Rev Assessment_WP_Hoke St Passage Homes

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
November 28, 2022
NCDEQ — Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Attn: Mr. Brad Atkinson
Re: Brownfields Assessment Work Plan
Hoke Street Passage Home
500 & 506 Hoke Street and 1402 & 1412 Garner Road
Raleigh, North Carolina
Brownfields Project No. 21007-17-092
H&H Job No. APT-001
Dear Brad:
On behalf of Hoke Street PH Redevelopment, LLC, enclosed please find a copy of the Brownfields
Assessment Work Plan prepared for the Hoke Street Passage Home Brownfields property and the parcel
located at 1402 Garner Road in Raleigh, Wake County. In addition, H&H has provided a completed copy
of the Brownfields Program Environmental Site Assessment Work Plan Minimum Requirements Checklist
for ease of your review.
Should you have any questions or need additional information, please do not hesitate to contact us at (919)
847-4241.
Sincerely,
Hart & Hickman, PC
Justin Ballard, PG
Project Manager
Enclosure:
Jared Wilke, PG
Project Geologist
cc: Ms. Aditi Posek, DEQ Brownfields (via email)
Mr. John Gallagher, Aptus Management, PLLC (via email)
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Environmental Site Assessment Work Plan
Minimum Requirements Checklist
NCDEQ Brownfields Program — November 2018
Title Page
The title page should include the following information. Letter style reports are acceptable, as long as this
information is somewhere on the first page.
X Title of Work Plan
X Brownfields Project Name (not the development name)
X Brownfields Project Number
X Date (updated with each revision)
NA Revision Number
X Firm PE/PG License Number
X Individual PE/PG seal & signature
Section 1— Introduction
X Provide the site location, address, and acreage.
X Provide a BRIEF summary of the history of the property and its history in the program. For
example: reiterating RECs from a Phase I ESA, indicate if the scope of work negotiated during a
Data Gap Meeting, etc.
X Briefly list and describe the data gaps the assessment is attempting to fill
NA Indicate if the assessment data is intended for use by any other DEQ programs in addition to the
Brownfields Program (i.e. UST, IHSB, etc.)
Section 2 — Scope of Work
X Provide a general description of proposed scope of work covered in this plan (i.e. 2 new monitoring
wells, six groundwater samples, 5 soil gas sampling points and 6 soil borings)
X Discuss samples to be collected by media and source area/location. Generally, the reasoning for the
sample locations selected.
X Describe depths of samples to be collected (Reference Table 1) or how that decision will be made
in the field, if needed.
X State for what each sample will be analyzed (briefly). Reference Table 1.
Section 3 — Sampling Methodology
X Reference the guidance documents you intend to use. ISHB, EPA SESD, VI Guidance, Well
Construction Rules (NCAC 2C). Note deviations or methodology planned that is not covered by
such guidance (e.g., multi -increment sampling, passive air samplers).
X Describe what will be installed (soil boring, temporary well, permanent well, sub slab, soil gas, etc.).
Include construction details.
X Discuss installation methodology (Hand Auger, DPT, etc.)
X Discuss sample collection procedures. Include the following, at a minimum:
• Equipment to be used
• Purging methods and volumes
• Stabilization parameters for groundwater sampling
• Field screening methods

Work Plan Checklist
Version 1 November 2018
Page 2 of 3
• Leak check procedures for sub -slab and soil gas samples
• Discuss how and when vacuum readings will be collected (for summa cans)
X Discuss sample point abandonment
Section 4 — Laboratory Analyses
X Discuss the proposed analyses (include method number, preparation method, if there are concerns
with short hold times, etc).
NA Discuss any proposed limitations on the contaminants of concern, if any, and the reason for such
limitation (sufficient previous data, indoor air interferences, etc).
X Discuss laboratory certifications. Please note, NC does not certify labs for air samples. Please
specify what certification the proposed air lab holds.
X Indicate the Reporting Limits/Method Detection Limits will meet applicable screening criteria (to
the extent feasible). Include Reporting of J-Flags to meet criteria.
X Indicate what Level QA/QC will be reported by the laboratory. Level II QA/QC is typically
acceptable.
Section 5 — QA/QC
X Specify the duplicate sample frequency. Minimum requirement: 1 duplicate per 20 samples, per
media, per method.
X Discuss Trip Blank. 1 Trip Blank per cooler/shipment of groundwater VOC analyses.
NA Discuss how the lab will have sufficient sample volume for MS/MSD analyses.
X Discuss chain of custody and shipping.
Section 6 — Investigation Derived Waste (IDW) Management
X Discuss what IDW will be generated and how it is proposed to be managed. Management
recommendations should be in accordance with 15A NCAC 02T.1503 and 15A NCAC 02H. 0106.
Generally, if the Brownfields Property has not previously been assessed, then all IDW must be
containerized and characterized prior to management. Previous assessment data that indicate no
Hazardous Waste (listed or characteristic) is likely to be encountered in the area of proposed
assessment will be required before thin spreading of IDW on -site is permitted.
Section 7 — Reporting
This section should discuss the components of the assessment report which will be prepared as a result of
the above sample collection. At a minimum, the report shall include:
X Reporting/summary of site work conducted for all sections outlined above in this checklist;
X Summary of findings and possible recommendations;
X All applicable tables and figures outlined below with the addition of:
Tables for tabulated analytical data per media sampled and analyzed, compared against
applicable screening levels;
Figure depicting actual sample locations collected, with each media depicted in the legend,
graphic scale and north arrow; and
Groundwater potentiometric map, with graphic scale and north arrow,
X Firm PE/PG License Number
X Individual PE/PG seal & signature

Work Plan Checklist
Version 1 November 2018
Page 3 of 3
Attachments
X Table 1 — Proposed Sample Locations and Analyses on a Summary Table that includes:
Sample ID
Sample Objective
Proposed Depth(s)
Analytical Method(s)
QA/QC Samples
Background Samples
X Figure 1 — Site Location Map
Site location on a topographic map base.
Graphic scale and north arrow
X Figure 2 — Site Map should include the following
Buildings
Historical sample locations
RECs or other areas of concern
Proposed sample locations
Sample Identification labels
Background Samples
QA/QC Samples
Graphic scale and north arrow
High quality aerial suggested as the base map
X Figure 3 — Proposed Development (if available)
Overlay of historical and proposed sample locations,
Graphic scale and north arrow.
NA Appendix — Summary of Historical Analytical Data (if needed)

Brownfields Assessment
Work Plan
Hoke Street Passage Home
500 & 506 Hoke Street and
1402 & 1412 Garner Road
Raleigh, North Carolina
Brownfields Project No.
21007-17-092
Revised November 28, 2022
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SMARTER ENVIRONMENTAL SOLUTIONS
#C-1269 Engineering
#C-245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.S86.0007 main 919.847.4241 main

Brownfields Assessment Work Plan
Hoke Street Passage Home
500 & 506 Hoke Street and 1402 & 1412 Garner Road
Raleigh, North Carolina
Brownfields Project No. 21007-17-092
H&H Job No. APT-001
Table of Contents
Section
Page No.
1.0 Introduction.............................................................................................................................1
2.0 Site Background...................................................................................................................... 2
3.0 Brownfields Assessment Activities....................................................................................... 7
3.1 Soil Assessment Activities................................................................................................... 7
3.2 Groundwater Assessment Activities..................................................................................... 9
3.3 Vapor Intrusion Assessment Activities.............................................................................. 11
4.0 Quality Assurance/Quality Control Samples.....................................................................14
5.0 Investigation Derived Waste(IDW)....................................................................................16
6.0 Reporting...............................................................................................................................17
Table
Table 1 Proposed Sampling Plan
Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 2 Proposed Sample Location Map
Appendices
Appendix A Redevelopment Plans
Appendix B Laboratory Certifications and Accreditations
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ph.docx

Brownfields Assessment Work Plan
Hoke Street Passage Home
500 & 506 Hoke Street and 1402 & 1412 Garner Road
Raleigh, North Carolina
Brownfields Project No. 21007-17-092
H&H Job No. APT-001
1.0 Introduction
On behalf of Hoke Street PH Redevelopment, LLC, Hart & Hickman, P.C. (H&H) has prepared
this Work Plan to conduct Brownfields assessment activities at the Hoke Street Passage Home
Brownfields property (Brownfields Project No. 21007-17-092) located at 500 and 506 Hoke Street,
and 1402 and 1412 Garner Road in Raleigh, Wake County, North Carolina (Site). The Site consists
of four contiguous parcels (Wake County Parcel Identification Nos. [PINS] 1703828886,
1703920846, 1703922815, and 1703920658) of land that total approximately 3.95 acres.
On January 6, 2020, the North Carolina Department of Environmental Quality (DEQ) and Hoke
Street PH Redevelopment, LLC entered into a Brownfields Agreement (BFA) for the 500 and 506
Hoke Street, and 1412 Garner Road parcels. On July 15, 2022, Hoke Street PH Redevelopment,
LLC submitted a Brownfields Property Application (BPA) for the 1402 Garner Road parcel. As
of the date of this Work Plan, the 1402 Garner Road parcel (PIN 1703922815) is awaiting
eligibility into the Brownfields Program.
Proposed redevelopment plans for the Site include razing the existing Site buildings, and the
construction of a four-story senior living apartment building with associated parking areas, access
drives, and stormwater control measures. A Site location map is provided as Figure 1, and the Site
and surrounding area are shown in Figure 2. A copy of the current proposed redevelopment plans
is included in Appendix A.
H&H reviewed available resources to obtain information regarding historical uses of the Site and
identify areas of potential environmental concern for proposed Brownfields assessment activities.
A brief summary of our review is provided in the following section.
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2.0 Site Background
500 and 506 Hoke Street, and 1412 Garner Road
As previously mentioned, the Hoke Street Passage Home Brownfields property consists of three
parcels. The north -central portion of the Site (506 Hoke Street) is unimproved and was historically
used primarily for parking. The northwestern portion of the Site (500 Hoke Street) is developed
with an approximately 14,500-square foot (sq ft) vacant warehouse building constructed in 1948.
Past uses of the warehouse and the unimproved 1412 Garner Road parcel adjacent to the south
included waste management operations by Nyetech Hazardous Waste Transport and other
commercial uses. Nyetech leased space in 2003 and 2004 and reportedly managed waste materials
brought to the property where they were temporarily stored, solidified, stockpiled, and repackaged
before being transported to other off -Site disposal locations.
During Nyetech's operational period, DEQ issued a series of enforcement orders and actions for
non-compliance, which limited their operations and subsequently resulted in the excavation and
off -Site disposal of 176.21 tons of soil, followed by Nyetech vacating the Site in 2004. H&H
understands that these activities were not well documented. However, according to the BFA,
arsenic, and polycyclic aromatic hydrocarbons (PAHs, a subset of SVOCs) benzo(a)anthracene,
benzo(b)fluoranthene, benzo(b)pyrene, and indeno(1,2,3-cd)pyrene were identified in post -
excavation confirmation soil samples at concentrations above the February 2018 DEQ Preliminary
Soil Remediation Goals (PSRGs). PAHs are commonly found in urban areas and industrial and
commercial properties such as the subject Site. As further discussed below, PAHs were not
identified during later soil assessments and as such, are not considered a constituent of concern for
the Brownfields Property as evident in their absence from Exhibit 2 of the BFA.
From 2016 through 2018, assessment activities were completed as part of property transaction due
diligence and under the purview of the DEQ Brownfields Program. These activities included the
collection of groundwater, soil, and vapor intrusion -related samples. The results of the assessment
activities are briefly summarized below:
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• Results of groundwater assessment activities indicated chromium (up to 29 micrograms
per liter [µg/L]), lead (up to 84 µg/L,), and the chlorinated compounds carbon tetrachloride
(2.5 µg/L), tetrachloroethylene (PCE, up to 37 µg/L), and trichloroethylene (TCE, 6 µg/L)
were detected in samples collected from monitoring wells MW-1, MW-2, MW-3, and/or
TW-1 at concentrations above the Title 15A NCAC 2L .0202 Groundwater Standards
(2L Standards). The upper -range detections of PCE and TCE are also above the DEQ
Residential Vapor Intrusion Screening Levels (VISLs) for groundwater.
In general, groundwater impacts were identified in the southeastern portion of the
Brownfields Property in monitoring wells MW-1, MW-2, and MW-3, and to a lesser extent,
TW-1, which is located in the eastern portion of the Brownfields Property and south of the
1402 Garner Road parcel. As further discussed below, the southeastern portion of the
Brownfields Property is located in close proximity to the former Ashland LLC Chemical
Distribution Facility.
• Results of soil assessment activities indicated naturally occurring levels of arsenic were
detected above the Residential PSRG. Of note, no other metals and no volatile organic
compounds (VOCs) or semi-VOCs (SVOCs) were detected in samples collected from the
former Nyetech waste management areas or in an area of a former underground storage
tank (UST) northeast of the vacant warehouse building. As it relates to liability protection
provided in the BFA, only arsenic and the insecticide -related compound delta-BHC (due
to the absence of PSRGs for delta-BHC) are included in the Soil section of Exhibit 2.
• Results of sub -slab vapor sampling completed in the vacant warehouse building indicated
PCE (590 micrograms per cubic meter [µg/m3]) was detected above the DEQ Residential
VISLs. Evaluation of the sub -slab vapor sampling results using the October 2017 DEQ
Risk Calculator indicated the soil gas to indoor air vapor intrusion pathway does not pose
an unacceptable risk to future residential building occupants.
Results of indoor sampling completed in the vacant warehouse building carbon
tetrachloride (0.48 µg/m3) and naphthalene (up to 2.4 µg/m3) were detected in indoor air
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samples above the DEQ Residential VISLs. Of note, carbon tetrachloride was also detected
in the ambient air sample at a similar concentration (0.47 µg/m3). H&H further evaluated
the indoor air results using the latest (July 2022) DEQ Risk Calculator by inputting the
highest concentrations of compounds detected in any indoor air sample collected during
the May 2018 sampling event to check a hypothetical worst -case scenario. Results of
indoor air assessment activities indicated that calculated cumulative risk values for the
indoor air vapor intrusion pathway were within the acceptable carcinogenic risk of less
than 1 x 10-4 and less than a hazard index of 1.
In summary, the results of the previously conducted vapor intrusion assessment activities
indicate that structural vapor intrusion into the warehouse building does not pose a
significant risk for residential uses.
As mentioned above, assessment activities completed at the Brownfields Property indicate
chlorinated VOCs have been identified in groundwater, sub -slab vapor, and indoor air. These
constituents were also identified during assessments completed to investigate the former Ashland
LLC Chemical Distribution Facility, which was located southwest and topographically
downgradient to cross -gradient of the Site. The former Ashland facility was developed in the late-
1960s for warehousing and bulk distribution of industrial chemicals and solvents. Bulk distribution
operations ceased in the late 1980s and Ashland vacated the facility in 2005. Since the mid- 1980s,
environmental investigations have been completed to evaluate subsurface VOC impacts associated
with the facility. Dating back to at least 2009, groundwater investigations have been conducted at
the facility property and surrounding properties as part of corrective action activities under
Ashland's Resource Conservation and Recovery Act (RCRA) Permit NCD088560032.
A brief description of the operational history of the 1402 Garner Road portion of the Site is
provided below.
1402 Garner Road
The northeastern portion of the Site (1402 Garner Road) is developed with two buildings. The
southern building is approximately 1,800-sq ft and was formerly utilized as an automotive repair
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shop. The northern building is approximately 2,500-sq-ft and is currently operating as a
convenience store. This portion of the Site has also been utilized for commercial purposes under
the address 1400 Garner Road. As part of due diligence activities completed in January 2022,
H&H prepared a Limited Site Evaluation that consisted of a desktop review of available records,
and Site reconnaissance. According to available records, the 1402 Garner Road parcel operated
from 1974 through 1987 as a gasoline service station under the name Stallings Douglas Union 76.
In addition, City of Raleigh directory listings indicate that the parcel was utilized as a filling station
as early as 1931. Other notable Site occupants include Stallings Pure Oil Service, Stallings
Wrecker Service, Coopers Mufflers & Brakes, K&L Auto Service, Roberts Auto Service, and
Bakers Upholstery & Trim Shop.
Although the property has been utilized as a service station and automotive repair shop for over
70 years, there are no reported environmental incidents, leaking tanks, spills, or releases associated
with the Site. In addition, the property is not a "Regulated site" in that it is neither listed as a DEQ
disposal or incident management site, nor currently subject to an assessment, cleanup agreement,
and/or other regulatory obligations. Based on H&H's limited record review and an inquiry made
to the former Site owner, no other environmental information (i.e., Phase I or Phase II ESAs, UST
closure reports, etc.) was available for review.
As part of the Site reconnaissance performed in January 2022, H&H contracted with GPRS to
perform a geophysical survey to identify potential subsurface Site features, including buried tanks.
To complete the survey, GPRS utilized electromagnetic and ground penetrating radar (GPR)
equipment. The results of the geophysical survey did not identify the presence of USTs at the Site,
although it should be noted that survey obstructions (parked vehicles, concrete slabs, etc.) may
have impacted the equipment's ability to detect subsurface Site features. However, evidence of
potential former petroleum operations was observed in the form of ventilation pipes and a fuel
dispenser concrete island. In addition, utility and/or product piping conduits were observed in the
southern portion of the parcel and in an area where vehicle obstructions were present. Although it
was not substantiated by the geophysical survey, it is possible that a UST is present or was formerly
located in the southern portion of the parcel.
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In early 2022, the automotive repair shop vacated the Site and on August 8, 2022, Hoke Street PH
Redevelopment, LLC assumed ownership of the parcel. Based on the parcel's historical use as a
service station and automotive repair shop, there is potential for releases to have occurred due to
some combination of leaking suspect USTs, potential in -ground hydraulic lifts and floor drains,
observed poor management practices of oil and hazardous substances, and use of the parcel as a
vehicle junkyard.
In order to address anticipated DEQ requests for additional assessment at the Site to support Hoke
Street PH Redevelopment, LLC's proposed redevelopment plans, H&H proposes to conduct soil,
groundwater, and vapor intrusion assessment activities to further evaluate potential impacts at the
Site. Based upon the results of previous assessment activities, proposed soil and groundwater
assessment will be targeted at the 1402 Garner Road property, and proposed vapor intrusion
assessment will be targeted for the footprint of the proposed senior living apartment building.
Proposed Brownfields assessment activities are outlined in the following sections.
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3.0 Brownfields Assessment Activities
The proposed Brownfields assessment activities will be performed in general accordance with the
DEQ Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup
(Guidelines) dated July 2021, the DEQ Division of Waste Management (DWM) Vapor Intrusion
Guidance dated March 2018, Brownfield's Vapor Intrusion Assessment Work Plan & Report
Checklist (VI Checklist) dated July 2021, and the most recent versions of the U.S. EPA Region IV
Laboratory Services and Applied Science Division (LSASD) Field Branches Quality System and
Technical Procedures guidance.
Prior to conducting field activities, H&H will contact North Carolina 811 One -Call, the public
utility locator service, to mark subsurface utilities at the Site. H&H will also team with a private
utility locator to identify and mark locations of sub -grade utilities at the Site that may not be
marked by the public locator.
3.1 Soil Assessment Activities
H&H proposes to advance soil borings on the 1402 Garner Road property to evaluate potential
impacts from historical operations at the Site relative to proposed redeveloped plans (i.e., areas of
potential soil disturbance [cut]) for on -Site management and/or off -Site disposal purposes. As
previously mentioned, proposed redevelopment plans for the Site include razing the existing Site
buildings, and the construction of a four-story senior living apartment building with associated
parking areas, access drives, and stormwater control measures.
H&H proposes to advance each boring via a decontaminated, stainless steel hand auger and/or
direct -push technology (DPT) drilling rig to depths up to the approximate groundwater table (see
Section 3.2). Continuous soil samples will be collected from the borings and logged for lithological
description and field screened for indication of potential impacts by observation for staining,
unusual odors, and the presence of volatile organic vapors using a calibrated photoionization
detector (PID). Soil borings will be advanced for laboratory analyses, which are also described in
Table 1. The approximate locations of the proposed soil borings in conjunction with the proposed
redevelopment are shown on Figure 3, and described below.
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• SB-16 (co -located with TW-3) will be advanced to a minimum depth of approximately 5
feet below ground surface (ft bgs) downgradient of a suspected underground storage tank
(UST), as identified during a Limited Phase I Site Assessment conducted by H&H in
December 2019. If field observations indicate potential impacts based on elevated PID
readings, staining, and/or petroleum/solvent odors, a sample will be collected from a 2-ft
interval representative of the potential impacts. If no evidence of potential impacts is
observed, soil samples will be collected from the interval with the highest PID reading or
surficial soil (i.e., 0-2 ft bgs). The soil sample will be submitted for laboratory analysis of
SVOCs by EPA Method 8270 and Resource Conservation and Recovery Act (RCRA)
metals plus hexavalent chromium by EPA Methods 6020/7471/7199.
• SB-17 (co -located with TW-4) will be advanced to a minimum depth of approximately 5
ft bgs in the east -central portion of the Site adjacent to a former fuel dispenser. If field
observations indicate potential impacts based on elevated PID readings, staining, and/or
petroleum/solvent odors, a sample will be collected from a 2-ft interval representative of
the potential impacts. If no evidence of potential impacts is observed, soil samples will be
collected from the interval with the highest PID reading or surficial soil. The soil sample
will be submitted for laboratory analysis of SVOCs by EPA Method 8270 and RCRA
metals plus hexavalent chromium by EPA Methods 6020/7471/7199.
• SB-18 and SB-19 will be advanced to a depth of approximately 2 ft bgs in the southeast
portion of the Site to evaluate surficial soils in this area. If field observations indicate
potential impacts in the 0 to 2 ft bgs interval based on elevated PID readings, staining,
and/or petroleum/solvent odors, the boring will be further advanced to a depth indicative
of the bottom of suspected impacts. In such a scenario, a sample will be collected from the
2-ft interval representative of potential impacts. If no evidence of potential impacts is
observed, soil samples will be collected from the 0 to 2 ft bgs interval. The soil samples
will be submitted for laboratory analysis of SVOCs by EPA Method 8270 and RCRA
metals plus hexavalent chromium by EPA Methods 6020/7471/7199.
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In addition to the soil samples described above, two representative grab soil samples will
be collected for analysis of volatile organic compounds (VOCs). Based on the results of
field screening, a grab soil sample will be collected from the aliquot exhibiting the highest
likelihood for impact in each boring. If field screening results do not identify the obvious
presence of impacts in an aliquot soil sample, the grab samples will be collected from the
interval with the highest PID reading. The grab soil samples will be submitted for
laboratory analysis of VOCs by EPA Method 8260.
Soil samples will be placed in dedicated laboratory -supplied sample containers, labeled with the
sample identification, date, and requested analysis, and placed in a laboratory -supplied cooler with
ice. The soil samples will then be submitted to a North Carolina -certified laboratory, Eurofins USA
(Eurofins), under standard chain of custody protocols for analyses as described above. Information
pertaining to Eurofins' certifications and accreditations is provided in Appendix B.
Following sampling activities at each location, including the collection of groundwater samples as
discussed in Sections 3.2 and 3.3, the soil borings will be properly abandoned with soil cuttings
and/or bentonite and the surface will be repaired similarly to pre -sampling conditions.
Additionally, the soil sample locations will be recorded using a hand-held GPS unit.
3.2 Groundwater Assessment Activities
H&H proposes to subcontract with a North Carolina licensed drilling contractor to advance borings
for the installation of two temporary monitoring wells on the 1402 Garner Road property using a
DPT drill rig with auger capabilities. The approximate locations of the proposed temporary
monitoring wells in conjunction with the proposed redevelopment plans are shown on Figure 3,
and are described below:
• TW-3 will be installed downgradient of the suspected UST; and
• TW-4 will be installed adjacent to a former fuel dispenser.
During drilling, soil samples will be collected and logged for lithologic description and field
screened for the presence of staining and elevated concentrations of volatile organic vapors using
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a calibrated PID. The temporary monitoring wells will be constructed of 1-inch diameter PVC
with 10 or 15 ft of pre -pack well screen (due to sampling for metals) set to bracket the water table
(estimated at between approximately 20 to 30 ft bgs) and 1-inch diameter PVC well casing to the
ground surface. A sand filter pack will extend from below the base to approximately 2 ft above
the top of the pre -packed well screens followed by at least 2 ft of hydrated bentonite. The
temporary monitoring well will be developed by removing a minimum of 3 to 5 well volumes and
observing stable field parameters (i.e., pH ± 0.1 SU and conductivity varies no more than 5%).
After development, groundwater samples will be collected from the temporary monitoring wells.
Temporary monitoring wells will be developed at least 24 hours prior to sampling. The locations
of the proposed temporary monitoring wells are depicted in Figure 3.
Prior to purging, depth to groundwater information will be collected for each monitoring well
sampled. A groundwater sample will then be collected utilizing low flow/low stress purging
techniques using a peristaltic pump and disposable polyethylene tubing. The intake point of the
pump tubing will be placed approximately in the mid -portion of the screened interval of the well
and groundwater will be removed at a rate no greater than 200 milliliters per minute. H&H will
utilize a water quality meter to measure pH, temperature, dissolved oxygen, oxidation reduction
potential, turbidity, and specific conductivity at 3 to 5-minute intervals during purging. Purging
will be considered complete when water quality parameters stabilize (i.e., pH ± 0.1 SU,
conductivity varies no more than 5%, and turbidity is less than 10 NTUs).
Once groundwater parameters stabilize, a groundwater sample from each monitoring well will be
collected directly into laboratory supplied sample containers. VOC samples will be collected using
the "soda straw" method to minimize volatile loss through the peristaltic pump head. Specifically,
sample tubing will be removed from the well and used to fill the sample containers by reversing
the flow direction of the peristaltic pump. The sample containers will be labeled with the sample
identification, date, and requested analysis, and then placed in a laboratory supplied cooler and
iced. The groundwater samples will be delivered to Eurofins under standard chain of custody
protocols for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA
metals by EPA Methods 6020/7471. Table 1 summarizes the proposed groundwater samples
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rationale and associated analyses. Information pertaining to Eurofins' certifications and
accreditations is provided in Appendix B.
Upon completion of groundwater sampling activities, the wells will be properly abandoned by a
licensed well driller and the ground surfaces will be repaired to generally match pre -drilling
conditions. The groundwater sample locations will be recorded in the field using a hand-held GPS
unit.
3.3 Vapor Intrusion Assessment Activities
H&H proposes to conduct sub -slab and exterior soil gas assessment activities to evaluate the
potential for structural vapor intrusion into the future senior living apartment building. The
approximate locations of the proposed sub -slab gas samples and exterior soil gas samples in
conjunction with the proposed redevelopment plan are shown on Figure 3, and are described
below:
• Four sub -slab gas samples (SS-5 through SS-8) will be collected from the existing Site
buildings within the footprint of the proposed apartment building;
• One exterior soil gas sample (SG-1) will be collected within the southeastern footprint of
the proposed apartment building; and
• Three exterior soil gas samples (SG-2 through SG-4) will be collected within the central
and western footprints of the proposed apartment building.
H&H proposes to install each sub -slab gas monitoring point by using a hammer drill and 5/8-inch
diameter decontaminated drill bit to advance the boring through the concrete slab. Slab thicknesses
and sub -slab materials (i.e., soil, gravel, etc.) will be documented at each location. Following
concrete borehole advancement, loose concrete cuttings will be removed from the boring using a
bottlebrush and vacuum with a high -efficiency particulate air (HEPA) filter. A Cox -Colvin Vapor
PinTM (vapor pin) assembly (brass sampling point and silicone sleeve) will be seated in the
borehole using an installation/extraction tool and hammer. The vapor pin will be connected at the
surface with'/4-inch new and dedicated Teflon® tubing and will be installed as temporary sub -slab
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gas points. Sample points will be allowed to equilibrate for at least two hours following
installation.
H&H proposes to install each exterior soil gas point to a depth of approximately 5.5 ft bgs using a
decontaminated stainless steel hand auger. The exterior soil gas points will each be installed with
a 6-inch long 0.010-inch slot stainless steel screen set at the base of the boring connected to the
surface with'/4-inch new and dedicated Teflon® tubing. The annular space will be filled with filter
sand followed by a bentonite seal to prevent short-circuiting of air from the surface. The exterior
soil gas points will be installed as temporary points and will be allowed to equilibrate for a
minimum of 48 hours after installation and prior to sample collection described below.
Prior to vapor sampling activities, a leak check will be conducted by constructing a shroud around
the sample train at each exterior soil gas and sub -slab gas sampling point and flooding the air with
helium gas. Helium concentrations inside the shroud will be measured using a calibrated helium
gas detector and maintained at concentrations of approximately 10% to 20% for the duration of
the leak check. Using a syringe and three-way valve, a minimum of three sample train volumes
(including both the tubing and annulus) will be purged at a maximum flow rate of 200 mL/min,
and a sample will be collected from the sample tubing outside the shroud into a Tedlar bag and
analyzed using the helium gas detector to ensure that helium concentrations are less than 10% of
the helium concentrations measured within the shroud. Note that the helium meter will not be
connected to the sampling train, as it is used independently to measure helium within the shroud
and from a Tedlar bag that is connected to the sampling train.
Following a successful leak check, the samples will be collected using batch -certified 1-liter or 3-
liter stainless steel Summa® canisters connected to an air -flow regulator calibrated by the
laboratory for collection of a sample at a rate of up to approximately 200 milliliters per minute.
To conduct the sampling, the intake valve on the Summa® canister will be fully opened to begin
collection of the sample and vacuum readings on the Summa® canister will be recorded prior to
and following the sampling period to ensure adequate sample volume was collected. A vacuum
will be maintained within the canisters at the conclusion of the sampling event, and vacuum
measurements which include pre- and post -sampling, and sample collection time durations will be
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recorded on the chain -of -custody. Canisters that have lost greater than 10% of their vacuum as
determined by comparing the vacuum recorded by the laboratory prior to shipment and the vacuum
recorded in the field during the leak test procedures will not be used for sampling. In addition, a
minimum of vacuum of five inches of mercury will be maintained on the sample canisters until
the conclusion of the sampling event.
After sample collection, the intake valve will be closed, and the regulator will be disconnected
from the sample canister. The canisters will be placed in laboratory supplied shipping containers,
properly labeled, and shipped under standard chain -of -custody protocols to Eurofins — Air Toxics
for analysis of VOCs by EPA Method TO-15. Table 1 summarizes the proposed sub -slab gas and
exterior soil gas samples and associated analyses. Information pertaining to Eurofins'
certifications and accreditations for TO-15 in New Jersey (North Carolina does not provide TO-15
certifications) is provided in Appendix B.
Upon completion of sampling activities, exterior soil gas and sub -slab gas point locations will be
recorded in the field using a hand-held GPS unit. The exterior soil gas and sub -slab gas points
will then be properly abandoned and surfaces will be repaired to generally match pre -sampling
conditions.
13 44
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4.0 Quality Assurance/Quality Control Samples
Non -dedicated equipment and tools will be decontaminated prior to use at each boring or sampling
location or following exposure to soil, soil gas, sub -slab gas, and/or groundwater samples.
Decontamination of non -dedicated equipment will follow U.S. EPA Region IV guidance
(LSASDPROC-205-R4) and will consist of wiping the equipment clean, a water -rinse of the
equipment, washing the equipment in water and detergent (i.e., Liquinox(v or Luminox®), and a
final rinse with water. The process will be repeated for grossly contaminated non -dedicated
equipment.
For quality assurance and quality control purposes (QA/QC), and to evaluate the reproducibility
of the sample results, H&H will collect the following: 1) one duplicate soil sample; 2) one
duplicate groundwater sample; 3) one duplicate exterior soil gas and one duplicate sub -slab gas
sample. The duplicate samples will be submitted for the same laboratory analysis as their
respective parent samples. For the duplicate soil gas/sub-slab gas samples, H&H will utilize a
laboratory -supplied "T-sampler" which allows for the collection of two samples from the same
location simultaneously. Per laboratory standard operating procedures, a vacuum of
approximately five inches of mercury will be maintained within all canisters at the conclusion of
the sampling event. In addition, one laboratory -provided trip blank sample will be included for
every cooler/shipment containing groundwater samples for VOC analysis.
Laboratory QA/QC procedures will be employed to ensure appropriate sample handling and
analysis and to aid in the review and validation of the analytical data. QA/QC procedures will be
conducted in accordance with the method protocols and will include regular equipment
maintenance, equipment calibrations, and adherence to specific sample custody and data
management procedures. Samples will be analyzed in conjunction with appropriate blanks,
laboratory duplicates, continuing calibration standards, surrogate standards, and matrix spiking
standards in accordance with approved methodologies to monitor both instrument and analyst
performance. Laboratory reporting limits for each analyte will be at or below appropriate
screening criteria, where possible. Additionally, H&H will request that the laboratory include
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SMARTER ENVIRONMENTAL 50LUMM

estimated concentrations for compounds that are detected at levels above the laboratory method
detection limit, but below the laboratory reporting limit (i.e., J flags).
The laboratory analytical data report and QA package for each group of samples submitted to and
analyzed by the subcontracted laboratory will be provided in an appendix to the final report.
Laboratory QA data consistent with Level II documentation will be requested for this project. A
copy of the completed chain -of -custody record and shipping receipt will be appended to the
corresponding laboratory analytical report included with the final report.
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5.0 Investigation Derived Waste (IDW)
Investigation derived waste (IDW) generated during the assessment activities will be thin spread
on -Site. However, if significant impacts are suspected (i.e., high PID readings, free -product, etc.),
the soil cuttings and generated groundwater will be containerized in 55-gallon drums and staged
on -Site pending analytical results of composite IDW samples.
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6.0 Reporting
Following completion of the assessment activities and receipt of the analytical data, H&H will
document our findings in a Brownfields Assessment Report. The report will include a description
of the sampling activities, pertinent figures (with appropriate graphic scale and north arrow)
depicting sample locations, tabulated sample data (reported to less than the reporting limit and
compared to applicable regulatory screening levels), soil boring logs (including sub -slab gas and
soil gas monitoring points), laboratory analytical data, a discussion of the data in comparison to
applicable regulatory screening levels with notes where the reporting limit exceeds the regulatory
screening level, risk calculations, IDW manifests (if applicable), and conclusions and
recommendations concerning our activities. The report will be sealed by a North Carolina
Professional Engineer (PE) or Licensed Geologist (LG) and the firm PE/LG numbers will be
provided.
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SMARTER ENVIRONMENTAL 5OLUT1OM

Table

Table 1
Proposed Sampling Plan
Hoke Street Passage Home
500 & 506 Hoke Street and
1402 & 1412 Garner Road
Raleigh, North Carolina
H&H Job No. APT-001
Sample ID
Sample Depth
(ft bgs)
Sample Objective
Analyses
VOCs
SVOCs
RCRA Metals
Hexavalent Chromium
EPA 8260D
EPA TO-15
EPA 8270E
EPA 6020/7470/7471
EPA 7199
Soil Samples
SB-16/TW-3
_5
Downgradient of the suspect UST and within the footprint of the
proposed apartment building
X (Grab)
X
X
X
SB-17/TW-4
—5
South of the former fuel dispenser island
X (Grab)
X
X
X
SB-18
—2
Surficial soil in the southeast portion of the Site
X (Grab)
X
X
X
SB-19
—2
X (Grab)
X
X
X
Field Duplicate
TBD
QA/QC
X (Grab)
X
X
X
Groundwater Samples
TW-3/SB-16
—20-30
Downgradient of the suspect UST and within the footprint of the
proposed apartment building
X
X
X
TW-4/SB-17
--20-30
South of the former fuel dispenser island
X
X
X
Field Duplicate
TBD
QA/QC
X
X
X
Trip Blank
N/A
X
Soil Gas and Sub -Slab Gas Samples
SS-5
—0.5
Within the footprint of the proposed apartment building and existing
onsite buildings
X
SS-6
—0.5
X
SS-7
—0.5
X
SS-8
—0.5
X
SG-1
—5.5
Within the footprint of the proposed apartment building
X
SG-2
—5.5
X
SG-3
—5.5
X
SG-4
—5.5
X
Field Duplicates
TBD
QA/QC
2X
TOTAL SOIL, GROUNDWATER, SOIL GAS, SUB -SLAB GAS, AND QA/QC SAMPLESI
9
1 10
8
8
5
Notes:
VOCs = volatile organic compounds; SVOCs = semi -volatile organic compounds; RCRA = Resource Conservation and Recovery Act
TBD = parent sample to be determined; QA/QC = quality assurance/quality control; ft bgs = feet below ground surface; N/A = not applicable
Table 1 (Page 1 of 1)
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11/28/2022 Hart & Hickman, PC

Figures

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Centers for Environmental Information, U.S. Coastal Relief Model. Data
refreshed August, 2021.
TITLE
SITE LOCATION MAP
1 0 2,000 4,000
N PROJECT HOKE STREET PASSAGE HOME
= SCALE IN FEET 500 & 506 HOKE STREET
1402 & 1412 GARNER ROAD
RALEIGH, NORTH CAROLINA
3 U.S.G.S. QUADRANGLE MAP 3921 Sunset Ridge Road, Suite301
hart ""+ h iC k m a n Raleigh, North Carolina 27607
RALEIGH WEST, NORTH CAROLINA2019 9i ense#C-1��919--245 e (�
SMARTER Er1VIRdP7 hRENgAL SOLIJTlONS License # C-1269 / # C-245 Geology
3 QUADRANGLE DATE: 8-23-22 REVISION NO: 0
7.5 MINUTE SERIES (TOPOGRAPHIC) JOB NO: APT-001 FIGURE NO: 1

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2. BASE DATA OBTAINED FROM WAKE COUNTY GIS, 2022.
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FRUJECT
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500 & 506 HOKE STREET,
1402 & 1412 GARNER ROAD
RALEIGH, NORTH CAROLINA
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+ hart "� h i c k m a n Raleigh, North Carolina 27607
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_ SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 8-23-22 REVISION NO. 0
+.bit
JOB NO. APT-001 FIGURE NO. 2

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` ' SITE PROPERTY BOUNDARY
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(1320 GARNER ROAD)
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• BUILDINGS TO BE DEMOLISHED
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GALATA DESIGNS MW-1/1S WELL TW-1 AND TW-2, AND SOIL BORINGS MW-1S, MW-2S,
(1407 S. BLOODWORTH STREET) MW-3S, AND SB-1 THROUGH SB-15 COMPLETED AND
_ SAMPLED BY PROCTOR ENVIRONMENTAL SERVICES, INC.
JULY THROUGH AUGUST 2016.
e-9 B 7 _ 4. SUB -SLAB SAMPLING CONDUCTED BY RDH
SB-11 B-8 ENVIRONMENTAL CONSULTING OCTOBER 2017.
i MW-4 SB 18 5. INDOOR AND OUTDOOR AIR SAMPLING CONDUCTED BY
SB 7 SB-3 B-10 RDH ENVIRONMENTAL CONSULTING MAY 2018.
3B-4 I 6. SOIL BORINGS B-1 THROUGH B-10 COMPLETED BY APTUS
SB-8 SB-2 MANAGEMENT, PLLC ON MARCH 27, 2018, AND MAY 18,
SB-5 2018.
SB-9 • 7. SAMPLE LOCATIONS BASED UPON HISTORICAL DATA AND
SLINGSHOT COFFEE COMPANY SB 1 SB-10 SB-6 APPROXIMATE FORMER • CONSIDERED APPROXIMATE.
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0 60
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- PROPOSED SAMPLE LOCATION MAP
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SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
% DATE: 11-8-22 REVISION NO. 0
a JOB NO. APT-001 FIGURE NO. 3

Appendix A
Redevelopment Plans

L
VICINITY MAP
NTS
f I L„ Z,Aim
jjmop,
�•r � e I re, I I , r
PROPOSED ACCESS J
r
,A• ` '�.
n HOKE STREET
50' R/w AIM
5' BUILDING SETBACK - - — —
10' PARKING SETBACK — — — — — — — — - — - I.
EXISTING UTILITY 0'
EASEMENT
20'LANDSCAPE!
BUFFER l
I • I ..
0 7 4-STORY BUILDING �+ '
104 UNITS -
I
ASSUMED OWNERSHIP
OF ABANDONED ALLEY'` -- -
y
cy—
F
o�
Q
t +oJj
11 10
8 ` — —
Q' 7
DUMPSTER
SITE AMENITIES ENCLOSURE
INDOOR AND OUTDOOR SITTING AREAS (MIN 3) t1 9 II / l�
I
U
MULTIPURPOSE ROOM
GAZEBO
COVERED DRIVE THIRD ENTRY 9 11
EXERCISE ROOM
RESIDENT COMPUTER CENTER , •�
PROPOSED ACCESS y `
SITE PLAN SUMMARY
PROJECT:
500 HOKE STREET
OWNER:
HOKE STREET PH REDEVELOPMENT LLC
PROJECT ADDRESS:
500 HOKE STREET; RALEIGH, NC
PROPERTY AREA:
4.07 ACRES
PIN #:
1703828886,1703920846,1703920658,1703922815
DEED:
IDS 16684 PG 686, DB 16684 PG 686,
DB 16684 PG 692, DB 16-E PG 16-E
ZONING:
EXISTING: IX-3
PROPOSED: OX4PL
ADJACENT PROPERTY
ZONING:
SOUTH & WEST: IX-3;
NORTH & EAST: R-10
EXISTING USE:
WAREHOUSE, VACANT, SERVICE GARAGE
PROPOSED USE:
104 SENIOR LIVING APARTMENTS
FLOOD ZONE:
NOT LOCATED IN FLOOD HAZARDS AREA PER
FEMA MAP #3720170300J (EFFECTIVE 5/2/2006)
VEHICLE PARKING SUMMARY
REQUIRED BY H
.1.4.B) B)
(UDO SEC 7.1.4
104 UNITS X 1 SPACE =104 SPACES
PROVIDED
118 SPACES (7 ADA)
GAZEBO
—
_
i
� _
—i
ST
CONTROL
CONTROL
- MEASURE
II
_
_
I
r
-y
I
� �M
_
•' •j'' ,
_ 20'LANDSCAPE BUFFER
h ,
hb�
+
`
-
EXISTING UTILITY EASEMENT
F ►
s
— —
• 10' PARKING SETBACK
1�
a
ti
5BUILDING SETBACK
2,685 SF OF RIGHT OF WAY DEDICATION REQUIRED
17•.
�►
NOTES: '
1. THIS PLAN IS CONCEPTUAL IN NATURE AND HAS NOT BEEN REVIEWED BY ANY .i
AGENCY.
2. DESIGN IS SUBJECT TO CHANGE PENDING PERMITTING, GRADING, SEWER AND
STORM WATER DESIGN.
PRELIMINARY SITE LAYOUT
500 Hoke Street - January 19, 2022
�IJ
r
r�i■*��
0
TIMMONS GROUP
ENGINEERING I DESIGN I TECHNOLOGY
s w�zwaacz rn.c•_�om•_�oKasnowc�sn..,�.mm�eeau vzcex,.asiTE a.� i Ao�a on,nazozz �,:.s an i na.a.on sn..,.,

Appendix B
Laboratory Certifications and Accreditations

Certificate No. 269
STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
LABORATORY CERTIFICATION BRANCH
In accordance with the prov
2022
Eurofins Savannah
a)(10) and NCAC 2H.0800:
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DEQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable. -
This certificate shall be valid until 12/31/2022
Todd Crawford

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number: 269
Address: 5102 La Roche Ave. Effective Date: 1/1/2022
Savannah, GA 31404 Expiration Date: 12/31/2022
Date of Last Amendment: 1/1/2022
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANIC
ALKALINITY
SM 2320 B-2011 (Aqueous)
BOD
SM 5210 B-2016 (Aqueous)
CBOD
SM 5210 B-2016 (Aqueous)
CHLORIDE
SM 4500 Cl- E-2011 (Aqueous)
SW-846 9251 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
COD
SM 5220 D-2011 (Aqueous)
EPA 410.4, Rev. 2.0, 1993 (Aqueous)
COLOR, PC
SM 2120 B-2011 (PtCo) (Aqueous)
CONDUCTIVITY
EPA 120.1, Rev. 1982 (Aqueous)
SM 2510 B-2011 (Aqueous)
SW-846 9050 A (Aqueous)
CYANIDE
EPA 335.4, Rev. 1.0, 1993 (Total) (Aqueous)
SW-846 9012 B (Available) (Aqueous)
SW-846 9012 B (Total) (Aqueous)
SW-846 9012 B (Total) (Non -Aqueous)
FLUORIDE
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
HARDNESS TOTAL - METALS
SM 2340 B-2011 (Ca EPA 200.7, Rev. 4.4, 1994 + Mg EPA 200.7, Rev. 4.4, 1994) (Aqueous)
HARDNESS TOTAL - WET CHEM
SM 2340 C-2011 (Aqueous)
IGNITABILITY
SW-846 1030 (Non -Aqueous)
INORGANIC PHENOLS
EPA 420.1, Rev. 1978 (Aqueous)
SW-846 9065 (Aqueous)
NITROGEN, AMMONIA
EPA 350.1, Rev. 2.0, 1993 (Aqueous)
SM 4500 NH3 G-2011 (Aqueous)
NITROGEN, NITRATE
(NO3 + NO2 EPA 353.2, Rev. 2.0, 1993) - (NO2 EPA 353.2, Rev. 2.0, 1993) (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
NITROGEN, NITRITE
EPA 353.2, Rev. 2.0, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
NITROGEN, NO3 + NO2
EPA 353.2, Rev. 2.0, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number:
Address: 5102 La Roche Ave. Effective Date:
Savannah, GA 31404 Expiration Date:
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
NITROGEN, TOTAL KJELDAHL
EPA 351.2, Rev. 2.0, 1993 (Aqueous)
OIL & GREASE
EPA 1664 Rev. B (Aqueous)
ORGANIC CARBON, TOTAL
SM 5310 B-2014 (Combustion) (Aqueous)
SW-846 9060 A (Combustion) (Aqueous)
PAINT FILTER LIQUIDS
SW-846 9095B
pH
SM 4500 H+B-2011 (Aqueous)
SW-846 9040 C (Aqueous)
SW-846 9045 D (Non -Aqueous)
PHOSPHATE,ORTHO
SM 4500 P F-2011 (Aqueous)
EPA 365.1, Rev. 2.0, 1993 (Aqueous)
PHOSPHORUS, TOTAL
EPA 365.4, 1974 (Aqueous)
RESIDUE, DISSOLVED 180 C
SM 2540 C-2015 (Aqueous)
RESIDUE, SETTLEABLE
SM 2540 F-2015 (Aqueous)
RESIDUE, SUSPENDED
SM 2540 D-2015 (Aqueous)
RESIDUE, TOTAL
SM 2540 B-2015 (Aqueous)
SALINITY
SM 2520 B-2011 (Aqueous)
SILICA - METALS
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
SULFATE
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Non -Aqueous)
SW-846 9056 A (Aqueous)
SW-846 9056 A (Non -Aqueous)
SW-846 9038 (Aqueous)
SULFIDE
SM 4500 Sr F-2011 (Aqueous)
SW-846 9034 (Aqueous)
SW-846 9034(Non-Aqueous)
TURBIDITY
EPA 180.1, Rev. 2.0, 1993 (Aqueous)
SM 2130 B-2011 (Aqueous)
METAL
ALUMINUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
ANTIMONY
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
269
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1 /1 /2022
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number:
Address: 5102 La Roche Ave. Effective Date:
Savannah, GA 31404 Expiration Date:
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
ARSENIC
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
BARIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
BERYLLIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
BORON
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
CADMIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
CALCIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
CHROMIUM HEXAVALENT
SM 3500-Cr-B-2011 (Aqueous)
SW-846 7196 A (Aqueous)
SW-846 7196 A (Non -Aqueous)
CHROMIUM TOTAL
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
COBALT
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
269
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1 /1 /2022
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number:
Address: 5102 La Roche Ave. Effective Date:
Savannah, GA 31404 Expiration Date:
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
COPPER
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
IRON
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
LEAD
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
MAGNESIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
MANGANESE
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
MERCURY
EPA 245.1, Rev. 3.0, 1994 (Aqueous)
SW-846 7470 A (Aqueous)
SW-846 7471 B (Non -Aqueous)
MOLYBDENUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
NICKEL
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
POTASSIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
269
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1 /1 /2022
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number:
Address: 5102 La Roche Ave. Effective Date:
Savannah, GA 31404 Expiration Date:
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
SELENIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
SILVER
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
SODIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
STRONTIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
THALLIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
TIN
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
TITANIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
VANADIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
ZINC
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
269
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1 /1 /2022
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Savannah Certificate Number:
Address: 5102 La Roche Ave. Effective Date:
Savannah, GA 31404 Expiration Date:
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6020 B (Non -Aqueous)
ORGANIC
1,2, DIBROMOETHANE (EDB)
EPA 504.1 (Includes DBCP & TCP) (Aqueous)
SW-846 8011 (Includes DBCP) (Aqueous)
ADSORBABLE ORGANIC HALIDES
EPA 1650, Rev. C, 1997 (Aqueous)
BASE NEUTRAL/ACID, ORGANICS
EPA 625.1 (Aqueous)
SW-846 8270 E (Aqueous)
SW-846 8270 E (Non -Aqueous)
CHLORINATED ACID HERBICIDES
EPA 615 (Aqueous)
SW-846 8151 A (Aqueous)
SW-846 8151 A (Non -Aqueous)
PESTICIDES, ORGANOCHLORINE
EPA 608.3 (Aqueous)
SW-846 8081 B (Aqueous)
SW-846 8081 B (Non -Aqueous)
POLYCHLORINATED BIPHENYLS (PCBs)
EPA 608.3 (Aqueous)
SW-846 8082 A (Aqueous)
SW-846 8082 A (Non -Aqueous)
SW-846 8082 A (Oil)
PURGEABLE, ORGANICS
EPA 624.1 (Aqueous)
SM 6200 B-2011 (Aqueous)
SW-846 8260 D (Aqueous)
SW-846 8260 D (Non -Aqueous)
TOTAL ORGANIC HALIDES
SW-846 9020 B (Aqueous)
TPH DIESEL RANGE, ORGANICS
SW-846 8015 C (Aqueous)
SW-846 8015 C (Non -Aqueous)
TPH GASOLINE RANGE, ORGANICS
SW-846 8015 C (Aqueous)
SW-846 8015 C (Non -Aqueous)
269
1 /1 /2022
12/31 /2022
1 /1 /2022
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

STATE OF NORTH CAROLiNA DEPARTMENT OF ENVIRONMENTAL QUALITY
Certificate No. 314
DIVISION OF WATER RESOURCES
LABORATORY CERTIFICATION BRANCH
In accordance with the provisions of N.C.G.S. 143-215.3 (a) (1), 143-215.3 (a)(10) and NCAC 214.0800:
Eurofins Pensacola
is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DEQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until 12/31/2022
Todd Crawford

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Pensacola Certificate Number: 314
Address: 3355 McLemore Drive Effective Date: 1/1/2022
Pensacola, FL 32514 Expiration Date: 12/31/2022
Date of Last Amendment: 9/1/2021
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANIC
ALKALINITY
SM 2320 B-2011 (Aqueous)
BOD
SM 5210 B-2016 (Aqueous)
CBOD
SM 5210 B-2016(Aqueous)
CHLORIDE
SM 4600 Cl- E-2011 (Aqueous)
SW-846 9251 (Aqueous)
COD
SM 5220 D-2011 (Aqueous)
EPA 410.4, Rev. 2.0, 1993 (Aqueous)
COLOR, PC
SM 2120 B-2011 (PtCo) (Aqueous)
CONDUCTIVITY
EPA 120.1, Rev. 1982 (Aqueous)
SM 2510 B-2011 (Aqueous)
SW-846 9050 A (Aqueous)
CYANIDE
SW-846 9014 (Available) (Colorimetric) (Non -Aqueous)
SM 4500 CN- D-2016 (Total) (Aqueous)
SM 4500 CN- E-2016 (Total) (Non -Aqueous)
FLASH POINT
SW-846 1010 B (D93-80) (Aqueous)
FLUORIDE
SM 4500 F- C-2011 (Aqueous)
HARDNESS TOTAL - METALS
SM 2340 B-2011 (Ca EPA 200.7, Rev. 4.4, 1994 + Mg EPA 200.7, Rev. 4.4, 1994) (Aqueous)
NITROGEN, AMMONIA
EPA 350.1, Rev. 2.0, 1993 (Aqueous)
SM 4500 NH3 H-2011 (Aqueous)
NITROGEN, NITRATE
(NO3 + NO2 SM 4500-NO3- F-2016) - (NO2 SM 4500-NO2- B-2011) (Aqueous)
NITROGEN, NITRITE
SM 4500-NO2- B-2011 (Automated) (Aqueous)
NITROGEN, NO3 + NO2
SM 4500 NO3- F-2016 (Aqueous)
EPA 353.2, Rev. 2.0, 1993 (Aqueous)
NITROGEN, TOTAL KJELDAHL
EPA 351.2, Rev. 2.0, 1993 (Aqueous)
OIL & GREASE
EPA 1664 Rev. B (Aqueous)
SW-846 9071 B (Non -Aqueous)
ORGANIC CARBON, TOTAL
SM 5310 B-2014 (Combustion) (Aqueous)
SW-846 9060 A (Heated Persulfate) (Aqueous)
PAINT FILTER LIQUIDS
SW-846 9095B
pH
SM 4500 H+B-2011 (Aqueous)
SW-846 9040 C (Aqueous)
SW-846 9045 D (Non -Aqueous)
PHOSPHATE,ORTHO
EPA 365.1, Rev. 2.0, 1993 (Aqueous)
PHOSPHORUS, TOTAL
EPA 365.4, 1974 (Aqueous)
RESIDUE, DISSOLVED 180 C
SM 2540 C-2015(Aqueous)
RESIDUE, SETTLEABLE
SM 2540 F-2015 (Aqueous)
RESIDUE, SUSPENDED
SM 2540 D-2015 (Aqueous)
SILICA - METALS
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
SULFATE
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions
as set forth in 15A NCAC 21-1.0807

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Pensacola Certificate Number:
314
Address: 3355 McLemore Drive Effective Date:
1/1/2022
Pensacola, FL 32514 Expiration Date:
12/31/2022
Date of Last Amendment:
9/1/2021
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
SM 4500 SO42 E-2011 (Aqueous)
SW-846 9038 (Aqueous)
METAL
ALUMINUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
ANTIMONY
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
ARSENIC
EPA 200.7. Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
BARIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
BERYLLIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
BORON
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
CADMIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
CALCIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
CHROMIUM HEXAVALENT
SM 3500-Cr-B-2011 (Aqueous)
SW-846 7196 A (Aqueous)
CHROMIUM TOTAL
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
COBALT
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
COPPER
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
IRON
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
LEAD
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
LITHIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
MAGNESIUM
EPA 200.7, Rev. 4A, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
MANGANESE
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2K0807

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Pensacola
Certificate Number: 314
Address: 3355 McLemore Drive
Effective Date: 1/1/2022
Pensacola, FL 32514
Expiration Date: 12/31/2022
Date of Last Amendment: 9/1/2021
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800,
is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
SW-846 6010 D (Aqueous)
THALLIUM
SW-846 6010 D (Non -Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
MERCURY
SW-846 6010 D (Aqueous)
EPA 245.1, Rev. 3.0, 1994 (Aqueous)
SW-846 6010 D (Non -Aqueous)
SW-846 7470 A (Aqueous)
TIN
SW-846 7471 B (Non -Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 1631 E (Aqueous)
SW-846 6010 D (Aqueous)
MOLYBDENUM
SW-846 6010 D (Non -Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
TITANIUM
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Non -Aqueous)
VANADIUM
NICKEL
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.71 Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
SW-846 6010 D (Non -Aqueous)
ZINC
POTASSIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Non -Aqueous)
SW-846 6010 D (Non -Aqueous)
ORGANIC
SELENIUM
1,2, DIBROMOETHANE (EDB)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 504.1 (Includes DBCP & TCP) (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 8011 (Includes DBCP) (Aqueous)
SW-846 6010 D (Non -Aqueous)
BASE NEUTRAL/ACID. ORGANICS
SILVER
EPA 625.1 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 8270 E (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 8270 E (Non -Aqueous)
SW-846 6010 D (Non -Aqueous)
CHLORINATED ACID HERBICIDES
SODIUM
SW-846 8151 A (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 8151 A (Non -Aqueous)
SW-846 6010 D (Aqueous)
EXTRACTABLE PETROLEUM HYDROCARBONS
SW-846 6010 D (Non -Aqueous)
MADEP, December 2019, Rev. 2.1 (Aqueous)
STRONTIUM
MADEP, December 2019, Rev. 2.1 (Non -Aqueous)
SW-846 6010 D (Aqueous)
NONHALOGENATED VOLATILE, ORGANICS
SW-846 6010 D (Non -Aqueous)
SW-846 8015 C (Aqueous)
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subjectto civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Eurofins Pensacola
Address: 3355 McLemore Drive
Pensacola, FL 32514
The above named laboratory, having duly met the requirements of 15A NCAC 211.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
SW-846 8015 C (Non -Aqueous)
PESTICIDES, ORGANOCHLORINE
EPA 608.3 (Aqueous)
SW-846 8081 B (Aqueous)
SW-846 8081 B (Non -Aqueous)
POLYCHLORINATED BIPHENYLS (PCBs)
EPA 608.3 (Aqueous)
SW-846 8082 A (Aqueous)
SW-846 8082 A (Non -Aqueous)
SW-846 8082 A (Oil)
PURGEABLE, ORGANICS
EPA 624.1 (Aqueous)
SM 6200 B-2011 (Aqueous)
SW-846 8260 D (Aqueous)
SW-846 8260 D (Non -Aqueous)
TPH DIESEL RANGE, ORGANICS
SW-846 8015 C (Aqueous)
SW-846 8015 C (Non -Aqueous)
TPH GASOLINE RANGE, ORGANICS
SW-846 8015 C (Aqueous)
SW-846 8015 C (Non -Aqueous)
VOLATILE PETROLEUM HYDROCARBONS
MADEP, Feb 2018, Rev. 2.1 (Aqueous)
MADEP, Feb 2018, Rev. 2.1 (Non -Aqueous)
Certificate Number:
314
Effective Date:
1/1/2022
Expiration Date:
12/31/2022
Date of Last Amendment:
9/1/2021
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.

State of New Jersey
Department of Environmental Protection
Certifies That
EUROFINS AIR TOXICS
Laboratory Certification ID # CA016
is hereby approved as a
Nationally Accredited Environmental Laboratory
to perform the analyses as indicated on the Annual Certified Parameter List
which must accompany this certificate to be valid
having duly met the requirements of the
Regulations Governing the Certification of
Laboratories and Environmental Measurements N.J.A.C. 7:18 et. seq.
and
having been found compliant with the 2016 TNI Standard approved by the
The NELAC Institute
Expires June 30, 2023
4mawv
Michele M. Potter
Manager
NJDEP is a NELAP Recognized Accreditation Body
wt, cei uucete is �a ❑e wnspccuousiy aispjayea at ine laooratory wrtn me annual cerrnhed parameter list in a location on the premises visible to the public. Consumers are urged to verify the laboratory's current accreditation
status with the State of NJ, NELAP.

New Jersey Department of Environment Protection
--
Environmental Laboratory Certification Program Oe aEco Q*".
Annual Certified Parameter List and Current Status
Effective as of 07/01/2022 until 6/30/2023 5w_w
Laboratory Name: EUROFINS AIR TOXICS Laboratory Number: CA016 Activity ID: NLC 220001
180 BLUE RAVINE RD-STE B
FOLSOM CA 95630
Category: AE04 --Organics Analysis
Eligible to
Status
Report NJ
Code
Parameter
Technique
4
Approved Methods
Primary
Data
State
Certified
Yes
AE04.14000
Acenaphthene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14050
Acenaphthylene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14100
Anthracene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14150
Benzo(a)anthracene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14200
Benzo(a)pyrene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14250
Ben zo(b)fluoranthene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04,14300
Benzo(ghi)perylene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14350
Benzo(k)fluoranthene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14450
Chrysene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14550
Dibenzo(a,h)anth race ne
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14600
Fluoranthene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14650
Flucrene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14700
Indeno(1,2,3-cd)pyrene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14750
Naphthalene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14850
Phenanthrene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04.14900
Pyrene
GCIMS
EPA TO-13A
OR
Certified
Yes
AE04,17950
Acetone
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04A8100
Acrolefn
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04,18300
Allyt chloride
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04.18400
Benzone
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04.18450
Benzyl chloride
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04,18600
Bromodichloromethane
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04.18650
Bromoform
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04,18700
Bromomethane
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04,18750
Butadiene (1,3-)
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04.18900
Carbon disulfide
GCIMS, Canisters
EPA TO-15
OR
Certified
Yes
AE04.19000
Carbon tetrachloride
GCIMS, Canisters
EPA TO-15
OR
KEY: AE = Air and Emissions, BT = Biological Tissues, DW = Drinking Water, NPW = Non -Potable Water, SCM = Solid and Chemical Materials Pagel of 6

New Jersey Department of Environment Protection
Environmental Laboratory Certification Program
Annual Certified Parameter List and Current Status
Effective as of 07101/2022 until 6/30/2023
Laboratory Name: EUROFINS AIR TOXICS
Laboratory Number: CA016 Activity ID: NLC 220001
180 SLUE RAVINE RD-STE B
FOLSOM CA 95630
Category: AE04 --Organics Analysis
Eligible to
Status Report NJ Code
Parameter Technique
Data
Certified Yes AE04.19150
Chlorobenzene GCIMS, Canisters
Certified Yes AE04.19200
Chloroethane GCIMS, Canisters
Certified Yes AE04.19250
Chloroform GCIMS, Canisters
Certified Yes AE04,19300
Chloromethane GCIMS, Canisters
Certified Yes AE04.19500
Cyclohexane GCIMS, Canisters
Certified Yes AE04.19650
Dibromochloromethane GCIMS, Canisters
Certified Yes AE04.19700
Dibromoethane (1,2-) GCIMS, Canisters
(EDS)
Certified
Yes
AE04.19750
Dichlorobenzene (1,2-)
Certified
Yes
AE04.19800
Dichlorobenzene (1,3-)
Certified
Yes
AE04.19850
❑ichlorobenzene(1,4-)
Certified
Yes
AE04.19900
pichlorodifluoromethane
Certified
Yes
AE04.19950
Dichloroethane (1,1-)
Certified
Yes
AE04.20D00
Dichloroethane (1,2-)
Certified
Yes
AE04.20050
❑icNoroethene (1,1-)
Certified
Yes
AE04.20100
Dichloroethene (cis-1,2-)
Certified
Yes
AE04.20150
Dichloroethene
(trans-1,2-)
Certified
Yes
AE04,20250
Dichloropropane (1,2-)
Certified
Yes
AE04.20300
Dichloropropene
(cis-1,3-)
Certified
Yes
AE04,20350
Dichloropropene
(trans-1.3-)
Certified
Yes
AE04.20400
Dichlorotetrafluoroethane
(1,2-)
Certified
Yes
AE04.20750
Dioxane (1,4-)
Certified
Yes
AE04.20900
Ethanol
Certified
Yes
AE04,21100
Ethylbenzene
Certified
Yes
AE04.21250
Ethyltoluene (4-)
Approved Methods
EPA TO-15
EPA TO-15
EPA TO-15
EPA TO-15
EPA TO-15
EPA TO-15
EPA TO-15
Ap REcvG4,
Primary
State
OR
OR
OR
OR
OR
OR
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
KEY: AE = Air and Emissions, BT = Biological Tissues, DW = Drinking Water, NPW = Non -Potable Water, SCM = Solid and Chemical Materials Page 2 of 6

New Jersey Department of Environment Protection
Environmental Laboratory Certification Program
Annual Certified Parameter
List and Current Status
Effective as of
07/01/2022 until 6/3012023
Laboratory Name: EUROFINS
AIR TOXICS
Laboratory Number: CA016
Activity ID- NLC 220001
180 BLUE RAVINE RD-STE B
FOLSOM
CA 95630
Category:
AE04 --Organics Analysis
Eligible to
Status
Report NJ
Code
Parameter
Technique
Data
Certified
Yes
AE04.21400
Heptane (n-)
GCIMS, Canisters
Certified
Yes
AE04.21450
Hexachlorobutadiene
GCIMS, Canisters
(1,3-)
Certified
Yes
AE04.21550
Hexane (n-)
GCIMS, Canisters
Certified
Yes
AE04.21600
Hexanone (2-)
GCIMS, Canisters
Certified
Yes
AE04,21700
Isopropanol
GCIMS, Canisters
Certified
Yes
AE04.21750
Isopropylbenzene
GCIMS, Canisters
Certified
Yes
AE04.21850
Methyl ethyl ketone
GCIMS, Canisters
(MEK)
Certified
Yes
AE04.21950
Methyl isobutyl ketone
GCIMS, Canisters
(MIBK)
Certified
Yes
AE04.22100
Methyl tert-butyl elher
GCIMS, Canisters
Certified
Yes
AE04.22150
Methylene chloride
GCIMS, Canisters
(Dichlaromethane)
Certified
Yes
AE04.22300
Naphthalene
GCIMS, Canisters
Certified
Yes
AE04.22850
Propylbenzene (n-)
GCIMS, Canisters
Certified
Yes
AE04.22950
Propylene
GCIMS, Canisters
Certified
Yes
AE04.23150
Styrene
GCIMS, Canisters
Certified
Yes
AE04.23350
Tetrachloroelhane
GCIMS, Canisters
(1,1,2,2-)
Certified
Yes
AE04.23400
Tetrachloroethene
GCIMS, Canisters
Certified
Yes
AE04.23450
Tetrahydrofuran
GCIMS, Canisters
Certified
Yes
AE04,23500
Toluene
GCIMS, Canisters
Certified
Yes
AE04.23550
Trichloro (1,1.2-)
GCIMS, Canisters
trifluorcethane (1,2,2-)
Certified
Yes
AE04.23600
Trichlorobenzene (1,2,4-)
GCIMS, Canisters
Certified
Yes
AE04.23650
Trichloroethane (1,1,1-)
GCIMS, Canisters
Certified
Yes
AE04.23700
Tdchloroethane (1,1,2-)
GCIMS, Canisters
Certified
Yes
AE04.23750
Trichloroethene
GCIMS, Canisters
Certified
Yes
AE04.23800
Trichlorofluoromethane
GCIMS, Canisters
_.Ap4ECp�
'j
Approved Methods
Primary
State
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
EPA TO-15
OR
KEY: AE = Air and Emissions, BT s Biological Tissues, DW = Drinking Water, NPW = Non -Potable Water, SCM = Solid and Chemical Materials Page 3 of 6

New Jersey Department of Environment Protection
Environmental Laboratory Certification Program
Annual Certified Parameter List and Current Status
Effective as of 07/01/2022 until 6/3012023
Laboratory Name: EUROFINS AIR TOXICS Laboratory Number: CA016 Activity ID: NLC 220001
180 BLUE RAVINE RD-STE B
FOLSOM CA 95630
Category: AE04 --Organics Analysis
Eligible to
Status Report NJ Code
Data
Certified Yes AE04.24050
Certified
Yes
AE04.24100
Certified
Yes
AE04.24150
Certified
Yes
AE04.24200
Certified
Yes
AE04.24300
Certified
Yes
AE04.24400
Certified
Yes
AE04,24500
Certified
Yes
AE04.24600
Certified
Yes
AE04,24650
Certified
Yes
AE04.25000
Certified
Yes
AE04,25050
Certifted
Yes
AE04.25350
Certified
Yes
AE04.25750
Certified
Yes
AE04,25800
Certified
Yes
AE04.25650
Certified
Yes
AE04.25900
Certified
Yes
AE04.25950
Certified
Yes
AE04.26100
Certified
Yes
AE04.26350
Certified
Yes
AE04,26400
Certified
Yes
AE04.26450
Certified
Yes
AE04.26550
Certified
Yes
AE04.26600
Certified
Yes
AE04.26650
Certified
Yes
AE04.26700
Certified
Yes
AE04.26750
Parameter
Trimethylbenzene
(1,2,4-)
Trimethylbenzene
(1,3,5-)
Trimethylpentane (2,2,4-)
Vinyl acetate
Vinyl chloride
Xylene (o-)
Xylenes (total)
Acenaphthene
Acenaphthylene
Anthracene
Benzene
Butadiene (1,3-)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethare
Chloroform
Cyclohexane
Dichlorobenzene (1,2-)
Dichlorobenzene (1,3-)
Dichlorobenzene (1,4-)
Dichloroethane (1,1-)
Dichloroethane (1,2-)
Dichloroethene (1,1-)
Dichloroethene (cis-1,2-)
Dichloroethene
(trans-1,2-)
"gip 4lECOC�.
V
�wNa
Technique
Approved Methods
Primary
State
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Canisters
EPA TO-15
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS. Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
KEY: AE M Air and Emissions, BT = Biological Tissues, DW = Drinking Water, NPW = Non -Potable Water. SCM = Solid and Chemical Materials Page 4 of 6

New Jersey Department of Environment Protection
Environmental Laboratory Certification Program
Annual Certified Parameter List and Current Status
Effective as of 07/01/2022 until 6/30/2023
Laboratory Name: EUROFINS AIR TOXICS Laboratory Number: CA016 Activity ID: NLC 220001
180 BLUE RAVINE RD-STE B
FOLSOM CA 95630
Category: AE04 --Organics Analysis
Eligible to
Status Report NJ Code
Data
Certified Yes AE04.26800
Certified Yes AE04 26950
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Certified
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
AED4.27000
AE04.27350
AE04.27500
AE04.27550
AE04.27600
AE04.27700
AE04.27750
AE04.27800
AE04.27850
AE04.28000
AE04.28100
AE04.28200
AE04.28550
AE04.28600
AE04.28700
AE04.28750
AE04.28800
AE04.28850
AE04,28900
AE04.29000
AE04.29300
Parameter
Dichloropropane (1,2-)
Dichlorotetrafluoroethane
(1,2-)
Dioxane (1,4-)
Ethylbenzene
Ethylbenzene (1-
methyl-4-) [Ethy[toluene
(4-)]
Fluoranthene
Fluorene
Heptane (n-)
Hexachlorobutadiene
(1,3-)
Hexane (n-)
Hexanone (2-)
isopentane
Isopropanot
Isopropylbenzene
Methyl ethyl ketone
(MEK)
Methyl isobutyl ketone
(MIRK)
Methyl tert-butyl ether
Methylcyclohexane
Methylene chloride
(Dichloromethane)
Methyl naphthalene (1-)
Methylnaphthalene (2-)
Naphthalene
Phenanthrene
Technique
GC/MS, Sorbent Tubes
GCIMS, Sorbent Tubes
GCIMS, Sorbent Tubes
GCIMS, Sorbent Tubes
GCIMS, Sorbent Tubes
Approved Methods
EPA TO-17
EPA TO-17
EPA TO-17
EPA TO-17
EPA TO-17
Primary
State
OR
OR
OR
OR
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
KEY: AE = Air and Emissions, BT = Biological Tissues, DW = Drinking Water, NPW = Non -Potable Water, SCM = Solid and Chemical Materials Page 5 of 6

New Jersey Department of Environment Protection
Environmental Laboratory Certification Program
Annual Certified Parameter List and Current Status
Effective as of 07/01/2022 until 6/3012023
Laboratory Name: EUROFINS AIR TOXICS Laboratory Number: CA016 Activity Ib: NLC 220001
180 BLUE RAVINE RD-STE B
FOLSOM CA 95630
Category: AE04 --Organics Analysis
Status
Certified
Certified
Certified
Certified
Certified
Certified
Eligible to
Report NJ
Data
Yes
Yes
Yes
Yes
Yes
Yes
Code
AE04.29550
AE04.29650
AE04.29750
AE04.29900
AE04.29950
AE04,30000
Certified
Yes
AE04.30050
Certified
Yes
AE04.30100
Certified
Yes
AE04.30150
Certified
Yes
AE04.30200
Certified
Yes
AE04.30250
Certified
Yes
AE04.30350
Certified
Yes
AE04.30400
Certified
Yes
AE04.30450
Certified
Yes
AE04.30600
Certified
Yes
AE04.30650
Certified
Yes
AE04.30700
Certified
Yes
AE04.30750
Parameter Technique
Propylbenzene (n-)
Pyrene
Styrene
Tetrachloroethene
Toluene
Trichtoro (1,1,2-)
trifluoroethane (1,2,2-)
Trichlorobenzene (1,2,4-)
Trichloroethane
Trichloroethane (1,1,2-)
Trichloroethene
Trichlorofluoromethane
Trimethylbenzene
(1,2,4-)
Trimethyibenzene
(1,3,5-)
Trimethylpentane (2,2,4-)
Vinyl chloride
Xylene (m- + p-)
Xylene (o-)
Xylenes (total)
Approved Methods
RECO
10W
Primary
State
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO.17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
GCIMS, Sorbent Tubes
EPA TO-17
OR
Michele M. Potter, Manager
KEY: AE = Air and Emissions, BT = Biological Tissues, OW = drinking Water, NPW = Non -Potable Water, SCM = Solid and Chemical Materials Page 6 of 6