WS-28333_47590_CA_CLO_20210628

UST CLOSURE REPORT
Site:
SHEETZ STORE 356
4319 WEST WENDOVER AVENUE
GREENSBORO, GUILFORD COUNTY, NORTH CAROLINA
Submitted To:
MR. MATHEW CUTSHALL
SHEETZ, INC.
351 SHEETZ WAY
CLAYSBURG, PENNSYLVANIA 16625
Prepared By:
ENVIROTRAC LTD.
7343 WEST FRIENDLY AVENUE, SUITE J
GREENSBORO, NORTH CAROLINA 27410
[phone]
JUNE 2021
Incident #: 47590
WS-28333

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© 2021 EnviroTrac

Report Prepared for:

Mr. Mathew Cutshall
Sheetz, Inc.
135 Sheetz Way
Claysburg, Pennsylvania 16625

UST CLOSURE REPORT
SHEETZ STORE 356
4319 WEST WENDOVER AVENURE
GREENSBORO, NORTH CAROLINA

Prepared by:

Annamarie Blauser, P.G.
Senior Scientist

Reviewed by:

Christopher W. Hay, EI
Principal

EnviroTrac Ltd.
7343 W. Friendly Avenue, Suite J
Greensboro, North Carolina 27410

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© 2021 EnviroTrac

TABLE OF CONTENTS
____________________________________________________________________________
1 SITE INFORMATION ........................................................................................................ 1 
2 UST CLOSURE ................................................................................................................ 1 
3 UST REMOVAL SOIL SAMPLE RESULTS ..................................................................... 3 
4 GROUNDWATER SAMPLNG AND RESULTS ................................................................ 4 
5 RESAMPLING PRODUCT LINES AND RESULTS ......................................................... 5 
6 CONCLUSIONS ................................................................................................................ 6 

TABLES

1 Site History and UST Information
2A UST Soil Sample Analytical Summary
2B Product Line Soil Sample Analytical Summary
3 Groundwater Sample Analytical Summary

FIGURES

1 Site Vicinity Map
2 Site Location Map
3 Receptor Map
4 Sample Location Map
5 Sample Location Results

APPENDICES

A Liquid and Tank Disposal Manifests
B UST Permanent Closure or Change-in-Service Forms (UST-2A and UST-3)
C Site Photographs
D Soil Manifests
E UST Laboratory Report and Chain-of-Custody
F Product Line Laboratory Report and Chain-of-Custody
G 24-Hour Release Reporting Form (UST-61)
H Groundwater Laboratory Report and Chain-of-Custody
I Resampled Soil Samples Laboratory Reports and Chain-of-Custodies

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UST CLOSURE REPORT
SHEETZ STORE 356
4319 WEST WENDOVER AVENUE
GREENSBORO, NORTH CAROLINA

1 SITE INFORMATION
____________________________________________________________________________

The site is located at 4319 West Wendover Avenue in Greensboro, North Carolina (Figures 1
and 2). The site consists of two tax parcels (Parcel Identification Number 7834701799 and
7834703637), currently owned by Sam H. Patterson Jr. Family Ltd Partnership. The underground
storage tanks (USTs) were reportedly installed in 2004.

The site is located in a commercial area consisting of shopping centers, retail stores, restaurants,
and hotels. Residential properties are further than 1,000 feet north of the site. South Buffalo
Creek runs through and along the southern border of the site. Neighboring land use areas are
shown on Figure 3.

Three 15,000-gallon USTs formerly contained gasoline, one 12,000-gallon UST formerly
contained diesel, and one 8,000-gallon UST formerly contained kerosene. The five USTs were
registered with the North Carolina Department of Environment Quality (NCDEQ).

The tanks were removed during a major remodel of the Sheetz Store 356.

2 UST CLOSURE
____________________________________________________________________________

Hazmat Emergency Response and Remediation, Inc. (HERR) of Whiteville, North Carolina
performed the UST closures on January 29, 2021. Prior to removing the USTs, 3,067 gallons of
sludge and 10,953 gallons of rinse liquids were removed from the tanks. During the UST closures,

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no petroleum odors or stained soil was observed in the soil at the base of the excavation. A copy
of the liquid disposal manifest is included in Appendix A.

The three 15,000-gallon gasoline USTs were constructed of coated steel double walled and was
approximately 10 feet in diameter and 26 feet long. The 12,000-gallon diesel UST was
constructed of coated steel double walled and was approximately 10 feet in diameter and 20 feet
long. The 8,000-gallon Kerosene UST was constructed of coated steel double walled and was
approximately 10 feet in diameter and 14 feet long. The UST information is summarized in Table
1. The exterior surface of the USTs appeared to be in good condition and no holes or corrosion
were observed. The USTs were loaded onto a truck and transported by HERR to D.H. Griffin in
Greensboro, North Carolina for disposal. A copy of the tank disposal manifest is included in
Appendix A. A copy of the UST-2 – UST Permanent Closure or Change-in-Service is included
in Appendix B. Attached are site photographs of the tank removal process in Appendix C.

Following removal of the gasoline USTs, three soil samples were collected from under each of
the USTs on January 29, 2021. Soil samples Gasoline UST 3, UST 4 and UST 5 were collected
from under the center and east and west ends. Following the removal of the diesel UST, two soil
samples were collected on January 29, 2021. Soil samples Diesel UST 2 was collected from
under the west and east ends. Following the removal of the kerosene UST 1, two soil samples
were collected on January 29, 2021. Kerosene UST-1 was collected from under the west and
east ends. Soils consisted of sandy silt. The soil samples were collected beneath the pea gravel
fill at a depth of 14 feet.

The soil samples collected under the gasoline USTs were analyzed for volatile organic compunds
by EPA Methods 8260 and for total petroleum hydrocarbons (TPH) by EPA Method 8015B
including gasoline range organics (GRO). Soil samples collected under the diesel UST and
kerosene UST were analyzed for TPH by EPA Method 8015B including diesel range organics
(DRO) and GRO.

The samples were collected and placed into laboratory provided containers, labeled, and
maintained on ice until delivered to a State certified laboratory under chain-of-custody. The
sample locations are shown on Figure 4.

The product lines from the five USTs and between the dispenser islands were uncovered.

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Thirteen soil samples were collected along the product lines and under the island dispensers
approximately ten feet apart (Samples 1 through 13). Three soil samples were collected
approximately 10 feet apart along the remote fill lines (Samples 14 through 16). One soil sample
was collected between the tank field and dispenser islands along the diesel product line (Sample
18). Two soil samples were collected along the kerosene product and beneath the kerosene
dispenser (Samples 17 and 19). The soil samples along the product lines were collected on
February 11, 2021 with a hand auger. The soil samples were collected approximately one foot
beneath the product lines and dispensers. The sample locations are shown on Figure 4.

Soil samples 1 through 8, 14 through 16 and 18 were collected for volatile organic compounds
(VOCs) by EPA Methods 8260 and for TPH by EPA Method 8015B including GRO and DRO.
Soil samples 9 through 13 were collected for VOCs by EPA Methods 8260 and for TPH by EPA
Method 8015B including GRO. Soil Samples 17 and 19 were collected for TPH by EPA Method
8015B including GRO and DRO.

The removed USTs were scheduled to be replaced with four new USTs. Prior to installing the
new USTs the onsite pea gravel and soil was removed to make room for the new USTs.
Approximately 745.06 tons of excess pea gravel and soil was transported by HERR to AES of NC
in Sanford, North Carolina for disposal. A copy of the soil disposal manifests are included in
Appendix D.

3 UST REMOVAL SOIL SAMPLE RESULTS
____________________________________________________________________________

The laboratory analysis of the soil samples collected under the USTs on January 29, 2021,
detected benzene above the Soil-to-Groundwater Maximum Soil Contaminant Concentrations
(MSCCs) in soil sample Gasoline UST 3 Center. Compounds were detected below the Soil-to-
Groundwater MSCCs and/or laboratory detection limit in the remaining soil samples collected
within the tank field. The laboratory results are summarized in Table 2A. The laboratory report
and associated chain-of-custody document are included in Appendix E.

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The laboratory analysis of the soil samples collected under the product lines, vapor lines and
dispenser islands on February 11, 2021, detected DRO above the State Action Level in Soil
Sample 17. Benzene was detected above the Soil-to-Groundwater MSCCs in Soil Samples 5, 9,
10 and 18. Naphthalene was detected above the Soil-to-Groundwater MSCC in Soil Samples 9
and 10. 1,2,4-Trimethylbenzene was detected above the Soil-to-Groundwater MSCC in Soil
Sample 10. The remaining analytical results were below the Soil-to-Groundwater MSCC and or
laboratory detection limits. The laboratory results are summarized in Table 2B and shown on
Figure 5. The laboratory report and associated chain-of-custody document are included in
Appendix F.

Upon receipt of the laboratory results, a 24-Hour Release and UST Leak Reporting Form (UST-
61) was submitted to the NCDEQ Raleigh Regional Office. A copy of the form is included in
Appendix G.

4 GROUNDWATER SAMPLNG AND RESULTS
____________________________________________________________________________

Prior to the UST closure, EnviroTrac collected groundwater samples from the three monitoring
wells (SW, NE and NW) in the tank field. Groundwater depth ranged from 9.37 to 10.01 feet
below ground surface. Prior to collecting groundwater samples, a minimum of three well volumes
of water were removed or the well was purged dry using a new disposable bailer. After allowing
the groundwater to recharge within the monitoring wells, groundwater samples were collected
with the bailer. The samples were placed in laboratory-supplied bottles, maintained on ice, and
transported under chain-of-custody to Pace Analytical Laboratories (Pace) to be analyzed for
Diesel Range Organics (DRO) and Gasoline Range Organics (GRO) by Standard Method 8015C
Modified.

Analytical results of the three monitoring wells (SW, NE and NW) did not detect DRO or GRO
above the laboratory detection limit. The laboratory results are summarized in Table 3. The
laboratory report and associated chain-of-custody document are included in Appendix H.

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5 RESAMPLING PRODUCT LINES AND RESULTS
____________________________________________________________________________

Following additional excavation within the product line trenches and beneath the dispensers, on
March 2, 2021 EnviroTrac resampled five locations. The locations were adjacent to Soil Sample
5, 9, and 10 under the product lines and dispenser islands, Soil Sample 18 along the diesel
product line between the tank field and dispenser islands, and Soil Sample 17 beneath to the
Kerosene dispenser. The sample locations are shown on Figure 4. Resampled Soil Samples 5,
9, 10 and 18 were collected for VOCs by EPA Method 8260. Resampled Soil Sample 17 was
collected for DRO. The soil samples were collected from an approximate depth 2 to 3 feet
beneath the product lines and dispenser.

The laboratory analysis of the resampled soil samples on March 2, 2021, detected benzene above
the Soil-to-Groundwater MSCC in Soil Sample 9-2 and 10-2. Toluene was detected above the
Soil-to-Groundwater MSCC in Soil Sample 9-2. The laboratory results are summarized in Table
2B and shown on Figure 5. The laboratory report and associated chain-of-custody document are
included in Appendix I.

Following additional excavation in the vicinity of Soil Samples 9 and 10, on March 8, 2021
EnviroTrac resampled two locations. The locations were adjacent to Soil Sample 9 and 10 under
the product lines and dispenser island. The sample locations are shown on Figure 4. Resampled
Soil Samples 9 and 10 were collected for VOCs by EPA Method 8260. The soil samples were
collected from an approximate depth 2 to 3 feet beneath the product lines and dispenser.

The laboratory analysis of the resampled soil samples collected on March 8, 2021, detected
benzene above the Soil-to-Groundwater MSCC in Soil Sample 10-3. The remaining analytical
results were below the Soil-to-Groundwater MSCC and/or laboratory detection limits. The
laboratory results are summarized in Table 2B and shown on Figure 5. The laboratory report
and associated chain-of-custody document are included in Appendix I.

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6 CONCLUSIONS
____________________________________________________________________________

Based on the field observations and results of the laboratory analysis, EnviroTrac presents the
following conclusions and recommendations:

 Three 15,000-gallon gasoline USTs were closed by removal on January 29, 2021.
The double walled UST was constructed of coated steel.
 One 12,000-gallon diesel UST was closed by removal on January 29, 2021. The
double walled UST was constructed of coated steel.
 One 8,000-gallon kerosene UST was closed by removal on January 29, 2021. The
double walled UST was constructed of coated steel.
 Laboratory analysis of the soil sample collected beneath the Gasoline UST 3
detected benzene above the Soil-to-Groundwater MSCC.
 Laboratory analysis for the soil collected beneath the soil sample 17 detected DRO
above the State Action Level.
 Laboratory analysis detected benzene above the Soil-to-Groundwater MSCCs in
soil samples 5, 9, 10 and 18. Naphthalene was detected above the Soil-to-
Groundwater MSCC in soil samples 9 and 10. 1,2,4-Trimethylbenzene was
detected above the Soil-to-Groundwater MSCC in soil sample 10.
 Laboratory analysis of the groundwater samples collected from the three
monitoring wells in the tank field did not detected DRO or GRO above the
laboratory analysis.
 Laboratory analysis detected benzene above the Soil-to-Groundwater MSCCs in
resampled soil samples 9 and 10. Toluene was detected above the Soil-to-
Groundwater MSCC in resampled soil sample 9.
 Laboratory analysis detected benzene above the Soil-to-Groundwater MSCCs in
additional resampled soil sample 10.
 More than 745 tons of soil and pea gravel were removed from the UST excavation
to the depth of groundwater.

TABLES

TABLE 1: SITE HISTORY AND UST INFORMATIONUST IDNumberLast ContentsUseCapacity (in Gallons)Construction DetailsTank DeminsionsLast Date UsedInstallation DateStatus ReleaseUST-1 Kerosene Fuel Station 8,000Coated Steel Double WalledCylindrical10' x 14' Unknown 1/1/2004Closed by Removal 1/27/2021NoUST-2Diesel, Diesel MixFuel Station 12,000Coated Steel Double WalledCylindrical10' x 20' Unknown 1/1/2004Closed by Removal 1/27/2021NoUST-3Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 1/1/2004Closed by Removal 1/27/2021YesUST-4Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 1/1/2004Closed by Removal 1/27/2021NoUST-5Gasoline, Gasoline MixFuel Station 15,000Coated Steel Double WalledCylindrical10' x 26' Unknown 1/1/2004Closed by Removal 1/27/2021NoNote:Locations of the USTs are shown on Figure 2.11.SZ0356.00Copyright 2021 EnviroTracApril 2021
TABLE 2A: UST SOIL SAMPLE ANALYTICAL SUMMARY ParameterANALYTICAL RESULTSSample IDKerosene UST 1EastKerosene UST 1 WestDiesel UST 2 EastDiesel UST 2 WestGAS UST 3 EastGAS UST 3CenterGAS UST 3 WestGAS UST 4 EastGAS UST 4 CenterGAS UST 4 WestGAS UST 5 EastGAS UST 5 CenterGAS UST 5 WestCollection Depth (feet bgs)14 14 14 14 14 14 14 14 14 14 14 14 14Collection Date01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21 01/29/21DROBDL BDL BDL BDL NA NA NA NA NA NA NA NA NA 100 540 1,500 40,000GROBDL BDL NA NA BDL BDL BDL BDL BDL BDL BDL BDL BDL 50- 31,000 810,000Volatile Organic Compounds by EPA Method 8260 (µg/kg)BenzeneNA NA NA NA BDL8.3BDL BDL BDL BDL BDL BDL BDL -5.6 18,000 164,000TolueneNA NA NA NA BDL 17.8 BDL BDL BDL 21.2 13.6 BDL 16.84,300 1,200,000 32,000,000EthylbenzeneNA NA NA NA BDL BDL BDL BDL BDL 9.4 BDL 8.2 18.7 - 4,900 1,560,000 40,000,000IsopropylbenzeneNA NA NA NA BDL BDL BDL BDL BDL BDL BDL BDL BDL - 17,000 1,564,000 4,088,000NaphthaleneNA NA NA NA BDL BDL BDL BDL BDL 11.9 BDL BDL 15.0 -160 313,000 8,176,000StyreneNA NA NA NA BDL BDL BDL BDL BDL BDL BDL BDL BDL - 1,500 3,128,000 81,760,0001,2,4-TrimethylbenzeneNA NA NA NA BDL 10.6 BDL 9.5 BDL 55.4 13.6 BDL 98.9 - 2,600 156,000 4,088,0001,3,5-TrimethylbenzeneNA NA NA NA BDL BDL BDL BDL BDL BDL BDL BDL BDL - 8,300 782,000 20,440,000Total XyleneNA NA NA NA BDL BDL BDL BDL BDL 74.7 BDL BDL 127 - 4,600 3,129,000 81,760,000Notes:Results presented in mg/kgMSCC = Maximum Soil Contaminant Concentration feet bgs = feet below ground surfaceBold denotes concentration is greater than the comparison criteriaBDL = Not detected at or above adjusted reporting limitNA = Not analyzed by this methodCOMPARISON CRITERIADiesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCCState Action Level 11.SZ0356.00Copyright 2021 EnviroTracApril 2021
TABLE 2B: PRODUCT LINE SOIL SAMPLE ANALYTICAL SUMMARYParameterANALYTICAL RESULTSSample IDDispenser 1Product Line 2Dispenser 3Product Line 4Dispenser 5Product Line 6Dispenser 7Product Line 8Dispenser 9Product Line 10Dispenser 11Product Line 12Collection Depth (feet bgs)2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5Collection Date02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21DRO21.6 BDL 7.1 BDL BDL 16.7 BDL 79.6 NA NA NA NA 100 540 1,500 40,000GROBDL BDL BDL BDL BDL BDL BDL BDL BDL 17 BDL BDL 50 - 31,000 810,000Volatile Organic Compounds by EPA Method 8260 (µg/kg)BenzeneBDL BDL BDL BDL86.5BDL BDL BDL41.0 14.4BDL BDL - 5.6 18,000 164,000Toluene23.7 BDL 65.2 18.4 203 BDL BDL BDL 71.5 59.3 10.2 12.0 - 4,300 1,200,000 32,000,000EthylbenzeneBDL BDL 9.9 15.4 11.9 BDL 26.5 BDL 331 207 12 10 - 4,900 1,560,000 40,000,000Diisopropyl etherBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - 370 156,000 4,088,000IsopropylbenzeneBDL BDL BDL BDL BDL BDL 10.6 BDL 196 216 BDL BDL - 17,000 1,564,000 4,088,000NaphthaleneBDL BDL BDL 17.4 BDL BDL 138 BDL281 62535 13 - 160 313,000 8,176,000n-PropylbenzeneBDL BDL BDL BDL BDL BDL BDL BDL BDL 1050.0 BDL BDL - 1,700 626,000 16,350,000p-IsopropyltolueneBDL BDL BDL BDL BDL BDL BDL 21.3 BDL BDL BDL BDL - 120 100,000 4,000,000sec-ButylbenzeneBDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 12.1 BDL - 3,300 626,000 16,350,0001,2,4-Trimethylbenzene26.2 BDL BDL BDL BDL BDL 198 BDL 2,370 7,350 32 14 - 2,600 156,000 4,088,0001,3,5-TrimethylbenzeneBDL BDL BDL BDL BDL BDL BDL BDL BDL 1,820 BDL BDL - 8,300 782,000 20,440,000Total Xylene30.7 BDL 40.4 BDL 49.8 BDL 39.1 BDL 1,470 785 23 17 - 4,600 3,129,000 81,760,000ParameterANALYTICAL RESULTSSample IDDispenser 13Remote Fill 14Remote Fill 15Remote Fill 16Kerosene Dispenser 17Product Line 18Kerosene Line 19Dispenser 5-2Dispenser 9-2Product Line 10-2Product Line 18-2Kerosene Dispenser 17-2Collection Depth (feet bgs)2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 3.0 4.0Collection Date02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 02/11/21 03/02/21 03/02/21 03/02/21 03/02/21 03/02/21DRONA BDL BDL BDL484BDL BDL NA NA NA NA BDL 100 540 1,500 40,000GRO BDL BDL BDL BDL BDL BDL BDL NA NA NA NA NA 50 - 31,000 810,000Volatile Organic Compounds by EPA Method 8260 (µg/kg)BenzeneBDL BDL BDL BDL NA160NA BDL1,840 11.3BDL BDL - 5.6 18,000 164,000TolueneBDL BDL BDL BDL NA 374 NA 1244,360BDL BDL BDL - 4,300 1,200,000 32,000,000EthylbenzeneBDL BDL BDL BDL NA 10.2 NA 21 664 BDL 10.9 BDL - 4,900 1,560,000 40,000,000Diisopropyl etherBDL BDL BDL BDL NA 13.0 NA BDL 21.9 BDL BDL BDL - 370 156,000 4,088,000IsopropylbenzeneBDL BDL BDL BDL NA BDL NA BDL 42.7 12 BDL BDL - 17,000 1,564,000 4,088,000NaphthaleneBDL BDL BDL BDL NA BDL NA BDL 83.6 BDL 25.2 BDL - 160 313,000 8,176,000n-PropylbenzeneBDL BDL BDL BDL NA BDL NA BDL 64.2 BDL 8.3 BDL - 1,700 626,000 16,350,000p-IsopropyltolueneBDL BDL BDL BDL NA BDL NA BDL BDL BDL BDL BDL - 120 100,000 4,000,000sec-ButylbenzeneBDL BDL BDL BDL NA BDL NA BDL BDL BDL BDL BDL - 3,300 626,000 16,350,0001,2,4-TrimethylbenzeneBDL BDL BDL BDL NA 27.8 NA 40 525 BDL BDL BDL - 2,600 156,000 4,088,0001,3,5-TrimethylbenzeneBDL BDL BDL BDL NA BDL NA 11 129 BDL BDL BDL - 8,300 782,000 20,440,000Total Xylene BDL BDL BDL BDL NA 322 NA 138 2,360 BDL 8.2 BDL - 4,600 3,129,000 81,760,000COMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCCDiesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)COMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCC11.SZ0356.00Copyright 2021 EnviroTrac1 of 2April 2021
TABLE 2B: PRODUCT LINE SOIL SAMPLE ANALYTICAL SUMMARYParameterANALYTICAL RESULTSSample IDDispenser 9-3Product Line 10-3Collection Depth (feet bgs)4.0 3.0Collection Date03/08/21 03/08/21DRONA NA100 540 1,500 40,000GRO NA NA50 - 31,000 810,000Volatile Organic Compounds by EPA Method 8260 (µg/kg)BenzeneBDL19.2- 5.6 18,000 164,000TolueneBDL BDL- 4,300 1,200,000 32,000,000EthylbenzeneBDL BDL- 4,900 1,560,000 40,000,000Diisopropyl etherBDL 10.3- 370 156,000 4,088,000Isopropylbenzene11.7 BDL- 17,000 1,564,000 4,088,000NaphthaleneBDL BDL- 160 313,000 8,176,000n-PropylbenzeneBDL BDL- 1,700 626,000 16,350,000p-IsopropyltolueneBDL BDL- 120 100,000 4,000,000sec-ButylbenzeneBDL BDL- 3,300 626,000 16,350,0001,2,4-TrimethylbenzeneBDL BDL- 2,600 156,000 4,088,0001,3,5-TrimethylbenzeneBDL BDL- 8,300 782,000 20,440,000Total Xylene BDL BDL- 4,600 3,129,000 81,760,000Notes:Results presented in mg/kg for DRO & GRO and in µg/kg for Votaile Orgainc Compounds.MSCC = Maximum Soil Contaminant Concentration feet bgs = feet below ground surfaceBold denotes concentration is greater than the State Action LevelBold and Shadded denotes concentrations is greater than Soil-to-Groundwater MSCCBDL = Not detected at or above adjusted reporting limitNA = Not analyzed by this methodDouble line indicates resampled locations.Diesel and Gasoline Range Organics by EPA Method 8015C (mg/kg)COMPARISON CRITERIAState Action Level Soil-to-Groundwater MSCCResidential MSCCIndustrialMSCC11.SZ0356.00Copyright 2021 EnviroTrac2 of 2April 2021
TABLE 3: GROUNDWATER SAMPLE ANALYTICAL SUMMARY
Parameter ANALYTICAL RESULTS
Sample ID SW NE NW
Collection Date 01/05/21 01/05/21 01/05/21
DRO BDL BDL BDL --
GRO BDL BDL BDL --
Notes:
Results presented in microgram per liter (µg/L)
2L Standard = North Carolina Groundwater Quality Standards
GCL = Gross Contamination Levels for Groundwater
Bold denotes concentration is greater than the comparison criteria
BDL = Not detected at or above adjusted reporting limit
Gasoline Range Organic by Method 5030B/8015C Modified (mg/L)
2L Standard GCLs
COMPARISON
CRITERIA
Diesel Range Organic by Method 8015C Modified (mg/L)
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FIGURES

7343 W. FRIENDLY AVENUE, SUITE JGREENSBORO, NORTH CAROLINAAPPROVED BY:CWHSCALE: AS SHOWNPROJECT NO: 11.SZ0356.00FIGURE 3RECEPTOR MAPDRAWN BY: ABDATE: 02/23/21REVISED BY:DATE:SOURCE: GUILFORD COUNTY AND CITY OF GREENSBORO GISCAD FILE: W:\Projects\11.SZ0356.00 Sheetz Greensboro (Wendover)\Figures\356 Greensboro_Figures.dwgENVIROTRAC - 7343 W. FRIENDLY AVE., SUITE J.| GREENSBORO, NC 27410 | PH: [phone] | FAX: [phone] | www.envirotrac.comSITE1,000' RADIUS1,500' RADIUSPONDPONDSheetz Store 3564319 West Wendover AvenueGreensboro, North CarolinaWestover VillageShopping MallCOSTCOWholesaleWishview ChildrenCenterGuilford CountyEmergency ServicesCVSCelebrationStationLowe's HomeImprovementBest BuyRestaurants &HotelsHotelsRestaurantsResidentialRestaurants &HotelsHotelsResidentialHotels

APPENDIX A
LIQUID and TANK DISPOSAL MANIFESTS

APPENDIX B
UST PERMANENT CLOUSRE OR
CHANGE-IN-SERVICE FORMS (UST-2A and UST-3)
____________________________________________________________________________

APPENDIX C
SITE PHOTOGRAHS
____________________________________________________________________________

Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 1: View cleaning out Kerosene UST 1.

Photograph 2: View of form location of Kerosene UST 1.
Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 3: View of Kerosene UST 1 being loaded on the truck.

Photograph 4: View of Kerosene UST 1 loaded on the truck.
Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 5: View of Diesel UST 2 in the tank field.

Photograph 6: View of Gasoline UST 3 being uncovered.

Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 7: View of Gasoline UST 3 in the tank field.

Photograph 8: View of Gasoline UST 4 and 5 in the tank field.

Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 9: View of Gasoline UST 4 and 5 in the tank field.

Photograph 10: View of Gasoline UST 5 in the tank field.

Photographic Documentation
Sheetz Store 356
4319 West Wendover Avenue
Greensboro, North Carolina

Photograph 11: View of Gasoline UST 4 loaded on the truck.

Photograph 12: View of Gasoline UST 4.

APPENDIX D
SOIL MANIFESTS
____________________________________________________________________________

APPENDIX E
UST LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
February 09, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92519570
92519570
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz Greensboro #356
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on February 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 47
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 47
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92519570001 Kerosene UST East EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92519570002 Kerosene UST West EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92519570003 Diesel UST East EPA 8015C Modified 2 PASI-CJMS1
SW-846 1 PASI-CKDF
92519570004 Diesel UST West EPA 8015C Modified 2 PASI-CJMS1
SW-846 1 PASI-CKDF
92519570005 Gas UST 3 East EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570006 Gas UST 3 Center EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570007 Gas UST 3 West EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570008 Gas UST 4 East EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570009 Gas UST 4 Center EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570010 Gas UST 4 West EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570011 Gas UST 5 East EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570012 Gas UST 5 Center EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92519570013 Gas UST 5 West EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 47
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 47
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92519570001 Kerosene UST East
Percent Moisture 30.3 %02/01/21 16:53 N20.10SW-846
92519570002 Kerosene UST West
Percent Moisture 26.0 %02/01/21 16:53 N20.10SW-846
92519570003 Diesel UST East
Percent Moisture 22.0 %02/01/21 16:53 N20.10SW-846
92519570004 Diesel UST West
Percent Moisture 22.8 %02/01/21 16:53 N20.10SW-846
92519570005 Gas UST 3 East
Percent Moisture 21.9 %02/01/21 16:53 N20.10SW-846
92519570006 Gas UST 3 Center
Benzene 8.3 ug/kg 02/05/21 16:108.2EPA 8260D
Toluene 17.8 ug/kg 02/05/21 16:108.2EPA 8260D
1,2,4-Trimethylbenzene 10.6 ug/kg 02/05/21 16:108.2EPA 8260D
Percent Moisture 19.6 %02/01/21 16:53 N20.10SW-846
92519570007 Gas UST 3 West
Percent Moisture 31.8 %02/01/21 16:53 N20.10SW-846
92519570008 Gas UST 4 East
1,2,4-Trimethylbenzene 9.5 ug/kg 02/05/21 16:469.1EPA 8260D
Percent Moisture 27.5 %02/01/21 16:53 N20.10SW-846
92519570009 Gas UST 4 Center
Percent Moisture 18.6 %02/01/21 16:53 N20.10SW-846
92519570010 Gas UST 4 West
Ethylbenzene 9.4 ug/kg 02/05/21 17:228.3EPA 8260D
Naphthalene 11.9 ug/kg 02/05/21 17:228.3EPA 8260D
Toluene 21.2 ug/kg 02/05/21 17:228.3EPA 8260D
1,2,4-Trimethylbenzene 55.4 ug/kg 02/05/21 17:228.3EPA 8260D
Xylene (Total)74.7 ug/kg 02/05/21 17:2216.7EPA 8260D
m&p-Xylene 51.5 ug/kg 02/05/21 17:2216.7EPA 8260D
o-Xylene 23.2 ug/kg 02/05/21 17:228.3EPA 8260D
Percent Moisture 23.4 %02/01/21 16:53 N20.10SW-846
92519570011 Gas UST 5 East
Toluene 13.6 ug/kg 02/05/21 17:4011.0EPA 8260D
1,2,4-Trimethylbenzene 13.6 ug/kg 02/05/21 17:4011.0EPA 8260D
Percent Moisture 29.4 %02/01/21 16:54 N20.10SW-846
92519570012 Gas UST 5 Center
Ethylbenzene 8.2 ug/kg 02/05/21 17:587.9EPA 8260D
Percent Moisture 25.3 %02/01/21 17:23 N20.10SW-846
92519570013 Gas UST 5 West
Ethylbenzene 18.7 ug/kg 02/05/21 18:169.2EPA 8260D
Naphthalene 15.0 ug/kg 02/05/21 18:169.2EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 47
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92519570013 Gas UST 5 West
Toluene 16.8 ug/kg 02/05/21 18:169.2EPA 8260D
1,2,4-Trimethylbenzene 98.9 ug/kg 02/05/21 18:169.2EPA 8260D
Xylene (Total)127 ug/kg 02/05/21 18:1618.3EPA 8260D
m&p-Xylene 85.2 ug/kg 02/05/21 18:1618.3EPA 8260D
o-Xylene 41.9 ug/kg 02/05/21 18:169.2EPA 8260D
Percent Moisture 25.1 %02/01/21 17:24 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Kerosene UST East Lab ID: 92519570001 Collected: 01/29/21 07:56 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/03/21 10:3702/02/21 13:387.2 1
Surrogates
n-Pentacosane (S)88 %02/03/21 10:37 629-99-202/02/21 13:3832-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 19:4902/04/21 11:3210.4 1
Surrogates
4-Bromofluorobenzene (S)94 %02/04/21 19:49 460-00-402/04/21 11:3266-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.3 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Kerosene UST West Lab ID: 92519570002 Collected: 01/29/21 08:04 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/03/21 11:0102/02/21 13:386.8 1
Surrogates
n-Pentacosane (S)76 %02/03/21 11:01 629-99-202/02/21 13:3832-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 20:2202/04/21 11:329.6 1
Surrogates
4-Bromofluorobenzene (S)91 %02/04/21 20:22 460-00-402/04/21 11:3266-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.0 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Diesel UST East Lab ID: 92519570003 Collected: 01/29/21 08:16 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/03/21 11:2502/02/21 13:386.5 1
Surrogates
n-Pentacosane (S)81 %02/03/21 11:25 629-99-202/02/21 13:3832-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.0 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Diesel UST West Lab ID: 92519570004 Collected: 01/29/21 08:21 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/03/21 11:4902/02/21 13:386.5 1
Surrogates
n-Pentacosane (S)79 %02/03/21 11:49 629-99-202/02/21 13:3832-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.8 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 East Lab ID: 92519570005 Collected: 01/29/21 08:50 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 20:5502/04/21 11:3211.1 1
Surrogates
4-Bromofluorobenzene (S)92 %02/04/21 20:55 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 15:34 67-64-102/05/21 13:35238 1
Benzene ND ug/kg 02/05/21 15:34 71-43-202/05/21 13:3511.9 1
Bromobenzene ND ug/kg 02/05/21 15:34 108-86-102/05/21 13:3511.9 1
Bromochloromethane ND ug/kg 02/05/21 15:34 74-97-502/05/21 13:3511.9 1
Bromodichloromethane ND ug/kg 02/05/21 15:34 75-27-402/05/21 13:3511.9 1
Bromoform ND ug/kg 02/05/21 15:34 75-25-202/05/21 13:3511.9 1
Bromomethane ND ug/kg 02/05/21 15:34 74-83-902/05/21 13:3523.8 1
2-Butanone (MEK)ND ug/kg 02/05/21 15:34 78-93-302/05/21 13:35238 1
n-Butylbenzene ND ug/kg 02/05/21 15:34 104-51-802/05/21 13:3511.9 1
sec-Butylbenzene ND ug/kg 02/05/21 15:34 135-98-802/05/21 13:3511.9 1
tert-Butylbenzene ND ug/kg 02/05/21 15:34 98-06-602/05/21 13:3511.9 1
Carbon tetrachloride ND ug/kg 02/05/21 15:34 56-23-502/05/21 13:3511.9 1
Chlorobenzene ND ug/kg 02/05/21 15:34 108-90-702/05/21 13:3511.9 1
Chloroethane ND ug/kg 02/05/21 15:34 75-00-302/05/21 13:3523.8 1
Chloroform ND ug/kg 02/05/21 15:34 67-66-302/05/21 13:3511.9 1
Chloromethane ND ug/kg 02/05/21 15:34 74-87-302/05/21 13:3523.8 1
2-Chlorotoluene ND ug/kg 02/05/21 15:34 95-49-802/05/21 13:3511.9 1
4-Chlorotoluene ND ug/kg 02/05/21 15:34 106-43-402/05/21 13:3511.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 15:34 96-12-802/05/21 13:3511.9 1
Dibromochloromethane ND ug/kg 02/05/21 15:34 124-48-102/05/21 13:3511.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 15:34 106-93-402/05/21 13:3511.9 1
Dibromomethane ND ug/kg 02/05/21 15:34 74-95-302/05/21 13:3511.9 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 15:34 95-50-102/05/21 13:3511.9 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 15:34 541-73-102/05/21 13:3511.9 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 15:34 106-46-702/05/21 13:3511.9 1
Dichlorodifluoromethane ND ug/kg 02/05/21 15:34 75-71-802/05/21 13:3523.8 1
1,1-Dichloroethane ND ug/kg 02/05/21 15:34 75-34-302/05/21 13:3511.9 1
1,2-Dichloroethane ND ug/kg 02/05/21 15:34 107-06-202/05/21 13:3511.9 1
1,1-Dichloroethene ND ug/kg 02/05/21 15:34 75-35-402/05/21 13:3511.9 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 15:34 156-59-202/05/21 13:3511.9 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 15:34 156-60-502/05/21 13:3511.9 1
1,2-Dichloropropane ND ug/kg 02/05/21 15:34 78-87-502/05/21 13:3511.9 1
1,3-Dichloropropane ND ug/kg 02/05/21 15:34 142-28-902/05/21 13:3511.9 1
2,2-Dichloropropane ND ug/kg 02/05/21 15:34 594-20-702/05/21 13:3511.9 1
1,1-Dichloropropene ND ug/kg 02/05/21 15:34 563-58-602/05/21 13:3511.9 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 15:34 10061-01-502/05/21 13:3511.9 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 15:34 10061-02-602/05/21 13:3511.9 1
Diisopropyl ether ND ug/kg 02/05/21 15:34 108-20-302/05/21 13:3511.9 1
Ethylbenzene ND ug/kg 02/05/21 15:34 100-41-402/05/21 13:3511.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 East Lab ID: 92519570005 Collected: 01/29/21 08:50 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 15:34 87-68-302/05/21 13:3523.8 1
2-Hexanone ND ug/kg 02/05/21 15:34 591-78-602/05/21 13:35119 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 15:34 98-82-802/05/21 13:3511.9 1
p-Isopropyltoluene ND ug/kg 02/05/21 15:34 99-87-602/05/21 13:3511.9 1
Methylene Chloride ND ug/kg 02/05/21 15:34 75-09-202/05/21 13:3547.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 15:34 108-10-102/05/21 13:35119 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 15:34 1634-04-402/05/21 13:3511.9 1
Naphthalene ND ug/kg 02/05/21 15:34 91-20-302/05/21 13:3511.9 1
n-Propylbenzene ND ug/kg 02/05/21 15:34 103-65-102/05/21 13:3511.9 1
Styrene ND ug/kg 02/05/21 15:34 100-42-502/05/21 13:3511.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 15:34 630-20-602/05/21 13:3511.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 15:34 79-34-502/05/21 13:3511.9 1
Tetrachloroethene ND ug/kg 02/05/21 15:34 127-18-402/05/21 13:3511.9 1
Toluene ND ug/kg 02/05/21 15:34 108-88-302/05/21 13:3511.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 15:34 87-61-602/05/21 13:3511.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 15:34 120-82-102/05/21 13:3511.9 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 15:34 71-55-602/05/21 13:3511.9 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 15:34 79-00-502/05/21 13:3511.9 1
Trichloroethene ND ug/kg 02/05/21 15:34 79-01-602/05/21 13:3511.9 1
Trichlorofluoromethane ND ug/kg 02/05/21 15:34 75-69-402/05/21 13:3511.9 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 15:34 96-18-402/05/21 13:3511.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/05/21 15:34 95-63-602/05/21 13:3511.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 15:34 108-67-802/05/21 13:3511.9 1
Vinyl acetate ND ug/kg 02/05/21 15:34 108-05-402/05/21 13:35119 1
Vinyl chloride ND ug/kg 02/05/21 15:34 75-01-402/05/21 13:3523.8 1
Xylene (Total)ND ug/kg 02/05/21 15:34 1330-20-702/05/21 13:3523.8 1
m&p-Xylene ND ug/kg 02/05/21 15:34 179601-23-102/05/21 13:3523.8 1
o-Xylene ND ug/kg 02/05/21 15:34 95-47-602/05/21 13:3511.9 1
Surrogates
Toluene-d8 (S)100 %02/05/21 15:34 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)101 %02/05/21 15:34 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)104 %02/05/21 15:34 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.9 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 Center Lab ID: 92519570006 Collected: 01/29/21 08:54 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 21:2302/04/21 11:3210.1 1
Surrogates
4-Bromofluorobenzene (S)85 %02/04/21 21:23 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 16:10 67-64-102/05/21 13:35163 1
Benzene 8.3 ug/kg 02/05/21 16:10 71-43-202/05/21 13:358.2 1
Bromobenzene ND ug/kg 02/05/21 16:10 108-86-102/05/21 13:358.2 1
Bromochloromethane ND ug/kg 02/05/21 16:10 74-97-502/05/21 13:358.2 1
Bromodichloromethane ND ug/kg 02/05/21 16:10 75-27-402/05/21 13:358.2 1
Bromoform ND ug/kg 02/05/21 16:10 75-25-202/05/21 13:358.2 1
Bromomethane ND ug/kg 02/05/21 16:10 74-83-902/05/21 13:3516.3 1
2-Butanone (MEK)ND ug/kg 02/05/21 16:10 78-93-302/05/21 13:35163 1
n-Butylbenzene ND ug/kg 02/05/21 16:10 104-51-802/05/21 13:358.2 1
sec-Butylbenzene ND ug/kg 02/05/21 16:10 135-98-802/05/21 13:358.2 1
tert-Butylbenzene ND ug/kg 02/05/21 16:10 98-06-602/05/21 13:358.2 1
Carbon tetrachloride ND ug/kg 02/05/21 16:10 56-23-502/05/21 13:358.2 1
Chlorobenzene ND ug/kg 02/05/21 16:10 108-90-702/05/21 13:358.2 1
Chloroethane ND ug/kg 02/05/21 16:10 75-00-302/05/21 13:3516.3 1
Chloroform ND ug/kg 02/05/21 16:10 67-66-302/05/21 13:358.2 1
Chloromethane ND ug/kg 02/05/21 16:10 74-87-302/05/21 13:3516.3 1
2-Chlorotoluene ND ug/kg 02/05/21 16:10 95-49-802/05/21 13:358.2 1
4-Chlorotoluene ND ug/kg 02/05/21 16:10 106-43-402/05/21 13:358.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 16:10 96-12-802/05/21 13:358.2 1
Dibromochloromethane ND ug/kg 02/05/21 16:10 124-48-102/05/21 13:358.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 16:10 106-93-402/05/21 13:358.2 1
Dibromomethane ND ug/kg 02/05/21 16:10 74-95-302/05/21 13:358.2 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 16:10 95-50-102/05/21 13:358.2 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 16:10 541-73-102/05/21 13:358.2 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 16:10 106-46-702/05/21 13:358.2 1
Dichlorodifluoromethane ND ug/kg 02/05/21 16:10 75-71-802/05/21 13:3516.3 1
1,1-Dichloroethane ND ug/kg 02/05/21 16:10 75-34-302/05/21 13:358.2 1
1,2-Dichloroethane ND ug/kg 02/05/21 16:10 107-06-202/05/21 13:358.2 1
1,1-Dichloroethene ND ug/kg 02/05/21 16:10 75-35-402/05/21 13:358.2 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 16:10 156-59-202/05/21 13:358.2 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 16:10 156-60-502/05/21 13:358.2 1
1,2-Dichloropropane ND ug/kg 02/05/21 16:10 78-87-502/05/21 13:358.2 1
1,3-Dichloropropane ND ug/kg 02/05/21 16:10 142-28-902/05/21 13:358.2 1
2,2-Dichloropropane ND ug/kg 02/05/21 16:10 594-20-702/05/21 13:358.2 1
1,1-Dichloropropene ND ug/kg 02/05/21 16:10 563-58-602/05/21 13:358.2 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 16:10 10061-01-502/05/21 13:358.2 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 16:10 10061-02-602/05/21 13:358.2 1
Diisopropyl ether ND ug/kg 02/05/21 16:10 108-20-302/05/21 13:358.2 1
Ethylbenzene ND ug/kg 02/05/21 16:10 100-41-402/05/21 13:358.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 Center Lab ID: 92519570006 Collected: 01/29/21 08:54 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 16:10 87-68-302/05/21 13:3516.3 1
2-Hexanone ND ug/kg 02/05/21 16:10 591-78-602/05/21 13:3581.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 16:10 98-82-802/05/21 13:358.2 1
p-Isopropyltoluene ND ug/kg 02/05/21 16:10 99-87-602/05/21 13:358.2 1
Methylene Chloride ND ug/kg 02/05/21 16:10 75-09-202/05/21 13:3532.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 16:10 108-10-102/05/21 13:3581.6 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 16:10 1634-04-402/05/21 13:358.2 1
Naphthalene ND ug/kg 02/05/21 16:10 91-20-302/05/21 13:358.2 1
n-Propylbenzene ND ug/kg 02/05/21 16:10 103-65-102/05/21 13:358.2 1
Styrene ND ug/kg 02/05/21 16:10 100-42-502/05/21 13:358.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 16:10 630-20-602/05/21 13:358.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 16:10 79-34-502/05/21 13:358.2 1
Tetrachloroethene ND ug/kg 02/05/21 16:10 127-18-402/05/21 13:358.2 1
Toluene 17.8 ug/kg 02/05/21 16:10 108-88-302/05/21 13:358.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 16:10 87-61-602/05/21 13:358.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 16:10 120-82-102/05/21 13:358.2 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 16:10 71-55-602/05/21 13:358.2 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 16:10 79-00-502/05/21 13:358.2 1
Trichloroethene ND ug/kg 02/05/21 16:10 79-01-602/05/21 13:358.2 1
Trichlorofluoromethane ND ug/kg 02/05/21 16:10 75-69-402/05/21 13:358.2 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 16:10 96-18-402/05/21 13:358.2 1
1,2,4-Trimethylbenzene 10.6 ug/kg 02/05/21 16:10 95-63-602/05/21 13:358.2 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 16:10 108-67-802/05/21 13:358.2 1
Vinyl acetate ND ug/kg 02/05/21 16:10 108-05-402/05/21 13:3581.6 1
Vinyl chloride ND ug/kg 02/05/21 16:10 75-01-402/05/21 13:3516.3 1
Xylene (Total)ND ug/kg 02/05/21 16:10 1330-20-702/05/21 13:3516.3 1
m&p-Xylene ND ug/kg 02/05/21 16:10 179601-23-102/05/21 13:3516.3 1
o-Xylene ND ug/kg 02/05/21 16:10 95-47-602/05/21 13:358.2 1
Surrogates
Toluene-d8 (S)100 %02/05/21 16:10 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)102 %02/05/21 16:10 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)104 %02/05/21 16:10 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.6 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 West Lab ID: 92519570007 Collected: 01/29/21 08:58 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 21:5102/04/21 11:3210.6 1
Surrogates
4-Bromofluorobenzene (S)85 %02/04/21 21:51 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 16:28 67-64-102/05/21 13:35181 1
Benzene ND ug/kg 02/05/21 16:28 71-43-202/05/21 13:359.0 1
Bromobenzene ND ug/kg 02/05/21 16:28 108-86-102/05/21 13:359.0 1
Bromochloromethane ND ug/kg 02/05/21 16:28 74-97-502/05/21 13:359.0 1
Bromodichloromethane ND ug/kg 02/05/21 16:28 75-27-402/05/21 13:359.0 1
Bromoform ND ug/kg 02/05/21 16:28 75-25-202/05/21 13:359.0 1
Bromomethane ND ug/kg 02/05/21 16:28 74-83-902/05/21 13:3518.1 1
2-Butanone (MEK)ND ug/kg 02/05/21 16:28 78-93-302/05/21 13:35181 1
n-Butylbenzene ND ug/kg 02/05/21 16:28 104-51-802/05/21 13:359.0 1
sec-Butylbenzene ND ug/kg 02/05/21 16:28 135-98-802/05/21 13:359.0 1
tert-Butylbenzene ND ug/kg 02/05/21 16:28 98-06-602/05/21 13:359.0 1
Carbon tetrachloride ND ug/kg 02/05/21 16:28 56-23-502/05/21 13:359.0 1
Chlorobenzene ND ug/kg 02/05/21 16:28 108-90-702/05/21 13:359.0 1
Chloroethane ND ug/kg 02/05/21 16:28 75-00-302/05/21 13:3518.1 1
Chloroform ND ug/kg 02/05/21 16:28 67-66-302/05/21 13:359.0 1
Chloromethane ND ug/kg 02/05/21 16:28 74-87-302/05/21 13:3518.1 1
2-Chlorotoluene ND ug/kg 02/05/21 16:28 95-49-802/05/21 13:359.0 1
4-Chlorotoluene ND ug/kg 02/05/21 16:28 106-43-402/05/21 13:359.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 16:28 96-12-802/05/21 13:359.0 1
Dibromochloromethane ND ug/kg 02/05/21 16:28 124-48-102/05/21 13:359.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 16:28 106-93-402/05/21 13:359.0 1
Dibromomethane ND ug/kg 02/05/21 16:28 74-95-302/05/21 13:359.0 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 16:28 95-50-102/05/21 13:359.0 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 16:28 541-73-102/05/21 13:359.0 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 16:28 106-46-702/05/21 13:359.0 1
Dichlorodifluoromethane ND ug/kg 02/05/21 16:28 75-71-802/05/21 13:3518.1 1
1,1-Dichloroethane ND ug/kg 02/05/21 16:28 75-34-302/05/21 13:359.0 1
1,2-Dichloroethane ND ug/kg 02/05/21 16:28 107-06-202/05/21 13:359.0 1
1,1-Dichloroethene ND ug/kg 02/05/21 16:28 75-35-402/05/21 13:359.0 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 16:28 156-59-202/05/21 13:359.0 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 16:28 156-60-502/05/21 13:359.0 1
1,2-Dichloropropane ND ug/kg 02/05/21 16:28 78-87-502/05/21 13:359.0 1
1,3-Dichloropropane ND ug/kg 02/05/21 16:28 142-28-902/05/21 13:359.0 1
2,2-Dichloropropane ND ug/kg 02/05/21 16:28 594-20-702/05/21 13:359.0 1
1,1-Dichloropropene ND ug/kg 02/05/21 16:28 563-58-602/05/21 13:359.0 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 16:28 10061-01-502/05/21 13:359.0 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 16:28 10061-02-602/05/21 13:359.0 1
Diisopropyl ether ND ug/kg 02/05/21 16:28 108-20-302/05/21 13:359.0 1
Ethylbenzene ND ug/kg 02/05/21 16:28 100-41-402/05/21 13:359.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 3 West Lab ID: 92519570007 Collected: 01/29/21 08:58 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 16:28 87-68-302/05/21 13:3518.1 1
2-Hexanone ND ug/kg 02/05/21 16:28 591-78-602/05/21 13:3590.3 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 16:28 98-82-802/05/21 13:359.0 1
p-Isopropyltoluene ND ug/kg 02/05/21 16:28 99-87-602/05/21 13:359.0 1
Methylene Chloride ND ug/kg 02/05/21 16:28 75-09-202/05/21 13:3536.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 16:28 108-10-102/05/21 13:3590.3 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 16:28 1634-04-402/05/21 13:359.0 1
Naphthalene ND ug/kg 02/05/21 16:28 91-20-302/05/21 13:359.0 1
n-Propylbenzene ND ug/kg 02/05/21 16:28 103-65-102/05/21 13:359.0 1
Styrene ND ug/kg 02/05/21 16:28 100-42-502/05/21 13:359.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 16:28 630-20-602/05/21 13:359.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 16:28 79-34-502/05/21 13:359.0 1
Tetrachloroethene ND ug/kg 02/05/21 16:28 127-18-402/05/21 13:359.0 1
Toluene ND ug/kg 02/05/21 16:28 108-88-302/05/21 13:359.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 16:28 87-61-602/05/21 13:359.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 16:28 120-82-102/05/21 13:359.0 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 16:28 71-55-602/05/21 13:359.0 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 16:28 79-00-502/05/21 13:359.0 1
Trichloroethene ND ug/kg 02/05/21 16:28 79-01-602/05/21 13:359.0 1
Trichlorofluoromethane ND ug/kg 02/05/21 16:28 75-69-402/05/21 13:359.0 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 16:28 96-18-402/05/21 13:359.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/05/21 16:28 95-63-602/05/21 13:359.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 16:28 108-67-802/05/21 13:359.0 1
Vinyl acetate ND ug/kg 02/05/21 16:28 108-05-402/05/21 13:3590.3 1
Vinyl chloride ND ug/kg 02/05/21 16:28 75-01-402/05/21 13:3518.1 1
Xylene (Total)ND ug/kg 02/05/21 16:28 1330-20-702/05/21 13:3518.1 1
m&p-Xylene ND ug/kg 02/05/21 16:28 179601-23-102/05/21 13:3518.1 1
o-Xylene ND ug/kg 02/05/21 16:28 95-47-602/05/21 13:359.0 1
Surrogates
Toluene-d8 (S)99 %02/05/21 16:28 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)100 %02/05/21 16:28 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)102 %02/05/21 16:28 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.8 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 East Lab ID: 92519570008 Collected: 01/29/21 09:51 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/04/21 22:1902/04/21 11:329.8 1
Surrogates
4-Bromofluorobenzene (S)87 %02/04/21 22:19 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 16:46 67-64-102/05/21 13:35182 1
Benzene ND ug/kg 02/05/21 16:46 71-43-202/05/21 13:359.1 1
Bromobenzene ND ug/kg 02/05/21 16:46 108-86-102/05/21 13:359.1 1
Bromochloromethane ND ug/kg 02/05/21 16:46 74-97-502/05/21 13:359.1 1
Bromodichloromethane ND ug/kg 02/05/21 16:46 75-27-402/05/21 13:359.1 1
Bromoform ND ug/kg 02/05/21 16:46 75-25-202/05/21 13:359.1 1
Bromomethane ND ug/kg 02/05/21 16:46 74-83-902/05/21 13:3518.2 1
2-Butanone (MEK)ND ug/kg 02/05/21 16:46 78-93-302/05/21 13:35182 1
n-Butylbenzene ND ug/kg 02/05/21 16:46 104-51-802/05/21 13:359.1 1
sec-Butylbenzene ND ug/kg 02/05/21 16:46 135-98-802/05/21 13:359.1 1
tert-Butylbenzene ND ug/kg 02/05/21 16:46 98-06-602/05/21 13:359.1 1
Carbon tetrachloride ND ug/kg 02/05/21 16:46 56-23-502/05/21 13:359.1 1
Chlorobenzene ND ug/kg 02/05/21 16:46 108-90-702/05/21 13:359.1 1
Chloroethane ND ug/kg 02/05/21 16:46 75-00-302/05/21 13:3518.2 1
Chloroform ND ug/kg 02/05/21 16:46 67-66-302/05/21 13:359.1 1
Chloromethane ND ug/kg 02/05/21 16:46 74-87-302/05/21 13:3518.2 1
2-Chlorotoluene ND ug/kg 02/05/21 16:46 95-49-802/05/21 13:359.1 1
4-Chlorotoluene ND ug/kg 02/05/21 16:46 106-43-402/05/21 13:359.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 16:46 96-12-802/05/21 13:359.1 1
Dibromochloromethane ND ug/kg 02/05/21 16:46 124-48-102/05/21 13:359.1 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 16:46 106-93-402/05/21 13:359.1 1
Dibromomethane ND ug/kg 02/05/21 16:46 74-95-302/05/21 13:359.1 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 16:46 95-50-102/05/21 13:359.1 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 16:46 541-73-102/05/21 13:359.1 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 16:46 106-46-702/05/21 13:359.1 1
Dichlorodifluoromethane ND ug/kg 02/05/21 16:46 75-71-802/05/21 13:3518.2 1
1,1-Dichloroethane ND ug/kg 02/05/21 16:46 75-34-302/05/21 13:359.1 1
1,2-Dichloroethane ND ug/kg 02/05/21 16:46 107-06-202/05/21 13:359.1 1
1,1-Dichloroethene ND ug/kg 02/05/21 16:46 75-35-402/05/21 13:359.1 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 16:46 156-59-202/05/21 13:359.1 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 16:46 156-60-502/05/21 13:359.1 1
1,2-Dichloropropane ND ug/kg 02/05/21 16:46 78-87-502/05/21 13:359.1 1
1,3-Dichloropropane ND ug/kg 02/05/21 16:46 142-28-902/05/21 13:359.1 1
2,2-Dichloropropane ND ug/kg 02/05/21 16:46 594-20-702/05/21 13:359.1 1
1,1-Dichloropropene ND ug/kg 02/05/21 16:46 563-58-602/05/21 13:359.1 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 16:46 10061-01-502/05/21 13:359.1 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 16:46 10061-02-602/05/21 13:359.1 1
Diisopropyl ether ND ug/kg 02/05/21 16:46 108-20-302/05/21 13:359.1 1
Ethylbenzene ND ug/kg 02/05/21 16:46 100-41-402/05/21 13:359.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 East Lab ID: 92519570008 Collected: 01/29/21 09:51 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 16:46 87-68-302/05/21 13:3518.2 1
2-Hexanone ND ug/kg 02/05/21 16:46 591-78-602/05/21 13:3591.0 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 16:46 98-82-802/05/21 13:359.1 1
p-Isopropyltoluene ND ug/kg 02/05/21 16:46 99-87-602/05/21 13:359.1 1
Methylene Chloride ND ug/kg 02/05/21 16:46 75-09-202/05/21 13:3536.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 16:46 108-10-102/05/21 13:3591.0 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 16:46 1634-04-402/05/21 13:359.1 1
Naphthalene ND ug/kg 02/05/21 16:46 91-20-302/05/21 13:359.1 1
n-Propylbenzene ND ug/kg 02/05/21 16:46 103-65-102/05/21 13:359.1 1
Styrene ND ug/kg 02/05/21 16:46 100-42-502/05/21 13:359.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 16:46 630-20-602/05/21 13:359.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 16:46 79-34-502/05/21 13:359.1 1
Tetrachloroethene ND ug/kg 02/05/21 16:46 127-18-402/05/21 13:359.1 1
Toluene ND ug/kg 02/05/21 16:46 108-88-302/05/21 13:359.1 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 16:46 87-61-602/05/21 13:359.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 16:46 120-82-102/05/21 13:359.1 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 16:46 71-55-602/05/21 13:359.1 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 16:46 79-00-502/05/21 13:359.1 1
Trichloroethene ND ug/kg 02/05/21 16:46 79-01-602/05/21 13:359.1 1
Trichlorofluoromethane ND ug/kg 02/05/21 16:46 75-69-402/05/21 13:359.1 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 16:46 96-18-402/05/21 13:359.1 1
1,2,4-Trimethylbenzene 9.5 ug/kg 02/05/21 16:46 95-63-602/05/21 13:359.1 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 16:46 108-67-802/05/21 13:359.1 1
Vinyl acetate ND ug/kg 02/05/21 16:46 108-05-402/05/21 13:3591.0 1
Vinyl chloride ND ug/kg 02/05/21 16:46 75-01-402/05/21 13:3518.2 1
Xylene (Total)ND ug/kg 02/05/21 16:46 1330-20-702/05/21 13:3518.2 1
m&p-Xylene ND ug/kg 02/05/21 16:46 179601-23-102/05/21 13:3518.2 1
o-Xylene ND ug/kg 02/05/21 16:46 95-47-602/05/21 13:359.1 1
Surrogates
Toluene-d8 (S)101 %02/05/21 16:46 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)103 %02/05/21 16:46 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)102 %02/05/21 16:46 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.5 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 Center Lab ID: 92519570009 Collected: 01/29/21 09:55 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/05/21 05:2102/04/21 11:328.0 1
Surrogates
4-Bromofluorobenzene (S)80 %02/05/21 05:21 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 17:04 67-64-102/05/21 13:35143 1
Benzene ND ug/kg 02/05/21 17:04 71-43-202/05/21 13:357.1 1
Bromobenzene ND ug/kg 02/05/21 17:04 108-86-102/05/21 13:357.1 1
Bromochloromethane ND ug/kg 02/05/21 17:04 74-97-502/05/21 13:357.1 1
Bromodichloromethane ND ug/kg 02/05/21 17:04 75-27-402/05/21 13:357.1 1
Bromoform ND ug/kg 02/05/21 17:04 75-25-202/05/21 13:357.1 1
Bromomethane ND ug/kg 02/05/21 17:04 74-83-902/05/21 13:3514.3 1
2-Butanone (MEK)ND ug/kg 02/05/21 17:04 78-93-302/05/21 13:35143 1
n-Butylbenzene ND ug/kg 02/05/21 17:04 104-51-802/05/21 13:357.1 1
sec-Butylbenzene ND ug/kg 02/05/21 17:04 135-98-802/05/21 13:357.1 1
tert-Butylbenzene ND ug/kg 02/05/21 17:04 98-06-602/05/21 13:357.1 1
Carbon tetrachloride ND ug/kg 02/05/21 17:04 56-23-502/05/21 13:357.1 1
Chlorobenzene ND ug/kg 02/05/21 17:04 108-90-702/05/21 13:357.1 1
Chloroethane ND ug/kg 02/05/21 17:04 75-00-302/05/21 13:3514.3 1
Chloroform ND ug/kg 02/05/21 17:04 67-66-302/05/21 13:357.1 1
Chloromethane ND ug/kg 02/05/21 17:04 74-87-302/05/21 13:3514.3 1
2-Chlorotoluene ND ug/kg 02/05/21 17:04 95-49-802/05/21 13:357.1 1
4-Chlorotoluene ND ug/kg 02/05/21 17:04 106-43-402/05/21 13:357.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 17:04 96-12-802/05/21 13:357.1 1
Dibromochloromethane ND ug/kg 02/05/21 17:04 124-48-102/05/21 13:357.1 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 17:04 106-93-402/05/21 13:357.1 1
Dibromomethane ND ug/kg 02/05/21 17:04 74-95-302/05/21 13:357.1 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 17:04 95-50-102/05/21 13:357.1 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 17:04 541-73-102/05/21 13:357.1 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 17:04 106-46-702/05/21 13:357.1 1
Dichlorodifluoromethane ND ug/kg 02/05/21 17:04 75-71-802/05/21 13:3514.3 1
1,1-Dichloroethane ND ug/kg 02/05/21 17:04 75-34-302/05/21 13:357.1 1
1,2-Dichloroethane ND ug/kg 02/05/21 17:04 107-06-202/05/21 13:357.1 1
1,1-Dichloroethene ND ug/kg 02/05/21 17:04 75-35-402/05/21 13:357.1 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 17:04 156-59-202/05/21 13:357.1 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 17:04 156-60-502/05/21 13:357.1 1
1,2-Dichloropropane ND ug/kg 02/05/21 17:04 78-87-502/05/21 13:357.1 1
1,3-Dichloropropane ND ug/kg 02/05/21 17:04 142-28-902/05/21 13:357.1 1
2,2-Dichloropropane ND ug/kg 02/05/21 17:04 594-20-702/05/21 13:357.1 1
1,1-Dichloropropene ND ug/kg 02/05/21 17:04 563-58-602/05/21 13:357.1 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 17:04 10061-01-502/05/21 13:357.1 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 17:04 10061-02-602/05/21 13:357.1 1
Diisopropyl ether ND ug/kg 02/05/21 17:04 108-20-302/05/21 13:357.1 1
Ethylbenzene ND ug/kg 02/05/21 17:04 100-41-402/05/21 13:357.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 Center Lab ID: 92519570009 Collected: 01/29/21 09:55 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 17:04 87-68-302/05/21 13:3514.3 1
2-Hexanone ND ug/kg 02/05/21 17:04 591-78-602/05/21 13:3571.4 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 17:04 98-82-802/05/21 13:357.1 1
p-Isopropyltoluene ND ug/kg 02/05/21 17:04 99-87-602/05/21 13:357.1 1
Methylene Chloride ND ug/kg 02/05/21 17:04 75-09-202/05/21 13:3528.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 17:04 108-10-102/05/21 13:3571.4 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 17:04 1634-04-402/05/21 13:357.1 1
Naphthalene ND ug/kg 02/05/21 17:04 91-20-302/05/21 13:357.1 1
n-Propylbenzene ND ug/kg 02/05/21 17:04 103-65-102/05/21 13:357.1 1
Styrene ND ug/kg 02/05/21 17:04 100-42-502/05/21 13:357.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 17:04 630-20-602/05/21 13:357.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 17:04 79-34-502/05/21 13:357.1 1
Tetrachloroethene ND ug/kg 02/05/21 17:04 127-18-402/05/21 13:357.1 1
Toluene ND ug/kg 02/05/21 17:04 108-88-302/05/21 13:357.1 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 17:04 87-61-602/05/21 13:357.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 17:04 120-82-102/05/21 13:357.1 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 17:04 71-55-602/05/21 13:357.1 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 17:04 79-00-502/05/21 13:357.1 1
Trichloroethene ND ug/kg 02/05/21 17:04 79-01-602/05/21 13:357.1 1
Trichlorofluoromethane ND ug/kg 02/05/21 17:04 75-69-402/05/21 13:357.1 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 17:04 96-18-402/05/21 13:357.1 1
1,2,4-Trimethylbenzene ND ug/kg 02/05/21 17:04 95-63-602/05/21 13:357.1 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 17:04 108-67-802/05/21 13:357.1 1
Vinyl acetate ND ug/kg 02/05/21 17:04 108-05-402/05/21 13:3571.4 1
Vinyl chloride ND ug/kg 02/05/21 17:04 75-01-402/05/21 13:3514.3 1
Xylene (Total)ND ug/kg 02/05/21 17:04 1330-20-702/05/21 13:3514.3 1
m&p-Xylene ND ug/kg 02/05/21 17:04 179601-23-102/05/21 13:3514.3 1
o-Xylene ND ug/kg 02/05/21 17:04 95-47-602/05/21 13:357.1 1
Surrogates
Toluene-d8 (S)100 %02/05/21 17:04 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)102 %02/05/21 17:04 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)108 %02/05/21 17:04 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 West Lab ID: 92519570010 Collected: 01/29/21 09:59 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/05/21 05:4902/04/21 11:3211.0 1
Surrogates
4-Bromofluorobenzene (S)83 %02/05/21 05:49 460-00-402/04/21 11:3266-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 17:22 67-64-102/05/21 13:35167 1
Benzene ND ug/kg 02/05/21 17:22 71-43-202/05/21 13:358.3 1
Bromobenzene ND ug/kg 02/05/21 17:22 108-86-102/05/21 13:358.3 1
Bromochloromethane ND ug/kg 02/05/21 17:22 74-97-502/05/21 13:358.3 1
Bromodichloromethane ND ug/kg 02/05/21 17:22 75-27-402/05/21 13:358.3 1
Bromoform ND ug/kg 02/05/21 17:22 75-25-202/05/21 13:358.3 1
Bromomethane ND ug/kg 02/05/21 17:22 74-83-902/05/21 13:3516.7 1
2-Butanone (MEK)ND ug/kg 02/05/21 17:22 78-93-302/05/21 13:35167 1
n-Butylbenzene ND ug/kg 02/05/21 17:22 104-51-802/05/21 13:358.3 1
sec-Butylbenzene ND ug/kg 02/05/21 17:22 135-98-802/05/21 13:358.3 1
tert-Butylbenzene ND ug/kg 02/05/21 17:22 98-06-602/05/21 13:358.3 1
Carbon tetrachloride ND ug/kg 02/05/21 17:22 56-23-502/05/21 13:358.3 1
Chlorobenzene ND ug/kg 02/05/21 17:22 108-90-702/05/21 13:358.3 1
Chloroethane ND ug/kg 02/05/21 17:22 75-00-302/05/21 13:3516.7 1
Chloroform ND ug/kg 02/05/21 17:22 67-66-302/05/21 13:358.3 1
Chloromethane ND ug/kg 02/05/21 17:22 74-87-302/05/21 13:3516.7 1
2-Chlorotoluene ND ug/kg 02/05/21 17:22 95-49-802/05/21 13:358.3 1
4-Chlorotoluene ND ug/kg 02/05/21 17:22 106-43-402/05/21 13:358.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 17:22 96-12-802/05/21 13:358.3 1
Dibromochloromethane ND ug/kg 02/05/21 17:22 124-48-102/05/21 13:358.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 17:22 106-93-402/05/21 13:358.3 1
Dibromomethane ND ug/kg 02/05/21 17:22 74-95-302/05/21 13:358.3 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 17:22 95-50-102/05/21 13:358.3 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 17:22 541-73-102/05/21 13:358.3 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 17:22 106-46-702/05/21 13:358.3 1
Dichlorodifluoromethane ND ug/kg 02/05/21 17:22 75-71-802/05/21 13:3516.7 1
1,1-Dichloroethane ND ug/kg 02/05/21 17:22 75-34-302/05/21 13:358.3 1
1,2-Dichloroethane ND ug/kg 02/05/21 17:22 107-06-202/05/21 13:358.3 1
1,1-Dichloroethene ND ug/kg 02/05/21 17:22 75-35-402/05/21 13:358.3 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 17:22 156-59-202/05/21 13:358.3 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 17:22 156-60-502/05/21 13:358.3 1
1,2-Dichloropropane ND ug/kg 02/05/21 17:22 78-87-502/05/21 13:358.3 1
1,3-Dichloropropane ND ug/kg 02/05/21 17:22 142-28-902/05/21 13:358.3 1
2,2-Dichloropropane ND ug/kg 02/05/21 17:22 594-20-702/05/21 13:358.3 1
1,1-Dichloropropene ND ug/kg 02/05/21 17:22 563-58-602/05/21 13:358.3 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 17:22 10061-01-502/05/21 13:358.3 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 17:22 10061-02-602/05/21 13:358.3 1
Diisopropyl ether ND ug/kg 02/05/21 17:22 108-20-302/05/21 13:358.3 1
Ethylbenzene 9.4 ug/kg 02/05/21 17:22 100-41-402/05/21 13:358.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 4 West Lab ID: 92519570010 Collected: 01/29/21 09:59 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 17:22 87-68-302/05/21 13:3516.7 1
2-Hexanone ND ug/kg 02/05/21 17:22 591-78-602/05/21 13:3583.5 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 17:22 98-82-802/05/21 13:358.3 1
p-Isopropyltoluene ND ug/kg 02/05/21 17:22 99-87-602/05/21 13:358.3 1
Methylene Chloride ND ug/kg 02/05/21 17:22 75-09-202/05/21 13:3533.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 17:22 108-10-102/05/21 13:3583.5 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 17:22 1634-04-402/05/21 13:358.3 1
Naphthalene 11.9 ug/kg 02/05/21 17:22 91-20-302/05/21 13:358.3 1
n-Propylbenzene ND ug/kg 02/05/21 17:22 103-65-102/05/21 13:358.3 1
Styrene ND ug/kg 02/05/21 17:22 100-42-502/05/21 13:358.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 17:22 630-20-602/05/21 13:358.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 17:22 79-34-502/05/21 13:358.3 1
Tetrachloroethene ND ug/kg 02/05/21 17:22 127-18-402/05/21 13:358.3 1
Toluene 21.2 ug/kg 02/05/21 17:22 108-88-302/05/21 13:358.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 17:22 87-61-602/05/21 13:358.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 17:22 120-82-102/05/21 13:358.3 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 17:22 71-55-602/05/21 13:358.3 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 17:22 79-00-502/05/21 13:358.3 1
Trichloroethene ND ug/kg 02/05/21 17:22 79-01-602/05/21 13:358.3 1
Trichlorofluoromethane ND ug/kg 02/05/21 17:22 75-69-402/05/21 13:358.3 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 17:22 96-18-402/05/21 13:358.3 1
1,2,4-Trimethylbenzene 55.4 ug/kg 02/05/21 17:22 95-63-602/05/21 13:358.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 17:22 108-67-802/05/21 13:358.3 1
Vinyl acetate ND ug/kg 02/05/21 17:22 108-05-402/05/21 13:3583.5 1
Vinyl chloride ND ug/kg 02/05/21 17:22 75-01-402/05/21 13:3516.7 1
Xylene (Total)74.7 ug/kg 02/05/21 17:22 1330-20-702/05/21 13:3516.7 1
m&p-Xylene 51.5 ug/kg 02/05/21 17:22 179601-23-102/05/21 13:3516.7 1
o-Xylene 23.2 ug/kg 02/05/21 17:22 95-47-602/05/21 13:358.3 1
Surrogates
Toluene-d8 (S)100 %02/05/21 17:22 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)102 %02/05/21 17:22 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)107 %02/05/21 17:22 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.4 %02/01/21 16:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 East Lab ID: 92519570011 Collected: 01/29/21 10:22 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/05/21 00:1202/04/21 12:0912.7 1
Surrogates
4-Bromofluorobenzene (S)85 %02/05/21 00:12 460-00-402/04/21 12:0966-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 17:40 67-64-102/05/21 13:35220 1
Benzene ND ug/kg 02/05/21 17:40 71-43-202/05/21 13:3511.0 1
Bromobenzene ND ug/kg 02/05/21 17:40 108-86-102/05/21 13:3511.0 1
Bromochloromethane ND ug/kg 02/05/21 17:40 74-97-502/05/21 13:3511.0 1
Bromodichloromethane ND ug/kg 02/05/21 17:40 75-27-402/05/21 13:3511.0 1
Bromoform ND ug/kg 02/05/21 17:40 75-25-202/05/21 13:3511.0 1
Bromomethane ND ug/kg 02/05/21 17:40 74-83-902/05/21 13:3522.0 1
2-Butanone (MEK)ND ug/kg 02/05/21 17:40 78-93-302/05/21 13:35220 1
n-Butylbenzene ND ug/kg 02/05/21 17:40 104-51-802/05/21 13:3511.0 1
sec-Butylbenzene ND ug/kg 02/05/21 17:40 135-98-802/05/21 13:3511.0 1
tert-Butylbenzene ND ug/kg 02/05/21 17:40 98-06-602/05/21 13:3511.0 1
Carbon tetrachloride ND ug/kg 02/05/21 17:40 56-23-502/05/21 13:3511.0 1
Chlorobenzene ND ug/kg 02/05/21 17:40 108-90-702/05/21 13:3511.0 1
Chloroethane ND ug/kg 02/05/21 17:40 75-00-302/05/21 13:3522.0 1
Chloroform ND ug/kg 02/05/21 17:40 67-66-302/05/21 13:3511.0 1
Chloromethane ND ug/kg 02/05/21 17:40 74-87-302/05/21 13:3522.0 1
2-Chlorotoluene ND ug/kg 02/05/21 17:40 95-49-802/05/21 13:3511.0 1
4-Chlorotoluene ND ug/kg 02/05/21 17:40 106-43-402/05/21 13:3511.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 17:40 96-12-802/05/21 13:3511.0 1
Dibromochloromethane ND ug/kg 02/05/21 17:40 124-48-102/05/21 13:3511.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 17:40 106-93-402/05/21 13:3511.0 1
Dibromomethane ND ug/kg 02/05/21 17:40 74-95-302/05/21 13:3511.0 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 17:40 95-50-102/05/21 13:3511.0 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 17:40 541-73-102/05/21 13:3511.0 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 17:40 106-46-702/05/21 13:3511.0 1
Dichlorodifluoromethane ND ug/kg 02/05/21 17:40 75-71-802/05/21 13:3522.0 1
1,1-Dichloroethane ND ug/kg 02/05/21 17:40 75-34-302/05/21 13:3511.0 1
1,2-Dichloroethane ND ug/kg 02/05/21 17:40 107-06-202/05/21 13:3511.0 1
1,1-Dichloroethene ND ug/kg 02/05/21 17:40 75-35-402/05/21 13:3511.0 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 17:40 156-59-202/05/21 13:3511.0 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 17:40 156-60-502/05/21 13:3511.0 1
1,2-Dichloropropane ND ug/kg 02/05/21 17:40 78-87-502/05/21 13:3511.0 1
1,3-Dichloropropane ND ug/kg 02/05/21 17:40 142-28-902/05/21 13:3511.0 1
2,2-Dichloropropane ND ug/kg 02/05/21 17:40 594-20-702/05/21 13:3511.0 1
1,1-Dichloropropene ND ug/kg 02/05/21 17:40 563-58-602/05/21 13:3511.0 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 17:40 10061-01-502/05/21 13:3511.0 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 17:40 10061-02-602/05/21 13:3511.0 1
Diisopropyl ether ND ug/kg 02/05/21 17:40 108-20-302/05/21 13:3511.0 1
Ethylbenzene ND ug/kg 02/05/21 17:40 100-41-402/05/21 13:3511.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 East Lab ID: 92519570011 Collected: 01/29/21 10:22 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 17:40 87-68-302/05/21 13:3522.0 1
2-Hexanone ND ug/kg 02/05/21 17:40 591-78-602/05/21 13:35110 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 17:40 98-82-802/05/21 13:3511.0 1
p-Isopropyltoluene ND ug/kg 02/05/21 17:40 99-87-602/05/21 13:3511.0 1
Methylene Chloride ND ug/kg 02/05/21 17:40 75-09-202/05/21 13:3544.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 17:40 108-10-102/05/21 13:35110 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 17:40 1634-04-402/05/21 13:3511.0 1
Naphthalene ND ug/kg 02/05/21 17:40 91-20-302/05/21 13:3511.0 1
n-Propylbenzene ND ug/kg 02/05/21 17:40 103-65-102/05/21 13:3511.0 1
Styrene ND ug/kg 02/05/21 17:40 100-42-502/05/21 13:3511.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 17:40 630-20-602/05/21 13:3511.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 17:40 79-34-502/05/21 13:3511.0 1
Tetrachloroethene ND ug/kg 02/05/21 17:40 127-18-402/05/21 13:3511.0 1
Toluene 13.6 ug/kg 02/05/21 17:40 108-88-302/05/21 13:3511.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 17:40 87-61-602/05/21 13:3511.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 17:40 120-82-102/05/21 13:3511.0 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 17:40 71-55-602/05/21 13:3511.0 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 17:40 79-00-502/05/21 13:3511.0 1
Trichloroethene ND ug/kg 02/05/21 17:40 79-01-602/05/21 13:3511.0 1
Trichlorofluoromethane ND ug/kg 02/05/21 17:40 75-69-402/05/21 13:3511.0 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 17:40 96-18-402/05/21 13:3511.0 1
1,2,4-Trimethylbenzene 13.6 ug/kg 02/05/21 17:40 95-63-602/05/21 13:3511.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 17:40 108-67-802/05/21 13:3511.0 1
Vinyl acetate ND ug/kg 02/05/21 17:40 108-05-402/05/21 13:35110 1
Vinyl chloride ND ug/kg 02/05/21 17:40 75-01-402/05/21 13:3522.0 1
Xylene (Total)ND ug/kg 02/05/21 17:40 1330-20-702/05/21 13:3522.0 1
m&p-Xylene ND ug/kg 02/05/21 17:40 179601-23-102/05/21 13:3522.0 1
o-Xylene ND ug/kg 02/05/21 17:40 95-47-602/05/21 13:3511.0 1
Surrogates
Toluene-d8 (S)100 %02/05/21 17:40 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)99 %02/05/21 17:40 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)104 %02/05/21 17:40 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.4 %02/01/21 16:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 Center Lab ID: 92519570012 Collected: 01/29/21 10:27 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/05/21 01:0802/04/21 12:0910.7 1
Surrogates
4-Bromofluorobenzene (S)84 %02/05/21 01:08 460-00-402/04/21 12:0966-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 17:58 67-64-102/05/21 13:35159 1
Benzene ND ug/kg 02/05/21 17:58 71-43-202/05/21 13:357.9 1
Bromobenzene ND ug/kg 02/05/21 17:58 108-86-102/05/21 13:357.9 1
Bromochloromethane ND ug/kg 02/05/21 17:58 74-97-502/05/21 13:357.9 1
Bromodichloromethane ND ug/kg 02/05/21 17:58 75-27-402/05/21 13:357.9 1
Bromoform ND ug/kg 02/05/21 17:58 75-25-202/05/21 13:357.9 1
Bromomethane ND ug/kg 02/05/21 17:58 74-83-902/05/21 13:3515.9 1
2-Butanone (MEK)ND ug/kg 02/05/21 17:58 78-93-302/05/21 13:35159 1
n-Butylbenzene ND ug/kg 02/05/21 17:58 104-51-802/05/21 13:357.9 1
sec-Butylbenzene ND ug/kg 02/05/21 17:58 135-98-802/05/21 13:357.9 1
tert-Butylbenzene ND ug/kg 02/05/21 17:58 98-06-602/05/21 13:357.9 1
Carbon tetrachloride ND ug/kg 02/05/21 17:58 56-23-502/05/21 13:357.9 1
Chlorobenzene ND ug/kg 02/05/21 17:58 108-90-702/05/21 13:357.9 1
Chloroethane ND ug/kg 02/05/21 17:58 75-00-302/05/21 13:3515.9 1
Chloroform ND ug/kg 02/05/21 17:58 67-66-302/05/21 13:357.9 1
Chloromethane ND ug/kg 02/05/21 17:58 74-87-302/05/21 13:3515.9 1
2-Chlorotoluene ND ug/kg 02/05/21 17:58 95-49-802/05/21 13:357.9 1
4-Chlorotoluene ND ug/kg 02/05/21 17:58 106-43-402/05/21 13:357.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 17:58 96-12-802/05/21 13:357.9 1
Dibromochloromethane ND ug/kg 02/05/21 17:58 124-48-102/05/21 13:357.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 17:58 106-93-402/05/21 13:357.9 1
Dibromomethane ND ug/kg 02/05/21 17:58 74-95-302/05/21 13:357.9 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 17:58 95-50-102/05/21 13:357.9 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 17:58 541-73-102/05/21 13:357.9 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 17:58 106-46-702/05/21 13:357.9 1
Dichlorodifluoromethane ND ug/kg 02/05/21 17:58 75-71-802/05/21 13:3515.9 1
1,1-Dichloroethane ND ug/kg 02/05/21 17:58 75-34-302/05/21 13:357.9 1
1,2-Dichloroethane ND ug/kg 02/05/21 17:58 107-06-202/05/21 13:357.9 1
1,1-Dichloroethene ND ug/kg 02/05/21 17:58 75-35-402/05/21 13:357.9 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 17:58 156-59-202/05/21 13:357.9 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 17:58 156-60-502/05/21 13:357.9 1
1,2-Dichloropropane ND ug/kg 02/05/21 17:58 78-87-502/05/21 13:357.9 1
1,3-Dichloropropane ND ug/kg 02/05/21 17:58 142-28-902/05/21 13:357.9 1
2,2-Dichloropropane ND ug/kg 02/05/21 17:58 594-20-702/05/21 13:357.9 1
1,1-Dichloropropene ND ug/kg 02/05/21 17:58 563-58-602/05/21 13:357.9 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 17:58 10061-01-502/05/21 13:357.9 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 17:58 10061-02-602/05/21 13:357.9 1
Diisopropyl ether ND ug/kg 02/05/21 17:58 108-20-302/05/21 13:357.9 1
Ethylbenzene 8.2 ug/kg 02/05/21 17:58 100-41-402/05/21 13:357.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 Center Lab ID: 92519570012 Collected: 01/29/21 10:27 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 17:58 87-68-302/05/21 13:3515.9 1
2-Hexanone ND ug/kg 02/05/21 17:58 591-78-602/05/21 13:3579.5 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 17:58 98-82-802/05/21 13:357.9 1
p-Isopropyltoluene ND ug/kg 02/05/21 17:58 99-87-602/05/21 13:357.9 1
Methylene Chloride ND ug/kg 02/05/21 17:58 75-09-202/05/21 13:3531.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 17:58 108-10-102/05/21 13:3579.5 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 17:58 1634-04-402/05/21 13:357.9 1
Naphthalene ND ug/kg 02/05/21 17:58 91-20-302/05/21 13:357.9 1
n-Propylbenzene ND ug/kg 02/05/21 17:58 103-65-102/05/21 13:357.9 1
Styrene ND ug/kg 02/05/21 17:58 100-42-502/05/21 13:357.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 17:58 630-20-602/05/21 13:357.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 17:58 79-34-502/05/21 13:357.9 1
Tetrachloroethene ND ug/kg 02/05/21 17:58 127-18-402/05/21 13:357.9 1
Toluene ND ug/kg 02/05/21 17:58 108-88-302/05/21 13:357.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 17:58 87-61-602/05/21 13:357.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 17:58 120-82-102/05/21 13:357.9 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 17:58 71-55-602/05/21 13:357.9 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 17:58 79-00-502/05/21 13:357.9 1
Trichloroethene ND ug/kg 02/05/21 17:58 79-01-602/05/21 13:357.9 1
Trichlorofluoromethane ND ug/kg 02/05/21 17:58 75-69-402/05/21 13:357.9 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 17:58 96-18-402/05/21 13:357.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/05/21 17:58 95-63-602/05/21 13:357.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 17:58 108-67-802/05/21 13:357.9 1
Vinyl acetate ND ug/kg 02/05/21 17:58 108-05-402/05/21 13:3579.5 1
Vinyl chloride ND ug/kg 02/05/21 17:58 75-01-402/05/21 13:3515.9 1
Xylene (Total)ND ug/kg 02/05/21 17:58 1330-20-702/05/21 13:3515.9 1
m&p-Xylene ND ug/kg 02/05/21 17:58 179601-23-102/05/21 13:3515.9 1
o-Xylene ND ug/kg 02/05/21 17:58 95-47-602/05/21 13:357.9 1
Surrogates
Toluene-d8 (S)101 %02/05/21 17:58 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)103 %02/05/21 17:58 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)102 %02/05/21 17:58 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.3 %02/01/21 17:23 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 West Lab ID: 92519570013 Collected: 01/29/21 10:33 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/05/21 01:3602/04/21 12:099.3 1
Surrogates
4-Bromofluorobenzene (S)83 %02/05/21 01:36 460-00-402/04/21 12:0966-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/05/21 18:16 67-64-102/05/21 13:35183 1
Benzene ND ug/kg 02/05/21 18:16 71-43-202/05/21 13:359.2 1
Bromobenzene ND ug/kg 02/05/21 18:16 108-86-102/05/21 13:359.2 1
Bromochloromethane ND ug/kg 02/05/21 18:16 74-97-502/05/21 13:359.2 1
Bromodichloromethane ND ug/kg 02/05/21 18:16 75-27-402/05/21 13:359.2 1
Bromoform ND ug/kg 02/05/21 18:16 75-25-202/05/21 13:359.2 1
Bromomethane ND ug/kg 02/05/21 18:16 74-83-902/05/21 13:3518.3 1
2-Butanone (MEK)ND ug/kg 02/05/21 18:16 78-93-302/05/21 13:35183 1
n-Butylbenzene ND ug/kg 02/05/21 18:16 104-51-802/05/21 13:359.2 1
sec-Butylbenzene ND ug/kg 02/05/21 18:16 135-98-802/05/21 13:359.2 1
tert-Butylbenzene ND ug/kg 02/05/21 18:16 98-06-602/05/21 13:359.2 1
Carbon tetrachloride ND ug/kg 02/05/21 18:16 56-23-502/05/21 13:359.2 1
Chlorobenzene ND ug/kg 02/05/21 18:16 108-90-702/05/21 13:359.2 1
Chloroethane ND ug/kg 02/05/21 18:16 75-00-302/05/21 13:3518.3 1
Chloroform ND ug/kg 02/05/21 18:16 67-66-302/05/21 13:359.2 1
Chloromethane ND ug/kg 02/05/21 18:16 74-87-302/05/21 13:3518.3 1
2-Chlorotoluene ND ug/kg 02/05/21 18:16 95-49-802/05/21 13:359.2 1
4-Chlorotoluene ND ug/kg 02/05/21 18:16 106-43-402/05/21 13:359.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/05/21 18:16 96-12-802/05/21 13:359.2 1
Dibromochloromethane ND ug/kg 02/05/21 18:16 124-48-102/05/21 13:359.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/05/21 18:16 106-93-402/05/21 13:359.2 1
Dibromomethane ND ug/kg 02/05/21 18:16 74-95-302/05/21 13:359.2 1
1,2-Dichlorobenzene ND ug/kg 02/05/21 18:16 95-50-102/05/21 13:359.2 1
1,3-Dichlorobenzene ND ug/kg 02/05/21 18:16 541-73-102/05/21 13:359.2 1
1,4-Dichlorobenzene ND ug/kg 02/05/21 18:16 106-46-702/05/21 13:359.2 1
Dichlorodifluoromethane ND ug/kg 02/05/21 18:16 75-71-802/05/21 13:3518.3 1
1,1-Dichloroethane ND ug/kg 02/05/21 18:16 75-34-302/05/21 13:359.2 1
1,2-Dichloroethane ND ug/kg 02/05/21 18:16 107-06-202/05/21 13:359.2 1
1,1-Dichloroethene ND ug/kg 02/05/21 18:16 75-35-402/05/21 13:359.2 1
cis-1,2-Dichloroethene ND ug/kg 02/05/21 18:16 156-59-202/05/21 13:359.2 1
trans-1,2-Dichloroethene ND ug/kg 02/05/21 18:16 156-60-502/05/21 13:359.2 1
1,2-Dichloropropane ND ug/kg 02/05/21 18:16 78-87-502/05/21 13:359.2 1
1,3-Dichloropropane ND ug/kg 02/05/21 18:16 142-28-902/05/21 13:359.2 1
2,2-Dichloropropane ND ug/kg 02/05/21 18:16 594-20-702/05/21 13:359.2 1
1,1-Dichloropropene ND ug/kg 02/05/21 18:16 563-58-602/05/21 13:359.2 1
cis-1,3-Dichloropropene ND ug/kg 02/05/21 18:16 10061-01-502/05/21 13:359.2 1
trans-1,3-Dichloropropene ND ug/kg 02/05/21 18:16 10061-02-602/05/21 13:359.2 1
Diisopropyl ether ND ug/kg 02/05/21 18:16 108-20-302/05/21 13:359.2 1
Ethylbenzene 18.7 ug/kg 02/05/21 18:16 100-41-402/05/21 13:359.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 47
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Sample: Gas UST 5 West Lab ID: 92519570013 Collected: 01/29/21 10:33 Received: 02/01/21 10:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/05/21 18:16 87-68-302/05/21 13:3518.3 1
2-Hexanone ND ug/kg 02/05/21 18:16 591-78-602/05/21 13:3591.7 1
Isopropylbenzene (Cumene)ND ug/kg 02/05/21 18:16 98-82-802/05/21 13:359.2 1
p-Isopropyltoluene ND ug/kg 02/05/21 18:16 99-87-602/05/21 13:359.2 1
Methylene Chloride ND ug/kg 02/05/21 18:16 75-09-202/05/21 13:3536.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/05/21 18:16 108-10-102/05/21 13:3591.7 1
Methyl-tert-butyl ether ND ug/kg 02/05/21 18:16 1634-04-402/05/21 13:359.2 1
Naphthalene 15.0 ug/kg 02/05/21 18:16 91-20-302/05/21 13:359.2 1
n-Propylbenzene ND ug/kg 02/05/21 18:16 103-65-102/05/21 13:359.2 1
Styrene ND ug/kg 02/05/21 18:16 100-42-502/05/21 13:359.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/05/21 18:16 630-20-602/05/21 13:359.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/05/21 18:16 79-34-502/05/21 13:359.2 1
Tetrachloroethene ND ug/kg 02/05/21 18:16 127-18-402/05/21 13:359.2 1
Toluene 16.8 ug/kg 02/05/21 18:16 108-88-302/05/21 13:359.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/05/21 18:16 87-61-602/05/21 13:359.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/05/21 18:16 120-82-102/05/21 13:359.2 1
1,1,1-Trichloroethane ND ug/kg 02/05/21 18:16 71-55-602/05/21 13:359.2 1
1,1,2-Trichloroethane ND ug/kg 02/05/21 18:16 79-00-502/05/21 13:359.2 1
Trichloroethene ND ug/kg 02/05/21 18:16 79-01-602/05/21 13:359.2 1
Trichlorofluoromethane ND ug/kg 02/05/21 18:16 75-69-402/05/21 13:359.2 1
1,2,3-Trichloropropane ND ug/kg 02/05/21 18:16 96-18-402/05/21 13:359.2 1
1,2,4-Trimethylbenzene 98.9 ug/kg 02/05/21 18:16 95-63-602/05/21 13:359.2 1
1,3,5-Trimethylbenzene ND ug/kg 02/05/21 18:16 108-67-802/05/21 13:359.2 1
Vinyl acetate ND ug/kg 02/05/21 18:16 108-05-402/05/21 13:3591.7 1
Vinyl chloride ND ug/kg 02/05/21 18:16 75-01-402/05/21 13:3518.3 1
Xylene (Total)127 ug/kg 02/05/21 18:16 1330-20-702/05/21 13:3518.3 1
m&p-Xylene 85.2 ug/kg 02/05/21 18:16 179601-23-102/05/21 13:3518.3 1
o-Xylene 41.9 ug/kg 02/05/21 18:16 95-47-602/05/21 13:359.2 1
Surrogates
Toluene-d8 (S)100 %02/05/21 18:16 2037-26-502/05/21 13:3570-130 1
4-Bromofluorobenzene (S)101 %02/05/21 18:16 460-00-402/05/21 13:3569-134 1
1,2-Dichloroethane-d4 (S)104 %02/05/21 18:16 17060-07-002/05/21 13:3570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.1 %02/01/21 17:24 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597663
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519570001, 92519570002, 92519570005, 92519570006, 92519570007, 92519570008, 92519570009,
92519570010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3151395
Associated Lab Samples: 92519570001, 92519570002, 92519570005, 92519570006, 92519570007, 92519570008, 92519570009,
92519570010
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 5.9 02/04/21 13:33
4-Bromofluorobenzene (S)%82 66-131 02/04/21 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151396LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.949.5 97 70-130
4-Bromofluorobenzene (S)%86 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151398MATRIX SPIKE SAMPLE:
MSSpike
Result
92519784010
Gas Range Organics (C6-C10)mg/kg 104109 94 70-145ND
4-Bromofluorobenzene (S)%87 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92519784009
3151397SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg 6.2JND
4-Bromofluorobenzene (S)%9092
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597677
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92519570011, 92519570012, 92519570013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3151571
Associated Lab Samples:92519570011, 92519570012, 92519570013
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 5.9 02/04/21 14:01
4-Bromofluorobenzene (S)%88 66-131 02/04/21 14:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151572LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.749.5 96 70-130
4-Bromofluorobenzene (S)%89 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151574MATRIX SPIKE SAMPLE:
MSSpike
Result
92519570012
Gas Range Organics (C6-C10)mg/kg 85.689.3 95 70-145ND
4-Bromofluorobenzene (S)%87 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92519570011
3151573SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%8185
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
598062
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519570005, 92519570006, 92519570007, 92519570008, 92519570009, 92519570010, 92519570011,
92519570012, 92519570013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3153622
Associated Lab Samples: 92519570005, 92519570006, 92519570007, 92519570008, 92519570009, 92519570010, 92519570011,
92519570012, 92519570013
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 02/05/21 11:21
1,1,1-Trichloroethane ug/kg ND 5.0 02/05/21 11:21
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 02/05/21 11:21
1,1,2-Trichloroethane ug/kg ND 5.0 02/05/21 11:21
1,1-Dichloroethane ug/kg ND 5.0 02/05/21 11:21
1,1-Dichloroethene ug/kg ND 5.0 02/05/21 11:21
1,1-Dichloropropene ug/kg ND 5.0 02/05/21 11:21
1,2,3-Trichlorobenzene ug/kg ND 5.0 02/05/21 11:21
1,2,3-Trichloropropane ug/kg ND 5.0 02/05/21 11:21
1,2,4-Trichlorobenzene ug/kg ND 5.0 02/05/21 11:21
1,2,4-Trimethylbenzene ug/kg ND 5.0 02/05/21 11:21
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 02/05/21 11:21
1,2-Dibromoethane (EDB)ug/kg ND 5.0 02/05/21 11:21
1,2-Dichlorobenzene ug/kg ND 5.0 02/05/21 11:21
1,2-Dichloroethane ug/kg ND 5.0 02/05/21 11:21
1,2-Dichloropropane ug/kg ND 5.0 02/05/21 11:21
1,3,5-Trimethylbenzene ug/kg ND 5.0 02/05/21 11:21
1,3-Dichlorobenzene ug/kg ND 5.0 02/05/21 11:21
1,3-Dichloropropane ug/kg ND 5.0 02/05/21 11:21
1,4-Dichlorobenzene ug/kg ND 5.0 02/05/21 11:21
2,2-Dichloropropane ug/kg ND 5.0 02/05/21 11:21
2-Butanone (MEK)ug/kg ND 100 02/05/21 11:21
2-Chlorotoluene ug/kg ND 5.0 02/05/21 11:21
2-Hexanone ug/kg ND 50.0 02/05/21 11:21
4-Chlorotoluene ug/kg ND 5.0 02/05/21 11:21
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 02/05/21 11:21
Acetone ug/kg ND 100 02/05/21 11:21
Benzene ug/kg ND 5.0 02/05/21 11:21
Bromobenzene ug/kg ND 5.0 02/05/21 11:21
Bromochloromethane ug/kg ND 5.0 02/05/21 11:21
Bromodichloromethane ug/kg ND 5.0 02/05/21 11:21
Bromoform ug/kg ND 5.0 02/05/21 11:21
Bromomethane ug/kg ND 10.0 02/05/21 11:21
Carbon tetrachloride ug/kg ND 5.0 02/05/21 11:21
Chlorobenzene ug/kg ND 5.0 02/05/21 11:21
Chloroethane ug/kg ND 10.0 02/05/21 11:21
Chloroform ug/kg ND 5.0 02/05/21 11:21
Chloromethane ug/kg ND 10.0 02/05/21 11:21
cis-1,2-Dichloroethene ug/kg ND 5.0 02/05/21 11:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3153622
Associated Lab Samples: 92519570005, 92519570006, 92519570007, 92519570008, 92519570009, 92519570010, 92519570011,
92519570012, 92519570013
Matrix: Solid
Analyzed
cis-1,3-Dichloropropene ug/kg ND 5.0 02/05/21 11:21
Dibromochloromethane ug/kg ND 5.0 02/05/21 11:21
Dibromomethane ug/kg ND 5.0 02/05/21 11:21
Dichlorodifluoromethane ug/kg ND 10.0 02/05/21 11:21
Diisopropyl ether ug/kg ND 5.0 02/05/21 11:21
Ethylbenzene ug/kg ND 5.0 02/05/21 11:21
Hexachloro-1,3-butadiene ug/kg ND 10.0 02/05/21 11:21
Isopropylbenzene (Cumene)ug/kg ND 5.0 02/05/21 11:21
m&p-Xylene ug/kg ND 10.0 02/05/21 11:21
Methyl-tert-butyl ether ug/kg ND 5.0 02/05/21 11:21
Methylene Chloride ug/kg ND 20.0 02/05/21 11:21
n-Butylbenzene ug/kg ND 5.0 02/05/21 11:21
n-Propylbenzene ug/kg ND 5.0 02/05/21 11:21
Naphthalene ug/kg ND 5.0 02/05/21 11:21
o-Xylene ug/kg ND 5.0 02/05/21 11:21
p-Isopropyltoluene ug/kg ND 5.0 02/05/21 11:21
sec-Butylbenzene ug/kg ND 5.0 02/05/21 11:21
Styrene ug/kg ND 5.0 02/05/21 11:21
tert-Butylbenzene ug/kg ND 5.0 02/05/21 11:21
Tetrachloroethene ug/kg ND 5.0 02/05/21 11:21
Toluene ug/kg ND 5.0 02/05/21 11:21
trans-1,2-Dichloroethene ug/kg ND 5.0 02/05/21 11:21
trans-1,3-Dichloropropene ug/kg ND 5.0 02/05/21 11:21
Trichloroethene ug/kg ND 5.0 02/05/21 11:21
Trichlorofluoromethane ug/kg ND 5.0 02/05/21 11:21
Vinyl acetate ug/kg ND 50.0 02/05/21 11:21
Vinyl chloride ug/kg ND 10.0 02/05/21 11:21
Xylene (Total)ug/kg ND 10.0 02/05/21 11:21
1,2-Dichloroethane-d4 (S)%105 70-130 02/05/21 11:21
4-Bromofluorobenzene (S)%99 69-134 02/05/21 11:21
Toluene-d8 (S)%99 70-130 02/05/21 11:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153623LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11401250 91 70-130
1,1,1-Trichloroethane ug/kg 11101250 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 11301250 91 70-130
1,1,2-Trichloroethane ug/kg 11201250 90 70-130
1,1-Dichloroethane ug/kg 11201250 90 70-130
1,1-Dichloroethene ug/kg 12201250 98 70-130
1,1-Dichloropropene ug/kg 11201250 90 70-130
1,2,3-Trichlorobenzene ug/kg 10701250 86 65-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153623LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 11101250 89 70-130
1,2,4-Trichlorobenzene ug/kg 11201250 90 68-130
1,2,4-Trimethylbenzene ug/kg 11001250 88 70-130
1,2-Dibromo-3-chloropropane ug/kg 11701250 93 70-130
1,2-Dibromoethane (EDB)ug/kg 11601250 93 70-130
1,2-Dichlorobenzene ug/kg 11401250 91 70-130
1,2-Dichloroethane ug/kg 11001250 88 63-130
1,2-Dichloropropane ug/kg 11201250 90 70-130
1,3,5-Trimethylbenzene ug/kg 11401250 91 70-130
1,3-Dichlorobenzene ug/kg 11201250 90 70-130
1,3-Dichloropropane ug/kg 11101250 89 70-130
1,4-Dichlorobenzene ug/kg 11301250 91 70-130
2,2-Dichloropropane ug/kg 11201250 90 66-130
2-Butanone (MEK)ug/kg 23302500 93 70-130
2-Chlorotoluene ug/kg 11801250 95 70-130
2-Hexanone ug/kg 23502500 94 70-130
4-Chlorotoluene ug/kg 11401250 91 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 22702500 91 70-130
Acetone ug/kg 22202500 89 69-130
Benzene ug/kg 10901250 87 70-130
Bromobenzene ug/kg 11601250 93 70-130
Bromochloromethane ug/kg 11001250 88 70-130
Bromodichloromethane ug/kg 11101250 89 69-130
Bromoform ug/kg 11801250 94 70-130
Bromomethane ug/kg 10301250 83 52-130
Carbon tetrachloride ug/kg 11801250 94 70-130
Chlorobenzene ug/kg 11001250 88 70-130
Chloroethane ug/kg 11801250 95 65-130
Chloroform ug/kg 10801250 86 70-130
Chloromethane ug/kg 9781250 78 55-130
cis-1,2-Dichloroethene ug/kg 11301250 91 70-130
cis-1,3-Dichloropropene ug/kg 11401250 91 70-130
Dibromochloromethane ug/kg 11901250 95 70-130
Dibromomethane ug/kg 11501250 92 70-130
Dichlorodifluoromethane ug/kg 10901250 87 45-156
Diisopropyl ether ug/kg 10801250 86 70-130
Ethylbenzene ug/kg 10501250 84 70-130
Hexachloro-1,3-butadiene ug/kg 12201250 98 66-130
Isopropylbenzene (Cumene)ug/kg 11301250 91 70-130
m&p-Xylene ug/kg 22002500 88 70-130
Methyl-tert-butyl ether ug/kg 10901250 87 70-130
Methylene Chloride ug/kg 10401250 83 65-130
n-Butylbenzene ug/kg 11901250 95 67-130
n-Propylbenzene ug/kg 11701250 93 70-130
Naphthalene ug/kg 11401250 91 70-130
o-Xylene ug/kg 11101250 89 70-130
p-Isopropyltoluene ug/kg 11601250 93 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153623LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 11401250 91 69-130
Styrene ug/kg 11801250 94 70-130
tert-Butylbenzene ug/kg 10801250 86 67-130
Tetrachloroethene ug/kg 10601250 85 70-130
Toluene ug/kg 10901250 87 70-130
trans-1,2-Dichloroethene ug/kg 11001250 88 70-130
trans-1,3-Dichloropropene ug/kg 11101250 89 68-130
Trichloroethene ug/kg 11301250 90 70-130
Trichlorofluoromethane ug/kg 11501250 92 70-130
Vinyl acetate ug/kg 25502500 102 70-130
Vinyl chloride ug/kg 10701250 85 61-130
Xylene (Total)ug/kg 33103750 88 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3153625MATRIX SPIKE SAMPLE:
MSSpike
Result
92519570006
1,1,1,2-Tetrachloroethane ug/kg 821816 101 70-131ND
1,1,1-Trichloroethane ug/kg 878816 108 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 820816 100 66-130ND
1,1,2-Trichloroethane ug/kg 843816 103 66-133ND
1,1-Dichloroethane ug/kg 847816 104 65-130ND
1,1-Dichloroethene ug/kg 913816 112 10-158ND
1,1-Dichloropropene ug/kg 903816 111 68-133ND
1,2,3-Trichlorobenzene ug/kg 803816 99 27-138ND
1,2,3-Trichloropropane ug/kg 794816 97 67-130ND
1,2,4-Trichlorobenzene ug/kg 867816 106 51-134ND
1,2,4-Trimethylbenzene ug/kg 889816 108 63-13610.6
1,2-Dibromo-3-chloropropane ug/kg 797816 98 32-130ND
1,2-Dibromoethane (EDB)ug/kg 830816 102 70-130ND
1,2-Dichlorobenzene ug/kg 876816 107 69-130ND
1,2-Dichloroethane ug/kg 831816 102 59-130ND
1,2-Dichloropropane ug/kg 862816 106 70-130ND
1,3,5-Trimethylbenzene ug/kg 882816 108 65-137ND
1,3-Dichlorobenzene ug/kg 860816 105 70-130ND
1,3-Dichloropropane ug/kg 826816 101 70-130ND
1,4-Dichlorobenzene ug/kg 876816 107 68-130ND
2,2-Dichloropropane ug/kg 807816 99 32-130ND
2-Butanone (MEK)ug/kg 14501630 89 10-136ND
2-Chlorotoluene ug/kg 916816 112 69-141ND
2-Hexanone ug/kg 15601630 95 10-144ND
4-Chlorotoluene ug/kg 882816 108 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 16101630 99 25-143ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3153625MATRIX SPIKE SAMPLE:
MSSpike
Result
92519570006
Acetone ug/kg 13301630 81 10-130ND
Benzene ug/kg 884816 107 67-1308.3
Bromobenzene ug/kg 876816 107 70-130ND
Bromochloromethane ug/kg 780816 96 69-134ND
Bromodichloromethane ug/kg 838816 103 64-130ND
Bromoform ug/kg 791816 97 62-130ND
Bromomethane ug/kg 622816 76 20-176ND
Carbon tetrachloride ug/kg 941816 115 65-140ND
Chlorobenzene ug/kg 840816 103 70-130ND
Chloroethane ug/kg 226816 28 10-130ND
Chloroform ug/kg 805816 99 63-130ND
Chloromethane ug/kg 844816 103 58-130ND
cis-1,2-Dichloroethene ug/kg 838816 103 66-130ND
cis-1,3-Dichloropropene ug/kg 856816 105 67-130ND
Dibromochloromethane ug/kg 870816 107 67-130ND
Dibromomethane ug/kg 864816 106 63-131ND
Dichlorodifluoromethane ug/kg 890816 109 44-180ND
Diisopropyl ether ug/kg 779816 96 63-130ND
Ethylbenzene ug/kg 815816 99 66-130ND
Hexachloro-1,3-butadiene ug/kg 960816 118 64-150ND
Isopropylbenzene (Cumene)ug/kg 892816 109 69-135ND
m&p-Xylene ug/kg 17201630 105 60-133ND
Methyl-tert-butyl ether ug/kg 782816 96 65-130ND
Methylene Chloride ug/kg 762816 93 61-130ND
n-Butylbenzene ug/kg 938816 115 65-140ND
n-Propylbenzene ug/kg 905816 111 67-140ND
Naphthalene ug/kg 888816 109 15-145ND
o-Xylene ug/kg 858816 104 66-133ND
p-Isopropyltoluene ug/kg 918816 113 56-147ND
sec-Butylbenzene ug/kg 924816 113 65-139ND
Styrene ug/kg 880816 108 70-132ND
tert-Butylbenzene ug/kg 888816 109 62-135ND
Tetrachloroethene ug/kg 825816 101 70-135ND
Toluene ug/kg 882816 106 67-13017.8
trans-1,2-Dichloroethene ug/kg 821816 101 69-130ND
trans-1,3-Dichloropropene ug/kg 837816 103 62-130ND
Trichloroethene ug/kg 911816 112 70-135ND
Trichlorofluoromethane ug/kg 321816 39 10-130ND
Vinyl acetate ug/kg 17801630 109 53-130ND
Vinyl chloride ug/kg 894816 110 61-148ND
Xylene (Total)ug/kg 25802450 105 63-132ND
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92519570005
3153624SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 6.6JND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 8.9JND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92519570005
3153624SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%105104
4-Bromofluorobenzene (S)%101101
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 47
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596970
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92519570001, 92519570002, 92519570003, 92519570004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3147966
Associated Lab Samples:92519570001, 92519570002, 92519570003, 92519570004
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 02/03/21 10:13
n-Pentacosane (S)%81 32-130 02/03/21 10:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3147967LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 53.867.8 79 47-130
n-Pentacosane (S)%82 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3147968MATRIX SPIKE SAMPLE:
MSSpike
Result
92519570001
Diesel Range Organics(C10-C28)mg/kg 88.594.1 90 10-133ND
n-Pentacosane (S)%82 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92519570002
3147969SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%8076
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596775
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519570001, 92519570002, 92519570003, 92519570004, 92519570005, 92519570006, 92519570007,
92519570008, 92519570009, 92519570010, 92519570011
Parameter Units
Dup
Result QualifiersRPDResult
92519381006
3147355SAMPLE DUPLICATE:
Percent Moisture %11.2 N2411.7
Parameter Units
Dup
Result QualifiersRPDResult
92519570011
3147356SAMPLE DUPLICATE:
Percent Moisture %30.3 N2329.4
REPORT OF LABORATORY ANALYSIS
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596805
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92519570012, 92519570013
Parameter Units
Dup
Result QualifiersRPDResult
92519570012
3147493SAMPLE DUPLICATE:
Percent Moisture %25.1 N2125.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:47 PM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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Page 41 of 47
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92519570
Sheetz Greensboro #356
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92519570001 596970 597198Kerosene UST East EPA 3546 EPA 8015C Modified
92519570002 596970 597198Kerosene UST West EPA 3546 EPA 8015C Modified
92519570003 596970 597198Diesel UST East EPA 3546 EPA 8015C Modified
92519570004 596970 597198Diesel UST West EPA 3546 EPA 8015C Modified
92519570001 597663 597674Kerosene UST East EPA 5030B EPA 8015C Modified
92519570002 597663 597674Kerosene UST West EPA 5030B EPA 8015C Modified
92519570005 597663 597674Gas UST 3 East EPA 5030B EPA 8015C Modified
92519570006 597663 597674Gas UST 3 Center EPA 5030B EPA 8015C Modified
92519570007 597663 597674Gas UST 3 West EPA 5030B EPA 8015C Modified
92519570008 597663 597674Gas UST 4 East EPA 5030B EPA 8015C Modified
92519570009 597663 597674Gas UST 4 Center EPA 5030B EPA 8015C Modified
92519570010 597663 597674Gas UST 4 West EPA 5030B EPA 8015C Modified
92519570011 597677 597681Gas UST 5 East EPA 5030B EPA 8015C Modified
92519570012 597677 597681Gas UST 5 Center EPA 5030B EPA 8015C Modified
92519570013 597677 597681Gas UST 5 West EPA 5030B EPA 8015C Modified
92519570005 598062 598082Gas UST 3 East EPA 5035A/5030B EPA 8260D
92519570006 598062 598082Gas UST 3 Center EPA 5035A/5030B EPA 8260D
92519570007 598062 598082Gas UST 3 West EPA 5035A/5030B EPA 8260D
92519570008 598062 598082Gas UST 4 East EPA 5035A/5030B EPA 8260D
92519570009 598062 598082Gas UST 4 Center EPA 5035A/5030B EPA 8260D
92519570010 598062 598082Gas UST 4 West EPA 5035A/5030B EPA 8260D
92519570011 598062 598082Gas UST 5 East EPA 5035A/5030B EPA 8260D
92519570012 598062 598082Gas UST 5 Center EPA 5035A/5030B EPA 8260D
92519570013 598062 598082Gas UST 5 West EPA 5035A/5030B EPA 8260D
92519570001 596775Kerosene UST East SW-846
92519570002 596775Kerosene UST West SW-846
92519570003 596775Diesel UST East SW-846
92519570004 596775Diesel UST West SW-846
92519570005 596775Gas UST 3 East SW-846
92519570006 596775Gas UST 3 Center SW-846
92519570007 596775Gas UST 3 West SW-846
92519570008 596775Gas UST 4 East SW-846
92519570009 596775Gas UST 4 Center SW-846
92519570010 596775Gas UST 4 West SW-846
92519570011 596775Gas UST 5 East SW-846
92519570012 596805Gas UST 5 Center SW-846
92519570013 596805Gas UST 5 West SW-846
REPORT OF LABORATORY ANALYSIS
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Page 43 of 47
Page 44 of 47
Page 45 of 47
Page 46 of 47
Page 47 of 47

APPENDIX F
PRODUCT LINE LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
February 22, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92522127
92522127
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz Greensboro #356
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on February 12, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 70
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 70
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92522127001 Dispenser 1 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127002 Product Line 2 EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127003 Dispenser 3 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127004 Product Line 4 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127005 Dispenser 5 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127006 Product Line 6 EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127007 Dispenser 7 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127008 Product Line 8 EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127009 Remote Fill 14 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127010 Remote Fill 15 EPA 8015C Modified 2 PASI-CJMS1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127011 Remote Fill 16 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127012 Product Line 18 EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127013 Dispenser 9 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127014 Product Line 10 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127015 Dispenser 11 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127016 Product Line 12 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127017 Dispenser 13 EPA 8015C Modified 2 PASI-CMAD
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92522127018 Kerosene Dispenser 17 EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
92522127019 Kerosene Line 19 EPA 8015C Modified 2 PASI-CJMS1
EPA 8015C Modified 2 PASI-CMAD
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92522127001 Dispenser 1
Diesel Range Organics(C10-C28)21.6 mg/kg 02/16/21 18:196.7EPA 8015C Modified
Toluene 23.7 ug/kg 02/17/21 13:4714.2EPA 8260D
1,2,4-Trimethylbenzene 26.2 ug/kg 02/17/21 13:4714.2EPA 8260D
Xylene (Total)30.7 ug/kg 02/17/21 13:4728.3EPA 8260D
m&p-Xylene 30.7 ug/kg 02/17/21 13:4728.3EPA 8260D
Percent Moisture 25.4 %02/15/21 13:15 N20.10SW-846
92522127002 Product Line 2
Percent Moisture 28.1 %02/15/21 13:15 N20.10SW-846
92522127003 Dispenser 3
Diesel Range Organics(C10-C28)7.1 mg/kg 02/17/21 14:206.8EPA 8015C Modified
Ethylbenzene 9.9 ug/kg 02/17/21 14:417.6EPA 8260D
Toluene 65.2 ug/kg 02/17/21 14:417.6EPA 8260D
Xylene (Total)40.4 ug/kg 02/17/21 14:4115.2EPA 8260D
m&p-Xylene 28.1 ug/kg 02/17/21 14:4115.2EPA 8260D
o-Xylene 12.4 ug/kg 02/17/21 14:417.6EPA 8260D
Percent Moisture 26.1 %02/15/21 13:15 N20.10SW-846
92522127004 Product Line 4
Ethylbenzene 15.4 ug/kg 02/17/21 15:0010.3EPA 8260D
Naphthalene 17.4 ug/kg 02/17/21 15:0010.3EPA 8260D
Toluene 18.4 ug/kg 02/17/21 15:0010.3EPA 8260D
Percent Moisture 26.3 %02/15/21 13:16 N20.10SW-846
92522127005 Dispenser 5
Benzene 86.5 ug/kg 02/17/21 15:188.3EPA 8260D
Ethylbenzene 11.9 ug/kg 02/17/21 15:188.3EPA 8260D
Toluene 203 ug/kg 02/17/21 15:188.3EPA 8260D
Xylene (Total)49.8 ug/kg 02/17/21 15:1816.7EPA 8260D
m&p-Xylene 34.1 ug/kg 02/17/21 15:1816.7EPA 8260D
o-Xylene 15.8 ug/kg 02/17/21 15:188.3EPA 8260D
Percent Moisture 23.3 %02/15/21 13:16 N20.10SW-846
92522127006 Product Line 6
Diesel Range Organics(C10-C28)16.7 mg/kg 02/17/21 15:086.4EPA 8015C Modified
Percent Moisture 22.2 %02/15/21 13:16 N20.10SW-846
92522127007 Dispenser 7
Ethylbenzene 26.5 ug/kg 02/17/21 15:548.8EPA 8260D
Isopropylbenzene (Cumene)10.6 ug/kg 02/17/21 15:548.8EPA 8260D
Naphthalene 138 ug/kg 02/17/21 15:548.8EPA 8260D
1,2,4-Trimethylbenzene 198 ug/kg 02/17/21 15:548.8EPA 8260D
Xylene (Total)39.1 ug/kg 02/17/21 15:5417.5EPA 8260D
m&p-Xylene 22.3 ug/kg 02/17/21 15:5417.5EPA 8260D
o-Xylene 16.8 ug/kg 02/17/21 15:548.8EPA 8260D
Percent Moisture 19.7 %02/15/21 13:16 N20.10SW-846
92522127008 Product Line 8
Diesel Range Organics(C10-C28)79.6 mg/kg 02/17/21 15:326.0EPA 8015C Modified
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92522127008 Product Line 8
p-Isopropyltoluene 21.3 ug/kg 02/17/21 16:1210.2EPA 8260D
Percent Moisture 17.3 %02/15/21 13:16 N20.10SW-846
92522127009 Remote Fill 14
Percent Moisture 26.3 %02/15/21 13:16 N20.10SW-846
92522127010 Remote Fill 15
Percent Moisture 12.5 %02/15/21 13:16 N20.10SW-846
92522127011 Remote Fill 16
Percent Moisture 18.9 %02/15/21 13:16 N20.10SW-846
92522127012 Product Line 18
Benzene 160 ug/kg 02/17/21 17:247.5EPA 8260D
Diisopropyl ether 13.0 ug/kg 02/17/21 17:247.5EPA 8260D
Ethylbenzene 10.2 ug/kg 02/17/21 17:247.5EPA 8260D
Toluene 374 ug/kg 02/17/21 17:247.5EPA 8260D
1,2,4-Trimethylbenzene 27.8 ug/kg 02/17/21 17:247.5EPA 8260D
Xylene (Total)322 ug/kg 02/17/21 17:2415.0EPA 8260D
m&p-Xylene 217 ug/kg 02/17/21 17:2415.0EPA 8260D
o-Xylene 105 ug/kg 02/17/21 17:247.5EPA 8260D
Percent Moisture 26.7 %02/15/21 13:16 N20.10SW-846
92522127013 Dispenser 9
Benzene 41.0 ug/kg 02/17/21 17:427.1EPA 8260D
Ethylbenzene 331 ug/kg 02/17/21 17:427.1EPA 8260D
Isopropylbenzene (Cumene)196 ug/kg 02/17/21 17:427.1EPA 8260D
Naphthalene 281 ug/kg 02/17/21 17:427.1EPA 8260D
Toluene 71.5 ug/kg 02/17/21 17:427.1EPA 8260D
1,2,4-Trimethylbenzene 2370 ug/kg 02/17/21 17:427.1EPA 8260D
Xylene (Total)1470 ug/kg 02/17/21 17:4214.3EPA 8260D
m&p-Xylene 926 ug/kg 02/17/21 17:4214.3EPA 8260D
o-Xylene 540 ug/kg 02/17/21 17:427.1EPA 8260D
Percent Moisture 15.8 %02/15/21 13:17 N20.10SW-846
92522127014 Product Line 10
Gas Range Organics (C6-C10)16.7 mg/kg 02/15/21 20:398.9EPA 8015C Modified
Benzene 14.4 ug/kg 02/17/21 18:008.5EPA 8260D
Ethylbenzene 207 ug/kg 02/17/21 18:008.5EPA 8260D
Isopropylbenzene (Cumene)216 ug/kg 02/17/21 18:008.5EPA 8260D
Naphthalene 625 ug/kg 02/17/21 18:008.5EPA 8260D
n-Propylbenzene 1050 ug/kg 02/17/21 18:008.5EPA 8260D
Toluene 59.3 ug/kg 02/17/21 18:008.5EPA 8260D
1,2,4-Trimethylbenzene 7350 ug/kg 02/17/21 18:008.5EPA 8260D
1,3,5-Trimethylbenzene 1820 ug/kg 02/17/21 18:008.5EPA 8260D
Xylene (Total)785 ug/kg 02/17/21 18:0016.9EPA 8260D
m&p-Xylene 721 ug/kg 02/17/21 18:0016.9EPA 8260D
o-Xylene 64.2 ug/kg 02/17/21 18:008.5EPA 8260D
Percent Moisture 23.4 %02/15/21 13:17 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 6 of 70
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92522127015 Dispenser 11
sec-Butylbenzene 12.1 ug/kg 02/18/21 11:158.6EPA 8260D
Ethylbenzene 11.8 ug/kg 02/18/21 11:158.6EPA 8260D
Naphthalene 35.0 ug/kg 02/18/21 11:158.6EPA 8260D
Toluene 10.2 ug/kg 02/18/21 11:158.6EPA 8260D
1,2,4-Trimethylbenzene 32.1 ug/kg 02/18/21 11:158.6EPA 8260D
Xylene (Total)22.8 ug/kg 02/18/21 11:1517.2EPA 8260D
m&p-Xylene 22.8 ug/kg 02/18/21 11:1517.2EPA 8260D
Percent Moisture 21.8 %02/15/21 13:17 N20.10SW-846
92522127016 Product Line 12
Ethylbenzene 9.5 ug/kg 02/17/21 18:377.0EPA 8260D
Naphthalene 13.2 ug/kg 02/17/21 18:377.0EPA 8260D
Toluene 12.0 ug/kg 02/17/21 18:377.0EPA 8260D
1,2,4-Trimethylbenzene 13.9 ug/kg 02/17/21 18:377.0EPA 8260D
Xylene (Total)17.2 ug/kg 02/17/21 18:3714.1EPA 8260D
m&p-Xylene 17.2 ug/kg 02/17/21 18:3714.1EPA 8260D
Percent Moisture 23.8 %02/15/21 13:17 N20.10SW-846
92522127017 Dispenser 13
Percent Moisture 10.8 %02/15/21 13:17 N20.10SW-846
92522127018 Kerosene Dispenser 17
Diesel Range Organics(C10-C28)484 mg/kg 02/17/21 23:0214.4EPA 8015C Modified
Percent Moisture 13.2 %02/15/21 13:17 N20.10SW-846
92522127019 Kerosene Line 19
Percent Moisture 29.6 %02/15/21 13:17 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 1 Lab ID: 92522127001 Collected: 02/11/21 08:50 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)21.6 mg/kg 02/16/21 18:1902/16/21 10:256.7 1
Surrogates
n-Pentacosane (S)77 %02/16/21 18:19 629-99-202/16/21 10:2532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 14:3302/15/21 11:3610.4 1
Surrogates
4-Bromofluorobenzene (S)81 %02/15/21 14:33 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 13:47 67-64-102/17/21 11:23283 1
Benzene ND ug/kg 02/17/21 13:47 71-43-202/17/21 11:2314.2 1
Bromobenzene ND ug/kg 02/17/21 13:47 108-86-102/17/21 11:2314.2 1
Bromochloromethane ND ug/kg 02/17/21 13:47 74-97-502/17/21 11:2314.2 1
Bromodichloromethane ND ug/kg 02/17/21 13:47 75-27-402/17/21 11:2314.2 1
Bromoform ND ug/kg 02/17/21 13:47 75-25-202/17/21 11:2314.2 1
Bromomethane ND ug/kg 02/17/21 13:47 74-83-902/17/21 11:2328.3 1
2-Butanone (MEK)ND ug/kg 02/17/21 13:47 78-93-302/17/21 11:23283 1
n-Butylbenzene ND ug/kg 02/17/21 13:47 104-51-802/17/21 11:2314.2 1
sec-Butylbenzene ND ug/kg 02/17/21 13:47 135-98-802/17/21 11:2314.2 1
tert-Butylbenzene ND ug/kg 02/17/21 13:47 98-06-602/17/21 11:2314.2 1
Carbon tetrachloride ND ug/kg 02/17/21 13:47 56-23-502/17/21 11:2314.2 1
Chlorobenzene ND ug/kg 02/17/21 13:47 108-90-702/17/21 11:2314.2 1
Chloroethane ND ug/kg 02/17/21 13:47 75-00-302/17/21 11:2328.3 1
Chloroform ND ug/kg 02/17/21 13:47 67-66-302/17/21 11:2314.2 1
Chloromethane ND ug/kg 02/17/21 13:47 74-87-302/17/21 11:2328.3 1
2-Chlorotoluene ND ug/kg 02/17/21 13:47 95-49-802/17/21 11:2314.2 1
4-Chlorotoluene ND ug/kg 02/17/21 13:47 106-43-402/17/21 11:2314.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 13:47 96-12-802/17/21 11:2314.2 1
Dibromochloromethane ND ug/kg 02/17/21 13:47 124-48-102/17/21 11:2314.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 13:47 106-93-402/17/21 11:2314.2 1
Dibromomethane ND ug/kg 02/17/21 13:47 74-95-302/17/21 11:2314.2 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 13:47 95-50-102/17/21 11:2314.2 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 13:47 541-73-102/17/21 11:2314.2 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 13:47 106-46-702/17/21 11:2314.2 1
Dichlorodifluoromethane ND ug/kg 02/17/21 13:47 75-71-802/17/21 11:2328.3 1
1,1-Dichloroethane ND ug/kg 02/17/21 13:47 75-34-302/17/21 11:2314.2 1
1,2-Dichloroethane ND ug/kg 02/17/21 13:47 107-06-202/17/21 11:2314.2 1
1,1-Dichloroethene ND ug/kg 02/17/21 13:47 75-35-402/17/21 11:2314.2 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 13:47 156-59-202/17/21 11:2314.2 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 13:47 156-60-502/17/21 11:2314.2 1
1,2-Dichloropropane ND ug/kg 02/17/21 13:47 78-87-502/17/21 11:2314.2 1
1,3-Dichloropropane ND ug/kg 02/17/21 13:47 142-28-902/17/21 11:2314.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 1 Lab ID: 92522127001 Collected: 02/11/21 08:50 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 13:47 594-20-702/17/21 11:2314.2 1
1,1-Dichloropropene ND ug/kg 02/17/21 13:47 563-58-602/17/21 11:2314.2 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 13:47 10061-01-502/17/21 11:2314.2 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 13:47 10061-02-602/17/21 11:2314.2 1
Diisopropyl ether ND ug/kg 02/17/21 13:47 108-20-302/17/21 11:2314.2 1
Ethylbenzene ND ug/kg 02/17/21 13:47 100-41-402/17/21 11:2314.2 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 13:47 87-68-302/17/21 11:2328.3 1
2-Hexanone ND ug/kg 02/17/21 13:47 591-78-602/17/21 11:23142 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 13:47 98-82-802/17/21 11:2314.2 1
p-Isopropyltoluene ND ug/kg 02/17/21 13:47 99-87-602/17/21 11:2314.2 1
Methylene Chloride ND ug/kg 02/17/21 13:47 75-09-202/17/21 11:2356.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 13:47 108-10-102/17/21 11:23142 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 13:47 1634-04-402/17/21 11:2314.2 1
Naphthalene ND ug/kg 02/17/21 13:47 91-20-302/17/21 11:2314.2 1
n-Propylbenzene ND ug/kg 02/17/21 13:47 103-65-102/17/21 11:2314.2 1
Styrene ND ug/kg 02/17/21 13:47 100-42-502/17/21 11:2314.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 13:47 630-20-602/17/21 11:2314.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 13:47 79-34-502/17/21 11:2314.2 1
Tetrachloroethene ND ug/kg 02/17/21 13:47 127-18-402/17/21 11:2314.2 1
Toluene 23.7 ug/kg 02/17/21 13:47 108-88-302/17/21 11:2314.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 13:47 87-61-602/17/21 11:2314.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 13:47 120-82-102/17/21 11:2314.2 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 13:47 71-55-602/17/21 11:2314.2 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 13:47 79-00-502/17/21 11:2314.2 1
Trichloroethene ND ug/kg 02/17/21 13:47 79-01-602/17/21 11:2314.2 1
Trichlorofluoromethane ND ug/kg 02/17/21 13:47 75-69-402/17/21 11:2314.2 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 13:47 96-18-402/17/21 11:2314.2 1
1,2,4-Trimethylbenzene 26.2 ug/kg 02/17/21 13:47 95-63-602/17/21 11:2314.2 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 13:47 108-67-802/17/21 11:2314.2 1
Vinyl acetate ND ug/kg 02/17/21 13:47 108-05-402/17/21 11:23142 1
Vinyl chloride ND ug/kg 02/17/21 13:47 75-01-402/17/21 11:2328.3 1
Xylene (Total)30.7 ug/kg 02/17/21 13:47 1330-20-702/17/21 11:2328.3 1
m&p-Xylene 30.7 ug/kg 02/17/21 13:47 179601-23-102/17/21 11:2328.3 1
o-Xylene ND ug/kg 02/17/21 13:47 95-47-602/17/21 11:2314.2 1
Surrogates
Toluene-d8 (S)101 %02/17/21 13:47 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 13:47 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)103 %02/17/21 13:47 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.4 %02/15/21 13:15 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 2 Lab ID: 92522127002 Collected: 02/11/21 09:04 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/16/21 18:1902/16/21 10:257.0 1
Surrogates
n-Pentacosane (S)88 %02/16/21 18:19 629-99-202/16/21 10:2532-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 15:0102/15/21 11:3611.8 1
Surrogates
4-Bromofluorobenzene (S)79 %02/15/21 15:01 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 14:23 67-64-102/17/21 11:23187 1
Benzene ND ug/kg 02/17/21 14:23 71-43-202/17/21 11:239.4 1
Bromobenzene ND ug/kg 02/17/21 14:23 108-86-102/17/21 11:239.4 1
Bromochloromethane ND ug/kg 02/17/21 14:23 74-97-502/17/21 11:239.4 1
Bromodichloromethane ND ug/kg 02/17/21 14:23 75-27-402/17/21 11:239.4 1
Bromoform ND ug/kg 02/17/21 14:23 75-25-202/17/21 11:239.4 1
Bromomethane ND ug/kg 02/17/21 14:23 74-83-902/17/21 11:2318.7 1
2-Butanone (MEK)ND ug/kg 02/17/21 14:23 78-93-302/17/21 11:23187 1
n-Butylbenzene ND ug/kg 02/17/21 14:23 104-51-802/17/21 11:239.4 1
sec-Butylbenzene ND ug/kg 02/17/21 14:23 135-98-802/17/21 11:239.4 1
tert-Butylbenzene ND ug/kg 02/17/21 14:23 98-06-602/17/21 11:239.4 1
Carbon tetrachloride ND ug/kg 02/17/21 14:23 56-23-502/17/21 11:239.4 1
Chlorobenzene ND ug/kg 02/17/21 14:23 108-90-702/17/21 11:239.4 1
Chloroethane ND ug/kg 02/17/21 14:23 75-00-302/17/21 11:2318.7 1
Chloroform ND ug/kg 02/17/21 14:23 67-66-302/17/21 11:239.4 1
Chloromethane ND ug/kg 02/17/21 14:23 74-87-302/17/21 11:2318.7 1
2-Chlorotoluene ND ug/kg 02/17/21 14:23 95-49-802/17/21 11:239.4 1
4-Chlorotoluene ND ug/kg 02/17/21 14:23 106-43-402/17/21 11:239.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 14:23 96-12-802/17/21 11:239.4 1
Dibromochloromethane ND ug/kg 02/17/21 14:23 124-48-102/17/21 11:239.4 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 14:23 106-93-402/17/21 11:239.4 1
Dibromomethane ND ug/kg 02/17/21 14:23 74-95-302/17/21 11:239.4 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 14:23 95-50-102/17/21 11:239.4 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 14:23 541-73-102/17/21 11:239.4 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 14:23 106-46-702/17/21 11:239.4 1
Dichlorodifluoromethane ND ug/kg 02/17/21 14:23 75-71-802/17/21 11:2318.7 1
1,1-Dichloroethane ND ug/kg 02/17/21 14:23 75-34-302/17/21 11:239.4 1
1,2-Dichloroethane ND ug/kg 02/17/21 14:23 107-06-202/17/21 11:239.4 1
1,1-Dichloroethene ND ug/kg 02/17/21 14:23 75-35-402/17/21 11:239.4 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 14:23 156-59-202/17/21 11:239.4 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 14:23 156-60-502/17/21 11:239.4 1
1,2-Dichloropropane ND ug/kg 02/17/21 14:23 78-87-502/17/21 11:239.4 1
1,3-Dichloropropane ND ug/kg 02/17/21 14:23 142-28-902/17/21 11:239.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 2 Lab ID: 92522127002 Collected: 02/11/21 09:04 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 14:23 594-20-702/17/21 11:239.4 1
1,1-Dichloropropene ND ug/kg 02/17/21 14:23 563-58-602/17/21 11:239.4 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 14:23 10061-01-502/17/21 11:239.4 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 14:23 10061-02-602/17/21 11:239.4 1
Diisopropyl ether ND ug/kg 02/17/21 14:23 108-20-302/17/21 11:239.4 1
Ethylbenzene ND ug/kg 02/17/21 14:23 100-41-402/17/21 11:239.4 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 14:23 87-68-302/17/21 11:2318.7 1
2-Hexanone ND ug/kg 02/17/21 14:23 591-78-602/17/21 11:2393.5 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 14:23 98-82-802/17/21 11:239.4 1
p-Isopropyltoluene ND ug/kg 02/17/21 14:23 99-87-602/17/21 11:239.4 1
Methylene Chloride ND ug/kg 02/17/21 14:23 75-09-202/17/21 11:2337.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 14:23 108-10-102/17/21 11:2393.5 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 14:23 1634-04-402/17/21 11:239.4 1
Naphthalene ND ug/kg 02/17/21 14:23 91-20-302/17/21 11:239.4 1
n-Propylbenzene ND ug/kg 02/17/21 14:23 103-65-102/17/21 11:239.4 1
Styrene ND ug/kg 02/17/21 14:23 100-42-502/17/21 11:239.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 14:23 630-20-602/17/21 11:239.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 14:23 79-34-502/17/21 11:239.4 1
Tetrachloroethene ND ug/kg 02/17/21 14:23 127-18-402/17/21 11:239.4 1
Toluene ND ug/kg 02/17/21 14:23 108-88-302/17/21 11:239.4 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 14:23 87-61-602/17/21 11:239.4 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 14:23 120-82-102/17/21 11:239.4 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 14:23 71-55-602/17/21 11:239.4 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 14:23 79-00-502/17/21 11:239.4 1
Trichloroethene ND ug/kg 02/17/21 14:23 79-01-602/17/21 11:239.4 1
Trichlorofluoromethane ND ug/kg 02/17/21 14:23 75-69-402/17/21 11:239.4 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 14:23 96-18-402/17/21 11:239.4 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 14:23 95-63-602/17/21 11:239.4 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 14:23 108-67-802/17/21 11:239.4 1
Vinyl acetate ND ug/kg 02/17/21 14:23 108-05-402/17/21 11:2393.5 1
Vinyl chloride ND ug/kg 02/17/21 14:23 75-01-402/17/21 11:2318.7 1
Xylene (Total)ND ug/kg 02/17/21 14:23 1330-20-702/17/21 11:2318.7 1
m&p-Xylene ND ug/kg 02/17/21 14:23 179601-23-102/17/21 11:2318.7 1
o-Xylene ND ug/kg 02/17/21 14:23 95-47-602/17/21 11:239.4 1
Surrogates
Toluene-d8 (S)101 %02/17/21 14:23 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 14:23 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)101 %02/17/21 14:23 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.1 %02/15/21 13:15 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 3 Lab ID: 92522127003 Collected: 02/11/21 09:12 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)7.1 mg/kg 02/17/21 14:2002/16/21 10:266.8 1
Surrogates
n-Pentacosane (S)83 %02/17/21 14:20 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 15:2902/15/21 11:369.4 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 15:29 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 14:41 67-64-102/17/21 11:23152 1
Benzene ND ug/kg 02/17/21 14:41 71-43-202/17/21 11:237.6 1
Bromobenzene ND ug/kg 02/17/21 14:41 108-86-102/17/21 11:237.6 1
Bromochloromethane ND ug/kg 02/17/21 14:41 74-97-502/17/21 11:237.6 1
Bromodichloromethane ND ug/kg 02/17/21 14:41 75-27-402/17/21 11:237.6 1
Bromoform ND ug/kg 02/17/21 14:41 75-25-202/17/21 11:237.6 1
Bromomethane ND ug/kg 02/17/21 14:41 74-83-902/17/21 11:2315.2 1
2-Butanone (MEK)ND ug/kg 02/17/21 14:41 78-93-302/17/21 11:23152 1
n-Butylbenzene ND ug/kg 02/17/21 14:41 104-51-802/17/21 11:237.6 1
sec-Butylbenzene ND ug/kg 02/17/21 14:41 135-98-802/17/21 11:237.6 1
tert-Butylbenzene ND ug/kg 02/17/21 14:41 98-06-602/17/21 11:237.6 1
Carbon tetrachloride ND ug/kg 02/17/21 14:41 56-23-502/17/21 11:237.6 1
Chlorobenzene ND ug/kg 02/17/21 14:41 108-90-702/17/21 11:237.6 1
Chloroethane ND ug/kg 02/17/21 14:41 75-00-302/17/21 11:2315.2 1
Chloroform ND ug/kg 02/17/21 14:41 67-66-302/17/21 11:237.6 1
Chloromethane ND ug/kg 02/17/21 14:41 74-87-302/17/21 11:2315.2 1
2-Chlorotoluene ND ug/kg 02/17/21 14:41 95-49-802/17/21 11:237.6 1
4-Chlorotoluene ND ug/kg 02/17/21 14:41 106-43-402/17/21 11:237.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 14:41 96-12-802/17/21 11:237.6 1
Dibromochloromethane ND ug/kg 02/17/21 14:41 124-48-102/17/21 11:237.6 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 14:41 106-93-402/17/21 11:237.6 1
Dibromomethane ND ug/kg 02/17/21 14:41 74-95-302/17/21 11:237.6 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 14:41 95-50-102/17/21 11:237.6 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 14:41 541-73-102/17/21 11:237.6 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 14:41 106-46-702/17/21 11:237.6 1
Dichlorodifluoromethane ND ug/kg 02/17/21 14:41 75-71-802/17/21 11:2315.2 1
1,1-Dichloroethane ND ug/kg 02/17/21 14:41 75-34-302/17/21 11:237.6 1
1,2-Dichloroethane ND ug/kg 02/17/21 14:41 107-06-202/17/21 11:237.6 1
1,1-Dichloroethene ND ug/kg 02/17/21 14:41 75-35-402/17/21 11:237.6 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 14:41 156-59-202/17/21 11:237.6 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 14:41 156-60-502/17/21 11:237.6 1
1,2-Dichloropropane ND ug/kg 02/17/21 14:41 78-87-502/17/21 11:237.6 1
1,3-Dichloropropane ND ug/kg 02/17/21 14:41 142-28-902/17/21 11:237.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 3 Lab ID: 92522127003 Collected: 02/11/21 09:12 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 14:41 594-20-702/17/21 11:237.6 1
1,1-Dichloropropene ND ug/kg 02/17/21 14:41 563-58-602/17/21 11:237.6 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 14:41 10061-01-502/17/21 11:237.6 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 14:41 10061-02-602/17/21 11:237.6 1
Diisopropyl ether ND ug/kg 02/17/21 14:41 108-20-302/17/21 11:237.6 1
Ethylbenzene 9.9 ug/kg 02/17/21 14:41 100-41-402/17/21 11:237.6 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 14:41 87-68-302/17/21 11:2315.2 1
2-Hexanone ND ug/kg 02/17/21 14:41 591-78-602/17/21 11:2376.1 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 14:41 98-82-802/17/21 11:237.6 1
p-Isopropyltoluene ND ug/kg 02/17/21 14:41 99-87-602/17/21 11:237.6 1
Methylene Chloride ND ug/kg 02/17/21 14:41 75-09-202/17/21 11:2330.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 14:41 108-10-102/17/21 11:2376.1 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 14:41 1634-04-402/17/21 11:237.6 1
Naphthalene ND ug/kg 02/17/21 14:41 91-20-302/17/21 11:237.6 1
n-Propylbenzene ND ug/kg 02/17/21 14:41 103-65-102/17/21 11:237.6 1
Styrene ND ug/kg 02/17/21 14:41 100-42-502/17/21 11:237.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 14:41 630-20-602/17/21 11:237.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 14:41 79-34-502/17/21 11:237.6 1
Tetrachloroethene ND ug/kg 02/17/21 14:41 127-18-402/17/21 11:237.6 1
Toluene 65.2 ug/kg 02/17/21 14:41 108-88-302/17/21 11:237.6 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 14:41 87-61-602/17/21 11:237.6 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 14:41 120-82-102/17/21 11:237.6 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 14:41 71-55-602/17/21 11:237.6 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 14:41 79-00-502/17/21 11:237.6 1
Trichloroethene ND ug/kg 02/17/21 14:41 79-01-602/17/21 11:237.6 1
Trichlorofluoromethane ND ug/kg 02/17/21 14:41 75-69-402/17/21 11:237.6 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 14:41 96-18-402/17/21 11:237.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 14:41 95-63-602/17/21 11:237.6 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 14:41 108-67-802/17/21 11:237.6 1
Vinyl acetate ND ug/kg 02/17/21 14:41 108-05-402/17/21 11:2376.1 1
Vinyl chloride ND ug/kg 02/17/21 14:41 75-01-402/17/21 11:2315.2 1
Xylene (Total)40.4 ug/kg 02/17/21 14:41 1330-20-702/17/21 11:2315.2 1
m&p-Xylene 28.1 ug/kg 02/17/21 14:41 179601-23-102/17/21 11:2315.2 1
o-Xylene 12.4 ug/kg 02/17/21 14:41 95-47-602/17/21 11:237.6 1
Surrogates
Toluene-d8 (S)99 %02/17/21 14:41 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 14:41 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)101 %02/17/21 14:41 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.1 %02/15/21 13:15 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 4 Lab ID: 92522127004 Collected: 02/11/21 09:20 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 14:4402/16/21 10:266.8 1
Surrogates
n-Pentacosane (S)79 %02/17/21 14:44 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 15:5702/15/21 11:369.3 1
Surrogates
4-Bromofluorobenzene (S)81 %02/15/21 15:57 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 15:00 67-64-102/17/21 11:23207 1
Benzene ND ug/kg 02/17/21 15:00 71-43-202/17/21 11:2310.3 1
Bromobenzene ND ug/kg 02/17/21 15:00 108-86-102/17/21 11:2310.3 1
Bromochloromethane ND ug/kg 02/17/21 15:00 74-97-502/17/21 11:2310.3 1
Bromodichloromethane ND ug/kg 02/17/21 15:00 75-27-402/17/21 11:2310.3 1
Bromoform ND ug/kg 02/17/21 15:00 75-25-202/17/21 11:2310.3 1
Bromomethane ND ug/kg 02/17/21 15:00 74-83-902/17/21 11:2320.7 1
2-Butanone (MEK)ND ug/kg 02/17/21 15:00 78-93-302/17/21 11:23207 1
n-Butylbenzene ND ug/kg 02/17/21 15:00 104-51-802/17/21 11:2310.3 1
sec-Butylbenzene ND ug/kg 02/17/21 15:00 135-98-802/17/21 11:2310.3 1
tert-Butylbenzene ND ug/kg 02/17/21 15:00 98-06-602/17/21 11:2310.3 1
Carbon tetrachloride ND ug/kg 02/17/21 15:00 56-23-502/17/21 11:2310.3 1
Chlorobenzene ND ug/kg 02/17/21 15:00 108-90-702/17/21 11:2310.3 1
Chloroethane ND ug/kg 02/17/21 15:00 75-00-302/17/21 11:2320.7 1
Chloroform ND ug/kg 02/17/21 15:00 67-66-302/17/21 11:2310.3 1
Chloromethane ND ug/kg 02/17/21 15:00 74-87-302/17/21 11:2320.7 1
2-Chlorotoluene ND ug/kg 02/17/21 15:00 95-49-802/17/21 11:2310.3 1
4-Chlorotoluene ND ug/kg 02/17/21 15:00 106-43-402/17/21 11:2310.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 15:00 96-12-802/17/21 11:2310.3 1
Dibromochloromethane ND ug/kg 02/17/21 15:00 124-48-102/17/21 11:2310.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 15:00 106-93-402/17/21 11:2310.3 1
Dibromomethane ND ug/kg 02/17/21 15:00 74-95-302/17/21 11:2310.3 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 15:00 95-50-102/17/21 11:2310.3 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 15:00 541-73-102/17/21 11:2310.3 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 15:00 106-46-702/17/21 11:2310.3 1
Dichlorodifluoromethane ND ug/kg 02/17/21 15:00 75-71-802/17/21 11:2320.7 1
1,1-Dichloroethane ND ug/kg 02/17/21 15:00 75-34-302/17/21 11:2310.3 1
1,2-Dichloroethane ND ug/kg 02/17/21 15:00 107-06-202/17/21 11:2310.3 1
1,1-Dichloroethene ND ug/kg 02/17/21 15:00 75-35-402/17/21 11:2310.3 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 15:00 156-59-202/17/21 11:2310.3 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 15:00 156-60-502/17/21 11:2310.3 1
1,2-Dichloropropane ND ug/kg 02/17/21 15:00 78-87-502/17/21 11:2310.3 1
1,3-Dichloropropane ND ug/kg 02/17/21 15:00 142-28-902/17/21 11:2310.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 4 Lab ID: 92522127004 Collected: 02/11/21 09:20 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 15:00 594-20-702/17/21 11:2310.3 1
1,1-Dichloropropene ND ug/kg 02/17/21 15:00 563-58-602/17/21 11:2310.3 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 15:00 10061-01-502/17/21 11:2310.3 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 15:00 10061-02-602/17/21 11:2310.3 1
Diisopropyl ether ND ug/kg 02/17/21 15:00 108-20-302/17/21 11:2310.3 1
Ethylbenzene 15.4 ug/kg 02/17/21 15:00 100-41-402/17/21 11:2310.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 15:00 87-68-302/17/21 11:2320.7 1
2-Hexanone ND ug/kg 02/17/21 15:00 591-78-602/17/21 11:23103 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 15:00 98-82-802/17/21 11:2310.3 1
p-Isopropyltoluene ND ug/kg 02/17/21 15:00 99-87-602/17/21 11:2310.3 1
Methylene Chloride ND ug/kg 02/17/21 15:00 75-09-202/17/21 11:2341.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 15:00 108-10-102/17/21 11:23103 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 15:00 1634-04-402/17/21 11:2310.3 1
Naphthalene 17.4 ug/kg 02/17/21 15:00 91-20-302/17/21 11:2310.3 1
n-Propylbenzene ND ug/kg 02/17/21 15:00 103-65-102/17/21 11:2310.3 1
Styrene ND ug/kg 02/17/21 15:00 100-42-502/17/21 11:2310.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 15:00 630-20-602/17/21 11:2310.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 15:00 79-34-502/17/21 11:2310.3 1
Tetrachloroethene ND ug/kg 02/17/21 15:00 127-18-402/17/21 11:2310.3 1
Toluene 18.4 ug/kg 02/17/21 15:00 108-88-302/17/21 11:2310.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 15:00 87-61-602/17/21 11:2310.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 15:00 120-82-102/17/21 11:2310.3 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 15:00 71-55-602/17/21 11:2310.3 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 15:00 79-00-502/17/21 11:2310.3 1
Trichloroethene ND ug/kg 02/17/21 15:00 79-01-602/17/21 11:2310.3 1
Trichlorofluoromethane ND ug/kg 02/17/21 15:00 75-69-402/17/21 11:2310.3 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 15:00 96-18-402/17/21 11:2310.3 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 15:00 95-63-602/17/21 11:2310.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 15:00 108-67-802/17/21 11:2310.3 1
Vinyl acetate ND ug/kg 02/17/21 15:00 108-05-402/17/21 11:23103 1
Vinyl chloride ND ug/kg 02/17/21 15:00 75-01-402/17/21 11:2320.7 1
Xylene (Total)ND ug/kg 02/17/21 15:00 1330-20-702/17/21 11:2320.7 1
m&p-Xylene ND ug/kg 02/17/21 15:00 179601-23-102/17/21 11:2320.7 1
o-Xylene ND ug/kg 02/17/21 15:00 95-47-602/17/21 11:2310.3 1
Surrogates
Toluene-d8 (S)100 %02/17/21 15:00 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 15:00 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)99 %02/17/21 15:00 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.3 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 5 Lab ID: 92522127005 Collected: 02/11/21 09:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 15:0802/16/21 10:266.5 1
Surrogates
n-Pentacosane (S)78 %02/17/21 15:08 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 16:2502/15/21 11:368.7 1
Surrogates
4-Bromofluorobenzene (S)81 %02/15/21 16:25 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 15:18 67-64-102/17/21 11:23167 1
Benzene 86.5 ug/kg 02/17/21 15:18 71-43-202/17/21 11:238.3 1
Bromobenzene ND ug/kg 02/17/21 15:18 108-86-102/17/21 11:238.3 1
Bromochloromethane ND ug/kg 02/17/21 15:18 74-97-502/17/21 11:238.3 1
Bromodichloromethane ND ug/kg 02/17/21 15:18 75-27-402/17/21 11:238.3 1
Bromoform ND ug/kg 02/17/21 15:18 75-25-202/17/21 11:238.3 1
Bromomethane ND ug/kg 02/17/21 15:18 74-83-902/17/21 11:2316.7 1
2-Butanone (MEK)ND ug/kg 02/17/21 15:18 78-93-302/17/21 11:23167 1
n-Butylbenzene ND ug/kg 02/17/21 15:18 104-51-802/17/21 11:238.3 1
sec-Butylbenzene ND ug/kg 02/17/21 15:18 135-98-802/17/21 11:238.3 1
tert-Butylbenzene ND ug/kg 02/17/21 15:18 98-06-602/17/21 11:238.3 1
Carbon tetrachloride ND ug/kg 02/17/21 15:18 56-23-502/17/21 11:238.3 1
Chlorobenzene ND ug/kg 02/17/21 15:18 108-90-702/17/21 11:238.3 1
Chloroethane ND ug/kg 02/17/21 15:18 75-00-302/17/21 11:2316.7 1
Chloroform ND ug/kg 02/17/21 15:18 67-66-302/17/21 11:238.3 1
Chloromethane ND ug/kg 02/17/21 15:18 74-87-302/17/21 11:2316.7 1
2-Chlorotoluene ND ug/kg 02/17/21 15:18 95-49-802/17/21 11:238.3 1
4-Chlorotoluene ND ug/kg 02/17/21 15:18 106-43-402/17/21 11:238.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 15:18 96-12-802/17/21 11:238.3 1
Dibromochloromethane ND ug/kg 02/17/21 15:18 124-48-102/17/21 11:238.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 15:18 106-93-402/17/21 11:238.3 1
Dibromomethane ND ug/kg 02/17/21 15:18 74-95-302/17/21 11:238.3 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 15:18 95-50-102/17/21 11:238.3 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 15:18 541-73-102/17/21 11:238.3 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 15:18 106-46-702/17/21 11:238.3 1
Dichlorodifluoromethane ND ug/kg 02/17/21 15:18 75-71-802/17/21 11:2316.7 1
1,1-Dichloroethane ND ug/kg 02/17/21 15:18 75-34-302/17/21 11:238.3 1
1,2-Dichloroethane ND ug/kg 02/17/21 15:18 107-06-202/17/21 11:238.3 1
1,1-Dichloroethene ND ug/kg 02/17/21 15:18 75-35-402/17/21 11:238.3 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 15:18 156-59-202/17/21 11:238.3 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 15:18 156-60-502/17/21 11:238.3 1
1,2-Dichloropropane ND ug/kg 02/17/21 15:18 78-87-502/17/21 11:238.3 1
1,3-Dichloropropane ND ug/kg 02/17/21 15:18 142-28-902/17/21 11:238.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 5 Lab ID: 92522127005 Collected: 02/11/21 09:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 15:18 594-20-702/17/21 11:238.3 1
1,1-Dichloropropene ND ug/kg 02/17/21 15:18 563-58-602/17/21 11:238.3 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 15:18 10061-01-502/17/21 11:238.3 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 15:18 10061-02-602/17/21 11:238.3 1
Diisopropyl ether ND ug/kg 02/17/21 15:18 108-20-302/17/21 11:238.3 1
Ethylbenzene 11.9 ug/kg 02/17/21 15:18 100-41-402/17/21 11:238.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 15:18 87-68-302/17/21 11:2316.7 1
2-Hexanone ND ug/kg 02/17/21 15:18 591-78-602/17/21 11:2383.3 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 15:18 98-82-802/17/21 11:238.3 1
p-Isopropyltoluene ND ug/kg 02/17/21 15:18 99-87-602/17/21 11:238.3 1
Methylene Chloride ND ug/kg 02/17/21 15:18 75-09-202/17/21 11:2333.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 15:18 108-10-102/17/21 11:2383.3 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 15:18 1634-04-402/17/21 11:238.3 1
Naphthalene ND ug/kg 02/17/21 15:18 91-20-302/17/21 11:238.3 1
n-Propylbenzene ND ug/kg 02/17/21 15:18 103-65-102/17/21 11:238.3 1
Styrene ND ug/kg 02/17/21 15:18 100-42-502/17/21 11:238.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 15:18 630-20-602/17/21 11:238.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 15:18 79-34-502/17/21 11:238.3 1
Tetrachloroethene ND ug/kg 02/17/21 15:18 127-18-402/17/21 11:238.3 1
Toluene 203 ug/kg 02/17/21 15:18 108-88-302/17/21 11:238.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 15:18 87-61-602/17/21 11:238.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 15:18 120-82-102/17/21 11:238.3 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 15:18 71-55-602/17/21 11:238.3 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 15:18 79-00-502/17/21 11:238.3 1
Trichloroethene ND ug/kg 02/17/21 15:18 79-01-602/17/21 11:238.3 1
Trichlorofluoromethane ND ug/kg 02/17/21 15:18 75-69-402/17/21 11:238.3 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 15:18 96-18-402/17/21 11:238.3 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 15:18 95-63-602/17/21 11:238.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 15:18 108-67-802/17/21 11:238.3 1
Vinyl acetate ND ug/kg 02/17/21 15:18 108-05-402/17/21 11:2383.3 1
Vinyl chloride ND ug/kg 02/17/21 15:18 75-01-402/17/21 11:2316.7 1
Xylene (Total)49.8 ug/kg 02/17/21 15:18 1330-20-702/17/21 11:2316.7 1
m&p-Xylene 34.1 ug/kg 02/17/21 15:18 179601-23-102/17/21 11:2316.7 1
o-Xylene 15.8 ug/kg 02/17/21 15:18 95-47-602/17/21 11:238.3 1
Surrogates
Toluene-d8 (S)100 %02/17/21 15:18 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)102 %02/17/21 15:18 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)104 %02/17/21 15:18 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.3 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 6 Lab ID: 92522127006 Collected: 02/11/21 09:38 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)16.7 mg/kg 02/17/21 15:0802/16/21 10:266.4 1
Surrogates
n-Pentacosane (S)75 %02/17/21 15:08 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 16:5402/15/21 11:3610.9 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 16:54 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 15:36 67-64-102/17/21 11:23138 1
Benzene ND ug/kg 02/17/21 15:36 71-43-202/17/21 11:236.9 1
Bromobenzene ND ug/kg 02/17/21 15:36 108-86-102/17/21 11:236.9 1
Bromochloromethane ND ug/kg 02/17/21 15:36 74-97-502/17/21 11:236.9 1
Bromodichloromethane ND ug/kg 02/17/21 15:36 75-27-402/17/21 11:236.9 1
Bromoform ND ug/kg 02/17/21 15:36 75-25-202/17/21 11:236.9 1
Bromomethane ND ug/kg 02/17/21 15:36 74-83-902/17/21 11:2313.8 1
2-Butanone (MEK)ND ug/kg 02/17/21 15:36 78-93-302/17/21 11:23138 1
n-Butylbenzene ND ug/kg 02/17/21 15:36 104-51-802/17/21 11:236.9 1
sec-Butylbenzene ND ug/kg 02/17/21 15:36 135-98-802/17/21 11:236.9 1
tert-Butylbenzene ND ug/kg 02/17/21 15:36 98-06-602/17/21 11:236.9 1
Carbon tetrachloride ND ug/kg 02/17/21 15:36 56-23-502/17/21 11:236.9 1
Chlorobenzene ND ug/kg 02/17/21 15:36 108-90-702/17/21 11:236.9 1
Chloroethane ND ug/kg 02/17/21 15:36 75-00-302/17/21 11:2313.8 1
Chloroform ND ug/kg 02/17/21 15:36 67-66-302/17/21 11:236.9 1
Chloromethane ND ug/kg 02/17/21 15:36 74-87-302/17/21 11:2313.8 1
2-Chlorotoluene ND ug/kg 02/17/21 15:36 95-49-802/17/21 11:236.9 1
4-Chlorotoluene ND ug/kg 02/17/21 15:36 106-43-402/17/21 11:236.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 15:36 96-12-802/17/21 11:236.9 1
Dibromochloromethane ND ug/kg 02/17/21 15:36 124-48-102/17/21 11:236.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 15:36 106-93-402/17/21 11:236.9 1
Dibromomethane ND ug/kg 02/17/21 15:36 74-95-302/17/21 11:236.9 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 15:36 95-50-102/17/21 11:236.9 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 15:36 541-73-102/17/21 11:236.9 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 15:36 106-46-702/17/21 11:236.9 1
Dichlorodifluoromethane ND ug/kg 02/17/21 15:36 75-71-802/17/21 11:2313.8 1
1,1-Dichloroethane ND ug/kg 02/17/21 15:36 75-34-302/17/21 11:236.9 1
1,2-Dichloroethane ND ug/kg 02/17/21 15:36 107-06-202/17/21 11:236.9 1
1,1-Dichloroethene ND ug/kg 02/17/21 15:36 75-35-402/17/21 11:236.9 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 15:36 156-59-202/17/21 11:236.9 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 15:36 156-60-502/17/21 11:236.9 1
1,2-Dichloropropane ND ug/kg 02/17/21 15:36 78-87-502/17/21 11:236.9 1
1,3-Dichloropropane ND ug/kg 02/17/21 15:36 142-28-902/17/21 11:236.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 6 Lab ID: 92522127006 Collected: 02/11/21 09:38 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 15:36 594-20-702/17/21 11:236.9 1
1,1-Dichloropropene ND ug/kg 02/17/21 15:36 563-58-602/17/21 11:236.9 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 15:36 10061-01-502/17/21 11:236.9 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 15:36 10061-02-602/17/21 11:236.9 1
Diisopropyl ether ND ug/kg 02/17/21 15:36 108-20-302/17/21 11:236.9 1
Ethylbenzene ND ug/kg 02/17/21 15:36 100-41-402/17/21 11:236.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 15:36 87-68-302/17/21 11:2313.8 1
2-Hexanone ND ug/kg 02/17/21 15:36 591-78-602/17/21 11:2369.0 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 15:36 98-82-802/17/21 11:236.9 1
p-Isopropyltoluene ND ug/kg 02/17/21 15:36 99-87-602/17/21 11:236.9 1
Methylene Chloride ND ug/kg 02/17/21 15:36 75-09-202/17/21 11:2327.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 15:36 108-10-102/17/21 11:2369.0 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 15:36 1634-04-402/17/21 11:236.9 1
Naphthalene ND ug/kg 02/17/21 15:36 91-20-302/17/21 11:236.9 1
n-Propylbenzene ND ug/kg 02/17/21 15:36 103-65-102/17/21 11:236.9 1
Styrene ND ug/kg 02/17/21 15:36 100-42-502/17/21 11:236.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 15:36 630-20-602/17/21 11:236.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 15:36 79-34-502/17/21 11:236.9 1
Tetrachloroethene ND ug/kg 02/17/21 15:36 127-18-402/17/21 11:236.9 1
Toluene ND ug/kg 02/17/21 15:36 108-88-302/17/21 11:236.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 15:36 87-61-602/17/21 11:236.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 15:36 120-82-102/17/21 11:236.9 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 15:36 71-55-602/17/21 11:236.9 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 15:36 79-00-502/17/21 11:236.9 1
Trichloroethene ND ug/kg 02/17/21 15:36 79-01-602/17/21 11:236.9 1
Trichlorofluoromethane ND ug/kg 02/17/21 15:36 75-69-402/17/21 11:236.9 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 15:36 96-18-402/17/21 11:236.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 15:36 95-63-602/17/21 11:236.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 15:36 108-67-802/17/21 11:236.9 1
Vinyl acetate ND ug/kg 02/17/21 15:36 108-05-402/17/21 11:2369.0 1
Vinyl chloride ND ug/kg 02/17/21 15:36 75-01-402/17/21 11:2313.8 1
Xylene (Total)ND ug/kg 02/17/21 15:36 1330-20-702/17/21 11:2313.8 1
m&p-Xylene ND ug/kg 02/17/21 15:36 179601-23-102/17/21 11:2313.8 1
o-Xylene ND ug/kg 02/17/21 15:36 95-47-602/17/21 11:236.9 1
Surrogates
Toluene-d8 (S)100 %02/17/21 15:36 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)102 %02/17/21 15:36 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)101 %02/17/21 15:36 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.2 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 7 Lab ID: 92522127007 Collected: 02/11/21 09:46 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 15:3202/16/21 10:266.2 1
Surrogates
n-Pentacosane (S)72 %02/17/21 15:32 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 17:2202/15/21 11:368.4 1
Surrogates
4-Bromofluorobenzene (S)82 %02/15/21 17:22 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 15:54 67-64-102/17/21 11:23175 1
Benzene ND ug/kg 02/17/21 15:54 71-43-202/17/21 11:238.8 1
Bromobenzene ND ug/kg 02/17/21 15:54 108-86-102/17/21 11:238.8 1
Bromochloromethane ND ug/kg 02/17/21 15:54 74-97-502/17/21 11:238.8 1
Bromodichloromethane ND ug/kg 02/17/21 15:54 75-27-402/17/21 11:238.8 1
Bromoform ND ug/kg 02/17/21 15:54 75-25-202/17/21 11:238.8 1
Bromomethane ND ug/kg 02/17/21 15:54 74-83-902/17/21 11:2317.5 1
2-Butanone (MEK)ND ug/kg 02/17/21 15:54 78-93-302/17/21 11:23175 1
n-Butylbenzene ND ug/kg 02/17/21 15:54 104-51-802/17/21 11:238.8 1
sec-Butylbenzene ND ug/kg 02/17/21 15:54 135-98-802/17/21 11:238.8 1
tert-Butylbenzene ND ug/kg 02/17/21 15:54 98-06-602/17/21 11:238.8 1
Carbon tetrachloride ND ug/kg 02/17/21 15:54 56-23-502/17/21 11:238.8 1
Chlorobenzene ND ug/kg 02/17/21 15:54 108-90-702/17/21 11:238.8 1
Chloroethane ND ug/kg 02/17/21 15:54 75-00-302/17/21 11:2317.5 1
Chloroform ND ug/kg 02/17/21 15:54 67-66-302/17/21 11:238.8 1
Chloromethane ND ug/kg 02/17/21 15:54 74-87-302/17/21 11:2317.5 1
2-Chlorotoluene ND ug/kg 02/17/21 15:54 95-49-802/17/21 11:238.8 1
4-Chlorotoluene ND ug/kg 02/17/21 15:54 106-43-402/17/21 11:238.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 15:54 96-12-802/17/21 11:238.8 1
Dibromochloromethane ND ug/kg 02/17/21 15:54 124-48-102/17/21 11:238.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 15:54 106-93-402/17/21 11:238.8 1
Dibromomethane ND ug/kg 02/17/21 15:54 74-95-302/17/21 11:238.8 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 15:54 95-50-102/17/21 11:238.8 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 15:54 541-73-102/17/21 11:238.8 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 15:54 106-46-702/17/21 11:238.8 1
Dichlorodifluoromethane ND ug/kg 02/17/21 15:54 75-71-802/17/21 11:2317.5 1
1,1-Dichloroethane ND ug/kg 02/17/21 15:54 75-34-302/17/21 11:238.8 1
1,2-Dichloroethane ND ug/kg 02/17/21 15:54 107-06-202/17/21 11:238.8 1
1,1-Dichloroethene ND ug/kg 02/17/21 15:54 75-35-402/17/21 11:238.8 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 15:54 156-59-202/17/21 11:238.8 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 15:54 156-60-502/17/21 11:238.8 1
1,2-Dichloropropane ND ug/kg 02/17/21 15:54 78-87-502/17/21 11:238.8 1
1,3-Dichloropropane ND ug/kg 02/17/21 15:54 142-28-902/17/21 11:238.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 7 Lab ID: 92522127007 Collected: 02/11/21 09:46 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 15:54 594-20-702/17/21 11:238.8 1
1,1-Dichloropropene ND ug/kg 02/17/21 15:54 563-58-602/17/21 11:238.8 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 15:54 10061-01-502/17/21 11:238.8 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 15:54 10061-02-602/17/21 11:238.8 1
Diisopropyl ether ND ug/kg 02/17/21 15:54 108-20-302/17/21 11:238.8 1
Ethylbenzene 26.5 ug/kg 02/17/21 15:54 100-41-402/17/21 11:238.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 15:54 87-68-302/17/21 11:2317.5 1
2-Hexanone ND ug/kg 02/17/21 15:54 591-78-602/17/21 11:2387.7 1
Isopropylbenzene (Cumene)10.6 ug/kg 02/17/21 15:54 98-82-802/17/21 11:238.8 1
p-Isopropyltoluene ND ug/kg 02/17/21 15:54 99-87-602/17/21 11:238.8 1
Methylene Chloride ND ug/kg 02/17/21 15:54 75-09-202/17/21 11:2335.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 15:54 108-10-102/17/21 11:2387.7 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 15:54 1634-04-402/17/21 11:238.8 1
Naphthalene 138 ug/kg 02/17/21 15:54 91-20-302/17/21 11:238.8 1
n-Propylbenzene ND ug/kg 02/17/21 15:54 103-65-102/17/21 11:238.8 1
Styrene ND ug/kg 02/17/21 15:54 100-42-502/17/21 11:238.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 15:54 630-20-602/17/21 11:238.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 15:54 79-34-502/17/21 11:238.8 1
Tetrachloroethene ND ug/kg 02/17/21 15:54 127-18-402/17/21 11:238.8 1
Toluene ND ug/kg 02/17/21 15:54 108-88-302/17/21 11:238.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 15:54 87-61-602/17/21 11:238.8 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 15:54 120-82-102/17/21 11:238.8 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 15:54 71-55-602/17/21 11:238.8 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 15:54 79-00-502/17/21 11:238.8 1
Trichloroethene ND ug/kg 02/17/21 15:54 79-01-602/17/21 11:238.8 1
Trichlorofluoromethane ND ug/kg 02/17/21 15:54 75-69-402/17/21 11:238.8 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 15:54 96-18-402/17/21 11:238.8 1
1,2,4-Trimethylbenzene 198 ug/kg 02/17/21 15:54 95-63-602/17/21 11:238.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 15:54 108-67-802/17/21 11:238.8 1
Vinyl acetate ND ug/kg 02/17/21 15:54 108-05-402/17/21 11:2387.7 1
Vinyl chloride ND ug/kg 02/17/21 15:54 75-01-402/17/21 11:2317.5 1
Xylene (Total)39.1 ug/kg 02/17/21 15:54 1330-20-702/17/21 11:2317.5 1
m&p-Xylene 22.3 ug/kg 02/17/21 15:54 179601-23-102/17/21 11:2317.5 1
o-Xylene 16.8 ug/kg 02/17/21 15:54 95-47-602/17/21 11:238.8 1
Surrogates
Toluene-d8 (S)101 %02/17/21 15:54 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 15:54 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)100 %02/17/21 15:54 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.7 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 8 Lab ID: 92522127008 Collected: 02/11/21 09:57 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)79.6 mg/kg 02/17/21 15:3202/16/21 10:266.0 1
Surrogates
n-Pentacosane (S)87 %02/17/21 15:32 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 17:5002/15/21 11:3612.0 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 17:50 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 16:12 67-64-102/17/21 11:23204 1
Benzene ND ug/kg 02/17/21 16:12 71-43-202/17/21 11:2310.2 1
Bromobenzene ND ug/kg 02/17/21 16:12 108-86-102/17/21 11:2310.2 1
Bromochloromethane ND ug/kg 02/17/21 16:12 74-97-502/17/21 11:2310.2 1
Bromodichloromethane ND ug/kg 02/17/21 16:12 75-27-402/17/21 11:2310.2 1
Bromoform ND ug/kg 02/17/21 16:12 75-25-202/17/21 11:2310.2 1
Bromomethane ND ug/kg 02/17/21 16:12 74-83-902/17/21 11:2320.4 1
2-Butanone (MEK)ND ug/kg 02/17/21 16:12 78-93-302/17/21 11:23204 1
n-Butylbenzene ND ug/kg 02/17/21 16:12 104-51-802/17/21 11:2310.2 1
sec-Butylbenzene ND ug/kg 02/17/21 16:12 135-98-802/17/21 11:2310.2 1
tert-Butylbenzene ND ug/kg 02/17/21 16:12 98-06-602/17/21 11:2310.2 1
Carbon tetrachloride ND ug/kg 02/17/21 16:12 56-23-502/17/21 11:2310.2 1
Chlorobenzene ND ug/kg 02/17/21 16:12 108-90-702/17/21 11:2310.2 1
Chloroethane ND ug/kg 02/17/21 16:12 75-00-302/17/21 11:2320.4 1
Chloroform ND ug/kg 02/17/21 16:12 67-66-302/17/21 11:2310.2 1
Chloromethane ND ug/kg 02/17/21 16:12 74-87-302/17/21 11:2320.4 1
2-Chlorotoluene ND ug/kg 02/17/21 16:12 95-49-802/17/21 11:2310.2 1
4-Chlorotoluene ND ug/kg 02/17/21 16:12 106-43-402/17/21 11:2310.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 16:12 96-12-802/17/21 11:2310.2 1
Dibromochloromethane ND ug/kg 02/17/21 16:12 124-48-102/17/21 11:2310.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 16:12 106-93-402/17/21 11:2310.2 1
Dibromomethane ND ug/kg 02/17/21 16:12 74-95-302/17/21 11:2310.2 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 16:12 95-50-102/17/21 11:2310.2 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 16:12 541-73-102/17/21 11:2310.2 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 16:12 106-46-702/17/21 11:2310.2 1
Dichlorodifluoromethane ND ug/kg 02/17/21 16:12 75-71-802/17/21 11:2320.4 1
1,1-Dichloroethane ND ug/kg 02/17/21 16:12 75-34-302/17/21 11:2310.2 1
1,2-Dichloroethane ND ug/kg 02/17/21 16:12 107-06-202/17/21 11:2310.2 1
1,1-Dichloroethene ND ug/kg 02/17/21 16:12 75-35-402/17/21 11:2310.2 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 16:12 156-59-202/17/21 11:2310.2 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 16:12 156-60-502/17/21 11:2310.2 1
1,2-Dichloropropane ND ug/kg 02/17/21 16:12 78-87-502/17/21 11:2310.2 1
1,3-Dichloropropane ND ug/kg 02/17/21 16:12 142-28-902/17/21 11:2310.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 8 Lab ID: 92522127008 Collected: 02/11/21 09:57 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 16:12 594-20-702/17/21 11:2310.2 1
1,1-Dichloropropene ND ug/kg 02/17/21 16:12 563-58-602/17/21 11:2310.2 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 16:12 10061-01-502/17/21 11:2310.2 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 16:12 10061-02-602/17/21 11:2310.2 1
Diisopropyl ether ND ug/kg 02/17/21 16:12 108-20-302/17/21 11:2310.2 1
Ethylbenzene ND ug/kg 02/17/21 16:12 100-41-402/17/21 11:2310.2 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 16:12 87-68-302/17/21 11:2320.4 1
2-Hexanone ND ug/kg 02/17/21 16:12 591-78-602/17/21 11:23102 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 16:12 98-82-802/17/21 11:2310.2 1
p-Isopropyltoluene 21.3 ug/kg 02/17/21 16:12 99-87-602/17/21 11:2310.2 1
Methylene Chloride ND ug/kg 02/17/21 16:12 75-09-202/17/21 11:2340.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 16:12 108-10-102/17/21 11:23102 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 16:12 1634-04-402/17/21 11:2310.2 1
Naphthalene ND ug/kg 02/17/21 16:12 91-20-302/17/21 11:2310.2 1
n-Propylbenzene ND ug/kg 02/17/21 16:12 103-65-102/17/21 11:2310.2 1
Styrene ND ug/kg 02/17/21 16:12 100-42-502/17/21 11:2310.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 16:12 630-20-602/17/21 11:2310.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 16:12 79-34-502/17/21 11:2310.2 1
Tetrachloroethene ND ug/kg 02/17/21 16:12 127-18-402/17/21 11:2310.2 1
Toluene ND ug/kg 02/17/21 16:12 108-88-302/17/21 11:2310.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 16:12 87-61-602/17/21 11:2310.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 16:12 120-82-102/17/21 11:2310.2 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 16:12 71-55-602/17/21 11:2310.2 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 16:12 79-00-502/17/21 11:2310.2 1
Trichloroethene ND ug/kg 02/17/21 16:12 79-01-602/17/21 11:2310.2 1
Trichlorofluoromethane ND ug/kg 02/17/21 16:12 75-69-402/17/21 11:2310.2 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 16:12 96-18-402/17/21 11:2310.2 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 16:12 95-63-602/17/21 11:2310.2 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 16:12 108-67-802/17/21 11:2310.2 1
Vinyl acetate ND ug/kg 02/17/21 16:12 108-05-402/17/21 11:23102 1
Vinyl chloride ND ug/kg 02/17/21 16:12 75-01-402/17/21 11:2320.4 1
Xylene (Total)ND ug/kg 02/17/21 16:12 1330-20-702/17/21 11:2320.4 1
m&p-Xylene ND ug/kg 02/17/21 16:12 179601-23-102/17/21 11:2320.4 1
o-Xylene ND ug/kg 02/17/21 16:12 95-47-602/17/21 11:2310.2 1
Surrogates
Toluene-d8 (S)100 %02/17/21 16:12 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)104 %02/17/21 16:12 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)101 %02/17/21 16:12 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.3 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 14 Lab ID: 92522127009 Collected: 02/11/21 10:56 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 15:5602/16/21 10:266.8 1
Surrogates
n-Pentacosane (S)72 %02/17/21 15:56 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 18:1802/15/21 11:269.4 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 18:18 460-00-402/15/21 11:2666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 16:30 67-64-102/17/21 11:23157 1
Benzene ND ug/kg 02/17/21 16:30 71-43-202/17/21 11:237.9 1
Bromobenzene ND ug/kg 02/17/21 16:30 108-86-102/17/21 11:237.9 1
Bromochloromethane ND ug/kg 02/17/21 16:30 74-97-502/17/21 11:237.9 1
Bromodichloromethane ND ug/kg 02/17/21 16:30 75-27-402/17/21 11:237.9 1
Bromoform ND ug/kg 02/17/21 16:30 75-25-202/17/21 11:237.9 1
Bromomethane ND ug/kg 02/17/21 16:30 74-83-902/17/21 11:2315.7 1
2-Butanone (MEK)ND ug/kg 02/17/21 16:30 78-93-302/17/21 11:23157 1
n-Butylbenzene ND ug/kg 02/17/21 16:30 104-51-802/17/21 11:237.9 1
sec-Butylbenzene ND ug/kg 02/17/21 16:30 135-98-802/17/21 11:237.9 1
tert-Butylbenzene ND ug/kg 02/17/21 16:30 98-06-602/17/21 11:237.9 1
Carbon tetrachloride ND ug/kg 02/17/21 16:30 56-23-502/17/21 11:237.9 1
Chlorobenzene ND ug/kg 02/17/21 16:30 108-90-702/17/21 11:237.9 1
Chloroethane ND ug/kg 02/17/21 16:30 75-00-302/17/21 11:2315.7 1
Chloroform ND ug/kg 02/17/21 16:30 67-66-302/17/21 11:237.9 1
Chloromethane ND ug/kg 02/17/21 16:30 74-87-302/17/21 11:2315.7 1
2-Chlorotoluene ND ug/kg 02/17/21 16:30 95-49-802/17/21 11:237.9 1
4-Chlorotoluene ND ug/kg 02/17/21 16:30 106-43-402/17/21 11:237.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 16:30 96-12-802/17/21 11:237.9 1
Dibromochloromethane ND ug/kg 02/17/21 16:30 124-48-102/17/21 11:237.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 16:30 106-93-402/17/21 11:237.9 1
Dibromomethane ND ug/kg 02/17/21 16:30 74-95-302/17/21 11:237.9 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 16:30 95-50-102/17/21 11:237.9 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 16:30 541-73-102/17/21 11:237.9 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 16:30 106-46-702/17/21 11:237.9 1
Dichlorodifluoromethane ND ug/kg 02/17/21 16:30 75-71-802/17/21 11:2315.7 1
1,1-Dichloroethane ND ug/kg 02/17/21 16:30 75-34-302/17/21 11:237.9 1
1,2-Dichloroethane ND ug/kg 02/17/21 16:30 107-06-202/17/21 11:237.9 1
1,1-Dichloroethene ND ug/kg 02/17/21 16:30 75-35-402/17/21 11:237.9 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 16:30 156-59-202/17/21 11:237.9 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 16:30 156-60-502/17/21 11:237.9 1
1,2-Dichloropropane ND ug/kg 02/17/21 16:30 78-87-502/17/21 11:237.9 1
1,3-Dichloropropane ND ug/kg 02/17/21 16:30 142-28-902/17/21 11:237.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 14 Lab ID: 92522127009 Collected: 02/11/21 10:56 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 16:30 594-20-702/17/21 11:237.9 1
1,1-Dichloropropene ND ug/kg 02/17/21 16:30 563-58-602/17/21 11:237.9 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 16:30 10061-01-502/17/21 11:237.9 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 16:30 10061-02-602/17/21 11:237.9 1
Diisopropyl ether ND ug/kg 02/17/21 16:30 108-20-302/17/21 11:237.9 1
Ethylbenzene ND ug/kg 02/17/21 16:30 100-41-402/17/21 11:237.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 16:30 87-68-302/17/21 11:2315.7 1
2-Hexanone ND ug/kg 02/17/21 16:30 591-78-602/17/21 11:2378.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 16:30 98-82-802/17/21 11:237.9 1
p-Isopropyltoluene ND ug/kg 02/17/21 16:30 99-87-602/17/21 11:237.9 1
Methylene Chloride ND ug/kg 02/17/21 16:30 75-09-202/17/21 11:2331.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 16:30 108-10-102/17/21 11:2378.6 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 16:30 1634-04-402/17/21 11:237.9 1
Naphthalene ND ug/kg 02/17/21 16:30 91-20-302/17/21 11:237.9 1
n-Propylbenzene ND ug/kg 02/17/21 16:30 103-65-102/17/21 11:237.9 1
Styrene ND ug/kg 02/17/21 16:30 100-42-502/17/21 11:237.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 16:30 630-20-602/17/21 11:237.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 16:30 79-34-502/17/21 11:237.9 1
Tetrachloroethene ND ug/kg 02/17/21 16:30 127-18-402/17/21 11:237.9 1
Toluene ND ug/kg 02/17/21 16:30 108-88-302/17/21 11:237.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 16:30 87-61-602/17/21 11:237.9 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 16:30 120-82-102/17/21 11:237.9 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 16:30 71-55-602/17/21 11:237.9 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 16:30 79-00-502/17/21 11:237.9 1
Trichloroethene ND ug/kg 02/17/21 16:30 79-01-602/17/21 11:237.9 1
Trichlorofluoromethane ND ug/kg 02/17/21 16:30 75-69-402/17/21 11:237.9 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 16:30 96-18-402/17/21 11:237.9 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 16:30 95-63-602/17/21 11:237.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 16:30 108-67-802/17/21 11:237.9 1
Vinyl acetate ND ug/kg 02/17/21 16:30 108-05-402/17/21 11:2378.6 1
Vinyl chloride ND ug/kg 02/17/21 16:30 75-01-402/17/21 11:2315.7 1
Xylene (Total)ND ug/kg 02/17/21 16:30 1330-20-702/17/21 11:2315.7 1
m&p-Xylene ND ug/kg 02/17/21 16:30 179601-23-102/17/21 11:2315.7 1
o-Xylene ND ug/kg 02/17/21 16:30 95-47-602/17/21 11:237.9 1
Surrogates
Toluene-d8 (S)100 %02/17/21 16:30 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)101 %02/17/21 16:30 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)104 %02/17/21 16:30 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.3 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 15 Lab ID: 92522127010 Collected: 02/11/21 11:14 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 15:5602/16/21 10:265.7 1
Surrogates
n-Pentacosane (S)76 %02/17/21 15:56 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 18:4602/15/21 11:3610 1
Surrogates
4-Bromofluorobenzene (S)77 %02/15/21 18:46 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 16:48 67-64-102/17/21 11:23117 1
Benzene ND ug/kg 02/17/21 16:48 71-43-202/17/21 11:235.8 1
Bromobenzene ND ug/kg 02/17/21 16:48 108-86-102/17/21 11:235.8 1
Bromochloromethane ND ug/kg 02/17/21 16:48 74-97-502/17/21 11:235.8 1
Bromodichloromethane ND ug/kg 02/17/21 16:48 75-27-402/17/21 11:235.8 1
Bromoform ND ug/kg 02/17/21 16:48 75-25-202/17/21 11:235.8 1
Bromomethane ND ug/kg 02/17/21 16:48 74-83-902/17/21 11:2311.7 1
2-Butanone (MEK)ND ug/kg 02/17/21 16:48 78-93-302/17/21 11:23117 1
n-Butylbenzene ND ug/kg 02/17/21 16:48 104-51-802/17/21 11:235.8 1
sec-Butylbenzene ND ug/kg 02/17/21 16:48 135-98-802/17/21 11:235.8 1
tert-Butylbenzene ND ug/kg 02/17/21 16:48 98-06-602/17/21 11:235.8 1
Carbon tetrachloride ND ug/kg 02/17/21 16:48 56-23-502/17/21 11:235.8 1
Chlorobenzene ND ug/kg 02/17/21 16:48 108-90-702/17/21 11:235.8 1
Chloroethane ND ug/kg 02/17/21 16:48 75-00-302/17/21 11:2311.7 1
Chloroform ND ug/kg 02/17/21 16:48 67-66-302/17/21 11:235.8 1
Chloromethane ND ug/kg 02/17/21 16:48 74-87-302/17/21 11:2311.7 1
2-Chlorotoluene ND ug/kg 02/17/21 16:48 95-49-802/17/21 11:235.8 1
4-Chlorotoluene ND ug/kg 02/17/21 16:48 106-43-402/17/21 11:235.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 16:48 96-12-802/17/21 11:235.8 1
Dibromochloromethane ND ug/kg 02/17/21 16:48 124-48-102/17/21 11:235.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 16:48 106-93-402/17/21 11:235.8 1
Dibromomethane ND ug/kg 02/17/21 16:48 74-95-302/17/21 11:235.8 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 16:48 95-50-102/17/21 11:235.8 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 16:48 541-73-102/17/21 11:235.8 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 16:48 106-46-702/17/21 11:235.8 1
Dichlorodifluoromethane ND ug/kg 02/17/21 16:48 75-71-802/17/21 11:2311.7 1
1,1-Dichloroethane ND ug/kg 02/17/21 16:48 75-34-302/17/21 11:235.8 1
1,2-Dichloroethane ND ug/kg 02/17/21 16:48 107-06-202/17/21 11:235.8 1
1,1-Dichloroethene ND ug/kg 02/17/21 16:48 75-35-402/17/21 11:235.8 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 16:48 156-59-202/17/21 11:235.8 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 16:48 156-60-502/17/21 11:235.8 1
1,2-Dichloropropane ND ug/kg 02/17/21 16:48 78-87-502/17/21 11:235.8 1
1,3-Dichloropropane ND ug/kg 02/17/21 16:48 142-28-902/17/21 11:235.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 15 Lab ID: 92522127010 Collected: 02/11/21 11:14 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 16:48 594-20-702/17/21 11:235.8 1
1,1-Dichloropropene ND ug/kg 02/17/21 16:48 563-58-602/17/21 11:235.8 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 16:48 10061-01-502/17/21 11:235.8 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 16:48 10061-02-602/17/21 11:235.8 1
Diisopropyl ether ND ug/kg 02/17/21 16:48 108-20-302/17/21 11:235.8 1
Ethylbenzene ND ug/kg 02/17/21 16:48 100-41-402/17/21 11:235.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 16:48 87-68-302/17/21 11:2311.7 1
2-Hexanone ND ug/kg 02/17/21 16:48 591-78-602/17/21 11:2358.4 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 16:48 98-82-802/17/21 11:235.8 1
p-Isopropyltoluene ND ug/kg 02/17/21 16:48 99-87-602/17/21 11:235.8 1
Methylene Chloride ND ug/kg 02/17/21 16:48 75-09-202/17/21 11:2323.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 16:48 108-10-102/17/21 11:2358.4 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 16:48 1634-04-402/17/21 11:235.8 1
Naphthalene ND ug/kg 02/17/21 16:48 91-20-302/17/21 11:235.8 1
n-Propylbenzene ND ug/kg 02/17/21 16:48 103-65-102/17/21 11:235.8 1
Styrene ND ug/kg 02/17/21 16:48 100-42-502/17/21 11:235.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 16:48 630-20-602/17/21 11:235.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 16:48 79-34-502/17/21 11:235.8 1
Tetrachloroethene ND ug/kg 02/17/21 16:48 127-18-402/17/21 11:235.8 1
Toluene ND ug/kg 02/17/21 16:48 108-88-302/17/21 11:235.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 16:48 87-61-602/17/21 11:235.8 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 16:48 120-82-102/17/21 11:235.8 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 16:48 71-55-602/17/21 11:235.8 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 16:48 79-00-502/17/21 11:235.8 1
Trichloroethene ND ug/kg 02/17/21 16:48 79-01-602/17/21 11:235.8 1
Trichlorofluoromethane ND ug/kg 02/17/21 16:48 75-69-402/17/21 11:235.8 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 16:48 96-18-402/17/21 11:235.8 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 16:48 95-63-602/17/21 11:235.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 16:48 108-67-802/17/21 11:235.8 1
Vinyl acetate ND ug/kg 02/17/21 16:48 108-05-402/17/21 11:2358.4 1
Vinyl chloride ND ug/kg 02/17/21 16:48 75-01-402/17/21 11:2311.7 1
Xylene (Total)ND ug/kg 02/17/21 16:48 1330-20-702/17/21 11:2311.7 1
m&p-Xylene ND ug/kg 02/17/21 16:48 179601-23-102/17/21 11:2311.7 1
o-Xylene ND ug/kg 02/17/21 16:48 95-47-602/17/21 11:235.8 1
Surrogates
Toluene-d8 (S)99 %02/17/21 16:48 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)103 %02/17/21 16:48 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)101 %02/17/21 16:48 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.5 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 16 Lab ID: 92522127011 Collected: 02/11/21 12:56 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 16:2002/16/21 10:266.2 1
Surrogates
n-Pentacosane (S)73 %02/17/21 16:20 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 19:1402/15/21 11:368.7 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 19:14 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 17:06 67-64-102/17/21 11:23146 1
Benzene ND ug/kg 02/17/21 17:06 71-43-202/17/21 11:237.3 1
Bromobenzene ND ug/kg 02/17/21 17:06 108-86-102/17/21 11:237.3 1
Bromochloromethane ND ug/kg 02/17/21 17:06 74-97-502/17/21 11:237.3 1
Bromodichloromethane ND ug/kg 02/17/21 17:06 75-27-402/17/21 11:237.3 1
Bromoform ND ug/kg 02/17/21 17:06 75-25-202/17/21 11:237.3 1
Bromomethane ND ug/kg 02/17/21 17:06 74-83-902/17/21 11:2314.6 1
2-Butanone (MEK)ND ug/kg 02/17/21 17:06 78-93-302/17/21 11:23146 1
n-Butylbenzene ND ug/kg 02/17/21 17:06 104-51-802/17/21 11:237.3 1
sec-Butylbenzene ND ug/kg 02/17/21 17:06 135-98-802/17/21 11:237.3 1
tert-Butylbenzene ND ug/kg 02/17/21 17:06 98-06-602/17/21 11:237.3 1
Carbon tetrachloride ND ug/kg 02/17/21 17:06 56-23-502/17/21 11:237.3 1
Chlorobenzene ND ug/kg 02/17/21 17:06 108-90-702/17/21 11:237.3 1
Chloroethane ND ug/kg 02/17/21 17:06 75-00-302/17/21 11:2314.6 1
Chloroform ND ug/kg 02/17/21 17:06 67-66-302/17/21 11:237.3 1
Chloromethane ND ug/kg 02/17/21 17:06 74-87-302/17/21 11:2314.6 1
2-Chlorotoluene ND ug/kg 02/17/21 17:06 95-49-802/17/21 11:237.3 1
4-Chlorotoluene ND ug/kg 02/17/21 17:06 106-43-402/17/21 11:237.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 17:06 96-12-802/17/21 11:237.3 1
Dibromochloromethane ND ug/kg 02/17/21 17:06 124-48-102/17/21 11:237.3 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 17:06 106-93-402/17/21 11:237.3 1
Dibromomethane ND ug/kg 02/17/21 17:06 74-95-302/17/21 11:237.3 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 17:06 95-50-102/17/21 11:237.3 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 17:06 541-73-102/17/21 11:237.3 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 17:06 106-46-702/17/21 11:237.3 1
Dichlorodifluoromethane ND ug/kg 02/17/21 17:06 75-71-802/17/21 11:2314.6 1
1,1-Dichloroethane ND ug/kg 02/17/21 17:06 75-34-302/17/21 11:237.3 1
1,2-Dichloroethane ND ug/kg 02/17/21 17:06 107-06-202/17/21 11:237.3 1
1,1-Dichloroethene ND ug/kg 02/17/21 17:06 75-35-402/17/21 11:237.3 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 17:06 156-59-202/17/21 11:237.3 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 17:06 156-60-502/17/21 11:237.3 1
1,2-Dichloropropane ND ug/kg 02/17/21 17:06 78-87-502/17/21 11:237.3 1
1,3-Dichloropropane ND ug/kg 02/17/21 17:06 142-28-902/17/21 11:237.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Remote Fill 16 Lab ID: 92522127011 Collected: 02/11/21 12:56 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 17:06 594-20-702/17/21 11:237.3 1
1,1-Dichloropropene ND ug/kg 02/17/21 17:06 563-58-602/17/21 11:237.3 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 17:06 10061-01-502/17/21 11:237.3 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 17:06 10061-02-602/17/21 11:237.3 1
Diisopropyl ether ND ug/kg 02/17/21 17:06 108-20-302/17/21 11:237.3 1
Ethylbenzene ND ug/kg 02/17/21 17:06 100-41-402/17/21 11:237.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 17:06 87-68-302/17/21 11:2314.6 1
2-Hexanone ND ug/kg 02/17/21 17:06 591-78-602/17/21 11:2372.8 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 17:06 98-82-802/17/21 11:237.3 1
p-Isopropyltoluene ND ug/kg 02/17/21 17:06 99-87-602/17/21 11:237.3 1
Methylene Chloride ND ug/kg 02/17/21 17:06 75-09-202/17/21 11:2329.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 17:06 108-10-102/17/21 11:2372.8 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 17:06 1634-04-402/17/21 11:237.3 1
Naphthalene ND ug/kg 02/17/21 17:06 91-20-302/17/21 11:237.3 1
n-Propylbenzene ND ug/kg 02/17/21 17:06 103-65-102/17/21 11:237.3 1
Styrene ND ug/kg 02/17/21 17:06 100-42-502/17/21 11:237.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 17:06 630-20-602/17/21 11:237.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 17:06 79-34-502/17/21 11:237.3 1
Tetrachloroethene ND ug/kg 02/17/21 17:06 127-18-402/17/21 11:237.3 1
Toluene ND ug/kg 02/17/21 17:06 108-88-302/17/21 11:237.3 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 17:06 87-61-602/17/21 11:237.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 17:06 120-82-102/17/21 11:237.3 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 17:06 71-55-602/17/21 11:237.3 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 17:06 79-00-502/17/21 11:237.3 1
Trichloroethene ND ug/kg 02/17/21 17:06 79-01-602/17/21 11:237.3 1
Trichlorofluoromethane ND ug/kg 02/17/21 17:06 75-69-402/17/21 11:237.3 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 17:06 96-18-402/17/21 11:237.3 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 17:06 95-63-602/17/21 11:237.3 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 17:06 108-67-802/17/21 11:237.3 1
Vinyl acetate ND ug/kg 02/17/21 17:06 108-05-402/17/21 11:2372.8 1
Vinyl chloride ND ug/kg 02/17/21 17:06 75-01-402/17/21 11:2314.6 1
Xylene (Total)ND ug/kg 02/17/21 17:06 1330-20-702/17/21 11:2314.6 1
m&p-Xylene ND ug/kg 02/17/21 17:06 179601-23-102/17/21 11:2314.6 1
o-Xylene ND ug/kg 02/17/21 17:06 95-47-602/17/21 11:237.3 1
Surrogates
Toluene-d8 (S)100 %02/17/21 17:06 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)100 %02/17/21 17:06 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)102 %02/17/21 17:06 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.9 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 18 Lab ID: 92522127012 Collected: 02/11/21 13:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 16:2002/16/21 10:266.8 1
Surrogates
n-Pentacosane (S)79 %02/17/21 16:20 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 19:4202/15/21 11:3611.0 1
Surrogates
4-Bromofluorobenzene (S)81 %02/15/21 19:42 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 17:24 67-64-102/17/21 11:23150 1
Benzene 160 ug/kg 02/17/21 17:24 71-43-202/17/21 11:237.5 1
Bromobenzene ND ug/kg 02/17/21 17:24 108-86-102/17/21 11:237.5 1
Bromochloromethane ND ug/kg 02/17/21 17:24 74-97-502/17/21 11:237.5 1
Bromodichloromethane ND ug/kg 02/17/21 17:24 75-27-402/17/21 11:237.5 1
Bromoform ND ug/kg 02/17/21 17:24 75-25-202/17/21 11:237.5 1
Bromomethane ND ug/kg 02/17/21 17:24 74-83-902/17/21 11:2315.0 1
2-Butanone (MEK)ND ug/kg 02/17/21 17:24 78-93-302/17/21 11:23150 1
n-Butylbenzene ND ug/kg 02/17/21 17:24 104-51-802/17/21 11:237.5 1
sec-Butylbenzene ND ug/kg 02/17/21 17:24 135-98-802/17/21 11:237.5 1
tert-Butylbenzene ND ug/kg 02/17/21 17:24 98-06-602/17/21 11:237.5 1
Carbon tetrachloride ND ug/kg 02/17/21 17:24 56-23-502/17/21 11:237.5 1
Chlorobenzene ND ug/kg 02/17/21 17:24 108-90-702/17/21 11:237.5 1
Chloroethane ND ug/kg 02/17/21 17:24 75-00-302/17/21 11:2315.0 1
Chloroform ND ug/kg 02/17/21 17:24 67-66-302/17/21 11:237.5 1
Chloromethane ND ug/kg 02/17/21 17:24 74-87-302/17/21 11:2315.0 1
2-Chlorotoluene ND ug/kg 02/17/21 17:24 95-49-802/17/21 11:237.5 1
4-Chlorotoluene ND ug/kg 02/17/21 17:24 106-43-402/17/21 11:237.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 17:24 96-12-802/17/21 11:237.5 1
Dibromochloromethane ND ug/kg 02/17/21 17:24 124-48-102/17/21 11:237.5 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 17:24 106-93-402/17/21 11:237.5 1
Dibromomethane ND ug/kg 02/17/21 17:24 74-95-302/17/21 11:237.5 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 17:24 95-50-102/17/21 11:237.5 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 17:24 541-73-102/17/21 11:237.5 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 17:24 106-46-702/17/21 11:237.5 1
Dichlorodifluoromethane ND ug/kg 02/17/21 17:24 75-71-802/17/21 11:2315.0 1
1,1-Dichloroethane ND ug/kg 02/17/21 17:24 75-34-302/17/21 11:237.5 1
1,2-Dichloroethane ND ug/kg 02/17/21 17:24 107-06-202/17/21 11:237.5 1
1,1-Dichloroethene ND ug/kg 02/17/21 17:24 75-35-402/17/21 11:237.5 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 17:24 156-59-202/17/21 11:237.5 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 17:24 156-60-502/17/21 11:237.5 1
1,2-Dichloropropane ND ug/kg 02/17/21 17:24 78-87-502/17/21 11:237.5 1
1,3-Dichloropropane ND ug/kg 02/17/21 17:24 142-28-902/17/21 11:237.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 18 Lab ID: 92522127012 Collected: 02/11/21 13:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
2,2-Dichloropropane ND ug/kg 02/17/21 17:24 594-20-702/17/21 11:237.5 1
1,1-Dichloropropene ND ug/kg 02/17/21 17:24 563-58-602/17/21 11:237.5 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 17:24 10061-01-502/17/21 11:237.5 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 17:24 10061-02-602/17/21 11:237.5 1
Diisopropyl ether 13.0 ug/kg 02/17/21 17:24 108-20-302/17/21 11:237.5 1
Ethylbenzene 10.2 ug/kg 02/17/21 17:24 100-41-402/17/21 11:237.5 1
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 17:24 87-68-302/17/21 11:2315.0 1
2-Hexanone ND ug/kg 02/17/21 17:24 591-78-602/17/21 11:2375.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 17:24 98-82-802/17/21 11:237.5 1
p-Isopropyltoluene ND ug/kg 02/17/21 17:24 99-87-602/17/21 11:237.5 1
Methylene Chloride ND ug/kg 02/17/21 17:24 75-09-202/17/21 11:2330.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 17:24 108-10-102/17/21 11:2375.2 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 17:24 1634-04-402/17/21 11:237.5 1
Naphthalene ND ug/kg 02/17/21 17:24 91-20-302/17/21 11:237.5 1
n-Propylbenzene ND ug/kg 02/17/21 17:24 103-65-102/17/21 11:237.5 1
Styrene ND ug/kg 02/17/21 17:24 100-42-502/17/21 11:237.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 17:24 630-20-602/17/21 11:237.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 17:24 79-34-502/17/21 11:237.5 1
Tetrachloroethene ND ug/kg 02/17/21 17:24 127-18-402/17/21 11:237.5 1
Toluene 374 ug/kg 02/17/21 17:24 108-88-302/17/21 11:237.5 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 17:24 87-61-602/17/21 11:237.5 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 17:24 120-82-102/17/21 11:237.5 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 17:24 71-55-602/17/21 11:237.5 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 17:24 79-00-502/17/21 11:237.5 1
Trichloroethene ND ug/kg 02/17/21 17:24 79-01-602/17/21 11:237.5 1
Trichlorofluoromethane ND ug/kg 02/17/21 17:24 75-69-402/17/21 11:237.5 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 17:24 96-18-402/17/21 11:237.5 1
1,2,4-Trimethylbenzene 27.8 ug/kg 02/17/21 17:24 95-63-602/17/21 11:237.5 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 17:24 108-67-802/17/21 11:237.5 1
Vinyl acetate ND ug/kg 02/17/21 17:24 108-05-402/17/21 11:2375.2 1
Vinyl chloride ND ug/kg 02/17/21 17:24 75-01-402/17/21 11:2315.0 1
Xylene (Total)322 ug/kg 02/17/21 17:24 1330-20-702/17/21 11:2315.0 1
m&p-Xylene 217 ug/kg 02/17/21 17:24 179601-23-102/17/21 11:2315.0 1
o-Xylene 105 ug/kg 02/17/21 17:24 95-47-602/17/21 11:237.5 1
Surrogates
Toluene-d8 (S)99 %02/17/21 17:24 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)97 %02/17/21 17:24 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)99 %02/17/21 17:24 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.7 %02/15/21 13:16 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 9 Lab ID: 92522127013 Collected: 02/11/21 10:11 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 20:1102/15/21 11:368.4 1
Surrogates
4-Bromofluorobenzene (S)78 %02/15/21 20:11 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 17:42 67-64-102/17/21 11:23143 1
Benzene 41.0 ug/kg 02/17/21 17:42 71-43-202/17/21 11:237.1 1
Bromobenzene ND ug/kg 02/17/21 17:42 108-86-102/17/21 11:237.1 1
Bromochloromethane ND ug/kg 02/17/21 17:42 74-97-502/17/21 11:237.1 1
Bromodichloromethane ND ug/kg 02/17/21 17:42 75-27-402/17/21 11:237.1 1
Bromoform ND ug/kg 02/17/21 17:42 75-25-202/17/21 11:237.1 1
Bromomethane ND ug/kg 02/17/21 17:42 74-83-902/17/21 11:2314.3 1
2-Butanone (MEK)ND ug/kg 02/17/21 17:42 78-93-302/17/21 11:23143 1
n-Butylbenzene ND ug/kg 02/17/21 17:42 104-51-802/17/21 11:237.1 1
sec-Butylbenzene ND ug/kg 02/17/21 17:42 135-98-802/17/21 11:237.1 1
tert-Butylbenzene ND ug/kg 02/17/21 17:42 98-06-602/17/21 11:237.1 1
Carbon tetrachloride ND ug/kg 02/17/21 17:42 56-23-502/17/21 11:237.1 1
Chlorobenzene ND ug/kg 02/17/21 17:42 108-90-702/17/21 11:237.1 1
Chloroethane ND ug/kg 02/17/21 17:42 75-00-302/17/21 11:2314.3 1
Chloroform ND ug/kg 02/17/21 17:42 67-66-302/17/21 11:237.1 1
Chloromethane ND ug/kg 02/17/21 17:42 74-87-302/17/21 11:2314.3 1
2-Chlorotoluene ND ug/kg 02/17/21 17:42 95-49-802/17/21 11:237.1 1
4-Chlorotoluene ND ug/kg 02/17/21 17:42 106-43-402/17/21 11:237.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 17:42 96-12-802/17/21 11:237.1 1
Dibromochloromethane ND ug/kg 02/17/21 17:42 124-48-102/17/21 11:237.1 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 17:42 106-93-402/17/21 11:237.1 1
Dibromomethane ND ug/kg 02/17/21 17:42 74-95-302/17/21 11:237.1 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 17:42 95-50-102/17/21 11:237.1 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 17:42 541-73-102/17/21 11:237.1 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 17:42 106-46-702/17/21 11:237.1 1
Dichlorodifluoromethane ND ug/kg 02/17/21 17:42 75-71-802/17/21 11:2314.3 1
1,1-Dichloroethane ND ug/kg 02/17/21 17:42 75-34-302/17/21 11:237.1 1
1,2-Dichloroethane ND ug/kg 02/17/21 17:42 107-06-202/17/21 11:237.1 1
1,1-Dichloroethene ND ug/kg 02/17/21 17:42 75-35-402/17/21 11:237.1 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 17:42 156-59-202/17/21 11:237.1 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 17:42 156-60-502/17/21 11:237.1 1
1,2-Dichloropropane ND ug/kg 02/17/21 17:42 78-87-502/17/21 11:237.1 1
1,3-Dichloropropane ND ug/kg 02/17/21 17:42 142-28-902/17/21 11:237.1 1
2,2-Dichloropropane ND ug/kg 02/17/21 17:42 594-20-702/17/21 11:237.1 1
1,1-Dichloropropene ND ug/kg 02/17/21 17:42 563-58-602/17/21 11:237.1 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 17:42 10061-01-502/17/21 11:237.1 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 17:42 10061-02-602/17/21 11:237.1 1
Diisopropyl ether ND ug/kg 02/17/21 17:42 108-20-302/17/21 11:237.1 1
Ethylbenzene 331 ug/kg 02/17/21 17:42 100-41-402/17/21 11:237.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 9 Lab ID: 92522127013 Collected: 02/11/21 10:11 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 17:42 87-68-302/17/21 11:2314.3 1
2-Hexanone ND ug/kg 02/17/21 17:42 591-78-602/17/21 11:2371.3 1
Isopropylbenzene (Cumene)196 ug/kg 02/17/21 17:42 98-82-802/17/21 11:237.1 1
p-Isopropyltoluene ND ug/kg 02/17/21 17:42 99-87-602/17/21 11:237.1 1
Methylene Chloride ND ug/kg 02/17/21 17:42 75-09-202/17/21 11:2328.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 17:42 108-10-102/17/21 11:2371.3 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 17:42 1634-04-402/17/21 11:237.1 1
Naphthalene 281 ug/kg 02/17/21 17:42 91-20-302/17/21 11:237.1 1
n-Propylbenzene ND ug/kg 02/17/21 17:42 103-65-102/17/21 11:237.1 1
Styrene ND ug/kg 02/17/21 17:42 100-42-502/17/21 11:237.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 17:42 630-20-602/17/21 11:237.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 17:42 79-34-502/17/21 11:237.1 1
Tetrachloroethene ND ug/kg 02/17/21 17:42 127-18-402/17/21 11:237.1 1
Toluene 71.5 ug/kg 02/17/21 17:42 108-88-302/17/21 11:237.1 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 17:42 87-61-602/17/21 11:237.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 17:42 120-82-102/17/21 11:237.1 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 17:42 71-55-602/17/21 11:237.1 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 17:42 79-00-502/17/21 11:237.1 1
Trichloroethene ND ug/kg 02/17/21 17:42 79-01-602/17/21 11:237.1 1
Trichlorofluoromethane ND ug/kg 02/17/21 17:42 75-69-402/17/21 11:237.1 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 17:42 96-18-402/17/21 11:237.1 1
1,2,4-Trimethylbenzene 2370 ug/kg 02/17/21 17:42 95-63-602/17/21 11:237.1 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 17:42 108-67-802/17/21 11:237.1 1
Vinyl acetate ND ug/kg 02/17/21 17:42 108-05-402/17/21 11:2371.3 1
Vinyl chloride ND ug/kg 02/17/21 17:42 75-01-402/17/21 11:2314.3 1
Xylene (Total)1470 ug/kg 02/17/21 17:42 1330-20-702/17/21 11:2314.3 1
m&p-Xylene 926 ug/kg 02/17/21 17:42 179601-23-102/17/21 11:2314.3 1
o-Xylene 540 ug/kg 02/17/21 17:42 95-47-602/17/21 11:237.1 1
Surrogates
Toluene-d8 (S)101 %02/17/21 17:42 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)104 %02/17/21 17:42 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)100 %02/17/21 17:42 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.8 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 10 Lab ID: 92522127014 Collected: 02/11/21 10:19 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)16.7 mg/kg 02/15/21 20:3902/15/21 11:368.9 1
Surrogates
4-Bromofluorobenzene (S)81 %02/15/21 20:39 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 18:00 67-64-102/17/21 11:23169 1
Benzene 14.4 ug/kg 02/17/21 18:00 71-43-202/17/21 11:238.5 1
Bromobenzene ND ug/kg 02/17/21 18:00 108-86-102/17/21 11:238.5 1
Bromochloromethane ND ug/kg 02/17/21 18:00 74-97-502/17/21 11:238.5 1
Bromodichloromethane ND ug/kg 02/17/21 18:00 75-27-402/17/21 11:238.5 1
Bromoform ND ug/kg 02/17/21 18:00 75-25-202/17/21 11:238.5 1
Bromomethane ND ug/kg 02/17/21 18:00 74-83-902/17/21 11:2316.9 1
2-Butanone (MEK)ND ug/kg 02/17/21 18:00 78-93-302/17/21 11:23169 1
n-Butylbenzene ND ug/kg 02/17/21 18:00 104-51-802/17/21 11:238.5 1
sec-Butylbenzene ND ug/kg 02/17/21 18:00 135-98-802/17/21 11:238.5 1
tert-Butylbenzene ND ug/kg 02/17/21 18:00 98-06-602/17/21 11:238.5 1
Carbon tetrachloride ND ug/kg 02/17/21 18:00 56-23-502/17/21 11:238.5 1
Chlorobenzene ND ug/kg 02/17/21 18:00 108-90-702/17/21 11:238.5 1
Chloroethane ND ug/kg 02/17/21 18:00 75-00-302/17/21 11:2316.9 1
Chloroform ND ug/kg 02/17/21 18:00 67-66-302/17/21 11:238.5 1
Chloromethane ND ug/kg 02/17/21 18:00 74-87-302/17/21 11:2316.9 1
2-Chlorotoluene ND ug/kg 02/17/21 18:00 95-49-802/17/21 11:238.5 1
4-Chlorotoluene ND ug/kg 02/17/21 18:00 106-43-402/17/21 11:238.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 18:00 96-12-802/17/21 11:238.5 1
Dibromochloromethane ND ug/kg 02/17/21 18:00 124-48-102/17/21 11:238.5 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 18:00 106-93-402/17/21 11:238.5 1
Dibromomethane ND ug/kg 02/17/21 18:00 74-95-302/17/21 11:238.5 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 18:00 95-50-102/17/21 11:238.5 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 18:00 541-73-102/17/21 11:238.5 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 18:00 106-46-702/17/21 11:238.5 1
Dichlorodifluoromethane ND ug/kg 02/17/21 18:00 75-71-802/17/21 11:2316.9 1
1,1-Dichloroethane ND ug/kg 02/17/21 18:00 75-34-302/17/21 11:238.5 1
1,2-Dichloroethane ND ug/kg 02/17/21 18:00 107-06-202/17/21 11:238.5 1
1,1-Dichloroethene ND ug/kg 02/17/21 18:00 75-35-402/17/21 11:238.5 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 18:00 156-59-202/17/21 11:238.5 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 18:00 156-60-502/17/21 11:238.5 1
1,2-Dichloropropane ND ug/kg 02/17/21 18:00 78-87-502/17/21 11:238.5 1
1,3-Dichloropropane ND ug/kg 02/17/21 18:00 142-28-902/17/21 11:238.5 1
2,2-Dichloropropane ND ug/kg 02/17/21 18:00 594-20-702/17/21 11:238.5 1
1,1-Dichloropropene ND ug/kg 02/17/21 18:00 563-58-602/17/21 11:238.5 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 18:00 10061-01-502/17/21 11:238.5 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 18:00 10061-02-602/17/21 11:238.5 1
Diisopropyl ether ND ug/kg 02/17/21 18:00 108-20-302/17/21 11:238.5 1
Ethylbenzene 207 ug/kg 02/17/21 18:00 100-41-402/17/21 11:238.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 10 Lab ID: 92522127014 Collected: 02/11/21 10:19 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 18:00 87-68-302/17/21 11:2316.9 1
2-Hexanone ND ug/kg 02/17/21 18:00 591-78-602/17/21 11:2384.6 1
Isopropylbenzene (Cumene)216 ug/kg 02/17/21 18:00 98-82-802/17/21 11:238.5 1
p-Isopropyltoluene ND ug/kg 02/17/21 18:00 99-87-602/17/21 11:238.5 1
Methylene Chloride ND ug/kg 02/17/21 18:00 75-09-202/17/21 11:2333.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 18:00 108-10-102/17/21 11:2384.6 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 18:00 1634-04-402/17/21 11:238.5 1
Naphthalene 625 ug/kg 02/17/21 18:00 91-20-302/17/21 11:238.5 1
n-Propylbenzene 1050 ug/kg 02/17/21 18:00 103-65-102/17/21 11:238.5 1
Styrene ND ug/kg 02/17/21 18:00 100-42-502/17/21 11:238.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 18:00 630-20-602/17/21 11:238.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 18:00 79-34-502/17/21 11:238.5 1
Tetrachloroethene ND ug/kg 02/17/21 18:00 127-18-402/17/21 11:238.5 1
Toluene 59.3 ug/kg 02/17/21 18:00 108-88-302/17/21 11:238.5 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 18:00 87-61-602/17/21 11:238.5 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 18:00 120-82-102/17/21 11:238.5 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 18:00 71-55-602/17/21 11:238.5 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 18:00 79-00-502/17/21 11:238.5 1
Trichloroethene ND ug/kg 02/17/21 18:00 79-01-602/17/21 11:238.5 1
Trichlorofluoromethane ND ug/kg 02/17/21 18:00 75-69-402/17/21 11:238.5 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 18:00 96-18-402/17/21 11:238.5 1
1,2,4-Trimethylbenzene 7350 ug/kg 02/17/21 18:00 95-63-602/17/21 11:238.5 1
1,3,5-Trimethylbenzene 1820 ug/kg 02/17/21 18:00 108-67-802/17/21 11:238.5 1
Vinyl acetate ND ug/kg 02/17/21 18:00 108-05-402/17/21 11:2384.6 1
Vinyl chloride ND ug/kg 02/17/21 18:00 75-01-402/17/21 11:2316.9 1
Xylene (Total)785 ug/kg 02/17/21 18:00 1330-20-702/17/21 11:2316.9 1
m&p-Xylene 721 ug/kg 02/17/21 18:00 179601-23-102/17/21 11:2316.9 1
o-Xylene 64.2 ug/kg 02/17/21 18:00 95-47-602/17/21 11:238.5 1
Surrogates
Toluene-d8 (S)101 %02/17/21 18:00 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)102 %02/17/21 18:00 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)104 %02/17/21 18:00 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.4 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 11 Lab ID: 92522127015 Collected: 02/11/21 10:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 21:0702/15/21 11:3610.6 1
Surrogates
4-Bromofluorobenzene (S)82 %02/15/21 21:07 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/18/21 11:15 67-64-102/18/21 09:42172 1
Benzene ND ug/kg 02/18/21 11:15 71-43-202/18/21 09:428.6 1
Bromobenzene ND ug/kg 02/18/21 11:15 108-86-102/18/21 09:428.6 1
Bromochloromethane ND ug/kg 02/18/21 11:15 74-97-502/18/21 09:428.6 1
Bromodichloromethane ND ug/kg 02/18/21 11:15 75-27-402/18/21 09:428.6 1
Bromoform ND ug/kg 02/18/21 11:15 75-25-202/18/21 09:428.6 1
Bromomethane ND ug/kg 02/18/21 11:15 74-83-902/18/21 09:4217.2 1
2-Butanone (MEK)ND ug/kg 02/18/21 11:15 78-93-302/18/21 09:42172 1
n-Butylbenzene ND ug/kg 02/18/21 11:15 104-51-802/18/21 09:428.6 1
sec-Butylbenzene 12.1 ug/kg 02/18/21 11:15 135-98-802/18/21 09:428.6 1
tert-Butylbenzene ND ug/kg 02/18/21 11:15 98-06-602/18/21 09:428.6 1
Carbon tetrachloride ND ug/kg 02/18/21 11:15 56-23-502/18/21 09:428.6 1
Chlorobenzene ND ug/kg 02/18/21 11:15 108-90-702/18/21 09:428.6 1
Chloroethane ND ug/kg 02/18/21 11:15 75-00-302/18/21 09:4217.2 1
Chloroform ND ug/kg 02/18/21 11:15 67-66-302/18/21 09:428.6 1
Chloromethane ND ug/kg 02/18/21 11:15 74-87-302/18/21 09:4217.2 1
2-Chlorotoluene ND ug/kg 02/18/21 11:15 95-49-802/18/21 09:428.6 1
4-Chlorotoluene ND ug/kg 02/18/21 11:15 106-43-402/18/21 09:428.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/18/21 11:15 96-12-802/18/21 09:428.6 1
Dibromochloromethane ND ug/kg 02/18/21 11:15 124-48-102/18/21 09:428.6 1
1,2-Dibromoethane (EDB)ND ug/kg 02/18/21 11:15 106-93-402/18/21 09:428.6 1
Dibromomethane ND ug/kg 02/18/21 11:15 74-95-302/18/21 09:428.6 1
1,2-Dichlorobenzene ND ug/kg 02/18/21 11:15 95-50-102/18/21 09:428.6 1
1,3-Dichlorobenzene ND ug/kg 02/18/21 11:15 541-73-102/18/21 09:428.6 1
1,4-Dichlorobenzene ND ug/kg 02/18/21 11:15 106-46-702/18/21 09:428.6 1
Dichlorodifluoromethane ND ug/kg 02/18/21 11:15 75-71-802/18/21 09:4217.2 1
1,1-Dichloroethane ND ug/kg 02/18/21 11:15 75-34-302/18/21 09:428.6 1
1,2-Dichloroethane ND ug/kg 02/18/21 11:15 107-06-202/18/21 09:428.6 1
1,1-Dichloroethene ND ug/kg 02/18/21 11:15 75-35-402/18/21 09:428.6 1
cis-1,2-Dichloroethene ND ug/kg 02/18/21 11:15 156-59-202/18/21 09:428.6 1
trans-1,2-Dichloroethene ND ug/kg 02/18/21 11:15 156-60-502/18/21 09:428.6 1
1,2-Dichloropropane ND ug/kg 02/18/21 11:15 78-87-502/18/21 09:428.6 1
1,3-Dichloropropane ND ug/kg 02/18/21 11:15 142-28-902/18/21 09:428.6 1
2,2-Dichloropropane ND ug/kg 02/18/21 11:15 594-20-702/18/21 09:428.6 1
1,1-Dichloropropene ND ug/kg 02/18/21 11:15 563-58-602/18/21 09:428.6 1
cis-1,3-Dichloropropene ND ug/kg 02/18/21 11:15 10061-01-502/18/21 09:428.6 1
trans-1,3-Dichloropropene ND ug/kg 02/18/21 11:15 10061-02-602/18/21 09:428.6 1
Diisopropyl ether ND ug/kg 02/18/21 11:15 108-20-302/18/21 09:428.6 1
Ethylbenzene 11.8 ug/kg 02/18/21 11:15 100-41-402/18/21 09:428.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 11 Lab ID: 92522127015 Collected: 02/11/21 10:27 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/18/21 11:15 87-68-302/18/21 09:4217.2 1
2-Hexanone ND ug/kg 02/18/21 11:15 591-78-602/18/21 09:4285.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/18/21 11:15 98-82-802/18/21 09:428.6 1
p-Isopropyltoluene ND ug/kg 02/18/21 11:15 99-87-602/18/21 09:428.6 1
Methylene Chloride ND ug/kg 02/18/21 11:15 75-09-202/18/21 09:4234.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/18/21 11:15 108-10-102/18/21 09:4285.9 1
Methyl-tert-butyl ether ND ug/kg 02/18/21 11:15 1634-04-402/18/21 09:428.6 1
Naphthalene 35.0 ug/kg 02/18/21 11:15 91-20-302/18/21 09:428.6 1
n-Propylbenzene ND ug/kg 02/18/21 11:15 103-65-102/18/21 09:428.6 1
Styrene ND ug/kg 02/18/21 11:15 100-42-502/18/21 09:428.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/18/21 11:15 630-20-602/18/21 09:428.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/18/21 11:15 79-34-502/18/21 09:428.6 1
Tetrachloroethene ND ug/kg 02/18/21 11:15 127-18-402/18/21 09:428.6 1
Toluene 10.2 ug/kg 02/18/21 11:15 108-88-302/18/21 09:428.6 1
1,2,3-Trichlorobenzene ND ug/kg 02/18/21 11:15 87-61-602/18/21 09:428.6 1
1,2,4-Trichlorobenzene ND ug/kg 02/18/21 11:15 120-82-102/18/21 09:428.6 1
1,1,1-Trichloroethane ND ug/kg 02/18/21 11:15 71-55-602/18/21 09:428.6 1
1,1,2-Trichloroethane ND ug/kg 02/18/21 11:15 79-00-502/18/21 09:428.6 1
Trichloroethene ND ug/kg 02/18/21 11:15 79-01-602/18/21 09:428.6 1
Trichlorofluoromethane ND ug/kg 02/18/21 11:15 75-69-402/18/21 09:428.6 1
1,2,3-Trichloropropane ND ug/kg 02/18/21 11:15 96-18-402/18/21 09:428.6 1
1,2,4-Trimethylbenzene 32.1 ug/kg 02/18/21 11:15 95-63-602/18/21 09:428.6 1
1,3,5-Trimethylbenzene ND ug/kg 02/18/21 11:15 108-67-802/18/21 09:428.6 1
Vinyl acetate ND ug/kg 02/18/21 11:15 108-05-402/18/21 09:4285.9 1
Vinyl chloride ND ug/kg 02/18/21 11:15 75-01-402/18/21 09:4217.2 1
Xylene (Total)22.8 ug/kg 02/18/21 11:15 1330-20-702/18/21 09:4217.2 1
m&p-Xylene 22.8 ug/kg 02/18/21 11:15 179601-23-102/18/21 09:4217.2 1
o-Xylene ND ug/kg 02/18/21 11:15 95-47-602/18/21 09:428.6 1
Surrogates
Toluene-d8 (S)100 %02/18/21 11:15 2037-26-502/18/21 09:4270-130 1
4-Bromofluorobenzene (S)103 %02/18/21 11:15 460-00-402/18/21 09:4269-134 1
1,2-Dichloroethane-d4 (S)100 %02/18/21 11:15 17060-07-002/18/21 09:4270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.8 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 12 Lab ID: 92522127016 Collected: 02/11/21 10:36 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 23:2802/15/21 11:369.3 1
Surrogates
4-Bromofluorobenzene (S)79 %02/15/21 23:28 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 18:37 67-64-102/17/21 11:23141 1
Benzene ND ug/kg 02/17/21 18:37 71-43-202/17/21 11:237.0 1
Bromobenzene ND ug/kg 02/17/21 18:37 108-86-102/17/21 11:237.0 1
Bromochloromethane ND ug/kg 02/17/21 18:37 74-97-502/17/21 11:237.0 1
Bromodichloromethane ND ug/kg 02/17/21 18:37 75-27-402/17/21 11:237.0 1
Bromoform ND ug/kg 02/17/21 18:37 75-25-202/17/21 11:237.0 1
Bromomethane ND ug/kg 02/17/21 18:37 74-83-902/17/21 11:2314.1 1
2-Butanone (MEK)ND ug/kg 02/17/21 18:37 78-93-302/17/21 11:23141 1
n-Butylbenzene ND ug/kg 02/17/21 18:37 104-51-802/17/21 11:237.0 1
sec-Butylbenzene ND ug/kg 02/17/21 18:37 135-98-802/17/21 11:237.0 1
tert-Butylbenzene ND ug/kg 02/17/21 18:37 98-06-602/17/21 11:237.0 1
Carbon tetrachloride ND ug/kg 02/17/21 18:37 56-23-502/17/21 11:237.0 1
Chlorobenzene ND ug/kg 02/17/21 18:37 108-90-702/17/21 11:237.0 1
Chloroethane ND ug/kg 02/17/21 18:37 75-00-302/17/21 11:2314.1 1
Chloroform ND ug/kg 02/17/21 18:37 67-66-302/17/21 11:237.0 1
Chloromethane ND ug/kg 02/17/21 18:37 74-87-302/17/21 11:2314.1 1
2-Chlorotoluene ND ug/kg 02/17/21 18:37 95-49-802/17/21 11:237.0 1
4-Chlorotoluene ND ug/kg 02/17/21 18:37 106-43-402/17/21 11:237.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 18:37 96-12-802/17/21 11:237.0 1
Dibromochloromethane ND ug/kg 02/17/21 18:37 124-48-102/17/21 11:237.0 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 18:37 106-93-402/17/21 11:237.0 1
Dibromomethane ND ug/kg 02/17/21 18:37 74-95-302/17/21 11:237.0 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 18:37 95-50-102/17/21 11:237.0 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 18:37 541-73-102/17/21 11:237.0 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 18:37 106-46-702/17/21 11:237.0 1
Dichlorodifluoromethane ND ug/kg 02/17/21 18:37 75-71-802/17/21 11:2314.1 1
1,1-Dichloroethane ND ug/kg 02/17/21 18:37 75-34-302/17/21 11:237.0 1
1,2-Dichloroethane ND ug/kg 02/17/21 18:37 107-06-202/17/21 11:237.0 1
1,1-Dichloroethene ND ug/kg 02/17/21 18:37 75-35-402/17/21 11:237.0 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 18:37 156-59-202/17/21 11:237.0 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 18:37 156-60-502/17/21 11:237.0 1
1,2-Dichloropropane ND ug/kg 02/17/21 18:37 78-87-502/17/21 11:237.0 1
1,3-Dichloropropane ND ug/kg 02/17/21 18:37 142-28-902/17/21 11:237.0 1
2,2-Dichloropropane ND ug/kg 02/17/21 18:37 594-20-702/17/21 11:237.0 1
1,1-Dichloropropene ND ug/kg 02/17/21 18:37 563-58-602/17/21 11:237.0 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 18:37 10061-01-502/17/21 11:237.0 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 18:37 10061-02-602/17/21 11:237.0 1
Diisopropyl ether ND ug/kg 02/17/21 18:37 108-20-302/17/21 11:237.0 1
Ethylbenzene 9.5 ug/kg 02/17/21 18:37 100-41-402/17/21 11:237.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Product Line 12 Lab ID: 92522127016 Collected: 02/11/21 10:36 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 18:37 87-68-302/17/21 11:2314.1 1
2-Hexanone ND ug/kg 02/17/21 18:37 591-78-602/17/21 11:2370.3 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 18:37 98-82-802/17/21 11:237.0 1
p-Isopropyltoluene ND ug/kg 02/17/21 18:37 99-87-602/17/21 11:237.0 1
Methylene Chloride ND ug/kg 02/17/21 18:37 75-09-202/17/21 11:2328.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 18:37 108-10-102/17/21 11:2370.3 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 18:37 1634-04-402/17/21 11:237.0 1
Naphthalene 13.2 ug/kg 02/17/21 18:37 91-20-302/17/21 11:237.0 1
n-Propylbenzene ND ug/kg 02/17/21 18:37 103-65-102/17/21 11:237.0 1
Styrene ND ug/kg 02/17/21 18:37 100-42-502/17/21 11:237.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 18:37 630-20-602/17/21 11:237.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 18:37 79-34-502/17/21 11:237.0 1
Tetrachloroethene ND ug/kg 02/17/21 18:37 127-18-402/17/21 11:237.0 1
Toluene 12.0 ug/kg 02/17/21 18:37 108-88-302/17/21 11:237.0 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 18:37 87-61-602/17/21 11:237.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 18:37 120-82-102/17/21 11:237.0 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 18:37 71-55-602/17/21 11:237.0 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 18:37 79-00-502/17/21 11:237.0 1
Trichloroethene ND ug/kg 02/17/21 18:37 79-01-602/17/21 11:237.0 1
Trichlorofluoromethane ND ug/kg 02/17/21 18:37 75-69-402/17/21 11:237.0 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 18:37 96-18-402/17/21 11:237.0 1
1,2,4-Trimethylbenzene 13.9 ug/kg 02/17/21 18:37 95-63-602/17/21 11:237.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 18:37 108-67-802/17/21 11:237.0 1
Vinyl acetate ND ug/kg 02/17/21 18:37 108-05-402/17/21 11:2370.3 1
Vinyl chloride ND ug/kg 02/17/21 18:37 75-01-402/17/21 11:2314.1 1
Xylene (Total)17.2 ug/kg 02/17/21 18:37 1330-20-702/17/21 11:2314.1 1
m&p-Xylene 17.2 ug/kg 02/17/21 18:37 179601-23-102/17/21 11:2314.1 1
o-Xylene ND ug/kg 02/17/21 18:37 95-47-602/17/21 11:237.0 1
Surrogates
Toluene-d8 (S)101 %02/17/21 18:37 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)100 %02/17/21 18:37 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)103 %02/17/21 18:37 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.8 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 13 Lab ID: 92522127017 Collected: 02/11/21 10:45 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/15/21 23:5602/15/21 11:368.4 1
Surrogates
4-Bromofluorobenzene (S)79 %02/15/21 23:56 460-00-402/15/21 11:3666-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 02/17/21 18:55 67-64-102/17/21 11:23131 1
Benzene ND ug/kg 02/17/21 18:55 71-43-202/17/21 11:236.6 1
Bromobenzene ND ug/kg 02/17/21 18:55 108-86-102/17/21 11:236.6 1
Bromochloromethane ND ug/kg 02/17/21 18:55 74-97-502/17/21 11:236.6 1
Bromodichloromethane ND ug/kg 02/17/21 18:55 75-27-402/17/21 11:236.6 1
Bromoform ND ug/kg 02/17/21 18:55 75-25-202/17/21 11:236.6 1
Bromomethane ND ug/kg 02/17/21 18:55 74-83-902/17/21 11:2313.1 1
2-Butanone (MEK)ND ug/kg 02/17/21 18:55 78-93-302/17/21 11:23131 1
n-Butylbenzene ND ug/kg 02/17/21 18:55 104-51-802/17/21 11:236.6 1
sec-Butylbenzene ND ug/kg 02/17/21 18:55 135-98-802/17/21 11:236.6 1
tert-Butylbenzene ND ug/kg 02/17/21 18:55 98-06-602/17/21 11:236.6 1
Carbon tetrachloride ND ug/kg 02/17/21 18:55 56-23-502/17/21 11:236.6 1
Chlorobenzene ND ug/kg 02/17/21 18:55 108-90-702/17/21 11:236.6 1
Chloroethane ND ug/kg 02/17/21 18:55 75-00-302/17/21 11:2313.1 1
Chloroform ND ug/kg 02/17/21 18:55 67-66-302/17/21 11:236.6 1
Chloromethane ND ug/kg 02/17/21 18:55 74-87-302/17/21 11:2313.1 1
2-Chlorotoluene ND ug/kg 02/17/21 18:55 95-49-802/17/21 11:236.6 1
4-Chlorotoluene ND ug/kg 02/17/21 18:55 106-43-402/17/21 11:236.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/17/21 18:55 96-12-802/17/21 11:236.6 1
Dibromochloromethane ND ug/kg 02/17/21 18:55 124-48-102/17/21 11:236.6 1
1,2-Dibromoethane (EDB)ND ug/kg 02/17/21 18:55 106-93-402/17/21 11:236.6 1
Dibromomethane ND ug/kg 02/17/21 18:55 74-95-302/17/21 11:236.6 1
1,2-Dichlorobenzene ND ug/kg 02/17/21 18:55 95-50-102/17/21 11:236.6 1
1,3-Dichlorobenzene ND ug/kg 02/17/21 18:55 541-73-102/17/21 11:236.6 1
1,4-Dichlorobenzene ND ug/kg 02/17/21 18:55 106-46-702/17/21 11:236.6 1
Dichlorodifluoromethane ND ug/kg 02/17/21 18:55 75-71-802/17/21 11:2313.1 1
1,1-Dichloroethane ND ug/kg 02/17/21 18:55 75-34-302/17/21 11:236.6 1
1,2-Dichloroethane ND ug/kg 02/17/21 18:55 107-06-202/17/21 11:236.6 1
1,1-Dichloroethene ND ug/kg 02/17/21 18:55 75-35-402/17/21 11:236.6 1
cis-1,2-Dichloroethene ND ug/kg 02/17/21 18:55 156-59-202/17/21 11:236.6 1
trans-1,2-Dichloroethene ND ug/kg 02/17/21 18:55 156-60-502/17/21 11:236.6 1
1,2-Dichloropropane ND ug/kg 02/17/21 18:55 78-87-502/17/21 11:236.6 1
1,3-Dichloropropane ND ug/kg 02/17/21 18:55 142-28-902/17/21 11:236.6 1
2,2-Dichloropropane ND ug/kg 02/17/21 18:55 594-20-702/17/21 11:236.6 1
1,1-Dichloropropene ND ug/kg 02/17/21 18:55 563-58-602/17/21 11:236.6 1
cis-1,3-Dichloropropene ND ug/kg 02/17/21 18:55 10061-01-502/17/21 11:236.6 1
trans-1,3-Dichloropropene ND ug/kg 02/17/21 18:55 10061-02-602/17/21 11:236.6 1
Diisopropyl ether ND ug/kg 02/17/21 18:55 108-20-302/17/21 11:236.6 1
Ethylbenzene ND ug/kg 02/17/21 18:55 100-41-402/17/21 11:236.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Dispenser 13 Lab ID: 92522127017 Collected: 02/11/21 10:45 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Hexachloro-1,3-butadiene ND ug/kg 02/17/21 18:55 87-68-302/17/21 11:2313.1 1
2-Hexanone ND ug/kg 02/17/21 18:55 591-78-602/17/21 11:2365.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/17/21 18:55 98-82-802/17/21 11:236.6 1
p-Isopropyltoluene ND ug/kg 02/17/21 18:55 99-87-602/17/21 11:236.6 1
Methylene Chloride ND ug/kg 02/17/21 18:55 75-09-202/17/21 11:2326.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/17/21 18:55 108-10-102/17/21 11:2365.6 1
Methyl-tert-butyl ether ND ug/kg 02/17/21 18:55 1634-04-402/17/21 11:236.6 1
Naphthalene ND ug/kg 02/17/21 18:55 91-20-302/17/21 11:236.6 1
n-Propylbenzene ND ug/kg 02/17/21 18:55 103-65-102/17/21 11:236.6 1
Styrene ND ug/kg 02/17/21 18:55 100-42-502/17/21 11:236.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/17/21 18:55 630-20-602/17/21 11:236.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/17/21 18:55 79-34-502/17/21 11:236.6 1
Tetrachloroethene ND ug/kg 02/17/21 18:55 127-18-402/17/21 11:236.6 1
Toluene ND ug/kg 02/17/21 18:55 108-88-302/17/21 11:236.6 1
1,2,3-Trichlorobenzene ND ug/kg 02/17/21 18:55 87-61-602/17/21 11:236.6 1
1,2,4-Trichlorobenzene ND ug/kg 02/17/21 18:55 120-82-102/17/21 11:236.6 1
1,1,1-Trichloroethane ND ug/kg 02/17/21 18:55 71-55-602/17/21 11:236.6 1
1,1,2-Trichloroethane ND ug/kg 02/17/21 18:55 79-00-502/17/21 11:236.6 1
Trichloroethene ND ug/kg 02/17/21 18:55 79-01-602/17/21 11:236.6 1
Trichlorofluoromethane ND ug/kg 02/17/21 18:55 75-69-402/17/21 11:236.6 1
1,2,3-Trichloropropane ND ug/kg 02/17/21 18:55 96-18-402/17/21 11:236.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/17/21 18:55 95-63-602/17/21 11:236.6 1
1,3,5-Trimethylbenzene ND ug/kg 02/17/21 18:55 108-67-802/17/21 11:236.6 1
Vinyl acetate ND ug/kg 02/17/21 18:55 108-05-402/17/21 11:2365.6 1
Vinyl chloride ND ug/kg 02/17/21 18:55 75-01-402/17/21 11:2313.1 1
Xylene (Total)ND ug/kg 02/17/21 18:55 1330-20-702/17/21 11:2313.1 1
m&p-Xylene ND ug/kg 02/17/21 18:55 179601-23-102/17/21 11:2313.1 1
o-Xylene ND ug/kg 02/17/21 18:55 95-47-602/17/21 11:236.6 1
Surrogates
Toluene-d8 (S)99 %02/17/21 18:55 2037-26-502/17/21 11:2370-130 1
4-Bromofluorobenzene (S)102 %02/17/21 18:55 460-00-402/17/21 11:2369-134 1
1,2-Dichloroethane-d4 (S)102 %02/17/21 18:55 17060-07-002/17/21 11:2370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.8 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Kerosene Dispenser 17 Lab ID: 92522127018 Collected: 02/11/21 13:11 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)484 mg/kg 02/17/21 23:0202/16/21 10:2614.4 2.5
Surrogates
n-Pentacosane (S)86 %02/17/21 23:02 629-99-202/16/21 10:2632-130 2.5
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/16/21 00:2402/15/21 11:367.1 1
Surrogates
4-Bromofluorobenzene (S)80 %02/16/21 00:24 460-00-402/15/21 11:3666-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.2 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Sample: Kerosene Line 19 Lab ID: 92522127019 Collected: 02/11/21 13:50 Received: 02/12/21 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 02/17/21 16:4402/16/21 10:267.1 1
Surrogates
n-Pentacosane (S)77 %02/17/21 16:44 629-99-202/16/21 10:2632-130 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 02/17/21 02:0802/16/21 11:2911.5 1
Surrogates
4-Bromofluorobenzene (S)78 %02/17/21 02:08 460-00-402/16/21 11:2966-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.6 %02/15/21 13:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
599997
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127015, 92522127016, 92522127017, 92522127018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3163032
Associated Lab Samples: 92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127015, 92522127016, 92522127017, 92522127018
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 02/15/21 12:40
4-Bromofluorobenzene (S)%78 66-131 02/15/21 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3163033LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.049.7 99 70-130
4-Bromofluorobenzene (S)%82 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3163035MATRIX SPIKE SAMPLE:
MSSpike
Result
92522097002
Gas Range Organics (C6-C10)mg/kg 97.972.3 103 70-14523.5
4-Bromofluorobenzene (S)%118 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92522097001
3163034SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%7579
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600277
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92522127019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3164328
Associated Lab Samples:92522127019
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 02/16/21 15:48
4-Bromofluorobenzene (S)%83 66-131 02/16/21 15:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3164329LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.749.7 100 70-130
4-Bromofluorobenzene (S)%82 66-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3164331MATRIX SPIKE SAMPLE:
MSSpike
Result
92522127019
Gas Range Organics (C6-C10)mg/kg 94.396.1 96 70-145ND
4-Bromofluorobenzene (S)%80 66-131
Parameter Units
Dup
Result QualifiersRPDResult
92522243001
3164330SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg 3.1JND
4-Bromofluorobenzene (S)%7983
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600647
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127016, 92522127017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3165682
Associated Lab Samples: 92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127016, 92522127017
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 02/17/21 12:17
1,1,1-Trichloroethane ug/kg ND 5.0 02/17/21 12:17
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 02/17/21 12:17
1,1,2-Trichloroethane ug/kg ND 5.0 02/17/21 12:17
1,1-Dichloroethane ug/kg ND 5.0 02/17/21 12:17
1,1-Dichloroethene ug/kg ND 5.0 02/17/21 12:17
1,1-Dichloropropene ug/kg ND 5.0 02/17/21 12:17
1,2,3-Trichlorobenzene ug/kg ND 5.0 02/17/21 12:17
1,2,3-Trichloropropane ug/kg ND 5.0 02/17/21 12:17
1,2,4-Trichlorobenzene ug/kg ND 5.0 02/17/21 12:17
1,2,4-Trimethylbenzene ug/kg ND 5.0 02/17/21 12:17
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 02/17/21 12:17
1,2-Dibromoethane (EDB)ug/kg ND 5.0 02/17/21 12:17
1,2-Dichlorobenzene ug/kg ND 5.0 02/17/21 12:17
1,2-Dichloroethane ug/kg ND 5.0 02/17/21 12:17
1,2-Dichloropropane ug/kg ND 5.0 02/17/21 12:17
1,3,5-Trimethylbenzene ug/kg ND 5.0 02/17/21 12:17
1,3-Dichlorobenzene ug/kg ND 5.0 02/17/21 12:17
1,3-Dichloropropane ug/kg ND 5.0 02/17/21 12:17
1,4-Dichlorobenzene ug/kg ND 5.0 02/17/21 12:17
2,2-Dichloropropane ug/kg ND 5.0 02/17/21 12:17
2-Butanone (MEK)ug/kg ND 100 02/17/21 12:17
2-Chlorotoluene ug/kg ND 5.0 02/17/21 12:17
2-Hexanone ug/kg ND 50.0 02/17/21 12:17
4-Chlorotoluene ug/kg ND 5.0 02/17/21 12:17
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 02/17/21 12:17
Acetone ug/kg ND 100 02/17/21 12:17
Benzene ug/kg ND 5.0 02/17/21 12:17
Bromobenzene ug/kg ND 5.0 02/17/21 12:17
Bromochloromethane ug/kg ND 5.0 02/17/21 12:17
Bromodichloromethane ug/kg ND 5.0 02/17/21 12:17
Bromoform ug/kg ND 5.0 02/17/21 12:17
Bromomethane ug/kg ND 10.0 02/17/21 12:17
Carbon tetrachloride ug/kg ND 5.0 02/17/21 12:17
Chlorobenzene ug/kg ND 5.0 02/17/21 12:17
Chloroethane ug/kg ND 10.0 02/17/21 12:17
Chloroform ug/kg ND 5.0 02/17/21 12:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3165682
Associated Lab Samples: 92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127016, 92522127017
Matrix: Solid
Analyzed
Chloromethane ug/kg ND 10.0 02/17/21 12:17
cis-1,2-Dichloroethene ug/kg ND 5.0 02/17/21 12:17
cis-1,3-Dichloropropene ug/kg ND 5.0 02/17/21 12:17
Dibromochloromethane ug/kg ND 5.0 02/17/21 12:17
Dibromomethane ug/kg ND 5.0 02/17/21 12:17
Dichlorodifluoromethane ug/kg ND 10.0 02/17/21 12:17
Diisopropyl ether ug/kg ND 5.0 02/17/21 12:17
Ethylbenzene ug/kg ND 5.0 02/17/21 12:17
Hexachloro-1,3-butadiene ug/kg ND 10.0 02/17/21 12:17
Isopropylbenzene (Cumene)ug/kg ND 5.0 02/17/21 12:17
m&p-Xylene ug/kg ND 10.0 02/17/21 12:17
Methyl-tert-butyl ether ug/kg ND 5.0 02/17/21 12:17
Methylene Chloride ug/kg ND 20.0 02/17/21 12:17
n-Butylbenzene ug/kg ND 5.0 02/17/21 12:17
n-Propylbenzene ug/kg ND 5.0 02/17/21 12:17
Naphthalene ug/kg ND 5.0 02/17/21 12:17
o-Xylene ug/kg ND 5.0 02/17/21 12:17
p-Isopropyltoluene ug/kg ND 5.0 02/17/21 12:17
sec-Butylbenzene ug/kg ND 5.0 02/17/21 12:17
Styrene ug/kg ND 5.0 02/17/21 12:17
tert-Butylbenzene ug/kg ND 5.0 02/17/21 12:17
Tetrachloroethene ug/kg ND 5.0 02/17/21 12:17
Toluene ug/kg ND 5.0 02/17/21 12:17
trans-1,2-Dichloroethene ug/kg ND 5.0 02/17/21 12:17
trans-1,3-Dichloropropene ug/kg ND 5.0 02/17/21 12:17
Trichloroethene ug/kg ND 5.0 02/17/21 12:17
Trichlorofluoromethane ug/kg ND 5.0 02/17/21 12:17
Vinyl acetate ug/kg ND 50.0 02/17/21 12:17
Vinyl chloride ug/kg ND 10.0 02/17/21 12:17
Xylene (Total)ug/kg ND 10.0 02/17/21 12:17
1,2-Dichloroethane-d4 (S)%104 70-130 02/17/21 12:17
4-Bromofluorobenzene (S)%98 69-134 02/17/21 12:17
Toluene-d8 (S)%99 70-130 02/17/21 12:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3165683LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12901250 103 70-130
1,1,1-Trichloroethane ug/kg 13001250 104 70-130
1,1,2,2-Tetrachloroethane ug/kg 12001250 96 70-130
1,1,2-Trichloroethane ug/kg 12701250 101 70-130
1,1-Dichloroethane ug/kg 12601250 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3165683LABORATORY CONTROL SAMPLE:
LCSSpike
1,1-Dichloroethene ug/kg 13601250 109 70-130
1,1-Dichloropropene ug/kg 12801250 102 70-130
1,2,3-Trichlorobenzene ug/kg 11801250 94 65-130
1,2,3-Trichloropropane ug/kg 11701250 93 70-130
1,2,4-Trichlorobenzene ug/kg 12501250 100 68-130
1,2,4-Trimethylbenzene ug/kg 12501250 100 70-130
1,2-Dibromo-3-chloropropane ug/kg 11301250 90 70-130
1,2-Dibromoethane (EDB)ug/kg 12601250 100 70-130
1,2-Dichlorobenzene ug/kg 12101250 97 70-130
1,2-Dichloroethane ug/kg 11901250 95 63-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3,5-Trimethylbenzene ug/kg 12301250 99 70-130
1,3-Dichlorobenzene ug/kg 12101250 97 70-130
1,3-Dichloropropane ug/kg 12301250 98 70-130
1,4-Dichlorobenzene ug/kg 12201250 98 70-130
2,2-Dichloropropane ug/kg 12801250 102 66-130
2-Butanone (MEK)ug/kg 23402500 94 70-130
2-Chlorotoluene ug/kg 12801250 102 70-130
2-Hexanone ug/kg 23502500 94 70-130
4-Chlorotoluene ug/kg 12401250 100 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23502500 94 70-130
Acetone ug/kg 22802500 91 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 12501250 100 70-130
Bromochloromethane ug/kg 11401250 91 70-130
Bromodichloromethane ug/kg 12801250 102 69-130
Bromoform ug/kg 13301250 106 70-130
Bromomethane ug/kg 14101250 113 52-130
Carbon tetrachloride ug/kg 13201250 105 70-130
Chlorobenzene ug/kg 12301250 98 70-130
Chloroethane ug/kg 11901250 95 65-130
Chloroform ug/kg 12001250 96 70-130
Chloromethane ug/kg 11101250 88 55-130
cis-1,2-Dichloroethene ug/kg 12201250 98 70-130
cis-1,3-Dichloropropene ug/kg 12801250 103 70-130
Dibromochloromethane ug/kg 13101250 105 70-130
Dibromomethane ug/kg 11901250 95 70-130
Dichlorodifluoromethane ug/kg 12601250 101 45-156
Diisopropyl ether ug/kg 11701250 93 70-130
Ethylbenzene ug/kg 11801250 94 70-130
Hexachloro-1,3-butadiene ug/kg 11501250 92 66-130
Isopropylbenzene (Cumene)ug/kg 12501250 100 70-130
m&p-Xylene ug/kg 24402500 97 70-130
Methyl-tert-butyl ether ug/kg 12001250 96 70-130
Methylene Chloride ug/kg 10701250 85 65-130
n-Butylbenzene ug/kg 12501250 100 67-130
n-Propylbenzene ug/kg 12401250 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3165683LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 12501250 100 70-130
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 12401250 99 67-130
sec-Butylbenzene ug/kg 12201250 98 69-130
Styrene ug/kg 13301250 106 70-130
tert-Butylbenzene ug/kg 11901250 95 67-130
Tetrachloroethene ug/kg 12301250 98 70-130
Toluene ug/kg 12301250 98 70-130
trans-1,2-Dichloroethene ug/kg 12401250 100 70-130
trans-1,3-Dichloropropene ug/kg 12901250 103 68-130
Trichloroethene ug/kg 13001250 104 70-130
Trichlorofluoromethane ug/kg 12401250 99 70-130
Vinyl acetate ug/kg 25802500 103 70-130
Vinyl chloride ug/kg 11501250 92 61-130
Xylene (Total)ug/kg 36803750 98 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3165685MATRIX SPIKE SAMPLE:
MSSpike
Result
92522127002
1,1,1,2-Tetrachloroethane ug/kg 1050936 113 70-131ND
1,1,1-Trichloroethane ug/kg 1070936 114 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 1000936 107 66-130ND
1,1,2-Trichloroethane ug/kg 1030936 110 66-133ND
1,1-Dichloroethane ug/kg 983936 105 65-130ND
1,1-Dichloroethene ug/kg 1110936 119 10-158ND
1,1-Dichloropropene ug/kg 1080936 115 68-133ND
1,2,3-Trichlorobenzene ug/kg 1040936 111 27-138ND
1,2,3-Trichloropropane ug/kg 946936 101 67-130ND
1,2,4-Trichlorobenzene ug/kg 1040936 111 51-134ND
1,2,4-Trimethylbenzene ug/kg 1060936 114 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 859936 92 32-130ND
1,2-Dibromoethane (EDB)ug/kg 1000936 107 70-130ND
1,2-Dichlorobenzene ug/kg 1010936 108 69-130ND
1,2-Dichloroethane ug/kg 966936 103 59-130ND
1,2-Dichloropropane ug/kg 1030936 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 1030936 110 65-137ND
1,3-Dichlorobenzene ug/kg 1010936 108 70-130ND
1,3-Dichloropropane ug/kg 1030936 110 70-130ND
1,4-Dichlorobenzene ug/kg 1020936 109 68-130ND
2,2-Dichloropropane ug/kg 964936 103 32-130ND
2-Butanone (MEK)ug/kg 17601880 94 10-136ND
2-Chlorotoluene ug/kg 1030936 110 69-141ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3165685MATRIX SPIKE SAMPLE:
MSSpike
Result
92522127002
2-Hexanone ug/kg 18601880 100 10-144ND
4-Chlorotoluene ug/kg 1010936 108 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 18801880 100 25-143ND
Acetone ug/kg 15901880 85 10-130ND
Benzene ug/kg 1000936 107 67-130ND
Bromobenzene ug/kg 1010936 108 70-130ND
Bromochloromethane ug/kg 869936 93 69-134ND
Bromodichloromethane ug/kg 1000936 107 64-130ND
Bromoform ug/kg 974936 104 62-130ND
Bromomethane ug/kg 873936 93 20-176ND
Carbon tetrachloride ug/kg 1070936 115 65-140ND
Chlorobenzene ug/kg 1040936 111 70-130ND
Chloroethane ug/kg 281936 30 10-130ND
Chloroform ug/kg 962936 103 63-130ND
Chloromethane ug/kg 1010936 108 58-130ND
cis-1,2-Dichloroethene ug/kg 990936 106 66-130ND
cis-1,3-Dichloropropene ug/kg 1010936 108 67-130ND
Dibromochloromethane ug/kg 1000936 107 67-130ND
Dibromomethane ug/kg 932936 100 63-131ND
Dichlorodifluoromethane ug/kg 1110936 119 44-180ND
Diisopropyl ether ug/kg 917936 98 63-130ND
Ethylbenzene ug/kg 1010936 108 66-130ND
Hexachloro-1,3-butadiene ug/kg 1030936 110 64-150ND
Isopropylbenzene (Cumene)ug/kg 1080936 116 69-135ND
m&p-Xylene ug/kg 20801880 111 60-133ND
Methyl-tert-butyl ether ug/kg 934936 100 65-130ND
Methylene Chloride ug/kg 868936 93 61-130ND
n-Butylbenzene ug/kg 1090936 116 65-140ND
n-Propylbenzene ug/kg 1030936 110 67-140ND
Naphthalene ug/kg 1030936 110 15-145ND
o-Xylene ug/kg 1040936 111 66-133ND
p-Isopropyltoluene ug/kg 1060936 113 56-147ND
sec-Butylbenzene ug/kg 1070936 114 65-139ND
Styrene ug/kg 1070936 114 70-132ND
tert-Butylbenzene ug/kg 990936 106 62-135ND
Tetrachloroethene ug/kg 1070936 115 70-135ND
Toluene ug/kg 1030936 111 67-130ND
trans-1,2-Dichloroethene ug/kg 1010936 108 69-130ND
trans-1,3-Dichloropropene ug/kg 1020936 109 62-130ND
Trichloroethene ug/kg 1110936 119 70-135ND
Trichlorofluoromethane ug/kg 396936 42 10-130ND
Vinyl acetate ug/kg 19601880 105 53-130ND
Vinyl chloride ug/kg 1080936 115 61-148ND
Xylene (Total)ug/kg 31102810 111 63-132ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92522127001
3165684SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 23.3 1226.2
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 13.6JND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92522127001
3165684SAMPLE DUPLICATE:
m&p-Xylene ug/kg 28.7 730.7
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 22.4 623.7
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg 28.7 730.7
1,2-Dichloroethane-d4 (S)%101103
4-Bromofluorobenzene (S)%99101
Toluene-d8 (S)%99101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600892
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92522127015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3166966
Associated Lab Samples:92522127015
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 02/18/21 10:39
1,1,1-Trichloroethane ug/kg ND 5.0 02/18/21 10:39
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 02/18/21 10:39
1,1,2-Trichloroethane ug/kg ND 5.0 02/18/21 10:39
1,1-Dichloroethane ug/kg ND 5.0 02/18/21 10:39
1,1-Dichloroethene ug/kg ND 5.0 02/18/21 10:39
1,1-Dichloropropene ug/kg ND 5.0 02/18/21 10:39
1,2,3-Trichlorobenzene ug/kg ND 5.0 02/18/21 10:39
1,2,3-Trichloropropane ug/kg ND 5.0 02/18/21 10:39
1,2,4-Trichlorobenzene ug/kg ND 5.0 02/18/21 10:39
1,2,4-Trimethylbenzene ug/kg ND 5.0 02/18/21 10:39
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 02/18/21 10:39
1,2-Dibromoethane (EDB)ug/kg ND 5.0 02/18/21 10:39
1,2-Dichlorobenzene ug/kg ND 5.0 02/18/21 10:39
1,2-Dichloroethane ug/kg ND 5.0 02/18/21 10:39
1,2-Dichloropropane ug/kg ND 5.0 02/18/21 10:39
1,3,5-Trimethylbenzene ug/kg ND 5.0 02/18/21 10:39
1,3-Dichlorobenzene ug/kg ND 5.0 02/18/21 10:39
1,3-Dichloropropane ug/kg ND 5.0 02/18/21 10:39
1,4-Dichlorobenzene ug/kg ND 5.0 02/18/21 10:39
2,2-Dichloropropane ug/kg ND 5.0 02/18/21 10:39
2-Butanone (MEK)ug/kg ND 100 02/18/21 10:39
2-Chlorotoluene ug/kg ND 5.0 02/18/21 10:39
2-Hexanone ug/kg ND 50.0 02/18/21 10:39
4-Chlorotoluene ug/kg ND 5.0 02/18/21 10:39
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 02/18/21 10:39
Acetone ug/kg ND 100 02/18/21 10:39
Benzene ug/kg ND 5.0 02/18/21 10:39
Bromobenzene ug/kg ND 5.0 02/18/21 10:39
Bromochloromethane ug/kg ND 5.0 02/18/21 10:39
Bromodichloromethane ug/kg ND 5.0 02/18/21 10:39
Bromoform ug/kg ND 5.0 02/18/21 10:39
Bromomethane ug/kg ND 10.0 02/18/21 10:39
Carbon tetrachloride ug/kg ND 5.0 02/18/21 10:39
Chlorobenzene ug/kg ND 5.0 02/18/21 10:39
Chloroethane ug/kg ND 10.0 02/18/21 10:39
Chloroform ug/kg ND 5.0 02/18/21 10:39
Chloromethane ug/kg ND 10.0 02/18/21 10:39
cis-1,2-Dichloroethene ug/kg ND 5.0 02/18/21 10:39
cis-1,3-Dichloropropene ug/kg ND 5.0 02/18/21 10:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3166966
Associated Lab Samples:92522127015
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 02/18/21 10:39
Dibromomethane ug/kg ND 5.0 02/18/21 10:39
Dichlorodifluoromethane ug/kg ND 10.0 02/18/21 10:39
Diisopropyl ether ug/kg ND 5.0 02/18/21 10:39
Ethylbenzene ug/kg ND 5.0 02/18/21 10:39
Hexachloro-1,3-butadiene ug/kg ND 10.0 02/18/21 10:39
Isopropylbenzene (Cumene)ug/kg ND 5.0 02/18/21 10:39
m&p-Xylene ug/kg ND 10.0 02/18/21 10:39
Methyl-tert-butyl ether ug/kg ND 5.0 02/18/21 10:39
Methylene Chloride ug/kg ND 20.0 02/18/21 10:39
n-Butylbenzene ug/kg ND 5.0 02/18/21 10:39
n-Propylbenzene ug/kg ND 5.0 02/18/21 10:39
Naphthalene ug/kg ND 5.0 02/18/21 10:39
o-Xylene ug/kg ND 5.0 02/18/21 10:39
p-Isopropyltoluene ug/kg ND 5.0 02/18/21 10:39
sec-Butylbenzene ug/kg ND 5.0 02/18/21 10:39
Styrene ug/kg ND 5.0 02/18/21 10:39
tert-Butylbenzene ug/kg ND 5.0 02/18/21 10:39
Tetrachloroethene ug/kg ND 5.0 02/18/21 10:39
Toluene ug/kg ND 5.0 02/18/21 10:39
trans-1,2-Dichloroethene ug/kg ND 5.0 02/18/21 10:39
trans-1,3-Dichloropropene ug/kg ND 5.0 02/18/21 10:39
Trichloroethene ug/kg ND 5.0 02/18/21 10:39
Trichlorofluoromethane ug/kg ND 5.0 02/18/21 10:39
Vinyl acetate ug/kg ND 50.0 02/18/21 10:39
Vinyl chloride ug/kg ND 10.0 02/18/21 10:39
Xylene (Total)ug/kg ND 10.0 02/18/21 10:39
1,2-Dichloroethane-d4 (S)%103 70-130 02/18/21 10:39
4-Bromofluorobenzene (S)%91 69-134 02/18/21 10:39
Toluene-d8 (S)%101 70-130 02/18/21 10:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3166967LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12901250 103 70-130
1,1,1-Trichloroethane ug/kg 13101250 105 70-130
1,1,2,2-Tetrachloroethane ug/kg 12301250 98 70-130
1,1,2-Trichloroethane ug/kg 12701250 102 70-130
1,1-Dichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethene ug/kg 13801250 111 70-130
1,1-Dichloropropene ug/kg 13201250 106 70-130
1,2,3-Trichlorobenzene ug/kg 12201250 97 65-130
1,2,3-Trichloropropane ug/kg 12101250 97 70-130
1,2,4-Trichlorobenzene ug/kg 12601250 101 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3166967LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12901250 103 70-130
1,2-Dibromo-3-chloropropane ug/kg 11901250 95 70-130
1,2-Dibromoethane (EDB)ug/kg 12701250 102 70-130
1,2-Dichlorobenzene ug/kg 12301250 98 70-130
1,2-Dichloroethane ug/kg 12101250 97 63-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3,5-Trimethylbenzene ug/kg 13001250 104 70-130
1,3-Dichlorobenzene ug/kg 12101250 97 70-130
1,3-Dichloropropane ug/kg 12501250 100 70-130
1,4-Dichlorobenzene ug/kg 12901250 103 70-130
2,2-Dichloropropane ug/kg 13001250 104 66-130
2-Butanone (MEK)ug/kg 24302500 97 70-130
2-Chlorotoluene ug/kg 13501250 108 70-130
2-Hexanone ug/kg 24802500 99 70-130
4-Chlorotoluene ug/kg 13201250 105 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24502500 98 70-130
Acetone ug/kg 25202500 101 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 13401250 107 70-130
Bromochloromethane ug/kg 11301250 91 70-130
Bromodichloromethane ug/kg 12801250 102 69-130
Bromoform ug/kg 13401250 107 70-130
Bromomethane ug/kg 13601250 109 52-130
Carbon tetrachloride ug/kg 13601250 109 70-130
Chlorobenzene ug/kg 12401250 99 70-130
Chloroethane ug/kg 12401250 99 65-130
Chloroform ug/kg 12101250 97 70-130
Chloromethane ug/kg 11401250 91 55-130
cis-1,2-Dichloroethene ug/kg 12401250 99 70-130
cis-1,3-Dichloropropene ug/kg 12801250 102 70-130
Dibromochloromethane ug/kg 13401250 107 70-130
Dibromomethane ug/kg 11901250 96 70-130
Dichlorodifluoromethane ug/kg 13801250 110 45-156
Diisopropyl ether ug/kg 11801250 95 70-130
Ethylbenzene ug/kg 11801250 94 70-130
Hexachloro-1,3-butadiene ug/kg 11501250 92 66-130
Isopropylbenzene (Cumene)ug/kg 12601250 100 70-130
m&p-Xylene ug/kg 24602500 98 70-130
Methyl-tert-butyl ether ug/kg 12101250 97 70-130
Methylene Chloride ug/kg 10901250 87 65-130
n-Butylbenzene ug/kg 12801250 103 67-130
n-Propylbenzene ug/kg 13001250 104 70-130
Naphthalene ug/kg 12501250 100 70-130
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 12501250 100 67-130
sec-Butylbenzene ug/kg 11901250 95 69-130
Styrene ug/kg 13301250 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3166967LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11601250 93 67-130
Tetrachloroethene ug/kg 12201250 98 70-130
Toluene ug/kg 12201250 98 70-130
trans-1,2-Dichloroethene ug/kg 12501250 100 70-130
trans-1,3-Dichloropropene ug/kg 12901250 103 68-130
Trichloroethene ug/kg 13301250 106 70-130
Trichlorofluoromethane ug/kg 13201250 105 70-130
Vinyl acetate ug/kg 27002500 108 70-130
Vinyl chloride ug/kg 12001250 96 61-130
Xylene (Total)ug/kg 36903750 98 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3166969MATRIX SPIKE SAMPLE:
MSSpike
Result
92522743002
1,1,1,2-Tetrachloroethane ug/kg 27502450 113 70-131ND
1,1,1-Trichloroethane ug/kg 28902450 118 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 25102450 103 66-130ND
1,1,2-Trichloroethane ug/kg 27002450 111 66-133ND
1,1-Dichloroethane ug/kg 26602450 109 65-130ND
1,1-Dichloroethene ug/kg 29602450 121 10-158ND
1,1-Dichloropropene ug/kg 29102450 119 68-133ND
1,2,3-Trichlorobenzene ug/kg 27102450 111 27-138ND
1,2,3-Trichloropropane ug/kg 23502450 96 67-130ND
1,2,4-Trichlorobenzene ug/kg 27602450 113 51-134ND
1,2,4-Trimethylbenzene ug/kg 28302450 116 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 22602450 93 32-130ND
1,2-Dibromoethane (EDB)ug/kg 24902450 102 70-130ND
1,2-Dichlorobenzene ug/kg 26402450 108 69-130ND
1,2-Dichloroethane ug/kg 25702450 105 59-130ND
1,2-Dichloropropane ug/kg 26902450 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 26802450 110 65-137ND
1,3-Dichlorobenzene ug/kg 27102450 111 70-130ND
1,3-Dichloropropane ug/kg 25402450 104 70-130ND
1,4-Dichlorobenzene ug/kg 26502450 109 68-130ND
2,2-Dichloropropane ug/kg 25302450 104 32-130ND
2-Butanone (MEK)ug/kg 42404880 87 10-136ND
2-Chlorotoluene ug/kg 27402450 112 69-141ND
2-Hexanone ug/kg 44404880 91 10-144ND
4-Chlorotoluene ug/kg 26802450 110 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 48004880 98 25-143ND
Acetone ug/kg 40504880 83 10-130ND
Benzene ug/kg 26602450 109 67-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3166969MATRIX SPIKE SAMPLE:
MSSpike
Result
92522743002
Bromobenzene ug/kg 27002450 110 70-130ND
Bromochloromethane ug/kg 23302450 95 69-134ND
Bromodichloromethane ug/kg 26502450 108 64-130ND
Bromoform ug/kg 24702450 101 62-130ND
Bromomethane ug/kg 21502450 88 20-176ND
Carbon tetrachloride ug/kg 28702450 117 65-140ND
Chlorobenzene ug/kg 26302450 108 70-130ND
Chloroethane ug/kg 6492450 27 10-130ND
Chloroform ug/kg 25402450 104 63-130ND
Chloromethane ug/kg 26802450 110 58-130ND
cis-1,2-Dichloroethene ug/kg 26502450 109 66-130ND
cis-1,3-Dichloropropene ug/kg 26702450 109 67-130ND
Dibromochloromethane ug/kg 25802450 106 67-130ND
Dibromomethane ug/kg 24402450 100 63-131ND
Dichlorodifluoromethane ug/kg 30702450 126 44-180ND
Diisopropyl ether ug/kg 24302450 100 63-130ND
Ethylbenzene ug/kg 25802450 106 66-130ND
Hexachloro-1,3-butadiene ug/kg 27202450 112 64-150ND
Isopropylbenzene (Cumene)ug/kg 27502450 113 69-135ND
m&p-Xylene ug/kg 52904880 108 60-133ND
Methyl-tert-butyl ether ug/kg 25202450 103 65-130ND
Methylene Chloride ug/kg 23002450 94 61-130ND
n-Butylbenzene ug/kg 28902450 118 65-140ND
n-Propylbenzene ug/kg 27302450 112 67-140ND
Naphthalene ug/kg 27702450 114 15-145ND
o-Xylene ug/kg 26502450 109 66-133ND
p-Isopropyltoluene ug/kg 28602450 117 56-147ND
sec-Butylbenzene ug/kg 28202450 115 65-139ND
Styrene ug/kg 27102450 111 70-132ND
tert-Butylbenzene ug/kg 26102450 107 62-135ND
Tetrachloroethene ug/kg 26902450 110 70-135ND
Toluene ug/kg 27202450 111 67-130ND
trans-1,2-Dichloroethene ug/kg 27102450 111 69-130ND
trans-1,3-Dichloropropene ug/kg 26502450 109 62-130ND
Trichloroethene ug/kg 28902450 119 70-135ND
Trichlorofluoromethane ug/kg 9842450 40 10-130ND
Vinyl acetate ug/kg 51704880 106 53-130ND
Vinyl chloride ug/kg 28802450 118 61-148ND
Xylene (Total)ug/kg 79407320 108 63-132ND
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%97 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
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Huntersville, NC 28078
[phone]
Page 57 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92522743001
3166968SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 120 3124
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 28.2ND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 22.2 820.4
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92522743001
3166968SAMPLE DUPLICATE:
m&p-Xylene ug/kg 83.0 486.6
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg 33.5 1539.0
o-Xylene ug/kg 44.5 647.1
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 19.4 1221.9
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg 128 5134
1,2-Dichloroethane-d4 (S)%103101
4-Bromofluorobenzene (S)%104106
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600230
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92522127001, 92522127002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3164145
Associated Lab Samples:92522127001, 92522127002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 02/16/21 13:54
n-Pentacosane (S)%77 32-130 02/16/21 13:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3164146LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 56.566.7 85 47-130
n-Pentacosane (S)%80 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3164147MATRIX SPIKE SAMPLE:
MSSpike
Result
92521621001
Diesel Range Organics(C10-C28)mg/kg 66.670.4 68 10-13318.5
n-Pentacosane (S)%84 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92521622002
3164148SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%7574
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600231
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92522127003, 92522127004, 92522127005, 92522127006, 92522127007, 92522127008, 92522127009,
92522127010, 92522127011, 92522127012, 92522127018, 92522127019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3164150
Associated Lab Samples: 92522127003, 92522127004, 92522127005, 92522127006, 92522127007, 92522127008, 92522127009,
92522127010, 92522127011, 92522127012, 92522127018, 92522127019
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 02/17/21 13:56
n-Pentacosane (S)%81 32-130 02/17/21 13:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3164151LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 55.466.7 83 47-130
n-Pentacosane (S)%82 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3164152MATRIX SPIKE SAMPLE:
MSSpike
Result
92522127003
Diesel Range Organics(C10-C28)mg/kg 72.890.3 73 10-1337.1
n-Pentacosane (S)%84 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92522127004
3164153SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%7979
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
600027
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92522127001, 92522127002, 92522127003, 92522127004, 92522127005, 92522127006, 92522127007,
92522127008, 92522127009, 92522127010, 92522127011, 92522127012, 92522127013, 92522127014,
92522127015, 92522127016, 92522127017, 92522127018, 92522127019
Parameter Units
Dup
Result QualifiersRPDResult
92522127001
3163266SAMPLE DUPLICATE:
Percent Moisture %25.3 N2025.4
Parameter Units
Dup
Result QualifiersRPDResult
92522164001
3163267SAMPLE DUPLICATE:
Percent Moisture %18.4 N21120.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 70
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 70
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92522127001 600230 600391Dispenser 1 EPA 3546 EPA 8015C Modified
92522127002 600230 600391Product Line 2 EPA 3546 EPA 8015C Modified
92522127003 600231 600700Dispenser 3 EPA 3546 EPA 8015C Modified
92522127004 600231 600700Product Line 4 EPA 3546 EPA 8015C Modified
92522127005 600231 600700Dispenser 5 EPA 3546 EPA 8015C Modified
92522127006 600231 600700Product Line 6 EPA 3546 EPA 8015C Modified
92522127007 600231 600700Dispenser 7 EPA 3546 EPA 8015C Modified
92522127008 600231 600700Product Line 8 EPA 3546 EPA 8015C Modified
92522127009 600231 600700Remote Fill 14 EPA 3546 EPA 8015C Modified
92522127010 600231 600700Remote Fill 15 EPA 3546 EPA 8015C Modified
92522127011 600231 600700Remote Fill 16 EPA 3546 EPA 8015C Modified
92522127012 600231 600700Product Line 18 EPA 3546 EPA 8015C Modified
92522127018 600231 600700Kerosene Dispenser 17 EPA 3546 EPA 8015C Modified
92522127019 600231 600700Kerosene Line 19 EPA 3546 EPA 8015C Modified
92522127001 599997 600005Dispenser 1 EPA 5030B EPA 8015C Modified
92522127002 599997 600005Product Line 2 EPA 5030B EPA 8015C Modified
92522127003 599997 600005Dispenser 3 EPA 5030B EPA 8015C Modified
92522127004 599997 600005Product Line 4 EPA 5030B EPA 8015C Modified
92522127005 599997 600005Dispenser 5 EPA 5030B EPA 8015C Modified
92522127006 599997 600005Product Line 6 EPA 5030B EPA 8015C Modified
92522127007 599997 600005Dispenser 7 EPA 5030B EPA 8015C Modified
92522127008 599997 600005Product Line 8 EPA 5030B EPA 8015C Modified
92522127009 599997 600005Remote Fill 14 EPA 5030B EPA 8015C Modified
92522127010 599997 600005Remote Fill 15 EPA 5030B EPA 8015C Modified
92522127011 599997 600005Remote Fill 16 EPA 5030B EPA 8015C Modified
92522127012 599997 600005Product Line 18 EPA 5030B EPA 8015C Modified
92522127013 599997 600005Dispenser 9 EPA 5030B EPA 8015C Modified
92522127014 599997 600005Product Line 10 EPA 5030B EPA 8015C Modified
92522127015 599997 600005Dispenser 11 EPA 5030B EPA 8015C Modified
92522127016 599997 600005Product Line 12 EPA 5030B EPA 8015C Modified
92522127017 599997 600005Dispenser 13 EPA 5030B EPA 8015C Modified
92522127018 599997 600005Kerosene Dispenser 17 EPA 5030B EPA 8015C Modified
92522127019 600277 600298Kerosene Line 19 EPA 5030B EPA 8015C Modified
92522127001 600647 600664Dispenser 1 EPA 5035A/5030B EPA 8260D
92522127002 600647 600664Product Line 2 EPA 5035A/5030B EPA 8260D
92522127003 600647 600664Dispenser 3 EPA 5035A/5030B EPA 8260D
92522127004 600647 600664Product Line 4 EPA 5035A/5030B EPA 8260D
92522127005 600647 600664Dispenser 5 EPA 5035A/5030B EPA 8260D
92522127006 600647 600664Product Line 6 EPA 5035A/5030B EPA 8260D
92522127007 600647 600664Dispenser 7 EPA 5035A/5030B EPA 8260D
92522127008 600647 600664Product Line 8 EPA 5035A/5030B EPA 8260D
92522127009 600647 600664Remote Fill 14 EPA 5035A/5030B EPA 8260D
92522127010 600647 600664Remote Fill 15 EPA 5035A/5030B EPA 8260D
92522127011 600647 600664Remote Fill 16 EPA 5035A/5030B EPA 8260D
92522127012 600647 600664Product Line 18 EPA 5035A/5030B EPA 8260D
92522127013 600647 600664Dispenser 9 EPA 5035A/5030B EPA 8260D
92522127014 600647 600664Product Line 10 EPA 5035A/5030B EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 70
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92522127
Sheetz Greensboro #356
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92522127015 600892 600900Dispenser 11 EPA 5035A/5030B EPA 8260D
92522127016 600647 600664Product Line 12 EPA 5035A/5030B EPA 8260D
92522127017 600647 600664Dispenser 13 EPA 5035A/5030B EPA 8260D
92522127001 600027Dispenser 1 SW-846
92522127002 600027Product Line 2 SW-846
92522127003 600027Dispenser 3 SW-846
92522127004 600027Product Line 4 SW-846
92522127005 600027Dispenser 5 SW-846
92522127006 600027Product Line 6 SW-846
92522127007 600027Dispenser 7 SW-846
92522127008 600027Product Line 8 SW-846
92522127009 600027Remote Fill 14 SW-846
92522127010 600027Remote Fill 15 SW-846
92522127011 600027Remote Fill 16 SW-846
92522127012 600027Product Line 18 SW-846
92522127013 600027Dispenser 9 SW-846
92522127014 600027Product Line 10 SW-846
92522127015 600027Dispenser 11 SW-846
92522127016 600027Product Line 12 SW-846
92522127017 600027Dispenser 13 SW-846
92522127018 600027Kerosene Dispenser 17 SW-846
92522127019 600027Kerosene Line 19 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/22/2021 02:09 PM
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[phone]
Page 65 of 70
Page 66 of 70
Page 67 of 70
Page 68 of 70
Page 69 of 70
Page 70 of 70

APPENDIX G
24-HOUR RELEASE REPORTING FORM (UST-61)
____________________________________________________________________________

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY)
Incident # ________ Risk (H,I,L,U)_______
Received On ________ Received By ________ Reported by (circle one): Phone, Fax or Report
Region _______

Suspected Contamination? (Y/N) ________
Confirmed GW Contamination? (Y/N) ______
Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______
Free Product? (Y/N) _____ If Yes, State Greatest
Thickness ______________

Facility ID Number ______________
Date Leak Discovered ___________
Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) GPS
Topographic map
GIS Address matching
Other
Unknown
Describe location:

HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
Release Detection Equipment or Methods
During UST Closure/Removal
Property Transfer
Visual/Odor
Water in Tank
Water Supply Well Contamination
Groundwater Contamination
Surface Water Contamination
Other (specify) _______________

SOURCE OF CONTAMINATION
Source of Release
(Check primary source) Cause of Release
(Check primary cause) Type of Release
(Check one) Product Type Released
(Check primary product type released)

Tank
Piping
Dispenser
Submersible Turbine Pump
Delivery Problem
Spill Bucket
 Other
Unknown

Definitions presented on reverse

Spill
Overfill
Corrosion
Physical/Mechanical
Damage
Install Problem
Other
Unknown

Definitions presented on reverse

Petroleum
Non-Petroleum
Both

Location
(Check one)

Facility
Residence
Other

Gasoline/ Diesel/
Kerosene
Heating Oil
Other Petroleum
Products
Metals
Other Inorganics
Other Organics

Diesel/Veg. Oil
Blend
Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State

Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

Sheetz Store 356
4319 West Wendover Ave.
Greensboro
Guilford
27407
36.056703 °N 79.888618 °W
Soil samples were collected on January 29, 2021 following the removal of the 5 USTs. Soil
samples were collected underneath the product lines and dispenser islands on February 11,
2021. Release was detected underneath the center of Gasoline UST 3, under the Kerosene
dispenser, along the product line between the tank field and dispenser islands, underneath
dispenser 5, 9 and between dispenser 9 and 10 from laboratory analysis. Soil staining, order, or
free product was not present during the USTs removal.
Lab results

IMPACT ON DRINKING WATER SUPPLIES

Water Supply Wells Affected? 1. Yes 2. No 3. Unknown

Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)

1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2

Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined

Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

Sheetz, Inc.
Sheetz, Inc.
4319 West Wendover Ave.
Greensboro NC 27407
Sheetz, Inc.
John Sieger 351 Sheetz Way
(814) 239-971416625ClaysburgPA
351 Sheetz Way
Claysburg PA 16625 [phone]
[phone]
Matt Cutshall Sheetz, Inc.814-239-1308
Environmental Compliance Manager 5700 6th Avenue, Altoona, PA 16602 02/23/2021

APPENDIX H
GROUNDWATER LABORATORY REPORT
and CHAIN-OF-CUSTUDY
____________________________________________________________________________

#=CL#
January 13, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92515110
92515110
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz Greensboro (Wendover)
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on January 06, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92515110001 SW EPA 8015C Modified 2 PASI-CJMS1
EPA 5030B/8015C Mod.2 PASI-CMAD
92515110002 NE EPA 8015C Modified 2 PASI-CJMS1
EPA 5030B/8015C Mod.2 PASI-CMAD
92515110003 NW EPA 8015C Modified 2 PASI-CJMS1
EPA 5030B/8015C Mod.2 PASI-CMAD
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Sample: SW Lab ID: 92515110001 Collected: 01/05/21 10:47 Received: 01/06/21 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 01/07/21 11:1001/07/21 09:540.50 1
Surrogates
n-Pentacosane (S)112 %01/07/21 11:10 629-99-201/07/21 09:5461-134 1
Analytical Method: EPA 5030B/8015C Mod.
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 01/11/21 17:020.080 1
Surrogates
4-Bromofluorobenzene (S)90 %01/11/21 17:02 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Sample: NE Lab ID: 92515110002 Collected: 01/05/21 09:42 Received: 01/06/21 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 01/07/21 11:3101/07/21 09:540.50 1
Surrogates
n-Pentacosane (S)107 %01/07/21 11:31 629-99-201/07/21 09:5461-134 1
Analytical Method: EPA 5030B/8015C Mod.
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 01/11/21 17:300.080 1
Surrogates
4-Bromofluorobenzene (S)90 %01/11/21 17:30 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Sample: NW Lab ID: 92515110003 Collected: 01/05/21 10:11 Received: 01/06/21 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 01/07/21 12:2301/07/21 09:540.50 1
Surrogates
n-Pentacosane (S)112 %01/07/21 12:23 629-99-201/07/21 09:5461-134 1
Analytical Method: EPA 5030B/8015C Mod.
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 01/11/21 17:580.080 1
Surrogates
4-Bromofluorobenzene (S)87 %01/11/21 17:58 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
591861
EPA 5030B/8015C Mod.
EPA 5030B/8015C Mod.
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92515110001, 92515110002, 92515110003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3124661
Associated Lab Samples:92515110001, 92515110002, 92515110003
Matrix: Water
Analyzed
Gas Range Organics (C6-C10)mg/L ND 0.080 01/11/21 14:14
4-Bromofluorobenzene (S)%89 70-130 01/11/21 14:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3124662LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/L 1.01 102 70-130
4-Bromofluorobenzene (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3125916MATRIX SPIKE SAMPLE:
MSSpike
Result
92515110002
Gas Range Organics (C6-C10)mg/L 0.991 97 68-145ND
4-Bromofluorobenzene (S)%92 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92515110001
3125915SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/L .024JND
4-Bromofluorobenzene (S)%9190
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
591174
EPA 3511
EPA 8015C Modified
8015 Diesel Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92515110001, 92515110002, 92515110003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3120912
Associated Lab Samples:92515110001, 92515110002, 92515110003
Matrix: Water
Analyzed
Diesel Range Organics(C10-C28)mg/L ND 0.50 01/07/21 10:26
n-Pentacosane (S)%114 61-134 01/07/21 10:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3120913LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/L 10.910 109 70-130
n-Pentacosane (S)%132 61-134
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3120914MATRIX SPIKE SAMPLE:
MSSpike
Result
92515110003
Diesel Range Organics(C10-C28)mg/L 10.310 103 51-143ND
n-Pentacosane (S)%118 61-134
Parameter Units
Dup
Result QualifiersRPDResult
92515113002
3120915SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/L NDND
n-Pentacosane (S)%110109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92515110
Sheetz Greensboro (Wendover)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92515110001 591174 591214SWEPA 3511 EPA 8015C Modified
92515110002 591174 591214NEEPA 3511 EPA 8015C Modified
92515110003 591174 591214NWEPA 3511 EPA 8015C Modified
92515110001 591861SWEPA 5030B/8015C Mod.
92515110002 591861NEEPA 5030B/8015C Mod.
92515110003 591861NWEPA 5030B/8015C Mod.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/13/2021 02:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 13
Page 11 of 13
Page 12 of 13
Page 13 of 13

APPENDIX I
RESAMPLED SOIL SAMPLES LABORATORY REPORTS
and CHAIN-OF-CUSTUDIES
____________________________________________________________________________

#=CL#
March 05, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92525426
92525426
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
SHEETZ STORE 356
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on March 03, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92525426001 KEROSENE DISPENSER 17-2 EPA 8015C Modified 2 PASI-CJMS1
SW-846 1 PASI-CKDF
92525426002 PRODUCT LINE 18-2 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92525426003 DISPENSER 5-2 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92525426004 DISPENSER 9-2 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92525426005 PRODUCT LINE 10-2 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92525426001 KEROSENE DISPENSER 17-2
Percent Moisture 31.7 %03/03/21 17:11 N20.10SW-846
92525426002 PRODUCT LINE 18-2
Ethylbenzene 10.9 ug/kg 03/05/21 07:297.7EPA 8260D
Naphthalene 25.2 ug/kg 03/05/21 07:297.7EPA 8260D
n-Propylbenzene 8.3 ug/kg 03/05/21 07:297.7EPA 8260D
o-Xylene 8.2 ug/kg 03/05/21 07:297.7EPA 8260D
Percent Moisture 27.7 %03/03/21 17:35 N20.10SW-846
92525426003 DISPENSER 5-2
Ethylbenzene 21.4 ug/kg 03/05/21 08:047.6EPA 8260D
Toluene 124 ug/kg 03/05/21 08:047.6EPA 8260D
1,2,4-Trimethylbenzene 40.4 ug/kg 03/05/21 08:047.6EPA 8260D
1,3,5-Trimethylbenzene 10.9 ug/kg 03/05/21 08:047.6EPA 8260D
Xylene (Total)138 ug/kg 03/05/21 08:0415.1EPA 8260D
m&p-Xylene 85.1 ug/kg 03/05/21 08:0415.1EPA 8260D
o-Xylene 53.3 ug/kg 03/05/21 08:047.6EPA 8260D
Percent Moisture 27.3 %03/03/21 17:36 N20.10SW-846
92525426004 DISPENSER 9-2
Benzene 1840 ug/kg 03/05/21 08:227.8EPA 8260D
Diisopropyl ether 21.9 ug/kg 03/05/21 08:227.8EPA 8260D
Ethylbenzene 664 ug/kg 03/05/21 08:227.8EPA 8260D
Isopropylbenzene (Cumene)42.7 ug/kg 03/05/21 08:227.8EPA 8260D
Naphthalene 83.6 ug/kg 03/05/21 08:227.8EPA 8260D
n-Propylbenzene 64.2 ug/kg 03/05/21 08:227.8EPA 8260D
Toluene 4360 ug/kg 03/05/21 08:227.8EPA 8260D
1,2,4-Trimethylbenzene 525 ug/kg 03/05/21 08:227.8EPA 8260D
1,3,5-Trimethylbenzene 129 ug/kg 03/05/21 08:227.8EPA 8260D
Xylene (Total)2360 ug/kg 03/05/21 08:2215.6EPA 8260D
m&p-Xylene 1560 ug/kg 03/05/21 08:2215.6EPA 8260D
o-Xylene 804 ug/kg 03/05/21 08:227.8EPA 8260D
Percent Moisture 27.7 %03/03/21 17:36 N20.10SW-846
92525426005 PRODUCT LINE 10-2
Benzene 11.3 ug/kg 03/05/21 08:398.5EPA 8260D
Isopropylbenzene (Cumene)11.7 ug/kg 03/05/21 08:398.5EPA 8260D
Percent Moisture 29.0 %03/03/21 17:56 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: KEROSENE DISPENSER
17-2
Lab ID: 92525426001 Collected: 03/02/21 08:23 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 03/05/21 11:4203/04/21 16:587.4 1
Surrogates
n-Pentacosane (S)88 %03/05/21 11:42 629-99-203/04/21 16:5832-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.7 %03/03/21 17:11 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: PRODUCT LINE 18-2 Lab ID: 92525426002 Collected: 03/02/21 08:32 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/05/21 07:29 67-64-103/04/21 16:36155 1
Benzene ND ug/kg 03/05/21 07:29 71-43-203/04/21 16:367.7 1
Bromobenzene ND ug/kg 03/05/21 07:29 108-86-103/04/21 16:367.7 1
Bromochloromethane ND ug/kg 03/05/21 07:29 74-97-503/04/21 16:367.7 1
Bromodichloromethane ND ug/kg 03/05/21 07:29 75-27-403/04/21 16:367.7 1
Bromoform ND ug/kg 03/05/21 07:29 75-25-203/04/21 16:367.7 1
Bromomethane ND ug/kg 03/05/21 07:29 74-83-9 IH,IK03/04/21 16:3615.5 1
2-Butanone (MEK)ND ug/kg 03/05/21 07:29 78-93-303/04/21 16:36155 1
n-Butylbenzene ND ug/kg 03/05/21 07:29 104-51-803/04/21 16:367.7 1
sec-Butylbenzene ND ug/kg 03/05/21 07:29 135-98-803/04/21 16:367.7 1
tert-Butylbenzene ND ug/kg 03/05/21 07:29 98-06-603/04/21 16:367.7 1
Carbon tetrachloride ND ug/kg 03/05/21 07:29 56-23-503/04/21 16:367.7 1
Chlorobenzene ND ug/kg 03/05/21 07:29 108-90-703/04/21 16:367.7 1
Chloroethane ND ug/kg 03/05/21 07:29 75-00-303/04/21 16:3615.5 1
Chloroform ND ug/kg 03/05/21 07:29 67-66-303/04/21 16:367.7 1
Chloromethane ND ug/kg 03/05/21 07:29 74-87-303/04/21 16:3615.5 1
2-Chlorotoluene ND ug/kg 03/05/21 07:29 95-49-803/04/21 16:367.7 1
4-Chlorotoluene ND ug/kg 03/05/21 07:29 106-43-403/04/21 16:367.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/05/21 07:29 96-12-803/04/21 16:367.7 1
Dibromochloromethane ND ug/kg 03/05/21 07:29 124-48-103/04/21 16:367.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/05/21 07:29 106-93-403/04/21 16:367.7 1
Dibromomethane ND ug/kg 03/05/21 07:29 74-95-303/04/21 16:367.7 1
1,2-Dichlorobenzene ND ug/kg 03/05/21 07:29 95-50-103/04/21 16:367.7 1
1,3-Dichlorobenzene ND ug/kg 03/05/21 07:29 541-73-103/04/21 16:367.7 1
1,4-Dichlorobenzene ND ug/kg 03/05/21 07:29 106-46-703/04/21 16:367.7 1
Dichlorodifluoromethane ND ug/kg 03/05/21 07:29 75-71-803/04/21 16:3615.5 1
1,1-Dichloroethane ND ug/kg 03/05/21 07:29 75-34-303/04/21 16:367.7 1
1,2-Dichloroethane ND ug/kg 03/05/21 07:29 107-06-203/04/21 16:367.7 1
1,1-Dichloroethene ND ug/kg 03/05/21 07:29 75-35-403/04/21 16:367.7 1
cis-1,2-Dichloroethene ND ug/kg 03/05/21 07:29 156-59-203/04/21 16:367.7 1
trans-1,2-Dichloroethene ND ug/kg 03/05/21 07:29 156-60-503/04/21 16:367.7 1
1,2-Dichloropropane ND ug/kg 03/05/21 07:29 78-87-503/04/21 16:367.7 1
1,3-Dichloropropane ND ug/kg 03/05/21 07:29 142-28-903/04/21 16:367.7 1
2,2-Dichloropropane ND ug/kg 03/05/21 07:29 594-20-703/04/21 16:367.7 1
1,1-Dichloropropene ND ug/kg 03/05/21 07:29 563-58-603/04/21 16:367.7 1
cis-1,3-Dichloropropene ND ug/kg 03/05/21 07:29 10061-01-503/04/21 16:367.7 1
trans-1,3-Dichloropropene ND ug/kg 03/05/21 07:29 10061-02-603/04/21 16:367.7 1
Diisopropyl ether ND ug/kg 03/05/21 07:29 108-20-303/04/21 16:367.7 1
Ethylbenzene 10.9 ug/kg 03/05/21 07:29 100-41-403/04/21 16:367.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/05/21 07:29 87-68-3 IK03/04/21 16:3615.5 1
2-Hexanone ND ug/kg 03/05/21 07:29 591-78-603/04/21 16:3677.3 1
Isopropylbenzene (Cumene)ND ug/kg 03/05/21 07:29 98-82-803/04/21 16:367.7 1
p-Isopropyltoluene ND ug/kg 03/05/21 07:29 99-87-603/04/21 16:367.7 1
Methylene Chloride ND ug/kg 03/05/21 07:29 75-09-203/04/21 16:3630.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/05/21 07:29 108-10-103/04/21 16:3677.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: PRODUCT LINE 18-2 Lab ID: 92525426002 Collected: 03/02/21 08:32 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 03/05/21 07:29 1634-04-403/04/21 16:367.7 1
Naphthalene 25.2 ug/kg 03/05/21 07:29 91-20-303/04/21 16:367.7 1
n-Propylbenzene 8.3 ug/kg 03/05/21 07:29 103-65-103/04/21 16:367.7 1
Styrene ND ug/kg 03/05/21 07:29 100-42-503/04/21 16:367.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/05/21 07:29 630-20-603/04/21 16:367.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/05/21 07:29 79-34-503/04/21 16:367.7 1
Tetrachloroethene ND ug/kg 03/05/21 07:29 127-18-403/04/21 16:367.7 1
Toluene ND ug/kg 03/05/21 07:29 108-88-303/04/21 16:367.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/05/21 07:29 87-61-603/04/21 16:367.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/05/21 07:29 120-82-103/04/21 16:367.7 1
1,1,1-Trichloroethane ND ug/kg 03/05/21 07:29 71-55-603/04/21 16:367.7 1
1,1,2-Trichloroethane ND ug/kg 03/05/21 07:29 79-00-503/04/21 16:367.7 1
Trichloroethene ND ug/kg 03/05/21 07:29 79-01-603/04/21 16:367.7 1
Trichlorofluoromethane ND ug/kg 03/05/21 07:29 75-69-403/04/21 16:367.7 1
1,2,3-Trichloropropane ND ug/kg 03/05/21 07:29 96-18-403/04/21 16:367.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/05/21 07:29 95-63-603/04/21 16:367.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/05/21 07:29 108-67-803/04/21 16:367.7 1
Vinyl acetate ND ug/kg 03/05/21 07:29 108-05-403/04/21 16:3677.3 1
Vinyl chloride ND ug/kg 03/05/21 07:29 75-01-403/04/21 16:3615.5 1
Xylene (Total)ND ug/kg 03/05/21 07:29 1330-20-703/04/21 16:3615.5 1
m&p-Xylene ND ug/kg 03/05/21 07:29 179601-23-103/04/21 16:3615.5 1
o-Xylene 8.2 ug/kg 03/05/21 07:29 95-47-603/04/21 16:367.7 1
Surrogates
Toluene-d8 (S)99 %03/05/21 07:29 2037-26-503/04/21 16:3670-130 1
4-Bromofluorobenzene (S)102 %03/05/21 07:29 460-00-403/04/21 16:3669-134 1
1,2-Dichloroethane-d4 (S)104 %03/05/21 07:29 17060-07-003/04/21 16:3670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.7 %03/03/21 17:35 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: DISPENSER 5-2 Lab ID: 92525426003 Collected: 03/02/21 08:51 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/05/21 08:04 67-64-103/04/21 16:36151 1
Benzene ND ug/kg 03/05/21 08:04 71-43-203/04/21 16:367.6 1
Bromobenzene ND ug/kg 03/05/21 08:04 108-86-103/04/21 16:367.6 1
Bromochloromethane ND ug/kg 03/05/21 08:04 74-97-503/04/21 16:367.6 1
Bromodichloromethane ND ug/kg 03/05/21 08:04 75-27-403/04/21 16:367.6 1
Bromoform ND ug/kg 03/05/21 08:04 75-25-203/04/21 16:367.6 1
Bromomethane ND ug/kg 03/05/21 08:04 74-83-9 IH,IK03/04/21 16:3615.1 1
2-Butanone (MEK)ND ug/kg 03/05/21 08:04 78-93-303/04/21 16:36151 1
n-Butylbenzene ND ug/kg 03/05/21 08:04 104-51-803/04/21 16:367.6 1
sec-Butylbenzene ND ug/kg 03/05/21 08:04 135-98-803/04/21 16:367.6 1
tert-Butylbenzene ND ug/kg 03/05/21 08:04 98-06-603/04/21 16:367.6 1
Carbon tetrachloride ND ug/kg 03/05/21 08:04 56-23-503/04/21 16:367.6 1
Chlorobenzene ND ug/kg 03/05/21 08:04 108-90-703/04/21 16:367.6 1
Chloroethane ND ug/kg 03/05/21 08:04 75-00-303/04/21 16:3615.1 1
Chloroform ND ug/kg 03/05/21 08:04 67-66-303/04/21 16:367.6 1
Chloromethane ND ug/kg 03/05/21 08:04 74-87-303/04/21 16:3615.1 1
2-Chlorotoluene ND ug/kg 03/05/21 08:04 95-49-803/04/21 16:367.6 1
4-Chlorotoluene ND ug/kg 03/05/21 08:04 106-43-403/04/21 16:367.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/05/21 08:04 96-12-803/04/21 16:367.6 1
Dibromochloromethane ND ug/kg 03/05/21 08:04 124-48-103/04/21 16:367.6 1
1,2-Dibromoethane (EDB)ND ug/kg 03/05/21 08:04 106-93-403/04/21 16:367.6 1
Dibromomethane ND ug/kg 03/05/21 08:04 74-95-303/04/21 16:367.6 1
1,2-Dichlorobenzene ND ug/kg 03/05/21 08:04 95-50-103/04/21 16:367.6 1
1,3-Dichlorobenzene ND ug/kg 03/05/21 08:04 541-73-103/04/21 16:367.6 1
1,4-Dichlorobenzene ND ug/kg 03/05/21 08:04 106-46-703/04/21 16:367.6 1
Dichlorodifluoromethane ND ug/kg 03/05/21 08:04 75-71-803/04/21 16:3615.1 1
1,1-Dichloroethane ND ug/kg 03/05/21 08:04 75-34-303/04/21 16:367.6 1
1,2-Dichloroethane ND ug/kg 03/05/21 08:04 107-06-203/04/21 16:367.6 1
1,1-Dichloroethene ND ug/kg 03/05/21 08:04 75-35-403/04/21 16:367.6 1
cis-1,2-Dichloroethene ND ug/kg 03/05/21 08:04 156-59-203/04/21 16:367.6 1
trans-1,2-Dichloroethene ND ug/kg 03/05/21 08:04 156-60-503/04/21 16:367.6 1
1,2-Dichloropropane ND ug/kg 03/05/21 08:04 78-87-503/04/21 16:367.6 1
1,3-Dichloropropane ND ug/kg 03/05/21 08:04 142-28-903/04/21 16:367.6 1
2,2-Dichloropropane ND ug/kg 03/05/21 08:04 594-20-703/04/21 16:367.6 1
1,1-Dichloropropene ND ug/kg 03/05/21 08:04 563-58-603/04/21 16:367.6 1
cis-1,3-Dichloropropene ND ug/kg 03/05/21 08:04 10061-01-503/04/21 16:367.6 1
trans-1,3-Dichloropropene ND ug/kg 03/05/21 08:04 10061-02-603/04/21 16:367.6 1
Diisopropyl ether ND ug/kg 03/05/21 08:04 108-20-303/04/21 16:367.6 1
Ethylbenzene 21.4 ug/kg 03/05/21 08:04 100-41-403/04/21 16:367.6 1
Hexachloro-1,3-butadiene ND ug/kg 03/05/21 08:04 87-68-3 IK03/04/21 16:3615.1 1
2-Hexanone ND ug/kg 03/05/21 08:04 591-78-603/04/21 16:3675.7 1
Isopropylbenzene (Cumene)ND ug/kg 03/05/21 08:04 98-82-803/04/21 16:367.6 1
p-Isopropyltoluene ND ug/kg 03/05/21 08:04 99-87-603/04/21 16:367.6 1
Methylene Chloride ND ug/kg 03/05/21 08:04 75-09-203/04/21 16:3630.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/05/21 08:04 108-10-103/04/21 16:3675.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: DISPENSER 5-2 Lab ID: 92525426003 Collected: 03/02/21 08:51 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 03/05/21 08:04 1634-04-403/04/21 16:367.6 1
Naphthalene ND ug/kg 03/05/21 08:04 91-20-303/04/21 16:367.6 1
n-Propylbenzene ND ug/kg 03/05/21 08:04 103-65-103/04/21 16:367.6 1
Styrene ND ug/kg 03/05/21 08:04 100-42-503/04/21 16:367.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/05/21 08:04 630-20-603/04/21 16:367.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/05/21 08:04 79-34-503/04/21 16:367.6 1
Tetrachloroethene ND ug/kg 03/05/21 08:04 127-18-403/04/21 16:367.6 1
Toluene 124 ug/kg 03/05/21 08:04 108-88-303/04/21 16:367.6 1
1,2,3-Trichlorobenzene ND ug/kg 03/05/21 08:04 87-61-603/04/21 16:367.6 1
1,2,4-Trichlorobenzene ND ug/kg 03/05/21 08:04 120-82-103/04/21 16:367.6 1
1,1,1-Trichloroethane ND ug/kg 03/05/21 08:04 71-55-603/04/21 16:367.6 1
1,1,2-Trichloroethane ND ug/kg 03/05/21 08:04 79-00-503/04/21 16:367.6 1
Trichloroethene ND ug/kg 03/05/21 08:04 79-01-603/04/21 16:367.6 1
Trichlorofluoromethane ND ug/kg 03/05/21 08:04 75-69-403/04/21 16:367.6 1
1,2,3-Trichloropropane ND ug/kg 03/05/21 08:04 96-18-403/04/21 16:367.6 1
1,2,4-Trimethylbenzene 40.4 ug/kg 03/05/21 08:04 95-63-603/04/21 16:367.6 1
1,3,5-Trimethylbenzene 10.9 ug/kg 03/05/21 08:04 108-67-803/04/21 16:367.6 1
Vinyl acetate ND ug/kg 03/05/21 08:04 108-05-403/04/21 16:3675.7 1
Vinyl chloride ND ug/kg 03/05/21 08:04 75-01-403/04/21 16:3615.1 1
Xylene (Total)138 ug/kg 03/05/21 08:04 1330-20-703/04/21 16:3615.1 1
m&p-Xylene 85.1 ug/kg 03/05/21 08:04 179601-23-103/04/21 16:3615.1 1
o-Xylene 53.3 ug/kg 03/05/21 08:04 95-47-603/04/21 16:367.6 1
Surrogates
Toluene-d8 (S)100 %03/05/21 08:04 2037-26-503/04/21 16:3670-130 1
4-Bromofluorobenzene (S)100 %03/05/21 08:04 460-00-403/04/21 16:3669-134 1
1,2-Dichloroethane-d4 (S)105 %03/05/21 08:04 17060-07-003/04/21 16:3670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.3 %03/03/21 17:36 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: DISPENSER 9-2 Lab ID: 92525426004 Collected: 03/02/21 09:06 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/05/21 08:22 67-64-103/04/21 16:36156 1
Benzene 1840 ug/kg 03/05/21 08:22 71-43-203/04/21 16:367.8 1
Bromobenzene ND ug/kg 03/05/21 08:22 108-86-103/04/21 16:367.8 1
Bromochloromethane ND ug/kg 03/05/21 08:22 74-97-503/04/21 16:367.8 1
Bromodichloromethane ND ug/kg 03/05/21 08:22 75-27-403/04/21 16:367.8 1
Bromoform ND ug/kg 03/05/21 08:22 75-25-203/04/21 16:367.8 1
Bromomethane ND ug/kg 03/05/21 08:22 74-83-9 IH,IK03/04/21 16:3615.6 1
2-Butanone (MEK)ND ug/kg 03/05/21 08:22 78-93-303/04/21 16:36156 1
n-Butylbenzene ND ug/kg 03/05/21 08:22 104-51-803/04/21 16:367.8 1
sec-Butylbenzene ND ug/kg 03/05/21 08:22 135-98-803/04/21 16:367.8 1
tert-Butylbenzene ND ug/kg 03/05/21 08:22 98-06-603/04/21 16:367.8 1
Carbon tetrachloride ND ug/kg 03/05/21 08:22 56-23-503/04/21 16:367.8 1
Chlorobenzene ND ug/kg 03/05/21 08:22 108-90-703/04/21 16:367.8 1
Chloroethane ND ug/kg 03/05/21 08:22 75-00-303/04/21 16:3615.6 1
Chloroform ND ug/kg 03/05/21 08:22 67-66-303/04/21 16:367.8 1
Chloromethane ND ug/kg 03/05/21 08:22 74-87-303/04/21 16:3615.6 1
2-Chlorotoluene ND ug/kg 03/05/21 08:22 95-49-803/04/21 16:367.8 1
4-Chlorotoluene ND ug/kg 03/05/21 08:22 106-43-403/04/21 16:367.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/05/21 08:22 96-12-803/04/21 16:367.8 1
Dibromochloromethane ND ug/kg 03/05/21 08:22 124-48-103/04/21 16:367.8 1
1,2-Dibromoethane (EDB)ND ug/kg 03/05/21 08:22 106-93-403/04/21 16:367.8 1
Dibromomethane ND ug/kg 03/05/21 08:22 74-95-303/04/21 16:367.8 1
1,2-Dichlorobenzene ND ug/kg 03/05/21 08:22 95-50-103/04/21 16:367.8 1
1,3-Dichlorobenzene ND ug/kg 03/05/21 08:22 541-73-103/04/21 16:367.8 1
1,4-Dichlorobenzene ND ug/kg 03/05/21 08:22 106-46-703/04/21 16:367.8 1
Dichlorodifluoromethane ND ug/kg 03/05/21 08:22 75-71-803/04/21 16:3615.6 1
1,1-Dichloroethane ND ug/kg 03/05/21 08:22 75-34-303/04/21 16:367.8 1
1,2-Dichloroethane ND ug/kg 03/05/21 08:22 107-06-203/04/21 16:367.8 1
1,1-Dichloroethene ND ug/kg 03/05/21 08:22 75-35-403/04/21 16:367.8 1
cis-1,2-Dichloroethene ND ug/kg 03/05/21 08:22 156-59-203/04/21 16:367.8 1
trans-1,2-Dichloroethene ND ug/kg 03/05/21 08:22 156-60-503/04/21 16:367.8 1
1,2-Dichloropropane ND ug/kg 03/05/21 08:22 78-87-503/04/21 16:367.8 1
1,3-Dichloropropane ND ug/kg 03/05/21 08:22 142-28-903/04/21 16:367.8 1
2,2-Dichloropropane ND ug/kg 03/05/21 08:22 594-20-703/04/21 16:367.8 1
1,1-Dichloropropene ND ug/kg 03/05/21 08:22 563-58-603/04/21 16:367.8 1
cis-1,3-Dichloropropene ND ug/kg 03/05/21 08:22 10061-01-503/04/21 16:367.8 1
trans-1,3-Dichloropropene ND ug/kg 03/05/21 08:22 10061-02-603/04/21 16:367.8 1
Diisopropyl ether 21.9 ug/kg 03/05/21 08:22 108-20-303/04/21 16:367.8 1
Ethylbenzene 664 ug/kg 03/05/21 08:22 100-41-403/04/21 16:367.8 1
Hexachloro-1,3-butadiene ND ug/kg 03/05/21 08:22 87-68-3 IK03/04/21 16:3615.6 1
2-Hexanone ND ug/kg 03/05/21 08:22 591-78-603/04/21 16:3678.0 1
Isopropylbenzene (Cumene)42.7 ug/kg 03/05/21 08:22 98-82-803/04/21 16:367.8 1
p-Isopropyltoluene ND ug/kg 03/05/21 08:22 99-87-603/04/21 16:367.8 1
Methylene Chloride ND ug/kg 03/05/21 08:22 75-09-203/04/21 16:3631.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/05/21 08:22 108-10-103/04/21 16:3678.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: DISPENSER 9-2 Lab ID: 92525426004 Collected: 03/02/21 09:06 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 03/05/21 08:22 1634-04-403/04/21 16:367.8 1
Naphthalene 83.6 ug/kg 03/05/21 08:22 91-20-303/04/21 16:367.8 1
n-Propylbenzene 64.2 ug/kg 03/05/21 08:22 103-65-103/04/21 16:367.8 1
Styrene ND ug/kg 03/05/21 08:22 100-42-503/04/21 16:367.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/05/21 08:22 630-20-603/04/21 16:367.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/05/21 08:22 79-34-503/04/21 16:367.8 1
Tetrachloroethene ND ug/kg 03/05/21 08:22 127-18-403/04/21 16:367.8 1
Toluene 4360 ug/kg 03/05/21 08:22 108-88-303/04/21 16:367.8 1
1,2,3-Trichlorobenzene ND ug/kg 03/05/21 08:22 87-61-603/04/21 16:367.8 1
1,2,4-Trichlorobenzene ND ug/kg 03/05/21 08:22 120-82-103/04/21 16:367.8 1
1,1,1-Trichloroethane ND ug/kg 03/05/21 08:22 71-55-603/04/21 16:367.8 1
1,1,2-Trichloroethane ND ug/kg 03/05/21 08:22 79-00-503/04/21 16:367.8 1
Trichloroethene ND ug/kg 03/05/21 08:22 79-01-603/04/21 16:367.8 1
Trichlorofluoromethane ND ug/kg 03/05/21 08:22 75-69-403/04/21 16:367.8 1
1,2,3-Trichloropropane ND ug/kg 03/05/21 08:22 96-18-403/04/21 16:367.8 1
1,2,4-Trimethylbenzene 525 ug/kg 03/05/21 08:22 95-63-603/04/21 16:367.8 1
1,3,5-Trimethylbenzene 129 ug/kg 03/05/21 08:22 108-67-803/04/21 16:367.8 1
Vinyl acetate ND ug/kg 03/05/21 08:22 108-05-403/04/21 16:3678.0 1
Vinyl chloride ND ug/kg 03/05/21 08:22 75-01-403/04/21 16:3615.6 1
Xylene (Total)2360 ug/kg 03/05/21 08:22 1330-20-703/04/21 16:3615.6 1
m&p-Xylene 1560 ug/kg 03/05/21 08:22 179601-23-103/04/21 16:3615.6 1
o-Xylene 804 ug/kg 03/05/21 08:22 95-47-603/04/21 16:367.8 1
Surrogates
Toluene-d8 (S)99 %03/05/21 08:22 2037-26-503/04/21 16:3670-130 1
4-Bromofluorobenzene (S)104 %03/05/21 08:22 460-00-403/04/21 16:3669-134 1
1,2-Dichloroethane-d4 (S)104 %03/05/21 08:22 17060-07-003/04/21 16:3670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.7 %03/03/21 17:36 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: PRODUCT LINE 10-2 Lab ID: 92525426005 Collected: 03/02/21 09:20 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/05/21 08:39 67-64-103/04/21 16:36170 1
Benzene 11.3 ug/kg 03/05/21 08:39 71-43-203/04/21 16:368.5 1
Bromobenzene ND ug/kg 03/05/21 08:39 108-86-103/04/21 16:368.5 1
Bromochloromethane ND ug/kg 03/05/21 08:39 74-97-503/04/21 16:368.5 1
Bromodichloromethane ND ug/kg 03/05/21 08:39 75-27-403/04/21 16:368.5 1
Bromoform ND ug/kg 03/05/21 08:39 75-25-203/04/21 16:368.5 1
Bromomethane ND ug/kg 03/05/21 08:39 74-83-9 IH,IK03/04/21 16:3617.0 1
2-Butanone (MEK)ND ug/kg 03/05/21 08:39 78-93-303/04/21 16:36170 1
n-Butylbenzene ND ug/kg 03/05/21 08:39 104-51-803/04/21 16:368.5 1
sec-Butylbenzene ND ug/kg 03/05/21 08:39 135-98-803/04/21 16:368.5 1
tert-Butylbenzene ND ug/kg 03/05/21 08:39 98-06-603/04/21 16:368.5 1
Carbon tetrachloride ND ug/kg 03/05/21 08:39 56-23-503/04/21 16:368.5 1
Chlorobenzene ND ug/kg 03/05/21 08:39 108-90-703/04/21 16:368.5 1
Chloroethane ND ug/kg 03/05/21 08:39 75-00-303/04/21 16:3617.0 1
Chloroform ND ug/kg 03/05/21 08:39 67-66-303/04/21 16:368.5 1
Chloromethane ND ug/kg 03/05/21 08:39 74-87-303/04/21 16:3617.0 1
2-Chlorotoluene ND ug/kg 03/05/21 08:39 95-49-803/04/21 16:368.5 1
4-Chlorotoluene ND ug/kg 03/05/21 08:39 106-43-403/04/21 16:368.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/05/21 08:39 96-12-803/04/21 16:368.5 1
Dibromochloromethane ND ug/kg 03/05/21 08:39 124-48-103/04/21 16:368.5 1
1,2-Dibromoethane (EDB)ND ug/kg 03/05/21 08:39 106-93-403/04/21 16:368.5 1
Dibromomethane ND ug/kg 03/05/21 08:39 74-95-303/04/21 16:368.5 1
1,2-Dichlorobenzene ND ug/kg 03/05/21 08:39 95-50-103/04/21 16:368.5 1
1,3-Dichlorobenzene ND ug/kg 03/05/21 08:39 541-73-103/04/21 16:368.5 1
1,4-Dichlorobenzene ND ug/kg 03/05/21 08:39 106-46-703/04/21 16:368.5 1
Dichlorodifluoromethane ND ug/kg 03/05/21 08:39 75-71-803/04/21 16:3617.0 1
1,1-Dichloroethane ND ug/kg 03/05/21 08:39 75-34-303/04/21 16:368.5 1
1,2-Dichloroethane ND ug/kg 03/05/21 08:39 107-06-203/04/21 16:368.5 1
1,1-Dichloroethene ND ug/kg 03/05/21 08:39 75-35-403/04/21 16:368.5 1
cis-1,2-Dichloroethene ND ug/kg 03/05/21 08:39 156-59-203/04/21 16:368.5 1
trans-1,2-Dichloroethene ND ug/kg 03/05/21 08:39 156-60-503/04/21 16:368.5 1
1,2-Dichloropropane ND ug/kg 03/05/21 08:39 78-87-503/04/21 16:368.5 1
1,3-Dichloropropane ND ug/kg 03/05/21 08:39 142-28-903/04/21 16:368.5 1
2,2-Dichloropropane ND ug/kg 03/05/21 08:39 594-20-703/04/21 16:368.5 1
1,1-Dichloropropene ND ug/kg 03/05/21 08:39 563-58-603/04/21 16:368.5 1
cis-1,3-Dichloropropene ND ug/kg 03/05/21 08:39 10061-01-503/04/21 16:368.5 1
trans-1,3-Dichloropropene ND ug/kg 03/05/21 08:39 10061-02-603/04/21 16:368.5 1
Diisopropyl ether ND ug/kg 03/05/21 08:39 108-20-303/04/21 16:368.5 1
Ethylbenzene ND ug/kg 03/05/21 08:39 100-41-403/04/21 16:368.5 1
Hexachloro-1,3-butadiene ND ug/kg 03/05/21 08:39 87-68-3 IK03/04/21 16:3617.0 1
2-Hexanone ND ug/kg 03/05/21 08:39 591-78-603/04/21 16:3684.8 1
Isopropylbenzene (Cumene)11.7 ug/kg 03/05/21 08:39 98-82-803/04/21 16:368.5 1
p-Isopropyltoluene ND ug/kg 03/05/21 08:39 99-87-603/04/21 16:368.5 1
Methylene Chloride ND ug/kg 03/05/21 08:39 75-09-203/04/21 16:3633.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/05/21 08:39 108-10-103/04/21 16:3684.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Sample: PRODUCT LINE 10-2 Lab ID: 92525426005 Collected: 03/02/21 09:20 Received: 03/03/21 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 03/05/21 08:39 1634-04-403/04/21 16:368.5 1
Naphthalene ND ug/kg 03/05/21 08:39 91-20-303/04/21 16:368.5 1
n-Propylbenzene ND ug/kg 03/05/21 08:39 103-65-103/04/21 16:368.5 1
Styrene ND ug/kg 03/05/21 08:39 100-42-503/04/21 16:368.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/05/21 08:39 630-20-603/04/21 16:368.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/05/21 08:39 79-34-503/04/21 16:368.5 1
Tetrachloroethene ND ug/kg 03/05/21 08:39 127-18-403/04/21 16:368.5 1
Toluene ND ug/kg 03/05/21 08:39 108-88-303/04/21 16:368.5 1
1,2,3-Trichlorobenzene ND ug/kg 03/05/21 08:39 87-61-603/04/21 16:368.5 1
1,2,4-Trichlorobenzene ND ug/kg 03/05/21 08:39 120-82-103/04/21 16:368.5 1
1,1,1-Trichloroethane ND ug/kg 03/05/21 08:39 71-55-603/04/21 16:368.5 1
1,1,2-Trichloroethane ND ug/kg 03/05/21 08:39 79-00-503/04/21 16:368.5 1
Trichloroethene ND ug/kg 03/05/21 08:39 79-01-603/04/21 16:368.5 1
Trichlorofluoromethane ND ug/kg 03/05/21 08:39 75-69-403/04/21 16:368.5 1
1,2,3-Trichloropropane ND ug/kg 03/05/21 08:39 96-18-403/04/21 16:368.5 1
1,2,4-Trimethylbenzene ND ug/kg 03/05/21 08:39 95-63-603/04/21 16:368.5 1
1,3,5-Trimethylbenzene ND ug/kg 03/05/21 08:39 108-67-803/04/21 16:368.5 1
Vinyl acetate ND ug/kg 03/05/21 08:39 108-05-403/04/21 16:3684.8 1
Vinyl chloride ND ug/kg 03/05/21 08:39 75-01-403/04/21 16:3617.0 1
Xylene (Total)ND ug/kg 03/05/21 08:39 1330-20-703/04/21 16:3617.0 1
m&p-Xylene ND ug/kg 03/05/21 08:39 179601-23-103/04/21 16:3617.0 1
o-Xylene ND ug/kg 03/05/21 08:39 95-47-603/04/21 16:368.5 1
Surrogates
Toluene-d8 (S)99 %03/05/21 08:39 2037-26-503/04/21 16:3670-130 1
4-Bromofluorobenzene (S)100 %03/05/21 08:39 460-00-403/04/21 16:3669-134 1
1,2-Dichloroethane-d4 (S)105 %03/05/21 08:39 17060-07-003/04/21 16:3670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.0 %03/03/21 17:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604347
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92525426002, 92525426003, 92525426004, 92525426005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3183972
Associated Lab Samples:92525426002, 92525426003, 92525426004, 92525426005
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/05/21 01:01
1,1,1-Trichloroethane ug/kg ND 5.0 03/05/21 01:01
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/05/21 01:01
1,1,2-Trichloroethane ug/kg ND 5.0 03/05/21 01:01
1,1-Dichloroethane ug/kg ND 5.0 03/05/21 01:01
1,1-Dichloroethene ug/kg ND 5.0 03/05/21 01:01
1,1-Dichloropropene ug/kg ND 5.0 03/05/21 01:01
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/05/21 01:01
1,2,3-Trichloropropane ug/kg ND 5.0 03/05/21 01:01
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/05/21 01:01
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/05/21 01:01
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/05/21 01:01
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/05/21 01:01
1,2-Dichlorobenzene ug/kg ND 5.0 03/05/21 01:01
1,2-Dichloroethane ug/kg ND 5.0 03/05/21 01:01
1,2-Dichloropropane ug/kg ND 5.0 03/05/21 01:01
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/05/21 01:01
1,3-Dichlorobenzene ug/kg ND 5.0 03/05/21 01:01
1,3-Dichloropropane ug/kg ND 5.0 03/05/21 01:01
1,4-Dichlorobenzene ug/kg ND 5.0 03/05/21 01:01
2,2-Dichloropropane ug/kg ND 5.0 03/05/21 01:01
2-Butanone (MEK)ug/kg ND 100 03/05/21 01:01
2-Chlorotoluene ug/kg ND 5.0 03/05/21 01:01
2-Hexanone ug/kg ND 50.0 03/05/21 01:01
4-Chlorotoluene ug/kg ND 5.0 03/05/21 01:01
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/05/21 01:01
Acetone ug/kg ND 100 03/05/21 01:01
Benzene ug/kg ND 5.0 03/05/21 01:01
Bromobenzene ug/kg ND 5.0 03/05/21 01:01
Bromochloromethane ug/kg ND 5.0 03/05/21 01:01
Bromodichloromethane ug/kg ND 5.0 03/05/21 01:01
Bromoform ug/kg ND 5.0 03/05/21 01:01
Bromomethane ug/kg ND 10.0 IH,IK03/05/21 01:01
Carbon tetrachloride ug/kg ND 5.0 03/05/21 01:01
Chlorobenzene ug/kg ND 5.0 03/05/21 01:01
Chloroethane ug/kg ND 10.0 03/05/21 01:01
Chloroform ug/kg ND 5.0 03/05/21 01:01
Chloromethane ug/kg ND 10.0 03/05/21 01:01
cis-1,2-Dichloroethene ug/kg ND 5.0 03/05/21 01:01
cis-1,3-Dichloropropene ug/kg ND 5.0 03/05/21 01:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3183972
Associated Lab Samples:92525426002, 92525426003, 92525426004, 92525426005
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 03/05/21 01:01
Dibromomethane ug/kg ND 5.0 03/05/21 01:01
Dichlorodifluoromethane ug/kg ND 10.0 03/05/21 01:01
Diisopropyl ether ug/kg ND 5.0 03/05/21 01:01
Ethylbenzene ug/kg ND 5.0 03/05/21 01:01
Hexachloro-1,3-butadiene ug/kg ND 10.0 IK03/05/21 01:01
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/05/21 01:01
m&p-Xylene ug/kg ND 10.0 03/05/21 01:01
Methyl-tert-butyl ether ug/kg ND 5.0 03/05/21 01:01
Methylene Chloride ug/kg ND 20.0 03/05/21 01:01
n-Butylbenzene ug/kg ND 5.0 03/05/21 01:01
n-Propylbenzene ug/kg ND 5.0 03/05/21 01:01
Naphthalene ug/kg ND 5.0 03/05/21 01:01
o-Xylene ug/kg ND 5.0 03/05/21 01:01
p-Isopropyltoluene ug/kg ND 5.0 03/05/21 01:01
sec-Butylbenzene ug/kg ND 5.0 03/05/21 01:01
Styrene ug/kg ND 5.0 03/05/21 01:01
tert-Butylbenzene ug/kg ND 5.0 03/05/21 01:01
Tetrachloroethene ug/kg ND 5.0 03/05/21 01:01
Toluene ug/kg ND 5.0 03/05/21 01:01
trans-1,2-Dichloroethene ug/kg ND 5.0 03/05/21 01:01
trans-1,3-Dichloropropene ug/kg ND 5.0 03/05/21 01:01
Trichloroethene ug/kg ND 5.0 03/05/21 01:01
Trichlorofluoromethane ug/kg ND 5.0 03/05/21 01:01
Vinyl acetate ug/kg ND 50.0 03/05/21 01:01
Vinyl chloride ug/kg ND 10.0 03/05/21 01:01
Xylene (Total)ug/kg ND 10.0 03/05/21 01:01
1,2-Dichloroethane-d4 (S)%111 70-130 03/05/21 01:01
4-Bromofluorobenzene (S)%98 69-134 03/05/21 01:01
Toluene-d8 (S)%101 70-130 03/05/21 01:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3183973LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11801250 94 70-130
1,1,1-Trichloroethane ug/kg 11801250 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 12001250 96 70-130
1,1,2-Trichloroethane ug/kg 12801250 102 70-130
1,1-Dichloroethane ug/kg 11801250 94 70-130
1,1-Dichloroethene ug/kg 12301250 98 70-130
1,1-Dichloropropene ug/kg 12001250 96 70-130
1,2,3-Trichlorobenzene ug/kg 12001250 96 65-130
1,2,3-Trichloropropane ug/kg 12101250 97 70-130
1,2,4-Trichlorobenzene ug/kg 12001250 96 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3183973LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12201250 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 13101250 105 70-130
1,2-Dibromoethane (EDB)ug/kg 12301250 99 70-130
1,2-Dichlorobenzene ug/kg 12601250 100 70-130
1,2-Dichloroethane ug/kg 11401250 91 63-130
1,2-Dichloropropane ug/kg 12301250 99 70-130
1,3,5-Trimethylbenzene ug/kg 12101250 97 70-130
1,3-Dichlorobenzene ug/kg 12201250 98 70-130
1,3-Dichloropropane ug/kg 12401250 100 70-130
1,4-Dichlorobenzene ug/kg 11701250 94 70-130
2,2-Dichloropropane ug/kg 12001250 96 66-130
2-Butanone (MEK)ug/kg 25102500 100 70-130
2-Chlorotoluene ug/kg 12301250 98 70-130
2-Hexanone ug/kg 24902500 99 70-130
4-Chlorotoluene ug/kg 12701250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25002500 100 70-130
Acetone ug/kg 25902500 104 69-130
Benzene ug/kg 12201250 97 70-130
Bromobenzene ug/kg 12301250 99 70-130
Bromochloromethane ug/kg 13201250 106 70-130
Bromodichloromethane ug/kg 11301250 90 69-130
Bromoform ug/kg 12601250 101 70-130
Bromomethane ug/kg 1430 IH,IK1250115 52-130
Carbon tetrachloride ug/kg 11801250 95 70-130
Chlorobenzene ug/kg 11901250 95 70-130
Chloroethane ug/kg 12201250 97 65-130
Chloroform ug/kg 12001250 96 70-130
Chloromethane ug/kg 12501250 100 55-130
cis-1,2-Dichloroethene ug/kg 11701250 94 70-130
cis-1,3-Dichloropropene ug/kg 12301250 99 70-130
Dibromochloromethane ug/kg 12601250 101 70-130
Dibromomethane ug/kg 12801250 102 70-130
Dichlorodifluoromethane ug/kg 13301250 106 45-156
Diisopropyl ether ug/kg 11601250 93 70-130
Ethylbenzene ug/kg 12101250 97 70-130
Hexachloro-1,3-butadiene ug/kg 1230 IK125098 66-130
Isopropylbenzene (Cumene)ug/kg 11801250 94 70-130
m&p-Xylene ug/kg 23402500 94 70-130
Methyl-tert-butyl ether ug/kg 12001250 96 70-130
Methylene Chloride ug/kg 12201250 97 65-130
n-Butylbenzene ug/kg 12001250 96 67-130
n-Propylbenzene ug/kg 12401250 100 70-130
Naphthalene ug/kg 12601250 100 70-130
o-Xylene ug/kg 12001250 96 70-130
p-Isopropyltoluene ug/kg 12001250 96 67-130
sec-Butylbenzene ug/kg 11901250 95 69-130
Styrene ug/kg 12401250 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3183973LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12001250 96 67-130
Tetrachloroethene ug/kg 12101250 97 70-130
Toluene ug/kg 11501250 92 70-130
trans-1,2-Dichloroethene ug/kg 12401250 99 70-130
trans-1,3-Dichloropropene ug/kg 12301250 98 68-130
Trichloroethene ug/kg 12401250 99 70-130
Trichlorofluoromethane ug/kg 12201250 98 70-130
Vinyl acetate ug/kg 28702500 115 70-130
Vinyl chloride ug/kg 12501250 100 61-130
Xylene (Total)ug/kg 35403750 94 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3183975MATRIX SPIKE SAMPLE:
MSSpike
Result
92525426003
1,1,1,2-Tetrachloroethane ug/kg 713756 94 70-131ND
1,1,1-Trichloroethane ug/kg 718756 95 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 706756 93 66-130ND
1,1,2-Trichloroethane ug/kg 793756 105 66-133ND
1,1-Dichloroethane ug/kg 715756 95 65-130ND
1,1-Dichloroethene ug/kg 704756 93 10-158ND
1,1-Dichloropropene ug/kg 747756 99 68-133ND
1,2,3-Trichlorobenzene ug/kg 651756 86 27-138ND
1,2,3-Trichloropropane ug/kg 714756 94 67-130ND
1,2,4-Trichlorobenzene ug/kg 634756 84 51-134ND
1,2,4-Trimethylbenzene ug/kg 758756 95 63-13640.4
1,2-Dibromo-3-chloropropane ug/kg 670756 89 32-130ND
1,2-Dibromoethane (EDB)ug/kg 743756 98 70-130ND
1,2-Dichlorobenzene ug/kg 740756 98 69-130ND
1,2-Dichloroethane ug/kg 708756 94 59-130ND
1,2-Dichloropropane ug/kg 759756 100 70-130ND
1,3,5-Trimethylbenzene ug/kg 726756 95 65-13710.9
1,3-Dichlorobenzene ug/kg 731756 97 70-130ND
1,3-Dichloropropane ug/kg 753756 99 70-130ND
1,4-Dichlorobenzene ug/kg 714756 94 68-130ND
2,2-Dichloropropane ug/kg 619756 82 32-130ND
2-Butanone (MEK)ug/kg 13901510 92 10-136ND
2-Chlorotoluene ug/kg 732756 97 69-141ND
2-Hexanone ug/kg 14401510 95 10-144ND
4-Chlorotoluene ug/kg 751756 99 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 14501510 96 25-143ND
Acetone ug/kg 11601510 76 10-130ND
Benzene ug/kg 773756 102 67-130ND
REPORT OF LABORATORY ANALYSIS
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Page 17 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3183975MATRIX SPIKE SAMPLE:
MSSpike
Result
92525426003
Bromobenzene ug/kg 722756 95 70-130ND
Bromochloromethane ug/kg 789756 104 69-134ND
Bromodichloromethane ug/kg 665756 88 64-130ND
Bromoform ug/kg 673756 89 62-130ND
Bromomethane ug/kg 664 IH,IK75688 20-176ND
Carbon tetrachloride ug/kg 684756 90 65-140ND
Chlorobenzene ug/kg 731756 97 70-130ND
Chloroethane ug/kg 209756 28 10-130ND
Chloroform ug/kg 748756 99 63-130ND
Chloromethane ug/kg 906756 120 58-130ND
cis-1,2-Dichloroethene ug/kg 745756 98 66-130ND
cis-1,3-Dichloropropene ug/kg 686756 91 67-130ND
Dibromochloromethane ug/kg 697756 92 67-130ND
Dibromomethane ug/kg 720756 95 63-131ND
Dichlorodifluoromethane ug/kg 778756 103 44-180ND
Diisopropyl ether ug/kg 691756 91 63-130ND
Ethylbenzene ug/kg 789756 101 66-13021.4
Hexachloro-1,3-butadiene ug/kg 666 IK75688 64-150ND
Isopropylbenzene (Cumene)ug/kg 732756 97 69-135ND
m&p-Xylene ug/kg 15401510 96 60-13385.1
Methyl-tert-butyl ether ug/kg 711756 94 65-130ND
Methylene Chloride ug/kg 785756 104 61-130ND
n-Butylbenzene ug/kg 712756 94 65-140ND
n-Propylbenzene ug/kg 745756 98 67-140ND
Naphthalene ug/kg 678756 89 15-145ND
o-Xylene ug/kg 783756 96 66-13353.3
p-Isopropyltoluene ug/kg 717756 95 56-147ND
sec-Butylbenzene ug/kg 722756 95 65-139ND
Styrene ug/kg 754756 100 70-132ND
tert-Butylbenzene ug/kg 533756 70 62-135ND
Tetrachloroethene ug/kg 681756 90 70-135ND
Toluene ug/kg 835756 94 67-130124
trans-1,2-Dichloroethene ug/kg 753756 100 69-130ND
trans-1,3-Dichloropropene ug/kg 672756 89 62-130ND
Trichloroethene ug/kg 771756 102 70-135ND
Trichlorofluoromethane ug/kg 244756 32 10-130ND
Vinyl acetate ug/kg 14301510 94 53-130ND
Vinyl chloride ug/kg 773756 102 61-148ND
Xylene (Total)ug/kg 23302270 96 63-132138
1,2-Dichloroethane-d4 (S)%119 70-130
4-Bromofluorobenzene (S)%102 69-134
Toluene-d8 (S)%100 70-130
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Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92525426002
3183974SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 4.5JND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IH,IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 10.8 110.9
Hexachloro-1,3-butadiene ug/kg ND IKND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92525426002
3183974SAMPLE DUPLICATE:
m&p-Xylene ug/kg 5.7JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg 7.4J8.3
Naphthalene ug/kg 23.4 725.2
o-Xylene ug/kg 8.0 38.2
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg 8JND
1,2-Dichloroethane-d4 (S)%104104
4-Bromofluorobenzene (S)%100102
Toluene-d8 (S)%10099
REPORT OF LABORATORY ANALYSIS
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Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604364
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92525426001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3184176
Associated Lab Samples:92525426001
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 03/05/21 10:54
n-Pentacosane (S)%91 32-130 03/05/21 10:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3184177LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 61.067.3 91 47-130
n-Pentacosane (S)%83 32-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3184178MATRIX SPIKE SAMPLE:
MSSpike
Result
92523987001
Diesel Range Organics(C10-C28)mg/kg 77.081.4 92 10-133ND
n-Pentacosane (S)%85 32-130
Parameter Units
Dup
Result QualifiersRPDResult
92525426001
3184179SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg NDND
n-Pentacosane (S)%7888
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Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604027
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92525426001
Parameter Units
Dup
Result QualifiersRPDResult
92524822001
3182241SAMPLE DUPLICATE:
Percent Moisture %13.5 N2113.4
Parameter Units
Dup
Result QualifiersRPDResult
92524937002
3182242SAMPLE DUPLICATE:
Percent Moisture %50.2 N21344.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604051
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92525426002, 92525426003, 92525426004
Parameter Units
Dup
Result QualifiersRPDResult
92524820002
3182456SAMPLE DUPLICATE:
Percent Moisture %17.5 N22121.7
Parameter Units
Dup
Result QualifiersRPDResult
92525352001
3182457SAMPLE DUPLICATE:
Percent Moisture %22.4 N2423.3
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 23 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604056
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92525426005
Parameter Units
Dup
Result QualifiersRPDResult
92525426005
3182496SAMPLE DUPLICATE:
Percent Moisture %29.3 N2129.0
Parameter Units
Dup
Result QualifiersRPDResult
92525494010
3182497SAMPLE DUPLICATE:
Percent Moisture %19.8 N2320.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 04:25 PM
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Huntersville, NC 28078
[phone]
Page 24 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 25 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92525426
SHEETZ STORE 356
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92525426001 604364 604549KEROSENE DISPENSER 17-2 EPA 3546 EPA 8015C Modified
92525426002 604347 604386PRODUCT LINE 18-2 EPA 5035A/5030B EPA 8260D
92525426003 604347 604386DISPENSER 5-2 EPA 5035A/5030B EPA 8260D
92525426004 604347 604386DISPENSER 9-2 EPA 5035A/5030B EPA 8260D
92525426005 604347 604386PRODUCT LINE 10-2 EPA 5035A/5030B EPA 8260D
92525426001 604027KEROSENE DISPENSER 17-2 SW-846
92525426002 604051PRODUCT LINE 18-2 SW-846
92525426003 604051DISPENSER 5-2 SW-846
92525426004 604051DISPENSER 9-2 SW-846
92525426005 604056PRODUCT LINE 10-2 SW-846
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 26 of 29
Page 27 of 29
Page 28 of 29
Page 29 of 29
#=CL#
March 16, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92526497
92526497
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
Sheetz 356
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on March 09, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc: Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92526497
Sheetz 356
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92526497
Sheetz 356
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92526497001 Dispenser 9-3 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92526497002 Product Line 10-3 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
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Page 3 of 21
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92526497
Sheetz 356
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92526497001 Dispenser 9-3
Isopropylbenzene (Cumene)11.7 ug/kg 03/11/21 16:348.4EPA 8260D
Percent Moisture 25.0 %03/09/21 16:51 N20.10SW-846
92526497002 Product Line 10-3
Benzene 19.2 ug/kg 03/11/21 16:528.7EPA 8260D
Diisopropyl ether 10.3 ug/kg 03/11/21 16:528.7EPA 8260D
Percent Moisture 26.0 %03/09/21 16:51 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
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Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92526497
Sheetz 356
Sample: Dispenser 9-3 Lab ID: 92526497001 Collected: 03/08/21 15:32 Received: 03/09/21 10:23 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/11/21 16:34 67-64-103/11/21 15:55168 1
Benzene ND ug/kg 03/11/21 16:34 71-43-203/11/21 15:558.4 1
Bromobenzene ND ug/kg 03/11/21 16:34 108-86-103/11/21 15:558.4 1
Bromochloromethane ND ug/kg 03/11/21 16:34 74-97-503/11/21 15:558.4 1
Bromodichloromethane ND ug/kg 03/11/21 16:34 75-27-403/11/21 15:558.4 1
Bromoform ND ug/kg 03/11/21 16:34 75-25-203/11/21 15:558.4 1
Bromomethane ND ug/kg 03/11/21 16:34 74-83-9 IH,IK,L1,
v103/11/21 15:5516.8 1
2-Butanone (MEK)ND ug/kg 03/11/21 16:34 78-93-303/11/21 15:55168 1
n-Butylbenzene ND ug/kg 03/11/21 16:34 104-51-803/11/21 15:558.4 1
sec-Butylbenzene ND ug/kg 03/11/21 16:34 135-98-803/11/21 15:558.4 1
tert-Butylbenzene ND ug/kg 03/11/21 16:34 98-06-603/11/21 15:558.4 1
Carbon tetrachloride ND ug/kg 03/11/21 16:34 56-23-503/11/21 15:558.4 1
Chlorobenzene ND ug/kg 03/11/21 16:34 108-90-703/11/21 15:558.4 1
Chloroethane ND ug/kg 03/11/21 16:34 75-00-303/11/21 15:5516.8 1
Chloroform ND ug/kg 03/11/21 16:34 67-66-303/11/21 15:558.4 1
Chloromethane ND ug/kg 03/11/21 16:34 74-87-303/11/21 15:5516.8 1
2-Chlorotoluene ND ug/kg 03/11/21 16:34 95-49-803/11/21 15:558.4 1
4-Chlorotoluene ND ug/kg 03/11/21 16:34 106-43-403/11/21 15:558.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/21 16:34 96-12-803/11/21 15:558.4 1
Dibromochloromethane ND ug/kg 03/11/21 16:34 124-48-103/11/21 15:558.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/21 16:34 106-93-403/11/21 15:558.4 1
Dibromomethane ND ug/kg 03/11/21 16:34 74-95-303/11/21 15:558.4 1
1,2-Dichlorobenzene ND ug/kg 03/11/21 16:34 95-50-103/11/21 15:558.4 1
1,3-Dichlorobenzene ND ug/kg 03/11/21 16:34 541-73-103/11/21 15:558.4 1
1,4-Dichlorobenzene ND ug/kg 03/11/21 16:34 106-46-703/11/21 15:558.4 1
Dichlorodifluoromethane ND ug/kg 03/11/21 16:34 75-71-803/11/21 15:5516.8 1
1,1-Dichloroethane ND ug/kg 03/11/21 16:34 75-34-303/11/21 15:558.4 1
1,2-Dichloroethane ND ug/kg 03/11/21 16:34 107-06-203/11/21 15:558.4 1
1,1-Dichloroethene ND ug/kg 03/11/21 16:34 75-35-403/11/21 15:558.4 1
cis-1,2-Dichloroethene ND ug/kg 03/11/21 16:34 156-59-203/11/21 15:558.4 1
trans-1,2-Dichloroethene ND ug/kg 03/11/21 16:34 156-60-503/11/21 15:558.4 1
1,2-Dichloropropane ND ug/kg 03/11/21 16:34 78-87-503/11/21 15:558.4 1
1,3-Dichloropropane ND ug/kg 03/11/21 16:34 142-28-903/11/21 15:558.4 1
2,2-Dichloropropane ND ug/kg 03/11/21 16:34 594-20-703/11/21 15:558.4 1
1,1-Dichloropropene ND ug/kg 03/11/21 16:34 563-58-603/11/21 15:558.4 1
cis-1,3-Dichloropropene ND ug/kg 03/11/21 16:34 10061-01-503/11/21 15:558.4 1
trans-1,3-Dichloropropene ND ug/kg 03/11/21 16:34 10061-02-603/11/21 15:558.4 1
Diisopropyl ether ND ug/kg 03/11/21 16:34 108-20-303/11/21 15:558.4 1
Ethylbenzene ND ug/kg 03/11/21 16:34 100-41-403/11/21 15:558.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/21 16:34 87-68-3 IK03/11/21 15:5516.8 1
2-Hexanone ND ug/kg 03/11/21 16:34 591-78-603/11/21 15:5583.8 1
Isopropylbenzene (Cumene)11.7 ug/kg 03/11/21 16:34 98-82-803/11/21 15:558.4 1
p-Isopropyltoluene ND ug/kg 03/11/21 16:34 99-87-603/11/21 15:558.4 1
Methylene Chloride ND ug/kg 03/11/21 16:34 75-09-203/11/21 15:5533.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92526497
Sheetz 356
Sample: Dispenser 9-3 Lab ID: 92526497001 Collected: 03/08/21 15:32 Received: 03/09/21 10:23 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/21 16:34 108-10-103/11/21 15:5583.8 1
Methyl-tert-butyl ether ND ug/kg 03/11/21 16:34 1634-04-403/11/21 15:558.4 1
Naphthalene ND ug/kg 03/11/21 16:34 91-20-303/11/21 15:558.4 1
n-Propylbenzene ND ug/kg 03/11/21 16:34 103-65-103/11/21 15:558.4 1
Styrene ND ug/kg 03/11/21 16:34 100-42-503/11/21 15:558.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/21 16:34 630-20-603/11/21 15:558.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/21 16:34 79-34-503/11/21 15:558.4 1
Tetrachloroethene ND ug/kg 03/11/21 16:34 127-18-403/11/21 15:558.4 1
Toluene ND ug/kg 03/11/21 16:34 108-88-303/11/21 15:558.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/21 16:34 87-61-603/11/21 15:558.4 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/21 16:34 120-82-103/11/21 15:558.4 1
1,1,1-Trichloroethane ND ug/kg 03/11/21 16:34 71-55-603/11/21 15:558.4 1
1,1,2-Trichloroethane ND ug/kg 03/11/21 16:34 79-00-503/11/21 15:558.4 1
Trichloroethene ND ug/kg 03/11/21 16:34 79-01-603/11/21 15:558.4 1
Trichlorofluoromethane ND ug/kg 03/11/21 16:34 75-69-403/11/21 15:558.4 1
1,2,3-Trichloropropane ND ug/kg 03/11/21 16:34 96-18-403/11/21 15:558.4 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/21 16:34 95-63-603/11/21 15:558.4 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/21 16:34 108-67-803/11/21 15:558.4 1
Vinyl acetate ND ug/kg 03/11/21 16:34 108-05-403/11/21 15:5583.8 1
Vinyl chloride ND ug/kg 03/11/21 16:34 75-01-403/11/21 15:5516.8 1
Xylene (Total)ND ug/kg 03/11/21 16:34 1330-20-703/11/21 15:5516.8 1
m&p-Xylene ND ug/kg 03/11/21 16:34 179601-23-103/11/21 15:5516.8 1
o-Xylene ND ug/kg 03/11/21 16:34 95-47-603/11/21 15:558.4 1
Surrogates
Toluene-d8 (S)100 %03/11/21 16:34 2037-26-503/11/21 15:5570-130 1
4-Bromofluorobenzene (S)96 %03/11/21 16:34 460-00-403/11/21 15:5569-134 1
1,2-Dichloroethane-d4 (S)108 %03/11/21 16:34 17060-07-003/11/21 15:5570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.0 %03/09/21 16:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92526497
Sheetz 356
Sample: Product Line 10-3 Lab ID: 92526497002 Collected: 03/08/21 14:57 Received: 03/09/21 10:23 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 03/11/21 16:52 67-64-103/11/21 15:55174 1
Benzene 19.2 ug/kg 03/11/21 16:52 71-43-203/11/21 15:558.7 1
Bromobenzene ND ug/kg 03/11/21 16:52 108-86-103/11/21 15:558.7 1
Bromochloromethane ND ug/kg 03/11/21 16:52 74-97-503/11/21 15:558.7 1
Bromodichloromethane ND ug/kg 03/11/21 16:52 75-27-403/11/21 15:558.7 1
Bromoform ND ug/kg 03/11/21 16:52 75-25-203/11/21 15:558.7 1
Bromomethane ND ug/kg 03/11/21 16:52 74-83-9 IH,IK,L1,
v103/11/21 15:5517.4 1
2-Butanone (MEK)ND ug/kg 03/11/21 16:52 78-93-303/11/21 15:55174 1
n-Butylbenzene ND ug/kg 03/11/21 16:52 104-51-803/11/21 15:558.7 1
sec-Butylbenzene ND ug/kg 03/11/21 16:52 135-98-803/11/21 15:558.7 1
tert-Butylbenzene ND ug/kg 03/11/21 16:52 98-06-6 v203/11/21 15:558.7 1
Carbon tetrachloride ND ug/kg 03/11/21 16:52 56-23-503/11/21 15:558.7 1
Chlorobenzene ND ug/kg 03/11/21 16:52 108-90-703/11/21 15:558.7 1
Chloroethane ND ug/kg 03/11/21 16:52 75-00-303/11/21 15:5517.4 1
Chloroform ND ug/kg 03/11/21 16:52 67-66-303/11/21 15:558.7 1
Chloromethane ND ug/kg 03/11/21 16:52 74-87-303/11/21 15:5517.4 1
2-Chlorotoluene ND ug/kg 03/11/21 16:52 95-49-803/11/21 15:558.7 1
4-Chlorotoluene ND ug/kg 03/11/21 16:52 106-43-403/11/21 15:558.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/11/21 16:52 96-12-803/11/21 15:558.7 1
Dibromochloromethane ND ug/kg 03/11/21 16:52 124-48-103/11/21 15:558.7 1
1,2-Dibromoethane (EDB)ND ug/kg 03/11/21 16:52 106-93-403/11/21 15:558.7 1
Dibromomethane ND ug/kg 03/11/21 16:52 74-95-303/11/21 15:558.7 1
1,2-Dichlorobenzene ND ug/kg 03/11/21 16:52 95-50-103/11/21 15:558.7 1
1,3-Dichlorobenzene ND ug/kg 03/11/21 16:52 541-73-103/11/21 15:558.7 1
1,4-Dichlorobenzene ND ug/kg 03/11/21 16:52 106-46-703/11/21 15:558.7 1
Dichlorodifluoromethane ND ug/kg 03/11/21 16:52 75-71-803/11/21 15:5517.4 1
1,1-Dichloroethane ND ug/kg 03/11/21 16:52 75-34-303/11/21 15:558.7 1
1,2-Dichloroethane ND ug/kg 03/11/21 16:52 107-06-203/11/21 15:558.7 1
1,1-Dichloroethene ND ug/kg 03/11/21 16:52 75-35-403/11/21 15:558.7 1
cis-1,2-Dichloroethene ND ug/kg 03/11/21 16:52 156-59-203/11/21 15:558.7 1
trans-1,2-Dichloroethene ND ug/kg 03/11/21 16:52 156-60-503/11/21 15:558.7 1
1,2-Dichloropropane ND ug/kg 03/11/21 16:52 78-87-503/11/21 15:558.7 1
1,3-Dichloropropane ND ug/kg 03/11/21 16:52 142-28-903/11/21 15:558.7 1
2,2-Dichloropropane ND ug/kg 03/11/21 16:52 594-20-703/11/21 15:558.7 1
1,1-Dichloropropene ND ug/kg 03/11/21 16:52 563-58-603/11/21 15:558.7 1
cis-1,3-Dichloropropene ND ug/kg 03/11/21 16:52 10061-01-503/11/21 15:558.7 1
trans-1,3-Dichloropropene ND ug/kg 03/11/21 16:52 10061-02-603/11/21 15:558.7 1
Diisopropyl ether 10.3 ug/kg 03/11/21 16:52 108-20-303/11/21 15:558.7 1
Ethylbenzene ND ug/kg 03/11/21 16:52 100-41-403/11/21 15:558.7 1
Hexachloro-1,3-butadiene ND ug/kg 03/11/21 16:52 87-68-3 IK03/11/21 15:5517.4 1
2-Hexanone ND ug/kg 03/11/21 16:52 591-78-603/11/21 15:5586.9 1
Isopropylbenzene (Cumene)ND ug/kg 03/11/21 16:52 98-82-803/11/21 15:558.7 1
p-Isopropyltoluene ND ug/kg 03/11/21 16:52 99-87-603/11/21 15:558.7 1
Methylene Chloride ND ug/kg 03/11/21 16:52 75-09-203/11/21 15:5534.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92526497
Sheetz 356
Sample: Product Line 10-3 Lab ID: 92526497002 Collected: 03/08/21 14:57 Received: 03/09/21 10:23 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/11/21 16:52 108-10-103/11/21 15:5586.9 1
Methyl-tert-butyl ether ND ug/kg 03/11/21 16:52 1634-04-403/11/21 15:558.7 1
Naphthalene ND ug/kg 03/11/21 16:52 91-20-303/11/21 15:558.7 1
n-Propylbenzene ND ug/kg 03/11/21 16:52 103-65-103/11/21 15:558.7 1
Styrene ND ug/kg 03/11/21 16:52 100-42-503/11/21 15:558.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/11/21 16:52 630-20-603/11/21 15:558.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/11/21 16:52 79-34-503/11/21 15:558.7 1
Tetrachloroethene ND ug/kg 03/11/21 16:52 127-18-403/11/21 15:558.7 1
Toluene ND ug/kg 03/11/21 16:52 108-88-303/11/21 15:558.7 1
1,2,3-Trichlorobenzene ND ug/kg 03/11/21 16:52 87-61-603/11/21 15:558.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/11/21 16:52 120-82-103/11/21 15:558.7 1
1,1,1-Trichloroethane ND ug/kg 03/11/21 16:52 71-55-603/11/21 15:558.7 1
1,1,2-Trichloroethane ND ug/kg 03/11/21 16:52 79-00-503/11/21 15:558.7 1
Trichloroethene ND ug/kg 03/11/21 16:52 79-01-603/11/21 15:558.7 1
Trichlorofluoromethane ND ug/kg 03/11/21 16:52 75-69-403/11/21 15:558.7 1
1,2,3-Trichloropropane ND ug/kg 03/11/21 16:52 96-18-403/11/21 15:558.7 1
1,2,4-Trimethylbenzene ND ug/kg 03/11/21 16:52 95-63-603/11/21 15:558.7 1
1,3,5-Trimethylbenzene ND ug/kg 03/11/21 16:52 108-67-803/11/21 15:558.7 1
Vinyl acetate ND ug/kg 03/11/21 16:52 108-05-403/11/21 15:5586.9 1
Vinyl chloride ND ug/kg 03/11/21 16:52 75-01-403/11/21 15:5517.4 1
Xylene (Total)ND ug/kg 03/11/21 16:52 1330-20-703/11/21 15:5517.4 1
m&p-Xylene ND ug/kg 03/11/21 16:52 179601-23-103/11/21 15:5517.4 1
o-Xylene ND ug/kg 03/11/21 16:52 95-47-603/11/21 15:558.7 1
Surrogates
Toluene-d8 (S)100 %03/11/21 16:52 2037-26-503/11/21 15:5570-130 1
4-Bromofluorobenzene (S)95 %03/11/21 16:52 460-00-403/11/21 15:5569-134 1
1,2-Dichloroethane-d4 (S)107 %03/11/21 16:52 17060-07-003/11/21 15:5570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.0 %03/09/21 16:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606023
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92526497001, 92526497002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3192814
Associated Lab Samples:92526497001, 92526497002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/11/21 13:56
1,1,1-Trichloroethane ug/kg ND 5.0 03/11/21 13:56
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/11/21 13:56
1,1,2-Trichloroethane ug/kg ND 5.0 03/11/21 13:56
1,1-Dichloroethane ug/kg ND 5.0 03/11/21 13:56
1,1-Dichloroethene ug/kg ND 5.0 03/11/21 13:56
1,1-Dichloropropene ug/kg ND 5.0 03/11/21 13:56
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/11/21 13:56
1,2,3-Trichloropropane ug/kg ND 5.0 03/11/21 13:56
1,2,4-Trichlorobenzene ug/kg ND 5.0 03/11/21 13:56
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/11/21 13:56
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/11/21 13:56
1,2-Dibromoethane (EDB)ug/kg ND 5.0 03/11/21 13:56
1,2-Dichlorobenzene ug/kg ND 5.0 03/11/21 13:56
1,2-Dichloroethane ug/kg ND 5.0 03/11/21 13:56
1,2-Dichloropropane ug/kg ND 5.0 03/11/21 13:56
1,3,5-Trimethylbenzene ug/kg ND 5.0 03/11/21 13:56
1,3-Dichlorobenzene ug/kg ND 5.0 03/11/21 13:56
1,3-Dichloropropane ug/kg ND 5.0 03/11/21 13:56
1,4-Dichlorobenzene ug/kg ND 5.0 03/11/21 13:56
2,2-Dichloropropane ug/kg ND 5.0 03/11/21 13:56
2-Butanone (MEK)ug/kg ND 100 03/11/21 13:56
2-Chlorotoluene ug/kg ND 5.0 03/11/21 13:56
2-Hexanone ug/kg ND 50.0 03/11/21 13:56
4-Chlorotoluene ug/kg ND 5.0 03/11/21 13:56
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 03/11/21 13:56
Acetone ug/kg ND 100 03/11/21 13:56
Benzene ug/kg ND 5.0 03/11/21 13:56
Bromobenzene ug/kg ND 5.0 03/11/21 13:56
Bromochloromethane ug/kg ND 5.0 03/11/21 13:56
Bromodichloromethane ug/kg ND 5.0 03/11/21 13:56
Bromoform ug/kg ND 5.0 03/11/21 13:56
Bromomethane ug/kg ND 10.0 IH,IK,v103/11/21 13:56
Carbon tetrachloride ug/kg ND 5.0 03/11/21 13:56
Chlorobenzene ug/kg ND 5.0 03/11/21 13:56
Chloroethane ug/kg ND 10.0 03/11/21 13:56
Chloroform ug/kg ND 5.0 03/11/21 13:56
Chloromethane ug/kg ND 10.0 03/11/21 13:56
cis-1,2-Dichloroethene ug/kg ND 5.0 03/11/21 13:56
cis-1,3-Dichloropropene ug/kg ND 5.0 03/11/21 13:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3192814
Associated Lab Samples:92526497001, 92526497002
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 03/11/21 13:56
Dibromomethane ug/kg ND 5.0 03/11/21 13:56
Dichlorodifluoromethane ug/kg ND 10.0 03/11/21 13:56
Diisopropyl ether ug/kg ND 5.0 03/11/21 13:56
Ethylbenzene ug/kg ND 5.0 03/11/21 13:56
Hexachloro-1,3-butadiene ug/kg ND 10.0 IK03/11/21 13:56
Isopropylbenzene (Cumene)ug/kg ND 5.0 03/11/21 13:56
m&p-Xylene ug/kg ND 10.0 03/11/21 13:56
Methyl-tert-butyl ether ug/kg ND 5.0 03/11/21 13:56
Methylene Chloride ug/kg ND 20.0 03/11/21 13:56
n-Butylbenzene ug/kg ND 5.0 03/11/21 13:56
n-Propylbenzene ug/kg ND 5.0 03/11/21 13:56
Naphthalene ug/kg ND 5.0 03/11/21 13:56
o-Xylene ug/kg ND 5.0 03/11/21 13:56
p-Isopropyltoluene ug/kg ND 5.0 03/11/21 13:56
sec-Butylbenzene ug/kg ND 5.0 03/11/21 13:56
Styrene ug/kg ND 5.0 03/11/21 13:56
tert-Butylbenzene ug/kg ND 5.0 03/11/21 13:56
Tetrachloroethene ug/kg ND 5.0 03/11/21 13:56
Toluene ug/kg ND 5.0 03/11/21 13:56
trans-1,2-Dichloroethene ug/kg ND 5.0 03/11/21 13:56
trans-1,3-Dichloropropene ug/kg ND 5.0 03/11/21 13:56
Trichloroethene ug/kg ND 5.0 03/11/21 13:56
Trichlorofluoromethane ug/kg ND 5.0 03/11/21 13:56
Vinyl acetate ug/kg ND 50.0 03/11/21 13:56
Vinyl chloride ug/kg ND 10.0 03/11/21 13:56
Xylene (Total)ug/kg ND 10.0 03/11/21 13:56
1,2-Dichloroethane-d4 (S)%111 70-130 03/11/21 13:56
4-Bromofluorobenzene (S)%96 69-134 03/11/21 13:56
Toluene-d8 (S)%101 70-130 03/11/21 13:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3192815LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,1-Trichloroethane ug/kg 11401250 91 70-130
1,1,2,2-Tetrachloroethane ug/kg 12601250 101 70-130
1,1,2-Trichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethane ug/kg 11201250 89 70-130
1,1-Dichloroethene ug/kg 11601250 93 70-130
1,1-Dichloropropene ug/kg 11401250 91 70-130
1,2,3-Trichlorobenzene ug/kg 12601250 101 65-130
1,2,3-Trichloropropane ug/kg 13001250 104 70-130
1,2,4-Trichlorobenzene ug/kg 12801250 102 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3192815LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12901250 103 70-130
1,2-Dibromo-3-chloropropane ug/kg 13601250 109 70-130
1,2-Dibromoethane (EDB)ug/kg 13001250 104 70-130
1,2-Dichlorobenzene ug/kg 13201250 106 70-130
1,2-Dichloroethane ug/kg 10901250 88 63-130
1,2-Dichloropropane ug/kg 12201250 97 70-130
1,3,5-Trimethylbenzene ug/kg 12601250 101 70-130
1,3-Dichlorobenzene ug/kg 12801250 102 70-130
1,3-Dichloropropane ug/kg 12701250 102 70-130
1,4-Dichlorobenzene ug/kg 12801250 102 70-130
2,2-Dichloropropane ug/kg 12201250 97 66-130
2-Butanone (MEK)ug/kg 23802500 95 70-130
2-Chlorotoluene ug/kg 12901250 103 70-130
2-Hexanone ug/kg 26502500 106 70-130
4-Chlorotoluene ug/kg 13201250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24702500 99 70-130
Acetone ug/kg 24302500 97 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 12701250 102 70-130
Bromochloromethane ug/kg 12501250 100 70-130
Bromodichloromethane ug/kg 11301250 90 69-130
Bromoform ug/kg 13601250 109 70-130
Bromomethane ug/kg 1640 IH,IK,L1,v11250132 52-130
Carbon tetrachloride ug/kg 11401250 91 70-130
Chlorobenzene ug/kg 12601250 101 70-130
Chloroethane ug/kg 11501250 92 65-130
Chloroform ug/kg 11501250 92 70-130
Chloromethane ug/kg 11301250 90 55-130
cis-1,2-Dichloroethene ug/kg 11201250 89 70-130
cis-1,3-Dichloropropene ug/kg 12301250 98 70-130
Dibromochloromethane ug/kg 13201250 105 70-130
Dibromomethane ug/kg 12601250 101 70-130
Dichlorodifluoromethane ug/kg 10901250 87 45-156
Diisopropyl ether ug/kg 10801250 87 70-130
Ethylbenzene ug/kg 13101250 105 70-130
Hexachloro-1,3-butadiene ug/kg 1370 IK1250110 66-130
Isopropylbenzene (Cumene)ug/kg 12801250 103 70-130
m&p-Xylene ug/kg 24902500 100 70-130
Methyl-tert-butyl ether ug/kg 11301250 90 70-130
Methylene Chloride ug/kg 11401250 91 65-130
n-Butylbenzene ug/kg 13001250 104 67-130
n-Propylbenzene ug/kg 13201250 105 70-130
Naphthalene ug/kg 12901250 103 70-130
o-Xylene ug/kg 12801250 102 70-130
p-Isopropyltoluene ug/kg 12901250 103 67-130
sec-Butylbenzene ug/kg 12701250 102 69-130
Styrene ug/kg 13101250 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3192815LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 9401250 75 67-130
Tetrachloroethene ug/kg 12601250 101 70-130
Toluene ug/kg 11501250 92 70-130
trans-1,2-Dichloroethene ug/kg 11701250 94 70-130
trans-1,3-Dichloropropene ug/kg 12101250 97 68-130
Trichloroethene ug/kg 12201250 98 70-130
Trichlorofluoromethane ug/kg 11801250 94 70-130
Vinyl acetate ug/kg 27602500 110 70-130
Vinyl chloride ug/kg 11301250 91 61-130
Xylene (Total)ug/kg 37703750 100 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3192817MATRIX SPIKE SAMPLE:
MSSpike
Result
92526497002
1,1,1,2-Tetrachloroethane ug/kg 857869 99 70-131ND
1,1,1-Trichloroethane ug/kg 847869 97 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 853869 98 66-130ND
1,1,2-Trichloroethane ug/kg 879869 101 66-133ND
1,1-Dichloroethane ug/kg 785869 90 65-130ND
1,1-Dichloroethene ug/kg 671869 77 10-158ND
1,1-Dichloropropene ug/kg 867869 100 68-133ND
1,2,3-Trichlorobenzene ug/kg 937869 108 27-138ND
1,2,3-Trichloropropane ug/kg 851869 98 67-130ND
1,2,4-Trichlorobenzene ug/kg 1000869 116 51-134ND
1,2,4-Trimethylbenzene ug/kg 930869 107 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 815869 94 32-130ND
1,2-Dibromoethane (EDB)ug/kg 859869 99 70-130ND
1,2-Dichlorobenzene ug/kg 951869 109 69-130ND
1,2-Dichloroethane ug/kg 768869 88 59-130ND
1,2-Dichloropropane ug/kg 884869 102 70-130ND
1,3,5-Trimethylbenzene ug/kg 923869 106 65-137ND
1,3-Dichlorobenzene ug/kg 953869 110 70-130ND
1,3-Dichloropropane ug/kg 871869 100 70-130ND
1,4-Dichlorobenzene ug/kg 918869 106 68-130ND
2,2-Dichloropropane ug/kg 914869 105 32-130ND
2-Butanone (MEK)ug/kg 14401740 83 10-136ND
2-Chlorotoluene ug/kg 916869 105 69-141ND
2-Hexanone ug/kg 7871740 45 10-144ND
4-Chlorotoluene ug/kg 945869 109 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 15801740 91 25-143ND
Acetone ug/kg 11501740 66 10-130ND
Benzene ug/kg 900869 101 67-13019.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3192817MATRIX SPIKE SAMPLE:
MSSpike
Result
92526497002
Bromobenzene ug/kg 864869 99 70-130ND
Bromochloromethane ug/kg 862869 99 69-134ND
Bromodichloromethane ug/kg 785869 90 64-130ND
Bromoform ug/kg 852869 98 62-130ND
Bromomethane ug/kg 886 IH,IK,v1869102 20-176ND
Carbon tetrachloride ug/kg 859869 99 65-140ND
Chlorobenzene ug/kg 911869 105 70-130ND
Chloroethane ug/kg 259869 30 10-130ND
Chloroform ug/kg 845869 97 63-130ND
Chloromethane ug/kg 1070869 124 58-130ND
cis-1,2-Dichloroethene ug/kg 828869 95 66-130ND
cis-1,3-Dichloropropene ug/kg 845869 97 67-130ND
Dibromochloromethane ug/kg 845869 97 67-130ND
Dibromomethane ug/kg 827869 95 63-131ND
Dichlorodifluoromethane ug/kg 978869 113 44-180ND
Diisopropyl ether ug/kg 788869 89 63-13010.3
Ethylbenzene ug/kg 943869 109 66-130ND
Hexachloro-1,3-butadiene ug/kg 1170 IK869135 64-150ND
Isopropylbenzene (Cumene)ug/kg 960869 111 69-135ND
m&p-Xylene ug/kg 18401740 106 60-133ND
Methyl-tert-butyl ether ug/kg 821869 94 65-130ND
Methylene Chloride ug/kg 965869 111 61-130ND
n-Butylbenzene ug/kg 1040869 119 65-140ND
n-Propylbenzene ug/kg 974869 112 67-140ND
Naphthalene ug/kg 858869 99 15-145ND
o-Xylene ug/kg 939869 108 66-133ND
p-Isopropyltoluene ug/kg 1000869 116 56-147ND
sec-Butylbenzene ug/kg 993869 114 65-139ND
Styrene ug/kg 924869 106 70-132ND
tert-Butylbenzene ug/kg 702 v286981 62-135ND
Tetrachloroethene ug/kg 931869 107 70-135ND
Toluene ug/kg 852869 98 67-130ND
trans-1,2-Dichloroethene ug/kg 878869 101 69-130ND
trans-1,3-Dichloropropene ug/kg 800869 92 62-130ND
Trichloroethene ug/kg 919869 106 70-135ND
Trichlorofluoromethane ug/kg 306869 35 10-130ND
Vinyl acetate ug/kg 17401740 100 53-130ND
Vinyl chloride ug/kg 887869 102 61-148ND
Xylene (Total)ug/kg 27802610 107 63-132ND
1,2-Dichloroethane-d4 (S)%117 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92526497001
3192816SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg 8.6ND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg ND IKND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 6.8JND
Hexachloro-1,3-butadiene ug/kg ND IKND
Isopropylbenzene (Cumene)ug/kg 10.8 811.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92526497001
3192816SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%94108
4-Bromofluorobenzene (S)%10696
Toluene-d8 (S)%98100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92526497
Sheetz 356
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
605321
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92526497001, 92526497002
Parameter Units
Dup
Result QualifiersRPDResult
92526131001
3189146SAMPLE DUPLICATE:
Percent Moisture %12.7 N2613.5
Parameter Units
Dup
Result QualifiersRPDResult
92526497002
3189147SAMPLE DUPLICATE:
Percent Moisture %26.9 N2326.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92526497
Sheetz 356
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92526497
Sheetz 356
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92526497001 606023 606063Dispenser 9-3 EPA 5035A/5030B EPA 8260D
92526497002 606023 606063Product Line 10-3 EPA 5035A/5030B EPA 8260D
92526497001 605321Dispenser 9-3 SW-846
92526497002 605321Product Line 10-3 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2021 07:56 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
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