WS-28426_47682_CA_IAAR_20210521_spill_IAAR

Initial Abatement Measures Report
Diesel Fuel Release – Circle K Store #2701526
Colfax, North Carolina
Page 2
B. Site History and Characterization
The subject property is a Circle K Store #2701526 located at 8400 Norcross Road, Colfax; Guilford County,
North Carolina. Please reference Figure 1 for depiction of site location. A topographic map of the site and
surrounding area is included as Figure 2. An aerial photograph of the site is included as Figure 3 in
Appendix A.
Highlands Environmental Solutions, Inc. (HES) was initially contacted by Circle K at 15:00 hours on March
29, 2021, and was advised that there had been a release of diesel fuel at the site. The release reportedly
occurred from the fill port of an underground storage tank (UST) that is located at the site. The cause of the
release was due to a malfunction of the submersible turbine pump motor to UST #7. This motor failure
caused the UST to pressurize, and fuel was expelled from the fill port to the ground surface. It should be
noted that this UST is manifolded to a second 20,000 gallon diesel fuel UST. The UST information is
presented in Table 1 and Table 2, included in Appendix B.
The site is located in a developed area of residential and commercial land uses. Surface water bodies are
not located near the subject property. The subject and surrounding properties utilize city water for drinking
water.
A small area of petroleum-impacted soil was discovered adjacent to the subject UST on March 29, 2021.
Once the release was contained, HES personnel inspected the off-site stormwater drainage features
located to the West and North of the release location and diesel fuel was not observed in these areas. HES
reported to the North Carolina Department of Environmental Quality (NCDEQ) and Guilford County
Environmental Health Department (GCEHD) on March 30, 2021. HES also prepared a site-specific health
and safety plan (HASP) to ensure the safety of the personnel. A copy of the HASP is included in Appendix
C.
C. Initial Response and Abatement Activities
On March 29, 2021, HES was advised that there had been a release of diesel fuel at the subject site. Store
personnel indicated that the release occurred unexpectedly from UST #7, which is connected to UST #6
via a manifold. Due to a suspected malfunction to the tank’s submersible pump motor, the UST system
pressurized and diesel fuel was ejected from the fill port from UST #7. The released fuel impacted the
paved surfaces around UST basin, and pooled in a downgradient stormwater inlet. A diagram depicting the
locations of the UST location is included as Figure 4.
HES contracted Zebra Environmental and Industrial Services (ZES) to provide emergency response
support. ZES and HES personnel mobilized to the site on March 29, 2021, and applied granular absorbents
during initial response activities. Once the release was contained, HES and ZES personnel inspected for
further impact of diesel fuel beyond the impacted stormwater inlet. A concrete culvert pipe adjacent to the
impacted stormwater drain was not impacted by the release. The residual diesel fuel was contained within
the sump of the impacted stormwater inlet. On March 29, 2021, a vacuum truck was utilized to recover the
diesel fuel contained in the stormwater inlet and the granular absorbents used at the site. The stormwater
inlet was flushed, and cleaned, while a vacuum truck was used to recover all waste materials.
Approximately 981 gallons of diesel fuel/water mixture was recovered and transported for disposal by
ZES during site response activities.
In addition to the impacted stormwater drain, diesel fuel was observed to have seeped under the concrete
curb and impacted a small area of soil. Impacted soils were observed, measuring approximately thirteen
feet long by eight foot wide and varying from three feet to four feet deep near the concrete curb and
stormwater inlet.
On March 30, 2021, absorbent booms were placed at the concrete culvert pipe and in the off-site stormwater
drainage feature as a precautionary measure from rain events pending excavation activities.
Initial Abatement Measures Report
Diesel Fuel Release Incident; 8400 Norcross Road; Colfax, NC
Page 3
HES and ZES personnel were on-site to conduct soil excavation activities in the impacted area on April 15,
2021. A diagram depicting the excavation and samples collection is included as Figure 4. As excavation
proceeded, a total of fifteen soil samples were collected and screened for organic vapors using a
photoionization detector (PID – MiniRae 3000). To field screen the samples, an aliquot of soil was placed
in a clean, labeled, zip-lock bag and allowed to volatilize in direct sunlight for approximately 10 minutes. At
the end of the volatilization period, the sampling probe for the PID was inserted into the bag to screen for
the presence of organic vapors. Field screening data were utilized to determine the horizontal and vertical
extents of the excavated areas.
Following completion of soil excavation activities, a total of eight post-excavation confirmation samples (S-
1 through S-8) were collected from the excavated area. Upon collection, the samples were placed in
labeled, pre-preserved, laboratory-supplied containers, and maintained on ice pending delivery to the
analytical laboratory. These samples were shipped via overnight courier to Waypoint analytical for
laboratory analysis of diesel range organics (DRO); gasoline range organics (GRO); volatile organic
compounds (VOCs) by Method 8260; semi-volatile organic compounds (SVOCs) by Method 8270; and
extractable and volatile petroleum hydrocarbons (EPH/VPH), by the MADEP method.
Laboratory analysis of the post-excavation confirmation samples did result in the detection of DRO at
concentrations greater than their respective State Action in samples S-1 and S-2 at concentrations of 445
mg/kg and 197 mg/kg, respectively. Sample S-2 also resulted in the detection of GRO at a concentration
of 54.2 mg/kg. This concentration exceeds the State Action Limit of 50 mg/kg. Low concentrations of
petroleum constituents were discovered in four of the eight soil samples collected, with the concentration
of C11-C22 Aromatics slightly exceeding the Soil-to-Water Maximum Soil Contaminant Concentrations
(MSCCs) in two samples (S-1 and S-2). Due to the risk of undermining the concrete curb and stormwater
inlet, the excavation depth at samples S-1 and S-2 were limited to four feet below surface grade. A summary
of the soil analytical data is presented in Table 3 included in Appendix B. The complete laboratory
analytical data report and chain-of-custody records for soil samples are included as Appendix D.
During excavation activities, 14.07 tons of petroleum-impacted soil were excavated and transported for
disposal by ZES during excavation activities. A PVC stormwater pipe utilized as an outfall to one of the
upgradient drains onsite was discovered during remediation activities. The open end of this stormwater that
was buried. Once exposed, stormwater trapped in the pipe was released. During soil remediation activities,
a vacuum truck was utilized to recover approximately 123 gallons of stormwater that was released to the
excavated area. Copies of the waste manifest documentations for the PCW and petroleum-impacted soil
are included in Appendix E. Riprap stones were placed downgradient of the excavated area post remedial
activities. Selected photographs of the remediation activities are included in Appendix F.
D. Source Investigation
As noted above, a diesel fuel release occurred from a 20,000 gallon diesel fuel UST at the Circle K Store
#2701526 located at 8400 Norcross Road, in Colfax, Guilford County, North Carolina. Store personnel
indicated that the release occurred that the release occurred unexpectedly from UST #7, and was due to
an apparent malfunction of the submersible pump motor which caused the UST system to become
pressurized. UST #6 and UST #7 are manifold together. An estimated 50-80 gallons of diesel fuel were
released from UST #7 during this incident. After excess liquids were removed from UST #7, the
submersible turbine pump motor was replaced.
The subject site is located in an area of residential and commercial land uses in Guilford County, North
Carolina. The subject area and adjacent properties are utilized for commercial/residential land uses. The
closest surface water body is an unnamed tributary of East Fork Deep River, located approximately 1700
feet East of the subject location. Surface water bodies were neither impacted nor threatened by this
release. Public water and sewer are available to the site and surrounding areas.
The majority of the released diesel fuel was contained on paved surfaces and in a stormwater inlet. A small
volume of diesel fuel seeped under the concrete curbing, and impacted an unpaved area. This area was
Initial Abatement Measures Report
Diesel Fuel Release Incident; 8400 Norcross Road; Colfax, NC
Page 4

excavated by a track-mounted mini-excavator, and post-excavation soil samples were collected.
Laboratory analysis of soil samples S-1 and S-2 resulted in the detection of C9-C22 Aromatics at
concentrations greater than their respective Soil to Water MSCCs. However, individual petroleum
constituent concentrations did not exceed their respective Soil to Water MSCCs in any post-excavation soil
sample. Furthermore, due to the risk of undermining the concrete curb and stormwater inlet on-site, the
depth of the excavation in the area of samples S-1 and S-2 were limited to four feet below surface grade.
Groundwater was not encountered during soil sampling activities.
The site is utilized for commercial land uses, and an interstate highway is located immediately adjacent to
the area of residual petroleum-impacted soil. Individual volatile and semi-volatile petroleum compounds
were not detected at concentrations greater than their respective Soil to Water MSCCs. HES recommends
this incident could be closed by filing a Notice of Residual Petroleum on the property deed.

APPENDIX A

Drawing / Project Name
Client
Project #
DB Fig. Scale
Date
N
Base diagram from Bing Maps.
Site Location Diagram
Diesel Fuel Release Incident
Circle K Store #2701526; Colfax, NC
Circle K Stores, Inc.
186481
JBAs Shown
April 2021
1
PM PG
JB
PE
JB
Site Location
Approximate Scale 
feet
0 2070 1035 

Drawing / Project Name
Client
Project #
DB Fig. Scale
Date
N
Base diagram from USGS Topographic Quadrangle; Guilford, NC, 1997
Topographic Location Diagram
Diesel Fuel Release Incident
Circle K Store #2701526; Colfax, NC
Circle K Stores, Inc.

186481
JBAs Shown
April 2021
2
PM PG
JB
PE

JB
Incident Location
Approximate Scale 
feet
0 2540 1270 

Drawing / Project Name
Client
Project #
DB Fig. Scale
Date
N
Base diagram from Google Earth
Area Diagram
Diesel Fuel Release Incident
Circle K Store #2701526; Colfax, NC
Circle K Stores, Inc.
186481
JBAs Shown
April 2021
3
PM PG
BA
PE
Approximate Scale 
feet
0 120 60 
JB
Incident Location
(Submersible pump
failure)
Impacted
Stormwater Inlet
Extent of Diesel
Fuel Release
Release Contained
(Boom Placement)
ReleaseLocationUST #7UST #6ImpactedStormwater InletPropertyFenceConcreteCulvert PipeApproximateExcavation LimitsS-1and Driveway AreaPaved ParkingGrassAreaGrassAreaConcrete CurbPVC StormwaterPipeS-2S-3S-3S-5S-6S-7S-8I-40 Exit RampUST Fill PortsArea of ImpactedPavementApproximate Scale510feet0LegendSoil Boring LocationExcavation Depth 36 inchesPG:DB:Project Number:Date:Scale:PE:PM:Drawing NameSite / Client NameFig.Excavation and Sample Location DiagramJBBAJB186481April 2021As ShownDiesel Fuel Release IncidentColfax, NC4Circle K Store #2701526 NExcavation Depth 48 inches

APPENDIX B

Tank Number Status Installation Date Size In Gallons Tank Dimensions Last Contents1 In service 9/30/1984 10000 8' x 26.75' Premium gasoline2 In service 9/30/1984 10000 8' x 26.75' Unleaded gasoline3 In service 9/30/1984 8000 8' x 21.33' Unleaded gasoline4 In service 9/30/1984 8000 8' x 21.33' Kerosene5 In service 9/30/1984 20000 10.5' x 31' Diesel fuel6 In service 9/30/1984 20000 10.5' x 31' Diesel fuel7 In service 9/30/1984 8000 8' x 21.33' Diesel fuelCircle K #2701526; Colfax, NCHES Project #186481Table 1Underground Storage Tank InformationDiesel Fuel Release Incident
UST ID Number Name of Owner or Operator Owner or Operator
Tanks 1-7 Circle K Stores, Inc. Owner and operator
Address Telephone Number
1100 Situs Court, #100; Raleigh, NC 27606 919-744-6700
Table 2
Site History
UST Owner/Operator Information
1984 to present
Diesel Fuel Release Incident
Circle K #2701526; Colfax, NC
HES Project #186481
Dates of
Ownership/Operation
FieldSample Collection DateSample Collection (ft. BGS)S-1 4/15/2021 4.0 200.0 234450.001 0.001 0.005 0.007 CS 0.084 CS ND 110.7 49.649.5S-2 4/15/2021 4.0 108.054.2 197ND ND ND 0.001 CS 0.022 CS ND 224.8 79.596.1S-3 4/15/2021 3.0 29.0 0.096 4.56 ND ND ND ND CS ND CS ND ND ND NDS-4 4/15/2021 3.0 25.7 23 25.3 0.0007 ND ND ND CS ND CS ND 4.92 ND NDS-5 4/15/2021 3.0 18.1 0.242 35.2 0.001 ND ND 0.001 CS ND CS ND 8.58 15.7 NDS-6 4/15/2021 3.0 12.0 ND 4.18 ND ND ND ND CS ND CS ND ND ND NDS-7 4/15/2021 3.0 3.5 0.083 5.44 ND ND ND ND CS ND CS ND ND ND NDS-8 4/15/2021 3.0 4.0 0.077 10.2 ND ND ND ND CS ND CS ND ND ND ND50 1004.3 3.3 0.12 0.16 CS 270 CS 68 540 imm 31Notes:BGS denotes "below ground surface" mg/Kg denotes "miligram per kilogram" ND denotes "not detected" CS denotes "Compound Specific"BOLD denotes greater than Regulatory Reporting LimitC19-C36 AliphaticsC9-C22 AromaticsTable 3Diesel Fuel Release IncidentCircle K #2701526; Colfax, NCHES Project #186481Summary of Soil Analytical Data8270E (mg/Kg)8260D (mg/Kg)Analytical Method (e.g., VOC by EPA 8260B)5035 / 8015 (mg/Kg)EPH and VPH (mg/Kg)All Other Target CompoundsC5-C8 AliphaticsC9-C18 AliphaticsNCDEQ State Action Limit (mg/kg)NCDEQ Soil-to-Water MSCC (mg/kg)sec-Butylbenzene4-Isopropyl tolueneNaphthaleneDiesel Range Organics All Other Target CompoundsSample ID NumberConstituent of ConcernPyrenePID Screening (ppm)Gasoline Range Organics n-Butylbenzene

APPENDIX C

Highlands Environmental Solutions, Inc.

HEALTH AND SAFETY PLAN

For Site Activities at:

Soil Remediation Activities
Circle K #2701526
8400 Norcross Road; Colfax, NC

April 2021

Minimum Level of Protection at this site is Level D
Contaminants of Concern are Petroleum Hydrocarbons

Joe Beaman
Project Manager

The information in this HASP is provided solely for the protection of the health and safety of Highlands
Environmental Solutions employees and subcontractors working under the direct supervision and control of
Highlands Environmental Solutions on this project. Highlands Environmental Solutions assumes no liability
for, or responsibility to, any other parties for the accuracy or completeness of the information contained herein
for any use or reliance upon this HASP by any other party.
Health and Safety Plan Page 2
8400 Norcross Road; Colfax, NC April 2021

IN THE EVENT OF ANY EMERGENCY, CONTACT PROJECT MANAGER OR
HEALTH AND SAFETY REPRESENTATIVE
SITE EMERGENCY FORM
Contaminants of Concern: Petroleum Hydrocarbons
Minimum Level of Protection: Level D

Do not endanger your life. Survey the situation before taking any action.
Highlands Environmental Solutions Office
Telephone: [phone]
Site Location Address: Circle K – 8400 Norcross Road; Colfax, NC
Telephone Located at: HES Personnel (cellular phone)

EMERGENCY
PHONE NUMBERS

Ambulance: 911
Fire: 911
Police: 911
Hospital Name: Novant Health Kernersville Medical Center
Hospital Phone: [phone]
Project Manager: Joe Beaman
Health and Safety Specialist: Bakri Abushouk
Client Contact: Connor Branam 919-774-6700
Poison Control: [phone]
State Agency: NCDEQ (WSRO) 704-663-1699

UTILITY MARKER EMERGENCY TELEPHONE NUMBERS

Utility Color Code

Telephone Number
Water
Gas
Electric
Telephone
Cable
Sewer
Blue
Yellow
Red
Orange
Orange
Green
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Dig Safe Telephone Number: [phone]
Health and Safety Plan Page 3
8400 Norcross Road; Colfax, NC April 2021

HOSPITAL LOCATION MAP

Directions:
Head west on Norcross Road toward Lakedale Road,
Turn left onto Lakedale; Turn right onto Adkins Road;
Turn right onto Boylston Road; Turn left onto S Bunker
Hill Rd; Turn right onto Macy Grove Road; Turn left
onto Kernersville Medical Blvd.

Hospital Information:
Name: Novant Health Kernersville Medical
Center
Address: 1750 Kernersville Medical Parkway
City, State: Colfax, NC
Phone: [phone]

Health and Safety Plan Page 4
8400 Norcross Road; Colfax, NC April 2021

FIRST AID FOR PETROLEUM HYDROCARBON EMERGENCIES

Ingestion: DO NOT INDUCE VOMITING. Call Poison Control; follow instructions. Administer
cardiopulmonary resuscitation (CPR), if necessary. Seek medical attention.

Inhalation: Remove person from contaminated environment. DO NOT ENTER A CONFINED
SPACE TO RESCUE SOMEONE WHO HAS BEEN OVERCOME UNLESS
PROPERLY EQUIPPED AND A STANDBY PERSON IS PRESENT. Administer
CPR if necessary. Seek medical attention.

Skin Contact: Brush off dry material, remove wet or contaminated clothing. Flush skin thoroughly
with water. Seek medical attention if irritation persists.

Eye Contact: Flush eyes with water for 15 minutes. Seek medical attention.

Exposure Symptoms: Headache, dizziness, nausea, drowsiness, irritation of eyes, nose, throat, breathing
difficulties.

Contingency Plan: Report incident to Project Manager (PM) after emergency procedures have been
implemented.

RESPONDER MUST HAVE A CURRENT CERTIFICATE TO ADMINISTER FIRST AID OR CPR

1. Survey the situation. Do not endanger your own life. DO NOT ENTER A CONFINED SPACE TO
RESCUE SOMEONE WHO HAS BEEN OVERCOME UNLESS PROPERLY EQUIPPED AND A
STANDBY PERSON IS PRESENT.

2. Call 911 (if available) or the fire department IMMEDIATELY. Explain the physical injury, chemical
exposure, fire, or release.

3. Decontaminate the victim without delaying life-saving procedures.

4. If the victim's condition appears to be noncritical, but seems to be more severe than minor cuts,
he/she should be transported to the nearest hospital by trained Emergency Medical Services (EMS)
personnel: let the doctor assume the responsibility for determining the severity of the injury. If the
condition is obviously serious, EMS must transport the victim.

5. Notify the PM.
Health and Safety Plan Page 5
8400 Norcross Road; Colfax, NC April 2021

EMERGENCY FIRST AID PROCEDURES
To Stop Bleeding CPR

1. Give medical statement.
2. Assure airway, breathing, and
circulation.
3. Use DIRECT PRESSURE over the
wound with clean dressing or your
hand (use nonpermeable gloves).
Direct pressure will control most
bleeding.
4. Bleeding from an artery or several
injury sites may require DIRECT
PRESSURE on a PRESSURE
POINT. Use pressure points for
30 - 60 seconds to help control
severe bleeding.
5. Continue primary care and seek
medical aid as needed.
1. Call for help.
2. Arousal: check for consciousness.
3. Open airway with chin-lift.
4. Look, listen, and feel for breathing.
5. If breathing is absent, give 2 slow, full
rescue breaths.
6. Check the pulse for 5 to 10 seconds.
7. If pulse is present, continue rescue
breathing: 1 breath every
5 seconds
8. If pulse is absent, start CPR:
15 compressions, 2 breaths (1 man)
Health and Safety Plan Page 6
8400 Norcross Road; Colfax, NC April 2021

Project and Health and Safety Information
HES will be performing an environmental remediation at the subject site on behalf of Circle K Stores at the
subject site.

All work will comply with the Occupational Safety and Health Act (OSHA) standard, "Hazardous Waste
Operations and Emergency Response," (29 CFR 1910.120), and other federal, state and local procedures
that require the development and implementation of a HASP. Generation of this document certifies that the
workplace has been evaluated for the hazards as described. A hazard assessment has been performed and
the adequacy of the personal protective equipment (PPE) selected is hereby certified per
29 CFR 1910.132(d) and is duly noted by the signature(s) and date appearing on the cover page of this
document. If any site conditions are encountered that are different from typical retail petroleum operations,
the field investigator is to stop work immediately and notify the Project Manager.

This plan addresses the safety issues associated environmental investigation and assessment activities
performed at retail petroleum operations. For this project, site investigation activities will involve the
following (checked items):

Phase I Environmental Site Assessment Phase II Environmental Site Assessment
x Spill Response and Abatement Soil sampling (hand auger)
Soil sampling (drilling) Monitoring well installation
UST removal (requires full HASP) x Soil excavation
Groundwater sampling/monitoring Groundwater remediation
Drum removal Site surveying
Soil Gas / VI assessment/survey Pump/Slug testing

All activities of this project will be carried out under Level D or Modified Level D. At a minimum, all personnel
will wear the following PPE based on the task to be performed at the site (checked items):

x Hard Hat x Safety Vest
x Steel Toe Boots Chemical Boots
x Nitrile gloves (sampling gloves) Heavy Nitrile gloves
x Safety glasses Ear plugs/ear muffs (sound suppression)
White Tyvek Yellow (polycoated) Tyvek
Health and Safety Plan Page 7
8400 Norcross Road; Colfax, NC April 2021

HAZARD IDENTIFICATION AND CONTROL
Precautions must be taken to prevent injuries and exposures to the following potential hazards.

. Potential Hazards and Control

Potential Hazard

Control

Exposure to
Petroleum
Products

1. Stand up-wind of petroleum products whenever possible.
2. Minimize contact and contact time with petroleum products.
3. Avoid walking through discolored areas, puddles, leaning on drums, or
contacting anything that is likely to be contaminated.
4. Do not eat, drink, smoke and/or apply cosmetics in the hot or warm
zones.
5. Wear gloves when in contact with contaminated surfaces.
6. Safety glasses must be worn at a minimum.
7. Splash goggles must be worn when working with liquids.
8. >25 ppm organic vapors in breathing zone requires upgrade to Level C.
9. >250 ppm organic vapors in breathing zone requires upgrade from
Level C to Level B.
10. If unknown materials are encountered, call the HSS.
Vehicular
Traffic

1. Wear traffic safety vest when vehicle hazard exists.
2. Use cones, flags, barricades, and caution tape to define work area.
3. Use vehicle to block work area.
4. Engage police detail for high-traffic situations.
Vault Entry

1. HES Personnel do not perform Confined Space Entry.

Utility Lines
Contact

1. Contact Dig Safe to have utility lines marked prior to excavation/trenching.
2. Refer to site drawings or customer interviews if on private property for
utility locations.
3. Hand dig 3 to 5 feet down and 5 feet each side of utility marker to avoid
breaking utility lines.
Inclement
Weather

1. Stop outdoor work during electrical storms and other extreme weather
conditions such as extreme heat or cold temperatures.
2. Take cover indoors or in vehicle.
3. Listen to local forecasts for warnings about specific weather hazards such
as tornados, hurricanes, and flash floods.
Noise

1. Wear hearing protection when equipment such as a drill rig, jackhammer,
cut saw, air compressor, blower or other heavy equipment is operating on
the site.
2. Wear hearing protection whenever you need to raise your voice above
normal conversational speech due to a loud noise source; this much noise
indicates the need for protection.
Health and Safety Plan Page 8
8400 Norcross Road; Colfax, NC April 2021

Potential Hazard

Control

Electric
Shock

1. Maintain appropriate distance from overhead utilities;
20-foot minimum clearance from power lines required;
10-foot minimum clearance from shielded power lines.
2. Use ground-fault circuit interrupters as required.
3. Perform lockout/tagout procedures (Appendix C).
4. Use three-pronged plugs and extension cords.
5. Contact your local underground utility-locating service.
6. Follow code requirements for electrical installations in hazardous
locations.
Physical
Injury

1. Wear hard hats and safety glasses when on-site.
2. Maintain visual contact with the equipment operator and wear orange
safety vest when heavy equipment is used on-site.
3. Avoid loose-fitting clothing (driller and driller's helper).
4. Prevent slips, trips and falls; keep work area uncluttered.
5. Keep your hands away from moving parts (i.e., augers).
6. Test the emergency shutoff switch on the drill rig daily.
Back Injury

1. Use a mechanical lifting device or a lifting aid where appropriate.
2. If you must lift, plan the lift before doing it.
3. Check your route for clearance.
4. Bend at the knees and use leg muscles when lifting.
5. Use the buddy system when lifting heavy or awkward objects.
6. Do not twist your body while lifting.
Heat Stress

1. Increase water intake while working.
2. Increase number of rest breaks and/or rotate workers in shorter work
shifts.
3. Watch for signs and symptoms of heat exhaustion and fatigue.
4. Plan work for early morning or evening during hot months.
5. Use ice vests when necessary.
6. Rest in cool, dry areas.
7. In the event of heat stroke, bring the victim to a cool environment and
initiate first aid procedures.
Cold Stress

1. Take breaks in heated shelters when working in extremely cold
temperatures .
2. Remove the outer layer of clothing and loosen other layers to promote
evaporation of perspiration, upon entering the shelter.
3. Drink warm liquids to reduce the susceptibility to cold stress.
High Crime
Areas

1. Be aware of surroundings.
2. Use the buddy system.
3. Request police detail when appropriate.
Insects

1. Tuck pants into socks.
2. Wear long sleeves.
3. Use insect repellent.
Poisonous Plants
(Such as Poison
Ivy, Oak, etc.)

1. Don't enter areas infested with poisonous plants.
2. Immediately wash any areas that come into contact with poisonous
plants.
Health and Safety Plan Page 9
8400 Norcross Road; Colfax, NC April 2021

Potential Hazard

Control

Ladders

1. Make sure ladder rungs are sturdy and free of cracks.
2. Use ladders with secure safety feet.
3. Pitch ladders at a 4:1 ratio.
4. Secure ladders at the top when possible.
5. Do not use ladders for access to air stripper towers.
6. Use non-conductive ladders near electrical wires.
Fire Control

1. Smoke only in designated areas.
2. Keep flammable liquids in closed containers.
3. Keep site clean; avoid accumulating combustible debris such as paper.
4. Follow Hot Work Safety Procedures when welding or performing other
activities requiring an open flame.
5. Isolate flammable and combustible materials from ignition sources.
6. Ensure fire safety integrity of equipment installations according to Hazard
Classification Diagram (Appendix G).
Static Electricity

1. Do not create static discharge in flammable atmospheres.
2. Electrically bond and ground pumps transfer vessels, tanks, drums,
bailers and probes, when moving liquids.
3. Electrically bond and ground vacuum trucks and the tanks they are
emptying.
4. Do not splash fill containers with flammable liquids.
Drilling/Boring
Operations

1. Driller and helper must be present during all active operations.
2. Driller helper and other site personnel must know location of emergency
shut off switch.
3. Unauthorized personnel must be kept clear of drilling rig.
4. Area of drilling operation must be cordoned off/barricaded.
5. When hazardous conditions are deemed present, operation must be shut
down.
Well Installation,
Well
Development,
Well Gauging,
Well Bailing,
Soil/Ground-
water Sampling

1. Wear appropriate PPE to avoid skin, eye, and inhalation contact with
contaminated groundwater and/or soil.
2. Stand upwind when conducting tasks and minimize possible inhalation
exposure; especially when first opening monitoring wells.
3. Conduct air monitoring to determine level of respiratory protection.
4. Utilize engineering controls such as portable venturi air movers to draw
away or blow away chemical vapors.
Welding, Cutting,
Brazing

1. Before conducting welding at a project site, contact the Project Manager..

Cleaning
Equipment

1. Wear appropriate PPE to avoid skin and eye contact with isopropyl
alcohol, alconox, or other cleaning materials.
2. Stand upwind to minimize any potential inhalation exposure.
3. Dispose of spent cleaning solutions and rinses accordingly.
First aid kit, emergency eye wash station, fire extinguisher, and absorbent
pads will be located on-site in the vehicle or site remediation system.
Health and Safety Plan Page 10
8400 Norcross Road; Colfax, NC April 2021

Signature Sheet

All persons entering the work zone, or visiting the subject site for the purposes associated with the subject
investigation(s), or activities associated with the subject investigation(s) are required to notify the HES
representative on-site immediately upon arrival. All persons entering the work zone, or visiting the subject
site for the purposes associated with the subject investigation(s), or activities associated with the subject
investigation(s) are required to review appropriate health and safety procedures, and provide a signature
documenting they have been properly briefed on health and safety policies and procedures to be followed
while on-site. HES will not be responsible for personal injuries or death resulting from personal actions that
are considered negligent, or that result from personal activities that are contrary to this health and safety plan.

By my signature, I acknowledge that I have been briefed on site specific health and safety procedures,
that I am familiar with said health and safety procedures, and that I will follow all indicated health and
safety procedures while on-site.

Name Signature

APPENDIX D

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/23/2021
Highland Environmental Solutions Joe Beaman
8410-D Falls of Neuse Road Raleigh, NC, 27615
Ref: Analytical Testing
Lab Report Number: 21-106-0032 Client Project Description: 186481
Dear Joe Beaman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/16/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 112
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202137735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202099012State ProgramSouth Carolina
Page 1 of 1 00016/21-106-0032
Page 2 of 112
Report Number:
Sample Summary Table
Client Project Description:
21-106-0032
186481
Lab No Client Sample ID Matrix Date Collected Date Received
04/15/2021 10:10Solids 96985 S-1 04/16/2021 16:45
04/15/2021 10:30Solids 96986 S-2 04/16/2021 16:45
04/15/2021 12:00Solids 96987 S-3 04/16/2021 16:45
04/15/2021 12:20Solids 96988 S-4 04/16/2021 16:45
04/15/2021 12:30Solids 96989 S-5 04/16/2021 16:45
04/15/2021 12:40Solids 96990 S-6 04/16/2021 16:45
04/15/2021 12:50Solids 96991 S-7 04/16/2021 16:45
04/15/2021 12:55Solids 96992 S-8 04/16/2021 16:45
Page 3 of 112
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-106-0032
Report Limit
Project:186481
V 96985S-1
445 04/21/2021 15:098015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 1.61
23.0 04/20/2021 10:428015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.037
J0.001 04/20/2021 13:298260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.001 04/20/2021 13:298260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.005 04/20/2021 13:298260D4-Isopropyl toluene mg/Kg - dry 0.001
J0.007 04/20/2021 13:298260DNaphthalenemg/Kg - dry 0.0007
J0.084 04/21/2021 17:398270EPyrenemg/Kg - dry 0.013
J49.6 04/21/2021 22:03MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 11.2
99.7 04/21/2021 22:03MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 3.33
J49.5 04/21/2021 22:03MADEP-EPH Aromatic C11-C22 mg/Kg - dry 18.2
11.0 04/19/2021 15:48MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 0.961
26.8 04/19/2021 17:20SW-DRYWT Moisture %
V 96986S-2
197 04/20/2021 15:588015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.315
54.2 04/20/2021 11:098015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.036
J0.001 04/20/2021 13:598260DNaphthalenemg/Kg - dry 0.0007
J0.022 04/21/2021 18:028270EPyrenemg/Kg - dry 0.012
79.5 04/21/2021 22:39MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 11.0
202 04/21/2021 22:39MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 3.27
96.1 04/21/2021 22:39MADEP-EPH Aromatic C11-C22 mg/Kg - dry 17.8
22.8 04/19/2021 16:17MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 0.942
J2.38 04/19/2021 16:17MADEP-VPH Aromatic C9-C10 mg/Kg - dry 1.01
25.3 04/19/2021 17:20SW-DRYWT Moisture %
V 96987S-3
JB4.56 04/20/2021 16:358015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.322
JB0.096 04/20/2021 11:378015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.036
26.1 04/19/2021 17:20SW-DRYWT Moisture %
V 96988S-4
25.3 04/20/2021 17:128015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.318
23.0 04/20/2021 12:048015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.036
J0.0007 04/19/2021 14:008260Dn-Butylbenzene mg/Kg - dry 0.0006
J4.92 04/21/2021 23:52MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 3.39
26.0 04/19/2021 17:20SW-DRYWT Moisture %
Page 4 of 112
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-106-0032
Report Limit
Project:186481
V 96989S-5
35.2 04/20/2021 17:498015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.321
JB0.242 04/20/2021 12:318015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.037
J0.001 04/19/2021 14:308260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.001 04/19/2021 14:308260DNaphthalenemg/Kg - dry 0.0007
J15.7 04/22/2021 00:28MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 11.4
J8.58 04/22/2021 00:28MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 3.39
26.9 04/19/2021 17:20SW-DRYWT Moisture %
V 96990S-6
JB4.18 04/20/2021 18:268015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.323
26.4 04/19/2021 17:20SW-DRYWT Moisture %
V 96991S-7
JB5.44 04/20/2021 19:038015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.320
JB0.083 04/20/2021 13:268015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.037
26.6 04/19/2021 17:20SW-DRYWT Moisture %
V 96992S-8
B10.2 04/20/2021 19:408015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 0.329
JB0.077 04/20/2021 13:538015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 0.038
28.6 04/19/2021 17:20SW-DRYWT Moisture %
Page 5 of 112

Client: Highland Environmental Solutions CASE NARRATIVE
Project: 186481 Lab Report Number: 21-106-0032
Date: 4/22/2021
Massachusetts EPH Method MADEP-EPH Analyte: Aliphatic C9-C18 QC Batch No: V3419/V3247
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 166.580 ug/mL which calculates to a recovery of 55.5% which is within the acceptable recovery range.
Sample 96987 (S-3)
Analyte: Aliphatic C9-C18 QC Batch No: V3419/V3247
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 163.069 ug/mL which calculates to a recovery of 54.4% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V3419/V3247 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 152.824 ug/mL which calculates to a recovery of 50.9% which is within the acceptable recovery range. Massachusetts VPH Method MADEP-VPH Sample 96988 (S-4)
Analyte: 2,5-Dibromotoluene (FID) QC Batch No: V3232/V3218 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Sample 96989 (S-5) Analyte: 2,5-Dibromotoluene (FID)
QC Batch No: V3232/V3218 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 96990 (S-6)
Analyte: 2,5-Dibromotoluene (FID) QC Batch No: V3232/V3218 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 96991 (S-7) Analyte: 2,5-Dibromotoluene (FID) QC Batch No: V3232/V3218 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Page 6 of 112

Sample 96992 (S-8) Analyte: 2,5-Dibromotoluene (FID)
QC Batch No: V3232/V3218 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 97092 Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V3407 The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to
the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates.
Analyte: o-Terphenyl QC Batch No: V3407
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Analyte: o-Terphenyl QC Batch No: V3407 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Analyte: o-Terphenyl QC Batch No: V3407 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone
QC Batch No: V3304/V3303 CCV result is below control limits but within method parameters. A standar at or below the RL was analyzed and found acceptable. Results are reported but considered estimated. Analyte: Acetone QC Batch No: V3256/V3303
CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated. Analyte: Acetone QC Batch No: V3304/V3303 CCV result is below control limits but within method parameters. A standar at or below the RL was analyzed and found acceptable. Results are reported but considered estimated. Analyte: Methylene chloride QC Batch No: V3256/V3303 CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Page 7 of 112

Analyte: Methylene chloride QC Batch No: V3304/V3303
CCV result is below control limits but within method parameters. A standar at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Analyte: n-Butylbenzene
QC Batch No: V3256/V3303 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Analyte: n-Butylbenzene
QC Batch No: V3304/V3303 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Analyte: sec-Butylbenzene
QC Batch No: V3304/V3303 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 96999 Analyte: Benzoic Acid
QC Batch No: V3441 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 817 ug/kg which calculates to a recovery of 48% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V3441
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 706 ug/kg which calculates to a recovery of 42% which is within the acceptable recovery range. Analyte: N-nitrosodimethylamine QC Batch No: V3441 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid
QC Batch No: V3441/V3284 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 1140 ug/kg which calculates to a recovery of 68.4% which is within the acceptable recovery range.
Page 8 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
49.6 J mg/Kg - dry 11.2 66.7Aliphatic C19-C36 1 04/21/21 22:03 MADEP-EPHZRC
<2.16 mg/Kg - dry 2.16 10.9Aliphatic C5-C8 100 04/19/21 15:48 MADEP-VPHTBL
11.0 mg/Kg - dry 0.961 10.9Aliphatic C9-C12 100 04/19/21 15:48 MADEP-VPHTBL
99.7 mg/Kg - dry 3.33 66.7Aliphatic C9-C18 1 04/21/21 22:03 MADEP-EPHZRC
49.5 J mg/Kg - dry 18.2 66.7Aromatic C11-C22 1 04/21/21 22:03 MADEP-EPHZRC
<1.03 mg/Kg - dry 1.03 10.9
Aromatic C9-C10 100 04/19/21 15:48 MADEP-VPHTBL
26.8 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 9 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
445 mg/Kg - dry 1.61 47.8Diesel Range Organics (C10-C28)5 04/21/21 15:09 V3407ZRC
Surrogate: OTP Surrogate 85.0 Limits: 31-123%04/21/21 15:095 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
23.0 mg/Kg - dry 0.037 6.83Gasoline Range Organics (C6-C10)50 04/20/21 10:42 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 111 Limits: 50-137%04/20/21 10:4250 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/20/21 13:29 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromodichloromethane 1 04/20/21 13:29 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/20/21 13:29 V3304TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/20/21 13:29 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
0.001 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/20/21 13:29 V3304TBL
0.001 J mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/20/21 13:29 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/20/21 13:29 V3304TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/20/21 13:29 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/20/21 13:29 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/20/21 13:29 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/20/21 13:29 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/20/21 13:29 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/20/21 13:29 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/20/21 13:29 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/20/21 13:29 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/20/21 13:29 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.068Ethyl Tertiary Butyl Ether (ETBE)1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/20/21 13:29 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/20/21 13:29 V3304TBL
0.005 J
mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/20/21 13:29 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.006Methyl tert-butyl ether (MTBE)1 04/20/21 13:29 V3304TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/20/21 13:29 V3304TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/20/21 13:29 V3304TBL
0.007 J mg/Kg - dry 0.0007 0.013Naphthalene 1 04/20/21 13:29 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/20/21 13:29 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.006Styrene 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/20/21 13:29 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/20/21 13:29 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,4-Trichlorobenzene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/20/21 13:29 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/20/21 13:29 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/20/21 13:29 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/20/21 13:29 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/20/21 13:29 V3304
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/20/21 13:291 TBL V3304
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/20/21 13:291 TBL V3304
Surrogate: Toluene-d8 117 Limits: 76-129%04/20/21 13:291 TBL V3304
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.901Acenaphthene 1 04/21/21 17:39 V3441JMV
<0.017 mg/Kg - dry 0.017 0.901Acenaphthylene 1 04/21/21 17:39 V3441JMV
<0.222 mg/Kg - dry 0.222 0.901Aniline 1 04/21/21 17:39 V3441JMV
<0.009 mg/Kg - dry 0.009 0.901Anthracene 1 04/21/21 17:39 V3441JMV
<0.010 mg/Kg - dry 0.010 0.901Benzo(a)anthracene 1 04/21/21 17:39 V3441JMV
<0.008 mg/Kg - dry 0.008 0.901Benzo(a)pyrene 1 04/21/21 17:39 V3441JMV
<0.008 mg/Kg - dry 0.008 0.901Benzo(b)fluoranthene 1 04/21/21 17:39 V3441JMV
<0.008 mg/Kg - dry 0.008 0.901Benzo(g,h,i)perylene 1 04/21/21 17:39 V3441JMV
<0.009 mg/Kg - dry 0.009 0.901
Benzo(k)fluoranthene 1 04/21/21 17:39 V3441JMV
<0.748 mg/Kg - dry 0.748 2.73Benzoic Acid 1 04/21/21 17:39 V3441JMV
<0.169 mg/Kg - dry 0.169 0.901Benzyl alcohol 1 04/21/21 17:39 V3441JMV
<0.172 mg/Kg - dry 0.172 0.901Bis(2-Chloroethoxy)methane 1 04/21/21 17:39 V3441JMV
<0.144 mg/Kg - dry 0.144 0.901Bis(2-Chloroethyl)ether 1 04/21/21 17:39 V3441JMV
<0.161 mg/Kg - dry 0.161 0.450Bis(2-Chloroisopropyl)ether 1 04/21/21 17:39 V3441JMV
<0.203 mg/Kg - dry 0.203 0.901Bis(2-ethylhexyl)phthalate 1 04/21/21 17:39 V3441JMV
<0.211 mg/Kg - dry 0.211 0.901
4-Bromophenyl phenyl ether 1 04/21/21 17:39 V3441JMV
<0.155 mg/Kg - dry 0.155 0.450Butyl benzyl phthalate 1 04/21/21 17:39 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9014-Chloro-3-methylphenol 1 04/21/21 17:39 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4504-Chloroaniline 1 04/21/21 17:39 V3441JMV
<0.219 mg/Kg - dry 0.219 0.9012-Chloronaphthalene 1 04/21/21 17:39 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9012-Chlorophenol 1 04/21/21 17:39 V3441JMV
<0.275 mg/Kg - dry 0.275 1.374-Chlorophenyl phenyl ether 1 04/21/21 17:39 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.901Chrysene 1 04/21/21 17:39 V3441JMV
<0.025 mg/Kg - dry 0.025 0.901Dibenz(a,h)anthracene 1 04/21/21 17:39 V3441JMV
<0.024 mg/Kg - dry 0.024 0.901Dibenzofuran 1 04/21/21 17:39 V3441JMV
<0.146 mg/Kg - dry 0.146 0.9011,2-Dichlorobenzene 1 04/21/21 17:39 V3441JMV
<0.132 mg/Kg - dry 0.132 0.9011,3-Dichlorobenzene 1 04/21/21 17:39 V3441JMV
<0.142 mg/Kg - dry 0.142 0.4501,4-Dichlorobenzene 1 04/21/21 17:39 V3441JMV
<0.178 mg/Kg - dry 0.178 0.9013,3'-Dichlorobenzidine 1 04/21/21 17:39 V3441JMV
<0.176 mg/Kg - dry 0.176 0.9012,4-Dichlorophenol 1 04/21/21 17:39 V3441JMV
<0.232 mg/Kg - dry 0.232 0.901
Diethyl phthalate 1 04/21/21 17:39 V3441JMV
<0.215 mg/Kg - dry 0.215 0.901Dimethyl phthalate 1 04/21/21 17:39 V3441JMV
<0.187 mg/Kg - dry 0.187 0.4502,4-Dimethylphenol 1 04/21/21 17:39 V3441JMV
<0.224 mg/Kg - dry 0.224 0.901Di-n-butyl phthalate 1 04/21/21 17:39 V3441JMV
<0.497 mg/Kg - dry 0.497 2.054,6-Dinitro-2-methylphenol 1 04/21/21 17:39 V3441JMV
<0.528 mg/Kg - dry 0.528 2.052,4-Dinitrophenol 1 04/21/21 17:39 V3441JMV
<0.239 mg/Kg - dry 0.239 0.9012,4-Dinitrotoluene 1 04/21/21 17:39 V3441JMV
<0.233 mg/Kg - dry 0.233 0.901
2,6-Dinitrotoluene 1 04/21/21 17:39 V3441JMV
<0.233 mg/Kg - dry 0.233 0.450Di-n-Octyl Phthalate 1 04/21/21 17:39 V3441JMV
<0.010 mg/Kg - dry 0.010 0.901Fluoranthene 1 04/21/21 17:39 V3441JMV
<0.019 mg/Kg - dry 0.019 0.901Fluorene 1 04/21/21 17:39 V3441JMV
<0.198 mg/Kg - dry 0.198 0.901Hexachlorobenzene 1 04/21/21 17:39 V3441JMV
<0.203 mg/Kg - dry 0.203 0.901Hexachlorobutadiene 1 04/21/21 17:39 V3441JMV
<0.310 mg/Kg - dry 0.310 0.901Hexachlorocyclopentadiene 1 04/21/21 17:39 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.142 mg/Kg - dry 0.142 0.901Hexachloroethane 1 04/21/21 17:39 V3441JMV
<0.025 mg/Kg - dry 0.025 0.901Indeno(1,2,3-cd)pyrene 1 04/21/21 17:39 V3441JMV
<0.193 mg/Kg - dry 0.193 0.901Isophorone 1 04/21/21 17:39 V3441JMV
<0.013 mg/Kg - dry 0.013 0.9011-Methylnaphthalene 1 04/21/21 17:39 V3441JMV
<0.017 mg/Kg - dry 0.017 0.9012-Methylnaphthalene 1 04/21/21 17:39 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9012-Methylphenol 1 04/21/21 17:39 V3441JMV
<0.195 mg/Kg - dry 0.195 0.9013&4 Methylphenol 1 04/21/21 17:39 V3441JMV
<0.019 mg/Kg - dry 0.019 0.901Naphthalene 1 04/21/21 17:39 V3441JMV
<0.193 mg/Kg - dry 0.193 0.901
2-Nitroaniline 1 04/21/21 17:39 V3441JMV
<0.163 mg/Kg - dry 0.163 0.9013-Nitroaniline 1 04/21/21 17:39 V3441JMV
<0.140 mg/Kg - dry 0.140 0.4504-Nitroaniline 1 04/21/21 17:39 V3441JMV
<0.191 mg/Kg - dry 0.191 0.450Nitrobenzene 1 04/21/21 17:39 V3441JMV
<0.150 mg/Kg - dry 0.150 0.9012-Nitrophenol 1 04/21/21 17:39 V3441JMV
<0.222 mg/Kg - dry 0.222 0.9014-Nitrophenol 1 04/21/21 17:39 V3441JMV
<0.007 mg/Kg - dry 0.007 0.232N-Nitrosodimethylamine 1 04/21/21 17:39 V3441JMV
<0.247 mg/Kg - dry 0.247 0.901
N-Nitrosodiphenylamine 1 04/21/21 17:39 V3441JMV
<0.207 mg/Kg - dry 0.207 0.901N-Nitroso-di-n-propylamine 1 04/21/21 17:39 V3441JMV
<0.575 mg/Kg - dry 0.575 1.37Pentachlorophenol 1 04/21/21 17:39 V3441JMV
<0.009 mg/Kg - dry 0.009 0.901Phenanthrene 1 04/21/21 17:39 V3441JMV
<0.147 mg/Kg - dry 0.147 0.901Phenol 1 04/21/21 17:39 V3441JMV
0.084 J mg/Kg - dry 0.013 0.901Pyrene 1 04/21/21 17:39 V3441JMV
<0.086 mg/Kg - dry 0.086 0.450Pyridine 1 04/21/21 17:39 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-1
96985 Matrix:
4/15/2021 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.159 mg/Kg - dry 0.159 0.9011,2,4-Trichlorobenzene 1 04/21/21 17:39 V3441JMV
<0.191 mg/Kg - dry 0.191 0.9012,4,5-Trichlorophenol 1 04/21/21 17:39 V3441JMV
<0.218 mg/Kg - dry 0.218 0.9012,4,6-Trichlorophenol 1 04/21/21 17:39 V3441JMV
Surrogate: Phenol-d5 75.3 Limits: 34-121%04/21/21 17:391 JMV V3441
Surrogate: 2-Fluorobiphenyl 84.9 Limits: 44-115%04/21/21 17:391 JMV V3441
Surrogate: 2-Fluorophenol 75.6 Limits: 35-115%04/21/21 17:391 JMV V3441
Surrogate: Nitrobenzene-d5 74.1 Limits: 37-122%04/21/21 17:391 JMV V3441
Surrogate: 4-Terphenyl-d14 81.9 Limits: 54-127%04/21/21 17:391 JMV V3441
Surrogate: 2,4,6-Tribromophenol 101 Limits: 39-132%04/21/21 17:391 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
79.5 mg/Kg - dry 11.0 65.3Aliphatic C19-C36 1 04/21/21 22:39 MADEP-EPHZRC
<2.12 mg/Kg - dry 2.12 10.7Aliphatic C5-C8 100 04/19/21 16:17 MADEP-VPHTBL
22.8 mg/Kg - dry 0.942 10.7Aliphatic C9-C12 100 04/19/21 16:17 MADEP-VPHTBL
202 mg/Kg - dry 3.27 65.3Aliphatic C9-C18 1 04/21/21 22:39 MADEP-EPHZRC
96.1 mg/Kg - dry 17.8 65.3Aromatic C11-C22 1 04/21/21 22:39 MADEP-EPHZRC
2.38 J
mg/Kg - dry 1.01 10.7
Aromatic C9-C10 100 04/19/21 16:17 MADEP-VPHTBL
25.3 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 18 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
197 mg/Kg - dry 0.315 9.37Diesel Range Organics (C10-C28)1 04/20/21 15:58 V3407ZRC
Surrogate: OTP Surrogate 74.5 Limits: 31-123%04/20/21 15:581 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
54.2 mg/Kg - dry 0.036 6.69Gasoline Range Organics (C6-C10)50 04/20/21 11:09 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 115 Limits: 50-137%04/20/21 11:0950 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.020 mg/Kg - dry 0.020 0.026Acetone 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/20/21 13:59 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/20/21 13:59 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 04/20/21 13:59 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/20/21 13:59 V3304TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/20/21 13:59 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/20/21 13:59 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/20/21 13:59 V3304TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/20/21 13:59 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/20/21 13:59 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2-Dibromo-3-Chloropropane 1 04/20/21 13:59 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/20/21 13:59 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/20/21 13:59 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/20/21 13:59 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/20/21 13:59 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.066Ethyl Tertiary Butyl Ether (ETBE)1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/20/21 13:59 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.0262-Hexanone 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.026Methyl Ethyl Ketone (MEK)1 04/20/21 13:59 V3304TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 04/20/21 13:59 V3304TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 04/20/21 13:59 V3304TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/20/21 13:59 V3304TBL
0.001 J mg/Kg - dry 0.0007 0.013Naphthalene 1 04/20/21 13:59 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/20/21 13:59 V3304TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3303 04/20/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/20/21 13:59 V3304TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/20/21 13:59 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/20/21 13:59 V3304TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2,4-Trichlorobenzene 1 04/20/21 13:59 V3304TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1,1-Trichloroethane 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/20/21 13:59 V3304TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/20/21 13:59 V3304TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/20/21 13:59 V3304TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/20/21 13:59 V3304
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/20/21 13:591 TBL V3304
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/20/21 13:591 TBL V3304
Surrogate: Toluene-d8 117 Limits: 76-129%04/20/21 13:591 TBL V3304
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.883Acenaphthene 1 04/21/21 18:02 V3441JMV
<0.017 mg/Kg - dry 0.017 0.883Acenaphthylene 1 04/21/21 18:02 V3441JMV
<0.218 mg/Kg - dry 0.218 0.883Aniline 1 04/21/21 18:02 V3441JMV
<0.009 mg/Kg - dry 0.009 0.883Anthracene 1 04/21/21 18:02 V3441JMV
<0.010 mg/Kg - dry 0.010 0.883Benzo(a)anthracene 1 04/21/21 18:02 V3441JMV
<0.007 mg/Kg - dry 0.007 0.883Benzo(a)pyrene 1 04/21/21 18:02 V3441JMV
<0.008 mg/Kg - dry 0.008 0.883Benzo(b)fluoranthene 1 04/21/21 18:02 V3441JMV
<0.008 mg/Kg - dry 0.008 0.883Benzo(g,h,i)perylene 1 04/21/21 18:02 V3441JMV
<0.009 mg/Kg - dry 0.009 0.883
Benzo(k)fluoranthene 1 04/21/21 18:02 V3441JMV
<0.733 mg/Kg - dry 0.733 2.68Benzoic Acid 1 04/21/21 18:02 V3441JMV
<0.165 mg/Kg - dry 0.165 0.883Benzyl alcohol 1 04/21/21 18:02 V3441JMV
<0.168 mg/Kg - dry 0.168 0.883Bis(2-Chloroethoxy)methane 1 04/21/21 18:02 V3441JMV
<0.141 mg/Kg - dry 0.141 0.883Bis(2-Chloroethyl)ether 1 04/21/21 18:02 V3441JMV
<0.157 mg/Kg - dry 0.157 0.441Bis(2-Chloroisopropyl)ether 1 04/21/21 18:02 V3441JMV
<0.199 mg/Kg - dry 0.199 0.883Bis(2-ethylhexyl)phthalate 1 04/21/21 18:02 V3441JMV
<0.207 mg/Kg - dry 0.207 0.883
4-Bromophenyl phenyl ether 1 04/21/21 18:02 V3441JMV
<0.152 mg/Kg - dry 0.152 0.441Butyl benzyl phthalate 1 04/21/21 18:02 V3441JMV
<0.168 mg/Kg - dry 0.168 0.8834-Chloro-3-methylphenol 1 04/21/21 18:02 V3441JMV
<0.107 mg/Kg - dry 0.107 0.4414-Chloroaniline 1 04/21/21 18:02 V3441JMV
<0.215 mg/Kg - dry 0.215 0.8832-Chloronaphthalene 1 04/21/21 18:02 V3441JMV
<0.168 mg/Kg - dry 0.168 0.8832-Chlorophenol 1 04/21/21 18:02 V3441JMV
<0.270 mg/Kg - dry 0.270 1.344-Chlorophenyl phenyl ether 1 04/21/21 18:02 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.883Chrysene 1 04/21/21 18:02 V3441JMV
<0.025 mg/Kg - dry 0.025 0.883Dibenz(a,h)anthracene 1 04/21/21 18:02 V3441JMV
<0.023 mg/Kg - dry 0.023 0.883Dibenzofuran 1 04/21/21 18:02 V3441JMV
<0.143 mg/Kg - dry 0.143 0.8831,2-Dichlorobenzene 1 04/21/21 18:02 V3441JMV
<0.129 mg/Kg - dry 0.129 0.8831,3-Dichlorobenzene 1 04/21/21 18:02 V3441JMV
<0.139 mg/Kg - dry 0.139 0.4411,4-Dichlorobenzene 1 04/21/21 18:02 V3441JMV
<0.175 mg/Kg - dry 0.175 0.8833,3'-Dichlorobenzidine 1 04/21/21 18:02 V3441JMV
<0.172 mg/Kg - dry 0.172 0.8832,4-Dichlorophenol 1 04/21/21 18:02 V3441JMV
<0.227 mg/Kg - dry 0.227 0.883
Diethyl phthalate 1 04/21/21 18:02 V3441JMV
<0.211 mg/Kg - dry 0.211 0.883Dimethyl phthalate 1 04/21/21 18:02 V3441JMV
<0.183 mg/Kg - dry 0.183 0.4412,4-Dimethylphenol 1 04/21/21 18:02 V3441JMV
<0.219 mg/Kg - dry 0.219 0.883Di-n-butyl phthalate 1 04/21/21 18:02 V3441JMV
<0.487 mg/Kg - dry 0.487 2.014,6-Dinitro-2-methylphenol 1 04/21/21 18:02 V3441JMV
<0.518 mg/Kg - dry 0.518 2.012,4-Dinitrophenol 1 04/21/21 18:02 V3441JMV
<0.234 mg/Kg - dry 0.234 0.8832,4-Dinitrotoluene 1 04/21/21 18:02 V3441JMV
<0.228 mg/Kg - dry 0.228 0.883
2,6-Dinitrotoluene 1 04/21/21 18:02 V3441JMV
<0.228 mg/Kg - dry 0.228 0.441Di-n-Octyl Phthalate 1 04/21/21 18:02 V3441JMV
<0.010 mg/Kg - dry 0.010 0.883Fluoranthene 1 04/21/21 18:02 V3441JMV
<0.019 mg/Kg - dry 0.019 0.883Fluorene 1 04/21/21 18:02 V3441JMV
<0.194 mg/Kg - dry 0.194 0.883Hexachlorobenzene 1 04/21/21 18:02 V3441JMV
<0.199 mg/Kg - dry 0.199 0.883Hexachlorobutadiene 1 04/21/21 18:02 V3441JMV
<0.303 mg/Kg - dry 0.303 0.883Hexachlorocyclopentadiene 1 04/21/21 18:02 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.139 mg/Kg - dry 0.139 0.883Hexachloroethane 1 04/21/21 18:02 V3441JMV
<0.024 mg/Kg - dry 0.024 0.883Indeno(1,2,3-cd)pyrene 1 04/21/21 18:02 V3441JMV
<0.190 mg/Kg - dry 0.190 0.883Isophorone 1 04/21/21 18:02 V3441JMV
<0.013 mg/Kg - dry 0.013 0.8831-Methylnaphthalene 1 04/21/21 18:02 V3441JMV
<0.017 mg/Kg - dry 0.017 0.8832-Methylnaphthalene 1 04/21/21 18:02 V3441JMV
<0.168 mg/Kg - dry 0.168 0.8832-Methylphenol 1 04/21/21 18:02 V3441JMV
<0.191 mg/Kg - dry 0.191 0.8833&4 Methylphenol 1 04/21/21 18:02 V3441JMV
<0.018 mg/Kg - dry 0.018 0.883Naphthalene 1 04/21/21 18:02 V3441JMV
<0.190 mg/Kg - dry 0.190 0.883
2-Nitroaniline 1 04/21/21 18:02 V3441JMV
<0.160 mg/Kg - dry 0.160 0.8833-Nitroaniline 1 04/21/21 18:02 V3441JMV
<0.137 mg/Kg - dry 0.137 0.4414-Nitroaniline 1 04/21/21 18:02 V3441JMV
<0.187 mg/Kg - dry 0.187 0.441Nitrobenzene 1 04/21/21 18:02 V3441JMV
<0.147 mg/Kg - dry 0.147 0.8832-Nitrophenol 1 04/21/21 18:02 V3441JMV
<0.218 mg/Kg - dry 0.218 0.8834-Nitrophenol 1 04/21/21 18:02 V3441JMV
<0.007 mg/Kg - dry 0.007 0.227N-Nitrosodimethylamine 1 04/21/21 18:02 V3441JMV
<0.242 mg/Kg - dry 0.242 0.883
N-Nitrosodiphenylamine 1 04/21/21 18:02 V3441JMV
<0.203 mg/Kg - dry 0.203 0.883N-Nitroso-di-n-propylamine 1 04/21/21 18:02 V3441JMV
<0.563 mg/Kg - dry 0.563 1.34Pentachlorophenol 1 04/21/21 18:02 V3441JMV
<0.009 mg/Kg - dry 0.009 0.883Phenanthrene 1 04/21/21 18:02 V3441JMV
<0.144 mg/Kg - dry 0.144 0.883Phenol 1 04/21/21 18:02 V3441JMV
0.022 J mg/Kg - dry 0.012 0.883Pyrene 1 04/21/21 18:02 V3441JMV
<0.084 mg/Kg - dry 0.084 0.441Pyridine 1 04/21/21 18:02 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-2
96986 Matrix:
4/15/2021 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.156 mg/Kg - dry 0.156 0.8831,2,4-Trichlorobenzene 1 04/21/21 18:02 V3441JMV
<0.187 mg/Kg - dry 0.187 0.8832,4,5-Trichlorophenol 1 04/21/21 18:02 V3441JMV
<0.214 mg/Kg - dry 0.214 0.8832,4,6-Trichlorophenol 1 04/21/21 18:02 V3441JMV
Surrogate: Phenol-d5 87.0 Limits: 34-121%04/21/21 18:021 JMV V3441
Surrogate: 2-Fluorobiphenyl 81.2 Limits: 44-115%04/21/21 18:021 JMV V3441
Surrogate: 2-Fluorophenol 87.9 Limits: 35-115%04/21/21 18:021 JMV V3441
Surrogate: Nitrobenzene-d5 85.5 Limits: 37-122%04/21/21 18:021 JMV V3441
Surrogate: 4-Terphenyl-d14 83.6 Limits: 54-127%04/21/21 18:021 JMV V3441
Surrogate: 2,4,6-Tribromophenol 100 Limits: 39-132%04/21/21 18:021 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<11.4 mg/Kg - dry 11.4 67.7Aliphatic C19-C36 1 04/21/21 23:16 MADEP-EPHZRC
<2.14 mg/Kg - dry 2.14 10.8Aliphatic C5-C8 100 04/19/21 16:46 MADEP-VPHTBL
<0.952 mg/Kg - dry 0.952 10.8Aliphatic C9-C12 100 04/19/21 16:46 MADEP-VPHTBL
<3.38 mg/Kg - dry 3.38 67.7Aliphatic C9-C18 1 04/21/21 23:16 MADEP-EPHZRC
<18.4 mg/Kg - dry 18.4 67.7Aromatic C11-C22 1 04/21/21 23:16 MADEP-EPHZRC
<1.02 mg/Kg - dry 1.02 10.8
Aromatic C9-C10 100 04/19/21 16:46 MADEP-VPHTBL
26.1 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 27 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
4.56 JB mg/Kg - dry 0.322 9.58Diesel Range Organics (C10-C28)1 04/20/21 16:35 V3407ZRC
Surrogate: OTP Surrogate 70.5 Limits: 31-123%04/20/21 16:351 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
0.096 JB mg/Kg - dry 0.036 6.77Gasoline Range Organics (C6-C10)50 04/20/21 11:37 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 108 Limits: 50-137%04/20/21 11:3750 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/19/21 13:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 04/19/21 13:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/19/21 13:30 V3256TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/19/21 13:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/19/21 13:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/19/21 13:30 V3256TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/19/21 13:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/19/21 13:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/19/21 13:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/19/21 13:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/19/21 13:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/19/21 13:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.067Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/19/21 13:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 04/19/21 13:30 V3256TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/19/21 13:30 V3256TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Naphthalene 1 04/19/21 13:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/19/21 13:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/19/21 13:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/19/21 13:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/19/21 13:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2,4-Trichlorobenzene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/19/21 13:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/19/21 13:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/19/21 13:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/19/21 13:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/19/21 13:30 V3256
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%04/19/21 13:301 TBL V3256
Surrogate: Dibromofluoromethane 107 Limits: 84-123%04/19/21 13:301 TBL V3256
Surrogate: Toluene-d8 118 Limits: 76-129%04/19/21 13:301 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.899Acenaphthene 1 04/21/21 18:24 V3441JMV
<0.017 mg/Kg - dry 0.017 0.899Acenaphthylene 1 04/21/21 18:24 V3441JMV
<0.221 mg/Kg - dry 0.221 0.899Aniline 1 04/21/21 18:24 V3441JMV
<0.009 mg/Kg - dry 0.009 0.899Anthracene 1 04/21/21 18:24 V3441JMV
<0.010 mg/Kg - dry 0.010 0.899Benzo(a)anthracene 1 04/21/21 18:24 V3441JMV
<0.008 mg/Kg - dry 0.008 0.899Benzo(a)pyrene 1 04/21/21 18:24 V3441JMV
<0.008 mg/Kg - dry 0.008 0.899Benzo(b)fluoranthene 1 04/21/21 18:24 V3441JMV
<0.008 mg/Kg - dry 0.008 0.899Benzo(g,h,i)perylene 1 04/21/21 18:24 V3441JMV
<0.009 mg/Kg - dry 0.009 0.899
Benzo(k)fluoranthene 1 04/21/21 18:24 V3441JMV
<0.748 mg/Kg - dry 0.748 2.73Benzoic Acid 1 04/21/21 18:24 V3441JMV
<0.169 mg/Kg - dry 0.169 0.899Benzyl alcohol 1 04/21/21 18:24 V3441JMV
<0.171 mg/Kg - dry 0.171 0.899Bis(2-Chloroethoxy)methane 1 04/21/21 18:24 V3441JMV
<0.144 mg/Kg - dry 0.144 0.899Bis(2-Chloroethyl)ether 1 04/21/21 18:24 V3441JMV
<0.161 mg/Kg - dry 0.161 0.450Bis(2-Chloroisopropyl)ether 1 04/21/21 18:24 V3441JMV
<0.202 mg/Kg - dry 0.202 0.899Bis(2-ethylhexyl)phthalate 1 04/21/21 18:24 V3441JMV
<0.211 mg/Kg - dry 0.211 0.899
4-Bromophenyl phenyl ether 1 04/21/21 18:24 V3441JMV
<0.155 mg/Kg - dry 0.155 0.450Butyl benzyl phthalate 1 04/21/21 18:24 V3441JMV
<0.171 mg/Kg - dry 0.171 0.8994-Chloro-3-methylphenol 1 04/21/21 18:24 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4504-Chloroaniline 1 04/21/21 18:24 V3441JMV
<0.219 mg/Kg - dry 0.219 0.8992-Chloronaphthalene 1 04/21/21 18:24 V3441JMV
<0.171 mg/Kg - dry 0.171 0.8992-Chlorophenol 1 04/21/21 18:24 V3441JMV
<0.276 mg/Kg - dry 0.276 1.374-Chlorophenyl phenyl ether 1 04/21/21 18:24 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.899Chrysene 1 04/21/21 18:24 V3441JMV
<0.025 mg/Kg - dry 0.025 0.899Dibenz(a,h)anthracene 1 04/21/21 18:24 V3441JMV
<0.024 mg/Kg - dry 0.024 0.899Dibenzofuran 1 04/21/21 18:24 V3441JMV
<0.146 mg/Kg - dry 0.146 0.8991,2-Dichlorobenzene 1 04/21/21 18:24 V3441JMV
<0.132 mg/Kg - dry 0.132 0.8991,3-Dichlorobenzene 1 04/21/21 18:24 V3441JMV
<0.142 mg/Kg - dry 0.142 0.4501,4-Dichlorobenzene 1 04/21/21 18:24 V3441JMV
<0.178 mg/Kg - dry 0.178 0.8993,3'-Dichlorobenzidine 1 04/21/21 18:24 V3441JMV
<0.175 mg/Kg - dry 0.175 0.8992,4-Dichlorophenol 1 04/21/21 18:24 V3441JMV
<0.231 mg/Kg - dry 0.231 0.899
Diethyl phthalate 1 04/21/21 18:24 V3441JMV
<0.215 mg/Kg - dry 0.215 0.899Dimethyl phthalate 1 04/21/21 18:24 V3441JMV
<0.186 mg/Kg - dry 0.186 0.4502,4-Dimethylphenol 1 04/21/21 18:24 V3441JMV
<0.223 mg/Kg - dry 0.223 0.899Di-n-butyl phthalate 1 04/21/21 18:24 V3441JMV
<0.495 mg/Kg - dry 0.495 2.044,6-Dinitro-2-methylphenol 1 04/21/21 18:24 V3441JMV
<0.527 mg/Kg - dry 0.527 2.042,4-Dinitrophenol 1 04/21/21 18:24 V3441JMV
<0.238 mg/Kg - dry 0.238 0.8992,4-Dinitrotoluene 1 04/21/21 18:24 V3441JMV
<0.232 mg/Kg - dry 0.232 0.899
2,6-Dinitrotoluene 1 04/21/21 18:24 V3441JMV
<0.234 mg/Kg - dry 0.234 0.450Di-n-Octyl Phthalate 1 04/21/21 18:24 V3441JMV
<0.010 mg/Kg - dry 0.010 0.899Fluoranthene 1 04/21/21 18:24 V3441JMV
<0.019 mg/Kg - dry 0.019 0.899Fluorene 1 04/21/21 18:24 V3441JMV
<0.197 mg/Kg - dry 0.197 0.899Hexachlorobenzene 1 04/21/21 18:24 V3441JMV
<0.202 mg/Kg - dry 0.202 0.899Hexachlorobutadiene 1 04/21/21 18:24 V3441JMV
<0.309 mg/Kg - dry 0.309 0.899Hexachlorocyclopentadiene 1 04/21/21 18:24 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.142 mg/Kg - dry 0.142 0.899Hexachloroethane 1 04/21/21 18:24 V3441JMV
<0.025 mg/Kg - dry 0.025 0.899Indeno(1,2,3-cd)pyrene 1 04/21/21 18:24 V3441JMV
<0.193 mg/Kg - dry 0.193 0.899Isophorone 1 04/21/21 18:24 V3441JMV
<0.013 mg/Kg - dry 0.013 0.8991-Methylnaphthalene 1 04/21/21 18:24 V3441JMV
<0.017 mg/Kg - dry 0.017 0.8992-Methylnaphthalene 1 04/21/21 18:24 V3441JMV
<0.171 mg/Kg - dry 0.171 0.8992-Methylphenol 1 04/21/21 18:24 V3441JMV
<0.194 mg/Kg - dry 0.194 0.8993&4 Methylphenol 1 04/21/21 18:24 V3441JMV
<0.019 mg/Kg - dry 0.019 0.899Naphthalene 1 04/21/21 18:24 V3441JMV
<0.193 mg/Kg - dry 0.193 0.899
2-Nitroaniline 1 04/21/21 18:24 V3441JMV
<0.163 mg/Kg - dry 0.163 0.8993-Nitroaniline 1 04/21/21 18:24 V3441JMV
<0.140 mg/Kg - dry 0.140 0.4504-Nitroaniline 1 04/21/21 18:24 V3441JMV
<0.190 mg/Kg - dry 0.190 0.450Nitrobenzene 1 04/21/21 18:24 V3441JMV
<0.150 mg/Kg - dry 0.150 0.8992-Nitrophenol 1 04/21/21 18:24 V3441JMV
<0.221 mg/Kg - dry 0.221 0.8994-Nitrophenol 1 04/21/21 18:24 V3441JMV
<0.007 mg/Kg - dry 0.007 0.231N-Nitrosodimethylamine 1 04/21/21 18:24 V3441JMV
<0.246 mg/Kg - dry 0.246 0.899
N-Nitrosodiphenylamine 1 04/21/21 18:24 V3441JMV
<0.207 mg/Kg - dry 0.207 0.899N-Nitroso-di-n-propylamine 1 04/21/21 18:24 V3441JMV
<0.575 mg/Kg - dry 0.575 1.37Pentachlorophenol 1 04/21/21 18:24 V3441JMV
<0.009 mg/Kg - dry 0.009 0.899Phenanthrene 1 04/21/21 18:24 V3441JMV
<0.147 mg/Kg - dry 0.147 0.899Phenol 1 04/21/21 18:24 V3441JMV
<0.013 mg/Kg - dry 0.013 0.899Pyrene 1 04/21/21 18:24 V3441JMV
<0.086 mg/Kg - dry 0.086 0.450Pyridine 1 04/21/21 18:24 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-3
96987 Matrix:
4/15/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.159 mg/Kg - dry 0.159 0.8991,2,4-Trichlorobenzene 1 04/21/21 18:24 V3441JMV
<0.190 mg/Kg - dry 0.190 0.8992,4,5-Trichlorophenol 1 04/21/21 18:24 V3441JMV
<0.217 mg/Kg - dry 0.217 0.8992,4,6-Trichlorophenol 1 04/21/21 18:24 V3441JMV
Surrogate: Phenol-d5 81.5 Limits: 34-121%04/21/21 18:241 JMV V3441
Surrogate: 2-Fluorobiphenyl 88.7 Limits: 44-115%04/21/21 18:241 JMV V3441
Surrogate: 2-Fluorophenol 81.5 Limits: 35-115%04/21/21 18:241 JMV V3441
Surrogate: Nitrobenzene-d5 77.4 Limits: 37-122%04/21/21 18:241 JMV V3441
Surrogate: 4-Terphenyl-d14 83.9 Limits: 54-127%04/21/21 18:241 JMV V3441
Surrogate: 2,4,6-Tribromophenol 97.3 Limits: 39-132%04/21/21 18:241 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<11.4 mg/Kg - dry 11.4 67.7Aliphatic C19-C36 1 04/21/21 23:52 MADEP-EPHZRC
<2.14 mg/Kg - dry 2.14 10.8Aliphatic C5-C8 100 04/19/21 17:15 MADEP-VPHTBL
<0.951 mg/Kg - dry 0.951 10.8Aliphatic C9-C12 100 04/19/21 17:15 MADEP-VPHTBL
4.92 J mg/Kg - dry 3.39 67.7Aliphatic C9-C18 1 04/21/21 23:52 MADEP-EPHZRC
<18.5 mg/Kg - dry 18.5 67.7Aromatic C11-C22 1 04/21/21 23:52 MADEP-EPHZRC
<1.02 mg/Kg - dry 1.02 10.8
Aromatic C9-C10 100 04/19/21 17:15 MADEP-VPHTBL
26.0 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 36 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
25.3 mg/Kg - dry 0.318 9.46Diesel Range Organics (C10-C28)1 04/20/21 17:12 V3407ZRC
Surrogate: OTP Surrogate 80.3 Limits: 31-123%04/20/21 17:121 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
23.0 mg/Kg - dry 0.036 6.76Gasoline Range Organics (C6-C10)50 04/20/21 12:04 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 109 Limits: 50-137%04/20/21 12:0450 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/19/21 14:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 04/19/21 14:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/19/21 14:00 V3256TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/19/21 14:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
0.0007 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/19/21 14:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/19/21 14:00 V3256TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/19/21 14:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/19/21 14:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/19/21 14:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/19/21 14:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/19/21 14:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/19/21 14:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.067Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/19/21 14:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 04/19/21 14:00 V3256TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/19/21 14:00 V3256TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Naphthalene 1 04/19/21 14:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/19/21 14:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/19/21 14:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/19/21 14:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/19/21 14:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2,4-Trichlorobenzene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/19/21 14:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/19/21 14:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/19/21 14:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/19/21 14:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/19/21 14:00 V3256
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/19/21 14:001 TBL V3256
Surrogate: Dibromofluoromethane 102 Limits: 84-123%04/19/21 14:001 TBL V3256
Surrogate: Toluene-d8 117 Limits: 76-129%04/19/21 14:001 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.906Acenaphthene 1 04/21/21 18:47 V3441JMV
<0.017 mg/Kg - dry 0.017 0.906Acenaphthylene 1 04/21/21 18:47 V3441JMV
<0.224 mg/Kg - dry 0.224 0.906Aniline 1 04/21/21 18:47 V3441JMV
<0.010 mg/Kg - dry 0.010 0.906Anthracene 1 04/21/21 18:47 V3441JMV
<0.010 mg/Kg - dry 0.010 0.906Benzo(a)anthracene 1 04/21/21 18:47 V3441JMV
<0.008 mg/Kg - dry 0.008 0.906Benzo(a)pyrene 1 04/21/21 18:47 V3441JMV
<0.008 mg/Kg - dry 0.008 0.906Benzo(b)fluoranthene 1 04/21/21 18:47 V3441JMV
<0.008 mg/Kg - dry 0.008 0.906Benzo(g,h,i)perylene 1 04/21/21 18:47 V3441JMV
<0.009 mg/Kg - dry 0.009 0.906
Benzo(k)fluoranthene 1 04/21/21 18:47 V3441JMV
<0.751 mg/Kg - dry 0.751 2.74Benzoic Acid 1 04/21/21 18:47 V3441JMV
<0.170 mg/Kg - dry 0.170 0.906Benzyl alcohol 1 04/21/21 18:47 V3441JMV
<0.172 mg/Kg - dry 0.172 0.906Bis(2-Chloroethoxy)methane 1 04/21/21 18:47 V3441JMV
<0.145 mg/Kg - dry 0.145 0.906Bis(2-Chloroethyl)ether 1 04/21/21 18:47 V3441JMV
<0.162 mg/Kg - dry 0.162 0.452Bis(2-Chloroisopropyl)ether 1 04/21/21 18:47 V3441JMV
<0.204 mg/Kg - dry 0.204 0.906Bis(2-ethylhexyl)phthalate 1 04/21/21 18:47 V3441JMV
<0.213 mg/Kg - dry 0.213 0.906
4-Bromophenyl phenyl ether 1 04/21/21 18:47 V3441JMV
<0.156 mg/Kg - dry 0.156 0.452Butyl benzyl phthalate 1 04/21/21 18:47 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9064-Chloro-3-methylphenol 1 04/21/21 18:47 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4524-Chloroaniline 1 04/21/21 18:47 V3441JMV
<0.221 mg/Kg - dry 0.221 0.9062-Chloronaphthalene 1 04/21/21 18:47 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9062-Chlorophenol 1 04/21/21 18:47 V3441JMV
<0.278 mg/Kg - dry 0.278 1.384-Chlorophenyl phenyl ether 1 04/21/21 18:47 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.906Chrysene 1 04/21/21 18:47 V3441JMV
<0.026 mg/Kg - dry 0.026 0.906Dibenz(a,h)anthracene 1 04/21/21 18:47 V3441JMV
<0.024 mg/Kg - dry 0.024 0.906Dibenzofuran 1 04/21/21 18:47 V3441JMV
<0.147 mg/Kg - dry 0.147 0.9061,2-Dichlorobenzene 1 04/21/21 18:47 V3441JMV
<0.133 mg/Kg - dry 0.133 0.9061,3-Dichlorobenzene 1 04/21/21 18:47 V3441JMV
<0.143 mg/Kg - dry 0.143 0.4521,4-Dichlorobenzene 1 04/21/21 18:47 V3441JMV
<0.179 mg/Kg - dry 0.179 0.9063,3'-Dichlorobenzidine 1 04/21/21 18:47 V3441JMV
<0.177 mg/Kg - dry 0.177 0.9062,4-Dichlorophenol 1 04/21/21 18:47 V3441JMV
<0.233 mg/Kg - dry 0.233 0.906
Diethyl phthalate 1 04/21/21 18:47 V3441JMV
<0.217 mg/Kg - dry 0.217 0.906Dimethyl phthalate 1 04/21/21 18:47 V3441JMV
<0.187 mg/Kg - dry 0.187 0.4522,4-Dimethylphenol 1 04/21/21 18:47 V3441JMV
<0.225 mg/Kg - dry 0.225 0.906Di-n-butyl phthalate 1 04/21/21 18:47 V3441JMV
<0.498 mg/Kg - dry 0.498 2.054,6-Dinitro-2-methylphenol 1 04/21/21 18:47 V3441JMV
<0.529 mg/Kg - dry 0.529 2.052,4-Dinitrophenol 1 04/21/21 18:47 V3441JMV
<0.240 mg/Kg - dry 0.240 0.9062,4-Dinitrotoluene 1 04/21/21 18:47 V3441JMV
<0.235 mg/Kg - dry 0.235 0.906
2,6-Dinitrotoluene 1 04/21/21 18:47 V3441JMV
<0.235 mg/Kg - dry 0.235 0.452Di-n-Octyl Phthalate 1 04/21/21 18:47 V3441JMV
<0.010 mg/Kg - dry 0.010 0.906Fluoranthene 1 04/21/21 18:47 V3441JMV
<0.019 mg/Kg - dry 0.019 0.906Fluorene 1 04/21/21 18:47 V3441JMV
<0.198 mg/Kg - dry 0.198 0.906Hexachlorobenzene 1 04/21/21 18:47 V3441JMV
<0.204 mg/Kg - dry 0.204 0.906Hexachlorobutadiene 1 04/21/21 18:47 V3441JMV
<0.312 mg/Kg - dry 0.312 0.906Hexachlorocyclopentadiene 1 04/21/21 18:47 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.143 mg/Kg - dry 0.143 0.906Hexachloroethane 1 04/21/21 18:47 V3441JMV
<0.025 mg/Kg - dry 0.025 0.906Indeno(1,2,3-cd)pyrene 1 04/21/21 18:47 V3441JMV
<0.194 mg/Kg - dry 0.194 0.906Isophorone 1 04/21/21 18:47 V3441JMV
<0.013 mg/Kg - dry 0.013 0.9061-Methylnaphthalene 1 04/21/21 18:47 V3441JMV
<0.017 mg/Kg - dry 0.017 0.9062-Methylnaphthalene 1 04/21/21 18:47 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9062-Methylphenol 1 04/21/21 18:47 V3441JMV
<0.195 mg/Kg - dry 0.195 0.9063&4 Methylphenol 1 04/21/21 18:47 V3441JMV
<0.019 mg/Kg - dry 0.019 0.906Naphthalene 1 04/21/21 18:47 V3441JMV
<0.194 mg/Kg - dry 0.194 0.906
2-Nitroaniline 1 04/21/21 18:47 V3441JMV
<0.164 mg/Kg - dry 0.164 0.9063-Nitroaniline 1 04/21/21 18:47 V3441JMV
<0.141 mg/Kg - dry 0.141 0.4524-Nitroaniline 1 04/21/21 18:47 V3441JMV
<0.191 mg/Kg - dry 0.191 0.452Nitrobenzene 1 04/21/21 18:47 V3441JMV
<0.151 mg/Kg - dry 0.151 0.9062-Nitrophenol 1 04/21/21 18:47 V3441JMV
<0.224 mg/Kg - dry 0.224 0.9064-Nitrophenol 1 04/21/21 18:47 V3441JMV
<0.007 mg/Kg - dry 0.007 0.233N-Nitrosodimethylamine 1 04/21/21 18:47 V3441JMV
<0.248 mg/Kg - dry 0.248 0.906
N-Nitrosodiphenylamine 1 04/21/21 18:47 V3441JMV
<0.209 mg/Kg - dry 0.209 0.906N-Nitroso-di-n-propylamine 1 04/21/21 18:47 V3441JMV
<0.579 mg/Kg - dry 0.579 1.38Pentachlorophenol 1 04/21/21 18:47 V3441JMV
<0.009 mg/Kg - dry 0.009 0.906Phenanthrene 1 04/21/21 18:47 V3441JMV
<0.148 mg/Kg - dry 0.148 0.906Phenol 1 04/21/21 18:47 V3441JMV
<0.013 mg/Kg - dry 0.013 0.906Pyrene 1 04/21/21 18:47 V3441JMV
<0.086 mg/Kg - dry 0.086 0.452Pyridine 1 04/21/21 18:47 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-4
96988 Matrix:
4/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.160 mg/Kg - dry 0.160 0.9061,2,4-Trichlorobenzene 1 04/21/21 18:47 V3441JMV
<0.191 mg/Kg - dry 0.191 0.9062,4,5-Trichlorophenol 1 04/21/21 18:47 V3441JMV
<0.220 mg/Kg - dry 0.220 0.9062,4,6-Trichlorophenol 1 04/21/21 18:47 V3441JMV
Surrogate: Phenol-d5 77.3 Limits: 34-121%04/21/21 18:471 JMV V3441
Surrogate: 2-Fluorobiphenyl 82.8 Limits: 44-115%04/21/21 18:471 JMV V3441
Surrogate: 2-Fluorophenol 80.8 Limits: 35-115%04/21/21 18:471 JMV V3441
Surrogate: Nitrobenzene-d5 75.1 Limits: 37-122%04/21/21 18:471 JMV V3441
Surrogate: 4-Terphenyl-d14 79.9 Limits: 54-127%04/21/21 18:471 JMV V3441
Surrogate: 2,4,6-Tribromophenol 90.3 Limits: 39-132%04/21/21 18:471 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.7 J mg/Kg - dry 11.4 67.7Aliphatic C19-C36 1 04/22/21 00:28 MADEP-EPHZRC
<2.16 mg/Kg - dry 2.16 10.9Aliphatic C5-C8 100 04/20/21 07:03 MADEP-VPHTBL
<0.963 mg/Kg - dry 0.963 10.9Aliphatic C9-C12 100 04/20/21 07:03 MADEP-VPHTBL
8.58 J mg/Kg - dry 3.39 67.7Aliphatic C9-C18 1 04/22/21 00:28 MADEP-EPHZRC
<18.5 mg/Kg - dry 18.5 67.7Aromatic C11-C22 1 04/22/21 00:28 MADEP-EPHZRC
<1.03 mg/Kg - dry 1.03 10.9
Aromatic C9-C10 100 04/20/21 07:03 MADEP-VPHTBL
26.9 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 45 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
35.2 mg/Kg - dry 0.321 9.58Diesel Range Organics (C10-C28)1 04/20/21 17:49 V3407ZRC
Surrogate: OTP Surrogate 76.7 Limits: 31-123%04/20/21 17:491 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
0.242 JB mg/Kg - dry 0.037 6.84Gasoline Range Organics (C6-C10)50 04/20/21 12:31 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 98.4 Limits: 50-137%04/20/21 12:3150 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/19/21 14:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromodichloromethane 1 04/19/21 14:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/19/21 14:30 V3256TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/19/21 14:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
0.001 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/19/21 14:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/19/21 14:30 V3256TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/19/21 14:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/19/21 14:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/19/21 14:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/19/21 14:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/19/21 14:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/19/21 14:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/19/21 14:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/19/21 14:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/19/21 14:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.068Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/19/21 14:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/19/21 14:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Methyl tert-butyl ether (MTBE)1 04/19/21 14:30 V3256TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/19/21 14:30 V3256TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/19/21 14:30 V3256TBL
0.001 J mg/Kg - dry 0.0007 0.013Naphthalene 1 04/19/21 14:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/19/21 14:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.006Styrene 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/19/21 14:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/19/21 14:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,4-Trichlorobenzene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/19/21 14:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/19/21 14:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/19/21 14:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/19/21 14:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/19/21 14:30 V3256
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%04/19/21 14:301 TBL V3256
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/19/21 14:301 TBL V3256
Surrogate: Toluene-d8 115 Limits: 76-129%04/19/21 14:301 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.902Acenaphthene 1 04/21/21 19:09 V3441JMV
<0.017 mg/Kg - dry 0.017 0.902Acenaphthylene 1 04/21/21 19:09 V3441JMV
<0.222 mg/Kg - dry 0.222 0.902Aniline 1 04/21/21 19:09 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902Anthracene 1 04/21/21 19:09 V3441JMV
<0.010 mg/Kg - dry 0.010 0.902Benzo(a)anthracene 1 04/21/21 19:09 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(a)pyrene 1 04/21/21 19:09 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(b)fluoranthene 1 04/21/21 19:09 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(g,h,i)perylene 1 04/21/21 19:09 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902
Benzo(k)fluoranthene 1 04/21/21 19:09 V3441JMV
<0.749 mg/Kg - dry 0.749 2.74Benzoic Acid 1 04/21/21 19:09 V3441JMV
<0.169 mg/Kg - dry 0.169 0.902Benzyl alcohol 1 04/21/21 19:09 V3441JMV
<0.172 mg/Kg - dry 0.172 0.902Bis(2-Chloroethoxy)methane 1 04/21/21 19:09 V3441JMV
<0.145 mg/Kg - dry 0.145 0.902Bis(2-Chloroethyl)ether 1 04/21/21 19:09 V3441JMV
<0.161 mg/Kg - dry 0.161 0.451Bis(2-Chloroisopropyl)ether 1 04/21/21 19:09 V3441JMV
<0.203 mg/Kg - dry 0.203 0.902Bis(2-ethylhexyl)phthalate 1 04/21/21 19:09 V3441JMV
<0.212 mg/Kg - dry 0.212 0.902
4-Bromophenyl phenyl ether 1 04/21/21 19:09 V3441JMV
<0.155 mg/Kg - dry 0.155 0.451Butyl benzyl phthalate 1 04/21/21 19:09 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9024-Chloro-3-methylphenol 1 04/21/21 19:09 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4514-Chloroaniline 1 04/21/21 19:09 V3441JMV
<0.220 mg/Kg - dry 0.220 0.9022-Chloronaphthalene 1 04/21/21 19:09 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9022-Chlorophenol 1 04/21/21 19:09 V3441JMV
<0.276 mg/Kg - dry 0.276 1.374-Chlorophenyl phenyl ether 1 04/21/21 19:09 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.902Chrysene 1 04/21/21 19:09 V3441JMV
<0.025 mg/Kg - dry 0.025 0.902Dibenz(a,h)anthracene 1 04/21/21 19:09 V3441JMV
<0.024 mg/Kg - dry 0.024 0.902Dibenzofuran 1 04/21/21 19:09 V3441JMV
<0.146 mg/Kg - dry 0.146 0.9021,2-Dichlorobenzene 1 04/21/21 19:09 V3441JMV
<0.132 mg/Kg - dry 0.132 0.9021,3-Dichlorobenzene 1 04/21/21 19:09 V3441JMV
<0.142 mg/Kg - dry 0.142 0.4511,4-Dichlorobenzene 1 04/21/21 19:09 V3441JMV
<0.179 mg/Kg - dry 0.179 0.9023,3'-Dichlorobenzidine 1 04/21/21 19:09 V3441JMV
<0.176 mg/Kg - dry 0.176 0.9022,4-Dichlorophenol 1 04/21/21 19:09 V3441JMV
<0.232 mg/Kg - dry 0.232 0.902
Diethyl phthalate 1 04/21/21 19:09 V3441JMV
<0.216 mg/Kg - dry 0.216 0.902Dimethyl phthalate 1 04/21/21 19:09 V3441JMV
<0.187 mg/Kg - dry 0.187 0.4512,4-Dimethylphenol 1 04/21/21 19:09 V3441JMV
<0.224 mg/Kg - dry 0.224 0.902Di-n-butyl phthalate 1 04/21/21 19:09 V3441JMV
<0.497 mg/Kg - dry 0.497 2.054,6-Dinitro-2-methylphenol 1 04/21/21 19:09 V3441JMV
<0.529 mg/Kg - dry 0.529 2.052,4-Dinitrophenol 1 04/21/21 19:09 V3441JMV
<0.239 mg/Kg - dry 0.239 0.9022,4-Dinitrotoluene 1 04/21/21 19:09 V3441JMV
<0.233 mg/Kg - dry 0.233 0.902
2,6-Dinitrotoluene 1 04/21/21 19:09 V3441JMV
<0.233 mg/Kg - dry 0.233 0.451Di-n-Octyl Phthalate 1 04/21/21 19:09 V3441JMV
<0.010 mg/Kg - dry 0.010 0.902Fluoranthene 1 04/21/21 19:09 V3441JMV
<0.019 mg/Kg - dry 0.019 0.902Fluorene 1 04/21/21 19:09 V3441JMV
<0.198 mg/Kg - dry 0.198 0.902Hexachlorobenzene 1 04/21/21 19:09 V3441JMV
<0.203 mg/Kg - dry 0.203 0.902Hexachlorobutadiene 1 04/21/21 19:09 V3441JMV
<0.310 mg/Kg - dry 0.310 0.902Hexachlorocyclopentadiene 1 04/21/21 19:09 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.142 mg/Kg - dry 0.142 0.902Hexachloroethane 1 04/21/21 19:09 V3441JMV
<0.025 mg/Kg - dry 0.025 0.902Indeno(1,2,3-cd)pyrene 1 04/21/21 19:09 V3441JMV
<0.194 mg/Kg - dry 0.194 0.902Isophorone 1 04/21/21 19:09 V3441JMV
<0.013 mg/Kg - dry 0.013 0.9021-Methylnaphthalene 1 04/21/21 19:09 V3441JMV
<0.017 mg/Kg - dry 0.017 0.9022-Methylnaphthalene 1 04/21/21 19:09 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9022-Methylphenol 1 04/21/21 19:09 V3441JMV
<0.195 mg/Kg - dry 0.195 0.9023&4 Methylphenol 1 04/21/21 19:09 V3441JMV
<0.019 mg/Kg - dry 0.019 0.902Naphthalene 1 04/21/21 19:09 V3441JMV
<0.194 mg/Kg - dry 0.194 0.902
2-Nitroaniline 1 04/21/21 19:09 V3441JMV
<0.164 mg/Kg - dry 0.164 0.9023-Nitroaniline 1 04/21/21 19:09 V3441JMV
<0.140 mg/Kg - dry 0.140 0.4514-Nitroaniline 1 04/21/21 19:09 V3441JMV
<0.191 mg/Kg - dry 0.191 0.451Nitrobenzene 1 04/21/21 19:09 V3441JMV
<0.150 mg/Kg - dry 0.150 0.9022-Nitrophenol 1 04/21/21 19:09 V3441JMV
<0.222 mg/Kg - dry 0.222 0.9024-Nitrophenol 1 04/21/21 19:09 V3441JMV
<0.007 mg/Kg - dry 0.007 0.232N-Nitrosodimethylamine 1 04/21/21 19:09 V3441JMV
<0.247 mg/Kg - dry 0.247 0.902
N-Nitrosodiphenylamine 1 04/21/21 19:09 V3441JMV
<0.207 mg/Kg - dry 0.207 0.902N-Nitroso-di-n-propylamine 1 04/21/21 19:09 V3441JMV
<0.575 mg/Kg - dry 0.575 1.37Pentachlorophenol 1 04/21/21 19:09 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902Phenanthrene 1 04/21/21 19:09 V3441JMV
<0.147 mg/Kg - dry 0.147 0.902Phenol 1 04/21/21 19:09 V3441JMV
<0.013 mg/Kg - dry 0.013 0.902Pyrene 1 04/21/21 19:09 V3441JMV
<0.086 mg/Kg - dry 0.086 0.451Pyridine 1 04/21/21 19:09 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-5
96989 Matrix:
4/15/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.160 mg/Kg - dry 0.160 0.9021,2,4-Trichlorobenzene 1 04/21/21 19:09 V3441JMV
<0.191 mg/Kg - dry 0.191 0.9022,4,5-Trichlorophenol 1 04/21/21 19:09 V3441JMV
<0.218 mg/Kg - dry 0.218 0.9022,4,6-Trichlorophenol 1 04/21/21 19:09 V3441JMV
Surrogate: Phenol-d5 76.3 Limits: 34-121%04/21/21 19:091 JMV V3441
Surrogate: 2-Fluorobiphenyl 84.3 Limits: 44-115%04/21/21 19:091 JMV V3441
Surrogate: 2-Fluorophenol 77.5 Limits: 35-115%04/21/21 19:091 JMV V3441
Surrogate: Nitrobenzene-d5 74.1 Limits: 37-122%04/21/21 19:091 JMV V3441
Surrogate: 4-Terphenyl-d14 75.3 Limits: 54-127%04/21/21 19:091 JMV V3441
Surrogate: 2,4,6-Tribromophenol 85.9 Limits: 39-132%04/21/21 19:091 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<11.3 mg/Kg - dry 11.3 67.1Aliphatic C19-C36 1 04/22/21 01:05 MADEP-EPHZRC
<2.15 mg/Kg - dry 2.15 10.9Aliphatic C5-C8 100 04/20/21 07:35 MADEP-VPHTBL
<0.956 mg/Kg - dry 0.956 10.9Aliphatic C9-C12 100 04/20/21 07:35 MADEP-VPHTBL
<3.36 mg/Kg - dry 3.36 67.1Aliphatic C9-C18 1 04/22/21 01:05 MADEP-EPHZRC
<18.3 mg/Kg - dry 18.3 67.1Aromatic C11-C22 1 04/22/21 01:05 MADEP-EPHZRC
<1.02 mg/Kg - dry 1.02 10.9
Aromatic C9-C10 100 04/20/21 07:35 MADEP-VPHTBL
26.4 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 54 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
4.18 JB mg/Kg - dry 0.323 9.63Diesel Range Organics (C10-C28)1 04/20/21 18:26 V3407ZRC
Surrogate: OTP Surrogate 75.6 Limits: 31-123%04/20/21 18:261 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
<0.037 mg/Kg - dry 0.037 6.79Gasoline Range Organics (C6-C10)50 04/20/21 12:58 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 101 Limits: 50-137%04/20/21 12:5850 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/19/21 15:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromodichloromethane 1 04/19/21 15:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/19/21 15:00 V3256TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/19/21 15:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/19/21 15:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/19/21 15:00 V3256TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/19/21 15:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/19/21 15:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/19/21 15:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/19/21 15:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/19/21 15:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/19/21 15:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/19/21 15:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/19/21 15:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/19/21 15:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.067Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/19/21 15:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/19/21 15:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Methyl tert-butyl ether (MTBE)1 04/19/21 15:00 V3256TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/19/21 15:00 V3256TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Naphthalene 1 04/19/21 15:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/19/21 15:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.006Styrene 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/19/21 15:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/19/21 15:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,4-Trichlorobenzene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/19/21 15:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/19/21 15:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/19/21 15:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/19/21 15:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/19/21 15:00 V3256
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%04/19/21 15:001 TBL V3256
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/19/21 15:001 TBL V3256
Surrogate: Toluene-d8 115 Limits: 76-129%04/19/21 15:001 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.902Acenaphthene 1 04/21/21 19:31 V3441JMV
<0.017 mg/Kg - dry 0.017 0.902Acenaphthylene 1 04/21/21 19:31 V3441JMV
<0.222 mg/Kg - dry 0.222 0.902Aniline 1 04/21/21 19:31 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902Anthracene 1 04/21/21 19:31 V3441JMV
<0.010 mg/Kg - dry 0.010 0.902Benzo(a)anthracene 1 04/21/21 19:31 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(a)pyrene 1 04/21/21 19:31 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(b)fluoranthene 1 04/21/21 19:31 V3441JMV
<0.008 mg/Kg - dry 0.008 0.902Benzo(g,h,i)perylene 1 04/21/21 19:31 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902
Benzo(k)fluoranthene 1 04/21/21 19:31 V3441JMV
<0.748 mg/Kg - dry 0.748 2.73Benzoic Acid 1 04/21/21 19:31 V3441JMV
<0.169 mg/Kg - dry 0.169 0.902Benzyl alcohol 1 04/21/21 19:31 V3441JMV
<0.172 mg/Kg - dry 0.172 0.902Bis(2-Chloroethoxy)methane 1 04/21/21 19:31 V3441JMV
<0.145 mg/Kg - dry 0.145 0.902Bis(2-Chloroethyl)ether 1 04/21/21 19:31 V3441JMV
<0.161 mg/Kg - dry 0.161 0.451Bis(2-Chloroisopropyl)ether 1 04/21/21 19:31 V3441JMV
<0.203 mg/Kg - dry 0.203 0.902Bis(2-ethylhexyl)phthalate 1 04/21/21 19:31 V3441JMV
<0.211 mg/Kg - dry 0.211 0.902
4-Bromophenyl phenyl ether 1 04/21/21 19:31 V3441JMV
<0.156 mg/Kg - dry 0.156 0.451Butyl benzyl phthalate 1 04/21/21 19:31 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9024-Chloro-3-methylphenol 1 04/21/21 19:31 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4514-Chloroaniline 1 04/21/21 19:31 V3441JMV
<0.220 mg/Kg - dry 0.220 0.9022-Chloronaphthalene 1 04/21/21 19:31 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9022-Chlorophenol 1 04/21/21 19:31 V3441JMV
<0.277 mg/Kg - dry 0.277 1.374-Chlorophenyl phenyl ether 1 04/21/21 19:31 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.902Chrysene 1 04/21/21 19:31 V3441JMV
<0.025 mg/Kg - dry 0.025 0.902Dibenz(a,h)anthracene 1 04/21/21 19:31 V3441JMV
<0.024 mg/Kg - dry 0.024 0.902Dibenzofuran 1 04/21/21 19:31 V3441JMV
<0.146 mg/Kg - dry 0.146 0.9021,2-Dichlorobenzene 1 04/21/21 19:31 V3441JMV
<0.132 mg/Kg - dry 0.132 0.9021,3-Dichlorobenzene 1 04/21/21 19:31 V3441JMV
<0.142 mg/Kg - dry 0.142 0.4511,4-Dichlorobenzene 1 04/21/21 19:31 V3441JMV
<0.179 mg/Kg - dry 0.179 0.9023,3'-Dichlorobenzidine 1 04/21/21 19:31 V3441JMV
<0.176 mg/Kg - dry 0.176 0.9022,4-Dichlorophenol 1 04/21/21 19:31 V3441JMV
<0.232 mg/Kg - dry 0.232 0.902
Diethyl phthalate 1 04/21/21 19:31 V3441JMV
<0.216 mg/Kg - dry 0.216 0.902Dimethyl phthalate 1 04/21/21 19:31 V3441JMV
<0.187 mg/Kg - dry 0.187 0.4512,4-Dimethylphenol 1 04/21/21 19:31 V3441JMV
<0.224 mg/Kg - dry 0.224 0.902Di-n-butyl phthalate 1 04/21/21 19:31 V3441JMV
<0.497 mg/Kg - dry 0.497 2.054,6-Dinitro-2-methylphenol 1 04/21/21 19:31 V3441JMV
<0.529 mg/Kg - dry 0.529 2.052,4-Dinitrophenol 1 04/21/21 19:31 V3441JMV
<0.239 mg/Kg - dry 0.239 0.9022,4-Dinitrotoluene 1 04/21/21 19:31 V3441JMV
<0.233 mg/Kg - dry 0.233 0.902
2,6-Dinitrotoluene 1 04/21/21 19:31 V3441JMV
<0.233 mg/Kg - dry 0.233 0.451Di-n-Octyl Phthalate 1 04/21/21 19:31 V3441JMV
<0.010 mg/Kg - dry 0.010 0.902Fluoranthene 1 04/21/21 19:31 V3441JMV
<0.019 mg/Kg - dry 0.019 0.902Fluorene 1 04/21/21 19:31 V3441JMV
<0.198 mg/Kg - dry 0.198 0.902Hexachlorobenzene 1 04/21/21 19:31 V3441JMV
<0.203 mg/Kg - dry 0.203 0.902Hexachlorobutadiene 1 04/21/21 19:31 V3441JMV
<0.309 mg/Kg - dry 0.309 0.902Hexachlorocyclopentadiene 1 04/21/21 19:31 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.142 mg/Kg - dry 0.142 0.902Hexachloroethane 1 04/21/21 19:31 V3441JMV
<0.025 mg/Kg - dry 0.025 0.902Indeno(1,2,3-cd)pyrene 1 04/21/21 19:31 V3441JMV
<0.194 mg/Kg - dry 0.194 0.902Isophorone 1 04/21/21 19:31 V3441JMV
<0.013 mg/Kg - dry 0.013 0.9021-Methylnaphthalene 1 04/21/21 19:31 V3441JMV
<0.017 mg/Kg - dry 0.017 0.9022-Methylnaphthalene 1 04/21/21 19:31 V3441JMV
<0.172 mg/Kg - dry 0.172 0.9022-Methylphenol 1 04/21/21 19:31 V3441JMV
<0.195 mg/Kg - dry 0.195 0.9023&4 Methylphenol 1 04/21/21 19:31 V3441JMV
<0.019 mg/Kg - dry 0.019 0.902Naphthalene 1 04/21/21 19:31 V3441JMV
<0.194 mg/Kg - dry 0.194 0.902
2-Nitroaniline 1 04/21/21 19:31 V3441JMV
<0.164 mg/Kg - dry 0.164 0.9023-Nitroaniline 1 04/21/21 19:31 V3441JMV
<0.141 mg/Kg - dry 0.141 0.4514-Nitroaniline 1 04/21/21 19:31 V3441JMV
<0.191 mg/Kg - dry 0.191 0.451Nitrobenzene 1 04/21/21 19:31 V3441JMV
<0.150 mg/Kg - dry 0.150 0.9022-Nitrophenol 1 04/21/21 19:31 V3441JMV
<0.222 mg/Kg - dry 0.222 0.9024-Nitrophenol 1 04/21/21 19:31 V3441JMV
<0.007 mg/Kg - dry 0.007 0.232N-Nitrosodimethylamine 1 04/21/21 19:31 V3441JMV
<0.247 mg/Kg - dry 0.247 0.902
N-Nitrosodiphenylamine 1 04/21/21 19:31 V3441JMV
<0.207 mg/Kg - dry 0.207 0.902N-Nitroso-di-n-propylamine 1 04/21/21 19:31 V3441JMV
<0.577 mg/Kg - dry 0.577 1.37Pentachlorophenol 1 04/21/21 19:31 V3441JMV
<0.009 mg/Kg - dry 0.009 0.902Phenanthrene 1 04/21/21 19:31 V3441JMV
<0.148 mg/Kg - dry 0.148 0.902Phenol 1 04/21/21 19:31 V3441JMV
<0.013 mg/Kg - dry 0.013 0.902Pyrene 1 04/21/21 19:31 V3441JMV
<0.086 mg/Kg - dry 0.086 0.451Pyridine 1 04/21/21 19:31 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-6
96990 Matrix:
4/15/2021 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.160 mg/Kg - dry 0.160 0.9021,2,4-Trichlorobenzene 1 04/21/21 19:31 V3441JMV
<0.191 mg/Kg - dry 0.191 0.9022,4,5-Trichlorophenol 1 04/21/21 19:31 V3441JMV
<0.218 mg/Kg - dry 0.218 0.9022,4,6-Trichlorophenol 1 04/21/21 19:31 V3441JMV
Surrogate: Phenol-d5 74.0 Limits: 34-121%04/21/21 19:311 JMV V3441
Surrogate: 2-Fluorobiphenyl 79.8 Limits: 44-115%04/21/21 19:311 JMV V3441
Surrogate: 2-Fluorophenol 76.7 Limits: 35-115%04/21/21 19:311 JMV V3441
Surrogate: Nitrobenzene-d5 70.8 Limits: 37-122%04/21/21 19:311 JMV V3441
Surrogate: 4-Terphenyl-d14 76.8 Limits: 54-127%04/21/21 19:311 JMV V3441
Surrogate: 2,4,6-Tribromophenol 86.3 Limits: 39-132%04/21/21 19:311 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<11.2 mg/Kg - dry 11.2 66.5Aliphatic C19-C36 1 04/22/21 01:41 MADEP-EPHZRC
<2.15 mg/Kg - dry 2.15 10.9Aliphatic C5-C8 100 04/20/21 06:04 MADEP-VPHTBL
<0.959 mg/Kg - dry 0.959 10.9Aliphatic C9-C12 100 04/20/21 06:04 MADEP-VPHTBL
<3.32 mg/Kg - dry 3.32 66.5Aliphatic C9-C18 1 04/22/21 01:41 MADEP-EPHZRC
<18.1 mg/Kg - dry 18.1 66.5Aromatic C11-C22 1 04/22/21 01:41 MADEP-EPHZRC
<1.02 mg/Kg - dry 1.02 10.9
Aromatic C9-C10 100 04/20/21 06:04 MADEP-VPHTBL
26.6 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 63 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
5.44 JB mg/Kg - dry 0.320 9.55Diesel Range Organics (C10-C28)1 04/20/21 19:03 V3407ZRC
Surrogate: OTP Surrogate 73.1 Limits: 31-123%04/20/21 19:031 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
0.083 JB mg/Kg - dry 0.037 6.81Gasoline Range Organics (C6-C10)50 04/20/21 13:26 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 103 Limits: 50-137%04/20/21 13:2650 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.020 mg/Kg - dry 0.020 0.027Acetone 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Benzene 1 04/19/21 15:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromochloromethane 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromodichloromethane 1 04/19/21 15:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 04/19/21 15:30 V3256TBL
<0.003 mg/Kg - dry 0.003 0.013Bromomethane 1 04/19/21 15:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006tert-Butyl benzene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorobenzene 1 04/19/21 15:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.006Chlorodibromomethane 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Chloroform 1 04/19/21 15:30 V3256TBL
<0.002 mg/Kg - dry 0.002 0.013Chloromethane 1 04/19/21 15:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0062-Chlorotoluene 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0064-Chlorotoluene 1 04/19/21 15:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/19/21 15:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2-Dibromo-3-Chloropropane 1 04/19/21 15:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichlorobenzene 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 04/19/21 15:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,4-Dichlorobenzene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dichloroethane 1 04/19/21 15:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloropropane 1 04/19/21 15:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3-Dichloropropane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/19/21 15:30 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.006
trans-1,3-Dichloropropene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Ethylbenzene 1 04/19/21 15:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.068Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.013n-Hexane 1 04/19/21 15:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0272-Hexanone 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.006Isopropylbenzene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.027Methyl Ethyl Ketone (MEK)1 04/19/21 15:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006Methyl tert-butyl ether (MTBE)1 04/19/21 15:30 V3256TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/19/21 15:30 V3256TBL
<0.006 mg/Kg - dry 0.006 0.013Methylene Chloride 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Naphthalene 1 04/19/21 15:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.006n-Propylbenzene 1 04/19/21 15:30 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.006Styrene 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 04/19/21 15:30 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 04/19/21 15:30 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.0131,2,3-Trichlorobenzene 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,4-Trichlorobenzene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,1,2-Trichloroethane 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Trichlorofluoromethane 1 04/19/21 15:30 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2,3-Trichloropropane 1 04/19/21 15:30 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,3,5-Trimethylbenzene 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Acetate 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013Vinyl Chloride 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006
o-Xylene 1 04/19/21 15:30 V3256TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/19/21 15:30 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/19/21 15:30 V3256
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/19/21 15:301 TBL V3256
Surrogate: Dibromofluoromethane 107 Limits: 84-123%04/19/21 15:301 TBL V3256
Surrogate: Toluene-d8 116 Limits: 76-129%04/19/21 15:301 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.020 mg/Kg - dry 0.020 0.904Acenaphthene 1 04/21/21 19:54 V3441JMV
<0.017 mg/Kg - dry 0.017 0.904Acenaphthylene 1 04/21/21 19:54 V3441JMV
<0.223 mg/Kg - dry 0.223 0.904Aniline 1 04/21/21 19:54 V3441JMV
<0.010 mg/Kg - dry 0.010 0.904Anthracene 1 04/21/21 19:54 V3441JMV
<0.010 mg/Kg - dry 0.010 0.904Benzo(a)anthracene 1 04/21/21 19:54 V3441JMV
<0.008 mg/Kg - dry 0.008 0.904Benzo(a)pyrene 1 04/21/21 19:54 V3441JMV
<0.008 mg/Kg - dry 0.008 0.904Benzo(b)fluoranthene 1 04/21/21 19:54 V3441JMV
<0.008 mg/Kg - dry 0.008 0.904Benzo(g,h,i)perylene 1 04/21/21 19:54 V3441JMV
<0.009 mg/Kg - dry 0.009 0.904
Benzo(k)fluoranthene 1 04/21/21 19:54 V3441JMV
<0.750 mg/Kg - dry 0.750 2.74Benzoic Acid 1 04/21/21 19:54 V3441JMV
<0.170 mg/Kg - dry 0.170 0.904Benzyl alcohol 1 04/21/21 19:54 V3441JMV
<0.173 mg/Kg - dry 0.173 0.904Bis(2-Chloroethoxy)methane 1 04/21/21 19:54 V3441JMV
<0.145 mg/Kg - dry 0.145 0.904Bis(2-Chloroethyl)ether 1 04/21/21 19:54 V3441JMV
<0.162 mg/Kg - dry 0.162 0.452Bis(2-Chloroisopropyl)ether 1 04/21/21 19:54 V3441JMV
<0.204 mg/Kg - dry 0.204 0.904Bis(2-ethylhexyl)phthalate 1 04/21/21 19:54 V3441JMV
<0.212 mg/Kg - dry 0.212 0.904
4-Bromophenyl phenyl ether 1 04/21/21 19:54 V3441JMV
<0.156 mg/Kg - dry 0.156 0.452Butyl benzyl phthalate 1 04/21/21 19:54 V3441JMV
<0.173 mg/Kg - dry 0.173 0.9044-Chloro-3-methylphenol 1 04/21/21 19:54 V3441JMV
<0.109 mg/Kg - dry 0.109 0.4524-Chloroaniline 1 04/21/21 19:54 V3441JMV
<0.220 mg/Kg - dry 0.220 0.9042-Chloronaphthalene 1 04/21/21 19:54 V3441JMV
<0.173 mg/Kg - dry 0.173 0.9042-Chlorophenol 1 04/21/21 19:54 V3441JMV
<0.277 mg/Kg - dry 0.277 1.384-Chlorophenyl phenyl ether 1 04/21/21 19:54 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.010 mg/Kg - dry 0.010 0.904Chrysene 1 04/21/21 19:54 V3441JMV
<0.026 mg/Kg - dry 0.026 0.904Dibenz(a,h)anthracene 1 04/21/21 19:54 V3441JMV
<0.024 mg/Kg - dry 0.024 0.904Dibenzofuran 1 04/21/21 19:54 V3441JMV
<0.147 mg/Kg - dry 0.147 0.9041,2-Dichlorobenzene 1 04/21/21 19:54 V3441JMV
<0.133 mg/Kg - dry 0.133 0.9041,3-Dichlorobenzene 1 04/21/21 19:54 V3441JMV
<0.143 mg/Kg - dry 0.143 0.4521,4-Dichlorobenzene 1 04/21/21 19:54 V3441JMV
<0.179 mg/Kg - dry 0.179 0.9043,3'-Dichlorobenzidine 1 04/21/21 19:54 V3441JMV
<0.177 mg/Kg - dry 0.177 0.9042,4-Dichlorophenol 1 04/21/21 19:54 V3441JMV
<0.232 mg/Kg - dry 0.232 0.904
Diethyl phthalate 1 04/21/21 19:54 V3441JMV
<0.216 mg/Kg - dry 0.216 0.904Dimethyl phthalate 1 04/21/21 19:54 V3441JMV
<0.188 mg/Kg - dry 0.188 0.4522,4-Dimethylphenol 1 04/21/21 19:54 V3441JMV
<0.224 mg/Kg - dry 0.224 0.904Di-n-butyl phthalate 1 04/21/21 19:54 V3441JMV
<0.498 mg/Kg - dry 0.498 2.064,6-Dinitro-2-methylphenol 1 04/21/21 19:54 V3441JMV
<0.531 mg/Kg - dry 0.531 2.062,4-Dinitrophenol 1 04/21/21 19:54 V3441JMV
<0.239 mg/Kg - dry 0.239 0.9042,4-Dinitrotoluene 1 04/21/21 19:54 V3441JMV
<0.234 mg/Kg - dry 0.234 0.904
2,6-Dinitrotoluene 1 04/21/21 19:54 V3441JMV
<0.234 mg/Kg - dry 0.234 0.452Di-n-Octyl Phthalate 1 04/21/21 19:54 V3441JMV
<0.010 mg/Kg - dry 0.010 0.904Fluoranthene 1 04/21/21 19:54 V3441JMV
<0.019 mg/Kg - dry 0.019 0.904Fluorene 1 04/21/21 19:54 V3441JMV
<0.198 mg/Kg - dry 0.198 0.904Hexachlorobenzene 1 04/21/21 19:54 V3441JMV
<0.204 mg/Kg - dry 0.204 0.904Hexachlorobutadiene 1 04/21/21 19:54 V3441JMV
<0.310 mg/Kg - dry 0.310 0.904Hexachlorocyclopentadiene 1 04/21/21 19:54 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.143 mg/Kg - dry 0.143 0.904Hexachloroethane 1 04/21/21 19:54 V3441JMV
<0.025 mg/Kg - dry 0.025 0.904Indeno(1,2,3-cd)pyrene 1 04/21/21 19:54 V3441JMV
<0.194 mg/Kg - dry 0.194 0.904Isophorone 1 04/21/21 19:54 V3441JMV
<0.013 mg/Kg - dry 0.013 0.9041-Methylnaphthalene 1 04/21/21 19:54 V3441JMV
<0.017 mg/Kg - dry 0.017 0.9042-Methylnaphthalene 1 04/21/21 19:54 V3441JMV
<0.173 mg/Kg - dry 0.173 0.9042-Methylphenol 1 04/21/21 19:54 V3441JMV
<0.196 mg/Kg - dry 0.196 0.9043&4 Methylphenol 1 04/21/21 19:54 V3441JMV
<0.019 mg/Kg - dry 0.019 0.904Naphthalene 1 04/21/21 19:54 V3441JMV
<0.194 mg/Kg - dry 0.194 0.904
2-Nitroaniline 1 04/21/21 19:54 V3441JMV
<0.164 mg/Kg - dry 0.164 0.9043-Nitroaniline 1 04/21/21 19:54 V3441JMV
<0.141 mg/Kg - dry 0.141 0.4524-Nitroaniline 1 04/21/21 19:54 V3441JMV
<0.192 mg/Kg - dry 0.192 0.452Nitrobenzene 1 04/21/21 19:54 V3441JMV
<0.151 mg/Kg - dry 0.151 0.9042-Nitrophenol 1 04/21/21 19:54 V3441JMV
<0.223 mg/Kg - dry 0.223 0.9044-Nitrophenol 1 04/21/21 19:54 V3441JMV
<0.007 mg/Kg - dry 0.007 0.232N-Nitrosodimethylamine 1 04/21/21 19:54 V3441JMV
<0.247 mg/Kg - dry 0.247 0.904
N-Nitrosodiphenylamine 1 04/21/21 19:54 V3441JMV
<0.208 mg/Kg - dry 0.208 0.904N-Nitroso-di-n-propylamine 1 04/21/21 19:54 V3441JMV
<0.579 mg/Kg - dry 0.579 1.38Pentachlorophenol 1 04/21/21 19:54 V3441JMV
<0.009 mg/Kg - dry 0.009 0.904Phenanthrene 1 04/21/21 19:54 V3441JMV
<0.148 mg/Kg - dry 0.148 0.904Phenol 1 04/21/21 19:54 V3441JMV
<0.013 mg/Kg - dry 0.013 0.904Pyrene 1 04/21/21 19:54 V3441JMV
<0.086 mg/Kg - dry 0.086 0.452Pyridine 1 04/21/21 19:54 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-7
96991 Matrix:
4/15/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.160 mg/Kg - dry 0.160 0.9041,2,4-Trichlorobenzene 1 04/21/21 19:54 V3441JMV
<0.192 mg/Kg - dry 0.192 0.9042,4,5-Trichlorophenol 1 04/21/21 19:54 V3441JMV
<0.219 mg/Kg - dry 0.219 0.9042,4,6-Trichlorophenol 1 04/21/21 19:54 V3441JMV
Surrogate: Phenol-d5 76.4 Limits: 34-121%04/21/21 19:541 JMV V3441
Surrogate: 2-Fluorobiphenyl 81.5 Limits: 44-115%04/21/21 19:541 JMV V3441
Surrogate: 2-Fluorophenol 77.3 Limits: 35-115%04/21/21 19:541 JMV V3441
Surrogate: Nitrobenzene-d5 73.8 Limits: 37-122%04/21/21 19:541 JMV V3441
Surrogate: 4-Terphenyl-d14 76.8 Limits: 54-127%04/21/21 19:541 JMV V3441
Surrogate: 2,4,6-Tribromophenol 86.6 Limits: 39-132%04/21/21 19:541 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<11.8 mg/Kg - dry 11.8 70.0Aliphatic C19-C36 1 04/22/21 02:18 MADEP-EPHZRC
<2.21 mg/Kg - dry 2.21 11.2Aliphatic C5-C8 100 04/20/21 06:33 MADEP-VPHTBL
<0.985 mg/Kg - dry 0.985 11.2Aliphatic C9-C12 100 04/20/21 06:33 MADEP-VPHTBL
<3.50 mg/Kg - dry 3.50 70.0Aliphatic C9-C18 1 04/22/21 02:18 MADEP-EPHZRC
<19.0 mg/Kg - dry 19.0 70.0Aromatic C11-C22 1 04/22/21 02:18 MADEP-EPHZRC
<1.05 mg/Kg - dry 1.05 11.2
Aromatic C9-C10 100 04/20/21 06:33 MADEP-VPHTBL
28.6 %Moisture 1 04/19/21 17:20 SW-DRYWTEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 72 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V3269 04/20/21 08:00
10.2 B mg/Kg - dry 0.329 9.80Diesel Range Organics (C10-C28)1 04/20/21 19:40 V3407ZRC
Surrogate: OTP Surrogate 73.7 Limits: 31-123%04/20/21 19:401 ZRC V3407
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V3285 04/20/21 08:00
0.077 JB mg/Kg - dry 0.038 7.00Gasoline Range Organics (C6-C10)50 04/20/21 13:53 V3286TBL
Surrogate: a,a,a-Trifluorotoluene 96.4 Limits: 50-137%04/20/21 13:5350 TBL V3286
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.021 mg/Kg - dry 0.021 0.028Acetone 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Benzene 1 04/19/21 16:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.007Bromobenzene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007
Bromochloromethane 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromodichloromethane 1 04/19/21 16:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.007Bromoform 1 04/19/21 16:00 V3256TBL
<0.003 mg/Kg - dry 0.003 0.014Bromomethane 1 04/19/21 16:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.007tert-Butyl benzene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Carbon Disulfide 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Carbon Tetrachloride 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorobenzene 1 04/19/21 16:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.007Chlorodibromomethane 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.007
Chloroform 1 04/19/21 16:00 V3256TBL
<0.002 mg/Kg - dry 0.002 0.014Chloromethane 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0072-Chlorotoluene 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0074-Chlorotoluene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2-Dibromo-3-Chloropropane 1 04/19/21 16:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dibromoethane 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.007
Dibromomethane 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dichlorobenzene 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,3-Dichlorobenzene 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dichloroethane 1 04/19/21 16:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0071,2-Dichloropropane 1 04/19/21 16:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichloropropane 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0072,2-Dichloropropane 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.007cis-1,3-Dichloropropene 1 04/19/21 16:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.007
trans-1,3-Dichloropropene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Ethylbenzene 1 04/19/21 16:00 V3256TBL
<0.0006 mg/Kg - dry 0.0006 0.070Ethyl Tertiary Butyl Ether (ETBE)1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.014n-Hexane 1 04/19/21 16:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0282-Hexanone 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.007Isopropylbenzene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007
4-Isopropyl toluene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.028Methyl Ethyl Ketone (MEK)1 04/19/21 16:00 V3256TBL
<0.0010 mg/Kg - dry 0.0010 0.007Methyl tert-butyl ether (MTBE)1 04/19/21 16:00 V3256TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 04/19/21 16:00 V3256TBL
<0.007 mg/Kg - dry 0.007 0.014Methylene Chloride 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.014Naphthalene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007n-Propylbenzene 1 04/19/21 16:00 V3256TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3255 04/19/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.007Styrene 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,1,1,2-Tetrachloroethane 1 04/19/21 16:00 V3256TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Toluene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0141,2,3-Trichlorobenzene 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.0141,2,4-Trichlorobenzene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1-Trichloroethane 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,1,2-Trichloroethane 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014Trichlorofluoromethane 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,2,3-Trichloropropane 1 04/19/21 16:00 V3256TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,3,5-Trimethylbenzene 1 04/19/21 16:00 V3256TBL
<0.0008 mg/Kg - dry 0.0008 0.014Vinyl Acetate 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014Vinyl Chloride 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.007
o-Xylene 1 04/19/21 16:00 V3256TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 04/19/21 16:00 V3256TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 04/19/21 16:00 V3256
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/19/21 16:001 TBL V3256
Surrogate: Dibromofluoromethane 106 Limits: 84-123%04/19/21 16:001 TBL V3256
Surrogate: Toluene-d8 115 Limits: 76-129%04/19/21 16:001 TBL V3256
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.021 mg/Kg - dry 0.021 0.934Acenaphthene 1 04/21/21 20:16 V3441JMV
<0.018 mg/Kg - dry 0.018 0.934Acenaphthylene 1 04/21/21 20:16 V3441JMV
<0.231 mg/Kg - dry 0.231 0.934Aniline 1 04/21/21 20:16 V3441JMV
<0.010 mg/Kg - dry 0.010 0.934Anthracene 1 04/21/21 20:16 V3441JMV
<0.011 mg/Kg - dry 0.011 0.934Benzo(a)anthracene 1 04/21/21 20:16 V3441JMV
<0.008 mg/Kg - dry 0.008 0.934Benzo(a)pyrene 1 04/21/21 20:16 V3441JMV
<0.008 mg/Kg - dry 0.008 0.934Benzo(b)fluoranthene 1 04/21/21 20:16 V3441JMV
<0.009 mg/Kg - dry 0.009 0.934Benzo(g,h,i)perylene 1 04/21/21 20:16 V3441JMV
<0.009 mg/Kg - dry 0.009 0.934
Benzo(k)fluoranthene 1 04/21/21 20:16 V3441JMV
<0.774 mg/Kg - dry 0.774 2.83Benzoic Acid 1 04/21/21 20:16 V3441JMV
<0.175 mg/Kg - dry 0.175 0.934Benzyl alcohol 1 04/21/21 20:16 V3441JMV
<0.177 mg/Kg - dry 0.177 0.934Bis(2-Chloroethoxy)methane 1 04/21/21 20:16 V3441JMV
<0.149 mg/Kg - dry 0.149 0.934Bis(2-Chloroethyl)ether 1 04/21/21 20:16 V3441JMV
<0.166 mg/Kg - dry 0.166 0.466Bis(2-Chloroisopropyl)ether 1 04/21/21 20:16 V3441JMV
<0.211 mg/Kg - dry 0.211 0.934Bis(2-ethylhexyl)phthalate 1 04/21/21 20:16 V3441JMV
<0.219 mg/Kg - dry 0.219 0.934
4-Bromophenyl phenyl ether 1 04/21/21 20:16 V3441JMV
<0.161 mg/Kg - dry 0.161 0.466Butyl benzyl phthalate 1 04/21/21 20:16 V3441JMV
<0.177 mg/Kg - dry 0.177 0.9344-Chloro-3-methylphenol 1 04/21/21 20:16 V3441JMV
<0.113 mg/Kg - dry 0.113 0.4664-Chloroaniline 1 04/21/21 20:16 V3441JMV
<0.228 mg/Kg - dry 0.228 0.9342-Chloronaphthalene 1 04/21/21 20:16 V3441JMV
<0.177 mg/Kg - dry 0.177 0.9342-Chlorophenol 1 04/21/21 20:16 V3441JMV
<0.285 mg/Kg - dry 0.285 1.414-Chlorophenyl phenyl ether 1 04/21/21 20:16 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.011 mg/Kg - dry 0.011 0.934Chrysene 1 04/21/21 20:16 V3441JMV
<0.026 mg/Kg - dry 0.026 0.934Dibenz(a,h)anthracene 1 04/21/21 20:16 V3441JMV
<0.025 mg/Kg - dry 0.025 0.934Dibenzofuran 1 04/21/21 20:16 V3441JMV
<0.151 mg/Kg - dry 0.151 0.9341,2-Dichlorobenzene 1 04/21/21 20:16 V3441JMV
<0.137 mg/Kg - dry 0.137 0.9341,3-Dichlorobenzene 1 04/21/21 20:16 V3441JMV
<0.147 mg/Kg - dry 0.147 0.4661,4-Dichlorobenzene 1 04/21/21 20:16 V3441JMV
<0.184 mg/Kg - dry 0.184 0.9343,3'-Dichlorobenzidine 1 04/21/21 20:16 V3441JMV
<0.182 mg/Kg - dry 0.182 0.9342,4-Dichlorophenol 1 04/21/21 20:16 V3441JMV
<0.240 mg/Kg - dry 0.240 0.934
Diethyl phthalate 1 04/21/21 20:16 V3441JMV
<0.224 mg/Kg - dry 0.224 0.934Dimethyl phthalate 1 04/21/21 20:16 V3441JMV
<0.193 mg/Kg - dry 0.193 0.4662,4-Dimethylphenol 1 04/21/21 20:16 V3441JMV
<0.232 mg/Kg - dry 0.232 0.934Di-n-butyl phthalate 1 04/21/21 20:16 V3441JMV
<0.516 mg/Kg - dry 0.516 2.134,6-Dinitro-2-methylphenol 1 04/21/21 20:16 V3441JMV
<0.549 mg/Kg - dry 0.549 2.132,4-Dinitrophenol 1 04/21/21 20:16 V3441JMV
<0.247 mg/Kg - dry 0.247 0.9342,4-Dinitrotoluene 1 04/21/21 20:16 V3441JMV
<0.242 mg/Kg - dry 0.242 0.934
2,6-Dinitrotoluene 1 04/21/21 20:16 V3441JMV
<0.242 mg/Kg - dry 0.242 0.466Di-n-Octyl Phthalate 1 04/21/21 20:16 V3441JMV
<0.010 mg/Kg - dry 0.010 0.934Fluoranthene 1 04/21/21 20:16 V3441JMV
<0.020 mg/Kg - dry 0.020 0.934Fluorene 1 04/21/21 20:16 V3441JMV
<0.205 mg/Kg - dry 0.205 0.934Hexachlorobenzene 1 04/21/21 20:16 V3441JMV
<0.211 mg/Kg - dry 0.211 0.934Hexachlorobutadiene 1 04/21/21 20:16 V3441JMV
<0.320 mg/Kg - dry 0.320 0.934Hexachlorocyclopentadiene 1 04/21/21 20:16 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.147 mg/Kg - dry 0.147 0.934Hexachloroethane 1 04/21/21 20:16 V3441JMV
<0.026 mg/Kg - dry 0.026 0.934Indeno(1,2,3-cd)pyrene 1 04/21/21 20:16 V3441JMV
<0.201 mg/Kg - dry 0.201 0.934Isophorone 1 04/21/21 20:16 V3441JMV
<0.014 mg/Kg - dry 0.014 0.9341-Methylnaphthalene 1 04/21/21 20:16 V3441JMV
<0.018 mg/Kg - dry 0.018 0.9342-Methylnaphthalene 1 04/21/21 20:16 V3441JMV
<0.177 mg/Kg - dry 0.177 0.9342-Methylphenol 1 04/21/21 20:16 V3441JMV
<0.203 mg/Kg - dry 0.203 0.9343&4 Methylphenol 1 04/21/21 20:16 V3441JMV
<0.019 mg/Kg - dry 0.019 0.934Naphthalene 1 04/21/21 20:16 V3441JMV
<0.201 mg/Kg - dry 0.201 0.934
2-Nitroaniline 1 04/21/21 20:16 V3441JMV
<0.169 mg/Kg - dry 0.169 0.9343-Nitroaniline 1 04/21/21 20:16 V3441JMV
<0.145 mg/Kg - dry 0.145 0.4664-Nitroaniline 1 04/21/21 20:16 V3441JMV
<0.197 mg/Kg - dry 0.197 0.466Nitrobenzene 1 04/21/21 20:16 V3441JMV
<0.155 mg/Kg - dry 0.155 0.9342-Nitrophenol 1 04/21/21 20:16 V3441JMV
<0.231 mg/Kg - dry 0.231 0.9344-Nitrophenol 1 04/21/21 20:16 V3441JMV
<0.007 mg/Kg - dry 0.007 0.240N-Nitrosodimethylamine 1 04/21/21 20:16 V3441JMV
<0.256 mg/Kg - dry 0.256 0.934
N-Nitrosodiphenylamine 1 04/21/21 20:16 V3441JMV
<0.215 mg/Kg - dry 0.215 0.934N-Nitroso-di-n-propylamine 1 04/21/21 20:16 V3441JMV
<0.595 mg/Kg - dry 0.595 1.41Pentachlorophenol 1 04/21/21 20:16 V3441JMV
<0.010 mg/Kg - dry 0.010 0.934Phenanthrene 1 04/21/21 20:16 V3441JMV
<0.152 mg/Kg - dry 0.152 0.934Phenol 1 04/21/21 20:16 V3441JMV
<0.013 mg/Kg - dry 0.013 0.934Pyrene 1 04/21/21 20:16 V3441JMV
<0.089 mg/Kg - dry 0.089 0.466Pyridine 1 04/21/21 20:16 V3441JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 112
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27615
21-106-0032
00055
Highland Environmental Solutions
8410-D Falls of Neuse Road
Joe Beaman
Raleigh
Received : 04/16/2021
186481
Report Date : 04/23/2021
Sample ID :
Lab No :
Sampled:S-8
96992 Matrix:
4/15/2021 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3284 04/20/21 11:48
<0.165 mg/Kg - dry 0.165 0.9341,2,4-Trichlorobenzene 1 04/21/21 20:16 V3441JMV
<0.197 mg/Kg - dry 0.197 0.9342,4,5-Trichlorophenol 1 04/21/21 20:16 V3441JMV
<0.226 mg/Kg - dry 0.226 0.9342,4,6-Trichlorophenol 1 04/21/21 20:16 V3441JMV
Surrogate: Phenol-d5 66.5 Limits: 34-121%04/21/21 20:161 JMV V3441
Surrogate: 2-Fluorobiphenyl 72.0 Limits: 44-115%04/21/21 20:161 JMV V3441
Surrogate: 2-Fluorophenol 67.1 Limits: 35-115%04/21/21 20:161 JMV V3441
Surrogate: Nitrobenzene-d5 64.3 Limits: 37-122%04/21/21 20:161 JMV V3441
Surrogate: 4-Terphenyl-d14 72.0 Limits: 54-127%04/21/21 20:161 JMV V3441
Surrogate: 2,4,6-Tribromophenol 74.5 Limits: 39-132%04/21/21 20:161 JMV V3441
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V3407QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3269
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3269 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/20/21 13:307.000.2351.61mg/KgDiesel Range Organics (C10-C28)
04/20/21 13:30OTP Surrogate (S)75.9 31-123
LCS-V3269Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.955.366.7mg/KgDiesel Range Organics (C10-C28)46-126
80.4OTP Surrogate (S)31-123
V 97092-MS-V3269 V 97092-MSD-V3269Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2560 1270*205066.466.41720mg/KgDiesel Range Organics (C10-C28)497*50-117 22.1 24
0.0*OTP Surrogate (S)0.0*31-123
Page 1 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 81 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V3286QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V3285
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3285 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/20/21 09:475.000.0270.285mg/KgGasoline Range Organics (C6-C10)
04/20/21 09:47a,a,a-Trifluorotoluene (S)101 50-137
LCS-V3285Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
13668.150.0mg/KgGasoline Range Organics (C6-C10)41-138
118a,a,a-Trifluorotoluene (S)50-137
V 96985-MS-V3285 V 96985-MSD-V3285Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
119 204*73.650.050.016.8mg/KgGasoline Range Organics (C6-C10)114 41-138 47.1*34
104a,a,a-Trifluorotoluene (S)104 50-137
Page 2 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 82 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
Associated Lab Samples: 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3255 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/19/21 12:300.0200.015<0.015mg/KgAcetone
04/19/21 12:300.0200.0009<0.0009mg/KgAcrolein
04/19/21 12:300.0200.001<0.001mg/KgAcrylonitrile
04/19/21 12:300.0050.0008<0.0008mg/KgBenzene
04/19/21 12:300.0050.0007<0.0007mg/KgBromobenzene
04/19/21 12:300.0050.0008<0.0008mg/KgBromochloromethane
04/19/21 12:300.0050.0005<0.0005mg/KgBromodichloromethane
04/19/21 12:300.0050.0004<0.0004mg/KgBromoform
04/19/21 12:300.0100.002<0.002mg/KgBromomethane
04/19/21 12:300.0050.0005<0.0005mg/Kgn-Butylbenzene
04/19/21 12:300.0050.0005<0.0005mg/Kgsec-Butyl benzene
04/19/21 12:300.0050.0006<0.0006mg/Kgtert-Butyl benzene
04/19/21 12:300.0050.0009<0.0009mg/KgCarbon Disulfide
04/19/21 12:300.0050.0010<0.0010mg/KgCarbon Tetrachloride
04/19/21 12:300.0050.0008<0.0008mg/KgChlorobenzene
04/19/21 12:300.0050.0003<0.0003mg/KgChlorodibromomethane
04/19/21 12:300.0100.0010<0.0010mg/KgChloroethane
04/19/21 12:300.0050.0006<0.0006mg/KgChloroform
04/19/21 12:300.0100.001<0.001mg/KgChloromethane
04/19/21 12:300.0050.0007<0.0007mg/Kg2-Chlorotoluene
04/19/21 12:300.0050.0006<0.0006mg/Kg4-Chlorotoluene
04/19/21 12:300.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/19/21 12:300.0100.0006<0.0006mg/Kg1,2-Dibromo-3-Chloropropane
04/19/21 12:300.0050.0005<0.0005mg/Kg1,2-Dibromoethane
04/19/21 12:300.0050.0006<0.0006mg/KgDibromomethane
04/19/21 12:300.0050.0006<0.0006mg/Kg1,2-Dichlorobenzene
04/19/21 12:300.0050.0006<0.0006mg/Kg1,3-Dichlorobenzene
Page 3 of 30Date:04/23/2021 12:35 PM
Page 83 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
Associated Lab Samples: 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3255 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/19/21 12:300.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/19/21 12:300.0100.001<0.001mg/KgDichlorodifluoromethane
04/19/21 12:300.0050.0009<0.0009mg/Kg1,1-Dichloroethane
04/19/21 12:300.0050.0006<0.0006mg/Kg1,2-Dichloroethane
04/19/21 12:300.0050.0009<0.0009mg/Kg1,1-Dichloroethene
04/19/21 12:300.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/19/21 12:300.0050.0010<0.0010mg/Kgtrans-1,2-Dichloroethene
04/19/21 12:300.0050.0008<0.0008mg/Kg1,2-Dichloropropane
04/19/21 12:300.0050.0004<0.0004mg/Kg1,3-Dichloropropane
04/19/21 12:300.0050.0006<0.0006mg/Kg2,2-Dichloropropane
04/19/21 12:300.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/19/21 12:300.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/19/21 12:300.0050.0004<0.0004mg/Kgtrans-1,3-Dichloropropene
04/19/21 12:300.0050.0008<0.0008mg/KgEthylbenzene
04/19/21 12:300.0500.0004<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/19/21 12:300.0100.0008<0.0008mg/KgHexachlorobutadiene
04/19/21 12:300.0100.0006<0.0006mg/Kgn-Hexane
04/19/21 12:300.0200.0004<0.0004mg/Kg2-Hexanone
04/19/21 12:300.0050.0006<0.0006mg/KgIsopropylbenzene
04/19/21 12:300.0050.001<0.001mg/Kg4-Isopropyl toluene
04/19/21 12:300.0200.001<0.001mg/KgMethyl Ethyl Ketone (MEK)
04/19/21 12:300.0050.0007<0.0007mg/KgMethyl tert-butyl ether (MTBE)
04/19/21 12:300.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/19/21 12:300.0100.005<0.005mg/KgMethylene Chloride
04/19/21 12:300.0100.0005<0.0005mg/KgNaphthalene
04/19/21 12:300.0050.0007<0.0007mg/Kgn-Propylbenzene
04/19/21 12:300.0050.0005<0.0005mg/KgStyrene
Page 4 of 30Date:04/23/2021 12:35 PM
Page 84 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
Associated Lab Samples: 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3255 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/19/21 12:300.0050.0006<0.0006mg/Kg1,1,1,2-Tetrachloroethane
04/19/21 12:300.0050.0004<0.0004mg/Kg1,1,2,2-Tetrachloroethane
04/19/21 12:300.0050.0009<0.0009mg/KgTetrachloroethene
04/19/21 12:300.0050.0008<0.0008mg/KgToluene
04/19/21 12:300.0100.0007<0.0007mg/Kg1,2,3-Trichlorobenzene
04/19/21 12:300.0100.0005<0.0005mg/Kg1,2,4-Trichlorobenzene
04/19/21 12:300.0050.0007<0.0007mg/Kg1,1,1-Trichloroethane
04/19/21 12:300.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/19/21 12:300.0050.0010<0.0010mg/KgTrichloroethene
04/19/21 12:300.0100.001<0.001mg/KgTrichlorofluoromethane
04/19/21 12:300.0050.0006<0.0006mg/Kg1,2,3-Trichloropropane
04/19/21 12:300.0050.0006<0.0006mg/Kg1,3,5-Trimethylbenzene
04/19/21 12:300.0100.0005<0.0005mg/KgVinyl Acetate
04/19/21 12:300.0100.0010<0.0010mg/KgVinyl Chloride
04/19/21 12:300.0050.0005<0.0005mg/Kgo-Xylene
04/19/21 12:300.0100.001<0.001mg/Kgm,p-Xylene
04/19/21 12:304-Bromofluorobenzene (S)101 70-130
04/19/21 12:30Dibromofluoromethane (S)102 84-123
04/19/21 12:30Toluene-d8 (S)114 76-129
LCS-V3255 LCSD-V3255Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.064 64.060.40.0600.100mg/KgAcetone 29-198 5.7 20
0.099 99.195.00.0950.100mg/KgAcrolein 70-130 4.2 20
0.095 95.389.60.0890.100mg/KgAcrylonitrile 65-134 6.1 20
Page 5 of 30Date:04/23/2021 12:35 PM
Page 85 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
LCS-V3255 LCSD-V3255Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.039 79.283.40.0410.050mg/KgBenzene 74-127 5.1 20
0.057 1141130.0560.050mg/KgBromobenzene 73-125 0.8 20
0.038 76.479.40.0390.050mg/KgBromochloromethane 72-134 3.8 20
0.041 83.085.20.0420.050mg/KgBromodichloromethane 75-122 2.6 20
0.050 10291.80.0450.050mg/KgBromoform 66-135 10.3 20
0.040 80.874.60.0370.050mg/KgBromomethane 20-180 7.9 20
0.056 1131190.0590.050mg/Kgn-Butylbenzene 65-135 4.6 20
0.054 1091160.0570.050mg/Kgsec-Butyl benzene 66-131 5.5 20
0.053 1071130.0560.050mg/Kgtert-Butyl benzene 67-132 5.8 20
0.041 82.689.20.0440.050mg/KgCarbon Disulfide 61-129 7.6 20
0.037 74.477.20.0380.050mg/KgCarbon Tetrachloride 64-143 3.6 20
0.047 95.698.00.0490.050mg/KgChlorobenzene 74-118 2.4 20
0.047 95.293.00.0460.050mg/KgChlorodibromomethane 73-122 2.3 20
0.041 82.892.80.0460.050mg/KgChloroethane 33-149 11.3 20
0.039 78.080.40.0400.050mg/KgChloroform 73-127 3.0 20
0.039 79.084.20.0420.050mg/KgChloromethane 45-143 6.3 20
0.056 1121140.0570.050mg/Kg2-Chlorotoluene 67-124 1.5 20
0.056 1121140.0570.050mg/Kg4-Chlorotoluene 71-126 1.7 20
0.041 83.484.20.0420.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.9 20
0.061 1221150.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.9 20
0.051 10299.20.0490.050mg/Kg1,2-Dibromoethane 70-132 2.9 20
0.041 82.083.60.0410.050mg/KgDibromomethane 74-133 1.9 20
0.057 1141130.0560.050mg/Kg1,2-Dichlorobenzene 72-123 1.4 20
0.054 1091130.0560.050mg/Kg1,3-Dichlorobenzene 71-120 3.9 20
0.056 1121150.0570.050mg/Kg1,4-Dichlorobenzene 71-123 2.2 20
0.043 86.094.20.0470.050mg/KgDichlorodifluoromethane 26-146 9.1 20
Page 6 of 30Date:04/23/2021 12:35 PM
Page 86 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
LCS-V3255 LCSD-V3255Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 76.881.20.0400.050mg/Kg1,1-Dichloroethane 74-127 5.5 20
0.039 78.680.40.0400.050mg/Kg1,2-Dichloroethane 68-128 2.2 20
0.036 72.277.40.0380.050mg/Kg1,1-Dichloroethene 67-149 6.9 20
0.039 79.280.40.0400.050mg/Kgcis-1,2-Dichloroethene 76-134 1.5 20
0.038 76.881.20.0400.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.5 20
0.042 84.086.40.0430.050mg/Kg1,2-Dichloropropane 73-130 2.8 20
0.050 10096.80.0480.050mg/Kg1,3-Dichloropropane 75-124 3.2 20
0.036 73.279.60.0390.050mg/Kg2,2-Dichloropropane 50-142 8.3 20
0.037 75.081.60.0400.050mg/Kg1,1-Dichloropropene 71-130 8.4 20
0.043 86.290.20.0450.050mg/Kgcis-1,3-Dichloropropene 71-125 4.5 20
0.043 86.885.80.0420.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.1 20
0.046 93.095.40.0470.050mg/KgEthylbenzene 74-128 2.5 20
0.086 86.587.10.0870.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.052 1051110.0550.050mg/KgHexachlorobutadiene 64-125 5.7 20
0.041 82.694.00.0470.050mg/Kgn-Hexane 70-130 12.9 20
0.053 10797.60.0480.050mg/Kg2-Hexanone 61-157 9.0 20
0.053 1081130.0560.050mg/KgIsopropylbenzene 68-126 4.8 20
0.055 1101150.0570.050mg/Kg4-Isopropyl toluene 68-129 4.2 20
0.041 83.078.40.0390.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.7 20
0.043 87.485.60.0420.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.0 20
0.045 90.686.60.0430.050mg/Kg4-Methyl-2-Pentanone 57-162 4.5 20
0.037 75.674.00.0370.050mg/KgMethylene Chloride 74-129 2.1 20
0.060 1221170.0580.050mg/KgNaphthalene 57-157 4.0 20
0.054 1101150.0570.050mg/Kgn-Propylbenzene 67-130 4.9 20
0.049 99.299.60.0490.050mg/KgStyrene 77-121 0.4 20
0.048 96.895.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.8 20
Page 7 of 30Date:04/23/2021 12:35 PM
Page 87 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3256QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3255
LCS-V3255 LCSD-V3255Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.060 1221190.0590.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.1 20
0.039 79.082.60.0410.050mg/KgTetrachloroethene 68-130 4.4 20
0.040 81.284.00.0420.050mg/KgToluene 71-129 3.3 20
0.056 1121110.0550.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.5 20
0.056 1121140.0560.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.4 20
0.036 73.678.60.0390.050mg/Kg1,1,1-Trichloroethane 67-131 6.5 20
0.050 10199.00.0490.050mg/Kg1,1,2-Trichloroethane 70-133 1.8 20
0.040 81.487.20.0430.050mg/KgTrichloroethene 75-133 6.8 20
0.038 76.085.60.0420.050mg/KgTrichlorofluoromethane 44-146 11.8 20
0.058 1171120.0560.050mg/Kg1,2,3-Trichloropropane 60-137 4.0 20
0.053 1081130.0560.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.8 20
0.048 97.498.40.0490.050mg/KgVinyl Acetate 85-161 1.0 20
0.041 82.088.20.0440.050mg/KgVinyl Chloride 48-147 7.2 20
0.047 94.696.80.0480.050mg/Kgo-Xylene 74-126 2.2 20
0.095 95.697.10.0970.100mg/Kgm,p-Xylene 75-124 1.5 20
1031024-Bromofluorobenzene (S)70-130
10498.2Dibromofluoromethane (S)84-123
116115Toluene-d8 (S)76-129
Page 8 of 30Date:04/23/2021 12:35 PM
Page 88 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
Associated Lab Samples: 96985, 96986
LRB-V3303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/20/21 11:240.0200.015<0.015mg/KgAcetone
04/20/21 11:240.0200.0009<0.0009mg/KgAcrolein
04/20/21 11:240.0200.001<0.001mg/KgAcrylonitrile
04/20/21 11:240.0050.0008<0.0008mg/KgBenzene
04/20/21 11:240.0050.0007<0.0007mg/KgBromobenzene
04/20/21 11:240.0050.0008<0.0008mg/KgBromochloromethane
04/20/21 11:240.0050.0005<0.0005mg/KgBromodichloromethane
04/20/21 11:240.0050.0004<0.0004mg/KgBromoform
04/20/21 11:240.0100.002<0.002mg/KgBromomethane
04/20/21 11:240.0050.0005<0.0005mg/Kgn-Butylbenzene
04/20/21 11:240.0050.0005<0.0005mg/Kgsec-Butyl benzene
04/20/21 11:240.0050.0006<0.0006mg/Kgtert-Butyl benzene
04/20/21 11:240.0050.0009<0.0009mg/KgCarbon Disulfide
04/20/21 11:240.0050.0010<0.0010mg/KgCarbon Tetrachloride
04/20/21 11:240.0050.0008<0.0008mg/KgChlorobenzene
04/20/21 11:240.0050.0003<0.0003mg/KgChlorodibromomethane
04/20/21 11:240.0100.0010<0.0010mg/KgChloroethane
04/20/21 11:240.0050.0006<0.0006mg/KgChloroform
04/20/21 11:240.0100.001<0.001mg/KgChloromethane
04/20/21 11:240.0050.0007<0.0007mg/Kg2-Chlorotoluene
04/20/21 11:240.0050.0006<0.0006mg/Kg4-Chlorotoluene
04/20/21 11:240.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/20/21 11:240.0100.0006<0.0006mg/Kg1,2-Dibromo-3-Chloropropane
04/20/21 11:240.0050.0005<0.0005mg/Kg1,2-Dibromoethane
04/20/21 11:240.0050.0006<0.0006mg/KgDibromomethane
04/20/21 11:240.0050.0006<0.0006mg/Kg1,2-Dichlorobenzene
04/20/21 11:240.0050.0006<0.0006mg/Kg1,3-Dichlorobenzene
Page 9 of 30Date:04/23/2021 12:35 PM
Page 89 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
Associated Lab Samples: 96985, 96986
LRB-V3303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/20/21 11:240.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/20/21 11:240.0100.001<0.001mg/KgDichlorodifluoromethane
04/20/21 11:240.0050.0009<0.0009mg/Kg1,1-Dichloroethane
04/20/21 11:240.0050.0006<0.0006mg/Kg1,2-Dichloroethane
04/20/21 11:240.0050.0009<0.0009mg/Kg1,1-Dichloroethene
04/20/21 11:240.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/20/21 11:240.0050.0010<0.0010mg/Kgtrans-1,2-Dichloroethene
04/20/21 11:240.0050.0008<0.0008mg/Kg1,2-Dichloropropane
04/20/21 11:240.0050.0004<0.0004mg/Kg1,3-Dichloropropane
04/20/21 11:240.0050.0006<0.0006mg/Kg2,2-Dichloropropane
04/20/21 11:240.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/20/21 11:240.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/20/21 11:240.0050.0004<0.0004mg/Kgtrans-1,3-Dichloropropene
04/20/21 11:240.0050.0008<0.0008mg/KgEthylbenzene
04/20/21 11:240.0500.0004<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/20/21 11:240.0100.0008<0.0008mg/KgHexachlorobutadiene
04/20/21 11:240.0100.0006<0.0006mg/Kgn-Hexane
04/20/21 11:240.0200.0004<0.0004mg/Kg2-Hexanone
04/20/21 11:240.0050.0006<0.0006mg/KgIsopropylbenzene
04/20/21 11:240.0050.001<0.001mg/Kg4-Isopropyl toluene
04/20/21 11:240.0200.001<0.001mg/KgMethyl Ethyl Ketone (MEK)
04/20/21 11:240.0050.0007<0.0007mg/KgMethyl tert-butyl ether (MTBE)
04/20/21 11:240.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/20/21 11:240.0100.005<0.005mg/KgMethylene Chloride
04/20/21 11:240.0100.0005<0.0005mg/KgNaphthalene
04/20/21 11:240.0050.0007<0.0007mg/Kgn-Propylbenzene
04/20/21 11:240.0050.0005<0.0005mg/KgStyrene
Page 10 of 30Date:04/23/2021 12:35 PM
Page 90 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
Associated Lab Samples: 96985, 96986
LRB-V3303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/20/21 11:240.0050.0006<0.0006mg/Kg1,1,1,2-Tetrachloroethane
04/20/21 11:240.0050.0004<0.0004mg/Kg1,1,2,2-Tetrachloroethane
04/20/21 11:240.0050.0009<0.0009mg/KgTetrachloroethene
04/20/21 11:240.0050.0008<0.0008mg/KgToluene
04/20/21 11:240.0100.0007<0.0007mg/Kg1,2,3-Trichlorobenzene
04/20/21 11:240.0100.0005<0.0005mg/Kg1,2,4-Trichlorobenzene
04/20/21 11:240.0050.0007<0.0007mg/Kg1,1,1-Trichloroethane
04/20/21 11:240.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/20/21 11:240.0050.0010<0.0010mg/KgTrichloroethene
04/20/21 11:240.0100.001<0.001mg/KgTrichlorofluoromethane
04/20/21 11:240.0050.0006<0.0006mg/Kg1,2,3-Trichloropropane
04/20/21 11:240.0050.0006<0.0006mg/Kg1,3,5-Trimethylbenzene
04/20/21 11:240.0100.0005<0.0005mg/KgVinyl Acetate
04/20/21 11:240.0100.0010<0.0010mg/KgVinyl Chloride
04/20/21 11:240.0050.0005<0.0005mg/Kgo-Xylene
04/20/21 11:240.0100.001<0.001mg/Kgm,p-Xylene
04/20/21 11:244-Bromofluorobenzene (S)105 70-130
04/20/21 11:24Dibromofluoromethane (S)104 84-123
04/20/21 11:24Toluene-d8 (S)118 76-129
LCS-V3303Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
54.90.0540.100mg/KgAcetone 29-198
85.20.0850.100mg/KgAcrolein 70-130
84.20.0840.100mg/KgAcrylonitrile 65-134
82.00.0410.050mg/KgBenzene 74-127
Page 11 of 30Date:04/23/2021 12:35 PM
Page 91 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
LCS-V3303Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1160.0580.050mg/KgBromobenzene 73-125
78.00.0390.050mg/KgBromochloromethane 72-134
84.80.0420.050mg/KgBromodichloromethane 75-122
94.20.0470.050mg/KgBromoform 66-135
82.40.0410.050mg/KgBromomethane 20-180
1240.0620.050mg/Kgn-Butylbenzene 65-135
1200.0590.050mg/Kgsec-Butyl benzene 66-131
1170.0580.050mg/Kgtert-Butyl benzene 67-132
87.80.0430.050mg/KgCarbon Disulfide 61-129
80.00.0400.050mg/KgCarbon Tetrachloride 64-143
96.40.0480.050mg/KgChlorobenzene 74-118
92.80.0460.050mg/KgChlorodibromomethane 73-122
87.20.0430.050mg/KgChloroethane 33-149
80.00.0400.050mg/KgChloroform 73-127
86.60.0430.050mg/KgChloromethane 45-143
1180.0590.050mg/Kg2-Chlorotoluene 67-124
1180.0590.050mg/Kg4-Chlorotoluene 71-126
84.60.0420.050mg/KgDi-Isopropyl Ether (DIPE)59-159
1110.0550.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157
95.20.0470.050mg/Kg1,2-Dibromoethane 70-132
83.40.0410.050mg/KgDibromomethane 74-133
1180.0580.050mg/Kg1,2-Dichlorobenzene 72-123
1160.0570.050mg/Kg1,3-Dichlorobenzene 71-120
1150.0570.050mg/Kg1,4-Dichlorobenzene 71-123
89.80.0440.050mg/KgDichlorodifluoromethane 26-146
81.00.0400.050mg/Kg1,1-Dichloroethane 74-127
79.20.0390.050mg/Kg1,2-Dichloroethane 68-128
Page 12 of 30Date:04/23/2021 12:35 PM
Page 92 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
LCS-V3303Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.60.0390.050mg/Kg1,1-Dichloroethene 67-149
81.40.0400.050mg/Kgcis-1,2-Dichloroethene 76-134
82.00.0410.050mg/Kgtrans-1,2-Dichloroethene 73-132
82.40.0410.050mg/Kg1,2-Dichloropropane 73-130
96.60.0480.050mg/Kg1,3-Dichloropropane 75-124
79.40.0390.050mg/Kg2,2-Dichloropropane 50-142
83.40.0410.050mg/Kg1,1-Dichloropropene 71-130
87.20.0430.050mg/Kgcis-1,3-Dichloropropene 71-125
86.40.0430.050mg/Kgtrans-1,3-Dichloropropene 68-123
97.60.0480.050mg/KgEthylbenzene 74-128
86.20.0860.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130
1220.0600.050mg/KgHexachlorobutadiene 64-125
92.40.0460.050mg/Kgn-Hexane 70-130
91.80.0450.050mg/Kg2-Hexanone 61-157
1170.0580.050mg/KgIsopropylbenzene 68-126
1190.0590.050mg/Kg4-Isopropyl toluene 68-129
69.80.0340.050mg/KgMethyl Ethyl Ketone (MEK)63-149
83.60.0410.050mg/KgMethyl tert-butyl ether (MTBE)70-130
82.60.0410.050mg/Kg4-Methyl-2-Pentanone 57-162
79.20.0390.050mg/KgMethylene Chloride 74-129
1190.0590.050mg/KgNaphthalene 57-157
1190.0590.050mg/Kgn-Propylbenzene 67-130
98.60.0490.050mg/KgStyrene 77-121
95.80.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115
1180.0580.050mg/Kg1,1,2,2-Tetrachloroethane 56-126
83.60.0410.050mg/KgTetrachloroethene 68-130
83.40.0410.050mg/KgToluene 71-129
Page 13 of 30Date:04/23/2021 12:35 PM
Page 93 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
LCS-V3303Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1140.0570.050mg/Kg1,2,3-Trichlorobenzene 68-130
1160.0570.050mg/Kg1,2,4-Trichlorobenzene 66-125
80.00.0400.050mg/Kg1,1,1-Trichloroethane 67-131
97.40.0480.050mg/Kg1,1,2-Trichloroethane 70-133
86.00.0430.050mg/KgTrichloroethene 75-133
88.00.0440.050mg/KgTrichlorofluoromethane 44-146
1100.0550.050mg/Kg1,2,3-Trichloropropane 60-137
1170.0580.050mg/Kg1,3,5-Trimethylbenzene 69-128
89.60.0440.050mg/KgVinyl Acetate 85-161
90.00.0450.050mg/KgVinyl Chloride 48-147
96.60.0480.050mg/Kgo-Xylene 74-126
98.10.0980.100mg/Kgm,p-Xylene 75-124
1054-Bromofluorobenzene (S)70-130
107Dibromofluoromethane (S)84-123
118Toluene-d8 (S)76-129
V 96985-MS-V3303 V 96985-MSD-V3303Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.029 29.8*0.0300.1000.100<0.015mg/KgAcetone 30.3*34-143 1.6 49
0.007 0.0*0.0050.1000.100<0.0009mg/KgAcrolein 0.0*70-130 0.0 20
0.050 50.5*0.0520.1000.100<0.001mg/KgAcrylonitrile 52.0*65-134 2.9 30
0.033 66.00.0330.0500.050<0.0008mg/KgBenzene 66.0 60-135 0.0 20
0.035 70.20.0370.0500.050<0.0007mg/KgBromobenzene 75.0 45-135 6.6 25
0.034 69.00.0340.0500.050<0.0008mg/KgBromochloromethane 68.4 55-136 0.8 18
0.028 57.40.0290.0500.050<0.0005mg/KgBromodichloromethane 58.0 55-127 1.0 17
Page 14 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 94 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
V 96985-MS-V3303 V 96985-MSD-V3303Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.031 63.00.0310.0500.050<0.0004mg/KgBromoform 63.6 40-136 0.9 35
0.024 48.80.0280.0500.050<0.002mg/KgBromomethane 56.2 30-137 14.0 30
0.034 68.00.0350.0500.0500.001mg/Kgn-Butylbenzene 70.8 23-148 4.0 39
0.029 58.80.0310.0500.0500.0009mg/Kgsec-Butyl benzene 62.0 34-144 5.2 28
0.030 60.80.0330.0500.050<0.0006mg/Kgtert-Butyl benzene 66.0 36-150 8.2 29
0.034 68.00.0330.0500.050<0.0009mg/KgCarbon Disulfide 67.0 49-139 1.4 26
0.027 55.80.0290.0500.050<0.0010mg/KgCarbon Tetrachloride 58.0 48-153 3.8 23
0.033 67.60.0350.0500.050<0.0008mg/KgChlorobenzene 71.4 57-125 5.4 14
0.033 66.80.0350.0500.050<0.0003mg/KgChlorodibromomethane 70.6 49-127 5.5 24
0.035 71.00.0350.0500.050<0.0010mg/KgChloroethane 71.4 16-177 0.5 47
0.031 62.40.0320.0500.050<0.0006mg/KgChloroform 64.4 56-137 3.1 18
0.024 49.00.0250.0500.050<0.001mg/KgChloromethane 51.0 40-145 4.0 26
0.032 65.80.0340.0500.050<0.0007mg/Kg2-Chlorotoluene 69.4 46-132 5.3 29
0.032 65.80.0340.0500.050<0.0006mg/Kg4-Chlorotoluene 69.2 44-135 5.0 23
0.031 62.00.0310.0500.050<0.0007mg/KgDi-Isopropyl Ether (DIPE)62.0 51-155 0.0 13
0.035 70.20.0390.0500.050<0.0006mg/Kg1,2-Dibromo-3-Chloropropane 79.4 27-132 12.2 25
0.035 71.60.0360.0500.050<0.0005mg/Kg1,2-Dibromoethane 72.8 49-132 1.6 15
0.031 63.00.0310.0500.050<0.0006mg/KgDibromomethane 62.2 59-133 1.2 15
0.030 61.60.0320.0500.050<0.0006mg/Kg1,2-Dichlorobenzene 65.6 42-130 6.2 21
0.031 63.60.0340.0500.050<0.0006mg/Kg1,3-Dichlorobenzene 69.0 41-129 8.1 24
0.032 64.40.0330.0500.050<0.0006mg/Kg1,4-Dichlorobenzene 67.6 44-134 4.8 21
0.017 35.60.0170.0500.050<0.001mg/KgDichlorodifluoromethane 34.2 25-151 4.0 37
0.034 69.20.0340.0500.050<0.0009mg/Kg1,1-Dichloroethane 69.0 59-137 0.2 21
0.028 56.00.0280.0500.050<0.0006mg/Kg1,2-Dichloroethane 56.6 51-131 1.0 13
0.032 65.60.0320.0500.050<0.0009mg/Kg1,1-Dichloroethene 65.6 54-162 0.0 22
0.031 62.20.0300.0500.050<0.0008mg/Kgcis-1,2-Dichloroethene 61.2 58-140 1.6 28
Page 15 of 30Date:04/23/2021 12:35 PM
Page 95 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
V 96985-MS-V3303 V 96985-MSD-V3303Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.032 64.40.0320.0500.050<0.0010mg/Kgtrans-1,2-Dichloroethene 65.4 57-141 1.5 18
0.034 68.60.0340.0500.050<0.0008mg/Kg1,2-Dichloropropane 69.8 55-138 1.7 16
0.037 74.20.0370.0500.050<0.0004mg/Kg1,3-Dichloropropane 74.4 53-129 0.2 15
0.030 61.20.0300.0500.050<0.0006mg/Kg2,2-Dichloropropane 60.4 30-147 1.3 20
0.032 64.60.0320.0500.050<0.0008mg/Kg1,1-Dichloropropene 64.4 55-137 0.3 19
0.031 62.00.0300.0500.050<0.0005mg/Kgcis-1,3-Dichloropropene 61.8 42-135 0.3 32
0.028 56.80.0280.0500.050<0.0004mg/Kgtrans-1,3-Dichloropropene 57.8 41-124 1.7 20
0.031 62.00.0320.0500.050<0.0008mg/KgEthylbenzene 64.8 44-144 4.4 19
0.064 64.6*0.0640.1000.100<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)64.1*70-130 0.7 20
0.017 34.80.0190.0500.050<0.0008mg/KgHexachlorobutadiene 38.0 30-126 8.7 26
0.024 48.8*0.0230.0500.050<0.0006mg/Kgn-Hexane 47.0*70-130 3.7 20
0.021 42.20.0210.0500.050<0.0004mg/Kg2-Hexanone 43.2 30-147 2.3 42
0.033 66.20.0350.0500.050<0.0006mg/KgIsopropylbenzene 70.2 41-140 5.8 27
0.044 88.40.0440.0500.0500.004mg/Kg4-Isopropyl toluene 89.8 32-144 1.5 22
0.018 0.0*0.0200.0500.050<0.001mg/KgMethyl Ethyl Ketone (MEK)40.2 24-160 0.4 42
0.030 61.20.0300.0500.050<0.0007mg/KgMethyl tert-butyl ether (MTBE)61.6 49-135 0.6 22
0.025 51.80.0260.0500.050<0.015mg/Kg4-Methyl-2-Pentanone 52.0 25-163 0.3 44
0.032 64.00.0320.0500.050<0.005mg/KgMethylene Chloride 64.0 53-144 0.0 14
0.025 50.60.0250.0500.0500.005mg/KgNaphthalene 50.8 32-127 0.3 44
0.030 61.80.0320.0500.050<0.0007mg/Kgn-Propylbenzene 65.0 35-144 5.0 27
0.030 60.00.0290.0500.050<0.0005mg/KgStyrene 58.8 42-132 2.0 28
0.033 66.60.0350.0500.050<0.0006mg/Kg1,1,1,2-Tetrachloroethane 71.0 60-120 6.3 15
0.043 86.80.0450.0500.050<0.0004mg/Kg1,1,2,2-Tetrachloroethane 91.6 39-135 5.3 22
0.028 56.00.0280.0500.050<0.0009mg/KgTetrachloroethene 57.8 47-142 3.1 26
0.030 60.80.0310.0500.050<0.0008mg/KgToluene 62.8 57-135 3.2 22
0.022 45.80.0240.0500.050<0.0007mg/Kg1,2,3-Trichlorobenzene 48.0 34-120 4.6 41
Page 16 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 96 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3304QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3303
V 96985-MS-V3303 V 96985-MSD-V3303Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.021 43.60.0230.0500.050<0.0005mg/Kg1,2,4-Trichlorobenzene 46.8 35-116 7.0 62
0.028 57.20.0300.0500.050<0.0007mg/Kg1,1,1-Trichloroethane 61.8 52-139 7.7 21
0.039 78.80.0400.0500.050<0.0005mg/Kg1,1,2-Trichloroethane 81.0 44-140 2.7 21
0.033 66.20.0320.0500.050<0.0010mg/KgTrichloroethene 64.2 38-164 3.0 18
0.028 56.40.0280.0500.050<0.001mg/KgTrichlorofluoromethane 56.6 30-157 0.3 27
0.041 83.20.0430.0500.050<0.0006mg/Kg1,2,3-Trichloropropane 86.8 45-139 4.2 25
0.033 66.20.0350.0500.050<0.0006mg/Kg1,3,5-Trimethylbenzene 70.2 44-140 5.8 29
0.004 0.0*0.0030.0500.050<0.0005mg/KgVinyl Acetate 0.0*61-154 0.0 35
0.027 54.60.0270.0500.050<0.0010mg/KgVinyl Chloride 54.2 40-156 0.7 35
0.031 62.80.0330.0500.050<0.0005mg/Kgo-Xylene 67.0 43-143 6.4 17
0.058 58.20.0580.1000.100<0.001mg/Kgm,p-Xylene 58.8 36-148 1.0 20
99.64-Bromofluorobenzene (S)103 70-130
100Dibromofluoromethane (S)102 84-123
117Toluene-d8 (S)118 76-129
Page 17 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 97 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3284 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/21/21 15:470.6600.015<0.015mg/KgAcenaphthene
04/21/21 15:470.6600.013<0.013mg/KgAcenaphthylene
04/21/21 15:470.6600.163<0.163mg/KgAniline
04/21/21 15:470.6600.007<0.007mg/KgAnthracene
04/21/21 15:470.6600.007<0.007mg/KgBenzo(a)anthracene
04/21/21 15:470.6600.005<0.005mg/KgBenzo(a)pyrene
04/21/21 15:470.6600.006<0.006mg/KgBenzo(b)fluoranthene
04/21/21 15:470.6600.006<0.006mg/KgBenzo(g,h,i)perylene
04/21/21 15:470.6600.007<0.007mg/KgBenzo(k)fluoranthene
04/21/21 15:472.000.548<0.548mg/KgBenzoic Acid
04/21/21 15:470.6600.124<0.124mg/KgBenzyl alcohol
04/21/21 15:470.6600.126<0.126mg/KgBis(2-Chloroethoxy)methane
04/21/21 15:470.6600.106<0.106mg/KgBis(2-Chloroethyl)ether
04/21/21 15:470.3300.118<0.118mg/KgBis(2-Chloroisopropyl)ether
04/21/21 15:470.6600.149<0.149mg/KgBis(2-ethylhexyl)phthalate
04/21/21 15:470.6600.155<0.155mg/Kg4-Bromophenyl phenyl ether
04/21/21 15:470.3300.114<0.114mg/KgButyl benzyl phthalate
04/21/21 15:470.6600.126<0.126mg/Kg4-Chloro-3-methylphenol
04/21/21 15:470.3300.080<0.080mg/Kg4-Chloroaniline
04/21/21 15:470.6600.161<0.161mg/Kg2-Chloronaphthalene
04/21/21 15:470.6600.126<0.126mg/Kg2-Chlorophenol
04/21/21 15:471.000.202<0.202mg/Kg4-Chlorophenyl phenyl ether
04/21/21 15:470.6600.007<0.007mg/KgChrysene
04/21/21 15:470.6600.019<0.019mg/KgDibenz(a,h)anthracene
04/21/21 15:470.6600.017<0.017mg/KgDibenzofuran
04/21/21 15:470.6600.107<0.107mg/Kg1,2-Dichlorobenzene
04/21/21 15:470.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 18 of 30Date:04/23/2021 12:35 PM
Page 98 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3284 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/21/21 15:470.3300.104<0.104mg/Kg1,4-Dichlorobenzene
04/21/21 15:470.6600.131<0.131mg/Kg3,3'-Dichlorobenzidine
04/21/21 15:470.6600.129<0.129mg/Kg2,4-Dichlorophenol
04/21/21 15:470.6600.170<0.170mg/KgDiethyl phthalate
04/21/21 15:470.6600.158<0.158mg/KgDimethyl phthalate
04/21/21 15:470.3300.137<0.137mg/Kg2,4-Dimethylphenol
04/21/21 15:470.6600.164<0.164mg/KgDi-n-butyl phthalate
04/21/21 15:471.500.364<0.364mg/Kg4,6-Dinitro-2-methylphenol
04/21/21 15:471.500.387<0.387mg/Kg2,4-Dinitrophenol
04/21/21 15:470.6600.175<0.175mg/Kg2,4-Dinitrotoluene
04/21/21 15:470.6600.171<0.171mg/Kg2,6-Dinitrotoluene
04/21/21 15:470.3300.171<0.171mg/KgDi-n-Octyl Phthalate
04/21/21 15:470.6600.007<0.007mg/KgFluoranthene
04/21/21 15:470.6600.014<0.014mg/KgFluorene
04/21/21 15:470.6600.145<0.145mg/KgHexachlorobenzene
04/21/21 15:470.6600.149<0.149mg/KgHexachlorobutadiene
04/21/21 15:470.6600.227<0.227mg/KgHexachlorocyclopentadiene
04/21/21 15:470.6600.104<0.104mg/KgHexachloroethane
04/21/21 15:470.6600.018<0.018mg/KgIndeno(1,2,3-cd)pyrene
04/21/21 15:470.6600.142<0.142mg/KgIsophorone
04/21/21 15:470.6600.010<0.010mg/Kg1-Methylnaphthalene
04/21/21 15:470.6600.012<0.012mg/Kg2-Methylnaphthalene
04/21/21 15:470.6600.126<0.126mg/Kg2-Methylphenol
04/21/21 15:470.6600.143<0.143mg/Kg3&4 Methylphenol
04/21/21 15:470.6600.014<0.014mg/KgNaphthalene
04/21/21 15:470.6600.142<0.142mg/Kg2-Nitroaniline
04/21/21 15:470.6600.120<0.120mg/Kg3-Nitroaniline
Page 19 of 30Date:04/23/2021 12:35 PM
Page 99 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3284 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/21/21 15:470.3300.103<0.103mg/Kg4-Nitroaniline
04/21/21 15:470.3300.140<0.140mg/KgNitrobenzene
04/21/21 15:470.6600.110<0.110mg/Kg2-Nitrophenol
04/21/21 15:470.6600.163<0.163mg/Kg4-Nitrophenol
04/21/21 15:470.1700.005<0.005mg/KgN-Nitrosodimethylamine
04/21/21 15:470.6600.181<0.181mg/KgN-Nitrosodiphenylamine
04/21/21 15:470.6600.152<0.152mg/KgN-Nitroso-di-n-propylamine
04/21/21 15:471.000.421<0.421mg/KgPentachlorophenol
04/21/21 15:470.6600.007<0.007mg/KgPhenanthrene
04/21/21 15:470.6600.108<0.108mg/KgPhenol
04/21/21 15:470.6600.009<0.009mg/KgPyrene
04/21/21 15:470.3300.063<0.063mg/KgPyridine
04/21/21 15:470.6600.117<0.117mg/Kg1,2,4-Trichlorobenzene
04/21/21 15:470.6600.140<0.140mg/Kg2,4,5-Trichlorophenol
04/21/21 15:470.6600.160<0.160mg/Kg2,4,6-Trichlorophenol
04/21/21 15:472-Fluorobiphenyl (S)95.8 44-115
04/21/21 15:472-Fluorophenol (S)91.8 35-115
04/21/21 15:47Nitrobenzene-d5 (S)86.8 37-122
04/21/21 15:474-Terphenyl-d14 (S)97.0 54-127
04/21/21 15:472,4,6-Tribromophenol (S)102 39-132
04/21/21 15:47Phenol-d5 (S)91.5 34-121
LCS-V3284Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.01.621.67mg/KgAcenaphthene 40-123
1021.711.67mg/KgAcenaphthylene 32-132
Page 20 of 30Date:04/23/2021 12:35 PM
Page 100 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
LCS-V3284Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.61.431.67mg/KgAniline 12-197
1011.681.67mg/KgAnthracene 47-123
97.61.631.67mg/KgBenzo(a)anthracene 49-126
1212.021.67mg/KgBenzo(a)pyrene 45-129
1071.791.67mg/KgBenzo(b)fluoranthene 45-132
1041.731.67mg/KgBenzo(g,h,i)perylene 43-134
1051.761.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.141.67mg/KgBenzoic Acid 10-83
1011.681.67mg/KgBenzyl alcohol 29-122
92.21.541.67mg/KgBis(2-Chloroethoxy)methane 36-121
85.61.431.67mg/KgBis(2-Chloroethyl)ether 31-120
88.61.481.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1041.741.67mg/KgBis(2-ethylhexyl)phthalate 51-133
98.21.641.67mg/Kg4-Bromophenyl phenyl ether 46-124
1071.791.67mg/KgButyl benzyl phthalate 48-132
89.81.501.67mg/Kg4-Chloro-3-methylphenol 45-122
76.01.271.67mg/Kg4-Chloroaniline 17-106
97.61.631.67mg/Kg2-Chloronaphthalene 41-114
94.61.581.67mg/Kg2-Chlorophenol 34-121
98.81.651.67mg/Kg4-Chlorophenyl phenyl ether 45-121
98.81.651.67mg/KgChrysene 50-124
94.61.581.67mg/KgDibenz(a,h)anthracene 45-134
98.21.641.67mg/KgDibenzofuran 44-120
82.61.381.67mg/Kg1,2-Dichlorobenzene 33-117
80.21.341.67mg/Kg1,3-Dichlorobenzene 30-115
79.61.331.67mg/Kg1,4-Dichlorobenzene 31-115
98.81.651.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 21 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 101 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
LCS-V3284Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/Kg2,4-Dichlorophenol 40-122
1011.681.67mg/KgDiethyl phthalate 50-124
97.61.631.67mg/KgDimethyl phthalate 48-124
94.01.571.67mg/Kg2,4-Dimethylphenol 30-127
1091.821.67mg/KgDi-n-butyl phthalate 51-128
1041.731.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1051.761.67mg/Kg2,4-Dinitrophenol 27-129
1021.701.67mg/Kg2,4-Dinitrotoluene 48-126
1041.731.67mg/Kg2,6-Dinitrotoluene 46-124
1081.811.67mg/KgDi-n-Octyl Phthalate 45-140
99.41.661.67mg/KgFluoranthene 50-127
98.81.651.67mg/KgFluorene 43-125
99.41.661.67mg/KgHexachlorobenzene 45-122
80.81.351.67mg/KgHexachlorobutadiene 32-123
76.01.271.67mg/KgHexachlorocyclopentadiene 32-117
81.41.361.67mg/KgHexachloroethane 28-117
1021.711.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
77.21.291.67mg/KgIsophorone 30-122
81.41.361.67mg/Kg1-Methylnaphthalene 40-119
81.41.361.67mg/Kg2-Methylnaphthalene 38-122
93.41.561.67mg/Kg2-Methylphenol 32-122
83.81.401.67mg/Kg3&4 Methylphenol 34-119
77.21.291.67mg/KgNaphthalene 35-123
99.41.661.67mg/Kg2-Nitroaniline 44-127
95.81.601.67mg/Kg3-Nitroaniline 33-119
1001.671.67mg/Kg4-Nitroaniline 63-147
78.41.311.67mg/KgNitrobenzene 34-122
Page 22 of 30Date:04/23/2021 12:35 PM
Page 102 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
LCS-V3284Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2-Nitrophenol 36-123
1141.911.67mg/Kg4-Nitrophenol 30-132
57.00.9521.67mg/KgN-Nitrosodimethylamine 10-146
1181.971.67mg/KgN-Nitrosodiphenylamine 38-127
88.01.471.67mg/KgN-Nitroso-di-n-propylamine 36-120
1171.951.67mg/KgPentachlorophenol 25-133
98.81.651.67mg/KgPhenanthrene 50-121
84.41.411.67mg/KgPhenol 34-121
1021.701.67mg/KgPyrene 47-127
45.50.7611.67mg/KgPyridine 10-60
77.21.291.67mg/Kg1,2,4-Trichlorobenzene 34-118
94.61.581.67mg/Kg2,4,5-Trichlorophenol 41-124
1001.671.67mg/Kg2,4,6-Trichlorophenol 39-126
97.62-Fluorobiphenyl (S)44-115
93.92-Fluorophenol (S)35-115
77.2Nitrobenzene-d5 (S)37-122
92.24-Terphenyl-d14 (S)54-127
1072,4,6-Tribromophenol (S)39-132
91.8Phenol-d5 (S)34-121
V 96999-MS-V3284 V 96999-MSD-V3284Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.81 1081.741.691.67<0.015mg/KgAcenaphthene 103 40-123 3.9 20
1.87 1121.841.691.67<0.013mg/KgAcenaphthylene 109 32-132 1.6 20
1.43 85.61.441.691.67<0.163mg/KgAniline 85.2 12-197 0.6 20
Page 23 of 30Date:04/23/2021 12:35 PM
Page 103 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
V 96999-MS-V3284 V 96999-MSD-V3284Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.78 1071.751.691.67<0.007mg/KgAnthracene 104 47-123 1.6 20
1.73 1041.721.691.67<0.007mg/KgBenzo(a)anthracene 102 49-126 0.5 20
2.16 129*2.131.691.67<0.005mg/KgBenzo(a)pyrene 126 45-129 1.3 20
1.89 1131.871.691.67<0.006mg/KgBenzo(b)fluoranthene 111 45-132 1.0 20
1.85 1111.811.691.67<0.006mg/KgBenzo(g,h,i)perylene 107 43-134 2.1 20
1.89 1131.841.691.67<0.007mg/KgBenzo(k)fluoranthene 109 47-132 2.6 20
0.706 0.0*0.8171.691.67<0.548mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.80 1081.811.691.67<0.124mg/KgBenzyl alcohol 107 29-122 0.5 20
1.67 1001.641.691.67<0.126mg/KgBis(2-Chloroethoxy)methane 97.0 36-121 1.8 20
1.52 91.01.531.691.67<0.106mg/KgBis(2-Chloroethyl)ether 90.5 31-120 0.6 20
1.61 96.41.601.691.67<0.118mg/KgBis(2-Chloroisopropyl)ether 94.6 33-131 0.6 20
1.86 1111.841.691.67<0.149mg/KgBis(2-ethylhexyl)phthalate 109 51-133 1.0 20
1.76 1051.711.691.67<0.155mg/Kg4-Bromophenyl phenyl ether 101 46-124 2.8 20
1.92 1151.871.691.67<0.114mg/KgButyl benzyl phthalate 111 48-132 2.6 20
1.61 96.41.621.691.67<0.126mg/Kg4-Chloro-3-methylphenol 95.8 45-122 0.6 20
1.38 82.61.361.691.67<0.080mg/Kg4-Chloroaniline 80.4 17-106 1.4 20
1.77 1061.761.691.67<0.161mg/Kg2-Chloronaphthalene 104 41-114 0.5 20
1.74 1041.701.691.67<0.126mg/Kg2-Chlorophenol 101 34-121 2.3 20
1.79 1071.781.691.67<0.202mg/Kg4-Chlorophenyl phenyl ether 105 45-121 0.5 20
1.76 1051.711.691.67<0.007mg/KgChrysene 101 50-124 2.8 20
1.69 1011.631.691.67<0.019mg/KgDibenz(a,h)anthracene 96.4 45-134 3.6 20
1.77 1061.741.691.67<0.017mg/KgDibenzofuran 103 44-120 1.7 20
1.52 91.01.531.691.67<0.107mg/Kg1,2-Dichlorobenzene 90.5 33-117 0.6 20
1.50 89.81.511.691.67<0.097mg/Kg1,3-Dichlorobenzene 89.3 30-115 0.6 20
1.50 89.81.481.691.67<0.104mg/Kg1,4-Dichlorobenzene 87.5 31-115 1.3 20
1.82 1091.771.691.67<0.131mg/Kg3,3'-Dichlorobenzidine 105 22-121 2.7 20
Page 24 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 104 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
V 96999-MS-V3284 V 96999-MSD-V3284Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.60 95.81.571.691.67<0.129mg/Kg2,4-Dichlorophenol 92.8 40-122 1.8 20
1.81 1081.771.691.67<0.170mg/KgDiethyl phthalate 105 50-124 2.2 20
1.75 1051.741.691.67<0.158mg/KgDimethyl phthalate 103 48-124 0.5 30
1.68 1011.691.691.67<0.137mg/Kg2,4-Dimethylphenol 100 30-127 0.5 20
1.91 1141.891.691.67<0.164mg/KgDi-n-butyl phthalate 112 51-128 1.0 20
1.79 1071.811.691.67<0.364mg/Kg4,6-Dinitro-2-methylphenol 107 29-132 1.1 20
1.71 1021.761.691.67<0.387mg/Kg2,4-Dinitrophenol 104 27-129 2.8 20
1.81 1081.791.691.67<0.175mg/Kg2,4-Dinitrotoluene 106 48-126 1.1 20
1.86 1111.861.691.67<0.171mg/Kg2,6-Dinitrotoluene 110 46-124 0.0 20
1.93 1161.901.691.67<0.172mg/KgDi-n-Octyl Phthalate 112 45-140 1.5 20
1.75 1051.741.691.67<0.007mg/KgFluoranthene 103 50-127 0.5 20
1.80 1081.801.691.67<0.014mg/KgFluorene 107 43-125 0.0 20
1.76 1051.741.691.67<0.145mg/KgHexachlorobenzene 103 45-122 1.1 20
1.47 88.01.481.691.67<0.149mg/KgHexachlorobutadiene 87.5 32-123 0.6 20
1.36 81.41.391.691.67<0.227mg/KgHexachlorocyclopentadiene 82.2 32-117 2.1 20
1.50 89.81.521.691.67<0.104mg/KgHexachloroethane 89.9 28-117 1.3 20
1.82 1091.771.691.67<0.018mg/KgIndeno(1,2,3-cd)pyrene 105 45-133 2.7 20
1.38 82.61.381.691.67<0.142mg/KgIsophorone 81.6 30-122 0.0 20
1.47 88.01.481.691.67<0.010mg/Kg1-Methylnaphthalene 87.5 40-119 0.6 20
1.49 89.21.471.691.67<0.012mg/Kg2-Methylnaphthalene 86.9 38-122 1.3 20
1.72 1031.721.691.67<0.126mg/Kg2-Methylphenol 102 32-122 0.0 20
1.51 90.41.481.691.67<0.143mg/Kg3&4 Methylphenol 87.5 34-119 2.0 20
1.40 83.81.401.691.67<0.014mg/KgNaphthalene 82.8 35-123 0.0 20
1.80 1081.771.691.67<0.142mg/Kg2-Nitroaniline 105 44-127 1.6 20
1.74 1041.711.691.67<0.120mg/Kg3-Nitroaniline 101 33-119 1.7 20
1.76 1051.751.691.67<0.103mg/Kg4-Nitroaniline 104 63-147 0.5 20
Page 25 of 30Date:04/23/2021 12:35 PM
Page 105 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3441QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3284
V 96999-MS-V3284 V 96999-MSD-V3284Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.441.691.67<0.140mg/KgNitrobenzene 85.2 34-122 0.6 20
1.45 86.81.441.691.67<0.110mg/Kg2-Nitrophenol 85.2 32-123 0.6 20
2.02 1212.001.691.67<0.163mg/Kg4-Nitrophenol 118 30-132 0.9 20
0.881 52.71.361.691.67<0.005mg/KgN-Nitrosodimethylamine 80.4 10-146 42.7*30
2.12 1272.081.691.67<0.181mg/KgN-Nitrosodiphenylamine 123 38-127 1.9 20
1.58 94.61.591.691.67<0.152mg/KgN-Nitroso-di-n-propylamine 94.0 36-120 0.6 20
1.95 1172.011.691.67<0.421mg/KgPentachlorophenol 119 25-133 3.0 20
1.75 1051.741.691.67<0.007mg/KgPhenanthrene 103 50-121 0.5 20
1.55 92.81.521.691.67<0.108mg/KgPhenol 89.9 34-121 1.9 20
1.83 1101.791.691.67<0.009mg/KgPyrene 106 47-127 2.2 20
0.767 45.90.8711.691.67<0.063mg/KgPyridine 51.5 10-60 12.6 20
1.43 85.61.421.691.67<0.117mg/Kg1,2,4-Trichlorobenzene 84.0 34-118 0.7 20
1.76 1051.721.691.67<0.140mg/Kg2,4,5-Trichlorophenol 102 41-124 2.2 20
1.81 1081.821.691.67<0.160mg/Kg2,4,6-Trichlorophenol 108 39-126 0.5 20
1082-Fluorobiphenyl (S)105 44-115
1022-Fluorophenol (S)99.7 35-115
84.4Nitrobenzene-d5 (S)83.4 37-122
98.84-Terphenyl-d14 (S)94.0 54-127
1122,4,6-Tribromophenol (S)110 39-132
100Phenol-d5 (S)97.0 34-121
Page 26 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 106 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V3419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V3247
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3247 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/21/21 18:2550.08.42<8.42mg/KgAliphatic C19-C36
04/21/21 18:2550.02.50<2.50mg/KgAliphatic C9-C18
04/21/21 18:2550.013.6<13.6mg/KgAromatic C11-C22
04/21/21 18:252-Fluorobiphenyl (S)88.2 40-140
04/21/21 18:252-Bromonaphthalene (S)86.5 40-140
04/21/21 18:25Chlorooctadecane (S)77.0 40-140
04/21/21 18:25OTP Surrogate (S)80.0 40-140
LCS-V3247Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
81.365.180.0mg/KgAliphatic C19-C36 40-140
0.0*33.360.0mg/KgAliphatic C9-C18 40-140
97.0165170mg/KgAromatic C11-C22 40-140
88.72-Fluorobiphenyl (S)40-140
89.02-Bromonaphthalene (S)40-140
69.5Chlorooctadecane (S)40-140
76.5OTP Surrogate (S)40-140
V 96987-MS-V3247 V 96987-MSD-V3247Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
65.3 81.566.278.980.1<8.44mg/KgAliphatic C19-C36 83.9 40-140 1.3 50
30.6 0.0*32.259.260.1<2.51mg/KgAliphatic C9-C18 0.0*40-140 0.0 50
157 92.3156168170<13.7mg/KgAromatic C11-C22 92.8 40-140 0.6 50
88.02-Fluorobiphenyl (S)87.5 40-140
Page 27 of 30* QC Fail Date:04/23/2021 12:35 PM
Page 107 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V3419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V3247
V 96987-MS-V3247 V 96987-MSD-V3247Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
89.72-Bromonaphthalene (S)89.3 40-140
65.5Chlorooctadecane (S)65.9 40-140
69.5OTP Surrogate (S)71.0 40-140
Page 28 of 30Date:04/23/2021 12:35 PM
Page 108 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V3232QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V3218
Associated Lab Samples: 96985, 96986, 96987, 96988, 96989, 96990, 96991, 96992
LRB-V3218 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/19/21 15:188.001.58<1.58mg/KgAliphatic C5-C8
04/19/21 15:188.000.704<0.704mg/KgAliphatic C9-C12
04/19/21 15:188.000.752<0.752mg/KgAromatic C9-C10
04/19/21 15:182,5-Dibromotoluene (FID) (S)105 70-130
04/19/21 15:182,5-Dibromotoluene (PID) (S)87.6 70-130
LCS-V3218 LCSD-V3218Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.6 10298.131.432.0mg/KgAliphatic C5-C8 70-130 3.7 50
34.4 10810633.932.0mg/KgAliphatic C9-C12 70-130 1.4 50
9.43 88.187.19.3210.7mg/KgAromatic C9-C10 70-130 1.1 50
95.397.12,5-Dibromotoluene (FID) (S)70-130
81.282.32,5-Dibromotoluene (PID) (S)70-130
Page 29 of 30Date:04/23/2021 12:35 PM
Page 109 of 112
Quality Control Data
21-106-0032Report No:
Project Description:
Client ID:Highland Environmental Solutions
186481
Dry Weight Determination
SW-DRYWT
V3251QC Analytical Batch:
Analysis Method:
Analysis Description:
V 97068-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/19/21 17:200.238.037.9%Moisture
V 97095-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/19/21 17:200.518.118.0%Moisture
Page 30 of 30Date:04/23/2021 12:35 PM
Page 110 of 112
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-106-0032
Highland Environmental Solutions
00055
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.6
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Stacy L Ortiz Date & Time:04/16/2021 17:00:05
Special precautions or instructions included?
Comments:
Page 111 of 112
Page 112 of 112

APPENDIX E

APPENDIX F

P
h
o
t
o
g
r
a
p
h

N
u
m
b
e
r

6
:

L
o
c
a
Photograph Number 1: Location of the incident. Approximately 50-80 gallons of diesel fuel were
released from UST #7 due to a motor feeder failure (3/29/2021).
Photograph Number 2: Photo of fuel seeped under the concrete curb and the impacted soil
downgradient from the release location. Initial response activities included vacuuming activities in
the impacted stormwater inlet.

Photograph Number 3: Photo of the submersible pump replacement and repairs completed
(3/30/21).
Photograph Number 4: Hydrocarbon boom staked downgradient of the release location as a
precautionary measure due to forecast rain events.

Photograph Number 5: Additional hydrocarbon boom placement at the end of the concrete
culvert pipe.
Photograph Number 6: Photo of the impacted soil near the stormwater inlet. Photo taken on the
day of the excavation activities (04/15/2021).

Photograph Number 7: A PVC stormwater piping was discovered during excavation activities,
backed up stormwater was allowed to release.

Photograph Number 8: A vacuum truck was utilized to recover the stormwater from the
excavated area (04/15/2021).

Photograph Number 9: Photo of the excavation activities.
Photograph Number 10: Photo of the sample locations and the excavated area.

Photograph Number 11: Photo of the backfill being placed after excavation activities.
Photograph Number 12: Photo of the riprap stones being placed after remediation activities.

Photograph Number 13: Photo of the excavated area and stone placement post remedial
activities.

APPENDIX G