WS-28875_48082_CA_IAAR_20210723

July 23, 2021
David Kane, AIA
LCS Development
Senior Design Manager
400 Locust Street, Suite 820
Des Moines, IA 50309-2334
Reference: 20-Day and Initial Abatement Action Report
Whitestone Assisted Living Facility
700 South Holden Road
Greensboro, Guilford County, North Carolina 27407
NCDEQ Incident No. Unassigned
ECS Project No. 49:12057-A
Dear Mr. Kane:
As authorized by your acceptance of our proposal 49:22916 dated June 25, 2021 and authorized on February
18, 2021, ECS Southeast, LLP (ECS) is pleased to provide you with this 20-Day and Initial Abatement Action
(IAA) Report for the subject site located in Greensboro, Guilford County, North Carolina. This report includes
a description of the work performed, the results obtained, and our conclusions and recommendations.
We appreciate the opportunity to work with you on this project. If you have any questions or require any
further information, please feel free to Samantha Szakasits at [phone].
Sincerely,
ECS SOUTHEAST, LLP
Samantha M. Szakasits, G.I.T. Roger A. Smith, P.G.
Environmental Staff Project Manager Principal Geologist
[e-mail] [e-mail]
[phone] [phone]
Attachment(s): 20-Day and IAA Report, Whitestone Assisted Living Facility
Cc: Division of Waste Management, NCDEQ, UST Section, Winston-Salem Regional Office, 450 West
Hanes Mill Road, Suite 300, Winston-Salem, NC 27105
Received: 10/21/2021
700 South Holden Road
Greensboro, Guilford County, NC 27407
1
20-DAY
And
INITIAL ABATEMENT ACTION REPORT
The IAA report should contain, at a minimum, the following information. Any other information that is
pertinent to the site should be included.
I. General Information
A. Ownership of UST(s)
1.Name of UST(s) owner/operator:
Masonic & Eastern Star Home of NC, Inc.
2.Owner / operator address and telephone number:
700 South Holden Road
Greensboro, Guilford County, North Carolina 27407
[phone]
B. Facility Information
1. Facility name:
Whitestone Assisted Living Facility
2. Facility ID #:
00-0-0000030330
3.Facility address, telephone number and county:
700 South Holden Road
Greensboro, Guilford County, North Carolina 27407
[phone]
C. Contacts
1.Name, address, telephone number and job title of primary contact person:
Mr. David Kane, AIA
400 Locust Street, Suite 820
Des Moines, IA 50309-2334
[phone]
700 South Holden Road
Greensboro, Guilford County, NC 27407
2
2.Name, address and telephone number of closure contractor:
Buckeye Elm Contracting (Buckeye)
PO Box 1026
Mocksville, NC 27028
[phone]
3.Name, address and telephone number of primary consultant:
ECS Southeast, LLP (ECS)
5260 Greens Dairy Road
Raleigh, NC 27616
[phone]
4.Name, address, telephone number, and state certification number of laboratory:
Red Lab, LLC (Red Lab)
5598 Marvin Moss Lane, Suite 2003
Wilmington, North Carolina 28409
[phone]
NCDEQ UVF accepted technology
&
Pace Analytical Services, Inc. (Pace)
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
[phone]
State Certification No. 12
D. UST Information
Tank No. Date
Installed
Size
(gallons)
Tank
Dimension
Last Contents Previous
Contents (if
any) UST-2 Unknown 10,000 26’5” x 8’ Heating Oil Unknown UST-A Unknown 10,000 16’9” x 10’ Diesel Unknown
E. Site Characteristics
1.Describe any past releases at this site:
Several past releases have been associated with the operations of several USTs located at the site with two
incidents identified on the Leaking Underground Storage Tank (LUST) database. ECS reviewed the NCDEQ file
for these incidents and are described below.
Incident No. 14620 indicated that one gasoline UST (UST-3) that was reportedly 150-gallons and one 275-
gallon heating oil UST (UST-4) were removed in 1995. At that same time, one 2,000-gallon heating oil UST
(UST-6) and one 275-gallon heating oil UST (UST-5) were closed in place at the site. Soil samples were not
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collected from beneath the two 275-gallon heating oil USTs and the 2,000-gallon gasoline UST during
removal or closure. One soil sample was collected from beneath the 150-gallon gasoline UST during
removal. Laboratory analysis detected 16,512 ppm (parts per million) total petroleum hydrocarbons (TPH) in
a sample collected from beneath the 150-gallon gasoline UST.
A Comprehensive Site Assessment (CSA) was performed in the vicinity of the 150-gallon gasoline UST. During
the assessment, one groundwater monitoring well was installed in the vicinity of the UST and four
groundwater monitoring wells were installed in proximity to the UST. Groundwater samples were collected
from the monitoring wells and analyzed for petroleum constituents. Petroleum constituents were not
detected above North Carolina 2L Ground Water Quality Standards (NC2LGWQS) in the four wells located in
proximity to the former UST. However, several petroleum constituents were detected above NC2LGWQS in
the sample collected from the monitoring well located at the former UST. The CSA indicates that the
groundwater contamination is confined to areas near the UST. Groundwater flow direction in the area of the
release was determined to be to the northwest.
Incident No. 19003 indicated that assessment took place during the removal of a 30,000-gallon heating oil
UST (UST-1) in 1998. During the removal, four soil samples were collected from beneath the UST and one
sample was collected from beneath the product line and analyzed for petroleum constituents. Several
petroleum constituents were detected above Maximum Soil Contamination Concentrations (MSCC) Soil-to-
Groundwater Standards in the sample collected from beneath the product piping.
A Phase I Limited Site Assessment was conducted in the vicinity of the 30,000-gallon heating oil UST. A
report issued January 29, 1999 indicated that one groundwater monitoring well was constructed in the
vicinity of the release and a groundwater sample was collected. The groundwater sample was analyzed for
petroleum constituents. No petroleum constituents were detected above NC2LGWQS.
ECS issued a Report of Environmental Assessment Services for this subject property in June 2008 (ECS
Project number 09-15656A). ECS was contracted to assess whether an undocumented release had occurred
from the three former USTs, and the existing UST that had not been assessed. The assessment was
conducted to assess the current concentrations in the soil and groundwater in the vicinity of the USTs.
Soil samples were collected from the vicinity of the former 150-gallon UST, the 30,000-gallon UST, the 2,000-
gallon UST, a previously closed in place 275-gallon UST and the existing 10,000-gallon UST (UST-2).
Laboratory analysis of soil samples collected from the former 2,000-gallon UST and the 275-gallon UST did
not identify petroleum-related compounds. ECS recommended that a No Further Action letter (NFA) be
issued for these areas.
Petroleum-related compounds were identified above action levels in soil samples collected from the vicinity
of the 10,000-gallon UST. Laboratory analysis of soil samples collected from the vicinity of the 30,000-gallon
UST identified petroleum-related compounds above their respective Soil-to-Groundwater and Residential
MSCCs.
Groundwater samples were collected from the vicinity of the 30,000-gallon UST and 10,000-gallon UST. Lead
was identified in one groundwater sample. Based on the lack of presence of other petroleum-related
compounds in the groundwater samples, it was ECS' opinion that the concentration of lead is naturally
occurring and related to a turbid sample. Due to the lack of additional petroleum-related compounds in the
vicinity of the former 150-gallon UST, ECS recommended that an NFA be issued in regards to the 150-gallon
UST.
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Greensboro, Guilford County, NC 27407
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ECS recommended that a NFA be issued for the site in regard to the 30,000-gallon UST and a Notice
of Residual Petroleum (NORP) be completed for the soil in the vicinity of the 30,000-gallon UST.
The NORP was recorded on November 18, 2009. The NORP indicated petroleum-contaminated soil is
present on the subject property and shall not be excavated or disturbed within three feet of the delineated
area. An NFA was issued for the Incident No. 19003 on November 9, 2009. An NFA was issued for Incident
No. 14620 on October 22, 2018.
2. Is the facility active or inactive at this time?
The approximate 39.78-acre subject property is occupied by the Whitestone Masonic and Eastern Star
Community. The subject property contains assisted living buildings, a care and wellness center, a boiler
building, dining building, a chapel, maintenance building, single-occupancy homes, cottages, a cemetery,
landscaped areas and asphalt roads and parking areas. The buildings are heated with natural gas, with the
exception of the Latham building, which is heated with steam produced in the boiler building. Water and
sanitary sewer services are provided by the City of Greensboro.
3.Describe surrounding property use (for example, residential, commercial, farming, etc.):
The site is located at 700 South Holden Road, Greensboro, Guilford County, North Carolina. The subject
property is located in a commercial/residential area of Greensboro, North Carolina. The subject property is
bound on the north by Wendover Avenue, followed by residential properties; on the east by South Holden
Road, followed by residential properties and a multi-unit retail building and a Dunkin Donuts; on the south
by an unnamed automobile repair facility, wooded land, single-family residence, Gay Terrace, Iglesia
Pentescostes, Crazy Tires, and Spring Garden Street, followed by Bain Oil, Phoenix Collision Repair, and Ray
Self Storage; and, on the west by Coapman Street, followed by residential properties and Wendover Ridge
Apartments. A portion of the Greensboro 7.5-minute NC quadrangle map has been included as Figure 1 and
details the site location and topography.
4.Describe site geology/hydrogeology:
Site geology has been characterized through observations of the two UST excavation sidewalls and bottom
as well as the sidewalls and bottom of the additional over-excavated area to the northwest of the two UST
basins. Based upon these observations, the site geology consisted of a reddish-brown silty clay from just
below ground surface (bgs) to the excavation’s maximum depth of 20-feet bgs. Neither bedrock nor
groundwater was encountered or observed in the UST excavation to its maximum dug depth of 20-feet bgs.
II.Closure Procedures
A. Describe preparations for closure including the steps taken to notify authorities, permits obtained
and the steps taken to clean and purge the tanks:
- On March 19, 2021, ECS conducted abandonment activities at monitoring wells MW-1-10K, MW-1, and
four additional monitoring wells located near MW-1. The additional monitoring wells were identified as
MW-2 through MW-5 by ECS personnel prior to conducting well abandonment activities. Upon arrival,
MW-1-10K was observed to have been damaged. ECS attempted to measure the depth of MW-1-10K
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but encountered refusal at approximately 8 feet below top of casing (ft btoc). After further inspection,
monitoring well MW-1-10K was presumed damaged and a groundwater sample was unable to be
collected. The combined 2-inch diameter monitoring well footage totaled 178 ft btoc. The monitoring
well abandonment records (Form GW-30) are included in Appendix A. Photo documentation depicting
abandonment activities is included in Appendix B.
- Prior to closure of the 10,000-gallon capacity heating oil UST, identified as UST-2, by removal, a
GW/UST-3 Form was submitted to the Guilford County Department of Health and Human Services on
April 20, 2021. A copy of the GW-UST-3 Form has been included in Appendix C.
- A total of 1,800-gallons of residual petroleum/ rinse water and 273-gallons of sludge were evacuated
from the two USTs in efforts to prepare the two USTs for removal on June 3, 2021 and June 9, 2021,
respectively. A copy of the liquid disposal manifests has been included in Appendix D.
- Buckeye Elm notified the City of Greensboro Fire Marshall’s Office of the UST removal and acquired
necessary permits. The two 10,000-gallon USTs (UST-2 and UST-A) were removed upon the Fire
Marshall's inspection and approval on April 2, 2019.
- A UST-2A and UST-2B Form, Site Investigation Report for Permanent Closure or Change-in-Service form
for both the registered tank and unregistered tank, were completed and emailed to the NCDEQ Central
office and the Guilford County Department of Health and Human Services on July 22, 2021. A copy of
the UST-2A has been included in Appendix E.
- Two 10,000-gallon capacity USTs respectively containing heating oil and diesel and approximately 20-
feet of associated product piping were removed as shown in Figure 2. The two 10,000-gallon capacity
USTs were measured to be 26’5” long by 8’ in diameter (UST-2), and 16’9” long by 10’ in diameter (UST-
A). Disposal manifests for the removed USTs are included in Appendix D.
B. Note the amount of residual material pumped from the tank(s):
- The two 10,000-gallon capacity USTs contained measurable fluids prior to removal on June 3, 2021 and
June 9, 2021, respectively. Buckeye Elm contracted with EVO to remove the residual materials. A
cumulative reported total of 1,800-gallons of petroleum impacted water and a total of 273-gallons of
sludge was measured on EVO’s vacuum truck on June 3, 2021 and June 8, 2021, respectively, prior to
mobilization offsite for disposal. A copy of the liquid disposal manifest has been included in Appendix D.
C. Describe the storage, handling, and disposal of the residual material:
- The residual material was transported by EVO to their facility in Winston-Salem, North Carolina for
disposal. A copy of the liquid disposal manifests has been included in Appendix D.
D. Excavation
1. Describe excavation procedures noting the condition of the soils and the dimensions of the excavation in
relation to the tanks, piping and/or pumps:
One 10,000-gallon capacity heating oil UST (UST-2) measuring 26’5” long by 8’ in diameter along 20 linear
feet of product line piping was removed on June 3, 2021. Additionally, one 10,000-gallon capacity “orphan”
diesel fuel UST (UST-A) measuring 16’9” long by 10’ wide was removed on June 9,2021. The locations of the
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removed USTs and product piping are shown on the Site Map included as Figure 2.

Excavation Procedures:

1.) The soils overlying UST-2 in the area of the fill port were noted to be stained from apparent
spillage/overfilling. This soil was excavated and temporarily stockpiled onto 10-mil thick poly
sheeting for future disposal. Additional apparent impacted soil was excavated from this area until it
was determined via field screening that the remaining soils no longer appeared to contained
petroleum impacts.

2.) Additional clean overburden soils were then excavated and stockpiled adjacent to the two UST
basin’s western sidewall until both USTs were fully uncovered and removed from their respective
basins. Upon removal, the USTs appeared to be in good condition with no corrosion holes observed.
See photo-documentation included in Appendix B. No evidence of a release was noted from either
of the two USTs upon their removal.

3.) Once removed from the basin, the two tanks were temporarily set upon the impacted
overburden soil stockpile. The tanks were then loaded onto a flat-bed trailer truck for
transportation to the recycling facility. UST-2 was transported offsite on June 3, 2021 following its
closure by removal and UST-A was transported offsite on June 9, 2021 following its closure by
removal. The Bill of Lading for the transport of the closed USTs has been included in Appendix D.

4.) Once the two 10,000-gallon USTs had been removed, over-excavation of impacted soils
associated with the former 30,000-gallon UST (UST-1) was conducted. These soils were load directly
into a stand-by dump truck following removal from the UST basin for transportation offsite.

5.) Over-excavation activities occurred throughout the previously delineated impacted soils
associated with the former 30,000-gallon UST release located to the northeast of the removed
10,000-gallon USTs. The overall horizontal extent of the over-excavation has also been illustrated on
Figure 2 and its vertical extent was terminated at depth of approximately 20 feet bgs.

2. Note the depth of tank burial(s) (from land surface to top of tank):

The first 10,000-gallon heating oil UST-2 was buried approximately 6 feet below ground surface and the
second 10,000-gallon “orphan” diesel UST-A was buried approximately 4 feet below ground surface.

3. Quantity of soil removed:

A total of approximately 683.33 tons of impacted soil was removed for disposal on June 3, 2021 through
June 4, 2021 and June 8, 2021, respectively. The removed impacted soil was transported by EVO to their
disposal facility located in Winston-Salem, NC. Certified weight tickets and disposal manifests have been
included in Appendix F.

4. Describe soil type(s):

Soil surrounding the UST was characterized through observations of the UST excavation sidewalls and
bottom. Based upon these observations, the surrounding soil consisted of a reddish-brown silty clay from
just below land surface to the excavation's maximum termination depth of 20 feet bgs. Neither competent
bedrock nor groundwater were encountered in the either of the two UST basins or the over excavated area
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to a depth of 20 feet bgs. See Photo-documentation attached in Appendix B.

5. Type and source of backfill used:

The excavation was backfilled with clean onsite materials and completed by the onsite grading contractor,
Frank L. Blum Construction Company.

E. Petroleum Hydrocarbon Impacted Soil

1. Describe how it was determined to what extent to excavate the soil:

A flame ionization detector (FID) was used to determine the presence of volatile organic vapor
concentrations in soils located near the fill port of the removed UST (UST-2) and soils associated with the
former 30,000-gallon UST (UST-1) release. Additionally, apparent petroleum staining and odors of the soils in
these locations were also used evaluate the extent of impacted soil. When these screening methods
suggested that the petroleum-impacted soils had been removed, ECS recommended that excavation be
terminated. The overall horizontal extent of the excavation has been illustrated on Figure 2 and its vertical
extent was terminated at depth of approximately 20 feet bgs.

2. Describe method of temporary storage, sampling, and treatment/disposal of soil:

Soils excavated for disposal from the fill port area were temporarily stockpiled on 10-mil thick poly sheeting.
Over-excavated soils that were associated with the former 30,000-gallon UST were loaded directly into
dump trucks for off-site disposal from June 3, 2021 through June 8, 2021, respectively. A total of
approximately 683.33 tons of impacted soil were removed for disposal. That total included the temporary
stockpiled fill port overburden and the over-excavated soil that was associated with the former 30,000-
gallon UST-1. The impacted soils were transported to EVO’s disposal facility located in Winston-Salem, NC.
Certified weight tickets and soil disposal manifests have been included in Appendix F.

Seven (7) UST closure samples were collected from directly beneath each bottom of the two 10,000-gallon
capacity USTs and the associated 20-feet of product line immediately following removal from their
respective basins. Closure soil samples, identified as UST-1A through UST-1C, were collected immediately
beneath the bottom of UST-2 at a depth of approximately 15-16 feet bgs and closure soil samples, identified
as UST-2A and UST-2B, were collected immediately beneath the bottom of UST-A at a depth of
approximately 14-15 feet bgs. The remaining closure samples, identified as L-1 and L-2, were collected
directly beneath the 20-foot length of product line associated UST-2 at a depth of approximately 5-6 feet
bgs. Each closure sample was submitted to the analytical laboratory for analyses of total petroleum
hydrocarbons (TPH) gasoline range organics (GRO) and diesel range organics (DRO) by ultraviolet
fluorescence (UVF) method. The closure soil samples was submitted to Red Labs, LLC (Red Labs), a North
Carolina certified laboratory located in Wilmington, NC per the dates and times included on the chain-of-
custody (COC) documentation. The Red Labs soil analytical laboratory report and COC has been included as
Appendix G.

Additionally, six (6) over-excavation soil samples were collected from the previously delineated impacted
soils associated with the former 30,000-gallon UST release. Two over-excavation samples were collected
from the base (B-1 and B-2) and four over-excavation samples were collected from the sidewalls (SW-1
through SW-4) of the excavated area as illustrated on Figure 2. B-1 and B-2 were collected along the
centerline of the base excavation area at a depth of ranging from approximately 16 to 20 feet bgs and SW-1
through SW-4 were collected along the sidewalls of the excavation area at a depth of ranging from
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approximately 16-20 feet bgs. Each over-excavation sample was submitted for analyses of volatile organic
compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270,
and Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons (EPH) by the
Massachusetts Department of Environmental Protection (MADEP) methods. The over-excavation soil
samples were submitted to Pace Analytical Services, LLC (Pace), a North Carolina certified laboratory located
in Huntersville, NC per the dates and times included on the COC documentation. The Pace soil analytical
laboratory report and COC has been included as Appendix G.
III. Site Investigation

A. Provide information on field screening and observations, include methods used to calibrate field
screening instrument(s):

Field screening was performed during soil excavation activities using a FID calibrated in accordance with
manufacturer’s instructions from June 3, 2021 through June 9, 2021. Additionally, the soils were visually
assessed for evidence of staining and evaluated for petroleum odors. FID measurements collected from the
soils taken directly below the center of the UST basins and associated product piping ranged from 7.1 parts
per million (ppm) to 21.6 ppm. Additionally, FID measurements collected from the soils taken from the
former 30,000-gallon UST over-excavation area ranged from 9.7 ppm to 28.7 ppm.

B. Describe soil sampling points and sampling procedures used, including:

- Location of samples
- Type of samples (from excavation, stockpiled soil, etc.)
- Sample collection procedures (grab, split spoon, hand auger, etc.)
- Depth of soil samples (below land surface)
- Whether samples were taken from side or floor of an excavation
- Sample identification and analyses

Stockpile Soil Sampling

One sample of the stockpiled soils was collected on June 3, 2021. The stockpile soil sample, identified as SP-
1, was collected from the overlying impacted soils surrounding the fill port of UST-2. The soil sample was
submitted in laboratory supplied containers to be analyzed for TPH GRO and DRO by UVF method.

UST Closure Soil Sampling

A total of seven (7) soil samples were collected for UST closure purposes on June 3, 2021 and June 9, 2021,
respectively, from the locations shown on Figure 2. Closure soil samples, identified as UST-1A through UST-
1C, were collected immediately beneath the bottom of UST-2 at a depth of approximately 15-16 feet bg.
Additionally, closure soil samples, identified as UST-2A and UST-2B, were collected immediately beneath the
bottom of UST-A at a depth of approximately 14-15 feet bgs. The remaining closure samples, identified as L-
1 and L-2, were collected directly beneath the 20-foot length of product line associated UST-2 at a depth of
approximately 5-6 feet bgs. Each closure soil sample was submitted in laboratory supplied containers to be
analyzed for TPH GRO and DRO by UVF method.

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Over-Excavation Soil Sampling

Excavation activities to remove the previously delineated impacted soils associated with the former 30,000-
gallon UST release were initiated on June 4, 2021. The final excavation limits of the area associated with the
30,000-gallon UST were measured to be 25-feet long by 12-feet wide by 20-feet deep as shown on Figure 2.
Following completion of over-excavation activities on June 8,2021, ECS collected six over-excavation soil
samples. Two over-excavation samples were collected from the base (B-1 and B-2) and four over-excavation
samples were collected from the sidewalls (SW-1 through SW-4) of the excavated area as illustrated on
Figure 2. B-1 and B-2 were collected along the centerline of the base excavation area at a depth of ranging
from approximately 16 to 20 feet bgs and SW-1 through SW-4 were collected along the sidewalls of the
excavation area at a depth of ranging from approximately 16-20 feet bgs.

Over-excavation soil samples were submitted in laboratory supplied containers to be analyzed for risk-based
soil characteristics including VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and VPH and EPH by
the MADEP methods. The post-excavation sample locations are illustrated on Figure 2.

C. Describe groundwater or surface water sampling procedures used, including:

Groundwater was not encountered or observed in the excavation to a depth of 20 feet bgs. No groundwater
or surface water sampling was performed.

D. Quality control measures

- Describe sample handling procedures including sample preservation and transportation:

The closure and over-excavation soil samples were collected in laboratory supplied/preserved containers
and transported to their respective North Carolina certified laboratories. Following placement in the
specified containers, the samples were placed within an ice chilled cooler and transported to the laboratory
for analyses per the dates and times listed in the COC included in Appendix G.

- Describe decontamination procedures used:

Each sample was collected from the excavator’s bucket using new disposable powder-free nitrile gloves.

- Describe time and date samples were collected and date submitted to laboratory:

Soil samples were collected on June 3, 2021, June 8, 2021, and June 9, 2021, respectively, during UST
removal and excavation activities. The samples were submitted to the analytical laboratory per the dates
and times listed in the COC included in Appendix G.

- Describe samples collected for quality control purposes (e.g., duplicates, field blanks, trip blanks,
etc.)
Include methods used to obtain these samples and analytical parameters: Not applicable
- Discuss how results of quality control samples may have affected your interpretation of soil,
groundwater, or surface water sample results: Not applicable

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E. Investigation results

- Describe methods of analyses used (include U.S. EPA method number)
- Describe analytical results for samples; discuss in relation to site specific cleanup level or action
level, as appropriate

Stockpile Soil Sample Quality

One stockpile soil sample was collected on June 3, 2021. The stockpile soil sample, identified as SP-1, was
collected from the overlying impacted soils surrounding the fill port of UST-2. The soil sample was submitted
for laboratory analysis for TPH GRO and DRO using the UVF method.

TPH GRO and DRO by UVF

Analysis by UVF for soil sample SP-1 reported a GRO concentration of 1,780 milligrams per kilogram (mg/Kg),
and DRO concentration of 11,892 mg/Kg. Both GRO and DRO concentrations were in excess of the NCDEQ
Soil Action Levels of 50 mg/Kg and 100 mg/Kg for GRO and DRO, respectively.

TPH GRO and DRO analytical results are presented in Table 1. Complete soil analytical laboratory reports
with COC documentation have been included in Appendix G.

UST Closure Soil Sample Quality

A total of seven (7) closure soil samples were collected on June 3, 2021 and June 9, 2021, respectively. The
samples, identified as UST-1A through UST-1C, were collected immediately beneath the bottom of UST-2 at
a depth of approximately 15-16 feet bgs and closure soil samples, identified as UST-2A and UST-2B, were
collected immediately beneath the bottom of UST-A at a depth of approximately 14-15 feet bgs. The
remaining closure samples, identified as L-1 and L-2, were collected directly beneath the 20-foot length of
product line associated UST-2 at a depth of approximately 5-6 feet bgs. Figure 2 illustrates the approximate
soil sample locations. Each closure soil sample were submitted for laboratory analysis for TPH GRO and DRO
using the UVF method.

TPH GRO and DRO by UVF

Analysis by UVF for each closure soil sample did not report GRO or DRO at a concentration above the NCDEQ
Soil Action Levels of 50 mg/Kg and 100 mg/Kg for GRO and DRO, respectively.

TPH GRO and DRO analytical results are presented in Table 1. Complete soil analytical laboratory reports
with COC documentation have been included in Appendix G.

Over-Excavation Soil Sample Quality – October 9, 2018

A total of six over-excavation soil samples were collected from the previously delineated impacted soils
associated with the former 30,000-gallon UST release. Two over-excavation samples were collected from the
base (B-1 and B-2) and four post-excavation samples were collected from the sidewalls (SW-1 through SW-4)
of the excavated area as illustrated on Figure 4. Each of the over-excavation soil samples were submitted for
analysis of VOCs, SVOCs, EPH) and VPH.

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VOCs Analytical Results

VOC analysis indicated several select targeted analytes to be above their respective laboratory reporting
limits, however, the concentrations do not exceed their respective Soil to Groundwater Maximum Soil
Contaminant Concentrations (MSCCs)or Residential MSCCs. A summary of VOC analytical results are
presented in Table 2. Complete laboratory reports with COC documentation have been included in
Appendix G.

SVOC Analytical Results

SVOC analysis indicated several select targeted analytes to be above their respective laboratory reporting
limits, however, the concentrations do not exceed their respective Soil to Groundwater MSCCs or
Residential MSCCs. A summary of SVOC analytical results are presented in Table 2. Complete laboratory
reports with COC documentation have been included in Appendix G.

EPH and VPH

Laboratory result so the EPS and VPH analysis indicated the following concentrations of method targeted
petroleum hydrocarbon fractions in soil samples SW-1 and SW-2: Aromatic petroleum hydrocarbon fraction
C9-C22 at 0.82 mg/Kg and at 1.6 mg/Kg respectively. Both concentrations are above the Soil to Groundwater
MSCC, however, do not exceed the Residential MSCC. No further EPH or VPH petroleum hydrocarbon
fractions were reported in excess of their respective Soil to Groundwater MSCCs or Residential MSCCs. A
summary of the results are provided in Table 3. Complete laboratory reports with COC documentation have
been included in Appendix G.

IV. Conclusions and Recommendations

Include probable sources of contamination, further investigation or remediation tasks, or whether no
further action is required.

Conclusions

The two former 10,000-gallon capacity USTs and their contents were removed from the site on June 3, 2021
and June 9, 2021, respectively. There are no further known USTs remaining on the property.

During the UST closure activities, the two USTs were observed to be in overall good condition with only
rusting and pitting observed on each UST. Residual fluids were measured in each UST prior to removal and a
recorded total of 1,800-gallons of petroleum impacted water and 273-gallons of sludge were evacuated
from the USTs on June 3, 2021 and June 8, 2021, respectively. Following evacuation of the residual liquids,
the two USTs were removed from their respective basins for disposal offsite.

Soil over-excavation activities were performed horizontally towards the northwest of the two 10,000-gallon
UST basins to a maximum excavation depth of 20-feet bgs. A total of approximately 683.33 tons of impacted
soil were removed for disposal. That total included the temporary stockpiled fill port overburden and the
over-excavated soil that was associated with the former 30,000-gallon UST-1 release. Over-excavation soil
quality sampling subsequently indicated that impacted soils were successfully removed to below their
700 South Holden Road
Greensboro, Guilford County, NC 27407

12
respective Residential MSCCs of the over-excavated area associated with the former 30,000-gallon UST-1
release.

Recommendations

ECS, on behalf of LCS Development, LLC, respectfully requests that return correspondence be made by the
NCDEQ following review of this report. Based upon the closure and over-excavation sample analytical results
collected from the two former UST basins and the over-excavation area associated with the former 30,000-
gallon UST-1 release, ECS recommends No Further Action (NFA) for this UST Closure and rescinding the
Notice of Residual Petroleum (NRP) placed on the property associated Incident No. 19003. However, due to
the Soil-to-Groundwater exceedances, the collection of one groundwater quality sample in the vicinity of
SW-1 and SW-2 may be determined necessary prior to obtaining a Letter of NFA.
V. Signature of Professional Engineer or Licensed Geologist

NC Licensed Geologist License #: 1724

Roger A. Smith ___________________________

700 South Holden Road
Greensboro, Guilford County, NC 27407

13

VI. Enclosures

A. Figures

1. Area Map(s) (can be USGS Topographic Quadrangle) showing:

- Adjacent streets, roads, highways with names and numbers
- Buildings
- Known distance to public water supply well(s)
- Distance to known private water supply well(s)
- Surface water bodies
- Groundwater flow direction (if available)
- Scale
- North arrow

2. Site map of UST excavation area drawn to scale, showing:

- Buildings
- Underground utilities such as sewer lines and other conduits
- Orientation of UST(s), pumps, and product lines
- Length, diameter and volume of USTs
- Type of material(s) stored in USTs (currently and previously)
- Sample locations (identified by letter or number)
- Final limits of excavation
- North arrow
- Scale
- Sample locations, depths, and identifications
- Analytical results
- Final limits of excavation(s)

B. Tables
- Soil Analytical Results Summary – GRO and DRO
- Summary of Soil Analytical Results - EPA Method 8260 and 8270
- Summary of Soil Analytical Results - MADEP EPH and VPH

C. Appendices

Appendix A: GW-30 Well Abandonment Forms
Appendix B: Photo-documentation
Appendix C: GW-UST-3 Form
Appendix D: Liquid and UST Disposal Manifests
Appendix E: GW-UST-2B Form
Appendix F: Soil Disposal Manifests and Certified Weight Tickets
Appendix G: Soil Laboratory Analytical Report with Chain of Custody Documentation

FIGURES

SOURCE:
USGS TOPOGRAPHIC MAP
7.5 –MINUTE SERIESGREENSBORO, NC QUADRANGLE
DATED: 2013
SCALE: 1 : 24,000
CONTOUR INTERVAL = 10’
FIGURE 1
SITE LOCATION MAP
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO 49:12057-A
SITE
SOURCE:
GOOGLE EARTH IMAGERYPUBLISHED: 2021
APPROXIMATE SCALE:
INITIAL ABATEMENT EXCAVATION AREAS
UST CLOSURE SAMPLE LOCATION
LEGEND
NOTES:
1.) SAMPLES COLLECTED ON 6/8/2021 THROUGH 6/9/2021.
2.) UST DIMENSIONS = 5’4” DIAMETER X 11’8” LONG
3.) “ORPHAN” UST DIMENSIONS = 5’4” DIAMETER X 11’8” LONG
FIGURE 2
SITE MAP
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO 49:12057-A
UST-1A
UST-1B
UST-1C
UST-2A
UST-2B
SW-1
SW-2SW-3
SW-4
B-1
B-2
= 30 FEET
10,000-GALLON “ORPHAN”
DIESEL UST REMOVED
10,000-GALLON HEATING
OIL UST REMOVED
OVER-EXCAVATION SAMPLE LOCATION
L-1
L-2
FORMER 30,000-GALLON UST
OVER-EXCAVATION AREA

TABLES

Sample GRO DROSampleSample Depth Sample FID Reading UFV UFV
ID Date (feet bgs)Type (ppm)Conc. in mg/Kg Conc. in mg/Kg
SP-1 6/3/2021 N/A Overburden Sample Grab 550 1,780 11,892
UST-1A 6/3/2021 15-16 UST Closure (Pre-excavation)Grab 9.7 5.8 39.7
UST-1B 6/3/2021 15-16 UST Closure (Pre-excavation)Grab 8.1 <0.34 0.57
UST-1C 6/3/2021 15-16 UST Closure (Pre-excavation)Grab 21.6 1.2 <0.63
L-1 6/9/2021 5-6 Line Closure (Pre-excavation)Grab 8.9 <0.54 1.7
L-2 6/9/2021 5-6 Line Closure (Pre-excavation)Grab 7.1 3.8 7.6
UST-2A 6/9/2021 14-15 UST Closure (Pre-excavation)Grab 11.2 <0.59 <0.59
UST-2B 6/9/2021 14-15 UST Closure (Pre-excavation)Grab 9.4 <0.47 0.47
NCDEQ Action Level -50 mg/Kg 100 mg/Kg
Notes:
1.) Bold Font indicates exceedance of the North Carolina Department of Environmental Quality (NCDEQ) Action Level.
2.) This table summary of results reflects analytical data for soil samples collected on 6/3/2021 and 6/9/2021, respectively.
3.) FID denotes Flame Ionization Detector.
4.) ppm denotes parts per million.
5.) UFV denotes Ultraviolet Fluorescence
Composite or
Grab Sample?
Table 1: Soil Analytical Results Summary - GRO and DRO
Whitestone Assisted Living Facility
700 South Holden Road
Greensboro, Guilford County, North Carolina
ECS Project No. 49:12057-A
EPA Method 8260
Sample ID SW-1 B-1 SW-2 B-2 SW-3 SW-4
Sample Depth (ft. bgs)16-18 18-19 16-18 18-20 16-18 16-18
FID Reading (ppm)12.5 10.6 11.8 28.7 9.7 15.1
Sample Date
Detected Compounds
sec-Butylbenzene BRL BRL 0.051 BRL BRL 0.10 2.2 1,560 23,300
Chlorobenzene 0.013 BRL BRL BRL BRL BRL 0.44 312 4,670
EPA Method 8270
Sample ID SW-1 B-1 SW-2 B-2 SW-3 SW-4
Sample Depth (ft. bgs)16-18 18-19 16-18 18-20 16-18 16-18
Percent Moisture (%)26.9 29.8 28.6 30.3 27.1 28.9
Sample Date
Detected Compounds
Phenanthrene BRL BRL 0.69 BRL BRL BRL 64 469 7,000
Notes:
1.) Results presented in (mg/kg)
2.) MSCCs denote Maximum Soil Contaminant Concentrations (DWM, NCDEQ, UST Section, 10/20/2020)
3.) ft. bgs denotes feet below ground surface.
4.) FID denotes Flame Ionization Detector.
5.) ppm denotes parts per million.
6.) BRL denotes below reporting limit as stated on analytical report.7.) Refer to analytical laboratory report for individual analyte reporting and method detection limits.
All Results in mg/Kg
All Results in mg/Kg
700 South Holden Road
Comparison Criteria
Table 2: Summary of Soil Laboratory Analytical Results - EPA Method 8260 & EPA Method 8270
Whitestone Assisted Living Facility
Comparison Criteria
Method (Parameter)EPA Method 8270
Method (Parameter)EPA Method 8260
Soil to Groundwater
MSCCs Residential MSCCs
Soil to Groundwater
MSCCs
Greensboro, Guilford County, North Carolina
ECS Project No. 49:12057-A
Industrial/Commercial
MSCCs6/8/2021
Residential MSCCs Industrial/Commercial
MSCCs6/8/2021
MADEP EPH and VPH
SW-1 B-1 SW-2 B-2 SW-3 SW-4
16-18 18-19 16-18 18-20 16-18 16-18
12.5 10.6 11.8 28.7 9.7 15.1
BRL BRL 17.0 BRL BRL BRL 68 939 24,528
C9-C12 Aliphatics
C9-C18 Aliphatics
BRL BRL BRL BRL 14.1 BRL Considered
Immobile 31,000 810,000
C9-C10 Aromatics
C11-C22 Aromatics
Massachusetts Department of Environmental Protection (MADEP) Extractable Petroleum Hydrocarbon (EPH) and Volatile Petroleum Hydrocarbon (VPH) notes:
1.) Results presented in (mg/Kg).
2.) MSCC denotes Maximum Soil Contaminant Concentration (DWM, NCDEQ, UST Section, 10/20/2020).
3.) ft. bgs denotes feet below ground surface.
4.) FID denotes Flame Ionization Detector.
5.) ppm denotes parts per million.
6.) BOLD denotes concentration exceeds the Soil to Groundwater MSCC.
7.) BRL denotes below reporting limit as stated on analytical report.
8.) Refer to analytical laboratory report for individual analyte reporting and method detection limits.
Table 3: Summary of Soil Analytical Results - MADEP EPH and VPH
Whitestone Assisted Living Facility
700 South Holden Road
Greensboro, Guilford County, North Carolina
ECS Project No. 49:12057-A
Sample ID Comparison Criteria
Sample Depth (ft. bgs)
Soil to
Groundwater
MSCCs
Residential
MSCCs
Industrial/
Commercial
MSCCs
FID Reading (ppm)
Sample Date 6/8/2021
Method (Parameter)MADEP EPH and VPH
Detected Hydrocarbon Fraction Ranges
BRL
All Results in mg/Kg
C5-C8 Aliphatics
C9-C18 Aliphatics 159.7 BRL 173.2 BRL 41.2 163
C19-C36 Aliphatics
C9-C22 Aromatics 41.0 BRL 48.9 BRL 14.9 31 469 12,264
540 1,500 40,000

Appendix A:

GW-30 Well Abandonment Forms

Appendix B:

Photo Documentation

Photo 1 –View of MW-1-10K upon arrival on 3/19/2021.
Photo 2 –View of MW-1-10K once well head was exposed.
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 3 –View of MW-1 and MW-2 following abandonment activities.
Photo 4 –View of MW-3 and MW-4 following abandonment activities.
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
MW-1
MW-2
MW-3
MW-4
Photo 5 –View of MW-5 following abandonment activities.
Photo 6 –View of MW-1-10K following abandonment activities.
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 7 –UST-1 Residual Liquids Being Removed Using a Vacuum Truck
Photo 8 –UST-1 Uncovered
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 9 –UST-1 Removed From Excavation
Photo 10 –Endcap Of UST-1
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 11 –Hole Near Top of UST-1
Photo 12 –Holes in Top of UST-1 Endcap
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 13 –UST-1 Transported Off-Site for Disposal
Photo 14 –Uncovering UST-2
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 15 –UST-2 Residual Liquids Being Removed Using a Vacuum Truck
Photo 16 –UST-2 Removed from Excavation
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A
Photo 17 –Loading UST-2 for Off-Site Disposal
Photo 20 –Backfill and Compaction of UST Excavation
PHOTO DOCUMENTATION
WHITESTONE ASSISTED LIVING FACILITY
700 SOUTH HOLDEN ROAD
GREENSBORO, GUILFORD COUNTY, NC
ECS PROJECT NO. 49:12057-A

Appendix C:

GW-UST-3 Form

UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY I.D. #_____________________ Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities. If a Professional Engineer (P.E.) or a Licensed
Geologist (L.G.) provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports then at least a five
(5) working days’ notice is acceptable.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted to the
appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be
submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank Closure
and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust. Note: To close tanks in place you must
obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address
Facility ID # (If known)

City

County
Street Address

State
Zip Code
City
County
Zip Code

Phone Number Email Phone Number

III. CONTACT PERSONNEL
Name:

Company Name:

Job Title:

Phone Number:

IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty (30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G. is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:

Contractor Company Name:

Address:

State:

Zip Code:

Phone No:

Primary Consultant Name:

Primary Consultant Company Name:

Consultant Phone No:

VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE

Tank ID No.

Size in Gallons

Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place * New Contents Stored

* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed

SCHEDULED REMOVAL DATE

Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 3/2020 3/2020
Masonic & Eastern Star Home of NC, Inc.
700 South Holden Road
Greensboro Guildford
NC 27407
336-299-0031
WhiteStone
00-0-0000030330
700 South Holden Road
Greensboro Guilford 27407
336-547-2961
David Kane, AIA Senior Design Manager LCS Development 515-875-4568
Matthew Gillis Buckeye Elm Contracting
PO Box 1026 27028 919-280-7175
Samantha M. Szakasits, G.I.T.ECS Southeast, LLP
NC
919-616-2679
■
Samantha M. Szakasits, G.I.T. / Environmental Staff Project Manager
4/20/2021 5/17/2021
■

Appendix D:

Liquid and UST Disposal Manifests

1333 Research Road
Columbus, Ohio 43230
Phone: [phone]
BUCKEYE ELM CONTRACTING, LLC
TANK DISPOSAL CERTIFICATE

Tank Owner: Masonic & AMP Eastern Star Home of NC

Site Address: 700 South Holden Road
Greensboro, NC

Description of Tank(s): Liquid and Vapor Free

Tank Number Size of Tank Contents
1 10,000 Diesel

Transporter: DH Griffin

Buckeye Elm Project: ECS UST Removal Whitestone Living Facility, Greensboro, NC

Buckeye Elm Project No: 20-21-0001

Disposal Certification:

Buckeye Elm Contracting does hereby certify that the above-named storage tank was transported to DH Griffin Wrecking
Company, 4716 Hilltop Road, Greensboro, North Carolina 27407 for proper disposal and recycling.

_________________________________________________
Signature

Matt Gillis
SE Regional Account Manager
Buckeye Elm Contracting

Appendix E:

GW-UST-2A & GW-UST-2B Form

Appendix F:

Soil Disposal Manifests and Certified Weight Tickets

Appendix G:

Soil Laboratory Analytical Report with Chain-of-Custody Documentation

Hydrocarbon Analysis Results
Client:ECS Samples taken Thursday, June 3, 2021
Address:GSO, NC 27407 Samples extracted Thursday, June 3, 2021
Samples analysed Friday, June 4, 2021
Contact:Randy Cavllier Operator Tori Kelly
Project:Whitestone
4 U04049
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s UST-1A 23.9 <0.6 5.8 39.7 45.5 11.8 0.44 <0.024 82.3 16.6 1 Deg.Diesel 78.8%,(FCM)
s UST-1B 13.7 <0.34 <0.34 0.57 0.57 0.32 <0.11 <0.014 0 69.6 30.4 V.Deg.PHC 77.3%,(FCM)
s UST-1C 25.0 <0.63 1.2 <0.63 1.2 <0.13 <0.2 <0.025 100 0 0 Residual HC
s SP-1 3959.0 <99 1780 11892 13672 3541 132.9 <4 80.1 19 0.9 Deg.Diesel 78.1%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 107.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
Hydrocarbon Analysis Results
Client:ECS Southeast Samples taken Wednesday, June 9, 2021
Address:Greensboro, NC Samples extracted Wednesday, June 9, 2021
Samples analysed Thursday, June 10, 2021
Contact:Randy Cavallier Operator Tori Kelly
Project:Whitestone
4 F03640
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s L-1 21.7 <0.54 <0.54 1.7 1.7 0.79 <0.17 <0.022 0 70.9 29.1 V.Deg.PHC 93.8%,(FCM)
s L-2 24.1 <0.6 3.8 7.6 11.4 8.6 0.4 <0.024 61.8 31.4 6.8 Deg.Fuel 80.1%,(FCM)
s UST-2A 23.4 <0.59 <0.59 <0.59 <0.59 <0.12 <0.19 <0.023 0 0 0 PHC not detected,(BO)
s UST-2B 18.9 <0.47 <0.47 0.47 0.47 0.3 <0.15 <0.019 0 50.6 49.4 Residual HC
Initial Calibrator QC check OK Final FCM QC Check OK 109.2 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
#=CL#
June 16, 2021
LIMS USE: FR - SAMANTHA
LIMS OBJECT ID: 92543280
92543280
Project:
Pace Project No.:
RE:
Samantha M. Szakasits, G.I.T.
ECS Southeast, LLP
5260 Greens Dary Road
Raleigh, NC 27616
Whitestone Assisted Living Fac
Dear Samantha Szakasits, G.I.T.:
Enclosed are the analytical results for sample(s) received by the laboratory on June 09, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
Scott Werley, ECS Southeast, LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92543280001 SW-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92543280002 B-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92543280003 SW-2 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92543280004 B-2 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92543280005 SW-3 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92543280006 SW-4 MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-1 Lab ID:92543280001 Collected:06/08/21 10:15 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)153 mg/kg 06/15/21 13:50 N206/11/21 17:1054.9 4
Aliphatic (C19-C36)ND mg/kg 06/15/21 13:50 N206/11/21 17:1054.9 4
Aromatic (C11-C22)41.0 mg/kg 06/14/21 16:51 N206/11/21 17:1013.7 1
Surrogates
1-Chlorooctadecane (S)106 %06/15/21 13:50 3386-33-206/11/21 17:1040-140 4
o-Terphenyl (S)100 %06/14/21 16:51 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)101 %06/14/21 16:51 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)113 %06/14/21 16:51 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 06/12/21 04:31 N206/11/21 15:004.0 1
Aliphatic (C09-C12)6.7 mg/kg 06/12/21 04:31 N206/11/21 15:004.0 1
Aliphatic(C09-C12) Adjusted 6.7 mg/kg 06/12/21 04:31 N206/11/21 15:004.0 1
Aromatic (C09-C10)ND mg/kg 06/12/21 04:31 N206/11/21 15:004.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)115 %06/12/21 04:31 460-00-406/11/21 15:0070-130 1
4-Bromofluorobenzene (PID) (S)114 %06/12/21 04:31 460-00-406/11/21 15:0070-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 13:16 83-32-906/10/21 13:030.44 1
Acenaphthylene ND mg/kg 06/11/21 13:16 208-96-806/10/21 13:030.44 1
Aniline ND mg/kg 06/11/21 13:16 62-53-306/10/21 13:030.44 1
Anthracene ND mg/kg 06/11/21 13:16 120-12-706/10/21 13:030.44 1
Benzo(a)anthracene ND mg/kg 06/11/21 13:16 56-55-306/10/21 13:030.44 1
Benzo(a)pyrene ND mg/kg 06/11/21 13:16 50-32-806/10/21 13:030.44 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 13:16 205-99-206/10/21 13:030.44 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 13:16 191-24-206/10/21 13:030.44 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 13:16 207-08-906/10/21 13:030.44 1
Benzoic Acid ND mg/kg 06/11/21 13:16 65-85-006/10/21 13:032.2 1
Benzyl alcohol ND mg/kg 06/11/21 13:16 100-51-606/10/21 13:030.89 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 13:16 101-55-306/10/21 13:030.44 1
Butylbenzylphthalate ND mg/kg 06/11/21 13:16 85-68-706/10/21 13:030.44 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 13:16 59-50-706/10/21 13:030.89 1
4-Chloroaniline ND mg/kg 06/11/21 13:16 106-47-806/10/21 13:030.89 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 13:16 111-91-106/10/21 13:030.44 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 13:16 111-44-406/10/21 13:030.44 1
2-Chloronaphthalene ND mg/kg 06/11/21 13:16 91-58-706/10/21 13:030.44 1
2-Chlorophenol ND mg/kg 06/11/21 13:16 95-57-806/10/21 13:030.44 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 13:16 7005-72-306/10/21 13:030.44 1
Chrysene ND mg/kg 06/11/21 13:16 218-01-906/10/21 13:030.44 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 13:16 53-70-306/10/21 13:030.44 1
Dibenzofuran ND mg/kg 06/11/21 13:16 132-64-906/10/21 13:030.44 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 13:16 95-50-106/10/21 13:030.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-1 Lab ID:92543280001 Collected:06/08/21 10:15 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 13:16 541-73-106/10/21 13:030.44 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 13:16 106-46-706/10/21 13:030.44 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 13:16 91-94-1 IL06/10/21 13:030.89 1
2,4-Dichlorophenol ND mg/kg 06/11/21 13:16 120-83-206/10/21 13:030.44 1
Diethylphthalate ND mg/kg 06/11/21 13:16 84-66-206/10/21 13:030.44 1
2,4-Dimethylphenol ND mg/kg 06/11/21 13:16 105-67-906/10/21 13:030.44 1
Dimethylphthalate ND mg/kg 06/11/21 13:16 131-11-306/10/21 13:030.44 1
Di-n-butylphthalate ND mg/kg 06/11/21 13:16 84-74-206/10/21 13:030.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 13:16 534-52-1 v106/10/21 13:030.89 1
2,4-Dinitrophenol ND mg/kg 06/11/21 13:16 51-28-5 v106/10/21 13:032.2 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 13:16 121-14-206/10/21 13:030.44 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 13:16 606-20-206/10/21 13:030.44 1
Di-n-octylphthalate ND mg/kg 06/11/21 13:16 117-84-006/10/21 13:030.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 13:16 117-81-706/10/21 13:030.44 1
Fluoranthene ND mg/kg 06/11/21 13:16 206-44-006/10/21 13:030.44 1
Fluorene ND mg/kg 06/11/21 13:16 86-73-706/10/21 13:030.44 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 13:16 87-68-306/10/21 13:030.44 1
Hexachlorobenzene ND mg/kg 06/11/21 13:16 118-74-106/10/21 13:030.44 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 13:16 77-47-406/10/21 13:030.44 1
Hexachloroethane ND mg/kg 06/11/21 13:16 67-72-106/10/21 13:030.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 13:16 193-39-506/10/21 13:030.44 1
Isophorone ND mg/kg 06/11/21 13:16 78-59-106/10/21 13:030.44 1
1-Methylnaphthalene ND mg/kg 06/11/21 13:16 90-12-006/10/21 13:030.44 1
2-Methylnaphthalene ND mg/kg 06/11/21 13:16 91-57-606/10/21 13:030.44 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 13:16 95-48-706/10/21 13:030.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 13:16 15831-10-406/10/21 13:030.44 1
Naphthalene ND mg/kg 06/11/21 13:16 91-20-306/10/21 13:030.44 1
2-Nitroaniline ND mg/kg 06/11/21 13:16 88-74-406/10/21 13:032.2 1
3-Nitroaniline ND mg/kg 06/11/21 13:16 99-09-2 IL06/10/21 13:032.2 1
4-Nitroaniline ND mg/kg 06/11/21 13:16 100-01-606/10/21 13:030.89 1
Nitrobenzene ND mg/kg 06/11/21 13:16 98-95-306/10/21 13:030.44 1
2-Nitrophenol ND mg/kg 06/11/21 13:16 88-75-506/10/21 13:030.44 1
4-Nitrophenol ND mg/kg 06/11/21 13:16 100-02-706/10/21 13:032.2 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 13:16 62-75-906/10/21 13:030.44 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 13:16 621-64-706/10/21 13:030.44 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 13:16 86-30-606/10/21 13:030.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 13:16 108-60-106/10/21 13:030.44 1
Pentachlorophenol ND mg/kg 06/11/21 13:16 87-86-506/10/21 13:030.89 1
Phenanthrene ND mg/kg 06/11/21 13:16 85-01-806/10/21 13:030.44 1
Phenol ND mg/kg 06/11/21 13:16 108-95-206/10/21 13:030.44 1
Pyrene ND mg/kg 06/11/21 13:16 129-00-006/10/21 13:030.44 1
Pyridine ND mg/kg 06/11/21 13:16 110-86-106/10/21 13:030.44 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 13:16 120-82-106/10/21 13:030.44 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 13:16 95-95-406/10/21 13:030.44 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 13:16 88-06-206/10/21 13:030.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-1 Lab ID:92543280001 Collected:06/08/21 10:15 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)67 %06/11/21 13:16 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)67 %06/11/21 13:16 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)64 %06/11/21 13:16 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)66 %06/11/21 13:16 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)65 %06/11/21 13:16 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)79 %06/11/21 13:16 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 21:17 67-64-106/09/21 16:540.16 1
Benzene ND mg/kg 06/10/21 21:17 71-43-206/09/21 16:540.0080 1
Bromobenzene ND mg/kg 06/10/21 21:17 108-86-106/09/21 16:540.0080 1
Bromochloromethane ND mg/kg 06/10/21 21:17 74-97-506/09/21 16:540.0080 1
Bromodichloromethane ND mg/kg 06/10/21 21:17 75-27-406/09/21 16:540.0080 1
Bromoform ND mg/kg 06/10/21 21:17 75-25-206/09/21 16:540.0080 1
Bromomethane ND mg/kg 06/10/21 21:17 74-83-9 IK06/09/21 16:540.016 1
2-Butanone (MEK)ND mg/kg 06/10/21 21:17 78-93-306/09/21 16:540.16 1
n-Butylbenzene ND mg/kg 06/10/21 21:17 104-51-806/09/21 16:540.0080 1
sec-Butylbenzene ND mg/kg 06/10/21 21:17 135-98-806/09/21 16:540.0080 1
tert-Butylbenzene ND mg/kg 06/10/21 21:17 98-06-606/09/21 16:540.0080 1
Carbon tetrachloride ND mg/kg 06/10/21 21:17 56-23-506/09/21 16:540.0080 1
Chlorobenzene 0.013 mg/kg 06/10/21 21:17 108-90-706/09/21 16:540.0080 1
Chloroethane ND mg/kg 06/10/21 21:17 75-00-306/09/21 16:540.016 1
Chloroform ND mg/kg 06/10/21 21:17 67-66-306/09/21 16:540.0080 1
Chloromethane ND mg/kg 06/10/21 21:17 74-87-306/09/21 16:540.016 1
2-Chlorotoluene ND mg/kg 06/10/21 21:17 95-49-806/09/21 16:540.0080 1
4-Chlorotoluene ND mg/kg 06/10/21 21:17 106-43-406/09/21 16:540.0080 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 21:17 96-12-806/09/21 16:540.0080 1
Dibromochloromethane ND mg/kg 06/10/21 21:17 124-48-106/09/21 16:540.0080 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 21:17 106-93-406/09/21 16:540.0080 1
Dibromomethane ND mg/kg 06/10/21 21:17 74-95-306/09/21 16:540.0080 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 21:17 95-50-106/09/21 16:540.0080 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 21:17 541-73-106/09/21 16:540.0080 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 21:17 106-46-706/09/21 16:540.0080 1
Dichlorodifluoromethane ND mg/kg 06/10/21 21:17 75-71-806/09/21 16:540.016 1
1,1-Dichloroethane ND mg/kg 06/10/21 21:17 75-34-306/09/21 16:540.0080 1
1,2-Dichloroethane ND mg/kg 06/10/21 21:17 107-06-206/09/21 16:540.0080 1
1,1-Dichloroethene ND mg/kg 06/10/21 21:17 75-35-406/09/21 16:540.0080 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 21:17 156-59-206/09/21 16:540.0080 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 21:17 156-60-506/09/21 16:540.0080 1
1,2-Dichloropropane ND mg/kg 06/10/21 21:17 78-87-506/09/21 16:540.0080 1
1,3-Dichloropropane ND mg/kg 06/10/21 21:17 142-28-906/09/21 16:540.0080 1
2,2-Dichloropropane ND mg/kg 06/10/21 21:17 594-20-706/09/21 16:540.0080 1
1,1-Dichloropropene ND mg/kg 06/10/21 21:17 563-58-606/09/21 16:540.0080 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-1 Lab ID:92543280001 Collected:06/08/21 10:15 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 21:17 10061-01-506/09/21 16:540.0080 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 21:17 10061-02-606/09/21 16:540.0080 1
Diisopropyl ether ND mg/kg 06/10/21 21:17 108-20-306/09/21 16:540.0080 1
Ethylbenzene ND mg/kg 06/10/21 21:17 100-41-406/09/21 16:540.0080 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 21:17 87-68-306/09/21 16:540.016 1
2-Hexanone ND mg/kg 06/10/21 21:17 591-78-606/09/21 16:540.080 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 21:17 98-82-806/09/21 16:540.0080 1
p-Isopropyltoluene ND mg/kg 06/10/21 21:17 99-87-606/09/21 16:540.0080 1
Methylene Chloride ND mg/kg 06/10/21 21:17 75-09-206/09/21 16:540.032 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 21:17 108-10-106/09/21 16:540.080 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 21:17 1634-04-406/09/21 16:540.0080 1
Naphthalene ND mg/kg 06/10/21 21:17 91-20-306/09/21 16:540.0080 1
n-Propylbenzene ND mg/kg 06/10/21 21:17 103-65-106/09/21 16:540.0080 1
Styrene ND mg/kg 06/10/21 21:17 100-42-506/09/21 16:540.0080 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 21:17 630-20-606/09/21 16:540.0080 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 21:17 79-34-506/09/21 16:540.0080 1
Tetrachloroethene ND mg/kg 06/10/21 21:17 127-18-406/09/21 16:540.0080 1
Toluene ND mg/kg 06/10/21 21:17 108-88-306/09/21 16:540.0080 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 21:17 87-61-606/09/21 16:540.0080 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 21:17 120-82-106/09/21 16:540.0080 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 21:17 71-55-606/09/21 16:540.0080 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 21:17 79-00-506/09/21 16:540.0080 1
Trichloroethene ND mg/kg 06/10/21 21:17 79-01-606/09/21 16:540.0080 1
Trichlorofluoromethane ND mg/kg 06/10/21 21:17 75-69-406/09/21 16:540.0080 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 21:17 96-18-406/09/21 16:540.0080 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 21:17 95-63-606/09/21 16:540.0080 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 21:17 108-67-806/09/21 16:540.0080 1
Vinyl acetate ND mg/kg 06/10/21 21:17 108-05-406/09/21 16:540.080 1
Vinyl chloride ND mg/kg 06/10/21 21:17 75-01-406/09/21 16:540.016 1
Xylene (Total)ND mg/kg 06/10/21 21:17 1330-20-706/09/21 16:540.016 1
m&p-Xylene ND mg/kg 06/10/21 21:17 179601-23-106/09/21 16:540.016 1
o-Xylene ND mg/kg 06/10/21 21:17 95-47-606/09/21 16:540.0080 1
Surrogates
Toluene-d8 (S)104 %06/10/21 21:17 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)97 %06/10/21 21:17 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)104 %06/10/21 21:17 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.9 %06/09/21 16:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-1 Lab ID:92543280002 Collected:06/08/21 10:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/14/21 17:19 N206/11/21 17:1014.2 1
Aliphatic (C19-C36)ND mg/kg 06/14/21 17:19 N206/11/21 17:1014.2 1
Aromatic (C11-C22)ND mg/kg 06/14/21 17:19 N206/11/21 17:1014.2 1
Surrogates
1-Chlorooctadecane (S)56 %06/14/21 17:19 3386-33-206/11/21 17:1040-140 1
o-Terphenyl (S)65 %06/14/21 17:19 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)92 %06/14/21 17:19 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)92 %06/14/21 17:19 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 06/14/21 15:53 N206/14/21 12:464.7 1
Aliphatic (C09-C12)ND mg/kg 06/14/21 15:53 N206/14/21 12:464.7 1
Aliphatic(C09-C12) Adjusted ND mg/kg 06/14/21 15:53 N206/14/21 12:464.7 1
Aromatic (C09-C10)ND mg/kg 06/14/21 15:53 N206/14/21 12:464.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)106 %06/14/21 15:53 460-00-406/14/21 12:4670-130 1
4-Bromofluorobenzene (PID) (S)103 %06/14/21 15:53 460-00-406/14/21 12:4670-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 13:43 83-32-906/10/21 13:030.47 1
Acenaphthylene ND mg/kg 06/11/21 13:43 208-96-806/10/21 13:030.47 1
Aniline ND mg/kg 06/11/21 13:43 62-53-306/10/21 13:030.47 1
Anthracene ND mg/kg 06/11/21 13:43 120-12-706/10/21 13:030.47 1
Benzo(a)anthracene ND mg/kg 06/11/21 13:43 56-55-306/10/21 13:030.47 1
Benzo(a)pyrene ND mg/kg 06/11/21 13:43 50-32-806/10/21 13:030.47 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 13:43 205-99-206/10/21 13:030.47 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 13:43 191-24-206/10/21 13:030.47 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 13:43 207-08-906/10/21 13:030.47 1
Benzoic Acid ND mg/kg 06/11/21 13:43 65-85-006/10/21 13:032.4 1
Benzyl alcohol ND mg/kg 06/11/21 13:43 100-51-606/10/21 13:030.94 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 13:43 101-55-306/10/21 13:030.47 1
Butylbenzylphthalate ND mg/kg 06/11/21 13:43 85-68-706/10/21 13:030.47 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 13:43 59-50-706/10/21 13:030.94 1
4-Chloroaniline ND mg/kg 06/11/21 13:43 106-47-806/10/21 13:030.94 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 13:43 111-91-106/10/21 13:030.47 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 13:43 111-44-406/10/21 13:030.47 1
2-Chloronaphthalene ND mg/kg 06/11/21 13:43 91-58-706/10/21 13:030.47 1
2-Chlorophenol ND mg/kg 06/11/21 13:43 95-57-806/10/21 13:030.47 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 13:43 7005-72-306/10/21 13:030.47 1
Chrysene ND mg/kg 06/11/21 13:43 218-01-906/10/21 13:030.47 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 13:43 53-70-306/10/21 13:030.47 1
Dibenzofuran ND mg/kg 06/11/21 13:43 132-64-906/10/21 13:030.47 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 13:43 95-50-106/10/21 13:030.47 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-1 Lab ID:92543280002 Collected:06/08/21 10:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 13:43 541-73-106/10/21 13:030.47 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 13:43 106-46-706/10/21 13:030.47 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 13:43 91-94-1 IL06/10/21 13:030.94 1
2,4-Dichlorophenol ND mg/kg 06/11/21 13:43 120-83-206/10/21 13:030.47 1
Diethylphthalate ND mg/kg 06/11/21 13:43 84-66-206/10/21 13:030.47 1
2,4-Dimethylphenol ND mg/kg 06/11/21 13:43 105-67-906/10/21 13:030.47 1
Dimethylphthalate ND mg/kg 06/11/21 13:43 131-11-306/10/21 13:030.47 1
Di-n-butylphthalate ND mg/kg 06/11/21 13:43 84-74-206/10/21 13:030.47 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 13:43 534-52-1 v106/10/21 13:030.94 1
2,4-Dinitrophenol ND mg/kg 06/11/21 13:43 51-28-5 v106/10/21 13:032.4 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 13:43 121-14-206/10/21 13:030.47 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 13:43 606-20-206/10/21 13:030.47 1
Di-n-octylphthalate ND mg/kg 06/11/21 13:43 117-84-006/10/21 13:030.47 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 13:43 117-81-706/10/21 13:030.47 1
Fluoranthene ND mg/kg 06/11/21 13:43 206-44-006/10/21 13:030.47 1
Fluorene ND mg/kg 06/11/21 13:43 86-73-706/10/21 13:030.47 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 13:43 87-68-306/10/21 13:030.47 1
Hexachlorobenzene ND mg/kg 06/11/21 13:43 118-74-106/10/21 13:030.47 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 13:43 77-47-406/10/21 13:030.47 1
Hexachloroethane ND mg/kg 06/11/21 13:43 67-72-106/10/21 13:030.47 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 13:43 193-39-506/10/21 13:030.47 1
Isophorone ND mg/kg 06/11/21 13:43 78-59-106/10/21 13:030.47 1
1-Methylnaphthalene ND mg/kg 06/11/21 13:43 90-12-006/10/21 13:030.47 1
2-Methylnaphthalene ND mg/kg 06/11/21 13:43 91-57-606/10/21 13:030.47 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 13:43 95-48-706/10/21 13:030.47 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 13:43 15831-10-406/10/21 13:030.47 1
Naphthalene ND mg/kg 06/11/21 13:43 91-20-306/10/21 13:030.47 1
2-Nitroaniline ND mg/kg 06/11/21 13:43 88-74-406/10/21 13:032.4 1
3-Nitroaniline ND mg/kg 06/11/21 13:43 99-09-2 IL06/10/21 13:032.4 1
4-Nitroaniline ND mg/kg 06/11/21 13:43 100-01-606/10/21 13:030.94 1
Nitrobenzene ND mg/kg 06/11/21 13:43 98-95-306/10/21 13:030.47 1
2-Nitrophenol ND mg/kg 06/11/21 13:43 88-75-506/10/21 13:030.47 1
4-Nitrophenol ND mg/kg 06/11/21 13:43 100-02-706/10/21 13:032.4 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 13:43 62-75-906/10/21 13:030.47 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 13:43 621-64-706/10/21 13:030.47 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 13:43 86-30-606/10/21 13:030.47 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 13:43 108-60-106/10/21 13:030.47 1
Pentachlorophenol ND mg/kg 06/11/21 13:43 87-86-506/10/21 13:030.94 1
Phenanthrene ND mg/kg 06/11/21 13:43 85-01-806/10/21 13:030.47 1
Phenol ND mg/kg 06/11/21 13:43 108-95-206/10/21 13:030.47 1
Pyrene ND mg/kg 06/11/21 13:43 129-00-006/10/21 13:030.47 1
Pyridine ND mg/kg 06/11/21 13:43 110-86-106/10/21 13:030.47 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 13:43 120-82-106/10/21 13:030.47 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 13:43 95-95-406/10/21 13:030.47 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 13:43 88-06-206/10/21 13:030.47 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-1 Lab ID:92543280002 Collected:06/08/21 10:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)72 %06/11/21 13:43 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)79 %06/11/21 13:43 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)77 %06/11/21 13:43 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)75 %06/11/21 13:43 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)76 %06/11/21 13:43 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)87 %06/11/21 13:43 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 21:52 67-64-106/09/21 16:540.20 1
Benzene ND mg/kg 06/10/21 21:52 71-43-206/09/21 16:540.0098 1
Bromobenzene ND mg/kg 06/10/21 21:52 108-86-106/09/21 16:540.0098 1
Bromochloromethane ND mg/kg 06/10/21 21:52 74-97-506/09/21 16:540.0098 1
Bromodichloromethane ND mg/kg 06/10/21 21:52 75-27-406/09/21 16:540.0098 1
Bromoform ND mg/kg 06/10/21 21:52 75-25-206/09/21 16:540.0098 1
Bromomethane ND mg/kg 06/10/21 21:52 74-83-9 IK06/09/21 16:540.020 1
2-Butanone (MEK)ND mg/kg 06/10/21 21:52 78-93-306/09/21 16:540.20 1
n-Butylbenzene ND mg/kg 06/10/21 21:52 104-51-806/09/21 16:540.0098 1
sec-Butylbenzene ND mg/kg 06/10/21 21:52 135-98-806/09/21 16:540.0098 1
tert-Butylbenzene ND mg/kg 06/10/21 21:52 98-06-606/09/21 16:540.0098 1
Carbon tetrachloride ND mg/kg 06/10/21 21:52 56-23-506/09/21 16:540.0098 1
Chlorobenzene ND mg/kg 06/10/21 21:52 108-90-706/09/21 16:540.0098 1
Chloroethane ND mg/kg 06/10/21 21:52 75-00-306/09/21 16:540.020 1
Chloroform ND mg/kg 06/10/21 21:52 67-66-306/09/21 16:540.0098 1
Chloromethane ND mg/kg 06/10/21 21:52 74-87-306/09/21 16:540.020 1
2-Chlorotoluene ND mg/kg 06/10/21 21:52 95-49-806/09/21 16:540.0098 1
4-Chlorotoluene ND mg/kg 06/10/21 21:52 106-43-406/09/21 16:540.0098 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 21:52 96-12-806/09/21 16:540.0098 1
Dibromochloromethane ND mg/kg 06/10/21 21:52 124-48-106/09/21 16:540.0098 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 21:52 106-93-406/09/21 16:540.0098 1
Dibromomethane ND mg/kg 06/10/21 21:52 74-95-306/09/21 16:540.0098 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 21:52 95-50-106/09/21 16:540.0098 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 21:52 541-73-106/09/21 16:540.0098 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 21:52 106-46-706/09/21 16:540.0098 1
Dichlorodifluoromethane ND mg/kg 06/10/21 21:52 75-71-806/09/21 16:540.020 1
1,1-Dichloroethane ND mg/kg 06/10/21 21:52 75-34-306/09/21 16:540.0098 1
1,2-Dichloroethane ND mg/kg 06/10/21 21:52 107-06-206/09/21 16:540.0098 1
1,1-Dichloroethene ND mg/kg 06/10/21 21:52 75-35-406/09/21 16:540.0098 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 21:52 156-59-206/09/21 16:540.0098 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 21:52 156-60-506/09/21 16:540.0098 1
1,2-Dichloropropane ND mg/kg 06/10/21 21:52 78-87-506/09/21 16:540.0098 1
1,3-Dichloropropane ND mg/kg 06/10/21 21:52 142-28-906/09/21 16:540.0098 1
2,2-Dichloropropane ND mg/kg 06/10/21 21:52 594-20-706/09/21 16:540.0098 1
1,1-Dichloropropene ND mg/kg 06/10/21 21:52 563-58-606/09/21 16:540.0098 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-1 Lab ID:92543280002 Collected:06/08/21 10:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 21:52 10061-01-506/09/21 16:540.0098 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 21:52 10061-02-606/09/21 16:540.0098 1
Diisopropyl ether ND mg/kg 06/10/21 21:52 108-20-306/09/21 16:540.0098 1
Ethylbenzene ND mg/kg 06/10/21 21:52 100-41-406/09/21 16:540.0098 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 21:52 87-68-306/09/21 16:540.020 1
2-Hexanone ND mg/kg 06/10/21 21:52 591-78-606/09/21 16:540.098 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 21:52 98-82-806/09/21 16:540.0098 1
p-Isopropyltoluene ND mg/kg 06/10/21 21:52 99-87-606/09/21 16:540.0098 1
Methylene Chloride ND mg/kg 06/10/21 21:52 75-09-206/09/21 16:540.039 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 21:52 108-10-106/09/21 16:540.098 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 21:52 1634-04-406/09/21 16:540.0098 1
Naphthalene ND mg/kg 06/10/21 21:52 91-20-306/09/21 16:540.0098 1
n-Propylbenzene ND mg/kg 06/10/21 21:52 103-65-106/09/21 16:540.0098 1
Styrene ND mg/kg 06/10/21 21:52 100-42-506/09/21 16:540.0098 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 21:52 630-20-606/09/21 16:540.0098 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 21:52 79-34-506/09/21 16:540.0098 1
Tetrachloroethene ND mg/kg 06/10/21 21:52 127-18-406/09/21 16:540.0098 1
Toluene ND mg/kg 06/10/21 21:52 108-88-306/09/21 16:540.0098 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 21:52 87-61-606/09/21 16:540.0098 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 21:52 120-82-106/09/21 16:540.0098 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 21:52 71-55-606/09/21 16:540.0098 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 21:52 79-00-506/09/21 16:540.0098 1
Trichloroethene ND mg/kg 06/10/21 21:52 79-01-606/09/21 16:540.0098 1
Trichlorofluoromethane ND mg/kg 06/10/21 21:52 75-69-406/09/21 16:540.0098 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 21:52 96-18-406/09/21 16:540.0098 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 21:52 95-63-606/09/21 16:540.0098 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 21:52 108-67-806/09/21 16:540.0098 1
Vinyl acetate ND mg/kg 06/10/21 21:52 108-05-406/09/21 16:540.098 1
Vinyl chloride ND mg/kg 06/10/21 21:52 75-01-406/09/21 16:540.020 1
Xylene (Total)ND mg/kg 06/10/21 21:52 1330-20-706/09/21 16:540.020 1
m&p-Xylene ND mg/kg 06/10/21 21:52 179601-23-106/09/21 16:540.020 1
o-Xylene ND mg/kg 06/10/21 21:52 95-47-606/09/21 16:540.0098 1
Surrogates
Toluene-d8 (S)101 %06/10/21 21:52 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)96 %06/10/21 21:52 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)103 %06/10/21 21:52 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.8 %06/09/21 16:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-2 Lab ID:92543280003 Collected:06/08/21 11:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)113 mg/kg 06/15/21 14:18 N206/11/21 17:1035.0 2.5
Aliphatic (C19-C36)ND mg/kg 06/15/21 14:18 N206/11/21 17:1035.0 2.5
Aromatic (C11-C22)48.9 mg/kg 06/14/21 17:46 N206/11/21 17:1014.0 1
Surrogates
1-Chlorooctadecane (S)84 %06/15/21 14:18 3386-33-206/11/21 17:1040-140 2.5
o-Terphenyl (S)94 %06/14/21 17:46 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)110 %06/14/21 17:46 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)112 %06/14/21 17:46 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)17.0 mg/kg 06/12/21 05:28 N206/11/21 15:004.5 1
Aliphatic (C09-C12)60.2 mg/kg 06/12/21 05:28 N206/11/21 15:004.5 1
Aliphatic(C09-C12) Adjusted 60.2 mg/kg 06/12/21 05:28 N206/11/21 15:004.5 1
Aromatic (C09-C10)ND mg/kg 06/12/21 05:28 N206/11/21 15:004.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)125 %06/12/21 05:28 460-00-406/11/21 15:0070-130 1
4-Bromofluorobenzene (PID) (S)102 %06/12/21 05:28 460-00-406/11/21 15:0070-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 14:10 83-32-906/10/21 13:030.46 1
Acenaphthylene ND mg/kg 06/11/21 14:10 208-96-806/10/21 13:030.46 1
Aniline ND mg/kg 06/11/21 14:10 62-53-306/10/21 13:030.46 1
Anthracene ND mg/kg 06/11/21 14:10 120-12-706/10/21 13:030.46 1
Benzo(a)anthracene ND mg/kg 06/11/21 14:10 56-55-306/10/21 13:030.46 1
Benzo(a)pyrene ND mg/kg 06/11/21 14:10 50-32-806/10/21 13:030.46 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 14:10 205-99-206/10/21 13:030.46 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 14:10 191-24-206/10/21 13:030.46 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 14:10 207-08-906/10/21 13:030.46 1
Benzoic Acid ND mg/kg 06/11/21 14:10 65-85-006/10/21 13:032.3 1
Benzyl alcohol ND mg/kg 06/11/21 14:10 100-51-606/10/21 13:030.91 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 14:10 101-55-306/10/21 13:030.46 1
Butylbenzylphthalate ND mg/kg 06/11/21 14:10 85-68-706/10/21 13:030.46 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 14:10 59-50-706/10/21 13:030.91 1
4-Chloroaniline ND mg/kg 06/11/21 14:10 106-47-806/10/21 13:030.91 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 14:10 111-91-106/10/21 13:030.46 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 14:10 111-44-406/10/21 13:030.46 1
2-Chloronaphthalene ND mg/kg 06/11/21 14:10 91-58-706/10/21 13:030.46 1
2-Chlorophenol ND mg/kg 06/11/21 14:10 95-57-806/10/21 13:030.46 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 14:10 7005-72-306/10/21 13:030.46 1
Chrysene ND mg/kg 06/11/21 14:10 218-01-906/10/21 13:030.46 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 14:10 53-70-306/10/21 13:030.46 1
Dibenzofuran ND mg/kg 06/11/21 14:10 132-64-906/10/21 13:030.46 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 14:10 95-50-106/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-2 Lab ID:92543280003 Collected:06/08/21 11:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 14:10 541-73-106/10/21 13:030.46 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 14:10 106-46-706/10/21 13:030.46 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 14:10 91-94-1 IL06/10/21 13:030.91 1
2,4-Dichlorophenol ND mg/kg 06/11/21 14:10 120-83-206/10/21 13:030.46 1
Diethylphthalate ND mg/kg 06/11/21 14:10 84-66-206/10/21 13:030.46 1
2,4-Dimethylphenol ND mg/kg 06/11/21 14:10 105-67-906/10/21 13:030.46 1
Dimethylphthalate ND mg/kg 06/11/21 14:10 131-11-306/10/21 13:030.46 1
Di-n-butylphthalate ND mg/kg 06/11/21 14:10 84-74-206/10/21 13:030.46 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 14:10 534-52-1 v106/10/21 13:030.91 1
2,4-Dinitrophenol ND mg/kg 06/11/21 14:10 51-28-5 v106/10/21 13:032.3 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 14:10 121-14-206/10/21 13:030.46 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 14:10 606-20-206/10/21 13:030.46 1
Di-n-octylphthalate ND mg/kg 06/11/21 14:10 117-84-006/10/21 13:030.46 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 14:10 117-81-706/10/21 13:030.46 1
Fluoranthene ND mg/kg 06/11/21 14:10 206-44-006/10/21 13:030.46 1
Fluorene ND mg/kg 06/11/21 14:10 86-73-706/10/21 13:030.46 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 14:10 87-68-306/10/21 13:030.46 1
Hexachlorobenzene ND mg/kg 06/11/21 14:10 118-74-106/10/21 13:030.46 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 14:10 77-47-406/10/21 13:030.46 1
Hexachloroethane ND mg/kg 06/11/21 14:10 67-72-106/10/21 13:030.46 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 14:10 193-39-506/10/21 13:030.46 1
Isophorone ND mg/kg 06/11/21 14:10 78-59-106/10/21 13:030.46 1
1-Methylnaphthalene ND mg/kg 06/11/21 14:10 90-12-006/10/21 13:030.46 1
2-Methylnaphthalene ND mg/kg 06/11/21 14:10 91-57-606/10/21 13:030.46 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 14:10 95-48-706/10/21 13:030.46 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 14:10 15831-10-406/10/21 13:030.46 1
Naphthalene ND mg/kg 06/11/21 14:10 91-20-306/10/21 13:030.46 1
2-Nitroaniline ND mg/kg 06/11/21 14:10 88-74-406/10/21 13:032.3 1
3-Nitroaniline ND mg/kg 06/11/21 14:10 99-09-2 IL06/10/21 13:032.3 1
4-Nitroaniline ND mg/kg 06/11/21 14:10 100-01-606/10/21 13:030.91 1
Nitrobenzene ND mg/kg 06/11/21 14:10 98-95-306/10/21 13:030.46 1
2-Nitrophenol ND mg/kg 06/11/21 14:10 88-75-506/10/21 13:030.46 1
4-Nitrophenol ND mg/kg 06/11/21 14:10 100-02-706/10/21 13:032.3 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 14:10 62-75-906/10/21 13:030.46 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 14:10 621-64-706/10/21 13:030.46 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 14:10 86-30-606/10/21 13:030.46 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 14:10 108-60-106/10/21 13:030.46 1
Pentachlorophenol ND mg/kg 06/11/21 14:10 87-86-506/10/21 13:030.91 1
Phenanthrene 0.69 mg/kg 06/11/21 14:10 85-01-806/10/21 13:030.46 1
Phenol ND mg/kg 06/11/21 14:10 108-95-206/10/21 13:030.46 1
Pyrene ND mg/kg 06/11/21 14:10 129-00-006/10/21 13:030.46 1
Pyridine ND mg/kg 06/11/21 14:10 110-86-106/10/21 13:030.46 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 14:10 120-82-106/10/21 13:030.46 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 14:10 95-95-406/10/21 13:030.46 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 14:10 88-06-206/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-2 Lab ID:92543280003 Collected:06/08/21 11:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)77 %06/11/21 14:10 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)79 %06/11/21 14:10 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)87 %06/11/21 14:10 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)80 %06/11/21 14:10 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)79 %06/11/21 14:10 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)108 %06/11/21 14:10 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 22:45 67-64-106/09/21 16:540.17 1
Benzene ND mg/kg 06/10/21 22:45 71-43-206/09/21 16:540.0084 1
Bromobenzene ND mg/kg 06/10/21 22:45 108-86-106/09/21 16:540.0084 1
Bromochloromethane ND mg/kg 06/10/21 22:45 74-97-506/09/21 16:540.0084 1
Bromodichloromethane ND mg/kg 06/10/21 22:45 75-27-406/09/21 16:540.0084 1
Bromoform ND mg/kg 06/10/21 22:45 75-25-206/09/21 16:540.0084 1
Bromomethane ND mg/kg 06/10/21 22:45 74-83-9 IK06/09/21 16:540.017 1
2-Butanone (MEK)ND mg/kg 06/10/21 22:45 78-93-306/09/21 16:540.17 1
n-Butylbenzene ND mg/kg 06/10/21 22:45 104-51-806/09/21 16:540.0084 1
sec-Butylbenzene 0.051 mg/kg 06/10/21 22:45 135-98-806/09/21 16:540.0084 1
tert-Butylbenzene ND mg/kg 06/10/21 22:45 98-06-606/09/21 16:540.0084 1
Carbon tetrachloride ND mg/kg 06/10/21 22:45 56-23-506/09/21 16:540.0084 1
Chlorobenzene ND mg/kg 06/10/21 22:45 108-90-706/09/21 16:540.0084 1
Chloroethane ND mg/kg 06/10/21 22:45 75-00-306/09/21 16:540.017 1
Chloroform ND mg/kg 06/10/21 22:45 67-66-306/09/21 16:540.0084 1
Chloromethane ND mg/kg 06/10/21 22:45 74-87-306/09/21 16:540.017 1
2-Chlorotoluene ND mg/kg 06/10/21 22:45 95-49-806/09/21 16:540.0084 1
4-Chlorotoluene ND mg/kg 06/10/21 22:45 106-43-406/09/21 16:540.0084 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 22:45 96-12-806/09/21 16:540.0084 1
Dibromochloromethane ND mg/kg 06/10/21 22:45 124-48-106/09/21 16:540.0084 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 22:45 106-93-406/09/21 16:540.0084 1
Dibromomethane ND mg/kg 06/10/21 22:45 74-95-306/09/21 16:540.0084 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 22:45 95-50-106/09/21 16:540.0084 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 22:45 541-73-106/09/21 16:540.0084 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 22:45 106-46-706/09/21 16:540.0084 1
Dichlorodifluoromethane ND mg/kg 06/10/21 22:45 75-71-806/09/21 16:540.017 1
1,1-Dichloroethane ND mg/kg 06/10/21 22:45 75-34-306/09/21 16:540.0084 1
1,2-Dichloroethane ND mg/kg 06/10/21 22:45 107-06-206/09/21 16:540.0084 1
1,1-Dichloroethene ND mg/kg 06/10/21 22:45 75-35-406/09/21 16:540.0084 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 22:45 156-59-206/09/21 16:540.0084 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 22:45 156-60-506/09/21 16:540.0084 1
1,2-Dichloropropane ND mg/kg 06/10/21 22:45 78-87-506/09/21 16:540.0084 1
1,3-Dichloropropane ND mg/kg 06/10/21 22:45 142-28-906/09/21 16:540.0084 1
2,2-Dichloropropane ND mg/kg 06/10/21 22:45 594-20-706/09/21 16:540.0084 1
1,1-Dichloropropene ND mg/kg 06/10/21 22:45 563-58-606/09/21 16:540.0084 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-2 Lab ID:92543280003 Collected:06/08/21 11:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 22:45 10061-01-506/09/21 16:540.0084 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 22:45 10061-02-606/09/21 16:540.0084 1
Diisopropyl ether ND mg/kg 06/10/21 22:45 108-20-306/09/21 16:540.0084 1
Ethylbenzene ND mg/kg 06/10/21 22:45 100-41-406/09/21 16:540.0084 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 22:45 87-68-306/09/21 16:540.017 1
2-Hexanone ND mg/kg 06/10/21 22:45 591-78-606/09/21 16:540.084 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 22:45 98-82-806/09/21 16:540.0084 1
p-Isopropyltoluene ND mg/kg 06/10/21 22:45 99-87-606/09/21 16:540.0084 1
Methylene Chloride ND mg/kg 06/10/21 22:45 75-09-206/09/21 16:540.034 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 22:45 108-10-106/09/21 16:540.084 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 22:45 1634-04-406/09/21 16:540.0084 1
Naphthalene ND mg/kg 06/10/21 22:45 91-20-306/09/21 16:540.0084 1
n-Propylbenzene ND mg/kg 06/10/21 22:45 103-65-106/09/21 16:540.0084 1
Styrene ND mg/kg 06/10/21 22:45 100-42-506/09/21 16:540.0084 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 22:45 630-20-606/09/21 16:540.0084 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 22:45 79-34-506/09/21 16:540.0084 1
Tetrachloroethene ND mg/kg 06/10/21 22:45 127-18-406/09/21 16:540.0084 1
Toluene ND mg/kg 06/10/21 22:45 108-88-306/09/21 16:540.0084 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 22:45 87-61-606/09/21 16:540.0084 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 22:45 120-82-106/09/21 16:540.0084 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 22:45 71-55-606/09/21 16:540.0084 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 22:45 79-00-506/09/21 16:540.0084 1
Trichloroethene ND mg/kg 06/10/21 22:45 79-01-606/09/21 16:540.0084 1
Trichlorofluoromethane ND mg/kg 06/10/21 22:45 75-69-406/09/21 16:540.0084 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 22:45 96-18-406/09/21 16:540.0084 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 22:45 95-63-606/09/21 16:540.0084 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 22:45 108-67-806/09/21 16:540.0084 1
Vinyl acetate ND mg/kg 06/10/21 22:45 108-05-406/09/21 16:540.084 1
Vinyl chloride ND mg/kg 06/10/21 22:45 75-01-406/09/21 16:540.017 1
Xylene (Total)ND mg/kg 06/10/21 22:45 1330-20-706/09/21 16:540.017 1
m&p-Xylene ND mg/kg 06/10/21 22:45 179601-23-106/09/21 16:540.017 1
o-Xylene ND mg/kg 06/10/21 22:45 95-47-606/09/21 16:540.0084 1
Surrogates
Toluene-d8 (S)101 %06/10/21 22:45 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)104 %06/10/21 22:45 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)101 %06/10/21 22:45 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.6 %06/09/21 16:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-2 Lab ID:92543280004 Collected:06/08/21 11:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/14/21 18:14 N206/11/21 17:1014.4 1
Aliphatic (C19-C36)ND mg/kg 06/14/21 18:14 N206/11/21 17:1014.4 1
Aromatic (C11-C22)ND mg/kg 06/14/21 18:14 N206/11/21 17:1014.4 1
Surrogates
1-Chlorooctadecane (S)53 %06/14/21 18:14 3386-33-206/11/21 17:1040-140 1
o-Terphenyl (S)61 %06/14/21 18:14 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)92 %06/14/21 18:14 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)92 %06/14/21 18:14 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 06/14/21 16:21 N206/14/21 12:464.5 1
Aliphatic (C09-C12)ND mg/kg 06/14/21 16:21 N206/14/21 12:464.5 1
Aliphatic(C09-C12) Adjusted ND mg/kg 06/14/21 16:21 N206/14/21 12:464.5 1
Aromatic (C09-C10)ND mg/kg 06/14/21 16:21 N206/14/21 12:464.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)99 %06/14/21 16:21 460-00-406/14/21 12:4670-130 1
4-Bromofluorobenzene (PID) (S)97 %06/14/21 16:21 460-00-406/14/21 12:4670-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 14:38 83-32-906/10/21 13:030.48 1
Acenaphthylene ND mg/kg 06/11/21 14:38 208-96-806/10/21 13:030.48 1
Aniline ND mg/kg 06/11/21 14:38 62-53-306/10/21 13:030.48 1
Anthracene ND mg/kg 06/11/21 14:38 120-12-706/10/21 13:030.48 1
Benzo(a)anthracene ND mg/kg 06/11/21 14:38 56-55-306/10/21 13:030.48 1
Benzo(a)pyrene ND mg/kg 06/11/21 14:38 50-32-806/10/21 13:030.48 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 14:38 205-99-206/10/21 13:030.48 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 14:38 191-24-206/10/21 13:030.48 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 14:38 207-08-906/10/21 13:030.48 1
Benzoic Acid ND mg/kg 06/11/21 14:38 65-85-006/10/21 13:032.4 1
Benzyl alcohol ND mg/kg 06/11/21 14:38 100-51-606/10/21 13:030.96 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 14:38 101-55-306/10/21 13:030.48 1
Butylbenzylphthalate ND mg/kg 06/11/21 14:38 85-68-706/10/21 13:030.48 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 14:38 59-50-706/10/21 13:030.96 1
4-Chloroaniline ND mg/kg 06/11/21 14:38 106-47-806/10/21 13:030.96 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 14:38 111-91-106/10/21 13:030.48 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 14:38 111-44-406/10/21 13:030.48 1
2-Chloronaphthalene ND mg/kg 06/11/21 14:38 91-58-706/10/21 13:030.48 1
2-Chlorophenol ND mg/kg 06/11/21 14:38 95-57-806/10/21 13:030.48 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 14:38 7005-72-306/10/21 13:030.48 1
Chrysene ND mg/kg 06/11/21 14:38 218-01-906/10/21 13:030.48 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 14:38 53-70-306/10/21 13:030.48 1
Dibenzofuran ND mg/kg 06/11/21 14:38 132-64-906/10/21 13:030.48 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 14:38 95-50-106/10/21 13:030.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-2 Lab ID:92543280004 Collected:06/08/21 11:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 14:38 541-73-106/10/21 13:030.48 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 14:38 106-46-706/10/21 13:030.48 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 14:38 91-94-1 IL06/10/21 13:030.96 1
2,4-Dichlorophenol ND mg/kg 06/11/21 14:38 120-83-206/10/21 13:030.48 1
Diethylphthalate ND mg/kg 06/11/21 14:38 84-66-206/10/21 13:030.48 1
2,4-Dimethylphenol ND mg/kg 06/11/21 14:38 105-67-906/10/21 13:030.48 1
Dimethylphthalate ND mg/kg 06/11/21 14:38 131-11-306/10/21 13:030.48 1
Di-n-butylphthalate ND mg/kg 06/11/21 14:38 84-74-206/10/21 13:030.48 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 14:38 534-52-1 v106/10/21 13:030.96 1
2,4-Dinitrophenol ND mg/kg 06/11/21 14:38 51-28-5 v106/10/21 13:032.4 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 14:38 121-14-206/10/21 13:030.48 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 14:38 606-20-206/10/21 13:030.48 1
Di-n-octylphthalate ND mg/kg 06/11/21 14:38 117-84-006/10/21 13:030.48 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 14:38 117-81-706/10/21 13:030.48 1
Fluoranthene ND mg/kg 06/11/21 14:38 206-44-006/10/21 13:030.48 1
Fluorene ND mg/kg 06/11/21 14:38 86-73-706/10/21 13:030.48 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 14:38 87-68-306/10/21 13:030.48 1
Hexachlorobenzene ND mg/kg 06/11/21 14:38 118-74-106/10/21 13:030.48 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 14:38 77-47-406/10/21 13:030.48 1
Hexachloroethane ND mg/kg 06/11/21 14:38 67-72-106/10/21 13:030.48 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 14:38 193-39-506/10/21 13:030.48 1
Isophorone ND mg/kg 06/11/21 14:38 78-59-106/10/21 13:030.48 1
1-Methylnaphthalene ND mg/kg 06/11/21 14:38 90-12-006/10/21 13:030.48 1
2-Methylnaphthalene ND mg/kg 06/11/21 14:38 91-57-606/10/21 13:030.48 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 14:38 95-48-706/10/21 13:030.48 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 14:38 15831-10-406/10/21 13:030.48 1
Naphthalene ND mg/kg 06/11/21 14:38 91-20-306/10/21 13:030.48 1
2-Nitroaniline ND mg/kg 06/11/21 14:38 88-74-406/10/21 13:032.4 1
3-Nitroaniline ND mg/kg 06/11/21 14:38 99-09-2 IL06/10/21 13:032.4 1
4-Nitroaniline ND mg/kg 06/11/21 14:38 100-01-606/10/21 13:030.96 1
Nitrobenzene ND mg/kg 06/11/21 14:38 98-95-306/10/21 13:030.48 1
2-Nitrophenol ND mg/kg 06/11/21 14:38 88-75-506/10/21 13:030.48 1
4-Nitrophenol ND mg/kg 06/11/21 14:38 100-02-706/10/21 13:032.4 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 14:38 62-75-906/10/21 13:030.48 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 14:38 621-64-706/10/21 13:030.48 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 14:38 86-30-606/10/21 13:030.48 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 14:38 108-60-106/10/21 13:030.48 1
Pentachlorophenol ND mg/kg 06/11/21 14:38 87-86-506/10/21 13:030.96 1
Phenanthrene ND mg/kg 06/11/21 14:38 85-01-806/10/21 13:030.48 1
Phenol ND mg/kg 06/11/21 14:38 108-95-206/10/21 13:030.48 1
Pyrene ND mg/kg 06/11/21 14:38 129-00-006/10/21 13:030.48 1
Pyridine ND mg/kg 06/11/21 14:38 110-86-106/10/21 13:030.48 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 14:38 120-82-106/10/21 13:030.48 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 14:38 95-95-406/10/21 13:030.48 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 14:38 88-06-206/10/21 13:030.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-2 Lab ID:92543280004 Collected:06/08/21 11:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)73 %06/11/21 14:38 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)77 %06/11/21 14:38 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)75 %06/11/21 14:38 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)74 %06/11/21 14:38 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)76 %06/11/21 14:38 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)86 %06/11/21 14:38 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 22:10 67-64-106/09/21 16:540.19 1
Benzene ND mg/kg 06/10/21 22:10 71-43-206/09/21 16:540.0093 1
Bromobenzene ND mg/kg 06/10/21 22:10 108-86-106/09/21 16:540.0093 1
Bromochloromethane ND mg/kg 06/10/21 22:10 74-97-506/09/21 16:540.0093 1
Bromodichloromethane ND mg/kg 06/10/21 22:10 75-27-406/09/21 16:540.0093 1
Bromoform ND mg/kg 06/10/21 22:10 75-25-206/09/21 16:540.0093 1
Bromomethane ND mg/kg 06/10/21 22:10 74-83-9 IK06/09/21 16:540.019 1
2-Butanone (MEK)ND mg/kg 06/10/21 22:10 78-93-306/09/21 16:540.19 1
n-Butylbenzene ND mg/kg 06/10/21 22:10 104-51-806/09/21 16:540.0093 1
sec-Butylbenzene ND mg/kg 06/10/21 22:10 135-98-806/09/21 16:540.0093 1
tert-Butylbenzene ND mg/kg 06/10/21 22:10 98-06-606/09/21 16:540.0093 1
Carbon tetrachloride ND mg/kg 06/10/21 22:10 56-23-506/09/21 16:540.0093 1
Chlorobenzene ND mg/kg 06/10/21 22:10 108-90-706/09/21 16:540.0093 1
Chloroethane ND mg/kg 06/10/21 22:10 75-00-306/09/21 16:540.019 1
Chloroform ND mg/kg 06/10/21 22:10 67-66-306/09/21 16:540.0093 1
Chloromethane ND mg/kg 06/10/21 22:10 74-87-306/09/21 16:540.019 1
2-Chlorotoluene ND mg/kg 06/10/21 22:10 95-49-806/09/21 16:540.0093 1
4-Chlorotoluene ND mg/kg 06/10/21 22:10 106-43-406/09/21 16:540.0093 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 22:10 96-12-806/09/21 16:540.0093 1
Dibromochloromethane ND mg/kg 06/10/21 22:10 124-48-106/09/21 16:540.0093 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 22:10 106-93-406/09/21 16:540.0093 1
Dibromomethane ND mg/kg 06/10/21 22:10 74-95-306/09/21 16:540.0093 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 22:10 95-50-106/09/21 16:540.0093 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 22:10 541-73-106/09/21 16:540.0093 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 22:10 106-46-706/09/21 16:540.0093 1
Dichlorodifluoromethane ND mg/kg 06/10/21 22:10 75-71-806/09/21 16:540.019 1
1,1-Dichloroethane ND mg/kg 06/10/21 22:10 75-34-306/09/21 16:540.0093 1
1,2-Dichloroethane ND mg/kg 06/10/21 22:10 107-06-206/09/21 16:540.0093 1
1,1-Dichloroethene ND mg/kg 06/10/21 22:10 75-35-406/09/21 16:540.0093 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 22:10 156-59-206/09/21 16:540.0093 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 22:10 156-60-506/09/21 16:540.0093 1
1,2-Dichloropropane ND mg/kg 06/10/21 22:10 78-87-506/09/21 16:540.0093 1
1,3-Dichloropropane ND mg/kg 06/10/21 22:10 142-28-906/09/21 16:540.0093 1
2,2-Dichloropropane ND mg/kg 06/10/21 22:10 594-20-706/09/21 16:540.0093 1
1,1-Dichloropropene ND mg/kg 06/10/21 22:10 563-58-606/09/21 16:540.0093 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:B-2 Lab ID:92543280004 Collected:06/08/21 11:20 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 22:10 10061-01-506/09/21 16:540.0093 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 22:10 10061-02-606/09/21 16:540.0093 1
Diisopropyl ether ND mg/kg 06/10/21 22:10 108-20-306/09/21 16:540.0093 1
Ethylbenzene ND mg/kg 06/10/21 22:10 100-41-406/09/21 16:540.0093 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 22:10 87-68-306/09/21 16:540.019 1
2-Hexanone ND mg/kg 06/10/21 22:10 591-78-606/09/21 16:540.093 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 22:10 98-82-806/09/21 16:540.0093 1
p-Isopropyltoluene ND mg/kg 06/10/21 22:10 99-87-606/09/21 16:540.0093 1
Methylene Chloride ND mg/kg 06/10/21 22:10 75-09-206/09/21 16:540.037 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 22:10 108-10-106/09/21 16:540.093 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 22:10 1634-04-406/09/21 16:540.0093 1
Naphthalene ND mg/kg 06/10/21 22:10 91-20-306/09/21 16:540.0093 1
n-Propylbenzene ND mg/kg 06/10/21 22:10 103-65-106/09/21 16:540.0093 1
Styrene ND mg/kg 06/10/21 22:10 100-42-506/09/21 16:540.0093 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 22:10 630-20-606/09/21 16:540.0093 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 22:10 79-34-506/09/21 16:540.0093 1
Tetrachloroethene ND mg/kg 06/10/21 22:10 127-18-406/09/21 16:540.0093 1
Toluene ND mg/kg 06/10/21 22:10 108-88-306/09/21 16:540.0093 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 22:10 87-61-606/09/21 16:540.0093 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 22:10 120-82-106/09/21 16:540.0093 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 22:10 71-55-606/09/21 16:540.0093 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 22:10 79-00-506/09/21 16:540.0093 1
Trichloroethene ND mg/kg 06/10/21 22:10 79-01-606/09/21 16:540.0093 1
Trichlorofluoromethane ND mg/kg 06/10/21 22:10 75-69-406/09/21 16:540.0093 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 22:10 96-18-406/09/21 16:540.0093 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 22:10 95-63-606/09/21 16:540.0093 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 22:10 108-67-806/09/21 16:540.0093 1
Vinyl acetate ND mg/kg 06/10/21 22:10 108-05-406/09/21 16:540.093 1
Vinyl chloride ND mg/kg 06/10/21 22:10 75-01-406/09/21 16:540.019 1
Xylene (Total)ND mg/kg 06/10/21 22:10 1330-20-706/09/21 16:540.019 1
m&p-Xylene ND mg/kg 06/10/21 22:10 179601-23-106/09/21 16:540.019 1
o-Xylene ND mg/kg 06/10/21 22:10 95-47-606/09/21 16:540.0093 1
Surrogates
Toluene-d8 (S)102 %06/10/21 22:10 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)97 %06/10/21 22:10 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)108 %06/10/21 22:10 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.3 %06/09/21 16:09 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-3 Lab ID:92543280005 Collected:06/08/21 11:30 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)41.2 mg/kg 06/14/21 18:41 N206/11/21 17:1013.8 1
Aliphatic (C19-C36)14.1 mg/kg 06/14/21 18:41 N206/11/21 17:1013.8 1
Aromatic (C11-C22)ND mg/kg 06/14/21 18:41 N206/11/21 17:1013.8 1
Surrogates
1-Chlorooctadecane (S)74 %06/14/21 18:41 3386-33-206/11/21 17:1040-140 1
o-Terphenyl (S)61 %06/14/21 18:41 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)93 %06/14/21 18:41 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)93 %06/14/21 18:41 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 06/12/21 06:24 N206/11/21 15:004.8 1
Aliphatic (C09-C12)ND mg/kg 06/12/21 06:24 N206/11/21 15:004.8 1
Aliphatic(C09-C12) Adjusted ND mg/kg 06/12/21 06:24 N206/11/21 15:004.8 1
Aromatic (C09-C10)ND mg/kg 06/12/21 06:24 N206/11/21 15:004.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %06/12/21 06:24 460-00-406/11/21 15:0070-130 1
4-Bromofluorobenzene (PID) (S)103 %06/12/21 06:24 460-00-406/11/21 15:0070-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 15:05 83-32-906/10/21 13:030.46 1
Acenaphthylene ND mg/kg 06/11/21 15:05 208-96-806/10/21 13:030.46 1
Aniline ND mg/kg 06/11/21 15:05 62-53-306/10/21 13:030.46 1
Anthracene ND mg/kg 06/11/21 15:05 120-12-706/10/21 13:030.46 1
Benzo(a)anthracene ND mg/kg 06/11/21 15:05 56-55-306/10/21 13:030.46 1
Benzo(a)pyrene ND mg/kg 06/11/21 15:05 50-32-806/10/21 13:030.46 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 15:05 205-99-206/10/21 13:030.46 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 15:05 191-24-206/10/21 13:030.46 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 15:05 207-08-906/10/21 13:030.46 1
Benzoic Acid ND mg/kg 06/11/21 15:05 65-85-006/10/21 13:032.3 1
Benzyl alcohol ND mg/kg 06/11/21 15:05 100-51-606/10/21 13:030.92 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 15:05 101-55-306/10/21 13:030.46 1
Butylbenzylphthalate ND mg/kg 06/11/21 15:05 85-68-706/10/21 13:030.46 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 15:05 59-50-706/10/21 13:030.92 1
4-Chloroaniline ND mg/kg 06/11/21 15:05 106-47-806/10/21 13:030.92 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 15:05 111-91-106/10/21 13:030.46 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 15:05 111-44-406/10/21 13:030.46 1
2-Chloronaphthalene ND mg/kg 06/11/21 15:05 91-58-706/10/21 13:030.46 1
2-Chlorophenol ND mg/kg 06/11/21 15:05 95-57-806/10/21 13:030.46 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 15:05 7005-72-306/10/21 13:030.46 1
Chrysene ND mg/kg 06/11/21 15:05 218-01-906/10/21 13:030.46 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 15:05 53-70-306/10/21 13:030.46 1
Dibenzofuran ND mg/kg 06/11/21 15:05 132-64-906/10/21 13:030.46 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 15:05 95-50-106/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-3 Lab ID:92543280005 Collected:06/08/21 11:30 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 15:05 541-73-106/10/21 13:030.46 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 15:05 106-46-706/10/21 13:030.46 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 15:05 91-94-1 IL06/10/21 13:030.92 1
2,4-Dichlorophenol ND mg/kg 06/11/21 15:05 120-83-206/10/21 13:030.46 1
Diethylphthalate ND mg/kg 06/11/21 15:05 84-66-206/10/21 13:030.46 1
2,4-Dimethylphenol ND mg/kg 06/11/21 15:05 105-67-906/10/21 13:030.46 1
Dimethylphthalate ND mg/kg 06/11/21 15:05 131-11-306/10/21 13:030.46 1
Di-n-butylphthalate ND mg/kg 06/11/21 15:05 84-74-206/10/21 13:030.46 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 15:05 534-52-1 v106/10/21 13:030.92 1
2,4-Dinitrophenol ND mg/kg 06/11/21 15:05 51-28-5 v106/10/21 13:032.3 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 15:05 121-14-206/10/21 13:030.46 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 15:05 606-20-206/10/21 13:030.46 1
Di-n-octylphthalate ND mg/kg 06/11/21 15:05 117-84-006/10/21 13:030.46 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 15:05 117-81-706/10/21 13:030.46 1
Fluoranthene ND mg/kg 06/11/21 15:05 206-44-006/10/21 13:030.46 1
Fluorene ND mg/kg 06/11/21 15:05 86-73-706/10/21 13:030.46 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 15:05 87-68-306/10/21 13:030.46 1
Hexachlorobenzene ND mg/kg 06/11/21 15:05 118-74-106/10/21 13:030.46 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 15:05 77-47-406/10/21 13:030.46 1
Hexachloroethane ND mg/kg 06/11/21 15:05 67-72-106/10/21 13:030.46 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 15:05 193-39-506/10/21 13:030.46 1
Isophorone ND mg/kg 06/11/21 15:05 78-59-106/10/21 13:030.46 1
1-Methylnaphthalene ND mg/kg 06/11/21 15:05 90-12-006/10/21 13:030.46 1
2-Methylnaphthalene ND mg/kg 06/11/21 15:05 91-57-606/10/21 13:030.46 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 15:05 95-48-706/10/21 13:030.46 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 15:05 15831-10-406/10/21 13:030.46 1
Naphthalene ND mg/kg 06/11/21 15:05 91-20-306/10/21 13:030.46 1
2-Nitroaniline ND mg/kg 06/11/21 15:05 88-74-406/10/21 13:032.3 1
3-Nitroaniline ND mg/kg 06/11/21 15:05 99-09-2 IL06/10/21 13:032.3 1
4-Nitroaniline ND mg/kg 06/11/21 15:05 100-01-606/10/21 13:030.92 1
Nitrobenzene ND mg/kg 06/11/21 15:05 98-95-306/10/21 13:030.46 1
2-Nitrophenol ND mg/kg 06/11/21 15:05 88-75-506/10/21 13:030.46 1
4-Nitrophenol ND mg/kg 06/11/21 15:05 100-02-706/10/21 13:032.3 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 15:05 62-75-906/10/21 13:030.46 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 15:05 621-64-706/10/21 13:030.46 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 15:05 86-30-606/10/21 13:030.46 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 15:05 108-60-106/10/21 13:030.46 1
Pentachlorophenol ND mg/kg 06/11/21 15:05 87-86-506/10/21 13:030.92 1
Phenanthrene ND mg/kg 06/11/21 15:05 85-01-806/10/21 13:030.46 1
Phenol ND mg/kg 06/11/21 15:05 108-95-206/10/21 13:030.46 1
Pyrene ND mg/kg 06/11/21 15:05 129-00-006/10/21 13:030.46 1
Pyridine ND mg/kg 06/11/21 15:05 110-86-106/10/21 13:030.46 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 15:05 120-82-106/10/21 13:030.46 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 15:05 95-95-406/10/21 13:030.46 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 15:05 88-06-206/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-3 Lab ID:92543280005 Collected:06/08/21 11:30 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)78 %06/11/21 15:05 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)80 %06/11/21 15:05 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)80 %06/11/21 15:05 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)70 %06/11/21 15:05 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)64 %06/11/21 15:05 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)84 %06/11/21 15:05 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 22:27 67-64-106/09/21 16:540.16 1
Benzene ND mg/kg 06/10/21 22:27 71-43-206/09/21 16:540.0081 1
Bromobenzene ND mg/kg 06/10/21 22:27 108-86-106/09/21 16:540.0081 1
Bromochloromethane ND mg/kg 06/10/21 22:27 74-97-506/09/21 16:540.0081 1
Bromodichloromethane ND mg/kg 06/10/21 22:27 75-27-406/09/21 16:540.0081 1
Bromoform ND mg/kg 06/10/21 22:27 75-25-206/09/21 16:540.0081 1
Bromomethane ND mg/kg 06/10/21 22:27 74-83-9 IK06/09/21 16:540.016 1
2-Butanone (MEK)ND mg/kg 06/10/21 22:27 78-93-306/09/21 16:540.16 1
n-Butylbenzene ND mg/kg 06/10/21 22:27 104-51-806/09/21 16:540.0081 1
sec-Butylbenzene ND mg/kg 06/10/21 22:27 135-98-806/09/21 16:540.0081 1
tert-Butylbenzene ND mg/kg 06/10/21 22:27 98-06-606/09/21 16:540.0081 1
Carbon tetrachloride ND mg/kg 06/10/21 22:27 56-23-506/09/21 16:540.0081 1
Chlorobenzene ND mg/kg 06/10/21 22:27 108-90-706/09/21 16:540.0081 1
Chloroethane ND mg/kg 06/10/21 22:27 75-00-306/09/21 16:540.016 1
Chloroform ND mg/kg 06/10/21 22:27 67-66-306/09/21 16:540.0081 1
Chloromethane ND mg/kg 06/10/21 22:27 74-87-306/09/21 16:540.016 1
2-Chlorotoluene ND mg/kg 06/10/21 22:27 95-49-806/09/21 16:540.0081 1
4-Chlorotoluene ND mg/kg 06/10/21 22:27 106-43-406/09/21 16:540.0081 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 22:27 96-12-806/09/21 16:540.0081 1
Dibromochloromethane ND mg/kg 06/10/21 22:27 124-48-106/09/21 16:540.0081 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 22:27 106-93-406/09/21 16:540.0081 1
Dibromomethane ND mg/kg 06/10/21 22:27 74-95-306/09/21 16:540.0081 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 22:27 95-50-106/09/21 16:540.0081 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 22:27 541-73-106/09/21 16:540.0081 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 22:27 106-46-706/09/21 16:540.0081 1
Dichlorodifluoromethane ND mg/kg 06/10/21 22:27 75-71-806/09/21 16:540.016 1
1,1-Dichloroethane ND mg/kg 06/10/21 22:27 75-34-306/09/21 16:540.0081 1
1,2-Dichloroethane ND mg/kg 06/10/21 22:27 107-06-206/09/21 16:540.0081 1
1,1-Dichloroethene ND mg/kg 06/10/21 22:27 75-35-406/09/21 16:540.0081 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 22:27 156-59-206/09/21 16:540.0081 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 22:27 156-60-506/09/21 16:540.0081 1
1,2-Dichloropropane ND mg/kg 06/10/21 22:27 78-87-506/09/21 16:540.0081 1
1,3-Dichloropropane ND mg/kg 06/10/21 22:27 142-28-906/09/21 16:540.0081 1
2,2-Dichloropropane ND mg/kg 06/10/21 22:27 594-20-706/09/21 16:540.0081 1
1,1-Dichloropropene ND mg/kg 06/10/21 22:27 563-58-606/09/21 16:540.0081 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-3 Lab ID:92543280005 Collected:06/08/21 11:30 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 22:27 10061-01-506/09/21 16:540.0081 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 22:27 10061-02-606/09/21 16:540.0081 1
Diisopropyl ether ND mg/kg 06/10/21 22:27 108-20-306/09/21 16:540.0081 1
Ethylbenzene ND mg/kg 06/10/21 22:27 100-41-406/09/21 16:540.0081 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 22:27 87-68-306/09/21 16:540.016 1
2-Hexanone ND mg/kg 06/10/21 22:27 591-78-606/09/21 16:540.081 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 22:27 98-82-806/09/21 16:540.0081 1
p-Isopropyltoluene ND mg/kg 06/10/21 22:27 99-87-606/09/21 16:540.0081 1
Methylene Chloride ND mg/kg 06/10/21 22:27 75-09-206/09/21 16:540.032 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 22:27 108-10-106/09/21 16:540.081 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 22:27 1634-04-406/09/21 16:540.0081 1
Naphthalene ND mg/kg 06/10/21 22:27 91-20-306/09/21 16:540.0081 1
n-Propylbenzene ND mg/kg 06/10/21 22:27 103-65-106/09/21 16:540.0081 1
Styrene ND mg/kg 06/10/21 22:27 100-42-506/09/21 16:540.0081 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 22:27 630-20-606/09/21 16:540.0081 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 22:27 79-34-506/09/21 16:540.0081 1
Tetrachloroethene ND mg/kg 06/10/21 22:27 127-18-406/09/21 16:540.0081 1
Toluene ND mg/kg 06/10/21 22:27 108-88-306/09/21 16:540.0081 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 22:27 87-61-606/09/21 16:540.0081 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 22:27 120-82-106/09/21 16:540.0081 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 22:27 71-55-606/09/21 16:540.0081 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 22:27 79-00-506/09/21 16:540.0081 1
Trichloroethene ND mg/kg 06/10/21 22:27 79-01-606/09/21 16:540.0081 1
Trichlorofluoromethane ND mg/kg 06/10/21 22:27 75-69-406/09/21 16:540.0081 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 22:27 96-18-406/09/21 16:540.0081 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 22:27 95-63-606/09/21 16:540.0081 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 22:27 108-67-806/09/21 16:540.0081 1
Vinyl acetate ND mg/kg 06/10/21 22:27 108-05-406/09/21 16:540.081 1
Vinyl chloride ND mg/kg 06/10/21 22:27 75-01-406/09/21 16:540.016 1
Xylene (Total)ND mg/kg 06/10/21 22:27 1330-20-706/09/21 16:540.016 1
m&p-Xylene ND mg/kg 06/10/21 22:27 179601-23-106/09/21 16:540.016 1
o-Xylene ND mg/kg 06/10/21 22:27 95-47-606/09/21 16:540.0081 1
Surrogates
Toluene-d8 (S)102 %06/10/21 22:27 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)97 %06/10/21 22:27 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)104 %06/10/21 22:27 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.1 %06/09/21 17:38 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-4 Lab ID:92543280006 Collected:06/08/21 13:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 06/14/21 19:08 N206/11/21 17:1014.3 1
Aliphatic (C19-C36)ND mg/kg 06/14/21 19:08 N206/11/21 17:1014.3 1
Aromatic (C11-C22)ND mg/kg 06/14/21 19:08 N206/11/21 17:1014.3 1
Surrogates
1-Chlorooctadecane (S)50 %06/14/21 19:08 3386-33-206/11/21 17:1040-140 1
o-Terphenyl (S)46 %06/14/21 19:08 84-15-106/11/21 17:1040-140 1
2-Fluorobiphenyl (S)81 %06/14/21 19:08 321-60-806/11/21 17:1040-140 1
2-Bromonaphthalene (S)83 %06/14/21 19:08 580-13-206/11/21 17:1040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 06/12/21 06:53 N206/11/21 15:004.3 1
Aliphatic (C09-C12)177 mg/kg 06/12/21 06:53 N206/11/21 15:004.3 1
Aliphatic(C09-C12) Adjusted 163 mg/kg 06/12/21 06:53 N206/11/21 15:004.3 1
Aromatic (C09-C10)14.9 mg/kg 06/12/21 06:53 N206/11/21 15:004.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)216 %06/12/21 06:53 460-00-4 S506/11/21 15:0070-130 1
4-Bromofluorobenzene (PID) (S)114 %06/12/21 06:53 460-00-406/11/21 15:0070-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 06/11/21 15:32 83-32-906/10/21 13:030.46 1
Acenaphthylene ND mg/kg 06/11/21 15:32 208-96-806/10/21 13:030.46 1
Aniline ND mg/kg 06/11/21 15:32 62-53-306/10/21 13:030.46 1
Anthracene ND mg/kg 06/11/21 15:32 120-12-706/10/21 13:030.46 1
Benzo(a)anthracene ND mg/kg 06/11/21 15:32 56-55-306/10/21 13:030.46 1
Benzo(a)pyrene ND mg/kg 06/11/21 15:32 50-32-806/10/21 13:030.46 1
Benzo(b)fluoranthene ND mg/kg 06/11/21 15:32 205-99-206/10/21 13:030.46 1
Benzo(g,h,i)perylene ND mg/kg 06/11/21 15:32 191-24-206/10/21 13:030.46 1
Benzo(k)fluoranthene ND mg/kg 06/11/21 15:32 207-08-906/10/21 13:030.46 1
Benzoic Acid ND mg/kg 06/11/21 15:32 65-85-006/10/21 13:032.3 1
Benzyl alcohol ND mg/kg 06/11/21 15:32 100-51-606/10/21 13:030.93 1
4-Bromophenylphenyl ether ND mg/kg 06/11/21 15:32 101-55-306/10/21 13:030.46 1
Butylbenzylphthalate ND mg/kg 06/11/21 15:32 85-68-706/10/21 13:030.46 1
4-Chloro-3-methylphenol ND mg/kg 06/11/21 15:32 59-50-706/10/21 13:030.93 1
4-Chloroaniline ND mg/kg 06/11/21 15:32 106-47-806/10/21 13:030.93 1
bis(2-Chloroethoxy)methane ND mg/kg 06/11/21 15:32 111-91-106/10/21 13:030.46 1
bis(2-Chloroethyl) ether ND mg/kg 06/11/21 15:32 111-44-406/10/21 13:030.46 1
2-Chloronaphthalene ND mg/kg 06/11/21 15:32 91-58-706/10/21 13:030.46 1
2-Chlorophenol ND mg/kg 06/11/21 15:32 95-57-806/10/21 13:030.46 1
4-Chlorophenylphenyl ether ND mg/kg 06/11/21 15:32 7005-72-306/10/21 13:030.46 1
Chrysene ND mg/kg 06/11/21 15:32 218-01-906/10/21 13:030.46 1
Dibenz(a,h)anthracene ND mg/kg 06/11/21 15:32 53-70-306/10/21 13:030.46 1
Dibenzofuran ND mg/kg 06/11/21 15:32 132-64-906/10/21 13:030.46 1
1,2-Dichlorobenzene ND mg/kg 06/11/21 15:32 95-50-106/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-4 Lab ID:92543280006 Collected:06/08/21 13:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 06/11/21 15:32 541-73-106/10/21 13:030.46 1
1,4-Dichlorobenzene ND mg/kg 06/11/21 15:32 106-46-706/10/21 13:030.46 1
3,3'-Dichlorobenzidine ND mg/kg 06/11/21 15:32 91-94-1 IL06/10/21 13:030.93 1
2,4-Dichlorophenol ND mg/kg 06/11/21 15:32 120-83-206/10/21 13:030.46 1
Diethylphthalate ND mg/kg 06/11/21 15:32 84-66-206/10/21 13:030.46 1
2,4-Dimethylphenol ND mg/kg 06/11/21 15:32 105-67-906/10/21 13:030.46 1
Dimethylphthalate ND mg/kg 06/11/21 15:32 131-11-306/10/21 13:030.46 1
Di-n-butylphthalate ND mg/kg 06/11/21 15:32 84-74-206/10/21 13:030.46 1
4,6-Dinitro-2-methylphenol ND mg/kg 06/11/21 15:32 534-52-1 v106/10/21 13:030.93 1
2,4-Dinitrophenol ND mg/kg 06/11/21 15:32 51-28-5 v106/10/21 13:032.3 1
2,4-Dinitrotoluene ND mg/kg 06/11/21 15:32 121-14-206/10/21 13:030.46 1
2,6-Dinitrotoluene ND mg/kg 06/11/21 15:32 606-20-206/10/21 13:030.46 1
Di-n-octylphthalate ND mg/kg 06/11/21 15:32 117-84-006/10/21 13:030.46 1
bis(2-Ethylhexyl)phthalate ND mg/kg 06/11/21 15:32 117-81-706/10/21 13:030.46 1
Fluoranthene ND mg/kg 06/11/21 15:32 206-44-006/10/21 13:030.46 1
Fluorene ND mg/kg 06/11/21 15:32 86-73-706/10/21 13:030.46 1
Hexachloro-1,3-butadiene ND mg/kg 06/11/21 15:32 87-68-306/10/21 13:030.46 1
Hexachlorobenzene ND mg/kg 06/11/21 15:32 118-74-106/10/21 13:030.46 1
Hexachlorocyclopentadiene ND mg/kg 06/11/21 15:32 77-47-406/10/21 13:030.46 1
Hexachloroethane ND mg/kg 06/11/21 15:32 67-72-106/10/21 13:030.46 1
Indeno(1,2,3-cd)pyrene ND mg/kg 06/11/21 15:32 193-39-506/10/21 13:030.46 1
Isophorone ND mg/kg 06/11/21 15:32 78-59-106/10/21 13:030.46 1
1-Methylnaphthalene ND mg/kg 06/11/21 15:32 90-12-006/10/21 13:030.46 1
2-Methylnaphthalene ND mg/kg 06/11/21 15:32 91-57-606/10/21 13:030.46 1
2-Methylphenol(o-Cresol)ND mg/kg 06/11/21 15:32 95-48-706/10/21 13:030.46 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 06/11/21 15:32 15831-10-406/10/21 13:030.46 1
Naphthalene ND mg/kg 06/11/21 15:32 91-20-306/10/21 13:030.46 1
2-Nitroaniline ND mg/kg 06/11/21 15:32 88-74-406/10/21 13:032.3 1
3-Nitroaniline ND mg/kg 06/11/21 15:32 99-09-2 IL06/10/21 13:032.3 1
4-Nitroaniline ND mg/kg 06/11/21 15:32 100-01-606/10/21 13:030.93 1
Nitrobenzene ND mg/kg 06/11/21 15:32 98-95-306/10/21 13:030.46 1
2-Nitrophenol ND mg/kg 06/11/21 15:32 88-75-506/10/21 13:030.46 1
4-Nitrophenol ND mg/kg 06/11/21 15:32 100-02-706/10/21 13:032.3 1
N-Nitrosodimethylamine ND mg/kg 06/11/21 15:32 62-75-906/10/21 13:030.46 1
N-Nitroso-di-n-propylamine ND mg/kg 06/11/21 15:32 621-64-706/10/21 13:030.46 1
N-Nitrosodiphenylamine ND mg/kg 06/11/21 15:32 86-30-606/10/21 13:030.46 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 06/11/21 15:32 108-60-106/10/21 13:030.46 1
Pentachlorophenol ND mg/kg 06/11/21 15:32 87-86-506/10/21 13:030.93 1
Phenanthrene ND mg/kg 06/11/21 15:32 85-01-806/10/21 13:030.46 1
Phenol ND mg/kg 06/11/21 15:32 108-95-206/10/21 13:030.46 1
Pyrene ND mg/kg 06/11/21 15:32 129-00-006/10/21 13:030.46 1
Pyridine ND mg/kg 06/11/21 15:32 110-86-106/10/21 13:030.46 1
1,2,4-Trichlorobenzene ND mg/kg 06/11/21 15:32 120-82-106/10/21 13:030.46 1
2,4,5-Trichlorophenol ND mg/kg 06/11/21 15:32 95-95-406/10/21 13:030.46 1
2,4,6-Trichlorophenol ND mg/kg 06/11/21 15:32 88-06-206/10/21 13:030.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-4 Lab ID:92543280006 Collected:06/08/21 13:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)75 %06/11/21 15:32 4165-60-006/10/21 13:0321-130 1
2-Fluorobiphenyl (S)72 %06/11/21 15:32 321-60-806/10/21 13:0319-130 1
Terphenyl-d14 (S)73 %06/11/21 15:32 1718-51-006/10/21 13:0315-130 1
Phenol-d6 (S)81 %06/11/21 15:32 13127-88-306/10/21 13:0318-130 1
2-Fluorophenol (S)81 %06/11/21 15:32 367-12-406/10/21 13:0318-130 1
2,4,6-Tribromophenol (S)97 %06/11/21 15:32 118-79-606/10/21 13:0318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 06/10/21 23:20 67-64-106/09/21 16:540.17 1
Benzene ND mg/kg 06/10/21 23:20 71-43-206/09/21 16:540.0087 1
Bromobenzene ND mg/kg 06/10/21 23:20 108-86-106/09/21 16:540.0087 1
Bromochloromethane ND mg/kg 06/10/21 23:20 74-97-506/09/21 16:540.0087 1
Bromodichloromethane ND mg/kg 06/10/21 23:20 75-27-406/09/21 16:540.0087 1
Bromoform ND mg/kg 06/10/21 23:20 75-25-206/09/21 16:540.0087 1
Bromomethane ND mg/kg 06/10/21 23:20 74-83-9 IK06/09/21 16:540.017 1
2-Butanone (MEK)ND mg/kg 06/10/21 23:20 78-93-306/09/21 16:540.17 1
n-Butylbenzene ND mg/kg 06/10/21 23:20 104-51-806/09/21 16:540.0087 1
sec-Butylbenzene 0.10 mg/kg 06/10/21 23:20 135-98-806/09/21 16:540.0087 1
tert-Butylbenzene ND mg/kg 06/10/21 23:20 98-06-606/09/21 16:540.0087 1
Carbon tetrachloride ND mg/kg 06/10/21 23:20 56-23-506/09/21 16:540.0087 1
Chlorobenzene ND mg/kg 06/10/21 23:20 108-90-706/09/21 16:540.0087 1
Chloroethane ND mg/kg 06/10/21 23:20 75-00-306/09/21 16:540.017 1
Chloroform ND mg/kg 06/10/21 23:20 67-66-306/09/21 16:540.0087 1
Chloromethane ND mg/kg 06/10/21 23:20 74-87-306/09/21 16:540.017 1
2-Chlorotoluene ND mg/kg 06/10/21 23:20 95-49-806/09/21 16:540.0087 1
4-Chlorotoluene ND mg/kg 06/10/21 23:20 106-43-406/09/21 16:540.0087 1
1,2-Dibromo-3-chloropropane ND mg/kg 06/10/21 23:20 96-12-806/09/21 16:540.0087 1
Dibromochloromethane ND mg/kg 06/10/21 23:20 124-48-106/09/21 16:540.0087 1
1,2-Dibromoethane (EDB)ND mg/kg 06/10/21 23:20 106-93-406/09/21 16:540.0087 1
Dibromomethane ND mg/kg 06/10/21 23:20 74-95-306/09/21 16:540.0087 1
1,2-Dichlorobenzene ND mg/kg 06/10/21 23:20 95-50-106/09/21 16:540.0087 1
1,3-Dichlorobenzene ND mg/kg 06/10/21 23:20 541-73-106/09/21 16:540.0087 1
1,4-Dichlorobenzene ND mg/kg 06/10/21 23:20 106-46-706/09/21 16:540.0087 1
Dichlorodifluoromethane ND mg/kg 06/10/21 23:20 75-71-806/09/21 16:540.017 1
1,1-Dichloroethane ND mg/kg 06/10/21 23:20 75-34-306/09/21 16:540.0087 1
1,2-Dichloroethane ND mg/kg 06/10/21 23:20 107-06-206/09/21 16:540.0087 1
1,1-Dichloroethene ND mg/kg 06/10/21 23:20 75-35-406/09/21 16:540.0087 1
cis-1,2-Dichloroethene ND mg/kg 06/10/21 23:20 156-59-206/09/21 16:540.0087 1
trans-1,2-Dichloroethene ND mg/kg 06/10/21 23:20 156-60-506/09/21 16:540.0087 1
1,2-Dichloropropane ND mg/kg 06/10/21 23:20 78-87-506/09/21 16:540.0087 1
1,3-Dichloropropane ND mg/kg 06/10/21 23:20 142-28-906/09/21 16:540.0087 1
2,2-Dichloropropane ND mg/kg 06/10/21 23:20 594-20-706/09/21 16:540.0087 1
1,1-Dichloropropene ND mg/kg 06/10/21 23:20 563-58-606/09/21 16:540.0087 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Sample:SW-4 Lab ID:92543280006 Collected:06/08/21 13:00 Received:06/09/21 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 06/10/21 23:20 10061-01-506/09/21 16:540.0087 1
trans-1,3-Dichloropropene ND mg/kg 06/10/21 23:20 10061-02-606/09/21 16:540.0087 1
Diisopropyl ether ND mg/kg 06/10/21 23:20 108-20-306/09/21 16:540.0087 1
Ethylbenzene ND mg/kg 06/10/21 23:20 100-41-406/09/21 16:540.0087 1
Hexachloro-1,3-butadiene ND mg/kg 06/10/21 23:20 87-68-306/09/21 16:540.017 1
2-Hexanone ND mg/kg 06/10/21 23:20 591-78-606/09/21 16:540.087 1
Isopropylbenzene (Cumene)ND mg/kg 06/10/21 23:20 98-82-806/09/21 16:540.0087 1
p-Isopropyltoluene ND mg/kg 06/10/21 23:20 99-87-606/09/21 16:540.0087 1
Methylene Chloride ND mg/kg 06/10/21 23:20 75-09-206/09/21 16:540.035 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 06/10/21 23:20 108-10-106/09/21 16:540.087 1
Methyl-tert-butyl ether ND mg/kg 06/10/21 23:20 1634-04-406/09/21 16:540.0087 1
Naphthalene ND mg/kg 06/10/21 23:20 91-20-306/09/21 16:540.0087 1
n-Propylbenzene ND mg/kg 06/10/21 23:20 103-65-106/09/21 16:540.0087 1
Styrene ND mg/kg 06/10/21 23:20 100-42-506/09/21 16:540.0087 1
1,1,1,2-Tetrachloroethane ND mg/kg 06/10/21 23:20 630-20-606/09/21 16:540.0087 1
1,1,2,2-Tetrachloroethane ND mg/kg 06/10/21 23:20 79-34-506/09/21 16:540.0087 1
Tetrachloroethene ND mg/kg 06/10/21 23:20 127-18-406/09/21 16:540.0087 1
Toluene ND mg/kg 06/10/21 23:20 108-88-306/09/21 16:540.0087 1
1,2,3-Trichlorobenzene ND mg/kg 06/10/21 23:20 87-61-606/09/21 16:540.0087 1
1,2,4-Trichlorobenzene ND mg/kg 06/10/21 23:20 120-82-106/09/21 16:540.0087 1
1,1,1-Trichloroethane ND mg/kg 06/10/21 23:20 71-55-606/09/21 16:540.0087 1
1,1,2-Trichloroethane ND mg/kg 06/10/21 23:20 79-00-506/09/21 16:540.0087 1
Trichloroethene ND mg/kg 06/10/21 23:20 79-01-606/09/21 16:540.0087 1
Trichlorofluoromethane ND mg/kg 06/10/21 23:20 75-69-406/09/21 16:540.0087 1
1,2,3-Trichloropropane ND mg/kg 06/10/21 23:20 96-18-406/09/21 16:540.0087 1
1,2,4-Trimethylbenzene ND mg/kg 06/10/21 23:20 95-63-606/09/21 16:540.0087 1
1,3,5-Trimethylbenzene ND mg/kg 06/10/21 23:20 108-67-806/09/21 16:540.0087 1
Vinyl acetate ND mg/kg 06/10/21 23:20 108-05-406/09/21 16:540.087 1
Vinyl chloride ND mg/kg 06/10/21 23:20 75-01-406/09/21 16:540.017 1
Xylene (Total)ND mg/kg 06/10/21 23:20 1330-20-706/09/21 16:540.017 1
m&p-Xylene ND mg/kg 06/10/21 23:20 179601-23-106/09/21 16:540.017 1
o-Xylene ND mg/kg 06/10/21 23:20 95-47-606/09/21 16:540.0087 1
Surrogates
Toluene-d8 (S)100 %06/10/21 23:20 2037-26-506/09/21 16:5470-130 1
4-Bromofluorobenzene (S)104 %06/10/21 23:20 460-00-406/09/21 16:5469-134 1
1,2-Dichloroethane-d4 (S)103 %06/10/21 23:20 17060-07-006/09/21 16:5470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.9 %06/09/21 17:38 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626592
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280001, 92543280003, 92543280005, 92543280006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3294598
Associated Lab Samples:92543280001, 92543280003, 92543280005, 92543280006
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N206/11/21 17:34
Aliphatic (C09-C12)mg/kg ND 2.5 N206/11/21 17:34
Aromatic (C09-C10)mg/kg ND 2.5 N206/11/21 17:34
4-Bromofluorobenzene (FID) (S)%105 70-130 06/11/21 17:34
4-Bromofluorobenzene (PID) (S)%103 70-130 06/11/21 17:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3294599LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3294600
Aliphatic (C05-C08)mg/kg 12.4 N2158270-1307811.8 5 25
Aliphatic (C09-C12)mg/kg 17.4 N21511670-13011417.1 2 25
Aromatic (C09-C10)mg/kg 5.6 N2511270-1301105.5 2 25
4-Bromofluorobenzene (FID) (S)%107 70-130107
4-Bromofluorobenzene (PID) (S)%103 70-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626950
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280002, 92543280004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3296369
Associated Lab Samples:92543280002, 92543280004
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N206/14/21 14:56
Aliphatic (C09-C12)mg/kg ND 2.5 N206/14/21 14:56
Aromatic (C09-C10)mg/kg ND 2.5 N206/14/21 14:56
4-Bromofluorobenzene (FID) (S)%105 70-130 06/14/21 14:56
4-Bromofluorobenzene (PID) (S)%103 70-130 06/14/21 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3296370LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3296371
Aliphatic (C05-C08)mg/kg 13.2 N215.2 87 70-1308412.7 4 25
Aliphatic (C09-C12)mg/kg 17.9 N215.2 118 70-13011417.2 4 25
Aromatic (C09-C10)mg/kg 5.8 N25.1 114 70-1301105.6 4 25
4-Bromofluorobenzene (FID) (S)%107 70-130101
4-Bromofluorobenzene (PID) (S)%102 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626031
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3291946
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 06/10/21 20:42
1,1,1-Trichloroethane mg/kg ND 0.0050 06/10/21 20:42
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 06/10/21 20:42
1,1,2-Trichloroethane mg/kg ND 0.0050 06/10/21 20:42
1,1-Dichloroethane mg/kg ND 0.0050 06/10/21 20:42
1,1-Dichloroethene mg/kg ND 0.0050 06/10/21 20:42
1,1-Dichloropropene mg/kg ND 0.0050 06/10/21 20:42
1,2,3-Trichlorobenzene mg/kg ND 0.0050 06/10/21 20:42
1,2,3-Trichloropropane mg/kg ND 0.0050 06/10/21 20:42
1,2,4-Trichlorobenzene mg/kg ND 0.0050 06/10/21 20:42
1,2,4-Trimethylbenzene mg/kg ND 0.0050 06/10/21 20:42
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 06/10/21 20:42
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 06/10/21 20:42
1,2-Dichlorobenzene mg/kg ND 0.0050 06/10/21 20:42
1,2-Dichloroethane mg/kg ND 0.0050 06/10/21 20:42
1,2-Dichloropropane mg/kg ND 0.0050 06/10/21 20:42
1,3,5-Trimethylbenzene mg/kg ND 0.0050 06/10/21 20:42
1,3-Dichlorobenzene mg/kg ND 0.0050 06/10/21 20:42
1,3-Dichloropropane mg/kg ND 0.0050 06/10/21 20:42
1,4-Dichlorobenzene mg/kg ND 0.0050 06/10/21 20:42
2,2-Dichloropropane mg/kg ND 0.0050 06/10/21 20:42
2-Butanone (MEK)mg/kg ND 0.10 06/10/21 20:42
2-Chlorotoluene mg/kg ND 0.0050 06/10/21 20:42
2-Hexanone mg/kg ND 0.050 06/10/21 20:42
4-Chlorotoluene mg/kg ND 0.0050 06/10/21 20:42
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 06/10/21 20:42
Acetone mg/kg ND 0.10 06/10/21 20:42
Benzene mg/kg ND 0.0050 06/10/21 20:42
Bromobenzene mg/kg ND 0.0050 06/10/21 20:42
Bromochloromethane mg/kg ND 0.0050 06/10/21 20:42
Bromodichloromethane mg/kg ND 0.0050 06/10/21 20:42
Bromoform mg/kg ND 0.0050 06/10/21 20:42
Bromomethane mg/kg ND 0.010 IK06/10/21 20:42
Carbon tetrachloride mg/kg ND 0.0050 06/10/21 20:42
Chlorobenzene mg/kg ND 0.0050 06/10/21 20:42
Chloroethane mg/kg ND 0.010 06/10/21 20:42
Chloroform mg/kg ND 0.0050 06/10/21 20:42
Chloromethane mg/kg ND 0.010 06/10/21 20:42
cis-1,2-Dichloroethene mg/kg ND 0.0050 06/10/21 20:42
cis-1,3-Dichloropropene mg/kg ND 0.0050 06/10/21 20:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3291946
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 06/10/21 20:42
Dibromomethane mg/kg ND 0.0050 06/10/21 20:42
Dichlorodifluoromethane mg/kg ND 0.010 06/10/21 20:42
Diisopropyl ether mg/kg ND 0.0050 06/10/21 20:42
Ethylbenzene mg/kg ND 0.0050 06/10/21 20:42
Hexachloro-1,3-butadiene mg/kg ND 0.010 06/10/21 20:42
Isopropylbenzene (Cumene)mg/kg ND 0.0050 06/10/21 20:42
m&p-Xylene mg/kg ND 0.010 06/10/21 20:42
Methyl-tert-butyl ether mg/kg ND 0.0050 06/10/21 20:42
Methylene Chloride mg/kg ND 0.020 06/10/21 20:42
n-Butylbenzene mg/kg ND 0.0050 06/10/21 20:42
n-Propylbenzene mg/kg ND 0.0050 06/10/21 20:42
Naphthalene mg/kg ND 0.0050 06/10/21 20:42
o-Xylene mg/kg ND 0.0050 06/10/21 20:42
p-Isopropyltoluene mg/kg ND 0.0050 06/10/21 20:42
sec-Butylbenzene mg/kg ND 0.0050 06/10/21 20:42
Styrene mg/kg ND 0.0050 06/10/21 20:42
tert-Butylbenzene mg/kg ND 0.0050 06/10/21 20:42
Tetrachloroethene mg/kg ND 0.0050 06/10/21 20:42
Toluene mg/kg ND 0.0050 06/10/21 20:42
trans-1,2-Dichloroethene mg/kg ND 0.0050 06/10/21 20:42
trans-1,3-Dichloropropene mg/kg ND 0.0050 06/10/21 20:42
Trichloroethene mg/kg ND 0.0050 06/10/21 20:42
Trichlorofluoromethane mg/kg ND 0.0050 06/10/21 20:42
Vinyl acetate mg/kg ND 0.050 06/10/21 20:42
Vinyl chloride mg/kg ND 0.010 06/10/21 20:42
Xylene (Total)mg/kg ND 0.010 06/10/21 20:42
1,2-Dichloroethane-d4 (S)%107 70-130 06/10/21 20:42
4-Bromofluorobenzene (S)%97 69-134 06/10/21 20:42
Toluene-d8 (S)%101 70-130 06/10/21 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3291947LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 94 70-130
1,1,1-Trichloroethane mg/kg 1.11.2 87 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 94 70-130
1,1,2-Trichloroethane mg/kg 1.11.2 89 70-130
1,1-Dichloroethane mg/kg 1.21.2 97 70-130
1,1-Dichloroethene mg/kg 1.31.2 102 70-130
1,1-Dichloropropene mg/kg 1.21.2 94 70-130
1,2,3-Trichlorobenzene mg/kg 1.11.2 89 65-130
1,2,3-Trichloropropane mg/kg 1.21.2 97 70-130
1,2,4-Trichlorobenzene mg/kg 1.11.2 90 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3291947LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 98 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.11.2 87 70-130
1,2-Dibromoethane (EDB)mg/kg 1.21.2 99 70-130
1,2-Dichlorobenzene mg/kg 1.21.2 96 70-130
1,2-Dichloroethane mg/kg 1.21.2 99 63-130
1,2-Dichloropropane mg/kg 1.21.2 98 70-130
1,3,5-Trimethylbenzene mg/kg 1.11.2 85 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 97 70-130
1,3-Dichloropropane mg/kg 1.31.2 102 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 95 70-130
2,2-Dichloropropane mg/kg 1.11.2 91 66-130
2-Butanone (MEK)mg/kg 2.42.5 95 70-130
2-Chlorotoluene mg/kg 1.21.2 95 70-130
2-Hexanone mg/kg 2.62.5 105 70-130
4-Chlorotoluene mg/kg 1.11.2 92 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 101 70-130
Acetone mg/kg 2.52.5 99 69-130
Benzene mg/kg 1.21.2 95 70-130
Bromobenzene mg/kg 1.21.2 95 70-130
Bromochloromethane mg/kg 1.31.2 101 70-130
Bromodichloromethane mg/kg 1.01.2 82 69-130
Bromoform mg/kg 1.11.2 90 70-130
Bromomethane mg/kg 1.5 IK1.2 117 52-130
Carbon tetrachloride mg/kg 1.11.2 90 70-130
Chlorobenzene mg/kg 1.31.2 101 70-130
Chloroethane mg/kg 1.21.2 92 65-130
Chloroform mg/kg 1.11.2 89 70-130
Chloromethane mg/kg 1.11.2 88 55-130
cis-1,2-Dichloroethene mg/kg 1.21.2 94 70-130
cis-1,3-Dichloropropene mg/kg 1.21.2 93 70-130
Dibromochloromethane mg/kg 1.21.2 97 70-130
Dibromomethane mg/kg 1.31.2 102 70-130
Dichlorodifluoromethane mg/kg 1.31.2 101 45-156
Diisopropyl ether mg/kg 1.11.2 86 70-130
Ethylbenzene mg/kg 1.21.2 94 70-130
Hexachloro-1,3-butadiene mg/kg 1.21.2 93 66-130
Isopropylbenzene (Cumene)mg/kg 1.21.2 98 70-130
m&p-Xylene mg/kg 2.42.5 95 70-130
Methyl-tert-butyl ether mg/kg 1.11.2 91 70-130
Methylene Chloride mg/kg 1.21.2 99 65-130
n-Butylbenzene mg/kg 1.11.2 90 67-130
n-Propylbenzene mg/kg 1.11.2 90 70-130
Naphthalene mg/kg 1.11.2 85 70-130
o-Xylene mg/kg 1.21.2 95 70-130
p-Isopropyltoluene mg/kg 1.11.2 88 67-130
sec-Butylbenzene mg/kg 1.11.2 90 69-130
Styrene mg/kg 1.21.2 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3291947LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 92 67-130
Tetrachloroethene mg/kg 1.31.2 106 70-130
Toluene mg/kg 1.11.2 90 70-130
trans-1,2-Dichloroethene mg/kg 1.21.2 95 70-130
trans-1,3-Dichloropropene mg/kg 1.11.2 91 68-130
Trichloroethene mg/kg 1.21.2 99 70-130
Trichlorofluoromethane mg/kg 1.21.2 96 70-130
Vinyl acetate mg/kg 2.52.5 101 70-130
Vinyl chloride mg/kg 1.21.2 93 61-130
Xylene (Total)mg/kg 3.63.8 95 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3291949MATRIX SPIKE SAMPLE:
MSSpike
Result
92543280002
1,1,1,2-Tetrachloroethane mg/kg 0.800.98 82 70-131ND
1,1,1-Trichloroethane mg/kg 0.850.98 86 65-133ND
1,1,2,2-Tetrachloroethane mg/kg 0.790.98 81 66-130ND
1,1,2-Trichloroethane mg/kg 0.790.98 80 66-133ND
1,1-Dichloroethane mg/kg 0.930.98 95 65-130ND
1,1-Dichloroethene mg/kg 1.10.98 108 10-158ND
1,1-Dichloropropene mg/kg 0.970.98 99 68-133ND
1,2,3-Trichlorobenzene mg/kg 0.720.98 73 27-138ND
1,2,3-Trichloropropane mg/kg 0.780.98 80 67-130ND
1,2,4-Trichlorobenzene mg/kg 0.780.98 79 51-134ND
1,2,4-Trimethylbenzene mg/kg 0.860.98 88 63-136ND
1,2-Dibromo-3-chloropropane mg/kg 0.580.98 59 32-130ND
1,2-Dibromoethane (EDB)mg/kg 0.890.98 90 70-130ND
1,2-Dichlorobenzene mg/kg 0.860.98 87 69-130ND
1,2-Dichloroethane mg/kg 0.930.98 95 59-130ND
1,2-Dichloropropane mg/kg 0.930.98 95 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.780.98 79 65-137ND
1,3-Dichlorobenzene mg/kg 0.860.98 88 70-130ND
1,3-Dichloropropane mg/kg 0.930.98 95 70-130ND
1,4-Dichlorobenzene mg/kg 0.860.98 87 68-130ND
2,2-Dichloropropane mg/kg 0.770.98 78 32-130ND
2-Butanone (MEK)mg/kg 1.62 80 10-136ND
2-Chlorotoluene mg/kg 0.850.98 87 69-141ND
2-Hexanone mg/kg 1.62 82 10-144ND
4-Chlorotoluene mg/kg 0.840.98 85 70-132ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.62 83 25-143ND
Acetone mg/kg 1.82 91 10-130ND
Benzene mg/kg 0.910.98 92 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3291949MATRIX SPIKE SAMPLE:
MSSpike
Result
92543280002
Bromobenzene mg/kg 0.870.98 88 70-130ND
Bromochloromethane mg/kg 0.960.98 98 69-134ND
Bromodichloromethane mg/kg 0.680.98 69 64-130ND
Bromoform mg/kg 0.640.98 65 62-130ND
Bromomethane mg/kg 0.94 IK0.98 95 20-176ND
Carbon tetrachloride mg/kg 0.800.98 82 65-140ND
Chlorobenzene mg/kg 0.970.98 99 70-130ND
Chloroethane mg/kg 0.240.98 24 10-130ND
Chloroform mg/kg 0.860.98 88 63-130ND
Chloromethane mg/kg 1.10.98 108 58-130ND
cis-1,2-Dichloroethene mg/kg 0.930.98 95 66-130ND
cis-1,3-Dichloropropene mg/kg 0.800.98 81 67-130ND
Dibromochloromethane mg/kg 0.730.98 75 67-130ND
Dibromomethane mg/kg 0.900.98 92 63-131ND
Dichlorodifluoromethane mg/kg 1.10.98 109 44-180ND
Diisopropyl ether mg/kg 0.830.98 85 63-130ND
Ethylbenzene mg/kg 0.900.98 91 66-130ND
Hexachloro-1,3-butadiene mg/kg 0.880.98 90 64-150ND
Isopropylbenzene (Cumene)mg/kg 0.930.98 95 69-135ND
m&p-Xylene mg/kg 1.82 91 60-133ND
Methyl-tert-butyl ether mg/kg 0.860.98 87 65-130ND
Methylene Chloride mg/kg 1.00.98 106 61-130ND
n-Butylbenzene mg/kg 0.820.98 84 65-140ND
n-Propylbenzene mg/kg 0.820.98 83 67-140ND
Naphthalene mg/kg 0.660.98 67 15-145ND
o-Xylene mg/kg 0.870.98 88 66-133ND
p-Isopropyltoluene mg/kg 0.810.98 82 56-147ND
sec-Butylbenzene mg/kg 0.860.98 88 65-139ND
Styrene mg/kg 0.880.98 90 70-132ND
tert-Butylbenzene mg/kg 0.650.98 66 62-135ND
Tetrachloroethene mg/kg 0.950.98 96 70-135ND
Toluene mg/kg 0.860.98 88 67-130ND
trans-1,2-Dichloroethene mg/kg 0.960.98 98 69-130ND
trans-1,3-Dichloropropene mg/kg 0.780.98 79 62-130ND
Trichloroethene mg/kg 0.950.98 96 70-135ND
Trichlorofluoromethane mg/kg 0.330.98 34 10-130ND
Vinyl acetate mg/kg 1.72 87 53-130ND
Vinyl chloride mg/kg 0.970.98 99 61-148ND
Xylene (Total)mg/kg 2.73 90 63-132ND
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92543280001
3291948SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg ND IKND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg ND0.013
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92543280001
3291948SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%105104
4-Bromofluorobenzene (S)%9697
Toluene-d8 (S)%101104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626142
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3292348
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 06/11/21 08:17
1,2-Dichlorobenzene mg/kg ND 0.33 06/11/21 08:17
1,3-Dichlorobenzene mg/kg ND 0.33 06/11/21 08:17
1,4-Dichlorobenzene mg/kg ND 0.33 06/11/21 08:17
1-Methylnaphthalene mg/kg ND 0.33 06/11/21 08:17
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 06/11/21 08:17
2,4,5-Trichlorophenol mg/kg ND 0.33 06/11/21 08:17
2,4,6-Trichlorophenol mg/kg ND 0.33 06/11/21 08:17
2,4-Dichlorophenol mg/kg ND 0.33 06/11/21 08:17
2,4-Dimethylphenol mg/kg ND 0.33 06/11/21 08:17
2,4-Dinitrophenol mg/kg ND 1.7 v106/11/21 08:17
2,4-Dinitrotoluene mg/kg ND 0.33 06/11/21 08:17
2,6-Dinitrotoluene mg/kg ND 0.33 06/11/21 08:17
2-Chloronaphthalene mg/kg ND 0.33 06/11/21 08:17
2-Chlorophenol mg/kg ND 0.33 06/11/21 08:17
2-Methylnaphthalene mg/kg ND 0.33 06/11/21 08:17
2-Methylphenol(o-Cresol)mg/kg ND 0.33 06/11/21 08:17
2-Nitroaniline mg/kg ND 1.7 06/11/21 08:17
2-Nitrophenol mg/kg ND 0.33 06/11/21 08:17
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 06/11/21 08:17
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL06/11/21 08:17
3-Nitroaniline mg/kg ND 1.7 IL06/11/21 08:17
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 v106/11/21 08:17
4-Bromophenylphenyl ether mg/kg ND 0.33 06/11/21 08:17
4-Chloro-3-methylphenol mg/kg ND 0.66 06/11/21 08:17
4-Chloroaniline mg/kg ND 0.66 06/11/21 08:17
4-Chlorophenylphenyl ether mg/kg ND 0.33 06/11/21 08:17
4-Nitroaniline mg/kg ND 0.66 06/11/21 08:17
4-Nitrophenol mg/kg ND 1.7 06/11/21 08:17
Acenaphthene mg/kg ND 0.33 06/11/21 08:17
Acenaphthylene mg/kg ND 0.33 06/11/21 08:17
Aniline mg/kg ND 0.33 06/11/21 08:17
Anthracene mg/kg ND 0.33 06/11/21 08:17
Benzo(a)anthracene mg/kg ND 0.33 06/11/21 08:17
Benzo(a)pyrene mg/kg ND 0.33 06/11/21 08:17
Benzo(b)fluoranthene mg/kg ND 0.33 06/11/21 08:17
Benzo(g,h,i)perylene mg/kg ND 0.33 06/11/21 08:17
Benzo(k)fluoranthene mg/kg ND 0.33 06/11/21 08:17
Benzoic Acid mg/kg ND 1.7 06/11/21 08:17
Benzyl alcohol mg/kg ND 0.66 06/11/21 08:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3292348
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 06/11/21 08:17
bis(2-Chloroethyl) ether mg/kg ND 0.33 06/11/21 08:17
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 06/11/21 08:17
Butylbenzylphthalate mg/kg ND 0.33 06/11/21 08:17
Chrysene mg/kg ND 0.33 06/11/21 08:17
Di-n-butylphthalate mg/kg ND 0.33 06/11/21 08:17
Di-n-octylphthalate mg/kg ND 0.33 06/11/21 08:17
Dibenz(a,h)anthracene mg/kg ND 0.33 06/11/21 08:17
Dibenzofuran mg/kg ND 0.33 06/11/21 08:17
Diethylphthalate mg/kg ND 0.33 06/11/21 08:17
Dimethylphthalate mg/kg ND 0.33 06/11/21 08:17
Fluoranthene mg/kg ND 0.33 06/11/21 08:17
Fluorene mg/kg ND 0.33 06/11/21 08:17
Hexachloro-1,3-butadiene mg/kg ND 0.33 06/11/21 08:17
Hexachlorobenzene mg/kg ND 0.33 06/11/21 08:17
Hexachlorocyclopentadiene mg/kg ND 0.33 06/11/21 08:17
Hexachloroethane mg/kg ND 0.33 06/11/21 08:17
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 06/11/21 08:17
Isophorone mg/kg ND 0.33 06/11/21 08:17
N-Nitroso-di-n-propylamine mg/kg ND 0.33 06/11/21 08:17
N-Nitrosodimethylamine mg/kg ND 0.33 06/11/21 08:17
N-Nitrosodiphenylamine mg/kg ND 0.33 06/11/21 08:17
Naphthalene mg/kg ND 0.33 06/11/21 08:17
Nitrobenzene mg/kg ND 0.33 06/11/21 08:17
Pentachlorophenol mg/kg ND 0.66 06/11/21 08:17
Phenanthrene mg/kg ND 0.33 06/11/21 08:17
Phenol mg/kg ND 0.33 06/11/21 08:17
Pyrene mg/kg ND 0.33 06/11/21 08:17
Pyridine mg/kg ND 0.33 06/11/21 08:17
2,4,6-Tribromophenol (S)%80 18-130 06/11/21 08:17
2-Fluorobiphenyl (S)%72 19-130 06/11/21 08:17
2-Fluorophenol (S)%70 18-130 06/11/21 08:17
Nitrobenzene-d5 (S)%64 21-130 06/11/21 08:17
Phenol-d6 (S)%72 18-130 06/11/21 08:17
Terphenyl-d14 (S)%79 15-130 06/11/21 08:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3292349LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.11.7 65 47-130
1,2-Dichlorobenzene mg/kg 1.11.7 65 49-130
1,3-Dichlorobenzene mg/kg 1.11.7 65 48-130
1,4-Dichlorobenzene mg/kg 1.11.7 67 49-130
1-Methylnaphthalene mg/kg 1.31.7 76 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3292349LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.01.7 62 38-130
2,4,5-Trichlorophenol mg/kg 1.31.7 79 49-130
2,4,6-Trichlorophenol mg/kg 1.31.7 80 50-130
2,4-Dichlorophenol mg/kg 1.21.7 75 51-130
2,4-Dimethylphenol mg/kg 1.21.7 72 53-130
2,4-Dinitrophenol mg/kg 8.3 v18.3 101 39-130
2,4-Dinitrotoluene mg/kg 1.41.7 84 53-130
2,6-Dinitrotoluene mg/kg 1.41.7 85 55-130
2-Chloronaphthalene mg/kg 1.21.7 75 48-130
2-Chlorophenol mg/kg 1.21.7 73 54-130
2-Methylnaphthalene mg/kg 1.21.7 76 57-130
2-Methylphenol(o-Cresol)mg/kg 1.21.7 73 50-130
2-Nitroaniline mg/kg 2.33.3 70 49-130
2-Nitrophenol mg/kg 1.31.7 79 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.21.7 75 50-130
3,3'-Dichlorobenzidine mg/kg 2.5 IL3.3 75 47-130
3-Nitroaniline mg/kg 2.6 IL3.3 80 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.4 v13.3 104 50-142
4-Bromophenylphenyl ether mg/kg 1.31.7 78 55-130
4-Chloro-3-methylphenol mg/kg 2.63.3 78 52-130
4-Chloroaniline mg/kg 2.43.3 74 49-130
4-Chlorophenylphenyl ether mg/kg 1.31.7 77 53-130
4-Nitroaniline mg/kg 2.73.3 81 51-130
4-Nitrophenol mg/kg 6.98.3 83 40-130
Acenaphthene mg/kg 1.31.7 82 56-130
Acenaphthylene mg/kg 1.41.7 82 58-130
Aniline mg/kg 1.11.7 66 44-130
Anthracene mg/kg 1.41.7 83 60-130
Benzo(a)anthracene mg/kg 1.41.7 85 59-130
Benzo(a)pyrene mg/kg 1.41.7 87 57-130
Benzo(b)fluoranthene mg/kg 1.41.7 85 54-130
Benzo(g,h,i)perylene mg/kg 1.41.7 83 59-130
Benzo(k)fluoranthene mg/kg 1.51.7 88 54-130
Benzoic Acid mg/kg 5.38.3 64 19-130
Benzyl alcohol mg/kg 2.43.3 72 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.7 72 55-130
bis(2-Chloroethyl) ether mg/kg 1.21.7 75 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.51.7 94 58-130
Butylbenzylphthalate mg/kg 1.61.7 99 46-138
Chrysene mg/kg 1.41.7 87 57-130
Di-n-butylphthalate mg/kg 1.51.7 88 57-130
Di-n-octylphthalate mg/kg 1.61.7 97 57-130
Dibenz(a,h)anthracene mg/kg 1.41.7 84 60-130
Dibenzofuran mg/kg 1.31.7 77 54-130
Diethylphthalate mg/kg 1.41.7 85 55-130
Dimethylphthalate mg/kg 1.41.7 83 57-130
Fluoranthene mg/kg 1.41.7 83 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3292349LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.41.7 82 56-130
Hexachloro-1,3-butadiene mg/kg 1.01.7 61 41-130
Hexachlorobenzene mg/kg 1.21.7 75 53-130
Hexachlorocyclopentadiene mg/kg 1.01.7 61 23-130
Hexachloroethane mg/kg 1.11.7 65 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.41.7 84 61-130
Isophorone mg/kg 1.21.7 71 49-130
N-Nitroso-di-n-propylamine mg/kg 1.21.7 70 52-130
N-Nitrosodimethylamine mg/kg 1.11.7 67 45-130
N-Nitrosodiphenylamine mg/kg 1.41.7 87 56-130
Naphthalene mg/kg 1.21.7 72 56-130
Nitrobenzene mg/kg 1.01.7 63 50-130
Pentachlorophenol mg/kg 2.73.3 83 33-130
Phenanthrene mg/kg 1.41.7 85 60-130
Phenol mg/kg 1.31.7 77 54-130
Pyrene mg/kg 1.51.7 90 61-130
Pyridine mg/kg 0.871.7 52 35-130
2,4,6-Tribromophenol (S)%88 18-130
2-Fluorobiphenyl (S)%75 19-130
2-Fluorophenol (S)%70 18-130
Nitrobenzene-d5 (S)%66 21-130
Phenol-d6 (S)%73 18-130
Terphenyl-d14 (S)%73 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3292350MATRIX SPIKE SAMPLE:
MSSpike
Result
92543010002
1,2,4-Trichlorobenzene mg/kg 1.42.2 64 22-130ND
1,2-Dichlorobenzene mg/kg 1.42.2 65 23-130ND
1,3-Dichlorobenzene mg/kg 1.42.2 63 26-130ND
1,4-Dichlorobenzene mg/kg 1.32.2 62 27-130ND
1-Methylnaphthalene mg/kg 1.62.2 73 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.7 v12.2 78 30-130ND
2,4,5-Trichlorophenol mg/kg 1.42.2 67 26-130ND
2,4,6-Trichlorophenol mg/kg 1.52.2 67 23-130ND
2,4-Dichlorophenol mg/kg 1.52.2 71 29-130ND
2,4-Dimethylphenol mg/kg 1.52.2 69 13-130ND
2,4-Dinitrophenol mg/kg 4.310.8 40 10-131ND
2,4-Dinitrotoluene mg/kg 1.52.2 70 28-130ND
2,6-Dinitrotoluene mg/kg 1.52.2 69 36-130ND
2-Chloronaphthalene mg/kg 1.52.2 67 27-130ND
2-Chlorophenol mg/kg 1.52.2 70 29-130ND
2-Methylnaphthalene mg/kg 1.52.2 71 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.62.2 72 20-130ND
2-Nitroaniline mg/kg 3.04.3 69 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3292350MATRIX SPIKE SAMPLE:
MSSpike
Result
92543010002
2-Nitrophenol mg/kg 1.52.2 68 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.62.2 75 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.7 IL4.3 63 15-130ND
3-Nitroaniline mg/kg 2.94.3 66 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 2.24.3 52 15-132ND
4-Bromophenylphenyl ether mg/kg 1.42.2 66 35-130ND
4-Chloro-3-methylphenol mg/kg 3.34.3 77 30-130ND
4-Chloroaniline mg/kg 2.84.3 65 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.52.2 69 32-130ND
4-Nitroaniline mg/kg 2.84.3 65 30-130ND
4-Nitrophenol mg/kg 7.110.8 65 17-130ND
Acenaphthene mg/kg 1.62.2 72 29-130ND
Acenaphthylene mg/kg 1.62.2 73 31-130ND
Aniline mg/kg 1.32.2 60 10-130ND
Anthracene mg/kg 1.52.2 71 33-130ND
Benzo(a)anthracene mg/kg 1.62.2 72 32-130ND
Benzo(a)pyrene mg/kg 1.62.2 74 32-130ND
Benzo(b)fluoranthene mg/kg 1.62.2 73 33-130ND
Benzo(g,h,i)perylene mg/kg 1.42.2 65 28-130ND
Benzo(k)fluoranthene mg/kg 1.72.2 79 31-130ND
Benzoic Acid mg/kg 1.1J10.8 10 10-130ND
Benzyl alcohol mg/kg 3.04.3 70 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.62.2 73 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.72.2 77 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 2.0 v12.2 93 40-130ND
Butylbenzylphthalate mg/kg 1.92.2 88 40-130ND
Chrysene mg/kg 1.62.2 74 30-130ND
Di-n-butylphthalate mg/kg 1.62.2 73 41-130ND
Di-n-octylphthalate mg/kg 1.82.2 84 42-130ND
Dibenz(a,h)anthracene mg/kg 1.42.2 66 27-130ND
Dibenzofuran mg/kg 1.52.2 71 32-130ND
Diethylphthalate mg/kg 1.62.2 73 40-130ND
Dimethylphthalate mg/kg 1.52.2 69 37-130ND
Fluoranthene mg/kg 1.52.2 68 26-130ND
Fluorene mg/kg 1.62.2 72 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.32.2 61 20-130ND
Hexachlorobenzene mg/kg 1.42.2 64 29-130ND
Hexachlorocyclopentadiene mg/kg 0.602.2 28 10-130ND
Hexachloroethane mg/kg 1.42.2 66 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.42.2 66 28-130ND
Isophorone mg/kg 1.62.2 72 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.62.2 76 31-130ND
N-Nitrosodimethylamine mg/kg 1.32.2 62 20-130ND
N-Nitrosodiphenylamine mg/kg 1.62.2 75 32-130ND
Naphthalene mg/kg 1.52.2 71 30-130ND
Nitrobenzene mg/kg 1.52.2 68 25-130ND
Pentachlorophenol mg/kg 2.54.3 57 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3292350MATRIX SPIKE SAMPLE:
MSSpike
Result
92543010002
Phenanthrene mg/kg 1.62.2 74 34-130ND
Phenol mg/kg 1.6 v12.2 76 14-130ND
Pyrene mg/kg 1.92.2 88 31-130ND
Pyridine mg/kg 1.02.2 48 10-130ND
2,4,6-Tribromophenol (S)%65 18-130
2-Fluorobiphenyl (S)%61 19-130
2-Fluorophenol (S)%64 18-130
Nitrobenzene-d5 (S)%66 21-130
Phenol-d6 (S)%69 18-130
Terphenyl-d14 (S)%70 15-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626553
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3294491
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004, 92543280005, 92543280006
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 9.9 N206/14/21 15:02
Aliphatic (C19-C36)mg/kg ND 9.9 N206/14/21 15:02
Aromatic (C11-C22)mg/kg ND 9.9 N206/14/21 15:02
1-Chlorooctadecane (S)%67 40-140 06/14/21 15:02
2-Bromonaphthalene (S)%94 40-140 06/14/21 15:02
2-Fluorobiphenyl (S)%95 40-140 06/14/21 15:02
o-Terphenyl (S)%86 40-140 06/14/21 15:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3294492LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3294493
Aliphatic (C09-C18)mg/kg ND N210.1 55 40-14070ND 50
Aliphatic (C19-C36)mg/kg ND N213.5 68 40-1408811.7 50
Aromatic (C11-C22)mg/kg 20.9 N228.6 73 40-1407521.1 1 50
1-Chlorooctadecane (S)%61 40-14078
2-Bromonaphthalene (S)%97 40-14094
2-Fluorobiphenyl (S)%98 40-14095
o-Terphenyl (S)%87 40-14084
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626005
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280001, 92543280002, 92543280003, 92543280004
Parameter Units
Dup
Result QualifiersRPDResult
92542760001
3291760SAMPLE DUPLICATE:
Percent Moisture %49.1 N2350.5
Parameter Units
Dup
Result QualifiersRPDResult
92543280004
3291779SAMPLE DUPLICATE:
Percent Moisture %29.6 N2230.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
626039
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92543280005, 92543280006
Parameter Units
Dup
Result QualifiersRPDResult
92542026001
3292052SAMPLE DUPLICATE:
Percent Moisture %14.5 N2415.0
Parameter Units
Dup
Result QualifiersRPDResult
92542861001
3292053SAMPLE DUPLICATE:
Percent Moisture %43.7 N2144.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92543280
Whitestone Assisted Living Fac
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92543280001 626553 626818SW-1 MADEP EPH MADEP EPH
92543280002 626553 626818B-1 MADEP EPH MADEP EPH
92543280003 626553 626818SW-2 MADEP EPH MADEP EPH
92543280004 626553 626818B-2 MADEP EPH MADEP EPH
92543280005 626553 626818SW-3 MADEP EPH MADEP EPH
92543280006 626553 626818SW-4 MADEP EPH MADEP EPH
92543280001 626592 626659SW-1 MADEP VPH MADEP VPH
92543280002 626950 626978B-1 MADEP VPH MADEP VPH
92543280003 626592 626659SW-2 MADEP VPH MADEP VPH
92543280004 626950 626978B-2 MADEP VPH MADEP VPH
92543280005 626592 626659SW-3 MADEP VPH MADEP VPH
92543280006 626592 626659SW-4 MADEP VPH MADEP VPH
92543280001 626142 626427SW-1 EPA 3546 EPA 8270E
92543280002 626142 626427B-1 EPA 3546 EPA 8270E
92543280003 626142 626427SW-2 EPA 3546 EPA 8270E
92543280004 626142 626427B-2 EPA 3546 EPA 8270E
92543280005 626142 626427SW-3 EPA 3546 EPA 8270E
92543280006 626142 626427SW-4 EPA 3546 EPA 8270E
92543280001 626031 626040SW-1 EPA 5035A/5030B EPA 8260D
92543280002 626031 626040B-1 EPA 5035A/5030B EPA 8260D
92543280003 626031 626040SW-2 EPA 5035A/5030B EPA 8260D
92543280004 626031 626040B-2 EPA 5035A/5030B EPA 8260D
92543280005 626031 626040SW-3 EPA 5035A/5030B EPA 8260D
92543280006 626031 626040SW-4 EPA 5035A/5030B EPA 8260D
92543280001 626005SW-1 SW-846
92543280002 626005B-1 SW-846
92543280003 626005SW-2 SW-846
92543280004 626005B-2 SW-846
92543280005 626039SW-3 SW-846
92543280006 626039SW-4 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2021 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 50
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