WS-10203_47461_CAS_CLO_20200402

WithersRavenel
Our People. Your Success.

115 MacKenan Drive | Cary, NC 27511 
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832 
Cary | Greensboro | Pittsboro | Raleigh | Wilmington 
April 2, 2020 

Guilford County Health Department 
400 W Friendly Ave, Suite 300 
Greensboro, North Carolina 27401 

Attn: Mr. Gene Mao 

RE: UST CLOSURE REPORT 
Signature Flight Support GSO 
1060 PTI Drive 
Greensboro, Guilford County, North Carolina 
Groundwater Incident Number:  Not Applicable 
WR Project Number: 02150228.03 

Mr. Mao: 

On behalf of Signature Flight Support Corporation (Signature), WithersRavenel (WR) has completed 
the closure‐in‐place of one 550‐gallon used oil underground storage tank (UST), one 2,000‐gallon 
gasoline UST, and one ~25,000‐gallon ethylene glycol UST at the above referenced site. The onsite work 
took place on February 25‐28, 2020. The below report documents the UST closure activities. 

Should you have any questions regarding the attached, please do not hesitate to contact G. Matthew 
James at (919) 469‐3340. 

Sincerely, 
WithersRavenel

G. Matthew James, P.G.  
Project Manager  

i 
Table of Contents
1. Site History and Characterization ........................................................................................... 1 
2. UST Closure Activities ............................................................................................................... 3 
3. Site Investigation ........................................................................................................................ 4 
4. Conclusions and Recommendations....................................................................................... 8 

FIGURES  
Figure 1 General Location Map 
Figure 2 Site Map 
Figure 3 Vicinity Map 
Figure 4 Soil Results Map 
Figure 5 Groundwater Results Map 
TABLES  
B‐1 Site History: UST System(s) 
B‐3 Summary of Soil Analytical Results 
B‐3A Summary of Soil Analytical Results – TPH  
B‐4 Summary of Groundwater Analytical Results 
B‐7 Monitoring & Remediation Well Construction Information 
APPENDICES  
Appendix A Sketch of the Tank Farm Area 
Appendix B UST‐3 Form  
Appendix C Liquid Waste and Drum Disposal Manifests  
Appendix D UST‐2A & UST‐2B Forms 
Appendix E Well Construction Records  
Appendix F Laboratory Analytical Reports 
Appendix G Photographic Record 

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1. SITE HISTORY AND CHARACTERIZATION
1.1. UST OWNER AND OPERATOR INFORMATION
According to Guilford County GIS information, the three USTs are located on an approximate 
±140.63‐acre parcel identified by PIN 7825‐26‐0163.  A general location map is provided as 
Figure 1 and a site map is provided as Figure 2.  The USTs are located within the tank farm 
area, approximately 100 feet southwest of the Signature Flight Support GSO building.  

The table below summarizes the UST information of the closed in‐place USTs. See the attached 
Table B‐1 for additional information regarding the UST systems. 

UST 
ID NO PRODUCT CAPACITY 
(GALLONS) 
DATE 
INSTALLED 
DATE 
CLOSED 
RELEASE 
DISCOVERED 
7 Gasoline ±2,000 Unknown 02/26/2020 Yes 
9 Waste Oil ±550 Unknown 02/26/2020 Yes 
Unk Ethylene Glycol ±25,000 Unknown 02/28/2020 No 

1.2. HISTORICAL & SURROUNDING UST INFORMATION
WR is aware of seven additional USTs in the tank farm area on the subject site, as follows: 

UST ID NO PRODUCT CAPACITY (GALLONS) 
1 Jet A Fuel ±30,000 
2 Jet A Fuel ±30,000 
3 Jet A Fuel ±20,000 
4 Jet A Fuel ±20,000 
5 Gasoline ‐ AvGas ±10,000 
6 Gasoline ‐ MoGas ±10,000 
8 Waste Oil/Fuel from Oil/Water Separator ±2,000 

See Appendix A for a sketch of the tank farm area displaying the layout of the onsite USTs. No 
information relating to the possible presence of USTs on the remainder of the subject property 
or surrounding properties was available to WR.  

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1.3. NON-UST INFORMATION
A spill occurred in or around 1998 during the filling of a mobile refueler with jet fuel.  Mobile 
refuelers are considered ASTs and are included in the facility’s SPCC Plan and such, we 
consider this a Non‐UST Event.  During the filling activity, the operator rigged the dead‐man 
device and either left the area and / or fell asleep.  Several thousand gallons of jet fuel were 
spilled and the spill advanced past the tank farm area and into a creek to the northwest of the 
tank farm.  The creek flows into a detention pond about a ½ mile away from the site.  The 
detention pond was on the airport property and no fuel left airport property during the 
event.  The spill was cleaned up by a subcontracted spill response company and it is believed 
that the state provided a no further action letter, however, no documentation was provided to 
WR.  

1.4. DESCRIPTION OF RELEASE / OFFSITE UST RELEASES
During closure activities of the used oil and gasoline USTs, soil and groundwater samples 
indicated a release. The ethylene glycol UST soil and groundwater samples indicated a clean 
closure.  

WR is unaware of any nearby UST incidents. 

1.5. SITE CHARACTERISTICS AND SURROUNDING PROPERTY
The subject property is currently owned by Piedmont Triad Airport Authority.  Signature Flight 
Support leases the area of the tank farm and multiple buildings used for aircraft maintenance 
and storage. The UST area is located between PTI Drive and the Signature Flight Support GSO 
building. The USTs are within the Signature Flight Support tank farm, with the exception of the 
ethylene glycol UST which is located southwest of the tank farm across a paved access road. 
The tank farm is an approximately ±9,000‐sqft gravel area. Based on tank farm area being 
constantly saturated, it is believed the tank farm is lined with an impermeable material.  
Perched water was observed in the tank pit monitoring wells within the gravel area. The 
drainage for the tank farm area is directed to an oil/water separator (OWS) that also collects 
storm runoff from the surrounding area. The tank farm is surrounded by concrete in most 
directions, with the exception of a grassy ditch running along the northwestern portion. The 
northwestern portion of the tank farm is built‐up to prevent surficial flow in this direction. 
Surficial flow not captured by the OWS system is channeled through subsurface stormwater 
devices. 

The contiguous properties in all directions are parcels related to Piedmont Triad International 
Airport. One stream is located approximately 500 feet northwest of the UST area.  
Additionally, the site is located within the City of Greensboro where properties are connected 
to municipal water and sewer. A vicinity map is provided as Figure 3. 
1.6. SUMMARIZE INITIAL ABATEMENT ACTIONS, ASSESSMENT
ACTIVITIES, AND CORRECTIVE ACTIONS PERFORMED TO DATE
AND LIST ALL REPORTS PREVIOUSLY SUBMITTED.
The gasoline UST and used oil UST were permanently closed by filling with foam on February 
26, 2020, and the ethylene glycol was closed by filling with foam on February 28, 2020. The 
UST closure activities are described further in Sections 2 and 3 of this report.  

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2. UST CLOSURE ACTIVITIES
2.1. DESCRIBE PREPARATIONS FOR CLOSURE INCLUDING
STEPS TAKEN TO NOTIFY AUTHORITIES, PERMITS OBTAINED, AND
STEPS TAKEN TO CLEAN AND PURGE THE TANKS.
 WR submitted the required UST‐3 (Notice of Intent: UST Permanent Closure or Change‐in‐
Service) form (Appendix B) to the Guilford County Health Department and NCDEQ, Central 
Regional Office on January 8, 2020. 
 EVO & WR obtained the requisite permission to close the USTs in‐place from the City of 
Greensboro. 
 Residual fluids contained within each UST were removed by EVO using vacuum equipped 
tanker trucks prior to filling each UST with foam. A total of 26,750‐gallons of non‐regulated 
petroleum/ethylene glycol contact water and sludge were pumped from the USTs prior to their 
closures. These residuals were disposed of at EVO’s permitted facility located in Winston‐
Salem, NC (see Appendix C for a copy of the disposal manifest). 
 Purging of vapors and reduction of oxygen content within each tank was accomplished 
through the removal of residual fluids and vapors from the USTs using the vacuum equipped 
tanker trucks.   

2.2. DESCRIBE THE CLOSURE PROCEDURE, REFERENCING SITE
AND SAMPLING LOCATION MAPS. CLEARLY STATE HOW THE
INITIAL ALARM OR CAUSE FOR SUSPICION, THE TYPE OF BACKFILL,
THE DEPTH TO GROUNDWATER, AND OTHER FACTORS
APPROPRIATE FOR IDENTIFYING THE PRESENCE AND SOURCE OF
A RELEASE. IF THE PRESENCE OF GROUNDWATER OR BEDROCK
REQUIRES THE INSTALLATION AND SAMPLING OF MONITORING
WELL(S), DESCRIBE THE PROCESS.

Once removal of the residual fluids was completed, each UST was filled with expanding foam. 
All associated piping for each UST was filled by pressure grouting, and the dispenser associated 
with the gasoline UST was removed and the sump was filled grout.  

WR, along with subcontractor Quantex, Inc., installed soil borings and permanent monitoring 
wells adjacent to each UST on February 27, 2020. Due to the perched water within the tank 
farm basin, for safety precautions, no borings or monitoring wells were installed within the 
gravel area of the tank farm.  Soil borings and monitoring well placements were discussed with 
the Guilford County Health Department prior to installation.  

One boring was completed and converted to a monitoring well (SB‐1/MW‐1) just outside of 
the gravel area to the northeast of the used oil UST and one boring was completed and 
converted to a monitoring well (SB‐2/MW‐2) just outside of the gravel area to the southwest 
of the gasoline UST. Four borings (SB‐3 through SB‐6) were completed around the ethylene 
glycol UST, with the northwestern boring being converted to a monitoring well (MW‐3). One 
boring (Dispenser) was also completed adjacent to the former gasoline dispenser island. See 

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Figure 4 for the location and layout of the soil borings and Figure 5 for the location and layout 
of the permanent monitoring wells. Waste boring cuttings were containerized in onsite drums 
and disposed of by EVO at their facility in Winston‐Salem, NC. See Appendix C for a copy of 
the drum disposal manifests. A strong petroleum odor was noted in the borings adjacent to the 
used oil UST and former dispenser. The depth of ground water measured approximately 8 to 
9 feet below land surface (BLS) adjacent to the tank farm and approximately 2 feet BLS 
adjacent to the ethylene glycol UST. 

Completed UST‐2A and UST‐2B forms are included as Appendix D. 

2.3. NOTE THE AMOUNT OF RESIDUAL MATERIAL PUMPED
FROM THE TANK AND DESCRIBES THE STORAGE, SAMPLING AND
DISPOSAL OF THE RESIDUAL MATERIAL AND THE DISPOSAL OF
THE TANK, PUMPS AND PIPING (REFER TO APPENDICES WITH
DISPOSAL MANIFESTS AND CERTIFICATE OF TANK DISPOSAL).
Information described in Section 2.1. 
2.4. IF A RELEASE IS DETERMINED, DOCUMENT INITIAL
RESPONSE ACTIONS (SUBMITTAL OF 24-HOUR RELEASE & REPORT
FORM; REPAIR, REPLACEMENT OR UPGRADING OF SYSTEM TO
PREVENT FURTHER RELEASE; MITIGATION OF HAZARDS) AND
INITIAL ABATEMENT ACTIONS (FREE PRODUCT REMOVAL;
SUBMITTAL OF 20-DAY REPORT):
Response actions described in Section 2.2. 

Analytical data from the onsite soil borings and monitoring wells adjacent to the used oil and 
gasoline USTs confirmed the presence of petroleum compounds above applicable regulatory 
standards. Soil analytical results are tabulated in Table B‐3 and Table B‐3A. Groundwater 
analytical results are tabulated in Table B‐4. Closure sample locations are illustrated on Figure 
4 and Figure 5. 

3. SITE INVESTIGATION
3.1. FIELD SCREENING TECHNIQUES

Clean nitrile gloves were utilized during the collection of soil samples. Continuous soil sampling 
was performed within each boring to allow for soil characterization including logging of 
materials recovered and screening of soils with a field calibrated Foxboro Thermo Scientific 
toxic vapor analyzer (TVA) analysis, which consists of a photo ionization detector (PID) and 
flame ionization detector (FID). Collected soil samples were placed in clean zip‐lock baggies 
and screened using the onsite TVA.  

3.2. SOIL SAMPLING PROCEDURES

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Soil samples were collected from each boring, and sample depths were determined as an 
attempt to be above the site’s surficial aquifer. The samples from SB‐1 and SB‐2 were collected 
from 5 to 7.5 feet BLS, SB‐3 was collected from 2.5 to 5 feet BLS, SB‐4 through SB‐6 were 
collected from 5 to 7.5 feet BLS, and Dispenser was collected from 2 feet BLS. Soil samples 
collected for laboratory analysis were immediately placed in laboratory supplied bottleware, 
placed in a cooler containing ice, and submitted under proper chain of custody procedures for 
the following analysis: 

 SB‐1 to REDLab for analysis of Total Petroleum Hydrocarbons – Gasoline/Diesel 
Range Organics (TPH‐GRO/DRO) by UVF methodology and to Contest Analytical 
Laboratory (Contest) for analysis of Volatile Organic Compounds (VOCs) by EPA 
Method 8260D, Semi‐VOCs (SVOCs) by EPA Method 8270E, Extractable/Volatile 
Petroleum Hydrocarbons (EPH/VPH) by MADEP methodology, and Chromium and 
Lead by EPA Method 6020B; 
 SB‐2 to REDLab for analysis of TPH‐GRO/DRO by UVF methodology and to 
Contest for analysis of VOCs by EPA Method 8260D, and VPH by MADEP 
methodology; and 
 SB‐3 through SB‐6 to Contest for analysis of Ethylene Glycol by EPA Method 
8015C. 
  Dispenser to REDLab for analysis of TPH‐GRO/DRO by UVF methodology. 

Soil sample locations were recorded with a sub‐meter GPS device. 

3.3. GROUNDWATER SAMPLING PROCEDURES

WR, along with drilling subcontractor Quantex, Inc., installed permanent Type II monitoring 
wells, MW‐1, MW‐2, and MW‐3, to depths of 22, 24, and 20 feet BLS, respectively, using 
4.25‐inch diameter (ID) hollow stem augers. MW‐1 was constructed with 10 feet of 2‐inch 
diameter 0.01‐slotted PVC well screen and 12 feet of 2‐inch diameter PVC casing, MW‐2 was 
constructed with 15 feet of 2‐inch diameter 0.01‐slotted PVC well screen and 9 feet of 2‐inch 
diameter PVC casing, and MW‐3 was constructed with 15 feet of 2‐inch diameter 0.01‐slotted 
PVC well screen and 5 feet of 2‐inch diameter PVC casing. Clean‐filter sand was placed into 
the annular space surrounding the well screen to approximately 2 ft above the screened 
section of each well. An approximate 1 to 2 ft bentonite seal was placed over the sand pack 
and hydrated for each well. Neat cement grout was then extended to land surface for each 
well. The wellheads were secured with 2‐inch locked expansion plugs and bolt‐down, flush‐
mount manholes stabilized in place by concrete pads. The monitoring wells were developed to 
remove fine sediments following installation. The tops‐of‐casing were surveyed to determine 
relative elevations, and the monitoring well locations were recorded with a sub‐meter GPS 
device. The wells were installed at the locations depicted on Figure 5. See the well construction 
records in Appendix E and Table B‐7 for more information regarding the construction of the 
onsite monitoring wells. 

Following installation and development, WR personnel gauged, purged, and sampled the 
monitoring wells on February 27, 2020. Prior to purging and sampling, the depth to 
groundwater within each well was gauged utilizing an electronic water level indicator. See 
Table B‐7 for the depths to water and relative elevations in the onsite monitoring wells. No 
determination of groundwater flow was made based on well gauging.   

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Each monitoring well was sufficiently purged using a peristaltic pump and dedicated 
polyethylene tubing. A groundwater sample was collected from each well in pre‐preserved 
laboratory supplied glassware and placed in a cooler containing ice then submitted under 
proper chain of custody procedures to Contest for analysis as follows: 

 MW‐1 for analysis of VOCs by EPA Method 6200B, SVOCs by EPA Method 625.1, 
and EPH/VPH by MADEP methodology; 
 MW‐2 for analysis of VOCs by EPA Method 6200B, 1,2‐Dibromoethane (EDB) by 
EPA Method 504.1, and Lead by EPA Method 6020B; and 
 MW‐3 for analysis of Ethylene Glycol by EPA Method 8015C. 

3.4. QUALITY CONTROL MEASURES

Quality control measures were employed during this project and included use of clean 
sampling tools, laboratory prepared sample bottle kits, calibrated field instruments, donning of 
clean sample gloves during each sample collection and preparation effort, and a use of third‐
party laboratories for analysis of samples obtained in association with completion of this 
project. 

3.5 INVESTIGATIVE RESULTS – CLOSURE ASSESSMENT

 3.5.1 Results of Used Oil and Gasoline UST Soil Sampling 

TPH‐GRO/DRO 
TPH‐GRO was reported at a concentration above the NCDEQ Action Level for the Dispenser 
sample.  
TPH‐DRO was reported at a concentration above the NCDEQ Action Level in SB‐1 and in the 
Dispenser sample.  
TPH‐GRO and TPH‐DRO were not reported at concentrations above the laboratory MDLs in 
SB‐2. 
VOCs 
Several targeted VOCs were reported in SB‐1 and SB‐2 at levels above the laboratory method 
detection limit (MDL). However, targeted VOC detections did not exceed any applicable 
NCDEQ UST Section Maximum Soil Contamination Concentrations (MSCCs). 
SVOCs 
No SVOC compounds were reported at concentrations above applicable Soil to Groundwater 
MSCCs. 
EPH/VPH 
C9‐C22 Aromatics was reported in SB‐1 at a concentration exceeding the Soil to Groundwater 
MSCC, but below the Residential and Industrial/Commercial MSCCs. No other targeted EPH 
/ VPH compounds in SB‐1 or SB‐2 were reported at concentrations above the Soil to 
Groundwater MSCCs. 
Chromium and Lead 

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Chromium was reported in SB‐1 at a concentration exceeding the Soil to Groundwater MSCC, 
but below the Residential and Industrial/Commercial MSCCs.  
Lead was not reported at a concentration that exceeded the Soil to Groundwater MSCC. 

 3.5.2 Results of Used Oil and Gasoline UST Groundwater Sampling 

VOCs 
Several targeted VOCs were reported in MW‐1 and MW‐2 at levels exceeding the NCAC 2L 
Standards but below the gross contaminant levels (GCLs). 
SVOCs 
Several targeted SVOCs were reported in MW‐1 at levels above the laboratory method 
detection limit (MDL). Two detected targeted SVOCs, diethyl phthalate and naphthalene, 
exceeded their respective NCAC 2L Standards. Detected targeted SVOCs did not exceed 
applicable NCDEQ gross contaminant levels (GCLs). 
EPH/VPH 
C5‐C8 Aliphatics and C9‐C18 Aliphatics were reported in MW‐1 at levels above the laboratory 
MDL, but below the NCAC 2L Standards. C9‐C22 Aromatics was reported in MW‐1 at a 
concentration exceeding the NCAC 2L Standard, but below the GCL. 
EDB 
EDB was not reported in MW‐2 at a concentration exceeding the laboratory MDL. 
Lead 
Lead was reported in MW‐2 at a concentration exceeding the NCAC 2L Standard, but below 
the GCL. 

 3.5.3 Results of Ethylene Glycol UST Soil and Groundwater Sampling 

Ethylene Glycol 
Ethylene glycol was not reported in soil or groundwater above the laboratory MDL in any 
sample collected around the ethylene glycol UST. 

A copy of each laboratory analytical report is included in Appendix F.  Sample locations are 
illustrated on Figure 4 and Figure 5, and results are provided in tabular form in Table B‐3, Table 
B‐3A, and Table B‐4. 

Signature Flight Support WR Project No. 02150228.03 
UST Closure Report April 2020 
Page 8 

4. CONCLUSIONS AND RECOMMENDATIONS

WR completed the closure‐in‐place of one 550‐gallon used oil UST, one 2,000‐gallon gasoline UST, 
and one ~25,000‐gallon ethylene glycol UST at the above referenced site. The onsite work took place 
on February 25‐28, 2020.  Conclusions regarding these UST closures and the results of 
laboratory testing of samples collected in association with these closures include the following: 

 A total of 26,750‐gallons of residual fluid was removed from the USTs prior to 
their closures. These liquids were transported and disposed of by EVO at their 
facility in Winston‐Salem, NC. 
 The USTs were closed in‐place through the injection of expanding foam into the 
tanks. 
 Remaining subsurface piping was filled by pressure grouting. 
 Soil borings and permanent monitoring wells were installed adjacent to each UST 
on February 27, 2020. 
o Based on soil and groundwater analytical results, the used oil and gasoline 
USTs are associated with a release of petroleum material. 
o Based on soil and groundwater analytical results, the ethylene glycol UST 
is not associated with a release of its contents. 

If you have any questions concerning this report, please call us at your earliest convenience. 

Sincerely, 
WithersRavenel

G. Matthew James, P.G.  
Project Manager  

FIGURES
AP
MJ
DRAWN BY:
03/17/2020 02150228.03
1
SUBJECT SITE
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
SIGNATURE FLIGHT SUPPORT
1060 PTI DRIVEGREENSBORO, GUILFORD COUNTY, NC
GENERAL LOCATION MAP
1"=2000 '
GRAPHIC SCALE
1 inch = 2000 ft.
0 20001000 4000
WithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832www.withersravenel.com
UST AREA
PRODUCT LINEDISPENSERGRAVEL TANK FARM AREAAIRPLANE HANGERXX XX XX
XX
XXXX XXXXXXXX XX XX
XX
XX
O
O
O
2,000-GALLON GASOLINE UST550-GALLON USED OIL UST±25,000-GALLON ETHYLENE GLYCOL USTSYSTEM OPERATIONS SHEDFUEL LOADING AREASCHAIN-LINK FENCE WITH GATEPTI DRIVE
APMJDRAWN BY:03/17/202002150228.032SCALE:FIGURE NO.:PROJECT NO.:DATE:APPROVED BY:SIGNATURE FLIGHT SUPPORT1060 PTI DRIVEGREENSBORO, GUILFORD COUNTY, NCSITE MAPWithersRavenelEngineers | Planners | Surveyors115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com1"=20 'GRAPHIC SCALE1 inch = 20 ft.0201040
FMFMFMFMF
MFMF
M FMFM FM FM
F
M
FM
F
MFM
FMFMFM
F
M
AREA OF 3 USTs
SUBJECT PROPERTY PARCEL
PTI
DR
IVE
PT
I PTI DRIVED
R
I
V
E
SI
G
N
A
T
U
R
E

F
L
I
G
H
T
SU
P
P
O
R
T

B
U
I
L
D
I
N
G
PIEDMONT TRIADINTERNATIONAL AIRPORT
500 FEET 1000 FEET APMJDRAWN BY:03/18/202002150228.033SCALE:FIGURE NO.:PROJECT NO.:DATE:APPROVED BY:SIGNATURE FLIGHT SUPPORT1060 PTI DRIVEGREENSBORO, GUILFORD COUNTY, NCVICINITY MAPWithersRavenelEngineers | Planners | Surveyors115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340license #: C-0832 | www.withersravenel.com1"=225 'GRAPHIC SCALE
1 inch = 225 ft.
0 225113 450
LEGEND
STREAM
CITY OF GREENSBORO WATER MAIN
NOTES:
1.) ALL LOCATIONS ARE APPROXIMATE AND NOT EXACT.
FM FM
FORMER DISPENSER ISLAND
AIRPLANE HANGERXX XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXOOOOOOO2,000-GALLON GASOLINE UST
550-GALLON USED OIL UST
±25,000-GALLON ETHYLENE GLYCOL UST
PR
O
D
U
C
T

L
I
N
E
SB-4
SB-5SB-6
SB-3
SB-2
DISPENSER
SB-1
SB-1 (5'-7.5' BLS) 02/27/2020
RESULTS mg/kgC9-C22 AROMATICS 46CHROMIUM21TPH-DRO 119.8
DISPENSER (2' BLS) 02/27/2020
RESULTS mg/kgTPH-GRO 1891TPH-DRO 5364 APMJDRAWN BY:03/18/202002150228.034SCALE:FIGURE NO.:PROJECT NO.:DATE:APPROVED BY:SIGNATURE FLIGHT SUPPORT1060 PTI DRIVEGREENSBORO, GUILFORD COUNTY, NCSOIL RESULTS MAP -EXCEEDANCES ONLYWithersRavenelEngineers | Planners | Surveyors115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340license #: C-0832 | www.withersravenel.com1"=10 'GRAPHIC SCALE
1 inch = 10 ft.
0 105 20
LEGEND
SOIL BORING LOCATION
RESULT EXCEEDS RESPECTIVE NCDEQ UST SECTION SOIL TO GROUNDWATER MSCC
RESULT EXCEEDS RESPECTIVE NCDEQ TPH ACTION LEVEL
NOTES:
1.) DETECTIONS OF TARGETED COMPOUNDS NOT SHOWN ON THE FIGURE DID NOT EXCEED APPLICABLE
REGULATORY STANDARDS, SEE THE LABORATORY REPORT FOR A FULL LIST OF TARGETED COMPOUNDS
2.) ALL VOCs, SVOCs, LEAD, AND ETHYLENE GLYCOL CONCENTRATIONS WERE BELOW APPLICABLE
REGULATORY STANDARDS
3.) NO REPORTED CONCENTRATIONS OF TARGETED COMPOUNDS EXCEEDED RESPECTIVE NCDEQ UST
SECTION RESIDENTIAL & INDUTRIAL/COMMERCIAL MSCCs
MW-3
MW-2
MW-1
FORMER DISPENSER ISLAND
2,000-GALLON GASOLINE UST
550-GALLON USED OIL UST
±25,000-GALLON ETHYLENE GLYCOL UST
MW-1 02/27/2020
RESULTS ug/LBENZENE70METHYLENE CHLORIDE 6.8NAPHTHALENE (VOC)330DIETHYL PHTHALATE 10.4NAPHTHALENE (SVOC)222C9-C22 AROMATICS 330
PR
O
D
U
C
T

L
I
N
E
AIRPLANE HANGER
MW-2 02/27/2020
RESULTS ug/LBENZENE330MTBE210NAPHTHALENE (VOC)28LEAD37
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXOOOOOOOAPMJDRAWN BY:03/18/202002150228.035SCALE:FIGURE NO.:PROJECT NO.:DATE:APPROVED BY:SIGNATURE FLIGHT SUPPORT1060 PTI DRIVEGREENSBORO, GUILFORD COUNTY, NCGROUNDWATER RESULTS MAP- EXCEEDANCES ONLYWithersRavenelEngineers | Planners | Surveyors115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340license #: C-0832 | www.withersravenel.com1"=10 'GRAPHIC SCALE
1 inch = 10 ft.
0 105 20
LEGEND
TYPE II MONITORING WELL LOCATION
RESULT EXCEEDS RESPECTIVE NCAC 2L GROUNDWATER QUALITY STANDARD
RESULT* EXCEEDS RESPECTIVE NCDEQ GROSS CONTAMINANT LEVEL (GCL)
NOTES:
1.) DETECTIONS OF TARGETED COMPOUNDS NOT SHOWN ON THE FIGURE DID NOT EXCEED APPLICABLE
REGULATORY STANDARDS, SEE THE LABORATORY REPORT FOR A FULL LIST OF TARGETED COMPOUNDS
2.) 1,2-DIBROMOETHANE (EDB) AND ETHYLENE GLYCOL CONCENTRATIONS WERE BELOW LABORATORY
METHOD DETECTION LIMITS
3.) NO REPORTED CONCENTRATIONS OF TARGETED COMPOUNDS EXCEEDED RESPECTIVE NCDEQ GCLs
IN ANY ONSITE MONITORING WELL

TABLES

UST IDNumberCurrent/LastContents*PreviousContents*Capacity(in gallons)ConstructionDetails**TankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUST***Was release associated with UST System? (Y/N)1Kerosene, Kero MixAviation Fuel30,000Single Wall Steel10'6" x 46'6" Steel 4/9/1980 Active N2Kerosene, Kero MixAviation Fuel30,000Single Wall Steel10'6" x 46'6" Steel 4/9/1980 Active N3Kerosene, Kero MixAviation Fuel20,000Single Wall Steel10'6" x 30'11" Steel 4/9/1980 Active N4Kerosene, Kero MixAviation Fuel20,000Single Wall Steel10'6" x 30'11" Steel 4/11/1972 Active N5Gasoline, Gas MixAviation Fuel10,000Single Wall Steel10'6" x 15'6" Steel 4/11/1972 Active N6Gasoline, Gas MixAviation Fuel10,000Single Wall Steel10'6" x 15'6" Steel 4/11/1972 Active N7Gasoline, Gas MixGasoline 2,000Single Wall Steel4' x 6' Steel 4/11/1972Permanently Closed in Place (February 26, 2020)Y9 Used Oil Used Oil 550Single Wall Steel45" x 92" Steel 4/9/1980Permanently Closed in Place (February 26, 2020)YN/A Ethylene GlycolEthylene Glycol~25,000Single Wall Steel~12'L x 6'W x 13'HSteel UnknownPermanently Closed in Place (February 28, 2020)NAST IDNumberCurrent/LastContents*PreviousContents*Capacity(in gallons)ConstructionDetails**TankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofAST***Was release associated with AST System? (Y/N)-IncidentNumberMaterialReleasedDateofReleaseN/AUsed Oil/Gasoline/Jet FuelUnknownNotes:1.) The ethylene glycol UST is believed to be rectangular in shape as opposed to cylindrical, based on site observations.* Gasoline (leaded or unleaded), Diesel, used oil, waste oil, aviation fuel, etc. or pesticides, non-halogenated or halogenated solvents, etc.** Fiberglass (single- or double-walled), steel (single- or double-walled), steel with FRP (single- or double-walled), steel with liner, other, unknown*** Incident Number: N/AWR has not identified any current or former ASTs in relation to the siteDescription of ReleaseCurrently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by Table B-1Site History: UST/AST System & Other Release InformationSignature Flight SupportA release of petroleum was discovered during UST closure activities conducted in February 2020.1060 PTI DriveGreensboro, Guilford County, NCPage 1 of 1
8015CAcetone Benzene Butylbenzene, n- Butylbenzene, sec- Butylbenzene, tert-Ethylbenzene Isopropylbenzene, (Cumene) Isopropyltoluene, 4- Methyl Ethyl Ketone, (2-Butanone) Naphthalene Propylbenzene, n-Trimethylbenzene, 1,2,4-Trimethylbenzene, 1,3,5-Xylenes, total Methylnaphthalene, 2-C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsChromiumLeadEthylene glycol67-64-1 71-43-2 104-51-8 135-98-8 98-06-6 100-41-4 98-82-8 99-87-6 78-93-3 91-20-3 103-65-1 95-63-6 108-67-8 1330-20-7 91-57-6 --- --- --- --- 7440-47-3 7439-92-1 107-21-1SB-1 (5-7.5) 2/27/2020 0.072 0.0013 0.0038 0.002 0.00055 0.0051 0.003 0.0081 0.0074 0.018 0.0045 0.012 0.0084 0.0019 0.14<10160<1246 21 11NASB-2 (5-7.5) 2/27/2020 0.026<0.000670.00098<0.00089 <0.00067 <0.00067 <0.00067 <0.00056 <0.00610.0057<0.000670.0022 0.0011<0.0011 NA <14 <14 NA <14 NA NA NASB-3 (2.5-5) 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <5.0SB-4 (5-7.5) 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <4.7SB-5 (5-7.5) 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <5.9SB-6 (5-7.5) 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <5.524 0.0056 4.3 3.3 3.4 4.9 1.7 0.12 16 0.16 1.7 8.5 8.3 4.6 3.6 68 540 Immobile 315.4 270 4014,000 18 626 626 626 1,560 1,564 100 9,385 313 626 782 782 3,129 63 939 1,500 31,000 469 47 400 31,290360,000 164 16,350 16,350 16,350 40,000 40,880 4,000 245,280 8,176 16,35020,440 20,440 81,760 1,635 24,528 40,000 810,000 12,264 1,226 400 817,600Notes:1.) All results and standards provided in mg/kg (milligrams per kilogram) or parts per million.2.) See the laboratory report included in the Appendix for a full list of constituents. 3.) MSCC - NCDEQ UST Section Maximum Soil Contamination Concentration levels.NL= Not ListedNA= Compound Not Analyzed for by LaboratoryResult= Result Exceeds Laboratory Detection LimitsResult= Result Exceeds Soil to Groundwater MSCCResult= Result Exceeds Residential MSCCResult= Result Exceeds Industrial/Commercial MSCCGreensboro, Guilford County, NCTable B-3Summary Of Soil Analytical ResultsSignature Flight SupportIncident Number: N/A1060 PTI DriveResidential MSCCSoil to groundwater MSCCIndustrial/Commercial MSCCSample ID (Depth in Feet)DateCollectedAnalytical Method8260D - Volatile Organic Compounds (VOCs)8270E - Semi-VOCsMADEP - Extractable/Volatile Petroleum HydrocarbonsMetals - 6020BPage 1 of 1
SB-1 5-7.5 2/27/2020 8.4 119.8
SB-2 5-7.5 2/27/2020 <0.35 <0.35
Dispenser 2.5 2/27/2020 1891 5364
10 10
50 100
Notes:
Result = Result Exceeds Laboratory Detection Limits
Result = Result Exceeds Minimum Reportable Concentration
Result = Result Exceeds NCDEQ Action Levels
Greensboro, Guilford County, NC
NCDEQ Action Levels
Sample
Depth
(feet BLS)Diesel Range Organics (DRO)UVF - Total Petroleum
Hydrocarbons (TPH)Gasoline Range Organics (GRO)Analytical Method
Table B-3A
Summary Of Soil Analytical Results (TPH)
Signature Flight Support
Incident Number: N/A
1060 PTI Drive
Sample
ID
Date
Collected
NCDEQ Minimum Reportable
Concentration
2.) BLS = Below Land Surface
1.) All results and standards provided in mg/kg (milligrams per
kilogram) or parts per million
Page 1 of 1
Table B-4Summary of Groundwater Analytical ResultsSignature Flight SupportIncident Number: N/A1060 PTI DriveGreensboro, Guilford County, NCBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChloroformcis-1,2-DichloroetheneDi-isopropyl etherEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethyl tert-butyl etherMethylene ChlorideNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem&p-Xyleneso-XyleneTotal Xylene71-43-2 104-51-8 135-98-8 98-06-6 67-66-3 156-59-2 108-20-3 100-41-4 98-82-8 99-87-6 1634-04-4 75-09-2 91-20-3 103-65-1 108-88-3 95-63-6 108-67-8 1330-20-7 95-47-6 NAMW-1 2/27/2020 70 13 15 2.9 24 6.6 1.6 7.5 27 3.2 2.8 6.8 330 30<0.70210 80 8.9 100 108.9MW-2 2/27/2020 330 5.9 12 2.9<0.17 <0.1310 2 25 0.9 210<0.3428 11 0.54 0.72<0.140.3 0.33 0.63MW-3 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA1 70 70 70 70 70 70 600 70 25 20 5 6 70 600 400 400 500 500 5005,000 6,900 8,500 15,000 70,000 70,000 70,000 84,500 25,000 11,700 20,0005,000 6,000 3,000 260,000 28,500 25,000 85,500 85,500 85,500Notes:1.) All results provided in ug/L (micrograms per liter) or parts per billion.2.) Compounds analyzed by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. 3.) NC 2L Standard - North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L.4.) GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater.NL= Not ListedNA= Compound Not Analyzed for by LaboratoryResult= Result Exceeds Laboratory Detection LimitsResult= Result Exceeds 2L StandardResult= Result Exceeds GCL ValueAnalytical Method6200B - Volatile Organic CompoundsNC 2L Standard GCLs for GroundwaterSampleIDDateCollectedPage 1 of 2
Table B-4Summary of Groundwater Analytical ResultsSignature Flight SupportIncident Number: N/A1060 PTI DriveGreensboro, Guilford County, NC504.1 6020B 8015CAcenaphtheneDiethyl phthalateFluoreneNaphthalene2-MethylnaphthalenePhenanthrene1(2H)-Naphthalenone, 3,4-di…Benzene, 1,2,3-trimethyl-Benzene, 1,3-dimethyl-Benzene, 1-ethyl-2-methyl-Benzene, 2-ethyl-1,4-dimethyl-Benzoic acid, 2,6-dimethyl-Naphthalene, 1,5-dimethyl-Naphthalene, 1,6-dimethyl-Naphthalene, 1,7-dimethyl-C5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 Aromatics1,2-Dibromoethane (EDB)LeadEthylene glycol83-32-9 84-66-2 86-73-7 91-20-3 91-57-6 85-01-8 529-34-0 526-73-8 108-38-3 611-14-3 1758-88-9 632-46-2 571-61-9 575-43-9 575-37-1 --- --- --- --- 106-93-4 7439-92-1 107-21-1MW-1 2/27/2020 0.545 10.4 2.01 222 125 0.366 29 130 58 59 38 79 26 49 28 310 420<961770NA NA NAMW-2 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0.01237NAMW-3 2/27/2020NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <4.06000 0.2 20 25 600 6 NL NL NL NL NL NL NL NL NL 400 700 10000 200 0.02 15 100006,000,000 200 20,000 11,700 84,500 6,000 NL NL NL NL NL NL NL NL NL NL NL NL NL 5015,000 10,000,000Notes:1.) All results provided in ug/L (micrograms per liter) or parts per billion.2.) Compounds analyzed by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. 3.) NC 2L Standard - North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L.4.) GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater.NL= Not ListedNA= Compound Not Analyzed for by LaboratoryResult= Result Exceeds Laboratory Detection LimitsResult= Result Exceeds 2L StandardResult= Result Exceeds GCL Value625.1 - Semi-Volatile Organic CompoundsMADEP - Extractable/Volatile Petroleum HydrocarbonsAnalytical MethodGCLs for GroundwaterSampleIDDateCollectedNC 2L Standard Page 2 of 2
Easting NorthingMW-1 02/27/2020 2 22.0 0-12 12-22 93.66 02/28/2020 8.02 --- 85.64 1721703.9493 856530.3296MW-2 02/27/2020 2 24.0 0-9 9-24 94.28 02/28/2020 9.03 --- 85.25 1721663.8755 856468.2519MW-3 02/27/2020 2 20.0 0-5 5-20 94.06 02/28/2020 2.32 --- 91.74 1721613.3703 856480.3943 1.) Top-of-Casing elevations are relative to an arbitrary spot on the site at an assumed elevation of 100 feet above mean sea level.Notes: Total Depth (feet) 2.) Groundwater elevation calculated by: (Top-of-Casing - Depth-to-Water) + (Free Product Thickness x 0.8581).Date Water Level MeasuredDate InstalledGroundwaterElevation (feet)Incident Number: N/AWell IDWell Coordinates(NC State Plane NAD 83 Feet)Depth-to-Water from Top-of-Casing(feet)Table B-71060 PTI DriveMonitoring & Remediation Well Construction InformationWell Casing Diameter(inches)Free Product Thickness(feet)Screened Interval (feet)Top-of-Casing Elevation (feet)Well Casing Depth (feet)Signature Flight SupportGreensboro, Guilford County, NCPage 1 of 1

APPENDIX A

SKETCH OF THE TANK FARM AREA

APPENDIX B

UST-3 FORM
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY I.D. #_____________________
Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted to the
appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be
submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank Closure
and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust. Note: To close tanks in place you must
obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address
Facility ID # (If known)
City

County
Street Address

State
Zip Code
City County Zip Code
Phone Number
Email
Phone Number

III. CONTACT PERSONNEL
Name:

Company Name:

Job Title:

Phone Number:

IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:

Contractor Company Name:

Address:

State:

Zip Code:

Phone No:

Primary Consultant Name:

Primary Consultant Company Name:

Consultant Phone No:

VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE

Tank ID No.

Size in Gallons

Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place * New Contents Stored

* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? □ Yes □ No □ Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed

SCHEDULED REMOVAL DATE

Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 5/13/2019
Signature Flight Support Corporation
6427 Bryan Blvd PTI Airport
Greensboro Guilford
NC 27409
336-668-0481 [e-mail]
Signature Flight Support GSO
00-0-0000009598
6427 Bryan Blvd PTI Airport
Greensboro Guilford 27409
336-668-0481
Donal Brookshire General ManagerSignature Flight Support Corporation 336-668-0481
Tony Disher EVO Corporation
1703 Vargrave St 27107 877-725-5844
G. Matthew James WithersRavenel
NC
919-469-3340
7 2000 Gasoline ■
9 550 Used Oil ■
Unk ~7500 Ethylene Glycol ■
12/10/2019 2/3/2020
■

APPENDIX C

LIQUID WASTE AND DRUM DISPOSAL
MANIFESTS

APPENDIX D

UST-2A AND UST-2B FORMS

UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY: Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City County Street Address
State

Zip Code

City

County

Zip Code

Phone Number
Phone Number

III. CONTACT PERSONNEL
Contact for Facility:

Job Title:

Phone #:

Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #

Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #

IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/ concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016

Signature Flight Support Corporation
1060 PTI Drive
Greensboro Guilford
NC 27409
336-668-0481
Signature Flight Support GSO
00-0-0000009598
1060 PTI Drive
Greensboro 27409Guilford
336-668-0481
Donald Brookshire General Manager
336-668-0481
Tony Disher EVO Corporation 1703 Vargrave St
877-725-5844
G. Matthew James WithersRavenel 115 MacKenan Drive, Ca 919-469-3340
7 2000 Gasoline Unk 02/26/2020 Filled with foam 02/25/2020 ■■
9 550 Used Oil Unk 02/26/2020 02/25/2020 ■■Filled with foam
G. Matthew James, on behalf of Signature Flight Support
3/24/20
UST-2B Site Investigation Report for Permanent Closure or Change-in-
Service of
UN-REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY:
Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where UST systems will be converted from storing a regulated substance to a non-regulated substance, complete sections I,
II, III, IV, and VI.
4. For more than 5 un-registered UST systems, attach additional forms as needed.
5. Un-Registered USTs may be subject to unpaid fees and late penalties.
6. REGISTERED USTs use Form UST-2A.
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City

County

Street Address

State
Zip Code
City

County

Zip Code

Phone Number
Phone Number

III. CONTACT PERSONNEL
Contact for Facility: Job Title: Phone #:
Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #

Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #

IV. UST INFORMATION FOR UN-REGISTERED UST SYSTEMS
REGISTERED USTs use Form UST-2A. V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/
concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or visible soil contamination
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016

Signature Flight Support Corporation
1060 PTI Drive
Greensboro Guilford
NC 27409
336-668-0481
Signature Flight Support GSO
00-0-0000009598
1060 PTI Drive
Greensboro 27409Guilford
336-668-0481
Donald Brookshire General Manager
336-668-0481
Tony Disher EVO Corporation 877-725-58441703 Vargrave St
G. Matthew James WithersRavenel 919-469-3340115 MacKenan Drive, Ca
Unk ~25000 Etylene GyUnk 02/28/2020 Filled with foam 2/28/2020 ■■
G. Matthew James, on behalf of Signature Flight Support
3/24/20

APPENDIX E

WELL CONSTRUCTION RECORDS


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APPENDIX F

LABORATORY ANALYTICAL REPORTS

Hydrocarbon Analysis ResultsClient:WithersRavenelSamples takenThursday, February 27, 2020Address:Cary, NCSamples extractedThursday, February 27, 2020Samples analysedMonday, March 2, 2020Contact:Austin Pote / Matt JamesOperatorCaroline StevensProject:02150228.03 Signature Flight5F03640Matrix Sample IDDilution usedBTEX (C6 - C9)GRO (C5 - C10)DRO (C10 - C35)TPH (C5 - C35)Total Aromatics (C10-C35)16 EPA PAHsBaP HC Fingerprint Match% light % mid% heavys SB-1 24.1 <0.6 8.4 119.8 128.2 6.2 0.24 <0.024 94.5 5.5 0Deg.Kerosene 90.3%,(FCM)sSB-2 14.0<0.35<0.35<0.35<0.35 <0.07<0.11<0.014000,(FCM)s DISPENSER 983.0 <24.6 1891 5364 7255 340.1 13.4 <0.98 97.7 2 0.3Deg.Gas 77%,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK 99 %Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone contentFingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate presentRatios
QED Hydrocarbon Fingerprints
Project: 02150228.03 Signature Flight ##################
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 10, 2020
Matt James
Withers-Ravenel, Cary, NC
115 Mackenan Drive
Cary, NC 27511
Project Location: Greensboro, NC
Client Job Number:
Project Number: 02150228.03
Laboratory Work Order Number: 20B1278
Enclosed are results of analyses for samples received by the laboratory on February 28, 2020. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 96
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 5
Sample Results 11
20B1278-01 11
20B1278-02 19
20B1278-03 23
20B1278-04 25
20B1278-05 27
20B1278-06 29
20B1278-07 31
20B1278-08 38
20B1278-09 42
Sample Preparation Information 43
QC Data 45
Volatile Organic Compounds by GC/MS 45
B253342 45
B253398 49
B253562 53
Semivolatile Organic Compounds by GC/MS 55
B253574 55
Semivolatile Organic Compounds by - GC/MS 60
B253589 60
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED) 67
B253589 67
Semivolatile Organic Compounds by GC 68
Page 2 of 96
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Table of Contents (continued)
B253829 68
B253891 68
Petroleum Hydrocarbons Analyses - EPH 69
B253408 69
B253771 70
Petroleum Hydrocarbons Analyses - VPH 73
B253385 73
B253413 74
Metals Analyses (Total) 76
B253508 76
B253629 76
Drinking Water Organics EPA 504.1 77
B253604 77
Dual Column RPD Report 78
Flag/Qualifier Summary 80
Certifications 81
Chain of Custody/Sample Receipt 92
Page 3 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/10/2020
Withers-Ravenel, Cary, NC
115 Mackenan Drive
Cary, NC 27511
ATTN: Matt James
02150228.03
20B1278
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Greensboro, NC
SB-1 20B1278-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 6020B
SW-846 8260D
SW-846 8270E
SB-2 20B1278-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260D
SB-3 20B1278-03 Soil SM 2540G
SW-846 8015C
SB-4 20B1278-04 Soil SM 2540G
SW-846 8015C
SB-5 20B1278-05 Soil SM 2540G
SW-846 8015C
SB-6 20B1278-06 Soil SM 2540G
SW-846 8015C
MW-1 20B1278-07 Ground Water 625.1
MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM21-22 6200B
MW-2 20B1278-08 Ground Water EPA 504.1
SM21-22 6200B
SW-846 6020B
MW-3 20B1278-09 Ground Water SW-846 8015C
[TOC_1]Sample Summary[TOC]
Page 4 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA VPH elevated reporting limit for sample 20B1278-07 due to high concentrations of target compounds.
For method 6200B elevated reporting limit for sample 20B1278-07 due to high concentrations of target compounds.
For method MA EPH, only hydrocarbon ranges were requested and reported for samples 1 and 7.
For method 6020, all dilutions were performed as per standard operating procedure.
[TOC_1]Case Narrative[TOC]
Page 5 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
625.1
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Hexachlorocyclopentadiene
20B1278-07[MW-1], B253589-BLK1, B253589-BS1, B253589-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.Analyte & Samples(s) Qualified:
L-07
2-Chloronaphthalene
B253589-BSD1
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low
bias for reported result or non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-09
Benzidine
20B1278-07[MW-1], B253589-MS1, B253589-MSD1
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
MS-22
2,4,6-Tribromophenol
B253589-MS1
Hexachloroethane
B253589-MS1
Naphthalene
B253589-MS1
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
outside of the method specified criteria. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
MS-23
2-Methylnaphthalene
B253589-MS1
Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for this compound in this sample.
Analyte & Samples(s) Qualified:
R-06
2-Methylnaphthalene
20B1278-07RE1[MW-1], B253589-MSD1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
2,4-Dinitrophenol
20B1278-07[MW-1], B253589-MS1, B253589-MSD1, S046374-CCV1
Benzidine
20B1278-07[MW-1], B253589-BLK1, B253589-BS1, B253589-BSD1, B253589-MS1, B253589-MSD1, S046340-CCV1, S046374-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Benzidine
20B1278-07[MW-1], B253589-BLK1, B253589-BS1, B253589-BSD1, B253589-MS1, B253589-MSD1, S046340-CCV1, S046374-CCV1
Hexachlorocyclopentadiene
B253589-BLK1, B253589-BS1, B253589-BSD1, S046340-CCV1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
N-Nitrosodimethylamine
B253589-BS1, B253589-BSD1, S046340-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
N-Nitrosodimethylamine
B253589-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
20B1278-07[MW-1], B253589-MS1, B253589-MSD1, S046374-CCV1
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.Analyte & Samples(s) Qualified:
L-07
Nonane
B253413-BS1
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with
less than the method-specified amount.Analyte & Samples(s) Qualified:
O-01
20B1278-01[SB-1]
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is attached.
Analyte & Samples(s) Qualified:
S-15
2,5-Dibromotoluene (FID)
20B1278-01[SB-1]
2,5-Dibromotoluene (PID)
20B1278-01[SB-1]
Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less than the reporting limit and
bias is on the high side.
Analyte & Samples(s) Qualified:
S-17
2,5-Dibromotoluene (FID)
20B1278-02[SB-2]
2,5-Dibromotoluene (PID)
20B1278-02[SB-2]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B253398-BS1, B253398-BSD1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Methyl tert-Butyl Ether (MTBE)
20B1278-07[MW-1], B253398-BLK1, B253398-BS1, B253398-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Vinyl Acetate
B253398-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
20B1278-07[MW-1]
SW-846 6020B
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Lead
B253629-BS1
SW-846 8260D
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
n-Butylbenzene
B253342-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Chloromethane
20B1278-01[SB-1], 20B1278-02[SB-2], B253342-BLK1, B253342-BS1, B253342-BSD1
Vinyl Chloride
20B1278-01[SB-1], 20B1278-02[SB-2], B253342-BLK1, B253342-BS1, B253342-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
4-Methyl-2-pentanone (MIBK)
20B1278-01[SB-1], 20B1278-02[SB-2], B253342-BLK1, B253342-BS1, B253342-BSD1, S046165-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
1,1,1,2-Tetrachloroethane
B253342-BS1, B253342-BSD1, S046165-CCV1
1,1,2-Trichloro-1,2,2-trifluoroethane (F
B253342-BS1, B253342-BSD1, S046165-CCV1
Bromochloromethane
B253342-BS1, B253342-BSD1, S046165-CCV1
Chloroethane
B253342-BS1, B253342-BSD1, S046165-CCV1
Page 8 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Bromomethane
20B1278-01[SB-1], 20B1278-02[SB-2], B253342-BLK1, B253342-BS1, B253342-BSD1, S046165-CCV1
SW-846 8270E
Qualifications:
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
2,4-Dinitrophenol
20B1278-01[SB-1], S046360-CCV1
Benzidine
20B1278-01[SB-1], B253574-BLK1, B253574-BS1, B253574-BSD1, S046263-CCV1, S046360-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Aniline
B253574-BLK1, B253574-BS1, B253574-BSD1, S046263-CCV1
Benzidine
20B1278-01[SB-1], B253574-BLK1, B253574-BS1, B253574-BSD1, S046263-CCV1, S046360-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
2,4-Dinitrophenol
B253574-BS1, B253574-BSD1, S046263-CCV1
Benzoic Acid
B253574-BS1, B253574-BSD1, S046263-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
2,4-Dinitrophenol
20B1278-01[SB-1], B253574-BLK1, S046360-CCV1
Benzoic Acid
B253574-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
20B1278-01[SB-1], S046360-CCV1
4-Chloroaniline
20B1278-01[SB-1], B253574-BLK1, B253574-BS1, B253574-BSD1, S046263-CCV1, S046360-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-35
Benzidine
B253574-BLK1, B253574-BS1, B253574-BSD1, S046263-CCV1
Page 9 of 96
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MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 10 of 96
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Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
[TOC_2]20B1278-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.072 0.092 3/2/20 17:36 MFFmg/Kg dry0.0078 3/2/20SW-846 8260D1JAcetone
ND 0.0055 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D1Acrylonitrile
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00028 3/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
0.0013 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1JBenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1Bromobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D1Bromochloromethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D1Bromodichloromethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1Bromoform
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.0010 3/2/20SW-846 8260D1V-34Bromomethane
0.0074 0.037 3/2/20 17:36 MFFmg/Kg dry0.0051 3/2/20SW-846 8260D1J2-Butanone (MEK)
ND 0.037 3/2/20 17:36 MFFmg/Kg dry0.0042 3/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
0.0038 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D1n-Butylbenzene
0.0020 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D1sec-Butylbenzene
0.00055 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1Jtert-Butylbenzene
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00018 3/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0055 3/2/20 17:36 MFFmg/Kg dry0.0050 3/2/20SW-846 8260D1Carbon Disulfide
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D1Chlorobenzene
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1Chlorodibromomethane
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D1Chloroethane
ND 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D1Chloroform
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1R-05Chloromethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00028 3/2/20SW-846 8260D12-Chlorotoluene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D14-Chlorotoluene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D1Dibromomethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.0010 3/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D11,2-Dichloropropane
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D11,1-Dichloropropene
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 11 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00018 3/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.092 3/2/20 17:36 MFFmg/Kg dry0.0049 3/2/20SW-846 8260D11,4-Dioxane
0.0051 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1Ethylbenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.0018 3/2/20SW-846 8260D12-Hexanone (MBK)
0.0030 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1Isopropylbenzene (Cumene)
0.0081 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00028 3/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D1Methylene Chloride
ND 0.018 3/2/20 17:36 MFFmg/Kg dry0.0023 3/2/20SW-846 8260D1V-054-Methyl-2-pentanone (MIBK)
0.018 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1Naphthalene
0.0045 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1n-Propylbenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D1Styrene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00092 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D1Tetrachloroethylene
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.0010 3/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1Toluene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00028 3/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00037 3/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D1Trichloroethylene
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.00065 3/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.00074 3/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
0.012 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00028 3/2/20SW-846 8260D11,2,4-Trimethylbenzene
0.0084 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00046 3/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0092 3/2/20 17:36 MFFmg/Kg dry0.00083 3/2/20SW-846 8260D1R-05Vinyl Chloride
0.0019 0.0037 3/2/20 17:36 MFFmg/Kg dry0.00092 3/2/20SW-846 8260D1Jm+p Xylene
ND 0.0018 3/2/20 17:36 MFFmg/Kg dry0.00055 3/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.0 3/2/20 17:3670-130
Toluene-d8 96.5 3/2/20 17:3670-130
4-Bromofluorobenzene 112 3/2/20 17:3670-130
Page 12 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E1Acenaphthene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Acenaphthylene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E1Acetophenone
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.096 3/5/20SW-846 8270E1Aniline
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E1Anthracene
ND 0.79 3/6/20 12:46 BGLmg/Kg dry0.22 3/5/20SW-846 8270E1V-04, V-05Benzidine
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Benzo(a)anthracene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Benzo(a)pyrene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.2 3/6/20 12:46 BGLmg/Kg dry0.71 3/5/20SW-846 8270E1Benzoic Acid
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.20 3/5/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.28 3/5/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E14-Bromophenylphenylether
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Butylbenzylphthalate
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E1Carbazole
ND 0.79 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E1V-344-Chloroaniline
ND 0.79 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E12-Chloronaphthalene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E12-Chlorophenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E14-Chlorophenylphenylether
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Chrysene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Dibenzofuran
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Di-n-butylphthalate
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E11,2-Dichlorobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E11,3-Dichlorobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E11,4-Dichlorobenzene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E1V-343,3-Dichlorobenzidine
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E12,4-Dichlorophenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E1Diethylphthalate
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E12,4-Dimethylphenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E1Dimethylphthalate
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.36 3/5/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.79 3/6/20 12:46 BGLmg/Kg dry0.55 3/5/20SW-846 8270E1V-04, V-202,4-Dinitrophenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.19 3/5/20SW-846 8270E12,4-Dinitrotoluene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.19 3/5/20SW-846 8270E12,6-Dinitrotoluene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.18 3/5/20SW-846 8270E1Di-n-octylphthalate
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Fluoranthene
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Fluorene
Page 13 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E1Hexachlorobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E1Hexachlorobutadiene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.34 3/5/20SW-846 8270E1Hexachlorocyclopentadiene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Hexachloroethane
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Isophorone
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E11-Methylnaphthalene
0.14 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1J2-Methylnaphthalene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E12-Methylphenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E13/4-Methylphenol
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Naphthalene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.24 3/5/20SW-846 8270E12-Nitroaniline
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E13-Nitroaniline
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E14-Nitroaniline
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E1Nitrobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.17 3/5/20SW-846 8270E12-Nitrophenol
ND 0.79 3/6/20 12:46 BGLmg/Kg dry0.29 3/5/20SW-846 8270E14-Nitrophenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.22 3/5/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.18 3/5/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Pentachloronitrobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.28 3/5/20SW-846 8270E1Pentachlorophenol
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.11 3/5/20SW-846 8270E1Phenanthrene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E1Phenol
ND 0.20 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E1Pyrene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.12 3/5/20SW-846 8270E1Pyridine
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.16 3/5/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.13 3/5/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.41 3/6/20 12:46 BGLmg/Kg dry0.14 3/5/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 49.3 3/6/20 12:4630-130
Phenol-d6 49.8 3/6/20 12:4630-130
Nitrobenzene-d5 47.4 3/6/20 12:4630-130
2-Fluorobiphenyl 59.5 3/6/20 12:4630-130
2,4,6-Tribromophenol 52.9 3/6/20 12:4630-130
p-Terphenyl-d14 59.2 3/6/20 12:4630-130
Page 14 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
140 23 3/5/20 14:43 RDDmg/Kg dry 3/3/20MADEP-EPH-04-1.12C9-C18 Aliphatics
ND 12 3/4/20 19:38 RDDmg/Kg dry 3/3/20MADEP-EPH-04-1.11C19-C36 Aliphatics
29 12 3/4/20 19:38 RDDmg/Kg dry 3/3/20MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
28 12 3/4/20 19:38 RDDmg/Kg dry 3/3/20MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)69.2 3/4/20 19:3840-140
Chlorooctadecane (COD)69.2 3/5/20 14:4340-140
o-Terphenyl (OTP)74.1 3/4/20 19:3840-140
2-Bromonaphthalene 84.6 3/4/20 19:3840-140
2-Fluorobiphenyl 83.0 3/4/20 19:3840-140
Page 15 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.47
Petroleum Hydrocarbons Analyses - VPH
ND 10 3/3/20 21:02 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 10 3/3/20 21:02 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
38 10 3/3/20 21:02 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
20 10 3/3/20 21:02 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
18 10 3/3/20 21:02 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)218 3/3/20 21:02*S-1570-130
2,5-Dibromotoluene (PID)177 3/3/20 21:02*S-1570-130
Page 16 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
21 5.0 3/9/20 11:06 QNWmg/Kg dry0.65 3/5/20SW-846 6020B5Chromium
11 2.0 3/9/20 11:06 QNWmg/Kg dry0.16 3/5/20SW-846 6020B5Lead
Page 17 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 2/27/2020 10:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.3 3/5/20 8:44 CAH% Wt 3/3/20SM 2540G1% Solids
Page 18 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-02
Field Sample #: SB-2
Sample Matrix: Soil
Sampled: 2/27/2020 17:45
[TOC_2]20B1278-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.026 0.11 3/2/20 16:39 MFFmg/Kg dry0.0093 3/2/20SW-846 8260D1JAcetone
ND 0.0067 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D1Acrylonitrile
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00033 3/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1Benzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1Bromobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D1Bromochloromethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1Bromodichloromethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1Bromoform
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.0012 3/2/20SW-846 8260D1V-34Bromomethane
ND 0.045 3/2/20 16:39 MFFmg/Kg dry0.0061 3/2/20SW-846 8260D12-Butanone (MEK)
ND 0.045 3/2/20 16:39 MFFmg/Kg dry0.0050 3/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
0.00098 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1Jn-Butylbenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00022 3/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0067 3/2/20 16:39 MFFmg/Kg dry0.0060 3/2/20SW-846 8260D1Carbon Disulfide
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1Chlorobenzene
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1Chlorodibromomethane
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D1Chloroethane
ND 0.0045 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1Chloroform
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1R-05Chloromethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00033 3/2/20SW-846 8260D12-Chlorotoluene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D14-Chlorotoluene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D1Dibromomethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0045 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.0012 3/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0045 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1Diethyl Ether
Page 19 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-02
Field Sample #: SB-2
Sample Matrix: Soil
Sampled: 2/27/2020 17:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00022 3/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.11 3/2/20 16:39 MFFmg/Kg dry0.0059 3/2/20SW-846 8260D11,4-Dioxane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1Ethylbenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.0022 3/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0045 3/2/20 16:39 MFFmg/Kg dry0.00033 3/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D1Methylene Chloride
ND 0.022 3/2/20 16:39 MFFmg/Kg dry0.0028 3/2/20SW-846 8260D1V-054-Methyl-2-pentanone (MIBK)
0.0057 0.0045 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1Naphthalene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1n-Propylbenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D1Styrene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0011 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.0013 3/2/20SW-846 8260D1Tetrachloroethylene
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.0012 3/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1Toluene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00033 3/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00045 3/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D1Trichloroethylene
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.00078 3/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.00089 3/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
0.0022 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00033 3/2/20SW-846 8260D1J1,2,4-Trimethylbenzene
0.0011 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00056 3/2/20SW-846 8260D1J1,3,5-Trimethylbenzene
ND 0.011 3/2/20 16:39 MFFmg/Kg dry0.0010 3/2/20SW-846 8260D1R-05Vinyl Chloride
ND 0.0045 3/2/20 16:39 MFFmg/Kg dry0.0011 3/2/20SW-846 8260D1m+p Xylene
ND 0.0022 3/2/20 16:39 MFFmg/Kg dry0.00067 3/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.7 3/2/20 16:3970-130
Toluene-d8 95.5 3/2/20 16:3970-130
4-Bromofluorobenzene 108 3/2/20 16:3970-130
Page 20 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-02
Field Sample #: SB-2
Sample Matrix: Soil
Sampled: 2/27/2020 17:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.08
Petroleum Hydrocarbons Analyses - VPH
ND 14 3/3/20 20:33 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 3/3/20 20:33 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 3/3/20 20:33 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 3/3/20 20:33 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 3/3/20 20:33 KMBmg/Kg dry 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)154 3/3/20 20:33*S-1770-130
2,5-Dibromotoluene (PID)137 3/3/20 20:33*S-1770-130
Page 21 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-02
Field Sample #: SB-2
Sample Matrix: Soil
Sampled: 2/27/2020 17:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.3 3/6/20 8:41 JS% Wt 3/6/20SM 2540G1% Solids
Page 22 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-03
Field Sample #: SB-3
Sample Matrix: Soil
Sampled: 2/27/2020 13:45
[TOC_2]20B1278-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC
ND 15 3/9/20 21:34 IMRmg/Kg dry5.0 3/9/20SW-846 8015C1Ethylene glycol
Page 23 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-03
Field Sample #: SB-3
Sample Matrix: Soil
Sampled: 2/27/2020 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.7 3/5/20 8:45 CAH% Wt 3/3/20SM 2540G1% Solids
Page 24 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-04
Field Sample #: SB-4
Sample Matrix: Soil
Sampled: 2/27/2020 14:00
[TOC_2]20B1278-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC
ND 14 3/9/20 21:58 IMRmg/Kg dry4.7 3/9/20SW-846 8015C1Ethylene glycol
Page 25 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-04
Field Sample #: SB-4
Sample Matrix: Soil
Sampled: 2/27/2020 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.7 3/5/20 8:45 CAH% Wt 3/3/20SM 2540G1% Solids
Page 26 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-05
Field Sample #: SB-5
Sample Matrix: Soil
Sampled: 2/27/2020 14:15
[TOC_2]20B1278-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC
ND 18 3/9/20 22:23 IMRmg/Kg dry5.9 3/9/20SW-846 8015C1Ethylene glycol
Page 27 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-05
Field Sample #: SB-5
Sample Matrix: Soil
Sampled: 2/27/2020 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.2 3/5/20 8:45 CAH% Wt 3/3/20SM 2540G1% Solids
Page 28 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-06
Field Sample #: SB-6
Sample Matrix: Soil
Sampled: 2/27/2020 14:30
[TOC_2]20B1278-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC
ND 17 3/9/20 22:48 IMRmg/Kg dry5.5 3/9/20SW-846 8015C1Ethylene glycol
Page 29 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-06
Field Sample #: SB-6
Sample Matrix: Soil
Sampled: 2/27/2020 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.9 3/5/20 8:45 CAH% Wt 3/3/20SM 2540G1% Solids
Page 30 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
[TOC_2]20B1278-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 250 3/5/20 6:16 EEHg/L19 3/3/20SM21-22 6200B5Acetone
70 2.5 3/5/20 6:16 EEHg/L0.90 3/3/20SM21-22 6200B5Benzene
ND 2.5 3/5/20 6:16 EEHg/L0.75 3/3/20SM21-22 6200B5Bromobenzene
ND 2.5 3/5/20 6:16 EEHg/L1.6 3/3/20SM21-22 6200B5Bromochloromethane
ND 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B5Bromodichloromethane
ND 2.5 3/5/20 6:16 EEHg/L2.3 3/3/20SM21-22 6200B5Bromoform
ND 5.0 3/5/20 6:16 EEHg/L3.9 3/3/20SM21-22 6200B5Bromomethane
ND 25 3/5/20 6:16 EEHg/L9.7 3/3/20SM21-22 6200B52-Butanone (MEK)
13 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B5n-Butylbenzene
15 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B5sec-Butylbenzene
2.9 2.5 3/5/20 6:16 EEHg/L0.85 3/3/20SM21-22 6200B5tert-Butylbenzene
ND 2.5 3/5/20 6:16 EEHg/L0.55 3/3/20SM21-22 6200B5Carbon Tetrachloride
ND 2.5 3/5/20 6:16 EEHg/L0.75 3/3/20SM21-22 6200B5Chlorobenzene
ND 250 3/5/20 6:16 EEHg/L53 3/3/20SM21-22 6200B5Ethanol
ND 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B5Chlorodibromomethane
ND 2.5 3/5/20 6:16 EEHg/L1.8 3/3/20SM21-22 6200B5Chloroethane
24 2.5 3/5/20 6:16 EEHg/L0.85 3/3/20SM21-22 6200B5Chloroform
ND 5.0 3/5/20 6:16 EEHg/L2.2 3/3/20SM21-22 6200B5Chloromethane
ND 2.5 3/5/20 6:16 EEHg/L0.60 3/3/20SM21-22 6200B52-Chlorotoluene
ND 2.5 3/5/20 6:16 EEHg/L0.70 3/3/20SM21-22 6200B54-Chlorotoluene
ND 2.5 3/5/20 6:16 EEHg/L0.95 3/3/20SM21-22 6200B51,2-Dibromoethane (EDB)
ND 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B51,2-Dichlorobenzene
ND 2.5 3/5/20 6:16 EEHg/L0.60 3/3/20SM21-22 6200B51,3-Dichlorobenzene
ND 2.5 3/5/20 6:16 EEHg/L0.65 3/3/20SM21-22 6200B51,4-Dichlorobenzene
ND 2.5 3/5/20 6:16 EEHg/L1.3 3/3/20SM21-22 6200B5Dichlorodifluoromethane (Freon 12)
ND 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B51,1-Dichloroethane
ND 5.0 3/5/20 6:16 EEHg/L2.0 3/3/20SM21-22 6200B51,2-Dichloroethane
ND 2.5 3/5/20 6:16 EEHg/L1.6 3/3/20SM21-22 6200B51,1-Dichloroethylene
6.6 2.5 3/5/20 6:16 EEHg/L0.65 3/3/20SM21-22 6200B5cis-1,2-Dichloroethylene
ND 2.5 3/5/20 6:16 EEHg/L1.6 3/3/20SM21-22 6200B5trans-1,2-Dichloroethylene
ND 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B51,2-Dichloropropane
ND 2.5 3/5/20 6:16 EEHg/L0.55 3/3/20SM21-22 6200B51,3-Dichloropropane
ND 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B52,2-Dichloropropane
ND 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B51,1-Dichloropropene
ND 2.5 3/5/20 6:16 EEHg/L0.65 3/3/20SM21-22 6200B5cis-1,3-Dichloropropene
ND 2.5 3/5/20 6:16 EEHg/L1.2 3/3/20SM21-22 6200B5trans-1,3-Dichloropropene
1.6 2.5 3/5/20 6:16 EEHg/L0.85 3/3/20SM21-22 6200B5JDiisopropyl Ether (DIPE)
7.5 2.5 3/5/20 6:16 EEHg/L0.65 3/3/20SM21-22 6200B5Ethylbenzene
ND 25 3/5/20 6:16 EEHg/L7.6 3/3/20SM21-22 6200B52-Hexanone (MBK)
27 2.5 3/5/20 6:16 EEHg/L0.85 3/3/20SM21-22 6200B5Isopropylbenzene (Cumene)
3.2 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B5p-Isopropyltoluene (p-Cymene)
2.8 2.5 3/5/20 6:16 EEHg/L1.2 3/3/20SM21-22 6200B5L-04Methyl tert-Butyl Ether (MTBE)
6.8 25 3/5/20 6:16 EEHg/L1.7 3/3/20SM21-22 6200B5JMethylene Chloride
ND 25 3/5/20 6:16 EEHg/L8.4 3/3/20SM21-22 6200B54-Methyl-2-pentanone (MIBK)
Page 31 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
330 25 3/5/20 6:16 EEHg/L1.6 3/3/20SM21-22 6200B5Naphthalene
30 2.5 3/5/20 6:16 EEHg/L0.65 3/3/20SM21-22 6200B5n-Propylbenzene
ND 2.5 3/5/20 6:16 EEHg/L0.55 3/3/20SM21-22 6200B5Styrene
ND 2.5 3/5/20 6:16 EEHg/L1.1 3/3/20SM21-22 6200B51,1,2,2-Tetrachloroethane
ND 2.5 3/5/20 6:16 EEHg/L0.90 3/3/20SM21-22 6200B5Tetrachloroethylene
ND 2.5 3/5/20 6:16 EEHg/L0.70 3/3/20SM21-22 6200B5Toluene
ND 10 3/5/20 6:16 EEHg/L2.8 3/3/20SM21-22 6200B51,2,3-Trichlorobenzene
ND 2.5 3/5/20 6:16 EEHg/L2.0 3/3/20SM21-22 6200B51,2,4-Trichlorobenzene
ND 2.5 3/5/20 6:16 EEHg/L1.0 3/3/20SM21-22 6200B51,1,1-Trichloroethane
ND 2.5 3/5/20 6:16 EEHg/L0.80 3/3/20SM21-22 6200B51,1,2-Trichloroethane
ND 2.5 3/5/20 6:16 EEHg/L1.2 3/3/20SM21-22 6200B5Trichloroethylene
ND 2.5 3/5/20 6:16 EEHg/L1.6 3/3/20SM21-22 6200B5Trichlorofluoromethane (Freon 11)
ND 2.5 3/5/20 6:16 EEHg/L1.2 3/3/20SM21-22 6200B51,2,3-Trichloropropane
210 2.5 3/5/20 6:16 EEHg/L0.90 3/3/20SM21-22 6200B51,2,4-Trimethylbenzene
80 2.5 3/5/20 6:16 EEHg/L0.70 3/3/20SM21-22 6200B51,3,5-Trimethylbenzene
ND 100 3/5/20 6:16 EEHg/L51 3/3/20SM21-22 6200B5Vinyl Acetate
ND 2.5 3/5/20 6:16 EEHg/L2.2 3/3/20SM21-22 6200B5Vinyl Chloride
8.9 5.0 3/5/20 6:16 EEHg/L1.5 3/3/20SM21-22 6200B5m+p Xylene
100 2.5 3/5/20 6:16 EEHg/L0.85 3/3/20SM21-22 6200B5o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.7 3/5/20 6:1670-130
Toluene-d8 97.4 3/5/20 6:1670-130
4-Bromofluorobenzene 94.6 3/5/20 6:1670-130
Page 32 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
0.545 4.95 3/7/20 13:22 KLBg/L0.229 3/5/20625.11JAcenaphthene
<0.229 4.95 3/7/20 13:22 KLBg/L0.229 3/5/20625.11Acenaphthylene
<0.200 4.95 3/7/20 13:22 KLBg/L0.200 3/5/20625.11Anthracene
<16.2 19.8 3/7/20 13:22 KLBg/L16.2 3/5/20625.11MS-09, V-04, V-05Benzidine
<0.250 4.95 3/7/20 13:22 KLBg/L0.250 3/5/20625.11Benzo(a)anthracene
<0.292 4.95 3/7/20 13:22 KLBg/L0.292 3/5/20625.11Benzo(a)pyrene
<0.250 4.95 3/7/20 13:22 KLBg/L0.250 3/5/20625.11Benzo(b)fluoranthene
<0.392 4.95 3/7/20 13:22 KLBg/L0.392 3/5/20625.11Benzo(g,h,i)perylene
<0.275 4.95 3/7/20 13:22 KLBg/L0.275 3/5/20625.11Benzo(k)fluoranthene
<0.293 9.90 3/7/20 13:22 KLBg/L0.293 3/5/20625.114-Bromophenylphenylether
<0.292 9.90 3/7/20 13:22 KLBg/L0.292 3/5/20625.11Butylbenzylphthalate
<0.476 9.90 3/7/20 13:22 KLBg/L0.476 3/5/20625.114-Chloro-3-methylphenol
<0.466 9.90 3/7/20 13:22 KLBg/L0.466 3/5/20625.11Bis(2-chloroethoxy)methane
<0.507 9.90 3/7/20 13:22 KLBg/L0.507 3/5/20625.11Bis(2-chloroethyl)ether
<0.722 9.90 3/7/20 13:22 KLBg/L0.722 3/5/20625.11Bis(2-chloroisopropyl)ether
<0.450 9.90 3/7/20 13:22 KLBg/L0.450 3/5/20625.112-Chloronaphthalene
<0.372 9.90 3/7/20 13:22 KLBg/L0.372 3/5/20625.112-Chlorophenol
<0.311 9.90 3/7/20 13:22 KLBg/L0.311 3/5/20625.114-Chlorophenylphenylether
<0.215 4.95 3/7/20 13:22 KLBg/L0.215 3/5/20625.11Chrysene
<0.450 4.95 3/7/20 13:22 KLBg/L0.450 3/5/20625.11Dibenz(a,h)anthracene
<0.453 9.90 3/7/20 13:22 KLBg/L0.453 3/5/20625.11Di-n-butylphthalate
<0.458 4.95 3/7/20 13:22 KLBg/L0.458 3/5/20625.111,3-Dichlorobenzene
<0.379 4.95 3/7/20 13:22 KLBg/L0.379 3/5/20625.111,4-Dichlorobenzene
<0.454 4.95 3/7/20 13:22 KLBg/L0.454 3/5/20625.111,2-Dichlorobenzene
<0.355 9.90 3/7/20 13:22 KLBg/L0.355 3/5/20625.11V-343,3-Dichlorobenzidine
<0.297 9.90 3/7/20 13:22 KLBg/L0.297 3/5/20625.112,4-Dichlorophenol
10.4 9.90 3/7/20 13:22 KLBg/L0.223 3/5/20625.11Diethylphthalate
<0.787 9.90 3/7/20 13:22 KLBg/L0.787 3/5/20625.112,4-Dimethylphenol
<0.304 9.90 3/7/20 13:22 KLBg/L0.304 3/5/20625.11Dimethylphthalate
<1.93 9.90 3/7/20 13:22 KLBg/L1.93 3/5/20625.114,6-Dinitro-2-methylphenol
<1.61 9.90 3/7/20 13:22 KLBg/L1.61 3/5/20625.11V-042,4-Dinitrophenol
<0.324 9.90 3/7/20 13:22 KLBg/L0.324 3/5/20625.112,4-Dinitrotoluene
<0.343 9.90 3/7/20 13:22 KLBg/L0.343 3/5/20625.112,6-Dinitrotoluene
<0.517 9.90 3/7/20 13:22 KLBg/L0.517 3/5/20625.11Di-n-octylphthalate
<0.371 9.90 3/7/20 13:22 KLBg/L0.371 3/5/20625.111,2-Diphenylhydrazine/Azobenzene
<0.514 9.90 3/7/20 13:22 KLBg/L0.514 3/5/20625.11Bis(2-Ethylhexyl)phthalate
<0.294 4.95 3/7/20 13:22 KLBg/L0.294 3/5/20625.11Fluoranthene
2.01 4.95 3/7/20 13:22 KLBg/L0.243 3/5/20625.11JFluorene
<0.429 9.90 3/7/20 13:22 KLBg/L0.429 3/5/20625.11Hexachlorobenzene
<0.586 9.90 3/7/20 13:22 KLBg/L0.586 3/5/20625.11Hexachlorobutadiene
<4.75 9.90 3/7/20 13:22 KLBg/L4.75 3/5/20625.11L-04Hexachlorocyclopentadiene
<0.524 9.90 3/7/20 13:22 KLBg/L0.524 3/5/20625.11Hexachloroethane
<0.509 4.95 3/7/20 13:22 KLBg/L0.509 3/5/20625.11Indeno(1,2,3-cd)pyrene
<0.297 9.90 3/7/20 13:22 KLBg/L0.297 3/5/20625.11Isophorone
Page 33 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by - GC/MS
222 24.8 3/7/20 15:02 KLBg/L2.19 3/5/20625.15Naphthalene
<0.406 9.90 3/7/20 13:22 KLBg/L0.406 3/5/20625.11Nitrobenzene
<0.411 9.90 3/7/20 13:22 KLBg/L0.411 3/5/20625.112-Nitrophenol
<0.621 9.90 3/7/20 13:22 KLBg/L0.621 3/5/20625.114-Nitrophenol
<1.81 9.90 3/7/20 13:22 KLBg/L1.81 3/5/20625.11N-Nitrosodimethylamine
<0.291 9.90 3/7/20 13:22 KLBg/L0.291 3/5/20625.11N-Nitrosodiphenylamine/Diphenylamine
<0.513 9.90 3/7/20 13:22 KLBg/L0.513 3/5/20625.11N-Nitrosodi-n-propylamine
<0.329 9.90 3/7/20 13:22 KLBg/L0.329 3/5/20625.11Pentachlorophenol
125 24.8 3/7/20 15:02 KLBg/L1.32 3/5/20625.15R-062-Methylnaphthalene
0.366 4.95 3/7/20 13:22 KLBg/L0.284 3/5/20625.11JPhenanthrene
<0.451 9.90 3/7/20 13:22 KLBg/L0.451 3/5/20625.112-Methylphenol
<0.196 9.90 3/7/20 13:22 KLBg/L0.196 3/5/20625.11Phenol
<0.202 19.8 3/7/20 13:22 KLBg/L0.202 3/5/20625.113/4-Methylphenol
<0.252 4.95 3/7/20 13:22 KLBg/L0.252 3/5/20625.11Pyrene
<0.552 4.95 3/7/20 13:22 KLBg/L0.552 3/5/20625.111,2,4-Trichlorobenzene
<0.330 9.90 3/7/20 13:22 KLBg/L0.330 3/5/20625.112,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 49.6 3/7/20 13:2215-110
2-Fluorophenol 42.8 3/7/20 15:0215-110
Phenol-d6 34.2 3/7/20 13:2215-110
Phenol-d6 30.3 3/7/20 15:0215-110
Nitrobenzene-d5 76.8 3/7/20 13:2230-130
Nitrobenzene-d5 68.0 3/7/20 15:0230-130
2-Fluorobiphenyl 87.4 3/7/20 13:2230-130
2-Fluorobiphenyl 87.4 3/7/20 15:0230-130
2,4,6-Tribromophenol 85.3 3/7/20 13:2215-110
2,4,6-Tribromophenol 74.0 3/7/20 15:0215-110
p-Terphenyl-d14 87.9 3/7/20 13:2230-130
p-Terphenyl-d14 79.9 3/7/20 15:0230-130
Page 34 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
Analyte MethodResponseDFUnitsRTResults
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)
Date
AnalystAnalyzed
Date/Time
PreparedCAS #Q#
1(2H)-Naphthalenone, 3,4-di...29 g/L 14.822616586 000529-34-0 625.1 3/5/20 KLB3/7/20 13:2295
Benzene, 1,2,3-trimethyl-130 g/L 13.2852109380 000526-73-8 625.1 3/5/20 KLB3/7/20 13:2297
Benzene, 1,3-dimethyl-58 g/L 12.824934359 000108-38-3 625.1 3/5/20 KLB3/7/20 13:2297
Benzene, 1-ethyl-2-methyl-59 g/L 13.213945772 000611-14-3 625.1 3/5/20 KLB3/7/20 13:2294
Benzene, 2-ethyl-1,4-dimethyl-38 g/L 13.545615594 001758-88-9 625.1 3/5/20 KLB3/7/20 13:2294
Benzoic acid, 2,6-dimethyl-79 g/L 14.6581690570 000632-46-2 625.1 3/5/20 KLB3/7/20 13:2291
Naphthalene, 1,5-dimethyl-26 g/L 14.992555639 000571-61-9 625.1 3/5/20 KLB3/7/20 13:2291
Naphthalene, 1,6-dimethyl-49 g/L 14.9281046030 000575-43-9 625.1 3/5/20 KLB3/7/20 13:2293
Naphthalene, 1,7-dimethyl-28 g/L 14.974611089 000575-37-1 625.1 3/5/20 KLB3/7/20 13:2298
Page 35 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
420 96 3/9/20 14:51 RDDg/L 3/8/20MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 96 3/9/20 14:51 RDDg/L 3/8/20MADEP-EPH-04-1.11C19-C36 Aliphatics
740 96 3/9/20 14:51 RDDg/L 3/8/20MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
470 96 3/9/20 14:51 RDDg/L 3/8/20MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)57.9 3/9/20 14:5140-140
o-Terphenyl (OTP)69.4 3/9/20 14:5140-140
2-Bromonaphthalene 73.1 3/9/20 14:5140-140
2-Fluorobiphenyl 72.4 3/9/20 14:5140-140
Page 36 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/27/2020 12:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
370 200 3/4/20 8:50 KMBg/L 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
2Unadjusted C5-C8 Aliphatics
310 200 3/4/20 8:50 KMBg/L 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
2C5-C8 Aliphatics
1300 200 3/4/20 8:50 KMBg/L 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
2Unadjusted C9-C12 Aliphatics
ND 200 3/4/20 8:50 KMBg/L 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
2C9-C12 Aliphatics
1300 200 3/4/20 8:50 KMBg/L 3/3/20MADEP-VPH-Feb 2018
Rev 2.1
2C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)109 3/4/20 8:5070-130
2,5-Dibromotoluene (PID)108 3/4/20 8:5070-130
Page 37 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-08
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/27/2020 14:50
[TOC_2]20B1278-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/5/20 5:48 EEHg/L3.8 3/3/20SM21-22 6200B1Acetone
330 12 3/5/20 23:25 LBDg/L4.5 3/5/20SM21-22 6200B25Benzene
ND 0.50 3/5/20 5:48 EEHg/L0.15 3/3/20SM21-22 6200B1Bromobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.32 3/3/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/5/20 5:48 EEHg/L0.46 3/3/20SM21-22 6200B1Bromoform
ND 1.0 3/5/20 5:48 EEHg/L0.78 3/3/20SM21-22 6200B1Bromomethane
ND 5.0 3/5/20 5:48 EEHg/L1.9 3/3/20SM21-22 6200B12-Butanone (MEK)
5.9 0.50 3/5/20 5:48 EEHg/L0.21 3/3/20SM21-22 6200B1n-Butylbenzene
12 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B1sec-Butylbenzene
2.9 0.50 3/5/20 5:48 EEHg/L0.17 3/3/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/5/20 5:48 EEHg/L0.11 3/3/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/5/20 5:48 EEHg/L0.15 3/3/20SM21-22 6200B1Chlorobenzene
ND 50 3/5/20 5:48 EEHg/L11 3/3/20SM21-22 6200B1Ethanol
ND 0.50 3/5/20 5:48 EEHg/L0.21 3/3/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/5/20 5:48 EEHg/L0.35 3/3/20SM21-22 6200B1Chloroethane
ND 0.50 3/5/20 5:48 EEHg/L0.17 3/3/20SM21-22 6200B1Chloroform
ND 1.0 3/5/20 5:48 EEHg/L0.45 3/3/20SM21-22 6200B1Chloromethane
ND 0.50 3/5/20 5:48 EEHg/L0.12 3/3/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/5/20 5:48 EEHg/L0.14 3/3/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/5/20 5:48 EEHg/L0.19 3/3/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.12 3/3/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.13 3/3/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.26 3/3/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 3/5/20 5:48 EEHg/L0.41 3/3/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/5/20 5:48 EEHg/L0.32 3/3/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/5/20 5:48 EEHg/L0.13 3/3/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/5/20 5:48 EEHg/L0.31 3/3/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/5/20 5:48 EEHg/L0.20 3/3/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/5/20 5:48 EEHg/L0.11 3/3/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/5/20 5:48 EEHg/L0.20 3/3/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/5/20 5:48 EEHg/L0.13 3/3/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/5/20 5:48 EEHg/L0.23 3/3/20SM21-22 6200B1trans-1,3-Dichloropropene
10 0.50 3/5/20 5:48 EEHg/L0.17 3/3/20SM21-22 6200B1Diisopropyl Ether (DIPE)
2.0 0.50 3/5/20 5:48 EEHg/L0.13 3/3/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/5/20 5:48 EEHg/L1.5 3/3/20SM21-22 6200B12-Hexanone (MBK)
25 0.50 3/5/20 5:48 EEHg/L0.17 3/3/20SM21-22 6200B1Isopropylbenzene (Cumene)
0.90 0.50 3/5/20 5:48 EEHg/L0.20 3/3/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
210 12 3/5/20 23:25 LBDg/L6.2 3/5/20SM21-22 6200B25Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/5/20 5:48 EEHg/L0.34 3/3/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/5/20 5:48 EEHg/L1.7 3/3/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 38 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-08
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/27/2020 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
28 5.0 3/5/20 5:48 EEHg/L0.31 3/3/20SM21-22 6200B1Naphthalene
11 0.50 3/5/20 5:48 EEHg/L0.13 3/3/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/5/20 5:48 EEHg/L0.11 3/3/20SM21-22 6200B1Styrene
ND 0.50 3/5/20 5:48 EEHg/L0.22 3/3/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/5/20 5:48 EEHg/L0.18 3/3/20SM21-22 6200B1Tetrachloroethylene
0.54 0.50 3/5/20 5:48 EEHg/L0.14 3/3/20SM21-22 6200B1Toluene
ND 2.0 3/5/20 5:48 EEHg/L0.57 3/3/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.40 3/3/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/5/20 5:48 EEHg/L0.20 3/3/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/5/20 5:48 EEHg/L0.16 3/3/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/5/20 5:48 EEHg/L0.24 3/3/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/5/20 5:48 EEHg/L0.33 3/3/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/5/20 5:48 EEHg/L0.25 3/3/20SM21-22 6200B11,2,3-Trichloropropane
0.72 0.50 3/5/20 5:48 EEHg/L0.18 3/3/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/5/20 5:48 EEHg/L0.14 3/3/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/5/20 5:48 EEHg/L10 3/3/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/5/20 5:48 EEHg/L0.45 3/3/20SM21-22 6200B1Vinyl Chloride
0.30 1.0 3/5/20 5:48 EEHg/L0.30 3/3/20SM21-22 6200B1Jm+p Xylene
0.33 0.50 3/5/20 5:48 EEHg/L0.17 3/3/20SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 3/5/20 23:2570-130
1,2-Dichloroethane-d4 91.6 3/5/20 5:4870-130
Toluene-d8 96.9 3/5/20 23:2570-130
Toluene-d8 97.8 3/5/20 5:4870-130
4-Bromofluorobenzene 91.9 3/5/20 23:2570-130
4-Bromofluorobenzene 96.6 3/5/20 5:4870-130
Page 39 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-08
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/27/2020 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
37 0.50 3/4/20 19:04 QNWg/L0.085 3/4/20SW-846 6020B1Lead
Page 40 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-08
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 2/27/2020 14:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Drinking Water Organics EPA 504.1
ND 0.020 3/5/20 16:20 JMBg/L0.012 3/5/20EPA 504.111,2-Dibromoethane (EDB) (1)
Surrogates % Recovery Recovery Limits Flag/Qual
1,3-Dibromopropane (1)124 3/5/20 16:2070-130
Page 41 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/28/2020
Work Order: 20B1278Sample Description:Project Location: Greensboro, NC
Sample ID: 20B1278-09
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/27/2020 16:00
[TOC_2]20B1278-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC
ND 10 3/10/20 13:25 IMRmg/L4.0 3/10/20SW-846 8015C1Ethylene glycol
Page 42 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3510C Analytical Method: 625.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253589 03/05/201010 1.0020B1278-07 [MW-1]
B253589 03/05/201010 1.0020B1278-07RE1 [MW-1]
Prep Method: EPA 504 water Analytical Method: EPA 504.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253604 03/05/2034.5 35.020B1278-08 [MW-2]
Prep Method: SW-846 3546 Analytical Method: MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253408 03/03/2020.9 2.0020B1278-01 [SB-1]
B253408 03/03/2020.9 2.0020B1278-01RE1 [SB-1]
Prep Method: SW-846 3510C Analytical Method: MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253771 03/08/20985 1.9020B1278-07 [MW-1]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253385 03/03/207.30 6.3020B1278-01 [SB-1]
B253385 03/03/205.40 6.0020B1278-02 [SB-2]
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253413 03/03/202.5 5.0020B1278-07 [MW-1]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B253382 03/03/2020B1278-01 [SB-1]
B253382 03/03/2020B1278-03 [SB-3]
B253382 03/03/2020B1278-04 [SB-4]
B253382 03/03/2020B1278-05 [SB-5]
B253382 03/03/2020B1278-06 [SB-6]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B253678 03/06/2020B1278-02 [SB-2]
[TOC_1]Sample Preparation Information[TOC]
Page 43 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B Analytical Method: SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253398 03/03/201 5.0020B1278-07 [MW-1]
B253398 03/03/205 5.0020B1278-08 [MW-2]
Prep Method: SW-846 5030B Analytical Method: SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253562 03/05/200.2 5.0020B1278-08RE1 [MW-2]
Prep Method: SW-846 3050B Analytical Method: SW-846 6020B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253629 03/05/201.51 50.020B1278-01 [SB-1]
Prep Method: SW-846 3005A Analytical Method: SW-846 6020B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253508 03/04/2050.0 50.020B1278-08 [MW-2]
Prep Method: Alcohol Prep Analytical Method: SW-846 8015C
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253829 03/09/2010.0 12.020B1278-03 [SB-3]
B253829 03/09/2010.8 12.220B1278-04 [SB-4]
B253829 03/09/2010.2 12.920B1278-05 [SB-5]
B253829 03/09/2010.1 12.520B1278-06 [SB-6]
Prep Method: Alcohol Prep Analytical Method: SW-846 8015C
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253891 03/10/201.00 1.0020B1278-09 [MW-3]
Prep Method: SW-846 5035 Analytical Method: SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253342 03/02/206.58 10.020B1278-01 [SB-1]
B253342 03/02/205.46 10.020B1278-02 [SB-2]
Prep Method: SW-846 3546 Analytical Method: SW-846 8270E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B253574 03/05/2030.3 1.0020B1278-01 [SB-1]
Page 44 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B253342 - SW-846 5035
[TOC_3]B253342[TOC]
Blank (B253342-BLK1) Prepared & Analyzed: 03/02/20
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010 V-34ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010 R-05ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 45 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253342 - SW-846 5035
Blank (B253342-BLK1) Prepared & Analyzed: 03/02/20
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 V-05ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010 R-05ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 76.80.0384
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 97.20.0486
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1130.0565
LCS (B253342-BS1) Prepared & Analyzed: 03/02/20
Acetone mg/Kg wet0.10 0.200 70-16088.90.178
Acrylonitrile mg/Kg wet0.0060 0.0200 70-13094.10.0188
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-1301100.0220
Benzene mg/Kg wet0.0020 0.0200 70-1301040.0207
Bromobenzene mg/Kg wet0.0020 0.0200 70-13099.00.0198
Bromochloromethane mg/Kg wet0.0020 0.0200 V-2070-1301200.0240
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-1301000.0201
Bromoform mg/Kg wet0.0020 0.0200 70-1301240.0247
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13093.50.0187
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-16087.00.174
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-1301050.209
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13075.10.0150
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-13094.10.0188
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16088.10.0176
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13085.50.0171
Carbon Disulfide mg/Kg wet0.0060 0.200 70-1301050.210
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-1301090.0218
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301170.0234
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301050.0210
Chloroethane mg/Kg wet0.020 0.0200 V-2070-1301000.0200
Chloroform mg/Kg wet0.0040 0.0200 70-13088.00.0176
Chloromethane mg/Kg wet0.010 0.0200 R-0570-13074.40.0149
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301010.0202
Page 46 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253342 - SW-846 5035
LCS (B253342-BS1) Prepared & Analyzed: 03/02/20
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13094.90.0190
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13085.30.0171
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301040.0207
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301180.0235
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13093.30.0187
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13096.90.0194
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.80.0186
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13091.60.0183
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 J40-16097.40.0195
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13082.30.0165
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301120.0225
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-13087.20.0174
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13086.60.0173
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13087.20.0174
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301070.0214
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301050.0210
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13080.00.0160
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13098.90.0198
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13096.50.0193
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13091.00.0182
Diethyl Ether mg/Kg wet0.020 0.0200 J70-13092.90.0186
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13073.50.0147
1,4-Dioxane mg/Kg wet0.10 0.200 40-1601020.203
Ethylbenzene mg/Kg wet0.0020 0.0200 70-13097.50.0195
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-1601030.0206
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-16083.00.166
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301150.0229
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13089.50.0179
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13090.70.0181
Methylene Chloride mg/Kg wet0.020 0.0200 40-1601020.0203
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 V-0570-16086.40.173
Naphthalene mg/Kg wet0.0040 0.0200 40-13081.40.0163
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-13099.20.0198
Styrene mg/Kg wet0.0020 0.0200 70-1301110.0222
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 V-2070-1301190.0238
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-1301020.0204
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301030.0207
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-1301140.0229
Toluene mg/Kg wet0.0020 0.0200 70-13095.00.0190
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.30.0185
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13096.60.0193
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.60.0185
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13083.10.0166
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13094.60.0189
Trichloroethylene mg/Kg wet0.0020 0.0200 70-1301090.0217
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-13098.60.0197
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301150.0230
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 V-2070-1301030.0205
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13082.50.0165
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301010.0203
Vinyl Chloride mg/Kg wet0.010 0.0200 R-0540-13079.80.0160
Page 47 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253342 - SW-846 5035
LCS (B253342-BS1) Prepared & Analyzed: 03/02/20
m+p Xylene mg/Kg wet0.0040 0.0400 70-1301000.0401
o-Xylene mg/Kg wet0.0020 0.0200 70-13099.20.0198
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 83.60.0418
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 87.00.0435
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1050.0523
LCS Dup (B253342-BSD1) Prepared & Analyzed: 03/02/20
Acetone mg/Kg wet0.10 0.200 2570-160112 23.20.225
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-130108 14.10.0217
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-130104 5.710.0208
Benzene mg/Kg wet0.0020 0.0200 2570-13094.3 9.300.0189
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13094.3 4.860.0189
Bromochloromethane mg/Kg wet0.0020 0.0200 25 V-2070-130118 1.850.0236
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-13097.5 2.830.0195
Bromoform mg/Kg wet0.0020 0.0200 2570-130114 7.560.0229
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-130117 22.10.0233
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-160107 20.70.214
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-130114 8.850.229
n-Butylbenzene mg/Kg wet0.0020 0.0200 25 L-0770-13069.6 7.60*0.0139
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13085.3 9.810.0171
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16085.6 2.880.0171
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-130102 17.80.0204
Carbon Disulfide mg/Kg wet0.0060 0.200 2570-13099.7 5.440.199
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-13099.9 8.900.0200
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130107 9.130.0213
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130108 2.530.0216
Chloroethane mg/Kg wet0.020 0.0200 25 V-2070-130115 14.20.0231
Chloroform mg/Kg wet0.0040 0.0200 2570-13093.1 5.630.0186
Chloromethane mg/Kg wet0.010 0.0200 25 R-0570-130101 30.1 *0.0202
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13094.6 6.640.0189
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13091.2 3.980.0182
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13089.7 5.030.0179
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130112 7.790.0224
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130107 8.980.0215
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13091.0 2.500.0182
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13090.5 6.830.0181
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13086.9 6.570.0174
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13093.1 1.620.0186
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 2540-160125 24.70.0250
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13098.1 17.50.0196
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130106 5.960.0212
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-13093.9 7.400.0188
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13092.6 6.700.0185
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13095.0 8.560.0190
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13098.8 8.060.0198
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-130103 1.730.0206
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13078.4 2.020.0157
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13089.8 9.640.0180
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13099.4 2.960.0199
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13099.0 8.420.0198
Diethyl Ether mg/Kg wet0.020 0.0200 2570-130109 16.10.0218
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-13092.7 23.10.0185
Page 48 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253342 - SW-846 5035
LCS Dup (B253342-BSD1) Prepared & Analyzed: 03/02/20
1,4-Dioxane mg/Kg wet0.10 0.200 5040-160120 17.10.241
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-13088.8 9.340.0178
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-16084.5 19.80.0169
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-16099.7 18.30.199
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-13099.6 14.10.0199
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13083.8 6.580.0168
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-130104 13.60.0208
Methylene Chloride mg/Kg wet0.020 0.0200 25 J40-16099.0 2.590.0198
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 25 V-0570-16099.8 14.50.200
Naphthalene mg/Kg wet0.0040 0.0200 2540-13071.8 12.50.0144
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-13087.4 12.60.0175
Styrene mg/Kg wet0.0020 0.0200 2570-130100 10.60.0200
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 25 V-2070-130106 11.20.0212
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-130104 1.940.0208
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130103 0.5830.0205
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-130113 0.9660.0227
Toluene mg/Kg wet0.0020 0.0200 2570-13096.5 1.570.0193
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13081.9 11.90.0164
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13077.8 21.60.0156
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13083.3 10.60.0167
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13090.8 8.860.0182
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130104 9.470.0208
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-13096.6 11.70.0193
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-130102 3.390.0204
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130110 4.360.0220
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 25 V-2070-130103 0.2920.0206
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13077.7 5.990.0155
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13091.6 10.20.0183
Vinyl Chloride mg/Kg wet0.010 0.0200 25 R-0540-130108 30.5 *0.0217
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13092.8 7.820.0371
o-Xylene mg/Kg wet0.0020 0.0200 2570-13090.5 9.170.0181
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 83.40.0417
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 97.40.0487
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1050.0525
Batch B253398 - SW-846 5030B
[TOC_3]B253398[TOC]
Blank (B253398-BLK1) Prepared: 03/03/20 Analyzed: 03/04/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Page 49 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253398 - SW-846 5030B
Blank (B253398-BLK1) Prepared: 03/03/20 Analyzed: 03/04/20
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50 L-04ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 87.621.9
g/L 25.0 70-130Surrogate: Toluene-d8 94.023.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 89.722.4
Page 50 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253398 - SW-846 5030B
LCS (B253398-BS1) Prepared: 03/03/20 Analyzed: 03/04/20
Acetone g/L50 100 70-13091.891.8
Benzene g/L0.50 10.0 70-13085.88.58
Bromobenzene g/L0.50 10.0 70-13010210.2
Bromochloromethane g/L0.50 10.0 70-13096.89.68
Bromodichloromethane g/L0.50 10.0 70-13010510.5
Bromoform g/L0.50 10.0 70-13010410.4
Bromomethane g/L1.0 10.0 60-14066.26.62
2-Butanone (MEK)g/L5.0 100 70-13082.582.5
n-Butylbenzene g/L0.50 10.0 70-13010810.8
sec-Butylbenzene g/L0.50 10.0 70-13011111.1
tert-Butylbenzene g/L0.50 10.0 70-13011011.0
Carbon Tetrachloride g/L0.50 10.0 70-13010510.5
Chlorobenzene g/L0.50 10.0 70-13010410.4
Ethanol g/L50 100 70-130117117
Chlorodibromomethane g/L0.50 10.0 70-13099.19.91
Chloroethane g/L0.50 10.0 60-14089.48.94
Chloroform g/L0.50 10.0 70-13087.28.72
Chloromethane g/L0.60 10.0 60-14087.28.72
2-Chlorotoluene g/L0.50 10.0 70-13099.49.94
4-Chlorotoluene g/L0.50 10.0 70-13010810.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13095.49.54
1,2-Dichlorobenzene g/L0.50 10.0 70-13010710.7
1,3-Dichlorobenzene g/L0.50 10.0 70-13011111.1
1,4-Dichlorobenzene g/L0.50 10.0 70-13010810.8
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14088.58.85
1,1-Dichloroethane g/L0.50 10.0 70-13094.79.47
1,2-Dichloroethane g/L0.50 10.0 70-13010510.5
1,1-Dichloroethylene g/L0.50 10.0 70-13010110.1
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13094.29.42
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13098.89.88
1,2-Dichloropropane g/L0.50 10.0 70-13099.19.91
1,3-Dichloropropane g/L0.50 10.0 70-13092.39.23
2,2-Dichloropropane g/L0.50 10.0 70-13093.19.31
1,1-Dichloropropene g/L0.50 10.0 70-13092.19.21
cis-1,3-Dichloropropene g/L0.50 10.0 70-13099.19.91
trans-1,3-Dichloropropene g/L0.50 10.0 70-13095.99.59
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010610.6
Ethylbenzene g/L0.50 10.0 70-13010810.8
2-Hexanone (MBK)g/L5.0 100 70-130102102
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011111.1
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010810.8
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 L-0470-13067.1 *6.71
Methylene Chloride g/L5.0 10.0 70-13096.89.68
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130109109
Naphthalene g/L0.50 10.0 70-13010710.7
n-Propylbenzene g/L0.50 10.0 70-13010610.6
Styrene g/L0.50 10.0 70-13010310.3
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13098.69.86
Tetrachloroethylene g/L0.50 10.0 70-13010810.8
Toluene g/L0.50 10.0 70-13010210.2
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13011611.6
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13011811.8
Page 51 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253398 - SW-846 5030B
LCS (B253398-BS1) Prepared: 03/03/20 Analyzed: 03/04/20
1,1,1-Trichloroethane g/L0.50 10.0 70-13010210.2
1,1,2-Trichloroethane g/L0.50 10.0 70-13094.79.47
Trichloroethylene g/L0.50 10.0 70-13099.39.93
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13097.39.73
1,2,3-Trichloropropane g/L0.50 10.0 70-13095.89.58
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010310.3
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010410.4
Vinyl Acetate g/L20 100 70-13070.370.3
Vinyl Chloride g/L0.50 10.0 L-0260-140288*28.8
m+p Xylene g/L1.0 20.0 70-13010821.6
o-Xylene g/L0.50 10.0 70-13010910.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 94.023.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.524.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.423.6
LCS Dup (B253398-BSD1) Prepared: 03/03/20 Analyzed: 03/04/20
Acetone g/L50 100 2570-13089.8 2.2589.8
Benzene g/L0.50 10.0 2570-13084.4 1.658.44
Bromobenzene g/L0.50 10.0 2570-130101 1.4810.1
Bromochloromethane g/L0.50 10.0 2570-13093.0 4.009.30
Bromodichloromethane g/L0.50 10.0 2570-130100 4.7710.0
Bromoform g/L0.50 10.0 2570-130102 1.4510.2
Bromomethane g/L1.0 10.0 2560-14071.8 8.127.18
2-Butanone (MEK)g/L5.0 100 2570-13076.8 7.2176.8
n-Butylbenzene g/L0.50 10.0 2570-130108 0.92610.8
sec-Butylbenzene g/L0.50 10.0 2570-130111 0.45011.1
tert-Butylbenzene g/L0.50 10.0 2570-130110 0.090811.0
Carbon Tetrachloride g/L0.50 10.0 2570-130101 4.4610.1
Chlorobenzene g/L0.50 10.0 2570-130103 0.87210.3
Ethanol g/L50 100 2570-130119 1.31119
Chlorodibromomethane g/L0.50 10.0 2570-13096.0 3.189.60
Chloroethane g/L0.50 10.0 2560-14090.7 1.449.07
Chloroform g/L0.50 10.0 2570-13086.3 1.048.63
Chloromethane g/L0.60 10.0 2560-14076.8 12.77.68
2-Chlorotoluene g/L0.50 10.0 2570-13094.2 5.379.42
4-Chlorotoluene g/L0.50 10.0 2570-130101 6.0410.1
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13092.0 3.639.20
1,2-Dichlorobenzene g/L0.50 10.0 2570-130107 0.37410.7
1,3-Dichlorobenzene g/L0.50 10.0 2570-130108 2.1910.8
1,4-Dichlorobenzene g/L0.50 10.0 2570-130107 0.46510.7
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14084.4 4.748.44
1,1-Dichloroethane g/L0.50 10.0 2570-13092.4 2.469.24
1,2-Dichloroethane g/L0.50 10.0 2570-13098.9 5.709.89
1,1-Dichloroethylene g/L0.50 10.0 2570-13097.3 3.939.73
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13092.4 1.939.24
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13098.0 0.8139.80
1,2-Dichloropropane g/L0.50 10.0 2570-13097.8 1.329.78
1,3-Dichloropropane g/L0.50 10.0 2570-13088.9 3.758.89
2,2-Dichloropropane g/L0.50 10.0 2570-13086.9 6.898.69
1,1-Dichloropropene g/L0.50 10.0 2570-13090.8 1.429.08
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13094.7 4.549.47
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13092.2 3.939.22
Page 52 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253398 - SW-846 5030B
LCS Dup (B253398-BSD1) Prepared: 03/03/20 Analyzed: 03/04/20
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130104 2.0010.4
Ethylbenzene g/L0.50 10.0 2570-130103 4.6510.3
2-Hexanone (MBK)g/L5.0 100 2570-13097.0 4.6597.0
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130107 3.3910.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130108 0.27910.8
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 25 L-0470-13062.0 7.90*6.20
Methylene Chloride g/L5.0 10.0 2570-13095.6 1.259.56
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130104 4.77104
Naphthalene g/L0.50 10.0 2570-130106 0.84410.6
n-Propylbenzene g/L0.50 10.0 2570-130103 3.3510.3
Styrene g/L0.50 10.0 2570-13098.5 4.179.85
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13095.3 3.409.53
Tetrachloroethylene g/L0.50 10.0 2570-130109 0.92310.9
Toluene g/L0.50 10.0 2570-13098.9 2.999.89
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130120 3.3012.0
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130118 0.33911.8
1,1,1-Trichloroethane g/L0.50 10.0 2570-13099.7 1.899.97
1,1,2-Trichloroethane g/L0.50 10.0 2570-13093.7 1.069.37
Trichloroethylene g/L0.50 10.0 2570-13097.4 1.939.74
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13093.0 4.529.30
1,2,3-Trichloropropane g/L0.50 10.0 2570-13092.3 3.729.23
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130102 1.6610.2
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130104 0.095710.4
Vinyl Acetate g/L20 100 25 L-0770-13065.2 7.53*65.2
Vinyl Chloride g/L0.50 10.0 25 L-0260-140272 5.93*27.2
m+p Xylene g/L1.0 20.0 2570-130105 2.9220.9
o-Xylene g/L0.50 10.0 2570-130106 2.6110.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 92.423.1
g/L 25.0 70-130Surrogate: Toluene-d8 97.024.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 92.823.2
Batch B253562 - SW-846 5030B
[TOC_3]B253562[TOC]
Blank (B253562-BLK1) Prepared & Analyzed: 03/05/20
Benzene g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.924.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 90.822.7
LCS (B253562-BS1) Prepared & Analyzed: 03/05/20
Benzene g/L0.50 10.0 70-13010210.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010010.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10325.8
g/L 25.0 70-130Surrogate: Toluene-d8 10025.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.524.1
Page 53 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253562 - SW-846 5030B
LCS Dup (B253562-BSD1) Prepared & Analyzed: 03/05/20
Benzene g/L0.50 10.0 2570-130102 0.0010.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130106 6.3010.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10325.8
g/L 25.0 70-130Surrogate: Toluene-d8 99.124.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.424.3
Page 54 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B253574 - SW-846 3546
[TOC_3]B253574[TOC]
Blank (B253574-BLK1) Prepared & Analyzed: 03/05/20
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-05ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-05, V-35, V-04ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0 V-20ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66 V-20ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 55 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253574 - SW-846 3546
Blank (B253574-BLK1) Prepared & Analyzed: 03/05/20
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.64 30-130Surrogate: 2-Fluorophenol 74.34.93
mg/Kg wet 6.64 30-130Surrogate: Phenol-d6 78.75.23
mg/Kg wet 3.32 30-130Surrogate: Nitrobenzene-d5 63.72.12
mg/Kg wet 3.32 30-130Surrogate: 2-Fluorobiphenyl 82.52.74
mg/Kg wet 6.64 30-130Surrogate: 2,4,6-Tribromophenol 68.74.56
mg/Kg wet 3.32 30-130Surrogate: p-Terphenyl-d14 81.22.70
LCS (B253574-BS1) Prepared & Analyzed: 03/05/20
Acenaphthene mg/Kg wet0.17 1.66 40-14065.41.09
Acenaphthylene mg/Kg wet0.17 1.66 40-14064.91.08
Acetophenone mg/Kg wet0.34 1.66 40-14064.01.06
Aniline mg/Kg wet0.34 1.66 V-0510-14057.70.959
Anthracene mg/Kg wet0.17 1.66 40-14070.91.18
Benzidine mg/Kg wet0.66 1.66 V-04, V-05, V-3540-1401071.78
Benzo(a)anthracene mg/Kg wet0.17 1.66 40-14070.11.16
Benzo(a)pyrene mg/Kg wet0.17 1.66 40-14070.01.16
Benzo(b)fluoranthene mg/Kg wet0.17 1.66 40-14069.41.15
Benzo(g,h,i)perylene mg/Kg wet0.17 1.66 40-14057.50.955
Benzo(k)fluoranthene mg/Kg wet0.17 1.66 40-14070.71.17
Benzoic Acid mg/Kg wet1.0 1.66 V-0630-13069.11.15
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.66 40-14068.91.14
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.66 40-14070.21.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.66 40-14085.91.43
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.66 40-14070.31.17
4-Bromophenylphenylether mg/Kg wet0.34 1.66 40-14067.01.11
Butylbenzylphthalate mg/Kg wet0.34 1.66 40-14074.01.23
Carbazole mg/Kg wet0.17 1.66 40-14068.21.13
4-Chloroaniline mg/Kg wet0.66 1.66 V-3410-14042.80.711
4-Chloro-3-methylphenol mg/Kg wet0.66 1.66 30-13069.71.16
2-Chloronaphthalene mg/Kg wet0.34 1.66 40-14060.91.01
Page 56 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253574 - SW-846 3546
LCS (B253574-BS1) Prepared & Analyzed: 03/05/20
2-Chlorophenol mg/Kg wet0.34 1.66 30-13068.41.14
4-Chlorophenylphenylether mg/Kg wet0.34 1.66 40-14064.91.08
Chrysene mg/Kg wet0.17 1.66 40-14068.31.13
Dibenz(a,h)anthracene mg/Kg wet0.17 1.66 40-14062.61.04
Dibenzofuran mg/Kg wet0.34 1.66 40-14070.01.16
Di-n-butylphthalate mg/Kg wet0.34 1.66 40-14069.61.16
1,2-Dichlorobenzene mg/Kg wet0.34 1.66 40-14060.00.997
1,3-Dichlorobenzene mg/Kg wet0.34 1.66 40-14058.70.975
1,4-Dichlorobenzene mg/Kg wet0.34 1.66 40-14059.00.980
3,3-Dichlorobenzidine mg/Kg wet0.17 1.66 20-14052.90.878
2,4-Dichlorophenol mg/Kg wet0.34 1.66 30-13069.51.15
Diethylphthalate mg/Kg wet0.34 1.66 40-14065.01.08
2,4-Dimethylphenol mg/Kg wet0.34 1.66 30-13067.51.12
Dimethylphthalate mg/Kg wet0.34 1.66 40-14065.61.09
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.66 30-13069.11.15
2,4-Dinitrophenol mg/Kg wet0.66 1.66 V-0630-13058.90.978
2,4-Dinitrotoluene mg/Kg wet0.34 1.66 40-14073.01.21
2,6-Dinitrotoluene mg/Kg wet0.34 1.66 40-14077.11.28
Di-n-octylphthalate mg/Kg wet0.34 1.66 40-14071.61.19
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.66 40-14072.11.20
Fluoranthene mg/Kg wet0.17 1.66 40-14068.61.14
Fluorene mg/Kg wet0.17 1.66 40-14067.81.13
Hexachlorobenzene mg/Kg wet0.34 1.66 40-14065.51.09
Hexachlorobutadiene mg/Kg wet0.34 1.66 40-14055.60.923
Hexachlorocyclopentadiene mg/Kg wet0.34 1.66 40-14051.30.852
Hexachloroethane mg/Kg wet0.34 1.66 40-14058.10.966
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.66 40-14068.61.14
Isophorone mg/Kg wet0.34 1.66 40-14070.71.17
1-Methylnaphthalene mg/Kg wet0.17 1.66 40-14063.41.05
2-Methylnaphthalene mg/Kg wet0.17 1.66 40-14073.41.22
2-Methylphenol mg/Kg wet0.34 1.66 30-13068.61.14
3/4-Methylphenol mg/Kg wet0.34 1.66 30-13070.61.17
Naphthalene mg/Kg wet0.17 1.66 40-14065.81.09
2-Nitroaniline mg/Kg wet0.34 1.66 40-14091.51.52
3-Nitroaniline mg/Kg wet0.34 1.66 30-14062.81.04
4-Nitroaniline mg/Kg wet0.34 1.66 40-14071.91.20
Nitrobenzene mg/Kg wet0.34 1.66 40-14066.21.10
2-Nitrophenol mg/Kg wet0.34 1.66 30-13073.21.22
4-Nitrophenol mg/Kg wet0.66 1.66 30-13066.21.10
N-Nitrosodimethylamine mg/Kg wet0.34 1.66 40-14057.40.954
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.66 40-14072.31.20
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.66 40-14067.91.13
Pentachloronitrobenzene mg/Kg wet0.34 1.66 40-14073.41.22
Pentachlorophenol mg/Kg wet0.34 1.66 30-13058.50.972
Phenanthrene mg/Kg wet0.17 1.66 40-14071.81.19
Phenol mg/Kg wet0.34 1.66 30-13069.21.15
Pyrene mg/Kg wet0.17 1.66 40-14076.11.26
Pyridine mg/Kg wet0.34 1.66 30-14044.10.732
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.66 40-14060.81.01
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.66 40-14060.81.01
2,4,5-Trichlorophenol mg/Kg wet0.34 1.66 30-13070.01.16
2,4,6-Trichlorophenol mg/Kg wet0.34 1.66 30-13068.61.14
Page 57 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253574 - SW-846 3546
LCS (B253574-BS1) Prepared & Analyzed: 03/05/20
mg/Kg wet 6.64 30-130Surrogate: 2-Fluorophenol 74.74.96
mg/Kg wet 6.64 30-130Surrogate: Phenol-d6 79.25.26
mg/Kg wet 3.32 30-130Surrogate: Nitrobenzene-d5 67.32.23
mg/Kg wet 3.32 30-130Surrogate: 2-Fluorobiphenyl 85.22.83
mg/Kg wet 6.64 30-130Surrogate: 2,4,6-Tribromophenol 72.94.84
mg/Kg wet 3.32 30-130Surrogate: p-Terphenyl-d14 80.82.69
LCS Dup (B253574-BSD1) Prepared & Analyzed: 03/05/20
Acenaphthene mg/Kg wet0.17 1.66 3040-14070.3 6.921.16
Acenaphthylene mg/Kg wet0.17 1.66 3040-14070.0 7.111.16
Acetophenone mg/Kg wet0.34 1.66 3040-14068.4 6.411.13
Aniline mg/Kg wet0.34 1.66 50 V-0510-14063.1 8.511.04
Anthracene mg/Kg wet0.17 1.66 3040-14076.0 6.691.26
Benzidine mg/Kg wet0.66 1.66 30 V-05, V-35, V-0440-140122 12.72.02
Benzo(a)anthracene mg/Kg wet0.17 1.66 3040-14075.1 6.531.24
Benzo(a)pyrene mg/Kg wet0.17 1.66 3040-14075.6 7.361.25
Benzo(b)fluoranthene mg/Kg wet0.17 1.66 3040-14074.6 6.891.24
Benzo(g,h,i)perylene mg/Kg wet0.17 1.66 3040-14064.7 11.41.07
Benzo(k)fluoranthene mg/Kg wet0.17 1.66 3040-14076.4 7.471.27
Benzoic Acid mg/Kg wet0.99 1.66 50 V-0630-13081.7 16.41.35
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.66 3040-14077.5 11.41.28
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.66 3040-14074.0 4.861.22
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.66 3040-14091.4 5.921.51
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.66 3040-14075.0 6.051.24
4-Bromophenylphenylether mg/Kg wet0.34 1.66 3040-14074.6 10.51.24
Butylbenzylphthalate mg/Kg wet0.34 1.66 3040-14078.9 6.111.31
Carbazole mg/Kg wet0.17 1.66 3040-14073.3 6.851.21
4-Chloroaniline mg/Kg wet0.66 1.66 30 V-3410-14045.4 5.610.752
4-Chloro-3-methylphenol mg/Kg wet0.66 1.66 3030-13076.2 8.551.26
2-Chloronaphthalene mg/Kg wet0.34 1.66 3040-14064.8 5.901.07
2-Chlorophenol mg/Kg wet0.34 1.66 3030-13074.2 7.751.23
4-Chlorophenylphenylether mg/Kg wet0.34 1.66 3040-14071.3 9.131.18
Chrysene mg/Kg wet0.17 1.66 3040-14072.2 5.251.20
Dibenz(a,h)anthracene mg/Kg wet0.17 1.66 3040-14069.2 9.591.15
Dibenzofuran mg/Kg wet0.34 1.66 3040-14075.2 6.721.24
Di-n-butylphthalate mg/Kg wet0.34 1.66 3040-14074.7 6.741.24
1,2-Dichlorobenzene mg/Kg wet0.34 1.66 3040-14063.7 5.621.05
1,3-Dichlorobenzene mg/Kg wet0.34 1.66 3040-14062.6 6.031.04
1,4-Dichlorobenzene mg/Kg wet0.34 1.66 3040-14062.7 5.721.04
3,3-Dichlorobenzidine mg/Kg wet0.17 1.66 5020-14057.2 7.490.946
2,4-Dichlorophenol mg/Kg wet0.34 1.66 3030-13076.6 9.331.27
Diethylphthalate mg/Kg wet0.34 1.66 3040-14071.5 9.221.18
2,4-Dimethylphenol mg/Kg wet0.34 1.66 3030-13074.0 8.861.23
Dimethylphthalate mg/Kg wet0.34 1.66 3040-14071.4 8.141.18
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.66 3030-13072.7 4.661.20
2,4-Dinitrophenol mg/Kg wet0.66 1.66 30 V-0630-13056.6 4.280.937
2,4-Dinitrotoluene mg/Kg wet0.34 1.66 3040-14079.0 7.541.31
2,6-Dinitrotoluene mg/Kg wet0.34 1.66 3040-14084.3 8.641.40
Di-n-octylphthalate mg/Kg wet0.34 1.66 3040-14077.5 7.531.28
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.66 3040-14080.0 10.11.33
Fluoranthene mg/Kg wet0.17 1.66 3040-14072.4 5.081.20
Fluorene mg/Kg wet0.17 1.66 3040-14072.5 6.431.20
Page 58 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253574 - SW-846 3546
LCS Dup (B253574-BSD1) Prepared & Analyzed: 03/05/20
Hexachlorobenzene mg/Kg wet0.34 1.66 3040-14070.9 7.611.17
Hexachlorobutadiene mg/Kg wet0.34 1.66 3040-14060.9 8.871.01
Hexachlorocyclopentadiene mg/Kg wet0.34 1.66 3040-14057.9 11.70.958
Hexachloroethane mg/Kg wet0.34 1.66 3040-14063.1 7.821.04
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.66 3040-14074.6 8.081.23
Isophorone mg/Kg wet0.34 1.66 3040-14075.5 6.291.25
1-Methylnaphthalene mg/Kg wet0.17 1.66 3040-14068.8 7.841.14
2-Methylnaphthalene mg/Kg wet0.17 1.66 3040-14079.5 7.641.32
2-Methylphenol mg/Kg wet0.34 1.66 3030-13074.0 7.241.23
3/4-Methylphenol mg/Kg wet0.34 1.66 3030-13075.9 6.931.26
Naphthalene mg/Kg wet0.17 1.66 3040-14069.8 5.571.16
2-Nitroaniline mg/Kg wet0.34 1.66 3040-14097.4 5.921.61
3-Nitroaniline mg/Kg wet0.34 1.66 3030-14066.7 5.691.10
4-Nitroaniline mg/Kg wet0.34 1.66 3040-14075.3 4.181.25
Nitrobenzene mg/Kg wet0.34 1.66 3040-14071.2 7.061.18
2-Nitrophenol mg/Kg wet0.34 1.66 3030-13079.5 7.891.32
4-Nitrophenol mg/Kg wet0.66 1.66 5030-13070.7 6.331.17
N-Nitrosodimethylamine mg/Kg wet0.34 1.66 3040-14063.0 8.941.04
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.66 3040-14078.7 8.041.30
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.66 3040-14072.9 6.771.21
Pentachloronitrobenzene mg/Kg wet0.34 1.66 3040-14074.4 1.021.23
Pentachlorophenol mg/Kg wet0.34 1.66 3030-13064.6 9.481.07
Phenanthrene mg/Kg wet0.17 1.66 3040-14075.8 5.121.25
Phenol mg/Kg wet0.34 1.66 3030-13075.8 8.831.26
Pyrene mg/Kg wet0.17 1.66 3040-14082.0 7.211.36
Pyridine mg/Kg wet0.34 1.66 3030-14047.3 6.850.784
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.66 3040-14066.7 8.861.10
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.66 3040-14066.7 8.901.10
2,4,5-Trichlorophenol mg/Kg wet0.34 1.66 3030-13076.4 8.471.27
2,4,6-Trichlorophenol mg/Kg wet0.34 1.66 3030-13074.3 7.561.23
mg/Kg wet 6.62 30-130Surrogate: 2-Fluorophenol 80.15.30
mg/Kg wet 6.62 30-130Surrogate: Phenol-d6 85.05.63
mg/Kg wet 3.31 30-130Surrogate: Nitrobenzene-d5 71.72.38
mg/Kg wet 3.31 30-130Surrogate: 2-Fluorobiphenyl 91.23.02
mg/Kg wet 6.62 30-130Surrogate: 2,4,6-Tribromophenol 77.85.16
mg/Kg wet 3.31 30-130Surrogate: p-Terphenyl-d14 86.42.86
Page 59 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by - GC/MS[TOC]
Batch B253589 - SW-846 3510C
[TOC_3]B253589[TOC]
Blank (B253589-BLK1) Prepared: 03/05/20 Analyzed: 03/06/20
Acenaphthene g/L5.00ND
Acenaphthylene g/L5.00ND
Anthracene g/L5.00ND
Benzidine g/L20.0 V-04, V-05ND
Benzo(a)anthracene g/L5.00ND
Benzo(a)pyrene g/L5.00ND
Benzo(b)fluoranthene g/L5.00ND
Benzo(g,h,i)perylene g/L5.00ND
Benzo(k)fluoranthene g/L5.00ND
4-Bromophenylphenylether g/L10.0ND
Butylbenzylphthalate g/L10.0ND
4-Chloro-3-methylphenol g/L10.0ND
Bis(2-chloroethoxy)methane g/L10.0ND
Bis(2-chloroethyl)ether g/L10.0ND
Bis(2-chloroisopropyl)ether g/L10.0ND
2-Chloronaphthalene g/L10.0ND
2-Chlorophenol g/L10.0ND
4-Chlorophenylphenylether g/L10.0ND
Chrysene g/L5.00ND
Dibenz(a,h)anthracene g/L5.00ND
Di-n-butylphthalate g/L10.0ND
1,3-Dichlorobenzene g/L5.00ND
1,4-Dichlorobenzene g/L5.00ND
1,2-Dichlorobenzene g/L5.00ND
3,3-Dichlorobenzidine g/L10.0ND
2,4-Dichlorophenol g/L10.0ND
Diethylphthalate g/L10.0ND
2,4-Dimethylphenol g/L10.0ND
Dimethylphthalate g/L10.0ND
4,6-Dinitro-2-methylphenol g/L10.0ND
2,4-Dinitrophenol g/L10.0ND
2,4-Dinitrotoluene g/L10.0ND
2,6-Dinitrotoluene g/L10.0ND
Di-n-octylphthalate g/L10.0ND
1,2-Diphenylhydrazine/Azobenzene g/L10.0ND
Bis(2-Ethylhexyl)phthalate g/L10.0ND
Fluoranthene g/L5.00ND
Fluorene g/L5.00ND
Hexachlorobenzene g/L10.0ND
Hexachlorobutadiene g/L10.0ND
Hexachlorocyclopentadiene g/L10.0 L-04, V-05ND
Hexachloroethane g/L10.0ND
Indeno(1,2,3-cd)pyrene g/L5.00ND
Isophorone g/L10.0ND
Naphthalene g/L5.00ND
Nitrobenzene g/L10.0ND
2-Nitrophenol g/L10.0ND
4-Nitrophenol g/L10.0ND
N-Nitrosodimethylamine g/L10.0 V-20ND
N-Nitrosodiphenylamine/Diphenylamine g/L10.0ND
N-Nitrosodi-n-propylamine g/L10.0ND
Pentachlorophenol g/L10.0ND
Page 60 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
Blank (B253589-BLK1) Prepared: 03/05/20 Analyzed: 03/06/20
2-Methylnaphthalene g/L5.00ND
Phenanthrene g/L5.00ND
2-Methylphenol g/L10.0ND
Phenol g/L10.0ND
3/4-Methylphenol g/L20.0ND
Pyrene g/L5.00ND
1,2,4-Trichlorobenzene g/L5.00ND
2,4,6-Trichlorophenol g/L10.0ND
g/L 200 15-110Surrogate: 2-Fluorophenol 53.0106
g/L 200 15-110Surrogate: Phenol-d6 40.781.4
g/L 100 30-130Surrogate: Nitrobenzene-d5 82.282.2
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 96.996.9
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 80.5161
g/L 100 30-130Surrogate: p-Terphenyl-d14 79.279.2
LCS (B253589-BS1) Prepared: 03/05/20 Analyzed: 03/06/20
Acenaphthene g/L5.00 50.0 47-14572.736.4
Acenaphthylene g/L5.00 50.0 33-14575.637.8
Anthracene g/L5.00 50.0 27-13381.140.6
Benzidine g/L20.0 50.0 V-04, V-0540-14072.036.0
Benzo(a)anthracene g/L5.00 50.0 33-14381.540.8
Benzo(a)pyrene g/L5.00 50.0 17-16377.138.6
Benzo(b)fluoranthene g/L5.00 50.0 24-15980.740.3
Benzo(g,h,i)perylene g/L5.00 50.0 10-21975.137.6
Benzo(k)fluoranthene g/L5.00 50.0 11-16280.240.1
4-Bromophenylphenylether g/L10.0 50.0 53-12777.638.8
Butylbenzylphthalate g/L10.0 50.0 10-15273.636.8
4-Chloro-3-methylphenol g/L10.0 50.0 22-14782.241.1
Bis(2-chloroethoxy)methane g/L10.0 50.0 33-18476.938.4
Bis(2-chloroethyl)ether g/L10.0 50.0 12-15874.137.0
Bis(2-chloroisopropyl)ether g/L10.0 50.0 36-16687.243.6
2-Chloronaphthalene g/L10.0 50.0 60-12067.033.5
2-Chlorophenol g/L10.0 50.0 23-13468.134.0
4-Chlorophenylphenylether g/L10.0 50.0 25-15879.639.8
Chrysene g/L5.00 50.0 17-16881.140.5
Dibenz(a,h)anthracene g/L5.00 50.0 10-22774.237.1
Di-n-butylphthalate g/L10.0 50.0 10-12080.040.0
1,3-Dichlorobenzene g/L5.00 50.0 10-17258.129.0
1,4-Dichlorobenzene g/L5.00 50.0 20-12460.630.3
1,2-Dichlorobenzene g/L5.00 50.0 32-12960.930.5
3,3-Dichlorobenzidine g/L10.0 50.0 10-26297.148.6
2,4-Dichlorophenol g/L10.0 50.0 39-13577.138.5
Diethylphthalate g/L10.0 50.0 10-12077.238.6
2,4-Dimethylphenol g/L10.0 50.0 32-12073.536.7
Dimethylphthalate g/L10.0 50.0 10-12078.039.0
4,6-Dinitro-2-methylphenol g/L10.0 50.0 10-18175.837.9
2,4-Dinitrophenol g/L10.0 50.0 10-19172.536.2
2,4-Dinitrotoluene g/L10.0 50.0 39-13987.443.7
2,6-Dinitrotoluene g/L10.0 50.0 50-15886.543.2
Di-n-octylphthalate g/L10.0 50.0 4-14676.238.1
1,2-Diphenylhydrazine/Azobenzene g/L10.0 50.0 40-14078.039.0
Bis(2-Ethylhexyl)phthalate g/L10.0 50.0 8-15876.438.2
Page 61 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
LCS (B253589-BS1) Prepared: 03/05/20 Analyzed: 03/06/20
Fluoranthene g/L5.00 50.0 26-13788.244.1
Fluorene g/L5.00 50.0 59-12181.140.6
Hexachlorobenzene g/L10.0 50.0 10-15278.639.3
Hexachlorobutadiene g/L10.0 50.0 24-12065.933.0
Hexachlorocyclopentadiene g/L10.0 50.0 V-05, L-0440-14039.0 *19.5
Hexachloroethane g/L10.0 50.0 40-12058.529.2
Indeno(1,2,3-cd)pyrene g/L5.00 50.0 10-17182.441.2
Isophorone g/L10.0 50.0 21-19684.142.0
Naphthalene g/L5.00 50.0 21-13371.335.6
Nitrobenzene g/L10.0 50.0 35-18076.438.2
2-Nitrophenol g/L10.0 50.0 29-18279.940.0
4-Nitrophenol g/L10.0 50.0 10-13239.619.8
N-Nitrosodimethylamine g/L10.0 50.0 V-0640-14057.628.8
N-Nitrosodiphenylamine/Diphenylamine g/L10.0 50.0 40-14082.241.1
N-Nitrosodi-n-propylamine g/L10.0 50.0 10-23080.240.1
Pentachlorophenol g/L10.0 50.0 14-17667.133.6
2-Methylnaphthalene g/L5.00 50.0 40-14083.641.8
Phenanthrene g/L5.00 50.0 54-12080.740.4
2-Methylphenol g/L10.0 50.0 40-14065.532.8
Phenol g/L10.0 50.0 5-12033.816.9
3/4-Methylphenol g/L20.0 50.0 40-14067.733.9
Pyrene g/L5.00 50.0 52-12067.033.5
1,2,4-Trichlorobenzene g/L5.00 50.0 44-14267.033.5
2,4,6-Trichlorophenol g/L10.0 50.0 37-14475.637.8
g/L 200 15-110Surrogate: 2-Fluorophenol 52.4105
g/L 200 15-110Surrogate: Phenol-d6 40.681.2
g/L 100 30-130Surrogate: Nitrobenzene-d5 81.081.0
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 94.894.8
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 90.3181
g/L 100 30-130Surrogate: p-Terphenyl-d14 75.575.5
LCS Dup (B253589-BSD1) Prepared: 03/05/20 Analyzed: 03/06/20
Acenaphthene g/L5.00 50.0 4847-14565.3 10.832.6
Acenaphthylene g/L5.00 50.0 7433-14568.3 10.234.1
Anthracene g/L5.00 50.0 6627-13374.6 8.3737.3
Benzidine g/L20.0 50.0 30 V-04, V-0540-14054.3 28.027.2
Benzo(a)anthracene g/L5.00 50.0 5333-14372.8 11.336.4
Benzo(a)pyrene g/L5.00 50.0 7217-16370.5 8.9935.2
Benzo(b)fluoranthene g/L5.00 50.0 7124-15972.8 10.336.4
Benzo(g,h,i)perylene g/L5.00 50.0 9710-21968.4 9.3934.2
Benzo(k)fluoranthene g/L5.00 50.0 6311-16272.2 10.536.1
4-Bromophenylphenylether g/L10.0 50.0 4353-12775.2 3.0937.6
Butylbenzylphthalate g/L10.0 50.0 6010-15266.9 9.6233.4
4-Chloro-3-methylphenol g/L10.0 50.0 7322-14775.8 8.1837.9
Bis(2-chloroethoxy)methane g/L10.0 50.0 5433-18470.6 8.4335.3
Bis(2-chloroethyl)ether g/L10.0 50.0 10812-15870.6 4.8435.3
Bis(2-chloroisopropyl)ether g/L10.0 50.0 7636-16683.0 4.9841.5
2-Chloronaphthalene g/L10.0 50.0 24 L-0760-12059.6 11.6*29.8
2-Chlorophenol g/L10.0 50.0 6123-13464.7 5.0932.4
4-Chlorophenylphenylether g/L10.0 50.0 6125-15868.8 14.534.4
Chrysene g/L5.00 50.0 8717-16873.2 10.136.6
Dibenz(a,h)anthracene g/L5.00 50.0 12610-22767.1 10.033.6
Page 62 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
LCS Dup (B253589-BSD1) Prepared: 03/05/20 Analyzed: 03/06/20
Di-n-butylphthalate g/L10.0 50.0 4710-12073.9 7.9237.0
1,3-Dichlorobenzene g/L5.00 50.0 3010-17253.3 8.5526.7
1,4-Dichlorobenzene g/L5.00 50.0 3020-12454.6 10.327.3
1,2-Dichlorobenzene g/L5.00 50.0 3032-12955.4 9.4227.7
3,3-Dichlorobenzidine g/L10.0 50.0 10810-26287.6 10.343.8
2,4-Dichlorophenol g/L10.0 50.0 5039-13571.1 8.1335.5
Diethylphthalate g/L10.0 50.0 10010-12072.3 6.5036.2
2,4-Dimethylphenol g/L10.0 50.0 5832-12066.6 9.8833.3
Dimethylphthalate g/L10.0 50.0 18310-12071.0 9.3235.5
4,6-Dinitro-2-methylphenol g/L10.0 50.0 20310-18171.9 5.2836.0
2,4-Dinitrophenol g/L10.0 50.0 13210-19164.9 11.132.4
2,4-Dinitrotoluene g/L10.0 50.0 4239-13977.6 11.938.8
2,6-Dinitrotoluene g/L10.0 50.0 4850-15880.2 7.4940.1
Di-n-octylphthalate g/L10.0 50.0 694-14669.3 9.5134.7
1,2-Diphenylhydrazine/Azobenzene g/L10.0 50.0 3040-14075.2 3.6537.6
Bis(2-Ethylhexyl)phthalate g/L10.0 50.0 828-15869.6 9.3234.8
Fluoranthene g/L5.00 50.0 6626-13778.6 11.439.3
Fluorene g/L5.00 50.0 3859-12174.8 8.0537.4
Hexachlorobenzene g/L10.0 50.0 5510-15276.8 2.3738.4
Hexachlorobutadiene g/L10.0 50.0 6224-12057.0 14.628.5
Hexachlorocyclopentadiene g/L10.0 50.0 30 L-04, V-0540-14033.5 15.2*16.7
Hexachloroethane g/L10.0 50.0 5240-12052.3 11.226.1
Indeno(1,2,3-cd)pyrene g/L5.00 50.0 9910-17170.7 15.235.4
Isophorone g/L10.0 50.0 9321-19675.6 10.637.8
Naphthalene g/L5.00 50.0 6521-13363.0 12.331.5
Nitrobenzene g/L10.0 50.0 6235-18067.8 12.033.9
2-Nitrophenol g/L10.0 50.0 5529-18270.1 13.035.1
4-Nitrophenol g/L10.0 50.0 13110-13235.3 11.317.7
N-Nitrosodimethylamine g/L10.0 50.0 30 V-0640-14055.6 3.5327.8
N-Nitrosodiphenylamine/Diphenylamine g/L10.0 50.0 3040-14076.4 7.3238.2
N-Nitrosodi-n-propylamine g/L10.0 50.0 8710-23077.3 3.6638.6
Pentachlorophenol g/L10.0 50.0 8614-17659.6 11.929.8
2-Methylnaphthalene g/L5.00 50.0 3040-14074.3 11.737.2
Phenanthrene g/L5.00 50.0 3954-12074.0 8.6137.0
2-Methylphenol g/L10.0 50.0 3040-14062.8 4.2431.4
Phenol g/L10.0 50.0 645-12032.5 3.7416.3
3/4-Methylphenol g/L20.0 50.0 3040-14063.8 6.0231.9
Pyrene g/L5.00 50.0 4952-12062.2 7.5231.1
1,2,4-Trichlorobenzene g/L5.00 50.0 5044-14257.5 15.228.8
2,4,6-Trichlorophenol g/L10.0 50.0 5837-14469.6 8.2434.8
g/L 200 15-110Surrogate: 2-Fluorophenol 49.198.3
g/L 200 15-110Surrogate: Phenol-d6 38.677.2
g/L 100 30-130Surrogate: Nitrobenzene-d5 71.071.0
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 86.186.1
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 80.8162
g/L 100 30-130Surrogate: p-Terphenyl-d14 70.370.3
Page 63 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
Matrix Spike (B253589-MS1) Prepared: 03/05/20 Analyzed: 03/07/20 Source: 20B1278-07
Acenaphthene g/L10.0 100 47-14590.591.1 0.545
Acenaphthylene g/L10.0 100 33-14588.188.1 ND
Anthracene g/L10.0 100 27-13397.397.3 ND
Benzidine g/L40.0 100 V-04, V-05,
MS-09, J
40-140-0.475 *0.0200 0.495
Benzo(a)anthracene g/L10.0 100 33-14396.596.5 ND
Benzo(a)pyrene g/L10.0 100 17-16395.395.3 ND
Benzo(b)fluoranthene g/L10.0 100 24-15998.498.4 ND
Benzo(g,h,i)perylene g/L10.0 100 10-219121121ND
Benzo(k)fluoranthene g/L10.0 100 11-16299.999.9 ND
4-Bromophenylphenylether g/L20.0 100 53-12792.892.8 ND
Butylbenzylphthalate g/L20.0 100 10-152104104ND
4-Chloro-3-methylphenol g/L20.0 100 22-147105105ND
Bis(2-chloroethoxy)methane g/L20.0 100 33-184100100ND
Bis(2-chloroethyl)ether g/L20.0 100 12-15892.492.4 ND
Bis(2-chloroisopropyl)ether g/L20.0 100 36-16690.390.3 ND
2-Chloronaphthalene g/L20.0 100 60-12076.476.4 ND
2-Chlorophenol g/L20.0 100 23-13487.787.7 ND
4-Chlorophenylphenylether g/L20.0 100 25-15893.593.5 ND
Chrysene g/L10.0 100 17-16895.595.5 ND
Dibenz(a,h)anthracene g/L10.0 100 10-227115115ND
Di-n-butylphthalate g/L20.0 100 10-12099.299.2 ND
1,3-Dichlorobenzene g/L10.0 100 10-17276.976.9 ND
1,4-Dichlorobenzene g/L10.0 100 20-12477.577.5 ND
1,2-Dichlorobenzene g/L10.0 100 32-12979.079.0 ND
3,3-Dichlorobenzidine g/L20.0 100 V-3410-26257.757.7 ND
2,4-Dichlorophenol g/L20.0 100 39-135100100ND
Diethylphthalate g/L20.0 100 10-12084.494.8 10.4
2,4-Dimethylphenol g/L20.0 100 32-12095.995.9 ND
Dimethylphthalate g/L20.0 100 10-12091.691.6 ND
4,6-Dinitro-2-methylphenol g/L20.0 100 10-181109109ND
2,4-Dinitrophenol g/L20.0 100 V-0410-191131131ND
2,4-Dinitrotoluene g/L20.0 100 39-139111111ND
2,6-Dinitrotoluene g/L20.0 100 50-158108108ND
Di-n-octylphthalate g/L20.0 100 4-146128128ND
1,2-Diphenylhydrazine/Azobenzene g/L20.0 100 40-14092.992.9 ND
Bis(2-Ethylhexyl)phthalate g/L20.0 100 8-158104104ND
Fluoranthene g/L10.0 100 26-13798.998.9 ND
Fluorene g/L10.0 100 59-12194.496.4 2.01
Hexachlorobenzene g/L20.0 100 10-15294.294.2 ND
Hexachlorobutadiene g/L20.0 100 24-12090.190.1 ND
Hexachlorocyclopentadiene g/L20.0 100 40-14081.581.5 ND
Hexachloroethane g/L20.0 100 MS-2240-120123*123 ND
Indeno(1,2,3-cd)pyrene g/L10.0 100 10-171125125ND
Isophorone g/L20.0 100 21-196103103ND
Naphthalene g/L10.0 100 MS-2221-133200*411 211
Nitrobenzene g/L20.0 100 35-18098.898.8 ND
2-Nitrophenol g/L20.0 100 29-182113113ND
4-Nitrophenol g/L20.0 100 10-13283.283.2 ND
N-Nitrosodimethylamine g/L20.0 100 40-14061.461.4 ND
N-Nitrosodiphenylamine/Diphenylamine g/L20.0 100 40-14096.796.7 ND
N-Nitrosodi-n-propylamine g/L20.0 100 10-23092.692.6 ND
Pentachlorophenol g/L20.0 100 14-17697.697.6 ND
Page 64 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
Matrix Spike (B253589-MS1) Prepared: 03/05/20 Analyzed: 03/07/20 Source: 20B1278-07
2-Methylnaphthalene g/L10.0 100 MS-2340-140171*303 132
Phenanthrene g/L10.0 100 54-12097.497.4 ND
2-Methylphenol g/L20.0 100 40-14087.487.4 ND
Phenol g/L20.0 100 5-12059.759.7 ND
3/4-Methylphenol g/L40.0 100 40-14088.088.0 ND
Pyrene g/L10.0 100 52-12099.699.6 ND
1,2,4-Trichlorobenzene g/L10.0 100 44-14290.390.3 ND
2,4,6-Trichlorophenol g/L20.0 100 37-14492.192.1 ND
g/L 400 15-110Surrogate: 2-Fluorophenol 80.0320
g/L 400 15-110Surrogate: Phenol-d6 68.9276
g/L 200 30-130Surrogate: Nitrobenzene-d5 102205
g/L 200 30-130Surrogate: 2-Fluorobiphenyl 115231
g/L 400 MS-2215-110Surrogate: 2,4,6-Tribromophenol 113450 *
g/L 200 30-130Surrogate: p-Terphenyl-d14 112225
Matrix Spike Dup (B253589-MSD1) Prepared: 03/05/20 Analyzed: 03/07/20 Source: 20B1278-07
Acenaphthene g/L10.0 100 4847-14578.2 14.678.7 0.545
Acenaphthylene g/L10.0 100 7433-14576.9 13.676.9 ND
Anthracene g/L10.0 100 6627-13383.8 14.983.8 ND
Benzidine g/L40.0 100 30 MS-09, V-04,
V-05, J
40-1400.345 *0.840 0.495
Benzo(a)anthracene g/L10.0 100 5333-14383.3 14.883.3 ND
Benzo(a)pyrene g/L10.0 100 7217-16381.3 15.981.3 ND
Benzo(b)fluoranthene g/L10.0 100 7124-15983.6 16.383.6 ND
Benzo(g,h,i)perylene g/L10.0 100 9710-219103 16.5103ND
Benzo(k)fluoranthene g/L10.0 100 6311-16285.6 15.485.6 ND
4-Bromophenylphenylether g/L20.0 100 4353-12780.5 14.380.5 ND
Butylbenzylphthalate g/L20.0 100 6010-15288.9 15.388.9 ND
4-Chloro-3-methylphenol g/L20.0 100 7322-14785.8 19.985.8 ND
Bis(2-chloroethoxy)methane g/L20.0 100 5433-18483.9 17.583.9 ND
Bis(2-chloroethyl)ether g/L20.0 100 10812-15876.5 18.876.5 ND
Bis(2-chloroisopropyl)ether g/L20.0 100 7636-16675.7 17.575.7 ND
2-Chloronaphthalene g/L20.0 100 2460-12069.2 10.069.2 ND
2-Chlorophenol g/L20.0 100 6123-13474.3 16.674.3 ND
4-Chlorophenylphenylether g/L20.0 100 6125-15879.4 16.379.4 ND
Chrysene g/L10.0 100 8717-16882.5 14.782.5 ND
Dibenz(a,h)anthracene g/L10.0 100 12610-22797.3 16.697.3 ND
Di-n-butylphthalate g/L20.0 100 4710-12085.1 15.385.1 ND
1,3-Dichlorobenzene g/L10.0 100 3010-17265.9 15.465.9 ND
1,4-Dichlorobenzene g/L10.0 100 3020-12466.6 15.066.6 ND
1,2-Dichlorobenzene g/L10.0 100 3032-12968.2 14.668.2 ND
3,3-Dichlorobenzidine g/L20.0 100 108 V-3410-26255.0 4.6955.0 ND
2,4-Dichlorophenol g/L20.0 100 5039-13584.6 16.884.6 ND
Diethylphthalate g/L20.0 100 10010-12071.0 15.381.4 10.4
2,4-Dimethylphenol g/L20.0 100 5832-12081.0 16.881.0 ND
Dimethylphthalate g/L20.0 100 18310-12080.1 13.580.1 ND
4,6-Dinitro-2-methylphenol g/L20.0 100 20310-18197.6 11.297.6 ND
2,4-Dinitrophenol g/L20.0 100 132 V-0410-191112 15.7112ND
2,4-Dinitrotoluene g/L20.0 100 4239-13996.8 13.696.8 ND
2,6-Dinitrotoluene g/L20.0 100 4850-15894.5 13.394.5 ND
Di-n-octylphthalate g/L20.0 100 694-146108 16.7108ND
1,2-Diphenylhydrazine/Azobenzene g/L20.0 100 3040-14079.2 16.079.2 ND
Bis(2-Ethylhexyl)phthalate g/L20.0 100 828-15889.3 15.589.3 ND
Page 65 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by - GC/MS - Quality Control
QUALITY CONTROL
Batch B253589 - SW-846 3510C
Matrix Spike Dup (B253589-MSD1) Prepared: 03/05/20 Analyzed: 03/07/20 Source: 20B1278-07
Fluoranthene g/L10.0 100 6626-13784.7 15.584.7 ND
Fluorene g/L10.0 100 3859-12181.0 15.083.0 2.01
Hexachlorobenzene g/L20.0 100 5510-15280.8 15.380.8 ND
Hexachlorobutadiene g/L20.0 100 6224-12075.8 17.275.8 ND
Hexachlorocyclopentadiene g/L20.0 100 3040-14070.9 13.870.9 ND
Hexachloroethane g/L20.0 100 5240-12097.1 23.497.1 ND
Indeno(1,2,3-cd)pyrene g/L10.0 100 9910-171105 17.6105ND
Isophorone g/L20.0 100 9321-19685.7 18.685.7 ND
Naphthalene g/L10.0 100 6521-13386.5 32.2297211
Nitrobenzene g/L20.0 100 6235-18083.3 17.083.3 ND
2-Nitrophenol g/L20.0 100 5529-18296.4 15.596.4 ND
4-Nitrophenol g/L20.0 100 13110-13278.8 5.4878.8 ND
N-Nitrosodimethylamine g/L20.0 100 3040-14055.1 10.855.1 ND
N-Nitrosodiphenylamine/Diphenylamine g/L20.0 100 3040-14083.0 15.283.0 ND
N-Nitrosodi-n-propylamine g/L20.0 100 8710-23076.8 18.776.8 ND
Pentachlorophenol g/L20.0 100 8614-17682.9 16.382.9 ND
2-Methylnaphthalene g/L10.0 100 30 R-0640-14090.5 30.5 *223 132
Phenanthrene g/L10.0 100 3954-12083.4 15.583.4 ND
2-Methylphenol g/L20.0 100 3040-14074.4 16.174.4 ND
Phenol g/L20.0 100 645-12055.1 8.0555.1 ND
3/4-Methylphenol g/L40.0 100 3040-14074.6 16.574.6 ND
Pyrene g/L10.0 100 4952-12084.1 16.984.1 ND
1,2,4-Trichlorobenzene g/L10.0 100 5044-14276.7 16.376.7 ND
2,4,6-Trichlorophenol g/L20.0 100 5837-14480.5 13.380.5 ND
g/L 400 15-110Surrogate: 2-Fluorophenol 71.6286
g/L 400 15-110Surrogate: Phenol-d6 64.6258
g/L 200 30-130Surrogate: Nitrobenzene-d5 86.4173
g/L 200 30-130Surrogate: 2-Fluorobiphenyl 102203
g/L 400 15-110Surrogate: 2,4,6-Tribromophenol 97.2389
g/L 200 30-130Surrogate: p-Terphenyl-d14 95.4191
Page 66 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Tentatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED) - Quality Control
QUALITY CONTROL
entatively Identified Compounds - SV Compounds (ESTIMATED VALUES REPORTED)[TOC]
Batch B253589 - SW-846 3510C
[TOC_3]B253589[TOC]
Blank (B253589-BLK1) Prepared: 03/05/20 Analyzed: 03/06/20
No TICs Found g/L0.0
Page 67 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC[TOC]
Batch B253829 - Alcohol Prep
[TOC_3]B253829[TOC]
Blank (B253829-BLK1) Prepared & Analyzed: 03/09/20
Ethylene glycol mg/Kg wet10ND
LCS (B253829-BS1) Prepared & Analyzed: 03/09/20
Ethylene glycol mg/Kg wet10 100 40-140118118
LCS Dup (B253829-BSD1) Prepared & Analyzed: 03/09/20
Ethylene glycol mg/Kg wet10 100 5040-140130 9.71130
Duplicate (B253829-DUP1) Prepared & Analyzed: 03/09/20 Source: 20B1278-03
Ethylene glycol mg/Kg dry15 NCNDND
Matrix Spike (B253829-MS1) Prepared & Analyzed: 03/09/20 Source: 20B1278-03
Ethylene glycol mg/Kg dry15 121 40-140103124ND
Batch B253891 - Alcohol Prep
[TOC_3]B253891[TOC]
Blank (B253891-BLK1) Prepared & Analyzed: 03/10/20
Ethylene glycol mg/L10ND
LCS (B253891-BS1) Prepared & Analyzed: 03/10/20
Ethylene glycol mg/L10 100 40-140120120
LCS Dup (B253891-BSD1) Prepared & Analyzed: 03/10/20
Ethylene glycol mg/L10 100 5040-140133 10.3133
Duplicate (B253891-DUP1) Prepared & Analyzed: 03/10/20 Source: 20B1278-09
Ethylene glycol mg/L10 NCNDND
Matrix Spike (B253891-MS1) Prepared & Analyzed: 03/10/20 Source: 20B1278-09
Ethylene glycol mg/L10 100 40-140110110ND
Page 68 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B253408 - SW-846 3546
[TOC_3]B253408[TOC]
Blank (B253408-BLK1) Prepared: 03/03/20 Analyzed: 03/04/20
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)74.43.72
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)84.14.21
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 89.14.46
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 85.04.25
LCS (B253408-BS1) Prepared: 03/03/20 Analyzed: 03/04/20
C9-C18 Aliphatics mg/Kg wet10 30.0 40-14080.224.1
C19-C36 Aliphatics mg/Kg wet10 40.0 40-14099.639.8
Unadjusted C11-C22 Aromatics mg/Kg wet10 85.0 40-14088.475.1
Acenaphthene mg/Kg wet0.10 5.00 40-14078.03.90
Acenaphthylene mg/Kg wet0.10 5.00 40-14071.53.58
Anthracene mg/Kg wet0.10 5.00 40-14086.74.33
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14088.94.45
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14086.84.34
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14086.94.34
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14085.34.26
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14087.54.38
Chrysene mg/Kg wet0.10 5.00 40-14091.14.56
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14089.54.47
Fluoranthene mg/Kg wet0.10 5.00 40-14089.04.45
Fluorene mg/Kg wet0.10 5.00 40-14080.44.02
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14084.94.24
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14067.53.38
Naphthalene mg/Kg wet0.10 5.00 40-14063.03.15
Phenanthrene mg/Kg wet0.10 5.00 40-14086.44.32
Pyrene mg/Kg wet0.10 5.00 40-14090.04.50
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)72.73.64
Page 69 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B253408 - SW-846 3546
LCS (B253408-BS1) Prepared: 03/03/20 Analyzed: 03/04/20
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)86.14.30
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 86.04.30
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 82.44.12
LCS Dup (B253408-BSD1) Prepared: 03/03/20 Analyzed: 03/04/20
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14076.5 4.7623.0
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14096.0 3.6938.4
Unadjusted C11-C22 Aromatics mg/Kg wet10 85.0 2540-14084.7 4.3372.0
Acenaphthene mg/Kg wet0.10 5.00 2540-14074.6 4.473.73
Acenaphthylene mg/Kg wet0.10 5.00 2540-14068.1 4.903.41
Anthracene mg/Kg wet0.10 5.00 2540-14084.1 3.064.20
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14085.9 3.454.30
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14083.6 3.674.18
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14083.7 3.714.19
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14082.6 3.264.13
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14084.5 3.584.22
Chrysene mg/Kg wet0.10 5.00 2540-14088.2 3.324.41
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14085.8 4.204.29
Fluoranthene mg/Kg wet0.10 5.00 2540-14086.2 3.184.31
Fluorene mg/Kg wet0.10 5.00 2540-14077.5 3.653.88
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14081.8 3.724.09
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14064.3 4.943.21
Naphthalene mg/Kg wet0.10 5.00 2540-14059.6 5.412.98
Phenanthrene mg/Kg wet0.10 5.00 2540-14083.9 3.034.19
Pyrene mg/Kg wet0.10 5.00 2540-14087.0 3.324.35
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)73.93.69
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)81.94.09
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 88.24.41
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 83.94.20
Batch B253771 - SW-846 3510C
[TOC_3]B253771[TOC]
Blank (B253771-BLK1) Prepared: 03/08/20 Analyzed: 03/09/20
C9-C18 Aliphatics g/L100ND
C19-C36 Aliphatics g/L100ND
Unadjusted C11-C22 Aromatics g/L100ND
C11-C22 Aromatics g/L100ND
Acenaphthene g/L2.0ND
Acenaphthylene g/L2.0ND
Anthracene g/L2.0ND
Benzo(a)anthracene g/L2.0ND
Benzo(a)pyrene g/L2.0ND
Benzo(b)fluoranthene g/L2.0ND
Benzo(g,h,i)perylene g/L2.0ND
Benzo(k)fluoranthene g/L2.0ND
Chrysene g/L2.0ND
Dibenz(a,h)anthracene g/L2.0ND
Fluoranthene g/L2.0ND
Fluorene g/L2.0ND
Indeno(1,2,3-cd)pyrene g/L2.0ND
2-Methylnaphthalene g/L2.0ND
Page 70 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B253771 - SW-846 3510C
Blank (B253771-BLK1) Prepared: 03/08/20 Analyzed: 03/09/20
Naphthalene g/L2.0ND
Phenanthrene g/L2.0ND
Pyrene g/L2.0ND
Naphthalene-aliphatic fraction g/L2.0ND
2-Methylnaphthalene-aliphatic fraction g/L2.0ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)71.871.8
g/L 100 40-140Surrogate: o-Terphenyl (OTP)73.073.0
g/L 100 40-140Surrogate: 2-Bromonaphthalene 78.678.6
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 75.175.1
LCS (B253771-BS1) Prepared: 03/08/20 Analyzed: 03/09/20
C9-C18 Aliphatics g/L100 600 40-14068.4410
C19-C36 Aliphatics g/L100 800 40-14086.8695
Unadjusted C11-C22 Aromatics g/L100 1700 40-14079.11340
Acenaphthene g/L2.0 100 40-14065.465.4
Acenaphthylene g/L2.0 100 40-14060.260.2
Anthracene g/L2.0 100 40-14074.374.3
Benzo(a)anthracene g/L2.0 100 40-14075.975.9
Benzo(a)pyrene g/L2.0 100 40-14073.973.9
Benzo(b)fluoranthene g/L2.0 100 40-14074.174.1
Benzo(g,h,i)perylene g/L2.0 100 40-14073.973.9
Benzo(k)fluoranthene g/L2.0 100 40-14074.974.9
Chrysene g/L2.0 100 40-14078.078.0
Dibenz(a,h)anthracene g/L2.0 100 40-14076.876.8
Fluoranthene g/L2.0 100 40-14076.276.2
Fluorene g/L2.0 100 40-14068.068.0
Indeno(1,2,3-cd)pyrene g/L2.0 100 40-14073.073.0
2-Methylnaphthalene g/L2.0 100 40-14057.757.7
Naphthalene g/L2.0 100 40-14054.554.5
Phenanthrene g/L2.0 100 40-14073.973.9
Pyrene g/L2.0 100 40-14076.976.9
Naphthalene-aliphatic fraction g/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction g/L2.0 100 0-5ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)67.567.5
g/L 100 40-140Surrogate: o-Terphenyl (OTP)72.972.9
g/L 100 40-140Surrogate: 2-Bromonaphthalene 77.877.8
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 74.374.3
LCS Dup (B253771-BSD1) Prepared: 03/08/20 Analyzed: 03/09/20
C9-C18 Aliphatics g/L100 600 2540-14071.6 4.67430
C19-C36 Aliphatics g/L100 800 2540-14090.8 4.49727
Unadjusted C11-C22 Aromatics g/L100 1700 2540-14080.1 1.221360
Acenaphthene g/L2.0 100 2540-14068.8 4.9668.8
Acenaphthylene g/L2.0 100 2540-14063.3 5.1063.3
Anthracene g/L2.0 100 2540-14077.6 4.2877.6
Benzo(a)anthracene g/L2.0 100 2540-14078.9 3.8978.9
Benzo(a)pyrene g/L2.0 100 2540-14076.6 3.6076.6
Benzo(b)fluoranthene g/L2.0 100 2540-14076.7 3.5476.7
Benzo(g,h,i)perylene g/L2.0 100 2540-14076.8 3.7876.8
Benzo(k)fluoranthene g/L2.0 100 2540-14077.5 3.3977.5
Chrysene g/L2.0 100 2540-14081.1 3.8881.1
Dibenz(a,h)anthracene g/L2.0 100 2540-14079.7 3.6479.7
Page 71 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B253771 - SW-846 3510C
LCS Dup (B253771-BSD1) Prepared: 03/08/20 Analyzed: 03/09/20
Fluoranthene g/L2.0 100 2540-14079.4 4.0879.4
Fluorene g/L2.0 100 2540-14071.5 4.9671.5
Indeno(1,2,3-cd)pyrene g/L2.0 100 2540-14075.4 3.3375.4
2-Methylnaphthalene g/L2.0 100 2540-14061.1 5.7061.1
Naphthalene g/L2.0 100 2540-14058.1 6.3858.1
Phenanthrene g/L2.0 100 2540-14077.5 4.7477.5
Pyrene g/L2.0 100 2540-14080.1 4.0480.1
Naphthalene-aliphatic fraction g/L2.0 100 0-5ND
2-Methylnaphthalene-aliphatic fraction g/L2.0 100 0-5ND
g/L 100 40-140Surrogate: Chlorooctadecane (COD)73.973.9
g/L 100 40-140Surrogate: o-Terphenyl (OTP)76.776.7
g/L 100 40-140Surrogate: 2-Bromonaphthalene 78.778.7
g/L 100 40-140Surrogate: 2-Fluorobiphenyl 75.375.3
Page 72 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B253385 - MA VPH
[TOC_3]B253385[TOC]
Blank (B253385-BLK1) Prepared & Analyzed: 03/03/20
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.737.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)92.236.9
LCS (B253385-BS1) Prepared & Analyzed: 03/03/20
Benzene mg/Kg wet0.0010 0.0500 70-1301040.0520
Butylcyclohexane mg/Kg wet0.0010 0.0500 70-1301220.0610
Decane mg/Kg wet0.0010 0.0500 70-13097.40.0487
Ethylbenzene mg/Kg wet0.0010 0.0500 70-1301060.0532
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.0500 70-1301010.0505
2-Methylpentane mg/Kg wet0.0010 0.0500 70-13095.90.0479
Naphthalene mg/Kg wet0.010 0.0500 70-13096.10.0481
Nonane mg/Kg wet0.0010 0.0500 30-1301180.0589
Pentane mg/Kg wet0.0010 0.0500 70-13084.00.0420
Toluene mg/Kg wet0.0010 0.0500 70-1301050.0523
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.0500 70-1301060.0530
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.0500 70-1301020.0512
m+p Xylene mg/Kg wet0.0020 0.100 70-1301070.107
o-Xylene mg/Kg wet0.0010 0.0500 70-1301080.0538
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12851.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12549.8
LCS Dup (B253385-BSD1) Prepared & Analyzed: 03/03/20
Benzene mg/Kg wet0.0010 0.0500 2570-130102 1.730.0511
Butylcyclohexane mg/Kg wet0.0010 0.0500 2570-130118 3.620.0589
Decane mg/Kg wet0.0010 0.0500 2570-13092.9 4.710.0464
Ethylbenzene mg/Kg wet0.0010 0.0500 2570-130104 2.340.0520
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.0500 2570-130102 0.5410.0508
2-Methylpentane mg/Kg wet0.0010 0.0500 2570-13089.3 7.050.0447
Naphthalene mg/Kg wet0.010 0.0500 2570-13094.9 1.250.0475
Nonane mg/Kg wet0.0010 0.0500 2530-130114 3.600.0568
Pentane mg/Kg wet0.0010 0.0500 2570-13081.1 3.510.0405
Toluene mg/Kg wet0.0010 0.0500 2570-130103 1.700.0514
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.0500 2570-130103 2.530.0517
Page 73 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B253385 - MA VPH
LCS Dup (B253385-BSD1) Prepared & Analyzed: 03/03/20
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.0500 2570-13096.0 6.530.0480
m+p Xylene mg/Kg wet0.0020 0.100 2570-130105 2.300.105
o-Xylene mg/Kg wet0.0010 0.0500 2570-130106 1.930.0528
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12851.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)12349.1
Batch B253413 - MA VPH
[TOC_3]B253413[TOC]
Blank (B253413-BLK1) Prepared & Analyzed: 03/03/20
Unadjusted C5-C8 Aliphatics g/L100ND
C5-C8 Aliphatics g/L100ND
Unadjusted C9-C12 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)76.530.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)81.832.7
LCS (B253413-BS1) Prepared & Analyzed: 03/03/20
Benzene g/L1.0 50.0 70-13087.343.6
Butylcyclohexane g/L1.0 50.0 70-13012964.7
Decane g/L1.0 50.0 70-13012863.8
Ethylbenzene g/L1.0 50.0 70-13091.945.9
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 70-13091.545.8
2-Methylpentane g/L1.0 50.0 70-13074.737.4
Naphthalene g/L5.0 50.0 70-13011155.7
Nonane g/L1.0 50.0 L-0770-130135*67.4
Pentane g/L1.0 50.0 70-13085.742.9
Toluene g/L1.0 50.0 70-13089.944.9
1,2,4-Trimethylbenzene g/L1.0 50.0 70-13093.146.5
2,2,4-Trimethylpentane g/L1.0 50.0 70-13012562.7
m+p Xylene g/L2.0 100 70-13094.194.1
o-Xylene g/L1.0 50.0 70-13097.448.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)81.032.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)85.934.4
Page 74 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B253413 - MA VPH
LCS Dup (B253413-BSD1) Prepared & Analyzed: 03/03/20
Benzene g/L1.0 50.0 2570-13091.9 5.1446.0
Butylcyclohexane g/L1.0 50.0 2570-130127 1.7063.6
Decane g/L1.0 50.0 2570-130124 3.1461.8
Ethylbenzene g/L1.0 50.0 2570-13095.5 3.8647.7
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 2570-13092.5 1.0846.2
2-Methylpentane g/L1.0 50.0 2570-13081.3 8.3940.6
Naphthalene g/L5.0 50.0 2570-130106 4.8653.0
Nonane g/L1.0 50.0 2570-130130 4.0464.8
Pentane g/L1.0 50.0 2570-13090.7 5.6145.3
Toluene g/L1.0 50.0 2570-13093.8 4.3146.9
1,2,4-Trimethylbenzene g/L1.0 50.0 2570-13096.0 3.1448.0
2,2,4-Trimethylpentane g/L1.0 50.0 2570-130124 1.4161.9
m+p Xylene g/L2.0 100 2570-13096.4 2.4296.4
o-Xylene g/L1.0 50.0 2570-13098.9 1.5149.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)87.134.9
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.134.8
Page 75 of 96
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B253508 - SW-846 3005A
[TOC_3]B253508[TOC]
Blank (B253508-BLK1) Prepared & Analyzed: 03/04/20
Lead g/L0.50ND
LCS (B253508-BS1) Prepared & Analyzed: 03/04/20
Lead g/L5.0 500 80-120106530
LCS Dup (B253508-BSD1) Prepared & Analyzed: 03/04/20
Lead g/L5.0 500 2080-120105 0.585527
Batch B253629 - SW-846 3050B
[TOC_3]B253629[TOC]
Blank (B253629-BLK1) Prepared: 03/05/20 Analyzed: 03/09/20
Chromium mg/Kg wet4.2ND
Lead mg/Kg wet1.7ND
LCS (B253629-BS1) Prepared: 03/05/20 Analyzed: 03/09/20
Chromium mg/Kg wet50 101 82.4-116.8114115
Lead mg/Kg wet20 125 L-0782.4-116.8119*149
LCS Dup (B253629-BSD1) Prepared: 03/05/20 Analyzed: 03/09/20
Chromium mg/Kg wet50 101 3082.4-116.8104 9.07105
Lead mg/Kg wet20 125 3082.4-116.8108 9.37136
Page 76 of 96
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Drinking Water Organics EPA 504.1 - Quality Control
QUALITY CONTROL
[TOC_2]Drinking Water Organics EPA 504.1[TOC]
Batch B253604 - EPA 504 water
[TOC_3]B253604[TOC]
Blank (B253604-BLK1) Prepared & Analyzed: 03/05/20
1,2-Dibromoethane (EDB)g/L0.021ND
g/L 1.06 70-130Surrogate: 1,3-Dibromopropane 1081.14
LCS (B253604-BS1) Prepared & Analyzed: 03/05/20
1,2-Dibromoethane (EDB)g/L0.021 0.184 70-13083.40.153
g/L 1.05 70-130Surrogate: 1,3-Dibromopropane 1051.10
LCS Dup (B253604-BSD1) Prepared & Analyzed: 03/05/20
1,2-Dibromoethane (EDB)g/L0.021 0.183 70-13097.1 14.90.178
g/L 1.05 70-130Surrogate: 1,3-Dibromopropane 1111.16
Page 77 of 96
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IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES LCS
EPA 504.1
Lab Sample ID:Date(s) Analyzed:B253604-BS1
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
Instrument ID (2):
03/05/2020 03/05/2020
ANALYTE CONCENTRATION %RPDCOLRTRT WINDOW
FROM TO
1,2-Dibromoethane (EDB)1 2.916 0.000 0.000 0.153
[TOC_1]Dual Column RPD Report[TOC]
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IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES LCS Dup
EPA 504.1
Lab Sample ID:Date(s) Analyzed:B253604-BSD1
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
Instrument ID (2):
03/05/2020 03/05/2020
ANALYTE CONCENTRATION %RPDCOLRTRT WINDOW
FROM TO
1,2-Dibromoethane (EDB)1 2.916 0.000 0.000 0.178
Page 79 of 96
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample
matrix effects that lead to a low bias for reported result or non-homogeneous sample aliquots cannot be
eliminated.
MS-09
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
MS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is outside of the method specified criteria. Reduced precision anticipated for any reported
result for this compound.
MS-23
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered
with methanol, but with less than the method-specified amount.
O-01
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for
this compound in this sample.
R-06
Elevated reporting limit due to high concentration of target compounds.RL-11
Surrogate recovery outside of control limits due to suspected sample matrix interference. Chromatogram(s) is
attached.
S-15
Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less
than the reporting limit and bias is on the high side.
S-17
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthene
CT,MA,NH,NY,NC,RI,ME,VAAcenaphthylene
NY,NCAcetophenone
CT,MA,NH,NY,NC,RI,ME,VAAnthracene
NCAniline
CT,MA,NH,NY,NC,RI,ME,VABenzidine
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)anthracene
CT,MA,NH,NY,NC,RI,ME,VABenzo(a)pyrene
CT,MA,NH,NY,NC,RI,ME,VABenzo(b)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VABenzo(g,h,i)perylene
CT,MA,NH,NY,NC,RI,ME,VABenzo(k)fluoranthene
CT,MA,NH,NY,NC,RI,ME,VA4-Bromophenylphenylether
CT,MA,NH,NY,NC,RI,ME,VAButylbenzylphthalate
CT,MA,NH,NY,NC,RI,VA4-Chloro-3-methylphenol
NCBenzoic Acid
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethoxy)methane
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroethyl)ether
CT,MA,NH,NY,NC,RI,ME,VABis(2-chloroisopropyl)ether
CT,MA,NH,NY,NC,RI,ME,VA2-Chloronaphthalene
CT,MA,NH,NY,NC,RI,ME,VA2-Chlorophenol
CT,MA,NH,NY,NC,RI,ME,VA4-Chlorophenylphenylether
NCCarbazole
CT,MA,NH,NY,NC,RI,ME,VAChrysene
NC4-Chloroaniline
CT,MA,NH,NY,NC,RI,ME,VADibenz(a,h)anthracene
CT,MA,NH,NY,NC,RI,ME,VADi-n-butylphthalate
MA,NC1,3-Dichlorobenzene
MA,NC1,4-Dichlorobenzene
MA,NC1,2-Dichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA3,3-Dichlorobenzidine
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dichlorophenol
NCDibenzofuran
CT,MA,NH,NY,NC,RI,ME,VADiethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dimethylphenol
CT,MA,NH,NY,NC,RI,ME,VADimethylphthalate
CT,MA,NH,NY,NC,RI,ME,VA4,6-Dinitro-2-methylphenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrophenol
CT,MA,NH,NY,NC,RI,ME,VA2,4-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VA2,6-Dinitrotoluene
CT,MA,NH,NY,NC,RI,ME,VADi-n-octylphthalate
NC1,2-Diphenylhydrazine/Azobenzene
CT,MA,NH,NY,NC,RI,ME,VABis(2-Ethylhexyl)phthalate
CT,MA,NH,NY,NC,RI,ME,VAFluoranthene
CT,MA,NH,NY,NC,RI,ME,VAFluorene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobenzene
CT,MA,NH,NY,NC,RI,ME,VAHexachlorobutadiene
NC3-Nitroaniline
[TOC_1]Certifications[TOC]
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CERTIFICATIONS
Certified Analyses included in this Report
625.1 in Water
CT,MA,NH,NY,NC,RI,ME,VAHexachlorocyclopentadiene
CT,MA,NH,NY,NC,RI,ME,VAHexachloroethane
CT,MA,NH,NY,NC,RI,ME,VAIndeno(1,2,3-cd)pyrene
CT,MA,NH,NY,NC,RI,ME,VAIsophorone
CT,MA,NH,NY,NC,RI,ME,VANaphthalene
CT,MA,NH,NY,NC,RI,ME,VANitrobenzene
CT,MA,NH,NY,NC,RI,ME,VA2-Nitrophenol
CT,MA,NH,NY,NC,RI,ME,VA4-Nitrophenol
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodimethylamine
CT,MA,NH,NY,NC,RI,ME,VAN-Nitrosodi-n-propylamine
NC1-Methylnaphthalene
CT,MA,NH,NY,NC,RI,ME,VAPentachlorophenol
NC2-Methylnaphthalene
CT,MA,NH,NY,NC,RI,ME,VAPhenanthrene
NY,NC2-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPhenol
NY,NC3/4-Methylphenol
CT,MA,NH,NY,NC,RI,ME,VAPyrene
CT,MA,NH,NY,NC,RI,ME,VA1,2,4-Trichlorobenzene
CT,MA,NH,NY,NC,RI,ME,VA2,4,6-Trichlorophenol
NC2-Nitroaniline
NC4-Nitroaniline
NCPentachloronitrobenzene
CT,MA,NH,NY,NC,VAPyridine
NC1,2,4,5-Tetrachlorobenzene
CT,MA,NH,NY,NC2,4,5-Trichlorophenol
NC2-Fluorophenol
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
Page 82 of 96
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CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-EPH-04-1.1 in Water
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
Page 83 of 96
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
Page 84 of 96
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 6020B in Soil
NY,NC,MEChromium
NY,NC,MELead
SW-846 6020B in Water
CT,NH,NY,ME,VA,NCLead
SW-846 8015C in Soil
NYEthylene glycol
SW-846 8015C in Water
NYEthanol
NYEthylene glycol
SW-846 8260D in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
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CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
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CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
Page 87 of 96
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Certified Analyses included in this Report
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Soil
NC2-Fluorophenol
SW-846 8270E in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
CT,NY,NC,ME,NH,VAAnthracene
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
Page 89 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Water
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
Page 90 of 96
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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APPENDIX G

PHOTOGRAPHIC RECORD

WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 1 

Description: View of saturated soil in the tank farm area.   

Frame No. 2 

Description: View of used oil UST area.     

WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 3 

Description: View of gasoline UST area.  

Frame No. 4 

Description: View of the dispenser.    

WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 5 

Description: View of the ethylene glycol UST area.   

Frame No. 6 

Description: View of typical foam filling activities.     

WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 7 

Description: Additional view of typical foam filling activities.  

Frame No. 8 

Description: View of the area of the removed dispenser.    

WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 9 

Description: View of MW‐1.   

Frame No. 10 

Description: View of MW‐2.     
WithersRavenel
Our People. Your Success. 

Signature Flight Support: Greensboro, NC WR No. 02150228.03
Photographic Record March 2020

Frame No. 11 

Description: View of MW‐3.