WS-2871_7246_CA_MRP_20210519

S&ME, Inc. | 8646 West Market Street, Suite 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com
May 19, 2021
McLeansville Fire Department
5326 Frieden Church Road
McLeansville, NC, 27301
Attention: Mr. Roy Rimmer
Reference: Letter Report – 2021 Groundwater Monitoring
McLeansville Fire Department - Incident # 7246
McLeansville, North Carolina
S&ME Project No. 1584-13-129C
Dear Mr. Rimmer:
The attached document describes sampling procedures; analytical results, and our findings for groundwater
samples collected on May 3, 2021 at the McLeansville Fire Department site in McLeansville, North Carolina. Our
services were performed in accordance with S&ME Proposal No. 212569 dated April 6, 2021.
If you have any questions please call Edmund Henriques [phone] at your convenience.
Sincerely,
S&ME, Inc.
Brian Wilson Edmund Q.B. Henriques, L.G.
Project Professional Project Manager / Senior Geologist
EQBH/DC
cc: Guilford County Department of Public Health
Division of Environmental Health
Attention: Mr. Gene Mao
400 West Market Street, Suite 300
Greensboro, North Carolina 27401
Letter Report – 2021 Groundwater Monitoring
McLeansville Fire Department - Incident # 7246
McLeansville, North Carolina
S&ME Project No. 1584-13-129C
May 19, 2021 3
Groundwater Sampling
S&ME, Inc. (S&ME) completed a groundwater monitoring event on May 3, 2021, at McLeansville Fire Department,
hereafter referred to as the subject site (see Figure 1). Historically, monitoring wells MW-1 and MW-4 had the
highest concentrations for constituents of concern. No other site monitoring wells had reported exceedances of
the corresponding 15A NCAC 02L groundwater standards (2L Standards), when sampled last. Monitoring well
MW-1 is near the source area for the release. Monitoring well MW-4 is located approximate 55 feet southeast of
well MW-1, and down-gradient of the release area as depicted in Figure 2.
For the May 3, 2021 monitoring event, groundwater samples were obtained from monitoring wells MW-1 and
MW-4. Each sampled monitoring well was purged of approximately three times the initial well volume with a
disposable PVC bailer or peristaltic pump. Each sample was handled with a new pair of nitrile gloves and was
placed into the laboratory provided sampling containers, and then placed in a cooler with ice. The samples were
submitted to Pace Analytical Services, Inc. (North Carolina Wastewater Certification #12) in Huntersville, North
Carolina, for laboratory analysis. The samples obtained from monitoring wells MW-1 and MW-4 were analyzed for
volatile organic compounds (VOCs) by EPA Method 602.
Groundwater Analytical Results
Table 1 provides a summary of the detected analytes for the May 3, 2021 monitoring event. Table 2 provides a
summary of the historical groundwater concentrations detected in samples obtained from site monitoring wells.
Table 3 provides a summary of the groundwater elevation data for this monitoring event and prior events. Table
4 provides monitoring well construction details. Figure 2 depicts the 2L Standard exceedances detected at the
sampled monitoring wells. The laboratory analytical report for this monitoring is included in Attachment I.
Drinking Well Sampling & Results
On May 3, 2021, S&ME collected a sample from the McLeansville Fire Department’s water supply well (sample ID
= WSW-1). The sample was submitted to Pace Analytical Laboratories, Inc. and analyzed for VOCs by EPA Method
602. No target constituents were detected above the corresponding method detection limit. A copy of the
laboratory analytical report for the event is included in Attachment I.
The Fire Department’s on-site water supply well is located approximately 170 feet cross-gradient of source area
monitoring well MW-1. The neighboring off-site Clapp water supply is approximately 200 feet up-gradient of
source area monitoring well MW-1. Figure 3 depicts properties with water supply wells identified during the
water well receptor survey update in May 2015. Table 5 provides water supply well survey information.
Discussion
Analytical results for the May 3, 2021 monitoring event finds that benzene and naphthalene at monitoring well
MW-1 were detected at concentrations that exceed their corresponding 2L Standards, which are also the CAP
established cleanup goals. Analytical results for monitoring well MW-4 report no target constituent was detected
with a concentration that exceeds the corresponding 2L Standards.
Letter Report – 2021 Groundwater Monitoring
McLeansville Fire Department - Incident # 7246
McLeansville, North Carolina
S&ME Project No. 1584-13-129C
May 19, 2021 4
Active remediation which ceased in May 2001, was effective at reducing VOC concentrations observed at site
monitoring wells. Post active remediation groundwater VOC trends can be summarized as follows:
At monitoring well MW-4, located down-gradient of the release source area, slow attenuation of VOCs in
groundwater is suggested, with current VOC concentrations meeting the CAP established cleanup goals.
Groundwater analytical data for source area monitoring well MW-1 indicates a spike in VOC
concentrations starting in 2007. Trends for some VOCs indicate attenuation following the 2007 spike in
benzene and MTBE concentrations, other VOCs exhibit sustained rises in concentrations (e.g.
naphthalene), and some exhibit little change in concentration (e.g. ethylbenzene) through 2017.
Analytical results for the May 3, 2021 monitoring event report detected petroleum constituent
concentrations that are less than the concentrations reported in 2017. This across the board reduction of
detected VOC concentrations is a positive sign. However, the analytical data set lack sufficient power to
forecast the time that may be required for natural attenuation to achieve the CAP stated cleanup goals,
the 2L Standard.
The cause for the apparent spike in VOC concentrations starting in 2007 at MW-1 has not been identified. In 2016
limited soil sampling was conducted in the source area. No residual petroleum hydrocarbons were detected at
the sampled locations within the gasoline UST release source area. Thus, no evidence of a residual secondary
source of petroleum constituents in the soil was discovered. With a negligible secondary source in soil, monitored
natural attenuation of groundwater is possible.
Analytical results for the on-site water supply well continue to report no detections of targeted petroleum
hydrocarbons.
As an incident with an NCDEQ a High-Risk classification, the pathway to incident closure could include:
1.Connect the on-site water supply well and nearby water supply well users to the available public water
supply. This would reduce the NCDEQ incident risk-classification from High-Risk to Low-Risk, and permit
closure of the incident following the completion of a Notice of Residual Petroleum. Or,
2.Conduct hot-spot remediation to reduce source area VOC concentrations to levels less than the
corresponding 2L Standards. Or,
3.Continue groundwater monitoring to track natural attenuation of the target VOCs until concentrations are
less than the corresponding 2L Standards.
Preparation of a detailed analysis of each remedial option and probable costs for each was beyond the scope of
this task authorization.
Considering the apparent limited horizontal extent of the groundwater impacts and no detections of petroleum
hydrocarbons in the on-site well, continued reliance on monitored natural attenuation as the remedial measure
remains plausible. Accordingly, S&ME recommends monitoring groundwater at wells MW-1 and MW-4, and the
on-site water supply well on an annual basis and a review of the potential to connect water supply well users to
municipal water.
TABLE 1
SUMMARY OF RECENT GROUNDWATER ANALYTICAL RESULTS
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
Well IDSample DateBenzeneEthylbenzeneIsopropylbenzeneMTBENaphthaleneTolueneTotal Xylenes602 602 602 602 602 602 602
MW-1 5/3/2021 52.0 298 19.4 < 10.0 1,110 23.7 398.6
MW-4 5/3/2021 <1.0 <1.0 1.6 11.7 <2.0 <1.0 <2.0
WSW 5/3/2021 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0
5,000 84,500 25,000 20,000 6,000 260,000 85,500
1 600 70 20 6 600 500
Notes:
Method
NCDEQ GCLs
Concentrations in bold print exceed NCAC 2L groundwater quality standards
NCAC 2L Std.
All concentrations in units of mg/l - micrograms per liter = ppb
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TABLE 2
SUMMARY OF ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
ID Sample Benzene Chloro-Ethyl-MTBE Toluene Total Total Isopropyl EDB Naph-1,2 dichloro-1,3 dichloro-1,4 dichloro-Lead
Date benzene benzene Xylenes BTEX ether thalene benzene benzene benzene
602/6200B 601/602 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 504 625/602 602/6200B 602/6200B 602/6200B 239.2
6/11/1992 2,030 58.1 2,850 31.6 7,580 11,200 23,660 <1 NA 206 360 116 334 NA
8/25/1995 28,000 <1,000 <1,000 6,200 32,000 <2,000 63,000 <1,000 4.3 250 <1 <1 <1 <5
12/4/1998 7,800 <20 1400 2,900 15,000 9100 33,300 NA <20 NA <20 <20 <20 NA
4/27/1999 640 NA 170 1,400 1,100 1490 3,400 210 NA NA NA NA NA NA
8/12/1999 22 NA 19 330 93 188 322 34 NA NA NA NA NA NA
11/3/1999 120 NA 140 210 340 800 1,400 35 <1 NA <1 <1 <1 NA
5/5/2000 <1 <1 <1 3 <1 2 5 <1 <1 <1 <1 <1 <1 NA
11/14/2000 5 <1 2 3 3 13 23 <1 <0.02 1 <1 <1 <1 NA
5/25/2001 <1 NA <1 <2 <1 <2 all BQL <1 <0.02 <1 NA NA NA NA
8/15/2001 3 NA 9 7 7 25 44 <2.5 <0.02 49 NA NA NA NA
11/13/2001 72*NA 34 8 44 70 220 <2 NA 130 NA NA NA NA
2/6/2002 78 NA 30 15 39 40 187 <5 NA 180 NA NA NA NA
5/2/2002 98 NA 61 41 76 179 414 <20 NA 330 NA NA NA NA
9/19/2002 13 NA 22 21 28 45 108 <5 NA 82 NA NA NA NA
3/31/2003 18 NA 33 28 58 90 199 <8 NA 200 NA NA NA NA
2/19/2004 60 NA 91 <100 210 241 602 <50 NA 610 NA NA NA NA
8/20/2007 388 NA 458 218 1,390 2,008 4,244 <80 NA 1,300 NA NA NA NA
6/23/2008 303 NA 286 <320 479 1,120 2,188 <60 NA 1,810 NA NA NA NA
9/7/2011 239 NA 564 126 889 1,980 3,672 <17.7 NA 2,430 NA NA NA NA
1/2/2014 175 <5.0 493 40.5 448 1,497 2,613 <5 NA 2,070 <5.0 <5.0 <5.0 NA
5/29/2015 199 <10.0 594 26.7 452 1,979 3,224 35.5 NA 2,210 <10.0 <10.0 <10.0 NA
10/6/2016 125 <12.5 435 13.4 142 863.1 1,579 <12.5 NA 2,280 <12.5 <12.5 <12.5 NA
11/16/2017 157 <20.0 593 <20.0 124 1,131.3 2,005 34.1 NA 2,680 <20.0 <20.0 <20.0 NA
5/3/2021 52 <10.0 298 <10.0 23.7 398.6 772 19.4 NA 1,110 <10.0 <10.0 <10.0 NA
1 50 600 20 600 500 -70 0.04 6 20 200 6 15
* Mass spectral screening confirms the presence of benzene. However, due to a co-eluting non-target compounds, the benzene concentration measured by this method
is falsely high. A GC/MS method is required for accurate benzene measurement in this matrix.
Green shaded cells represent time frame for active remediation
MW-1
NCAC 2L Std.
All concentrations in units of mg/l - micrograms per liter = ppb
Notes: Only detected analyses are displayed in the table
NA = not analyzed
Concentrations in bold print exceed NCAC 2L groundwater quality standards
Method
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TABLE 2
SUMMARY OF ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
ID Sample Benzene Chloro-Ethyl-MTBE Toluene Total Total Isopropyl EDB Naph-1,2 dichloro-1,3 dichloro-1,4 dichloro-Lead
Date benzene benzene Xylenes BTEX ether thalene benzene benzene benzene
602/6200B 601/602 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 504 625/602 602/6200B 602/6200B 602/6200B 239.2
MW-1
Method
9/22/1992 4,690 <5 639 <50 5,830 3,290 14,449 NA NA 10.8 <5 <5 127 NA
8/25/1995 5,600 <100 <100 1,200 5,300 1,000 12,000 <100 0.56 <10 <1 <1 <1 <5
12/4/1998 4,400 <10 570 1,600 3,400 1,900 10,270 580 <10 NA <10 <10 <10 NA
4/27/1999 1,300 NA 220 2,100 2,400 3,900 7,820 650 NA NA NA NA NA NA
8/12/1999 840 NA 140 1,300 530 1,360 2,870 310 NA NA NA NA NA NA
11/3/1999 1,400 NA 350 1,300 450 1,500 3,700 420 <1 NA <1 <1 <1 NA
5/5/2000 100 <1 140 310 210 710 1,160 <20 <1 47 <1 <1 <1 NA
11/14/2000 130 <1 130 470 50 245 555 120 0.03 110 <1 <1 <1 NA
5/25/2001 34 NA 140 160 48 243 465 47 <0.02 79 NA NA NA NA
8/15/2001 27 NA 150 110 21 140 338 62 <0.02 110 NA NA NA NA
11/13/2001 34 NA 98 85 18 60 210 27 NA 110 NA NA NA NA
2/6/2002 23 NA 27 180 <8 19 69 35 NA 49 NA NA NA NA
5/2/2002 8 NA 14 48 5 32 59 18 NA 15 NA NA NA NA
9/19/2002 2 NA 4 66 <1 2 8 11 NA 9 NA NA NA NA
3/31/2003 5.3 NA 49 89 2.7 57.7 114.7 30 NA 46 NA NA NA NA
2/19/2004 2.3 NA 12 72 <1 3.4 17.7 18 NA 9.1 NA NA NA NA
8/22/2007 2.73 NA <1 17.9 <1 <2 2.73 2.81 NA 2.84 NA NA NA NA
6/23/2008 1.70 NA 2.14 10.7 <1 <2 3.84 1.98 NA 2.45 NA NA NA NA
9/7/2011 1.66 NA <0.932 36.5 2.20 <1.91 3.86 6.77 NA <4.0 NA NA NA NA
1/2/2014 <1 <1 <1 58.3 <1 <2 all BQL 5.7 NA <2.0 <1 <1 <1 NA
5/29/2015 <0.50 <0.50 <0.50 5.7 <0.50 <1.50 all BQL 0.56 NA <2.0 <0.50 <0.50 <0.50 NA
11/16/2017 <1.0 <1.0 <1.0 91.3 <1.0 <2.0 all BQL 9.1 NA <2.0 <1.0 <1.0 <1.0 NA
5/3/2021 <1.0 <1.0 <1.0 11.7 <1.0 <2.0 all BQL 1.6 NA <2.0 <1.0 <1.0 <1.0 NA
1 50 600 20 600 500 -70 0.04 6 20 200 6 15
* Mass spectral screening confirms the presence of benzene. However, due to a co-eluting non-target compounds, the benzene concentration measured by this method
is falsely high. A GC/MS method is required for accurate benzene measurement in this matrix.
Notes: Only detected analyses are displayed in the table
All concentrations in units of mg/l - micrograms per liter = ppb
NCAC 2L Std.
MW-4
NA = not analyzed
Concentrations in bold print exceed NCAC 2L groundwater quality standards
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TABLE 2
SUMMARY OF ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
ID Sample Benzene Chloro-Ethyl-MTBE Toluene Total Total Isopropyl EDB Naph-1,2 dichloro-1,3 dichloro-1,4 dichloro-Lead
Date benzene benzene Xylenes BTEX ether thalene benzene benzene benzene
602/6200B 601/602 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 504 625/602 602/6200B 602/6200B 602/6200B 239.2
MW-1
Method
9/22/1992 <1 <1 <1 <10 <1 <2 all BQL NA NA <10 <1 <1 <1 NA
8/25/1995 <1 <1 <1 <10 <1 <2 all BQL <1 <0.02 <10 <1 <1 <1 <5
12/4/1998 <1 <1 <1 <10 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
4/27/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA NA NA NA NA
8/12/1999 <1 NA <1 <2 <1 <2 all BQL <1 NA NA NA NA NA NA
11/3/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
5/5/2000 <1 NA <1 <2 <1 <2 all BQL <1 <1 <1 NA NA NA NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
8/22/2007 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
6/23/2008 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
9/7/2011 <0.233 NA <0.233 <0.440 <0.226 <0.478 all BQL <0.221 NA <1.0 NA NA NA NA
1/2/2014 <1 <1 <1 <1 <1 <2 all BQL <1 NA <2.0 <1 <1 <1 NA
5/29/2015 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 all BQL <0.50 NA <0.50 <0.50 <0.50 <0.50 NA
MW-6 8/25/1995 <1 <1 <1 <10 <1 <2 all BQL <1 <0.02 <10 <1 <1 <1 <5
12/4/1998 <1 <1 <1 <10 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
4/27/1999 <1 NA <1 <10 <1 <2 all BQL <1 NA NA NA NA NA NA
8/12/1999 <1 NA <1 <2 <1 <2 all BQL <1 NA NA NA NA NA NA
11/3/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
MW-7 8/25/1995 95 <1 <1 <1 <1 <2 99 <2 <0.02 <10 <1 <1 <1 <5
4/22/1996 63 <1 <1 9 <1 <2 67 4 <0.02 <10 <1 <1 <1 20.8
MW-8 4/22/1996 <1 <1 <1 <2 <1 <2 all BQL <1 <0.02 <10 <1 <1 <1 7.26
12/4/1998 <1 <1 <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/3/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
5/25/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
8/15/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
11/13/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
2/6/2002 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
5/2/2002 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
3/31/2003 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
1 50 600 20 600 500 -70 0.04 6 20 200 6 15
Green shaded cells represent time frame for active remediation
NCAC 2L Std.
NA = not analyzed
Concentrations in bold print exceed NCAC 2L groundwater quality standards
All concentrations in units of mg/l - micrograms per liter = ppbNotes: Only detected analyses are displayed in the table
MW-5
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TABLE 2
SUMMARY OF ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
ID Sample Benzene Chloro-Ethyl-MTBE Toluene Total Total Isopropyl EDB Naph-1,2 dichloro-1,3 dichloro-1,4 dichloro-Lead
Date benzene benzene Xylenes BTEX ether thalene benzene benzene benzene
602/6200B 601/602 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 602/6200B 504 625/602 602/6200B 602/6200B 602/6200B 239.2
MW-1
Method
MW-2 9/22/1992 <1 <1 <1 <10 <1 <2 all BQL NA NA <10 <1 <1 <1 NA
8/25/1995 <1 <1 <1 <1 <1 <2 all BQL <1 0.02 <10 <1 <1 <1 <5
12/4/1998 <1 <1 <1 <1 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/3/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
MW-3 9/22/1992 <1 <1 <1 <10 <1 <2 all BQL NA NA <10 <1 <1 <1 NA
8/25/1995 <1 <1 <1 <1 <1 <2 all BQL <1 <0.02 <10 <1 <1 <1 <5
12/4/1998 <1 <1 <1 <1 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
4/27/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA NA NA NA NA
8/12/1999 <1 NA <1 <2 <1 <2 all BQL <1 NA NA NA NA NA NA
11/3/1999 <1 NA <1 <2 <1 <2 all BQL <1 <1 NA <1 <1 <1 NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA 6 NA NA NA NA
2/19/2004 <1 NA <1 <2 <1 <2 all BQL <1 NA 1.1 NA NA NA NA
MW-9 4/27/1999 <1 NA <1 <2 <1 <2 all BQL <1 NA NA NA NA NA NA
8/12/1999 <1 NA <1 <2 <1 <2 all BQL <1 NA NA NA NA NA NA
11/14/2000 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
5/25/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
8/15/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
11/13/2001 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
2/6/2002 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
5/2/2002 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
3/31/2003 <1 NA <1 <2 <1 <2 all BQL <1 NA <1 NA NA NA NA
2/19/2004 <1 NA <1 <2 <2 <2 all BQL <1 NA <1 NA NA NA NA
1 50 600 20 600 500 -70 0.04 6 20 200 6 15
Green shaded cells represent time frame for active remediation
NA = not analyzed
Concentrations in bold print exceed NCAC 2L groundwater quality standards
Notes: Only detected analyses are displayed in the table
All concentrations in units of mg/l - micrograms per liter = ppb
NCAC 2L Std.
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WELL ID DATE TOC ELEVATION (feet)DEPTH TO WATER
(feet)
GROUNDWATER ELEVATION
(feet)
24-Aug-95 97.95 15.82 82.13
04-Dec-98 97.95 18.13 79.82
27-Apr-99 97.95 14.82 83.13
24-May-99 97.95 14.65 83.30
12-Aug-99 97.95 15.26 82.69
05-Oct-99 97.95 12.84 85.11
03-Nov-99 97.95 13.25 84.70
03-Dec-99 97.95 9.71 88.24
06-Jan-00 97.95 14.09 83.86
16-Feb-00 97.95 12.70 85.25
15-Mar-00 97.95 4.15 93.80
17-Apr-00 97.95 13.80 84.15
05-May-00 97.95 10.94 87.01
06-Jun-00 97.95 12.46 85.49
06-Jul-00 97.95 6.39 91.56
14-Nov-00 97.95 11.97 85.98
24-May-01 97.95 12.59 85.36
15-Aug-01 97.95 14.95 83.00
13-Nov-01 97.95 16.90 81.05
06-Feb-02 97.95 15.02 82.93
02-May-02 97.95 14.51 83.44
19-Sep-02 97.95 16.70 81.25
31-Mar-03 97.95 8.28 89.67
19-Feb-04 97.95 10.42 87.53
20-Aug-07 97.95 16.12 81.83
23-Jun-08 97.95 14.99 82.96
07-Sep-11 97.95 16.60 81.35
02-Jan-14 97.95 10.86 87.09
29-May-15 97.95 12.92 85.03
06-Oct-16 97.95 15.87 82.08
16-Nov-17 97.95 15.84 82.11
03-May-21 97.95 9.18 88.77
MW-2 24-Aug-95 98.50 15.47 83.03
04-Dec-98 98.50 17.53 80.97
03-Nov-99 98.50 12.63 85.87
03-Dec-99 98.50 13.06 85.44
16-Feb-00 98.50 10.42 88.08
05-May-00 98.50 9.97 88.53
14-Nov-00 98.50 12.53 85.97
19-Feb-04 98.50 9.51 88.99
MW-3 24-Aug-95 97.80 15.89 81.91
04-Dec-98 97.80 17.65 80.15
27-Apr-99 97.80 13.21 84.59
24-May-99 97.80 11.97 85.83
12-Aug-99 97.80 15.77 82.03
05-Oct-99 97.80 12.35 85.45
03-Nov-99 97.80 12.82 84.98
03-Dec-99 97.80 13.03 84.77
16-Feb-00 97.80 10.63 87.17
17-Apr-00 97.80 9.99 87.81
05-May-00 97.80 10.61 87.19
06-Jun-00 97.80 12.58 85.22
06-Jul-00 97.80 12.20 85.60
14-Nov-00 97.80 13.02 84.78
19-Feb-04 97.80 10.16 87.64
S&ME PROJECT NO. 1584-13-129C
HISTORIAL GROUNDWATER ELEVATION DATA
TABLE 3
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
MW-1
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WELL ID DATE TOC ELEVATION (feet)DEPTH TO WATER
(feet)
GROUNDWATER ELEVATION
(feet)
S&ME PROJECT NO. 1584-13-129C
HISTORIAL GROUNDWATER ELEVATION DATA
TABLE 3
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
MW-1 24-Aug-95 97.33 15.37 81.96
04-Dec-98 97.33 17.04 80.29
27-Apr-99 97.33 12.98 84.35
24-May-99 97.33 11.97 85.36
12-Aug-99 97.33 16.04 81.29
05-Oct-99 97.33 14.93 82.40
03-Nov-99 97.33 14.46 82.87
03-Dec-99 97.33 15.42 81.91
06-Jan-00 97.33 12.93 84.40
16-Feb-00 97.33 10.49 86.84
15-Mar-00 97.33 11.55 85.78
17-Apr-00 97.33 9.88 87.45
05-May-00 97.33 10.35 86.98
06-Jun-00 97.33 12.50 84.83
06-Jul-00 97.33 12.44 84.89
14-Nov-00 97.33 15.21 82.12
24-May-01 97.33 13.59 83.74
15-Aug-01 97.33 14.29 83.04
13-Nov-01 97.33 16.24 81.09
06-Feb-02 97.33 14.40 82.93
02-May-02 97.33 13.99 83.34
19-Sep-02 97.33 16.10 81.23
31-Mar-03 97.33 8.98 88.35
19-Feb-04 97.33 9.98 87.35
20-Aug-07 97.33 15.57 81.76
23-Jun-08 97.33 14.31 83.02
07-Sep-11 97.33 15.87 81.46
02-Jan-14 97.33 10.65 86.68
29-May-15 97.33 12.43 84.90
16-Nov-17 97.33 15.28 82.05
03-May-21 97.33 9.14 88.19
MW-5 24-Aug-95 96.15 13.84 82.31
04-Dec-98 96.15 16.19 79.96
27-Apr-99 96.15 11.80 84.35
24-May-99 96.15 NM NM
12-Aug-99 96.15 14.03 82.12
05-Oct-99 96.15 10.88 85.27
03-Nov-99 96.15 11.11 85.04
03-Dec-99 96.15 11.66 84.49
16-Feb-00 96.15 9.36 86.79
17-Apr-00 96.15 9.69 86.46
05-May-00 96.15 8.85 87.30
14-Nov-00 96.15 11.02 85.13
19-Feb-04 96.15 11.08 85.07
20-Aug-07 96.15 14.25 81.90
23-Jun-08 96.15 13.08 83.07
07-Sep-11 96.15 14.88 81.27
02-Jan-14 96.15 10.49 85.66
29-May-15 96.15 11.45 84.70
MW-4
Z:\Shared\SME\Ops\ENV\Projects\2013\1584-13-129C McLeansville FD Groundwater Monitoring_North Carolina\Working Documents\(McLeansville) Data_Updated 20210514.xlsx
WELL ID DATE TOC ELEVATION (feet)DEPTH TO WATER
(feet)
GROUNDWATER ELEVATION
(feet)
S&ME PROJECT NO. 1584-13-129C
HISTORIAL GROUNDWATER ELEVATION DATA
TABLE 3
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
MW-1MW-6 24-Aug-95 86.97 6.30 80.67
04-Dec-98 86.97 7.53 79.44
27-Apr-99 86.97 3.24 83.73
12-Aug-99 86.97 5.94 81.03
03-Nov-99 86.97 2.82 84.15
03-Dec-99 86.97 3.01 83.96
16-Feb-00 86.97 0.45 86.52
05-May-00 86.97 0.81 86.16
14-Nov-00 86.97 3.10 83.87
MW-7 24-Aug-95 97.97 14.53 83.44
24-Aug-95 98.04 Not measured Not measured
04-Dec-98 98.04 17.86 80.18
27-Apr-99 98.04 Not measured Not measured
24-May-99 98.04 Not measured Not measured
12-Aug-99 98.04 Not measured Not measured
05-Oct-99 98.04 13.04 85.00
03-Nov-99 98.04 13.06 84.98
03-Dec-99 98.04 13.52 84.52
16-Feb-00 98.04 11.57 86.47
17-Apr-00 98.04 11.51 86.53
05-May-00 98.04 10.79 87.25
06-Jun-00 98.04 12.25 85.79
14-Nov-00 98.04 12.76 85.28
24-May-01 98.04 12.30 85.74
15-Aug-01 98.04 14.67 83.37
13-Nov-01 98.04 16.73 81.31
06-Feb-02 98.04 15.18 82.86
02-May-02 98.04 14.42 83.62
19-Feb-04 98.04 10.34 87.70
MW-9 24-Aug-95 97.14 NM NM
04-Dec-98 97.14 15.89 81.25
27-Apr-99 97.14 13.08 84.06
24-May-99 97.14 11.75 85.39
12-Aug-99 97.14 15.28 81.86
05-Oct-99 97.14 12.06 85.08
03-Dec-99 97.14 12.83 84.31
16-Feb-00 97.14 10.49 86.65
17-Apr-00 97.14 10.25 86.89
05-May-00 97.14 9.93 87.21
06-Jun-00 97.14 11.73 85.41
06-Jul-00 97.14 11.66 85.48
14-Nov-00 97.14 12.21 84.93
24-May-01 97.14 11.75 85.39
15-Aug-01 97.14 14.28 82.86
13-Nov-01 97.14 15.95 81.19
06-Feb-02 97.14 14.40 82.74
02-May-02 97.14 13.80 83.34
31-Mar-03 97.14 6.77 90.37
19-Feb-04 97.14 9.61 87.53
MW-8
Z:\Shared\SME\Ops\ENV\Projects\2013\1584-13-129C McLeansville FD Groundwater Monitoring_North Carolina\Working Documents\(McLeansville) Data_Updated 20210514.xlsx
WELL ID TOTAL WELL DEPTH
(feet)
WELL SCREEN
LENGTH
(feet)
TOP OF CASING
ELEVATION
(feet)
MW-1 25.0 10 97.95
MW-2 25.0 15 98.50
MW-3 20.0 10 Not Located
MW-4 20.0 10 97.33
MW-5 20.0 10 96.15
MW-6 21.0 10 86.97
MW-7**51.0 5 97.97
MW-8 NM 10 Abandoned
MW-9 20.0 10 Destroyed
Notes: ns = Not surveyed
NM = Not measured
** = Well MW-7 converted and currently configures as a groundwater air sparge well
MCLEANSVILLE FIRE DEPARTMENT
S&ME PROJECT NO. 1584-13-129C
TABLE 4
SUMMARY OF WELL CONSTRUCTION DETAILS
MCLEANSVILLE, NORTH CAROLINA
MAP ID Address Property Owner - Address
Approximate Distance
From Source Area (feet)Comment
1 5333 Frieden Church Rd.
Charles Terry - 2917 Rogers Rd, Graham, NC
27353 370
House with well visible,
no water account
2 5335 Frieden Church Rd.
Charles Terry - 2917 Rogers Rd., Graham, NC
27353 450
Business (Lynn's Furniture Gallery)
with well visible, no water account
3 5609 Bethel Church Rd.
Cathy Justis - 5335 Bethel Church Rd.,
McLeansville NC, 27301 940
House, no well visible,
no water account
4 5322 McLeansville Rd.
Kim & Sharon Foust - 5322 McLeansville Rd.,
McLeansville NC, 27301 700
House, no well visible, no water
account
5 5304 Frieden Church Rd.
Robert Payne - P.O. Box 100, McLeansville NC,
27301 575
Duplex, new well visible,
no water account
6 5212 Frieden Church Rd.
Herman Stanley - 5312 Frieden Church Rd.,
McLeansville NC, 27301 850
House with well visible,
no water account
7 5314 Frieden Church Rd.
John & Emma Jones - 5314 Frieden Church
Rd., McLeansville NC, 27301 400
House, no well visible,
no water account
11 5316 Frieden Church Rd.
David & Salley Jones - 5316 Frieden Church
Rd., McLeansville NC, 27301 350
House, no well visible,
no water account
8 5318 Frieden Church Rd.
Mary Fields - 5318 Frieden Church Rd.,
McLeansville NC, 27301 250
House, no well visible,
no water account
9 5320 Frieden Church Rd.
John & Galdys Clapp - 5320 Frieden Church
Rd., McLeansville NC, 27301 200
House, well visible & no water
account
10 5326 Frieden Church Rd.
McLeansville Fire Department - 5326 Frieden
Church Rd., McLeansville, NC 27301 170
On Well, water meter observed,
no water account
Receptor Survey Updated in May 2015
TABLE 5
WATER SUPPLY WELL RECEPTOR SURVEY SUMMARY (2015)
MCLEANSVILLE FIRE DEPARTMENT
MCLEANSVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-13-129C
Z:\Shared\SME\Ops\ENV\Projects\2013\1584-13-129C McLeansville FD Groundwater Monitoring_North Carolina\Working Documents\(McLeansville) Data_Updated 20210514.xlsx
SITEFIGURE NO.Drawing path: R:\CADData\Greensboro\1584\2013\13-129 - McLEANSVILLE FIRE DEPARTMENT\C\MFD Site Plan.dwg
PROJECT NUMBERDATE:SCALE:020004000 (IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALEMcLEANSVILLE FIRE DEPARTMENT
McLEANSVILLE, NORTH CAROLINA1MAY 2021VICINITY MAPAS SHOWN1584-13-129CN
N
FRAMEMW-6ASW-2MW-5E
Q
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A BLDGMW-1VEW-2MW-4ASW-3ASW-1MW-9METALVEW-1A
S
T MW-8BUILDINGMW-3McLEANSVILLEFIRE DEPT.FIRE DEPT.MW-2PHIPPS(ABANDONED)(DESTROYED)FORMERB-1B-2CLAPP WELL(ABANDONED) KEY - MONITORING WELL- SOIL VAPOR EXTRACTION WELL- AIR SPARGE WELL- WATER SUPPLY WELL- VAULT- TRENCH LINE- SOIL BORING LOCATION (10-6-16)FREIDEN CHURCH RD
BUILDINGMcLEANSVILLEFIRE DEPT.CURRENTFORMER USTBASIN- MICROGRAMS PER LITERug/LMW-1ug/LBenzene52Naphthalene1,110WSWug/LAll < 2L StandardFIGURE NO.Drawing path: R:\CADData\Greensboro\1584\2013\13-129 - McLEANSVILLE FIRE DEPARTMENT\C\MFD Site Plan.dwg
PROJECT NUMBERDATE:SCALE:04080 (IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALEMcLEANSVILLE FIRE DEPARTMENT
McLEANSVILLE, NORTH CAROLINA2MAY 2021CONSTITUENT MAPAS SHOWN1584-13-129CNMW-4ug/LAll < 2L Standard
657891110234XXXXXLEGEND- WATER SUPPLY WELL LOCATION- HOUSE REMOVED FOR HIGHWAY CONSTRUCTIONSOURCE: 2014 AERIAL PHOTOGRAPH OBTAINED FROM http://data.nconemap.gov.2015 PARCEL DATA OBTAINED GROM THE GUILFORD COUNTY GIS WEBSITE.FREIDEN
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FIGURE NO.Drawing path: R:\CADData\Greensboro\1584\2013\13-129 - McLEANSVILLE FIRE DEPARTMENT\C\MFD Receptor Map.dwg
PROJECT NUMBERDATE:SCALE:0400800 (IN FEET)GRAPHIC SCALE (IN FEET)GRAPHIC SCALEMcLEANSVILLE FIRE DEPARTMENT
McLEANSVILLE, NORTH CAROLINA3MAY 2021UPDATED RECEPTOR SURVEY MAPAS SHOWN1584-13-129CN
Attachments
Attachment I – Analytical Reports
#=CL#
May 11, 2021
LIMS USE: FR - ED HENRIQUES
LIMS OBJECT ID: 92537129
92537129
Project:
Pace Project No.:
RE:
Mr. Ed Henriques
S&ME, Inc.
8646 West Market Street
Suite 105
Greensboro, NC 27409
McLeansville Fire Department
Dear Mr. Henriques:
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 18
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Lab ID Sample ID Matrix Date Collected Date Received
92537129001 MW-1 Water 05/03/21 09:25 05/05/21 10:35
92537129002 MW-4 Water 05/03/21 10:05 05/05/21 10:35
92537129003 WSW-1 Water 05/03/21 10:45 05/05/21 10:35
92537129004 Trip Blank Water 05/03/21 00:00 05/05/21 10:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92537129001 MW-1 SM 6200B 16 PASI-CSAS
92537129002 MW-4 SM 6200B 16 PASI-CSAS
92537129003 WSW-1 SM 6200B 16 PASI-CSAS
92537129004 Trip Blank SM 6200B 16 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 18
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Method:
Client:S&ME - Greensboro
SM 6200B
Date:May 11, 2021
Description:602 Volatiles by Method 6200
General Information:
4 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 618938
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92537129001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3256600)
• Diisopropyl ether
• Naphthalene
• MSD (Lab ID: 3256601)
• Diisopropyl ether
• Naphthalene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Sample:MW-1 Lab ID:92537129001 Collected:05/03/21 09:25 Received:05/05/21 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene 52.0 ug/L 05/07/21 18:31 71-43-210.0 3.4 10
Chlorobenzene <10.0 ug/L 05/07/21 18:31 108-90-710.0 2.8 10
1,2-Dichlorobenzene <10.0 ug/L 05/07/21 18:31 95-50-110.0 3.4 10
1,3-Dichlorobenzene <10.0 ug/L 05/07/21 18:31 541-73-110.0 3.4 10
1,4-Dichlorobenzene <10.0 ug/L 05/07/21 18:31 106-46-710.0 3.3 10
Diisopropyl ether <10.0 ug/L 05/07/21 18:31 108-20-3 M110.0 3.1 10
Ethylbenzene 298 ug/L 05/07/21 18:31 100-41-410.0 3.0 10
Isopropylbenzene (Cumene)19.4 ug/L 05/07/21 18:31 98-82-810.0 3.3 10
Methyl-tert-butyl ether <10.0 ug/L 05/07/21 18:31 1634-04-410.0 4.2 10
Naphthalene 1110 ug/L 05/07/21 18:31 91-20-3 M120.0 6.4 10
Toluene 23.7 ug/L 05/07/21 18:31 108-88-310.0 4.8 10
m&p-Xylene 382 ug/L 05/07/21 18:31 179601-23-120.0 7.1 10
o-Xylene 16.6 ug/L 05/07/21 18:31 95-47-610.0 3.4 10
Surrogates
4-Bromofluorobenzene (S)98 %05/07/21 18:31 460-00-470-130 10
1,2-Dichloroethane-d4 (S)101 %05/07/21 18:31 17060-07-070-130 10
Toluene-d8 (S)104 %05/07/21 18:31 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Sample:MW-4 Lab ID:92537129002 Collected:05/03/21 10:05 Received:05/05/21 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene <1.0 ug/L 05/07/21 01:02 71-43-21.0 0.34 1
Chlorobenzene <1.0 ug/L 05/07/21 01:02 108-90-71.0 0.28 1
1,2-Dichlorobenzene <1.0 ug/L 05/07/21 01:02 95-50-11.0 0.34 1
1,3-Dichlorobenzene <1.0 ug/L 05/07/21 01:02 541-73-11.0 0.34 1
1,4-Dichlorobenzene <1.0 ug/L 05/07/21 01:02 106-46-71.0 0.33 1
Diisopropyl ether 1.6 ug/L 05/07/21 01:02 108-20-31.0 0.31 1
Ethylbenzene <1.0 ug/L 05/07/21 01:02 100-41-41.0 0.30 1
Isopropylbenzene (Cumene)<1.0 ug/L 05/07/21 01:02 98-82-81.0 0.33 1
Methyl-tert-butyl ether 11.7 ug/L 05/07/21 01:02 1634-04-41.0 0.42 1
Naphthalene <2.0 ug/L 05/07/21 01:02 91-20-32.0 0.64 1
Toluene <1.0 ug/L 05/07/21 01:02 108-88-31.0 0.48 1
m&p-Xylene <2.0 ug/L 05/07/21 01:02 179601-23-12.0 0.71 1
o-Xylene <1.0 ug/L 05/07/21 01:02 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)90 %05/07/21 01:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %05/07/21 01:02 17060-07-070-130 1
Toluene-d8 (S)101 %05/07/21 01:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Sample:WSW-1 Lab ID:92537129003 Collected:05/03/21 10:45 Received:05/05/21 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene <1.0 ug/L 05/07/21 00:44 71-43-21.0 0.34 1
Chlorobenzene <1.0 ug/L 05/07/21 00:44 108-90-71.0 0.28 1
1,2-Dichlorobenzene <1.0 ug/L 05/07/21 00:44 95-50-11.0 0.34 1
1,3-Dichlorobenzene <1.0 ug/L 05/07/21 00:44 541-73-11.0 0.34 1
1,4-Dichlorobenzene <1.0 ug/L 05/07/21 00:44 106-46-71.0 0.33 1
Diisopropyl ether <1.0 ug/L 05/07/21 00:44 108-20-31.0 0.31 1
Ethylbenzene <1.0 ug/L 05/07/21 00:44 100-41-41.0 0.30 1
Isopropylbenzene (Cumene)<1.0 ug/L 05/07/21 00:44 98-82-81.0 0.33 1
Methyl-tert-butyl ether <1.0 ug/L 05/07/21 00:44 1634-04-41.0 0.42 1
Naphthalene <2.0 ug/L 05/07/21 00:44 91-20-32.0 0.64 1
Toluene <1.0 ug/L 05/07/21 00:44 108-88-31.0 0.48 1
m&p-Xylene <2.0 ug/L 05/07/21 00:44 179601-23-12.0 0.71 1
o-Xylene <1.0 ug/L 05/07/21 00:44 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)95 %05/07/21 00:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %05/07/21 00:44 17060-07-070-130 1
Toluene-d8 (S)102 %05/07/21 00:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Sample:Trip Blank Lab ID:92537129004 Collected:05/03/21 00:00 Received:05/05/21 10:35 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
602 Volatiles by Method 6200
Benzene <1.0 ug/L 05/07/21 00:26 71-43-21.0 0.34 1
Chlorobenzene <1.0 ug/L 05/07/21 00:26 108-90-71.0 0.28 1
1,2-Dichlorobenzene <1.0 ug/L 05/07/21 00:26 95-50-11.0 0.34 1
1,3-Dichlorobenzene <1.0 ug/L 05/07/21 00:26 541-73-11.0 0.34 1
1,4-Dichlorobenzene <1.0 ug/L 05/07/21 00:26 106-46-71.0 0.33 1
Diisopropyl ether <1.0 ug/L 05/07/21 00:26 108-20-31.0 0.31 1
Ethylbenzene <1.0 ug/L 05/07/21 00:26 100-41-41.0 0.30 1
Isopropylbenzene (Cumene)<1.0 ug/L 05/07/21 00:26 98-82-81.0 0.33 1
Methyl-tert-butyl ether <1.0 ug/L 05/07/21 00:26 1634-04-41.0 0.42 1
Naphthalene <2.0 ug/L 05/07/21 00:26 91-20-32.0 0.64 1
Toluene <1.0 ug/L 05/07/21 00:26 108-88-31.0 0.48 1
m&p-Xylene <2.0 ug/L 05/07/21 00:26 179601-23-12.0 0.71 1
o-Xylene <1.0 ug/L 05/07/21 00:26 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)94 %05/07/21 00:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %05/07/21 00:26 17060-07-070-130 1
Toluene-d8 (S)99 %05/07/21 00:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
618706
SM 6200B
SM 6200B
602 by 6200B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92537129002, 92537129003, 92537129004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3255336
Associated Lab Samples:92537129002, 92537129003, 92537129004
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L <1.0 1.0 05/07/21 00:080.34
1,3-Dichlorobenzene ug/L <1.0 1.0 05/07/21 00:080.34
1,4-Dichlorobenzene ug/L <1.0 1.0 05/07/21 00:080.33
Benzene ug/L <1.0 1.0 05/07/21 00:080.34
Chlorobenzene ug/L <1.0 1.0 05/07/21 00:080.28
Diisopropyl ether ug/L <1.0 1.0 05/07/21 00:080.31
Ethylbenzene ug/L <1.0 1.0 05/07/21 00:080.30
Isopropylbenzene (Cumene)ug/L <1.0 1.0 05/07/21 00:080.33
m&p-Xylene ug/L <2.0 2.0 05/07/21 00:080.71
Methyl-tert-butyl ether ug/L <1.0 1.0 05/07/21 00:080.42
Naphthalene ug/L <2.0 2.0 05/07/21 00:080.64
o-Xylene ug/L <1.0 1.0 05/07/21 00:080.34
Toluene ug/L <1.0 1.0 05/07/21 00:080.48
1,2-Dichloroethane-d4 (S)%105 70-130 05/07/21 00:08
4-Bromofluorobenzene (S)%97 70-130 05/07/21 00:08
Toluene-d8 (S)%99 70-130 05/07/21 00:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3255337LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 44.650 89 60-140
1,3-Dichlorobenzene ug/L 44.650 89 60-140
1,4-Dichlorobenzene ug/L 44.550 89 60-140
Benzene ug/L 53.850 108 60-140
Chlorobenzene ug/L 50.650 101 60-140
Diisopropyl ether ug/L 62.150 124 60-140
Ethylbenzene ug/L 50.450 101 60-140
Isopropylbenzene (Cumene)ug/L 45.550 91 60-140
m&p-Xylene ug/L 99.9100 100 60-140
Methyl-tert-butyl ether ug/L 52.550 105 60-140
Naphthalene ug/L 40.050 80 60-140
o-Xylene ug/L 48.250 96 60-140
Toluene ug/L 50.050 100 60-140
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3255338MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92537129003
3255339
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 97 60-14098 1 3020<1.0 19.4 19.6
1,3-Dichlorobenzene ug/L 20 100 60-14099 1 3020<1.0 20.0 19.9
1,4-Dichlorobenzene ug/L 20 98 60-14099 1 3020<1.0 19.6 19.8
Benzene ug/L 20 118 60-140122 3 3020<1.0 23.7 24.3
Chlorobenzene ug/L 20 112 60-140113 1 3020<1.0 22.4 22.7
Diisopropyl ether ug/L 20 134 60-140134 0 3020<1.0 26.9 26.9
Ethylbenzene ug/L 20 113 60-140115 2 3020<1.0 22.5 22.9
Isopropylbenzene
(Cumene)ug/L 20 104 60-140106 2 3020<1.0 20.8 21.3
m&p-Xylene ug/L 40 111 60-140113 2 3040<2.0 44.5 45.2
Methyl-tert-butyl ether ug/L 20 112 60-140112 1 3020<1.0 22.3 22.5
Naphthalene ug/L 20 87 60-14089 2 3020<2.0 17.4 17.9
o-Xylene ug/L 20 106 60-140108 2 3020<1.0 21.2 21.6
Toluene ug/L 20 110 60-140112 2 3020<1.0 22.0 22.3
1,2-Dichloroethane-d4 (S)%103 70-130102
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
618938
SM 6200B
SM 6200B
602 by 6200B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92537129001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3256598
Associated Lab Samples:92537129001
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L <1.0 1.0 05/07/21 11:540.34
1,3-Dichlorobenzene ug/L <1.0 1.0 05/07/21 11:540.34
1,4-Dichlorobenzene ug/L <1.0 1.0 05/07/21 11:540.33
Benzene ug/L <1.0 1.0 05/07/21 11:540.34
Chlorobenzene ug/L <1.0 1.0 05/07/21 11:540.28
Diisopropyl ether ug/L <1.0 1.0 05/07/21 11:540.31
Ethylbenzene ug/L <1.0 1.0 05/07/21 11:540.30
Isopropylbenzene (Cumene)ug/L <1.0 1.0 05/07/21 11:540.33
m&p-Xylene ug/L <2.0 2.0 05/07/21 11:540.71
Methyl-tert-butyl ether ug/L <1.0 1.0 05/07/21 11:540.42
Naphthalene ug/L <2.0 2.0 05/07/21 11:540.64
o-Xylene ug/L <1.0 1.0 05/07/21 11:540.34
Toluene ug/L <1.0 1.0 05/07/21 11:540.48
1,2-Dichloroethane-d4 (S)%101 70-130 05/07/21 11:54
4-Bromofluorobenzene (S)%94 70-130 05/07/21 11:54
Toluene-d8 (S)%100 70-130 05/07/21 11:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3256599LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 49.450 99 60-140
1,3-Dichlorobenzene ug/L 50.050 100 60-140
1,4-Dichlorobenzene ug/L 49.750 99 60-140
Benzene ug/L 56.350 113 60-140
Chlorobenzene ug/L 54.350 109 60-140
Diisopropyl ether ug/L 64.150 128 60-140
Ethylbenzene ug/L 54.850 110 60-140
Isopropylbenzene (Cumene)ug/L 50.950 102 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 52.850 106 60-140
Naphthalene ug/L 44.450 89 60-140
o-Xylene ug/L 51.850 104 60-140
Toluene ug/L 51.950 104 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3256600MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92537129001
3256601
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 200 106 60-140108 1 30200<10.0 212 215
1,3-Dichlorobenzene ug/L 200 108 60-140108 0 30200<10.0 217 216
1,4-Dichlorobenzene ug/L 200 107 60-140106 1 30200<10.0 215 213
Benzene ug/L 200 137 60-140129 5 3020052.0 326 310
Chlorobenzene ug/L 200 126 60-140123 3 30200<10.0 252 245
Diisopropyl ether ug/L M120015560-140142 8 30200<10.0 309 285
Ethylbenzene ug/L 200 135 60-140132 1 30200298568562
Isopropylbenzene
(Cumene)ug/L 200 121 60-140116 4 3020019.4 262 252
m&p-Xylene ug/L 400 132 60-140128 2 30400382909893
Methyl-tert-butyl ether ug/L 200 125 60-140118 6 30200<10.0 250 235
Naphthalene ug/L M120016760-140170 0 30200111014401450
o-Xylene ug/L 200 121 60-140118 3 3020016.6 259 252
Toluene ug/L 200 124 60-140123 1 3020023.7 272 270
1,2-Dichloroethane-d4 (S)%97 70-130100
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%100 70-130103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92537129
McLeansville Fire Department
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92537129
McLeansville Fire Department
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92537129001 618938MW-1 SM 6200B
92537129002 618706MW-4 SM 6200B
92537129003 618706WSW-1 SM 6200B
92537129004 618706Trip Blank SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/11/2021 01:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 18
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