.5
Chrysene ug/L 50 109 38-141117 750ND54.7 58.7
Di-n-butylphthalate ug/L 50 124 32-153134 850ND61.8 67.0
Di-n-octylphthalate ug/L 50 122 30-175133 950ND60.8 66.5
Dibenz(a,h)anthracene ug/L 50 125 39-148143 1450ND62.4 71.5
Dibenzofuran ug/L 50 95 20-130105 1150ND47.4 52.7
Diethylphthalate ug/L 50 106 28-142114 750ND53.2 57.2
Dimethylphthalate ug/L 50 101 26-136111 950ND50.7 55.3
Fluoranthene ug/L 50 112 39-143126 1150ND56.1 62.8
Fluorene ug/L 50 101 24-132109 750ND50.5 54.5
Hexachloro-1,3-butadiene ug/L 50 35 10-13035 150ND17.7 17.5
Hexachlorobenzene ug/L 50 101 29-130111 950ND50.5 55.3
Hexachlorocyclopentadiene ug/L 50 62 10-13072 1550ND30.9 36.0
Hexachloroethane ug/L 50 24 10-13023 350ND11.9 11.6
Indeno(1,2,3-cd)pyrene ug/L 50 128 39-148143 1150ND64.0 71.6
Isophorone ug/L 50 92 23-130102 1150ND45.9 51.2
N-Nitroso-di-n-propylamine ug/L 50 92 25-130104 1150ND46.2 51.9
N-Nitrosodimethylamine ug/L 50 82 22-13094 1350ND41.1 46.8
N-Nitrosodiphenylamine ug/L 50 108 26-134120 1050ND54.2 59.9
Naphthalene ug/L 50 61 14-13066 750ND30.7 32.9
Nitrobenzene ug/L 50 95 25-130107 1250ND47.7 53.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3664256MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607644001
3664257
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 100 16 10-175111100ND15.7J 111
Phenanthrene ug/L 50 107 36-133118 1050ND53.7 59.2
Phenol ug/L R1504810-13072 4150ND23.8 36.1
Pyrene ug/L 50 111 40-143115 350ND55.5 57.4
2,4,6-Tribromophenol (S)%40 10-144114
2-Fluorobiphenyl (S)%63 10-13070
2-Fluorophenol (S)%18 10-13075
Nitrobenzene-d5 (S)%87 10-144101
Phenol-d6 (S)%42 10-13066
Terphenyl-d14 (S)%116 34-163114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 26
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 26
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92607644
2501 WILKINSON BLVD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92607644001 702093 702262TMW-1 EPA 3510C EPA 8270E
92607644002 702093 702262TMW-2 EPA 3510C EPA 8270E
92607644001 702473TMW-1 EPA 8260D
92607644002 702473TMW-2 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/06/2022 03:30 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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