06001_Alamac Lumberton_FinalAWP_20231106

envirDl I
Environmental Services
October 31, 2023
NC Department of Environmental Quality
Division of Waste Management
Brownfields Program
217 West Jones Street
Raleigh, North Carolina 27603
Reference: Work Plan for Evaluation of a Requested Pause of the Groundwater
Treatment System
Alamac American Site
1885 Alamac Road
Lumberton, North Carolina 28358
Brownfields No. 06001-02-78
EnviroTrac Ltd. has been contracted as a Registered Environmental Consultant (REC) by
Verdantas, LLC to review work prepared for the referenced site. I have reviewed the enclosed
work plan and supporting documents and believe that the information contained herein is, to the
best of my knowledge, true, accurate, and complete and complies with the Inactive Hazardous
Response Act N.C.G.S. 130A-310, et seq, and the remedial action program Rules 15A NCAC
13C .0300. Should you have any questions regarding this information, please do not hesitate to
contact the undersigned.
ENVIROTRAC LTD.
Lw�
Christopher %ay, El, RSM
Principal
7343 West Friendly Avenue, Suite J, Greensboro, NC 27410 [phone] Fax: [phone]
www.envirotrac.com
Offices in CT, FL, GA, MA, NC, NH, NJ, NY,, OH, PA, VA, WV

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NORTH CAROLINA DEQ BROWNFIELDS PROGRAM
WORK PLAN FOR EVALUATION OF A REQUESTED PAUSE
OF THE GROUNDWATER TREATMENT SYSTEM
Alamac American Site
Brownfields No. 06001-02-78
1885 Alamac Road
Lumberton, North Carolina 28358
October 2023
Revision No. 2
Prepared for:
NC Department of Environmental Quality
Division of Waste Management
Brownfields Program
217 West Jones Street
Raleigh, NC 27603 _
Prepared by:
Verdantas LLC
4 Hemisphere Way
Prepared on Behalf of:
Phoenix Investors LLC (Owner)
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Borton Lawson American Engineering, PC NC PE Firm License No. C-4805
Document Number: 15104.0014

October 2023 verdantas
Document Number 15104.0014
TABLE OF CONTENTS
SECTION PAGE
SECTION 1.0 INTRODUCTION................................................................................................ 1
SECTION 2.0 BACKGROUND................................................................................................ 1
SECTION 3.0 SCOPE OF WORK (SOW)................................................................................. 3
SECTION 4.0
SAMPLING METHODOLOGY........................................................................... 4
4.1
INDOOR AIR SAMPLING................................................................................. 4
4.2
SUB -SLAB SOIL VAPOR SAMPLING................................................................. 5
4.3
GROUNDWATER GAUGING AND STREAM STAGE MEASUREMENT .............. 6
4.4
REDEVELOPMENT OF WELLS TO BE SAMPLED ............................................... 7
4.5
GROUNDWATER SAMPLING.......................................................................... 7
4.6
SURFACE WATER SAMPLING.......................................................................... 8
4.7
SEDIMENT SAMPLING..................................................................................... 8
SECTION 5.0 LABORATORY ANALYSES................................................................................. 8
SECTION 6.0 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC).................................... 9
SECTION 7.0 INVESTIGATION DERIVED WASTE (IDW) MANAGEMENT ................................ 9
SECTION 8.0 RISK EVALUATION............................................................................................. 9
TABLES
TABLE 1
Property Summary
TABLE 2
Sampling Summary
TABLE 3
Groundwater Monitoring Wells to be Sampled
FIGURES
FIGURE 1 Site Location Map
FIGURE 2 Proposed Paired Indoor Air/Sub-Slab VAP or Sampling Locations
FIGURE 3 Proposed Groundwater Sampling Locations
FIGURE 4 Proposed Surface Water and Sediment Sampling Locations (Excepting VSW-6)
FIGURE 5 Location of Proposed Surface Water Sampling Location VSW-6
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October 2023
Document Number 15104.0014
APPENDICES
verdantas
APPENDIX A Diagram of Former Manufacturing Building Showing Leased Areas
APPENDIX B Letter Summarizing November 30, 2022 Sampling of Recovery Wells
APPENDIX C Protocols for PFAS Sampling
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Document Number 15104.0014
SECTION 1.0 INTRODUCTION
This letter Work Plan Revision No. 2 has been prepared in response to NC DEQ's comments
provided on October 12, 2023, in response to the Work Plan Revision 1 (Verdantas
Document #15104.0014). The property is located at 1885 Alamac Road, Lumberton,
Robeson County, North Carolina (the Subject Property - refer to Figure 1).
SECTION 2.0 BACKGROUND
Phoenix Investors LLC (Phoenix) acquired the 151.79-acre Subject Property, consisting of
Parcel # 101702033 and Parcel # 10170203301, in July 2022. Verdantas reviewed
ownership information maintained by the Robeson County Auditor. Historical Subject
Property ownership is summarized below.
Parcel # 101702033
Date
Grantor
Grantee
5/31/1971
Not provided
West Point-Pepperell Inc.
Not Provided
West Point-Pepperell Inc.
Alamac Knit Fabrics, Inc.
9/28/2001
Alamac Knit Fabrics, Inc.
Alamac Acquisition LLC
9/15/2016
Alamac Acquisition LLC
Alamac Holdings, LLC
3/26/2019
Alamac Holdings, LLC
Lumberton Energy Holdings,
LLC
Parcel # 10170203301
Date
Grantor
Grantee
10/10/1994
Not provided
Alamac Knit Fabrics, Inc.
8/27/1997
Alamac Knit Fabrics, Inc.
Alamac Knit Fabrics Inc.
9/28/2001
Alamac Knit Fabrics Inc.
Alamac Acquisition LLC
9/15/2016
Alamac Acquisition LLC
Alamac Holdings, LLC
3/26/2019
Alamac Holdings, LLC
Lumberton Energy Holdings,
LLC
Table 1 provides a property summary for the subject Property.
Phoenix currently leases a part of the Subject Property to a tenant that occupies only the
western portion of the building. A diagram of the leased area is attached at Appendix
A. Note that the leased area is not within the area that the North Carolina DEQ Brownfield
Program identified in their December 6, 2022, correspondence related to evaluation of
indoor air at the Subject Property.
Tetrachloroethene (PCE) and its daughter products were detected in environmental
media beneath and in the vicinity of a PCE containment pad at the Subject Property in
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Document Number 15104.0014
1997. In 1999 and 2000, environmental remedial efforts were conducted under the
direction of S&ME, Inc. (S&ME) to address the contamination, including:
1. removal and disposal of the concrete PCE pad;
2. removal and disposal of underground piping beneath the PCE pad and
between the pad and the manufacturing building;
3. excavation and stockpiling of approximately 582 cubic yards of soil to
depths slightly below the water table [four to five ft. below ground surface
(bgs) in the vicinity of the pad];
4. thermally treating the soil on -site;
5. construction and use of an infiltration gallery to introduce a water -molasses
mixture into contaminated groundwater;
6. installation and operation of three groundwater recovery wells within the
monitored source area (refer to Figure 2);
7. discharge of extracted groundwater to the Subject Property's wastewater
treatment plant (WWTP); and
8. implementation of monitored natural attenuation downgradient of the
monitored source area extending southward to the Jacob Swamp Canal,
where S&ME, through head measurements within monitoring wells near the
canal and heads within the canal, identified a stream recharge boundary,
indicating groundwater north of the canal would not migrate south of the
canal.
Documentation was provided to Verdantas that indicated that S&ME submitted an
injection permit application for direct -push injection of food -grade soybean oil into
groundwater within the Monitored Source Area to enhance biodegradation of PCE and
daughter products.
The groundwater recovery system has operated since November 1999. Between 1999
and June 2004, water was sampled quarterly from the recovery wells, an off -site
production well located at 2237 Alamac Road (designated WSW-1) and selected
monitoring wells. The samples were tested at an analytical laboratory for volatile organic
compounds (VOCs) by U.S. EPA Method 8260B, pursuant to a Water Quality Monitoring
Plan prepared by S&ME and approved by the North Carolina Department of
Environmental and Natural Resources [currently the North Carolina Department of
Environmental Quality (NC DEQ)] on August 16, 1999. Following June 2004, per NC DEQ's
approval, sampling became once per year and testing remained as described above.
On February 24, 2006, Alamac Knits LLC, then owner of the Subject Property, entered into
a Brownfields Agreement with NC DEQ. In September 2008, approval was provided to
sample only the three recovery wells and the off -site production well. The recovery wells
are operating at present.
In February 2022, the NC DEQ sampled surface water from the Jacob Swamp Canal
upstream and downstream of the Subject Property, as well as effluent from the WWTP
outfall, and tested the samples for polyfluoroalkyl substances (PFAS). PFAS compounds
were detected in all samples collected.
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Document Number 15104.0014
verdantas
On November 30, 2022, Verdantas collected groundwater samples from recovery wells
RW-1, RW-2 and RW-3 and submitted the samples for analysis of PFAS, VOCs and
inorganic analytes for evaluating alternative treatment options for extracted
groundwater. Sampling and findings are detailed in a December 9 summary letter
(Verdantas Document No. 15104.0016). A copy of that summary letter is attached as
Appendix B.
SECTION 3.0 SCOPE OF WORK (SOW)
Phoenix has asked the Brownfields Program to allow it to pause pumping from the
recovery wells for a period of 90 days. The purpose of this work plan is to provide
information and analysis to assist in:
1. evaluating whether pausing the recovery system for 90 days would result in
an unacceptable increase in risks resulting from potential changes in
movement of groundwater; and
2. evaluating whether pausing the recovery system would affect risks to on -
site commercial/industrial workers from indoor air conditions at the Subject
Property.
Verdantas recommends conducting the following activities to support the risk
evaluations:
Prior to initiating a pause to the system:
a. Perform a Brownfields Property Receptor Survey;
b. Collect and analyze paired sub slab soil vapor and indoor air
samples (SS-1/IA-1A through SS-5/IA-5) in the eastern portion of the
former manufacturing building, adjacent to the Monitored Source
Area as shown on Figure 2 and described on Table 2. Evaluate the
sample results using NC DEQ's Risk Calculator for Non -Residential
Worker Indoor Air (January 2023).
C. Gauge groundwater levels in all accessible monitoring wells located
on the Site to obtain water elevations, as shown on Table 2, locate
production well DW-1 A and document conditions of all the wells.
d. Collect groundwater samples from a subset of the existing
monitoring well network. Groundwater samples will be collected
from monitoring wells RW-1, RW-2, RW-3, MW-4, MW-7, MW-8, MW-12,
MW-13, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20 and MW-21
for laboratory analysis of VOCs in accordance with U.S. EPA Method
8260 and PFAS in accordance with U.S. EPA Method 537.1 Modified.
Samples collected from MW-7, MW-8, MW-19, and MW-20 will also
be tested for nitrate and boron by U.S. EPA Methods 300.1 and 200.7,
respectively. Samples collected from MW-19 and MW-20 will be
analyzed for nitrate and boron to determine potential influences
from septic systems and samples from MW-7 and MW-8 will be
analyzed for nitrate and boron for comparative purposes. Locations
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verdantas
of the wells to be sampled are shown on Figure 3 and described on
Table 3. Groundwater samples will be collected prior to system
shutdown and 60 days after system shutdown.
e. Collect upstream and downstream surface water samples from
Jacob Swamp Canal, on -Property ponds and on -Property pond
effluent (VSW-1 through VSW-6) for laboratory analysis of VOCs in
accordance with U.S. EPA Method 8260 and PFAS in accordance
with U.S. EPA Method 537.1 Modified. Proposed sampling locations
for surface water locations VSW-1 through VSW-5 are shown on
Figure 4. The proposed sampling location for VSW-6 is shown on
Figure 5.
f. Collect sediment samples from on -Property ponds (VSED-1 through
VSED-3) for laboratory analysis of VOCs in accordance with U.S. EPA
Method 8260 and PFAS in accordance with U.S. EPA Method 537.1
Modified. Proposed sampling locations are shown on Figure 4.
2. Assuming that NC DEQ approves the 90-day pause, at the end of the 90-
day period a complete round of depth to water measurements will be
collected. Paired indoor air samples followed by sub slab soil vapor
sampling (HVP-1 /IA-1 through HVP-5/IA-5) in the eastern portion of the
former manufacturing building, adjacent to the Monitored Source Area
collect and analyzed. Evaluate the sample results using NC DEQ's Risk
Calculator for Non -Residential Worker Indoor Air (January 2023).
SECTION 4.0
4.1 INDOOR AIR SAMPLING
SAMPLING METHODOLOGY
Indoor air samples (IA-1 through IA-5) will be collected within the occupied portions of
the building, biased toward the area of the known groundwater plume. Additionally, an
outdoor ambient air sample (AA-2) will also be collected. The sampling locations are
shown on Figure 2.
At least 24 hours prior to the indoor air sampling activities, a pre -sampling inspection will
be performed to document conditions within the building that could potentially affect
indoor air analytical results. Any materials that could create interferences with sampling
results will be removed from the building and Safety Data Sheets will be provided in an
Appendix to the report.
The owner will communicate with its on -site employees to request that they do not access
the portion of the building to be sampled during the sampling period. The owner will also
maintain typical HVAC operation during the sampling period.
Also prior to sampling, a photoionization detector (PID - equipped with a 11.7 eV bulb)
reading will also be collected prior to sampling from each proposed vapor sample
location.
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Canisters will be positioned between 3 and 6 feet above the floor within the breathing
zone. Based on the anticipated continued use of the Subject Property for
commercial/industrial purposes, individually laboratory -certified six -liter Summa canisters
for indoor air sampling will be calibrated to fill over an 8-hour sampling period at a flow
rate of approximately 12.5 milliliters per minute. The 8-hour sampling period will replicate
a commercial/industrial worker's exposure. Summa canisters will be placed
approximately 3 to 6 feet above the ground surface to provide representative
concentrations with the commercial/industrial worker breathing zone. The ambient air
sample will also be collected via a Summa canister over an 8-hour period. A final vacuum
reading of at least -5" Hg in each of the canisters will be targeted.
One duplicate indoor air sample will be collected during the sampling period. The
canister for the indoor air duplicate will be set up within two or three lateral feet of the
primary canister.
The laboratory will be requested to report received vacuum for all sampling canisters. If
the sampling canister is evacuated to 0" Hg in the field or if the laboratory notes that the
sampling canister is received at a vacuum of 0" Hg, laboratory analytical results will not
be accepted.
Following completion of the 90-day pause in groundwater extraction, Verdantas will re-
mobilize to the Subject Property to collect additional paired indoor air/soil vapor samples
at the same locations, using the same procedures and presenting the same
documentation described above.
4.2 SUB -SLAB SOIL VAPOR SAMPLING
The proposed locations for paired sub slab soil vapor SS-1 through SS-5 are shown on
Figure 2. After the proposed indoor air samples have been collected, a vapor pin will be
installed at each of the indoor air sampling locations. The vapor pins are proposed to be
installed a minimum of five (5) feet from any walls or cracks in the concrete slab with a
5/8-inch diameter HiltiTM (or equivalent) hammer drill bit to approximately 1-inch below
the concrete slab and a 1 1/2-inch diameter HiltiTM (or equivalent) hammer drill bit to
create a countersink for the placement of a stainless steel flush mount cover. The vapor
pins will then be installed in the pilot holes and following installation, leak testing of the
vapor pin construction will be performed using a helium shroud, helium detector, and
helium tracer gas. Leak testing methodologies will consist of the connection of the vapor
pin to an outlet port on a helium shroud via 1/4-inch or 3/8-inch Teflon® or Teflon® -lined
tubing, the introduction of Grade 5 helium tracer gas via the shroud inlet port, and the
monitoring of the outlet port with a helium detector to ensure helium is not migrating into
the vapor pin. The slab thickness and type of material found under the slab will be
documented for each vapor pin location. At least 30 minutes of stabilization below
capped vapor pins will be required prior to collection of sub slab vapor samples.
In addition to the leak testing of the sub -slab vapor pin to ensure proper construction,
leak testing of the sampling train is proposed to be completed with the helium shroud
apparatus described above. The sampling trains will be leak tested using a helium shroud
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to which a Grade 5 helium source will be connected via '/4-inch or 3/8-inch Teflon® or
Teflon® -lined tubing. The sampling train will be connected to the sub -slab vapor pin via
tubing ('/4-inch or 3/8-inch Teflon® or Teflon® -lined tubing), secured with appropriate
fittings and connections to both the Summa Canister (with the valve closed) and to a
tedlar bag equipped with a backflow preventer. Prior to sample collection, purging 3 to
4 system volumes of sub -slab vapor will be completed with a personal air pump at a rate
not to exceed 200 ml/min into a tedlar bag for field screening with a PID meter and a
calibrated helium detector to ensure helium is not entering the sampling train. Detection
of significant amounts of helium during the test will require re -connecting all fittings and
re -testing. A second detection of helium will require replacement of tubing and
connections and possibly re -seating of the vapor pin. Leak testing will be repeated until
no helium is detected.
Based on the anticipated continued use of the Subject Property for commercial/industrial
purposes, individually laboratory -certified six -liter Summa canisters for indoor air sampling
will be calibrated to fill over an 8-hour sampling period at a flow rate of approximately
12.5 milliliters per minute. The 8-hour sampling period will replicate a
commercial/industrial worker's exposure. One duplicate sub slab vapor sample will be
collected during the period of sampling. A three-way valve, or "T" connecter will provide
flow to both the primary and duplicate canisters. A final vacuum reading of at least -5"
Hg in each of the canisters will be targeted.
The laboratory will be requested to report received vacuum for all sampling canisters. If
the sampling canister is evacuated to 0" Hg in the field or if the laboratory notes that the
sampling canister is received at a vacuum of 0" Hg, laboratory analytical results will not
be accepted.
Following sampling, the vapor pins will be secured with sealable caps. Following
completion of the 90-day pause in groundwater extraction, Verdantas will re -mobilize to
the Subject Property to collect additional sub -slab vapor samples at the same locations,
using the same procedures and presenting the same documentation described above.
4.3 GROUNDWATER GAUGING AND STREAM STAGE MEASUREMENT
All accessible groundwater monitoring wells at the Subject Property will be gauged using
an electrical conductivity sonde attached to a graduated tape that will permit
measurement of the well's total depth and the groundwater surface interface to 0.01
inch, using the top of riser for each well as a reference. The condition of the each well
will be documented based on visual observation and/or the presence of obstructions
within the risers. During the gauging event, production well DW-1 A will also be located.
The graduated tape and sonde will be decontaminated by a water/AlconoxTM solution
followed by a distilled water rinse between gauging of each monitoring well.
Stream stage elevations will be measured within the Jacob Swamp Canal at two
locations: near on -site monitoring well MW-12; and near on -site monitoring well MW-13.
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Tops of risers for the monitoring wells will be used for reference elevations for a survey level
system; a surveyor's rod will be deployed in the surface water.
All monitoring wells and the surface water measurement locations will be located by a
global positioning unit. This will permit the locations to be accurately shown on
Verdantas' base maps.
Groundwater gauging and surface water elevation data will be tabulated and
contoured on the Subject Property base map. Observations on monitoring well
conditions will also be tabulated. Verdantas will evaluate the data and document the
extent to which a stream recharge flow boundary is still present along the southern
property line for the Subject Property.
4.4 REDEVELOPMENT OF WELLS TO BE SAMPLED
All monitoring wells to be sampled (RW-1, RW-2, RW-3, MW-4, MW-7, MW-8, MW-12, MW-
13, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, and MW-21) will be redeveloped.
Monitoring well redevelopment may be performed using a variety of methods, though a
combination of surging and purging is expected. Redevelopment may be performed
manually with a bailer or surge block or mechanically with a submersible pump. If a
submersible pump is used, the pump will be surged (lowered up and down) within the
well screen while pumping is on -going. A minimum of five well volumes will be removed.
Purged water will be monitored for stability of groundwater indicator parameters
including pH, conductivity, temperature, dissolved oxygen (DO), oxygen/reduction
potential (ORP) and turbidity. Well development will continue until the water quality
parameters have stabilized and the water is visually clear of turbidity or a maximum of 10
well volumes have been removed. If development is implemented using a submersible
pump, the aforementioned groundwater indicator parameters will be collected using a
multi -parameter sonde and flow through cell. If bailers are used during development, the
groundwater indicator parameters will not be collected in a flow through cell.
Extracted groundwater will be containerized in Department of Transportation (DOT)
approved drums, sampled, and characterized, and either disposed within the facility's
water treatment system upon re -activation or sent off -Site to a licensed disposal facility.
4.5 GROUNDWATER SAMPLING
A low -flow sampling pump will be used for sampling the selected monitoring well. Clean
gloves will be worn by each individual handling the sampling equipment. The following
steps will be adhered to during sampling:
1. The pump will not be dropped into the monitoring well, as this may cause
degassing of the water on impact;
2. Groundwater will be transferred from the pump into the proper laboratory
supplied glassware in a manner which will minimize agitation and aeration;
and
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3. In order to preserve sample quality, the sampling order will be as follows:
volatile organic compounds, non-volatile organic compounds, and in -situ
parameters (e.g., pH, temperature, conductivity, and turbidity).
Additional protocols for sampling PFAS compounds are described in Appendix C. Water
not used for sample make-up will be containerized in a DOT approved drum, sampled,
and characterized, and either disposed within the facility's water treatment system upon
re -activation or sent off -Site to a licensed disposal facility.
4.6 SURFACE WATER SAMPLING
Surface water samples will be collected from banks of surface water bodies shown on
Figure 4 using a decontaminated glass container affixed to a rigid pole. Surface water
samples will be transferred to laboratory -supplied bottles. Clean gloves will be worn by
each individual handling the sampling equipment. Water not used for sample make-up
will be containerized in a DOT approved drum, sampled, and characterized, and either
disposed within the facility's water treatment system upon re -activation or sent off -Site to
a licensed disposal facility.
4.7 SEDIMENT SAMPLING
Surface water samples will be collected from banks of surface water bodies shown on
Figure 4 using a decontaminated ponar sampler. Sediment samples will be transferred
from the ponar sampler to laboratory -supplied bottles. Clean gloves will be worn by each
individual handling the sampling equipment.
SECTION 5.0 LABORATORY ANALYSES
Summa canister samples of sub slab vapors and indoor air, collected prior to and at the
end of the 90-day pause, will be tested at the ALS Cincinnati, Ohio laboratory for VOCs
in accordance with U.S. EPA Method TO-15 (full analyte list). To the extent feasible,
Method Reporting and Detection Limits will meet all applicable screening levels for
indoor air. Furthermore, ALS will report the vacuum within each summa canister when
received at the laboratory. All J values will be reported by ALS.
Groundwater samples collected prior to and at the end of the 90-day pause, will be
tested at the ALS Cincinnati, Ohio laboratory for VOCs in accordance with U.S. EPA
Method 8260 and PFAS in accordance with U.S. EPA Method 537.1 Modified. Sampled
collected from MW-7, MW-8, MW-19, and MW-20 will also be analyzed for nitrate and
boron for U.S. EPA Methods 300.1 and 200.7, respectively. All J values will be reported by
ALS.
Surface water and sediment samples collected prior to the 90-day pause will be tested
at the ALS Cincinnati, Ohio laboratory for VOCs in accordance with U.S. EPA Method
8260 and PFAS in accordance with U.S. EPA Method 537.1 Modified.
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SECTION 6.0 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC)
One duplicate sample will be collected per r per day when collecting indoor air and sub
slab samples. Following sample collection, Summa canisters will be shipped overnight to
ALS laboratory in Cincinnati, Ohio under completed chain -of -custody for log -in and
testing. The ALS laboratory will perform testing under Level II QA/QC protocols.
One duplicate sample will be collected per day during each groundwater sampling
event. A trip blank will accompany all coolers that contain samples for VOC analysis.
Additionally, one field blank and one equipment blank will be collected during each
sampling event. Following sample collection, sample jars will be shipped overnight to ALS
laboratory in Cincinnati, Ohio under completed chain -of -custody for log -in and testing.
The ALS laboratory will perform testing under Level II QA/QC protocols.
One duplicate sample will be collected per 20 surface water samples per day during
each sampling event. A trip blank will accompany all coolers that contain samples for
VOC analysis. Additionally, one field blank and one equipment blank will be collected
during the sampling event. Following sample collection, sample jars will be shipped
overnight to ALS laboratory in Cincinnati, Ohio under completed chain -of -custody for
log -in and testing. The ALS laboratory will perform testing under Level II QA/QC protocols.
A trip blank will accompany all coolers that contain sediment samples for VOC analysis.
Additionally, one field blank and one equipment blank will be collected during the
sediment sampling event. Following sample collection, sample jars will be shipped
overnight to ALS laboratory in Cincinnati, Ohio under completed chain -of -custody for
log -in and testing. The ALS laboratory will perform testing under Level II QA/QC protocols.
SECTION 7.0 INVESTIGATION DERIVED WASTE (IDW) MANAGEMENT
To the extent that IDW is generated, soil cuttings, purged groundwater, and
decontamination water will be drummed and staged on the Subject Property at a
location identified by the Client. Verdantas will segregate soil cuttings and
decontamination water, which are assumed to be classified as non -hazardous, but will
require disposal. Verdantas will arrange for disposal and characterization of this material
(consistent with the NC DEQ's Brownfields Assessment Work Plan Assessment Work Plan
Checklist); however, the Client will be identified as the generator and will be responsible
for signing manifests. Verdantas has included costs for disposal of this material, assuming
that it is classified as non -hazardous.
SECTION 8.0 RISK EVALUATION
Verdantas will perform two risk evaluations as part of this work plan. First, pursuant to
conversations with the Brownfields Program, and based on the collected data and
proposed modeling, it will assess whether pausing the groundwater recovery system for
90-days would pose an unacceptable risk to potable groundwater users south of the
Jacob Swamp Canal including the Lumberton River and points east. Second, based on
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the findings from the indoor air/soil vapor sampling, it will assess whether pausing the
recovery system affected risks to on -site commercial/industrial workers from indoor air
conditions.
Risk calculations will be generated based on the NC DEQ's Risk Calculator for Non -
Residential Worker Indoor Air (January 2023) and will utilize the maximum concentration
for each compound for each media to generate the most conservative risk. The reporting
limit concentration will be utilized for non -detect compounds.
SECTION 9.0 REPORTING
Upon receiving laboratory analytical reports, Verdantas will transmit them to the DEQ.
Verdantas will prepare an initial summary report that describes groundwater gauging
and the model(s) selected and employed, inputs, simulation results and findings as they
pertain to estimated site conditions over the period of the proposed pause in
groundwater extraction. This summary report will also describe the initial paired sub -slab
vapor/indoor air sampling efforts, groundwater sampling efforts, and findings. Based on
the above, risks will be examined in the context of a pause in groundwater recovery. To
the extent these risks are determined to be acceptable, the report will include a formal
request and schedule for the pause.
At the conclusion of the pause, assuming a pause is completed, a report will be prepared
documenting field efforts and the findings of the second sub -slab vapor/indoor air
sampling event along with an examination of risk as influenced by these findings.
All reporting will be completed under the guidance of a North Carolina Professional
Engineer/Professional Geologist and will be sealed prior to submittal to the agency.
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TABLES
verdantas
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

NORTH CAROLINA DEQ BROWNFIELDS PROGRAM WORK PLAN FOR EVALUATION OF A REQUESTED PAUSE
OF THE GROUNDWATER TREATMENT SYSTEM
1885 ALAMAC ROAD, LUMBERTON, NORTH CAROLINA
TABLE 1
PROPERTY SUMMARY
Brownfields Project
No.
Parcel No.
Address
Site Acreage
Former/ Current Use
REC
Proposed Use
Monitored Source Area
Textiles
101702033 and
1885 Alamac Road, Lumberton,
(chlorinated volatile
06001 02-78
151.79
Manufacturingpping ou
Commercial/Industrial
10170203301
North Carolina 28358
organic compounds in
sing and Shipping
groundwater)
VERDANTAS LLC
BEDFORD, OHIO
Page 1 of 1
OCTOBER 2023
15104.0008 Revision No. 2

NORTH CAROLINA DEQ BROWNFIELDS PROGRAM WORK PLAN FOR EVALUATION OF A REQUESTED PAUSE
OF THE GROUNDWATER TREATMENT SYSTEM
1885 ALAMAC ROAD, LUMBERTON, NORTH CAROLINA
TABLE 2
SAMPLING SUMMARY
Data Gap
Parcel/Bldg. No.
Sampling Objective
Type of Sample
Number of Samples
Depth of Samples
Analytical Program
Detection range for
TCE
Determine Sub Slab Vapor and
Six Sub Slab Vapor
Several Inches below Slab
Sub Slab Vapor and Indoor Air
101702033/Eastern
Indoor Air Quality and Risk in
Sub Slab Vapor
Samples (including
(depending on slab thickness)
Chemicals of Concern
Portion of Former
of Former Manufacturing
and Indoor
duplicate); Six Indoor Air
for Sub Slab Samples; and
U.S. EPA Method TO-
3
ug/m
Adjacent to Monitored Source
1
ManufacturingPortion
Building Adjacent to Monitored
Air/Outdoor
Samples (includingApproximate
p
Breathing Zone
g
15 full anal to list)1.07
( Y
Area
Building
Source Area
Ambient Air
duplicate); and One
r I
for Indoor Air and Ambient Air
Ambient Air Sample
1 Samples
VERDANTAS LLC OCTOBER 2023
BEDFORD, OHIO Page 1 of 1 15104.0008 Revision No. 2

NORTH CAROLINA DEQ BROWNFIELDS PROGRAM WORK PLAN FOR EVALUATION OF A REQUESTED PAUSE
OF THE GROUNDWATER TREATMENT SYSTEM
1885 ALAMAC ROAD, LUMBERTON, NORTH CAROLINA
TABLE 3
PROPOSED MONITORING WELLS TO BE SAMPLED
Well ID
Top at asing Elevation
(ft. MSI
Screen Interval
(ft. bgs)
Analyses
RW-1
110.25
10.00 to 20.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
RW 2
113.55
10.00 to 20.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
RW 3
110.32
10.00 to 20.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW 4
115.16
8.60 to 18.60
VOCs, U.S. EPA Method 8260PFAS,
U.S. EPA Method 537.1 Modified
MW-7
115.93
5.21 to 20.21
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
Nitrate, U.S. EPA Method 300.1
Boron, U.S. EPA Method 200.7
MW-8
113.86
9.59 to 19.59
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
Nitrate, U.S. EPA Method 300.1
Boron, U.S. EPA Method 200.7
MW-12
113.62
26.00 to 31.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-13
116.32
20.50 to 20.50
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-15
113.74
27.50 to 32.50
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-16
114.62
27.50 to 32.50
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-17
113.46
4.00 to 14.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-18
112.82
4.00 to 14.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
MW-19
109.94
8.00 to 18.00
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
Nitrate, U.S. EPA Method 300.1
Boron, U.S. EPA Method 200.7
MW-20
112.67
11.50 to 21.50
VOCs, U.S. EPA Method 8260
PFAS, U.S. EPA Method 537.1 Modified
Nitrate, U.S. EPA Method 300.1
Boron, U.S. EPA Method 200.7
MW-21
TBD
TBD
I VOCs, PFAS
Note: TBD - To be determined.
VERDANTAS LLC OCTOBER 2023
BEDFORD, OHIO PAGE 1 OF 1 15104.0009 Revision No. 2

October 2023
Document Number 15104.0014
FIGURES
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Source: The topographic map was acquired through the USGS
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The aerial photo was acquired through the Esri Imagery Web Service.
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Groundwater Treatment Re -Evaluation Work Plan
Date:
Alamac Road Property
October 2023
Verdantas
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_ T exclusive use as a preliminary planning and screening tool and field verification is necessary to confirm Alamac Road Property
these data. This map is reproduced from geospatial information compiled from third -parry sources which
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Verdantas LLC has furnished this map to the company identified in the title block (Client) for its sole and Groundwater Treatment Re -Evaluation Work Plan Figure
exclusive use as a preliminary planning and screening tool and field verification is necessary to confirm Alamac Road Property
these data. This map is reproduced from geospatial information compiled from third -party sources which
may change over time. Areas depicted by the map are approximate and may not be accurate to mapping, Proposed Surface Water and Sediment
(� ve r d a n t a s surveying or engineering standards. Verdantas LLC makes no representation or guarantee as to the content, p
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provided without warranty of any kind, including but not limited to, the implied warranties of merchantability
- or fitness for a particular purpose. In no event will Verdantas LLC, its owners, officers, employees or agents, 1885 Alamac Road
' be liable for damages of any kind arising out of the use of this map by Client or any other party.
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DISCLAIMER: October 2023
Verdantas LLC has furnished this map to the company identified in the title block (Client) for its sole and Groundwater Treatment Re -Evaluation Work Plan Figure
exclusive use as a preliminary planning and screening tool and field verification is necessary to confirm Alamac Road Property
these data. This map is reproduced from geospatial information compiled from third -party sources which may
j� ve r d a n t a s change over time. Areas depicted er the map are approximate and may not ar accurate to mapping
surveying i engineering standards. Verdantas LLC makes p representation or guarantee m p. the content, Location Of Proposed Surface Water
accuracy, timeliness or completeness of any information or spatial location depicted on this map. This map is Sampling Location VSW-6
P E O P t E FOCUSED F U T U R E provided without warranty of any kind, including but not limited to, the implied warranties of merchantability p 9
or fitness for a particular purpose. In no event will Verdantas LLC, its owners, officers, employees or agents,
be liable for damages of any kind arising out of the use of this map by Client or any other parry. 1885 Alamac Road
Lumberton, Robeson County, North Carolina
Ed,t.d:10/17/2023 J.e dre

October 2023
Document Number 15104.0014
APPENDIX A
verdantas
DIAGRAM OF FORMER MANUFACTURING BUILDING SHOWING LEASED AREAS
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

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- LEASED PREMISES
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October 2023
Document Number 15104.0014
APPENDIX B
verdantas
LETTER SUMMARIZING NOVEMBER 30, 2022, SAMPLING OF RECOVERY WELLS
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

1 verdantas
PEOPLE FOCUSED FUTURE
January 24, 2023
Kelly G. Johnson, P.G.
Brownfields Vapor Intrusion Specialist
NC Department of Environmental Quality
Division of Waste Management
217 West Jones Street
Raleigh, NC 276031
Re: Summary of Groundwater Sampling Efforts and Results at the Alamac Road Property
Located at 1885 Alamac Road, Lumberton, NC; 15104.0016.
Dear Mr. Johnson:
This letter has been prepared by Verdantas, LLC (Verdantas), a subcontractor to Borton Lawson
American Engineering, PC, NC License #: C-4805, to describe November 30, 2022 sampling of
three recovery wells, RW-1 through RW-3, on at the Alamac Road Property located at 1885
Alamac Road, Lumberton, Robeson County, North Carolina (referred to herein as the Subject
Property - refer to Figure 1). The letter also summarizes results from analysis of the samples. The
objective of the groundwater sampling was to provide a basis for evaluating potential treatment
of groundwater recovered from the Monitored Source Area at the Subject Property. Refer to
Figure 2 for the location of the recovery wells and the Monitored Source Area.
BACKGROUND
Tetrachloroethene (PCE) and its daughter products were detected in environmental media
beneath and in the vicinity of a PCE containment pad at the Subject Property in 1997. In 1999
and 2000, environmental remedial efforts were conducted under the direction of S&ME, Inc.
(S&ME) to address the contamination, including:
removal and disposal of the concrete PCE pad;
2. removal and disposal of underground piping beneath the PCE pad and between
the pad and the manufacturing building;
3. excavation and stockpiling of approximately 582 cubic yards of soil to depths
slightly below the water table [four to five ft. below ground surface (bgs) in the
vicinity of the pad];
4. thermally treating the soil on -site;
5. construction and use of an infiltration gallery to introduce a water -molasses mixture
into contaminated groundwater;
6. installation and operation of three groundwater recovery wells within the
Monitored Source Area (refer to Figure 2);
7. discharge of extracted groundwater to the Subject Property's wastewater
treatment plant (WWTP); and
4 Hemisphere Way, Bedford, OH, 44146 1 verdantas.com

Document Number 15104.0016
verdantas
8. implementation of monitored natural attenuation downgradient of the Monitored
Source Area extending southward to the Jacob Swamp Canal, where S&ME,
through head measurements within monitoring wells near the canal and heads
within the canal, identified a stream recharge boundary, indicating groundwater
north of the canal would not migrate south of the canal.
Documentation was provided to Verdantas that indicated that S&ME submitted an injection
permit application for direct -push injection of food -grade soybean oil into groundwater within the
Monitored Source Area to enhance biodegradation of PCE and daughter products.
The groundwater recovery system has operated since November 1999. Between 1999 and June
2004, water was sampled quarterly from the recovery wells, an off -site production well located at
2237 Alamac Road (designated WSW-1) and selected monitoring wells. The samples were tested
at an analytical laboratory for volatile organic compounds (VOCs) by U.S. EPA Method 8260B,
pursuant to a Water Quality Monitoring Plan prepared by S&ME and approved by the North
Carolina Department of Environmental and Natural Resources [currently the North Carolina
Department of Environmental Quality (NC DEQ)] on August 16, 1999. Following June 2004, per NC
DEQ's approval, sampling became once per year and testing remained as described above. On
February 24, 2006, Alamac Knits LLC, then owner of the Subject Property, entered into a
Brownfields Agreement with NC DEQ. In September 2008, approval was provided to sample only
the three recovery wells and the off -site production well. The recovery wells are operating at
present.
In February 2022, INC DEQ sampled surface water from the Jacob Swamp Canal upstream and
downstream of the Subject Property, as well as effluent from the WWTP outfall, and tested the
samples for polyfluoroalkyl substances (PFAS). PFAS compounds were detected in all samples
collected.
GROUNDWATER
On November 30, 2022, a Verdantas employee purged recovery wells RW-1, RW- 2 and RW-3 for
several minutes and collected samples from sampling ports located on the former treatment
system pad. Purged groundwater was containerized for on -site disposal. Samples were carefully
transferred to the laboratory -supplied, pre -preserved (as applicable) sample containers and the
sample containers were immediately packaged and transferred to iced coolers.
The samples coolers were shipped under chain -of -custody to the ALS Group laboratory in
Cincinnati, Ohio. Requested analyses were:
VOCs by U.S. EPA Method 826013;
Perfluoroalkyl and polyfluoralkyl substances (PFAS) by U.S. EPA Modified Method
E537 MOD;
Low level alkalinity by Standard Method A2320 B-1 1;
4. Chloride by Standard Method A4500-CL C-1 1;
Hardness by Standard Method A2340 C-11;
4 Hemisphere Way, Bedford, OH, 44146 1 verdantas.com 2

Document Number 15104.0016
verdantas
6. Nitrogen, nitrate -nitrite by Standard Method E353.2 R2.0;
7. pH (laboratory) by Standard Method E150.1;
8. Sulfate by Standard Method A4500-SO4 E-11;
9. Total dissolved solids by Standard Method A2540 C-15;
10. Total organic carbon by Standard Method A5310C-14;
11. Total suspended solids by Standard Method A2540 D-15; and
12. Iron by Standard Method E200.8.
The ALS Global laboratory analytical report and chain -of -custody are included in Attachment A.
Table 1 summarizes laboratory analytical results.
Please contact Lindsay Crow at [phone] with any questions regarding the contents of this
letter.
Sincerely,
00'w� a^00--'
Lindsay Crow Mark J. Bonifas, PE
Senior Project Manager Senior Consultant
cc: Bruce Nicholson, Program Manager, NC DEQ
Sharon Eckard, Project Manager, NC DEQ
Jay L. Osborne, Assistant General Counsel, NC DEQ
Frank Crivello, Founder & Chairman, Phoenix Investors
Attachments
4 Hemisphere Way, Bedford, OH, 44146 1 verdantas.com 3

Document Number 15104.0016
j® verdantas
TABLE
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

SUMMARY OF RECOVERY WELL SAMPLING RESULTS
ALAMAC ROAD PROPERTY
1885 ALAMAC ROAD, LUMBERTON, NORTH CAROLINA
TABLE 1
RECOVERY WELL GROUNDWATER SAMPLING RESULTS
Client Sample ID
North Carolina
Groundwater
Standards
IRY165:RW-1:G113022
IRY165:RW-2:G113022
IRY165:RW-3:G113022
IRY165:RW-3:G713022A
Well ID
RW-1
RW-2
RW-3
RW-3(Duplicate)
Lab ID
22120229-01
22120229-02
22120229-03
22120229-04
Sample Date
11/30/2022
11/30/2022
11/30/2022
11/30/2022
Matrix
Groundwater
Groundwater
Groundwater
Groundwater
PFAS and PFOA - U.S. EPA Method 527 Modified (ng/L)
Fluorotelomer sulphonic acid 4:2 (FtS 4:2)
M
<0.95
<0.94
<0.91
<0.90
Fluorotelomer sulphonic acid 6:2 (FtS 6:2)
NS
2.1 J
20
2.5 J
3.9 J
Fluorotelomer sulphonic acid 8:2(FtS 8:2
NS
19
22
4.6 J
6.8
Fluorotelomer sulphonic acid 10:2(FtS 10:2)
NS
4.7J
<2.4
<2.3
<2.3
Perfluorobutanesulfonic acid PFBS
NS
26
72
32
31
Perfluorobutanoic acid (PFBA)
NS
62
610
170
170
Perfluorodecanesulfonic acid (PFDS)
NS
<1.4
<1.4
<1.3
<1.3
Perfluorodecanoic acid IPFDAI
NS
72
250
51
52
Perfluorododecanesulfonic acid PFDoS
NS
<0.63
<0.63
<0.61
<0.60
Perfluorododeconoic acid PFDoA
NS
22
14
2.1 J
2.7 J
Pe luoroheptanesul onic acid PFHpS
NS
25
SB
27
33
Perfluorohe tanoic acid PFH A
NS
210
1,100
360
390
Perfluorohexadecanoic acid (PFHxDA)
NS
<1.8
<1.8
<1.8
<1.7
Perfluorohexanesulfonic acid PFHxS
NS
65
150
55
75
Perfluorohexanoic acid PFHxA
NS
220
2,900
600
530
Perfluoronononesulfonic acid (PFNS)
NS
<0.5
<0.50
<0.48
<0.48
Perfluorononanoic acid PFNA
NS
55
320
75
81
Perfluorooctadecanoic acid (PFODA)
NS
<0.66
<0.65
<0.63
<0.62
Perfluorooctonesulfonamide PFOSA
NS
8.8
7.1
1.8 J
1.4 J
Perfluorooctanesulfonic acid PFOS
NS
670
830
520
450
Perfluorooctanoic acid PFOA
NS
3"
2,500
580
530
Perfluoropentanesulfonic acid (PFPeS)
NS
19
49
19
28
Perfluoro entanoic acid PFPeA
NS
ISO
2,700
540
500
Perfluorotetradecanoic acid PFTeA
NS
<2.7
<2.7
<2.6
<2.5
Perfluorotridecanoic Acid PFTNA
NS
<2.0
<2.9
<1.9
<1.9
Perfluoroundecanoic acid PFUnA
NS
22
16
12
11
N-eth erfluoro-I cntanesulfonamide
NS
<1.2
<1.2
<1.1
<1.1
N-eth erfluorooctaesulfonamidoacefic acid
NS
<1.6
<1.6
<1.5
<1.5
N-eth erfluorooctanesulfonamidoethanol
NS
<1.1
<1.1
<1.0
<1.0
N-meth erfluoro-l-octonesulfonamide
NS
1.51
1.3J
<0.77
<0.76
N-methylperfluorooctanesulfonamidoacetic acid
NS
48
SB
40
38
N-methylperfluorooctanesulfonamidoethanoI
NS
<1.5
<1.5
<1.5
<1.4
Hexafluoro ro Iene oxide dimer acid HFPO-DA
NS
4.1
11
8.3
8.2
4,8-Dioxa-3H-perfluorononanoic acid (DONA)
NS
<0.57
<0.57
<0.55
<0.54
11 CI-P3OUdS
NS
<0.47
<0.47
<0.45
<0.45
9CI-PF30NS
NS
<0.45
<0.45
<0.44
<0.43
Pe luoro-4-ethylcyclohexonesul onic acid PFecHS
NS
<U.90
<U.89
<0.86
<0.85
Perfluorobutylsulfonamide (PFBSA)
NS
?.1
27
6.2
6.1
Perfluorohexanesulfonamide PFHxSA
NS
6.4
16
3.71
4.1 J
VOCs - U.S. EPA Method 8260C (ug/L)
1,1,1-trichloroethane
200
<0.46
<0.46
<0.46
<0.46
1, 1,2,2-tetrachloroethane
0.2
<0.40
<0.40
<0.40
<0.40
1,1,2-trichloroethane
0.6
<0.46
<0.46
<0.46
<0.46
1, 1,2-trichlorotrifluoroethane
NS
<0.52
<0.52
<0.52
<0.52
1,1-dichloroethane
6
2.9
1.2
0.651
0.79J
1,1-dichloroethene
350
13
14
4.7
5.0
1,2,3-tichloobenzene
NS
<0.42
<0.42
<0.42
<0.42
1,2,3-trichloropropane
0.005
<0.40
<0.40
<0.40
<0.40
1,2,4-tichlorobenzene
70
<0.45
<0.45
<0.45
<0.45
1,2,4-trimethylbenzene
NS
<0.45
<0.45
<0.45
<0.45
1,2-dibromo-3-chloropropane
0.04
<0.43
<0.43
<0.43
<0.43
1,2-dibromoethane
NS
<0.41
<0.41
<0.41
<0.41
1,2-dichlorobenzene
20
0.75 J
0.94 J
<0.32
<0.32
1,2-dichloroethane
0.4
<0.44
<0.44
<0.44
<0.44
1,2-dichlompropane
0.6
<0.48
<0.48
<0.48
<0.48
1,3,5-trimethylbenzene
400
<0.65
<0.65
<0.65
<0.65
1,3-dichlorobenzene
200
<0.33
<0.33
<0.33
<0.33
1,4-dichlorobenzene
6
<0.35
<0.35
0.61 J
0.75 J
2-butanone
4,000
<0.52
<0.52
<0.52
<0.52
2-hexanone
NS
<0.59
<0.59
<0.59
<0.59
4-methyl-2-pentanone
NS
<0.52
<0.52
<0.52
<0.52
Acetone
6,000
6.5 J
6.3 J
<6.2
<6.2
Benzene
Bromochloromethane
1
NS
1.1
<0.45
19000001=
<0.45
0.62 J
<0.45
0.82 J
<0.45
Bromodichloromethane
0.6
<0.49
<0.49
<0.49
<0.49
Bromoform
4
<0.56
<0.56
<0.56
<0.56
Bromomethane
10
<0.90
<0.90
<0.90
<0.90
Carbon disulfide
700
<0.49
0.93 J
<0.49
0.52 J
Carbon tetrachloride
0.3
<0.40
<0.40
<0.40
<0.40
Chlorobenzene
50
<0.40
<0.40
0.82 J
0.83 J
Chloroethane
3,000
<0.68
<0.68
<0.68
<0.68
Chloroform
70
<0.46
<0.46
<0.46
<0.46
Chloromethane
3
<0.83
<0.83
<0.83
<0.83
cis-1,2-dichloroethene
70
2,000
6,100
1,800
1,700
cis-1,3-dichloropropene
NS
<0.57
<0.57
<0.57
<0.57
Cyclohexane
NS
<0.63
<0.63
<0.63
<0.63
Dibromochloromethane
0.5
<0.40
<0.40
<0.40
<0.40
Dichlorodifluoromethane
1,000
<0.68
<0.68
<0.68
<0.68
Ethylbenzene
600
0.76 J
<0.34
<0.34
<0.34
Isopropylbenzene
70
<0.35
<0.35
<0.35
<0.35
m,p-xylene
500
1.8 J
0.89 J
<0.81
<0.81
Methyl acetate
NS
<0.59
1 <0.59
<0.59
<0.59
Methyl tern -butyl ether
20
<0.45
<0.45
<0.45
<0.45
Methylcyclohexsne
NS
<0.35
<0.35
<0.35
<0.35
Methylene chloride
5
<0.86
<0.86
<0.86
<0.86
o-xylene
500
0.88 J
1.5
0.31 J
0.48 J
Styrene
70
<0.33
<0.33
<0.33
<0.33
Tetrachloroethene
0.7
2,300
100
60
57
Toluene
600
2.0
0.47 J
<0.45
<0.45
trans-1,2dichloroethene
100
74
60
12
14
trans-1,3dichloropropene
0.4
<0.38
<0.38
<0.38
<0.38
Trichloroethene
3
1,100
100
31
31
Trichlorofluoromethane
2,000
i <0.52
<0.52
<0.52
<0.52
Vinyl chloride
0.03
160
500
310
280
Xylenes, total
500
2.1 J
2.4 J
<0.81
<0.81
VERDANTAS LLC JANUARY 2023
BEDFORD, OHIO PAGE 1 OF 2 15104.0007

SUMMARY OF RECOVERY WELL SAMPLING RESULTS
ALAMAC ROAD PROPERTY
1885 ALAMAC ROAD, LUMBERTON, NORTH CAROLINA
12E' B
Notes:
a: No standard established for this parameter.
b: < indicates paromter not reported above laboratory reporting limit for the onalyte.
Shaded cells exceeds North Carolina Standards.
J - Analyte is present at an estimated concentration between the MDL and Report Limit.
H - Analyzed outside of Holding Time.
VERDANTAS LLC JANUARY 2023
BEDFORD, OHIO PAGE 2 OF 2 15104.0007

Document Number 15104.0016
j® verdantas
FIGURES
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

© 2022, Verdantas LLC
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DISCLAIMER: 0
1,000 2,000 4,000
Verdantas LLC has furnished this map to the company identified in the title block (Client) for its sole and IllFeet
North Carolina exclusive use as a preliminary planning and screening tool and Feld verification is necessary to confirm
1 Inch = 2,000 Feet
these data. This map is reproduced from geospatial information compiled from third -party sources which
may change over time. Areas map are approximate epre may not be accurate to mapping, QUaCirangl@. Southwest Lumberton, NC
dardsedbythe
surveying or engineering standards. Verdantas LLC makes no representation or guarantee as to the
makes
content, accuracy, timeliness or completeness of any information or spatial location depicted on this map.
This map is provided without warranty of any kind, including but not limited to, the implied warranties of
Source: The topographic map was acquired through the USGS
merchantability or fitness for a particular purpose. In no event will Verdantas LLC, its owners, officers,
Topographic Map Web Service.
employees or agents, be liable for damages of any kind arising out of the use of this map by Client or any
other party.
The aerial photo was acquired through the Esri
Imagery web service. Aerial photography dated 2018 and 2020.
Summary of Recovery Well Sampling
Date:
Alamac Road Property
January 2023
vardantas-
Subject Property Location Map
Figure
P 1 0 P L E re Ci1'-
File Name:
0000015104_06_Fig01_SLM.mxd
1885 ARoad
Lumberton, Robesonn County, North Carolina
ou
Edited: 12112/2022 User: dread
I
Produced Using Esd's ArcGIS Software

Document Number 15104.0016
j® verdantas
ATTACHMENT A
ALS GLOBAL LABORATORY ANALYTICAL REPORT AND SAMPLE CHAIN -OF -CUSTODY DOCUMENTATION
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

09-Dec-2022
Pamela Nixon
Verdantas
4 Hemisphere Way
Bedford, OH 44146
Re: Phoenix Lumberton
Dear Pamela,
Work Order: 22120229
ALS Environmental received 7 samples on 01-Dec-2022 09:00 AM for the analyses presented in the
following report.
The analytical data provided relates directly to the samples received by ALS Environmental - Holland and
for only the analyses requested.
Sample results are compliant with industry accepted practices and Quality Control results achieved
laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the
report or QC batch information. Should this laboratory report need to be reproduced, it should be
reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be
disposed in 30 days unless storage arrangements are made.
The total number of pages in this report is 92.
If you have any questions regarding this report, please feel free to contact me:
ADDRESS: 3352 128th Avenue, Holland, MI, USA
PHONE: [phone] FAX: [phone]
Sincerely,
Electronically approved by: Bill Carey
Bill Carey
Project Manager
Report of Laboratory Analysis
Certificate No: OH: CL 103
ALS GROUP USA, CORP Part ipbell Brothers Limited Company
www.alsglobal.com

ALS Group, USA Date: 09-Dec-22
Client:
Project:
Work Order:
Verdantas
Phoenix Lumberton
22120229
Work Order Sample Summary
Lab Samp ID Client Sample ID
Matrix
Tau Number
Collection Date
Date Received
Hold
22120229-01
IRY165:RW-1:G113022
Water
RW-1
11/30/2022 16:15
12/1/2022 09:00
22120229-02
IRY165:RW-2:G113022
Water
RW-2
11/30/2022 16:24
12/1/2022 09:00
22120229-03
IRY165:RW-3:G113022
Water
RW-3
11/30/2022 16:30
12/1/2022 09:00
22120229-04
IRY165:RW-3:G113022A
Water
RW-3
11/30/2022 16:30
12/1/2022 09:00
22120229-05
IRY165:FB-1:W113022
Water
FB-1
11/30/2022 16:19
12/1/2022 09:00
22120229-06
IRY165:TB-1:W113022
Water
TB-1
11/30/2022
12/1/2022 09:00
22120229-07
IRY165:TB-2:W113022
Water
TB-2
11/30/2022
12/1/2022 09:00
Sample Summary Page 1 of 1

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
WorkOrder: 22120229
Date: 09-Dec-22
QUALIFIERS,
ACRONYMS, UNITS
QF Page 1 of 2

ALS Group, USA
Date: 09-Dec-22
Qualifier Description
* Value exceeds Regulatory Limit
** Estimated Value
a Analyte is non -accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
Hr BOD/CBOD - Sample was reset outside Hold Time, value should be considered estimated.
J Analyte is present at an estimated concentration between the MDL and Report Limit
n Analyte accreditation is not offered
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL
X Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or
reagent contamination at the observed level.
Acronym Description
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
LOD Limit of Detection (see MDL)
LOQ Limit of Quantitation (see PQL)
MBLK Method Blank
MDL Method Detection Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PQL Practical Quantitation Limit
RPD Relative Percent Difference
TDL Target Detection Limit
TNTC Too Numerous To Count
A APHA Standard Methods
D ASTM
E EPA
SW SW-846 Update III
Units Reported Description
°C Degrees Celcius
µg/L Micrograms per Liter
mg/L Milligrams per Liter
mg/L CaCO3 Milligrams per Liter as Calcium Carbonate
ng/L Nanograms per Liter
s.u. Standard Units
QF Page 2 of 2

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Date: 09-Dec-22
Case Narrative
The attached "Sample Receipt Checklist" documents the date of receipt, status of custody
seals, container integrity, preservation, and temperature compliance.
Samples were analyzed according to the analytical methodology previously transmitted in the
"Work Order Acknowledgement". Methodologies are also documented in the "Analytical
Result" section for each sample. Quality control results are listed in the "QC Report" section.
A copy of the laboratory's scope of accreditation is available upon request.
Sample association for the reported quality control is located at the end of each batch
summary. If applicable, results are appropriately qualified in the Analytical Result and QC
Report sections. The "Qualifiers" section documents the various qualifiers, units, and
acronyms utilized in reporting.
Any flags on MS/MSD samples not addressed in this narrative are unrelated to samples in this
report.
With the following exceptions, all sample analyses achieved analytical criteria.
Batch 207682, Method E537 Mod, Sample IRY165:RW-1:G113022 (22120229-01 E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. 1802-PFHxS
Batch 207682, Method E537 Mod, Sample IRY165:RW-2:G113022 (22120229-02E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. See attached QC report.
Batch 207682, Method E537 Mod, Sample IRY165:RW-3:G113022 (22120229-03E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. d3-N-McFOSA, d5-N-EtFOSA
Batch 207682, Method E537 Mod, Sample IRY165:RW-3:G113022 (22120229-03E): One or
more surrogate recoveries were above the upper control limits. The sample was non -detect,
therefore, no qualification is needed. 13C2-FtS 4:2
Batch 207682, Method E537 Mod, Sample IRY165:RW-3:G113022A (22120229-04E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. d5-N-EtFOSA, 1802-PFHxS
Case Narrative Page 1 of 3

Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Case Narrative
Batch 207682, Method E537 Mod, Sample IRY165:FB-1:W113022 (22120229-05E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. See attached QC report.
Batch 207682, Method E537 Mod, Sample IRY165:RW-3:G113022A (22120229-04E): One or
more surrogate recoveries were below the lower control limits. The sample results may be
biased low. 13C2-PFHxA, 13C4-PFHpA
Batch R359519, Method E150.1, Sample IRY165:RW-1:G113022 (22120229-01C): This is
considered a "field test" and, as such, the recommended sample holding time expired prior to
sample receipt.
Batch R359519, Method E150.1, Sample IRY165:RW-2:G113022 (22120229-02C): This is
considered a "field test" and, as such, the recommended sample holding time expired prior to
sample receipt.
Batch 207809, Method A2540 D-15, Sample IRY165:RW-2:G113022 (22120229-02D):
Sample filtration exceeded 10 minutes. Reduced volume of sample utilized for analysis of
TSS.
Batch R359519, Method E150.1, Sample IRY165:RW-3:G113022 (22120229-03C): This is
considered a "field test" and, as such, the recommended sample holding time expired prior to
sample receipt.
Batch R359519, Method E150.1, Sample IRY165:RW-3:G113022A (22120229-04C): This is
considered a "field test" and, as such, the recommended sample holding time expired prior to
sample receipt.
Batch R359519, Method E150.1, Sample IRY165:FB-1:W113022 (22120229-05C): This is
considered a "field test" and, as such, the recommended sample holding time expired prior to
sample receipt.
Batch R359835b, Method SW8260C, Sample 22120229-02H DUP: The RPD between the
sample and its duplicate was out of control. The corresponding sample result should be
considered estimated for this analyte. trans-1,2-Dichloroethene, Carbon Disulfide
Batch R359715, Method A4500-SO4 E-11, Sample 22120229-05C MS: The MS recovery was
below the lower control limit. The corresponding result in the parent sample may be biased
low for this analyte.
Batch R359835b, Method SW8260C, Sample 22120229-01 H MS: The MS recovery was
above the upper control limit. The corresponding result in the parent sample may be biased
Case Narrative Page 2 of 3

Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
high for this analyte: trans- 1,2-Dichloroethene
Case Narrative
Batch R359648C, Method E353.2 R2.0, Sample 22120229-03A MS: The MS recovery was
above the upper control limit. The corresponding result in the parent sample may be biased
high for this analyte.
Batch R359835b, Method SW8260C, Sample 22120229-01 H MS: The MS recovery was
above the upper control limit. The corresponding result in the parent sample was non -detect,
therefore no qualification is necessary: 1,1,2-Trichloroethene, Dichlorodifluoromethane,
Chloromethane, Trichlorofluoromethane
Batch R359835b, Method SW8260C, Sample 22120229-01 H MS: The MS recovery was
outside of the control limit; however, the result in the parent sample is greater than 4x the
spike amount. No qualification is required for this analyte: cis-1,2-Dichloroethene,
Tetrachloroethene, Trichloroethene, Vinyl Chloride
Batch R359715, Method A4500-SO4 E-11, Sample 22120229-05C MSD: The MSD recovery
was below the lower control limit. The corresponding result in the parent sample may be
biased low for this analyte.
Batch R359648C, Method E353.2 R2.0, Sample 22120229-03A MSD: The MSD recovery was
above the upper control limit. The corresponding result in the parent sample may be biased
high for this analyte.
Case Narrative Page 3 of 3

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-1:G113022
Collection Date: 11/30/2022 04:15 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-01
Matrix: WATER
Dilution
Units Factor Date Analyzed
METALS BY ICP-MS
Method: E200.8
Prep: CEM-NPDES / 12/5/22
Analyst: STP
Iron
4.25
0.047
0.080
mg/L
1
12/5/202218:16
PFAS BY EPA 537 MODIFIED
Method: E537 MOD
Prep: E537 Mod / 12/5/22
Analyst: ENS
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
0.95
5.1
ng/L
1
12/5/2022 18:18
4:2)
Fluorotelomer Sulphonic Acid 6:2
2.1
J 1.9
5.1
ng/L
1
12/5/2022 18:18
(FtS 6:2)
Fluorotelomer Sulphonic Acid 8:2
19
1.1
5.1
ng/L
1
12/5/2022 18:18
(FtS 8:2)
Fluorotelomer Sulphonic Acid 10:2
4.7
J 2.4
5.1
ng/L
1
12/5/2022 18:18
(FtS 10:2)
Perfluorobutanesulfonic Acid (PFBS)
26
0.36
5.1
ng/L
1
12/5/2022 18:18
Perfluorobutanoic Acid (PFBA)
62
2.6
5.1
ng/L
1
12/5/2022 18:18
Perfluorodecanesulfonic Acid (PFDS)
U
1.4
5.1
ng/L
1
12/5/2022 18:18
Perfluorodecanoic Acid (PFDA)
72
1.3
5.1
ng/L
1
12/5/2022 18:18
Perfluorododecanesulfonic Acid
U
0.63
5.1
ng/L
1
12/5/2022 18:18
(PFDoS)
Perfluorododecanoic Acid (PFDoA)
22
0.70
5.1
ng/L
1
12/5/2022 18:18
Perfluoroheptanesulfonic Acid
25
0.57
5.1
ng/L
1
12/5/2022 18:18
(PFHpS)
Perfluoroheptanoic Acid (PFHpA)
210
1.8
5.1
ng/L
1
12/5/2022 18:18
Perfluorohexadecanoic Acid (PFHxDA)
U
1.8
5.1
ng/L
1
12/5/2022 18:18
Perfluorohexanesulfonic Acid
65
0.92
5.1
ng/L
1
12/5/2022 18:18
(PFHxS)
Perfluorohexanoic Acid (PFHxA)
220
1.2
5.1
ng/L
1
12/5/2022 18:18
Perfluorononanesulfonic Acid (PFNS)
U
0.50
5.1
ng/L
1
12/5/2022 18:18
Perfluorononanoic Acid (PFNA)
55
0.88
5.1
ng/L
1
12/5/2022 18:18
Perfluorooctadecanoic Acid (PFODA)
U
0.66
5.1
ng/L
1
12/5/2022 18:18
Perfluorooctanesulfonamide
8.8
0.72
5.1
ng/L
1
12/5/2022 18:18
(PFOSA)
Perfluorooctanesulfonic Acid (PFDS)
670
9.1
20
ng/L
10
12/6/2022 12:23
Perfluorooctanoic Acid (PFDA)
390
6.4
20
ng/L
10
12/6/2022 12:23
Perfluoropentanesulfonic Acid
19
0.56
5.1
ng/L
1
12/5/2022 18:18
(PFPeS)
Perfluoropentanoic Acid (PFPeA)
150
1.3
5.1
ng/L
1
12/5/2022 18:18
Perfluorotetradecanoic Acid (PFTeA)
U
2.7
5.1
ng/L
1
12/5/2022 18:18
Perfluorotridecanoic Acid (PFTriA)
U
2.0
5.1
ng/L
1
12/5/2022 18:18
Perfluoroundecanoic Acid (PFUnA)
22
0.99
5.1
ng/L
1
12/5/2022 18:18
N-ethylperfluoro-1-octanesulfonamide
U
1.2
5.1
ng/L
1
12/5/2022 18:18
N-
U
1.6
5.1
ng/L
1
12/5/2022 18:18
Ethyl perfluorooctanesulfonamidoacetic
Acid
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page 1 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-I:Gl l3022
Collection Date: 11/30/2022 04:15 PM
Analyses
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-01
Matrix: WATER
Report Dilution
Result Qual MDL Limit Units Factor Date Analyzed
N-
U
Ethyl perfluorooctanesulfonamidoethano
I
N-methylperfluoro-1-
1.5 J
octanesulfonamide
N-
48
Methyl perfluorooctanesulfonamidoa
cetic Acid
N-
U
Methylperfluorooctanesulfonamidoetha
nol
Hexafluoropropylene oxide dimer
4.0 J
acid (HFPO-DA)
4,8-Dioxa-3H-perfluorononanoic Acid
U
(DONA)
11 CI-Pf30UdS
U
9CI-PF30NS
U
Perfluoro-4-ethylcyclohexanesulfonic
U
Acid (PFecHS)
Perfluorobutylsulfonamide (PFBSA)
9.1
Perfluorohexanesulfonamide
6.4
(PFHxSA)
Surr: 13C2-FtS 4:2
105
Surr. 13C2-FtS 6:2
85.9
Surr 13C2-FtS 8:2
90.7
Surr 13C2-PFDA
62.5
Surr 13C2-PFDoA
78.6
Surr 13C2-PFHxA
71.7
Surr 13C2-PFHxDA
72.9
Surr 13C2-PFTeA
83.5
Surr: 13C2-PFUnA
64.5
Surr. 13C3-HFPO-DA
64.6
Surr: 13C3-PFBS
64.2
Surr. 13C4-PFBA
68.9
Surr. 13C4-PFHpA
81.9
Surr. 13C4-PFOA
66.7
Surr. 13C4-PFOS
60.6
Surr 13C5-PFNA
79.3
Surr 13C5-PFPeA
71.3
Surr 13C8-FOSA
74.8
Surr 1802-PFHxS
49.6 S
Surr d5-N-EtFOSA
50.4
Surr d5-N-EtFOSAA
93.1
Note: See Qualifiers page for a list of qualifiers and their definitions
1.1 5.1 ng/L 1 12/5/202218:18
0.81
5.1
ng/L
1
12/6/2022 01:32
0.65
5.1
ng/L
1
12/5/202218:18
1.5
5.1
ng/L
1
12/5/202218:18
1.2
5.1
ng/L
1
12/5/202218:18
0.57
5.1
ng/L
1
12/6/202214:03
0.47
5.1
ng/L
1
12/5/202218:18
0.45
5.1
ng/L
1
12/5/202218:18
0.90
5.1
ng/L
1
12/5/202218:18
2.0
5.1
ng/L
1
12/5/202218:18
0.89
5.1
ng/L
1
12/6/2022 01:32
50-150
%REC
1
12/6/202214:03
50-150
%REC
1
12/6/2022 01:32
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/6/202214:03
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/6/202214:03
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
50-150
%REC
1
12/5/202218:18
AR Page 2 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-1:G113022
Collection Date: 11/30/2022 04:15 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-01
Matrix: WATER
Dilution
Units Factor Date Analyzed
Surr: d9-N-EtFOSE
69.9
50-150
%REC
1
12/5/2022 18:18
Surr: d3-N-McFOSA
67.6
50-150
%REC
1
12/5/2022 18:18
Surr: d3-N-McFOSAA
78.0
50-150
%REC
1
12/5/2022 18:18
Surr. d7-N-McFOSE
70.3
50-150
%REC
1
12/5/2022 18:18
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 08:19
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 08:19
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 08:19
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 08:19
1,1-Dichloroethane
2.9
0.44
1.0
pg/L
1
12/8/2022 08:19
1,1-Dichloroethene
13
0.40
1.0
pg/L
1
12/8/2022 08:19
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 08:19
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 08:19
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 08:19
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 08:19
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 08:19
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 08:19
1,2-Dichlorobenzene
0.75
J 0.32
1.0
pg/L
1
12/8/2022 08:19
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 08:19
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 08:19
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 08:19
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 08:19
1,4-Dichlorobenzene
U
0.35
1.0
pg/L
1
12/8/2022 08:19
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 08:19
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 08:19
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 08:19
Acetone
6.5
J 6.2
10
pg/L
1
12/8/2022 08:19
Benzene
1.1
0.46
1.0
pg/L
1
12/8/2022 08:19
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 08:19
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 08:19
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 08:19
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 08:19
Carbon disulfide
U
0.49
1.0
pg/L
1
12/8/2022 08:19
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 08:19
Chlorobenzene
U
0.40
1.0
pg/L
1
12/8/2022 08:19
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 08:19
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 08:19
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 08:19
cis-1,2-Dichloroethene
2,000
21
50
pg/L
50
12/9/202213:44
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 3 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:RW-1:G113022
Lab ID: 22120229-01
Collection Date: 11/30/2022 04:15 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 08:19
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 08:19
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 08:19
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 08:19
Ethylbenzene
0.76
J 0.34
1.0
pg/L
1
12/8/2022 08:19
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 08:19
m,p-Xylene
1.3
J 0.81
2.0
pg/L
1
12/8/2022 08:19
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 08:19
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 08:19
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 08:19
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 08:19
o-Xylene
0.88
J 0.31
1.0
pg/L
1
12/8/2022 08:19
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 08:19
Tetrachloroethene
2,300
20
50
pg/L
50
12/9/2022 13:44
Toluene
2.0
0.45
1.0
pg/L
1
12/8/2022 08:19
trans-1,2-Dichloroethene
74
0.48
1.0
pg/L
1
12/8/2022 08:19
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 08:19
Trichloroethene
1,100
22
50
pg/L
50
12/9/2022 13:44
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 08:19
Vinyl chloride
160
5.3
10
pg/L
10
12/8/2022 17:03
Xylenes, Total
2.1
J 0.81
3.0
pg/L
1
12/8/2022 08:19
Surr. 1,2-Dichloroethane-d4
102
80-120
%REC
1
12/8/2022 08:19
Surr 1,2-Dichloroethane-d4
112
80-120
%REC
10
12/8/2022 17:03
Surr 1,2-Dichloroethane-d4
112
80-120
%REC
50
12/9/2022 13:44
Surr. 4-Bromofluorobenzene
99.0
80-120
%REC
1
12/8/2022 08:19
Surr 4-Bromofluorobenzene
90.4
80-120
%REC
10
12/8/2022 17:03
Surr 4-Bromofluorobenzene
90.8
80-120
%REC
50
12/9/2022 13:44
Surr. Dibromofluoromethane
102
80-120
%REC
1
12/8/2022 08:19
Surr. Dibromofluoromethane
102
80-120
%REC
10
12/8/2022 17:03
Surr. Dibromofluoromethane
103
80-120
%REC
50
12/9/2022 13:44
Surr. Toluene-d8
99.4
80-120
%REC
1
12/8/2022 08:19
Surr Toluene-d8
97.1
80-120
%REC
10
12/8/2022 17:03
Surr Toluene-d8
103
80-120
%REC
50
12/9/2022 13:44
LOW LEVEL ALKALINITY
Method:A2320 B-11
Analyst: JMJ
Alkalinity, Bicarbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Carbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Hydroxide (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Total (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
CHLORIDE
Method:A4500-CL C-11
Analyst: AML
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 4 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-1:G113022
Collection Date: 11/30/2022 04:15 PM
Analyses
Chloride
HARDNESS
Hardness
NITROGEN, NITRATE -NITRITE
Nitrogen, Nitrate -Nitrite
PH (LABORATORY)
pH (laboratory)
Temperature
SULFATE
Sulfate
TOTAL DISSOLVED SOLIDS
Total Dissolved Solids
ORGANIC CARBON, TOTAL
Organic Carbon, Total
TOTAL SUSPENDED SOLIDS
Total Suspended Solids
Report
Result Qual MDL Limit
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-01
Matrix: WATER
Dilution
Units Factor Date Analyzed
5.00
2.2
3.0
mg/L
1
Method:A2340 C-11
1,300
2.2
5.0
mg/L CaCO3
1
Method: E353.2 R2.0
0.29
0.012
0.020
mg/L
1
Method: E150.1
5.59
H 0.10
0.10
s.u.
1
19.6
H 0.10
0.10
°C
1
Method:A4500-SO4 E-11
7.3
0.71
1.0
mg/L
1
Method:A2540 C-15
Prep: FILTER / 12/5/22
98
22
30
mg/L
1
Method: A531OC-14
6.0
0.14
0.50
mg/L
1
Method:A2540 D-15
Prep: FILTER / 12/6/22
29.0
3.8
6.0
mg/L
1
Note: See Qualifiers page for a list of qualifiers and their definitions.
12/6/2022 16:00
Analyst: TJH
12/6/2022 08:30
Analyst: JLS
12/6/2022 14:59
Analyst: JMJ
12/5/2022 10:42
12/5/2022 10:42
Analyst: AML
12/6/2022 15:25
Analyst: LAD
12/8/2022 12:10
Analyst: JB
12/3/2022 17:23
Analyst: SRN
12/7/2022 14:27
AR Page 5 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-2:G113022
Collection Date: 11/30/2022 04:24 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-02
Matrix: WATER
Dilution
Units Factor Date Analyzed
METALS BY ICP-MS
Method: E200.8
Prep: CEM-NPDES / 12/5/22
Analyst: STP
Iron
3.12
0.047
0.080
mg/L
1
12/5/202218:21
PFAS BY EPA 537 MODIFIED
Method: E537 MOD
Prep: E537 Mod / 12/5/22
Analyst: ENS
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
0.94
5.0
ng/L
1
12/5/2022 18:26
4:2)
Fluorotelomer Sulphonic Acid 6:2
20
1.9
5.0
ng/L
1
12/5/2022 18:26
(FtS 6:2)
Fluorotelomer Sulphonic Acid 8:2
22
1.1
5.0
ng/L
1
12/5/2022 18:26
(FtS 8:2)
Fluorotelomer Sulphonic Acid 10:2 (FtS
U
2.4
5.0
ng/L
1
12/5/2022 18:26
10:2)
Perfluorobutanesulfonic Acid (PFBS)
72
0.35
5.0
ng/L
1
12/5/2022 18:26
Perfluorobutanoic Acid (PFBA)
610
26
50
ng/L
10
12/6/2022 12:31
Perfluorodecanesulfonic Acid (PFDS)
U
1.4
5.0
ng/L
1
12/5/2022 18:26
Perfluorodecanoic Acid (PFDA)
250
1.3
5.0
ng/L
1
12/5/2022 18:26
Perfluorododecanesulfonic Acid
U
0.63
5.0
ng/L
1
12/5/2022 18:26
(PFDoS)
Perfluorododecanoic Acid (PFDoA)
14
0.70
5.0
ng/L
1
12/5/2022 18:26
Perfluoroheptanesulfonic Acid
58
0.57
5.0
ng/L
1
12/5/2022 18:26
(PFHpS)
Perfluoroheptanoic Acid (PFHpA)
1,100
17
50
ng/L
10
12/6/2022 12:31
Perfluorohexadecanoic Acid (PFHxDA)
U
1.8
5.0
ng/L
1
12/5/2022 18:26
Perfluorohexanesulfonic Acid
150
0.91
5.0
ng/L
1
12/5/2022 18:26
(PFHxS)
Perfluorohexanoic Acid (PFHxA)
2,900
12
50
ng/L
10
12/6/2022 12:31
Perfluorononanesulfonic Acid (PFNS)
U
0.50
5.0
ng/L
1
12/5/2022 18:26
Perfluorononanoic Acid (PFNA)
320
0.88
5.0
ng/L
1
12/5/2022 18:26
Perfluorooctadecanoic Acid (PFODA)
U
0.65
5.0
ng/L
1
12/5/2022 18:26
Perfluorooctanesulfonamide
7.1
0.72
5.0
ng/L
1
12/5/2022 18:26
(PFOSA)
Perfluorooctanesulfonic Acid (PFDS)
830
9.0
20
ng/L
10
12/6/2022 12:31
Perfluorooctanoic Acid (PFDA)
2,500
6.4
20
ng/L
10
12/6/2022 12:31
Perfluoropentanesulfonic Acid
49
0.56
5.0
ng/L
1
12/5/2022 18:26
(PFPeS)
Perfluoropentanoic Acid (PFPeA)
2,700
13
50
ng/L
10
12/6/2022 12:31
Perfluorotetradecanoic Acid (PFTeA)
U
2.7
5.0
ng/L
1
12/5/2022 18:26
Perfluorotridecanoic Acid (PFTriA)
U
1.9
5.0
ng/L
1
12/5/2022 18:26
Perfluoroundecanoic Acid (PFUnA)
16
0.98
5.0
ng/L
1
12/5/2022 18:26
N-ethylperfluoro-1-octanesulfonamide
U
1.2
5.0
ng/L
1
12/5/2022 18:26
N-
U
1.6
5.0
ng/L
1
12/5/2022 18:26
Ethyl perfluorooctanesulfonamidoacetic
Acid
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page 6 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-2:G113022
Collection Date: 11/30/2022 04:24 PM
Analyses
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-02
Matrix: WATER
Report Dilution
Result Qual MDL Limit Units Factor Date Analyzed
N-
U
Ethyl perfluorooctanesulfonamidoethano
I
N-methylperfluoro-1-
1.3
J
octanesulfonamide
N-
58
Methyl perfluorooctanesulfonamidoa
cetic Acid
N-
U
Methylperfluorooctanesulfonamidoetha
nol
Hexafluoropropylene oxide dimer
11
acid (HFPO-DA)
4,8-Dioxa-3H-perfluorononanoic Acid
U
(DONA)
11 CI-Pf30UdS
U
9CI-PF30NS
U
Perfluoro-4-ethylcyclohexanesulfonic
U
Acid (PFecHS)
Perfluorobutylsulfonamide (PFBSA)
27
Perfluorohexanesulfonamide
16
(PFHxSA)
Surr: 13C2-FtS 4:2
137
Surr. 13C2-FtS 6:2
71.9
Surr 13C2-FtS 8:2
88.8
Surr 13C2-PFDA
58.2
Surr 13C2-PFDoA
73.8
Surr 13C2-PFHxA
64.9
Surr 13C2-PFHxDA
62.9
Surr 13C2-PFTeA
72.9
Surr: 13C2-PFUnA
63.4
Surr. 13C3-HFPO-DA
65.7
Surr: 13C3-PFBS
62.0
Surr. 13C4-PFBA
55.7
Surr. 13C4-PFHpA
76.8
Surr 13C4-PFOA
46.3
S
Surr. 13C4-PFOS
56.0
Surr 13C5-PFNA
75.5
Surr 13C5-PFPeA
42.4
S
Surr 13C8-FOSA
69.4
Surr 1802-PFHxS
46.7
S
Surr d5-N-EtFOSA
40.5
S
Surr d5-N-EtFOSAA
86.2
Note: See Qualifiers page for a list of qualifiers and their definitions
1.1 5.0 ng/L 1 12/5/202218:26
0.80
5.0
ng/L
1
12/6/2022 01:41
0.65
5.0
ng/L
1
12/5/202218:26
1.5
5.0
ng/L
1
12/5/202218:26
1.2
5.0
ng/L
1
12/5/202218:26
0.57
5.0
ng/L
1
12/6/202214:11
0.47
5.0
ng/L
1
12/5/202218:26
0.45
5.0
ng/L
1
12/5/202218:26
0.89
5.0
ng/L
1
12/5/202218:26
2.0
5.0
ng/L
1
12/5/202218:26
0.89
5.0
ng/L
1
12/6/2022 01:41
50-150
%REC
1
12/6/202214:11
50-150
%REC
1
12/6/2022 01:41
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/6/202214:11
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/6/202214:11
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
50-150
%REC
1
12/5/202218:26
AR Page 7 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-2:G113022
Collection Date: 11/30/2022 04:24 PM
Analyses
Result
Qual
MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-02
Matrix: WATER
Dilution
Units Factor Date Analyzed
Surr: d9-N-EtFOSE
59.0
50-150
%REC
1
12/5/2022 18:26
Surr: d3-N-McFOSA
42.3
S
50-150
%REC
1
12/5/2022 18:26
Surr: d3-N-McFOSAA
68.7
50-150
%REC
1
12/5/2022 18:26
Surr. d7-N-McFOSE
65.8
50-150
%REC
1
12/5/2022 18:26
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 08:42
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 08:42
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 08:42
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 08:42
1,1-Dichloroethane
1.2
0.44
1.0
pg/L
1
12/8/2022 08:42
1,1-Dichloroethene
14
0.40
1.0
pg/L
1
12/8/2022 08:42
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 08:42
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 08:42
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 08:42
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 08:42
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 08:42
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 08:42
1,2-Dichlorobenzene
0.94
J
0.32
1.0
pg/L
1
12/8/2022 08:42
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 08:42
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 08:42
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 08:42
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 08:42
1,4-Dichlorobenzene
U
0.35
1.0
pg/L
1
12/8/2022 08:42
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 08:42
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 08:42
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 08:42
Acetone
6.3
J
6.2
10
pg/L
1
12/8/2022 08:42
Benzene
1.8
0.46
1.0
pg/L
1
12/8/2022 08:42
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 08:42
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 08:42
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 08:42
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 08:42
Carbon disulfide
0.93
J
0.49
1.0
pg/L
1
12/8/2022 08:42
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 08:42
Chlorobenzene
U
0.40
1.0
pg/L
1
12/8/2022 08:42
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 08:42
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 08:42
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 08:42
cis-1,2-Dichloroethene
6,100
42
100
pg/L
100
12/9/202214:00
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 8 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-2:G113022
Collection Date: 11/30/2022 04:24 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-02
Matrix: WATER
Dilution
Units Factor Date Analyzed
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 08:42
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 08:42
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 08:42
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 08:42
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 08:42
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 08:42
m,p-Xylene
0.89
J 0.81
2.0
pg/L
1
12/8/2022 08:42
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 08:42
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 08:42
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 08:42
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 08:42
o-Xylene
1.5
0.31
1.0
pg/L
1
12/8/2022 08:42
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 08:42
Tetrachloroethene
100
39
100
pg/L
100
12/9/2022 14:00
Toluene
0.47
J 0.45
1.0
pg/L
1
12/8/2022 08:42
trans-1,2-Dichloroethene
60
0.48
1.0
pg/L
1
12/8/2022 08:42
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 08:42
Trichloroethene
100
43
100
pg/L
100
12/9/2022 14:00
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 08:42
Vinyl chloride
500
53
100
pg/L
100
12/9/2022 14:00
Xylenes, Total
2.4
J 0.81
3.0
pg/L
1
12/8/2022 08:42
Surr. 1,2-Dichloroethane-d4
105
80-120
%REC
1
12/8/2022 08:42
Surr 1,2-Dichloroethane-d4
118
80-120
%REC
100
12/9/2022 14:00
Surr 4-Bromofluorobenzene
95.0
80-120
%REC
1
12/8/2022 08:42
Surr 4-Bromofluorobenzene
87.3
80-120
%REC
100
12/9/2022 14:00
Surr. Dibromofluoromethane
105
80-120
%REC
1
12/8/2022 08:42
Surr. Dibromofluoromethane
102
80-120
%REC
100
12/9/2022 14:00
Surr. Toluene-d8
98.4
80-120
%REC
1
12/8/2022 08:42
Surr. Toluene-d8
101
80-120
%REC
100
12/9/2022 14:00
LOW LEVEL ALKALINITY
Method:A2320 B-11
Analyst: JMJ
Alkalinity, Bicarbonate (as CaCO3)
24
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Carbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Hydroxide (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Total (as CaCO3)
24
1.4
2.0
mg/L
1
12/6/2022 12:27
CHLORIDE
Method:A4500-CL C-11
Analyst: AML
Chloride
25.0
2.2
3.0
mg/L
1
12/6/202216:00
HARDNESS
Method:A2340 C-11
Analyst: TJH
Hardness
120
2.2
5.0
mg/L CaCO3 1
12/7/2022 11:00
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 9 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-2:G113022
Collection Date: 11/30/2022 04:24 PM
Analyses
NITROGEN, NITRATE -NITRITE
Nitrogen, Nitrate -Nitrite
PH (LABORATORY)
pH (laboratory)
Temperature
SULFATE
Sulfate
TOTAL DISSOLVED SOLIDS
Total Dissolved Solids
ORGANIC CARBON, TOTAL
Organic Carbon, Total
TOTAL SUSPENDED SOLIDS
Total Suspended Solids
Report
Result Qual MDL Limit
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-02
Matrix: WATER
Dilution
Units Factor Date Analyzed
Method: E353.2 R2.0
0.21
0.012
0.020
mg/L 1
Method: El50.1
5.57
H 0.10
0.10
s.u. 1
19.8
H 0.10
0.10
°C 1
Method:A4500-SO4 E-11
16
0.71
1.0
mg/L 1
Method:A2540 C-15
Prep: FILTER / 12/5/22
160
22
30
mg/L 1
Method: A531OC-14
9.6
0.14
0.50
mg/L 1
Method:A2540 D-15
Prep: FILTER / 12/6/22
U
0.76
1.2
mg/L 1
Note: See Qualifiers page for a list of qualifiers and their definitions.
Analyst: JLS
12/6/2022 15:00
Analyst: JMJ
12/5/2022 10:42
12/5/2022 10:42
Analyst: AML
12/6/2022 13:13
Analyst: LAD
12/8/2022 12:10
Analyst: JB
12/3/2022 17:57
Analyst: SRN
12/7/2022 14:27
AR Page 10 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022
Collection Date: 11/30/2022 04:30 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-03
Matrix: WATER
Dilution
Units Factor Date Analyzed
METALS BY ICP-MS
Method: E200.8
Prep: CEM-NPDES / 12/5/22
Analyst: STP
Iron
1.65
0.047
0.080
mg/L
1
12/5/202218:23
PFAS BY EPA 537 MODIFIED
Method: E537 MOD
Prep: E537 Mod / 12/5/22
Analyst: ENS
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
0.91
4.9
ng/L
1
12/5/2022 18:35
4:2)
Fluorotelomer Sulphonic Acid 6:2
2.5
J 1.9
4.9
ng/L
1
12/5/2022 18:35
(FtS 6:2)
Fluorotelomer Sulphonic Acid 8:2
4.6
J 1.1
4.9
ng/L
1
12/5/2022 18:35
(FtS 8:2)
Fluorotelomer Sulphonic Acid 10:2 (FtS
U
2.3
4.9
ng/L
1
12/5/2022 18:35
10:2)
Perfluorobutanesulfonic Acid (PFBS)
32
0.34
4.9
ng/L
1
12/5/2022 18:35
Perfluorobutanoic Acid (PFBA)
170
2.5
4.9
ng/L
1
12/5/2022 18:35
Perfluorodecanesulfonic Acid (PFDS)
U
1.3
4.9
ng/L
1
12/5/2022 18:35
Perfluorodecanoic Acid (PFDA)
51
1.2
4.9
ng/L
1
12/5/2022 18:35
Perfluorododecanesulfonic Acid
U
0.61
4.9
ng/L
1
12/5/2022 18:35
(PFDoS)
Perfluorododecanoic Acid (PFDoA)
2.1
J 0.67
4.9
ng/L
1
12/5/2022 18:35
Perfluoroheptanesulfonic Acid
27
0.55
4.9
ng/L
1
12/5/2022 18:35
(PFHpS)
Perfluoroheptanoic Acid (PFHpA)
360
1.7
4.9
ng/L
1
12/5/2022 18:35
Perfluorohexadecanoic Acid (PFHxDA)
U
1.8
4.9
ng/L
1
12/5/2022 18:35
Perfluorohexanesulfonic Acid
55
0.88
4.9
ng/L
1
12/5/2022 18:35
(PFHxS)
Perfluorohexanoic Acid (PFHxA)
600
12
49
ng/L
10
12/6/2022 12:39
Perfluorononanesulfonic Acid (PFNS)
U
0.48
4.9
ng/L
1
12/5/2022 18:35
Perfluorononanoic Acid (PFNA)
75
0.85
4.9
ng/L
1
12/5/2022 18:35
Perfluorooctadecanoic Acid (PFODA)
U
0.63
4.9
ng/L
1
12/5/2022 18:35
Perfluorooctanesulfonamide
1.8
J 0.69
4.9
ng/L
1
12/5/2022 18:35
(PFOSA)
Perfluorooctanesulfonic Acid (PFDS)
520
8.7
19
ng/L
10
12/6/2022 12:39
Perfluorooctanoic Acid (PFDA)
580
6.1
19
ng/L
10
12/6/2022 12:39
Perfluoropentanesulfonic Acid
19
0.54
4.9
ng/L
1
12/5/2022 18:35
(PFPeS)
Perfluoropentanoic Acid (PFPeA)
540
12
49
ng/L
10
12/6/2022 12:39
Perfluorotetradecanoic Acid (PFTeA)
U
2.6
4.9
ng/L
1
12/5/2022 18:35
Perfluorotridecanoic Acid (PFTriA)
U
1.9
4.9
ng/L
1
12/5/2022 18:35
Perfluoroundecanoic Acid (PFUnA)
12
0.95
4.9
ng/L
1
12/5/2022 18:35
N-ethylperfluoro-1-octanesulfonamide
U
1.1
4.9
ng/L
1
12/5/2022 18:35
N-
U
1.5
4.9
ng/L
1
12/5/2022 18:35
Ethyl perfluorooctanesulfonamidoacetic
Acid
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page I I of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:RW-3:G113022
Lab ID: 22120229-03
Collection Date: 11/30/2022 04:30 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
N-
U
1.0
4.9
ng/L
1
12/5/2022 18:35
Ethyl perfluorooctanesulfonamidoethano
I
N-methylperfluoro-1-octanesulfonamide
U
0.77
4.9
ng/L
1
12/6/2022 01:49
N-
40
0.63
4.9
ng/L
1
12/5/2022 18:35
Methylperfluorooctanesulfonamidoa
cetic Acid
N-
U
1.5
4.9
ng/L
1
12/5/2022 18:35
Methylperfluorooctanesulfonamidoetha
nol
Hexafluoropropylene oxide dimer
8.3
1.1
4.9
ng/L
1
12/5/2022 18:35
acid (HFPO-DA)
4,8-Dioxa-3H-perfluorononanoic Acid
U
0.55
4.9
ng/L
1
12/6/2022 14:20
(DONA)
11 CI-Pf30UdS
U
0.45
4.9
ng/L
1
12/5/2022 18:35
9CI-PF30NS
U
0.44
4.9
ng/L
1
12/5/2022 18:35
Perfluoro-4-ethylcyclohexanesulfonic
U
0.86
4.9
ng/L
1
12/5/2022 18:35
Acid (PFecHS)
Perfluorobutylsulfonamide (PFBSA)
6.2
1.9
4.9
ng/L
1
12/5/2022 18:35
Perfluorohexanesulfonamide
3.9
J 0.85
4.9
ng/L
1
12/6/2022 01:49
(PFHxSA)
Surr: 13C2-FtS 4:2
160
S
50-150
%REC
1
12/6/2022 14:20
Surr: 13C2-FtS 6:2
112
50-150
%REC
1
12/6/2022 01:49
Surr. 13C2-FtS 8:2
102
50-150
%REC
1
12/5/2022 18:35
Surr 13C2-PFDA
57.5
50-150
%REC
1
12/5/2022 18:35
Surr 13C2-PFDoA
71.5
50-150
%REC
1
12/5/2022 18:35
Surr 13C2-PFHxA
108
50-150
%REC
1
12/6/2022 14:20
Surr 13C2-PFHxDA
63.7
50-150
%REC
1
12/5/2022 18:35
Surr 13C2-PFTeA
77.9
50-150
%REC
1
12/5/2022 18:35
Surr 13C2-PFUnA
69.4
50-150
%REC
1
12/5/2022 18:35
Surr 13C3-HFPO-DA
68.6
50-150
%REC
1
12/5/2022 18:35
Surr 13C3-PFBS
56.0
50-150
%REC
1
12/5/2022 18:35
Surr 13C4-PFBA
60.8
50-150
%REC
1
12/5/2022 18:35
Surr 13C4-PFHpA
126
50-150
%REC
1
12/6/2022 14:20
Surr 13C4-PFOA
53.3
50-150
%REC
1
12/5/2022 18:35
Surr 13C4-PFOS
53.7
50-150
%REC
1
12/5/2022 18:35
Surr 13C5-PFNA
83.6
50-150
%REC
1
12/5/2022 18:35
Surr 13C5-PFPeA
60.3
50-150
%REC
1
12/5/2022 18:35
Surr 13C8-FOSA
70.2
50-150
%REC
1
12/5/2022 18:35
Surr 1802-PFHxS
57.8
50-150
%REC
1
12/5/2022 18:35
Surr d5-N-EtFOSA
47.7
S
50-150
%REC
1
12/5/2022 18:35
Surr d5-N-EtFOSAA
94.6
50-150
%REC
1
12/5/2022 18:35
Surr: d9-N-EtFOSE
63.6
50-150
%REC
1
12/5/2022 18:35
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page 12 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022
Collection Date: 11/30/2022 04:30 PM
Analyses
Result
Qual
MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-03
Matrix: WATER
Dilution
Units Factor Date Analyzed
Surr: d3-N-McFOSA
46.5
S
50-150
%REC
1
12/5/2022 18:35
Surr: d3-N-McFOSAA
66.6
50-150
%REC
1
12/5/2022 18:35
Surr: d7-N-McFOSE
67.4
50-150
%REC
1
12/5/2022 18:35
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 09:06
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 09:06
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 09:06
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 09:06
1,1-Dichloroethane
0.65
J
0.44
1.0
pg/L
1
12/8/2022 09:06
1,1-Dichloroethene
4.7
0.40
1.0
pg/L
1
12/8/2022 09:06
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 09:06
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 09:06
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 09:06
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 09:06
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 09:06
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 09:06
1,2-Dichlorobenzene
U
0.32
1.0
pg/L
1
12/8/2022 09:06
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 09:06
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 09:06
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 09:06
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 09:06
1,4-Dichlorobenzene
0.61
J
0.35
1.0
pg/L
1
12/8/2022 09:06
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 09:06
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 09:06
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 09:06
Acetone
U
6.2
10
pg/L
1
12/8/2022 09:06
Benzene
0.62
J
0.46
1.0
pg/L
1
12/8/2022 09:06
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 09:06
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 09:06
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 09:06
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 09:06
Carbon disulfide
U
0.49
1.0
pg/L
1
12/8/2022 09:06
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 09:06
Chlorobenzene
0.82
J
0.40
1.0
pg/L
1
12/8/2022 09:06
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 09:06
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 09:06
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 09:06
cis-1,2-Dichloroethene
1,800
8.4
20
pg/L
20
12/8/202217:58
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 09:06
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 13 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022
Collection Date: 11/30/2022 04:30 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-03
Matrix: WATER
Dilution
Units Factor Date Analyzed
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 09:06
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 09:06
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 09:06
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 09:06
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 09:06
m,p-Xylene
U
0.81
2.0
pg/L
1
12/8/2022 09:06
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 09:06
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 09:06
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 09:06
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 09:06
o-Xylene
0.31
J 0.31
1.0
pg/L
1
12/8/2022 09:06
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 09:06
Tetrachloroethene
60
0.39
1.0
pg/L
1
12/8/2022 09:06
Toluene
U
0.45
1.0
pg/L
1
12/8/2022 09:06
trans-1,2-Dichloroethene
12
0.48
1.0
pg/L
1
12/8/2022 09:06
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 09:06
Trichloroethene
31
0.43
1.0
pg/L
1
12/8/2022 09:06
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 09:06
Vinyl chloride
310
11
20
pg/L
20
12/8/2022 17:58
Xylenes, Total
U
0.81
3.0
pg/L
1
12/8/2022 09:06
Surr. 1,2-Dichloroethane-d4
105
80-120
%REC
1
12/8/2022 09:06
Surr 1,2-Dichloroethane-d4
105
80-120
%REC
20
12/8/2022 17:58
Surr 4-Bromofluorobenzene
97.3
80-120
%REC
1
12/8/2022 09:06
Surr 4-Bromofluorobenzene
99.0
80-120
%REC
20
12/8/2022 17:58
Surr. Dibromofluoromethane
102
80-120
%REC
1
12/8/2022 09:06
Surr. Dibromofluoromethane
98.6
80-120
%REC
20
12/8/2022 17:58
Surr: Toluene-d8
98.2
80-120
%REC
1
12/8/2022 09:06
Surr. Toluene-d8
101
80-120
%REC
20
12/8/2022 17:58
LOW LEVEL ALKALINITY
Method:A2320 B-11
Analyst: JMJ
Alkalinity, Bicarbonate (as CaCO3)
8.2
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Carbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Hydroxide (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Total (as CaCO3)
8.2
1.4
2.0
mg/L
1
12/6/2022 12:27
CHLORIDE
Method:A4500-CL C-11
Analyst: AML
Chloride
15.0
2.2
3.0
mg/L
1
12/6/202216:00
HARDNESS
Method:A2340 C-11
Analyst: TJH
Hardness
65
2.2
5.0
mg/L CaCO3 1
12/7/2022 11:00
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 14 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022
Collection Date: 11/30/2022 04:30 PM
Analyses
NITROGEN, NITRATE -NITRITE
Nitrogen, Nitrate -Nitrite
PH (LABORATORY)
pH (laboratory)
Temperature
SULFATE
Sulfate
TOTAL DISSOLVED SOLIDS
Total Dissolved Solids
ORGANIC CARBON, TOTAL
Organic Carbon, Total
TOTAL SUSPENDED SOLIDS
Total Suspended Solids
Report
Result Qual MDL Limit
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-03
Matrix: WATER
Dilution
Units Factor Date Analyzed
Method: E353.2 R2.0
0.30
0.012
0.020
mg/L 1
Method: El50.1
5.51
H 0.10
0.10
s.u. 1
19.8
H 0.10
0.10
°C 1
Method:A4500-SO4 E-11
15
0.71
1.0
mg/L 1
Method:A2540 C-15
Prep: FILTER / 12/5/22
140
22
30
mg/L 1
Method: A531OC-14
7.3
0.14
0.50
mg/L 1
Method:A2540 D-15
Prep: FILTER / 12/6/22
0.500
J 0.38
0.60
mg/L 1
Note: See Qualifiers page for a list of qualifiers and their definitions.
Analyst: JLS
12/6/2022 15:03
Analyst: JMJ
12/5/2022 10:42
12/5/2022 10:42
Analyst: AML
12/6/2022 13:13
Analyst: LAD
12/8/2022 12:10
Analyst: JB
12/3/2022 18:31
Analyst: SRN
12/7/2022 14:27
AR Page 15 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022A
Collection Date: 11/30/2022 04:30 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-04
Matrix: WATER
Dilution
Units Factor Date Analyzed
METALS BY ICP-MS
Method: E200.8
Prep: CEM-NPDES / 12/5/22
Analyst: STP
Iron
1.65
0.047
0.080
mg/L
1
12/5/202218:25
PFAS BY EPA 537 MODIFIED
Method: E537 MOD
Prep: E537 Mod / 12/5/22
Analyst: ENS
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
0.90
4.8
ng/L
1
12/5/2022 18:43
4:2)
Fluorotelomer Sulphonic Acid 6:2
3.9
J 1.8
4.8
ng/L
1
12/5/2022 18:43
(FtS 6:2)
Fluorotelomer Sulphonic Acid 8:2
6.8
1.1
4.8
ng/L
1
12/5/2022 18:43
(FtS 8:2)
Fluorotelomer Sulphonic Acid 10:2 (FtS
U
2.3
4.8
ng/L
1
12/5/2022 18:43
10:2)
Perfluorobutanesulfonic Acid (PFBS)
31
0.34
4.8
ng/L
1
12/5/2022 18:43
Perfluorobutanoic Acid (PFBA)
170
2.5
4.8
ng/L
1
12/5/2022 18:43
Perfluorodecanesulfonic Acid (PFDS)
U
1.3
4.8
ng/L
1
12/5/2022 18:43
Perfluorodecanoic Acid (PFDA)
52
1.2
4.8
ng/L
1
12/5/2022 18:43
Perfluorododecanesulfonic Acid
U
0.60
4.8
ng/L
1
12/5/2022 18:43
(PFDoS)
Perfluorododecanoic Acid (PFDoA)
2.7
J 0.66
4.8
ng/L
1
12/5/2022 18:43
Perfluoroheptanesulfonic Acid
33
0.54
4.8
ng/L
1
12/5/2022 18:43
(PFHpS)
Perfluoroheptanoic Acid (PFHpA)
390
1.7
4.8
ng/L
1
12/5/2022 18:43
Perfluorohexadecanoic Acid (PFHxDA)
U
1.7
4.8
ng/L
1
12/5/2022 18:43
Perfluorohexanesulfonic Acid
75
0.87
4.8
ng/L
1
12/5/2022 18:43
(PFHxS)
Perfluorohexanoic Acid (PFHxA)
530
12
48
ng/L
10
12/6/2022 12:47
Perfluorononanesulfonic Acid (PFNS)
U
0.48
4.8
ng/L
1
12/5/2022 18:43
Perfluorononanoic Acid (PFNA)
81
0.84
4.8
ng/L
1
12/5/2022 18:43
Perfluorooctadecanoic Acid (PFODA)
U
0.62
4.8
ng/L
1
12/5/2022 18:43
Perfluorooctanesulfonamide
1.4
J 0.68
4.8
ng/L
1
12/5/2022 18:43
(PFOSA)
Perfluorooctanesulfonic Acid (PFDS)
450
8.6
19
ng/L
10
12/6/2022 12:47
Perfluorooctanoic Acid (PFDA)
530
6.1
19
ng/L
10
12/6/2022 12:47
Perfluoropentanesulfonic Acid
28
0.53
4.8
ng/L
1
12/5/2022 18:43
(PFPeS)
Perfluoropentanoic Acid (PFPeA)
500
12
48
ng/L
10
12/6/2022 12:47
Perfluorotetradecanoic Acid (PFTeA)
U
2.5
4.8
ng/L
1
12/5/2022 18:43
Perfluorotridecanoic Acid (PFTriA)
U
1.9
4.8
ng/L
1
12/5/2022 18:43
Perfluoroundecanoic Acid (PFUnA)
11
0.94
4.8
ng/L
1
12/5/2022 18:43
N-ethylperfluoro-1-octanesulfonamide
U
1.1
4.8
ng/L
1
12/5/2022 18:43
N-
U
1.5
4.8
ng/L
1
12/5/2022 18:43
Ethyl perfluorooctanesulfonamidoacetic
Acid
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page 16 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:RW-3:G113022A
Lab ID: 22120229-04
Collection Date: 11/30/2022 04:30 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
N-
U
1.0
4.8
ng/L
1
12/5/2022 18:43
Ethyl perfluorooctanesulfonamidoethano
I
N-methylperfluoro-1-octanesulfonamide
U
0.76
4.8
ng/L
1
12/6/2022 01:57
N-
38
0.62
4.8
ng/L
1
12/5/2022 18:43
Methylperfluorooctanesulfonamidoa
cetic Acid
N-
U
1.4
4.8
ng/L
1
12/5/2022 18:43
Methylperfluorooctanesulfonamidoetha
nol
Hexafluoropropylene oxide dimer
8.2
1.1
4.8
ng/L
1
12/5/2022 18:43
acid (HFPO-DA)
4,8-Dioxa-3H-perfluorononanoic Acid
U
0.54
4.8
ng/L
1
12/6/2022 14:28
(DONA)
11 CI-Pf30UdS
U
0.45
4.8
ng/L
1
12/5/2022 18:43
9CI-PF30NS
U
0.43
4.8
ng/L
1
12/5/2022 18:43
Perfluoro-4-ethylcyclohexanesulfonic
U
0.85
4.8
ng/L
1
12/5/2022 18:43
Acid (PFecHS)
Perfluorobutylsulfonamide (PFBSA)
6.1
1.9
4.8
ng/L
1
12/5/2022 18:43
Perfluorohexanesulfonamide
4.1
J 0.84
4.8
ng/L
1
12/6/2022 01:57
(PFHxSA)
Surr: 13C2-FtS 4:2
56.4
50-150
%REC
1
12/6/2022 14:28
Surr: 13C2-FtS 6:2
105
50-150
%REC
1
12/6/2022 01:57
Surr. 13C2-FtS 8:2
91.3
50-150
%REC
1
12/5/2022 18:43
Surr 13C2-PFDA
64.0
50-150
%REC
1
12/5/2022 18:43
Surr 13C2-PFDoA
71.3
50-150
%REC
1
12/5/2022 18:43
Surr 13C2-PFHxA
40.9
S
50-150
%REC
1
12/6/2022 14:28
Surr 13C2-PFHxDA
60.9
50-150
%REC
1
12/5/2022 18:43
Surr 13C2-PFTeA
69.8
50-150
%REC
1
12/5/2022 18:43
Surr 13C2-PFUnA
62.5
50-150
%REC
1
12/5/2022 18:43
Surr 13C3-HFPO-DA
68.7
50-150
%REC
1
12/5/2022 18:43
Surr 13C3-PFBS
61.4
50-150
%REC
1
12/5/2022 18:43
Surr 13C4-PFBA
61.6
50-150
%REC
1
12/5/2022 18:43
Surr 13C4-PFHpA
44.9
S
50-150
%REC
1
12/6/2022 14:28
Surr 13C4-PFOA
59.0
50-150
%REC
1
12/5/2022 18:43
Surr 13C4-PFOS
62.7
50-150
%REC
1
12/5/2022 18:43
Surr 13C5-PFNA
77.6
50-150
%REC
1
12/5/2022 18:43
Surr 13C5-PFPeA
61.2
50-150
%REC
1
12/5/2022 18:43
Surr 13C8-FOSA
70.8
50-150
%REC
1
12/5/2022 18:43
Surr 1802-PFHxS
46.1
S
50-150
%REC
1
12/5/2022 18:43
Surr d5-N-EtFOSA
45.9
S
50-150
%REC
1
12/5/2022 18:43
Surr d5-N-EtFOSAA
90.3
50-150
%REC
1
12/5/2022 18:43
Surr: d9-N-EtFOSE
64.2
50-150
%REC
1
12/5/2022 18:43
Note: See Qualifiers page for a list of qualifiers and their definitions
AR Page 17 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:RW-3:G113022A
Lab ID: 22120229-04
Collection Date: 11/30/2022 04:30 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual
MDL
Limit
Units
Factor Date Analyzed
Surr: d3-N-McFOSA
50.4
50-150
%REC
1
12/5/2022 18:43
Surr: d3-N-McFOSAA
73.1
50-150
%REC
1
12/5/2022 18:43
Surr: d7-N-McFOSE
62.5
50-150
%REC
1
12/5/2022 18:43
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 00:54
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 00:54
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 00:54
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 00:54
1,1-Dichloroethane
0.79
J
0.44
1.0
pg/L
1
12/8/2022 00:54
1,1-Dichloroethene
5.0
0.40
1.0
pg/L
1
12/8/2022 00:54
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 00:54
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 00:54
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 00:54
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 00:54
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 00:54
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 00:54
1,2-Dichlorobenzene
U
0.32
1.0
pg/L
1
12/8/2022 00:54
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 00:54
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 00:54
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 00:54
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 00:54
1,4-Dichlorobenzene
0.75
J
0.35
1.0
pg/L
1
12/8/2022 00:54
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 00:54
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 00:54
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 00:54
Acetone
U
6.2
10
pg/L
1
12/8/2022 00:54
Benzene
0.82
J
0.46
1.0
pg/L
1
12/8/2022 00:54
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 00:54
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 00:54
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 00:54
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 00:54
Carbon disulfide
0.52
J
0.49
1.0
pg/L
1
12/8/2022 00:54
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 00:54
Chlorobenzene
0.83
J
0.40
1.0
pg/L
1
12/8/2022 00:54
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 00:54
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 00:54
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 00:54
cis-1,2-Dichloroethene
1,700
21
50
pg/L
50
12/8/202218:16
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 00:54
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 18 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022A
Collection Date: 11/30/2022 04:30 PM
Analyses
Result
Qual MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-04
Matrix: WATER
Dilution
Units Factor Date Analyzed
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 00:54
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 00:54
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 00:54
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 00:54
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 00:54
m,p-Xylene
U
0.81
2.0
pg/L
1
12/8/2022 00:54
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 00:54
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 00:54
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 00:54
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 00:54
o-Xylene
0.48
J 0.31
1.0
pg/L
1
12/8/2022 00:54
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 00:54
Tetrachloroethene
57
0.39
1.0
pg/L
1
12/8/2022 00:54
Toluene
U
0.45
1.0
pg/L
1
12/8/2022 00:54
trans-1,2-Dichloroethene
14
0.48
1.0
pg/L
1
12/8/2022 00:54
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 00:54
Trichloroethene
31
0.43
1.0
pg/L
1
12/8/2022 00:54
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 00:54
Vinyl chloride
280
26
50
pg/L
50
12/8/2022 18:16
Xylenes, Total
U
0.81
3.0
pg/L
1
12/8/2022 00:54
Surr. 1,2-Dichloroethane-d4
95.1
80-120
%REC
1
12/8/2022 00:54
Surr 1,2-Dichloroethane-d4
108
80-120
%REC
50
12/8/2022 18:16
Surr 4-Bromofluorobenzene
98.2
80-120
%REC
1
12/8/2022 00:54
Surr 4-Bromofluorobenzene
101
80-120
%REC
50
12/8/2022 18:16
Surr. Dibromofluoromethane
95.7
80-120
%REC
1
12/8/2022 00:54
Surr. Dibromofluoromethane
99.4
80-120
%REC
50
12/8/2022 18:16
Surr: Toluene-d8
95.6
80-120
%REC
1
12/8/2022 00:54
Surr. Toluene-d8
102
80-120
%REC
50
12/8/2022 18:16
LOW LEVEL ALKALINITY
Method:A2320 B-11
Analyst: JMJ
Alkalinity, Bicarbonate (as CaCO3)
2.9
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Carbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Hydroxide (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Total (as CaCO3)
2.9
1.4
2.0
mg/L
1
12/6/2022 12:27
CHLORIDE
Method:A4500-CL C-11
Analyst: AML
Chloride
10.0
2.2
3.0
mg/L
1
12/6/202216:00
HARDNESS
Method:A2340 C-11
Analyst: TJH
Hardness
40
2.2
5.0
mg/L CaCO3 1
12/7/2022 11:00
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 19 of 29

ALS Group, USA
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:RW-3:G113022A
Collection Date: 11/30/2022 04:30 PM
Analyses
NITROGEN, NITRATE -NITRITE
Nitrogen, Nitrate -Nitrite
PH (LABORATORY)
pH (laboratory)
Temperature
SULFATE
Sulfate
TOTAL DISSOLVED SOLIDS
Total Dissolved Solids
ORGANIC CARBON, TOTAL
Organic Carbon, Total
TOTAL SUSPENDED SOLIDS
Total Suspended Solids
Report
Result Qual MDL Limit
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-04
Matrix: WATER
Dilution
Units Factor Date Analyzed
Method: E353.2 R2.0
0.32
0.012
0.020
mg/L 1
Method: El50.1
5.47
H 0.10
0.10
s.u. 1
19.8
H 0.10
0.10
°C 1
Method:A4500-SO4 E-11
16
0.71
1.0
mg/L 1
Method:A2540 C-15
Prep: FILTER / 12/5/22
140
22
30
mg/L 1
Method: A531OC-14
7.3
0.14
0.50
mg/L 1
Method:A2540 D-15
Prep: FILTER / 12/6/22
U
0.38
0.60
mg/L 1
Note: See Qualifiers page for a list of qualifiers and their definitions.
Analyst: JLS
12/6/2022 15:07
Analyst: JMJ
12/5/2022 10:42
12/5/2022 10:42
Analyst: AML
12/6/2022 13:13
Analyst: LAD
12/8/2022 12:10
Analyst: JB
12/3/2022 19:04
Analyst: SRN
12/7/2022 14:27
AR Page 20 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:FB-1:W113022
Lab ID: 22120229-05
Collection Date: 11/30/2022 04:19 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
METALS BY ICP-MS
Method: E200.8
Prep: CEM-NPDES / 12/5/22
Analyst: STP
Iron
U
0.047
0.080
mg/L
1
12/5/202218:26
PFAS BY EPA 537 MODIFIED
Method: E537 MOD
Prep: E537 Mod / 12/5/22
Analyst: ENS
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
0.93
4.9
ng/L
1
12/5/2022 18:51
4:2)
Fluorotelomer Sulphonic Acid 6:2 (FtS
U
1.9
4.9
ng/L
1
12/5/2022 18:51
6:2)
Fluorotelomer Sulphonic Acid 8:2 (FtS
U
1.1
4.9
ng/L
1
12/5/2022 18:51
8:2)
Fluorotelomer Sulphonic Acid 10:2 (FtS
U
2.3
4.9
ng/L
1
12/5/2022 18:51
10:2)
Perfluorobutanesulfonic Acid (PFBS)
U
0.35
4.9
ng/L
1
12/5/2022 18:51
Perfluorobutanoic Acid (PFBA)
U
2.6
4.9
ng/L
1
12/5/2022 18:51
Perfluorodecanesulfonic Acid (PFDS)
U
1.4
4.9
ng/L
1
12/5/2022 18:51
Perfluorodecanoic Acid (PFDA)
U
1.2
4.9
ng/L
1
12/5/2022 18:51
Perfluorododecanesulfonic Acid
U
0.62
4.9
ng/L
1
12/5/2022 18:51
(PFDoS)
Perfluorododecanoic Acid (PFDoA)
U
0.68
4.9
ng/L
1
12/5/2022 18:51
Perfluoroheptanesulfonic Acid (PFHpS)
U
0.56
4.9
ng/L
1
12/5/2022 18:51
Perfluoroheptanoic Acid (PFHpA)
U
1.7
4.9
ng/L
1
12/5/2022 18:51
Perfluorohexadecanoic Acid (PFHxDA)
U
1.8
4.9
ng/L
1
12/5/2022 18:51
Perfluorohexanesulfonic Acid (PFHxS)
U
0.89
4.9
ng/L
1
12/5/2022 18:51
Perfluorohexanoic Acid (PFHxA)
U
1.2
4.9
ng/L
1
12/5/2022 18:51
Perfluorononanesulfonic Acid (PFNS)
U
0.49
4.9
ng/L
1
12/5/2022 18:51
Perfluorononanoic Acid (PFNA)
U
0.86
4.9
ng/L
1
12/5/2022 18:51
Perfluorooctadecanoic Acid (PFODA)
U
0.64
4.9
ng/L
1
12/5/2022 18:51
Perfluorooctanesulfonamide (PFOSA)
U
0.70
4.9
ng/L
1
12/5/2022 18:51
Perfluorooctanesulfonic Acid (PFOS)
U
0.88
2.0
ng/L
1
12/5/2022 18:51
Perfluorooutanoic Acid (PFOA)
U
0.62
2.0
ng/L
1
12/5/2022 18:51
Perfluoropentanesulfonic Acid (PFPeS)
U
0.55
4.9
ng/L
1
12/5/2022 18:51
Perfluoropentanoic Acid (PFPeA)
U
1.3
4.9
ng/L
1
12/5/2022 18:51
Perfluorotetradecanoic Acid (PFTeA)
U
2.6
4.9
ng/L
1
12/5/2022 18:51
Perfluorotridecanoic Acid (PFTriA)
U
1.9
4.9
ng/L
1
12/5/2022 18:51
Perfluoroundecanoic Acid (PFUnA)
U
0.96
4.9
ng/L
1
12/5/2022 18:51
N-ethylperfluoro-1-octanesulfonamide
U
1.1
4.9
ng/L
1
12/5/2022 18:51
N-
U
1.5
4.9
ng/L
1
12/5/2022 18:51
Ethyl perfluorooctanesulfonamidoacetic
Acid
N-
U
1.0
4.9
ng/L
1
12/5/2022 18:51
Ethyl perfluorooctanesulfonamidoethano
I
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 21 of 29

ALS Group, USA
Client:
Verdantas
Project:
Phoenix Lumberton
Sample ID:
IRY165:FB-1:W113022
Collection Date:
11/30/2022 04:19 PM
Analyses
Report
Result Qual MDL Limit
N-methylperfluoro-1-octanesulfonamide
U
N-
U
Methyl perfluorooctanesulfonamidoaceti
c Acid
N-
U
Methylperfluorooctanesulfonamidoetha
nol
Hexafluoropropylene oxide dimer acid
U
(HFPO-DA)
4,8-Dioxa-3H-perfluorononanoic Acid
U
(DONA)
11 CI-Pf30UdS
U
9CI-PF30NS
U
Perfluoro-4-ethylcyclohexanesulfonic
U
Acid (PFecHS)
Perfluorobutylsulfonamide (PFBSA)
U
Perfluorohexanesulfonamide (PFHxSA)
U
Sum 13C2-FtS 4:2
117
Sum 13C2-FtS 6:2
87.2
Sum 13C2-FtS 8:2
84.8
Sum 13C2-PFDA
46.7
S
Surr. 13C2-PFDoA
70.5
Surr. 13C2-PFHxA
127
Surr. 13C2-PFHxDA
65.4
Surr. 13C2-PFTeA
73.4
Surr. 13C2-PFUnA
69.8
Sum- 13C3-HFPO-DA
78.8
Sum- 13C3-PFBS
51.6
Sum- 13C4-PFBA
58.4
Sum 13C4-PFHpA
128
Sum 13C4-PFOA
40.6
S
Sum 13C4-PFOS
43.1
S
Sum- 13C5-PFNA
63.3
Sum 13C5-PFPeA
59.7
Sum 13C8-FOSA
70.5
Sum 1802-PFHxS
66.4
Sum- d5-N-EtFOSA
45.6
S
Surr. d5-N-EtFOSAA
88.6
Surr. d9-N-EtFOSE
55.5
Surr. d3-N-McFOSA
42.8
S
Sum d3-N-McFOSAA
60.2
Sum d7-N-McFOSE
63.5
Note: See Qualifiers page for a list of qualifiers and their definitions
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-05
Matrix: WATER
Dilution
Units Factor Date Analyzed
0.78 4.9 ng/L 1 12/6/2022 02:05
0.64 4.9 ng/L 1 12/5/202218:51
1.5
4.9
ng/L
1
12/5/202218:51
1.2
4.9
ng/L
1
12/5/202218:51
0.56
4.9
ng/L
1
12/6/202214:36
0.46
4.9
ng/L
1
12/5/202218:51
0.44
4.9
ng/L
1
12/5/202218:51
0.88
4.9
ng/L
1
12/5/202218:51
2.0
4.9
ng/L
1
12/5/202218:51
0.87
4.9
ng/L
1
12/6/2022 02:05
50-150
%REC
1
12/6/202214:36
50-150
%REC
1
12/6/2022 02:05
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/6/202214:36
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/6/202214:36
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
50-150
%REC
1
12/5/202218:51
AR Page 22 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:FB-1:W113022
Lab ID: 22120229-05
Collection Date: 11/30/2022 04:19 PM
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 05:05
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 05:05
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 05:05
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 05:05
1,1-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 05:05
1,1-Dichloroethene
U
0.40
1.0
pg/L
1
12/8/2022 05:05
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 05:05
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 05:05
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 05:05
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 05:05
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 05:05
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 05:05
1,2-Dichlorobenzene
U
0.32
1.0
pg/L
1
12/8/2022 05:05
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 05:05
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 05:05
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 05:05
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 05:05
1,4-Dichlorobenzene
U
0.35
1.0
pg/L
1
12/8/2022 05:05
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 05:05
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 05:05
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 05:05
Acetone
U
6.2
10
pg/L
1
12/8/2022 05:05
Benzene
U
0.46
1.0
pg/L
1
12/8/2022 05:05
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 05:05
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 05:05
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 05:05
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 05:05
Carbon disulfide
U
0.49
1.0
pg/L
1
12/8/2022 05:05
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 05:05
Chlorobenzene
U
0.40
1.0
pg/L
1
12/8/2022 05:05
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 05:05
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 05:05
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 05:05
cis- 1,2-Dichloroethene
U
0.42
1.0
pg/L
1
12/8/2022 05:05
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 05:05
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 05:05
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 05:05
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 05:05
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 23 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:FB-1:W113022
Collection Date: 11/30/2022 04:19 PM
Analyses
Result
Report
Qual MDL Limit
Work Order: 22120229
Lab ID: 22120229-05
Matrix: WATER
Dilution
Units Factor Date Analyzed
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 05:05
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 05:05
m,p-Xylene
U
0.81
2.0
pg/L
1
12/8/2022 05:05
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 05:05
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 05:05
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 05:05
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 05:05
o-Xylene
U
0.31
1.0
pg/L
1
12/8/2022 05:05
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 05:05
Tetrachloroethene
U
0.39
1.0
pg/L
1
12/8/2022 05:05
Toluene
U
0.45
1.0
pg/L
1
12/8/2022 05:05
trans- 1,2-Dichloroethene
U
0.48
1.0
pg/L
1
12/8/2022 05:05
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 05:05
Trichloroethene
U
0.43
1.0
pg/L
1
12/8/2022 05:05
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 05:05
Vinyl chloride
U
0.53
1.0
pg/L
1
12/8/2022 05:05
Xylenes, Total
U
0.81
3.0
pg/L
1
12/8/2022 05:05
Surr. 1,2-Dichloroethane-d4
102
80-120
%REC
1
12/8/2022 05:05
Surr 4-Bromofluorobenzene
99.0
80-120
%REC
1
12/8/2022 05:05
Surr Dibromofluoromethane
97.4
80-120
%REC
1
12/8/2022 05:05
Surr Toluene-d8
96.4
80-120
%REC
1
12/8/2022 05:05
LOW LEVEL ALKALINITY
Method:A2320 B-11
Analyst: JMJ
Alkalinity, Bicarbonate (as CaCO3)
31
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Carbonate (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Hydroxide (as CaCO3)
U
1.4
2.0
mg/L
1
12/6/2022 12:27
Alkalinity, Total (as CaCO3)
31
1.4
2.0
mg/L
1
12/6/2022 12:27
CHLORIDE
Method:A4500-CL C-11
Analyst: AML
Chloride
U
2.2
3.0
mg/L
1
12/6/202216:00
HARDNESS
Method:A2340 C-11
Analyst: TJH
Hardness
35
2.2
5.0
mg/L CaCO3 1
12/7/2022 11:00
NITROGEN, NITRATE -NITRITE
Method:E353.2 R2.0
Analyst: JLS
Nitrogen, Nitrate -Nitrite
0.33
0.012
0.020
mg/L
1
12/6/2022 15:08
PH (LABORATORY)
Method: El50.1
Analyst: JMJ
pH (laboratory)
6.56
H 0.10
0.10
s.u.
1
12/5/2022 10:42
Temperature
19.7
H 0.10
0.10
°C
1
12/5/202210:42
SULFATE
Method:A4500-SO4
E-11
Analyst: AML
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 24 of 29

ALS Group, USA
Client:
Verdantas
Project:
Phoenix Lumberton
Sample ID:
IRY165:FB-1:W113022
Collection Date:
11/30/2022 04:19 PM
Analyses
Date: 09-Dec-22
Work Order: 22120229
Lab ID: 22120229-05
Matrix: WATER
Report Dilution
Result Qual MDL Limit Units Factor Date Analyzed
Sulfate
17
0.71
1.0
mg/L 1
12/6/202213:14
TOTAL DISSOLVED SOLIDS
Method:A2540 C-15
Prep: FILTER / 12/5/22
Analyst: LAD
Total Dissolved Solids
94
22
30
mg/L 1
12/8/2022 12:10
ORGANIC CARBON, TOTAL
Method:A531OC-14
Analyst: JB
Organic Carbon, Total
U
0.14
0.50
mg/L 1
12/3/2022 20:42
TOTAL SUSPENDED SOLIDS
Method:A2540 D-15
Prep: FILTER / 12/6/22
Analyst: SRN
Total Suspended Solids
U
0.38
0.60
mg/L 1
12/7/2022 14:27
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 25 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:TB-I:WI13022
Lab ID: 22120229-06
Collection Date: 11/30/2022
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 04:14
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 04:14
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 04:14
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 04:14
1,1-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 04:14
1,1-Dichloroethene
U
0.40
1.0
pg/L
1
12/8/2022 04:14
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 04:14
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 04:14
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 04:14
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 04:14
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 04:14
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 04:14
1,2-Dichlorobenzene
U
0.32
1.0
pg/L
1
12/8/2022 04:14
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 04:14
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 04:14
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 04:14
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 04:14
1,4-Dichlorobenzene
U
0.35
1.0
pg/L
1
12/8/2022 04:14
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 04:14
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 04:14
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 04:14
Acetone
U
6.2
10
pg/L
1
12/8/2022 04:14
Benzene
U
0.46
1.0
pg/L
1
12/8/2022 04:14
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 04:14
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 04:14
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 04:14
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 04:14
Carbon disulfide
U
0.49
1.0
pg/L
1
12/8/2022 04:14
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 04:14
Chlorobenzene
U
0.40
1.0
pg/L
1
12/8/2022 04:14
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 04:14
Chloroform
U
0.46
1.0
pg/L
1
12/8/2022 04:14
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 04:14
cis- 1,2-Dichloroethene
U
0.42
1.0
pg/L
1
12/8/2022 04:14
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 04:14
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 04:14
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 04:14
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 04:14
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 26 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:TB-I:WI13022
Collection Date: 11/30/2022
Analyses
Result Qual
MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-06
Matrix: WATER
Dilution
Units Factor Date Analyzed
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 04:14
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 04:14
m,p-Xylene
U
0.81
2.0
pg/L
1
12/8/2022 04:14
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 04:14
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 04:14
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 04:14
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 04:14
o-Xylene
U
0.31
1.0
pg/L
1
12/8/2022 04:14
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 04:14
Tetrachloroethene
U
0.39
1.0
pg/L
1
12/8/2022 04:14
Toluene
U
0.45
1.0
pg/L
1
12/8/2022 04:14
trans- 1,2-Dichloroethene
U
0.48
1.0
pg/L
1
12/8/2022 04:14
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 04:14
Trichloroethene
U
0.43
1.0
pg/L
1
12/8/2022 04:14
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 04:14
Vinyl chloride
U
0.53
1.0
pg/L
1
12/8/2022 04:14
Xylenes, Total
U
0.81
3.0
pg/L
1
12/8/2022 04:14
Surr. 1,2-Dichloroethane-d4
103
80-120
%REC
1
12/8/2022 04:14
Surr 4-Bromofluorobenzene
95.5
80-120
%REC
1
12/8/2022 04:14
Surr Dibromofluoromethane
99.6
80-120
%REC
1
12/8/2022 04:14
Surr Toluene-d8
97.2
80-120
%REC
1
12/8/2022 04:14
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 27 of 29

ALS Group, USA
Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Work Order: 22120229
Sample ID: IRY165:TB-2:WI13022
Lab ID: 22120229-07
Collection Date: 11/30/2022
Matrix: WATER
Report
Dilution
Analyses
Result
Qual MDL
Limit
Units
Factor Date Analyzed
VOLATILE ORGANIC COMPOUNDS
Method:SW8260C
Analyst: SBR
1,1,1-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 04:41
1,1,2,2-Tetrachloroethane
U
0.40
1.0
pg/L
1
12/8/2022 04:41
1,1,2-Trichloroethane
U
0.46
1.0
pg/L
1
12/8/2022 04:41
1,1,2-Trichlorotrifluoroethane
U
0.52
1.0
pg/L
1
12/8/2022 04:41
1,1-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 04:41
1,1-Dichloroethene
U
0.40
1.0
pg/L
1
12/8/2022 04:41
1,2,3-Trichlorobenzene
U
0.42
1.0
pg/L
1
12/8/2022 04:41
1,2,3-Trichloropropane
U
0.40
1.0
pg/L
1
12/8/2022 04:41
1,2,4-Trichlorobenzene
U
0.45
1.0
pg/L
1
12/8/2022 04:41
1,2,4-Trimethyl benzene
U
0.45
1.0
pg/L
1
12/8/2022 04:41
1,2-Dibromo-3-chloropropane
U
0.43
1.0
pg/L
1
12/8/2022 04:41
1,2-Dibromoethane
U
0.41
1.0
pg/L
1
12/8/2022 04:41
1,2-Dichlorobenzene
U
0.32
1.0
pg/L
1
12/8/2022 04:41
1,2-Dichloroethane
U
0.44
1.0
pg/L
1
12/8/2022 04:41
1,2-Dichloropropane
U
0.48
1.0
pg/L
1
12/8/2022 04:41
1,3,5-Trimethyl benzene
U
0.65
1.0
pg/L
1
12/8/2022 04:41
1,3-Dichlorobenzene
U
0.33
1.0
pg/L
1
12/8/2022 04:41
1,4-Dichlorobenzene
U
0.35
1.0
pg/L
1
12/8/2022 04:41
2-Butanone
U
0.52
5.0
pg/L
1
12/8/2022 04:41
2-Hexanone
U
0.59
5.0
pg/L
1
12/8/2022 04:41
4-Methyl-2-pentanone
U
0.52
1.0
pg/L
1
12/8/2022 04:41
Acetone
U
6.2
10
pg/L
1
12/8/2022 04:41
Benzene
U
0.46
1.0
pg/L
1
12/8/2022 04:41
Bromochloromethane
U
0.45
1.0
pg/L
1
12/8/2022 04:41
Bromodichloromethane
U
0.49
1.0
pg/L
1
12/8/2022 04:41
Bromoform
U
0.56
1.0
pg/L
1
12/8/2022 04:41
Bromomethane
U
0.90
1.0
pg/L
1
12/8/2022 04:41
Carbon disulfide
U
0.49
1.0
pg/L
1
12/8/2022 04:41
Carbon tetrachloride
U
0.40
1.0
pg/L
1
12/8/2022 04:41
Chlorobenzene
U
0.40
1.0
pg/L
1
12/8/2022 04:41
Chloroethane
U
0.68
1.0
pg/L
1
12/8/2022 04:41
Chloroform
0.53
J 0.46
1.0
pg/L
1
12/8/2022 04:41
Chloromethane
U
0.83
1.0
pg/L
1
12/8/2022 04:41
cis- 1,2-Dichloroethene
U
0.42
1.0
pg/L
1
12/8/2022 04:41
cis-1,3-Dichloropropene
U
0.57
1.0
pg/L
1
12/8/2022 04:41
Cyclohexane
U
0.63
2.0
pg/L
1
12/8/2022 04:41
Dibromochloromethane
U
0.40
1.0
pg/L
1
12/8/2022 04:41
Dichlorodifluoromethane
U
0.68
1.0
pg/L
1
12/8/2022 04:41
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 28 of 29

ALS Group, USA Date: 09-Dec-22
Client: Verdantas
Project: Phoenix Lumberton
Sample ID: IRY165:TB-2:WI13022
Collection Date: 11/30/2022
Analyses
Result Qual
MDL
Report
Limit
Work Order: 22120229
Lab ID: 22120229-07
Matrix: WATER
Dilution
Units Factor Date Analyzed
Ethylbenzene
U
0.34
1.0
pg/L
1
12/8/2022 04:41
Isopropyl benzene
U
0.35
1.0
pg/L
1
12/8/2022 04:41
m,p-Xylene
U
0.81
2.0
pg/L
1
12/8/2022 04:41
Methyl acetate
U
0.59
2.0
pg/L
1
12/8/2022 04:41
Methyl tert-butyl ether
U
0.45
1.0
pg/L
1
12/8/2022 04:41
Methylcyclohexane
U
0.35
1.0
pg/L
1
12/8/2022 04:41
Methylene chloride
U
0.86
5.0
pg/L
1
12/8/2022 04:41
o-Xylene
U
0.31
1.0
pg/L
1
12/8/2022 04:41
Styrene
U
0.33
1.0
pg/L
1
12/8/2022 04:41
Tetrachloroethene
U
0.39
1.0
pg/L
1
12/8/2022 04:41
Toluene
U
0.45
1.0
pg/L
1
12/8/2022 04:41
trans- 1,2-Dichloroethene
U
0.48
1.0
pg/L
1
12/8/2022 04:41
trans- 1,3-Dichloropropene
U
0.38
1.0
pg/L
1
12/8/2022 04:41
Trichloroethene
U
0.43
1.0
pg/L
1
12/8/2022 04:41
Trichlorofluoromethane
U
0.52
1.0
pg/L
1
12/8/2022 04:41
Vinyl chloride
U
0.53
1.0
pg/L
1
12/8/2022 04:41
Xylenes, Total
U
0.81
3.0
pg/L
1
12/8/2022 04:41
Surr. 1,2-Dichloroethane-d4
99.6
80-120
%REC
1
12/8/2022 04:41
Surr 4-Bromofluorobenzene
96.4
80-120
%REC
1
12/8/2022 04:41
Surr Dibromofluoromethane
97.0
80-120
%REC
1
12/8/2022 04:41
Surr Toluene-d8
99.3
80-120
%REC
1
12/8/2022 04:41
Note: See Qualifiers page for a list of qualifiers and their definitions.
AR Page 29 of 29

ALS Group, USA Date: 09-Dec-22
Client:
Verdantas
QC BATCH REPORT
Work Order:
22120229
Project:
Phoenix Lumberton
Batch ID: 207715
Instrument ID ICPMS3
Method:
E200.8
MBLK
Sample ID: MBLK-207715-207715
Units: mg/L
Analysis Date: 12/5/2022 05:54 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075375
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
U
0.080
LCS
Sample ID: LCS-207715-207715
Units: mg/L
Analysis Date: 12/5/2022 05:55 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075376
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
9.459
0.080 10
0 94.6 85-115
0
MS
Sample ID: 22112580-14AMS
Units: mg/L
Analysis Date: 12/5/2022 06:04 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075381
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
10.13
0.080 10
0.2739
98.5 70-130
0
MS
Sample ID: 22112580-16AMS
Units: mg/L
Analysis Date: 12/5/2022 06:11 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075385
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
11.72
0.080 10
1.872
98.5 70-130
0
MSD
Sample ID: 22112580-14AMSD
Units: mg/L
Analysis Date: 12/5/2022 06:05 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075382
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
9.934
0.080 10
0.2739
96.6 70-130
10.13 1.94 20
MSD
Sample ID: 22112580-16AMSD
Units: mg/L
Analysis Date: 12/5/2022 06:13 PM
Client ID:
Run ID:
ICPMS3_221205A
SegNo: 9075386
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD Limit Qual
Iron
11.65
0.080 10
1.872
97.8 70-130
11.72 0.623 20
The following samples were analyzed in this batch: 22120229-01 B 22120229-02B 22120229-03B
22120229-04B 22120229-05B
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 1 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
MBLK Sample ID: MBLK-207682-207682 I Units: ng/L
Client ID: R Run ID: LCMS2_221205A SegNo: 9077169
SPK Ref Control
A I R It PQL SPK Va I Value 0/ nGr Limit
na yte
esu
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
5.0
Fluorotelomer Sulphonic Acid 6:2 (FtS
U
5.0
Fluorotelomer Sulphonic Acid 8:2 (FtS
U
5.0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
U
5.0
Perfluorobutanesulfonic Acid (PFBS)
U
5.0
Perfluorobutanoic Acid (PFBA)
U
5.0
Perfluorodecanesulfonic Acid (PFDS)
U
5.0
Perfluorodecanoic Acid (PFDA)
U
5.0
Perfluorododecanesulfonic Acid (PFDc
U
5.0
Perfluorododecanoic Acid (PFDoA)
U
5.0
Perfluoroheptanesulfonic Acid (PFHpS
U
5.0
Perfluoroheptanoic Acid (PFHpA)
U
5.0
Perfluorohexadecanoic Acid (PFHxDA
U
5.0
Perfluorohexanesulfonic Acid (PFHxS)
U
5.0
Perfluorohexanoic Acid (PFHxA)
U
5.0
Perfluorononanesulfonic Acid (PFNS)
U
5.0
Perfluorononanoic Acid (PFNA)
U
5.0
Perfluorooctadecanoic Acid (PFODA)
U
5.0
Perfluorooctanesulfonamide (PFOSA)
U
5.0
Perfluorooctanesulfonic Acid (PFDS)
U
2.0
Perfluorooctanoic Acid (PFDA)
0.9248
2.0
Perfluoropentanesulfonic Acid (PFPeS
U
5.0
Perfluoropentanoic Acid (PFPeA)
U
5.0
Perfluorotetradecanoic Acid (PFTeA)
U
5.0
Perfluorotridecanoic Acid (PFTriA)
U
5.0
Perfluoroundecanoic Acid (PFUnA)
U
5.0
N-ethylperfluoro-1-octanesulfonamide
U
5.0
N-Ethylperfluorooctanesulfonamidoace
U
5.0
N-Ethylperfluorooctanesulfonamidoeth
U
5.0
N-methylperfluoro-1-octanesulfonamid
U
5.0
N-Methylperfluorooctanesulfonamidoai
0.8128
5.0
N-Methylperfluorooctanesulfonamidoel
U
5.0
Hexafluoropropylene oxide dimer acid
U
5.0
11CI-Pf30UdS
U
5.0
9CI-PF30NS
U
5.0
QC BATCH REPORT
Analysis Date: 12/5/2022 09:37 PM
Prep Date: 12/5/2022 DF: 1
RPD Ref RPD
Value %RPD Limit Qual
Perfluoro-4-ethylcyclohexanesulfonic F U 5.0
Perfluorobutylsulfonamide (PFBSA) U 5.0
Perfluorohexanesulfonamide (PFHxSA U 5.0
Surr. 13C2-FtS 4:2 102.2 0 149.4 0 68.4 50-150 0
Surr 13C2-FtS 6:2 108.1 0 152 0 71.1 50-150 0
Surr 13C2-FtS 8:2 132.7 0 153.3 0 86.6 50-150 0
Surr 13C2-PFDA 121.8 0 160 0 76.1 50-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
J
J
QC Page: 2 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
QC BATCH REPORT
Surr 13C2-PFDoA 114.7 0 160 0 71.7 50-150 0
Surr 13C2-PFHxA 124.2 0 160 0 77.6 50-150 0
Surr 13C2-PFHxDA 145.7 0 160 0 91.1 50-150 0
Surr 13C2-PFTeA
Surr 13C2-PFUnA
Surr 13C3-HFPO-DA
Surr: 13C3-PFBS
Surr. 13C4-PFBA
Surr 13C4-PFHpA
Surr. 13C4-PFOA
Surr. 13C4-PFOS
Surr. 13C5-PFNA
Surr. 13C5-PFPeA
Surr 13C8-F0SA
Surr 1802-PFHxS
114.6
0
160
0
71.6
50-150 0
100.8
0
160
0
63
50-150 0
129.1
0
160
0
80.7
50-150 0
120.9
0
148.8
0
81.3
50-150 0
124.6
0
160
0
77.8
50-150 0
135.2
0
160
0
84.5
50-150 0
117.3
0
160
0
73.3
50-150 0
112.3
0
152.8
0
73.5
50-150 0
137.3
0
160
0
85.8
50-150 0
132.5
0
160
0
82.8
50-150 0
120.1
0
160
0
75
50-150 0
85.26
0
151.2
0
56.4
50-150 0
Surr: d5-N-EfFOSA
100.6
0
160
0
62.9
50-150 0
Surr d5-N-EtFOSAA
160.3
0
160
0
100
50-150 0
Surr: d9-N-EtFOSE
119.2
0
160
0
74.5
50-150 0
Surr d3-N-McFOSA
115.4
0
160
0
72.1
50-150 0
Surr. d3-N-McFOSAA
149.8
0
160
0 93.6
50-150
0
Surr: d7-N-McFOSE
114.9
0
160
0 71.8
50-150
0
-1
MBLK Sample ID: MBLK-207682-207682
Units: ng/L
Analysis Date: 12/6/2022 12:16 PM
Client ID: '
Run ID:
LCMS1_221206A
SegNo:9078563
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val Value
%REC
Limit
Value %RPD Limit Qual
4,8-Dioxa-3H-perFluorononanoic Acid (
U
5.0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 3 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
MBLK Sample ID: MBLK-207682-207682
I
Units: ng/L
Analysis Date: 12/6/2022 09:30 AM
Client ID: R
Run ID:
LCMS2_221206A
SegNo:
Prep Date: 12/5/2022 DF: 1
9080549
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
U
5.0
Fluorotelomer Sulphonic Acid 6:2 (FtS
U
5.0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
U
5.0
Perfluorobutanesulfonic Acid (PFBS)
U
5.0
Perfluorobutanoic Acid (PFBA)
U
5.0
Perfluorodecanesulfonic Acid (PFDS)
U
5.0
Perfluorodecanoic Acid (PFDA)
U
5.0
Perfluorododecanesulfonic Acid (PFDc
U
5.0
Perfluorododecanoic Acid (PFDoA)
U
5.0
Perfluoroheptanoic Acid (PFHpA)
U
5.0
Perfluorohexadecanoic Acid (PFHxDA
U
5.0
Perfluorohexanesulfonic Acid (PFHxS)
U
5.0
Perfluorohexanoic Acid (PFHxA)
U
5.0
Perfluorononanesulfonic Acid (PFNS)
U
5.0
Perfluorononanoic Acid (PFNA)
U
5.0
Perfluorooctadecanoic Acid (PFODA)
U
5.0
Perfluorooctanesulfonamide (PFOSA)
U
5.0
Perfluorooctanesulfonic Acid (PFDS)
U
2.0
Perfluorooctanoic Acid (PFDA)
U
2.0
Pernuoropentanoic Acid (PFPeA)
U
5.0
Perfluorotetradecanoic Acid (PFTeA)
U
5.0
Perfluorotridecanoic Acid (PFTriA)
U
5.0
Perfluoroundecanoic Acid (PFUnA)
U
5.0
N-ethylperfluoro-1-octanesulfonamide
U
5.0
N-Ethylperfluorooctanesulfonamidoace
U
5.0
N-Ethylperfluorooctanesulfonamidoeth
U
5.0
N-methylperfluoro-1-octanesulfonamid
U
5.0
N-Methylperfluorooctanesulfonamidoai
U
5.0
N-Methylperfluorooctanesulfonamidoel
U
5.0
11 CI-Pf30UdS
U
5.0
9CI-PF30NS
U
5.0
Surr. 13C2-FtS 4:2
89.1
0
149.4
0
59.6
25-150
0
Surr 13C2-FtS 6.2
84.79
0
152
0
55.8
25-150
0
Surr 13C2-FtS 8:2
124.2
0
153.3
0
81
25-150
0
Surr 13C2-PFDA
78.79
0
160
0
49.2
25-150
0
Surr 13C2-PFDoA
116.6
0
160
0
72.9
25-150
0
Surr 13C2-PFHxDA
119.9
0
160
0
74.9
25-150
0
Surr 13C2-PFTeA
113.9
0
160
0
71.2
25-150
0
Surr 13C2-PFUnA
98.5
0
160
0
61.6
25-150
0
Surr 13C3-HFPO-DA
136.1
0
160
0
85.1
25-150
0
Surr:13C3-PFBS
94.02
0
148.8
0
63.2
25-150
0
Surr. 13C4-PFBA
97.07
0
160
0
60.7
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 4 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: 207682
Instrument ID LCMS2
Method:
E537 Mod
Surr 13C4-PFHpA
81.07
0 160
0 50.7 25-150 0
Surr 13C4-PFOA
Surr 13C4-PFOS
61.9
66.91
0 160
0 152.8
0 38.7 25-150 0
0 43.8 25-150 0
Surr 13C5-PFNA
Surr 13C5-PFPeA
101.5 0 160 0 63.4 25-150 0
110.2 0 160 0 68.9 25-150 0
Surr. • 13C8-FOSA 123.4 0 160 0 77.2 10-150 0
Surr:1802-PFHxS 97.37 0 151.2 0 64.4 25-150 0
Surr. d5-N-EtFOSA
74.87
0
160
0 46.8
10-150
0
Surr. d9-N-EtFOSE
103.6
0
160
0 64.8
10-150
0
Surr. • d3-N-McFOSA
72.29
0
160
0 45.2
10-150
0
Surr. • d7-N-McFOSE
104.7
0
160
0 65.5
10-150
0
MBLK Sample ID: MBLK-207682-207682
Units: ng/L
JL-
Analysis Date: 12/6/2022 06:11 PM
Client ID: Ir
Run ID:
LCMS1_221206B
SegNo: 9081482
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
U
5.0
Perfluoroheptanesulfonic Acid (PFHpS
U
5.0
Hexafluoropropylene oxide dimer acid
U
5.0
MBLK Sample ID: MBLK-207682-207682
Units: ng/L
Analysis Date: 12/7/2022 12:15 PM
Client ID:
Run ID:
LCMS1_221207B
SegNo: 9082330
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
4,8-Dioxa-3H-perfluorononanoic Acid (
U
5.0
LCS Sample ID: LCS-207682-207682
Units: ng/L
Analysis Date: 12/5/2022
05:20 PM
Client ID:
Run ID:
LCMS2_221205A
SegNo: 9077145
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Perfluorooctanesulfonic Acid (PFOS)
35.39
2.0
29.7
0 119
65-140
0
Perfluoropentanesulfonic Acid (PFPeS
25.12
5.0
30
0 83.7
71-127
0
Surr 13C5-PFNA
86.45
0
160
0 54
50-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 5 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
LCS Sample ID: LCS-207682-207682
Client ID: , Run ID: LCMS2_221205A
Analyte Result PQL SPK Val
Fluorotelomer Sulphonic Acid 4:2 (FtS
31.14
5.0
29.9
Fluorotelomer Sulphonic Acid 6:2 (FtS
30.17
5.0
30.3
Fluorotelomer Sulphonic Acid 8:2 (FtS
30.12
5.0
30.7
Fluorotelomer Sulphonic Acid 10:2 (Ft:
18.13
5.0
30.8
Perfluorobutanesulfonic Acid (PFBS)
28.68
5.0
28.3
Perfluorobutanoic Acid (PFBA)
39.39
5.0
32
Perfluorodecanoic Acid (PFDA)
35.58
5.0
32
Perfluorododecanesulfonic Acid (PFDc
36.85
5.0
31
Pernuorododecanoic Acid (PFDoA)
37.09
5.0
32
Perfluoroheptanesulfonic Acid (PFHpS
35.17
5.0
30.5
Perfluoroheptanoic Acid (PFHpA)
35.19
5.0
32
Perfluorohexadecanoic Acid (PFHxDA
28.22
5.0
32
Perfluorohexanesulfonic Acid (PFHxS)
22.52
5.0
29.1
Perfluorohexanoic Acid (PFHxA)
39.84
5.0
32
Perfluorononanoic Acid (PFNA)
36.37
5.0
32
Perfluorooctadecanoic Acid (PFODA)
29.36
5.0
32
Perfluorooctanesulfonamide (PFOSA)
24.85
5.0
32
Perfluorooctanoic Acid (PFDA)
38.43
2.0
32
Perfluoropentanoic Acid (PFPeA)
31.19
5.0
32
Perfluorotetradecanoic Acid (PFTeA)
29.06
5.0
32
Perfluorotridecanoic Acid (PFTriA)
22.46
5.0
32
Perfluoroundecanoic Acid (PFUnA)
42.18
5.0
32
N-ethylperfluoro-1-octanesulfonamide
29.9
5.0
32
N-Ethylperfluorooctanesulfonamidoace
31.67
5.0
32
N-Ethylperfluorooctanesulfonamidoeth
30.24
5.0
32
N-methylperfluoro-1-octanesulfonamid
30.89
5.0
32
N-Methylperfluorooctanesulfonamidoai
36.25
5.0
32
N-Methylperfluorooctanesulfonamidoei
23.67
5.0
32
Hexafluoropropylene oxide dimer acid
26.16
5.0
32
11 CI-Pf30UdS
27.69
5.0
30.1
PerHuoro-4-ethylcyclohexanesulfonic F
25.29
5.0
28.8
Perfluorobutylsulfonamide (PFBSA)
25.29
5.0
32
Perfluorohexanesulfonamide (PFHxDA
28.35
5.0
32
Surr. 13C2-FtS 4:2
78.17
0
149.4
Surr 13C2-FtS 6:2
101.2
0
152
Surr 13C2-FtS 8:2
116.8
0
153.3
Units: ng/L
SegNo:9077170
SPK Ref
Control
Value
%REC
Limit
0
104
63-143
0
99.6
63-162
0
98.1
61-165
0
58.9
40-160
0
101
72-130
0
123
73-129
0
111
71-129
0
119
69-134
0
116
72-134
0
115
69-134
0
110
72-130
0
88.2
70-130
0
77.4
68-131
0
124
72-129
0
114
69-130
0
91.8
70-130
0 77.6
67-137
0 120
71-133
0 97.5
72-129
0 90.8
71-132
Analysis Date: 12/5/2022 09:45 PM
Prep Date: 12/5/2022 DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0
70.2
65-144
0
132
69-133
0
93.4
70-130
0
99
61-135
0
94.5
70-130
0
96.5
70-130
0
113
65-136
0
74
68-141
0
81.8
70-130
0
92
70-130
0
87.8
70-130
0
79
70-130
0
88.6
70-130
0
52.3
50-150
0
66.6
50-150
0
76.2
50-150
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Surr 13C2-PFDoA 82.34 0 160 0 51.5 50-150 0
Surr 13C2-PFHxDA 98.82 0 160 0 61.8 50-150 0
Surr 13C2-PFTeA
119.6
0
160
0
74.7
50-150
0
Surr 13C2-PFUnA
103.6
0
160
0
64.8
50-150
0
Surr 13C3-HFPO-DA
131.6
0
160
0
82.2
50-150
0
Surr 13C3-PFBS
75.66
0
148.8
0
50.8
50-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 6 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
Surr 13C4-PFBA
Surr 13C5-PFPeA
81.63
93.63
0
0
160
160
0
0
51
58.5
50-150
50-150
Surr:13C8-F0SA
106.7
0
160
0
66.7
50-150
Surr 1802-PFHxS
101.9
0
151.2
0
67.4
50-150
Surr. d5-N-EtFOSAA
118.7
0
160
0
74.2
50-150
Surr. d9-N-EtFOSE
80.92
0
160
0
50.6
50-150
Surr. d3-N-McFOSAA
80.37
0
160
0
50.2
50-150
Surr. • d7-N-McFOSE
96.59
0
160
0
60.4
50-150
LCS
Client ID:
in
Sample ID: LCS-207682-207682
Run ID: LCMS2_221205B
Analyte Result PQL SPK Val
Pernuorononanesulfonic Acid (PFNS) 29.1 5.0 30.7
LCS
Sample ID: LCS-207682-207682
Run ID:
LCMS2 221205B
Analyte
Result
PQL
SPK Val
Perfluorodecanesulfonic Acid (PFDS) 37.53
5.0
30.8
9CI-PF30NS
25.18
5.0
29.8
Surr 13C4-PFHpA
110.4
0
160
Surr 13C4-PFDS
77.28
0
152.8
Surr: d5-N-EfFOSA
90.03
0
160
LCS
Sample ID: LCS-207682-207682
Client ID:
Run ID:
LCMS1 221206A
Analyte
Result
PQL
SPK Val
4,8-Dioxa-3H-perfluorononanoic Acid (
26.6
5.0
30.1
Surr 13C2-PFDA
117.5
0
160
Surr 13C2-PFHxA
155.4
0
160
Surr: 13C4-PFDA
Surr. • d3-N-McFOSA
150.8 0 160
101.2 0 160
-v Units: ng/�
SegNo:9077760
SPK Ref Control
Value %REC Limit
0 94.8 69-127
Units: ng/L
SegNo:9077788
SPK Ref Control
Value %REC Limit
0
0
0
0
0
0
0
0
Analysis Date: 12/6/2022 12:18 AM
Prep Date: 12/5/2022 DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0
Analysis Date: 12/6/2022 04:59 AM
Prep Date: 12/5/2022 DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0 122 53-142 0
0 84.5 70-130 0
0 69 50-150 0
0 50.6 50-150 0
0 56.3 50-150 0
Units: ng/l!� Analysis Date: 12/6/2022 12:49 PM
SegNo: 9078567 Prep Date: 12/5/2022 DF: 1
SPK Ref Control RPD Ref RPD
Value %REC Limit Value %RPD Limit Qual
0 88.4
70-130 0
0 73.4
50-150 0
0 97.2
50-150 0
0 94.3
50-150 0
0 63.3
50-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 7 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
LCS Sample ID: LCS-207682-WI-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 09:38 AM
Client ID: R
Run ID:
LCMS2_221206A
SegNo:
9080550
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit
Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
3.434
5.0
3.738
0
91.9
50-150
0
J
Fluorotelomer Sulphonic Acid 6:2 (FtS
3.978
5.0
3.788
0
105
50-150
0
J
Fluorotelomer Sulphonic Acid 10:2 (Ft:
3.437
5.0
3.85
0
89.3
50-150
0
J
Perfluorobutanesulfonic Acid (PFBS)
3.37
5.0
3.538
0
95.3
50-150
0
J
Perfluorobutanoic Acid (PFBA)
4.038
5.0
4
0
101
50-150
0
J
Perfluorodecanesulfonic Acid (PFDS)
4.08
5.0
3.85
0
106
50-150
0
J
Perfluorodecanoic Acid (PFDA)
4.298
5.0
4
0
107
50-150
0
J
Perfluorododecanesulfonic Acid (PFDc
3.562
5.0
3.875
0
91.9
50-150
0
J
Perfluorododecanoic Acid (PFDoA)
4.518
5.0
4
0
113
50-150
0
J
Perfluoroheptanoic Acid (PFHpA)
3.926
5.0
4
0
98.2
50-150
0
J
Perfluorohexadecanoic Acid (PFHxDA
3.133
5.0
4
0
78.3
50-150
0
J
Perfluorohexanesulfonic Acid (PFHxS)
5.411
5.0
3.638
0
149
50-150
0
Perfluorohexanoic Acid (PFHxA)
4.451
5.0
4
0
111
50-150
0
J
Perfluorononanesulfonic Acid (PFNS)
5.152
5.0
3.838
0
134
50-150
0
Perfluorononanoic Acid (PFNA)
3.914
5.0
4
0
97.8
50-150
0
J
Perfluorooctadecanoic Acid (PFODA)
3.222
5.0
4
0
80.6
50-150
0
J
Perfluorooctanesulfonamide (PFOSA)
3.782
5.0
4
0
94.6
50-150
0
J
Perfluorooctanesulfonic Acid (PFDS)
3.782
2.0
3.712
0
102
50-150
0
Perfluorooctanoic Acid (PFDA)
3.818
2.0
4
0
95.4
50-150
0
Pernuoropentanoic Acid (PFPeA)
3.408
5.0
4
0
85.2
50-150
0
J
Perfluorotetradecanoic Acid (PFTeA)
3.526
5.0
4
0
88.2
50-150
0
J
Perfluorotridecanoic Acid (PFTriA)
4.061
5.0
4
0
102
50-150
0
J
Pernuoroundecanoic Acid (PFUnA)
4.298
5.0
4
0
107
50-150
0
J
N-ethylperfluoro-1-octanesulfonamide
2.784
5.0
4
0
69.6
50-150
0
J
N-Ethylperfluorooctanesulfonamidoace
3.619
5.0
4
0
90.5
50-150
0
J
N-Ethylperfluorooctanesulfonamidoeth
3.363
5.0
4
0
84.1
50-150
0
J
N-methylperfluoro-1-octanesulfonamid
3.718
5.0
4
0
93
50-150
0
J
N-Methylperfluorooctanesulfonamidoai
4.499
5.0
4
0
112
50-150
0
J
N-Methylperfluorooctanesulfonamidoei
2.128
5.0
4
0
53.2
50-150
0
J
11 CI-Pf30UdS
2.906
5.0
3.762
0
77.2
50-150
0
J
9CI-PF30NS
3.264
5.0
3.725
0
87.6
50-150
0
J
Surr. 13C2-FtS 4:2
127.5
0
149.4
0
85.3
25-150
0
Surr 13C2-FtS 6.2
149.2
0
152
0
98.2
25-150
0
Surr 13C2-FtS 8:2
128.3
0
153.3
0
83.7
25-150
0
Surr 13C2-PFDA
120.8
0
160
0
75.5
25-150
0
Surr 13C2-PFDoA
111.8
0
160
0
69.9
25-150
0
Surr 13C2-PFHxDA
181.2
0
160
0
113
25-150
0
Surr 13C2-PFTeA
137.2
0
160
0
85.8
25-150
0
Surr 13C2-PFUnA
123.2
0
160
0
77
25-150
0
Surr 13C3-HFPO-DA
114.1
0
160
0
71.3
25-150
0
Surr:13C3-PFBS
147.8
0
148.8
0
99.3
25-150
0
Surr. 13C4-PFBA
150.4
0
160
0
94
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 8 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: 207682
Instrument ID LCMS2
Method:
E537 Mod
Surr 13C4-PFHpA
192.2
0 160
0 120 25-150 0
Surr 13C4-PFOA
153.6
0 160
0 96 25-150 0
Surr 13C4-PFOS
127.6
0 152.8
0 83.5 25-150 0
Surr 13C5-PFNA 143 0 160 0 89.4 25-150 0
Surr 13C5-PFPeA 159.4 0 160 0 99.6 25-150 0
Surr. • 13C8-FOSA 133.8 0 160 0 83.6 10-150 0
Surr:1802-PFHxS 106.4 0 151.2 0 70.4 25-150 0
Surr. d5-N-EtFOSA
131.9
0
160
0
82.4
10-150
0
Surr. d9-N-EtFOSE
141.1
0
160
0
88.2
10-150
0
Surr. • d3-N-McFOSA
123.1
0
160
0
76.9
10-150
0
Surr. • d7-N-McFOSE
164.3
0
160
0
103
10-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 9 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
QC BATCH REPORT
LCS Sample ID: LCS-207682-A-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 09:46 AM
Client ID: ,
Run ID:
LCMS2_221206A
SegNo:
9080551
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
31.47
5.0
29.9
0
105
50-150
0
Fluorotelomer Sulphonic Acid 6:2 (FtS
33
5.0
30.3
0
109
50-150
0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
26.98
5.0
30.8
0
87.6
50-150
0
PerHuorobutanesulfonic Acid (PFBS)
27.42
5.0
28.3
0
96.9
50-150
0
PerHuorobutanoic Acid (PFBA)
38.77
5.0
32
0
121
50-150
0
Pernuorodecanesulfonic Acid (PFDS)
23.17
5.0
30.8
0
75.2
50-150
0
Perfluorodecanoic Acid (PFDA)
34.86
5.0
32
0
109
50-150
0
Pernuorododecanesulfonic Acid (PFDc
21.89
5.0
31
0
70.6
50-150
0
Pernuorododecanoic Acid (PFDoA)
43.48
5.0
32
0
136
50-150
0
Pernuoroheptanoic Acid (PFHpA)
30.92
5.0
32
0
96.6
50-150
0
Pernuorohexadecanoic Acid (PFHxDA
29.51
5.0
32
0
92.2
50-150
0
Perfluorohexanesulfonic Acid (PFHxS)
36.43
5.0
29.1
0
125
50-150
0
Pernuorohexanoic Acid (PFHxA)
37.41
5.0
32
0
117
50-150
0
Perfluorononanesulfonic Acid (PFNS)
27.18
5.0
30.7
0
88.5
50-150
0
Perfluorononanoic Acid (PFNA)
37.28
5.0
32
0
116
50-150
0
Pernuorooctadecanoic Acid (PFODA)
30.15
5.0
32
0
94.2
50-150
0
Perfluorooctanesulfonamide (PFOSA)
29.39
5.0
32
0
91.8
50-150
0
Perfluorooctanesulfonic Acid (PFDS)
31.9
2.0
29.7
0
107
50-150
0
Perfluorooctanoic Acid (PFOA)
34.8
2.0
32
0
109
50-150
0
Perfluoropentanoic Acid (PFPeA)
29.4
5.0
32
0
91.9
50-150
0
Pernuorotetradecanoic Acid (PFTeA)
28.97
5.0
32
0
90.5
50-150
0
PerHuorotridecanoic Acid (PFTriA)
34.63
5.0
32
0
108
50-150
0
Perfluoroundecanoic Acid (PFUnA)
45.09
5.0
32
0
141
50-150
0
N-ethylperfluoro-1-octanesulfonamide
25.2
5.0
32
0
78.8
50-150
0
N-Ethylperfluorooctanesulfonamidoace
24.75
5.0
32
0
77.3
50-150
0
N-Ethylperfluorooctanesulfonamidoeth
26.87
5.0
32
0
84
50-150
0
N-methylperfluoro-1-octanesulfonamid
24.03
5.0
32
0
75.1
50-150
0
N-Methylperfluorooctanesulfonamidoai
29.59
5.0
32
0
92.5
50-150
0
N-Methylperfluorooctanesulfonamidoel
32.69
5.0
32
0
102
50-150
0
11CI-Pf30UdS
32.46
5.0
30.1
0
108
50-150
0
9CI-PF30NS
39.1
5.0
29.8
0
131
50-150
0
Surr. 13C2-FtS 4:2
119
0
149.4
0
79.6
25-150
0
Surr 13C2-FtS 6:2
106.4
0
152
0
70
25-150
0
Surr 13C2-FtS 8:2
142.6
0
153.3
0
93.1
25-150
0
Surr 13C2-PFDA
114.1
0
160
0
71.3
25-150
0
Surr 13C2-PFDoA
108.7
0
160
0
68
25-150
0
Surr 13C2-PFHxDA 149.2 0 160 0 93.2 25-150 0
Surr 13C2-PFTeA 131.8 0 160 0 82.4 25-150 0
Surr 13C2-PFUnA
102.1
0
160
0
63.8
25-150
0
Surr 13C3-HFPO-DA
127.6
0
160
0
79.8
25-150
0
Surr 13C3-PFBS
129.5
0
148.8
0
87
25-150
0
Surr 13C4-PFBA
122.1
0
160
0
76.3
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 10 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
QC BATCH REPORT
Surr:13C4-PFHpA
124
0
160
0
77.5
25-150
0
Surr 13C4-PF0A
104.9
0
160
0
65.5
25-150
0
Surr 13C4-PFOS
103.6
0
152.8
0
67.8
25-150
0
Surr 13C5-PFNA
140.6
0
160
0
87.8
25-150
0
Surr 13C5-PFPeA
137.1
0
160
0
85.7
25-150
0
Surr. • 13C8-FOSA
129.5
0
160
0
80.9
10-150
0
Surr 1802-PFHxS
79.25
0
151.2
0
52.4
25-150
0
Surr. d5-N-EtFOSA
102.2
0
160
0
63.9
10-150
0
Surr d9-N-EtFOSE 135.9 0 160 0 84.9 10-150 0
Surr: d3-N-McFOSA 122.9 0 160 0 76.8 10-150 0
Surr: d7-N-McFOSE 111.8 0 160 0 69.9 10-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 11 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method:
E537 Mod
LCS Sample ID: LCS-207682-B-MGM-207682
Units:
ng/L
Analysis Date: 12/6/2022 09:55 AM
Client ID: R
Run ID:
LCMS2_221206A
SegNo: 9080552
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
28.54
5.0
29.9
0
95.5
50-150
0
Fluorotelomer Sulphonic Acid 6:2 (FtS
31.97
5.0
30.3
0
106
50-150
0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
33.89
5.0
30.8
0
110
50-150
0
PerHuorobutanesulfonic Acid (PFBS)
29.97
5.0
28.3
0
106
50-150
0
PerHuorobutanoic Acid (PFBA)
39.54
5.0
32
0
124
50-150
0
Perfluorodecanesulfonic Acid (PFDS)
40.9
5.0
30.8
0
133
50-150
0
Perfluorodecanoic Acid (PFDA)
39.29
5.0
32
0
123
50-150
0
Pernuorododecanesulfonic Acid (PFDc
29.24
5.0
31
0
94.3
50-150
0
Perfluorododecanoic Acid (PFDoA)
37.05
5.0
32
0
116
50-150
0
Perfluoroheptanoic Acid (PFHpA)
30.11
5.0
32
0
94.1
50-150
0
Perfluorohexadecanoic Acid (PFHxDA
29.46
5.0
32
0
92
50-150
0
Perfluorohexanesulfonic Acid (PFHxS)
43.16
5.0
29.1
0
148
50-150
0
Pernuorohexanoic Acid (PFHxA)
37.88
5.0
32
0
118
50-150
0
Pernuorononanoic Acid (PFNA)
41.72
5.0
32
0
130
50-150
0
Pernuorooctadecanoic Acid (PFODA)
28.47
5.0
32
0
89
50-150
0
Perfluorooctanesulfonamide (PFOSA)
31.92
5.0
32
0
99.7
50-150
0
Pernuorooctanesulfonic Acid (PFOS)
37.58
2.0
29.7
0
127
50-150
0
Pernuorooctanoic Acid (PFDA)
43.63
2.0
32
0
136
50-150
0
Pernuoropentanoic Acid (PFPeA)
33.73
5.0
32
0
105
50-150
0
Pernuorotetradecanoic Acid (PFTeA)
29.47
5.0
32
0
92.1
50-150
0
Pernuorotridecanoic Acid (PFTriA)
30.34
5.0
32
0
94.8
50-150
0
Pernuoroundecanoic Acid (PFUnA)
33.21
5.0
32
0
104
50-150
0
N-ethylperfluoro-1-octanesulfonamide
28.01
5.0
32
0
87.5
50-150
0
N-Ethylperfluorooctanesulfonamidoace
38.91
5.0
32
0
122
50-150
0
N-Ethylperfluorooctanesulfonamidoeth
31.63
5.0
32
0
98.8
50-150
0
N-methylperfluoro-1-octanesulfonamid
39.37
5.0
32
0
123
50-150
0
N-Methylperfluorooctanesulfonamidoai
33.43
5.0
32
0
104
50-150
0
N-Methylperfluorooctanesulfonamidoel
17.45
5.0
32
0
54.5
50-150
0
11 CI-Pf30UdS
26.07
5.0
30.1
0
86.6
50-150
0
9CI-PF30NS
30.8
5.0
29.8
0
103
50-150
0
Surr. 13C2-FtS 4:2
107.9
0
149.4
0
72.2
25-150
0
Surr. 13C2-FtS 6.2
166.2
0
152
0
109
25-150
0
Surr 13C2-FtS 8:2
123.8
0
153.3
0
80.8
25-150
0
Surr 13C2-PFDA
98.92
0
160
0
61.8
25-150
0
Surr 13C2-PFDoA
91.06
0
160
0
56.9
25-150
0
Surr 13C2-PFHxDA
160.6
0
160
0
100
25-150
0
Surr 13C2-PFTeA
124.2
0
160
0
77.6
25-150
0
Surr 13C2-PFUnA
124.8
0
160
0
78
25-150
0
Surr 13C3-HFPO-DA
107
0
160
0
66.9
25-150
0
Surr 13C3-PFBS 125.5 0 148.8 0 84.4 25-150 0
Surr 13C4-PFBA 135.6 0 160 0 84.7 25-150 0
Surr 13C4-PFHpA 214.3 0 160 0 134 25-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 12 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
QC BATCH REPORT
Surr 13C4-PFOA 124.2 0 160 0 77.6 25-150 0
Surr 13C4-PFOS 102 0 152.8 0 66.8 25-150 0
Surr 13C5-PFNA 113.6 0 160 0 71 25-150 0
Surr 13C5-PFPeA
Surr. • 13C8-FOSA
Surr: 1802-PFHxS
Surr d5-N-EtFOSA
Surr. d9-N-EfFOSE
Surr. d3-N-McFOSA
Surr. • d7-N-McFOSE
147.7 0 160 0 92.3 25-150 0
119.2 0 160 0 74.5 10-150 0
117.6 0 151.2 0 77.8 25-150 0
103.2 0 160 0 64.5 10-150 0
114.9 0 160 0 71.8 10-150 0
83.83 0 160 0 52.4 10-150 0
146 0 160 0 91.3 10-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 13 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
QC BATCH REPORT
LCS Sample ID: LCS-207682-C-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 10:03 AM
Client ID: ,
Run ID:
LCMS2_221206A
SegNo:
9080553
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
29.96
5.0
29.9
0
100
50-150
0
Fluorotelomer Sulphonic Acid 6:2 (FtS
37.67
5.0
30.3
0
124
50-150
0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
26.98
5.0
30.8
0
87.6
50-150
0
PerHuorobutanesulfonic Acid (PFBS)
28.3
5.0
28.3
0
100
50-150
0
PerHuorobutanoic Acid (PFBA)
39.17
5.0
32
0
122
50-150
0
Pernuorodecanesulfonic Acid (PFDS)
26.38
5.0
30.8
0
85.7
50-150
0
Perfluorodecanoic Acid (PFDA)
37.08
5.0
32
0
116
50-150
0
Pernuorododecanesulfonic Acid (PFDc
25.96
5.0
31
0
83.7
50-150
0
Pernuorododecanoic Acid (PFDoA)
41.09
5.0
32
0
128
50-150
0
Pernuoroheptanoic Acid (PFHpA)
32.82
5.0
32
0
103
50-150
0
Pernuorohexadecanoic Acid (PFHxDA
29
5.0
32
0
90.6
50-150
0
Perfluorohexanesulfonic Acid (PFHxS)
34.12
5.0
29.1
0
117
50-150
0
Pernuorohexanoic Acid (PFHxA)
39.53
5.0
32
0
124
50-150
0
Perfluorononanesulfonic Acid (PFNS)
35.7
5.0
30.7
0
116
50-150
0
Perfluorononanoic Acid (PFNA)
36.79
5.0
32
0
115
50-150
0
Pernuorooctadecanoic Acid (PFODA)
29.15
5.0
32
0
91.1
50-150
0
Perfluorooctanesulfonamide (PFOSA)
35.06
5.0
32
0
110
50-150
0
Perfluorooctanesulfonic Acid (PFDS)
41.6
2.0
29.7
0
140
50-150
0
Perfluorooctanoic Acid (PFOA)
35.37
2.0
32
0
111
50-150
0
Perfluoropentanoic Acid (PFPeA)
30.46
5.0
32
0
95.2
50-150
0
Pernuorotetradecanoic Acid (PFTeA)
31.88
5.0
32
0
99.6
50-150
0
PerHuorotridecanoic Acid (PFTriA)
34.54
5.0
32
0
108
50-150
0
Perfluoroundecanoic Acid (PFUnA)
44.52
5.0
32
0
139
50-150
0
N-ethylperfluoro-1-octanesulfonamide
22.94
5.0
32
0
71.7
50-150
0
N-Ethylperfluorooctanesulfonamidoace
25.8
5.0
32
0
80.6
50-150
0
N-Ethylperfluorooctanesulfonamidoeth
29.08
5.0
32
0
90.9
50-150
0
N-methylperfluoro-1-octanesulfonamid
28.11
5.0
32
0
87.8
50-150
0
N-Methylperfluorooctanesulfonamidoai
37.91
5.0
32
0
118
50-150
0
N-Methylperfluorooctanesulfonamidoel
32.5
5.0
32
0
102
50-150
0
11 CI-Pf30UdS
34.09
5.0
30.1
0
113
50-150
0
Surr. 13C2-FtS 4:2
121
0
149.4
0
81
25-150
0
Surr 13C2-FtS 6:2
94.11
0
152
0
61.9
25-150
0
Surr 13C2-FtS 8:2
139.3
0
153.3
0
90.9
25-150
0
Surr 13C2-PFDA
100.7
0
160
0
62.9
25-150
0
Surr 13C2-PFDoA
114.5
0
160
0
71.6
25-150
0
Surr 13C2-PFHxDA
145.3
0
160
0
90.8
25-150
0
Surr 13C2-PFTeA 124.9 0 160 0 78 25-150 0
Surr 13C2-PFUnA 102.2 0 160 0 63.9 25-150 0
Surr 13C3-HFPO-DA
129.9
0
160
0
81.2
25-150
0
Surr. 13C3-PFBS
120
0
148.8
0
80.6
25-150
0
Surr. 13C4-PFBA
108
0
160
0
67.5
25-150
0
Surr 13C4-PFHpA
108.1
0
160
0
67.5
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 14 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
QC BATCH REPORT
Surr 13C4-PFOA
89.28
0
160
0
55.8
25-150 0
Surr 13C4-PFOS
85.98
0
152.8
0
56.3
25-150 0
Surr 13C5-PFNA
139.9
0
160
0
87.5
25-150 0
Surr 13C5-PFPeA
126
0
160
0
78.8
25-150 0
Surr. • 13C8-FOSA
131.9
0
160
0
82.5
10-150
0
Surr:1802-PFHxS
79.66
0
151.2
0
52.7
25-150
0
Surr. d5-N-EtFOSA
91.29
0
160
0
57.1
10-150
0
Surr. d9-N-EtFOSE
114.9
0
160
0
71.8
10-150
0
Surr. • d3-N-McFOSA
102
0
160
0
63.7
10-150 0
Surr. • d7-N-McFOSE
109.9
0
160
0
68.7
10-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 15 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
LCS Sample ID: LCS-207682-D-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 10:11 AM
Client ID: R
Run ID:
LCMS2_221206A
SegNo:
9080554
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Fluorotelomer Sulphonic Acid 4:2 (FtS
26.53
5.0
29.9
0
88.7
50-150
0
Fluorotelomer Sulphonic Acid 6:2 (FtS
35.14
5.0
30.3
0
116
50-150
0
Fluorotelomer Sulphonic Acid 10:2 (Ft:
33.06
5.0
30.8
0
107
50-150
0
PerHuorobutanesulfonic Acid (PFBS)
28.83
5.0
28.3
0
102
50-150
0
PerHuorobutanoic Acid (PFBA)
37.31
5.0
32
0
117
50-150
0
Perfluorodecanesulfonic Acid (PFDS)
29.4
5.0
30.8
0
95.4
50-150
0
Perfluorodecanoic Acid (PFDA)
37.06
5.0
32
0
116
50-150
0
Pernuorododecanesulfonic Acid (PFDc
23.81
5.0
31
0
76.8
50-150
0
Perfluorododecanoic Acid (PFDoA)
38.94
5.0
32
0
122
50-150
0
Perfluoroheptanoic Acid (PFHpA)
31.55
5.0
32
0
98.6
50-150
0
Perfluorohexadecanoic Acid (PFHxDA
31.6
5.0
32
0
98.8
50-150
0
Perfluorohexanesulfonic Acid (PFHxS)
27.68
5.0
29.1
0
95.1
50-150
0
Pernuorohexanoic Acid (PFHxA)
35.72
5.0
32
0
112
50-150
0
Pernuorononanesulfonic Acid (PFNS)
25.33
5.0
30.7
0
82.5
50-150
0
Pernuorononanoic Acid (PFNA)
36.48
5.0
32
0
114
50-150
0
Pernuorooctadecanoic Acid (PFODA)
30.62
5.0
32
0
95.7
50-150
0
Pernuorooctanesulfonamide (PFOSA)
29.8
5.0
32
0
93.1
50-150
0
Pernuorooctanesulfonic Acid (PFDS)
38.08
2.0
29.7
0
128
50-150
0
Pernuorooctanoic Acid (PFDA)
34.15
2.0
32
0
107
50-150
0
Pernuoropentanoic Acid (PFPeA)
31.86
5.0
32
0
99.6
50-150
0
Pernuorotetradecanoic Acid (PFTeA)
30.31
5.0
32
0
94.7
50-150
0
Pernuorotridecanoic Acid (PFTriA)
34.9
5.0
32
0
109
50-150
0
Pernuoroundecanoic Acid (PFUnA)
41.13
5.0
32
0
129
50-150
0
N-ethylperfluoro-1-octanesulfonamide
24.34
5.0
32
0
76.1
50-150
0
N-Ethylperfluorooctanesulfonamidoace
28.09
5.0
32
0
87.8
50-150
0
N-Ethylperfluorooctanesulfonamidoeth
29.27
5.0
32
0
91.5
50-150
0
N-methylperfluoro-1-octanesulfonamid
22.85
5.0
32
0
71.4
50-150
0
N-Methylperfluorooctanesulfonamidoai
27.62
5.0
32
0
86.3
50-150
0
N-Methylperfluorooctanesulfonamidoei
27.44
5.0
32
0
85.8
50-150
0
11 CI-Pf30UdS
33.8
5.0
30.1
0
112
50-150
0
9CI-PF30NS
37.48
5.0
29.8
0
126
50-150
0
Surr. 13C2-FtS 4:2
136.1
0
149.4
0
91.1
25-150
0
Surr 13C2-FtS 6.2
120.8
0
152
0
79.5
25-150
0
Surr 13C2-FtS 8:2
144.4
0
153.3
0
94.2
25-150
0
Surr 13C2-PFDA
133.3
0
160
0
83.3
25-150
0
Surr 13C2-PFDoA
120.3
0
160
0
75.2
25-150
0
Surr 13C2-PFHxDA
148.6
0
160
0
92.9
25-150
0
Surr 13C2-PFTeA
130.6
0
160
0
81.6
25-150
0
Surr 13C2-PFUnA
113.8
0
160
0
71.1
25-150
0
Surr 13C3-HFPO-DA
115.9
0
160
0
72.4
25-150
0
Surr:13C3-PFBS
128
0
148.8
0
86
25-150
0
Surr. 13C4-PFBA
133.1
0
160
0
83.2
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 16 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: 207682
Instrument ID LCMS2
Method:
E537 Mod
Surr 13C4-PFHpA
141.8
0 160
0 88.6 25-150 0
Surr 13C4-PFOA
Surr 13C4-PFOS
118
119.2
0 160
0 152.8
0 73.7 25-150 0
0 78 25-150 0
Surr 13C5-PFNA
Surr 13C5-PFPeA
Surr. • 13C8-FOSA
Surr: 1802-PFHxS
153.2 0 160
137.6 0 160
134.8 0 160
98.56 0 151.2
0 95.8
25-150
0 86
25-150
0 84.3
10-150
0 65.2
25-150
0
0
0
0
Surr. d5-N-EtFOSA
110.5
0
160
0
69.1
10-150
0
Surr. d9-N-EtFOSE
133.4
0
160
0
83.4
10-150
0
Surr. • d3-N-McFOSA
123
0
160
0
76.9
10-150
0
Surr. • d7-N-McFOSE
132.2
0
160
0
82.7
10-150
0
LCS Sample ID: LCS-207682-WI-MGM-207682
Units: ng/L
JL-
Analysis Date: 12/6/2022 06:19
PM
Run ID:
LCMS1_221206B
SegNo:
9081483
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit
Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
3.264
5.0
3.838
0
85.1
50-150
0
J
Perfluoroheptanesulfonic Acid (PFHpS
3.699
5.0
3.812
0
97
50-150
0
J
Hexafluoropropylene oxide dimer acid
4.269
5.0
4
0
107
50-150
0
J
4,8-Dioxa-3H-perfluorononanoic Acid (
4.922
5.0
3.762
0
131
50-150
0
J
Surr 13C2-PFHxA
129.6
0
160
0
81
25-150
0
Surr d3-N-McFOSAA
222.9
0
160
0 139
25-150
0
LCS Sample ID: LCS-207682-A-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 06:27 PM
-
Client ID:
Run ID:
LCMS1_221206B
SegNo:9081484 Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
26.82
5.0
30.7
0 87.4
50-150
0
Perfluoroheptanesulfonic Acid (PFHpS
34.5
5.0
30.5
0 113
50-150
0
Hexafluoropropylene oxide dimer acid
32.44
5.0
32
0 101
50-150
0
Surr 13C2-PFHxA
126.6
0
160
0 79.1
25-150
0
Surr d5-N-EtFOSAA
156.5
0
160
0 97.8
25-150
0
Surr d3-N-McFOSAA
135
0
160
0 84.3
25-150
0
LCS Sample ID: LCS-207682-B-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 06:36 PM
Client ID:
Run ID:
LCMS1_221206B
SegNo: 9081485 Prep
Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
30.49
5.0
30.7
0 99.3
50-150
0
Hexafluoropropylene oxide dimer acid
27.61
5.0
32
0 86.3
50-150
0
Surr 13C2-PFHxA
76.82
0
160
0 48
25-150
0
Surr d5-N-EtFOSAA
93.73
0
160
0 58.6
25-150
0
Surr d3-N-McFOSAA
123.7
0
160
0 77.3
25-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 17 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: 207682 Instrument ID LCMS2
Method:
E537 Mod
LCS Sample ID: LCS-207682-C-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 06:44 PM
Client ID: ,
Run ID:
LCMS1_221206B
SegNo: 9081486
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %oRPD Limit Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
27.19
5.0
30.7
0 88.6
50-150
0
Pernuoroheptanesulfonic Acid (PFHpS
32.23
5.0
30.5
0 106
50-150
0
Hexafluoropropylene oxide dimer acid
38.09
5.0
32
0 119
50-150
0
Surr 13C2-PFHxA
123.4
0
160
0 77.2
25-150
0
Surr d5-N-EtFOSAA
141.2
0
160
0 88.2
25-150
0
Surr d3-N-McFOSAA
126.2
0
160
0 78.9
25-150
0
LCS Sample ID: LCS-207682-D-MGM-207682
Units: ng/L
Analysis Date: 12/6/2022 06:52 PM
Client ID:
Run ID:
LCMS1_221206B
SegNo: 9081487
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %aRPD Limit Qual
Fluorotelomer Sulphonic Acid 8:2 (FtS
24.84
5.0
30.7
0 80.9
50-150
0
Pernuoroheptanesulfonic Acid (PFHpS
31.89
5.0
30.5
0 105
50-150
0
Hexafluoropropylene oxide dimer acid
34.31
5.0
32
0 107
50-150
0
Surr 13C2-PFHxA
144.2
0
160
0 90.1
25-150
0
Surr. d5-N-EtFOSAA
159
0
160
0 99.4
25-150
0
Surr d3-N-McFOSAA
137.7
0
160
0 86.1
25-150
0
LCS Sample ID: LCS-207682-B-MGM-207682
T
Units: ng/L
Analysis Date: 12/7/2022 12:40 PM
Client ID: '
Run ID:
LCMS1_221207B
SegNo: 9082333
Prep Date: 12/5/2022 DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
4,8-Dioxa-3H-perfluorononanoic Acid (
39.13
5.0
30.1
0 130
50-150
0
LCS Sample ID: LCS-207682-C-MGM-207682
Units: ng/L
I Analysis Date: 12/7/2022 12:48 PM
Client ID: �01111
Run ID: LCMS1_221207B
SegNo: 9082334
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result PQL SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
4,8-Dioxa-3H-perfluorononanoic Acid (
32.34 5.0 30.1
0 107
50-150
0
LCS Sample ID: LCS-207682-D-MGM-207682
Units: ng/L
Analysis Date: 12/7/2022 12:56 PM
Client ID:
Run ID: LCMS1_221207B
SegNo:9082335
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result PQL SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
4,8-Dioxa-3H-perfluorononanoic Acid (
26.64 5.0 30.1
0 88.5
50-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 18 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2 Method: E537 Mod
MS Sample ID: 22112061-09A MS
Client ID: , Run ID: LCMS2_221205A
Analyte Result POL SPK Val
Fluorotelomer Sulphonic Acid 4:2 (FtS
31.74
4.9
29.2
Fluorotelomer Sulphonic Acid 6:2 (FtS
39.7
4.9
29.59
Fluorotelomer Sulphonic Acid 8:2 (FtS
40.42
4.9
29.98
Fluorotelomer Sulphonic Acid 10:2 (Ft!
37.62
4.9
30.07
Perfluorobutanesulfonic Acid (PFBS)
33.81
4.9
27.63
Perfluorodecanoic Acid (PFDA)
37.88
4.9
31.25
Perfluorododecanesulfonic Acid (PFDc
39.06
4.9
30.27
Perfluorododecanoic Acid (PFDoA)
38.79
4.9
31.25
Perfluoroheptanesulfonic Acid (PFHpS
28.17
4.9
29.78
Perfluorohexadecanoic Acid (PFHxDA
34.83
4.9
31.25
Perfluorohexanesulfonic Acid (PFHxS)
40.2
4.9
28.41
Perfluorononanoic Acid (PFNA)
34.81
4.9
31.25
Perfluorooctadecanoic Acid (PFDDA)
33.46
4.9
31.25
Perfluorooctanesulfonamide (PFOSA)
30.82
4.9
31.25
Perfluoropentanesulfonic Acid (PFPeS
33.86
4.9
29.29
Perfluoropentanoic Acid (PFPeA)
40.17
4.9
31.25
Units: ng/L
SegNo:9077147
SPK Ref Control
Value 0/ REC Limit
0
0
109
63-143
0
134
63-162
0
135
61-165
0
125
40-160
0.3466
121
72-130
0
121
71-129
0
129
69-134
0.7205
122
72-134
0
94.6
69-134
0
111
70-130
3.037
131
68-131
0
111
69-130
0
107
70-130
0
98.6
67-137
1.161
112
71-127
6.156
109
72-129
QC BATCH REPORT
Analysis Date: 12/5/2022 06:02 PM
Prep Date: 12/5/2022 DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Perfluorotetradecanoic Acid (PFTeA)
33.43
4.9
31.25
0
107
71-132
0
Perfluorotridecanoic Acid (PFTriA)
39
4.9
31.25
0
125
65-144
0
Perfluoroundecanoic Acid (PFUnA)
33.39
4.9
31.25
0
107
69-133
0
N-ethylperfluoro-1-octanesulfonamide
29.54
4.9
31.25
0
94.6
70-130
0
N-Ethylpernuorooctanesulfonamidoeth
36.01
4.9
31.25
1.931
109
70-130
0
N-Methylperfluorooctanesulfonamidoai
35.72
4.9
31.25
0
114
65-136
0
N-Methylperfluorooctanesulfonamidoei
23.25
4.9
31.25
1.815
68.6
68-141
0
Hexafluoropropylene oxide dimer acid
37.45
4.9
31.25
1.949
114
70-130
0
11CI-Pf30UdS
31.57
4.9
29.39
0
107
70-130
0
9CI-PF30NS
34.09
4.9
29.1
0
117
70-130
0
Perfluoro-4-ethylcyclohexanesulfonic F
35.73
4.9
28.12
0
127
70-130
0
Perfluorobutylsulfonamide (PFBSA)
26.36
4.9
31.25
0
84.4
70-130
0
Surr. 13C2-FtS 8:2
123.2
0
149.7
0
82.3
50-150
0
Surr 13C2-PFDA
85.81
0
156.2
0
54.9
50-150
0
Surr 13C2-PFDoA
102.2
0
156.2
0
65.4
50-150 0
Surr 13C2-PFHxDA
140.9
0
156.2
0
90.2
50-150 0
Surr 13C2-PFTeA
112.2
0
156.2
0
71.8
50-150 0
Surr 13C2-PFUnA
133.2
0
156.2
0
85.3
50-150 0
Surr 13C3-HFPO-DA
109.5
0
156.2
0
70.1
50-150 0
Surr 13C3-PFBS
127.8
0
145.3
0
88
50-150 0
Surr. 13C4-PFBA 158.4 0 156.2 0 101 50-150 0
Surr 13C4-PFDA 102.9 0 156.2 0 65.9 50-150 0
Surr 13C4-PFOS
87.79
0
149.2
0
58.8
50-150 0
Surr 13C5-PFNA
120.1
0
156.2
0
76.9
50-150 0
Surr 13C5-PFPeA
162.8
0
156.2
0
104
50-150 0
Surr 13C8-FOSA
132.5
0
156.2
0
84.8
50-150 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 19 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: 207682
Instrument ID LCMS2
Method:
E537 Mod
Surr.1802-PFHxS
160.9
0
147.6
0
109
50-150 0
Surr. d5-N-EtFOSA
129.7
0
156.2
0
83
50-150 0
Surr d5-N-EtFOSAA
101
0
156.2
0
64.6
50-150 0
Surr. d9-N-EtFOSE
123.4
0
156.2
0
79
50-150 0
Surr.• d3-N-McFOSA
120.5
0
156.2
0
77.1
50-150
0
Surr. d3-N-McFOSAA
96.29
0
156.2
0
61.6
50-150
0
Surr. d7-N-McFOSE
157.3
0
156.2
0
101
50-150
0
I
MS Sample ID: 22112061-09A MS
Units: ng/L
Analysis Date: 12/6/2022 01:16 AM
Client ID:
Run ID:
LCMS2_221205B
SegNo: 9077765
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%aREC
Limit
Value %RPD
Limit Qual
Perfluorobutanoic Acid (PFBA)
39.03
4.9
31.25
0
125
73-129
0
Perfluorononanesulfonic Acid (PFNS)
30.85
4.9
29.98
0
103
69-127
0
N-Ethylperfluorooctanesulfonamidoace
29.86
4.9
31.25
0
95.6
61-135
0
N-methylperfluoro-1-octanesulfonamid
27.98
4.9
31.25
0
89.6
70-130
0
Perfluorohexanesulfonamide (PFHxSA
25.44
4.9
31.25
0
81.4
70-130
0
Surr. 13C2-FtS 6:2
142.1
0
148.4
0
95.8
50-150
0
MS Sample ID: 22112061-09A MS
Units: ng/L
Analysis Date: 12/6/2022 01:30 PM
Client ID:
Run ID:
LCMS1_221206A
SegNo:9078576
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Perfluorodecanesulfonic Acid (PFDS)
28.75
4.9
30.07
2.125
88.5
53-142
0
Perfluoroheptanoic Acid (PFHpA)
40.55
4.9
31.25
0
130
72-130
0
Perfluorohexanoic Acid (PFHxA)
40.23
4.9
31.25
0
129
72-129
0
Perfluorooctanesulfonic Acid (PFOS)
33.87
2.0
29
0
117
65-140
0
Perfluorooctanoic Acid (PFOA)
44.84
2.0
31.25
0.7813
141
71-133
0
S
4,8-Dioxa-3H-perfluorononanoic Acid (
43.75
4.9
29.39
1.614
143
70-130
0
S
Surr. 13C2-FtS 4:2
245.4
0
145.9
0
168
50-150
0
S
Surr.13C2-PFHxA
202.2
0
156.2
0
129
50-150
0
Surr.13C4-PFHpA
223.7
0
156.2
0
143
50-150
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 20 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
DUP Sample ID: 22112061-03A DUP
Client ID: R Run ID: LCMS2 221205A
Fluorotelomer Sulphonic Acid 4:2 (FtS
Fluorotelomer Sulphonic Acid 6:2 (FtS
Fluorotelomer Sulphonic Acid 8:2 (FtS
Fluorotelomer Sulphonic Acid 10:2 (Ft:
Perfluorobutanesulfonic Acid (PFBS)
Perfluorodecanesulfonic Acid (PFDS)
Perfluorodecanoic Acid (PFDA)
Perfluorododecanesulfonic Acid (PFDc
Perfluorododecanoic Acid (PFDoA)
Perfluoroheptanesulfonic Acid (PFHpS
Perfluoroheptanoic Acid (PFHpA)
Perfluorohexadecanoic Acid (PFHxDA
Perfluorohexanesulfonic Acid (PFHxS)
Perfluorohexanoic Acid (PFHxA)
Perfluorononanesulfonic Acid (PFNS)
Perfluorononanoic Acid (PFNA)
Perfluorooctadecanoic Acid (PFODA)
Perfluorooctanesulfonamide (PFOSA)
Perfluorooctanesulfonic Acid (PFOS)
Perfluorooctanoic Acid (PFDA)
Perfluoropentanesulfonic Acid (PFPeS
Perfluoropentanoic Acid (PFPeA)
Perfluorotetradecanoic Acid (PFTeA)
Perfluorotridecanoic Acid (PFTriA)
Perlluoroundecanoic Acid (PFUnA)
N-ethylperfluoro-1-octanesulfonamide
N-Ethylperfl uorooctanesulfonam idoace
N-Ethylperfl uorooctanesu Ifonamidoeth
N-Methylperfl uorooctanesulfonamidoai
N-Methylperfl uoroocta nesu Ifonam idoel
HexafluoroorODVlene oxide dimer acid
SPK Ref
Result PQL SPK Val Value
Units: ng/L Analysis Date: 12/5/2022 06:10 PM
SegNo: 9077148 Prep Date: 12/5/2022 DF: 1
Control RPD Ref RPD
%REC Limit Value %RPD Limit Qual
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
2.865
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
1.112
4.7
0
0
0
0-0
1.086
0
30
J
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
0.8826
4.7
0
0
0
0-0
0
0
30
J
0.6232
4.7
0
0
0
0-0
0
0
30
J
2.955
4.7
0
0
0
0-0
2.682
0
30
J
U
4.7
0
0
0
0-0
0
0
30
1.649
4.7
0
0
0
0-0
1.681
0
30
J
5.084
4.7
0
0
0
0-0
5.419
6.39
30
U
4.7
0
0
0
0-0
0
0
30
2.15
4.7
0
0
0
0-0
2.347
0
30
J
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
18.58
1.9
0
0
0
0-0
21.89
16.3
30
10.43
1.9
0
0
0
0-0
10.72
2.74
30
0.5546
4.7
0
0
0
0-0
1.614
0
30
J
2.705
4.7
0
0
0
0-0
3.134
0
30
J
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
0.7842
4.7
0
0
0
0-0
0
0
30
J
U
4.7
0
0
0
0-0
0
0
30
U
4.7
0
0
0
0-0
0
0
30
i
-
w.l
v
v
v
v-v
v
v
liv
9CI-PF30NS
U
4.7
0
0
0
0-0
0
0
30
Perfluoro-4-ethylcyclohexanesulfonic F
U
4.7
0
0
0
0
0
30
Perfluorobutylsulfonamide (PFBSA)
U
4.7
0
0
0
0
0
30
Surr 13C2-PFDoA
64.55
0
149.1
0
43.3
50-150
120.6
60.5
30
SR
Surr 13C4-PFDA
62.79
0
149.1
0
42.1
50-150
183.5
98
30
SR
Surr 13C4-PFDS
49.95
0
142.4
0
35.1
50-150
122.9
84.4
30
SR
Surr. d9-N-EtFOSE
52.04
0
149.1
0
34.9
50-150
123.9
81.7
30
SR
Surr. d3-N-McFOSAA 59.74 0 149.1
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
0 40.1 50-150 109.2 58.6 30 SR
QC Page: 21 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207682 Instrument ID LCMS2
Method: E537 Mod
QC BATCH REPORT
DUP Sample ID: 22112061-03A DUP
I
Units: ng/L
Analysis Date: 12/6/2022 01:24 AM
IF
Client ID:
Run ID:
LCMS2_221205B
SegNo: 9077766
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
Per luorobutanoic Acid (PFBA)
U
4.7
0
0 0
0-0
0 0
30
N-methylperfluoro-1-octanesulfonamid
U
4.7
0
0 0
0-0
0 0
30
Perfluorohexanesulfonamide (PFHxSA
U
4.7
0
0 0
0 0
30
Surr. 13C2-FtS 6:2
136.8
0
141.6
0 96.6
50-150
200.6 37.8
30 R
DUP Sample ID: 22112061-03A DUP
Units: ng/L
Analysis Date: 12/6/2022 01:38 PM
Client ID:
Run ID:
LCMS1_221206A
SegNo: 9078578
Prep Date: 12/5/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD
Limit Qual
4,8-Dioxa-3H-perfluorononanoic Acid (
U
4.7
0
0 0
0-0
0 0
30
Surr. 13C2-FtS 4:2
167.8
0
139.3
0 120
50-150
246 37.8
30 R
Surr. 13C2-FtS 8:2
94.08
0
142.8
0 65.9
50-150
137.3 37.3
30 R
Surr 13C2-PFDA
74.7
0
149.1
0 50.1
50-150
129.7 53.8
30 R
Surr 13C2-PFHxA
129.1
0
149.1
0 86.6
50-150
201.7 43.9
30 R
Surr 13C2-PFHxDA 106.6 0 149.1 0 71.5 50-150 137.2 25.2 30
Surr 13C2-PFTeA 88.33 0 149.1 0 59.2 50-150 114.1 25.5 30
Surr: 13C2-PFUnA
Surr: 13C3-HFP0-DA
Surr: 13C3-PFBS
Surr: 13C4-PFBA
Surr. 13C4-PFHpA
Surr 13C5-PFNA
Surr 13C5-PFPeA
Surr. • 13CB-FOSA
Surr: 1802-PFHxS
Surr d5-N-EtFOSA
Surr. d5-N-EtFOSAA
Surr. d3-N-McFOSA
Surr: d7-N-McFOSE
59.62 0 149.1
114.8 0 149.1
127.1
121.8
0
0
138.7
149.1
155.5
0
149.1
113.8
0
149.1
133.2
0
149.1
64.51
0
149.1
124.9
0
140.9
74.47
0
149.1
89.66
0
149.1
60.21
0
149.1
0 40
50-150
0 77
50-150
0 91.7
50-150
0 81.7
50-150
0 104
50-150
0 76.3
50-150
0 89.3
50-150
0 43.3
50-150
0 88.6
50-150
0 50
50-150
0 60.1
50-150
0 40.4
50-150
126.7 72 30 SR
107.5 6.55 30
129.6
1.92
30
167.8
31.7
30 R
202.6
26.3
30
140.6
21.1
30
152.6
13.6
30
111.3
53.2
30 SR
127
1.64
30
129.6
54
30 SR
97.21
8.09
30
123.4
68.8
30 SR
98.18 0 149.1 0 65.9 50-150 111.9 13.1 30
The following samples were analyzed in this batch: 22120229-01E 22120229-02E 22120229-03E
22120229-04E 22120229-05E
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 22 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11
Method: SW8260C
QC BATCH REPORT
MBLK Sample ID: 11V-BLKW2-221207-R359809b Units: pg/L Analysis Date: 12/7/2022 10:43 PM
Client ID: ow Run ID: VMS11_221207A SegNo: 9084603 Prep Date: DF: 1
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %RPD Limit Qual
1,1,1-Trichloroethane U 1.0
1,1,2,2-Tetrachloroethane U 1.0
1,1,2-Trichloroethane U 1.0
1,1,2-Trichlorotrifluoroethane
1,1-Dichloroethane
U 1.0
U 1.0
1,1-Dichloroethene U 1.0
1,2,3-Trichlorobenzene U 1.0
1,2,3-Trichloropropane
U
1.0
1,2,4-Trichlorobenzene
U
1.0
1,2,4-Trimethyl benzene
U
1.0
1,2-Dibromo-3-chloropropane
U
1.0
1,2-Dibromoethane
U
1.0
1,2-Dichlorobenzene
U
1.0
1,2-Dichloroethane
U
1.0
1,2-Dichloropropane
U
1.0
1,3,5-Trimethyl benzene
U
1.0
1,3-Dichlorobenzene
U
1.0
1,4-Dichlorobenzene
U
1.0
2-Butanone
U
5.0
2-Hexanone
U
5.0
4-Methyl-2-pentanone
U
1.0
Acetone
U
10
Benzene
U
1.0
Bromochloromethane
U
1.0
Bromodichloromethane
U
1.0
Bromoform
U
1.0
Bromomethane
U
1.0
Carbon disulfide
U
1.0
Carbon tetrachloride
U
1.0
Chlorobenzene
U
1.0
Chloroethane
U
1.0
Chloroform
U
1.0
Chloromethane
U
1.0
cis- 1, 3-Dichloropropene
U
1.0
Cyclohexane
U
2.0
Dibromochloromethane
U
1.0
Dichlorodifluoromethane
U
1.0
Ethylbenzene
U
1.0
Isopropyl benzene
U
1.0
m,p-Xylene
U
2.0
Methyl acetate
U
2.0
Methyl tert-butyl ether
U
1.0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 23 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11
Methylcyclohexane
Methylene chloride
o-Xylene
Styrene
Tetrachloroethene
U 1.0
U 5.0
U 1.0
U 1.0
U 1.0
Toluene U 1.0
trans-1,2-Dichloroethene U 1.0
trans- 1,3-Dichloropropene U 1.0
Trichloroethene U 1.0
Method: SW8260C
QC BATCH REPORT
Trichlorofluoromethane
U
1.0
Xylenes, Total
U
3.0
Surr 1,2-Dichloroethane-d4
19.71
0
20
0
98.6
80-120 0
Surr 4-Bromofluorobenzene
19.37
0
20
0
96.8
80-120 0
Surr: Dibromofluoromethane
19.08
0
20
0
95.4
80-120 0
Surr: Toluene-d8
19.78
0
20
0
98.9
80-120 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 24 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11
Method:
SW8260C
LCS Sample ID: 11V-LCSW2-221207-R359809b
Units: pg/L
Client ID:
Run ID:
VMS11_221207A
SegNo:
9084599
SPK Ref
Control
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
1,1,1-Trichloroethane
19.05
1.0
20
0
95.2
75-119
1,1,2,2-Tetrachloroethane
19.11
1.0
20
0
95.6
80-123
1,1,2-Trichloroethane
18.77
1.0
20
0
93.8
83-118
1,1,2-Trichlorotrifluoroethane
20.59
1.0
20
0
103
64-133
1,1-Dichloroethane
19.76
1.0
20
0
98.8
73-122
1,1-Dichloroethene
21.69
1.0
20
0
108
66-131
1,2,3-Trichlorobenzene
22.83
1.0
20
0
114
65-140
1,2,3-Trichloropropane
18.65
1.0
20
0
93.2
78-119
1,2,4-Trichlorobenzene
19.78
1.0
20
0
98.9
73-127
1,2,4-Trimethyl benzene
19.44
1.0
20
0
97.2
74-118
1,2-Dibromo-3-chloropropane
19.29
1.0
20
0
96.4
52-141
1,2-Dibromoethane
18.83
1.0
20
0
94.2
60-159
1,2-Dichlorobenzene
19.11
1.0
20
0
95.6
80-119
1,2-Dichloroethane
19.81
1.0
20
0
99
78-121
1,2-Dichloropropane
19.69
1.0
20
0
98.4
78-120
1,3,5-Trimethyl benzene
19.77
1.0
20
0
98.8
76-120
1,3-Dichlorobenzene
19.2
1.0
20
1,4-Dichlorobenzene
19.27
1.0
20
2-Butanone
18.44
5.0
20
2-Hexanone
19.16
5.0
20
4-Methyl-2-pentanone
24.68
1.0
20
Acetone
18.93
10
20
Benzene
20.26
1.0
20
Bromochloromethane
18.88
1.0
20
Bromodichloromethane
20.31
1.0
20
Bromoform
18
1.0
20
Bromomethane
22.42
1.0
20
Carbon disulfide
18.72
1.0
20
0
0
0
0
96 80-120
96.4 81-119
92.2 69-147
95.8 67-140
123 68-199
94.6 70-166
QC BATCH REPORT
Analysis Date: 12/7/2022 09:38 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0 101
78-120 0
0 94.4
70-125 0
0 102
73-126 0
0 90
60-124 0
0 112
20-183 0
0 93.6
67-159 0
Carbon tetrachloride
19.44
1.0
20
0
97.2
69-124
0
Chlorobenzene
18.93
1.0
20
0
94.6
80-118
0
Chloroethane
21.48
1.0
20
0
107
35-136
0
Chloroform
19.18
1.0
20
0
95.9
75-119
0
Chloromethane
18.47
1.0
20
0
92.4
26-117
0
cis- 1,3-Dichloropropene
19.13
1.0
20
0
95.6
69-120
0
Cyclohexane
19.94
2.0
20
0
99.7
66-128
0
Dibromochloromethane
17.36
1.0
20
0
86.8
63-117
0
Dichlorodifluoromethane
22.2
1.0
20
0
111
36-133
0
Ethylbenzene
19.31
1.0
20
0
96.6
76-116
0
Isopropyl benzene
19.54
1.0
20
0
97.7
77-118
0
m,p-Xylene
38.97
2.0
40
0
97.4
76-119
0
Methyl tert-butyl ether
19.95
1.0
20
0
99.8
77-137
0
Methylcyclohexane
20.04
1.0
20
0
100
66-125
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 25 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: R359809b
Instrument ID VMS11
Method:
SW8260C
Methylene chloride
19.72
5.0
20
0
98.6
68-125
0
o-Xylene
19.83
1.0
20
0
99.2
77-116
0
Styrene
19.17
1.0
20
0
95.8
76-123
0
Tetrachloroethene
19.45
1.0
20
0
97.2
80-124
0
Toluene
19.74
1.0
20
0
98.7
78-116
0
trans-1,2-Dichloroethene
20.12
1.0
20
0
101
73-124
0
trans- 1,3-Dichloropropene
18.43
1.0
20
0
92.2
67-118
0
Trichloroethene
19.6
1.0
20
0
98
75-122
0
Trichlorofluoromethane
Xylenes, Total
Surr. 1, 2-Dichloroethane-d4
Surr 4-Bromofluorobenzene
Surr Dibromofluoromethane
Surr. Toluene-d8
18.69
1.0
20
0
93.4
52-115
58.8
3.0
60
0
98
77-119
19.35
0
20
0
96.8
80-120
20.27
0
20
0
101
80-120
20.59
0
20
0
103
80-120
19.62
0
20
0
98.1
80-120
0
0
0
0
0
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 26 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11 Method: SW8260C
MS Sample ID: 22120007-09A MS
I
Units: pg/L
Analysis Date: 12/8/2022 07:05 AM
Client ID: ow
Run ID:
VMS11_221207A
SegNo:
9084645
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit
Qual
1,1,1-Trichloroethane
22.46
1.0
20
0
112
75-119
0
1,1,2,2-Tetrachloroethane
18.45
1.0
20
0
92.2
80-123
0
1,1,2-Trichloroethane
19.89
1.0
20
0
99.4
83-118
0
1,1,2-Trichlorotrifluoroethane
28.13
1.0
20
0
141
64-133
0
S
1,1-Dichloroethane
25.73
1.0
20
0
129
73-122
0
S
1,1-Dichloroethene
29.03
1.0
20
0
145
66-131
0
S
1,2,3-Trichlorobenzene
13.39
1.0
20
0
67
65-140
0
1,2,3-Trichloropropane
17.57
1.0
20
0
87.8
78-119
0
1,2,4-Trichlorobenzene
16.22
1.0
20
0
81.1
73-127
0
1,2,4-Trimethyl benzene
20.64
1.0
20
0
103
74-118
0
1,2-Dibromo-3-chloropropane
15.37
1.0
20
0
76.8
52-141
0
1,2-Dibromoethane
19.6
1.0
20
0
98
60-159
0
1,2-Dichlorobenzene
19.45
1.0
20
0
97.2
80-119
0
1,2-Dichloroethane
22.51
1.0
20
0
113
78-121
0
1,2-Dichloropropane
23.08
1.0
20
0
115
78-120
0
1,3,5-Trimethyl benzene
20.95
1.0
20
0
105
76-120
0
1,3-Dichlorobenzene
19.28
1.0
20
0
96.4
80-120
0
1,4-Dichlorobenzene
19.25
1.0
20
0
96.2
81-119
0
2-Butanone
22.99
5.0
20
0
115
69-147
0
2-Hexanone
17.83
5.0
20
0
89.2
67-140
0
4-Methyl-2-pentanone
23.68
1.0
20
0
118
68-199
0
Acetone
26.45
10
20
0.38
130
70-166
0
Benzene
24.59
1.0
20
0
123
78-120
0
S
Bromochloromethane
23.37
1.0
20
0
117
70-125
0
Bromodichloromethane
22.16
1.0
20
0
111
73-126
0
Bromoform
16.99
1.0
20
0
85
60-124
0
Bromomethane
15.09
1.0
20
0
75.4
20-183
0
Carbon disulfide
23.77
1.0
20
0
119
67-159
0
Carbon tetrachloride
22.19
1.0
20
0
111
69-124
0
Chlorobenzene
20.92
1.0
20
0
105
80-118
0
Chloroethane
27.9
1.0
20
0
140
35-136
0
S
Chloroform
24.57
1.0
20
0
123
75-119
0
S
Chloromethane
23.29
1.0
20
0
116
26-117
0
cis- 1,3-Dichloropropene
20.34
1.0
20
0
102
69-120
0
Cyclohexane
27.16
2.0
20
0
136
66-128
0
S
Dibromochloromethane
17.48
1.0
20
0
87.4
63-117
0
Dichlorodifluoromethane
33.46
1.0
20
0
167
36-133
0
S
Ethylbenzene
21.22
1.0
20
0
106
76-116
0
Isopropyl benzene
20.87
1.0
20
0
104
77-118
0
m,p-Xylene
42.57
2.0
40
0
106
76-119
0
Methyl tert-butyl ether
24.93
1.0
20
0
125
77-137
0
Methylcyclohexane
22.99
1.0
20
0
115
66-125
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 27 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: R359809b Instrument ID VMS11
Method:
SW8260C
Methylene chloride
25.52
5.0
20
0
128
68-125
0 S
o-Xylene
21.24
1.0
20
0
106
77-116
0
Styrene
20.02
1.0
20
0
100
76-123
0
Tetrachloroethene
21.7
1.0
20
0
108
80-124
0
Toluene
21.9
1.0
20
0
110
78-116
0
trans-1,2-Dichloroethene
26.64
1.0
20
0
133
73-124
0 S
trans-1,3-Dichloropropene
18.7
1.0
20
0
93.5
67-118
0
Trichloroethene
22.34
1.0
20
0
112
75-122
0
Trichlorofluoromethane
26.12
1.0
20
0
131
52-115
0 S
Xylenes, Total
63.81
3.0
60
0
106
77-119
0
Surr 1,2-Dichloroethane-d4
19.51
0
20
0
97.6
80-120
0
Surr 4-Bromofluorobenzene
21.13
0
20
0
106
80-120
0
Surr Dibromofluoromethane
20.1
0
20
0
100
80-120
0
Surr: Toluene-d8
18.62
0
20
0
93.1
80-120
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 28 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11
Method: SW8260C
QC BATCH REPORT
I
Analysis Date: 12/8/2022 06:43 AM
DUP Sample ID: 22120007-08A DUP
Units: pg/L
Client ID:
Run ID:
VMS11_221207A
SegNo: 9084641
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
�Analyte
Result
PQL
SPK Val Value
%REC Limit
Value
%RPD
Limit Qual
1,1,1-Trichloroethane
U
1.0
0
0 0
0
0
30
1,1,2,2-Tetrachloroethane
U
1.0
0
0 0
0
0
30
1,1,2-Trichloroethane
U
1.0
0
0 0
0
0
30
1,1,2-Trichlorotrifluoroethane
U
1.0
0
0 0
0
0
30
1,1-Dichloroethane
U
1.0
0
0 0
0.25
0
30
1,1-Dichloroethene
U
1.0
0
0 0
0
0
30
1,2,3-Trichlorobenzene
U
1.0
0
0 0
0
0
30
1,2,3-Trichloropropane
U
1.0
0
0 0
0
0
30
1,2,4-Trichlorobenzene
U
1.0
0
0 0
0
0
30
1,2,4-Trimethyl benzene
U
1.0
0
0 0
0
0
30
1,2-Dibromo-3-chloropropane
U
1.0
0
0 0
0
0
30
1,2-Dibromoethane
U
1.0
0
0 0
0
0
30
1,2-Dichlorobenzene
U
1.0
0
0
0
0
0
30
1,2-Dichloroethane
U
1.0
0
0
0
0
0
30
1,2-Dichloropropane
U
1.0
0
0
0
0
0
30
1,3,5-Trimethyl benzene
U
1.0
0
0
0
0
0
30
1,3-Dichlorobenzene
U
1.0
0
0
0
0
0
30
1,4-Dichlorobenzene
U
1.0
0
0
0
0
0
30
2-Butanone
U
5.0
0
0
0
0
0
30
2-Hexanone
U
5.0
0
0
0
0
0
30
4-Methyl-2-pentanone
U
1.0
0
0
0
0
0
30
Acetone
U
10
0
0
0
0.47
0
30
Benzene
U
1.0
0
0
0
0
0
30
Bromochloromethane
U
1.0
0
0
0
0
0
30
Bromodichloromethane
U
1.0
0
0
0
0
0
30
Bromoform
U
1.0
0
0
0
0
0
30
Bromomethane
U
1.0
0
0
0
0
0
30
Carbon disulfide
U
1.0
0
0
0
0
0
30
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
U 1.0 0 0 0
U 1.0 0 0 0
0 0 30
0 0 30
U 1.0
0
0
0
0
0
30
U 1.0
0
0
0
0
0
30
U 1.0
0
0
0
0
0
30
U 1.0
0
0
0
0
0
30
U 2.0
0
0
0
0
0
30
U 1.0
0
0
0
0
0
30
Dichlorodifluoromethane
U
1.0
0
0
0
0
0
30
Ethylbenzene
U
1.0
0
0
0
0
0
30
Isopropyl benzene
U
1.0
0
0
0
0
0
30
m,p-Xylene
U
2.0
0
0
0
0
0
30
Methyl acetate
U
2.0
0
0
0
0
0
30
Methyl tert-butyl ether
U
1.0
0
0
0
0
0
30
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 29 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359809b Instrument ID VMS11
Methylcyclohexane
Methylene chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Xylenes, Total
Surr. 1, 2-Dichloroethane-d4
Surr 4-Bromofluorobenzene
Surr. Dibromofluoromethane
Surr.• Toluene-d8
Method: SW8260C
U
1.0
0
U
5.0
0
U
1.0
0
U
1.0
0
U
1.0
0
U
1.0
0
1.66
1.0
0
U
1.0
0
U
1.0
0
U
1.0
0
U
3.0
0
19.7
0
20
20.12
0
20
19.11
0
20
18.8
0
20
The following samples were analyzed in this batch: 22120229-04H
QC BATCH REPORT
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 0
1.84
10.3
30
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 0
0
0
30
0 98.5 80-120
19.7
0
30
0 101
0 95.6
80-120
80-120
20.15
19.37
0.149
1.35
30
30
0 94
80-120
19.63
4.32
30
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 30 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: R359826a Instrument ID VMS8
Method:
SW8260C
MBLK Sample ID: 8V-BLKW1-221208-R359826a
Units: pg/L
Analysis Date: 12/8/2022 11:33 AM
Client ID: Mll
Run ID:
VMS8_221208A
SegNo: 9087929
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
cis-1,2-Dichloroethene
U
1.0
Vinyl chloride
U
1.0
Surr. 1,2-Dichloroethane-d4
20.84
0
20
0 104
80-120
0
Surr 4-Bromofluorobenzene
19.54
0
20
0 97.7
80-120
0
Surr Dibromofluoromethane
20.42
0
20
0 102
80-120
0
Surr: Toluene-d8
19.79
0
20
0 99
80-120
0
LCS Sample ID: 8V-LCSW1-221208-R359826a
Units: pg/L
Analysis Date: 12/8/2022 11:15 AM
Client ID:
Run ID:
VMS8_221208A
SegNo: 9087928
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
-
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
cis-1,2-Dichloroethene
21.76
1.0
20
0 109
75-123
0
Vinyl chloride
20.9
1.0
20
0 104
49-122
0
Surr 1,2-Dichloroethane-d4
19.95
0
20
0 99.8
80-120
0
Surr:4-Bromofluorobenzene
20.22
0
20
0
101
80-120
0
Surr Dibromofluoromethane
19.8
0
20
0
99
80-120
0
Surr Toluene-d8
19.57
0
20
0
97.8
80-120
0
MS Sample ID: 22120229-03H
MS
Units: pg/L
Analysis Date: 12/8/2022 06:34 PM
Client ID: IRY165:RW-3:G113022
Run ID:
VMS8_221208A
SegNo:
9087951
Prep Date: DF: 20
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
cis-1,2-Dichloroethene
2036
20
400
1763
68.4
75-123
0 SEO
Vinyl chloride
901.2
20
400
309
148
49-122
0
S
Surr:1,2-Dichloroethane-d4
408
0
400
0
102
80-120
0
Surr 4-Bromofluorobenzene
401.2
0
400
0
100
80-120
0
Surr. Dibromofluoromethane
397
0
400
0
99.2
80-120
0
Surr: Toluene-d8
399.4
0
400
0
99.8
80-120
0
MENEU
MSD Sample ID: 22120229-03H
MSD
Units: pg/L
Analysis
Date: 12/8/2022 06:53 PM
Client ID: IRY165:RW-3:G113022
Run ID:
VMS8_221208A
SegNo: 9087952
Prep Date:
DF: 20
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value
%RPD
Limit
Qual
cis-1,2-Dichloroethene
2080
20
400
1763
79.3
75-123
2036
2.13
30
EO
Vinyl chloride
903.2
20
400
309
149
49-122
901.2
0.222
30
S
Surr:1,2-Dichloroethane-d4
410.8
0
400
0
103
80-120
408
0.684
30
Surr 4-Bromofluorobenzene
383
0
400
0
95.8
80-120
401.2
4.64
30
Surr: Dibromofluoromethane
394.2
0
400
0
98.6
80-120
397
0.708
30
Surr Toluene-d8
398.6
0
400
0
99.6
80-120
399.4
0.201
30
The following samples were analyzed in this batch:
22120229-03H
22120229-04H
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 31 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: R359833b Instrument ID VMS7 Method: SW8260C
MBLK Sample ID: 7V-BLKW1-221208-R359833b Units: pg/L Analysis Date: 12/8/2022 12:00 PM
Client ID: Run ID: VMS7_221208A SegNo: 9089885 Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
Vinyl chloride
U
1.0
Surr 1,2-Dichloroethane-d4
21.56
0
20
0
108
80-120
0
Surr 4-Bromofluorobenzene
17.77
0
20
0
88.8
80-120
0
Surr Dibromofluoromethane
19.58
0
20
0
97.9
80-120
0
Surr Toluene-d8
20.98
0
20
0
105
80-120
0
LCS Sample ID: 7V-LCSW1-221208-R359833b
Units: pg/L� Analysis Date: 12/8/2022 11:10 AM
Client ID: '
Run ID: VMS7_221208A
SegNo: 9089883
Prep Date: DF: 1
SPK Ref Control
RPD Ref RPD
Analyte
Result PQL
SPK Val
Value %REC Limit
Value %RPD Limit Qual
Vinyl chloride
20.54 1.0
20
0 103 49-122
0
Surr 1,2-Dichloroethane-d4
20.76 0
20
0 104 80-120
0
Surr 4-Bromofluorobenzene
20.15 0
20
0 101 80-120
0
Surr. Dibromofluoromethane
20.28 0
20
0 101 80-120
0
Surr Toluene-d8
20.51 0
20
0 103 80-120
0
MS Sample ID: 22120229-04H MS
Units: pg/L
Analysis Date: 12/8/2022 06:41 PM
Client ID: IRY165:RW-3:G113022A
Run ID: VMS7_221208A
SegNo: 9089908
Prep Date: DF: 50
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL
SPK Val
Value
%REC
Limit
Value
%RPD
Limit Qual
Vinyl chloride
1349
50
1000
167.5
118
49-122
0
Surr:1,2-Dichloroethane-d4
1091
0
1000
0
109
80-120
0
Surr 4-Bromofluorobenzene
1011
0
1000
0
101
80-120
0
Surr Dibromofluoromethane
1014
0
1000
0
101
80-120
0
Surr: Toluene-d8
1002
0
1000
0
100
80-120
0
MSD Sample ID: 22120229-04H MSD
'
Units: pg/L
Analysis
Date: 12/8/2022
06:58 PM
Client ID: IRY165:RW-3:G113022A
Run ID:
VMS7_221208A
SegNo:9089909
Prep Date:
DF: 50
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC
Limit
Value
%RPD
Limit Qual
Vinyl chloride
1439
50
1000
167.5
127
49-122
1349
6.46
30 S
Surr. 1,2-Dichloroethane-d4
1066
0
1000
0
107
80-120
1091
2.36
30
Surr 4-Bromofluorobenzene
1004
0
1000
0
100
80-120
1011
0.745
30
Surr Dibromofluoromethane
1032
0
1000
0
103
80-120
1014
1.71
30
Surr Toluene-d8
997.5
0
1000
0
99.8
80-120
1002
0.4
30
The following samples were analyzed in this batch:
22120229-01 H
22120229-02H
22120229-04H
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 32 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12 Method: SW8260C
QC BATCH REPORT
Units: pg/L Analysis Date: 12/8/2022 12:38 AM
MBLK Sample ID: 12V-BLKW2-221207-R359835b
Client ID:
Run ID:
VMS12_221207A
SegNo: 9085737 Prep Date: DF: 1
SPK Ref
Control RPD Ref RPD
�Analyte
Result
PQL SPK Val Value
%REC Limit Value %RPD Limit Qual
1,1,1-Trichloroethane
U
1.0
1,1,2,2-Tetrachloroethane
U
1.0
1,1,2-Trichloroethane
U
1.0
1,1,2-Trichlorotrifluoroethane
U
1.0
1,1-Dichloroethane
U
1.0
1,1-Dichloroethene
U
1.0
1,2,3-Trichlorobenzene
U
1.0
1,2,3-Trichloropropane
U
1.0
1,2,4-Trichlorobenzene
U
1.0
1,2,4-Trimethyl benzene
U
1.0
1,2-Dibromo-3-chloropropane
U
1.0
1,2-Dibromoethane
U
1.0
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethyl benzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone
2-Hexanone
4-Methyl-2-pentanone
Acetone
U
U
U
U
U
U
U
U
U
U
1.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
10
Benzene
U
1.0
Bromochloromethane
U
1.0
Bromodichloromethane
U
1.0
Bromoform
U
1.0
Bromomethane
U
1.0
Carbon disulfide
U
1.0
Carbon tetrachloride
U
1.0
Chlorobenzene
U
1.0
Chloroethane
U
1.0
Chloroform
U
1.0
Chloromethane
U
1.0
cis- 1,2-Dichloroethene
U
1.0
cis- 1,3-Dichloropropene
U
1.0
Cyclohexane
U
2.0
Dibromochloromethane
U
1.0
Dichlorodifluoromethane
U
1.0
Ethylbenzene U 1.0
Isopropyl benzene U 1.0
m,p-Xylene U 2.0
Methyl acetate U 2.0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 33 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Methyl tert-butyl ether
U
1.0
Methylcyclohexane
U
1.0
Methylene chloride
U
5.0
o-Xylene
U
1.0
Styrene
U
1.0
Tetrachloroethene
U
1.0
Toluene
U
1.0
trans-1,2-Dichloroethene
U
1.0
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes, Total
Surr. 1, 2-Dichloroethane-d4
Surr 4-Bromofluorobenzene
Surr Dibromofluoromethane
Surr Toluene-d8
Method: SW8260C
U
1.0
U
1.0
U
1.0
U
1.0
U
3.0
20.41
0 20
19.82
0 20
19.68
0 20
19.57 0 20
0 102
80-120
0 99.1
80-120
0 98.4
80-120
0 97.8
80-120
QC BATCH REPORT
0
0
0
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 34 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12 Method: SW8260C
LCS Sample ID: 12V-LCSW1-221207-R359835b
Units: pg/L
Analysis Date: 12/7/2022 11:24 PM
Client ID: ow
Run ID:
VMS12_221207A
SegNo: 9085735
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL
SPK Val Value
%REC
Limit
Value %RPD Limit Qual
1,1,1-Trichloroethane
18.45
1.0
20
0 92.2
75-119
0
1,1,2,2-Tetrachloroethane
19.01
1.0
20
0 95
80-123
0
1,1,2-Trichloroethane
19.16
1.0
20
0 95.8
83-118
0
1,1,2-Trichlorotrifluoroethane
20.38
1.0
20
0 102
64-133
0
1,1-Dichloroethane
19.95
1.0
20
0 99.8
73-122
0
1,1-Dichloroethene
21.93
1.0
20
0 110
66-131
0
1,2,3-Trichlorobenzene
18.93
1.0
20
0 94.6
65-140
0
1,2,3-Trichloropropane
18.61
1.0
20
0
93
78-119
0
1,2,4-Trichlorobenzene
19.03
1.0
20
0
95.2
73-127
0
1,2,4-Trimethyl benzene
18.94
1.0
20
0
94.7
74-118
0
1,2-Dibromo-3-chloropropane
18.44
1.0
20
0
92.2
52-141
0
1,2-Dibromoethane
18.74
1.0
20
0
93.7
60-159
0
1,2-Dichlorobenzene
19.26
1.0
20
0
96.3
80-119
0
1,2-Dichloroethane
18.8
1.0
20
0
94
78-121
1,2-Dichloropropane
18.89
1.0
20
0
94.4
78-120
1,3,5-Trimethyl benzene
19.22
1.0
20
0
96.1
76-120
1,3-Dichlorobenzene
19.43
1.0
20
0
97.2
80-120
1,4-Dichlorobenzene
18.71
1.0
20
0
93.6
81-119
2-Butanone
20.45
5.0
20
0
102
69-147
2-Hexanone
17.83
5.0
20
0
89.2
67-140
4-Methyl-2-pentanone
23.51
1.0
20
0
118
68-199
Acetone
21.14
10
20
0
106
70-166
Benzene
19.2
1.0
20
0
96
78-120
0
0
0
0
0
0
0
0
0
0
Bromochloromethane
20.23
1.0
20
0
101
70-125
0
Bromodichloromethane
20.03
1.0
20
0
100
73-126
0
Bromoform
17.33
1.0
20
0
86.6
60-124
0
Bromomethane
24.22
1.0
20
0
121
20-183
0
Carbon disulfide
18.84
1.0
20
0
94.2
67-159
0
Carbon tetrachloride
20.27
1.0
20
0
101
69-124
0
Chlorobenzene
19.42
1.0
20
0
97.1
80-118
0
Chloroethane
21.25
1.0
20
0
106
35-136
0
Chloroform
19.04
1.0
20
0
95.2
75-119
0
Chloromethane
19.58
1.0
20
0
97.9
26-117
0
cis- 1,2-Dichloroethene
19.79
1.0
20
0
99
75-123
0
cis- 1,3-Dichloropropene
19.05
1.0
20
0
95.2
69-120
0
Cyclohexane
19.4
2.0
20
0
97
66-128
0
Dibromochloromethane
17.15
1.0
20
0
85.8
63-117
0
Dichlorodifluoromethane
22.88
1.0
20
0
114
36-133
0
Ethylbenzene
18.64
1.0
20
0
93.2
76-116
0
Isopropyl benzene
19.35
1.0
20
0
96.8
77-118
0
m,p-Xylene
37.33
2.0
40
0
93.3
76-119
0
Methyl tert-butyl ether
21.13
1.0
20
0
106
77-137
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 35 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Method: SW8260C
QC BATCH REPORT
Methylcyclohexane
18.73
1.0
20
0
93.6
66-125
0
Methylene chloride
19.64
5.0
20
0
98.2
68-125
0
o-Xylene
20.3
1.0
20
0
102
77-116
0
Styrene
18.95
1.0
20
0
94.8
76-123
0
Tetrachloroethene
18.16
1.0
20
0
90.8
80-124
0
Toluene
19.84
1.0
20
0
99.2
78-116
0
trans-1,2-Dichloroethene
19.39
1.0
20
0
97
73-124
0
trans- 1,3-Dichloropropene
17.81
1.0
20
0
89
67-118
0
Trichloroethene
18.14
1.0
20
0
90.7
75-122
0
Trichlorofluoromethane
Vinyl chloride
Xylenes, Total
Surr. 1, 2-Dichloroethane-d4
Surr: 4-Bromofluorobenzene
Surr. Dibromofluoromethane
Surr. Toluene-d8
21.44
1.0
20
0
107
52-115 0
21.24
1.0
20
0
106
49-122 0
57.63
3.0
60
0
96
77-119 0
20.26
0
20
0
101
80-120 0
20.09
0
20
0
100
80-120 0
20.92
0
20
0
105
80-120 0
19.38 0 20 0 96.9 80-120 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 36 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Method: SW8260C
QC BATCH REPORT
MS Sample ID: 22120229-01 H MS I Units: pg/L Analysis Date: 12/8/2022 09:53 AM
Client ID: IRY165:RW-1:G113022 Run ID: VMS12_221207A SegNo: 9085760 Prep Date: DF: 1
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1,2-Trichlorotrifluoroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethyl benzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethyl benzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone
2-Hexanone
4-Methyl-2-pentanone
Acetone
Result
20.55
19.98
41.49
22.36
24.75
35.93
16.81
20.21
17.16
19.86
17.69
19.75
19.44
19.89
20.21
20.23
19.83
19.09
23.61
20.09
25.38
34.83
SPK Ref
Control
RPD Ref RPD
PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
1.0
20
0
103
75-119
0
1.0
20
0
99.9
80-123
0
1.0
20
0
207
83-118
0 S
1.0
20
0
112
64-133
0
1.0
20
2.89
109
73-122
0
1.0
20
13.23
114
66-131
0
1.0
20
0
84
65-140
0
1.0
20
0
101
78-119
0
1.0
20
0
85.8
73-127
0
1.0
20
0
99.3
74-118
0
1.0
20
0
88.4
52-141
0
1.0
20
0
98.8
60-159
0
1.0
20
0.75
93.4
80-119
0
1.0
20
0
99.4
78-121
0
1.0
20
0
101
78-120
0
1.0
20
0
101
76-120
0
1.0
20
0
99.2
80-120
0
1.0
20
0
95.4
81-119
0
5.0
20
0
118
69-147
0
5.0
20
0
100
67-140
0
1.0
20
0
127
68-199
0
10
20
6.53
142
70-166
0
Benzene
22.35
1.0
20
1.1
106
78-120
0
Bromochloromethane
21.79
1.0
20
0
109
70-125
0
Bromodichloromethane
20.3
1.0
20
0
102
73-126
0
Bromoform
15.35
1.0
20
0
76.8
60-124
0
Bromomethane
16.12
1.0
20
0
80.6
20-183
0
Carbon disulfide
24.35
1.0
20
0
122
67-159
0
Carbon tetrachloride
19.71
1.0
20
0
98.6
69-124
0
Chlorobenzene
20.99
1.0
20
0
105
80-118
0
Chloroethane
25.22
1.0
20
0
126
35-136
0
Chloroform
21.43
1.0
20
0
107
75-119
0
Chloromethane
23.68
1.0
20
0
118
26-117
0 S
cis- 1,2-Dichloroethene
832.8
1.0
20
1047
-1070
75-123
0 SEO
cis- 1,3-Dichloropropene
17.75
1.0
20
0
88.8
69-120
0
Cyclohexane
22.93
2.0
20
0
115
66-128
0
Dibromochloromethane
16.98
1.0
20
0
84.9
63-117
0
Dichlorodifluoromethane
29.72
1.0
20
0
149
36-133
0 S
Ethylbenzene
21.13
1.0
20
0.76
102
76-116
0
Isopropyl benzene
21.22
1.0
20
0
106
77-118
0
m,p-Xylene
41.89
2.0
40
1.26
102
76-119
0
Methyl tert-butyl ether
21.69
1.0
20
0
108
77-137
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 37 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Methylcyclohexane
Methylene chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes, Total
Surr. 1, 2-Dichloroethane-d4
Surr. 4-Bromofluorobenzene
Surr.• Dibromofluoromethane
Surr: Toluene-d8
QC BATCH REPORT
Method: SW8260C
LU.33
1.0
20
0
102
66-125
0
21.73
5.0
20
0
109
68-125
0
22.34
1.0
20
0.88
107
77-116
0
19.11
1.0
20
0
95.6
76-123
0
1599
1.0
20
1952
-1770
80-124
0
24.25
1.0
20
1.96
111
78-116
0
58.03
1.0
20
74.48
-82.2
73-124
0
16.26
1.0
20
0
81.3
67-118
0
1054
1.0
20
1467
-2070
75-122
26.71
1.0
20
0
134
52-115
151.4
1.0
20
185.7
-171
49-122
64.23
3.0
60
2.14
103
77-119
20.36
0
20
0
102
80-120
20.44
0
20
0
102
80-120
21
0
20
0
105
80-120
19.64
0
20
0
98.2
80-120
c
0 SEO
0 S
0 SEO
0
0
0
0
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 38 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Method: SW8260C
QC BATCH REPORT
I
Units: pg/L
Analysis Date: 12/8/2022 09:30 AM
DUP Sample ID: 22120229-02H DUP
Client ID: IRY165:RW-2:G113022
Run ID:
VMS12_221207A
SegNo: 9085759
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
�Analyte
Result
PQL
SPK Val Value
%REC Limit
Value
%RPD
Limit Qual
1,1,1-Trichloroethane
U
1.0
0
0 0
0
0
30
1,1,2,2-Tetrachloroethane
U
1.0
0
0 0
0
0
30
1,1,2-Trichloroethane
U
1.0
0
0 0
0
0
30
1,1,2-Trichlorotrifluoroethane
U
1.0
0
0 0
0
0
30
1,1-Dichloroethane
1.19
1.0
0
0 0
1.24
4.12
30
1,1-Dichloroethene 13.87 1.0 0 0 0 14.01 1 30
1,2,3-Trichlorobenzene U 1.0 0 0 0 0 0 30
1,2,3-Trichloropropane
U
1.0
0
0
0
0
0
30
1,2,4-Trichlorobenzene
U
1.0
0
0
0
0
0
30
1,2,4-Trimethyl benzene
U
1.0
0
0
0
0
0
30
1,2-Dibromo-3-chloropropane
U
1.0
0
0
0
0
0
30
1,2-Dibromoethane
U
1.0
0
0
0
0
0
30
1,2-Dichlorobenzene
0.81
1.0
0
0
0
0.94
0
30 J
1,2-Dichloroethane
U
1.0
0
0
0
0
0
30
1,2-Dichloropropane
U
1.0
0
0
0
0
0
30
1,3,5-Trimethyl benzene
U
1.0
0
0
0
0
0
30
1,3-Dichlorobenzene
U
1.0
0
0
0
0
0
30
1,4-Dichlorobenzene
U
1.0
0
0
0
0
0
30
2-Butanone
U
5.0
0
0
0
0
0
30
2-Hexanone
U
5.0
0
0
0
0
0
30
4-Methyl-2-pentanone
U
1.0
0
0
0
0
0
30
Acetone
U
10
0
0
0
6.27
0
30
Benzene
1.72
1.0
0
0
0
1.83
6.2
30
Bromochloromethane
U
1.0
0
0
0
0
0
30
Bromodichloromethane
U
1.0
0
0
0
0
0
30
Bromoform
U
1.0
0
0
0
0
0
30
Bromomethane
U
1.0
0
0
0
0
0
30
Carbon disulfide
1.44
1.0
0
0
0
0.93
43
30 R
Carbon tetrachloride
U
1.0
0
0
0
0
0
30
Chlorobenzene
U
1.0
0
0
0
0.37
0
30
Chloroethane
U
1.0
0
0
0
0
0
30
Chloroform
U
1.0
0
0 0
Chloromethane
U
1.0
0
0 0
cis- 1,2-Dichloroethene
1254
1.0
0
0 0
cis- 1,3-Dichloropropene
U
1.0
0
0 0
Cyclohexane
U
2.0
0
0 0
Dibromochloromethane
U
1.0
0
0 0
Dichlorodifluoromethane
U
1.0
0
0 0
Ethylbenzene
U
1.0
0
0 0
Isopropyl benzene
U
1.0
0
0 0
m,p-Xylene
0.93
2.0
0
0 0
Methyl acetate
U
2.0
0
0 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation
0
0
30
0
0
30
1234
1.67
30 E
0
0
30
0
0
30
0
0
30
0
0
30
0
0
30
0
0
30
0.89
0
30 J
0
0
30
QC Page: 39 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359835b Instrument ID VMS12
Methyl tert-butyl ether
U
Methylcyclohexane
U
Methylene chloride
U
o-Xylene
1.51
Styrene
U
Tetrachloroethene
106.9
Toluene
0.51
trans- 1,2-Dichloroethene
102.2
trans- 1,3-Dichloropropene
U
Trichloroethene
137.3
Trichlorofluoromethane
U
Vinyl chloride
268
Xylenes, Total
2.44
Surr. 1, 2-Dichloroethane-d4
20.47
Surr 4-Bromofluorobenzene
19.72
Surr Dibromofluoromethane
20.66
Surr Toluene-d8
19.79
The following samples were analyzed in this batch:
QC BATCH REPORT
Method: SW8260C
1.0 0
0 0
0
0
30
1.0 0
0 0
0
0
30
5.0 0
0 0
0
0
30
1.0 0
0 0
1.52
0.66
30
1.0 0
0 0
0
0
30
1.0 0
0 0
106.8
0.0561
30
E
1.0 0
0 0
0.47
0
30
J
1.0 0
0 0
60.26
51.6
30
RE
1.0 0
0 0
0
0
30
1.0 0
0 0
136.8
0.343
30
E
1.0 0
0 0
0
0
30
1.0 0
0 0
268.2
0.0895
30
E
3.0 0
0 0
2.41
0
30
J
0 20
0 102
80-120 21.05
2.79
30
0 20
0 98.6
80-120 19
3.72
30
0 20
0 103
80-120 20.94
1.35
30
0 20
0 99
80-120 19.68
0.557
30
22120229-01H
22120229-02H
22120229-03H
22120229-05H
22120229-06A
22120229-07A
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 40 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
QC BATCH REPORT
Batch ID: R359948a Instrument ID VMS7 Method: SW8260C
MBLK Sample ID: 7V-BLKW1-221209-R359948a Units: pg/L Analysis Date: 12/9/2022 12:54 PM
Client ID: Run ID: VMS7_221209A SegNo: 9091435 Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result PQL
SPK Val
Value
%REC
Limit
Value %RPD Limit Qual
cis- 1,2-Dichloroethene
U 1.0
Tetrachloroethene
U 1.0
Trichloroethene
U 1.0
Vinyl chloride
U 1.0
Surr 1,2-Dichloroethane-d4
22.59 0
20
0
113
80-120
0
Surr 4-Bromofluorobenzene
18.04 0
20
0
90.2
80-120
0
Surr Dibromofluoromethane
20.23 0
20
0
101
80-120
0
Surr Toluene-d8
20.07 0
20
0
100
80-120
0
LCS Sample ID: 7V-LCSW1-221209-R359948a
T
Units: Ng/L
Analysis Date: 12/9/2022 12:05 PM
Client ID:
Run ID: VMS7_221209A
SegNo:9091433
Prep Date: DF: 1
Analyte Result
cis- 1,2-Dichloroethene
Tetrachloroethene
21.44
19.47
Trichloroethene
18.35
Vinyl chloride
21.06
Surr 1,2-Dichloroethane-d4
21.92
Surr 4-Bromofluorobenzene
20.24
Surr Dibromofluoromethane
20.35
Surr Toluene-d8
20.26
The following samples were analyzed in this batch:
PQL
SPK Val
SPK Ref
Value
%REC
Control
Limit
RPD Ref RPD
Value %RPD Limit Qual
1.0
20
0
107
75-123
0
1.0
20
0
97.4
80-124
0
1.0
20
0
91.8
75-122
0
1.0
20
0
105
49-122
0
0
20
0
110
80-120
0
0
20
0
101
80-120
0
0
20
0
102
80-120
0
0
20
0
101
80-120
0
22120229-01H 22120229-02H
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 41 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207727 Instrument ID TDS
MBLK
Client ID: IF
Method: A2540 C-15
Units: mg/L Analysis Date: 12/8/2022 12:10 PM
SegNo: 9085993 Prep Date: 12/5/2022 DF: 1
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %oRPD Limit Qual
Total Dissolved Solids U 30
LCS Sample ID: LCS-207727-207727
Client ID: Run ID: TDS 221208A
Sample ID: MBLK-207727-207727
Run ID: TDS 221208A
SPK Ref
IAnalyte
Result PQL SPK Val
Value
Total Dissolved Solids
504 30 495
DUP
Sample ID: 22112527-01C DUP
Client ID:
Run ID: TDS 221208A
SPK Ref
Analyte
Result PQL SPK Val
Value
Total Dissolved Solids
283.3 50 0
DUP
Sample ID: 22112540-03C DUP
Client ID:
Run ID: TDS 221208A
Total Dissolved Solids
SPK Ref
Result PQL SPK Val Value
1780 150 0
Units: mg/L
Analysis Date: 12/8/2022 12:10 PM
SegNo: 9085992
Prep Date: 12/5/2022
DF: 1
Control
RPD Ref
RPD
%REC Limit
Value %RPD
Limit Qual
D 102 85-109
0
Units: mg/L
Analysis Date: 12/8/2022 12:10 PM
SegNo: 9085978
Prep Date: 12/5/2022
DF: 1
Control
RPD Ref
RPD
%REC Limit
Value %RPD
Limit Qual
D 0 0-0 260 8.59 10
Units: mg/L Analysis Date: 12/8/2022 12:10 PM
SegNo: 9085985 Prep Date: 12/5/2022 DF: 1
Control RPD Ref RPD
%REC Limit Value %oRPD Limit Qual
D 0 0-0 1850 3.86 10
The following samples were analyzed in this batch: 22120229-01 F 22120229-02F 22120229-03F
22120229-04F 22120229-05F
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 42 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: 207809 Instrument ID TSS
Method: A2540 D-15
QC BATCH REPORT
MBLK Sample ID: MBLK-207809-207809 Units: mg/L Analysis Date: 12/7/2022 02:27 PM
Client ID: R Run ID: TSS_221207A SegNo: 9082676 Prep Date: 12/6/2022 DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD
Limit Qual
Total Suspended Solids
U
0.60
LCS Sample ID: LCS-207809-207809
Units: mg/L
Analysis Date: 12/7/2022 02:27 PM
Client ID:
Run ID:
TSS_221207A
SegNo: 9082675
Prep Date: 12/6/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD
Limit Qual
Total Suspended Solids
99
6.0 100
0 99 75-111
0
DUP Sample ID: 22120106-02B DUP
Units: mg/L
Analysis Date: 12/7/2022 02:27 PM
Client ID:
Run ID:
TSS_221207A
SegNo: 9082656
Prep Date: 12/6/2022
DF: 1
�Analyte
SPK Ref
Control
RPD Ref
RPD
Result
PQL SPK Val
Value
%REC Limit
Value %RPD
Limit Qual
Total Suspended Solids
17.33
4.0 0
0 0 0-0
16.67 3.92
10
DUP Sample ID: 22120111-02B DUP
Units: mg/L
Analysis Date: 12/7/2022 02:27 PM
Client ID:
Run ID:
TSS_221207A
SegNo: 9082659
Prep Date: 12/6/2022
DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL SPK Val
Value
%REC Limit
Value %RPD
Limit Qual
Total Suspended Solids
3.778
1.3 0
0 0 0-0
4 5.71
10
The following samples were analyzed in this batch:
22120229-01 D
22120229-02D 22120229-03D
22120229-04D
22120229-05D
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 43 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359455b Instrument ID TOC3
MBLK
Client ID:
QC BATCH REPORT
Method: A531OC-14
Units: mg/L Analysis Date: 12/3/2022 12:55 PM
SegNo: 9070908 Prep Date: DF: 1
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %RPD Limit Qual
Sample ID: MB-R359455-R359455b
W Run ID: TOC3_221203A
Organic Carbon, Total
U 0.50
LCS
Sample ID: LCS-R359455-R359455b
Units: mg/L
Analysis Date: 12/3/2022 01:27 PM
Client ID:
Run ID: TOC3_221203A
SegNo: 9070909
Prep Date: DF: 1
SPK Ref Control
RPD Ref RPD
IAnalyte
Result PQL SPK Val
Value %REC Limit
Value %RPD Limit Qual
Organic Carbon, Total
4.918 0.50 5
0 98.4 80-120
0
MS
Sample ID: 22120207-01 E MS
Units: mg/L
Analysis Date: 12/3/2022 09:49 PM
Client ID:
Run ID: TOC3_221203A
SegNo: 9070892
Prep Date: DF: 40
SPK Ref Control
RPD Ref RPD
Analyte
Result PQL SPK Val
Value %REC Limit
Value %RPD Limit Qual
Organic Carbon, Total
204.4 20 200
5.8 99.3 65-133
0
MSD
Sample ID: 22120207-01E MSD
Units: mg/L
Analysis Date: 12/3/2022 10:23 PM
Client ID:
Run ID: TOC3_221203A
SegNo: 9070893
Prep Date: DF: 40
SPK Ref Control
RPD Ref RPD
IAnalyte
Result PQL SPK Val
Value %REC Limit
Value %RPD Limit Qual
Organic Carbon, Total
204.5 20 200
5.8 99.4 65-133
204.4 0.0587 6.16
The following samples were analyzed in this batch: 22120229-01G 22120229-02G 22120229-03G
22120229-04G 22120229-05G
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 44 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359519 Instrument ID Titrator 1 Method: E150.1
LCS
Sample ID: LCS-R359519-R359519
I
Units: s.u.
Analysis Date: 12/5/2022 10:42 AM
Client ID: ,
Run ID: TITRATOR 1_221205A
SegNo: 9073379
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL SPK Val Value
%REC
Limit
Value %RPD Limit Qual
pH (laboratory)
4.04
0.10 4
0 101
92-108
0
LCS
Sample ID: LCS-R359519-R359519
Units: s.u.
'
Analysis Date: 12/5/2022 10:42 AM
Client ID:
Run ID: TITRATOR 1_221205A
SegNo: 9073434
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result
PQL SPK Val Value
%REC
Limit
Value %RPD Limit Qual
pH (laboratory)
4.04
0.10 4
0 101
92-108
0
DUP
Sample ID: 22120229-01C dup
Units: s.u.
Analysis Date: 12/5/2022 10:42 AM
Client ID: IRY165:RW-1:G113022 Run ID: TITRATOR
1_221205A
SegNo: 9073381
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result
PQL SPK Val Value
%REC
Limit
Value %RPD Limit Qual
pH (laboratory)
5.57
0.10 0
0 0
0-0
5.59 0.358 5 H
Temperature
19.55
0.10 0
0 0
19.61 0.306 H
DUP
Sample ID: 22120258-03C dup
Units: s.u.
Analysis Date: 12/5/2022 10:42 AM
Client ID:
Run ID: TITRATOR 1_221205A
SegNo:9073443
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val Value
%REC
Limit
Value %RPD Limit Qual
pH (laboratory)
7.3
0.10 0
0 0
0-0
7.29 0.137 5
Temperature
20.58
0.10 0
0 0
20.67 0.436
The following samples were analyzed in this batch:
22120229-01C 22120229-02C
22120229-03C
22120229-04C 22120229-05C
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 45 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359609 Instrument ID WETCHEM Method: A2340 C-11
QC BATCH REPORT
MBLK
Sample ID: MB-R359609-R359609
Units: mg/L CaCO3
Analysis Date: 12/6/2022 08:30 AM
Client ID:
, Run ID: WETCHEM_221206C
SegNo: 9077005
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
U 5.0
LCS
Sample ID: LCS-R359609-R359609
Units: mg/L CaCO3
Analysis Date: 12/6/2022 08:30 AM
Client ID:
Run ID: WETCHEM_221206C
SegNo: 9077006
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
100 5.0 100
0 100 95-105
0
DUP
Sample ID: 22120125-01B DUP
Units: mg/L CaCO3
Analysis Date: 12/6/2022 08:30 AM
Client ID:
Run ID: WETCHEM_221206C
SegNo: 9077010
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
485 5.0 0
0 0 0-0
485 0 10
DUP
Sample ID: 22120125-07B DUP
Units: mg/L CaCO3
Analysis Date: 12/6/2022 08:30 AM
Client ID:
Run ID: WETCHEM_221206C
SegNo: 9077017
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
730 5.0 0
0 0 0-0
730 0 10
The following samples were analyzed in this batch: 22120229-01 B
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 46 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359641 Instrument ID Titrator 1 Method: A2320 B-11
MBLK Sample ID: MB-R359641-R359641 I Units: mg/L
Client ID: R Run ID: TITRATOR 1_221206B SegNo: 9078171
SPK Ref Control
A I R It PQL SPK Va I Value 0/ nGr Limit
na yte
esu
Alkalinity, Bicarbonate (as CaCO3)
U
2.0
Alkalinity, Carbonate (as CaCO3)
U
2.0
Alkalinity, Hydroxide (as CaCO3)
U
2.0
Alkalinity, Total (as CaCO3)
U
2.0
MBLK Sample ID: MB-R359641-R359641
Client ID:
Run ID: TITRATOR 1 221206B
SPK Re
�Analyte
Result
PQL
SPK Val Value
Alkalinity, Bicarbonate (as CaCC3)
U
10
Alkalinity, Carbonate (as CaCO3)
U
10
Alkalinity, Hydroxide (as CaCO3)
U
10
Alkalinity, Total (as CaCO3)
U
10
DUP Sample ID: 22120118-01A
dup
Client ID:
Run ID: TITRATOR 1 221206B
SPK Re
Analyte
Result
PQL
SPK Val Value
Alkalinity, Bicarbonate (as CaCO3)
113.7
10
0
Alkalinity, Carbonate (as CaCO3)
U
10
0
Alkalinity, Hydroxide (as CaCO3)
U
10
0
Alkalinity, Total (as CaCO3)
113.7
10
0
DUP Sample ID: 22120118-02A
dup
Client ID:
Run ID: TITRATOR 1_221206B
SPK Re
�Analyte
Result
PQL
SPK Val Value
Alkalinity, Bicarbonate (as CaCO3)
95.19
10
0
Alkalinity, Carbonate (as CaCO3)
U
10
0
Alkalinity, Hydroxide (as CaCO3)
U
10
0
Alkalinity, Total (as CaCO3)
95.19
10
0
DUP Sample ID: 22120118-01A DUP
Client ID: Run ID: TITRATOR 1 221206B
SPK Ref
Analyte Result PQL SPK Val Value
Alkalinity, Bicarbonate (as CaCO3) 95.19 2.0 0
Alkalinity, Carbonate (as CaCO3) U 2.0 0
Alkalinity, Hydroxide (as CaCO3) U 2.0 0
Alkalinity, Total (as CaCO3) 95.19 2.0 0
Note: See Qualifiers Page for a list of Qualifiers and their explanation
Analysis Date: 12/6/2022 12:27 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
Units: mg/L Analysis Date: 12/6/2022 12:27 PM
SegNo: 9078179 Prep Date: DF: 1
Control RPD Ref RPD
%REC Limit Value %RPD Limit Qual
KIND,
SegNo:9078183
Control
%REC Limit
0 0-0
0 0 0-0
0 0 0-0
0 0 0-0
Units: mg/L
SegNo:9078185
Control
%REC Limit
0 0 0-0
0 0 0-0
0 0 0-0
0 0 0-0
Units: mg/L
SegNo:9078197
Control
%REC Limit
0 0 0-0
0 0 0-0
0 0 0-0
0 0 0-0
Analysis Date: 12/6/2022 12:27 PM
Prep Date: DF: 1
RPD Ref RPD
Value ' %RPD Limit Qual
119.9 5.27 10
0
0 10
0
0 10
119.9
5.27 10
Analysis
Date: 12/6/2022 12:27 PM
Prep Date:
DF: 1
RPD Ref
RPD
Value
%RPD Limit Qual
89.58
6.07 10
0
0 10
0
0 10
89.58
6.07 10
Analysis
Date: 12/6/2022 12:27 PM
Prep Date:
DF: 1
RPD Ref
RPD
Value
%RPD Limit Qual
89.58
6.07
0 0 10
0 0
89.58 6.07 10
QC Page: 47 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359641 Instrument ID Titrator 1 Method: A2320 B-11
The following samples were analyzed in this batch: 22120229-01C 22120229-02C 22120229-03C
22120229-04C 22120229-05C
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 48 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359648B Instrument ID LACHAT Method: E353.2 R2.0
QC BATCH REPORT
MBLK Sample ID: MBLK 2-111359648113 1 Units: mg/L Analysis Date: 12/6/2022 01:46 PM
Client ID: Run ID: LACHAT_221206A SegNo: 9078380 Prep Date: DF: 1
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %RPD Limit Qual
Nitrogen, Nitrate -Nitrite
U
0.020
LCS Sample ID: LCS
2-R359648B
Units: mg/L
Analysis
Date: 12/6/2022 01:47 PM
Client ID:
Run ID:
LACHAT_221206A
SegNo: 9078381
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL
SPK Val
Value
%REC Limit
Value
%RPD Limit Qual
Nitrogen, Nitrate -Nitrite
2.631
0.020
2.5
0 105 91-114
0
MS Sample ID: 22120087-02A MS
Units: mg/L
Analysis
Date: 12/6/2022 02:01 PM
Client ID:
Run ID:
LACHAT_221206A
SegNo: 9078392
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC Limit
Value
%RPD Limit Qual
Nitrogen, Nitrate -Nitrite
4.531
0.020
2.5
0.4001 165 91-114
0
S
MS Sample ID: 22120087-06B MS
Units: mg/L
Analysis
Date: 12/6/2022 02:45 PM
Client ID:
Run ID:
LACHAT_221206A
SegNo: 9079314
Prep Date:
DF: 5
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL
SPK Val
Value
%REC Limit
Value
%RPD Limit Qual
Nitrogen, Nitrate -Nitrite
15.82
0.10
2.5
12.52 132 91-114
0
SO
MSD Sample ID: 22120087-02A MSD
Units: mg/L
Analysis
Date: 12/6/2022 02:02 PM
Client ID:
Run ID:
LACHAT_221206A
SegNo: 9078393
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC Limit
Value
%RPD Limit Qual
Nitrogen, Nitrate -Nitrite
4.515
0.020
2.5
0.4001 165 91-114
4.531
0.354 20 S
MSD Sample ID: 22120087-06B MSD
Units: mg/L
Analysis
Date: 12/6/2022 02:47 PM
Client ID:
Run ID:
LACHAT_221206A
SegNo: 9079315
Prep Date:
DF: 5
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL
SPK Val
Value
%REC Limit
Value
%RPD Limit Qual
Nitrogen, Nitrate -Nitrite
15.74
0.10
2.5
12.52 129 91-114
15.82
0.507 20 SO
The following samples were analyzed in this batch: 22120229-01A 22120229-02A
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 49 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359648C Instrument ID LACHAT Method: E353.2 R2.0
MBLK Sample ID: MBLK 3-R359648C I Units: mg/L
Client ID: Run ID: LACHAT_221206A SegNo: 9079327
SPK Ref Control
Analyte Result PQL SPK Val Value %REC Limit
Nitrogen, Nitrate -Nitrite
U
0.020
LCS Sample ID: LCS 3-R359648C
Client ID:
Run ID:
LACHAT 221206A
SPK Ref
IAnalyte
Result
PQL
SPK Val
Value
Nitrogen, Nitrate -Nitrite
2.696
0.020
2.5
MS Sample ID: 22120229-03A
MS
Client ID: IRY165:RW-3:G113022
Run ID:
LACHAT 221206A
SPK Ref
Analyte
Result
PQL
SPK Val
Value
Nitrogen, Nitrate -Nitrite
4.354
0.020
2.5
0.295
MSD Sample ID: 22120229-03A
MSD
Client ID: IRY165:RW-3:G113022
Run ID:
LACHAT 221206A
SPK Ref
IAnalyte
Result
PQL
SPK Val
Value
Nitrogen, Nitrate -Nitrite
4.134
0.020
2.5
0.295
Units: mg/L
SegNo:9079328
Control
%REC Limit
0 108 91-114
Units: mg/L
SegNo:9079330
Control
%REC Limit
1 162 91-114
Units: mg/L
SegNo:9079331
Control
%REC Limit
1 154 91-114
The following samples were analyzed in this batch: 22120229-03A 22120229-04A
QC BATCH REPORT
Analysis Date: 12/6/2022 03:01 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
Analysis Date: 12/6/2022 03:02 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0
Analysis Date: 12/6/2022 03:05 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
0 S
Analysis Date: 12/6/2022 03:06 PM
Prep Date: DF: 1
RPD Ref RPD
Value %RPD Limit Qual
4.354 5.18 20 S
22120229-05A
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 50 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359680 Instrument ID WETCHEM Method: A4500-CI C-11
MBLK Sample ID: MB-R359680-R359680 I Units: mg/L Analysis Date: 12/6/2022 04:00 PM
Client ID: , Run ID: WETCHEM_2212061 SegNo: 9079485 Prep Date: DF: 1
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %RPD Limit Qual
Chloride
U
3.0
LCS
Sample ID: LCS-R359680-R359680
Units: mg/L
Analysis
Date: 12/6/2022 04:00 PM
Client ID:
Run ID: WETCHEM_2212061
SegNo: 9079486
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value
%RPD Limit Qual
Chloride
50.99
3.0 50
0 102 91-111
0
MS
Sample ID: 22120291-01B MS
Units: mg/L
Analysis
Date: 12/6/2022 04:00 PM
Client ID:
Run ID: WETCHEM_2212061
SegNo: 9079493
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL SPK Val Value
%REC Limit
Value
%RPD Limit Qual
Chloride
2150
3.0 50 2899 -1500 91-111
0
SO
MSD
Sample ID: 22120291-01B MSD
Units: mg/L
Analysis
Date: 12/6/2022 04:00 PM
Client ID:
Run ID: WETCHEM_2212061
SegNo: 9079494
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value
%RPD Limit Qual
Chloride
2349
3.0 50 2899 -1100 91-111
2150
8.89 10 SO
The following samples were analyzed in this batch: 22120229-01C 22120229-02C
22120229-04C 22120229-05C
22120229-03C
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 51 of 54

Client: Verdantas
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359715 Instrument ID GALLERY Method: A4500-SO4 E-11
QC BATCH REPORT
MBLK
Sample ID: MBLK-R359715
Units: mg/L
Analysis Date: 12/6/2022 03:26 PM
Client ID:
, Run ID:
GALLERY_221206A
SegNo: 9081092
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Sulfate
U
1.0
MS
Sample ID: 22120229-05C MS
Units: mg/L
Analysis Date: 12/6/2022 01:03 PM
Client ID: IRY165:FB-1:W113022 Run ID:
GALLERY_221206A
SegNo:9080949
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Sulfate
57.45
1.0 50 16.84 81.2 88-124
0 S
MS
Sample ID: 22112497-02A MS
Units: mg/L
Analysis Date: 12/6/2022 01:32 PM
Client ID: Run ID: GALLERY_221206A SegNo: 9081030 Prep Date: DF: 30
SPK Ref Control RPD Ref RPD
Analyte Result PQL SPK Val Value %REC Limit Value %RPD Limit Qual
Sulfate 2123 30 50 2197 -148 88-124 0 SO
MSD
Sample ID: 22120229-05C MSD
Units: mg/L
Analysis
Date: 12/6/2022 01:04 PM
Client ID: IRY165:FB-1:W113022
Run ID:
GALLERY_221206A
SegNo: 9080950
Prep Date:
DF: 1
SPK Ref
Control
RPD Ref
RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value
%RPD Limit Qual
Sulfate
59.43
1.0 50 16.84 85.2 88-124
57.45
3.4 10 S
MSD
Sample ID: 22112497-02A MSD
Units: mg/L
Analysis
Date: 12/6/2022 01:32 PM
Client ID:
Run ID:
GALLERY_221206A
SegNo: 9081032
Prep Date:
DF: 30
SPK Ref
Control
RPD Ref
RPD
Analyte
Result
PQL SPK Val Value
%REC Limit
Value
%RPD Limit Qual
Sulfate
2199
30 50 2197 3.96 88-124
2123
3.52 10 SO
LCS1
Sample ID: LCS1-R359715
Units: mg/L
Analysis Date: 12/6/2022 05:27 PM
Client ID:
Run ID:
GALLERY_221206A
SegNo: 9081154
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Sulfate
10.73
1.0 10
0 107 90-117
0
LCS2
Sample ID: LCS2-R359715
Units: mg/L
Analysis Date: 12/6/2022 12:58 PM
Client ID:
Run ID:
GALLERY_221206A
SegNo: 9080930
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Sulfate
50.39
1.0 50
0 101 88-124
0
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 52 of 54

Client: Verdantas QC BATCH REPORT
Work Order: 22120229
Project: Phoenix Lumberton
Batch ID: R359715 Instrument ID GALLERY Method: A4500-SO4 E-11
The following samples were analyzed in this batch: 22120229-01C 22120229-02C 22120229-03C
22120229-04C 22120229-05C
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 53 of 54

Client:
Verdantas
QC BATCH REPORT
Work Order:
22120229
Project:
Phoenix Lumberton
Batch ID: R359749
Instrument ID WETCHEM
Method: A2340 C-11
MBLK
Sample ID: MB-R359749-R359749
Units: mg/L CaCO3
Analysis Date: 12/7/2022 11:00 AM
Client ID: ,
Run ID: WETCHEM_221207L
SegNo: 9082224
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
�Analyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
U
5.0
LCS
Sample ID: LCS-R359749-R359749
Units: mg/L CaCO3
Analysis Date: 12/7/2022 11:00 AM
Client ID:
Run ID: WETCHEM_221207L
SegNo: 9082225
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
IAnalyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
100
5.0 100
0 100 95-105
0
DUP
Sample ID: 22120503-011 DUP
Units: mg/L CaCO3
Analysis Date: 12/7/2022 11:00 AM
Client ID:
Run ID: WETCHEM_221207L
SegNo: 9082233
Prep Date: DF: 1
SPK Ref
Control
RPD Ref RPD
Analyte
Result
PQL SPK Val Value
%REC Limit
Value %RPD Limit Qual
Hardness
450
5.0 0
0 0 0-0
470 4.35 10
The following samples were analyzed in this batch:
22120229-02B 22120229-03B
22120229-04B
22120229-05B
Note: See Qualifiers Page for a list of Qualifiers and their explanation.
QC Page: 54 of 54

22120229
hULL&AEDFORD Verdtas?ht,;�O,sa er-dantas Project Phoenix Lumberton
PEOPLE
FOCUSED FUTURE
Dublin, OH O
Indianapolis, IN C3
Mason.OH D
Bedford, OH A
Toledo. OH
-6397 Emerald PkVltl
8443 K CmsSmg
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47799."11 r.
4ldlsm-,,, phh"Wray
3401 Glendale Ave.
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Suite 200
Dublin, OH 43016
P: [phone]
Suite 135
Indianapolis, IN 46240
P:[phone]
Suite 300
Mason, OH 45040
P: [phone]
Bedford, OH 44146
P. [phone]
Suite 300
Toledo, OH 43614 St. Clairsville, OH 43950 Pittsburgh, PA 15205
P:[phone] P'.[phone] P: [phone] -
�ESER%
V
S LE ATBA
PRESERVATIVES
METALS
Client:
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1
AA -AMBIENT AIR
A -Cool only, 44 deg. C
H-EDTA
(!r 1 f1)
y` ` \t— C Y V
,;-ASBESTOS
B-HNO3 pH-2
1-5m11:1 HCL
N -Not filtered
Site: d'(lr �'1
�+r
.iS
D-SEDIMENT
C-H2SO4 pHQ
J-none
F45u- with
G-GROUNDWATER
D-NaOH pH>12
K-Stored in dark
micron
0.45 mlLrtln
Project #: 1 q/a
o %
V
Phase:
WINDOOR AIR
L-NH4CI
E-ZnAcetate + NaOH, pH>9
FSu- filtered with 5
4�
L-LEACHATE
P-PRODUCT
F-Na2S2 03 (0.008 %)
G-HCL <2
M-Methanol
SSodium
micron
Samplers:
s-SOIL
pH
L-1
SG -SOIL GAS
SS -SUB sLAB
Purchase Order #
VAPOR
PROJECT NO.:
SAMPLE LOCATION
SAMPLE MATRIX & ID
NO. OF CONT.
-X,,�LN U5
�-
: 6, it 3c2a A
D BY: l "] I DATE:
RELIN)UISHHEAD BY:-
DATE:
TIME:
RELINQUISHED BY:
DATE:
TIME:
COOLER TEMPERATURE I
L
AS RECEIVED
.3 ^C
H �' z PU3z
SAM L€ TYPE
iiscrete, composite)
COLLECTION DATE/TNE
METALS
yj' S
wjo �a /16 �5
MQ? /1
/V
Al
wv2-1
,iv
A
/
D BY: DATE:
TIME:
D BY: /1 DATE:
BY {DATE:
DISTRIBUTION: WHITE -LAB USE (MUST BE RETURNED WITH REPORT)
YELLOW -LAB USE
PINK -RETAINED BY VERDANTAS
PAGE _ OF
NO, _0390
TO:��X44i iN
1 . 4: :.
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X
x
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Deliver To:
Method of Delivery:
Airbill Number:
Regulatory Program:
Required Limits:
NOTES:
TURN AROUND TIME: W DAYS

ALS Group, USA
Holland, Michigan
Client Name: HULL&ASSOC-BEDFORD
Work Order: 22120229
Checklist completed by --Z�—S'
eSignature
Matrices: Water
Carrier name: FedEx
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Sample(s) received on ice?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes: off check <2.
Client Contacted:
Contacted By:
Comments:
CorrectiveAction:
Sample Receipt Checklist
Date Contacted:
Regarding:
Date/Time Received
Received by:
01-Dec-22 09:00
IDS
02-Dec-22
Reviewed by:%�
Date
eSignature
Yes
❑d
No ❑
Not Present ❑
Yes
❑d
No ❑
Not Present ❑
Yes
❑
No ❑
Not Present ❑d
Yes
❑d
No ❑
Yes
No ❑
Yes
No ❑
Yes
❑10
No ❑
Yes
❑d
No ❑
Yes
❑d
No ❑
Yes
❑d
No ❑
Yes
❑d
No ❑
Yes
❑d
No ❑
4.3/5.3. 4.7/5.7 c
IR3
12/2/2022 3:04:52 PM
Yes ❑d No ❑ No VOA vials submitted ❑
Yes ❑10 No ❑ N/A ❑
Yes ❑ No ❑d N/A ❑
Person Contacted:
05-Dec-22
Date
SRC Page 1 of 1

October 2023
Document Number 15104.0014
APPENDIX C
PROTOCOLS FOR PFAS SAMPLING
verdantas
4 Hemisphere Way, Bedford, OH 44146 1 verdantas.com

r< verdantas
PFAS SAMPLING GUIDELINES
Background
Per -and polyfluoroalkyl substances (PFAS) are a large group of manufactured compounds used in a
variety of industries, such as aerospace, automotive, textiles, electronics, some food packaging and
firefighting materials. Due to the ubiquitous nature of the wide array PFAS chemicals and the low parts
per trillion screening levels, all aspects of a sampling and analytical protocols must be considered for
PFAS specific sensitivity to avoid cross contamination. The following aspects are sampling
considerations beyond typical groundwater sampling standard operating procedure (FDEP-SOP-
001 /01 FS 2200: Groundwater Sampling) necessary for project quality assurance and quality control.
HAS Specific Sampling Guidelines
• Remove any Teflon containing materials or low -density polyethylene from wells at
least one week prior to sampling.
• Communication with the laboratory before, during, and after sampling to ensure
project needs and laboratory requirements are met. For PFAS analysis, Trip Blanks
are not necessary.
• Water used for field sample blanks (examples include field, trip, and
decontamination blanks) should be PFAS-free water, supplied by the laboratory
performing the analysis. Documentation of PFAS-free water used by the
laboratory is required to be maintained for data validation purposes.
• Alconox will be used as decontamination materials followed by a laboratory
grade alcohol rinse. Use laboratory -verified PFAS-free water for the final rinse
during decontamination of sampling equipment.
• Samples to be analyzed for PFAS must be collected in a high -density
polyethylene (HDPE) containers with an unlined plastic screw cap.
• Only use nitrite gloves for sampling.
• Use new HDPE tubing for each sample.
• When using submersible pump sampling equipment, familiarize yourself with
the sampling pump/accessory to confirm that device components do not
contain Teflon® or PTFE.
• Equipment blanks should be collected from each equipment setup that comes in
contact with the sample.
• Field staff do not use cosmetics, moisturizers, hand cream, or other related
products the morning of sampling. Only use approved sunscreens or insect
repellants.
• Use plain paper, metal clipboard, and ball point pens for field documentation.
Do not use Rite in the Rain field books or plastic clipboards.
• Keep PFAS samples in separate cooler, away from sampling containers that may
contain PFAS.
• Coolers filled with regular ice only, do not keep the ice in the bags, loose ice in PFAS
cooler only.
• Do not use chemical (blue) ice packs.
605 East Robinson Street, Suite 308, Orlando, FI 32765 1 verdantas.com 1 of 2
P:\1 C136 Cardno\PFAS\PFAS Sampling Guidelines.docx

PFAS Sampling Guidelines
HSW Project Number 4AA6001 B1
Field QC Samples
verdantas
Collection and analysis of field quality control (QC) samples are important for PFAS investigations because
of very low detection limits and regulatory criteria (ppt), to ensure accuracy and representativeness of the
results to the sampled media, and to assess potential cross -contamination due to the ubiquitous nature of
PFAS. Such field QC samples typically include
• field blanks (5% for total field blanks and equipment blanks per matrix)
• equipment blanks (one sample for each equipment setup)
• sample duplicates (if needed)
Materials to Be Avoided
Many materials used in the course of environmental investigation can potentially contain PFAS. With
limited information known on certain materials used by field staff or sampling equipment may affect
sample results, the following materials should be avoided in order to protect the integrity of samples.
• Teflon®, polytetrafluoroethylene (PTFE) lined lid
• LDPE or polypropylene containing materials (e.g., bags or containers used to transport
samples)
• Decontamination soaps containing fluoro-surfactants such as Decon 90
• waterproof coatings containing PFAS
o sharpies or permanent markers
o waterproof field books
o plastic clipboard
o post -it, sticky notes, glues
o aluminum foil
o waterproof Clothing or shoes including Gore-TexTM and Tyvek®. Wet
weather gear made of PVC and polyurethane only.
o chemical (blue) ice packs
o food containers
• anything with fluoro in the name
• low density polyethylene (LDPE)
• polyvinylidene fluoride (PVDF)
• If unavoidable, materials in question can be sampled and analyzed for PFAS
content, such as Luminox detergent.
Relevant References
EPA. PFAS Methods and Guidance for Sampling and Analyzing Water and Other
Environmental Media- Technical BRIEF. September 28, 2018, EPA/600/F-17/022d.
USDoD. Bottle Selection and other Sampling Considerations When Sampling for Per -and
Poly-6923 Fluoroalkyl Substances (PFAS). July 2017.
NHDES. Sampling for Per- and Polyfluoroalkyl Substances/Perfluorinated Chemicals
(PFASs/PFCs) at Contaminated Sites. November 22, 2016.
Alpha Analytical Inc. EPA 537 (PFAS) Field Sampling Guidelines.
https://alphalab.com/images/stories/PFAA%2OSampling%201nsfructions%2OSheef%205 24 2
017.pdf.
MIDEQ. Wastewater PFAS Sampling Guidance. October 11, 2018.
605 East Robinson Street, Suite 308, Orlando, FI 32765 1 verdantas.com 2 of 2

This is a suggested Checklist that can help to
prevent/minimize PFAS cross contamination from field Date
personnel, materials and equipment. Please review and
check all that apply prior to the start of each sampling Weather
event. Any noncompliance issues should be addressed
prior to commencement of that day's work. Corrective Site Name
action shall include removal of noncompliance items from
the site. _
FIELD CLOTHING AND PPE:
❑ No clothing or boots containing Gore-TeXTM
❑ All safety boots made from polyurethane and PVC
❑ No materials containing TyvekTM
❑ Field crew has not used fabric softener on clothing
❑ Field crew has not used cosmetics, moisturizers,
hand cream, or other related products this morning
❑ Field crew has not applied unauthorized sunscreen
or insect repellent (see MDEQ and NHDES
reference for acceptable products)
WET WEATHER (as applicable)
❑ Wet weather gear made of polyurethane or PVC
EQUIPMENT DECONTAMINATION
❑ "PFAS-free" waterfor decontamination of sample
equipment. No other water source can be used.
❑ Alconox and Liquinox to be used as
decontamination materials
SITE DEPENDENT
❑ Equipment / Consumables manufacturer
information known
FIELD EQUIPMENT
❑ No Teflon TM
or LDPE containing materials on -site
❑ All sample materials made from stainless steel, HDPE,
acetate, silicon, nitrile, PVC, or polypropylene
Flow Cells &
Barbs O-Rings
.� Bailers (Check Ball) Water
d Tubing
`** Buckets or Container
D No waterproof field books on -site
❑ No plastic clipboards, binders, or spiral hard cover
notebooks on -site
❑ Coolers filled with regular ice only. No chemical
(blue) ice packs in possession
❑ The packaging units for any items taken to the site
❑ Bags for sample collection (Made from Polypropylene)
FOOD CONSIDERATIONS
❑ No food or drink on -site with exception of bottled
water and/or hydration drinks (i.e. Gatorade and
Powerade) that is available for consumption only in
the staging area
Describe the noncompliance issues (include personnel not in compliance) and action/outcome of noncompliance
Name
Signature:
4 Hemisphere Way, Bedford, OH, 44146 1 verdantas.com
Time: