25093_N Mangum St Prop_Soil, SG, GW Assessment Report_20221104

Soil Gas, Soil, and Groundwater Assessment Report
Brownfields Project Name: N. Mangum St. Properties II
Durham, Durham County, North Carolina
Brownfields Project No. 20593-21-032
S&ME Project No. 213673A
PREPARED FOR:
Mangum St. Partners, LLC
c/o Four Points Development, LLC
1805 7th Street, NW
Washington, NC 20001

PREPARED BY:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616

Corporate Registration for Licensing of NC Geologists No. C-145
NC Engineering Firm No. F-0176

November 4, 2022

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com

November 4, 2022
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfields Program
217 West Jones Street
Raleigh, North Carolina 27605
Attention: Ms. Sharon Eckhard via email: [e-mail]
Brownfields Project Manager
Reference: Soil Gas, Soil, and Groundwater Assessment Report
601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
S&ME Project No. 213673
Dear Ms. Eckhart:
S&ME, Inc. (S&ME) on behalf of our client, Mangum Street Partners, LLC, is submitting the enclosed report
documenting soil gas, soil, and groundwater assessment at the above-referenced site. The assessment was
performed in accordance with the Assessment Work Plan for Soil, Soil Gas, and Groundwater, dated June 8, 2022,
and submitted to the NC Brownfields Program on June 8, 2022.
Mangum Street Partners, LLC plans to improve the Site under the North Carolina Department of Environmental
Quality (NCDEQ) Brownfields Program (NCBP). This assessment was performed to collect soil, soil gas, and
groundwater samples from selected areas to support development design and considerations regarding possible
exposures and environmental management of groundwater and soil gas during redevelopment.
We look forward to your favorable review of the assessment report. If you have any questions about the
information contained in our report, please contact the undersigned.
Sincerely,
S&ME, Inc.

Michael W. Pfeifer Samuel P. Watts, PG
Senior Project Manager Principal Geologist
[e-mail] [e-mail]
Enclosure: Soil Gas, Soil, and Groundwater Assessment Report, dated November 4, 2022

cc: Shirley Liggins ([e-mail]) – NC Brownfields Program
John Sunter ([e-mail]) - Mangum Street Partners, LLC
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022 i

Table of Contents
CERTIFICATION......................................................................................................................................................... ii
1.0 Project Background ........................................................................................................... 1
2.0 Deviations from the Work Plan ..................................................................................... 2
3.0 Sampling Methodology ................................................................................................... 2
3.1 Health and Safety / Utility Location / Site Setting ..................................................................... 2
3.2 Soil Sampling .................................................................................................................................. 3
3.3 Soil Gas Sampling ........................................................................................................................... 3
3.4 Temporary Monitor Well Installation and Groundwater Sampling ....................................... 4
3.5 Quality Assurance/Quality Control ............................................................................................. 5
4.0 Analytical Results ............................................................................................................. 5
4.1 Soil Analytical Results ................................................................................................................... 5
4.2 Soil Gas Analytical Results ............................................................................................................ 6
4.3 Groundwater Analytical Results .................................................................................................. 6
4.4 Quality Assurance/Quality Control Analytical Results ............................................................ 6
5.0 Discussion of Results ....................................................................................................... 7
5.1 Soil Discussion ................................................................................................................................ 7
5.2 Soil Gas Discussion ........................................................................................................................ 7
5.3 Groundwater Discussion ............................................................................................................... 7
5.4 Sitewide Environmental Risks - NCDEQ Risk Calculator ........................................................ 7
5.5 Quality Assurance/Quality Control Discussion ......................................................................... 8
6.0 Conclusions ........................................................................................................................ 8
6.1 Soil .................................................................................................................................................... 8
Groundwater ................................................................................................................................... 8
6.2 8
6.3 Soil Gas ............................................................................................................................................ 8
7.0 Recommendations ............................................................................................................. 8
8.0 References ........................................................................................................................... 9

Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022 ii
Table of Contents (cont’d)

Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Photographic Log
Appendix IV – Field Documents
Appendix V – Analytical Laboratory Reports and Chain-of-Custody Records
Appendix VI – NCDEQ Risk Calculator Output

Figures
Figure 1 – Vicinity Map
Figure 2 – Site Map
Figure 3 – Soil Sample Results
Figure 4 – Soil Gas Sample Results
Figure 5 – Groundwater Sample Results

Tables
Table 1 – Sample Location Coordinates
Table 2 – Soil Field Screening Results
Table 3 – Soil Gas Implant Installation Details
Table 4 – Temporary Well Construction Details and Groundwater Elevations
Table 5 – Groundwater Field Parameters Summary
Table 6 – Soil Sample Analytical Results Summary
Table 7 – Soil Gas Sample Analytical Results Summary
Table 8 – Groundwater Sample Analytical Results Summary

Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
1.0 Project Background
S&ME, Inc. (S&ME) on behalf of our client, Mangum Street Partners, LLC, has performed soil, soil gas, and
groundwater assessment activities at the Brownfields Project Site: Greenhouse Project/Mangum Street Properties
II (Brownfields Project No.: 20593-21-032). Mangum Street Properties intends to develop the Site under the North
Carolina Department of Environmental Quality (NCDEQ) Brownfields Program (NCBP). The referenced property is
west of North Mangum Street, south of Broadway Street and north of Hunt Street in Durham, Durham County,
North Carolina and is owned by Mangum Street Partners, LLC. A site vicinity map is provided as Figure 1 and a
site map showing the parcel boundaries is provided as Figure 2. The property consists of 10 property parcels,
totaling approximately 1.52 acres:
Durham County Parcel ID Property Address Acreage
104952 110 Hunt Street 0.15
104951 108 Hunt Street 0.114
104953 106 Hunt Street 0.148
104594 601 N. Mangum Street 0.188
104955 603 N. Mangum Street 0.233
104956 605 N. Mangum Street 0.161
104957 607 N. Mangum Street 0.127
104958 103 Broadway Street 0.073
104959 107 Broadway Street 0.153
104960 109 Broadway Street 0.173

Based on prior environmental reports prepared by others, the site was historically developed with residential
structures, beginning in 1913. An auto repair shop and gasoline filling station with two underground storage tanks
(USTs) were formerly present on the northeast corner of the site (607 N. Mangum Street). The UST system was
reportedly removed from the site in 1988, and approximately 50 cubic yards of petroleum-impacted soils were
spread on the ground surface near the center of the site at approximately 0.5 to one foot thick.
Historical assessment activities at the site identified total petroleum hydrocarbons (TPH) gasoline range organics
(GRO) in soil and volatile organic compounds (VOCs) in groundwater in the vicinity of the former UST basin on the
northeastern corner of the site. VOC constituents historically detected in groundwater included benzene, toluene,
chlorobenzene, ethylbenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene, and 1,2-dichlorobenzene. The UST
incident (Incident# 3788) was closed by the North Carolina Department of Environmental Quality (DEQ) in 1989.
DEQ issued a second No Further Action letter on April 23, 2007. A groundwater monitor well was reportedly
grouted by the City of Durham sometime in 2007.
In May 2021, S&ME conducted a Geotechnical Exploration at the site, consisting of installing eight geotechnical
soil borings across the site. Due to the potential for encountering contaminated soils, S&ME environmental
personnel were also present during the installation of the soil borings to monitor VOCs in the soil cuttings utilizing
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
a hand-held photo-ionization detector (PID). Elevated readings on the photo-ionization detector (PID) were
encountered in two of the soil borings (B-2 and B-5). Petroleum odors were noted in B-2 (located on the
northeastern portion of the site) from approximately six feet below ground surface (ft-bgs) continuing to the
boring termination depth of 39 ft-bgs. The PID measurements from B-2 ranged from 77.6 ppm at a depth of
approximately 8.5 feet to 4.5 ppm at a depth of approximately 23.5 feet. The PID measurements collected from
boring B-5 (located on the eastern portion of the site) ranged from 412 parts per million (ppm) at a depth of
approximately 3.5 feet, to 1.4 ppm at a depth of approximately 33.5 feet.
The assessment was performed in accordance with the Assessment Work Plan for Soil, Soil Gas, and Groundwater,
dated June 8, 2022, prepared by S&ME. The assessment Work Plan was submitted to Ms. Sharon Eckard, Eastern
District Supervisor, with the NCBP on June 8, 2022. Ms. Eckard acknowledged receipt of the Work Plan and
indicated a project manager was not assigned to the site and therefore the NCBP was not in a position to review
nor approve the workplan. The field work for the work plan was conducted in June and July 2022, the methods,
results, conclusions, and recommendations are presented below.
2.0 Deviations from the Work Plan
Deviations from the June 8, 2022, Work Plan are detailed below.
 Six-liter Summa® canisters were used to collect the soil gas samples rather than one-liter Summa®
canisters. Deviation in the sample canister size was due to the limited availability of canisters from
analytical laboratories. The change to larger canisters did not impact field sampling techniques or
laboratory data quality.
 Three of the four temporary monitor wells were installed to depths deeper than the 20 ft-bgs depth
specified in the work plan. Deviation in the drilling depth was due to lower observed water table. The
change in depths of the temporary monitor wells did not impact field sampling techniques of
laboratory data quality.
 Soil gas implant sample location SG-4 failed the helium leak test three times. Sample tubing fittings
and valves were adjusted after each leak test attempt; the leak failed each time. A soil gas sample was
collected. Soil gas sample results from SG-4 were reported with detections of several VOCs at
concentrations similar to some of the other soil gas probe sample results. Soil gas sample results from
SG-4 may have been affected by infiltrating air into the sample canister along with collected soil gas.
 The soil samples were analyzed for hexavalent chromium by Method 7199 versus the Work Plan
proposed Method 7196. Method 7199 generally provides more accurate results.
During the June and July 2022 assessment, there were no other deviations from the submitted Work Plan.
3.0 Sampling Methodology
3.1 Health and Safety / Utility Location / Site Setting
S&ME prepared a site-specific Health and Safety Plan (HASP) in general accordance with the 29 CFR 1910.120
hazardous waste operations and emergency response (HAZWOPER) rule for the protection of workers at
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
uncontrolled hazardous sites. The HASP addressed the contaminants known or suspected to be present on-site,
personal protective equipment, monitoring performed during the field activities, and response actions to be taken
in the event monitoring thresholds are exceeded.
Prior to site mobilization, S&ME contracted with a private utility locating service to avoid damaging underground
utilities at the proposed sample locations. Figure 1 presents a Site Topography Map, depicting the limits of the
Brownfield property. The locations of each of the sampling points were recorded using a Trimble® handheld GPS
unit with sub-meter accuracy. The soil, soil gas, and temporary groundwater monitor well locations are shown on
Figure 2, and the coordinates of the sample locations are listed in Table 1.
3.2 Soil Sampling
S&ME personnel mobilized to the site on June 28, 2022, to collect soil samples and install soil gas implants.
S&ME’s subcontracted driller, Quantex, utilized a Geoprobe® drill rig using direct push technology and Macro-
Core® push rods at the proposed sample locations. Soil was collected in acetate sleeves in five-foot intervals to
the proposed depths ranging from five ft.-bgs to a depth of 20 ft-bgs. The soils from each soil sample boring
(SG-1 through SG-8) were visually classified on site by S&ME personnel and field screened with a photo-ionization
detector (PID) to measure relative headspace concentrations of VOCs. One soil sample, with the highest level of
VOCs detected with the PID or at an interval chosen to characterize the soil at a specific depth, was selected for
laboratory analysis of VOCs by EPA Method 8260D, semi-volatile organic compounds (SVOCs) by EPA Method
8270E, eight RCRA metals by EPA Methods 6020B/7471B. Selected soil samples were additionally analyzed for
hexavalent chromium by EPA Method 7199. The soil boring logs describing the lithology and the PID screening
results for each location are included in Appendix IV. The PID readings recorded during soil sampling are
summarized on Table 2.
3.3 Soil Gas Sampling
S&ME installed eight soil gas implants (SGIs) on June 29, 2022. The SGIs were installed with Macro-Core® push
rods in general conformance with Geoprobe’s® “Implants Operation” manual. Each boring was installed to the
proposed six ft-bgs depth as specified in the work plan. Once the proposed depth was reached, a SGI was placed
at the bottom of the borehole with a section of Teflon tubing extending from the SGI to the ground surface. A
sand pack was placed within the annulus of the boring to a depth of approximately six inches above the top of the
SGI. A bentonite seal was placed in the annulus of the boring from the top of the sand pack interval to the
ground surface. Following installation, the tubing extending from the SGIs to the ground surface was capped and
allowed to equilibrate for at least 48 hours. The SGI installation details are shown on Table 3 and S&ME
personnel’s field notes documenting the SGI installations are included in Appendix IV.
S&ME personnel returned to the site on July 5, 2022, to perform the soil gas sampling. Prior to sample collection,
the sample train on each point was tested for leaks by attaching a brass T-connector to the end of the SGI tubing
and connecting a section of Teflon tubing to one part of the T-connector and another section to a certified six-
liter summa canister. A plastic shroud was placed overtop the SGI tubing array and summa canister. The other
section of tubing from the T-connector was fitted through the shroud and attached to a Tedlar® bag. S&ME then
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
injected helium (tracer) gas into the plastic shroud. The shroud was filled with helium to a concentration of least
15%, while a soil gas sample was collected into the Tedlar® bag for analysis of helium content.
After successfully passing the leak test (with the exception of SG-4), three volumes of air were purged from the
SGI sampling array using a calibrated low flow pump, at a rate of approximately 200 milliliters per minute
(mL/min). Three volumes of air were calculated based on the construction of the sampling array to include the
tubing and sand pack interval’s void space. After purging the three volumes of the sampling array, the valve of
the T-connector leading to the purge port was closed and the regulator valve of the six-liter summa canister was
opened to allow the collection of the soil gas sample. The sample collection rate was set with a one-hour
regulator to collect the sample at approximately 100 mL/min. The soil gas samples were shipped under standard
chain-of-custody protocol to Eurofins, a North Carolina-certified laboratory for analysis of VOCs by EPA Method
TO-15 plus naphthalene.
The locations of the soil and soil gas samples are depicted on Figure 2 and photographs of the soil gas sample
locations are included in Appendix III.
3.4 Temporary Monitor Well Installation and Groundwater Sampling
On June 28 to 29, 2022, temporary groundwater monitoring wells (labeled as GW-1 through GW-4) were installed
using a Geoprobe® drill rig equipped with 3-¼“ hollow-stem augers at each proposed location. Temporary
monitoring well GW-1 was installed to a depth of 20 ft-bgs with a 10-feet section of 0.01-inch slotted PVC screen
set to intersect the groundwater table; GW-2 was installed to 29 ft-bgs with a 15-foot screen; GW-3 was installed
to 30 ft-bgs with a 10-foot screen; and GW-4 was installed to a depth of 30 ft-bgs with a 20-foot screen. Each
temporary well was installed with sufficient length of two-inch diameter, Schedule 40 PVC riser to bring the well to
the ground surface. A sand pack was placed within the annulus of the borings to a depth of approximately one
foot above the top of the screened interval. A bentonite seal was placed in the annulus of the borings to a depth
of approximately two feet above the top of the sand pack interval. The construction details for the temporary
monitor wells are summarized on Table 4.

Following installation, the wells were allowed to equilibrate for at least 24 hours prior to sampling. On June 29,
2022, S&ME personnel measured the depth to groundwater in each of the temporary wells using an electric water
level indicator. After measuring the depth to water in each well, S&ME utilized dedicated, disposable polyethylene
tubing to develop the wells by removing approximately three well volumes from each well.

On June 30, 2022, S&ME personnel sampled each of the temporary monitoring wells via low-flow techniques.
S&ME with a peristaltic pump and dedicated, disposable Teflon®-lined polyethylene tubing to pump groundwater
from each well at a rate of approximately 200 mL/min. During purging field parameters of pH, temperature,
specific conductivity, dissolved oxygen, oxidation reduction potential, and turbidity were collected. Purging was
considered complete when the pH remained consistent within 0.1 standard units (SU) and the specific conductivity
varied no more than 5%. The final purge parameters recorded for each temporary monitor well are summarized
on Table 5, and a copy of the low-flow groundwater sampling forms inclusive of full purge groundwater
parameters are included in Appendix IV.

Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
Following well purging, the groundwater samples were collected using the peristaltic pump and dedicated,
disposable Teflon®-lined polyethylene tubing to pump groundwater directly into the laboratory supplied
containers. The collected samples were placed in an ice filled cooler and shipped under standard chain-of-
custody protocol to Con-Test. The samples were submitted for laboratory analysis of VOCs by EPA Method
8260D, SVOCs by EPA Method 8270E, and eight RCRA metals by EPA Methods 6020B/7470A. The locations of the
temporary groundwater monitoring wells are shown on Figure 2.
3.5 Quality Assurance/Quality Control
During the soil, soil gas, and groundwater sampling activities, S&ME collected additional samples for QA/QC
purposes, consisting of duplicate samples. The duplicate soil sample (sample ID: Soil Dup) was collected as a blind
duplicate for the record soil sample SG-2 (2-6’). The duplicate soil gas sample (sample ID: Duplicate) was
collected as a blind duplicate of the record soil gas sample SG-1. The duplicate groundwater sample (sample ID:
Duplicate) was collected as a duplicate of the record groundwater sample GW-1. The duplicate samples were
submitted for analysis of the same constituents as the record samples.
4.0 Analytical Results
4.1 Soil Analytical Results
The laboratory analytical results of the soil samples indicated that benzene, n-heptane, naphthalene, arsenic, and
hexavalent chromium were detected in soil samples GW-1 (10-15) and GW-2 (11-14) in concentrations exceeding
either the Residential Health Based Preliminary Soil Remediation Goal (PSRG), the Protection of Groundwater
PSRG, or both. In addition, total xylenes were detected in a concentration exceeding the Protection of
Groundwater PSRG in soil sample GW-2 (11-14).
Arsenic was detected in concentrations exceeding the Residential Health Based PSRG in each soil sample except
from GW-1 (10-15) and SG-1 (2-6). Selenium was detected exceeding the Protection of Groundwater PSRG in soil
samples GW-2 (11-14), GW-4 (13-17), SG-4 (2-6), and SG-6 (2-6).
Hexavalent chromium was detected in concentrations exceeding the Residential PSRG in each soil sample.
Several additional targeted contaminant constituents were detected in concentrations exceeding their respective
laboratory detection limits, but below their respective regulatory standards. Multiple reported sample
concentrations were qualified as being between the laboratory’s detection limits and reporting limits, and
therefore, are estimated. See the laboratory analytical report for further qualifiers on this data
A summary of the analytical results of the soil samples is presented on Tables 6 in Appendix II and the soil
analytical results are identified on Figure 3 in Appendix I. A copy of the laboratory’s analytical report is included
in Appendix V.
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
4.2 Soil Gas Analytical Results
The laboratory analytical results of the soil gas samples indicate that benzene, ethylbenzene, and naphthalene
were detected in concentrations exceeding their respective Residential Soil Gas Screening Levels (SGSLs) in soil
gas sample SG-1. These constituents were also detected in the soil gas sample SG-DUP at relative concentrations,
which is a blind duplicate sample of SG-1. In addition, benzene and trichloroethylene were detected in
concentrations exceeding their respective Residential SGSLs in soil gas sample SG-2. Several other VOCs were
detected in each of the soil gas samples, however, there were no detections exceeding their respective Residential
SGSLs.
A summary of the analytical results of the soil gas samples is presented on Table 7 in Appendix II and the soil
gas concentrations which exceeded their respective laboratory detection limits are displayed on Figure 4 in
Appendix I. A copy of the laboratory’s analytical report is included in Appendix V.
4.3 Groundwater Analytical Results
The laboratory analytical results of the groundwater samples indicated that benzene, 1,2-dichloroethane,
naphthalene, and 2-methylnaphthalene were detected in the sample collected from GW-1 in concentrations
exceeding their respective NCDEQ 2L Standards. These constituents were also detected in the groundwater
sample GW-DUP at relative concentrations, which is a blind duplicate sample of GW-1. In addition, benzene, 2-
methylnaphthalene, and naphthalene were detected in concentrations exceeding their respective 2L Standards in
the groundwater sample collected from GW-2. No targeted contaminant constituents were detected in
concentrations exceeding their respective 2L Standards in the samples collected from GW-3 and GW-4.
Several VOC and SVOC constituents were reported in groundwater samples from GW-1 and GW-2 exceeding
NCDEQ Groundwater Screening Levels for Residential Vapor Intrusion Screening Levels (VISLs). The groundwater
sample from GW-3 marginally exceeded the VISL for chloroform.
A summary of the analytical results of the groundwater samples is presented on Table 8 in Appendix II and the
groundwater concentrations which exceeded their respective laboratory detection limits are displayed on Figure 5
in Appendix I. A copy of the laboratory’s analytical report is included in Appendix V.
4.4 Quality Assurance/Quality Control Analytical Results
During the soil, soil gas, and groundwater sampling, a comparison of the analytical results of the duplicate
samples to the record samples indicated similar concentrations of detected constituents. The blind duplicate
groundwater sample (GW-DUP) was a blind duplicate sample of GW-1. The blind duplicate soil sample(Soil Dup)
was a blind duplicate of sample SG-2 (11-14). The blind duplicate soil gas sample (SG-DUP) was a blind duplicate
of sample SG-1. The laboratory results of the record samples compared to the duplicate samples were all with
acceptable relative differences for quality control for the media sampled.
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
5.0 Discussion of Results
5.1 Soil Discussion
Petroleum-related VOCs (benzene and naphthalene) were detected in concentrations exceeding their respective
Protection of Groundwater PSRGs in soil samples from GW-1 (10-15) and GW-2 (11-14). Arsenic was detected in
all samples, except GW-1 (10-15), at concentrations exceeding the Residential or Industrial Health Based PSRGs.
Hexavalent chromium was detected in each of the soil samples at concentrations exceeding the Residential Health
Based PSRG. Selenium was detected exceeding the Protection of Groundwater PSRG in soil samples GW-2 (11-14),
GW-4 (13-17), SG-4 (2-6), and SG-6 (2-6).
5.2 Soil Gas Discussion
Two soil gas samples (SG-1 and SG-2 or SG-DUP) were reported with benzene, ethylbenzene and naphthalene at
concentrations exceeding their respective Residential SGSLs. Trichloroethylene was detected in SG-2 at a
concentration exceeding the Residential SGSL.
5.3 Groundwater Discussion
Groundwater has historically been contaminated with petroleum compounds in the northeastern portion of the
site from historical use. Groundwater samples collected from temporary monitor well GW-1 installed in this area
were reported with benzene, 1,2-dichloroethane, naphthalene, and 2-methylnaphthalene at concentrations
exceeding their respective 2L Standards. The groundwater sample collected from GW-2 and GW-DUP (also
installed in this area) contained benzene, isopropyl ether and naphthalene in concentrations exceeding their
respective 2L Standards. Several other VOCs, SVOCs, and Metals were detected in samples GW-1 through GW-4
at concentrations above the laboratory method detection limit but below their respective 2L Standards.
5.4 Sitewide Environmental Risks - NCDEQ Risk Calculator
NCDEQ’s Risk Calculator was used to evaluate environmental exposure risks of multiple contaminants and
exposure pathways associated with the contaminated environmental media on site. S&ME used the newest
version (July 2022) of NCDEQ’s Risk Calculator, downloaded from the NCDEQ website.
The highest concentration of each constituent from each media sampled during the assessment was input into the
NCDEQ Risk Calculator. The outputs from the Risk Calculator provided the following:
 The risk was not exceeded for residential, non-residential, construction worker and recreator/trespasser
receptors exposure to soil.
 The risk was exceeded for all receptors for groundwater use. However, groundwater will not be used at this
site.
 The risk was exceeded for indoor air vapor intrusion for residential receptors for the groundwater to indoor
air, and soil gas to indoor air pathways.
 The risk was exceeded for indoor air vapor intrusion for non-residential worker receptors for the
groundwater to indoor air pathway.
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
A copy of the NCDEQ Risk Calculator Summary is included as Appendix VI.
5.5 Quality Assurance/Quality Control Discussion
Blind duplicate samples were collected from each sampling media (soil, soil gas, and groundwater). The laboratory
results of the record samples compared to the duplicate samples were all with acceptable relative differences for
quality control for the media sampled.
6.0 Conclusions
Based on the results of the assessment activities performed at the during the June and July 2022 site assessment,
the following conclusions are presented:
6.1 Soil
Constituents (benzene, naphthalene, total xylenes, arsenic, selenium, and hexavalent chromium) were detected
above their respective PSRGs in several of the soil samples collected across the site. The NCDEQ Risk Calculator
output showed the risk was not exceeded for residential, non-residential, construction worker and
recreator/trespasser receptors exposure to soil.
6.2 Groundwater
Shallow groundwater was shown to be impacted in monitor wells GW-1 and GW-2 with benzene, 1,2-
dichloroethane, naphthalene, and 2-methylnaphthalene detected above their respective 2L Standards.
Groundwater will not be used on this site.
6.3 Soil Gas
Soil gas sampling results were reported with benzene, ethylbenzene, naphthalene, and trichloroethylene in two of
the sample locations above their respective residential SGSLs. The residential receptor vapor intrusion risk is
exceeded for both groundwater and soil gas to indoor air pathways, and the non-residential worker receptor
vapor intrusion risk is exceeded for groundwater to indoor air pathway.
7.0 Recommendations
The analytical results from the assessment in June and July 2022 indicate the soil, groundwater, and soil gas are
impacted with contaminants above their respective screening levels as a result from historic operations at the site.
Based on the soil, groundwater analytical results discussed above and the applicable Health Based PSRGs, the
onsite soils and groundwater will be subject to the best practices in a DEQ-approved Environmental Management
Plan (EMP) to support site development.
Soil Gas, Soil, and Groundwater Assessment Report
Greenhouse Project/601 N. Mangum St., Durham, NC
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No. 20593-21-032
S&ME Project No. 213673

November 4, 2022
Because the vapor intrusion risk calculated with the NCDEQ Risk Calculator is exceeded for both residential and
non-residential workers, S&ME recommends planning and design of a vapor intrusion mitigation system (VIMS)
below the proposed structure. The VIMS design should be included in the EMP for site development.
8.0 References
Pertinent information for this was obtained from the following external sources.
 Geotechnical Exploration Report - Greenhouse Project, dated June 9, 2021, prepared by S&ME, Inc.
 Stormwater Soil Evaluation Report - Greenhouse Project, dated June 3, 2021, prepared by S&ME, Inc.

Appendices

Appendix I – Figures
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed August, 2021.Subject Property
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 1,500 '
8-29-22
213673
NORTH MANGUM ST. PROPERTIES II / BF# 20593-21-032GREENHOUSE PROJECT - 601 SOUTH MANGUM STREETDURHAM, DURHAM COUNTY, NORTH CAROLINADrawing Path: T:\GEO\Projects\2021\213673_Mangum(Four Points Dev)_Greenhouse Project_Durham, NC\!GIS\Brownfields Assessment\1 - usgs.mxd plotted by lhester 08-29-20220 1,500 3,000(FEET)
VICINITY MAP
³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE USGS NATIONAL TOPOGRAPHIC BASEMAP.THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYEDARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESSSTATED OTHERWISE.
!(
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!(N Mangum StDowd St
Broadway St
Hunt St
SG-1
SG-2
SG-3
SG-4
SG-5
SG-6
SG-7
SG-8
GW-3
GW-1
GW-2
GW-4
SS-1
SS-2
SS-3
NC OneMap, NC Center for Geographic Information and Analysis, NC 911 Board
!(Soil Sample Locations
!(Ground Water & Soil Sample Locations
!(Soil Gas Probe & Soil Sample Location
Subject Property
Durham County Parcels
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.2
1 " = 50 '
8-29-22
213673NORTH MANGUM ST. PROPERTIES II / BF# 20593-21-032GREENHOUSE PROJECT - 601 SOUTH MANGUM STREETDURHAM, DURHAM COUNTY, NORTH CAROLINADrawing Path: T:\GEO\Projects\2021\213673_Mangum(Four Points Dev)_Greenhouse Project_Durham, NC\!GIS\Brownfields Assessment\2 - site map.mxd plotted by lhester 08-29-20220 50 100
(FEET)SITE MAP³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE NC ONEMAP LATEST ORTHOIMAGERY BASELAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
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!U
!U
!U
!U
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GW-1 (10-15') mg/KgBenzene 0.135Naphthalene (VOC) 2.21*Naphthalene (SVOC) 0.701Hexavalent Chromium 3.45*
GW-2 (11-14') mg/KgBenzene 3.38*Naphthalene (VOC) 3.49*Total Xylenes 21.1Naphthalene (SVOC) 2.49*Arsenic 3.40*Selenium 3.77Hexavalent Chromium 1.19*
GW-3 (7-12') mg/KgArsenic 4.26*Hexavalent Chromium 0.31*
GW-4 (13-17') mg/KgArsenic 1.57*Selenium 3.97Hexavalent Chromium 0.53*
SS-1 (2-6') mg/KgArsenic 1.59*Hexavalent Chromium 2.61*
SS-2 (2-6') mg/KgArsenic 1.80*Hexavalent Chromium 0.67*
SS-3 (2-6') mg/KgArsenic 0.854*Hexavalent Chromium 0.87*
Soil Duplicate (2-6') mg/KgArsenic 2.23*Hexavalent Chromium 0.40*
SG-1 (2-6') mg/KgHexavalent Chromium 1.22*
SG-2 (2-6') mg/KgArsenic 1.50*Hexavalent Chromium 0.89*
SG-3 (2-6') mg/KgArsenic 1.12*Hexavalent Chromium 0.77*
SG-4 (2-6') mg/KgArsenic 1.52*Selenium 3.54Hexavalent Chromium 0.45*
SG-6 (2-6') mg/KgArsenic 3.07*Selenium 2.66Hexavalent Chromium 1.07*
SG-7 (2-6') mg/KgArsenic 2.27*Hexavalent Chromium 0.58*
SG-8 (2-6') mg/KgArsenic 3.44*Hexavalent Chromium 0.74*
SG-5Not Sampled N Mangum StDowd St
Broadway St
Hunt St
!>Soil Sample Locations
!U Ground Water & Soil Sample Locations
!?Soil Gas Probe & Soil Sample Location
Subject Property
Durham County Parcels
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.3
1 " = 40 '
7-25-22
213673NORTH MANGUM ST. PROPERTIES II / BF# 20593‐21‐032 GREENHOUSE PROJECT ‐ 601 SOUTH MAGNUM STREET DURHAM, DURHAM COUNTY, NORTH CAROLINA Drawing Path: T:\GEO\Projects\2021\213673_Mangum(Four Points Dev)_Greenhouse Project_Durham, NC\!GIS\Brownfields Assessment\soil sample results.mxd plotted by lhester 07-25-20220 50 100
(FEET)SOIL SAMPLE RESULTS³
NOTES:Samples collected on June 28 and 29, 2022.Only detections exceeding the North Carolina Division of Waste Managment Preliminary SoilRemediation Goals (PSRGs) (2021) are shown.Detections shown in bold exceeded the Protection of Groundwater PSRGs.Detections shown with an * exceeded the Residential Health Based PSRG.REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE NC ONEMAP ORTHOIMAGERY BASEMAP.THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYEDARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESSSTATED OTHERWISE.
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SG-1 ug/m3Benzene 50Ethylbenzene 110Naphthalene 29
SG-2 ug/m3Benzene 12Trichloroethylene 28
SG-DUP ug/m3Benzene 54Ethylbenzene 110Naphthalene 25
SG-3Detections below SGSLs
SG-4Detections below SGSLs
SG-5Detections below SGSLs
SG-6Detections below SGSLs
SG-7Detections below SGSLs
SG-8Detections below SGSLs
N Mangum StDowd St
Broadway St
Hunt St
GW-3
GW-1
GW-2
GW-4
SS-1
SS-2
SS-3
!>Soil Sample Locations
!U Ground Water & Soil Sample Locations
!?Soil Gas Probe & Soil Sample Location
Subject Property
Durham County Parcels
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.4
1 " = 40 '
7-25-22
213673NORTH MANGUM ST. PROPERTIES II / BF# 20593‐21‐032 GREENHOUSE PROJECT ‐ 601 SOUTH MAGNUM STREET DURHAM, DURHAM COUNTY, NORTH CAROLINA Drawing Path: T:\GEO\Projects\2021\213673_Mangum(Four Points Dev)_Greenhouse Project_Durham, NC\!GIS\Brownfields Assessment\soil gas sample results.mxd plotted by lhester 07-25-20220 50 100
(FEET)SOIL GAS SAMPLE RESULTS³
NOTES: Samples collected on July 5, 2022. Only detections exceeding the North Carolina Division of Waste Managment Vapor IntrusionResidential Soil Gas Screening Levels (SGSLs) (January 2022) are shown. See Table 7 - Soil Gas Sample Analytical Results Summary for all other detections. REFERENCE: GIS BASE LAYERS WERE OBTAINED FROM THE NC ONEMAP ORTHOIMAGERY BASEMAP. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYEDARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
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GW-1 ug/LBenzene 229*1,2-dichloroethane 6.49*Ethylbenzene 232*n-heptane 3.11*Hexane 51.2*Naphthalene (VOC) 358*1,2,4-trimethylbenzene 58.1*Total Xylenes 94.1*2-methylnaphthalene 44.7Naphthalene (SVOC) 153*
GW-2 ug/LBenzene 284*Ethylbenzene 47*Isopropyl ether 246Total Xylenes 100*Naphthalene (SVOC) 24.4*
GW-4Detections below 2L Standards and GWSLs
GW-2 ug/LChloroform 0.867*
GW-DUP ug/LBenzene 229*1,2-dichloroethane 5.57*Ethylbenzene 263*n-heptane 4.43*Hexane 51.6*Naphthalene (VOC) 388*1,2,4-trimethylbenzene 81.1*Total Xylenes 119*2-methylnaphthalene 57.9Naphthalene (SVOC) 184*N Mangum StDowd St
Broadway St
Hunt St
SG-1
SG-2
SG-3
SG-4
SG-5
SG-6
SG-7
SG-8
SS-1
SS-2
SS-3
!>Soil Sample Locations
!U Ground Water & Soil Sample Locations
!?Soil Gas Probe & Soil Sample Location
Subject Property
Durham County Parcels
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.5
1 " = 40 '
9-16-22
213673GREENHOUSE PROJECT601 SOUTH MAGNUM STREETDURHAM, DURHAM COUNTY, NORTH CAROLINADrawing Path: T:\GEO\Projects\2021\213673_Mangum(Four Points Dev)_Greenhouse Project_Durham, NC\!GIS\Brownfields Assessment\groundwater sample results.mxd plotted by dkehoe 09-16-20220 50 100
(FEET)GROUNDWATER SAMPLE RESULTS³
NOTES: Samples collected on June 30, 2022. Only detections exceeding NCDEQ or USEPA standards are shown. Detections in BOLD exceed North Carolina Groundwater Quality 2L Standards (15 NCAC 2L). * indicates a detection above the Groundwater Screening Level for Residential Vapor Intrusion Screening Levels. See Table 8 - Groundwater Sample Analytical Results Summary for all other detections. REFERENCE: GIS BASE LAYERS WERE OBTAINED FROM THE NC ONEMAP ORTHOIMAGERY BASEMAP. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS

Appendix II – Tables

Sample ID Northing Easting Latitude Longitude
GW-1 819011.3920 2030648.031 36.0002666 -78.8963888
GW-2 818912.4690 203056.924 35.8491348 -85.0673046
GW-3 818987.9510 2030513.946 36.0002026 -78.8968422
GW-4 819010.9230 2030332.04 36.0002662 -78.8974571
SG-1 819002.9530 2030598.335 36.0002436 -78.8965569
SG-2 818940.1300 2030598.335 36.000071 -78.8965571
SG-3 818851.9900 2030529.4170 35.9998291 -78.8967904
SG-4 818899.8110 2030512.071 35.9999605 -78.8968489
SG-5 818878.2440 2030465.188 35.9999014 -78.8970074
SG-6 818907.7810 2030416.429 35.9999827 -78.8971722
SG-7 819032.9580 2030450.185 36.0003264 -78.8970576
SG-8 819066.7140 2030536.918 36.0004189 -78.8967643
SS-1 818994.0450 2030639.1230 36.000219 -78.896419
SS-2 819018.8930 2030631.153 36.0002873 -78.8964459
SS-3 818965.4470 2030610.056 36.0001405 -78.8965174
Notes:
North and Easting are in feet in the North Carolina State Plane Coordinate System (NAD83).
Latitude and longitude are reported in decimal degrees.
Figure 2 depicts the sample locations.
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
TABLE 1
Sample Location Coordinates
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum Street Properties II
Sample ID Collection Date Depth of Sample
(ft-bgs)PID (ppm)
GW-1 6/28/2022 10 - 15 2,000
GW-2 6/28/2022 11 - 14 2,000
GW-3 6/28/2022 7 - 12 1.5
GW-4 6/29/2022 13 - 17 2.7
SG-1 6/29/2022 2 - 6 2.7
SG-2 6/29/2022 2 - 6 3.3
SG-3 6/29/2022 2 - 6 1.3
SG-4 6/29/2022 2 - 6 1.8
SG-6 6/29/2022 2 - 6 0.8
SG-7 6/29/2022 2 - 6 2.1
SG-8 6/29/2022 2 - 6 0.9
SS-1 6/29/2022 2 - 6 0.6
SS-2 6/29/2022 2 - 6 0.8
SS-3 6/29/2022 2 - 6 1.6
NOTES:
ft-bgs: feet below ground surface
PID: photo ionization detector
ppm: parts per million
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
TABLE 2
SOIL SCREENING RESULTS
Brownfields Project Name: N. Mangum Street Properties II
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
Sample ID Date Installed Date Sampled
Boring
Diameter
(inches)
Total Depth
(ft-bgs)
#2 Filter Sand
Pack Interval
(ft-bgs)
*Implant
Placement Depth
(ft-bgs)
Hydrated
Granular
BentoniteSG-1 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-2 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-3 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-4 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-5 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-6 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-7 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
SG-8 6/29/2022 7/5/2022 2 6.0 4.5 - 6.0 5.0 - 5.75 0.0 - 4.5
Notes:
ft-bgs = feet below ground surface
*Implant length = 9 inches or approximately 0.75 feet.
The soil gas implant borings were properly abandoned after sampling on July 5, 2022.
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
Brownfields Project Name: N. Mangum St. Properties II
TABLE 3
Soil Gas Implant Installation Details
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Well ID Date Installed Date Sampled
Well
Diameter
(inches)
Screen
Length
(feet)
Screened
Interval
(ft-bgs)
Total Well
Depth
(ft-btoc)
Casing
Stickup
Height (ft)
Date Water
Level
Measured
Depth to
Water
(ft-btoc)
GW-1 6/28/2022 6/30/2022 2 10 10.0 -20.0 20 0.0 6/29/2022 6.69
GW-2 6/28/2022 6/30/2022 2 15 14.0 - 29.0 29 -0.9 6/29/2022 9.59
GW-3 6/28/2022 6/30/2022 2 10 20.0 - 30.0 30 -1.1 6/29/2022 18.12
GW-4 6/29/2022 6/30/2022 2 20 10.0 - 30.0 30 -0.8 6/29/2022 18.10
Notes:
ft-bgs = feet below ground surface
ft-btoc = feet below top of casing
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
Brownfields Project Name: N. Mangum St. Properties II
TABLE 4
Temporary Well Construction Details and Groundwater Elevations
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Field Parameters
(units) --->
Date Collected
GW-1 6/30/2022 21.1 6.1 359 1.9 92 9.24
GW-2 6/30/2022 22.2 6.4 640 4.3 110 9.55
GW-3 6/30/2022 20.5 6.9 470 5.3 28.5 5.27
GW-4 6/30/2022 23.4 6.6 479 3.8 91 9.43
Notes:
Readings displayed are the stabilized readings taken immediately prior to sampling. A complete field paramter summary for each well is included in Appendix IV.
°C = degrees Celsius
s.u. = standard units
µS/cm = microsiemens per centimeter
mg/L= miligrams per liter
mV = milivolts
NTUs = nephelometric turbidity units
Turbidity
(NTUs)Well ID Temperature
(°C)
pH
(s.u.)
Spec. Conductivity
(µS/cm)
Dissolved Oxygen
(mg/L)
Oxidation-
Reduction Potential
(mV)
S&ME Project No.: 213673
TABLE 5
Groundwater Field Parameters Summary
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
Page 1 of 2
Sample ID Date Collected
GW-1 (10-15)6/28/2022 0.310 B 0.135 0.0277 0.00797 <0.0132 2.37 5.09 6.32 0.0227 0.00534 J 2.21 0.0873 0.195 0.0445 0.00823 3.5
GW-2 (11-14)6/28/2022 <1.14 3.38 1.17 <0.207 <0.954 5.35 11.1 13.9 0.389 J 0.417 J 3.49 1.43 3.57 9.86 3.50 21.1
GW-3 (7-12)6/28/2022 0.0844 B <0.00215 <0.00170 <0.00179 <0.00825 <0.00188 <0.00386 <0.00152 <0.00197 <0.00233 <0.00278 <0.00197 <0.00233 <0.00224 <0.00215 <0.00323
GW-4 (13-17)6/29/2022 0.0502 B <0.00226 <0.00179 <0.00188 <0.00866 <0.00198 <0.00405 <0.00160 <0.00207 <0.00245 <0.00292 <0.00207 <0.00245 <0.00235 <0.00226 <0.00339
SS-1 (2-6)6/29/2022 0.0186 J B <0.00225 <0.00179 <0.00188 <0.00864 <0.00197 <0.00404 <0.00160 <0.00207 <0.00244 <0.00291 <0.00207 <0.00244 <0.00235 <0.00225 <0.00338
SS-2 (2-6)6/29/2022 0.0655 B <0.00277 <0.00219 <0.00231 <0.0106 <0.00243 <0.00497 <0.00196 <0.00254 <0.00300 <0.00358 <0.00254 <0.00300 <0.00289 <0.00277 <0.00416
SS-3 (2-6)6/29/2022 0.0392 J B <0.00202 <0.00160 <0.00168 <0.00775 <0.00177 <0.00362 <0.00143 <0.00185 <0.00219 <0.00261 <0.00185 <0.00219 <0.00211 <0.00202 <0.00303
Soil Dup 6/29/2022 0.0594 B <0.00226 0.0235 0.00467 J <0.00867 <0.0713 <0.146 <0.0578 0.00651 <0.00245 <0.105 0.0326 <0.00245 0.174 0.0787 0.00450 J
SG-1 (2-6)6/29/2022 0.0201 J B <0.00224 <0.00177 <0.00187 <0.00859 <0.00196 <0.00402 <0.00159 <0.00206 <0.00243 <0.00290 <0.00206 <0.00243 <0.00234 <0.00224 <0.00336
SG-2 (2-6)6/29/2022 0.0349 J B <0.00218 0.00288 J <0.00181 <0.00834 <0.00190 0.0590 0.0584 <0.00453 <0.00236 <0.00281 0.00362 J <0.00236 0.0211 0.00931 <0.00326
SG-3 (2-6)6/29/2022 0.0398 J B <0.00238 <0.00188 <0.00198 <0.00912 <0.00208 <0.00426 <0.00168 <0.00496 <0.00258 <0.00307 <0.00218 <0.00258 <0.00248 <0.00238 <0.00357
SG-4 (2-6)6/29/2022 0.0929 B <0.00254 <0.00201 <0.00212 0.0119 J <0.00222 <0.00455 <0.00180 <0.00233 <0.00275 0.0168 <0.00233 <0.00275 <0.00265 <0.00254 <0.00381
SG-6 (2-6)6/29/2022 0.140 B <0.00226 <0.00179 <0.00188 0.00982 J <0.00198 <0.00497 <0.00160 <0.00207 <0.00245 <0.00292 <0.00207 <0.00245 <0.00236 <0.00226 <0.00339
SG-7 (2-6)6/29/2022 0.0802 B <0.00247 <.00195 <0.00205 <0.00945 <0.00216 <0.00442 <0.00175 <0.00226 <0.00267 <0.00318 <0.00226 <0.00267 <0.00257 <0.00247 <0.00370
SG-8 (2-6)6/29/2022 <0.0101 <0.00221 <0.00175 <0.00184 <0.00846 <0.00193 <0.00395 <0.00156 <0.00202 <0.00239 <0.00285 <0.00202 <0.00239 <0.00230 <0.00221 <0.00331
Residential Health Based PSRG 12,000 1.2 780 1,600 5,500 6.1 4.4 130 410 NE 2.1 780 990 63 56 120
140,000 5.4 12,000 23,000 23,000 27 58 540 2,100 NE 8.8 5,100 9,700 370 320 530
Protection of GW PSRG 25 0.01 4.5 4.1 3.1 13.0 62 55 2.3 NE 0.39 2.6 8.3 12 11 9.9
Notes:
Soil sample concentrations are reported in mg/Kg.B: Analyte was also detected in the associated method blank at a concentration that may have contributed to the sample result.
mg/Kg - milligrams per kilogram.
NE - not established.
< - indicates the constituent was not detected above the method detection limit.
PSRG: Division of Waste Management Preliminary Soil Remediation Goals (June 2021).
Concentrations shown in BOLD exceed the laboratory detection limits.
Concentrations that exceed the Residential Health Based PSRG are highlighted yellow.
Concentrations that exceed the Industrial PSRG are highlighted orange.
The depth from which each soil sample was collected is identified in the parenthesis of the Sample ID and is expressed in feet below ground surface.
*The soil sample GW-3 (8-10') was collected from below the water table. At the time of drilling the soils appeared dry.
Duplicate sample SG-DUP is associated with the record sample SG-2 (2'-6').
J: Estimated - detection is between the Method Detection Limit and Repoted Detection Limit - therefore the concentration
is an estimate.
Data Qualifiers:
S&ME Project No.: 213673
Analytical Method
Analyte
acetone1,2,4-trimethylbenzene1,3,5-trimethylbenzenetotal xylenesTABLE 6
Soil Sample Analytical Results Summary
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
p-isopropyltoluenenaphthalenen-propylbenzenetolueneIndustrial PSRG
Volatile Organic Compunds by EPA Method 8260D (mg/Kg)hexanen- heptaneisopropylbenzenebenzenen-butylbenzenesec-butylbenzene2-butanone (MEK)ethylbenzene
Page 2 of 2
Method
7199
(mg/kg)
Sample ID Date Collected
chromiumleadmercuryGW-1 (10-15)6/28/2022 <0.0427 <0.0601 <0.0348 <0.0332 <0.0506 1.15 0.701 0.0901 J B <0.0427 <0.0537 <0.0427 0.600 194 0.0909 185 B 1.82 0.0150 J 1.12 <0.0147 3.45
GW-2 (11-14)6/28/2022 <0.0321 <0.0452 <0.0262 <0.0250 <0.0381 2.42 2.49 0.0697 J B <0.0321 0.176 J <0.0321 3.40 215 <0.0170 60.5 B 11.5 0.0112 J 3.77 <0.0113 1.19
GW-3 (7-12)6/28/2022 <0.0320 <0.0450 <0.0260 <0.0249 <0.0379 <0.0450 <0.0355 0.0706 J B <0.0320 <0.0402 <0.0320 4.26 145 0.0289 J 215 B 10.4 0.0645 1.51 0.0132 J 0.31
GW-4 (13-17)6/29/2022 <0.0320 <0.0450 <0.0261 <0.0249 <0.0379 <0.0450 <0.0355 0.0847 J B <0.0320 <0.0403 <0.0320 1.57 104 0.0459 J 25.4 B 13.2 0.0146 J 3.97 <0.0112 0.53
SS-1 (2-6)6/29/2022 0.0334 J <0.0465 <0.0269 <0.0257 0.0514 J <0.0465 <0.0367 0.0737 J B 0.0693 J <0.0416 0.0520 J 1.59 67.9 <0.0179 60.2 B 14.1 0.0126 J 1.29 <0.0119 2.61
SS-2 (2-6)6/29/2022 <0.0312 <0.0439 <0.0254 0.0270 J <0.0370 <0.0439 <0.0347 0.0626 J B <0.0312 <0.0393 0.0326 J 1.80 32.0 0.0627 7.87 B 12.2 0.0116 J 1.18 0.0277 J 0.67
SS-3 (2-6)6/29/2022 <0.0290 <0.0409 <0.0237 <0.0226 <0.0344 <0.0409 <0.0323 0.0731 J B <0.0290 <0.0366 <0.0290 0.854 43.0 0.0163 J 13.0 B 11.1 0.0526 0.954 0.0196 J 0.87
Soil Dup 6/29/2022 <0.0307 <0.0432 <0.0250 <0.0239 <0.0364 <0.0432 <0.0341 0.0581 J B <0.0307 <0.0387 <0.0307 2.23 64.9 <0.0162 20.6 B 9.37 <0.00887 1.26 <0.0108 0.40
SG-1 (2-6)6/29/2022 <0.0313 <0.0440 <0.0255 <0.0243 <0.0371 <0.0440 <0.0348 0.0606 J B <0.0313 <0.0394 <0.0313 0.641 23.2 <0.0180 14.0 B 7.48 0.0221 J 0.422 J <0.0120 1.22
SG-2 (2-6)6/29/2022 <0.0304 <0.0428 <0.0248 <0.0237 <0.0361 <0.0428 <0.0338 0.0685 J B <0.0304 <0.0383 <0.0304 1.50 16.4 <0.0169 13.2 B 6.17 0.0141 J 0.705 <0.0112 0.89
SG-3 (2-6)6/29/2022 <0.0295 <0.0415 <0.0240 <0.0229 <0.0349 <0.0415 <0.0327 0.0628 J B <0.0295 <0.0371 <0.0295 1.12 17.6 <0.0159 11.4 B 6.28 0.0239 J 0.404 J <0.0106 0.77
SG-4 (2-6)6/29/2022 0.0405 J 0.0484 J 0.0299 J 0.0336 J 0.0616 J <0.0452 <0.0356 0.0727 J B <0.0321 <0.0404 0.0595 J 1.52 75.3 0.0571 J 15.6 B 18.5 0.0274 J 3.54 0.0116 J 0.45
SG-6 (2-6)6/29/2022 <0.0303 <0.0426 <0.0247 <0.0236 <0.0359 <0.0426 <0.0336 0.0649 J B <0.0303 <0.0381 <0.0303 3.07 116 0.0997 20.6 B 63.2 0.149 2.66 0.0805 J 1.07
SG-7 (2-6)6/29/2022 <0.0317 <0.0446 <0.0258 <0.0247 0.0460 J <0.0446 <0.0352 0.0625 J B <0.0317 <0.0399 0.0456 J 2.27 17.9 <0.0178 14.9 B 8.97 0.0197 J 0.933 <0.0119 0.58
SG-8 (2-6)6/29/2022 <0.0324 <0.0455 <0.0264 <0.0252 <0.0384 <0.0455 <0.0360 0.0582 J B <0.0324 <0.0408 <0.0324 3.44 35.4 0.105 13.1 B 26.9 0.0253 J 1.18 <0.0114 0.74
Residential Health Based PSRG 1.1 1.1 NE 110 480 48 2.1 39 NE 3,800 360 0.68 3,100 1.4 23,000 400 4.7 78 78 0.31
21 21 NE 2,100 6,000 600 8.8 160 NE 49,000 4,500 3 47,000 20 350,000 800 70.0 1,200 1,200 6.5
Protection of GW PSRG 0.35 1.2 NE 36 670 3.1 0.39 14 NE 0.34 440 5.8 580 3 360,000 250 1.0 2.1 3.4 3.8
Notes:
Soil sample concentrations are reported in mg/Kg.B: Analyte was also detected in the associated method blank at a concentration that may have contributed to the sample result.
mg/Kg - milligrams per kilogram.J: Estimated - detection is between the Method Detection Limit and Repoted Detection Limit - therefore the concentration is an estimate.
NE - not established.
< - indicates the constituent was not detected above the method detection limit.
PSRG: Division of Waste Management Preliminary Soil Remediation Goals (June 2021).
Concentrations shown in BOLD exceed the laboratory detection limits.
Concentrations that exceed the Residential Health Based PSRG are highlighted yellow.
Concentrations that exceed the Industrial PSRG are highlighted orange.
The depth from which each soil sample was collected is identified in the parenthesis of the Sample ID and is expressed in feet below ground surface.
*The soil sample GW-3 (8-10') was collected from below the water table. At the time of drilling the soils appeared dry.
Duplicate sample SG-DUP is associated with the record sample SG-2 (2'-6').
Data Qualifiers:
TABLE 6
Soil Sample Analytical Results Summary
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
Metals by EPA Method 6010D (mg/Kg)benzo(a)anthracenesilvernaphthalenefluoranthenebenzo(b)fluoranthenehexavalent chromiumbenzo(g,h,i)perylenechrysenepyrenephenolarsenicbariumcadmiumseleniumphenanthreneSemi-Volatile Organic Compounds by EPA Method 8270E (mg/Kg)
Industrial PSRG bis(2-ethylhexyl)phthalate2-MethylnaphthaleneAnalytical Method
Analyte
Sample ID Date Collected
PropylbenzeneSG-1 7/5/2022 170 50 20 <14 10 180 44 110 30 7.7 25 36 29 24 9.8 74 <6.2 130 58 17 99
SG-2 7/5/2022 160 12 <31 <33 19 2,900 <50 33 35 170 2,200 34 <28 61 <18 97 28 62 100 1600 58
SG-3 7/5/2022 160 <3.9 <14 <15 <6.0 <4.2 35 <5.3 <6.0 <5.0 <4.3 20 <13 <6.0 31 <4.6 <6.5 <6.0 <6.0 <5.7 <5.3
SG-4 7/5/2022 180 6.1 <14 <15 <5.9 94 45 <5.2 <5.9 18 38 32 <13 <5.9 <8.2 9.4 <6.5 <5.9 <5.9 580 5.6
SG-5 7/5/2022 270 6.8 14 22 <5.7 47 34 5.4 <5.7 61 110 34 <12 <5.7 <7.9 18 <6.2 <5.7 <5.7 21 17.1
SG-6 7/5/2022 140 <3.5 <13 61 <5.4 <3.8 43 <4.8 <5.4 <4.5 4.0 21 <12 <5.4 <7.5 4.8 <5.9 <5.4 <5.4 <5.2 <4.8
SG-7 7/5/2022 97 <3.6 <13 30 <5.6 8.2 35 <4.9 <5.6 <4.6 <4.0 16 <12 <5.6 <7.7 4.7 <6.1 <5.6 <5.6 <5.3 <4.9
SG-8 7/5/2022 140 <4.0 <15 36 <6.2 11 38 <5.5 <6.2 <5.2 <4.4 25 <13 <6.2 <8.5 7.2 <6.8 <6.2 <6.2 <5.9 <5.5
SG-DUP 7/5/2022 150 54 16 <14 10 180 38 110 32 6.9 28 22 25 23 8.4 82 <6.2 130 57 17 100
22,000 12 35,000 4,900 2,800 42,000 NE 37 NE 2,800 4,900 1,400 2.8 7,000 280 35,000 14 420 420 NE 700
2,700,000 160 440,000 61,000 35,000 530,000 NE 490 NE 35,000 61,000 18,000 360 88,000 3,500 440,000 180 5,300 5,300 NE 8,800
Notes:
µg/m3: micrograms per cubic meter.
SGSL: Division of Waste Management Vapor Intrusion Soil Gas Screening Levels (July 2022).
Constituents not shown were not detected by the method.
Concentrations shown in BOLD exceed the laboratory method detection limit.
No constituents were detected at concentrations above their respective Non-Residential SGSL.
Duplicate sample SG-DUP is associated with the record sample SG-1.
Concentrations shown in BOLD and highlighted exceed the Residential SGSL.
Residential SGSL
Non-Residential SGSL AcetoneXylenes (total)Analytical Method
Analyte
Benzene1,3,5-Trimethylbenzene2-Butanone (MEK)Carbon DisulfideVolatile Organic Compunds(VOCs) by Method TO-15 (µg/m3)CyclohexaneTrichloroethyleneTolueneTetrachloroethyleneNaphthalene4-EthyltolueneTABLE 7
Soil Gas Sample Analytical Results Summary
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
2,2,4-Trimethylpentane2-Propanol (isopropanol)Cumene (isopropylbenzene)1,2,4-TrimethylbenzeneEthanolEthylbenzeneHeptaneHexane
Hexavalent
Chromium by
Method 7199
(mg/L)
Sample ID Date Collected
GW-1 6/30/2022 229 8.39 <1.35 6.49 232 3.11 J 51.2 15.9 18.9 J 17.6 J 358 30.5 12.6 31.4 58.1 9.78 94.1 8.03 J 44.7 153 0.500 0.000105 J 0.000625 J <0.002
GW-2 6/30/2022 284 <5.20 <2.70 <2.50 47 <4.30 <6.50 <2.60 246 <27.0 <24.0 4.27 J <2.70 36.2 16.2 5.21 J 100 9.33 J 8.49 J 24.4 0.288 <0.0000780 0.00580 J <0.002
GW-3 6/30/2022 <0.270 <0.520 0.867 J <0.250 <0.200 <0.430 <0.650 <0.260 <0.700 <2.70 <2.40 <0.410 <0.270 <0.250 <0.430 <0.280 <0.230 11.3 <4.22 <3.21 0.223 <0.0000780 <0.000340 <0.002
GW-4 6/30/2022 <0.270 <0.520 <0.270 <0.250 <0.200 <0.430 <0.650 <0.260 <0.700 <2.70 <2.40 <0.410 <0.270 <0.250 <0.430 <0.280 <0.230 17.5 <4.28 <3.26 0.236 <0.0000780 <0.000340 <0.002
GW-DUP 6/30/2022 229 9.78 <1.35 5.57 263 4.43 J 51.6 18.7 17.8 17 J 388 35.6 13.5 34.3 81.1 12.4 119 7.57 J 57.9 184 0.511 0.000115 J 0.000630 J <0.002
1 70 70 0.4 600 400 400 70 70 100 6 70 70 600 400 400 500 6,000 30 6 0.7 0.002 0.015 10
1.6 NE 0.81 2.2 3.5 1 2 NE NE 110,000 4.6 490 1,900 3,800 50 35 77 NE NE 4.6 NV NV NV NV
.Notes:
Only concentrations that were detected are shown. See the laboratory analytical report for full results.J: Estimated - detection is between the Method Detection Limit and Repoted Detection Limit - therefore the concentration is an estimate.
Volaile and Semi-Volatile Organic concentrations are reported in micrograms per liter (µg/L).
Metals concentrations are reported in milligrams per liter (mg/L).
< - indicates the constituent was not detected above the method detection limit.
2L Standards - North Carolina Groundwater Quality Standards (15A NCAC 2L)
Ground Water Screening Levels (GWSLs) for Residential Vapor Intrusion Screening Levels (VISLs) - based on May 2022 USEPA Regional Screening Tables.
Concentrations shown in BOLD exceed the laboratory detection limits.
Analytes highlighted in yellow exceed the NCDEQ 2L standards for groundwater and/or GWSLs for Residential VISLs.
Duplicate sample GW-DUP is associated with record sample GW-1.
NE: Standard has not been established by NCDEQ or USEPA.
NV: Constituent is not volatile and therefore does not have a standard set.
Data Qualifiers:
GWSLs for Residential VISLs
Analytical Method
total xylenesnaphthalenechloroformethylbenzeneisopropyl ether1,2,4-trimethylbenzene1,3,5-trimethylbenznen-propylbenzenetoluene1,2-dichloroethane4-methyl-2-pentanone (MIBK)2L Groundwater Standards
Metals by EPA Methods 6020B and
7470A (mg/L)
Analyte
TABLE 8
Groundwater Sample Analytical Results Summary
Greenhouse Project - 601 N. Mangum Street, Durham, North Carolina
Brownfields Project Name: N. Mangum St. Properties II
Brownfields Project No.: 20593-21-032
S&ME Project No.: 213673
Volatile Organic Compounds by EPA Method 8260B (µg/L)benzeneSemi-Volatile Organic
Compounds by EPA Method
8270D (µg/L)diethyl phthalate2-methylnaphthalenen-butylbenzenen-heptanehexavalent chromiumnaphthalenecadmiumhexaneisopropylbenzenestyreneleadbarium

Appendix III – Photographic Log

Mangum St. Brownfields Assessment
Greenhouse Brownfields
Durham, NC
S&ME Project No. 213673A
September 14, 2022 Date: 7/5/2022Photographer: J. WatersLocation / Orientation GW-1
Remarks Corner of Broadway and N. Mangum Date: 7/5/2022Photographer: J. WatersLocation / Orientation GW-2
Remarks Click here.
Date: 7/5/2022Photographer: J. WatersLocation / Orientation GW-3
Remarks Click here.Date: 7/5/2022Photographer: J. WatersLocation / Orientation GW-4
Remarks
Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-1
Remarks Duplicate taken here. Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-2
Remarks Click here.
Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-3
Remarks Click here.Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-4
Remarks Click here.
Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-5
Remarks Click here.Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-6
Remarks Click here.
Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-7
Remarks Click here.Date: 7/5/2022Photographer: J. WatersLocation / Orientation SG-8
Remarks Click here.

Appendix IV – Field Documents

S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE▼
2000
DATE DRILLED:Tuesday, June 28, 2022 20
DRILL RIG: Geoprobe 7822 DT 6.75
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: GW-1601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Clay, Tan, Brown, Moist,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
Sandy Clay, Tan, Orange, Moist,
5
Clay, Gray, Orange, Wet, Petroleum Odors
10 Yes
15
20 Boring Terminated at 20 Ft-BGS
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE▼
2000
DATE DRILLED:Tuesday, June 28, 2022 30
DRILL RIG: Geoprobe 7822 DT 9.54
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: GW-2601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESClayey Silt, Red, Orange, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Clayey Silt, Brown, Orange, Dry,
10
Clayey Silt, Red, Brown, Moist,
15
Silty Clay, Gray, Brown, Wet, Stained with Petroleum Odors Yes
20
25
Sandy Silt, Tan, Light, Brown, Dry,
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE▼
DATE DRILLED:Tuesday, June 28, 2022 30
DRILL RIG: Geoprobe 7822 DT 10.62
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: GW-3601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESClayey Silt, Brown, Red, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5 Clayey Silt, Brown, Red, Moist,
Silty Sand, Tan, Dry,
10
Yes
Clay, Gray, Organics, Wet,
Sandy Silt, Tan, Orange, Moist,
15
Sandy Silt, Light, Brown, Dry,
20
Sandy Silt, Gray, Dry,
25
Sandy Silt, Gray, Dry,
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE▼
2.7
DATE DRILLED:Wednesday, June 29, 2022 30
DRILL RIG: Geoprobe 7822 DT 9.92
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: GW-4601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Gray, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
10
15 Sandy Silt, Light, Red, Gray, Wet,
Sandy Silt, Light, Brown, Moist, Yes
Sandy Silt, Light, Red, Gray, Dry,
20 Sandy Silt, Red, Brown, Moist,
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.7
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-1601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Red, Brown, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Yes
Silty Clay, Orange, Gray, Dry,
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE3.3
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-2601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Brown, Orange, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE1.3
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-3601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Orange, Brown, Moist,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE1.8
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-4601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Light, Brown, Moist,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
Sandy Silt, Orange, Brown, Dry,
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.8
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-6601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Light, Brown, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
Sandy Silt, Gray, Brown, Dry,
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE2.1
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-7601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Light, Brown, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Yes
Clayey Silt, Gray, Orange, Dry,
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.9
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SG-8601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Light, Brown, Tan, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Clayey Silt, Gray, Orange, Moist, Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.6
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SS-1601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESClayey Silt, Light, Brown, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Clay, Gray, Dry, Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE0.8
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SS-2601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Orange, Brown, Dry,
SAMPLING METHOD:
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
Sandy Silt, Black, Moist,
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30
S&ME Project No. 213673A
BORING DEPTH (FT):
WATER LEVEL:
CAVE-IN DEPTH:
LOGGED BY:
NORTHING:
EASTING:WATER LEVELSAMPLEPID READING (PPM)Sample Time / 1st 6in2nd 6in3rd 6inN VALUE1.6
DATE DRILLED:Wednesday, June 29, 2022 6
DRILL RIG: Geoprobe 7822 DT
PROJECT:Greenhouse Project - Mangum Street Brownfields
BORING LOG: SS-3601 Mangum St, Durham, NC
DEPTH(feet)GRAPHICLOGMATERIAL DESCRIPTION
LABORATORY ANALYSESSandy Silt, Light, Brown, Dry,
SAMPLING METHOD: Macro-Core Sampler
DRILLING METHOD: Macro-Core Sampler (2.25-in. OD)
DRILLER: Quantex
HAMMER TYPE: Logan Hester
5
Yes
10
Boring Terminated at 6 Ft-BGS
15
20
25
30

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com
Environmental Field Report
Date:
June 29, 2022
Job Number:
213673A
Project Name:
Magnum Street Brownfield
Weather/Temperature:
Cloudy, 80°F
Project Location:
601 Mangum St. Durham, NC
Notes By:
☒
Present at the Site:
James Waters
☐ Logan Hester

Purpose: Develop the monitor wells located on site.

0930- Arrive at the site. Set out to develop the monitor wells. See the table below for well development
data.

ID Approx.
Total Well
Depth (ft.)
Depth from
Top of
Casing (ft.)
Stick Up
Height (ft.)
Water
Column
Height (ft.)
One Well
Volume
Gallons
Purged
During
Development
GW-1 20 6.69 0.00 13.31 2.17 7
GW-2 29 9.59 0.90 19.05 3.11 9.5
GW-3 30 18.12 1.10 11.88 1.93 6
GW-4 30 18.10 0.75 11.90 1.94 6

1330- Left site to pick up rental equipment.

1500- Arrived back at the site. Assisted Logan Hester with jarring soil samples.

1700- Left the site for the day.

Hours Mileage Signature of S&ME Personnel
6 onsite 90

Equipment Used
Monsoon Pump/Peristaltic Pump
Tubing
Water Level Meter

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com
Environmental Field Report
Date:
June 30, 2022
Job Number:
213673A
Project Name:
Magnum Street Brownfield
Weather/Temperature:
Sunny, 85°F
Project Location:
601 Mangum St. Durham, NC
Notes By:
☒
Present at the Site:
James Waters
☐

Purpose: Purge, record parameters, and sample the monitor wells located onsite.

1300- Arrive at the site.

1310- Calibration of sampling instruments. See the attached electronic field form for calibration
information.

1330- Set out to sample the monitor wells located onsite. See the attached electronic field forms for data
and sampling information. The water level depths are different than they were the day before, prior to
developing.

1755- Finished sampling the monitor wells onsite. Tidied up equipment and loaded the truck.

1800- Exchanged samples to the Eurofins carrier. Left the site for the day.

Hours Mileage Signature of S&ME Personnel
5 onsite 50

Equipment Used
YSI Flow Through Cell
Turbidity Meter
Monsoon Pump/Peristaltic Pump
Tubing
Water Level Meter
Time Completed:
Make /Model /Serial Number Unit:Reference:Reading:% Deviation
Water Level Meter Heron /Dipper-T /12FF2102138EC NA NA NA
Submersible Pump Pegasus /Alexis /24226 NA NA NA
4.0 NA #VALUE!
7.0 NA #VALUE!
10.0 NA #VALUE!
Temperature NA NA NA
NA NA #VALUE!
1,413 NA #VALUE!
Oxidation-Reduction Potential NA NA #VALUE!
0.02 0.02 0%
10.00 10.00 0%
1,000 1,000 0%
Name Signature Date
(1)
Comments:
Equipment/Meter
GROUNDWATER SAMPLING - METER CALIBRATION FORM
Date of Calibration:
(MM/DD/YY)6/30/2022 Weather/Temperature (°F):Sunny/85
Field Equipment, Meters, and Verifications 13:10
Feet
(0.01 feet)
NA
pH
YSI /Pro Plus /3898 (GeoTech)
Standard Unit
(0.1 s.u.)
Degees Celcius
(0.1 °C)
Dissolved Oxygen milligrams per liter
(0.1 %)
Conductivity microSiemens per centimeter
(1 µS/cm)
millivolts
(1 mV)
201607359
Nephelometric Turbidity Unit
(0.01 NTU ≤ 10.0 NTU,
0.1 NTU > 10.0 NTU and ≤ 100 NTU,
or 1 NTU >100 NTU)
James Waters 6/30/2022
YSI ProPlus was calibrated by GeoTech.
Turbidity MircroTPW /20000 /
30
6.75 ft-TOC 2 inch
20.00 ft-TOC 2.2 Gal
13.25 feet 6.49 Gal
10 feet Stickup: 0 ft-GRD 10.81 Gal
Start Time:16:55 End Time:
On (sec):Off (sec):Pressure:psi
ft-TOC
feet 250 mL
ft-TOC
Gallons
mL/min
(Yes/No)
Field Parameters (Taken at time intervals ≥ 5 minutes and purge volumes ≥ 1 flow-through cell volume)
Time
Volume
Purged Flow Rate
Depth to
Water Temp pH Spec. Cond.
Dissolved
Oxygen ORP*Turbidity
(gal)(mL/min)(ft)(°C)(s.u.)(µS/cm)(mg/L)(mV)(NTU)
16:55 0.0 ------------------------
17:00 0.2 150 7.25 21.4 6.2 366 2.3 87.8 24.9
17:05 0.4 150 8.00 21.2 6.1 363 2.0 86.2 19.5
17:10 0.6 150 8.60 21.3 6.1 363 1.9 86.7 18.8
17:15 0.8 150 9.35 21.3 6.1 362 1.8 89.0 14.3
17:20 1.0 150 9.80 21.1 6.1 363 1.9 90.7 11.1
17:25 1.2 150 10.60 21.1 6.1 359 1.9 92.1 9.24
Final: 17:25 1.2 150 10.60 21.1 6.1 359 1.9 92 9.2
Sample Method:17:25 17:50
Qty Container Qty Container
3 40mL VOAs
2 500mL A
1 500mL P
1 250mL P
Name Signature Date
(1)
(2)
Notes:
Form Revision Date:
Project Number:213673A Purge Date:June 30, 2022
Source Well:GW-1 Purge Time: Minutes
LOW FLOW GROUNDWATER SAMPLING FORM
Project Name:Mangum Street Brownfield
Project Location:601 Mangum St. Durham, NC
Weather:Sunny Air Temp:85° F
Water Level & Well Data
Locked?:Yes Sample Date:June 30, 2022
Sampled By:James Waters Sample Time:17:25
Measuring Point:Top of Casing Well Volume
Total Well Depth:Water Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
Well Purging Information
Depth to Water:Well Diameter
(If Used)Bladder Pump Control Settings:
Purge Method:Peristaltic Pump 17:25
Pump Intake Depth from Top of Casing: 12.0
Water Column Above Pump Intake: 5.25 Flow Through Cell Vol:
Final Volume Purged: 1.2
Final Volume Purge Rate: 150
Well Purged Dry?: No
DTW-TOC at 25% Drawdown of WC Above Pump: 8.06 Comments:
Comment
Start Purging
End of Purging
Peristaltic Pump Sample Start Time:Sample End Time:
Analytical Data
Method Preservative Method Preservative
SVOCs 8270 Unpreserved
VOCs 8260D HCl
Hex Cr 7199 Unpreserved
2/12/18 16:00
James Waters 6/30/2022
Duplicate is taken at GW-1.
6020B/7470A HNO3
30
9.54 ft-TOC 2 inch
29.00 ft-TOC 3.2 Gal
19.46 feet 9.53 Gal
15 feet Stickup: 0.9 ft-GRD 15.88 Gal
Start Time:15:50 End Time:
On (sec):Off (sec):Pressure:psi
ft-TOC
feet 250 mL
ft-TOC
Gallons
mL/min
(Yes/No)
Field Parameters (Taken at time intervals ≥ 5 minutes and purge volumes ≥ 1 flow-through cell volume)
Time
Volume
Purged Flow Rate
Depth to
Water Temp pH Spec. Cond.
Dissolved
Oxygen ORP*Turbidity
(gal)(mL/min)(ft)(°C)(s.u.)(µS/cm)(mg/L)(mV)(NTU)
15:50 0.0 ------------------------
15:55 0.2 150 10.10 22.7 6.5 656 5.1 86.2 28.0
16:00 0.4 150 11.20 22.2 6.4 635 4.5 95.0 23.0
16:05 0.6 150 12.30 22.0 6.4 637 4.3 101.8 16.6
16:10 0.8 150 13.70 22.1 6.4 641 4.4 106.3 11.8
16:15 1.0 150 14.70 22.0 6.4 638 4.3 108.4 9.06
16:20 1.2 150 15.80 22.2 6.4 640 4.3 110.1 9.55
Final: 16:20 1.2 150 15.80 22.2 6.4 640 4.3 110 9.6
Sample Method:16:20 16:45
Qty Container Qty Container
3 40mL VOAs
2 500mL A
1 500mL P
1 250mL P
Name Signature Date
(1)
(2)
Notes:
Form Revision Date:
Project Number:213673A Purge Date:June 30, 2022
Source Well:GW-2 Purge Time: Minutes
LOW FLOW GROUNDWATER SAMPLING FORM
Project Name:Mangum Street Brownfield
Project Location:601 Mangum St. Durham, NC
Weather:Sunny Air Temp:85° F
Water Level & Well Data
Locked?:Yes Sample Date:June 30, 2022
Sampled By:James Waters Sample Time:16:20
Measuring Point:Top of Casing Well Volume
Total Well Depth:Water Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
Well Purging Information
Depth to Water:Well Diameter
(If Used)Bladder Pump Control Settings:
Purge Method:Peristaltic Pump 16:20
Pump Intake Depth from Top of Casing: 20.0
Water Column Above Pump Intake: 10.46 Flow Through Cell Vol:
Final Volume Purged: 1.2
Final Volume Purge Rate: 150
Well Purged Dry?: No
DTW-TOC at 25% Drawdown of WC Above Pump: 12.16 Comments:
Comment
Start Purging
End of Purging
Peristaltic Pump Sample Start Time:Sample End Time:
Analytical Data
Method Preservative Method Preservative
SVOCs 8270 Unpreserved
VOCs 8260D HCl
Hex Cr 7199 Unpreserved
2/12/18 16:00
James Waters 6/30/2022
6020B/7470A HNO3
30
10.62 ft-TOC 2 inch
30.00 ft-TOC 3.2 Gal
19.38 feet 9.49 Gal
10 feet Stickup: 1.1 ft-GRD 15.81 Gal
Start Time:14:45 End Time:
On (sec):Off (sec):Pressure:psi
ft-TOC
feet 250 mL
ft-TOC
Gallons
mL/min
(Yes/No)
Field Parameters (Taken at time intervals ≥ 5 minutes and purge volumes ≥ 1 flow-through cell volume)
Time
Volume
Purged Flow Rate
Depth to
Water Temp pH Spec. Cond.
Dissolved
Oxygen ORP*Turbidity
(gal)(mL/min)(ft)(°C)(s.u.)(µS/cm)(mg/L)(mV)(NTU)
14:45 0.0 ------------------------
14:50 0.2 150 11.40 20.8 7.0 467 5.4 36.2 4.70
14:55 0.4 150 12.60 20.7 7.0 471 5.3 29.3 4.43
15:00 0.6 150 13.35 20.8 7.0 470 5.2 29.0 4.72
15:05 0.8 150 14.50 20.7 6.9 471 5.2 28.2 4.23
15:10 1.0 150 16.00 20.5 6.9 470 5.3 28.3 6.71
15:15 1.2 150 17.30 20.5 6.9 470 5.3 28.5 5.27
Final: 15:15 1.2 150 17.30 20.5 6.9 470 5.3 29 5.3
Sample Method:15:15 15:40
Qty Container Qty Container
3 40mL VOAs
2 500mL A
1 500mL P
1 250mL P
Name Signature Date
(1)
(2)
Notes:
Form Revision Date:
Project Number:213673A Purge Date:June 30, 2022
Source Well:GW-3 Purge Time: Minutes
LOW FLOW GROUNDWATER SAMPLING FORM
Project Name:Mangum Street Brownfield
Project Location:601 Mangum St. Durham, NC
Weather:Sunny Air Temp:85° F
Water Level & Well Data
Locked?:Yes Sample Date:June 30, 2022
Sampled By:James Waters Sample Time:15:15
Measuring Point:Top of Casing Well Volume
Total Well Depth:Water Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
Well Purging Information
Depth to Water:Well Diameter
(If Used)Bladder Pump Control Settings:
Purge Method:Peristaltic Pump 15:15
Pump Intake Depth from Top of Casing: 22.0
Water Column Above Pump Intake: 11.38 Flow Through Cell Vol:
Final Volume Purged: 1.2
Final Volume Purge Rate: 150
Well Purged Dry?: No
DTW-TOC at 25% Drawdown of WC Above Pump: 13.47 Comments:
Comment
Start Purging
End of Purging
Peristaltic Pump Sample Start Time:Sample End Time:
Analytical Data
Method Preservative Method Preservative
SVOCs 8270 Unpreserved
VOCs 8260D HCl
Hex Cr 7199 Unpreserved
2/12/18 16:00
James Waters 6/30/2022
6020B/7470A HNO3
30
9.92 ft-TOC 2 inch
30.00 ft-TOC 3.3 Gal
20.08 feet 9.83 Gal
20 feet Stickup: 0.75 ft-GRD 16.38 Gal
13:40 End Time:
On (sec):Off (sec):Pressure:psi
ft-TOC
feet 250 mL
ft-TOC
Gallons
mL/min
(Yes/No)
Field Parameters (Taken at time intervals ≥ 5 minutes and purge volumes ≥ 1 flow-through cell volume)
Time
Volume
Purged Flow Rate
Depth to
Water Temp pH Spec. Cond.
Dissolved
Oxygen ORP*Turbidity
(gal)(mL/min)(ft)(°C)(s.u.)(µS/cm)(mg/L)(mV)(NTU)
13:40 0.0 ------------------------
13:45 0.2 150 10.18 22.4 6.8 522 4.2 93.9 18.7
13:50 0.4 150 10.53 22.0 6.6 514 3.8 95.6 28.3
13:55 0.6 150 10.75 22.7 6.6 498 3.6 94.6 20.1
14:00 0.8 150 11.01 23.7 6.6 487 3.7 93.8 15.7
14:05 1.0 150 11.17 23.3 6.6 483 3.8 92.7 12.6
14:10 1.2 150 11.35 23.4 6.6 479 3.8 90.5 9.43
Final: 14:10 1.2 150 11.35 23.4 6.6 479 3.8 91 9.4
Sample Method:14:10 14:35
Qty Container Qty Container
3 40mL VOAs
2 500mL A
1 500mL P
1 250mL P
Name Signature Date
(1)
(2)
Notes:
Form Revision Date:
Project Number:213673A Purge Date:June 30, 2022
Source Well:GW-4 Purge Time: Minutes
LOW FLOW GROUNDWATER SAMPLING FORM
Project Name:Mangum Street Brownfield
Project Location:601 Mangum St. Durham, NC
Weather:Sunny Air Temp:85° F
Water Level & Well Data
Locked?:Yes Sample Date:June 30, 2022
Sampled By:James Waters Sample Time:14:10
Measuring Point:Top of Casing Well Volume
Total Well Depth:Water Volume
Height of Water Column:3 * Well Volume
Screen Length:5 * Well Volume
Well Purging Information
Depth to Water:Well Diameter
(If Used)Bladder Pump Control Settings:
Purge Method:Peristaltic Pump 14:10
Pump Intake Depth from Top of Casing: 15.0
Water Column Above Pump Intake: 5.08 Flow Through Cell Vol:
Final Volume Purged: 1.2
Final Volume Purge Rate: 150
Well Purged Dry?: No
DTW-TOC at 25% Drawdown of WC Above Pump: 11.19 Comments:
Comment
Start Purging
End of Purging
Peristaltic Pump Sample Start Time:Sample End Time:
Analytical Data
Method Preservative Method Preservative
SVOCs 8270 Unpreserved
VOCs 8260D HCl
Hex Cr 7199 Unpreserved
2/12/18 16:00
James Waters 6/30/2022
6020B/7470A HNO3

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com
Environmental Field Report
Date:
July 5, 2022
Job Number:
213673A
Project Name:
Greenhouse Project-
Magnum Street Brownfields
Weather/Temperature:
Sunny, 90°F
Project Location:
601 Mangum St. Durham, NC
Notes By:
☒
Present at the Site:
James Waters
☐ Bob Bryant

Purpose: Sample the soil gas with the summa canisters and screen with equipment at the same locations.

0900- Arrive at the site. Construct summa canisters and tubing.

0945- Set up to begin sampling at Mangum Street. See electronic field forms for data and sampling
information.

1640- Finish soil gas sampling.

1645- Load the truck with equipment.

1700- Leave the site for the day.

Hours Mileage Signature of S&ME Personnel
8 onsite 50

Equipment Used
Tools/Fittings
Sampling Port Equipment
Summa Canisters
Tubing

0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
6.5 0 18 6.5 0 18 6.5 0 18 6.5 0 18 6.5 0 18
54 to 72 54 to 72 54 to 72 54 to 72 54 to 72
Date:
Notes:
Revision Date:
2. Duplicate is taken at SG-1. 3. SG-4 failed the leak test 3 times. Project manager gave the approval to run the sample. 4. Analysis also includes naphthalene.
VOCs by TO-15 VOCs by TO-15 VOCs by TO-15
End Time 11:25 12:00 12:20 12:50
Approximate Total Time (min)60 65 60 55
Final Vacuum (inHg)6 7 6 7
15:20
7
65
Sampler Information
7/5/2022Sampler Signature:James Waters
5/3/18 11:30
Sample Analysis VOCs by TO-15
Sampled by:
VOCs by TO-15
1. Per the NCDEQ DWM VI Guidance dated March 2018, the helium concentration detected during the leak test shall not exceed 10% of the helium concentration in the shroud.
Purge Flow Rate (mL/min)200 200 200 200
28 26 29 29
Purge Interval (3x Vol.) (min)6.1 6.1 6.1 6.1
Initial Vacuum (inHg)
8.0 8.0 8.0
Sample Collection
Start Time 10:25 10:55 11:20 11:55
Actual Purge Time (min)8.0
14:15
8.0
Volume (mL)404 404 404 404
Leak Test Passed (Yes/No)1 Yes Yes Yes No Yes
Purge Information
Enter
Construction Details
→
404
Sand Pack Interval Depth (in-bgs)
He Detected in Leak Test (Y or N)No No No No No
Percent of He in the Leak Test versus the
Shroud 0.000%0.000%0.000%8.840%
He Conc. Detected in Leak Test (ppm)0 0
He Concentration in Shroud (%)15.6 18.4 16.7 18.1
1
90
Leak Test Information
Purge Method Personal Pump
16.4
30.2
Personal Pump
Ambient Temp (°F)90 90 90 90
Personal Pump Personal Pump Personal Pump
Barometric Pressure (inHg)30.1 30.1
23433 24542
1L3556
24743
Sample ID SG-1 SG-2 SG-3 SG-4
24043 23522
Canister ID 1L3957 1L3480 1L3020 1L2586
Sample Type Soil Gas Implant Soil Gas Implant Soil Gas Implant Soil Gas Implant
Helium Detector Serial No.:
Sample Information
30
30.1 30.1
0 16,000 1,075
0.655%
200
6.1
Canister Volume (L)1 1 1 1
Soil Gas Implant
SG-5
Regulator ID
90
6/27/2022
Date:
Air Temp (°F):
Calibration Date:
601 Mangum St. Durham, NC
Sunny
Dielectric Multi-Gas Detector MGD (Pine Environmental 21836)
SOIL VAPOR FIELD SAMPLING FORM
Location:
Greenhouse Project-Mangum Street Brownfields
213673A
Weather:
Project Name:
Project Number:
7/5/2022
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
0.17" ID
Total Tubing
(ft)
0.25" ID
Total Tubing
(in)
Sand Pack
Interval
(in)
6.5 0 18 6.5 0 18 6.5 0 18 6.5 0 18
54 to 72 54 to 72 54 to 72 54 to 72 to
Date:
Notes:
Revision Date:
SOIL VAPOR FIELD SAMPLING FORM
Project Name:Greenhouse Project-Mangum Street Brownfields
Project Number:213673A
Location:601 Mangum St. Durham, NC Date:
Sample Information
Sample Type Soil Gas Implant Soil Gas Implant Soil Gas Implant Soil Gas Implant
7/5/2022
Weather:Sunny Air Temp (°F):90
Helium Detector Serial No.:Dielectric Multi-Gas Detector MGD (Pine Environmental 21836)Calibration Date:6/27/2022
Canister ID 1L2809 1L3857 1L2217 1L3572
Sample ID SG-6 SG-7 SG-8 Duplicate
Canister Volume (L)1 1 1 1
Regulator ID 23153 25260 23712 24300
Barometric Pressure (inHg)30.2 30.2 30.2 30.1
Ambient Temp (°F)90 90 90 90
He Concentration in Shroud (%)25.5 19.7 22.7 15.6
Leak Test Information
Purge Method Personal Pump Personal Pump Personal Pump Personal Pump
He Conc. Detected in Leak Test (ppm)0 0 0 0
He Detected in Leak Test (Y or N)No No No No
Leak Test Passed (Yes/No)1 Yes Yes Yes Yes
Percent of He in the Leak Test versus the
Shroud 0.000%0.000%0.000%0.000%
Purge Information
Enter
Construction Details
→
Sand Pack Interval Depth (in-bgs)
Volume (mL)404 404 404 404
Purge Interval (3x Vol.) (min)6.1 6.1 6.1 6.1
Purge Flow Rate (mL/min)200 200 200 200
Initial Vacuum (inHg)30 29 29 29
Sample Collection
Start Time 14:35 15:05 15:25 10:25
Actual Purge Time (min)8.0 8.0 8.0 8.0
Final Vacuum (inHg)1 7 8 7
End Time 15:45 16:15 16:40 11:25
Sample Analysis VOCs by TO-15 VOCs by TO-15 VOCs by TO-15 VOCs by TO-15
Approximate Total Time (min)70 70 75 60
1. Per the NCDEQ DWM VI Guidance dated March 2018, the helium concentration detected during the leak test shall not exceed 10% of the helium concentration in the shroud.
2. Duplicate is taken at SG-1. 3. SG-4 failed the leak test 3 times. Project manager gave the approval to run the sample. 4. Analysis also includes naphthalene.
5/3/18 11:30
Sampler Information
Sampled by:James Waters Sampler Signature:7/5/2022

Appendix V – Analytical Laboratory Reports and Chain-of-Custody
Records

ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-218317-1
Client Project/Site: Greenhouse Project (Mangum St.)
For:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, North Carolina 27616
Attn: Michael Pfeifer
Authorized for release by:
7/19/2022 10:51:34 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
Definitions/Glossary
Job ID: 680-218317-1Client: S&ME, Inc.
Project/Site: Greenhouse Project (Mangum St.)
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 2 of 40 7/19/2022
1
2
3
4
5
6
7
Sample Summary
Client: S&ME, Inc.Job ID: 680-218317-1
Project/Site: Greenhouse Project (Mangum St.)
Lab Sample ID Client Sample ID Matrix Collected Received
680-218317-1 SG-1 Air 07/05/22 11:25 07/07/22 10:30
680-218317-2 SG-2 Air 07/05/22 12:00 07/07/22 10:30
680-218317-3 SG-3 Air 07/05/22 12:20 07/07/22 10:30
680-218317-4 SG-4 Air 07/05/22 12:50 07/07/22 10:30
680-218317-5 SG-5 Air 07/05/22 15:20 07/07/22 10:30
680-218317-6 SG-6 Air 07/05/22 15:45 07/07/22 10:30
680-218317-7 SG-7 Air 07/05/22 16:15 07/07/22 10:30
680-218317-8 SG-8 Air 07/05/22 16:40 07/07/22 10:30
680-218317-9 Duplicate Air 07/05/22 11:25 07/07/22 10:30
Eurofins SavannahPage 3 of 40 7/19/2022
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Case Narrative
Client: S&ME, Inc.Job ID: 680-218317-1
Project/Site: Greenhouse Project (Mangum St.)
Job ID: 680-218317-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-218317-1
Comments
No additional comments.
Receipt
The samples were received on 7/7/2022 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins SavannahPage 4 of 40 7/19/2022
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Method Summary
Job ID: 680-218317-1Client: S&ME, Inc.
Project/Site: Greenhouse Project (Mangum St.)
Method Method Description LaboratoryProtocol
EPAT014/T015 Volatiles - T0-14/T0-15 Eurofins
Protocol References:
EPA = US Environmental Protection Agency
Laboratory References:
Eurofins = Eurofins Air Toxics, 180 Blue Ravine Road, Suite B, Folsom, CA 95630
Eurofins Savannah
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7/15/2022
Mr. John Andros
Eurofins Test America
5102 LaRoche
Savannah GA 31404
Project Name: Greenhouse Project Mangum St.
Project #: 213673A
Dear Mr. John Andros
The following report includes the data for the above referenced project for sample(s)
received on 7/7/2022 at Eurofins Air Toxics LLC.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics LLC. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contact the Project Manager: Brian Whittaker at 916-985-1000 if you have any
questions regarding the data in this report.
Regards,
Brian Whittaker
Project Manager
Workorder #: 2207268
Page 1 of 34
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Mr. John Andros
Eurofins Environment Testing
5102 LaRoche
Savannah, GA 31404
WORK ORDER #: 2207268
CLIENT:BILL TO:
PHONE:
Accounts Payable
Eurofins Environment Testing
4104 Shuffel St NW
North Canton, OH 44720
912-354-7858
07/07/2022
DATE COMPLETED:07/15/2022
P.O. #680-218317-1
PROJECT #213673A Greenhouse Project Mangum
St.
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Brian Whittaker
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SG-1 TO-15 8.2 "Hg 9.9 psi
02A SG-2 TO-15 9 "Hg 10 psi
03A SG-3 TO-15 9.2 "Hg 10.1 psi
04A SG-4 TO-15 9.2 "Hg 10 psi
05A SG-5 TO-15 8.4 "Hg 9.9 psi
06A SG-6 TO-15 7.3 "Hg 9.9 psi
07A SG-7 TO-15 7.8 "Hg 10 psi
08A SG-8 TO-15 10 "Hg 10 psi
09A Duplicate TO-15 8.4 "Hg 9.8 psi
10A Lab Blank TO-15 NA NA
11A CCV TO-15 NA NA
12A LCS TO-15 NA NA
12AA LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE: 07/15/22
Page 2 of 34
Certification numbers: AZ Licensure AZ0775, FL NELAP – E87680, LA NELAP – 02089, NH NELAP - 209221, NJ NELAP - CA016,
NY NELAP - 11291, TX NELAP - T104704434-21-17, UT NELAP – CA009332021-13, VA NELAP - 10615, WA NELAP - C935
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005-015, Effective date: 10/18/2021, Expiration date: 10/17/2022.
Eurofins Air Toxics, LLC certifies that the test results contained in this report meet all requirements of the NELAC standards
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, LLC.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
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LABORATORY NARRATIVE
EPA Method TO-15
Eurofins Test America
Workorder# 2207268
Nine 1 Liter Summa Canister (100% Certified) samples were received on July 07, 2022. The laboratory
performed analysis via EPA Method TO-15 using GC/MS in the full scan mode.
The Chain of Custody (COC) information for sample SG-1 did not match the information on the canister
with regard to canister barcode. The sample labeled 1L3957 on the COC is labeled as 1L3597 on the
canister. The client was notified of the discrepancy and the information on the canister was used to
process and report the sample.
Receiving Notes
Dilution was performed on sample SG-2 due to the presence of high level target species.
Analytical Notes
Ten qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
M - Reported value may be biased due to apparent matrix interferences.
CN - See Case Narrative.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 34
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EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SG-1
Lab ID#: 2207268-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
12 23 22 44Ethanol
12 70 27 170Acetone
4.6 15 11 362-Propanol
1.2 7.2 4.0 25Hexane
4.6 6.9 14 202-Butanone (Methyl Ethyl Ketone)
1.2 52 4.0 180Cyclohexane
1.2 3.6 5.4 172,2,4-Trimethylpentane
1.2 16 3.7 50Benzene
1.2 1.9 4.7 7.7Heptane
1.2 20 4.3 74Toluene
1.2 1.4 7.8 9.8Tetrachloroethene
1.2 26 5.0 110Ethyl Benzene
1.2 14 5.0 63m,p-Xylene
1.2 8.4 5.0 36o-Xylene
1.2 2.0 5.6 10Cumene
1.2 4.8 5.6 24Propylbenzene
1.2 6.2 5.6 304-Ethyltoluene
1.2 12 5.6 581,3,5-Trimethylbenzene
1.2 27 5.6 1301,2,4-Trimethylbenzene
2.3 5.5 12 29Naphthalene
Client Sample ID: SG-2
Lab ID#: 2207268-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
27 66 63 160Acetone
11 14 26 342-Propanol
2.7 640 9.4 2200Hexane
2.7 840 9.2 2900Cyclohexane
2.7 340 12 16002,2,4-Trimethylpentane
2.7 3.7 8.5 12Benzene
2.7 41 11 170Heptane
2.7 5.2 14 28Trichloroethene
Page 4 of 34
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EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SG-2
Lab ID#: 2207268-02A
2.7 26 10 97Toluene
2.7 7.6 12 33Ethyl Benzene
2.7 9.7 12 42m,p-Xylene
2.7 3.7 12 16o-Xylene
2.7 3.9 13 19Cumene
2.7 12 13 61Propylbenzene
2.7 7.2 13 354-Ethyltoluene
2.7 21 13 1001,3,5-Trimethylbenzene
2.7 13 13 621,2,4-Trimethylbenzene
Client Sample ID: SG-3
Lab ID#: 2207268-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
12 19 23 35Ethanol
12 67 29 160Acetone
4.9 8.0 12 202-Propanol
1.2 4.5 8.2 31Tetrachloroethene
Client Sample ID: SG-4
Lab ID#: 2207268-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
12 24 23 45Ethanol
12 75 29 180Acetone
4.8 13 12 322-Propanol
1.2 11 4.3 38Hexane
1.2 27 4.2 94Cyclohexane
1.2 120 5.6 5802,2,4-Trimethylpentane
1.2 1.9 3.9 6.1Benzene
1.2 4.5 5.0 18Heptane
1.2 2.5 4.6 9.4Toluene
1.2 1.3 5.2 5.6m,p-Xylene
Page 5 of 34
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EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SG-5
Lab ID#: 2207268-05A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
12 18 22 34Ethanol
12 110 28 270Acetone
4.6 14 11 342-Propanol
4.6 7.2 14 22Carbon Disulfide
1.2 31 4.1 110Hexane
4.6 4.9 14 142-Butanone (Methyl Ethyl Ketone)
1.2 14 4.0 47Cyclohexane
1.2 4.6 5.4 212,2,4-Trimethylpentane
1.2 2.1 3.7 6.8Benzene
1.2 15 4.8 61Heptane
1.2 4.9 4.4 18Toluene
1.2 1.2 5.0 5.4Ethyl Benzene
1.2 2.7 5.0 12m,p-Xylene
1.2 1.2 5.0 5.1o-Xylene
Client Sample ID: SG-6
Lab ID#: 2207268-06A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
11 23 21 43Ethanol
11 60 26 140Acetone
4.4 8.5 11 212-Propanol
4.4 20 14 61Carbon Disulfide
1.1 1.1 3.9 4.0Hexane
1.1 1.3 4.2 4.8Toluene
Client Sample ID: SG-7
Lab ID#: 2207268-07A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
11 18 21 35Ethanol
11 41 27 97Acetone
4.5 6.5 11 162-Propanol
Page 6 of 34
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EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SG-7
Lab ID#: 2207268-07A
4.5 9.6 14 30Carbon Disulfide
1.1 2.4 3.9 8.2Cyclohexane
1.1 1.2 4.3 4.7Toluene
Client Sample ID: SG-8
Lab ID#: 2207268-08A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
13 20 24 38Ethanol
13 58 30 140Acetone
5.0 10 12 252-Propanol
5.0 12 16 36Carbon Disulfide
1.3 3.1 4.3 11Cyclohexane
1.3 1.9 4.7 7.2Toluene
Client Sample ID: Duplicate
Lab ID#: 2207268-09A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
12 20 22 38Ethanol
12 62 27 150Acetone
4.6 9.0 11 222-Propanol
1.2 7.9 4.1 28Hexane
4.6 5.4 14 162-Butanone (Methyl Ethyl Ketone)
1.2 54 4.0 180Cyclohexane
1.2 3.6 5.4 172,2,4-Trimethylpentane
1.2 17 3.7 54Benzene
1.2 1.7 4.7 6.9Heptane
1.2 22 4.4 82Toluene
1.2 1.2 7.8 8.4Tetrachloroethene
1.2 26 5.0 110Ethyl Benzene
1.2 14 5.0 63m,p-Xylene
1.2 8.5 5.0 37o-Xylene
1.2 2.0 5.7 10Cumene
Page 7 of 34
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EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: Duplicate
Lab ID#: 2207268-09A
1.2 4.7 5.7 23Propylbenzene
1.2 6.6 5.7 324-Ethyltoluene
1.2 12 5.7 571,3,5-Trimethylbenzene
1.2 26 5.7 1301,2,4-Trimethylbenzene
2.3 4.7 12 25Naphthalene
Page 8 of 34
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Client Sample ID: SG-1
Lab ID#: 2207268-01A
EPA METHOD TO-15 GC/MS FULL SCAN
p071415File Name:
Dil. Factor:2.30
Date of Collection: 7/5/22 11:25:00 AM
Date of Analysis: 7/14/22 06:27 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.7 Not DetectedFreon 12
1.2 Not Detected 8.0 Not DetectedFreon 114
12 Not Detected 24 Not DetectedChloromethane
1.2 Not Detected 2.9 Not DetectedVinyl Chloride
1.2 Not Detected 2.5 Not Detected1,3-Butadiene
12 Not Detected 45 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.2 Not Detected 6.5 Not DetectedFreon 11
12 23 22 44Ethanol
1.2 Not Detected 8.8 Not DetectedFreon 113
1.2 Not Detected 4.6 Not Detected1,1-Dichloroethene
12 70 27 170Acetone
4.6 15 11 362-Propanol
4.6 Not Detected 14 Not DetectedCarbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
12 Not Detected 40 Not DetectedMethylene Chloride
4.6 Not Detected 16 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.6 Not Detectedtrans-1,2-Dichloroethene
1.2 7.2 4.0 25Hexane
1.2 Not Detected 4.6 Not Detected1,1-Dichloroethane
4.6 6.9 14 202-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.6 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.4 Not DetectedTetrahydrofuran
1.2 Not Detected 5.6 Not DetectedChloroform
1.2 Not Detected 6.3 Not Detected1,1,1-Trichloroethane
1.2 52 4.0 180Cyclohexane
1.2 Not Detected 7.2 Not DetectedCarbon Tetrachloride
1.2 3.6 5.4 172,2,4-Trimethylpentane
1.2 16 3.7 50Benzene
1.2 Not Detected 4.6 Not Detected1,2-Dichloroethane
1.2 1.9 4.7 7.7Heptane
1.2 Not Detected 6.2 Not DetectedTrichloroethene
1.2 Not Detected 5.3 Not Detected1,2-Dichloropropane
4.6 Not Detected 16 Not Detected1,4-Dioxane
1.2 Not Detected 7.7 Not DetectedBromodichloromethane
1.2 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 4.7 Not Detected4-Methyl-2-pentanone
1.2 20 4.3 74Toluene
1.2 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.3 Not Detected1,1,2-Trichloroethane
1.2 1.4 7.8 9.8Tetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 9 of 34
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Client Sample ID: SG-1
Lab ID#: 2207268-01A
EPA METHOD TO-15 GC/MS FULL SCAN
p071415File Name:
Dil. Factor:2.30
Date of Collection: 7/5/22 11:25:00 AM
Date of Analysis: 7/14/22 06:27 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 9.8 Not DetectedDibromochloromethane
1.2 Not Detected 8.8 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.3 Not DetectedChlorobenzene
1.2 26 5.0 110Ethyl Benzene
1.2 14 5.0 63m,p-Xylene
1.2 8.4 5.0 36o-Xylene
1.2 Not Detected 4.9 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 2.0 5.6 10Cumene
1.2 Not Detected 7.9 Not Detected1,1,2,2-Tetrachloroethane
1.2 4.8 5.6 24Propylbenzene
1.2 6.2 5.6 304-Ethyltoluene
1.2 12 5.6 581,3,5-Trimethylbenzene
1.2 27 5.6 1301,2,4-Trimethylbenzene
1.2 Not Detected 6.9 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 6.9 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.0 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 6.9 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
2.3 5.5 12 29Naphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
103 70-1301,2-Dichloroethane-d4
105 70-1304-Bromofluorobenzene
Page 10 of 34
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Client Sample ID: SG-2
Lab ID#: 2207268-02A
EPA METHOD TO-15 GC/MS FULL SCAN
p071418File Name:
Dil. Factor:5.33
Date of Collection: 7/5/22 12:00:00 PM
Date of Analysis: 7/14/22 09:54 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.7 Not Detected 13 Not DetectedFreon 12
2.7 Not Detected 19 Not DetectedFreon 114
27 Not Detected 55 Not DetectedChloromethane
2.7 Not Detected 6.8 Not DetectedVinyl Chloride
2.7 Not Detected 5.9 Not Detected1,3-Butadiene
27 Not Detected 100 Not DetectedBromomethane
11 Not Detected 28 Not DetectedChloroethane
2.7 Not Detected 15 Not DetectedFreon 11
27 Not Detected 50 Not DetectedEthanol
2.7 Not Detected 20 Not DetectedFreon 113
2.7 Not Detected 10 Not Detected1,1-Dichloroethene
27 66 63 160Acetone
11 14 26 342-Propanol
11 Not Detected 33 Not DetectedCarbon Disulfide
11 Not Detected 33 Not Detected3-Chloropropene
27 Not Detected 92 Not DetectedMethylene Chloride
11 Not Detected 38 Not DetectedMethyl tert-butyl ether
2.7 Not Detected 10 Not Detectedtrans-1,2-Dichloroethene
2.7 640 9.4 2200Hexane
2.7 Not Detected 11 Not Detected1,1-Dichloroethane
11 Not Detected 31 Not Detected2-Butanone (Methyl Ethyl Ketone)
2.7 Not Detected 10 Not Detectedcis-1,2-Dichloroethene
2.7 Not Detected 7.8 Not DetectedTetrahydrofuran
2.7 Not Detected 13 Not DetectedChloroform
2.7 Not Detected 14 Not Detected1,1,1-Trichloroethane
2.7 840 9.2 2900Cyclohexane
2.7 Not Detected 17 Not DetectedCarbon Tetrachloride
2.7 340 12 16002,2,4-Trimethylpentane
2.7 3.7 8.5 12Benzene
2.7 Not Detected 11 Not Detected1,2-Dichloroethane
2.7 41 11 170Heptane
2.7 5.2 14 28Trichloroethene
2.7 Not Detected 12 Not Detected1,2-Dichloropropane
11 Not Detected 38 Not Detected1,4-Dioxane
2.7 Not Detected 18 Not DetectedBromodichloromethane
2.7 Not Detected 12 Not Detectedcis-1,3-Dichloropropene
2.7 Not Detected 11 Not Detected4-Methyl-2-pentanone
2.7 26 10 97Toluene
2.7 Not Detected 12 Not Detectedtrans-1,3-Dichloropropene
2.7 Not Detected 14 Not Detected1,1,2-Trichloroethane
2.7 Not Detected 18 Not DetectedTetrachloroethene
11 Not Detected 44 Not Detected2-Hexanone
Page 11 of 34
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Client Sample ID: SG-2
Lab ID#: 2207268-02A
EPA METHOD TO-15 GC/MS FULL SCAN
p071418File Name:
Dil. Factor:5.33
Date of Collection: 7/5/22 12:00:00 PM
Date of Analysis: 7/14/22 09:54 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
2.7 Not Detected 23 Not DetectedDibromochloromethane
2.7 Not Detected 20 Not Detected1,2-Dibromoethane (EDB)
2.7 Not Detected 12 Not DetectedChlorobenzene
2.7 7.6 12 33Ethyl Benzene
2.7 9.7 12 42m,p-Xylene
2.7 3.7 12 16o-Xylene
2.7 Not Detected 11 Not DetectedStyrene
2.7 Not Detected 28 Not DetectedBromoform
2.7 3.9 13 19Cumene
2.7 Not Detected 18 Not Detected1,1,2,2-Tetrachloroethane
2.7 12 13 61Propylbenzene
2.7 7.2 13 354-Ethyltoluene
2.7 21 13 1001,3,5-Trimethylbenzene
2.7 13 13 621,2,4-Trimethylbenzene
2.7 Not Detected 16 Not Detected1,3-Dichlorobenzene
2.7 Not Detected 16 Not Detected1,4-Dichlorobenzene
2.7 Not Detected 14 Not Detectedalpha-Chlorotoluene
2.7 Not Detected 16 Not Detected1,2-Dichlorobenzene
11 Not Detected 79 Not Detected1,2,4-Trichlorobenzene
11 Not Detected 110 Not DetectedHexachlorobutadiene
5.3 Not Detected 28 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
116 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 12 of 34
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Client Sample ID: SG-3
Lab ID#: 2207268-03A
EPA METHOD TO-15 GC/MS FULL SCAN
p071419File Name:
Dil. Factor:2.43
Date of Collection: 7/5/22 12:20:00 PM
Date of Analysis: 7/14/22 10:24 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 6.0 Not DetectedFreon 12
1.2 Not Detected 8.5 Not DetectedFreon 114
12 Not Detected 25 Not DetectedChloromethane
1.2 Not Detected 3.1 Not DetectedVinyl Chloride
1.2 Not Detected 2.7 Not Detected1,3-Butadiene
12 Not Detected 47 Not DetectedBromomethane
4.9 Not Detected 13 Not DetectedChloroethane
1.2 Not Detected 6.8 Not DetectedFreon 11
12 19 23 35Ethanol
1.2 Not Detected 9.3 Not DetectedFreon 113
1.2 Not Detected 4.8 Not Detected1,1-Dichloroethene
12 67 29 160Acetone
4.9 8.0 12 202-Propanol
4.9 Not Detected 15 Not DetectedCarbon Disulfide
4.9 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 42 Not DetectedMethylene Chloride
4.9 Not Detected 18 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.8 Not Detectedtrans-1,2-Dichloroethene
1.2 Not Detected 4.3 Not DetectedHexane
1.2 Not Detected 4.9 Not Detected1,1-Dichloroethane
4.9 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.8 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.6 Not DetectedTetrahydrofuran
1.2 Not Detected 5.9 Not DetectedChloroform
1.2 Not Detected 6.6 Not Detected1,1,1-Trichloroethane
1.2 Not Detected 4.2 Not DetectedCyclohexane
1.2 Not Detected 7.6 Not DetectedCarbon Tetrachloride
1.2 Not Detected 5.7 Not Detected2,2,4-Trimethylpentane
1.2 Not Detected 3.9 Not DetectedBenzene
1.2 Not Detected 4.9 Not Detected1,2-Dichloroethane
1.2 Not Detected 5.0 Not DetectedHeptane
1.2 Not Detected 6.5 Not DetectedTrichloroethene
1.2 Not Detected 5.6 Not Detected1,2-Dichloropropane
4.9 Not Detected 18 Not Detected1,4-Dioxane
1.2 Not Detected 8.1 Not DetectedBromodichloromethane
1.2 Not Detected 5.5 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 5.0 Not Detected4-Methyl-2-pentanone
1.2 Not Detected 4.6 Not DetectedToluene
1.2 Not Detected 5.5 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.6 Not Detected1,1,2-Trichloroethane
1.2 4.5 8.2 31Tetrachloroethene
4.9 Not Detected 20 Not Detected2-Hexanone
Page 13 of 34
Page 18 of 40 7/19/2022
1
2
3
4
5
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7
Client Sample ID: SG-3
Lab ID#: 2207268-03A
EPA METHOD TO-15 GC/MS FULL SCAN
p071419File Name:
Dil. Factor:2.43
Date of Collection: 7/5/22 12:20:00 PM
Date of Analysis: 7/14/22 10:24 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.3 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.6 Not DetectedChlorobenzene
1.2 Not Detected 5.3 Not DetectedEthyl Benzene
1.2 Not Detected 5.3 Not Detectedm,p-Xylene
1.2 Not Detected 5.3 Not Detectedo-Xylene
1.2 Not Detected 5.2 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 Not Detected 6.0 Not DetectedCumene
1.2 Not Detected 8.3 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 6.0 Not DetectedPropylbenzene
1.2 Not Detected 6.0 Not Detected4-Ethyltoluene
1.2 Not Detected 6.0 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 6.0 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.3 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.3 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.3 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.3 Not Detected1,2-Dichlorobenzene
4.9 Not Detected 36 Not Detected1,2,4-Trichlorobenzene
4.9 Not Detected 52 Not DetectedHexachlorobutadiene
2.4 Not Detected 13 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 14 of 34
Page 19 of 40 7/19/2022
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2
3
4
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7
Client Sample ID: SG-4
Lab ID#: 2207268-04A
EPA METHOD TO-15 GC/MS FULL SCAN
p071421File Name:
Dil. Factor:2.42
Date of Collection: 7/5/22 12:50:00 PM
Date of Analysis: 7/14/22 11:23 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 6.0 Not DetectedFreon 12
1.2 Not Detected 8.4 Not DetectedFreon 114
12 Not Detected 25 Not DetectedChloromethane
1.2 Not Detected 3.1 Not DetectedVinyl Chloride
1.2 Not Detected 2.7 Not Detected1,3-Butadiene
12 Not Detected 47 Not DetectedBromomethane
4.8 Not Detected 13 Not DetectedChloroethane
1.2 Not Detected 6.8 Not DetectedFreon 11
12 24 23 45Ethanol
1.2 Not Detected 9.3 Not DetectedFreon 113
1.2 Not Detected 4.8 Not Detected1,1-Dichloroethene
12 75 29 180Acetone
4.8 13 12 322-Propanol
4.8 Not Detected 15 Not DetectedCarbon Disulfide
4.8 Not Detected 15 Not Detected3-Chloropropene
12 Not Detected 42 Not DetectedMethylene Chloride
4.8 Not Detected 17 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.8 Not Detectedtrans-1,2-Dichloroethene
1.2 11 4.3 38Hexane
1.2 Not Detected 4.9 Not Detected1,1-Dichloroethane
4.8 Not Detected 14 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.8 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.6 Not DetectedTetrahydrofuran
1.2 Not Detected 5.9 Not DetectedChloroform
1.2 Not Detected 6.6 Not Detected1,1,1-Trichloroethane
1.2 27 4.2 94Cyclohexane
1.2 Not Detected 7.6 Not DetectedCarbon Tetrachloride
1.2 120 5.6 5802,2,4-Trimethylpentane
1.2 1.9 3.9 6.1Benzene
1.2 Not Detected 4.9 Not Detected1,2-Dichloroethane
1.2 4.5 5.0 18Heptane
1.2 Not Detected 6.5 Not DetectedTrichloroethene
1.2 Not Detected 5.6 Not Detected1,2-Dichloropropane
4.8 Not Detected 17 Not Detected1,4-Dioxane
1.2 Not Detected 8.1 Not DetectedBromodichloromethane
1.2 Not Detected 5.5 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 5.0 Not Detected4-Methyl-2-pentanone
1.2 2.5 4.6 9.4Toluene
1.2 Not Detected 5.5 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.6 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 8.2 Not DetectedTetrachloroethene
4.8 Not Detected 20 Not Detected2-Hexanone
Page 15 of 34
Page 20 of 40 7/19/2022
1
2
3
4
5
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Client Sample ID: SG-4
Lab ID#: 2207268-04A
EPA METHOD TO-15 GC/MS FULL SCAN
p071421File Name:
Dil. Factor:2.42
Date of Collection: 7/5/22 12:50:00 PM
Date of Analysis: 7/14/22 11:23 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 10 Not DetectedDibromochloromethane
1.2 Not Detected 9.3 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.6 Not DetectedChlorobenzene
1.2 Not Detected 5.2 Not DetectedEthyl Benzene
1.2 1.3 5.2 5.6m,p-Xylene
1.2 Not Detected 5.2 Not Detectedo-Xylene
1.2 Not Detected 5.2 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 Not Detected 5.9 Not DetectedCumene
1.2 Not Detected 8.3 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 5.9 Not DetectedPropylbenzene
1.2 Not Detected 5.9 Not Detected4-Ethyltoluene
1.2 Not Detected 5.9 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 5.9 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.3 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.3 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.3 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.3 Not Detected1,2-Dichlorobenzene
4.8 Not Detected 36 Not Detected1,2,4-Trichlorobenzene
4.8 Not Detected 52 Not DetectedHexachlorobutadiene
2.4 Not Detected 13 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 16 of 34
Page 21 of 40 7/19/2022
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2
3
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Client Sample ID: SG-5
Lab ID#: 2207268-05A
EPA METHOD TO-15 GC/MS FULL SCAN
p071422File Name:
Dil. Factor:2.32
Date of Collection: 7/5/22 3:20:00 PM
Date of Analysis: 7/14/22 11:52 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.7 Not DetectedFreon 12
1.2 Not Detected 8.1 Not DetectedFreon 114
12 Not Detected 24 Not DetectedChloromethane
1.2 Not Detected 3.0 Not DetectedVinyl Chloride
1.2 Not Detected 2.6 Not Detected1,3-Butadiene
12 Not Detected 45 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.2 Not Detected 6.5 Not DetectedFreon 11
12 18 22 34Ethanol
1.2 Not Detected 8.9 Not DetectedFreon 113
1.2 Not Detected 4.6 Not Detected1,1-Dichloroethene
12 110 28 270Acetone
4.6 14 11 342-Propanol
4.6 7.2 14 22Carbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
12 Not Detected 40 Not DetectedMethylene Chloride
4.6 Not Detected 17 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.6 Not Detectedtrans-1,2-Dichloroethene
1.2 31 4.1 110Hexane
1.2 Not Detected 4.7 Not Detected1,1-Dichloroethane
4.6 4.9 14 142-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.6 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.4 Not DetectedTetrahydrofuran
1.2 Not Detected 5.7 Not DetectedChloroform
1.2 Not Detected 6.3 Not Detected1,1,1-Trichloroethane
1.2 14 4.0 47Cyclohexane
1.2 Not Detected 7.3 Not DetectedCarbon Tetrachloride
1.2 4.6 5.4 212,2,4-Trimethylpentane
1.2 2.1 3.7 6.8Benzene
1.2 Not Detected 4.7 Not Detected1,2-Dichloroethane
1.2 15 4.8 61Heptane
1.2 Not Detected 6.2 Not DetectedTrichloroethene
1.2 Not Detected 5.4 Not Detected1,2-Dichloropropane
4.6 Not Detected 17 Not Detected1,4-Dioxane
1.2 Not Detected 7.8 Not DetectedBromodichloromethane
1.2 Not Detected 5.3 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 4.8 Not Detected4-Methyl-2-pentanone
1.2 4.9 4.4 18Toluene
1.2 Not Detected 5.3 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.3 Not Detected1,1,2-Trichloroethane
1.2 Not Detected 7.9 Not DetectedTetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 17 of 34
Page 22 of 40 7/19/2022
1
2
3
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7
Client Sample ID: SG-5
Lab ID#: 2207268-05A
EPA METHOD TO-15 GC/MS FULL SCAN
p071422File Name:
Dil. Factor:2.32
Date of Collection: 7/5/22 3:20:00 PM
Date of Analysis: 7/14/22 11:52 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 9.9 Not DetectedDibromochloromethane
1.2 Not Detected 8.9 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.3 Not DetectedChlorobenzene
1.2 1.2 5.0 5.4Ethyl Benzene
1.2 2.7 5.0 12m,p-Xylene
1.2 1.2 5.0 5.1o-Xylene
1.2 Not Detected 4.9 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 Not Detected 5.7 Not DetectedCumene
1.2 Not Detected 8.0 Not Detected1,1,2,2-Tetrachloroethane
1.2 Not Detected 5.7 Not DetectedPropylbenzene
1.2 Not Detected 5.7 Not Detected4-Ethyltoluene
1.2 Not Detected 5.7 Not Detected1,3,5-Trimethylbenzene
1.2 Not Detected 5.7 Not Detected1,2,4-Trimethylbenzene
1.2 Not Detected 7.0 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 7.0 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.0 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 7.0 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
2.3 Not Detected 12 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
97 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 18 of 34
Page 23 of 40 7/19/2022
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2
3
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Client Sample ID: SG-6
Lab ID#: 2207268-06A
EPA METHOD TO-15 GC/MS FULL SCAN
p071423File Name:
Dil. Factor:2.21
Date of Collection: 7/5/22 3:45:00 PM
Date of Analysis: 7/15/22 12:22 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.5 Not DetectedFreon 12
1.1 Not Detected 7.7 Not DetectedFreon 114
11 Not Detected 23 Not DetectedChloromethane
1.1 Not Detected 2.8 Not DetectedVinyl Chloride
1.1 Not Detected 2.4 Not Detected1,3-Butadiene
11 Not Detected 43 Not DetectedBromomethane
4.4 Not Detected 12 Not DetectedChloroethane
1.1 Not Detected 6.2 Not DetectedFreon 11
11 23 21 43Ethanol
1.1 Not Detected 8.5 Not DetectedFreon 113
1.1 Not Detected 4.4 Not Detected1,1-Dichloroethene
11 60 26 140Acetone
4.4 8.5 11 212-Propanol
4.4 20 14 61Carbon Disulfide
4.4 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 38 Not DetectedMethylene Chloride
4.4 Not Detected 16 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.4 Not Detectedtrans-1,2-Dichloroethene
1.1 1.1 3.9 4.0Hexane
1.1 Not Detected 4.5 Not Detected1,1-Dichloroethane
4.4 Not Detected 13 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.4 Not Detectedcis-1,2-Dichloroethene
1.1 Not Detected 3.2 Not DetectedTetrahydrofuran
1.1 Not Detected 5.4 Not DetectedChloroform
1.1 Not Detected 6.0 Not Detected1,1,1-Trichloroethane
1.1 Not Detected 3.8 Not DetectedCyclohexane
1.1 Not Detected 7.0 Not DetectedCarbon Tetrachloride
1.1 Not Detected 5.2 Not Detected2,2,4-Trimethylpentane
1.1 Not Detected 3.5 Not DetectedBenzene
1.1 Not Detected 4.5 Not Detected1,2-Dichloroethane
1.1 Not Detected 4.5 Not DetectedHeptane
1.1 Not Detected 5.9 Not DetectedTrichloroethene
1.1 Not Detected 5.1 Not Detected1,2-Dichloropropane
4.4 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.4 Not DetectedBromodichloromethane
1.1 Not Detected 5.0 Not Detectedcis-1,3-Dichloropropene
1.1 Not Detected 4.5 Not Detected4-Methyl-2-pentanone
1.1 1.3 4.2 4.8Toluene
1.1 Not Detected 5.0 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 6.0 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.5 Not DetectedTetrachloroethene
4.4 Not Detected 18 Not Detected2-Hexanone
Page 19 of 34
Page 24 of 40 7/19/2022
1
2
3
4
5
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7
Client Sample ID: SG-6
Lab ID#: 2207268-06A
EPA METHOD TO-15 GC/MS FULL SCAN
p071423File Name:
Dil. Factor:2.21
Date of Collection: 7/5/22 3:45:00 PM
Date of Analysis: 7/15/22 12:22 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.4 Not DetectedDibromochloromethane
1.1 Not Detected 8.5 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.1 Not DetectedChlorobenzene
1.1 Not Detected 4.8 Not DetectedEthyl Benzene
1.1 Not Detected 4.8 Not Detectedm,p-Xylene
1.1 Not Detected 4.8 Not Detectedo-Xylene
1.1 Not Detected 4.7 Not DetectedStyrene
1.1 Not Detected 11 Not DetectedBromoform
1.1 Not Detected 5.4 Not DetectedCumene
1.1 Not Detected 7.6 Not Detected1,1,2,2-Tetrachloroethane
1.1 Not Detected 5.4 Not DetectedPropylbenzene
1.1 Not Detected 5.4 Not Detected4-Ethyltoluene
1.1 Not Detected 5.4 Not Detected1,3,5-Trimethylbenzene
1.1 Not Detected 5.4 Not Detected1,2,4-Trimethylbenzene
1.1 Not Detected 6.6 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.6 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.7 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.6 Not Detected1,2-Dichlorobenzene
4.4 Not Detected 33 Not Detected1,2,4-Trichlorobenzene
4.4 Not Detected 47 Not DetectedHexachlorobutadiene
2.2 Not Detected 12 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
107 70-1304-Bromofluorobenzene
Page 20 of 34
Page 25 of 40 7/19/2022
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2
3
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Client Sample ID: SG-7
Lab ID#: 2207268-07A
EPA METHOD TO-15 GC/MS FULL SCAN
p071424File Name:
Dil. Factor:2.27
Date of Collection: 7/5/22 4:15:00 PM
Date of Analysis: 7/15/22 12:52 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 5.6 Not DetectedFreon 12
1.1 Not Detected 7.9 Not DetectedFreon 114
11 Not Detected 23 Not DetectedChloromethane
1.1 Not Detected 2.9 Not DetectedVinyl Chloride
1.1 Not Detected 2.5 Not Detected1,3-Butadiene
11 Not Detected 44 Not DetectedBromomethane
4.5 Not Detected 12 Not DetectedChloroethane
1.1 Not Detected 6.4 Not DetectedFreon 11
11 18 21 35Ethanol
1.1 Not Detected 8.7 Not DetectedFreon 113
1.1 Not Detected 4.5 Not Detected1,1-Dichloroethene
11 41 27 97Acetone
4.5 6.5 11 162-Propanol
4.5 9.6 14 30Carbon Disulfide
4.5 Not Detected 14 Not Detected3-Chloropropene
11 Not Detected 39 Not DetectedMethylene Chloride
4.5 Not Detected 16 Not DetectedMethyl tert-butyl ether
1.1 Not Detected 4.5 Not Detectedtrans-1,2-Dichloroethene
1.1 Not Detected 4.0 Not DetectedHexane
1.1 Not Detected 4.6 Not Detected1,1-Dichloroethane
4.5 Not Detected 13 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.1 Not Detected 4.5 Not Detectedcis-1,2-Dichloroethene
1.1 Not Detected 3.3 Not DetectedTetrahydrofuran
1.1 Not Detected 5.5 Not DetectedChloroform
1.1 Not Detected 6.2 Not Detected1,1,1-Trichloroethane
1.1 2.4 3.9 8.2Cyclohexane
1.1 Not Detected 7.1 Not DetectedCarbon Tetrachloride
1.1 Not Detected 5.3 Not Detected2,2,4-Trimethylpentane
1.1 Not Detected 3.6 Not DetectedBenzene
1.1 Not Detected 4.6 Not Detected1,2-Dichloroethane
1.1 Not Detected 4.6 Not DetectedHeptane
1.1 Not Detected 6.1 Not DetectedTrichloroethene
1.1 Not Detected 5.2 Not Detected1,2-Dichloropropane
4.5 Not Detected 16 Not Detected1,4-Dioxane
1.1 Not Detected 7.6 Not DetectedBromodichloromethane
1.1 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.1 Not Detected 4.6 Not Detected4-Methyl-2-pentanone
1.1 1.2 4.3 4.7Toluene
1.1 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.1 Not Detected 6.2 Not Detected1,1,2-Trichloroethane
1.1 Not Detected 7.7 Not DetectedTetrachloroethene
4.5 Not Detected 18 Not Detected2-Hexanone
Page 21 of 34
Page 26 of 40 7/19/2022
1
2
3
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7
Client Sample ID: SG-7
Lab ID#: 2207268-07A
EPA METHOD TO-15 GC/MS FULL SCAN
p071424File Name:
Dil. Factor:2.27
Date of Collection: 7/5/22 4:15:00 PM
Date of Analysis: 7/15/22 12:52 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.1 Not Detected 9.7 Not DetectedDibromochloromethane
1.1 Not Detected 8.7 Not Detected1,2-Dibromoethane (EDB)
1.1 Not Detected 5.2 Not DetectedChlorobenzene
1.1 Not Detected 4.9 Not DetectedEthyl Benzene
1.1 Not Detected 4.9 Not Detectedm,p-Xylene
1.1 Not Detected 4.9 Not Detectedo-Xylene
1.1 Not Detected 4.8 Not DetectedStyrene
1.1 Not Detected 12 Not DetectedBromoform
1.1 Not Detected 5.6 Not DetectedCumene
1.1 Not Detected 7.8 Not Detected1,1,2,2-Tetrachloroethane
1.1 Not Detected 5.6 Not DetectedPropylbenzene
1.1 Not Detected 5.6 Not Detected4-Ethyltoluene
1.1 Not Detected 5.6 Not Detected1,3,5-Trimethylbenzene
1.1 Not Detected 5.6 Not Detected1,2,4-Trimethylbenzene
1.1 Not Detected 6.8 Not Detected1,3-Dichlorobenzene
1.1 Not Detected 6.8 Not Detected1,4-Dichlorobenzene
1.1 Not Detected 5.9 Not Detectedalpha-Chlorotoluene
1.1 Not Detected 6.8 Not Detected1,2-Dichlorobenzene
4.5 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.5 Not Detected 48 Not DetectedHexachlorobutadiene
2.3 Not Detected 12 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
104 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 22 of 34
Page 27 of 40 7/19/2022
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2
3
4
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7
Client Sample ID: SG-8
Lab ID#: 2207268-08A
EPA METHOD TO-15 GC/MS FULL SCAN
p071425File Name:
Dil. Factor:2.52
Date of Collection: 7/5/22 4:40:00 PM
Date of Analysis: 7/15/22 01:21 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 6.2 Not DetectedFreon 12
1.3 Not Detected 8.8 Not DetectedFreon 114
13 Not Detected 26 Not DetectedChloromethane
1.3 Not Detected 3.2 Not DetectedVinyl Chloride
1.3 Not Detected 2.8 Not Detected1,3-Butadiene
13 Not Detected 49 Not DetectedBromomethane
5.0 Not Detected 13 Not DetectedChloroethane
1.3 Not Detected 7.1 Not DetectedFreon 11
13 20 24 38Ethanol
1.3 Not Detected 9.6 Not DetectedFreon 113
1.3 Not Detected 5.0 Not Detected1,1-Dichloroethene
13 58 30 140Acetone
5.0 10 12 252-Propanol
5.0 12 16 36Carbon Disulfide
5.0 Not Detected 16 Not Detected3-Chloropropene
13 Not Detected 44 Not DetectedMethylene Chloride
5.0 Not Detected 18 Not DetectedMethyl tert-butyl ether
1.3 Not Detected 5.0 Not Detectedtrans-1,2-Dichloroethene
1.3 Not Detected 4.4 Not DetectedHexane
1.3 Not Detected 5.1 Not Detected1,1-Dichloroethane
5.0 Not Detected 15 Not Detected2-Butanone (Methyl Ethyl Ketone)
1.3 Not Detected 5.0 Not Detectedcis-1,2-Dichloroethene
1.3 Not Detected 3.7 Not DetectedTetrahydrofuran
1.3 Not Detected 6.2 Not DetectedChloroform
1.3 Not Detected 6.9 Not Detected1,1,1-Trichloroethane
1.3 3.1 4.3 11Cyclohexane
1.3 Not Detected 7.9 Not DetectedCarbon Tetrachloride
1.3 Not Detected 5.9 Not Detected2,2,4-Trimethylpentane
1.3 Not Detected 4.0 Not DetectedBenzene
1.3 Not Detected 5.1 Not Detected1,2-Dichloroethane
1.3 Not Detected 5.2 Not DetectedHeptane
1.3 Not Detected 6.8 Not DetectedTrichloroethene
1.3 Not Detected 5.8 Not Detected1,2-Dichloropropane
5.0 Not Detected 18 Not Detected1,4-Dioxane
1.3 Not Detected 8.4 Not DetectedBromodichloromethane
1.3 Not Detected 5.7 Not Detectedcis-1,3-Dichloropropene
1.3 Not Detected 5.2 Not Detected4-Methyl-2-pentanone
1.3 1.9 4.7 7.2Toluene
1.3 Not Detected 5.7 Not Detectedtrans-1,3-Dichloropropene
1.3 Not Detected 6.9 Not Detected1,1,2-Trichloroethane
1.3 Not Detected 8.5 Not DetectedTetrachloroethene
5.0 Not Detected 21 Not Detected2-Hexanone
Page 23 of 34
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Client Sample ID: SG-8
Lab ID#: 2207268-08A
EPA METHOD TO-15 GC/MS FULL SCAN
p071425File Name:
Dil. Factor:2.52
Date of Collection: 7/5/22 4:40:00 PM
Date of Analysis: 7/15/22 01:21 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.3 Not Detected 11 Not DetectedDibromochloromethane
1.3 Not Detected 9.7 Not Detected1,2-Dibromoethane (EDB)
1.3 Not Detected 5.8 Not DetectedChlorobenzene
1.3 Not Detected 5.5 Not DetectedEthyl Benzene
1.3 Not Detected 5.5 Not Detectedm,p-Xylene
1.3 Not Detected 5.5 Not Detectedo-Xylene
1.3 Not Detected 5.4 Not DetectedStyrene
1.3 Not Detected 13 Not DetectedBromoform
1.3 Not Detected 6.2 Not DetectedCumene
1.3 Not Detected 8.6 Not Detected1,1,2,2-Tetrachloroethane
1.3 Not Detected 6.2 Not DetectedPropylbenzene
1.3 Not Detected 6.2 Not Detected4-Ethyltoluene
1.3 Not Detected 6.2 Not Detected1,3,5-Trimethylbenzene
1.3 Not Detected 6.2 Not Detected1,2,4-Trimethylbenzene
1.3 Not Detected 7.6 Not Detected1,3-Dichlorobenzene
1.3 Not Detected 7.6 Not Detected1,4-Dichlorobenzene
1.3 Not Detected 6.5 Not Detectedalpha-Chlorotoluene
1.3 Not Detected 7.6 Not Detected1,2-Dichlorobenzene
5.0 Not Detected 37 Not Detected1,2,4-Trichlorobenzene
5.0 Not Detected 54 Not DetectedHexachlorobutadiene
2.5 Not Detected 13 Not DetectedNaphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
101 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 24 of 34
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Client Sample ID: Duplicate
Lab ID#: 2207268-09A
EPA METHOD TO-15 GC/MS FULL SCAN
p071416File Name:
Dil. Factor:2.31
Date of Collection: 7/5/22 11:25:00 AM
Date of Analysis: 7/14/22 06:57 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.7 Not DetectedFreon 12
1.2 Not Detected 8.1 Not DetectedFreon 114
12 Not Detected 24 Not DetectedChloromethane
1.2 Not Detected 3.0 Not DetectedVinyl Chloride
1.2 Not Detected 2.6 Not Detected1,3-Butadiene
12 Not Detected 45 Not DetectedBromomethane
4.6 Not Detected 12 Not DetectedChloroethane
1.2 Not Detected 6.5 Not DetectedFreon 11
12 20 22 38Ethanol
1.2 Not Detected 8.8 Not DetectedFreon 113
1.2 Not Detected 4.6 Not Detected1,1-Dichloroethene
12 62 27 150Acetone
4.6 9.0 11 222-Propanol
4.6 Not Detected 14 Not DetectedCarbon Disulfide
4.6 Not Detected 14 Not Detected3-Chloropropene
12 Not Detected 40 Not DetectedMethylene Chloride
4.6 Not Detected 17 Not DetectedMethyl tert-butyl ether
1.2 Not Detected 4.6 Not Detectedtrans-1,2-Dichloroethene
1.2 7.9 4.1 28Hexane
1.2 Not Detected 4.7 Not Detected1,1-Dichloroethane
4.6 5.4 14 162-Butanone (Methyl Ethyl Ketone)
1.2 Not Detected 4.6 Not Detectedcis-1,2-Dichloroethene
1.2 Not Detected 3.4 Not DetectedTetrahydrofuran
1.2 Not Detected 5.6 Not DetectedChloroform
1.2 Not Detected 6.3 Not Detected1,1,1-Trichloroethane
1.2 54 4.0 180Cyclohexane
1.2 Not Detected 7.3 Not DetectedCarbon Tetrachloride
1.2 3.6 5.4 172,2,4-Trimethylpentane
1.2 17 3.7 54Benzene
1.2 Not Detected 4.7 Not Detected1,2-Dichloroethane
1.2 1.7 4.7 6.9Heptane
1.2 Not Detected 6.2 Not DetectedTrichloroethene
1.2 Not Detected 5.3 Not Detected1,2-Dichloropropane
4.6 Not Detected 17 Not Detected1,4-Dioxane
1.2 Not Detected 7.7 Not DetectedBromodichloromethane
1.2 Not Detected 5.2 Not Detectedcis-1,3-Dichloropropene
1.2 Not Detected 4.7 Not Detected4-Methyl-2-pentanone
1.2 22 4.4 82Toluene
1.2 Not Detected 5.2 Not Detectedtrans-1,3-Dichloropropene
1.2 Not Detected 6.3 Not Detected1,1,2-Trichloroethane
1.2 1.2 7.8 8.4Tetrachloroethene
4.6 Not Detected 19 Not Detected2-Hexanone
Page 25 of 34
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Client Sample ID: Duplicate
Lab ID#: 2207268-09A
EPA METHOD TO-15 GC/MS FULL SCAN
p071416File Name:
Dil. Factor:2.31
Date of Collection: 7/5/22 11:25:00 AM
Date of Analysis: 7/14/22 06:57 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 9.8 Not DetectedDibromochloromethane
1.2 Not Detected 8.9 Not Detected1,2-Dibromoethane (EDB)
1.2 Not Detected 5.3 Not DetectedChlorobenzene
1.2 26 5.0 110Ethyl Benzene
1.2 14 5.0 63m,p-Xylene
1.2 8.5 5.0 37o-Xylene
1.2 Not Detected 4.9 Not DetectedStyrene
1.2 Not Detected 12 Not DetectedBromoform
1.2 2.0 5.7 10Cumene
1.2 Not Detected 7.9 Not Detected1,1,2,2-Tetrachloroethane
1.2 4.7 5.7 23Propylbenzene
1.2 6.6 5.7 324-Ethyltoluene
1.2 12 5.7 571,3,5-Trimethylbenzene
1.2 26 5.7 1301,2,4-Trimethylbenzene
1.2 Not Detected 6.9 Not Detected1,3-Dichlorobenzene
1.2 Not Detected 6.9 Not Detected1,4-Dichlorobenzene
1.2 Not Detected 6.0 Not Detectedalpha-Chlorotoluene
1.2 Not Detected 6.9 Not Detected1,2-Dichlorobenzene
4.6 Not Detected 34 Not Detected1,2,4-Trichlorobenzene
4.6 Not Detected 49 Not DetectedHexachlorobutadiene
2.3 4.7 12 25Naphthalene
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
101 70-1304-Bromofluorobenzene
Page 26 of 34
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Client Sample ID: Lab Blank
Lab ID#: 2207268-10A
EPA METHOD TO-15 GC/MS FULL SCAN
p071406File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 01:06 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
5.0 Not Detected 9.4 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
2.0 Not Detected 7.2 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 27 of 34
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Client Sample ID: Lab Blank
Lab ID#: 2207268-10A
EPA METHOD TO-15 GC/MS FULL SCAN
p071406File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 01:06 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene
2.0 Not Detected 21 Not DetectedHexachlorobutadiene
1.0 Not Detected 5.2 Not DetectedNaphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
100 70-1304-Bromofluorobenzene
Page 28 of 34
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Client Sample ID: CCV
Lab ID#: 2207268-11A
EPA METHOD TO-15 GC/MS FULL SCAN
p071402File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 10:14 AM
%RecoveryCompound
102Freon 12
102Freon 114
119Chloromethane
90Vinyl Chloride
941,3-Butadiene
93Bromomethane
96Chloroethane
102Freon 11
101Ethanol
97Freon 113
1021,1-Dichloroethene
93Acetone
1022-Propanol
99Carbon Disulfide
1043-Chloropropene
102Methylene Chloride
102Methyl tert-butyl ether
99trans-1,2-Dichloroethene
102Hexane
1051,1-Dichloroethane
1002-Butanone (Methyl Ethyl Ketone)
106cis-1,2-Dichloroethene
104Tetrahydrofuran
104Chloroform
1031,1,1-Trichloroethane
103Cyclohexane
110Carbon Tetrachloride
1082,2,4-Trimethylpentane
100Benzene
1071,2-Dichloroethane
110Heptane
104Trichloroethene
971,2-Dichloropropane
1011,4-Dioxane
107Bromodichloromethane
105cis-1,3-Dichloropropene
1024-Methyl-2-pentanone
104Toluene
104trans-1,3-Dichloropropene
991,1,2-Trichloroethane
102Tetrachloroethene
1032-Hexanone
Page 29 of 34
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Client Sample ID: CCV
Lab ID#: 2207268-11A
EPA METHOD TO-15 GC/MS FULL SCAN
p071402File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 10:14 AM
%RecoveryCompound
104Dibromochloromethane
1021,2-Dibromoethane (EDB)
101Chlorobenzene
106Ethyl Benzene
105m,p-Xylene
105o-Xylene
110Styrene
102Bromoform
112Cumene
991,1,2,2-Tetrachloroethane
108Propylbenzene
1114-Ethyltoluene
1101,3,5-Trimethylbenzene
1181,2,4-Trimethylbenzene
1071,3-Dichlorobenzene
1061,4-Dichlorobenzene
110alpha-Chlorotoluene
1071,2-Dichlorobenzene
1001,2,4-Trichlorobenzene
101Hexachlorobutadiene
98Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
104 70-1301,2-Dichloroethane-d4
109 70-1304-Bromofluorobenzene
Page 30 of 34
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Client Sample ID: LCS
Lab ID#: 2207268-12A
EPA METHOD TO-15 GC/MS FULL SCAN
p071403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 10:40 AM
Limits%RecoveryCompound
Method
97 70-130Freon 12
79 70-130Freon 114
116 70-130Chloromethane
83 70-130Vinyl Chloride
93 70-1301,3-Butadiene
88 70-130Bromomethane
97 70-130Chloroethane
96 70-130Freon 11
93 70-130Ethanol
93 70-130Freon 113
93 70-1301,1-Dichloroethene
89 70-130Acetone
104 70-1302-Propanol
94 70-130Carbon Disulfide
101 70-1303-Chloropropene
92 70-130Methylene Chloride
100 70-130Methyl tert-butyl ether
94 70-130trans-1,2-Dichloroethene
99 70-130Hexane
99 70-1301,1-Dichloroethane
97 70-1302-Butanone (Methyl Ethyl Ketone)
101 70-130cis-1,2-Dichloroethene
100 70-130Tetrahydrofuran
96 70-130Chloroform
100 70-1301,1,1-Trichloroethane
103 70-130Cyclohexane
105 70-130Carbon Tetrachloride
106 70-1302,2,4-Trimethylpentane
99 70-130Benzene
103 70-1301,2-Dichloroethane
109 70-130Heptane
101 70-130Trichloroethene
95 70-1301,2-Dichloropropane
100 70-1301,4-Dioxane
99 70-130Bromodichloromethane
103 70-130cis-1,3-Dichloropropene
104 70-1304-Methyl-2-pentanone
100 70-130Toluene
104 70-130trans-1,3-Dichloropropene
99 70-1301,1,2-Trichloroethane
103 70-130Tetrachloroethene
105 70-1302-Hexanone
Page 31 of 34
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Client Sample ID: LCS
Lab ID#: 2207268-12A
EPA METHOD TO-15 GC/MS FULL SCAN
p071403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 10:40 AM
Limits%RecoveryCompound
Method
103 70-130Dibromochloromethane
100 70-1301,2-Dibromoethane (EDB)
99 70-130Chlorobenzene
105 70-130Ethyl Benzene
106 70-130m,p-Xylene
105 70-130o-Xylene
109 70-130Styrene
102 70-130Bromoform
110 70-130Cumene
102 70-1301,1,2,2-Tetrachloroethane
107 70-130Propylbenzene
109 70-1304-Ethyltoluene
109 70-1301,3,5-Trimethylbenzene
115 70-1301,2,4-Trimethylbenzene
104 70-1301,3-Dichlorobenzene
102 70-1301,4-Dichlorobenzene
107 70-130alpha-Chlorotoluene
104 70-1301,2-Dichlorobenzene
84 70-1301,2,4-Trichlorobenzene
85 70-130Hexachlorobutadiene
80 60-140Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
102 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
106 70-1304-Bromofluorobenzene
Page 32 of 34
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Client Sample ID: LCSD
Lab ID#: 2207268-12AA
EPA METHOD TO-15 GC/MS FULL SCAN
p071404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 11:08 AM
Limits%RecoveryCompound
Method
97 70-130Freon 12
78 70-130Freon 114
115 70-130Chloromethane
84 70-130Vinyl Chloride
93 70-1301,3-Butadiene
86 70-130Bromomethane
94 70-130Chloroethane
94 70-130Freon 11
102 70-130Ethanol
91 70-130Freon 113
95 70-1301,1-Dichloroethene
91 70-130Acetone
105 70-1302-Propanol
94 70-130Carbon Disulfide
105 70-1303-Chloropropene
92 70-130Methylene Chloride
101 70-130Methyl tert-butyl ether
94 70-130trans-1,2-Dichloroethene
98 70-130Hexane
97 70-1301,1-Dichloroethane
99 70-1302-Butanone (Methyl Ethyl Ketone)
101 70-130cis-1,2-Dichloroethene
102 70-130Tetrahydrofuran
96 70-130Chloroform
98 70-1301,1,1-Trichloroethane
105 70-130Cyclohexane
104 70-130Carbon Tetrachloride
106 70-1302,2,4-Trimethylpentane
96 70-130Benzene
100 70-1301,2-Dichloroethane
107 70-130Heptane
98 70-130Trichloroethene
93 70-1301,2-Dichloropropane
97 70-1301,4-Dioxane
98 70-130Bromodichloromethane
102 70-130cis-1,3-Dichloropropene
102 70-1304-Methyl-2-pentanone
98 70-130Toluene
100 70-130trans-1,3-Dichloropropene
96 70-1301,1,2-Trichloroethane
98 70-130Tetrachloroethene
104 70-1302-Hexanone
Page 33 of 34
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Client Sample ID: LCSD
Lab ID#: 2207268-12AA
EPA METHOD TO-15 GC/MS FULL SCAN
p071404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/22 11:08 AM
Limits%RecoveryCompound
Method
101 70-130Dibromochloromethane
98 70-1301,2-Dibromoethane (EDB)
97 70-130Chlorobenzene
104 70-130Ethyl Benzene
105 70-130m,p-Xylene
103 70-130o-Xylene
106 70-130Styrene
100 70-130Bromoform
108 70-130Cumene
99 70-1301,1,2,2-Tetrachloroethane
104 70-130Propylbenzene
106 70-1304-Ethyltoluene
106 70-1301,3,5-Trimethylbenzene
112 70-1301,2,4-Trimethylbenzene
101 70-1301,3-Dichlorobenzene
98 70-1301,4-Dichlorobenzene
104 70-130alpha-Chlorotoluene
101 70-1301,2-Dichlorobenzene
100 70-1301,2,4-Trichlorobenzene
98 70-130Hexachlorobutadiene
99 60-140Naphthalene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
100 70-130Toluene-d8
101 70-1301,2-Dichloroethane-d4
105 70-1304-Bromofluorobenzene
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ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-217621-1
Client Project/Site: Greenhouse Project
For:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, North Carolina 27616
Attn: Michael Pfeifer
Authorized for release by:
7/14/2022 5:51:13 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Definitions/Glossary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1+Surrogate recovery exceeds control limits, high biased.
GC/MS Semi VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Lab Sample ID Client Sample ID Matrix Collected Received
680-217621-1 GW-1 (10-15)Soil 06/28/22 10:15 06/30/22 10:30
680-217621-2 GW-2 (11-14)Soil 06/28/22 12:05 06/30/22 10:30
680-217621-3 GW-3 (7-12)Soil 06/28/22 14:15 06/30/22 10:30
680-217621-4 GW-4 (13-17)Soil 06/29/22 10:15 06/30/22 10:30
680-217621-5 SS-1 (2-6)Soil 06/29/22 11:40 06/30/22 10:30
680-217621-6 SS-2 (2-6)Soil 06/29/22 13:00 06/30/22 10:30
680-217621-7 SS-3 (2-6)Soil 06/29/22 13:15 06/30/22 10:30
680-217621-8 SG-1 (2-6)Soil 06/29/22 11:50 06/30/22 10:30
680-217621-9 SG-2 (2-6)Soil 06/29/22 11:15 06/30/22 10:30
680-217621-10 SG-3 (2-6)Soil 06/29/22 13:05 06/30/22 10:30
680-217621-11 SG-4 (2-6)Soil 06/29/22 13:25 06/30/22 10:30
680-217621-12 SG-6 (2-6)Soil 06/29/22 13:45 06/30/22 10:30
680-217621-13 SG-7 (2-6)Soil 06/29/22 14:30 06/30/22 10:30
680-217621-14 SG-8 (2-6)Soil 06/29/22 14:15 06/30/22 10:30
680-217621-15 Soil Dup Soil 06/29/22 00:00 06/30/22 10:30
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Case Narrative
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Job ID: 680-217621-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-217621-1
Comments
No additional comments.
Receipt
The samples were received on 6/30/2022 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 3.9º C, 4.2º C and 4.5º C.
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-1Client Sample ID: GW-1 (10-15)
Matrix: SoilDate Collected: 06/28/22 10:15
Percent Solids: 62.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00715 0.00186 mg/Kg ☼07/05/22 15:31 07/08/22 21:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1,1-Trichloroethane ND
0.00715 0.00300 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1,2,2-Tetrachloroethane ND
0.00715 0.00415 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00715 0.00214 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1,2-Trichloroethane ND
0.00715 0.00415 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1-Dichloroethane ND
0.00715 0.00515 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1-Dichloroethene ND
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,1-Dichloropropene ND
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2,3-Trichlorobenzene ND
0.00715 0.00257 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2,3-Trichloropropane ND
0.00715 0.00357 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2,4-Trichlorobenzene ND
0.00715 0.00357 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2,4-Trimethylbenzene 0.0445
0.0143 0.00229 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2-Dibromo-3-Chloropropane ND
0.00715 0.00243 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2-Dichlorobenzene ND
0.00715 0.00329 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2-Dichloroethane ND
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,2-Dichloropropane ND
0.00715 0.00343 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,3,5-Trimethylbenzene 0.00823
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,3-Dichlorobenzene ND
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,3-Dichloropropane ND
0.00715 0.00257 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼1,4-Dichlorobenzene ND
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼2,2-Dichloropropane ND
0.0357 0.0132 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼2-Butanone (MEK)ND
0.00715 0.00329 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼2-Chlorotoluene ND
0.0357 0.0272 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼2-Hexanone ND
0.00715 0.00300 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼4-Chlorotoluene ND
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼4-Isopropyltoluene 0.00534 J
0.0357 0.0257 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼4-Methyl-2-pentanone (MIBK)ND
0.0715 0.0157 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Acetone 0.310 B
0.00715 0.00343 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Benzene 0.135
0.00715 0.00243 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Bromobenzene ND
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Bromoform ND
0.00715 0.00343 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Bromomethane ND
0.00715 0.00300 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Carbon disulfide ND
0.00715 0.00300 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Carbon tetrachloride ND
0.00715 0.00200 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chlorobenzene ND
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chlorobromomethane ND
0.00715 0.00300 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chlorodibromomethane ND
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chloroethane ND *+
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chloroform ND
0.00715 0.00343 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Chloromethane ND
0.00715 0.00415 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼cis-1,2-Dichloroethene ND
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼cis-1,3-Dichloropropene ND
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Dibromomethane ND
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Dichlorobromomethane ND
0.00715 0.00457 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Dichlorodifluoromethane ND
0.0143 0.0143 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Ethyl acetate ND
0.00715 0.00243 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Ethylene Dibromide ND
0.00715 0.00586 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Hexachlorobutadiene ND
0.00715 0.00243 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Iodomethane ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-1Client Sample ID: GW-1 (10-15)
Matrix: SoilDate Collected: 06/28/22 10:15
Percent Solids: 62.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Isopropyl ether ND 0.0143 0.00214 mg/Kg ☼07/05/22 15:31 07/08/22 21:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Isopropylbenzene 0.0227
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼m,p-Xylene 0.0319
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Methyl tert-butyl ether ND
0.0143 0.0114 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Methylene Chloride ND
0.00715 0.00272 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼n-Butylbenzene 0.0277
0.00715 0.00314 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼N-Propylbenzene 0.0873
0.00715 0.00286 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼sec-Butylbenzene 0.00797
0.00715 0.00272 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Styrene ND
0.00715 0.00357 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼tert-Butylbenzene ND
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Tetrachloroethene ND
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Toluene 0.195
0.00715 0.00329 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼trans-1,2-Dichloroethene ND
0.00715 0.00372 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼trans-1,3-Dichloropropene ND
0.0143 0.00343 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼trans-1,4-Dichloro-2-butene ND
0.00715 0.00257 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Trichloroethene ND
0.00715 0.00443 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Trichlorofluoromethane ND
0.0143 0.00786 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Vinyl acetate ND *+
0.00715 0.00400 mg/Kg 07/05/22 15:31 07/08/22 21:17 1☼Vinyl chloride ND
1,2-Dichloroethane-d4 (Surr)141 S1+65-130 07/05/22 15:31 07/08/22 21:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)73 07/05/22 15:31 07/08/22 21:17 165-130
Dibromofluoromethane (Surr)149 S1+07/05/22 15:31 07/08/22 21:17 165-130
Toluene-d8 (Surr)95 07/05/22 15:31 07/08/22 21:17 165-130
Method: 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
Ethylbenzene 2.37 0.288 0.121 mg/Kg ☼07/05/22 15:31 07/11/22 19:49 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.288 0.0980 mg/Kg 07/05/22 15:31 07/11/22 19:49 40☼Hexane 6.32
0.288 0.179 mg/Kg 07/05/22 15:31 07/11/22 19:49 40☼Naphthalene 2.21
0.288 0.248 mg/Kg 07/05/22 15:31 07/11/22 19:49 40☼n-Heptane 5.09
0.288 0.133 mg/Kg 07/05/22 15:31 07/11/22 19:49 40☼o-Xylene 1.46
0.576 0.207 mg/Kg 07/05/22 15:31 07/11/22 19:49 40☼Xylenes, Total 3.50
1,2-Dichloroethane-d4 (Surr)98 65-130 07/05/22 15:31 07/11/22 19:49 40
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 07/05/22 15:31 07/11/22 19:49 4065-130
Dibromofluoromethane (Surr)96 07/05/22 15:31 07/11/22 19:49 4065-130
Toluene-d8 (Surr)97 07/05/22 15:31 07/11/22 19:49 4065-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.69 2.69 mg/Kg ☼07/11/22 13:00 07/12/22 13:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.522 0.0553 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4,5-Trichlorophenol ND
0.522 0.0458 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4,6-Trichlorophenol ND
0.522 0.0553 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4-Dichlorophenol ND
0.522 0.0696 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4-Dimethylphenol ND
2.69 1.31 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4-Dinitrophenol ND
0.522 0.0775 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2,4-Dinitrotoluene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-1Client Sample ID: GW-1 (10-15)
Matrix: SoilDate Collected: 06/28/22 10:15
Percent Solids: 62.0Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2,6-Dinitrotoluene ND 0.522 0.0664 mg/Kg ☼07/11/22 13:00 07/12/22 13:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.522 0.0553 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Chloronaphthalene ND
0.522 0.0632 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Chlorophenol ND
0.522 0.0601 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Methylnaphthalene 1.15
0.522 0.0427 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Methylphenol ND
2.69 0.0711 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Nitroaniline ND
0.522 0.0648 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼2-Nitrophenol ND
0.522 0.0680 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼3 & 4 Methylphenol ND
1.04 0.0443 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼3,3'-Dichlorobenzidine ND
2.69 0.0727 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼3-Nitroaniline ND
2.69 0.269 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4,6-Dinitro-2-methylphenol ND
0.522 0.0569 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Bromophenyl phenyl ether ND
0.522 0.0553 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Chloro-3-methylphenol ND
1.04 0.0822 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Chloroaniline ND
0.522 0.0696 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Chlorophenyl phenyl ether ND
2.69 0.0775 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Nitroaniline ND
2.69 0.522 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼4-Nitrophenol ND
0.522 0.0648 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Acenaphthene ND
0.522 0.0569 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Acenaphthylene ND
0.522 0.0443 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Acetophenone ND
0.522 0.0395 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Anthracene ND
0.522 0.0364 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Atrazine ND
0.522 0.0917 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzaldehyde ND
0.522 0.0427 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzo[a]anthracene ND
0.522 0.0822 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzo[a]pyrene ND
0.522 0.0601 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzo[b]fluoranthene ND
0.522 0.0348 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzo[g,h,i]perylene ND
0.522 0.103 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Benzo[k]fluoranthene ND
0.522 0.0474 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼bis (2-chloroisopropyl) ether ND
0.522 0.0616 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Bis(2-chloroethoxy)methane ND
0.522 0.0711 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Bis(2-chloroethyl)ether ND
0.522 0.0458 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Bis(2-ethylhexyl) phthalate 0.0901 J B
0.522 0.0411 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Butyl benzyl phthalate ND
0.522 0.104 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Caprolactam ND
0.522 0.0474 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Carbazole ND
0.522 0.0332 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Chrysene ND
0.522 0.0616 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Dibenz(a,h)anthracene ND
0.522 0.0522 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Dibenzofuran ND
0.522 0.0585 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Diethyl phthalate ND
0.522 0.0537 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Dimethyl phthalate ND
0.522 0.0474 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Di-n-butyl phthalate ND
0.522 0.0458 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Di-n-octyl phthalate ND
0.522 0.0506 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Fluoranthene ND
0.522 0.0569 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Fluorene ND
0.522 0.0616 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Hexachlorobenzene ND
0.522 0.0569 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Hexachlorobutadiene ND
0.522 0.0648 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Hexachlorocyclopentadiene ND
0.522 0.0443 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Hexachloroethane ND
0.522 0.0443 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Indeno[1,2,3-cd]pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-1Client Sample ID: GW-1 (10-15)
Matrix: SoilDate Collected: 06/28/22 10:15
Percent Solids: 62.0Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Isophorone ND 0.522 0.0522 mg/Kg ☼07/11/22 13:00 07/12/22 13:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.522 0.0474 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Naphthalene 0.701
0.522 0.0411 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Nitrobenzene ND
0.522 0.0506 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼N-Nitrosodi-n-propylamine ND
0.522 0.0522 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼N-Nitrosodiphenylamine ND
2.69 0.522 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Pentachlorophenol ND
0.522 0.0427 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Phenanthrene ND
0.522 0.0537 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Phenol ND
0.522 0.0427 mg/Kg 07/11/22 13:00 07/12/22 13:37 1☼Pyrene ND
2,4,6-Tribromophenol (Surr)71 21-132 07/11/22 13:00 07/12/22 13:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 07/11/22 13:00 07/12/22 13:37 125-130
2-Fluorophenol (Surr)54 07/11/22 13:00 07/12/22 13:37 118-130
Nitrobenzene-d5 (Surr)61 07/11/22 13:00 07/12/22 13:37 119-130
Phenol-d5 (Surr)55 07/11/22 13:00 07/12/22 13:37 121-130
Terphenyl-d14 (Surr)78 07/11/22 13:00 07/12/22 13:37 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 0.600 0.440 0.147 mg/Kg ☼07/01/22 07:41 07/01/22 15:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.733 0.0879 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Barium 194
0.0733 0.0220 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Cadmium 0.0909
1.47 0.161 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Chromium 185 B
0.293 0.0733 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Lead 1.82
0.733 0.147 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Selenium 1.12
0.147 0.0147 mg/Kg 07/01/22 07:41 07/01/22 15:49 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0150 J 0.0380 0.0122 mg/Kg ☼07/05/22 16:32 07/06/22 11:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-2Client Sample ID: GW-2 (11-14)
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.518 0.135 mg/Kg ☼07/05/22 15:31 07/11/22 20:37 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1,1-Trichloroethane ND
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1,2,2-Tetrachloroethane ND
0.518 0.301 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.518 0.155 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1,2-Trichloroethane ND
0.518 0.301 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1-Dichloroethane ND
0.518 0.373 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1-Dichloroethene ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,1-Dichloropropene ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2,3-Trichlorobenzene ND
0.518 0.187 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2,3-Trichloropropane ND
0.518 0.259 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2,4-Trichlorobenzene ND
0.518 0.259 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2,4-Trimethylbenzene 9.86
1.04 0.166 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2-Dibromo-3-Chloropropane ND
0.518 0.176 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2-Dichlorobenzene ND
0.518 0.238 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2-Dichloroethane ND
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,2-Dichloropropane ND
0.518 0.249 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,3,5-Trimethylbenzene 3.50
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,3-Dichlorobenzene ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,3-Dichloropropane ND
0.518 0.187 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼1,4-Dichlorobenzene ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼2,2-Dichloropropane ND
2.59 0.954 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼2-Butanone (MEK)ND
0.518 0.238 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼2-Chlorotoluene ND
2.59 1.97 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼2-Hexanone ND
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼4-Chlorotoluene ND
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼4-Isopropyltoluene 0.417 J
2.59 1.87 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼4-Methyl-2-pentanone (MIBK)ND
5.18 1.14 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Acetone ND
0.518 0.249 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Benzene 3.38
0.518 0.176 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Bromobenzene ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Bromoform ND
0.518 0.249 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Bromomethane ND *+
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Carbon disulfide ND
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Carbon tetrachloride ND
0.518 0.145 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chlorobenzene ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chlorobromomethane ND
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chlorodibromomethane ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chloroethane ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chloroform ND
0.518 0.249 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Chloromethane ND
0.518 0.301 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼cis-1,2-Dichloroethene ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼cis-1,3-Dichloropropene ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Dibromomethane ND
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Dichlorobromomethane ND
0.518 0.332 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Dichlorodifluoromethane ND
1.04 1.04 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Ethyl acetate ND
0.518 0.218 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Ethylbenzene 5.35
0.518 0.176 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Ethylene Dibromide ND
0.518 0.425 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-2Client Sample ID: GW-2 (11-14)
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane 13.9 0.518 0.176 mg/Kg ☼07/05/22 15:31 07/11/22 20:37 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.518 0.176 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Iodomethane ND
1.04 0.155 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Isopropyl ether ND
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Isopropylbenzene 0.389 J
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼m,p-Xylene 15.4
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Methyl tert-butyl ether ND *+
1.04 0.829 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Methylene Chloride ND
0.518 0.321 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Naphthalene 3.49
0.518 0.197 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼n-Butylbenzene 1.17
0.518 0.446 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼n-Heptane 11.1
0.518 0.228 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼N-Propylbenzene 1.43
0.518 0.238 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼o-Xylene 5.66
0.518 0.207 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼sec-Butylbenzene ND
0.518 0.197 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Styrene ND
0.518 0.259 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼tert-Butylbenzene ND
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Tetrachloroethene ND
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Toluene 3.57
0.518 0.238 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼trans-1,2-Dichloroethene ND
0.518 0.270 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼trans-1,3-Dichloropropene ND
1.04 0.249 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼trans-1,4-Dichloro-2-butene ND
0.518 0.187 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Trichloroethene ND
0.518 0.321 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Trichlorofluoromethane ND
1.04 0.570 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Vinyl acetate ND
0.518 0.290 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Vinyl chloride ND
1.04 0.373 mg/Kg 07/05/22 15:31 07/11/22 20:37 100☼Xylenes, Total 21.1
1,2-Dichloroethane-d4 (Surr)95 65-130 07/05/22 15:31 07/11/22 20:37 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 07/05/22 15:31 07/11/22 20:37 10065-130
Dibromofluoromethane (Surr)93 07/05/22 15:31 07/11/22 20:37 10065-130
Toluene-d8 (Surr)97 07/05/22 15:31 07/11/22 20:37 10065-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.02 2.02 mg/Kg ☼07/11/22 13:00 07/12/22 15:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.393 0.0416 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4,5-Trichlorophenol ND
0.393 0.0345 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4,6-Trichlorophenol ND
0.393 0.0416 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4-Dichlorophenol ND
0.393 0.0523 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4-Dimethylphenol ND
2.02 0.987 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4-Dinitrophenol ND
0.393 0.0583 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,4-Dinitrotoluene ND
0.393 0.0500 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2,6-Dinitrotoluene ND
0.393 0.0416 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Chloronaphthalene ND
0.393 0.0476 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Chlorophenol ND
0.393 0.0452 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Methylnaphthalene 2.42
0.393 0.0321 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Methylphenol ND
2.02 0.0535 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Nitroaniline ND
0.393 0.0488 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼2-Nitrophenol ND
0.393 0.0511 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼3 & 4 Methylphenol ND
0.785 0.0333 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-2Client Sample ID: GW-2 (11-14)
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.02 0.0547 mg/Kg ☼07/11/22 13:00 07/12/22 15:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.02 0.202 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4,6-Dinitro-2-methylphenol ND
0.393 0.0428 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Bromophenyl phenyl ether ND
0.393 0.0416 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Chloro-3-methylphenol ND
0.785 0.0619 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Chloroaniline ND
0.393 0.0523 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Chlorophenyl phenyl ether ND
2.02 0.0583 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Nitroaniline ND
2.02 0.393 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼4-Nitrophenol ND
0.393 0.0488 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Acenaphthene ND
0.393 0.0428 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Acenaphthylene ND
0.393 0.0333 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Acetophenone ND
0.393 0.0297 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Anthracene ND
0.393 0.0274 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Atrazine ND
0.393 0.0690 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzaldehyde ND
0.393 0.0321 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzo[a]anthracene ND
0.393 0.0619 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzo[a]pyrene ND
0.393 0.0452 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzo[b]fluoranthene ND
0.393 0.0262 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzo[g,h,i]perylene ND
0.393 0.0773 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Benzo[k]fluoranthene ND
0.393 0.0357 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼bis (2-chloroisopropyl) ether ND
0.393 0.0464 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Bis(2-chloroethoxy)methane ND
0.393 0.0535 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Bis(2-chloroethyl)ether ND
0.393 0.0345 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Bis(2-ethylhexyl) phthalate 0.0697 J B
0.393 0.0309 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Butyl benzyl phthalate ND
0.393 0.0785 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Caprolactam ND
0.393 0.0357 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Carbazole ND
0.393 0.0250 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Chrysene ND
0.393 0.0464 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Dibenz(a,h)anthracene ND
0.393 0.0393 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Dibenzofuran ND
0.393 0.0440 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Diethyl phthalate ND
0.393 0.0404 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Dimethyl phthalate ND
0.393 0.0357 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Di-n-butyl phthalate ND
0.393 0.0345 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Di-n-octyl phthalate ND
0.393 0.0381 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Fluoranthene ND
0.393 0.0428 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Fluorene ND
0.393 0.0464 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Hexachlorobenzene ND
0.393 0.0428 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Hexachlorobutadiene ND
0.393 0.0488 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Hexachlorocyclopentadiene ND
0.393 0.0333 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Hexachloroethane ND
0.393 0.0333 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Indeno[1,2,3-cd]pyrene ND
0.393 0.0393 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Isophorone ND
0.393 0.0357 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Naphthalene 2.49
0.393 0.0309 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Nitrobenzene ND
0.393 0.0381 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼N-Nitrosodi-n-propylamine ND
0.393 0.0393 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼N-Nitrosodiphenylamine ND
2.02 0.393 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Pentachlorophenol ND
0.393 0.0321 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Phenanthrene ND
0.393 0.0404 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Phenol 0.176 J
0.393 0.0321 mg/Kg 07/11/22 13:00 07/12/22 15:50 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-2Client Sample ID: GW-2 (11-14)
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)71 21-132 07/11/22 13:00 07/12/22 15:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)63 07/11/22 13:00 07/12/22 15:50 125-130
2-Fluorophenol (Surr)57 07/11/22 13:00 07/12/22 15:50 118-130
Nitrobenzene-d5 (Surr)60 07/11/22 13:00 07/12/22 15:50 119-130
Phenol-d5 (Surr)56 07/11/22 13:00 07/12/22 15:50 121-130
Terphenyl-d14 (Surr)79 07/11/22 13:00 07/12/22 15:50 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 3.40 0.340 0.113 mg/Kg ☼07/01/22 07:41 07/01/22 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.566 0.0680 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Barium 215
0.0566 0.0170 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Cadmium ND
1.13 0.125 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Chromium 60.5 B
0.227 0.0566 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Lead 11.5
0.566 0.113 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Selenium 3.77
0.113 0.0113 mg/Kg 07/01/22 07:41 07/01/22 16:02 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0112 J 0.0268 0.00859 mg/Kg ☼07/05/22 16:32 07/06/22 11:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-3Client Sample ID: GW-3 (7-12)
Matrix: SoilDate Collected: 06/28/22 14:15
Percent Solids: 81.5Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00448 0.00117 mg/Kg ☼07/05/22 15:31 07/08/22 20:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1,1-Trichloroethane ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1,2,2-Tetrachloroethane ND
0.00448 0.00260 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00448 0.00134 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1,2-Trichloroethane ND
0.00448 0.00260 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1-Dichloroethane ND
0.00448 0.00323 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1-Dichloroethene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,1-Dichloropropene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2,3-Trichlorobenzene ND
0.00448 0.00161 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2,3-Trichloropropane ND
0.00448 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2,4-Trichlorobenzene ND
0.00448 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2,4-Trimethylbenzene ND
0.00897 0.00143 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2-Dibromo-3-Chloropropane ND
0.00448 0.00152 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2-Dichlorobenzene ND
0.00448 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2-Dichloroethane ND
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,2-Dichloropropane ND
0.00448 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,3,5-Trimethylbenzene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,3-Dichlorobenzene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,3-Dichloropropane ND
0.00448 0.00161 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼1,4-Dichlorobenzene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼2,2-Dichloropropane ND
0.0224 0.00825 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼2-Butanone (MEK)ND
0.00448 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼2-Chlorotoluene ND
0.0224 0.0170 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼2-Hexanone ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼4-Chlorotoluene ND
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼4-Isopropyltoluene ND
0.0224 0.0161 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼4-Methyl-2-pentanone (MIBK)ND
0.0448 0.00986 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Acetone 0.0844 B
0.00448 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Benzene ND
0.00448 0.00152 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Bromobenzene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Bromoform ND
0.00448 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Bromomethane ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Carbon disulfide ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Carbon tetrachloride ND
0.00448 0.00126 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chlorobenzene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chlorobromomethane ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chlorodibromomethane ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chloroethane ND *+
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chloroform ND
0.00448 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Chloromethane ND
0.00448 0.00260 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼cis-1,2-Dichloroethene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼cis-1,3-Dichloropropene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Dibromomethane ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Dichlorobromomethane ND
0.00448 0.00287 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Dichlorodifluoromethane ND
0.00897 0.00897 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Ethyl acetate ND
0.00448 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Ethylbenzene ND
0.00448 0.00152 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Ethylene Dibromide ND
0.00448 0.00368 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-3Client Sample ID: GW-3 (7-12)
Matrix: SoilDate Collected: 06/28/22 14:15
Percent Solids: 81.5Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00448 0.00152 mg/Kg ☼07/05/22 15:31 07/08/22 20:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00448 0.00152 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Iodomethane ND
0.00897 0.00134 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Isopropyl ether ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Isopropylbenzene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼m,p-Xylene ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Methyl tert-butyl ether ND
0.00897 0.00717 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Methylene Chloride ND
0.00448 0.00278 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Naphthalene ND
0.00448 0.00170 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼n-Butylbenzene ND
0.00448 0.00386 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼n-Heptane ND
0.00448 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼N-Propylbenzene ND
0.00448 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼o-Xylene ND
0.00448 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼sec-Butylbenzene ND
0.00448 0.00170 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Styrene ND
0.00448 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼tert-Butylbenzene ND
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Tetrachloroethene ND
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Toluene ND
0.00448 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼trans-1,2-Dichloroethene ND
0.00448 0.00233 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼trans-1,3-Dichloropropene ND
0.00897 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼trans-1,4-Dichloro-2-butene ND
0.00448 0.00161 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Trichloroethene ND
0.00448 0.00278 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Trichlorofluoromethane ND
0.00897 0.00493 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Vinyl acetate ND *+
0.00448 0.00251 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Vinyl chloride ND
0.00897 0.00323 mg/Kg 07/05/22 15:31 07/08/22 20:56 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)122 65-130 07/05/22 15:31 07/08/22 20:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 07/05/22 15:31 07/08/22 20:56 165-130
Dibromofluoromethane (Surr)104 07/05/22 15:31 07/08/22 20:56 165-130
Toluene-d8 (Surr)97 07/05/22 15:31 07/08/22 20:56 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.01 2.01 mg/Kg ☼07/11/22 13:00 07/12/22 16:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.391 0.0414 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4,5-Trichlorophenol ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4,6-Trichlorophenol ND
0.391 0.0414 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4-Dichlorophenol ND
0.391 0.0521 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4-Dimethylphenol ND
2.01 0.983 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4-Dinitrophenol ND
0.391 0.0580 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,4-Dinitrotoluene ND
0.391 0.0497 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2,6-Dinitrotoluene ND
0.391 0.0414 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Chloronaphthalene ND
0.391 0.0474 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Chlorophenol ND
0.391 0.0450 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Methylnaphthalene ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Methylphenol ND
2.01 0.0533 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Nitroaniline ND
0.391 0.0485 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼2-Nitrophenol ND
0.391 0.0509 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼3 & 4 Methylphenol ND
0.781 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-3Client Sample ID: GW-3 (7-12)
Matrix: SoilDate Collected: 06/28/22 14:15
Percent Solids: 81.5Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.01 0.0545 mg/Kg ☼07/11/22 13:00 07/12/22 16:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.01 0.201 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4,6-Dinitro-2-methylphenol ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Bromophenyl phenyl ether ND
0.391 0.0414 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Chloro-3-methylphenol ND
0.781 0.0616 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Chloroaniline ND
0.391 0.0521 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Chlorophenyl phenyl ether ND
2.01 0.0580 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Nitroaniline ND
2.01 0.391 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼4-Nitrophenol ND
0.391 0.0485 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Acenaphthene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Acenaphthylene ND
0.391 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Acetophenone ND
0.391 0.0296 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Anthracene ND
0.391 0.0272 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Atrazine ND
0.391 0.0687 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzaldehyde ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzo[a]anthracene ND
0.391 0.0616 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzo[a]pyrene ND
0.391 0.0450 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzo[b]fluoranthene ND
0.391 0.0260 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzo[g,h,i]perylene ND
0.391 0.0769 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Benzo[k]fluoranthene ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼bis (2-chloroisopropyl) ether ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Bis(2-chloroethoxy)methane ND
0.391 0.0533 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Bis(2-chloroethyl)ether ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Bis(2-ethylhexyl) phthalate 0.0706 J B
0.391 0.0308 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Butyl benzyl phthalate ND
0.391 0.0781 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Caprolactam ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Carbazole ND
0.391 0.0249 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Chrysene ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Dibenz(a,h)anthracene ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Dibenzofuran ND
0.391 0.0438 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Diethyl phthalate ND
0.391 0.0402 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Dimethyl phthalate ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Di-n-butyl phthalate ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Di-n-octyl phthalate ND
0.391 0.0379 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Fluoranthene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Fluorene ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Hexachlorobenzene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Hexachlorobutadiene ND
0.391 0.0485 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Hexachlorocyclopentadiene ND
0.391 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Hexachloroethane ND
0.391 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Indeno[1,2,3-cd]pyrene ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Isophorone ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Naphthalene ND
0.391 0.0308 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Nitrobenzene ND
0.391 0.0379 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼N-Nitrosodi-n-propylamine ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼N-Nitrosodiphenylamine ND
2.01 0.391 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Pentachlorophenol ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Phenanthrene ND
0.391 0.0402 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Phenol ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:12 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-3Client Sample ID: GW-3 (7-12)
Matrix: SoilDate Collected: 06/28/22 14:15
Percent Solids: 81.5Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)59 21-132 07/11/22 13:00 07/12/22 16:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 07/11/22 13:00 07/12/22 16:12 125-130
2-Fluorophenol (Surr)47 07/11/22 13:00 07/12/22 16:12 118-130
Nitrobenzene-d5 (Surr)53 07/11/22 13:00 07/12/22 16:12 119-130
Phenol-d5 (Surr)53 07/11/22 13:00 07/12/22 16:12 121-130
Terphenyl-d14 (Surr)72 07/11/22 13:00 07/12/22 16:12 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 4.26 0.361 0.120 mg/Kg ☼07/01/22 07:41 07/01/22 16:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.602 0.0722 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Barium 145
0.0602 0.0180 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Cadmium 0.0289 J
1.20 0.132 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Chromium 215 B
0.241 0.0602 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Lead 10.4
0.602 0.120 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Selenium 1.51
0.120 0.0120 mg/Kg 07/01/22 07:41 07/01/22 16:05 1☼Silver 0.0132 J
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0645 0.0264 0.00846 mg/Kg ☼07/05/22 16:32 07/06/22 11:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-4Client Sample ID: GW-4 (13-17)
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00471 0.00122 mg/Kg ☼07/05/22 15:31 07/08/22 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1,1-Trichloroethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1,2,2-Tetrachloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00471 0.00141 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1,2-Trichloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1-Dichloroethane ND
0.00471 0.00339 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1-Dichloroethene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,1-Dichloropropene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2,3-Trichlorobenzene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2,3-Trichloropropane ND
0.00471 0.00235 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2,4-Trichlorobenzene ND
0.00471 0.00235 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2,4-Trimethylbenzene ND
0.00942 0.00151 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2-Dibromo-3-Chloropropane ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2-Dichlorobenzene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2-Dichloroethane ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,2-Dichloropropane ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,3,5-Trimethylbenzene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,3-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,3-Dichloropropane ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼1,4-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼2,2-Dichloropropane ND
0.0235 0.00866 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼2-Butanone (MEK)ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼2-Chlorotoluene ND
0.0235 0.0179 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼2-Hexanone ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼4-Chlorotoluene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼4-Isopropyltoluene ND
0.0235 0.0170 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼4-Methyl-2-pentanone (MIBK)ND
0.0471 0.0104 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Acetone 0.0502 B
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Benzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Bromobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Bromoform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Bromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Carbon disulfide ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Carbon tetrachloride ND
0.00471 0.00132 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chlorobenzene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chlorobromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chlorodibromomethane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chloroethane ND *+
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chloroform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Chloromethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼cis-1,2-Dichloroethene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼cis-1,3-Dichloropropene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Dibromomethane ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Dichlorobromomethane ND
0.00471 0.00301 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Dichlorodifluoromethane ND
0.00942 0.00942 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Ethyl acetate ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Ethylbenzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Ethylene Dibromide ND
0.00471 0.00386 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-4Client Sample ID: GW-4 (13-17)
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00471 0.00160 mg/Kg ☼07/05/22 15:31 07/08/22 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Iodomethane ND
0.00942 0.00141 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Isopropyl ether ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Isopropylbenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼m,p-Xylene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Methyl tert-butyl ether ND
0.00942 0.00753 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Methylene Chloride ND
0.00471 0.00292 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Naphthalene ND
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼n-Butylbenzene ND
0.00471 0.00405 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼n-Heptane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼N-Propylbenzene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼o-Xylene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼sec-Butylbenzene ND
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Styrene ND
0.00471 0.00235 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼tert-Butylbenzene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Tetrachloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Toluene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼trans-1,2-Dichloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼trans-1,3-Dichloropropene ND
0.00942 0.00226 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼trans-1,4-Dichloro-2-butene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Trichloroethene ND
0.00471 0.00292 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Trichlorofluoromethane ND
0.00942 0.00518 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Vinyl acetate ND *+
0.00471 0.00264 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Vinyl chloride ND
0.00942 0.00339 mg/Kg 07/05/22 15:31 07/08/22 19:54 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)123 65-130 07/05/22 15:31 07/08/22 19:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 07/05/22 15:31 07/08/22 19:54 165-130
Dibromofluoromethane (Surr)105 07/05/22 15:31 07/08/22 19:54 165-130
Toluene-d8 (Surr)92 07/05/22 15:31 07/08/22 19:54 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.01 2.01 mg/Kg ☼07/11/22 13:00 07/12/22 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.391 0.0415 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4,5-Trichlorophenol ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4,6-Trichlorophenol ND
0.391 0.0415 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4-Dichlorophenol ND
0.391 0.0521 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4-Dimethylphenol ND
2.01 0.983 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4-Dinitrophenol ND
0.391 0.0580 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,4-Dinitrotoluene ND
0.391 0.0497 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2,6-Dinitrotoluene ND
0.391 0.0415 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Chloronaphthalene ND
0.391 0.0474 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Chlorophenol ND
0.391 0.0450 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Methylnaphthalene ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Methylphenol ND
2.01 0.0533 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Nitroaniline ND
0.391 0.0486 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼2-Nitrophenol ND
0.391 0.0509 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼3 & 4 Methylphenol ND
0.782 0.0332 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-4Client Sample ID: GW-4 (13-17)
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.01 0.0545 mg/Kg ☼07/11/22 13:00 07/12/22 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.01 0.201 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4,6-Dinitro-2-methylphenol ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Bromophenyl phenyl ether ND
0.391 0.0415 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Chloro-3-methylphenol ND
0.782 0.0616 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Chloroaniline ND
0.391 0.0521 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Chlorophenyl phenyl ether ND
2.01 0.0580 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Nitroaniline ND
2.01 0.391 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼4-Nitrophenol ND
0.391 0.0486 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Acenaphthene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Acenaphthylene ND
0.391 0.0332 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Acetophenone ND
0.391 0.0296 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Anthracene ND
0.391 0.0272 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Atrazine ND
0.391 0.0687 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzaldehyde ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzo[a]anthracene ND
0.391 0.0616 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzo[a]pyrene ND
0.391 0.0450 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzo[b]fluoranthene ND
0.391 0.0261 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzo[g,h,i]perylene ND
0.391 0.0770 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Benzo[k]fluoranthene ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼bis (2-chloroisopropyl) ether ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Bis(2-chloroethoxy)methane ND
0.391 0.0533 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Bis(2-chloroethyl)ether ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Bis(2-ethylhexyl) phthalate 0.0847 J B
0.391 0.0308 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Butyl benzyl phthalate ND
0.391 0.0782 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Caprolactam ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Carbazole ND
0.391 0.0249 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Chrysene ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Dibenz(a,h)anthracene ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Dibenzofuran ND
0.391 0.0438 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Diethyl phthalate ND
0.391 0.0403 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Dimethyl phthalate ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Di-n-butyl phthalate ND
0.391 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Di-n-octyl phthalate ND
0.391 0.0379 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Fluoranthene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Fluorene ND
0.391 0.0462 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Hexachlorobenzene ND
0.391 0.0426 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Hexachlorobutadiene ND
0.391 0.0486 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Hexachlorocyclopentadiene ND
0.391 0.0332 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Hexachloroethane ND
0.391 0.0332 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Indeno[1,2,3-cd]pyrene ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Isophorone ND
0.391 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Naphthalene ND
0.391 0.0308 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Nitrobenzene ND
0.391 0.0379 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼N-Nitrosodi-n-propylamine ND
0.391 0.0391 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼N-Nitrosodiphenylamine ND
2.01 0.391 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Pentachlorophenol ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Phenanthrene ND
0.391 0.0403 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Phenol ND
0.391 0.0320 mg/Kg 07/11/22 13:00 07/12/22 16:34 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-4Client Sample ID: GW-4 (13-17)
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)66 21-132 07/11/22 13:00 07/12/22 16:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)71 07/11/22 13:00 07/12/22 16:34 125-130
2-Fluorophenol (Surr)57 07/11/22 13:00 07/12/22 16:34 118-130
Nitrobenzene-d5 (Surr)60 07/11/22 13:00 07/12/22 16:34 119-130
Phenol-d5 (Surr)61 07/11/22 13:00 07/12/22 16:34 121-130
Terphenyl-d14 (Surr)74 07/11/22 13:00 07/12/22 16:34 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.57 0.336 0.112 mg/Kg ☼07/01/22 07:41 07/01/22 16:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.560 0.0671 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Barium 104
0.0560 0.0168 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Cadmium 0.0459 J
1.12 0.123 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Chromium 25.4 B
0.224 0.0560 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Lead 13.2
0.560 0.112 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Selenium 3.97
0.112 0.0112 mg/Kg 07/01/22 07:41 07/01/22 16:07 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0146 J 0.0282 0.00904 mg/Kg ☼07/05/22 16:32 07/06/22 11:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-5Client Sample ID: SS-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:40
Percent Solids: 77.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00470 0.00122 mg/Kg ☼07/05/22 15:31 07/08/22 20:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1,1-Trichloroethane ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1,2,2-Tetrachloroethane ND
0.00470 0.00272 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00470 0.00141 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1,2-Trichloroethane ND
0.00470 0.00272 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1-Dichloroethane ND
0.00470 0.00338 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1-Dichloroethene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,1-Dichloropropene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2,3-Trichlorobenzene ND
0.00470 0.00169 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2,3-Trichloropropane ND
0.00470 0.00235 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2,4-Trichlorobenzene ND
0.00470 0.00235 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2,4-Trimethylbenzene ND
0.00939 0.00150 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2-Dibromo-3-Chloropropane ND
0.00470 0.00160 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2-Dichlorobenzene ND
0.00470 0.00216 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2-Dichloroethane ND
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,2-Dichloropropane ND
0.00470 0.00225 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,3,5-Trimethylbenzene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,3-Dichlorobenzene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,3-Dichloropropane ND
0.00470 0.00169 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼1,4-Dichlorobenzene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼2,2-Dichloropropane ND
0.0235 0.00864 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼2-Butanone (MEK)ND
0.00470 0.00216 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼2-Chlorotoluene ND
0.0235 0.0179 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼2-Hexanone ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼4-Chlorotoluene ND
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼4-Isopropyltoluene ND
0.0235 0.0169 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼4-Methyl-2-pentanone (MIBK)ND
0.0470 0.0103 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Acetone 0.0186 J B
0.00470 0.00225 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Benzene ND
0.00470 0.00160 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Bromobenzene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Bromoform ND
0.00470 0.00225 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Bromomethane ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Carbon disulfide ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Carbon tetrachloride ND
0.00470 0.00132 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chlorobenzene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chlorobromomethane ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chlorodibromomethane ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chloroethane ND *+
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chloroform ND
0.00470 0.00225 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Chloromethane ND
0.00470 0.00272 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼cis-1,2-Dichloroethene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼cis-1,3-Dichloropropene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Dibromomethane ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Dichlorobromomethane ND
0.00470 0.00301 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Dichlorodifluoromethane ND
0.00939 0.00939 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Ethyl acetate ND
0.00470 0.00197 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Ethylbenzene ND
0.00470 0.00160 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Ethylene Dibromide ND
0.00470 0.00385 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-5Client Sample ID: SS-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:40
Percent Solids: 77.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00470 0.00160 mg/Kg ☼07/05/22 15:31 07/08/22 20:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00470 0.00160 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Iodomethane ND
0.00939 0.00141 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Isopropyl ether ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Isopropylbenzene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼m,p-Xylene ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Methyl tert-butyl ether ND
0.00939 0.00752 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Methylene Chloride ND
0.00470 0.00291 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Naphthalene ND
0.00470 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼n-Butylbenzene ND
0.00470 0.00404 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼n-Heptane ND
0.00470 0.00207 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼N-Propylbenzene ND
0.00470 0.00216 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼o-Xylene ND
0.00470 0.00188 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼sec-Butylbenzene ND
0.00470 0.00179 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Styrene ND
0.00470 0.00235 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼tert-Butylbenzene ND
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Tetrachloroethene ND
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Toluene ND
0.00470 0.00216 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼trans-1,2-Dichloroethene ND
0.00470 0.00244 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼trans-1,3-Dichloropropene ND
0.00939 0.00225 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼trans-1,4-Dichloro-2-butene ND
0.00470 0.00169 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Trichloroethene ND
0.00470 0.00291 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Trichlorofluoromethane ND
0.00939 0.00517 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Vinyl acetate ND *+
0.00470 0.00263 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Vinyl chloride ND
0.00939 0.00338 mg/Kg 07/05/22 15:31 07/08/22 20:15 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)121 65-130 07/05/22 15:31 07/08/22 20:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 07/05/22 15:31 07/08/22 20:15 165-130
Dibromofluoromethane (Surr)102 07/05/22 15:31 07/08/22 20:15 165-130
Toluene-d8 (Surr)99 07/05/22 15:31 07/08/22 20:15 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.08 2.08 mg/Kg ☼07/11/22 13:00 07/12/22 16:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.404 0.0428 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4,5-Trichlorophenol ND
0.404 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4,6-Trichlorophenol ND
0.404 0.0428 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4-Dichlorophenol ND
0.404 0.0539 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4-Dimethylphenol ND
2.08 1.02 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4-Dinitrophenol ND
0.404 0.0600 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,4-Dinitrotoluene ND
0.404 0.0514 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2,6-Dinitrotoluene ND
0.404 0.0428 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Chloronaphthalene ND
0.404 0.0490 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Chlorophenol ND
0.404 0.0465 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Methylnaphthalene ND
0.404 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Methylphenol ND
2.08 0.0551 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Nitroaniline ND
0.404 0.0502 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼2-Nitrophenol ND
0.404 0.0526 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼3 & 4 Methylphenol ND
0.808 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-5Client Sample ID: SS-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:40
Percent Solids: 77.6Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.08 0.0563 mg/Kg ☼07/11/22 13:00 07/12/22 16:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.08 0.208 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4,6-Dinitro-2-methylphenol ND
0.404 0.0441 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Bromophenyl phenyl ether ND
0.404 0.0428 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Chloro-3-methylphenol ND
0.808 0.0637 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Chloroaniline ND
0.404 0.0539 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Chlorophenyl phenyl ether ND
2.08 0.0600 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Nitroaniline ND
2.08 0.404 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼4-Nitrophenol ND
0.404 0.0502 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Acenaphthene ND
0.404 0.0441 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Acenaphthylene ND
0.404 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Acetophenone ND
0.404 0.0306 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Anthracene ND
0.404 0.0282 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Atrazine ND
0.404 0.0710 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzaldehyde ND
0.404 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzo[a]anthracene 0.0334 J
0.404 0.0637 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzo[a]pyrene ND
0.404 0.0465 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzo[b]fluoranthene ND
0.404 0.0269 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzo[g,h,i]perylene ND
0.404 0.0796 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Benzo[k]fluoranthene ND
0.404 0.0367 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼bis (2-chloroisopropyl) ether ND
0.404 0.0477 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Bis(2-chloroethoxy)methane ND
0.404 0.0551 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Bis(2-chloroethyl)ether ND
0.404 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Bis(2-ethylhexyl) phthalate 0.0737 J B
0.404 0.0318 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Butyl benzyl phthalate ND
0.404 0.0808 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Caprolactam ND
0.404 0.0367 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Carbazole ND
0.404 0.0257 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Chrysene ND
0.404 0.0477 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Dibenz(a,h)anthracene ND
0.404 0.0404 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Dibenzofuran ND
0.404 0.0453 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Diethyl phthalate ND
0.404 0.0416 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Dimethyl phthalate ND
0.404 0.0367 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Di-n-butyl phthalate ND
0.404 0.0355 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Di-n-octyl phthalate ND
0.404 0.0392 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Fluoranthene 0.0514 J
0.404 0.0441 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Fluorene ND
0.404 0.0477 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Hexachlorobenzene ND
0.404 0.0441 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Hexachlorobutadiene ND
0.404 0.0502 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Hexachlorocyclopentadiene ND
0.404 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Hexachloroethane ND
0.404 0.0343 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Indeno[1,2,3-cd]pyrene ND
0.404 0.0404 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Isophorone ND
0.404 0.0367 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Naphthalene ND
0.404 0.0318 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Nitrobenzene ND
0.404 0.0392 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼N-Nitrosodi-n-propylamine ND
0.404 0.0404 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼N-Nitrosodiphenylamine ND
2.08 0.404 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Pentachlorophenol ND
0.404 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Phenanthrene 0.0693 J
0.404 0.0416 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Phenol ND
0.404 0.0331 mg/Kg 07/11/22 13:00 07/12/22 16:56 1☼Pyrene 0.0520 J
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-5Client Sample ID: SS-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:40
Percent Solids: 77.6Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)68 21-132 07/11/22 13:00 07/12/22 16:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)70 07/11/22 13:00 07/12/22 16:56 125-130
2-Fluorophenol (Surr)56 07/11/22 13:00 07/12/22 16:56 118-130
Nitrobenzene-d5 (Surr)61 07/11/22 13:00 07/12/22 16:56 119-130
Phenol-d5 (Surr)59 07/11/22 13:00 07/12/22 16:56 121-130
Terphenyl-d14 (Surr)75 07/11/22 13:00 07/12/22 16:56 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.59 0.358 0.119 mg/Kg ☼07/01/22 07:41 07/01/22 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.597 0.0716 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Barium 67.9
0.0597 0.0179 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Cadmium ND
1.19 0.131 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Chromium 60.2 B
0.239 0.0597 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Lead 14.1
0.597 0.119 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Selenium 1.29
0.119 0.0119 mg/Kg 07/01/22 07:41 07/01/22 16:15 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0126 J 0.0316 0.0101 mg/Kg ☼07/05/22 16:32 07/06/22 11:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-6Client Sample ID: SS-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00578 0.00150 mg/Kg ☼07/05/22 15:31 07/08/22 19:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1,1-Trichloroethane ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1,2,2-Tetrachloroethane ND
0.00578 0.00335 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00578 0.00173 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1,2-Trichloroethane ND
0.00578 0.00335 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1-Dichloroethane ND
0.00578 0.00416 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1-Dichloroethene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,1-Dichloropropene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2,3-Trichlorobenzene ND
0.00578 0.00208 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2,3-Trichloropropane ND
0.00578 0.00289 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2,4-Trichlorobenzene ND
0.00578 0.00289 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2,4-Trimethylbenzene ND
0.0116 0.00185 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2-Dibromo-3-Chloropropane ND
0.00578 0.00196 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2-Dichlorobenzene ND
0.00578 0.00266 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2-Dichloroethane ND
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,2-Dichloropropane ND
0.00578 0.00277 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,3,5-Trimethylbenzene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,3-Dichlorobenzene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,3-Dichloropropane ND
0.00578 0.00208 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼1,4-Dichlorobenzene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼2,2-Dichloropropane ND
0.0289 0.0106 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼2-Butanone (MEK)ND
0.00578 0.00266 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼2-Chlorotoluene ND
0.0289 0.0219 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼2-Hexanone ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼4-Chlorotoluene ND
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼4-Isopropyltoluene ND
0.0289 0.0208 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼4-Methyl-2-pentanone (MIBK)ND
0.0578 0.0127 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Acetone 0.0655 B
0.00578 0.00277 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Benzene ND
0.00578 0.00196 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Bromobenzene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Bromoform ND
0.00578 0.00277 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Bromomethane ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Carbon disulfide ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Carbon tetrachloride ND
0.00578 0.00162 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chlorobenzene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chlorobromomethane ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chlorodibromomethane ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chloroethane ND *+
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chloroform ND
0.00578 0.00277 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Chloromethane ND
0.00578 0.00335 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼cis-1,2-Dichloroethene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼cis-1,3-Dichloropropene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Dibromomethane ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Dichlorobromomethane ND
0.00578 0.00370 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Dichlorodifluoromethane ND
0.0116 0.0116 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Ethyl acetate ND
0.00578 0.00243 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Ethylbenzene ND
0.00578 0.00196 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Ethylene Dibromide ND
0.00578 0.00474 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-6Client Sample ID: SS-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00578 0.00196 mg/Kg ☼07/05/22 15:31 07/08/22 19:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00578 0.00196 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Iodomethane ND
0.0116 0.00173 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Isopropyl ether ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Isopropylbenzene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼m,p-Xylene ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Methyl tert-butyl ether ND
0.0116 0.00924 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Methylene Chloride ND
0.00578 0.00358 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Naphthalene ND
0.00578 0.00219 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼n-Butylbenzene ND
0.00578 0.00497 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼n-Heptane ND
0.00578 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼N-Propylbenzene ND
0.00578 0.00266 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼o-Xylene ND
0.00578 0.00231 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼sec-Butylbenzene ND
0.00578 0.00219 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Styrene ND
0.00578 0.00289 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼tert-Butylbenzene ND
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Tetrachloroethene ND
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Toluene ND
0.00578 0.00266 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼trans-1,2-Dichloroethene ND
0.00578 0.00300 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼trans-1,3-Dichloropropene ND
0.0116 0.00277 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼trans-1,4-Dichloro-2-butene ND
0.00578 0.00208 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Trichloroethene ND
0.00578 0.00358 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Trichlorofluoromethane ND
0.0116 0.00635 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Vinyl acetate ND *+
0.00578 0.00323 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Vinyl chloride ND
0.0116 0.00416 mg/Kg 07/05/22 15:31 07/08/22 19:33 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)120 65-130 07/05/22 15:31 07/08/22 19:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 07/05/22 15:31 07/08/22 19:33 165-130
Dibromofluoromethane (Surr)103 07/05/22 15:31 07/08/22 19:33 165-130
Toluene-d8 (Surr)100 07/05/22 15:31 07/08/22 19:33 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.97 1.97 mg/Kg ☼07/11/22 13:00 07/12/22 17:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4,5-Trichlorophenol ND
0.382 0.0335 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4,6-Trichlorophenol ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4-Dichlorophenol ND
0.382 0.0509 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4-Dimethylphenol ND
1.97 0.960 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4-Dinitrophenol ND
0.382 0.0567 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,4-Dinitrotoluene ND
0.382 0.0486 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2,6-Dinitrotoluene ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Chloronaphthalene ND
0.382 0.0463 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Chlorophenol ND
0.382 0.0439 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Methylnaphthalene ND
0.382 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Methylphenol ND
1.97 0.0520 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Nitroaniline ND
0.382 0.0474 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼2-Nitrophenol ND
0.382 0.0497 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼3 & 4 Methylphenol ND
0.763 0.0324 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-6Client Sample ID: SS-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.97 0.0532 mg/Kg ☼07/11/22 13:00 07/12/22 17:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.97 0.197 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4,6-Dinitro-2-methylphenol ND
0.382 0.0416 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Bromophenyl phenyl ether ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Chloro-3-methylphenol ND
0.763 0.0601 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Chloroaniline ND
0.382 0.0509 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Chlorophenyl phenyl ether ND
1.97 0.0567 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Nitroaniline ND
1.97 0.382 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼4-Nitrophenol ND
0.382 0.0474 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Acenaphthene ND
0.382 0.0416 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Acenaphthylene ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Acetophenone ND
0.382 0.0289 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Anthracene ND
0.382 0.0266 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Atrazine ND
0.382 0.0671 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzaldehyde ND
0.382 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzo[a]anthracene ND
0.382 0.0601 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzo[a]pyrene ND
0.382 0.0439 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzo[b]fluoranthene ND
0.382 0.0254 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzo[g,h,i]perylene ND
0.382 0.0752 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Benzo[k]fluoranthene ND
0.382 0.0347 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼bis (2-chloroisopropyl) ether ND
0.382 0.0451 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Bis(2-chloroethoxy)methane ND
0.382 0.0520 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Bis(2-chloroethyl)ether ND
0.382 0.0335 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Bis(2-ethylhexyl) phthalate 0.0626 J B
0.382 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Butyl benzyl phthalate ND
0.382 0.0763 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Caprolactam ND
0.382 0.0347 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Carbazole ND
0.382 0.0243 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Chrysene 0.0270 J
0.382 0.0451 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Dibenz(a,h)anthracene ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Dibenzofuran ND
0.382 0.0428 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Diethyl phthalate ND
0.382 0.0393 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Dimethyl phthalate ND
0.382 0.0347 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Di-n-butyl phthalate ND
0.382 0.0335 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Di-n-octyl phthalate ND
0.382 0.0370 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Fluoranthene ND
0.382 0.0416 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Fluorene ND
0.382 0.0451 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Hexachlorobenzene ND
0.382 0.0416 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Hexachlorobutadiene ND
0.382 0.0474 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Hexachlorocyclopentadiene ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Hexachloroethane ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Indeno[1,2,3-cd]pyrene ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Isophorone ND
0.382 0.0347 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Naphthalene ND
0.382 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Nitrobenzene ND
0.382 0.0370 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼N-Nitrosodi-n-propylamine ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼N-Nitrosodiphenylamine ND
1.97 0.382 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Pentachlorophenol ND
0.382 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Phenanthrene ND
0.382 0.0393 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Phenol ND
0.382 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:19 1☼Pyrene 0.0326 J
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-6Client Sample ID: SS-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)65 21-132 07/11/22 13:00 07/12/22 17:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)58 07/11/22 13:00 07/12/22 17:19 125-130
2-Fluorophenol (Surr)47 07/11/22 13:00 07/12/22 17:19 118-130
Nitrobenzene-d5 (Surr)49 07/11/22 13:00 07/12/22 17:19 119-130
Phenol-d5 (Surr)51 07/11/22 13:00 07/12/22 17:19 121-130
Terphenyl-d14 (Surr)68 07/11/22 13:00 07/12/22 17:19 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.80 0.333 0.111 mg/Kg ☼07/01/22 07:41 07/01/22 16:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.555 0.0665 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Barium 32.0
0.0555 0.0166 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Cadmium 0.0627
1.11 0.122 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Chromium 7.87 B
0.222 0.0555 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Lead 12.2
0.555 0.111 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Selenium 1.18
0.111 0.0111 mg/Kg 07/01/22 07:41 07/01/22 16:17 1☼Silver 0.0277 J
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0116 J 0.0258 0.00825 mg/Kg ☼07/05/22 16:32 07/06/22 11:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-7Client Sample ID: SS-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:15
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00421 0.00110 mg/Kg ☼07/05/22 15:31 07/08/22 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1,1-Trichloroethane ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1,2,2-Tetrachloroethane ND
0.00421 0.00244 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00421 0.00126 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1,2-Trichloroethane ND
0.00421 0.00244 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1-Dichloroethane ND
0.00421 0.00303 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1-Dichloroethene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,1-Dichloropropene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2,3-Trichlorobenzene ND
0.00421 0.00152 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2,3-Trichloropropane ND
0.00421 0.00211 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2,4-Trichlorobenzene ND
0.00421 0.00211 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2,4-Trimethylbenzene ND
0.00842 0.00135 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2-Dibromo-3-Chloropropane ND
0.00421 0.00143 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2-Dichlorobenzene ND
0.00421 0.00194 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2-Dichloroethane ND
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,2-Dichloropropane ND
0.00421 0.00202 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,3,5-Trimethylbenzene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,3-Dichlorobenzene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,3-Dichloropropane ND
0.00421 0.00152 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼1,4-Dichlorobenzene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼2,2-Dichloropropane ND
0.0211 0.00775 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼2-Butanone (MEK)ND
0.00421 0.00194 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼2-Chlorotoluene ND
0.0211 0.0160 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼2-Hexanone ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼4-Chlorotoluene ND
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼4-Isopropyltoluene ND
0.0211 0.0152 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼4-Methyl-2-pentanone (MIBK)ND
0.0421 0.00927 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Acetone 0.0392 J B
0.00421 0.00202 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Benzene ND
0.00421 0.00143 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Bromobenzene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Bromoform ND
0.00421 0.00202 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Bromomethane ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Carbon disulfide ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Carbon tetrachloride ND
0.00421 0.00118 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chlorobenzene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chlorobromomethane ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chlorodibromomethane ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chloroethane ND *+
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chloroform ND
0.00421 0.00202 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Chloromethane ND
0.00421 0.00244 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼cis-1,2-Dichloroethene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼cis-1,3-Dichloropropene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Dibromomethane ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Dichlorobromomethane ND
0.00421 0.00270 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Dichlorodifluoromethane ND
0.00842 0.00842 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Ethyl acetate ND
0.00421 0.00177 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Ethylbenzene ND
0.00421 0.00143 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Ethylene Dibromide ND
0.00421 0.00345 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-7Client Sample ID: SS-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:15
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00421 0.00143 mg/Kg ☼07/05/22 15:31 07/08/22 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00421 0.00143 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Iodomethane ND
0.00842 0.00126 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Isopropyl ether ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Isopropylbenzene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼m,p-Xylene ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Methyl tert-butyl ether ND
0.00842 0.00674 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Methylene Chloride ND
0.00421 0.00261 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Naphthalene ND
0.00421 0.00160 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼n-Butylbenzene ND
0.00421 0.00362 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼n-Heptane ND
0.00421 0.00185 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼N-Propylbenzene ND
0.00421 0.00194 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼o-Xylene ND
0.00421 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼sec-Butylbenzene ND
0.00421 0.00160 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Styrene ND
0.00421 0.00211 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼tert-Butylbenzene ND
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Tetrachloroethene ND
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Toluene ND
0.00421 0.00194 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼trans-1,2-Dichloroethene ND
0.00421 0.00219 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼trans-1,3-Dichloropropene ND
0.00842 0.00202 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼trans-1,4-Dichloro-2-butene ND
0.00421 0.00152 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Trichloroethene ND
0.00421 0.00261 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Trichlorofluoromethane ND
0.00842 0.00463 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Vinyl acetate ND *+
0.00421 0.00236 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Vinyl chloride ND
0.00842 0.00303 mg/Kg 07/05/22 15:31 07/08/22 18:08 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)121 65-130 07/05/22 15:31 07/08/22 18:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 07/05/22 15:31 07/08/22 18:08 165-130
Dibromofluoromethane (Surr)104 07/05/22 15:31 07/08/22 18:08 165-130
Toluene-d8 (Surr)98 07/05/22 15:31 07/08/22 18:08 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.83 1.83 mg/Kg ☼07/11/22 13:00 07/12/22 17:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.355 0.0376 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4,5-Trichlorophenol ND
0.355 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4,6-Trichlorophenol ND
0.355 0.0376 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4-Dichlorophenol ND
0.355 0.0473 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4-Dimethylphenol ND
1.83 0.893 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4-Dinitrophenol ND
0.355 0.0527 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,4-Dinitrotoluene ND
0.355 0.0452 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2,6-Dinitrotoluene ND
0.355 0.0376 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Chloronaphthalene ND
0.355 0.0430 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Chlorophenol ND
0.355 0.0409 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Methylnaphthalene ND
0.355 0.0290 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Methylphenol ND
1.83 0.0484 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Nitroaniline ND
0.355 0.0441 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼2-Nitrophenol ND
0.355 0.0462 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼3 & 4 Methylphenol ND
0.710 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-7Client Sample ID: SS-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:15
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.83 0.0495 mg/Kg ☼07/11/22 13:00 07/12/22 17:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.83 0.183 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4,6-Dinitro-2-methylphenol ND
0.355 0.0387 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Bromophenyl phenyl ether ND
0.355 0.0376 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Chloro-3-methylphenol ND
0.710 0.0559 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Chloroaniline ND
0.355 0.0473 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Chlorophenyl phenyl ether ND
1.83 0.0527 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Nitroaniline ND
1.83 0.355 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼4-Nitrophenol ND
0.355 0.0441 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Acenaphthene ND
0.355 0.0387 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Acenaphthylene ND
0.355 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Acetophenone ND
0.355 0.0269 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Anthracene ND
0.355 0.0247 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Atrazine ND
0.355 0.0624 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzaldehyde ND
0.355 0.0290 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzo[a]anthracene ND
0.355 0.0559 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzo[a]pyrene ND
0.355 0.0409 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzo[b]fluoranthene ND
0.355 0.0237 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzo[g,h,i]perylene ND
0.355 0.0699 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Benzo[k]fluoranthene ND
0.355 0.0323 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼bis (2-chloroisopropyl) ether ND
0.355 0.0419 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Bis(2-chloroethoxy)methane ND
0.355 0.0484 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Bis(2-chloroethyl)ether ND
0.355 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Bis(2-ethylhexyl) phthalate 0.0731 J B
0.355 0.0280 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Butyl benzyl phthalate ND
0.355 0.0710 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Caprolactam ND
0.355 0.0323 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Carbazole ND
0.355 0.0226 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Chrysene ND
0.355 0.0419 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Dibenz(a,h)anthracene ND
0.355 0.0355 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Dibenzofuran ND
0.355 0.0398 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Diethyl phthalate ND
0.355 0.0366 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Dimethyl phthalate ND
0.355 0.0323 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Di-n-butyl phthalate ND
0.355 0.0312 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Di-n-octyl phthalate ND
0.355 0.0344 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Fluoranthene ND
0.355 0.0387 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Fluorene ND
0.355 0.0419 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Hexachlorobenzene ND
0.355 0.0387 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Hexachlorobutadiene ND
0.355 0.0441 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Hexachlorocyclopentadiene ND
0.355 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Hexachloroethane ND
0.355 0.0301 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Indeno[1,2,3-cd]pyrene ND
0.355 0.0355 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Isophorone ND
0.355 0.0323 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Naphthalene ND
0.355 0.0280 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Nitrobenzene ND
0.355 0.0344 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼N-Nitrosodi-n-propylamine ND
0.355 0.0355 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼N-Nitrosodiphenylamine ND
1.83 0.355 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Pentachlorophenol ND
0.355 0.0290 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Phenanthrene ND
0.355 0.0366 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Phenol ND
0.355 0.0290 mg/Kg 07/11/22 13:00 07/12/22 17:41 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-7Client Sample ID: SS-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:15
Percent Solids: 88.3Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)64 21-132 07/11/22 13:00 07/12/22 17:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)60 07/11/22 13:00 07/12/22 17:41 125-130
2-Fluorophenol (Surr)46 07/11/22 13:00 07/12/22 17:41 118-130
Nitrobenzene-d5 (Surr)50 07/11/22 13:00 07/12/22 17:41 119-130
Phenol-d5 (Surr)50 07/11/22 13:00 07/12/22 17:41 121-130
Terphenyl-d14 (Surr)74 07/11/22 13:00 07/12/22 17:41 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 0.854 0.327 0.109 mg/Kg ☼07/01/22 07:41 07/01/22 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.545 0.0654 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Barium 43.0
0.0545 0.0163 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Cadmium 0.0163 J
1.09 0.120 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Chromium 13.0 B
0.218 0.0545 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Lead 11.1
0.545 0.109 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Selenium 0.954
0.109 0.0109 mg/Kg 07/01/22 07:41 07/01/22 16:20 1☼Silver 0.0196 J
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0526 0.0248 0.00795 mg/Kg ☼07/05/22 16:32 07/06/22 11:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-8Client Sample ID: SG-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:50
Percent Solids: 81.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00467 0.00121 mg/Kg ☼07/05/22 15:31 07/08/22 20:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1,1-Trichloroethane ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1,2,2-Tetrachloroethane ND
0.00467 0.00271 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00467 0.00140 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1,2-Trichloroethane ND
0.00467 0.00271 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1-Dichloroethane ND
0.00467 0.00336 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1-Dichloroethene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,1-Dichloropropene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2,3-Trichlorobenzene ND
0.00467 0.00168 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2,3-Trichloropropane ND
0.00467 0.00234 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2,4-Trichlorobenzene ND
0.00467 0.00234 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2,4-Trimethylbenzene ND
0.00934 0.00149 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2-Dibromo-3-Chloropropane ND
0.00467 0.00159 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2-Dichlorobenzene ND
0.00467 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2-Dichloroethane ND
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,2-Dichloropropane ND
0.00467 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,3,5-Trimethylbenzene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,3-Dichlorobenzene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,3-Dichloropropane ND
0.00467 0.00168 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼1,4-Dichlorobenzene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼2,2-Dichloropropane ND
0.0234 0.00859 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼2-Butanone (MEK)ND
0.00467 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼2-Chlorotoluene ND
0.0234 0.0177 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼2-Hexanone ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼4-Chlorotoluene ND
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼4-Isopropyltoluene ND
0.0234 0.0168 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼4-Methyl-2-pentanone (MIBK)ND
0.0467 0.0103 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Acetone 0.0201 J B
0.00467 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Benzene ND
0.00467 0.00159 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Bromobenzene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Bromoform ND
0.00467 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Bromomethane ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Carbon disulfide ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Carbon tetrachloride ND
0.00467 0.00131 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chlorobenzene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chlorobromomethane ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chlorodibromomethane ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chloroethane ND *+
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chloroform ND
0.00467 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Chloromethane ND
0.00467 0.00271 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼cis-1,2-Dichloroethene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼cis-1,3-Dichloropropene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Dibromomethane ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Dichlorobromomethane ND
0.00467 0.00299 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Dichlorodifluoromethane ND
0.00934 0.00934 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Ethyl acetate ND
0.00467 0.00196 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Ethylbenzene ND
0.00467 0.00159 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Ethylene Dibromide ND
0.00467 0.00383 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-8Client Sample ID: SG-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:50
Percent Solids: 81.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00467 0.00159 mg/Kg ☼07/05/22 15:31 07/08/22 20:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00467 0.00159 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Iodomethane ND
0.00934 0.00140 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Isopropyl ether ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Isopropylbenzene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼m,p-Xylene ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Methyl tert-butyl ether ND
0.00934 0.00747 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Methylene Chloride ND
0.00467 0.00290 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Naphthalene ND
0.00467 0.00177 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼n-Butylbenzene ND
0.00467 0.00402 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼n-Heptane ND
0.00467 0.00206 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼N-Propylbenzene ND
0.00467 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼o-Xylene ND
0.00467 0.00187 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼sec-Butylbenzene ND
0.00467 0.00177 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Styrene ND
0.00467 0.00234 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼tert-Butylbenzene ND
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Tetrachloroethene ND
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Toluene ND
0.00467 0.00215 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼trans-1,2-Dichloroethene ND
0.00467 0.00243 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼trans-1,3-Dichloropropene ND
0.00934 0.00224 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼trans-1,4-Dichloro-2-butene ND
0.00467 0.00168 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Trichloroethene ND
0.00467 0.00290 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Trichlorofluoromethane ND
0.00934 0.00514 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Vinyl acetate ND *+
0.00467 0.00262 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Vinyl chloride ND
0.00934 0.00336 mg/Kg 07/05/22 15:31 07/08/22 20:35 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)122 65-130 07/05/22 15:31 07/08/22 20:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)108 07/05/22 15:31 07/08/22 20:35 165-130
Dibromofluoromethane (Surr)105 07/05/22 15:31 07/08/22 20:35 165-130
Toluene-d8 (Surr)99 07/05/22 15:31 07/08/22 20:35 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.97 1.97 mg/Kg ☼07/11/22 13:00 07/12/22 18:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4,5-Trichlorophenol ND
0.382 0.0336 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4,6-Trichlorophenol ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4-Dichlorophenol ND
0.382 0.0510 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4-Dimethylphenol ND
1.97 0.961 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4-Dinitrophenol ND
0.382 0.0568 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,4-Dinitrotoluene ND
0.382 0.0487 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2,6-Dinitrotoluene ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Chloronaphthalene ND
0.382 0.0463 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Chlorophenol ND
0.382 0.0440 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Methylnaphthalene ND
0.382 0.0313 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Methylphenol ND
1.97 0.0521 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Nitroaniline ND
0.382 0.0475 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼2-Nitrophenol ND
0.382 0.0498 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼3 & 4 Methylphenol ND
0.765 0.0324 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-8Client Sample ID: SG-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:50
Percent Solids: 81.6Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.97 0.0533 mg/Kg ☼07/11/22 13:00 07/12/22 18:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.97 0.197 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4,6-Dinitro-2-methylphenol ND
0.382 0.0417 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Bromophenyl phenyl ether ND
0.382 0.0405 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Chloro-3-methylphenol ND
0.765 0.0602 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Chloroaniline ND
0.382 0.0510 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Chlorophenyl phenyl ether ND
1.97 0.0568 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Nitroaniline ND
1.97 0.382 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼4-Nitrophenol ND
0.382 0.0475 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Acenaphthene ND
0.382 0.0417 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Acenaphthylene ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Acetophenone ND
0.382 0.0290 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Anthracene ND
0.382 0.0266 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Atrazine ND
0.382 0.0672 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzaldehyde ND
0.382 0.0313 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzo[a]anthracene ND
0.382 0.0602 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzo[a]pyrene ND
0.382 0.0440 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzo[b]fluoranthene ND
0.382 0.0255 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzo[g,h,i]perylene ND
0.382 0.0753 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Benzo[k]fluoranthene ND
0.382 0.0348 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼bis (2-chloroisopropyl) ether ND
0.382 0.0452 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Bis(2-chloroethoxy)methane ND
0.382 0.0521 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Bis(2-chloroethyl)ether ND
0.382 0.0336 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Bis(2-ethylhexyl) phthalate 0.0606 J B
0.382 0.0301 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Butyl benzyl phthalate ND
0.382 0.0765 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Caprolactam ND
0.382 0.0348 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Carbazole ND
0.382 0.0243 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Chrysene ND
0.382 0.0452 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Dibenz(a,h)anthracene ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Dibenzofuran ND
0.382 0.0429 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Diethyl phthalate ND
0.382 0.0394 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Dimethyl phthalate ND
0.382 0.0348 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Di-n-butyl phthalate ND
0.382 0.0336 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Di-n-octyl phthalate ND
0.382 0.0371 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Fluoranthene ND
0.382 0.0417 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Fluorene ND
0.382 0.0452 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Hexachlorobenzene ND
0.382 0.0417 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Hexachlorobutadiene ND
0.382 0.0475 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Hexachlorocyclopentadiene ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Hexachloroethane ND
0.382 0.0324 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Indeno[1,2,3-cd]pyrene ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Isophorone ND
0.382 0.0348 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Naphthalene ND
0.382 0.0301 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Nitrobenzene ND
0.382 0.0371 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼N-Nitrosodi-n-propylamine ND
0.382 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼N-Nitrosodiphenylamine ND
1.97 0.382 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Pentachlorophenol ND
0.382 0.0313 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Phenanthrene ND
0.382 0.0394 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Phenol ND
0.382 0.0313 mg/Kg 07/11/22 13:00 07/12/22 18:04 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-8Client Sample ID: SG-1 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:50
Percent Solids: 81.6Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)60 21-132 07/11/22 13:00 07/12/22 18:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)55 07/11/22 13:00 07/12/22 18:04 125-130
2-Fluorophenol (Surr)47 07/11/22 13:00 07/12/22 18:04 118-130
Nitrobenzene-d5 (Surr)48 07/11/22 13:00 07/12/22 18:04 119-130
Phenol-d5 (Surr)49 07/11/22 13:00 07/12/22 18:04 121-130
Terphenyl-d14 (Surr)75 07/11/22 13:00 07/12/22 18:04 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 0.641 0.360 0.120 mg/Kg ☼07/01/22 07:41 07/01/22 16:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.600 0.0720 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Barium 23.2
0.0600 0.0180 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Cadmium ND
1.20 0.132 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Chromium 14.0 B
0.240 0.0600 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Lead 7.48
0.600 0.120 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Selenium 0.422 J
0.120 0.0120 mg/Kg 07/01/22 07:41 07/01/22 16:23 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0221 J 0.0278 0.00891 mg/Kg ☼07/05/22 16:32 07/06/22 11:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-9Client Sample ID: SG-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:15
Percent Solids: 85.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00453 0.00118 mg/Kg ☼07/05/22 15:31 07/08/22 19:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1,1-Trichloroethane ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1,2,2-Tetrachloroethane ND
0.00453 0.00263 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00453 0.00136 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1,2-Trichloroethane ND
0.00453 0.00263 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1-Dichloroethane ND
0.00453 0.00326 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1-Dichloroethene ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,1-Dichloropropene ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2,3-Trichlorobenzene ND
0.00453 0.00163 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2,3-Trichloropropane ND
0.00453 0.00227 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2,4-Trichlorobenzene ND
0.00453 0.00227 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2,4-Trimethylbenzene 0.0211
0.00907 0.00145 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2-Dibromo-3-Chloropropane ND
0.00453 0.00154 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2-Dichlorobenzene ND
0.00453 0.00209 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2-Dichloroethane ND
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,2-Dichloropropane ND
0.00453 0.00218 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,3,5-Trimethylbenzene 0.00931
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,3-Dichlorobenzene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,3-Dichloropropane ND
0.00453 0.00163 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼1,4-Dichlorobenzene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼2,2-Dichloropropane ND
0.0227 0.00834 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼2-Butanone (MEK)ND
0.00453 0.00209 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼2-Chlorotoluene ND
0.0227 0.0172 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼2-Hexanone ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼4-Chlorotoluene ND
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼4-Isopropyltoluene ND
0.0227 0.0163 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼4-Methyl-2-pentanone (MIBK)ND
0.0453 0.00997 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Acetone 0.0349 J B
0.00453 0.00218 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Benzene ND
0.00453 0.00154 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Bromobenzene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Bromoform ND
0.00453 0.00218 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Bromomethane ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Carbon disulfide ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Carbon tetrachloride ND
0.00453 0.00127 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chlorobenzene ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chlorobromomethane ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chlorodibromomethane ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chloroethane ND *+
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chloroform ND
0.00453 0.00218 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Chloromethane ND
0.00453 0.00263 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼cis-1,2-Dichloroethene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼cis-1,3-Dichloropropene ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Dibromomethane ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Dichlorobromomethane ND
0.00453 0.00290 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Dichlorodifluoromethane ND
0.00907 0.00907 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Ethyl acetate ND
0.00453 0.00190 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Ethylbenzene ND
0.00453 0.00154 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Ethylene Dibromide ND
0.00453 0.00372 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-9Client Sample ID: SG-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:15
Percent Solids: 85.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane 0.0584 0.00453 0.00154 mg/Kg ☼07/05/22 15:31 07/08/22 19:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00453 0.00154 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Iodomethane ND
0.00907 0.00136 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Isopropyl ether ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Isopropylbenzene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼m,p-Xylene ND
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Methyl tert-butyl ether ND
0.00907 0.00725 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Methylene Chloride ND
0.00453 0.00281 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Naphthalene ND
0.00453 0.00172 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼n-Butylbenzene 0.00288 J
0.00453 0.00390 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼n-Heptane 0.0590
0.00453 0.00199 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼N-Propylbenzene 0.00362 J
0.00453 0.00209 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼o-Xylene ND
0.00453 0.00181 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼sec-Butylbenzene ND
0.00453 0.00172 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Styrene ND
0.00453 0.00227 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼tert-Butylbenzene ND
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Tetrachloroethene ND
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Toluene ND
0.00453 0.00209 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼trans-1,2-Dichloroethene ND
0.00453 0.00236 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼trans-1,3-Dichloropropene ND
0.00907 0.00218 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼trans-1,4-Dichloro-2-butene ND
0.00453 0.00163 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Trichloroethene ND
0.00453 0.00281 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Trichlorofluoromethane ND
0.00907 0.00499 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Vinyl acetate ND *+
0.00453 0.00254 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Vinyl chloride ND
0.00907 0.00326 mg/Kg 07/05/22 15:31 07/08/22 19:11 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)129 65-130 07/05/22 15:31 07/08/22 19:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 07/05/22 15:31 07/08/22 19:11 165-130
Dibromofluoromethane (Surr)115 07/05/22 15:31 07/08/22 19:11 165-130
Toluene-d8 (Surr)97 07/05/22 15:31 07/08/22 19:11 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.92 1.92 mg/Kg ☼07/11/22 13:00 07/12/22 18:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.372 0.0395 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4,5-Trichlorophenol ND
0.372 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4,6-Trichlorophenol ND
0.372 0.0395 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4-Dichlorophenol ND
0.372 0.0496 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4-Dimethylphenol ND
1.92 0.936 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4-Dinitrophenol ND
0.372 0.0552 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,4-Dinitrotoluene ND
0.372 0.0473 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2,6-Dinitrotoluene ND
0.372 0.0395 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Chloronaphthalene ND
0.372 0.0451 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Chlorophenol ND
0.372 0.0428 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Methylnaphthalene ND
0.372 0.0304 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Methylphenol ND
1.92 0.0507 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Nitroaniline ND
0.372 0.0462 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼2-Nitrophenol ND
0.372 0.0485 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼3 & 4 Methylphenol ND
0.744 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-9Client Sample ID: SG-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:15
Percent Solids: 85.6Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.92 0.0519 mg/Kg ☼07/11/22 13:00 07/12/22 18:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.92 0.192 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4,6-Dinitro-2-methylphenol ND
0.372 0.0406 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Bromophenyl phenyl ether ND
0.372 0.0395 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Chloro-3-methylphenol ND
0.744 0.0586 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Chloroaniline ND
0.372 0.0496 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Chlorophenyl phenyl ether ND
1.92 0.0552 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Nitroaniline ND
1.92 0.372 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼4-Nitrophenol ND
0.372 0.0462 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Acenaphthene ND
0.372 0.0406 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Acenaphthylene ND
0.372 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Acetophenone ND
0.372 0.0282 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Anthracene ND
0.372 0.0259 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Atrazine ND
0.372 0.0654 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzaldehyde ND
0.372 0.0304 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzo[a]anthracene ND
0.372 0.0586 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzo[a]pyrene ND
0.372 0.0428 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzo[b]fluoranthene ND
0.372 0.0248 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzo[g,h,i]perylene ND
0.372 0.0733 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Benzo[k]fluoranthene ND
0.372 0.0338 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼bis (2-chloroisopropyl) ether ND
0.372 0.0440 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Bis(2-chloroethoxy)methane ND
0.372 0.0507 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Bis(2-chloroethyl)ether ND
0.372 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Bis(2-ethylhexyl) phthalate 0.0685 J B
0.372 0.0293 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Butyl benzyl phthalate ND
0.372 0.0744 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Caprolactam ND
0.372 0.0338 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Carbazole ND
0.372 0.0237 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Chrysene ND
0.372 0.0440 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Dibenz(a,h)anthracene ND
0.372 0.0372 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Dibenzofuran ND
0.372 0.0417 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Diethyl phthalate ND
0.372 0.0383 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Dimethyl phthalate ND
0.372 0.0338 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Di-n-butyl phthalate ND
0.372 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Di-n-octyl phthalate ND
0.372 0.0361 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Fluoranthene ND
0.372 0.0406 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Fluorene ND
0.372 0.0440 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Hexachlorobenzene ND
0.372 0.0406 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Hexachlorobutadiene ND
0.372 0.0462 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Hexachlorocyclopentadiene ND
0.372 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Hexachloroethane ND
0.372 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Indeno[1,2,3-cd]pyrene ND
0.372 0.0372 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Isophorone ND
0.372 0.0338 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Naphthalene ND
0.372 0.0293 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Nitrobenzene ND
0.372 0.0361 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼N-Nitrosodi-n-propylamine ND
0.372 0.0372 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼N-Nitrosodiphenylamine ND
1.92 0.372 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Pentachlorophenol ND
0.372 0.0304 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Phenanthrene ND
0.372 0.0383 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Phenol ND
0.372 0.0304 mg/Kg 07/11/22 13:00 07/12/22 18:26 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-9Client Sample ID: SG-2 (2-6)
Matrix: SoilDate Collected: 06/29/22 11:15
Percent Solids: 85.6Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)63 21-132 07/11/22 13:00 07/12/22 18:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)53 07/11/22 13:00 07/12/22 18:26 125-130
2-Fluorophenol (Surr)46 07/11/22 13:00 07/12/22 18:26 118-130
Nitrobenzene-d5 (Surr)46 07/11/22 13:00 07/12/22 18:26 119-130
Phenol-d5 (Surr)49 07/11/22 13:00 07/12/22 18:26 121-130
Terphenyl-d14 (Surr)72 07/11/22 13:00 07/12/22 18:26 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.50 0.337 0.112 mg/Kg ☼07/01/22 07:41 07/01/22 16:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.562 0.0674 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Barium 16.4
0.0562 0.0169 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Cadmium ND
1.12 0.124 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Chromium 13.2 B
0.225 0.0562 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Lead 6.17
0.562 0.112 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Selenium 0.705
0.112 0.0112 mg/Kg 07/01/22 07:41 07/01/22 16:25 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0141 J 0.0252 0.00806 mg/Kg ☼07/05/22 16:32 07/06/22 11:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-10Client Sample ID: SG-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:05
Percent Solids: 86.8Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00496 0.00129 mg/Kg ☼07/05/22 15:31 07/08/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1,1-Trichloroethane ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1,2,2-Tetrachloroethane ND
0.00496 0.00287 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00496 0.00149 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1,2-Trichloroethane ND
0.00496 0.00287 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1-Dichloroethane ND
0.00496 0.00357 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1-Dichloroethene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,1-Dichloropropene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2,3-Trichlorobenzene ND
0.00496 0.00178 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2,3-Trichloropropane ND
0.00496 0.00248 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2,4-Trichlorobenzene ND
0.00496 0.00248 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2,4-Trimethylbenzene ND
0.00991 0.00159 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2-Dibromo-3-Chloropropane ND
0.00496 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2-Dichlorobenzene ND
0.00496 0.00228 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2-Dichloroethane ND
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,2-Dichloropropane ND
0.00496 0.00238 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,3,5-Trimethylbenzene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,3-Dichlorobenzene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,3-Dichloropropane ND
0.00496 0.00178 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼1,4-Dichlorobenzene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼2,2-Dichloropropane ND
0.0248 0.00912 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼2-Butanone (MEK)ND
0.00496 0.00228 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼2-Chlorotoluene ND
0.0248 0.0188 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼2-Hexanone ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼4-Chlorotoluene ND
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼4-Isopropyltoluene ND
0.0248 0.0178 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼4-Methyl-2-pentanone (MIBK)ND
0.0496 0.0109 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Acetone 0.0398 J B
0.00496 0.00238 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Benzene ND
0.00496 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Bromobenzene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Bromoform ND
0.00496 0.00238 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Bromomethane ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Carbon disulfide ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Carbon tetrachloride ND
0.00496 0.00139 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chlorobenzene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chlorobromomethane ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chlorodibromomethane ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chloroethane ND *+
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chloroform ND
0.00496 0.00238 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Chloromethane ND
0.00496 0.00287 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼cis-1,2-Dichloroethene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼cis-1,3-Dichloropropene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Dibromomethane ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Dichlorobromomethane ND
0.00496 0.00317 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Dichlorodifluoromethane ND
0.00991 0.00991 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Ethyl acetate ND
0.00496 0.00208 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Ethylbenzene ND
0.00496 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Ethylene Dibromide ND
0.00496 0.00406 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-10Client Sample ID: SG-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:05
Percent Solids: 86.8Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00496 0.00168 mg/Kg ☼07/05/22 15:31 07/08/22 18:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00496 0.00168 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Iodomethane ND
0.00991 0.00149 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Isopropyl ether ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Isopropylbenzene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼m,p-Xylene ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Methyl tert-butyl ether ND
0.00991 0.00793 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Methylene Chloride ND
0.00496 0.00307 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Naphthalene ND
0.00496 0.00188 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼n-Butylbenzene ND
0.00496 0.00426 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼n-Heptane ND
0.00496 0.00218 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼N-Propylbenzene ND
0.00496 0.00228 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼o-Xylene ND
0.00496 0.00198 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼sec-Butylbenzene ND
0.00496 0.00188 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Styrene ND
0.00496 0.00248 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼tert-Butylbenzene ND
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Tetrachloroethene ND
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Toluene ND
0.00496 0.00228 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼trans-1,2-Dichloroethene ND
0.00496 0.00258 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼trans-1,3-Dichloropropene ND
0.00991 0.00238 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼trans-1,4-Dichloro-2-butene ND
0.00496 0.00178 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Trichloroethene ND
0.00496 0.00307 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Trichlorofluoromethane ND
0.00991 0.00545 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Vinyl acetate ND *+
0.00496 0.00278 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Vinyl chloride ND
0.00991 0.00357 mg/Kg 07/05/22 15:31 07/08/22 18:50 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)117 65-130 07/05/22 15:31 07/08/22 18:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 07/05/22 15:31 07/08/22 18:50 165-130
Dibromofluoromethane (Surr)111 07/05/22 15:31 07/08/22 18:50 165-130
Toluene-d8 (Surr)100 07/05/22 15:31 07/08/22 18:50 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.85 1.85 mg/Kg ☼07/11/22 13:00 07/12/22 18:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.360 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4,5-Trichlorophenol ND
0.360 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4,6-Trichlorophenol ND
0.360 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4-Dichlorophenol ND
0.360 0.0480 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4-Dimethylphenol ND
1.85 0.905 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4-Dinitrophenol ND
0.360 0.0535 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,4-Dinitrotoluene ND
0.360 0.0458 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2,6-Dinitrotoluene ND
0.360 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Chloronaphthalene ND
0.360 0.0436 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Chlorophenol ND
0.360 0.0415 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Methylnaphthalene ND
0.360 0.0295 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Methylphenol ND
1.85 0.0491 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Nitroaniline ND
0.360 0.0447 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼2-Nitrophenol ND
0.360 0.0469 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼3 & 4 Methylphenol ND
0.720 0.0305 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-10Client Sample ID: SG-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:05
Percent Solids: 86.8Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.85 0.0502 mg/Kg ☼07/11/22 13:00 07/12/22 18:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.85 0.185 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4,6-Dinitro-2-methylphenol ND
0.360 0.0393 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Bromophenyl phenyl ether ND
0.360 0.0382 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Chloro-3-methylphenol ND
0.720 0.0567 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Chloroaniline ND
0.360 0.0480 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Chlorophenyl phenyl ether ND
1.85 0.0535 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Nitroaniline ND
1.85 0.360 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼4-Nitrophenol ND
0.360 0.0447 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Acenaphthene ND
0.360 0.0393 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Acenaphthylene ND
0.360 0.0305 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Acetophenone ND
0.360 0.0273 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Anthracene ND
0.360 0.0251 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Atrazine ND
0.360 0.0633 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzaldehyde ND
0.360 0.0295 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzo[a]anthracene ND
0.360 0.0567 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzo[a]pyrene ND
0.360 0.0415 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzo[b]fluoranthene ND
0.360 0.0240 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzo[g,h,i]perylene ND
0.360 0.0709 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Benzo[k]fluoranthene ND
0.360 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼bis (2-chloroisopropyl) ether ND
0.360 0.0425 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Bis(2-chloroethoxy)methane ND
0.360 0.0491 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Bis(2-chloroethyl)ether ND
0.360 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Bis(2-ethylhexyl) phthalate 0.0628 J B
0.360 0.0284 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Butyl benzyl phthalate ND
0.360 0.0720 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Caprolactam ND
0.360 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Carbazole ND
0.360 0.0229 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Chrysene ND
0.360 0.0425 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Dibenz(a,h)anthracene ND
0.360 0.0360 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Dibenzofuran ND
0.360 0.0404 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Diethyl phthalate ND
0.360 0.0371 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Dimethyl phthalate ND
0.360 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Di-n-butyl phthalate ND
0.360 0.0316 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Di-n-octyl phthalate ND
0.360 0.0349 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Fluoranthene ND
0.360 0.0393 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Fluorene ND
0.360 0.0425 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Hexachlorobenzene ND
0.360 0.0393 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Hexachlorobutadiene ND
0.360 0.0447 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Hexachlorocyclopentadiene ND
0.360 0.0305 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Hexachloroethane ND
0.360 0.0305 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Indeno[1,2,3-cd]pyrene ND
0.360 0.0360 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Isophorone ND
0.360 0.0327 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Naphthalene ND
0.360 0.0284 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Nitrobenzene ND
0.360 0.0349 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼N-Nitrosodi-n-propylamine ND
0.360 0.0360 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼N-Nitrosodiphenylamine ND
1.85 0.360 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Pentachlorophenol ND
0.360 0.0295 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Phenanthrene ND
0.360 0.0371 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Phenol ND
0.360 0.0295 mg/Kg 07/11/22 13:00 07/12/22 18:48 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-10Client Sample ID: SG-3 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:05
Percent Solids: 86.8Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)64 21-132 07/11/22 13:00 07/12/22 18:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 07/11/22 13:00 07/12/22 18:48 125-130
2-Fluorophenol (Surr)52 07/11/22 13:00 07/12/22 18:48 118-130
Nitrobenzene-d5 (Surr)56 07/11/22 13:00 07/12/22 18:48 119-130
Phenol-d5 (Surr)55 07/11/22 13:00 07/12/22 18:48 121-130
Terphenyl-d14 (Surr)71 07/11/22 13:00 07/12/22 18:48 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.12 0.317 0.106 mg/Kg ☼07/01/22 07:41 07/01/22 16:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.528 0.0634 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Barium 17.6
0.0528 0.0159 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Cadmium ND
1.06 0.116 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Chromium 11.4 B
0.211 0.0528 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Lead 6.28
0.528 0.106 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Selenium 0.404 J
0.106 0.0106 mg/Kg 07/01/22 07:41 07/01/22 16:28 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0239 J 0.0257 0.00823 mg/Kg ☼07/05/22 16:32 07/06/22 11:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-11Client Sample ID: SG-4 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:25
Percent Solids: 82.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00529 0.00138 mg/Kg ☼07/05/22 15:31 07/08/22 18:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1,1-Trichloroethane ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1,2,2-Tetrachloroethane ND
0.00529 0.00307 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00529 0.00159 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1,2-Trichloroethane ND
0.00529 0.00307 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1-Dichloroethane ND
0.00529 0.00381 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1-Dichloroethene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,1-Dichloropropene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2,3-Trichlorobenzene ND
0.00529 0.00191 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2,3-Trichloropropane ND
0.00529 0.00265 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2,4-Trichlorobenzene ND
0.00529 0.00265 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2,4-Trimethylbenzene ND
0.0106 0.00169 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2-Dibromo-3-Chloropropane ND
0.00529 0.00180 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2-Dichlorobenzene ND
0.00529 0.00243 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2-Dichloroethane ND
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,2-Dichloropropane ND
0.00529 0.00254 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,3,5-Trimethylbenzene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,3-Dichlorobenzene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,3-Dichloropropane ND
0.00529 0.00191 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼1,4-Dichlorobenzene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼2,2-Dichloropropane ND
0.0265 0.00974 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼2-Butanone (MEK)0.0119 J
0.00529 0.00243 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼2-Chlorotoluene ND
0.0265 0.0201 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼2-Hexanone ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼4-Chlorotoluene ND
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼4-Isopropyltoluene ND
0.0265 0.0191 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼4-Methyl-2-pentanone (MIBK)ND
0.0529 0.0116 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Acetone 0.0929 B
0.00529 0.00254 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Benzene ND
0.00529 0.00180 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Bromobenzene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Bromoform ND
0.00529 0.00254 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Bromomethane ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Carbon disulfide ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Carbon tetrachloride ND
0.00529 0.00148 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chlorobenzene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chlorobromomethane ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chlorodibromomethane ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chloroethane ND *+
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chloroform ND
0.00529 0.00254 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Chloromethane ND
0.00529 0.00307 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼cis-1,2-Dichloroethene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼cis-1,3-Dichloropropene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Dibromomethane ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Dichlorobromomethane ND
0.00529 0.00339 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Dichlorodifluoromethane ND
0.0106 0.0106 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Ethyl acetate ND
0.00529 0.00222 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Ethylbenzene ND
0.00529 0.00180 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Ethylene Dibromide ND
0.00529 0.00434 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-11Client Sample ID: SG-4 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:25
Percent Solids: 82.6Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00529 0.00180 mg/Kg ☼07/05/22 15:31 07/08/22 18:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00529 0.00180 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Iodomethane ND
0.0106 0.00159 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Isopropyl ether ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Isopropylbenzene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼m,p-Xylene ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Methyl tert-butyl ether ND
0.0106 0.00847 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Methylene Chloride ND
0.00529 0.00328 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Naphthalene 0.0168
0.00529 0.00201 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼n-Butylbenzene ND
0.00529 0.00455 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼n-Heptane ND
0.00529 0.00233 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼N-Propylbenzene ND
0.00529 0.00243 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼o-Xylene ND
0.00529 0.00212 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼sec-Butylbenzene ND
0.00529 0.00201 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Styrene ND
0.00529 0.00265 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼tert-Butylbenzene ND
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Tetrachloroethene ND
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Toluene ND
0.00529 0.00243 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼trans-1,2-Dichloroethene ND
0.00529 0.00275 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼trans-1,3-Dichloropropene ND
0.0106 0.00254 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼trans-1,4-Dichloro-2-butene ND
0.00529 0.00191 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Trichloroethene ND
0.00529 0.00328 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Trichlorofluoromethane ND
0.0106 0.00582 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Vinyl acetate ND *+
0.00529 0.00296 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Vinyl chloride ND
0.0106 0.00381 mg/Kg 07/05/22 15:31 07/08/22 18:29 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)121 65-130 07/05/22 15:31 07/08/22 18:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)103 07/05/22 15:31 07/08/22 18:29 165-130
Dibromofluoromethane (Surr)104 07/05/22 15:31 07/08/22 18:29 165-130
Toluene-d8 (Surr)101 07/05/22 15:31 07/08/22 18:29 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.02 2.02 mg/Kg ☼07/11/22 13:00 07/12/22 19:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.392 0.0416 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4,5-Trichlorophenol ND
0.392 0.0345 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4,6-Trichlorophenol ND
0.392 0.0416 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4-Dichlorophenol ND
0.392 0.0523 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4-Dimethylphenol ND
2.02 0.986 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4-Dinitrophenol ND
0.392 0.0582 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,4-Dinitrotoluene ND
0.392 0.0499 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2,6-Dinitrotoluene ND
0.392 0.0416 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Chloronaphthalene ND
0.392 0.0475 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Chlorophenol ND
0.392 0.0452 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Methylnaphthalene ND
0.392 0.0321 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Methylphenol ND
2.02 0.0535 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Nitroaniline ND
0.392 0.0487 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼2-Nitrophenol ND
0.392 0.0511 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼3 & 4 Methylphenol ND
0.784 0.0333 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-11Client Sample ID: SG-4 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:25
Percent Solids: 82.6Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.02 0.0547 mg/Kg ☼07/11/22 13:00 07/12/22 19:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.02 0.202 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4,6-Dinitro-2-methylphenol ND
0.392 0.0428 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Bromophenyl phenyl ether ND
0.392 0.0416 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Chloro-3-methylphenol ND
0.784 0.0618 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Chloroaniline ND
0.392 0.0523 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Chlorophenyl phenyl ether ND
2.02 0.0582 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Nitroaniline ND
2.02 0.392 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼4-Nitrophenol ND
0.392 0.0487 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Acenaphthene ND
0.392 0.0428 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Acenaphthylene ND
0.392 0.0333 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Acetophenone ND
0.392 0.0297 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Anthracene ND
0.392 0.0273 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Atrazine ND
0.392 0.0689 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzaldehyde ND
0.392 0.0321 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzo[a]anthracene 0.0405 J
0.392 0.0618 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzo[a]pyrene ND
0.392 0.0452 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzo[b]fluoranthene 0.0484 J
0.392 0.0261 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzo[g,h,i]perylene 0.0299 J
0.392 0.0772 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Benzo[k]fluoranthene ND
0.392 0.0356 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼bis (2-chloroisopropyl) ether ND
0.392 0.0463 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Bis(2-chloroethoxy)methane ND
0.392 0.0535 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Bis(2-chloroethyl)ether ND
0.392 0.0345 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Bis(2-ethylhexyl) phthalate 0.0727 J B
0.392 0.0309 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Butyl benzyl phthalate ND
0.392 0.0784 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Caprolactam ND
0.392 0.0356 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Carbazole ND
0.392 0.0250 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Chrysene 0.0336 J
0.392 0.0463 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Dibenz(a,h)anthracene ND
0.392 0.0392 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Dibenzofuran ND
0.392 0.0440 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Diethyl phthalate ND
0.392 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Dimethyl phthalate ND
0.392 0.0356 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Di-n-butyl phthalate ND
0.392 0.0345 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Di-n-octyl phthalate ND
0.392 0.0380 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Fluoranthene 0.0616 J
0.392 0.0428 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Fluorene ND
0.392 0.0463 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Hexachlorobenzene ND
0.392 0.0428 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Hexachlorobutadiene ND
0.392 0.0487 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Hexachlorocyclopentadiene ND
0.392 0.0333 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Hexachloroethane ND
0.392 0.0333 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Indeno[1,2,3-cd]pyrene ND
0.392 0.0392 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Isophorone ND
0.392 0.0356 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Naphthalene ND
0.392 0.0309 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Nitrobenzene ND
0.392 0.0380 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼N-Nitrosodi-n-propylamine ND
0.392 0.0392 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼N-Nitrosodiphenylamine ND
2.02 0.392 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Pentachlorophenol ND
0.392 0.0321 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Phenanthrene ND
0.392 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Phenol ND
0.392 0.0321 mg/Kg 07/11/22 13:00 07/12/22 19:10 1☼Pyrene 0.0595 J
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-11Client Sample ID: SG-4 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:25
Percent Solids: 82.6Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)65 21-132 07/11/22 13:00 07/12/22 19:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)69 07/11/22 13:00 07/12/22 19:10 125-130
2-Fluorophenol (Surr)54 07/11/22 13:00 07/12/22 19:10 118-130
Nitrobenzene-d5 (Surr)57 07/11/22 13:00 07/12/22 19:10 119-130
Phenol-d5 (Surr)58 07/11/22 13:00 07/12/22 19:10 121-130
Terphenyl-d14 (Surr)71 07/11/22 13:00 07/12/22 19:10 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.52 0.349 0.116 mg/Kg ☼07/01/22 07:41 07/01/22 16:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.582 0.0699 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Barium 75.3
0.0582 0.0175 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Cadmium 0.0571 J
1.16 0.128 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Chromium 15.6 B
0.233 0.0582 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Lead 18.5
0.582 0.116 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Selenium 3.54
0.116 0.0116 mg/Kg 07/01/22 07:41 07/01/22 16:30 1☼Silver 0.0116 J
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0274 J 0.0280 0.00897 mg/Kg ☼07/05/22 16:32 07/06/22 11:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-12Client Sample ID: SG-6 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:45
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00471 0.00123 mg/Kg ☼07/05/22 15:31 07/08/22 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1,1-Trichloroethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1,2,2-Tetrachloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00471 0.00141 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1,2-Trichloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1-Dichloroethane ND
0.00471 0.00339 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1-Dichloroethene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,1-Dichloropropene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2,3-Trichlorobenzene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2,3-Trichloropropane ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2,4-Trichlorobenzene ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2,4-Trimethylbenzene ND
0.00942 0.00151 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2-Dibromo-3-Chloropropane ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2-Dichlorobenzene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2-Dichloroethane ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,2-Dichloropropane ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,3,5-Trimethylbenzene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,3-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,3-Dichloropropane ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼1,4-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼2,2-Dichloropropane ND
0.0236 0.00867 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼2-Butanone (MEK)0.00982 J
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼2-Chlorotoluene ND
0.0236 0.0179 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼2-Hexanone ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼4-Chlorotoluene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼4-Isopropyltoluene ND
0.0236 0.0170 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼4-Methyl-2-pentanone (MIBK)ND
0.0471 0.0104 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Acetone 0.140 B
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Benzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Bromobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Bromoform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Bromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Carbon disulfide ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Carbon tetrachloride ND
0.00471 0.00132 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chlorobenzene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chlorobromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chlorodibromomethane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chloroethane ND *+
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chloroform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Chloromethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼cis-1,2-Dichloroethene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼cis-1,3-Dichloropropene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Dibromomethane ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Dichlorobromomethane ND
0.00471 0.00302 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Dichlorodifluoromethane ND
0.00942 0.00942 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Ethyl acetate ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Ethylbenzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Ethylene Dibromide ND
0.00471 0.00386 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-12Client Sample ID: SG-6 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:45
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00471 0.00160 mg/Kg ☼07/05/22 15:31 07/08/22 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Iodomethane ND
0.00942 0.00141 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Isopropyl ether ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Isopropylbenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼m,p-Xylene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Methyl tert-butyl ether ND
0.00942 0.00754 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Methylene Chloride ND
0.00471 0.00292 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Naphthalene ND
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼n-Butylbenzene ND
0.00471 0.00405 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼n-Heptane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼N-Propylbenzene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼o-Xylene ND
0.00471 0.00188 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼sec-Butylbenzene ND
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Styrene ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼tert-Butylbenzene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Tetrachloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Toluene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼trans-1,2-Dichloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼trans-1,3-Dichloropropene ND
0.00942 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼trans-1,4-Dichloro-2-butene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Trichloroethene ND
0.00471 0.00292 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Trichlorofluoromethane ND
0.00942 0.00518 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Vinyl acetate ND *+
0.00471 0.00264 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Vinyl chloride ND
0.00942 0.00339 mg/Kg 07/05/22 15:31 07/08/22 17:47 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)112 65-130 07/05/22 15:31 07/08/22 17:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 07/05/22 15:31 07/08/22 17:47 165-130
Dibromofluoromethane (Surr)119 07/05/22 15:31 07/08/22 17:47 165-130
Toluene-d8 (Surr)101 07/05/22 15:31 07/08/22 17:47 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.91 1.91 mg/Kg ☼07/11/22 13:00 07/12/22 19:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.370 0.0393 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4,5-Trichlorophenol ND
0.370 0.0325 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4,6-Trichlorophenol ND
0.370 0.0393 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4-Dichlorophenol ND
0.370 0.0493 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4-Dimethylphenol ND
1.91 0.931 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4-Dinitrophenol ND
0.370 0.0550 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,4-Dinitrotoluene ND
0.370 0.0471 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2,6-Dinitrotoluene ND
0.370 0.0393 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Chloronaphthalene ND
0.370 0.0449 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Chlorophenol ND
0.370 0.0426 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Methylnaphthalene ND
0.370 0.0303 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Methylphenol ND
1.91 0.0505 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Nitroaniline ND
0.370 0.0460 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼2-Nitrophenol ND
0.370 0.0482 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼3 & 4 Methylphenol ND
0.740 0.0314 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-12Client Sample ID: SG-6 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:45
Percent Solids: 88.3Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 1.91 0.0516 mg/Kg ☼07/11/22 13:00 07/12/22 19:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.91 0.191 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4,6-Dinitro-2-methylphenol ND
0.370 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Bromophenyl phenyl ether ND
0.370 0.0393 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Chloro-3-methylphenol ND
0.740 0.0583 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Chloroaniline ND
0.370 0.0493 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Chlorophenyl phenyl ether ND
1.91 0.0550 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Nitroaniline ND
1.91 0.370 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼4-Nitrophenol ND
0.370 0.0460 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Acenaphthene ND
0.370 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Acenaphthylene ND
0.370 0.0314 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Acetophenone ND
0.370 0.0280 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Anthracene ND
0.370 0.0258 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Atrazine ND
0.370 0.0650 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzaldehyde ND
0.370 0.0303 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzo[a]anthracene ND
0.370 0.0583 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzo[a]pyrene ND
0.370 0.0426 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzo[b]fluoranthene ND
0.370 0.0247 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzo[g,h,i]perylene ND
0.370 0.0729 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Benzo[k]fluoranthene ND
0.370 0.0336 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼bis (2-chloroisopropyl) ether ND
0.370 0.0437 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Bis(2-chloroethoxy)methane ND
0.370 0.0505 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Bis(2-chloroethyl)ether ND
0.370 0.0325 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Bis(2-ethylhexyl) phthalate 0.0649 J B
0.370 0.0292 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Butyl benzyl phthalate ND
0.370 0.0740 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Caprolactam ND
0.370 0.0336 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Carbazole ND
0.370 0.0236 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Chrysene ND
0.370 0.0437 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Dibenz(a,h)anthracene ND
0.370 0.0370 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Dibenzofuran ND
0.370 0.0415 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Diethyl phthalate ND
0.370 0.0381 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Dimethyl phthalate ND
0.370 0.0336 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Di-n-butyl phthalate ND
0.370 0.0325 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Di-n-octyl phthalate ND
0.370 0.0359 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Fluoranthene ND
0.370 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Fluorene ND
0.370 0.0437 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Hexachlorobenzene ND
0.370 0.0404 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Hexachlorobutadiene ND
0.370 0.0460 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Hexachlorocyclopentadiene ND
0.370 0.0314 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Hexachloroethane ND
0.370 0.0314 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Indeno[1,2,3-cd]pyrene ND
0.370 0.0370 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Isophorone ND
0.370 0.0336 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Naphthalene ND
0.370 0.0292 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Nitrobenzene ND
0.370 0.0359 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼N-Nitrosodi-n-propylamine ND
0.370 0.0370 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼N-Nitrosodiphenylamine ND
1.91 0.370 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Pentachlorophenol ND
0.370 0.0303 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Phenanthrene ND
0.370 0.0381 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Phenol ND
0.370 0.0303 mg/Kg 07/11/22 13:00 07/12/22 19:32 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-12Client Sample ID: SG-6 (2-6)
Matrix: SoilDate Collected: 06/29/22 13:45
Percent Solids: 88.3Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)64 21-132 07/11/22 13:00 07/12/22 19:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)68 07/11/22 13:00 07/12/22 19:32 125-130
2-Fluorophenol (Surr)53 07/11/22 13:00 07/12/22 19:32 118-130
Nitrobenzene-d5 (Surr)58 07/11/22 13:00 07/12/22 19:32 119-130
Phenol-d5 (Surr)56 07/11/22 13:00 07/12/22 19:32 121-130
Terphenyl-d14 (Surr)72 07/11/22 13:00 07/12/22 19:32 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 3.07 0.312 0.104 mg/Kg ☼07/01/22 07:41 07/01/22 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.519 0.0623 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Barium 116
0.0519 0.0156 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Cadmium 0.0997
1.04 0.114 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Chromium 20.6 B
0.208 0.0519 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Lead 63.2
0.519 0.104 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Selenium 2.66
0.104 0.0104 mg/Kg 07/01/22 07:41 07/01/22 16:33 1☼Silver 0.0805 J
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.149 0.0262 0.00838 mg/Kg ☼07/05/22 16:32 07/06/22 12:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-13Client Sample ID: SG-7 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:30
Percent Solids: 81.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00514 0.00134 mg/Kg ☼07/05/22 15:31 07/08/22 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1,1-Trichloroethane ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1,2,2-Tetrachloroethane ND
0.00514 0.00298 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00514 0.00154 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1,2-Trichloroethane ND
0.00514 0.00298 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1-Dichloroethane ND
0.00514 0.00370 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1-Dichloroethene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,1-Dichloropropene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2,3-Trichlorobenzene ND
0.00514 0.00185 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2,3-Trichloropropane ND
0.00514 0.00257 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2,4-Trichlorobenzene ND
0.00514 0.00257 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2,4-Trimethylbenzene ND
0.0103 0.00164 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2-Dibromo-3-Chloropropane ND
0.00514 0.00175 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2-Dichlorobenzene ND
0.00514 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2-Dichloroethane ND
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,2-Dichloropropane ND
0.00514 0.00247 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,3,5-Trimethylbenzene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,3-Dichlorobenzene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,3-Dichloropropane ND
0.00514 0.00185 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼1,4-Dichlorobenzene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼2,2-Dichloropropane ND
0.0257 0.00945 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼2-Butanone (MEK)ND
0.00514 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼2-Chlorotoluene ND
0.0257 0.0195 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼2-Hexanone ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼4-Chlorotoluene ND
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼4-Isopropyltoluene ND
0.0257 0.0185 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼4-Methyl-2-pentanone (MIBK)ND
0.0514 0.0113 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Acetone 0.0802 B
0.00514 0.00247 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Benzene ND
0.00514 0.00175 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Bromobenzene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Bromoform ND
0.00514 0.00247 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Bromomethane ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Carbon disulfide ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Carbon tetrachloride ND
0.00514 0.00144 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chlorobenzene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chlorobromomethane ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chlorodibromomethane ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chloroethane ND *+
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chloroform ND
0.00514 0.00247 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Chloromethane ND
0.00514 0.00298 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼cis-1,2-Dichloroethene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼cis-1,3-Dichloropropene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Dibromomethane ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Dichlorobromomethane ND
0.00514 0.00329 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Dichlorodifluoromethane ND
0.0103 0.0103 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Ethyl acetate ND
0.00514 0.00216 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Ethylbenzene ND
0.00514 0.00175 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Ethylene Dibromide ND
0.00514 0.00421 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-13Client Sample ID: SG-7 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:30
Percent Solids: 81.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00514 0.00175 mg/Kg ☼07/05/22 15:31 07/08/22 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00514 0.00175 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Iodomethane ND
0.0103 0.00154 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Isopropyl ether ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Isopropylbenzene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼m,p-Xylene ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Methyl tert-butyl ether ND
0.0103 0.00822 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Methylene Chloride ND
0.00514 0.00318 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Naphthalene ND
0.00514 0.00195 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼n-Butylbenzene ND
0.00514 0.00442 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼n-Heptane ND
0.00514 0.00226 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼N-Propylbenzene ND
0.00514 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼o-Xylene ND
0.00514 0.00205 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼sec-Butylbenzene ND
0.00514 0.00195 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Styrene ND
0.00514 0.00257 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼tert-Butylbenzene ND
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Tetrachloroethene ND
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Toluene ND
0.00514 0.00236 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼trans-1,2-Dichloroethene ND
0.00514 0.00267 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼trans-1,3-Dichloropropene ND
0.0103 0.00247 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼trans-1,4-Dichloro-2-butene ND
0.00514 0.00185 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Trichloroethene ND
0.00514 0.00318 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Trichlorofluoromethane ND
0.0103 0.00565 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Vinyl acetate ND *+
0.00514 0.00288 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Vinyl chloride ND
0.0103 0.00370 mg/Kg 07/05/22 15:31 07/08/22 17:05 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)118 65-130 07/05/22 15:31 07/08/22 17:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 07/05/22 15:31 07/08/22 17:05 165-130
Dibromofluoromethane (Surr)102 07/05/22 15:31 07/08/22 17:05 165-130
Toluene-d8 (Surr)114 07/05/22 15:31 07/08/22 17:05 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.00 2.00 mg/Kg ☼07/11/22 13:00 07/12/22 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.388 0.0411 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4,5-Trichlorophenol ND
0.388 0.0341 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4,6-Trichlorophenol ND
0.388 0.0411 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4-Dichlorophenol ND
0.388 0.0517 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4-Dimethylphenol ND
2.00 0.975 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4-Dinitrophenol ND
0.388 0.0576 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,4-Dinitrotoluene ND
0.388 0.0493 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2,6-Dinitrotoluene ND
0.388 0.0411 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Chloronaphthalene ND
0.388 0.0470 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Chlorophenol ND
0.388 0.0446 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Methylnaphthalene ND
0.388 0.0317 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Methylphenol ND
2.00 0.0529 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Nitroaniline ND
0.388 0.0482 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼2-Nitrophenol ND
0.388 0.0505 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼3 & 4 Methylphenol ND
0.775 0.0329 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-13Client Sample ID: SG-7 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:30
Percent Solids: 81.0Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.00 0.0540 mg/Kg ☼07/11/22 13:00 07/12/22 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 0.200 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4,6-Dinitro-2-methylphenol ND
0.388 0.0423 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Bromophenyl phenyl ether ND
0.388 0.0411 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Chloro-3-methylphenol ND
0.775 0.0611 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Chloroaniline ND
0.388 0.0517 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Chlorophenyl phenyl ether ND
2.00 0.0576 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Nitroaniline ND
2.00 0.388 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼4-Nitrophenol ND
0.388 0.0482 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Acenaphthene ND
0.388 0.0423 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Acenaphthylene ND
0.388 0.0329 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Acetophenone ND
0.388 0.0294 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Anthracene ND
0.388 0.0270 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Atrazine ND
0.388 0.0681 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzaldehyde ND
0.388 0.0317 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzo[a]anthracene ND
0.388 0.0611 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzo[a]pyrene ND
0.388 0.0446 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzo[b]fluoranthene ND
0.388 0.0258 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzo[g,h,i]perylene ND
0.388 0.0764 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Benzo[k]fluoranthene ND
0.388 0.0352 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼bis (2-chloroisopropyl) ether ND
0.388 0.0458 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Bis(2-chloroethoxy)methane ND
0.388 0.0529 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Bis(2-chloroethyl)ether ND
0.388 0.0341 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Bis(2-ethylhexyl) phthalate 0.0625 J B
0.388 0.0305 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Butyl benzyl phthalate ND
0.388 0.0775 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Caprolactam ND
0.388 0.0352 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Carbazole ND
0.388 0.0247 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Chrysene ND
0.388 0.0458 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Dibenz(a,h)anthracene ND
0.388 0.0388 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Dibenzofuran ND
0.388 0.0435 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Diethyl phthalate ND
0.388 0.0399 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Dimethyl phthalate ND
0.388 0.0352 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Di-n-butyl phthalate ND
0.388 0.0341 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Di-n-octyl phthalate ND
0.388 0.0376 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Fluoranthene 0.0460 J
0.388 0.0423 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Fluorene ND
0.388 0.0458 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Hexachlorobenzene ND
0.388 0.0423 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Hexachlorobutadiene ND
0.388 0.0482 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Hexachlorocyclopentadiene ND
0.388 0.0329 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Hexachloroethane ND
0.388 0.0329 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Indeno[1,2,3-cd]pyrene ND
0.388 0.0388 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Isophorone ND
0.388 0.0352 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Naphthalene ND
0.388 0.0305 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Nitrobenzene ND
0.388 0.0376 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼N-Nitrosodi-n-propylamine ND
0.388 0.0388 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼N-Nitrosodiphenylamine ND
2.00 0.388 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Pentachlorophenol ND
0.388 0.0317 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Phenanthrene ND
0.388 0.0399 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Phenol ND
0.388 0.0317 mg/Kg 07/11/22 13:00 07/12/22 19:54 1☼Pyrene 0.0456 J
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-13Client Sample ID: SG-7 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:30
Percent Solids: 81.0Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)65 21-132 07/11/22 13:00 07/12/22 19:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 07/11/22 13:00 07/12/22 19:54 125-130
2-Fluorophenol (Surr)52 07/11/22 13:00 07/12/22 19:54 118-130
Nitrobenzene-d5 (Surr)58 07/11/22 13:00 07/12/22 19:54 119-130
Phenol-d5 (Surr)55 07/11/22 13:00 07/12/22 19:54 121-130
Terphenyl-d14 (Surr)72 07/11/22 13:00 07/12/22 19:54 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.27 0.356 0.119 mg/Kg ☼07/01/22 07:41 07/01/22 16:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.594 0.0713 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Barium 17.9
0.0594 0.0178 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Cadmium ND
1.19 0.131 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Chromium 14.9 B
0.238 0.0594 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Lead 8.97
0.594 0.119 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Selenium 0.933
0.119 0.0119 mg/Kg 07/01/22 07:41 07/01/22 16:36 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0197 J 0.0262 0.00837 mg/Kg ☼07/06/22 09:50 07/06/22 16:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-14Client Sample ID: SG-8 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00460 0.00120 mg/Kg ☼07/05/22 15:31 07/11/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1,1-Trichloroethane ND
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1,2,2-Tetrachloroethane ND
0.00460 0.00267 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00460 0.00138 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1,2-Trichloroethane ND
0.00460 0.00267 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1-Dichloroethane ND
0.00460 0.00331 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1-Dichloroethene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,1-Dichloropropene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2,3-Trichlorobenzene ND
0.00460 0.00165 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2,3-Trichloropropane ND
0.00460 0.00230 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2,4-Trichlorobenzene ND
0.00460 0.00230 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2,4-Trimethylbenzene ND
0.00919 0.00147 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2-Dibromo-3-Chloropropane ND
0.00460 0.00156 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2-Dichlorobenzene ND
0.00460 0.00211 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2-Dichloroethane ND
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,2-Dichloropropane ND
0.00460 0.00221 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,3,5-Trimethylbenzene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,3-Dichlorobenzene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,3-Dichloropropane ND
0.00460 0.00165 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼1,4-Dichlorobenzene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼2,2-Dichloropropane ND
0.0230 0.00846 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼2-Butanone (MEK)ND
0.00460 0.00211 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼2-Chlorotoluene ND
0.0230 0.0175 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼2-Hexanone ND
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼4-Chlorotoluene ND
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼4-Isopropyltoluene ND
0.0230 0.0165 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼4-Methyl-2-pentanone (MIBK)ND
0.0460 0.0101 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Acetone ND
0.00460 0.00221 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Benzene ND
0.00460 0.00156 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Bromobenzene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Bromoform ND
0.00460 0.00221 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Bromomethane ND *+
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Carbon disulfide ND
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Carbon tetrachloride ND
0.00460 0.00129 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chlorobenzene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chlorobromomethane ND
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chlorodibromomethane ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chloroethane ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chloroform ND
0.00460 0.00221 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Chloromethane ND
0.00460 0.00267 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼cis-1,2-Dichloroethene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼cis-1,3-Dichloropropene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Dibromomethane ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Dichlorobromomethane ND
0.00460 0.00294 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Dichlorodifluoromethane ND
0.00919 0.00919 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Ethyl acetate ND
0.00460 0.00193 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Ethylbenzene ND
0.00460 0.00156 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Ethylene Dibromide ND
0.00460 0.00377 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-14Client Sample ID: SG-8 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.00460 0.00156 mg/Kg ☼07/05/22 15:31 07/11/22 17:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00460 0.00156 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Iodomethane ND
0.00919 0.00138 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Isopropyl ether ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Isopropylbenzene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼m,p-Xylene ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Methyl tert-butyl ether ND *+
0.00919 0.00736 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Methylene Chloride ND
0.00460 0.00285 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Naphthalene ND
0.00460 0.00175 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼n-Butylbenzene ND
0.00460 0.00395 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼n-Heptane ND
0.00460 0.00202 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼N-Propylbenzene ND
0.00460 0.00211 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼o-Xylene ND
0.00460 0.00184 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼sec-Butylbenzene ND
0.00460 0.00175 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Styrene ND
0.00460 0.00230 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼tert-Butylbenzene ND
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Tetrachloroethene ND
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Toluene ND
0.00460 0.00211 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼trans-1,2-Dichloroethene ND
0.00460 0.00239 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼trans-1,3-Dichloropropene ND
0.00919 0.00221 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼trans-1,4-Dichloro-2-butene ND
0.00460 0.00165 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Trichloroethene ND
0.00460 0.00285 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Trichlorofluoromethane ND
0.00919 0.00506 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Vinyl acetate ND
0.00460 0.00257 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Vinyl chloride ND
0.00919 0.00331 mg/Kg 07/05/22 15:31 07/11/22 17:24 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)108 65-130 07/05/22 15:31 07/11/22 17:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)106 07/05/22 15:31 07/11/22 17:24 165-130
Dibromofluoromethane (Surr)103 07/05/22 15:31 07/11/22 17:24 165-130
Toluene-d8 (Surr)102 07/05/22 15:31 07/11/22 17:24 165-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 2.04 2.04 mg/Kg ☼07/11/22 13:00 07/12/22 20:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.396 0.0420 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4,5-Trichlorophenol ND
0.396 0.0348 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4,6-Trichlorophenol ND
0.396 0.0420 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4-Dichlorophenol ND
0.396 0.0527 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4-Dimethylphenol ND
2.04 0.995 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4-Dinitrophenol ND
0.396 0.0587 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,4-Dinitrotoluene ND
0.396 0.0503 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2,6-Dinitrotoluene ND
0.396 0.0420 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Chloronaphthalene ND
0.396 0.0479 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Chlorophenol ND
0.396 0.0455 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Methylnaphthalene ND
0.396 0.0324 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Methylphenol ND
2.04 0.0539 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Nitroaniline ND
0.396 0.0491 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼2-Nitrophenol ND
0.396 0.0515 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼3 & 4 Methylphenol ND
0.791 0.0336 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼3,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-14Client Sample ID: SG-8 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 2.04 0.0551 mg/Kg ☼07/11/22 13:00 07/12/22 20:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.04 0.204 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4,6-Dinitro-2-methylphenol ND
0.396 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Bromophenyl phenyl ether ND
0.396 0.0420 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Chloro-3-methylphenol ND
0.791 0.0623 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Chloroaniline ND
0.396 0.0527 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Chlorophenyl phenyl ether ND
2.04 0.0587 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Nitroaniline ND
2.04 0.396 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼4-Nitrophenol ND
0.396 0.0491 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Acenaphthene ND
0.396 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Acenaphthylene ND
0.396 0.0336 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Acetophenone ND
0.396 0.0300 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Anthracene ND
0.396 0.0276 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Atrazine ND
0.396 0.0695 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzaldehyde ND
0.396 0.0324 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzo[a]anthracene ND
0.396 0.0623 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzo[a]pyrene ND
0.396 0.0455 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzo[b]fluoranthene ND
0.396 0.0264 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzo[g,h,i]perylene ND
0.396 0.0779 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Benzo[k]fluoranthene ND
0.396 0.0360 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼bis (2-chloroisopropyl) ether ND
0.396 0.0467 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Bis(2-chloroethoxy)methane ND
0.396 0.0539 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Bis(2-chloroethyl)ether ND
0.396 0.0348 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Bis(2-ethylhexyl) phthalate 0.0582 J B
0.396 0.0312 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Butyl benzyl phthalate ND
0.396 0.0791 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Caprolactam ND
0.396 0.0360 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Carbazole ND
0.396 0.0252 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Chrysene ND
0.396 0.0467 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Dibenz(a,h)anthracene ND
0.396 0.0396 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Dibenzofuran ND
0.396 0.0444 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Diethyl phthalate ND
0.396 0.0408 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Dimethyl phthalate ND
0.396 0.0360 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Di-n-butyl phthalate ND
0.396 0.0348 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Di-n-octyl phthalate ND
0.396 0.0384 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Fluoranthene ND
0.396 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Fluorene ND
0.396 0.0467 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Hexachlorobenzene ND
0.396 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Hexachlorobutadiene ND
0.396 0.0491 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Hexachlorocyclopentadiene ND
0.396 0.0336 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Hexachloroethane ND
0.396 0.0336 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Indeno[1,2,3-cd]pyrene ND
0.396 0.0396 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Isophorone ND
0.396 0.0360 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Naphthalene ND
0.396 0.0312 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Nitrobenzene ND
0.396 0.0384 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼N-Nitrosodi-n-propylamine ND
0.396 0.0396 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼N-Nitrosodiphenylamine ND
2.04 0.396 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Pentachlorophenol ND
0.396 0.0324 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Phenanthrene ND
0.396 0.0408 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Phenol ND
0.396 0.0324 mg/Kg 07/11/22 13:00 07/12/22 20:17 1☼Pyrene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-14Client Sample ID: SG-8 (2-6)
Matrix: SoilDate Collected: 06/29/22 14:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
2,4,6-Tribromophenol (Surr)60 21-132 07/11/22 13:00 07/12/22 20:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)48 07/11/22 13:00 07/12/22 20:17 125-130
2-Fluorophenol (Surr)39 07/11/22 13:00 07/12/22 20:17 118-130
Nitrobenzene-d5 (Surr)40 07/11/22 13:00 07/12/22 20:17 119-130
Phenol-d5 (Surr)41 07/11/22 13:00 07/12/22 20:17 121-130
Terphenyl-d14 (Surr)72 07/11/22 13:00 07/12/22 20:17 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 3.44 0.342 0.114 mg/Kg ☼07/01/22 07:41 07/01/22 16:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.570 0.0684 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Barium 35.4
0.0570 0.0171 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Cadmium 0.105
1.14 0.125 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Chromium 13.1 B
0.228 0.0570 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Lead 26.9
0.570 0.114 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Selenium 1.18
0.114 0.0114 mg/Kg 07/01/22 07:41 07/01/22 16:38 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.0253 J 0.0263 0.00842 mg/Kg ☼07/06/22 09:50 07/06/22 16:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-15Client Sample ID: Soil Dup
Matrix: SoilDate Collected: 06/29/22 00:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00471 0.00123 mg/Kg ☼07/05/22 15:31 07/08/22 21:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1,1-Trichloroethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1,2,2-Tetrachloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
0.00471 0.00141 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1,2-Trichloroethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1-Dichloroethane ND
0.00471 0.00339 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1-Dichloroethene ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,1-Dichloropropene ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2,3-Trichlorobenzene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2,3-Trichloropropane ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2,4-Trichlorobenzene ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2,4-Trimethylbenzene 0.174
0.00943 0.00151 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2-Dibromo-3-Chloropropane ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2-Dichlorobenzene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2-Dichloroethane ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,2-Dichloropropane ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,3,5-Trimethylbenzene 0.0787
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,3-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,3-Dichloropropane ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼1,4-Dichlorobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼2,2-Dichloropropane ND
0.0236 0.00867 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼2-Butanone (MEK)ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼2-Chlorotoluene ND
0.0236 0.0179 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼2-Hexanone ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼4-Chlorotoluene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼4-Isopropyltoluene ND
0.0236 0.0170 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼4-Methyl-2-pentanone (MIBK)ND
0.0471 0.0104 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Acetone 0.0594 B
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Benzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Bromobenzene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Bromoform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Bromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Carbon disulfide ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Carbon tetrachloride ND
0.00471 0.00132 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chlorobenzene ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chlorobromomethane ND
0.00471 0.00198 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chlorodibromomethane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chloroethane ND *+
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chloroform ND
0.00471 0.00226 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Chloromethane ND
0.00471 0.00273 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼cis-1,2-Dichloroethene ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼cis-1,3-Dichloropropene ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Dibromomethane ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Dichlorobromomethane ND
0.00471 0.00302 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Dichlorodifluoromethane ND
0.00943 0.00943 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Ethyl acetate ND
0.170 0.0713 mg/Kg 07/05/22 15:31 07/13/22 18:42 40☼Ethylbenzene ND
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Ethylene Dibromide ND
0.00471 0.00386 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Hexachlorobutadiene ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-15Client Sample ID: Soil Dup
Matrix: SoilDate Collected: 06/29/22 00:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 0.170 0.0578 mg/Kg ☼07/05/22 15:31 07/13/22 18:42 40
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00471 0.00160 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Iodomethane ND
0.00943 0.00141 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Isopropyl ether ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Isopropylbenzene 0.00651
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼m,p-Xylene 0.00450 J
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Methyl tert-butyl ether ND
0.00943 0.00754 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Methylene Chloride ND
0.170 0.105 mg/Kg 07/05/22 15:31 07/13/22 18:42 40☼Naphthalene ND
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼n-Butylbenzene 0.0235
0.170 0.146 mg/Kg 07/05/22 15:31 07/13/22 18:42 40☼n-Heptane ND
0.00471 0.00207 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼N-Propylbenzene 0.0326
0.170 0.0781 mg/Kg 07/05/22 15:31 07/13/22 18:42 40☼o-Xylene ND
0.00471 0.00189 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼sec-Butylbenzene 0.00467 J
0.00471 0.00179 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Styrene ND
0.00471 0.00236 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼tert-Butylbenzene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Tetrachloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Toluene ND
0.00471 0.00217 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼trans-1,2-Dichloroethene ND
0.00471 0.00245 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼trans-1,3-Dichloropropene ND
0.00943 0.00226 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼trans-1,4-Dichloro-2-butene ND
0.00471 0.00170 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Trichloroethene ND
0.00471 0.00292 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Trichlorofluoromethane ND
0.00943 0.00518 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Vinyl acetate ND *+
0.00471 0.00264 mg/Kg 07/05/22 15:31 07/08/22 21:37 1☼Vinyl chloride ND
0.340 0.122 mg/Kg 07/05/22 15:31 07/13/22 18:42 40☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)132 S1+65-130 07/05/22 15:31 07/08/22 21:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
1,2-Dichloroethane-d4 (Surr)98 07/05/22 15:31 07/13/22 18:42 4065-130
4-Bromofluorobenzene (Surr)89 07/05/22 15:31 07/08/22 21:37 165-130
4-Bromofluorobenzene (Surr)108 07/05/22 15:31 07/13/22 18:42 4065-130
Dibromofluoromethane (Surr)126 07/05/22 15:31 07/08/22 21:37 165-130
Dibromofluoromethane (Surr)98 07/05/22 15:31 07/13/22 18:42 4065-130
Toluene-d8 (Surr)101 07/05/22 15:31 07/08/22 21:37 165-130
Toluene-d8 (Surr)101 07/05/22 15:31 07/13/22 18:42 4065-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 1.93 1.93 mg/Kg ☼07/11/22 13:00 07/12/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.375 0.0398 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4,5-Trichlorophenol ND
0.375 0.0330 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4,6-Trichlorophenol ND
0.375 0.0398 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4-Dichlorophenol ND
0.375 0.0501 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4-Dimethylphenol ND
1.93 0.944 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4-Dinitrophenol ND
0.375 0.0557 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,4-Dinitrotoluene ND
0.375 0.0478 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2,6-Dinitrotoluene ND
0.375 0.0398 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2-Chloronaphthalene ND
0.375 0.0455 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2-Chlorophenol ND
0.375 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2-Methylnaphthalene ND
0.375 0.0307 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2-Methylphenol ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-15Client Sample ID: Soil Dup
Matrix: SoilDate Collected: 06/29/22 00:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitroaniline ND 1.93 0.0512 mg/Kg ☼07/11/22 13:00 07/12/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.375 0.0466 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼2-Nitrophenol ND
0.375 0.0489 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼3 & 4 Methylphenol ND
0.751 0.0319 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼3,3'-Dichlorobenzidine ND
1.93 0.0523 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼3-Nitroaniline ND
1.93 0.193 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4,6-Dinitro-2-methylphenol ND
0.375 0.0410 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Bromophenyl phenyl ether ND
0.375 0.0398 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Chloro-3-methylphenol ND
0.751 0.0592 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Chloroaniline ND
0.375 0.0501 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Chlorophenyl phenyl ether ND
1.93 0.0557 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Nitroaniline ND
1.93 0.375 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼4-Nitrophenol ND
0.375 0.0466 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Acenaphthene ND
0.375 0.0410 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Acenaphthylene ND
0.375 0.0319 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Acetophenone ND
0.375 0.0284 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Anthracene ND
0.375 0.0262 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Atrazine ND
0.375 0.0660 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzaldehyde ND
0.375 0.0307 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzo[a]anthracene ND
0.375 0.0592 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzo[a]pyrene ND
0.375 0.0432 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzo[b]fluoranthene ND
0.375 0.0250 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzo[g,h,i]perylene ND
0.375 0.0739 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Benzo[k]fluoranthene ND
0.375 0.0341 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼bis (2-chloroisopropyl) ether ND
0.375 0.0444 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Bis(2-chloroethoxy)methane ND
0.375 0.0512 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Bis(2-chloroethyl)ether ND
0.375 0.0330 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Bis(2-ethylhexyl) phthalate 0.0581 J B
0.375 0.0296 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Butyl benzyl phthalate ND
0.375 0.0751 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Caprolactam ND
0.375 0.0341 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Carbazole ND
0.375 0.0239 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Chrysene ND
0.375 0.0444 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Dibenz(a,h)anthracene ND
0.375 0.0375 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Dibenzofuran ND
0.375 0.0421 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Diethyl phthalate ND
0.375 0.0387 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Dimethyl phthalate ND
0.375 0.0341 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Di-n-butyl phthalate ND
0.375 0.0330 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Di-n-octyl phthalate ND
0.375 0.0364 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Fluoranthene ND
0.375 0.0410 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Fluorene ND
0.375 0.0444 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Hexachlorobenzene ND
0.375 0.0410 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Hexachlorobutadiene ND
0.375 0.0466 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Hexachlorocyclopentadiene ND
0.375 0.0319 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Hexachloroethane ND
0.375 0.0319 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Indeno[1,2,3-cd]pyrene ND
0.375 0.0375 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Isophorone ND
0.375 0.0341 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Naphthalene ND
0.375 0.0296 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Nitrobenzene ND
0.375 0.0364 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼N-Nitrosodi-n-propylamine ND
0.375 0.0375 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼N-Nitrosodiphenylamine ND
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Client Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217621-15Client Sample ID: Soil Dup
Matrix: SoilDate Collected: 06/29/22 00:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Pentachlorophenol ND 1.93 0.375 mg/Kg ☼07/11/22 13:00 07/12/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.375 0.0307 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Phenanthrene ND
0.375 0.0387 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Phenol ND
0.375 0.0307 mg/Kg 07/11/22 13:00 07/12/22 20:39 1☼Pyrene ND
2,4,6-Tribromophenol (Surr)57 21-132 07/11/22 13:00 07/12/22 20:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)53 07/11/22 13:00 07/12/22 20:39 125-130
2-Fluorophenol (Surr)42 07/11/22 13:00 07/12/22 20:39 118-130
Nitrobenzene-d5 (Surr)47 07/11/22 13:00 07/12/22 20:39 119-130
Phenol-d5 (Surr)45 07/11/22 13:00 07/12/22 20:39 121-130
Terphenyl-d14 (Surr)74 07/11/22 13:00 07/12/22 20:39 131-133
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.23 0.324 0.108 mg/Kg ☼07/01/22 07:41 07/01/22 16:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.539 0.0647 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Barium 64.9
0.0539 0.0162 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Cadmium ND
1.08 0.119 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Chromium 20.6 B
0.216 0.0539 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Lead 9.37
0.539 0.108 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Selenium 1.26
0.108 0.0108 mg/Kg 07/01/22 07:41 07/01/22 16:46 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.0277 0.00887 mg/Kg ☼07/06/22 09:50 07/06/22 16:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-729742/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/08/22 16:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/08/22 16:24 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/08/22 16:24 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/08/22 16:24 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/08/22 16:24 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/08/22 16:24 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/08/22 16:24 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/08/22 16:24 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/08/22 16:24 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/08/22 16:24 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/08/22 16:24 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/08/22 16:24 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/08/22 16:24 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/08/22 16:24 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/08/22 16:24 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/08/22 16:24 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/08/22 16:24 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/08/22 16:24 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/08/22 16:24 12-Hexanone
ND 0.002100.00500 mg/Kg 07/08/22 16:24 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/08/22 16:24 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/08/22 16:24 14-Methyl-2-pentanone (MIBK)
0.01608 J 0.01100.0500 mg/Kg 07/08/22 16:24 1Acetone
ND 0.002400.00500 mg/Kg 07/08/22 16:24 1Benzene
ND 0.001700.00500 mg/Kg 07/08/22 16:24 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1Bromoform
ND 0.002400.00500 mg/Kg 07/08/22 16:24 1Bromomethane
ND 0.002100.00500 mg/Kg 07/08/22 16:24 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/08/22 16:24 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/08/22 16:24 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/08/22 16:24 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1Chloroethane
ND 0.002000.00500 mg/Kg 07/08/22 16:24 1Chloroform
ND 0.002400.00500 mg/Kg 07/08/22 16:24 1Chloromethane
ND 0.002900.00500 mg/Kg 07/08/22 16:24 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/08/22 16:24 1Dichlorobromomethane
ND 0.003200.00500 mg/Kg 07/08/22 16:24 1Dichlorodifluoromethane
ND 0.01000.0100 mg/Kg 07/08/22 16:24 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/08/22 16:24 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/08/22 16:24 1Ethylene Dibromide
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-729742/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
RL MDL
Hexachlorobutadiene ND 0.00500 0.00410 mg/Kg 07/08/22 16:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.001700.00500 mg/Kg 07/08/22 16:24 1Hexane
ND 0.001700.00500 mg/Kg 07/08/22 16:24 1Iodomethane
ND 0.001500.0100 mg/Kg 07/08/22 16:24 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1m,p-Xylene
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/08/22 16:24 1Methylene Chloride
ND 0.003100.00500 mg/Kg 07/08/22 16:24 1Naphthalene
ND 0.001900.00500 mg/Kg 07/08/22 16:24 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/08/22 16:24 1n-Heptane
ND 0.002200.00500 mg/Kg 07/08/22 16:24 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/08/22 16:24 1o-Xylene
ND 0.002000.00500 mg/Kg 07/08/22 16:24 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/08/22 16:24 1Styrene
ND 0.002500.00500 mg/Kg 07/08/22 16:24 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/08/22 16:24 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/08/22 16:24 1Toluene
ND 0.002300.00500 mg/Kg 07/08/22 16:24 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/08/22 16:24 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/08/22 16:24 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/08/22 16:24 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/08/22 16:24 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/08/22 16:24 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/08/22 16:24 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/08/22 16:24 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)105 65-130 07/08/22 16:24 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 07/08/22 16:24 14-Bromofluorobenzene (Surr)65-130
104 07/08/22 16:24 1Dibromofluoromethane (Surr)65-130
103 07/08/22 16:24 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729742/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
1,1,1,2-Tetrachloroethane 0.0500 0.05463 mg/Kg 109 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04845 mg/Kg 97 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05270 mg/Kg 105 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04118 mg/Kg 82 70 -130
1,1,2-Trichloroethane 0.0500 0.04914 mg/Kg 98 56 -146
1,1-Dichloroethane 0.0500 0.04952 mg/Kg 99 70 -130
1,1-Dichloroethene 0.0500 0.04202 mg/Kg 84 69 -130
1,1-Dichloropropene 0.0500 0.04893 mg/Kg 98 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05552 mg/Kg 111 70 -130
1,2,3-Trichloropropane 0.0500 0.05189 mg/Kg 104 64 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729742/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
1,2,4-Trichlorobenzene 0.0500 0.05450 mg/Kg 109 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trimethylbenzene 0.0500 0.05062 mg/Kg 101 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.05872 mg/Kg 117 42 -145
1,2-Dichlorobenzene 0.0500 0.05185 mg/Kg 104 70 -130
1,2-Dichloroethane 0.0500 0.04935 mg/Kg 99 68 -139
1,2-Dichloropropane 0.0500 0.04981 mg/Kg 100 70 -130
1,3,5-Trimethylbenzene 0.0500 0.05067 mg/Kg 101 70 -130
1,3-Dichlorobenzene 0.0500 0.05097 mg/Kg 102 70 -130
1,3-Dichloropropane 0.0500 0.05120 mg/Kg 102 54 -150
1,4-Dichlorobenzene 0.0500 0.04958 mg/Kg 99 70 -130
2,2-Dichloropropane 0.0500 0.04920 mg/Kg 98 70 -130
2-Butanone (MEK)0.250 0.2587 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.04924 mg/Kg 98 70 -130
2-Hexanone 0.250 0.2157 mg/Kg 86 30 -150
4-Chlorotoluene 0.0500 0.04836 mg/Kg 97 70 -130
4-Isopropyltoluene 0.0500 0.05083 mg/Kg 102 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2253 mg/Kg 90 34 -150
Acetone 0.250 0.2399 mg/Kg 96 10 -150
Benzene 0.0500 0.04981 mg/Kg 100 70 -130
Bromobenzene 0.0500 0.04971 mg/Kg 99 70 -130
Bromoform 0.0500 0.05191 mg/Kg 104 68 -130
Bromomethane 0.0500 0.05359 mg/Kg 107 70 -130
Carbon disulfide 0.0500 0.04336 mg/Kg 87 70 -130
Carbon tetrachloride 0.0500 0.04797 mg/Kg 96 70 -130
Chlorobenzene 0.0500 0.05109 mg/Kg 102 70 -130
Chlorobromomethane 0.0500 0.05178 mg/Kg 104 66 -130
Chlorodibromomethane 0.0500 0.05176 mg/Kg 104 64 -133
Chloroethane 0.0500 0.06741 *+mg/Kg 135 70 -130
Chloroform 0.0500 0.04902 mg/Kg 98 70 -130
Chloromethane 0.0500 0.04238 mg/Kg 85 70 -130
cis-1,2-Dichloroethene 0.0500 0.04850 mg/Kg 97 70 -130
cis-1,3-Dichloropropene 0.0500 0.05241 mg/Kg 105 70 -130
Dibromomethane 0.0500 0.05100 mg/Kg 102 59 -142
Dichlorobromomethane 0.0500 0.05139 mg/Kg 103 70 -130
Dichlorodifluoromethane 0.0500 0.04393 mg/Kg 88 43 -131
Ethylbenzene 0.0500 0.05107 mg/Kg 102 70 -130
Ethylene Dibromide 0.0500 0.05036 mg/Kg 101 48 -150
Hexachlorobutadiene 0.0500 0.04611 mg/Kg 92 70 -130
Hexane 0.0500 0.04273 mg/Kg 85 70 -130
Iodomethane 0.0500 0.04998 mg/Kg 100 65 -138
Isopropylbenzene 0.0500 0.04961 mg/Kg 99 70 -130
m,p-Xylene 0.0500 0.04846 mg/Kg 97 70 -130
Methyl tert-butyl ether 0.0500 0.04589 mg/Kg 92 70 -130
Methylene Chloride 0.0500 0.05093 mg/Kg 102 54 -149
Naphthalene 0.0500 0.05929 mg/Kg 119 46 -150
n-Butylbenzene 0.0500 0.05161 mg/Kg 103 70 -130
n-Heptane 0.0500 0.04616 mg/Kg 92 70 -130
N-Propylbenzene 0.0500 0.04891 mg/Kg 98 70 -130
o-Xylene 0.0500 0.04967 mg/Kg 99 70 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729742/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
sec-Butylbenzene 0.0500 0.05017 mg/Kg 100 69 -142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Styrene 0.0500 0.05167 mg/Kg 103 70 -130
tert-Butylbenzene 0.0500 0.04929 mg/Kg 99 67 -145
Tetrachloroethene 0.0500 0.04910 mg/Kg 98 70 -130
Toluene 0.0500 0.04857 mg/Kg 97 70 -130
trans-1,2-Dichloroethene 0.0500 0.04738 mg/Kg 95 67 -130
trans-1,3-Dichloropropene 0.0500 0.05288 mg/Kg 106 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.05127 mg/Kg 103 54 -150
Trichloroethene 0.0500 0.04530 mg/Kg 91 70 -130
Trichlorofluoromethane 0.0500 0.04281 mg/Kg 86 70 -130
Vinyl acetate 0.100 0.1601 *+mg/Kg 160 53 -150
Vinyl chloride 0.0500 0.03821 mg/Kg 76 70 -130
Xylenes, Total 0.100 0.09813 mg/Kg 98 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
100Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-729742/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
1,1,1,2-Tetrachloroethane 0.0500 0.05041 mg/Kg 101 70 -130 8 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04313 mg/Kg 86 70 -130 12 30
1,1,2,2-Tetrachloroethane 0.0500 0.04430 mg/Kg 89 64 -130 17 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04051 mg/Kg 81 70 -130 2 40
1,1,2-Trichloroethane 0.0500 0.03653 mg/Kg 73 56 -146 29 30
1,1-Dichloroethane 0.0500 0.04464 mg/Kg 89 70 -130 10 30
1,1-Dichloroethene 0.0500 0.04396 mg/Kg 88 69 -130 5 50
1,1-Dichloropropene 0.0500 0.04403 mg/Kg 88 70 -130 11 30
1,2,3-Trichlorobenzene 0.0500 0.05016 mg/Kg 100 70 -130 10 30
1,2,3-Trichloropropane 0.0500 0.04845 mg/Kg 97 64 -130 7 30
1,2,4-Trichlorobenzene 0.0500 0.04592 mg/Kg 92 70 -130 17 30
1,2,4-Trimethylbenzene 0.0500 0.04738 mg/Kg 95 70 -130 7 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05204 mg/Kg 104 42 -145 12 30
1,2-Dichlorobenzene 0.0500 0.04764 mg/Kg 95 70 -130 8 30
1,2-Dichloroethane 0.0500 0.04413 mg/Kg 88 68 -139 11 30
1,2-Dichloropropane 0.0500 0.04466 mg/Kg 89 70 -130 11 30
1,3,5-Trimethylbenzene 0.0500 0.04602 mg/Kg 92 70 -130 10 30
1,3-Dichlorobenzene 0.0500 0.04554 mg/Kg 91 70 -130 11 30
1,3-Dichloropropane 0.0500 0.03847 mg/Kg 77 54 -150 28 30
1,4-Dichlorobenzene 0.0500 0.04513 mg/Kg 90 70 -130 9 30
2,2-Dichloropropane 0.0500 0.04403 mg/Kg 88 70 -130 11 30
2-Butanone (MEK)0.250 0.2166 mg/Kg 87 40 -150 18 30
2-Chlorotoluene 0.0500 0.04569 mg/Kg 91 70 -130 7 30
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-729742/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729742
2-Hexanone 0.250 0.1830 mg/Kg 73 30 -150 16 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 0.0500 0.04453 mg/Kg 89 70 -130 8 30
4-Isopropyltoluene 0.0500 0.04465 mg/Kg 89 70 -130 13 30
4-Methyl-2-pentanone (MIBK)0.250 0.1919 mg/Kg 77 34 -150 16 30
Acetone 0.250 0.2201 mg/Kg 88 10 -150 9 50
Benzene 0.0500 0.04528 mg/Kg 91 70 -130 10 30
Bromobenzene 0.0500 0.04831 mg/Kg 97 70 -130 3 30
Bromoform 0.0500 0.05076 mg/Kg 102 68 -130 2 30
Bromomethane 0.0500 0.06458 mg/Kg 129 70 -130 19 30
Carbon disulfide 0.0500 0.04436 mg/Kg 89 70 -130 2 30
Carbon tetrachloride 0.0500 0.04296 mg/Kg 86 70 -130 11 30
Chlorobenzene 0.0500 0.04586 mg/Kg 92 70 -130 11 30
Chlorobromomethane 0.0500 0.04595 mg/Kg 92 66 -130 12 30
Chlorodibromomethane 0.0500 0.04272 mg/Kg 85 64 -133 19 30
Chloroethane 0.0500 0.05974 mg/Kg 119 70 -130 12 30
Chloroform 0.0500 0.04336 mg/Kg 87 70 -130 12 30
Chloromethane 0.0500 0.04910 mg/Kg 98 70 -130 15 30
cis-1,2-Dichloroethene 0.0500 0.04333 mg/Kg 87 70 -130 11 30
cis-1,3-Dichloropropene 0.0500 0.03943 mg/Kg 79 70 -130 28 30
Dibromomethane 0.0500 0.04517 mg/Kg 90 59 -142 12 30
Dichlorobromomethane 0.0500 0.04529 mg/Kg 91 70 -130 13 30
Dichlorodifluoromethane 0.0500 0.04643 mg/Kg 93 43 -131 6 30
Ethylbenzene 0.0500 0.04508 mg/Kg 90 70 -130 12 30
Ethylene Dibromide 0.0500 0.04014 mg/Kg 80 48 -150 23 30
Hexachlorobutadiene 0.0500 0.04090 mg/Kg 82 70 -130 12 30
Hexane 0.0500 0.03849 mg/Kg 77 70 -130 10 30
Iodomethane 0.0500 0.04550 mg/Kg 91 65 -138 9 30
Isopropylbenzene 0.0500 0.04604 mg/Kg 92 70 -130 7 30
m,p-Xylene 0.0500 0.04349 mg/Kg 87 70 -130 11 30
Methyl tert-butyl ether 0.0500 0.04314 mg/Kg 86 70 -130 6 30
Methylene Chloride 0.0500 0.04662 mg/Kg 93 54 -149 9 30
Naphthalene 0.0500 0.05264 mg/Kg 105 46 -150 12 30
n-Butylbenzene 0.0500 0.04451 mg/Kg 89 70 -130 15 30
n-Heptane 0.0500 0.04268 mg/Kg 85 70 -130 8 30
N-Propylbenzene 0.0500 0.04426 mg/Kg 89 70 -130 10 30
o-Xylene 0.0500 0.04353 mg/Kg 87 70 -130 13 30
sec-Butylbenzene 0.0500 0.04852 mg/Kg 97 69 -142 3 30
Styrene 0.0500 0.04552 mg/Kg 91 70 -130 13 30
tert-Butylbenzene 0.0500 0.04766 mg/Kg 95 67 -145 3 30
Tetrachloroethene 0.0500 0.04182 mg/Kg 84 70 -130 16 30
Toluene 0.0500 0.03677 mg/Kg 74 70 -130 28 30
trans-1,2-Dichloroethene 0.0500 0.04508 mg/Kg 90 67 -130 5 30
trans-1,3-Dichloropropene 0.0500 0.04037 mg/Kg 81 54 -150 27 30
trans-1,4-Dichloro-2-butene 0.0500 0.04921 mg/Kg 98 54 -150 4 30
Trichloroethene 0.0500 0.04058 mg/Kg 81 70 -130 11 30
Trichlorofluoromethane 0.0500 0.05081 mg/Kg 102 70 -130 17 30
Vinyl acetate 0.100 0.1423 mg/Kg 142 53 -150 12 30
Vinyl chloride 0.0500 0.04769 mg/Kg 95 70 -130 22 30
Xylenes, Total 0.100 0.08702 mg/Kg 87 70 -130 12 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
85
LCSD LCSD
Qualifier Limits%Recovery
824-Bromofluorobenzene (Surr)65 -130
89Dibromofluoromethane (Surr)65 -130
89Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-730073/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/11/22 13:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/11/22 13:18 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/11/22 13:18 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/11/22 13:18 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/11/22 13:18 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/11/22 13:18 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/11/22 13:18 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/11/22 13:18 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/11/22 13:18 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/11/22 13:18 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/11/22 13:18 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/11/22 13:18 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/11/22 13:18 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/11/22 13:18 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/11/22 13:18 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/11/22 13:18 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/11/22 13:18 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/11/22 13:18 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/11/22 13:18 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/11/22 13:18 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/11/22 13:18 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/11/22 13:18 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/11/22 13:18 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/11/22 13:18 12-Hexanone
ND 0.002100.00500 mg/Kg 07/11/22 13:18 14-Chlorotoluene
ND 0.002600.00500 mg/Kg 07/11/22 13:18 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/11/22 13:18 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/11/22 13:18 1Acetone
ND 0.002400.00500 mg/Kg 07/11/22 13:18 1Benzene
ND 0.001700.00500 mg/Kg 07/11/22 13:18 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1Bromoform
ND 0.002400.00500 mg/Kg 07/11/22 13:18 1Bromomethane
ND 0.002100.00500 mg/Kg 07/11/22 13:18 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/11/22 13:18 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/11/22 13:18 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/11/22 13:18 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/11/22 13:18 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1Chloroethane
ND 0.002000.00500 mg/Kg 07/11/22 13:18 1Chloroform
ND 0.002400.00500 mg/Kg 07/11/22 13:18 1Chloromethane
ND 0.002900.00500 mg/Kg 07/11/22 13:18 1cis-1,2-Dichloroethene
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-730073/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
RL MDL
cis-1,3-Dichloropropene ND 0.00500 0.00220 mg/Kg 07/11/22 13:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002000.00500 mg/Kg 07/11/22 13:18 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/11/22 13:18 1Dichlorobromomethane
ND 0.003200.00500 mg/Kg 07/11/22 13:18 1Dichlorodifluoromethane
ND 0.01000.0100 mg/Kg 07/11/22 13:18 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/11/22 13:18 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/11/22 13:18 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/11/22 13:18 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/11/22 13:18 1Hexane
ND 0.001700.00500 mg/Kg 07/11/22 13:18 1Iodomethane
ND 0.001500.0100 mg/Kg 07/11/22 13:18 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1m,p-Xylene
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/11/22 13:18 1Methylene Chloride
ND 0.003100.00500 mg/Kg 07/11/22 13:18 1Naphthalene
ND 0.001900.00500 mg/Kg 07/11/22 13:18 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/11/22 13:18 1n-Heptane
ND 0.002200.00500 mg/Kg 07/11/22 13:18 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/11/22 13:18 1o-Xylene
ND 0.002000.00500 mg/Kg 07/11/22 13:18 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/11/22 13:18 1Styrene
ND 0.002500.00500 mg/Kg 07/11/22 13:18 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/11/22 13:18 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/11/22 13:18 1Toluene
ND 0.002300.00500 mg/Kg 07/11/22 13:18 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/11/22 13:18 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/11/22 13:18 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/11/22 13:18 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/11/22 13:18 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/11/22 13:18 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/11/22 13:18 1Vinyl chloride
ND 0.003600.0100 mg/Kg 07/11/22 13:18 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)96 65-130 07/11/22 13:18 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 07/11/22 13:18 14-Bromofluorobenzene (Surr)65-130
98 07/11/22 13:18 1Dibromofluoromethane (Surr)65-130
103 07/11/22 13:18 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730073/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
1,1,1,2-Tetrachloroethane 0.0500 0.04835 mg/Kg 97 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04358 mg/Kg 87 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.05230 mg/Kg 105 64 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730073/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04386 mg/Kg 88 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2-Trichloroethane 0.0500 0.05100 mg/Kg 102 56 -146
1,1-Dichloroethane 0.0500 0.04898 mg/Kg 98 70 -130
1,1-Dichloroethene 0.0500 0.04402 mg/Kg 88 69 -130
1,1-Dichloropropene 0.0500 0.04432 mg/Kg 89 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05288 mg/Kg 106 70 -130
1,2,3-Trichloropropane 0.0500 0.04958 mg/Kg 99 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05109 mg/Kg 102 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04446 mg/Kg 89 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.05224 mg/Kg 104 42 -145
1,2-Dichlorobenzene 0.0500 0.05144 mg/Kg 103 70 -130
1,2-Dichloroethane 0.0500 0.04982 mg/Kg 100 68 -139
1,2-Dichloropropane 0.0500 0.05145 mg/Kg 103 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04339 mg/Kg 87 70 -130
1,3-Dichlorobenzene 0.0500 0.05036 mg/Kg 101 70 -130
1,3-Dichloropropane 0.0500 0.05059 mg/Kg 101 54 -150
1,4-Dichlorobenzene 0.0500 0.05070 mg/Kg 101 70 -130
2,2-Dichloropropane 0.0500 0.04606 mg/Kg 92 70 -130
2-Butanone (MEK)0.250 0.2568 mg/Kg 103 40 -150
2-Chlorotoluene 0.0500 0.04723 mg/Kg 94 70 -130
2-Hexanone 0.250 0.2654 mg/Kg 106 30 -150
4-Chlorotoluene 0.0500 0.04382 mg/Kg 88 70 -130
4-Isopropyltoluene 0.0500 0.04602 mg/Kg 92 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2657 mg/Kg 106 34 -150
Acetone 0.250 0.2550 mg/Kg 102 10 -150
Benzene 0.0500 0.04770 mg/Kg 95 70 -130
Bromobenzene 0.0500 0.04689 mg/Kg 94 70 -130
Bromoform 0.0500 0.04822 mg/Kg 96 68 -130
Bromomethane 0.0500 0.06573 *+mg/Kg 131 70 -130
Carbon disulfide 0.0500 0.04466 mg/Kg 89 70 -130
Carbon tetrachloride 0.0500 0.04202 mg/Kg 84 70 -130
Chlorobenzene 0.0500 0.04901 mg/Kg 98 70 -130
Chlorobromomethane 0.0500 0.04719 mg/Kg 94 66 -130
Chlorodibromomethane 0.0500 0.04923 mg/Kg 98 64 -133
Chloroethane 0.0500 0.05300 mg/Kg 106 70 -130
Chloroform 0.0500 0.05087 mg/Kg 102 70 -130
Chloromethane 0.0500 0.04457 mg/Kg 89 70 -130
cis-1,2-Dichloroethene 0.0500 0.05052 mg/Kg 101 70 -130
cis-1,3-Dichloropropene 0.0500 0.05103 mg/Kg 102 70 -130
Dibromomethane 0.0500 0.04905 mg/Kg 98 59 -142
Dichlorobromomethane 0.0500 0.05048 mg/Kg 101 70 -130
Dichlorodifluoromethane 0.0500 0.04047 mg/Kg 81 43 -131
Ethyl acetate 0.100 0.1031 mg/Kg 103 70 -130
Ethylbenzene 0.0500 0.04708 mg/Kg 94 70 -130
Ethylene Dibromide 0.0500 0.04870 mg/Kg 97 48 -150
Hexachlorobutadiene 0.0500 0.04233 mg/Kg 85 70 -130
Hexane 0.0500 0.04172 mg/Kg 83 70 -130
Iodomethane 0.0500 0.04847 mg/Kg 97 65 -138
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730073/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
Isopropyl ether 0.100 0.09961 mg/Kg 100 50 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Isopropylbenzene 0.0500 0.04486 mg/Kg 90 70 -130
m,p-Xylene 0.0500 0.04722 mg/Kg 94 70 -130
Methyl tert-butyl ether 0.0500 0.07113 *+mg/Kg 142 70 -130
Methylene Chloride 0.0500 0.04704 mg/Kg 94 54 -149
Naphthalene 0.0500 0.05578 mg/Kg 112 46 -150
n-Butylbenzene 0.0500 0.04616 mg/Kg 92 70 -130
n-Heptane 0.0500 0.04058 mg/Kg 81 70 -130
N-Propylbenzene 0.0500 0.04441 mg/Kg 89 70 -130
o-Xylene 0.0500 0.04869 mg/Kg 97 70 -130
sec-Butylbenzene 0.0500 0.04199 mg/Kg 84 69 -142
Styrene 0.0500 0.04779 mg/Kg 96 70 -130
tert-Butylbenzene 0.0500 0.04246 mg/Kg 85 67 -145
Tetrachloroethene 0.0500 0.04215 mg/Kg 84 70 -130
Toluene 0.0500 0.04665 mg/Kg 93 70 -130
trans-1,2-Dichloroethene 0.0500 0.04714 mg/Kg 94 67 -130
trans-1,3-Dichloropropene 0.0500 0.04894 mg/Kg 98 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04977 mg/Kg 100 54 -150
Trichloroethene 0.0500 0.04481 mg/Kg 90 70 -130
Trichlorofluoromethane 0.0500 0.04505 mg/Kg 90 70 -130
Vinyl acetate 0.100 0.1385 mg/Kg 139 53 -150
Vinyl chloride 0.0500 0.04528 mg/Kg 91 70 -130
Xylenes, Total 0.100 0.09591 mg/Kg 96 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
1154-Bromofluorobenzene (Surr)65 -130
102Dibromofluoromethane (Surr)65 -130
105Toluene-d8 (Surr)65 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730073/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
1,1,1,2-Tetrachloroethane 0.0500 0.04786 mg/Kg 96 70 -130 1 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04366 mg/Kg 87 70 -130 0 30
1,1,2,2-Tetrachloroethane 0.0500 0.05167 mg/Kg 103 64 -130 1 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04400 mg/Kg 88 70 -130 0 40
1,1,2-Trichloroethane 0.0500 0.05078 mg/Kg 102 56 -146 0 30
1,1-Dichloroethane 0.0500 0.04862 mg/Kg 97 70 -130 1 30
1,1-Dichloroethene 0.0500 0.04474 mg/Kg 89 69 -130 2 50
1,1-Dichloropropene 0.0500 0.04401 mg/Kg 88 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05383 mg/Kg 108 70 -130 2 30
1,2,3-Trichloropropane 0.0500 0.04924 mg/Kg 98 64 -130 1 30
1,2,4-Trichlorobenzene 0.0500 0.05198 mg/Kg 104 70 -130 2 30
1,2,4-Trimethylbenzene 0.0500 0.04448 mg/Kg 89 70 -130 0 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05388 mg/Kg 108 42 -145 3 30
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730073/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
1,2-Dichlorobenzene 0.0500 0.05169 mg/Kg 103 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloroethane 0.0500 0.04928 mg/Kg 99 68 -139 1 30
1,2-Dichloropropane 0.0500 0.05054 mg/Kg 101 70 -130 2 30
1,3,5-Trimethylbenzene 0.0500 0.04387 mg/Kg 88 70 -130 1 30
1,3-Dichlorobenzene 0.0500 0.05145 mg/Kg 103 70 -130 2 30
1,3-Dichloropropane 0.0500 0.04943 mg/Kg 99 54 -150 2 30
1,4-Dichlorobenzene 0.0500 0.05111 mg/Kg 102 70 -130 1 30
2,2-Dichloropropane 0.0500 0.04574 mg/Kg 91 70 -130 1 30
2-Butanone (MEK)0.250 0.2570 mg/Kg 103 40 -150 0 30
2-Chlorotoluene 0.0500 0.04725 mg/Kg 95 70 -130 0 30
2-Hexanone 0.250 0.2633 mg/Kg 105 30 -150 1 30
4-Chlorotoluene 0.0500 0.04350 mg/Kg 87 70 -130 1 30
4-Isopropyltoluene 0.0500 0.04646 mg/Kg 93 70 -130 1 30
4-Methyl-2-pentanone (MIBK)0.250 0.2623 mg/Kg 105 34 -150 1 30
Acetone 0.250 0.2570 mg/Kg 103 10 -150 1 50
Benzene 0.0500 0.04695 mg/Kg 94 70 -130 2 30
Bromobenzene 0.0500 0.04689 mg/Kg 94 70 -130 0 30
Bromoform 0.0500 0.04746 mg/Kg 95 68 -130 2 30
Bromomethane 0.0500 0.06786 *+mg/Kg 136 70 -130 3 30
Carbon disulfide 0.0500 0.04467 mg/Kg 89 70 -130 0 30
Carbon tetrachloride 0.0500 0.04206 mg/Kg 84 70 -130 0 30
Chlorobenzene 0.0500 0.04821 mg/Kg 96 70 -130 2 30
Chlorobromomethane 0.0500 0.04602 mg/Kg 92 66 -130 3 30
Chlorodibromomethane 0.0500 0.04841 mg/Kg 97 64 -133 2 30
Chloroethane 0.0500 0.05356 mg/Kg 107 70 -130 1 30
Chloroform 0.0500 0.05064 mg/Kg 101 70 -130 0 30
Chloromethane 0.0500 0.04499 mg/Kg 90 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.05094 mg/Kg 102 70 -130 1 30
cis-1,3-Dichloropropene 0.0500 0.05030 mg/Kg 101 70 -130 1 30
Dibromomethane 0.0500 0.04929 mg/Kg 99 59 -142 0 30
Dichlorobromomethane 0.0500 0.04984 mg/Kg 100 70 -130 1 30
Dichlorodifluoromethane 0.0500 0.04144 mg/Kg 83 43 -131 2 30
Ethyl acetate 0.100 0.1031 mg/Kg 103 70 -130 0 30
Ethylbenzene 0.0500 0.04706 mg/Kg 94 70 -130 0 30
Ethylene Dibromide 0.0500 0.04788 mg/Kg 96 48 -150 2 30
Hexachlorobutadiene 0.0500 0.04266 mg/Kg 85 70 -130 1 30
Hexane 0.0500 0.04208 mg/Kg 84 70 -130 1 30
Iodomethane 0.0500 0.04935 mg/Kg 99 65 -138 2 30
Isopropyl ether 0.100 0.1012 mg/Kg 101 50 -150 2 30
Isopropylbenzene 0.0500 0.04460 mg/Kg 89 70 -130 1 30
m,p-Xylene 0.0500 0.04662 mg/Kg 93 70 -130 1 30
Methyl tert-butyl ether 0.0500 0.06998 *+mg/Kg 140 70 -130 2 30
Methylene Chloride 0.0500 0.04670 mg/Kg 93 54 -149 1 30
Naphthalene 0.0500 0.05563 mg/Kg 111 46 -150 0 30
n-Butylbenzene 0.0500 0.04724 mg/Kg 94 70 -130 2 30
n-Heptane 0.0500 0.04041 mg/Kg 81 70 -130 0 30
N-Propylbenzene 0.0500 0.04421 mg/Kg 88 70 -130 0 30
o-Xylene 0.0500 0.04801 mg/Kg 96 70 -130 1 30
sec-Butylbenzene 0.0500 0.04225 mg/Kg 84 69 -142 1 30
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730073/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730073
Styrene 0.0500 0.04664 mg/Kg 93 70 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
tert-Butylbenzene 0.0500 0.04257 mg/Kg 85 67 -145 0 30
Tetrachloroethene 0.0500 0.04208 mg/Kg 84 70 -130 0 30
Toluene 0.0500 0.04623 mg/Kg 92 70 -130 1 30
trans-1,2-Dichloroethene 0.0500 0.04771 mg/Kg 95 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04739 mg/Kg 95 54 -150 3 30
trans-1,4-Dichloro-2-butene 0.0500 0.05006 mg/Kg 100 54 -150 1 30
Trichloroethene 0.0500 0.04431 mg/Kg 89 70 -130 1 30
Trichlorofluoromethane 0.0500 0.04578 mg/Kg 92 70 -130 2 30
Vinyl acetate 0.100 0.1387 mg/Kg 139 53 -150 0 30
Vinyl chloride 0.0500 0.04668 mg/Kg 93 70 -130 3 30
Xylenes, Total 0.100 0.09463 mg/Kg 95 70 -130 1 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
1164-Bromofluorobenzene (Surr)65 -130
100Dibromofluoromethane (Surr)65 -130
103Toluene-d8 (Surr)65 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-730419/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00500 0.00130 mg/Kg 07/13/22 13:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/13/22 13:11 11,1,1-Trichloroethane
ND 0.002100.00500 mg/Kg 07/13/22 13:11 11,1,2,2-Tetrachloroethane
ND 0.002900.00500 mg/Kg 07/13/22 13:11 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.001500.00500 mg/Kg 07/13/22 13:11 11,1,2-Trichloroethane
ND 0.002900.00500 mg/Kg 07/13/22 13:11 11,1-Dichloroethane
ND 0.003600.00500 mg/Kg 07/13/22 13:11 11,1-Dichloroethene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 11,1-Dichloropropene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 11,2,3-Trichlorobenzene
ND 0.001800.00500 mg/Kg 07/13/22 13:11 11,2,3-Trichloropropane
ND 0.002500.00500 mg/Kg 07/13/22 13:11 11,2,4-Trichlorobenzene
ND 0.002500.00500 mg/Kg 07/13/22 13:11 11,2,4-Trimethylbenzene
ND 0.001600.0100 mg/Kg 07/13/22 13:11 11,2-Dibromo-3-Chloropropane
ND 0.001700.00500 mg/Kg 07/13/22 13:11 11,2-Dichlorobenzene
ND 0.002300.00500 mg/Kg 07/13/22 13:11 11,2-Dichloroethane
ND 0.002600.00500 mg/Kg 07/13/22 13:11 11,2-Dichloropropane
ND 0.002400.00500 mg/Kg 07/13/22 13:11 11,3,5-Trimethylbenzene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 11,3-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 11,3-Dichloropropane
ND 0.001800.00500 mg/Kg 07/13/22 13:11 11,4-Dichlorobenzene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 12,2-Dichloropropane
ND 0.009200.0250 mg/Kg 07/13/22 13:11 12-Butanone (MEK)
ND 0.002300.00500 mg/Kg 07/13/22 13:11 12-Chlorotoluene
ND 0.01900.0250 mg/Kg 07/13/22 13:11 12-Hexanone
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-730419/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
RL MDL
4-Chlorotoluene ND 0.00500 0.00210 mg/Kg 07/13/22 13:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.002600.00500 mg/Kg 07/13/22 13:11 14-Isopropyltoluene
ND 0.01800.0250 mg/Kg 07/13/22 13:11 14-Methyl-2-pentanone (MIBK)
ND 0.01100.0500 mg/Kg 07/13/22 13:11 1Acetone
ND 0.002400.00500 mg/Kg 07/13/22 13:11 1Benzene
ND 0.001700.00500 mg/Kg 07/13/22 13:11 1Bromobenzene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1Bromoform
ND 0.002400.00500 mg/Kg 07/13/22 13:11 1Bromomethane
ND 0.002100.00500 mg/Kg 07/13/22 13:11 1Carbon disulfide
ND 0.002100.00500 mg/Kg 07/13/22 13:11 1Carbon tetrachloride
ND 0.001400.00500 mg/Kg 07/13/22 13:11 1Chlorobenzene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 1Chlorobromomethane
ND 0.002100.00500 mg/Kg 07/13/22 13:11 1Chlorodibromomethane
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1Chloroethane
ND 0.002000.00500 mg/Kg 07/13/22 13:11 1Chloroform
ND 0.002400.00500 mg/Kg 07/13/22 13:11 1Chloromethane
ND 0.002900.00500 mg/Kg 07/13/22 13:11 1cis-1,2-Dichloroethene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1cis-1,3-Dichloropropene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 1Dibromomethane
ND 0.002000.00500 mg/Kg 07/13/22 13:11 1Dichlorobromomethane
ND 0.003200.00500 mg/Kg 07/13/22 13:11 1Dichlorodifluoromethane
ND 0.01000.0100 mg/Kg 07/13/22 13:11 1Ethyl acetate
ND 0.002100.00500 mg/Kg 07/13/22 13:11 1Ethylbenzene
ND 0.001700.00500 mg/Kg 07/13/22 13:11 1Ethylene Dibromide
ND 0.004100.00500 mg/Kg 07/13/22 13:11 1Hexachlorobutadiene
ND 0.001700.00500 mg/Kg 07/13/22 13:11 1Hexane
ND 0.001700.00500 mg/Kg 07/13/22 13:11 1Iodomethane
ND 0.001500.0100 mg/Kg 07/13/22 13:11 1Isopropyl ether
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1Isopropylbenzene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1m,p-Xylene
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1Methyl tert-butyl ether
ND 0.008000.0100 mg/Kg 07/13/22 13:11 1Methylene Chloride
ND 0.003100.00500 mg/Kg 07/13/22 13:11 1Naphthalene
ND 0.001900.00500 mg/Kg 07/13/22 13:11 1n-Butylbenzene
ND 0.004300.00500 mg/Kg 07/13/22 13:11 1n-Heptane
ND 0.002200.00500 mg/Kg 07/13/22 13:11 1N-Propylbenzene
ND 0.002300.00500 mg/Kg 07/13/22 13:11 1o-Xylene
ND 0.002000.00500 mg/Kg 07/13/22 13:11 1sec-Butylbenzene
ND 0.001900.00500 mg/Kg 07/13/22 13:11 1Styrene
ND 0.002500.00500 mg/Kg 07/13/22 13:11 1tert-Butylbenzene
ND 0.002600.00500 mg/Kg 07/13/22 13:11 1Tetrachloroethene
ND 0.002600.00500 mg/Kg 07/13/22 13:11 1Toluene
ND 0.002300.00500 mg/Kg 07/13/22 13:11 1trans-1,2-Dichloroethene
ND 0.002600.00500 mg/Kg 07/13/22 13:11 1trans-1,3-Dichloropropene
ND 0.002400.0100 mg/Kg 07/13/22 13:11 1trans-1,4-Dichloro-2-butene
ND 0.001800.00500 mg/Kg 07/13/22 13:11 1Trichloroethene
ND 0.003100.00500 mg/Kg 07/13/22 13:11 1Trichlorofluoromethane
ND 0.005500.0100 mg/Kg 07/13/22 13:11 1Vinyl acetate
ND 0.002800.00500 mg/Kg 07/13/22 13:11 1Vinyl chloride
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-730419/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
RL MDL
Xylenes, Total ND 0.0100 0.00360 mg/Kg 07/13/22 13:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1,2-Dichloroethane-d4 (Surr)98 65-130 07/13/22 13:11 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
106 07/13/22 13:11 14-Bromofluorobenzene (Surr)65-130
101 07/13/22 13:11 1Dibromofluoromethane (Surr)65-130
101 07/13/22 13:11 1Toluene-d8 (Surr)65-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730419/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
1,1,1,2-Tetrachloroethane 0.0500 0.04621 mg/Kg 92 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 0.0500 0.04302 mg/Kg 86 70 -130
1,1,2,2-Tetrachloroethane 0.0500 0.04985 mg/Kg 100 64 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04219 mg/Kg 84 70 -130
1,1,2-Trichloroethane 0.0500 0.04902 mg/Kg 98 56 -146
1,1-Dichloroethane 0.0500 0.04833 mg/Kg 97 70 -130
1,1-Dichloroethene 0.0500 0.04331 mg/Kg 87 69 -130
1,1-Dichloropropene 0.0500 0.04355 mg/Kg 87 70 -130
1,2,3-Trichlorobenzene 0.0500 0.05143 mg/Kg 103 70 -130
1,2,3-Trichloropropane 0.0500 0.04834 mg/Kg 97 64 -130
1,2,4-Trichlorobenzene 0.0500 0.05037 mg/Kg 101 70 -130
1,2,4-Trimethylbenzene 0.0500 0.04563 mg/Kg 91 70 -130
1,2-Dibromo-3-Chloropropane 0.0500 0.04946 mg/Kg 99 42 -145
1,2-Dichlorobenzene 0.0500 0.04973 mg/Kg 99 70 -130
1,2-Dichloroethane 0.0500 0.04810 mg/Kg 96 68 -139
1,2-Dichloropropane 0.0500 0.05099 mg/Kg 102 70 -130
1,3,5-Trimethylbenzene 0.0500 0.04497 mg/Kg 90 70 -130
1,3-Dichlorobenzene 0.0500 0.04900 mg/Kg 98 70 -130
1,3-Dichloropropane 0.0500 0.04917 mg/Kg 98 54 -150
1,4-Dichlorobenzene 0.0500 0.04952 mg/Kg 99 70 -130
2,2-Dichloropropane 0.0500 0.04520 mg/Kg 90 70 -130
2-Butanone (MEK)0.250 0.2552 mg/Kg 102 40 -150
2-Chlorotoluene 0.0500 0.04802 mg/Kg 96 70 -130
2-Hexanone 0.250 0.2616 mg/Kg 105 30 -150
4-Chlorotoluene 0.0500 0.04444 mg/Kg 89 70 -130
4-Isopropyltoluene 0.0500 0.04763 mg/Kg 95 70 -130
4-Methyl-2-pentanone (MIBK)0.250 0.2606 mg/Kg 104 34 -150
Acetone 0.250 0.2614 mg/Kg 105 10 -150
Benzene 0.0500 0.04680 mg/Kg 94 70 -130
Bromobenzene 0.0500 0.04658 mg/Kg 93 70 -130
Bromoform 0.0500 0.04586 mg/Kg 92 68 -130
Bromomethane 0.0500 0.06728 *+mg/Kg 135 70 -130
Carbon disulfide 0.0500 0.04339 mg/Kg 87 70 -130
Carbon tetrachloride 0.0500 0.04104 mg/Kg 82 70 -130
Chlorobenzene 0.0500 0.04778 mg/Kg 96 70 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730419/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
Chlorobromomethane 0.0500 0.04575 mg/Kg 91 66 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chlorodibromomethane 0.0500 0.04814 mg/Kg 96 64 -133
Chloroethane 0.0500 0.05473 mg/Kg 109 70 -130
Chloroform 0.0500 0.05065 mg/Kg 101 70 -130
Chloromethane 0.0500 0.04455 mg/Kg 89 70 -130
cis-1,2-Dichloroethene 0.0500 0.04956 mg/Kg 99 70 -130
cis-1,3-Dichloropropene 0.0500 0.04908 mg/Kg 98 70 -130
Dibromomethane 0.0500 0.04832 mg/Kg 97 59 -142
Dichlorobromomethane 0.0500 0.04913 mg/Kg 98 70 -130
Dichlorodifluoromethane 0.0500 0.03982 mg/Kg 80 43 -131
Ethyl acetate 0.100 0.1024 mg/Kg 102 70 -130
Ethylbenzene 0.0500 0.04750 mg/Kg 95 70 -130
Ethylene Dibromide 0.0500 0.04689 mg/Kg 94 48 -150
Hexachlorobutadiene 0.0500 0.04491 mg/Kg 90 70 -130
Hexane 0.0500 0.04063 mg/Kg 81 70 -130
Iodomethane 0.0500 0.04702 mg/Kg 94 65 -138
Isopropyl ether 0.100 0.1009 mg/Kg 101 50 -150
Isopropylbenzene 0.0500 0.04582 mg/Kg 92 70 -130
m,p-Xylene 0.0500 0.04673 mg/Kg 93 70 -130
Methyl tert-butyl ether 0.0500 0.06774 *+mg/Kg 135 70 -130
Methylene Chloride 0.0500 0.04508 mg/Kg 90 54 -149
Naphthalene 0.0500 0.05218 mg/Kg 104 46 -150
n-Butylbenzene 0.0500 0.04803 mg/Kg 96 70 -130
n-Heptane 0.0500 0.04038 mg/Kg 81 70 -130
N-Propylbenzene 0.0500 0.04607 mg/Kg 92 70 -130
o-Xylene 0.0500 0.04879 mg/Kg 98 70 -130
sec-Butylbenzene 0.0500 0.04425 mg/Kg 88 69 -142
Styrene 0.0500 0.04673 mg/Kg 93 70 -130
tert-Butylbenzene 0.0500 0.04409 mg/Kg 88 67 -145
Tetrachloroethene 0.0500 0.04378 mg/Kg 88 70 -130
Toluene 0.0500 0.04635 mg/Kg 93 70 -130
trans-1,2-Dichloroethene 0.0500 0.04696 mg/Kg 94 67 -130
trans-1,3-Dichloropropene 0.0500 0.04745 mg/Kg 95 54 -150
trans-1,4-Dichloro-2-butene 0.0500 0.04800 mg/Kg 96 54 -150
Trichloroethene 0.0500 0.04457 mg/Kg 89 70 -130
Trichlorofluoromethane 0.0500 0.04526 mg/Kg 91 70 -130
Vinyl acetate 0.100 0.1343 mg/Kg 134 53 -150
Vinyl chloride 0.0500 0.04649 mg/Kg 93 70 -130
Xylenes, Total 0.100 0.09552 mg/Kg 96 70 -130
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
1124-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
102Toluene-d8 (Surr)65 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730419/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
1,1,1,2-Tetrachloroethane 0.0500 0.04789 mg/Kg 96 70 -130 4 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 0.0500 0.04337 mg/Kg 87 70 -130 1 30
1,1,2,2-Tetrachloroethane 0.0500 0.05031 mg/Kg 101 64 -130 1 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
0.0500 0.04256 mg/Kg 85 70 -130 1 40
1,1,2-Trichloroethane 0.0500 0.05130 mg/Kg 103 56 -146 5 30
1,1-Dichloroethane 0.0500 0.04846 mg/Kg 97 70 -130 0 30
1,1-Dichloroethene 0.0500 0.04334 mg/Kg 87 69 -130 0 50
1,1-Dichloropropene 0.0500 0.04315 mg/Kg 86 70 -130 1 30
1,2,3-Trichlorobenzene 0.0500 0.05192 mg/Kg 104 70 -130 1 30
1,2,3-Trichloropropane 0.0500 0.04941 mg/Kg 99 64 -130 2 30
1,2,4-Trichlorobenzene 0.0500 0.05078 mg/Kg 102 70 -130 1 30
1,2,4-Trimethylbenzene 0.0500 0.04461 mg/Kg 89 70 -130 2 30
1,2-Dibromo-3-Chloropropane 0.0500 0.05065 mg/Kg 101 42 -145 2 30
1,2-Dichlorobenzene 0.0500 0.05101 mg/Kg 102 70 -130 3 30
1,2-Dichloroethane 0.0500 0.04840 mg/Kg 97 68 -139 1 30
1,2-Dichloropropane 0.0500 0.05043 mg/Kg 101 70 -130 1 30
1,3,5-Trimethylbenzene 0.0500 0.04347 mg/Kg 87 70 -130 3 30
1,3-Dichlorobenzene 0.0500 0.05031 mg/Kg 101 70 -130 3 30
1,3-Dichloropropane 0.0500 0.04955 mg/Kg 99 54 -150 1 30
1,4-Dichlorobenzene 0.0500 0.05085 mg/Kg 102 70 -130 3 30
2,2-Dichloropropane 0.0500 0.04497 mg/Kg 90 70 -130 1 30
2-Butanone (MEK)0.250 0.2548 mg/Kg 102 40 -150 0 30
2-Chlorotoluene 0.0500 0.04780 mg/Kg 96 70 -130 0 30
2-Hexanone 0.250 0.2638 mg/Kg 106 30 -150 1 30
4-Chlorotoluene 0.0500 0.04423 mg/Kg 88 70 -130 0 30
4-Isopropyltoluene 0.0500 0.04577 mg/Kg 92 70 -130 4 30
4-Methyl-2-pentanone (MIBK)0.250 0.2604 mg/Kg 104 34 -150 0 30
Acetone 0.250 0.2624 mg/Kg 105 10 -150 0 50
Benzene 0.0500 0.04713 mg/Kg 94 70 -130 1 30
Bromobenzene 0.0500 0.04642 mg/Kg 93 70 -130 0 30
Bromoform 0.0500 0.04668 mg/Kg 93 68 -130 2 30
Bromomethane 0.0500 0.06743 *+mg/Kg 135 70 -130 0 30
Carbon disulfide 0.0500 0.04344 mg/Kg 87 70 -130 0 30
Carbon tetrachloride 0.0500 0.04159 mg/Kg 83 70 -130 1 30
Chlorobenzene 0.0500 0.04791 mg/Kg 96 70 -130 0 30
Chlorobromomethane 0.0500 0.04590 mg/Kg 92 66 -130 0 30
Chlorodibromomethane 0.0500 0.04833 mg/Kg 97 64 -133 0 30
Chloroethane 0.0500 0.05581 mg/Kg 112 70 -130 2 30
Chloroform 0.0500 0.05114 mg/Kg 102 70 -130 1 30
Chloromethane 0.0500 0.04506 mg/Kg 90 70 -130 1 30
cis-1,2-Dichloroethene 0.0500 0.05004 mg/Kg 100 70 -130 1 30
cis-1,3-Dichloropropene 0.0500 0.04934 mg/Kg 99 70 -130 1 30
Dibromomethane 0.0500 0.04861 mg/Kg 97 59 -142 1 30
Dichlorobromomethane 0.0500 0.04960 mg/Kg 99 70 -130 1 30
Dichlorodifluoromethane 0.0500 0.04012 mg/Kg 80 43 -131 1 30
Ethyl acetate 0.100 0.1008 mg/Kg 101 70 -130 2 30
Ethylbenzene 0.0500 0.04708 mg/Kg 94 70 -130 1 30
Ethylene Dibromide 0.0500 0.04820 mg/Kg 96 48 -150 3 30
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730419/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730419
Hexachlorobutadiene 0.0500 0.04239 mg/Kg 85 70 -130 6 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Hexane 0.0500 0.04099 mg/Kg 82 70 -130 1 30
Iodomethane 0.0500 0.04812 mg/Kg 96 65 -138 2 30
Isopropyl ether 0.100 0.1021 mg/Kg 102 50 -150 1 30
Isopropylbenzene 0.0500 0.04438 mg/Kg 89 70 -130 3 30
m,p-Xylene 0.0500 0.04754 mg/Kg 95 70 -130 2 30
Methyl tert-butyl ether 0.0500 0.06932 *+mg/Kg 139 70 -130 2 30
Methylene Chloride 0.0500 0.04545 mg/Kg 91 54 -149 1 30
Naphthalene 0.0500 0.05409 mg/Kg 108 46 -150 4 30
n-Butylbenzene 0.0500 0.04619 mg/Kg 92 70 -130 4 30
n-Heptane 0.0500 0.03981 mg/Kg 80 70 -130 1 30
N-Propylbenzene 0.0500 0.04450 mg/Kg 89 70 -130 3 30
o-Xylene 0.0500 0.04909 mg/Kg 98 70 -130 1 30
sec-Butylbenzene 0.0500 0.04267 mg/Kg 85 69 -142 4 30
Styrene 0.0500 0.04709 mg/Kg 94 70 -130 1 30
tert-Butylbenzene 0.0500 0.04313 mg/Kg 86 67 -145 2 30
Tetrachloroethene 0.0500 0.04619 mg/Kg 92 70 -130 5 30
Toluene 0.0500 0.04628 mg/Kg 93 70 -130 0 30
trans-1,2-Dichloroethene 0.0500 0.04753 mg/Kg 95 67 -130 1 30
trans-1,3-Dichloropropene 0.0500 0.04776 mg/Kg 96 54 -150 1 30
trans-1,4-Dichloro-2-butene 0.0500 0.04858 mg/Kg 97 54 -150 1 30
Trichloroethene 0.0500 0.04473 mg/Kg 89 70 -130 0 30
Trichlorofluoromethane 0.0500 0.04580 mg/Kg 92 70 -130 1 30
Vinyl acetate 0.100 0.1350 mg/Kg 135 53 -150 1 30
Vinyl chloride 0.0500 0.04736 mg/Kg 95 70 -130 2 30
Xylenes, Total 0.100 0.09663 mg/Kg 97 70 -130 1 30
1,2-Dichloroethane-d4 (Surr)65 -130
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
1134-Bromofluorobenzene (Surr)65 -130
99Dibromofluoromethane (Surr)65 -130
104Toluene-d8 (Surr)65 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-729956/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
RL MDL
1,1'-Biphenyl ND 1.69 1.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03470.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4,5-Trichlorophenol
ND 0.02880.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4,6-Trichlorophenol
ND 0.03470.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4-Dichlorophenol
ND 0.04360.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4-Dimethylphenol
ND 0.8231.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4-Dinitrophenol
ND 0.04860.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,4-Dinitrotoluene
ND 0.04160.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12,6-Dinitrotoluene
ND 0.03470.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12-Chloronaphthalene
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-729956/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
RL MDL
2-Chlorophenol ND 0.327 0.0397 mg/Kg 07/11/22 13:00 07/12/22 12:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03770.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12-Methylnaphthalene
ND 0.02680.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12-Methylphenol
ND 0.04461.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 12-Nitroaniline
ND 0.04060.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 12-Nitrophenol
ND 0.04260.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 13 & 4 Methylphenol
ND 0.02780.654 mg/Kg 07/11/22 13:00 07/12/22 12:09 13,3'-Dichlorobenzidine
ND 0.04561.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 13-Nitroaniline
ND 0.1691.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 14,6-Dinitro-2-methylphenol
ND 0.03570.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Bromophenyl phenyl ether
ND 0.03470.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Chloro-3-methylphenol
ND 0.05160.654 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Chloroaniline
ND 0.04360.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Chlorophenyl phenyl ether
ND 0.04861.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Nitroaniline
ND 0.3271.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 14-Nitrophenol
ND 0.04060.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Acenaphthene
ND 0.03570.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Acenaphthylene
ND 0.02780.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Acetophenone
ND 0.02480.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Anthracene
ND 0.02280.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Atrazine
ND 0.05750.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzaldehyde
ND 0.02680.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzo[a]anthracene
ND 0.05160.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzo[a]pyrene
ND 0.03770.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzo[b]fluoranthene
ND 0.02180.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzo[g,h,i]perylene
ND 0.06440.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Benzo[k]fluoranthene
ND 0.02970.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1bis (2-chloroisopropyl) ether
ND 0.03870.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Bis(2-chloroethoxy)methane
ND 0.04460.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Bis(2-chloroethyl)ether
0.06217 J 0.02880.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Bis(2-ethylhexyl) phthalate
ND 0.02580.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Butyl benzyl phthalate
ND 0.06540.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Caprolactam
ND 0.02970.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Carbazole
ND 0.02080.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Chrysene
ND 0.03870.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Dibenz(a,h)anthracene
ND 0.03270.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Dibenzofuran
ND 0.03670.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Diethyl phthalate
ND 0.03370.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Dimethyl phthalate
ND 0.02970.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Di-n-butyl phthalate
ND 0.02880.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Di-n-octyl phthalate
ND 0.03170.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Fluoranthene
ND 0.03570.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Fluorene
ND 0.03870.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Hexachlorobenzene
ND 0.03570.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Hexachlorobutadiene
ND 0.04060.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Hexachlorocyclopentadiene
ND 0.02780.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Hexachloroethane
ND 0.02780.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Indeno[1,2,3-cd]pyrene
ND 0.03270.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Isophorone
ND 0.02970.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Naphthalene
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-729956/19-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
RL MDL
Nitrobenzene ND 0.327 0.0258 mg/Kg 07/11/22 13:00 07/12/22 12:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.03170.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1N-Nitrosodi-n-propylamine
ND 0.03270.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1N-Nitrosodiphenylamine
ND 0.3271.69 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Pentachlorophenol
ND 0.02680.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Phenanthrene
ND 0.03370.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Phenol
ND 0.02680.327 mg/Kg 07/11/22 13:00 07/12/22 12:09 1Pyrene
2,4,6-Tribromophenol (Surr)69 21-132 07/12/22 12:09 1
MB MB
Surrogate
07/11/22 13:00
Dil FacPreparedAnalyzedQualifierLimits%Recovery
69 07/11/22 13:00 07/12/22 12:09 12-Fluorobiphenyl (Surr)25-130
55 07/11/22 13:00 07/12/22 12:09 12-Fluorophenol (Surr)18-130
59 07/11/22 13:00 07/12/22 12:09 1Nitrobenzene-d5 (Surr)19-130
60 07/11/22 13:00 07/12/22 12:09 1Phenol-d5 (Surr)21-130
86 07/11/22 13:00 07/12/22 12:09 1Terphenyl-d14 (Surr)31-133
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729956/20-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
1,1'-Biphenyl 6.55 4.443 mg/Kg 68 32 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4,5-Trichlorophenol 6.55 5.360 mg/Kg 82 33 -130
2,4,6-Trichlorophenol 6.55 4.966 mg/Kg 76 31 -130
2,4-Dichlorophenol 6.55 4.602 mg/Kg 70 30 -130
2,4-Dimethylphenol 6.55 4.579 mg/Kg 70 34 -130
2,4-Dinitrophenol 13.1 10.21 mg/Kg 78 10 -130
2,4-Dinitrotoluene 6.55 5.434 mg/Kg 83 34 -130
2,6-Dinitrotoluene 6.55 4.780 mg/Kg 73 33 -130
2-Chloronaphthalene 6.55 4.508 mg/Kg 69 30 -130
2-Chlorophenol 6.55 4.046 mg/Kg 62 28 -130
2-Methylnaphthalene 6.55 3.826 mg/Kg 58 28 -130
2-Methylphenol 6.55 4.217 mg/Kg 64 30 -130
2-Nitroaniline 6.55 4.758 mg/Kg 73 26 -130
2-Nitrophenol 6.55 4.393 mg/Kg 67 24 -130
3 & 4 Methylphenol 6.55 4.526 mg/Kg 69 31 -130
3,3'-Dichlorobenzidine 6.55 5.636 mg/Kg 86 10 -130
3-Nitroaniline 6.55 4.139 mg/Kg 63 10 -130
4,6-Dinitro-2-methylphenol 13.1 11.02 mg/Kg 84 22 -130
4-Bromophenyl phenyl ether 6.55 5.557 mg/Kg 85 32 -130
4-Chloro-3-methylphenol 6.55 4.641 mg/Kg 71 31 -130
4-Chloroaniline 6.55 3.822 mg/Kg 58 10 -130
4-Chlorophenyl phenyl ether 6.55 4.746 mg/Kg 72 32 -130
4-Nitroaniline 6.55 4.237 mg/Kg 65 25 -130
4-Nitrophenol 13.1 8.419 mg/Kg 64 25 -130
Acenaphthene 6.55 4.608 mg/Kg 70 33 -130
Acenaphthylene 6.55 4.648 mg/Kg 71 34 -130
Acetophenone 6.55 3.994 mg/Kg 61 28 -130
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729956/20-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
Anthracene 6.55 5.233 mg/Kg 80 39 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Atrazine 6.55 5.077 mg/Kg 77 27 -130
Benzaldehyde 6.55 4.017 mg/Kg 61 10 -130
Benzo[a]anthracene 6.55 5.324 mg/Kg 81 40 -130
Benzo[a]pyrene 6.55 5.341 mg/Kg 82 37 -131
Benzo[b]fluoranthene 6.55 5.292 mg/Kg 81 35 -130
Benzo[g,h,i]perylene 6.55 4.465 mg/Kg 68 39 -130
Benzo[k]fluoranthene 6.55 5.565 mg/Kg 85 35 -130
bis (2-chloroisopropyl) ether 6.55 3.702 mg/Kg 56 12 -130
Bis(2-chloroethoxy)methane 6.55 4.198 mg/Kg 64 29 -130
Bis(2-chloroethyl)ether 6.55 4.517 mg/Kg 69 18 -130
Bis(2-ethylhexyl) phthalate 6.55 5.511 mg/Kg 84 39 -130
Butyl benzyl phthalate 6.55 5.335 mg/Kg 81 38 -130
Caprolactam 6.55 4.729 mg/Kg 72 27 -148
Carbazole 6.55 5.125 mg/Kg 78 43 -130
Chrysene 6.55 4.898 mg/Kg 75 40 -130
Dibenz(a,h)anthracene 6.55 5.004 mg/Kg 76 37 -130
Dibenzofuran 6.55 4.988 mg/Kg 76 34 -130
Diethyl phthalate 6.55 4.765 mg/Kg 73 36 -130
Dimethyl phthalate 6.55 4.916 mg/Kg 75 36 -130
Di-n-butyl phthalate 6.55 5.307 mg/Kg 81 39 -130
Di-n-octyl phthalate 6.55 5.459 mg/Kg 83 38 -131
Fluoranthene 6.55 4.944 mg/Kg 75 38 -130
Fluorene 6.55 4.836 mg/Kg 74 34 -130
Hexachlorobenzene 6.55 5.371 mg/Kg 82 28 -130
Hexachlorobutadiene 6.55 4.225 mg/Kg 64 22 -130
Hexachlorocyclopentadiene 6.55 5.496 mg/Kg 84 11 -130
Hexachloroethane 6.55 3.628 mg/Kg 55 21 -130
Indeno[1,2,3-cd]pyrene 6.55 4.880 mg/Kg 74 40 -130
Isophorone 6.55 4.323 mg/Kg 66 26 -130
Naphthalene 6.55 4.056 mg/Kg 62 25 -130
Nitrobenzene 6.55 3.928 mg/Kg 60 25 -130
N-Nitrosodi-n-propylamine 6.55 4.106 mg/Kg 63 24 -130
N-Nitrosodiphenylamine 6.55 5.200 mg/Kg 79 37 -130
Pentachlorophenol 13.1 8.790 mg/Kg 67 16 -135
Phenanthrene 6.55 5.104 mg/Kg 78 38 -130
Phenol 6.55 3.658 mg/Kg 56 27 -130
Pyrene 6.55 4.740 mg/Kg 72 40 -130
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
75
LCS LCS
Qualifier Limits%Recovery
742-Fluorobiphenyl (Surr)25 -130
612-Fluorophenol (Surr)18 -130
62Nitrobenzene-d5 (Surr)19 -130
60Phenol-d5 (Surr)21 -130
73Terphenyl-d14 (Surr)31 -133
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
1,1'-Biphenyl ND 10.3 5.661 mg/Kg 55 32 -130☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
2,4,5-Trichlorophenol ND 10.3 7.572 mg/Kg 74 33 -130☼
2,4,6-Trichlorophenol ND 10.3 6.934 mg/Kg 68 31 -130☼
2,4-Dichlorophenol ND 10.3 5.535 mg/Kg 54 30 -130☼
2,4-Dimethylphenol ND 10.3 5.503 mg/Kg 54 34 -130☼
2,4-Dinitrophenol ND 20.5 13.18 mg/Kg 64 10 -130☼
2,4-Dinitrotoluene ND 10.3 7.978 mg/Kg 78 34 -130☼
2,6-Dinitrotoluene ND 10.3 6.977 mg/Kg 68 33 -130☼
2-Chloronaphthalene ND 10.3 5.692 mg/Kg 55 30 -130☼
2-Chlorophenol ND 10.3 4.657 mg/Kg 45 28 -130☼
2-Methylnaphthalene 1.15 10.3 4.642 mg/Kg 34 28 -130☼
2-Methylphenol ND 10.3 4.986 mg/Kg 49 30 -130☼
2-Nitroaniline ND 10.3 7.028 mg/Kg 69 26 -130☼
2-Nitrophenol ND 10.3 5.004 mg/Kg 49 24 -130☼
3 & 4 Methylphenol ND 10.3 5.375 mg/Kg 52 31 -130☼
3,3'-Dichlorobenzidine ND 10.3 8.457 mg/Kg 82 10 -130☼
3-Nitroaniline ND 10.3 6.538 mg/Kg 64 10 -130☼
4,6-Dinitro-2-methylphenol ND 20.5 16.48 mg/Kg 80 22 -130☼
4-Bromophenyl phenyl ether ND 10.3 8.211 mg/Kg 80 32 -130☼
4-Chloro-3-methylphenol ND 10.3 6.453 mg/Kg 63 31 -130☼
4-Chloroaniline ND 10.3 5.133 mg/Kg 50 10 -130☼
4-Chlorophenyl phenyl ether ND 10.3 6.778 mg/Kg 66 32 -130☼
4-Nitroaniline ND 10.3 6.419 mg/Kg 63 25 -130☼
4-Nitrophenol ND 20.5 13.35 mg/Kg 65 25 -130☼
Acenaphthene ND 10.3 6.257 mg/Kg 61 33 -130☼
Acenaphthylene ND 10.3 6.285 mg/Kg 61 34 -130☼
Acetophenone ND 10.3 4.691 mg/Kg 46 28 -130☼
Anthracene ND 10.3 7.580 mg/Kg 74 39 -130☼
Atrazine ND 10.3 7.638 mg/Kg 74 27 -130☼
Benzaldehyde ND 10.3 4.454 mg/Kg 43 10 -130☼
Benzo[a]anthracene ND 10.3 7.990 mg/Kg 78 40 -130☼
Benzo[a]pyrene ND 10.3 7.988 mg/Kg 78 37 -131☼
Benzo[b]fluoranthene ND 10.3 8.822 mg/Kg 86 35 -130☼
Benzo[g,h,i]perylene ND 10.3 6.529 mg/Kg 64 39 -130☼
Benzo[k]fluoranthene ND 10.3 7.231 mg/Kg 71 35 -130☼
bis (2-chloroisopropyl) ether ND 10.3 4.102 mg/Kg 40 12 -130☼
Bis(2-chloroethoxy)methane ND 10.3 4.903 mg/Kg 48 29 -130☼
Bis(2-chloroethyl)ether ND 10.3 5.193 mg/Kg 51 18 -130☼
Bis(2-ethylhexyl) phthalate 0.0901 J B 10.3 8.227 mg/Kg 79 39 -130☼
Butyl benzyl phthalate ND 10.3 8.023 mg/Kg 78 38 -130☼
Caprolactam ND 10.3 3.790 mg/Kg 37 27 -148☼
Carbazole ND 10.3 7.904 mg/Kg 77 43 -130☼
Chrysene ND 10.3 7.145 mg/Kg 70 40 -130☼
Dibenz(a,h)anthracene ND 10.3 7.353 mg/Kg 72 37 -130☼
Dibenzofuran ND 10.3 6.851 mg/Kg 67 34 -130☼
Diethyl phthalate ND 10.3 7.208 mg/Kg 70 36 -130☼
Dimethyl phthalate ND 10.3 7.316 mg/Kg 71 36 -130☼
Di-n-butyl phthalate ND 10.3 8.098 mg/Kg 79 39 -130☼
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
Di-n-octyl phthalate ND 10.3 8.126 mg/Kg 79 38 -131☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Fluoranthene ND 10.3 7.790 mg/Kg 76 38 -130☼
Fluorene ND 10.3 6.882 mg/Kg 67 34 -130☼
Hexachlorobenzene ND 10.3 8.066 mg/Kg 79 28 -130☼
Hexachlorobutadiene ND 10.3 3.924 mg/Kg 38 22 -130☼
Hexachlorocyclopentadiene ND 10.3 5.959 mg/Kg 58 11 -130☼
Hexachloroethane ND 10.3 3.540 mg/Kg 35 21 -130☼
Indeno[1,2,3-cd]pyrene ND 10.3 7.127 mg/Kg 69 40 -130☼
Isophorone ND 10.3 5.182 mg/Kg 51 26 -130☼
Naphthalene 0.701 10.3 4.510 mg/Kg 37 25 -130☼
Nitrobenzene ND 10.3 4.254 mg/Kg 41 25 -130☼
N-Nitrosodi-n-propylamine ND 10.3 4.773 mg/Kg 47 24 -130☼
N-Nitrosodiphenylamine ND 10.3 7.672 mg/Kg 75 37 -130☼
Pentachlorophenol ND 20.5 15.01 mg/Kg 73 16 -135☼
Phenanthrene ND 10.3 7.473 mg/Kg 73 38 -130☼
Phenol ND 10.3 4.434 mg/Kg 43 27 -130☼
Pyrene ND 10.3 7.262 mg/Kg 71 40 -130☼
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
71
MS MS
Qualifier Limits%Recovery
572-Fluorobiphenyl (Surr)25 -130
462-Fluorophenol (Surr)18 -130
42Nitrobenzene-d5 (Surr)19 -130
47Phenol-d5 (Surr)21 -130
71Terphenyl-d14 (Surr)31 -133
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
1,1'-Biphenyl ND 10.5 6.481 mg/Kg 62 32 -130 14 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
2,4,5-Trichlorophenol ND 10.5 7.913 mg/Kg 75 33 -130 4 50☼
2,4,6-Trichlorophenol ND 10.5 7.609 mg/Kg 73 31 -130 9 50☼
2,4-Dichlorophenol ND 10.5 6.483 mg/Kg 62 30 -130 16 50☼
2,4-Dimethylphenol ND 10.5 6.527 mg/Kg 62 34 -130 17 50☼
2,4-Dinitrophenol ND 21.0 15.50 mg/Kg 74 10 -130 16 50☼
2,4-Dinitrotoluene ND 10.5 8.020 mg/Kg 76 34 -130 1 50☼
2,6-Dinitrotoluene ND 10.5 7.176 mg/Kg 68 33 -130 3 50☼
2-Chloronaphthalene ND 10.5 6.475 mg/Kg 62 30 -130 13 50☼
2-Chlorophenol ND 10.5 5.485 mg/Kg 52 28 -130 16 50☼
2-Methylnaphthalene 1.15 10.5 6.070 mg/Kg 47 28 -130 27 50☼
2-Methylphenol ND 10.5 5.795 mg/Kg 55 30 -130 15 50☼
2-Nitroaniline ND 10.5 7.306 mg/Kg 70 26 -130 4 50☼
2-Nitrophenol ND 10.5 5.713 mg/Kg 54 24 -130 13 50☼
3 & 4 Methylphenol ND 10.5 6.132 mg/Kg 58 31 -130 13 50☼
3,3'-Dichlorobenzidine ND 10.5 8.450 mg/Kg 81 10 -130 0 50☼
3-Nitroaniline ND 10.5 6.100 mg/Kg 58 10 -130 7 50☼
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
4,6-Dinitro-2-methylphenol ND 21.0 16.44 mg/Kg 78 22 -130 0 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
4-Bromophenyl phenyl ether ND 10.5 8.414 mg/Kg 80 32 -130 2 50☼
4-Chloro-3-methylphenol ND 10.5 6.949 mg/Kg 66 31 -130 7 50☼
4-Chloroaniline ND 10.5 5.413 mg/Kg 52 10 -130 5 50☼
4-Chlorophenyl phenyl ether ND 10.5 7.084 mg/Kg 68 32 -130 4 50☼
4-Nitroaniline ND 10.5 5.983 mg/Kg 57 25 -130 7 50☼
4-Nitrophenol ND 21.0 13.23 mg/Kg 63 25 -130 1 50☼
Acenaphthene ND 10.5 6.734 mg/Kg 64 33 -130 7 50☼
Acenaphthylene ND 10.5 6.877 mg/Kg 66 34 -130 9 50☼
Acetophenone ND 10.5 5.647 mg/Kg 54 28 -130 19 50☼
Anthracene ND 10.5 7.792 mg/Kg 74 39 -130 3 50☼
Atrazine ND 10.5 7.410 mg/Kg 71 27 -130 3 50☼
Benzaldehyde ND 10.5 5.145 mg/Kg 49 10 -130 14 50☼
Benzo[a]anthracene ND 10.5 8.028 mg/Kg 77 40 -130 0 50☼
Benzo[a]pyrene ND 10.5 8.187 mg/Kg 78 37 -131 2 50☼
Benzo[b]fluoranthene ND 10.5 8.151 mg/Kg 78 35 -130 8 50☼
Benzo[g,h,i]perylene ND 10.5 6.841 mg/Kg 65 39 -130 5 50☼
Benzo[k]fluoranthene ND 10.5 7.975 mg/Kg 76 35 -130 10 50☼
bis (2-chloroisopropyl) ether ND 10.5 4.832 mg/Kg 46 12 -130 16 50☼
Bis(2-chloroethoxy)methane ND 10.5 5.716 mg/Kg 54 29 -130 15 50☼
Bis(2-chloroethyl)ether ND 10.5 6.090 mg/Kg 58 18 -130 16 50☼
Bis(2-ethylhexyl) phthalate 0.0901 J B 10.5 8.353 mg/Kg 79 39 -130 2 50☼
Butyl benzyl phthalate ND 10.5 7.972 mg/Kg 76 38 -130 1 50☼
Caprolactam ND 10.5 4.583 mg/Kg 44 27 -148 19 50☼
Carbazole ND 10.5 7.636 mg/Kg 73 43 -130 3 50☼
Chrysene ND 10.5 7.329 mg/Kg 70 40 -130 3 50☼
Dibenz(a,h)anthracene ND 10.5 7.624 mg/Kg 73 37 -130 4 50☼
Dibenzofuran ND 10.5 7.258 mg/Kg 69 34 -130 6 50☼
Diethyl phthalate ND 10.5 7.370 mg/Kg 70 36 -130 2 50☼
Dimethyl phthalate ND 10.5 7.494 mg/Kg 71 36 -130 2 50☼
Di-n-butyl phthalate ND 10.5 8.200 mg/Kg 78 39 -130 1 50☼
Di-n-octyl phthalate ND 10.5 8.073 mg/Kg 77 38 -131 1 50☼
Fluoranthene ND 10.5 7.403 mg/Kg 71 38 -130 5 50☼
Fluorene ND 10.5 7.116 mg/Kg 68 34 -130 3 50☼
Hexachlorobenzene ND 10.5 8.134 mg/Kg 78 28 -130 1 50☼
Hexachlorobutadiene ND 10.5 5.148 mg/Kg 49 22 -130 27 50☼
Hexachlorocyclopentadiene ND 10.5 6.889 mg/Kg 66 11 -130 14 50☼
Hexachloroethane ND 10.5 4.580 mg/Kg 44 21 -130 26 50☼
Indeno[1,2,3-cd]pyrene ND 10.5 7.249 mg/Kg 69 40 -130 2 50☼
Isophorone ND 10.5 6.046 mg/Kg 58 26 -130 15 50☼
Naphthalene 0.701 10.5 5.712 mg/Kg 48 25 -130 24 50☼
Nitrobenzene ND 10.5 5.357 mg/Kg 51 25 -130 23 50☼
N-Nitrosodi-n-propylamine ND 10.5 5.515 mg/Kg 53 24 -130 14 50☼
N-Nitrosodiphenylamine ND 10.5 7.751 mg/Kg 74 37 -130 1 50☼
Pentachlorophenol ND 21.0 14.26 mg/Kg 68 16 -135 5 50☼
Phenanthrene ND 10.5 7.789 mg/Kg 74 38 -130 4 50☼
Phenol ND 10.5 5.086 mg/Kg 48 27 -130 14 50☼
Pyrene ND 10.5 7.553 mg/Kg 72 40 -130 4 50☼
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 730228 Prep Batch: 729956
2,4,6-Tribromophenol (Surr)21 -132
Surrogate
69
MSD MSD
Qualifier Limits%Recovery
632-Fluorobiphenyl (Surr)25 -130
482-Fluorophenol (Surr)18 -130
51Nitrobenzene-d5 (Surr)19 -130
51Phenol-d5 (Surr)21 -130
69Terphenyl-d14 (Surr)31 -133
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-728664/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 728886 Prep Batch: 728664
RL MDL
Arsenic ND 0.273 0.0909 mg/Kg 07/01/22 07:40 07/01/22 15:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.05450.455 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Barium
ND 0.01360.0455 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Cadmium
0.1300 J 0.1000.909 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Chromium
ND 0.04550.182 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Lead
ND 0.09090.455 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Selenium
ND 0.009090.0909 mg/Kg 07/01/22 07:40 07/01/22 15:44 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-728664/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 728886 Prep Batch: 728664
Arsenic 9.09 9.092 mg/Kg 100 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Barium 9.09 9.384 mg/Kg 103 80 -120
Cadmium 4.55 4.545 mg/Kg 100 80 -120
Chromium 9.09 9.605 mg/Kg 106 80 -120
Lead 45.9 45.29 mg/Kg 99 80 -120
Selenium 9.11 9.358 mg/Kg 103 80 -120
Silver 4.55 4.605 mg/Kg 101 80 -120
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 728886 Prep Batch: 728664
Arsenic 0.600 14.7 11.74 mg/Kg 76 75 -125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Barium 194 14.7 218.4 4 mg/Kg 166 75 -125☼
Cadmium 0.0909 7.33 6.736 mg/Kg 91 75 -125☼
Chromium 185 B 14.7 200.7 4 mg/Kg 110 75 -125☼
Lead 1.82 73.9 70.79 mg/Kg 93 75 -125☼
Selenium 1.12 14.7 13.26 mg/Kg 83 75 -125☼
Silver ND 7.33 6.759 mg/Kg 92 75 -125☼
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 728886 Prep Batch: 728664
Arsenic 0.600 15.2 12.24 mg/Kg 77 75 -125 4 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Barium 194 15.2 234.3 4 mg/Kg 265 75 -125 7 20☼
Cadmium 0.0909 7.61 7.157 mg/Kg 93 75 -125 6 20☼
Chromium 185 B 15.2 217.3 4 mg/Kg 215 75 -125 8 20☼
Lead 1.82 76.7 73.62 mg/Kg 94 75 -125 4 20☼
Selenium 1.12 15.2 13.36 mg/Kg 80 75 -125 1 20☼
Silver ND 7.61 6.959 mg/Kg 92 75 -125 3 20☼
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-729170/12-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729345 Prep Batch: 729170
RL MDL
Mercury ND 0.0212 0.00678 mg/Kg 07/05/22 16:32 07/06/22 10:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729170/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729345 Prep Batch: 729170
Mercury 0.208 0.2148 mg/Kg 103 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Method BlankLab Sample ID: MB 680-729271/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729638 Prep Batch: 729271
RL MDL
Mercury ND 0.0227 0.00727 mg/Kg 07/06/22 09:50 07/06/22 16:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729271/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 729638 Prep Batch: 729271
Mercury 0.245 0.2177 mg/Kg 89 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: SG-7 (2-6)Lab Sample ID: 680-217621-13 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 729638 Prep Batch: 729271
Mercury 0.0197 J 0.106 0.1144 mg/Kg 89 80 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
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QC Sample Results
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 7471B - Mercury (CVAA) (Continued)
Client Sample ID: SG-7 (2-6)Lab Sample ID: 680-217621-13 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 729638 Prep Batch: 729271
Mercury 0.0197 J 0.112 0.1162 mg/Kg 86 80 -120 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
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QC Association Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
GC/MS VOA
Prep Batch: 729142
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035A680-217621-1 GW-1 (10-15)Total/NA
Soil 5035A680-217621-1 - DL GW-1 (10-15)Total/NA
Soil 5035A680-217621-2 GW-2 (11-14)Total/NA
Soil 5035A680-217621-3 GW-3 (7-12)Total/NA
Soil 5035A680-217621-4 GW-4 (13-17)Total/NA
Soil 5035A680-217621-5 SS-1 (2-6)Total/NA
Soil 5035A680-217621-6 SS-2 (2-6)Total/NA
Soil 5035A680-217621-7 SS-3 (2-6)Total/NA
Soil 5035A680-217621-8 SG-1 (2-6)Total/NA
Soil 5035A680-217621-9 SG-2 (2-6)Total/NA
Soil 5035A680-217621-10 SG-3 (2-6)Total/NA
Soil 5035A680-217621-11 SG-4 (2-6)Total/NA
Soil 5035A680-217621-12 SG-6 (2-6)Total/NA
Soil 5035A680-217621-13 SG-7 (2-6)Total/NA
Soil 5035A680-217621-14 SG-8 (2-6)Total/NA
Soil 5035A680-217621-15 Soil Dup Total/NA
Soil 5035A680-217621-15 Soil Dup Total/NA
Analysis Batch: 729742
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 729142680-217621-1 GW-1 (10-15)Total/NA
Soil 8260D 729142680-217621-3 GW-3 (7-12)Total/NA
Soil 8260D 729142680-217621-4 GW-4 (13-17)Total/NA
Soil 8260D 729142680-217621-5 SS-1 (2-6)Total/NA
Soil 8260D 729142680-217621-6 SS-2 (2-6)Total/NA
Soil 8260D 729142680-217621-7 SS-3 (2-6)Total/NA
Soil 8260D 729142680-217621-8 SG-1 (2-6)Total/NA
Soil 8260D 729142680-217621-9 SG-2 (2-6)Total/NA
Soil 8260D 729142680-217621-10 SG-3 (2-6)Total/NA
Soil 8260D 729142680-217621-11 SG-4 (2-6)Total/NA
Soil 8260D 729142680-217621-12 SG-6 (2-6)Total/NA
Soil 8260D 729142680-217621-13 SG-7 (2-6)Total/NA
Soil 8260D 729142680-217621-15 Soil Dup Total/NA
Solid 8260DMB 680-729742/8 Method Blank Total/NA
Solid 8260DLCS 680-729742/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-729742/5 Lab Control Sample Dup Total/NA
Analysis Batch: 730073
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 729142680-217621-1 - DL GW-1 (10-15)Total/NA
Soil 8260D 729142680-217621-2 GW-2 (11-14)Total/NA
Soil 8260D 729142680-217621-14 SG-8 (2-6)Total/NA
Solid 8260DMB 680-730073/8 Method Blank Total/NA
Solid 8260DLCS 680-730073/4 Lab Control Sample Total/NA
Solid 8260DLCSD 680-730073/5 Lab Control Sample Dup Total/NA
Analysis Batch: 730419
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260D 729142680-217621-15 Soil Dup Total/NA
Solid 8260DMB 680-730419/8 Method Blank Total/NA
Solid 8260DLCS 680-730419/4 Lab Control Sample Total/NA
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QC Association Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
GC/MS VOA (Continued)
Analysis Batch: 730419 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260DLCSD 680-730419/5 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 729956
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3546680-217621-1 GW-1 (10-15)Total/NA
Soil 3546680-217621-2 GW-2 (11-14)Total/NA
Soil 3546680-217621-3 GW-3 (7-12)Total/NA
Soil 3546680-217621-4 GW-4 (13-17)Total/NA
Soil 3546680-217621-5 SS-1 (2-6)Total/NA
Soil 3546680-217621-6 SS-2 (2-6)Total/NA
Soil 3546680-217621-7 SS-3 (2-6)Total/NA
Soil 3546680-217621-8 SG-1 (2-6)Total/NA
Soil 3546680-217621-9 SG-2 (2-6)Total/NA
Soil 3546680-217621-10 SG-3 (2-6)Total/NA
Soil 3546680-217621-11 SG-4 (2-6)Total/NA
Soil 3546680-217621-12 SG-6 (2-6)Total/NA
Soil 3546680-217621-13 SG-7 (2-6)Total/NA
Soil 3546680-217621-14 SG-8 (2-6)Total/NA
Soil 3546680-217621-15 Soil Dup Total/NA
Solid 3546MB 680-729956/19-A Method Blank Total/NA
Solid 3546LCS 680-729956/20-A Lab Control Sample Total/NA
Soil 3546680-217621-1 MS GW-1 (10-15)Total/NA
Soil 3546680-217621-1 MSD GW-1 (10-15)Total/NA
Analysis Batch: 730228
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270E 729956680-217621-1 GW-1 (10-15)Total/NA
Soil 8270E 729956680-217621-2 GW-2 (11-14)Total/NA
Soil 8270E 729956680-217621-3 GW-3 (7-12)Total/NA
Soil 8270E 729956680-217621-4 GW-4 (13-17)Total/NA
Soil 8270E 729956680-217621-5 SS-1 (2-6)Total/NA
Soil 8270E 729956680-217621-6 SS-2 (2-6)Total/NA
Soil 8270E 729956680-217621-7 SS-3 (2-6)Total/NA
Soil 8270E 729956680-217621-8 SG-1 (2-6)Total/NA
Soil 8270E 729956680-217621-9 SG-2 (2-6)Total/NA
Soil 8270E 729956680-217621-10 SG-3 (2-6)Total/NA
Soil 8270E 729956680-217621-11 SG-4 (2-6)Total/NA
Soil 8270E 729956680-217621-12 SG-6 (2-6)Total/NA
Soil 8270E 729956680-217621-13 SG-7 (2-6)Total/NA
Soil 8270E 729956680-217621-14 SG-8 (2-6)Total/NA
Soil 8270E 729956680-217621-15 Soil Dup Total/NA
Solid 8270E 729956MB 680-729956/19-A Method Blank Total/NA
Solid 8270E 729956LCS 680-729956/20-A Lab Control Sample Total/NA
Soil 8270E 729956680-217621-1 MS GW-1 (10-15)Total/NA
Soil 8270E 729956680-217621-1 MSD GW-1 (10-15)Total/NA
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QC Association Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Metals
Prep Batch: 728664
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3050B680-217621-1 GW-1 (10-15)Total/NA
Soil 3050B680-217621-2 GW-2 (11-14)Total/NA
Soil 3050B680-217621-3 GW-3 (7-12)Total/NA
Soil 3050B680-217621-4 GW-4 (13-17)Total/NA
Soil 3050B680-217621-5 SS-1 (2-6)Total/NA
Soil 3050B680-217621-6 SS-2 (2-6)Total/NA
Soil 3050B680-217621-7 SS-3 (2-6)Total/NA
Soil 3050B680-217621-8 SG-1 (2-6)Total/NA
Soil 3050B680-217621-9 SG-2 (2-6)Total/NA
Soil 3050B680-217621-10 SG-3 (2-6)Total/NA
Soil 3050B680-217621-11 SG-4 (2-6)Total/NA
Soil 3050B680-217621-12 SG-6 (2-6)Total/NA
Soil 3050B680-217621-13 SG-7 (2-6)Total/NA
Soil 3050B680-217621-14 SG-8 (2-6)Total/NA
Soil 3050B680-217621-15 Soil Dup Total/NA
Solid 3050BMB 680-728664/1-A Method Blank Total/NA
Solid 3050BLCS 680-728664/2-A Lab Control Sample Total/NA
Soil 3050B680-217621-1 MS GW-1 (10-15)Total/NA
Soil 3050B680-217621-1 MSD GW-1 (10-15)Total/NA
Analysis Batch: 728886
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6020B 728664680-217621-1 GW-1 (10-15)Total/NA
Soil 6020B 728664680-217621-2 GW-2 (11-14)Total/NA
Soil 6020B 728664680-217621-3 GW-3 (7-12)Total/NA
Soil 6020B 728664680-217621-4 GW-4 (13-17)Total/NA
Soil 6020B 728664680-217621-5 SS-1 (2-6)Total/NA
Soil 6020B 728664680-217621-6 SS-2 (2-6)Total/NA
Soil 6020B 728664680-217621-7 SS-3 (2-6)Total/NA
Soil 6020B 728664680-217621-8 SG-1 (2-6)Total/NA
Soil 6020B 728664680-217621-9 SG-2 (2-6)Total/NA
Soil 6020B 728664680-217621-10 SG-3 (2-6)Total/NA
Soil 6020B 728664680-217621-11 SG-4 (2-6)Total/NA
Soil 6020B 728664680-217621-12 SG-6 (2-6)Total/NA
Soil 6020B 728664680-217621-13 SG-7 (2-6)Total/NA
Soil 6020B 728664680-217621-14 SG-8 (2-6)Total/NA
Soil 6020B 728664680-217621-15 Soil Dup Total/NA
Solid 6020B 728664MB 680-728664/1-A Method Blank Total/NA
Solid 6020B 728664LCS 680-728664/2-A Lab Control Sample Total/NA
Soil 6020B 728664680-217621-1 MS GW-1 (10-15)Total/NA
Soil 6020B 728664680-217621-1 MSD GW-1 (10-15)Total/NA
Prep Batch: 729170
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B680-217621-1 GW-1 (10-15)Total/NA
Soil 7471B680-217621-2 GW-2 (11-14)Total/NA
Soil 7471B680-217621-3 GW-3 (7-12)Total/NA
Soil 7471B680-217621-4 GW-4 (13-17)Total/NA
Soil 7471B680-217621-5 SS-1 (2-6)Total/NA
Soil 7471B680-217621-6 SS-2 (2-6)Total/NA
Soil 7471B680-217621-7 SS-3 (2-6)Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Metals (Continued)
Prep Batch: 729170 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B680-217621-8 SG-1 (2-6)Total/NA
Soil 7471B680-217621-9 SG-2 (2-6)Total/NA
Soil 7471B680-217621-10 SG-3 (2-6)Total/NA
Soil 7471B680-217621-11 SG-4 (2-6)Total/NA
Soil 7471B680-217621-12 SG-6 (2-6)Total/NA
Solid 7471BMB 680-729170/12-A Method Blank Total/NA
Solid 7471BLCS 680-729170/13-A Lab Control Sample Total/NA
Prep Batch: 729271
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B680-217621-13 SG-7 (2-6)Total/NA
Soil 7471B680-217621-14 SG-8 (2-6)Total/NA
Soil 7471B680-217621-15 Soil Dup Total/NA
Solid 7471BMB 680-729271/1-A Method Blank Total/NA
Solid 7471BLCS 680-729271/2-A Lab Control Sample Total/NA
Soil 7471B680-217621-13 MS SG-7 (2-6)Total/NA
Soil 7471B680-217621-13 MSD SG-7 (2-6)Total/NA
Analysis Batch: 729345
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 729170680-217621-1 GW-1 (10-15)Total/NA
Soil 7471B 729170680-217621-2 GW-2 (11-14)Total/NA
Soil 7471B 729170680-217621-3 GW-3 (7-12)Total/NA
Soil 7471B 729170680-217621-4 GW-4 (13-17)Total/NA
Soil 7471B 729170680-217621-5 SS-1 (2-6)Total/NA
Soil 7471B 729170680-217621-6 SS-2 (2-6)Total/NA
Soil 7471B 729170680-217621-7 SS-3 (2-6)Total/NA
Soil 7471B 729170680-217621-8 SG-1 (2-6)Total/NA
Soil 7471B 729170680-217621-9 SG-2 (2-6)Total/NA
Soil 7471B 729170680-217621-10 SG-3 (2-6)Total/NA
Soil 7471B 729170680-217621-11 SG-4 (2-6)Total/NA
Soil 7471B 729170680-217621-12 SG-6 (2-6)Total/NA
Solid 7471B 729170MB 680-729170/12-A Method Blank Total/NA
Solid 7471B 729170LCS 680-729170/13-A Lab Control Sample Total/NA
Analysis Batch: 729638
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 729271680-217621-13 SG-7 (2-6)Total/NA
Soil 7471B 729271680-217621-14 SG-8 (2-6)Total/NA
Soil 7471B 729271680-217621-15 Soil Dup Total/NA
Solid 7471B 729271MB 680-729271/1-A Method Blank Total/NA
Solid 7471B 729271LCS 680-729271/2-A Lab Control Sample Total/NA
Soil 7471B 729271680-217621-13 MS SG-7 (2-6)Total/NA
Soil 7471B 729271680-217621-13 MSD SG-7 (2-6)Total/NA
General Chemistry
Analysis Batch: 729914
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture680-217621-1 GW-1 (10-15)Total/NA
Soil Moisture680-217621-2 GW-2 (11-14)Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
General Chemistry (Continued)
Analysis Batch: 729914 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture680-217621-3 GW-3 (7-12)Total/NA
Soil Moisture680-217621-4 GW-4 (13-17)Total/NA
Soil Moisture680-217621-5 SS-1 (2-6)Total/NA
Soil Moisture680-217621-6 SS-2 (2-6)Total/NA
Soil Moisture680-217621-7 SS-3 (2-6)Total/NA
Soil Moisture680-217621-8 SG-1 (2-6)Total/NA
Soil Moisture680-217621-9 SG-2 (2-6)Total/NA
Soil Moisture680-217621-10 SG-3 (2-6)Total/NA
Soil Moisture680-217621-11 SG-4 (2-6)Total/NA
Soil Moisture680-217621-12 SG-6 (2-6)Total/NA
Soil Moisture680-217621-13 SG-7 (2-6)Total/NA
Soil Moisture680-217621-14 SG-8 (2-6)Total/NA
Soil Moisture680-217621-15 Soil Dup Total/NA
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1
Matrix: SoilDate Collected: 06/28/22 10:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: GW-1 (10-15)Lab Sample ID: 680-217621-1
Matrix: SoilDate Collected: 06/28/22 10:15
Percent Solids: 62.0Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.64 g 5 mL
Analysis 8260D 1 729742 07/08/22 21:17 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A DL 729142 07/05/22 15:31 FES TAL SAVTotal/NA 5.595 g 5 mL
Analysis 8260D DL 40 730073 07/11/22 19:49 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.30 g 1 mL
Analysis 8270E 1 730228 07/12/22 13:37 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.10 g 500 mL
Analysis 6020B 1 728886 07/01/22 15:49 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.53 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:20 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: GW-2 (11-14)Lab Sample ID: 680-217621-2
Matrix: SoilDate Collected: 06/28/22 12:05
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: GW-2 (11-14)Lab Sample ID: 680-217621-2
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.009 g 5 mL
Analysis 8260D 100 730073 07/11/22 20:37 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.71 g 1 mL
Analysis 8270E 1 730228 07/12/22 15:50 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.10 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:02 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: GW-2 (11-14)Lab Sample ID: 680-217621-2
Matrix: SoilDate Collected: 06/28/22 12:05
Percent Solids: 80.3Date Received: 06/30/22 10:30
Prep 7471B JKL07/05/22 16:32 TAL SAV729170
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.58 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:24 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: GW-3 (7-12)Lab Sample ID: 680-217621-3
Matrix: SoilDate Collected: 06/28/22 14:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: GW-3 (7-12)Lab Sample ID: 680-217621-3
Matrix: SoilDate Collected: 06/28/22 14:15
Percent Solids: 81.5Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.844 g 5 mL
Analysis 8260D 1 729742 07/08/22 20:56 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.55 g 1 mL
Analysis 8270E 1 730228 07/12/22 16:12 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.02 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:05 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.58 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:27 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: GW-4 (13-17)Lab Sample ID: 680-217621-4
Matrix: SoilDate Collected: 06/29/22 10:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: GW-4 (13-17)Lab Sample ID: 680-217621-4
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.476 g 5 mL
Analysis 8260D 1 729742 07/08/22 19:54 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: GW-4 (13-17)Lab Sample ID: 680-217621-4
Matrix: SoilDate Collected: 06/29/22 10:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Prep 3546 MEW07/11/22 13:00 TAL SAV729956
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.45 g 1 mL
Analysis 8270E 1 730228 07/12/22 16:34 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.09 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:07 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.54 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:30 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SS-1 (2-6)Lab Sample ID: 680-217621-5
Matrix: SoilDate Collected: 06/29/22 11:40
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SS-1 (2-6)Lab Sample ID: 680-217621-5
Matrix: SoilDate Collected: 06/29/22 11:40
Percent Solids: 77.6Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.858 g 5 mL
Analysis 8260D 1 729742 07/08/22 20:15 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.79 g 1 mL
Analysis 8270E 1 730228 07/12/22 16:56 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.08 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:15 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.51 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:33 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SS-2 (2-6)Lab Sample ID: 680-217621-6
Matrix: SoilDate Collected: 06/29/22 13:00
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: SS-2 (2-6)Lab Sample ID: 680-217621-6
Matrix: SoilDate Collected: 06/29/22 13:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.089 g 5 mL
Analysis 8260D 1 729742 07/08/22 19:33 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.25 g 1 mL
Analysis 8270E 1 730228 07/12/22 17:19 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.06 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:17 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.57 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:37 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SS-3 (2-6)Lab Sample ID: 680-217621-7
Matrix: SoilDate Collected: 06/29/22 13:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SS-3 (2-6)Lab Sample ID: 680-217621-7
Matrix: SoilDate Collected: 06/29/22 13:15
Percent Solids: 88.3Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.724 g 5 mL
Analysis 8260D 1 729742 07/08/22 18:08 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.80 g 1 mL
Analysis 8270E 1 730228 07/12/22 17:41 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.04 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:20 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.57 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:40 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-1 (2-6)Lab Sample ID: 680-217621-8
Matrix: SoilDate Collected: 06/29/22 11:50
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: SG-1 (2-6)Lab Sample ID: 680-217621-8
Matrix: SoilDate Collected: 06/29/22 11:50
Percent Solids: 81.6Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.556 g 5 mL
Analysis 8260D 1 729742 07/08/22 20:35 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.86 g 1 mL
Analysis 8270E 1 730228 07/12/22 18:04 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.02 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:23 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.55 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:43 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-2 (2-6)Lab Sample ID: 680-217621-9
Matrix: SoilDate Collected: 06/29/22 11:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SG-2 (2-6)Lab Sample ID: 680-217621-9
Matrix: SoilDate Collected: 06/29/22 11:15
Percent Solids: 85.6Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.445 g 5 mL
Analysis 8260D 1 729742 07/08/22 19:11 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.55 g 1 mL
Analysis 8270E 1 730228 07/12/22 18:26 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.04 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:25 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.58 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:53 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-3 (2-6)Lab Sample ID: 680-217621-10
Matrix: SoilDate Collected: 06/29/22 13:05
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: SG-3 (2-6)Lab Sample ID: 680-217621-10
Matrix: SoilDate Collected: 06/29/22 13:05
Percent Solids: 86.8Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.811 g 5 mL
Analysis 8260D 1 729742 07/08/22 18:50 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.84 g 1 mL
Analysis 8270E 1 730228 07/12/22 18:48 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.09 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:28 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.56 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:56 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-4 (2-6)Lab Sample ID: 680-217621-11
Matrix: SoilDate Collected: 06/29/22 13:25
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SG-4 (2-6)Lab Sample ID: 680-217621-11
Matrix: SoilDate Collected: 06/29/22 13:25
Percent Solids: 82.6Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.721 g 5 mL
Analysis 8260D 1 729742 07/08/22 18:29 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.29 g 1 mL
Analysis 8270E 1 730228 07/12/22 19:10 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.04 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:30 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.54 g 50 mL
Analysis 7471B 1 729345 07/06/22 11:59 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-6 (2-6)Lab Sample ID: 680-217621-12
Matrix: SoilDate Collected: 06/29/22 13:45
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: SG-6 (2-6)Lab Sample ID: 680-217621-12
Matrix: SoilDate Collected: 06/29/22 13:45
Percent Solids: 88.3Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.005 g 5 mL
Analysis 8260D 1 729742 07/08/22 17:47 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.14 g 1 mL
Analysis 8270E 1 730228 07/12/22 19:32 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.09 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:33 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729170 07/05/22 16:32 JKL TAL SAVTotal/NA 0.54 g 50 mL
Analysis 7471B 1 729345 07/06/22 12:03 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-7 (2-6)Lab Sample ID: 680-217621-13
Matrix: SoilDate Collected: 06/29/22 14:30
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: SG-7 (2-6)Lab Sample ID: 680-217621-13
Matrix: SoilDate Collected: 06/29/22 14:30
Percent Solids: 81.0Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.012 g 5 mL
Analysis 8260D 1 729742 07/08/22 17:05 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.77 g 1 mL
Analysis 8270E 1 730228 07/12/22 19:54 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.04 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:36 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729271 07/06/22 09:50 JKL TAL SAVTotal/NA 0.59 g 50 mL
Analysis 7471B 1 729638 07/06/22 16:45 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: SG-8 (2-6)Lab Sample ID: 680-217621-14
Matrix: SoilDate Collected: 06/29/22 14:15
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Client Sample ID: SG-8 (2-6)Lab Sample ID: 680-217621-14
Matrix: SoilDate Collected: 06/29/22 14:15
Percent Solids: 82.0Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.636 g 5 mL
Analysis 8260D 1 730073 07/11/22 17:24 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.27 g 1 mL
Analysis 8270E 1 730228 07/12/22 20:17 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.07 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:38 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729271 07/06/22 09:50 JKL TAL SAVTotal/NA 0.58 g 50 mL
Analysis 7471B 1 729638 07/06/22 16:54 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Client Sample ID: Soil Dup Lab Sample ID: 680-217621-15
Matrix: SoilDate Collected: 06/29/22 00:00
Date Received: 06/30/22 10:30
Analysis Moisture AA07/09/22 19:211 TAL SAV729914
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID:NOEQUIP
Client Sample ID: Soil Dup Lab Sample ID: 680-217621-15
Matrix: SoilDate Collected: 06/29/22 00:00
Percent Solids: 85.1Date Received: 06/30/22 10:30
Prep 5035A FES07/05/22 15:31 TAL SAV729142
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.236 g 5 mL
Analysis 8260D 1 729742 07/08/22 21:37 Y1S TAL SAVTotal/NA 5 g 5 g
CMSADInstrument ID:
Prep 5035A 729142 07/05/22 15:31 FES TAL SAVTotal/NA 6.92 g 5 mL
Analysis 8260D 40 730419 07/13/22 18:42 Y1S TAL SAVTotal/NA 5 g 5 g
CMSP2Instrument ID:
Prep 3546 729956 07/11/22 13:00 MEW TAL SAVTotal/NA 15.50 g 1 mL
Analysis 8270E 1 730228 07/12/22 20:39 T1C TAL SAVTotal/NA
CMSGInstrument ID:
Prep 3050B 728664 07/01/22 07:41 RR TAL SAVTotal/NA 1.09 g 500 mL
Analysis 6020B 1 728886 07/01/22 16:46 BWR TAL SAVTotal/NA
ICPMSDInstrument ID:
Prep 7471B 729271 07/06/22 09:50 JKL TAL SAVTotal/NA 0.53 g 50 mL
Analysis 7471B 1 729638 07/06/22 16:58 JKL TAL SAVTotal/NA
LEEMAN2Instrument ID:
Laboratory References:
Rochester = Rochester, NY, 1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-217621-1
Project/Site: Greenhouse Project
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Eurofins Savannah
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Method Summary
Job ID: 680-217621-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)TAL SAV
SW8466020BMetals (ICP/MS)TAL SAV
SW8467471BMercury (CVAA)TAL SAV
EPAMoisturePercent Moisture TAL SAV
NoneSubcontractGeneral Subcontract Method Rochester
SW8463050BPreparation, Metals TAL SAV
SW8463546Microwave Extraction TAL SAV
SW8465035AClosed System Purge & Trap TAL SAV
SW8467471BPreparation, Mercury TAL SAV
Protocol References:
EPA = US Environmental Protection Agency
None = None
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
Rochester = Rochester, NY, 1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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July 14, 2022 Service Request No:R2206083
John Andros
Eurofins ET NW (formerly TestAmerica)
Savannah, GA 31404
All testing was performed according to our laboratory’s quality assurance program and met the
requirements of the TNI standards except as noted in the case narrative report. Any testing not
included in the lab's accreditation is identified on a Non-Certified Analytes report. All results are
intended to be considered in their entirety. ALS Environmental is not responsible for use of less than
the complete report. Results apply only to the individual samples submitted to the lab for analysis, as
listed in the report. The measurement uncertainty of the results included in this report is within that
expected when using the prescribed method(s), and represented by Laboratory Control Sample
control limits. Any events, such as QC failures or Holding Time exceedances, which may add to the
uncertainty are explained in the report narrative or are flagged with qualifiers. The flags are explained
in the Report Qualifiers and Definitions page of this report.
For your reference, these analyses have been assigned our service request number
Enclosed are the results of the sample(s) submitted to our laboratory
Laboratory Results for:Greenhouse Project 680-217621
Dear John,
July 06, 2022
R2206083.
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Nicole Mansen
Project Manager
dba ALS Environmental
ALS Group USA, Corp.
ADDRESS
FAXPHONE
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
[phone]+1 585 288 5380 |
Page 1 of 69Page 105 of 176 7/14/2022
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Narrative Documents
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 2 of 69Page 106 of 176 7/14/2022
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CASE NARRATIVE
Client:
Project:
Sample Matrix:
Service Request:
Date Received:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621
Soil
R2206083
07/06/2022
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains
analytical results for samples for the Tier II level requested by the client.
Sample Receipt:
Fifteen soil samples were received for analysis at ALS Environmental on 07/06/2022. Any discrepancies upon initial sample
inspection are annotated on the sample receipt and preservation form included within this report. The samples were stored at
minimum in accordance with the analytical method requirements.
General Chemistry:
Method 7199, 07/13/2022: The Relative Percent Difference (RPD) for the analysis of one or more analyte(s) in the replicates of a
Duplicate Sample associated with the samples this report is greater than the RPD limit, but is acceptable as evaluated against
the alternate limit of duplicates within ±MRL when one or both of the replicates are within five times the MRL.
Method 7196A/7199: The matrix spike recovery for Hexavalent Chromium was below the specified control limit in one or more
spiked samples, likely due to a reducing characteristic of the sample matrix. The low matrix spike recovery suggests that the
chemistry of the sample will not sustain chromium in the hexavalent form. The digestion and analysis was repeated and
confirmed the matrix interference. The matrix spike is flagged to indicate the discrepancy. No further corrective action was
appropriate.
1565 Jefferson Rd, Building 300, Rochester, NY 14623 | 585-288-5380 | www.alsglobal.com
Approved by Date 07/14/2022
Page 3 of 69Page 107 of 176 7/14/2022
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CLIENT ID:GW-1 (10-15)Lab ID:R2206083-001
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 3.45 0.07 0.64 mg/Kg 7199
Total Solids 60.9 Percent ALS SOP
Chromium, Hexavalent 1.84 0.07 0.64 mg/Kg 7199
CLIENT ID:GW-2 (11-14)Lab ID:R2206083-002
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 1.19 0.05 0.47 mg/Kg 7199
Total Solids 83.6 Percent ALS SOP
Chromium, Hexavalent 0.97 0.05 0.47 mg/Kg 7199
CLIENT ID:GW-3 (7-12)Lab ID:R2206083-003
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.31 J 0.05 0.47 mg/Kg 7199
Total Solids 85.0 Percent ALS SOP
Chromium, Hexavalent 0.14 J 0.05 0.45 mg/Kg 7199
CLIENT ID:GW-4 (13-17)Lab ID:R2206083-004
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.53 0.06 0.52 mg/Kg 7199
Total Solids 74.6 Percent ALS SOP
Chromium, Hexavalent 0.47 J 0.06 0.53 mg/Kg 7199
CLIENT ID:SS-1 (2-6)Lab ID:R2206083-005
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 2.61 0.06 0.50 mg/Kg 7199
Total Solids 76.7 Percent ALS SOP
Chromium, Hexavalent 1.72 0.06 0.51 mg/Kg 7199
CLIENT ID:SS-2 (2-6)Lab ID:R2206083-006
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.67 0.06 0.50 mg/Kg 7199
Total Solids 79.1 Percent ALS SOP
Chromium, Hexavalent 0.16 J 0.06 0.51 mg/Kg 7199
CLIENT ID:SS-3 (2-6)Lab ID:R2206083-007
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.87 0.05 0.47 mg/Kg 7199
Total Solids 82.4 Percent ALS SOP
Chromium, Hexavalent 0.39 J 0.06 0.48 mg/Kg 7199
CLIENT ID:SG-1 (2-6)Lab ID:R2206083-008
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 1.22 0.05 0.47 mg/Kg 7199
Total Solids 83.5 Percent ALS SOP
SAMPLE DETECTION SUMMARY
This form includes only detections above the reporting levels. For a full listing of sample results, continue to the Sample Results section of this Report.
Page 4 of 69Page 108 of 176 7/14/2022
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CLIENT ID:SG-1 (2-6)Lab ID:R2206083-008
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.96 0.06 0.48 mg/Kg 7199
CLIENT ID:SG-2 (2-6)Lab ID:R2206083-009
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.89 0.06 0.49 mg/Kg 7199
Total Solids 78.3 Percent ALS SOP
Chromium, Hexavalent 0.32 J 0.06 0.50 mg/Kg 7199
CLIENT ID:SG-3 (2-6)Lab ID:R2206083-010
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.77 0.06 0.57 mg/Kg 7199
Total Solids 70.2 Percent ALS SOP
Chromium, Hexavalent 0.41 J 0.06 0.55 mg/Kg 7199
CLIENT ID:SG-4 (2-6)Lab ID:R2206083-011
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.45 J 0.06 0.48 mg/Kg 7199
Total Solids 83.0 Percent ALS SOP
Chromium, Hexavalent 0.16 J 0.05 0.47 mg/Kg 7199
CLIENT ID:SG-6 (2-6)Lab ID:R2206083-012
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 1.07 0.05 0.47 mg/Kg 7199
Total Solids 85.0 Percent ALS SOP
Chromium, Hexavalent 0.22 J 0.05 0.47 mg/Kg 7199
CLIENT ID:SG-7 (2-6)Lab ID:R2206083-013
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.58 0.05 0.48 mg/Kg 7199
Total Solids 81.2 Percent ALS SOP
Chromium, Hexavalent 0.20 J 0.06 0.49 mg/Kg 7199
CLIENT ID:SG-8 (2-6)Lab ID:R2206083-014
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.74 0.05 0.45 mg/Kg 7199
Total Solids 85.0 Percent ALS SOP
Chromium, Hexavalent 0.23 J 0.05 0.46 mg/Kg 7199
CLIENT ID:Soil Dup Lab ID:R2206083-015
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.40 J 0.06 0.54 mg/Kg 7199
Total Solids 73.2 Percent ALS SOP
Chromium, Hexavalent 0.37 J 0.06 0.55 mg/Kg 7199
SAMPLE DETECTION SUMMARY
This form includes only detections above the reporting levels. For a full listing of sample results, continue to the Sample Results section of this Report.
Page 5 of 69Page 109 of 176 7/14/2022
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Sample Receipt Information
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 6 of 69Page 110 of 176 7/14/2022
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GW-1 (10-15)R2206083-001 6/28/2022 1015
GW-2 (11-14)R2206083-002 6/28/2022 1205
GW-3 (7-12)R2206083-003 6/28/2022 1415
GW-4 (13-17)R2206083-004 6/28/2022 1015
SS-1 (2-6)R2206083-005 6/28/2022 1140
SS-2 (2-6)R2206083-006 6/28/2022 1300
SS-3 (2-6)R2206083-007 6/28/2022 1315
SG-1 (2-6)R2206083-008 6/28/2022 1150
SG-2 (2-6)R2206083-009 6/28/2022 1115
SG-3 (2-6)R2206083-010 6/28/2022 1305
SG-4 (2-6)R2206083-011 6/28/2022 1325
SG-6 (2-6)R2206083-012 6/28/2022 1345
SG-7 (2-6)R2206083-013 6/28/2022 1430
SG-8 (2-6)R2206083-014 6/28/2022 1415
Soil DupR2206083-015 6/28/2022
Client:Eurofins ET NW (formerly TestAmerica)Service Request:R2206083
Project:Greenhouse Project 680-217621/68027092
SAMPLE CROSS-REFERENCE
SAMPLE #CLIENT SAMPLE ID DATE TIME
Printed 7/14/2022 3:32:54 PM Sample Summary
Page 7 of 69Page 111 of 176 7/14/2022
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Eurofins Savannah
5102 LaRoche Avenue
Savannah.GA 31404
Phone:[phone] Fax:[phone]
Chain of Custody Record 1111]11~II~IIII~II~mil ml ~I~~1;llmml ~II~II ~::eurofins I Eovfronment Testing
America
III
Sampler;U1bPM:carTierTrnckingNo(sj:cae No:
Clienl Informalion (Sub Conlract Labl Andros,John 68Q..700299.1
ClientContact:"""",E.M!liI:SllIteo!OrIgin'Page:
ShlppingfReceiving [e-mail] North Carolina Page 1 of 2
Company:Accred,I1I1KlnsReqvtred (See nole):Job":
ALS Laboratory Group Slate.North Carolina (WW/SW)68()'217621.1
Addren:Duo OlilloRtlquetltl!d:Preservation Codes:
1565 Jefferson Road.Building 300,Suile 360,7/812022 Analysis Requested M.HcwaneA.HCLCity:TATRequestod (dil)'5):B.NIIOH N.None
Rochester .!c.Zn Acetate O.AsNa02
p.NII20IlSSlate.Zip:!D.NItricAcid O.N.2S03NY,14623 •E.NIlHS04 R.N1I2S203"""",PO'"F.MeOH S.H2SO4.G .AmchIor.T•TSP Dodecllhydr9te;;x H •AICOtbicAcid~U.AcetoneEmDll:WOI::Z j 1.Ice~;;J-01Water V.MCAA
•Z •K.EOTA W.pH4.5
ProjectName:~tfl:•~'0 •y.Ttizma!:~~c l.EDAGreenhouseProject68027092•:;;Z•othel'(spedfyJ~•cSite:SSQW1l':!:c g 0 Other:E 0_u0C~u
0 0 ,~0
"~0'jSampleMatrix•e~~:It ~'EType(_t.<,~.0 0•..•...0:o'zSample(C=comp,•....-"~;i :;;
SamDle Identification -Client 10 lLab 1m Sam Die Date Time G=arabl il'0 ,-{!.Spcclallnstructlons/Note:IlTon •••••,••••Alr ..-'"Preservation Code:IX X X
GW-1 (10-15)(680-217621-1)6128122 10:15 Solid X 1E,"om
GW-2 (11-14)(680-217621-21 6128/22 12:05 Solid X 1Ea!':f~rn
GW-3 (7-12)(680-217621-3)6/28/22 14:15 Solid X 1Fa!':tprn
GW-4 (13-17)(680-217621-4)6129122 10:15 Solid X 1Fa.torn
55-1 (2-6)(680-217621-5)6/29/22 11:40 Solid X 1FastPrn
55-2 (2-6)(680-217621-6)6/29122 13:00 Solid X 1F••l.,n
55-3 (2-6)(680-217621-7)6/29122 13:15 Solid X 1F.".'n
5G-1 (2-6)(680-217621-8)6129122 11:50 Solid X 1ERS'om
5G-2 (2-6)(680-217621-9)6/29/22 11:15 Solid X 1E."om
Nole:Since laborDloryIccreclitations ItOs\Jtljeeltochll~,Eurofll"Envi~Testing Southeasl,llC places!hll'~hip 01method,lInt1ty1e8 8ccmdl11tioncomtIIillnceupon out.ubconltllct ll1bofltones,This 5lImpieshipment isforwarded under d\lIl~l<vstocty.1I!hIl'18bomtory
d06 not currentlymainllm llocred<lIl1onin 1MSUlleof Originlistedabove loranalyslsltestsImBtrixbeing Inaly1ed,lhe IImples must belhipped back tolne Eurofins EnvironmentTesting Sou!hellst,llC InbotntOtyorOUterinstructions winbe provided.Arlych&nge5to accreditation
111:115lhould be!broughl to Eurofrns Environment Testing SouthOllst,llC Inenlion immediltely.IIon request~lIccredlUltionsIre eur:ent todille.returnthe signod Chll;n01Cuslody onesting 10snid compliCllnceto Euroflns Envi~t TeslJhg 5ouIMlllt,llC.
Possible Hazard Identlflcatlon Sample Disposal (A fee may be assessed If samples arc retained longer than 1 month)
Unconfirmed oRerum To Client 0 Disposal Bv Lab 0 ArchfveFor Months
Deliverable Requested:I,II,III,IV,Other (specify)Primary Deliverable Rank:2 SpeciallnstructlonSlOC Requirements:
Empty Kit Relinquished by:IDale:ITime:IMethod01Shipment:
Rellnqulshed oalcfT7'~Com".,Rr;~iJ"~£"",'1.1",;':77 Ol 0 Z'L }((pICoAtS."17o~
Rellnquis~by.Ol'lternme:Com".,R~by,(J I Oat~lime:R2206083'"".5ReUnquishedby:OalefTime:Com1><.,Rec~by:Oll~lme:Euro"nl ET NW Irorm'r1y TutAm.rtC:IIGrtlnhou"ProJ.c:1 880-217821
Custody Seals Intact:ICustodY Seal No.:Cooler Temperature(I)-c Ind O'Jler Remarb:
111111111 I11II111 1111111111 111111111111111111111I:J.Yes •No Page 8 of 69Page 112 of 176 7/14/2022
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Eurofins Savannah
5102 LaRoche Avenue
Savannah,GA 31404
Phone:[phone] Fax:912.3S2.()165
Chain of Custody Record .';::eurofins 1 Envlronmlent TestlngAm(lrica
Sllmpler.U1b PM:carrier Tracking No(s):coe No:
Client Information ISub Contract Labl Andros,John 680-700299,2
Client Contact "hon"E.MaU:State of Origin:Page:
ShippinglReceiving [e-mail],com North Carolina Page 2 of 2
Company;Accrl!d,llIlions Required (8M!nole)'0'"AlS laboratory Group Stale -North Carolina (WI/WSW)680-217621-1
A,C1dr~s:Duo D.to Roquestod:PresorvaUon Codes:
1565 Jefferson Road.Building 300,Suite 360,7/812022 Analysis Requested M.Ho.-oneA.HCLCity:TATRnqulllllod(daYII):B -NaOH N.None
Rochester E c •Zn Acetate O.A$NilO2•p.NI204SStlllo,Zip:~O.NltricAckl O.Na2S03NY,14623 E •NaHS04 R •N1I2S203•F -M&OHPhone:PQIt:u 5.H2SO4"G -Amehlor•T •TSP Dodec3hyclrale<;x H •Ascorble Acid~U.AcetOMEma":WO":z ~1.lce~<;•J.DIWaler V.MCAA
•Z >;f K .EDTA W.pH4.5ProjedName:Projeclll:0 "~~•y.Trizma~0 0 l.EDAGreenhouseProject68027092•g~••z.other (SPecify)!!0 0Site:550M:0 ~o.0 Other:E 0_u0~e•••'0••.-u ~~0 jSampleMatrIx!~~!!:e ••EType(_....,IE E ~"?•1••_.Z
Sample (C"comp,o-a.lOJOII.~{!(,if ••Sample Identification.Client 10 (Lab 10)Samole Oato Time G=orab'~,-~Speclallnstructions/Note:IlTo'••••••.••••,u,."-:><..Preservation Code:X IX
SG.3 (2-6)(680.21762'.10)6129122 13:05 Solid X 1Fa<:;lern
SG-4 (2-6)(680-21762'.11)6129122 13:25 Solid X 1FJ'I<:;tprn
SG-6 (2-6)(680-21762'.12)6129122 13:45 Solid X 1Fao:.tprn
SG.7 (2-6)(680.21762'.13)6129122 14:30 Solid X 1Fa<:t"'rn
SG.8 (2-6)(680-21762'.14)6129122 14:15 Solid X 1Fadern
Soil Dup (680-217621-15)6129122 Eastern Solid X 1
Note:Sinal labor1l1oryaeeredllPtiOns llr(ltvbject ta chlIngc,EUfOlinsEnvfrorIm(!nt Testing Southl!!lsl.LlC places till!owml!flrnp 01 method.IInlilyleSoaceteditatiorl compllllrce upon out subcontract laborllt~.This Slimp/a snipment islOM1lrdl!d uncterehaln-ol-wslody.IIthe laborlllory
does not currently maln'.aln aoercditetlon In the State 01 Origin lisled above lor aMtysislteststmatrix b(!inganalyzed.till!samples musllK!lhippl!d blletl ta the Eurofms Environment Tesling Southeasl.LlC Iaborlllory oro'.hl!tInslructions willbe provided.Anychanges ta aweditation
statll$Itlould be brought ta Eurofms Environment Testing Southeast,LlC atlentlon Immediately.IIall requested accreditations Ire eurrenllo dale.return the Ilgned Chain V.Cuslody lIt1esllng 113IBid eompliearce 10 EUfOfmsEnvimnment Testing Southeast.UC.
Possible Hazard Idenfification Sample Disposal (A fcc may be assessed If samples are retslned longer than 1month)
Unconfirmod oReturn ToClient 0 Disposol Bv Lob 0 ArcMveFor Months
Deliverable Requested:I,II,Ill,IV,Other (specify)Primary Deliverable Rank:2 Speciallnstructions/OC Requirements:
Empty Kit Relinquished by:IDale:!Time:Melhocl01Shipment
Retmquished 2lc Z 0817i~Comj)8ny ""'7'"by:I,;'-t.IIJu!r le;,rrJOW2z lOCO 1~1.)I .••••••
RelinQuished by:Oatctrime:Company ""'''lP'by:V ,Oalcnime:iCom••ny -R2206083 5Rll1lnquithedby:Dillefrime:Complny Received by:Dalernme'Euronnl ET ~Itann,rty TntAm,rtCiIGI'••nhou'l PraJlet SS00217G21
Custody Seals Intact:ICustodY Seal No.:Cooler Tempetalure(l)-C Ind Olher Remarill.
11111111111111111111111111111111111111111111111111Ii.Yes Ii.No Page 9 of 69Page 113 of 176 7/14/2022
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Y N
Y N
Same Day Rule
lit...(R22060si-5o;ooler Receipt and Preservation Check FO),\\nm~\\i~'\Wlul,mi"i,\i,\,,\\\\\,,\
Project/Client EGI r()f rflJ FolderNumber _
Cooler received onrnjtJ.e12 7.by:M COURIER:ALS UP~VELOCITY CLIENT,
I Were Custody seals on outside of cooler?N Sa Perchlorate samples have required headspace?Y N NA
2 Custody papers properly completed (ink,signed)?N 5b Did VOA vials,Alk,or Sulfide have sig"bubbles?Y N
3 .Did all bottles arrive in good condition (unbroken).N 6 Where did the bottles originate?ALS/ROC CL
4 Circle:etl ry Ice Gel packs present?N 7 SoilVOA received as:Bulk Encore
8.Temperature Readings From:Temp Blank
Observed Temp (0C)
Within (l.60C?Y N Y N Y N
If <O°C,were samples frozen?Y N Y N.Y N
If out of Temperature,note packinglice condition:.Ice melted Poorly Packed (described below)
&Client Approval to Run Samples:Standing Approval Client aware at drop-off Client notified by:_
All samples held in storage location:£-002-by on OJbjlzat \OD-t
5035 samples placed in storage location:by on __at __within 48 hours of sampling?Y N
""""--""",•••,7/6/;11 ,••.~[3:B !£':JIt9.Were allbottle labels coinplete (i.e.analysiS;pr<iservation,etc.)?.7.i NO .
10.Did all bottle labels and tags agree with custody papers?.NO
11 Were correct containers used for the tests indicated?NO
12.Were 5035 vials acceptable (no extra labels,not leaking)?YES NO ~13.Air Samples:Cassettes I Tubes Intact YIN with MS YIN Canisters Pressurized Tedlar@B8l!SInflated N/ApHLotoftestReagentPreserved?Lot Rei:eived Exp Sample ID Vol.Lot Added FinalpaperYesNo.Adjusted Added pH>12 NaOH
<2 HNo,
~H2SO4<4 NaHS045-9 .For608"""No='Notiryfor 3day
Residual ForCN,If +.contact PM to add
Chlorine Phenol,625,NlbS,o,(625.608.
(-)608pest 522 CNJ.ascorbic(phenol).
Na2S2o,
ZnAcetate --"VOAs and 1664 Not to be tested before analysis.
HCI """"Otherwise,all bottles of all samples with chemical preservativesarechecked--inot iust reoresentativesl.
Bottle lot numbers:C/fM '\Jar.5
Explain all Discrepancies!Other Comments:
Labels secondaryreviewed by:-L
PC SecondaryReview:_
P:\INTRANET\QAQC\Fonns Controlled\Cooler Receipt rl9.doc
HPROD BULK
HTR FLDT
SUB HOFB
ALS LL3541
"significant air bubbles:VOA >.5-6 mm:WC>1 in.diameter
0310212021
Page 10 of 69Page 114 of 176 7/14/2022
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Miscellaneous Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 11 of 69Page 115 of 176 7/14/2022
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RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\QUALIF_routine rev 6.doc 9/30/21
REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
J Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
DoD: concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
“Notes” column of the Form I, this qualifier
denotes analysis was performed out of
Holding Time.
H Analysis was performed out of hold time for
tests that have an “immediate” hold time
criteria.
# Spike was diluted out.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post-Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% difference between the two
GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesticide/Aroclor is not
confirmed (≥100% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value derived
from a study designed to provide the lowest
concentration that will be detected 99% of the time.
Values between the MDL and MRL are estimated
(see J qualifier).
LOD Limit of Detection. A value at or above the MDL
which has been verified to be detectable.
ND Non-Detect. Analyte was not detected at the
concentration listed. Same as U qualifier.

Rochester Lab ID # for State Accreditations¹

¹ Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements of the current NELAP/TNI standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited. For a specific list of accredited analytes, contact the laboratory or go to
https://www.alsglobal.com/locations/americas/north-america/usa/new-york/rochester-environmental

NELAP States
Florida ID # E87674
New Hampshire ID # 2941
New York ID # 10145
Pennsylvania ID# 68-786
Virginia #460167
Non-NELAP States
Connecticut ID #PH0556
Delaware Approved
Maine ID #NY01587
North Carolina #36701
North Carolina #676
Rhode Island LAO00333
Page 12 of 69Page 116 of 176 7/14/2022
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ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources Board
CAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental Quality
DHS Department of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation Program
GC Gas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LUFT Leaking Underground Fuel Tank
M Modified
MCL Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable Number
MRL Method Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not Detected
NIOSH National Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum Hydrocarbons
tr Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
Acronyms
ALS Laboratory Group
Page 13 of 69Page 117 of 176 7/14/2022
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ALS SOP Total SolidsSoil
ALS Group USA, Corp.
dba ALS Environmental
Client:
Analyte
New York Department of HealthCertifying Agency:
Non-Certified Analytes
Matrix
Project:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621/68027092
Service Request:R2206083
Method
22-0000632534 rev 00Superset Reference:Printed 7/14/2022 3:33:08 PM Page 14 of 69Page 118 of 176 7/14/2022
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-1 (10-15)Sample Name:
Lab Code:R2206083-001
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-1 (10-15)Sample Name:
Lab Code:R2206083-001.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-2 (11-14)Sample Name:
Lab Code:R2206083-002
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-2 (11-14)Sample Name:
Lab Code:R2206083-002.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
Printed 7/14/2022 3:32:55 PM 22-0000632534 rev 00Superset Reference:
Page 15 of 69Page 119 of 176 7/14/2022
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-3 (7-12)Sample Name:
Lab Code:R2206083-003
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-3 (7-12)Sample Name:
Lab Code:R2206083-003.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-4 (13-17)Sample Name:
Lab Code:R2206083-004
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-4 (13-17)Sample Name:
Lab Code:R2206083-004.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
Printed 7/14/2022 3:32:55 PM 22-0000632534 rev 00Superset Reference:
Page 16 of 69Page 120 of 176 7/14/2022
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-1 (2-6)Sample Name:
Lab Code:R2206083-005
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-1 (2-6)Sample Name:
Lab Code:R2206083-005.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-2 (2-6)Sample Name:
Lab Code:R2206083-006
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-2 (2-6)Sample Name:
Lab Code:R2206083-006.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
Printed 7/14/2022 3:32:55 PM 22-0000632534 rev 00Superset Reference:
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-3 (2-6)Sample Name:
Lab Code:R2206083-007
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SS-3 (2-6)Sample Name:
Lab Code:R2206083-007.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-1 (2-6)Sample Name:
Lab Code:R2206083-008
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-1 (2-6)Sample Name:
Lab Code:R2206083-008.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
Printed 7/14/2022 3:32:55 PM 22-0000632534 rev 00Superset Reference:
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-2 (2-6)Sample Name:
Lab Code:R2206083-009
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-2 (2-6)Sample Name:
Lab Code:R2206083-009.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-3 (2-6)Sample Name:
Lab Code:R2206083-010
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-3 (2-6)Sample Name:
Lab Code:R2206083-010.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
Printed 7/14/2022 3:32:55 PM 22-0000632534 rev 00Superset Reference:
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-4 (2-6)Sample Name:
Lab Code:R2206083-011
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-4 (2-6)Sample Name:
Lab Code:R2206083-011.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-6 (2-6)Sample Name:
Lab Code:R2206083-012
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-6 (2-6)Sample Name:
Lab Code:R2206083-012.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-7 (2-6)Sample Name:
Lab Code:R2206083-013
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-7 (2-6)Sample Name:
Lab Code:R2206083-013.R01
7199 KWONG KWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-8 (2-6)Sample Name:
Lab Code:R2206083-014
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
SG-8 (2-6)Sample Name:
Lab Code:R2206083-014.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
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07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
Soil DupSample Name:
Lab Code:R2206083-015
7199 KWONG KWONG
ALS SOP KAWONG
07/6/22Date Received:
Date Collected:
SoilSample Matrix:
06/28/22
Extracted/Digested ByAnalysis Method Analyzed By
Soil DupSample Name:
Lab Code:R2206083-015.R01
7199 KWONG KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206083
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RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev 2.doc 12/20/19

INORGANIC PREPARATION METHODS
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.

Water/Liquid Matrix Solid/Soil/Non-Aqueous Matrix

Analytical Method Preparation Method Analytical Method Preparation
Method
200.7 200.2 6010C 3050B
200.8 200.2 6020A 3050B
6010C 3005A/3010A 6010C TCLP (1311)
extract
3005A/3010A
6020A ILM05.3 6010 SPLP (1312) extract 3005A/3010A
9034 Sulfide Acid Soluble 9030B 7199 3060A
SM 4500-CN-E Residual
Cyanide
SM 4500-CN-G 300.0 Anions/ 350.1/
353.2/ SM 2320B/ SM
5210B/ 9056A Anions
DI extraction
SM 4500-CN-E WAD
Cyanide
SM 4500-CN-I For analytical methods not listed, the preparation
method is the same as the analytical method reference.

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Sample Results
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
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General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
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Client:
07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 10:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-1 (10-15)
Lab Code:R2206083-001
Chromium, Hexavalent 07/07/22 20:32 07/07/2210.070.643.457199 mg/Kg
Chromium, Hexavalent 07/13/22 13:46 07/12/2210.070.641.847199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 10:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-1 (10-15)
Lab Code:R2206083-001
Total Solids 07/07/22 06:15 NA1--60.9ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 12:05
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-2 (11-14)
Lab Code:R2206083-002
Chromium, Hexavalent 07/07/22 22:23 07/07/2210.050.471.197199 mg/Kg
Chromium, Hexavalent 07/13/22 15:18 07/12/2210.050.470.977199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 12:05
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-2 (11-14)
Lab Code:R2206083-002
Total Solids 07/07/22 06:15 NA1--83.6ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-3 (7-12)
Lab Code:R2206083-003
Chromium, Hexavalent 07/07/22 22:38 07/07/2210.050.47 J0.317199 mg/Kg
Chromium, Hexavalent 07/13/22 15:34 07/12/2210.050.45 J0.147199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-3 (7-12)
Lab Code:R2206083-003
Total Solids 07/07/22 06:15 NA1--85.0ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 10:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-4 (13-17)
Lab Code:R2206083-004
Chromium, Hexavalent 07/07/22 23:10 07/07/2210.060.520.537199 mg/Kg
Chromium, Hexavalent 07/13/22 15:49 07/12/2210.060.53 J0.477199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 10:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:GW-4 (13-17)
Lab Code:R2206083-004
Total Solids 07/07/22 06:15 NA1--74.6ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:40
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-1 (2-6)
Lab Code:R2206083-005
Chromium, Hexavalent 07/07/22 23:25 07/07/2210.060.502.617199 mg/Kg
Chromium, Hexavalent 07/13/22 16:22 07/12/2210.060.511.727199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:40
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-1 (2-6)
Lab Code:R2206083-005
Total Solids 07/07/22 06:15 NA1--76.7ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:00
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-2 (2-6)
Lab Code:R2206083-006
Chromium, Hexavalent 07/07/22 23:41 07/07/2210.060.500.677199 mg/Kg
Chromium, Hexavalent 07/13/22 16:37 07/12/2210.060.51 J0.167199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:00
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-2 (2-6)
Lab Code:R2206083-006
Total Solids 07/07/22 06:15 NA1--79.1ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-3 (2-6)
Lab Code:R2206083-007
Chromium, Hexavalent 07/07/22 23:56 07/07/2210.050.470.877199 mg/Kg
Chromium, Hexavalent 07/13/22 16:56 07/12/2210.060.48 J0.397199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SS-3 (2-6)
Lab Code:R2206083-007
Total Solids 07/07/22 06:15 NA1--82.4ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:50
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-1 (2-6)
Lab Code:R2206083-008
Chromium, Hexavalent 07/08/22 00:11 07/07/2210.050.471.227199 mg/Kg
Chromium, Hexavalent 07/13/22 17:11 07/12/2210.060.480.967199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:50
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-1 (2-6)
Lab Code:R2206083-008
Total Solids 07/07/22 06:15 NA1--83.5ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-2 (2-6)
Lab Code:R2206083-009
Chromium, Hexavalent 07/08/22 00:44 07/07/2210.060.490.897199 mg/Kg
Chromium, Hexavalent 07/13/22 17:26 07/12/2210.060.50 J0.327199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 11:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-2 (2-6)
Lab Code:R2206083-009
Total Solids 07/07/22 06:15 NA1--78.3ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:05
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-3 (2-6)
Lab Code:R2206083-010
Chromium, Hexavalent 07/08/22 01:00 07/07/2210.060.570.777199 mg/Kg
Chromium, Hexavalent 07/13/22 17:58 07/12/2210.060.55 J0.417199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:05
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-3 (2-6)
Lab Code:R2206083-010
Total Solids 07/07/22 06:15 NA1--70.2ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:25
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-4 (2-6)
Lab Code:R2206083-011
Chromium, Hexavalent 07/08/22 01:15 07/07/2210.060.48 J0.457199 mg/Kg
Chromium, Hexavalent 07/13/22 18:13 07/12/2210.050.47 J0.167199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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Client:
07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:25
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-4 (2-6)
Lab Code:R2206083-011
Total Solids 07/07/22 06:15 NA1--83.0ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:45
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-6 (2-6)
Lab Code:R2206083-012
Chromium, Hexavalent 07/08/22 01:30 07/07/2210.050.471.077199 mg/Kg
Chromium, Hexavalent 07/13/22 18:28 07/12/2210.050.47 J0.227199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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Client:
07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 13:45
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-6 (2-6)
Lab Code:R2206083-012
Total Solids 07/07/22 06:15 NA1--85.0ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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Client:
07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:30
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-7 (2-6)
Lab Code:R2206083-013
Chromium, Hexavalent 07/08/22 01:46 07/07/2210.050.480.587199 mg/Kg
Chromium, Hexavalent 07/13/22 18:43 07/12/2210.060.49 J0.207199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:30
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-7 (2-6)
Lab Code:R2206083-013
Total Solids 07/07/22 06:15 NA1--81.2ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:15
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-8 (2-6)
Lab Code:R2206083-014
Chromium, Hexavalent 07/08/22 02:17 07/07/2210.050.450.747199 mg/Kg
Chromium, Hexavalent 07/13/22 18:59 07/12/2210.050.46 J0.237199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22 14:15
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:SG-8 (2-6)
Lab Code:R2206083-014
Total Solids 07/07/22 06:15 NA1--85.0ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:Soil Dup
Lab Code:R2206083-015
Chromium, Hexavalent 07/08/22 02:32 07/07/2210.060.54 J0.407199 mg/Kg
Chromium, Hexavalent 07/13/22 19:32 07/12/2210.060.55 J0.377199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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07/06/22 10:00
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/28/22
Inorganic Parameters
Basis:As Received
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:Soil Dup
Lab Code:R2206083-015
Total Solids 07/07/22 06:15 NA1--73.2ALS SOP Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:57 PM 22-0000632534 rev 00Superset Reference:
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QC Summary Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 56 of 69Page 160 of 176 7/14/2022
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General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 57 of 69Page 161 of 176 7/14/2022
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Client:
NA
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:Method Blank
Lab Code:R2206083-MB1
Chromium, Hexavalent 07/07/22 20:01 07/07/2210.050.40 UND7199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
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Client:
NA
R2206083
Date Received:
Date Collected:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLMRLResultUnits
Sample Name:Method Blank
Lab Code:R2206083-MB2
Chromium, Hexavalent 07/13/22 13:16 07/12/2210.050.40 UND7199 mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/14/2022 3:32:58 PM 22-0000632534 rev 00Superset Reference:
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QA/QC Report
mg/Kg
R2206083-001 Basis:Lab Code:
Units:Sample Name:GW-1 (10-15)
Chromium, Hexavalent
Matrix Spike Summary
Dry
Client:
Project:
Sample Matrix:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621/68027092
Soil
Service Request:
Date Analyzed:
Date Received:
R2206083
07/7/22
07/06/22
Date Collected:06/28/22
EPA 3060A
7199
Prep Method:
Analysis Method:
Analyte Name ResultSample Result Spike Amount % Rec
Matrix Spike
R2206083-001MS1
% Rec Limits
ALS Group USA, Corp.dba ALS Environmental
07/7/22Date Extracted:
Chromium, Hexavalent 3.45 60.2 65.7 86 75-125
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
Matrix Spike and Matrix Spike Duplicate Data is presented for information purposes only. The matrix may or may not be relevant to samples reported in this report. The laboratory evaluates
system performance based on the LCS and LCSD control limits.
Page 60 of 69Page 164 of 176 7/14/2022
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QA/QC Report
mg/Kg
R2206083-001 Basis:Lab Code:
Units:Sample Name:GW-1 (10-15)
Chromium, Hexavalent
Matrix Spike Summary
Dry
Client:
Project:
Sample Matrix:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621/68027092
Soil
Service Request:
Date Analyzed:
Date Received:
R2206083
07/7/22
07/06/22
Date Collected:06/28/22
EPA 3060A
7199
Prep Method:
Analysis Method:
Analyte Name ResultSample Result Spike Amount % Rec
Matrix Spike
R2206083-001MS2
% Rec Limits
ALS Group USA, Corp.dba ALS Environmental
07/7/22Date Extracted:
Chromium, Hexavalent 3.45 673 1070 63 *75-125
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
Matrix Spike and Matrix Spike Duplicate Data is presented for information purposes only. The matrix may or may not be relevant to samples reported in this report. The laboratory evaluates
system performance based on the LCS and LCSD control limits.
Page 61 of 69Page 165 of 176 7/14/2022
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QA/QC Report
mg/Kg
R2206083-001 Basis:Lab Code:
Units:Sample Name:GW-1 (10-15)
Chromium, Hexavalent
Matrix Spike Summary
Dry
Client:
Project:
Sample Matrix:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621/68027092
Soil
Service Request:
Date Analyzed:
Date Received:
R2206083
07/13/22
07/06/22
Date Collected:06/28/22
EPA 3060A
7199
Prep Method:
Analysis Method:
Analyte Name ResultSample Result Spike Amount % Rec
Matrix Spike
R2206083-001MS3
% Rec Limits
ALS Group USA, Corp.dba ALS Environmental
07/12/22Date Extracted:
Chromium, Hexavalent 3.45 59.0 64.6 86 75-125
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
Matrix Spike and Matrix Spike Duplicate Data is presented for information purposes only. The matrix may or may not be relevant to samples reported in this report. The laboratory evaluates
system performance based on the LCS and LCSD control limits.
Page 62 of 69Page 166 of 176 7/14/2022
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QA/QC Report
mg/Kg
R2206083-001 Basis:Lab Code:
Units:Sample Name:GW-1 (10-15)
Chromium, Hexavalent
Matrix Spike Summary
Dry
Client:
Project:
Sample Matrix:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project 680-217621/68027092
Soil
Service Request:
Date Analyzed:
Date Received:
R2206083
07/13/22
07/06/22
Date Collected:06/28/22
EPA 3060A
7199
Prep Method:
Analysis Method:
Analyte Name ResultSample Result Spike Amount % Rec
Matrix Spike
R2206083-001MS4
% Rec Limits
ALS Group USA, Corp.dba ALS Environmental
07/12/22Date Extracted:
Chromium, Hexavalent 3.45 956 1160 82 75-125
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
Matrix Spike and Matrix Spike Duplicate Data is presented for information purposes only. The matrix may or may not be relevant to samples reported in this report. The laboratory evaluates
system performance based on the LCS and LCSD control limits.
Page 63 of 69Page 167 of 176 7/14/2022
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ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)Service Request:R2206083
06/28/22Date Collected:
Date Received:07/06/22
07/07/22Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
GW-1 (10-15)mg/Kg
Basis:
Units:
R2206083-001 DryLab Code:
Sample Name:
RPD LimitMRLMDL
Analysis
Method RPD
Duplicate
Sample
R2206083-
001DUP1
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Chromium, Hexavalent 28 *0.65 0.07 3.45 4.55 4.00 207199
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
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ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)Service Request:R2206083
06/28/22Date Collected:
Date Received:07/06/22
07/13/22Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
GW-1 (10-15)mg/Kg
Basis:
Units:
R2206083-001 DryLab Code:
Sample Name:
RPD LimitMRLMDL
Analysis
Method RPD
Duplicate
Sample
R2206083-
001DUP2
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Chromium, Hexavalent 71 #0.64 0.07 3.45 1.64 2.55 207199
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:56 PM 22-0000632534 rev 00Superset Reference:
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ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)Service Request:R2206083
06/28/22Date Collected:
Date Received:07/06/22
07/07/22Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
GW-2 (11-14)Percent
Basis:
Units:
R2206083-002 As ReceivedLab Code:
Sample Name:
RPD LimitMRLMDL
Analysis
Method RPD
Duplicate
Sample
R2206083-
002DUP
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Total Solids <1 --83.6 83.4 83.5 20ALS SOP
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:58 PM 22-0000632534 rev 00Superset Reference:
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ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)Service Request:R2206083
06/28/22Date Collected:
Date Received:07/06/22
07/07/22Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
SG-3 (2-6)Percent
Basis:
Units:
R2206083-010 As ReceivedLab Code:
Sample Name:
RPD LimitMRLMDL
Analysis
Method RPD
Duplicate
Sample
R2206083-
010DUP
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Total Solids <1 --70.2 70.4 70.3 20ALS SOP
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 7/14/2022 3:32:58 PM 22-0000632534 rev 00Superset Reference:
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Analyte Name
R2206083
Date Analyzed:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
General Chemistry Parameters
Dry
mg/Kg
Basis:
Units:
Lab Control Sample
R2206083-LCS1
07/07/22
Spike AmountResult % Rec % Rec LimitsAnalytical Method
dba ALS EnvironmentalALS Group USA, Corp.
QA/QC Report
Chromium, Hexavalent 80-12093 611571 7199
22-0000632534 rev 00Superset Reference:Printed 7/14/2022 3:32:57 PM
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Analyte Name
R2206083
Date Analyzed:
Service Request:
Soil
Greenhouse Project 680-217621/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
General Chemistry Parameters
Dry
mg/Kg
Basis:
Units:
Lab Control Sample
R2206083-LCS2
07/13/22
Spike AmountResult % Rec % Rec LimitsAnalytical Method
dba ALS EnvironmentalALS Group USA, Corp.
QA/QC Report
Chromium, Hexavalent 80-12097 605587 7199
22-0000632534 rev 00Superset Reference:Printed 7/14/2022 3:32:58 PM
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-217621-1
Login Number: 217621
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
Page 176 of 176 7/14/2022
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ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-217736-1
Client Project/Site: Greenhouse Project
For:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, North Carolina 27616
Attn: Michael Pfeifer
Authorized for release by:
7/12/2022 4:11:04 PM
John Andros, Project Manager I
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Definitions/Glossary
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Qualifiers
GC/MS VOA
Qualifier Description
*-LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
*+LCS and/or LCSD is outside acceptance limits, high biased.
E Result exceeded calibration range.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: S&ME, Inc.Job ID: 680-217736-1
Project/Site: Greenhouse Project
Lab Sample ID Client Sample ID Matrix Collected Received
680-217736-1 GW-4 Water 06/30/22 14:10 07/01/22 11:00
680-217736-2 GW-3 Water 06/30/22 15:15 07/01/22 11:00
680-217736-3 GW-2 Water 06/30/22 16:20 07/01/22 11:00
680-217736-4 GW-1 Water 06/30/22 17:25 07/01/22 11:00
680-217736-5 Duplicate Water 06/30/22 00:00 07/01/22 11:00
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Case Narrative
Client: S&ME, Inc.Job ID: 680-217736-1
Project/Site: Greenhouse Project
Job ID: 680-217736-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-217736-1
Comments
No additional comments.
Receipt
The samples were received on 7/1/2022 11:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.1º C.
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-1Client Sample ID: GW-4
Matrix: WaterDate Collected: 06/30/22 14:10
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 0.360 ug/L 07/08/22 19:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.210 ug/L 07/08/22 19:24 11,1,1-Trichloroethane ND
1.00 0.400 ug/L 07/08/22 19:24 11,1,2,2-Tetrachloroethane ND
1.00 0.230 ug/L 07/08/22 19:24 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.00 0.320 ug/L 07/08/22 19:24 11,1,2-Trichloroethane ND
1.00 0.330 ug/L 07/08/22 19:24 11,1-Dichloroethane ND
1.00 0.330 ug/L 07/08/22 19:24 11,1-Dichloroethene ND
1.00 0.280 ug/L 07/08/22 19:24 11,1-Dichloropropene ND
5.00 0.810 ug/L 07/08/22 19:24 11,2,3-Trichlorobenzene ND
1.00 0.480 ug/L 07/08/22 19:24 11,2,3-Trichloropropane ND
5.00 0.530 ug/L 07/08/22 19:24 11,2,4-Trichlorobenzene ND
1.00 0.430 ug/L 07/08/22 19:24 11,2,4-Trimethylbenzene ND
5.00 1.80 ug/L 07/08/22 19:24 11,2-Dibromo-3-Chloropropane ND
1.00 0.310 ug/L 07/08/22 19:24 11,2-Dichlorobenzene ND
1.00 0.250 ug/L 07/08/22 19:24 11,2-Dichloroethane ND
1.00 0.220 ug/L 07/08/22 19:24 11,2-Dichloropropane ND
1.00 0.280 ug/L 07/08/22 19:24 11,3,5-Trimethylbenzene ND
1.00 0.310 ug/L 07/08/22 19:24 11,3-Dichlorobenzene ND
1.00 0.360 ug/L 07/08/22 19:24 11,3-Dichloropropane ND
1.00 0.310 ug/L 07/08/22 19:24 11,4-Dichlorobenzene ND
1.00 0.350 ug/L 07/08/22 19:24 12,2-Dichloropropane ND
10.0 6.40 ug/L 07/08/22 19:24 12-Butanone (MEK)ND
1.00 0.250 ug/L 07/08/22 19:24 12-Chlorotoluene ND
10.0 3.20 ug/L 07/08/22 19:24 12-Hexanone ND
1.00 0.410 ug/L 07/08/22 19:24 14-Chlorotoluene ND
1.00 0.440 ug/L 07/08/22 19:24 14-Isopropyltoluene ND
10.0 2.70 ug/L 07/08/22 19:24 14-Methyl-2-pentanone (MIBK)ND
10.0 3.70 ug/L 07/08/22 19:24 1AcetoneND
1.00 0.270 ug/L 07/08/22 19:24 1BenzeneND
1.00 0.240 ug/L 07/08/22 19:24 1BromobenzeneND
1.00 0.590 ug/L 07/08/22 19:24 1BromoformND
5.00 3.70 ug/L 07/08/22 19:24 1BromomethaneND*+
2.00 0.430 ug/L 07/08/22 19:24 1Carbon disulfide ND
1.00 0.300 ug/L 07/08/22 19:24 1Carbon tetrachloride ND
1.00 0.150 ug/L 07/08/22 19:24 1ChlorobenzeneND
1.00 0.340 ug/L 07/08/22 19:24 1ChlorobromomethaneND
1.00 0.390 ug/L 07/08/22 19:24 1ChlorodibromomethaneND
5.00 4.60 ug/L 07/08/22 19:24 1ChloroethaneND*+
1.00 0.270 ug/L 07/08/22 19:24 1ChloroformND
1.00 0.540 ug/L 07/08/22 19:24 1ChloromethaneND
1.00 0.250 ug/L 07/08/22 19:24 1cis-1,2-Dichloroethene ND
1.00 0.260 ug/L 07/08/22 19:24 1cis-1,3-Dichloropropene ND
1.00 0.340 ug/L 07/08/22 19:24 1DibromomethaneND
1.00 0.250 ug/L 07/08/22 19:24 1DichlorobromomethaneND
1.00 0.360 ug/L 07/08/22 19:24 1DichlorodifluoromethaneND
10.0 5.00 ug/L 07/08/22 19:24 1Ethyl acetate ND
1.00 0.200 ug/L 07/08/22 19:24 1EthylbenzeneND
1.00 0.330 ug/L 07/08/22 19:24 1Ethylene Dibromide ND
5.00 0.220 ug/L 07/08/22 19:24 1HexachlorobutadieneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-1Client Sample ID: GW-4
Matrix: WaterDate Collected: 06/30/22 14:10
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 5.00 0.650 ug/L 07/08/22 19:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 3.90 ug/L 07/08/22 19:24 1IodomethaneND*+
10.0 0.700 ug/L 07/08/22 19:24 1Isopropyl ether ND
1.00 0.260 ug/L 07/08/22 19:24 1IsopropylbenzeneND
1.00 0.490 ug/L 07/08/22 19:24 1m,p-Xylene ND
5.00 0.810 ug/L 07/08/22 19:24 1Methyl tert-butyl ether ND
5.00 3.20 ug/L 07/08/22 19:24 1Methylene Chloride ND
5.00 2.40 ug/L 07/08/22 19:24 1NaphthaleneND
1.00 0.520 ug/L 07/08/22 19:24 1n-Butylbenzene ND
1.00 0.430 ug/L 07/08/22 19:24 1n-Heptane ND *+
1.00 0.410 ug/L 07/08/22 19:24 1N-Propylbenzene ND
1.00 0.260 ug/L 07/08/22 19:24 1o-Xylene ND
1.00 0.530 ug/L 07/08/22 19:24 1sec-Butylbenzene ND
1.00 0.270 ug/L 07/08/22 19:24 1StyreneND
1.00 0.430 ug/L 07/08/22 19:24 1tert-Butylbenzene ND
0.500 0.350 ug/L 07/08/22 19:24 1TetrachloroetheneND
1.00 0.250 ug/L 07/08/22 19:24 1TolueneND
1.00 0.340 ug/L 07/08/22 19:24 1trans-1,2-Dichloroethene ND
1.00 0.230 ug/L 07/08/22 19:24 1trans-1,3-Dichloropropene ND
2.00 1.25 ug/L 07/08/22 19:24 1trans-1,4-Dichloro-2-butene ND
1.00 0.200 ug/L 07/08/22 19:24 1TrichloroetheneND
1.00 0.330 ug/L 07/08/22 19:24 1TrichlorofluoromethaneND
2.00 0.690 ug/L 07/08/22 19:24 1Vinyl acetate ND *+
1.00 0.400 ug/L 07/08/22 19:24 1Vinyl chloride ND
1.00 0.230 ug/L 07/08/22 19:24 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)84 60-124 07/08/22 19:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 07/08/22 19:24 170-130
Dibromofluoromethane (Surr)100 07/08/22 19:24 170-130
Toluene-d8 (Surr)108 07/08/22 19:24 170-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 9.31 4.28 ug/L 07/07/22 11:34 07/07/22 23:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.31 3.07 ug/L 07/07/22 11:34 07/07/22 23:47 12,4,5-Trichlorophenol ND
9.31 2.05 ug/L 07/07/22 11:34 07/07/22 23:47 12,4,6-Trichlorophenol ND
9.31 3.45 ug/L 07/07/22 11:34 07/07/22 23:47 12,4-Dichlorophenol ND
9.31 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 12,4-Dimethylphenol ND
46.6 14.9 ug/L 07/07/22 11:34 07/07/22 23:47 12,4-Dinitrophenol ND
9.31 2.14 ug/L 07/07/22 11:34 07/07/22 23:47 12,4-Dinitrotoluene ND
9.31 2.61 ug/L 07/07/22 11:34 07/07/22 23:47 12,6-Dinitrotoluene ND
9.31 4.47 ug/L 07/07/22 11:34 07/07/22 23:47 12-Chloronaphthalene ND
9.31 2.98 ug/L 07/07/22 11:34 07/07/22 23:47 12-Chlorophenol ND
9.31 4.28 ug/L 07/07/22 11:34 07/07/22 23:47 12-Methylnaphthalene ND
9.31 1.68 ug/L 07/07/22 11:34 07/07/22 23:47 12-Methylphenol ND
46.6 2.70 ug/L 07/07/22 11:34 07/07/22 23:47 12-Nitroaniline ND
9.31 3.63 ug/L 07/07/22 11:34 07/07/22 23:47 12-Nitrophenol ND
9.31 1.30 ug/L 07/07/22 11:34 07/07/22 23:47 13 & 4 Methylphenol ND
55.9 9.31 ug/L 07/07/22 11:34 07/07/22 23:47 13,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-1Client Sample ID: GW-4
Matrix: WaterDate Collected: 06/30/22 14:10
Date Received: 07/01/22 11:00
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 46.6 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
46.6 4.93 ug/L 07/07/22 11:34 07/07/22 23:47 14,6-Dinitro-2-methylphenol ND
9.31 4.38 ug/L 07/07/22 11:34 07/07/22 23:47 14-Bromophenyl phenyl ether ND
9.31 2.33 ug/L 07/07/22 11:34 07/07/22 23:47 14-Chloro-3-methylphenol ND
18.6 0.931 ug/L 07/07/22 11:34 07/07/22 23:47 14-Chloroaniline ND
9.31 4.93 ug/L 07/07/22 11:34 07/07/22 23:47 14-Chlorophenyl phenyl ether ND
46.6 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 14-Nitroaniline ND
46.6 7.54 ug/L 07/07/22 11:34 07/07/22 23:47 14-Nitrophenol ND
9.31 4.10 ug/L 07/07/22 11:34 07/07/22 23:47 1AcenaphtheneND
9.31 3.35 ug/L 07/07/22 11:34 07/07/22 23:47 1AcenaphthyleneND
9.31 2.05 ug/L 07/07/22 11:34 07/07/22 23:47 1AcetophenoneND
9.31 3.35 ug/L 07/07/22 11:34 07/07/22 23:47 1AnthraceneND
9.31 2.05 ug/L 07/07/22 11:34 07/07/22 23:47 1AtrazineND
9.31 4.47 ug/L 07/07/22 11:34 07/07/22 23:47 1BenzaldehydeND
9.31 3.91 ug/L 07/07/22 11:34 07/07/22 23:47 1Benzo[a]anthracene ND
9.31 2.61 ug/L 07/07/22 11:34 07/07/22 23:47 1Benzo[a]pyrene ND
9.31 2.89 ug/L 07/07/22 11:34 07/07/22 23:47 1Benzo[b]fluoranthene ND
9.31 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 1Benzo[g,h,i]perylene ND
9.31 2.70 ug/L 07/07/22 11:34 07/07/22 23:47 1Benzo[k]fluoranthene ND
9.31 2.89 ug/L 07/07/22 11:34 07/07/22 23:47 1bis (2-chloroisopropyl) ether ND
9.31 1.68 ug/L 07/07/22 11:34 07/07/22 23:47 1Bis(2-chloroethoxy)methane ND
9.31 3.35 ug/L 07/07/22 11:34 07/07/22 23:47 1Bis(2-chloroethyl)ether ND
9.31 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 1Bis(2-ethylhexyl) phthalate ND
9.31 2.61 ug/L 07/07/22 11:34 07/07/22 23:47 1Butyl benzyl phthalate ND
9.31 2.61 ug/L 07/07/22 11:34 07/07/22 23:47 1CaprolactamND
9.31 1.68 ug/L 07/07/22 11:34 07/07/22 23:47 1CarbazoleND
9.31 3.54 ug/L 07/07/22 11:34 07/07/22 23:47 1ChryseneND
9.31 2.79 ug/L 07/07/22 11:34 07/07/22 23:47 1Dibenz(a,h)anthracene ND
9.31 1.77 ug/L 07/07/22 11:34 07/07/22 23:47 1DibenzofuranND
9.31 2.05 ug/L 07/07/22 11:34 07/07/22 23:47 1Diethyl phthalate 17.5
9.31 1.96 ug/L 07/07/22 11:34 07/07/22 23:47 1Dimethyl phthalate ND
9.31 2.14 ug/L 07/07/22 11:34 07/07/22 23:47 1Di-n-butyl phthalate ND
9.31 2.61 ug/L 07/07/22 11:34 07/07/22 23:47 1Di-n-octyl phthalate ND
9.31 1.49 ug/L 07/07/22 11:34 07/07/22 23:47 1FluorantheneND
9.31 3.17 ug/L 07/07/22 11:34 07/07/22 23:47 1FluoreneND
9.31 1.49 ug/L 07/07/22 11:34 07/07/22 23:47 1HexachlorobenzeneND
9.31 3.72 ug/L 07/07/22 11:34 07/07/22 23:47 1HexachlorobutadieneND
9.31 3.26 ug/L 07/07/22 11:34 07/07/22 23:47 1HexachlorocyclopentadieneND
9.31 3.35 ug/L 07/07/22 11:34 07/07/22 23:47 1HexachloroethaneND
9.31 4.00 ug/L 07/07/22 11:34 07/07/22 23:47 1Indeno[1,2,3-cd]pyrene ND
9.31 1.86 ug/L 07/07/22 11:34 07/07/22 23:47 1IsophoroneND
9.31 3.26 ug/L 07/07/22 11:34 07/07/22 23:47 1NaphthaleneND
9.31 3.26 ug/L 07/07/22 11:34 07/07/22 23:47 1NitrobenzeneND
9.31 2.23 ug/L 07/07/22 11:34 07/07/22 23:47 1N-Nitrosodi-n-propylamine ND
9.31 2.70 ug/L 07/07/22 11:34 07/07/22 23:47 1N-Nitrosodiphenylamine ND
46.6 9.22 ug/L 07/07/22 11:34 07/07/22 23:47 1PentachlorophenolND
9.31 4.00 ug/L 07/07/22 11:34 07/07/22 23:47 1PhenanthreneND
9.31 1.40 ug/L 07/07/22 11:34 07/07/22 23:47 1PhenolND
9.31 3.45 ug/L 07/07/22 11:34 07/07/22 23:47 1PyreneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-1Client Sample ID: GW-4
Matrix: WaterDate Collected: 06/30/22 14:10
Date Received: 07/01/22 11:00
2,4,6-Tribromophenol (Surr)103 30-130 07/07/22 11:34 07/07/22 23:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)61 07/07/22 11:34 07/07/22 23:47 125-130
2-Fluorophenol (Surr)37 07/07/22 11:34 07/07/22 23:47 110-130
Nitrobenzene-d5 (Surr)60 07/07/22 11:34 07/07/22 23:47 130-130
Phenol-d5 (Surr)25 07/07/22 11:34 07/07/22 23:47 110-130
Terphenyl-d14 (Surr)83 07/07/22 11:34 07/07/22 23:47 135-131
Method: 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 22:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00500 0.000890 mg/L 07/05/22 17:15 07/06/22 22:18 1Barium0.236
0.000500 0.0000780 mg/L 07/05/22 17:15 07/06/22 22:18 1CadmiumND
0.00500 0.00260 mg/L 07/05/22 17:15 07/06/22 22:18 1ChromiumND
0.00250 0.000340 mg/L 07/05/22 17:15 07/06/22 22:18 1LeadND
0.00250 0.00120 mg/L 07/05/22 17:15 07/06/22 22:18 1SeleniumND
0.00100 0.000390 mg/L 07/05/22 17:15 07/06/22 22:18 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 14:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-2Client Sample ID: GW-3
Matrix: WaterDate Collected: 06/30/22 15:15
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 0.360 ug/L 07/12/22 00:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.210 ug/L 07/12/22 00:18 11,1,1-Trichloroethane ND
1.00 0.400 ug/L 07/12/22 00:18 11,1,2,2-Tetrachloroethane ND
1.00 0.230 ug/L 07/12/22 00:18 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.00 0.320 ug/L 07/12/22 00:18 11,1,2-Trichloroethane ND
1.00 0.330 ug/L 07/12/22 00:18 11,1-Dichloroethane ND
1.00 0.330 ug/L 07/12/22 00:18 11,1-Dichloroethene ND
1.00 0.280 ug/L 07/12/22 00:18 11,1-Dichloropropene ND
5.00 0.810 ug/L 07/12/22 00:18 11,2,3-Trichlorobenzene ND
1.00 0.480 ug/L 07/12/22 00:18 11,2,3-Trichloropropane ND
5.00 0.530 ug/L 07/12/22 00:18 11,2,4-Trichlorobenzene ND
1.00 0.430 ug/L 07/12/22 00:18 11,2,4-Trimethylbenzene ND
5.00 1.80 ug/L 07/12/22 00:18 11,2-Dibromo-3-Chloropropane ND
1.00 0.310 ug/L 07/12/22 00:18 11,2-Dichlorobenzene ND
1.00 0.250 ug/L 07/12/22 00:18 11,2-Dichloroethane ND
1.00 0.220 ug/L 07/12/22 00:18 11,2-Dichloropropane ND
1.00 0.280 ug/L 07/12/22 00:18 11,3,5-Trimethylbenzene ND
1.00 0.310 ug/L 07/12/22 00:18 11,3-Dichlorobenzene ND
1.00 0.360 ug/L 07/12/22 00:18 11,3-Dichloropropane ND
1.00 0.310 ug/L 07/12/22 00:18 11,4-Dichlorobenzene ND
1.00 0.350 ug/L 07/12/22 00:18 12,2-Dichloropropane ND
10.0 6.40 ug/L 07/12/22 00:18 12-Butanone (MEK)ND
1.00 0.250 ug/L 07/12/22 00:18 12-Chlorotoluene ND
10.0 3.20 ug/L 07/12/22 00:18 12-Hexanone ND
1.00 0.410 ug/L 07/12/22 00:18 14-Chlorotoluene ND
1.00 0.440 ug/L 07/12/22 00:18 14-Isopropyltoluene ND
10.0 2.70 ug/L 07/12/22 00:18 14-Methyl-2-pentanone (MIBK)ND
10.0 3.70 ug/L 07/12/22 00:18 1AcetoneND
1.00 0.270 ug/L 07/12/22 00:18 1BenzeneND
1.00 0.240 ug/L 07/12/22 00:18 1BromobenzeneND
1.00 0.590 ug/L 07/12/22 00:18 1BromoformND*+
5.00 3.70 ug/L 07/12/22 00:18 1BromomethaneND
2.00 0.430 ug/L 07/12/22 00:18 1Carbon disulfide ND
1.00 0.300 ug/L 07/12/22 00:18 1Carbon tetrachloride ND
1.00 0.150 ug/L 07/12/22 00:18 1ChlorobenzeneND
1.00 0.340 ug/L 07/12/22 00:18 1ChlorobromomethaneND
1.00 0.390 ug/L 07/12/22 00:18 1ChlorodibromomethaneND
5.00 4.60 ug/L 07/12/22 00:18 1ChloroethaneND
1.00 0.270 ug/L 07/12/22 00:18 1Chloroform0.867 J
1.00 0.540 ug/L 07/12/22 00:18 1ChloromethaneND
1.00 0.250 ug/L 07/12/22 00:18 1cis-1,2-Dichloroethene ND
1.00 0.260 ug/L 07/12/22 00:18 1cis-1,3-Dichloropropene ND
1.00 0.340 ug/L 07/12/22 00:18 1DibromomethaneND
1.00 0.250 ug/L 07/12/22 00:18 1DichlorobromomethaneND
1.00 0.360 ug/L 07/12/22 00:18 1DichlorodifluoromethaneND*-
10.0 5.00 ug/L 07/12/22 00:18 1Ethyl acetate ND
1.00 0.200 ug/L 07/12/22 00:18 1EthylbenzeneND
1.00 0.330 ug/L 07/12/22 00:18 1Ethylene Dibromide ND
5.00 0.220 ug/L 07/12/22 00:18 1HexachlorobutadieneND
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Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-2Client Sample ID: GW-3
Matrix: WaterDate Collected: 06/30/22 15:15
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 5.00 0.650 ug/L 07/12/22 00:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 3.90 ug/L 07/12/22 00:18 1IodomethaneND
10.0 0.700 ug/L 07/12/22 00:18 1Isopropyl ether ND
1.00 0.260 ug/L 07/12/22 00:18 1IsopropylbenzeneND
1.00 0.490 ug/L 07/12/22 00:18 1m,p-Xylene ND
5.00 0.810 ug/L 07/12/22 00:18 1Methyl tert-butyl ether ND
5.00 3.20 ug/L 07/12/22 00:18 1Methylene Chloride ND
5.00 2.40 ug/L 07/12/22 00:18 1NaphthaleneND
1.00 0.520 ug/L 07/12/22 00:18 1n-Butylbenzene ND
1.00 0.430 ug/L 07/12/22 00:18 1n-Heptane ND
1.00 0.410 ug/L 07/12/22 00:18 1N-Propylbenzene ND
1.00 0.260 ug/L 07/12/22 00:18 1o-Xylene ND
1.00 0.530 ug/L 07/12/22 00:18 1sec-Butylbenzene ND
1.00 0.270 ug/L 07/12/22 00:18 1StyreneND
1.00 0.430 ug/L 07/12/22 00:18 1tert-Butylbenzene ND
0.500 0.350 ug/L 07/12/22 00:18 1TetrachloroetheneND
1.00 0.250 ug/L 07/12/22 00:18 1TolueneND
1.00 0.340 ug/L 07/12/22 00:18 1trans-1,2-Dichloroethene ND
1.00 0.230 ug/L 07/12/22 00:18 1trans-1,3-Dichloropropene ND
2.00 1.25 ug/L 07/12/22 00:18 1trans-1,4-Dichloro-2-butene ND
1.00 0.200 ug/L 07/12/22 00:18 1TrichloroetheneND
1.00 0.330 ug/L 07/12/22 00:18 1TrichlorofluoromethaneND
2.00 0.690 ug/L 07/12/22 00:18 1Vinyl acetate ND *+
1.00 0.400 ug/L 07/12/22 00:18 1Vinyl chloride ND
1.00 0.230 ug/L 07/12/22 00:18 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)90 60-124 07/12/22 00:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)106 07/12/22 00:18 170-130
Dibromofluoromethane (Surr)104 07/12/22 00:18 170-130
Toluene-d8 (Surr)104 07/12/22 00:18 170-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 9.18 4.22 ug/L 07/07/22 11:34 07/08/22 00:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.18 3.03 ug/L 07/07/22 11:34 07/08/22 00:11 12,4,5-Trichlorophenol ND
9.18 2.02 ug/L 07/07/22 11:34 07/08/22 00:11 12,4,6-Trichlorophenol ND
9.18 3.40 ug/L 07/07/22 11:34 07/08/22 00:11 12,4-Dichlorophenol ND
9.18 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 12,4-Dimethylphenol ND
45.9 14.7 ug/L 07/07/22 11:34 07/08/22 00:11 12,4-Dinitrophenol ND
9.18 2.11 ug/L 07/07/22 11:34 07/08/22 00:11 12,4-Dinitrotoluene ND
9.18 2.57 ug/L 07/07/22 11:34 07/08/22 00:11 12,6-Dinitrotoluene ND
9.18 4.41 ug/L 07/07/22 11:34 07/08/22 00:11 12-Chloronaphthalene ND
9.18 2.94 ug/L 07/07/22 11:34 07/08/22 00:11 12-Chlorophenol ND
9.18 4.22 ug/L 07/07/22 11:34 07/08/22 00:11 12-Methylnaphthalene ND
9.18 1.65 ug/L 07/07/22 11:34 07/08/22 00:11 12-Methylphenol ND
45.9 2.66 ug/L 07/07/22 11:34 07/08/22 00:11 12-Nitroaniline ND
9.18 3.58 ug/L 07/07/22 11:34 07/08/22 00:11 12-Nitrophenol ND
9.18 1.28 ug/L 07/07/22 11:34 07/08/22 00:11 13 & 4 Methylphenol ND
55.1 9.18 ug/L 07/07/22 11:34 07/08/22 00:11 13,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-2Client Sample ID: GW-3
Matrix: WaterDate Collected: 06/30/22 15:15
Date Received: 07/01/22 11:00
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 45.9 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
45.9 4.86 ug/L 07/07/22 11:34 07/08/22 00:11 14,6-Dinitro-2-methylphenol ND
9.18 4.31 ug/L 07/07/22 11:34 07/08/22 00:11 14-Bromophenyl phenyl ether ND
9.18 2.29 ug/L 07/07/22 11:34 07/08/22 00:11 14-Chloro-3-methylphenol ND
18.4 0.918 ug/L 07/07/22 11:34 07/08/22 00:11 14-Chloroaniline ND
9.18 4.86 ug/L 07/07/22 11:34 07/08/22 00:11 14-Chlorophenyl phenyl ether ND
45.9 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 14-Nitroaniline ND
45.9 7.43 ug/L 07/07/22 11:34 07/08/22 00:11 14-Nitrophenol ND
9.18 4.04 ug/L 07/07/22 11:34 07/08/22 00:11 1AcenaphtheneND
9.18 3.30 ug/L 07/07/22 11:34 07/08/22 00:11 1AcenaphthyleneND
9.18 2.02 ug/L 07/07/22 11:34 07/08/22 00:11 1AcetophenoneND
9.18 3.30 ug/L 07/07/22 11:34 07/08/22 00:11 1AnthraceneND
9.18 2.02 ug/L 07/07/22 11:34 07/08/22 00:11 1AtrazineND
9.18 4.41 ug/L 07/07/22 11:34 07/08/22 00:11 1BenzaldehydeND
9.18 3.85 ug/L 07/07/22 11:34 07/08/22 00:11 1Benzo[a]anthracene ND
9.18 2.57 ug/L 07/07/22 11:34 07/08/22 00:11 1Benzo[a]pyrene ND
9.18 2.85 ug/L 07/07/22 11:34 07/08/22 00:11 1Benzo[b]fluoranthene ND
9.18 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 1Benzo[g,h,i]perylene ND
9.18 2.66 ug/L 07/07/22 11:34 07/08/22 00:11 1Benzo[k]fluoranthene ND
9.18 2.85 ug/L 07/07/22 11:34 07/08/22 00:11 1bis (2-chloroisopropyl) ether ND
9.18 1.65 ug/L 07/07/22 11:34 07/08/22 00:11 1Bis(2-chloroethoxy)methane ND
9.18 3.30 ug/L 07/07/22 11:34 07/08/22 00:11 1Bis(2-chloroethyl)ether ND
9.18 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 1Bis(2-ethylhexyl) phthalate ND
9.18 2.57 ug/L 07/07/22 11:34 07/08/22 00:11 1Butyl benzyl phthalate ND
9.18 2.57 ug/L 07/07/22 11:34 07/08/22 00:11 1CaprolactamND
9.18 1.65 ug/L 07/07/22 11:34 07/08/22 00:11 1CarbazoleND
9.18 3.49 ug/L 07/07/22 11:34 07/08/22 00:11 1ChryseneND
9.18 2.75 ug/L 07/07/22 11:34 07/08/22 00:11 1Dibenz(a,h)anthracene ND
9.18 1.74 ug/L 07/07/22 11:34 07/08/22 00:11 1DibenzofuranND
9.18 2.02 ug/L 07/07/22 11:34 07/08/22 00:11 1Diethyl phthalate 11.8
9.18 1.93 ug/L 07/07/22 11:34 07/08/22 00:11 1Dimethyl phthalate ND
9.18 2.11 ug/L 07/07/22 11:34 07/08/22 00:11 1Di-n-butyl phthalate ND
9.18 2.57 ug/L 07/07/22 11:34 07/08/22 00:11 1Di-n-octyl phthalate ND
9.18 1.47 ug/L 07/07/22 11:34 07/08/22 00:11 1FluorantheneND
9.18 3.12 ug/L 07/07/22 11:34 07/08/22 00:11 1FluoreneND
9.18 1.47 ug/L 07/07/22 11:34 07/08/22 00:11 1HexachlorobenzeneND
9.18 3.67 ug/L 07/07/22 11:34 07/08/22 00:11 1HexachlorobutadieneND
9.18 3.21 ug/L 07/07/22 11:34 07/08/22 00:11 1HexachlorocyclopentadieneND
9.18 3.30 ug/L 07/07/22 11:34 07/08/22 00:11 1HexachloroethaneND
9.18 3.95 ug/L 07/07/22 11:34 07/08/22 00:11 1Indeno[1,2,3-cd]pyrene ND
9.18 1.84 ug/L 07/07/22 11:34 07/08/22 00:11 1IsophoroneND
9.18 3.21 ug/L 07/07/22 11:34 07/08/22 00:11 1NaphthaleneND
9.18 3.21 ug/L 07/07/22 11:34 07/08/22 00:11 1NitrobenzeneND
9.18 2.20 ug/L 07/07/22 11:34 07/08/22 00:11 1N-Nitrosodi-n-propylamine ND
9.18 2.66 ug/L 07/07/22 11:34 07/08/22 00:11 1N-Nitrosodiphenylamine ND
45.9 9.09 ug/L 07/07/22 11:34 07/08/22 00:11 1PentachlorophenolND
9.18 3.95 ug/L 07/07/22 11:34 07/08/22 00:11 1PhenanthreneND
9.18 1.38 ug/L 07/07/22 11:34 07/08/22 00:11 1PhenolND
9.18 3.40 ug/L 07/07/22 11:34 07/08/22 00:11 1PyreneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-2Client Sample ID: GW-3
Matrix: WaterDate Collected: 06/30/22 15:15
Date Received: 07/01/22 11:00
2,4,6-Tribromophenol (Surr)98 30-130 07/07/22 11:34 07/08/22 00:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)55 07/07/22 11:34 07/08/22 00:11 125-130
2-Fluorophenol (Surr)34 07/07/22 11:34 07/08/22 00:11 110-130
Nitrobenzene-d5 (Surr)55 07/07/22 11:34 07/08/22 00:11 130-130
Phenol-d5 (Surr)23 07/07/22 11:34 07/08/22 00:11 110-130
Terphenyl-d14 (Surr)77 07/07/22 11:34 07/08/22 00:11 135-131
Method: 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 22:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00500 0.000890 mg/L 07/05/22 17:15 07/06/22 22:20 1Barium0.223
0.000500 0.0000780 mg/L 07/05/22 17:15 07/06/22 22:20 1CadmiumND
0.00500 0.00260 mg/L 07/05/22 17:15 07/06/22 22:20 1ChromiumND
0.00250 0.000340 mg/L 07/05/22 17:15 07/06/22 22:20 1LeadND
0.00250 0.00120 mg/L 07/05/22 17:15 07/06/22 22:20 1SeleniumND
0.00100 0.000390 mg/L 07/05/22 17:15 07/06/22 22:20 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 15:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-3Client Sample ID: GW-2
Matrix: WaterDate Collected: 06/30/22 16:20
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 10.0 3.60 ug/L 07/08/22 21:00 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 2.10 ug/L 07/08/22 21:00 101,1,1-Trichloroethane ND
10.0 4.00 ug/L 07/08/22 21:00 101,1,2,2-Tetrachloroethane ND
10.0 2.30 ug/L 07/08/22 21:00 101,1,2-Trichloro-1,2,2-trifluoroethane ND
10.0 3.20 ug/L 07/08/22 21:00 101,1,2-Trichloroethane ND
10.0 3.30 ug/L 07/08/22 21:00 101,1-Dichloroethane ND
10.0 3.30 ug/L 07/08/22 21:00 101,1-Dichloroethene ND
10.0 2.80 ug/L 07/08/22 21:00 101,1-Dichloropropene ND
50.0 8.10 ug/L 07/08/22 21:00 101,2,3-Trichlorobenzene ND
10.0 4.80 ug/L 07/08/22 21:00 101,2,3-Trichloropropane ND
50.0 5.30 ug/L 07/08/22 21:00 101,2,4-Trichlorobenzene ND
10.0 4.30 ug/L 07/08/22 21:00 101,2,4-Trimethylbenzene 16.2
50.0 18.0 ug/L 07/08/22 21:00 101,2-Dibromo-3-Chloropropane ND
10.0 3.10 ug/L 07/08/22 21:00 101,2-Dichlorobenzene ND
10.0 2.50 ug/L 07/08/22 21:00 101,2-Dichloroethane ND
10.0 2.20 ug/L 07/08/22 21:00 101,2-Dichloropropane ND
10.0 2.80 ug/L 07/08/22 21:00 101,3,5-Trimethylbenzene 5.21 J
10.0 3.10 ug/L 07/08/22 21:00 101,3-Dichlorobenzene ND
10.0 3.60 ug/L 07/08/22 21:00 101,3-Dichloropropane ND
10.0 3.10 ug/L 07/08/22 21:00 101,4-Dichlorobenzene ND
10.0 3.50 ug/L 07/08/22 21:00 102,2-Dichloropropane ND
100 64.0 ug/L 07/08/22 21:00 102-Butanone (MEK)ND
10.0 2.50 ug/L 07/08/22 21:00 102-Chlorotoluene ND
100 32.0 ug/L 07/08/22 21:00 102-Hexanone ND
10.0 4.10 ug/L 07/08/22 21:00 104-Chlorotoluene ND
10.0 4.40 ug/L 07/08/22 21:00 104-Isopropyltoluene ND
100 27.0 ug/L 07/08/22 21:00 104-Methyl-2-pentanone (MIBK)ND
100 37.0 ug/L 07/08/22 21:00 10AcetoneND
10.0 2.70 ug/L 07/08/22 21:00 10Benzene284
10.0 2.40 ug/L 07/08/22 21:00 10BromobenzeneND
10.0 5.90 ug/L 07/08/22 21:00 10BromoformND
50.0 37.0 ug/L 07/08/22 21:00 10BromomethaneND*+
20.0 4.30 ug/L 07/08/22 21:00 10Carbon disulfide ND
10.0 3.00 ug/L 07/08/22 21:00 10Carbon tetrachloride ND
10.0 1.50 ug/L 07/08/22 21:00 10ChlorobenzeneND
10.0 3.40 ug/L 07/08/22 21:00 10ChlorobromomethaneND
10.0 3.90 ug/L 07/08/22 21:00 10ChlorodibromomethaneND
50.0 46.0 ug/L 07/08/22 21:00 10ChloroethaneND*+
10.0 2.70 ug/L 07/08/22 21:00 10ChloroformND
10.0 5.40 ug/L 07/08/22 21:00 10ChloromethaneND
10.0 2.50 ug/L 07/08/22 21:00 10cis-1,2-Dichloroethene ND
10.0 2.60 ug/L 07/08/22 21:00 10cis-1,3-Dichloropropene ND
10.0 3.40 ug/L 07/08/22 21:00 10DibromomethaneND
10.0 2.50 ug/L 07/08/22 21:00 10DichlorobromomethaneND
10.0 3.60 ug/L 07/08/22 21:00 10DichlorodifluoromethaneND
100 50.0 ug/L 07/08/22 21:00 10Ethyl acetate ND
10.0 2.00 ug/L 07/08/22 21:00 10Ethylbenzene47.1
10.0 3.30 ug/L 07/08/22 21:00 10Ethylene Dibromide ND
50.0 2.20 ug/L 07/08/22 21:00 10HexachlorobutadieneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-3Client Sample ID: GW-2
Matrix: WaterDate Collected: 06/30/22 16:20
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane ND 50.0 6.50 ug/L 07/08/22 21:00 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
100 39.0 ug/L 07/08/22 21:00 10IodomethaneND*+
100 7.00 ug/L 07/08/22 21:00 10Isopropyl ether 246
10.0 2.60 ug/L 07/08/22 21:00 10IsopropylbenzeneND
10.0 4.90 ug/L 07/08/22 21:00 10m,p-Xylene 65.0
50.0 8.10 ug/L 07/08/22 21:00 10Methyl tert-butyl ether ND
50.0 32.0 ug/L 07/08/22 21:00 10Methylene Chloride ND
50.0 24.0 ug/L 07/08/22 21:00 10NaphthaleneND
10.0 5.20 ug/L 07/08/22 21:00 10n-Butylbenzene ND
10.0 4.30 ug/L 07/08/22 21:00 10n-Heptane ND *+
10.0 4.10 ug/L 07/08/22 21:00 10N-Propylbenzene 4.27 J
10.0 2.60 ug/L 07/08/22 21:00 10o-Xylene 17.5
10.0 5.30 ug/L 07/08/22 21:00 10sec-Butylbenzene ND
10.0 2.70 ug/L 07/08/22 21:00 10StyreneND
10.0 4.30 ug/L 07/08/22 21:00 10tert-Butylbenzene ND
5.00 3.50 ug/L 07/08/22 21:00 10TetrachloroetheneND
10.0 2.50 ug/L 07/08/22 21:00 10Toluene36.2
10.0 3.40 ug/L 07/08/22 21:00 10trans-1,2-Dichloroethene ND
10.0 2.30 ug/L 07/08/22 21:00 10trans-1,3-Dichloropropene ND
20.0 12.5 ug/L 07/08/22 21:00 10trans-1,4-Dichloro-2-butene ND
10.0 2.00 ug/L 07/08/22 21:00 10TrichloroetheneND
10.0 3.30 ug/L 07/08/22 21:00 10TrichlorofluoromethaneND
20.0 6.90 ug/L 07/08/22 21:00 10Vinyl acetate ND *+
10.0 4.00 ug/L 07/08/22 21:00 10Vinyl chloride ND
10.0 2.30 ug/L 07/08/22 21:00 10Xylenes, Total 82.5
1,2-Dichloroethane-d4 (Surr)84 60-124 07/08/22 21:00 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)101 07/08/22 21:00 1070-130
Dibromofluoromethane (Surr)94 07/08/22 21:00 1070-130
Toluene-d8 (Surr)105 07/08/22 21:00 1070-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 9.71 4.47 ug/L 07/07/22 11:34 07/08/22 00:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.71 3.20 ug/L 07/07/22 11:34 07/08/22 00:36 12,4,5-Trichlorophenol ND
9.71 2.14 ug/L 07/07/22 11:34 07/08/22 00:36 12,4,6-Trichlorophenol ND
9.71 3.59 ug/L 07/07/22 11:34 07/08/22 00:36 12,4-Dichlorophenol ND
9.71 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 12,4-Dimethylphenol ND
48.5 15.5 ug/L 07/07/22 11:34 07/08/22 00:36 12,4-Dinitrophenol ND
9.71 2.23 ug/L 07/07/22 11:34 07/08/22 00:36 12,4-Dinitrotoluene ND
9.71 2.72 ug/L 07/07/22 11:34 07/08/22 00:36 12,6-Dinitrotoluene ND
9.71 4.66 ug/L 07/07/22 11:34 07/08/22 00:36 12-Chloronaphthalene ND
9.71 3.11 ug/L 07/07/22 11:34 07/08/22 00:36 12-Chlorophenol ND
9.71 4.47 ug/L 07/07/22 11:34 07/08/22 00:36 12-Methylnaphthalene 8.49 J
9.71 1.75 ug/L 07/07/22 11:34 07/08/22 00:36 12-Methylphenol ND
48.5 2.82 ug/L 07/07/22 11:34 07/08/22 00:36 12-Nitroaniline ND
9.71 3.79 ug/L 07/07/22 11:34 07/08/22 00:36 12-Nitrophenol ND
9.71 1.36 ug/L 07/07/22 11:34 07/08/22 00:36 13 & 4 Methylphenol ND
58.3 9.71 ug/L 07/07/22 11:34 07/08/22 00:36 13,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-3Client Sample ID: GW-2
Matrix: WaterDate Collected: 06/30/22 16:20
Date Received: 07/01/22 11:00
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 48.5 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
48.5 5.15 ug/L 07/07/22 11:34 07/08/22 00:36 14,6-Dinitro-2-methylphenol ND
9.71 4.56 ug/L 07/07/22 11:34 07/08/22 00:36 14-Bromophenyl phenyl ether ND
9.71 2.43 ug/L 07/07/22 11:34 07/08/22 00:36 14-Chloro-3-methylphenol ND
19.4 0.971 ug/L 07/07/22 11:34 07/08/22 00:36 14-Chloroaniline ND
9.71 5.15 ug/L 07/07/22 11:34 07/08/22 00:36 14-Chlorophenyl phenyl ether ND
48.5 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 14-Nitroaniline ND
48.5 7.86 ug/L 07/07/22 11:34 07/08/22 00:36 14-Nitrophenol ND
9.71 4.27 ug/L 07/07/22 11:34 07/08/22 00:36 1AcenaphtheneND
9.71 3.50 ug/L 07/07/22 11:34 07/08/22 00:36 1AcenaphthyleneND
9.71 2.14 ug/L 07/07/22 11:34 07/08/22 00:36 1AcetophenoneND
9.71 3.50 ug/L 07/07/22 11:34 07/08/22 00:36 1AnthraceneND
9.71 2.14 ug/L 07/07/22 11:34 07/08/22 00:36 1AtrazineND
9.71 4.66 ug/L 07/07/22 11:34 07/08/22 00:36 1BenzaldehydeND
9.71 4.08 ug/L 07/07/22 11:34 07/08/22 00:36 1Benzo[a]anthracene ND
9.71 2.72 ug/L 07/07/22 11:34 07/08/22 00:36 1Benzo[a]pyrene ND
9.71 3.01 ug/L 07/07/22 11:34 07/08/22 00:36 1Benzo[b]fluoranthene ND
9.71 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 1Benzo[g,h,i]perylene ND
9.71 2.82 ug/L 07/07/22 11:34 07/08/22 00:36 1Benzo[k]fluoranthene ND
9.71 3.01 ug/L 07/07/22 11:34 07/08/22 00:36 1bis (2-chloroisopropyl) ether ND
9.71 1.75 ug/L 07/07/22 11:34 07/08/22 00:36 1Bis(2-chloroethoxy)methane ND
9.71 3.50 ug/L 07/07/22 11:34 07/08/22 00:36 1Bis(2-chloroethyl)ether ND
9.71 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 1Bis(2-ethylhexyl) phthalate ND
9.71 2.72 ug/L 07/07/22 11:34 07/08/22 00:36 1Butyl benzyl phthalate ND
9.71 2.72 ug/L 07/07/22 11:34 07/08/22 00:36 1CaprolactamND
9.71 1.75 ug/L 07/07/22 11:34 07/08/22 00:36 1CarbazoleND
9.71 3.69 ug/L 07/07/22 11:34 07/08/22 00:36 1ChryseneND
9.71 2.91 ug/L 07/07/22 11:34 07/08/22 00:36 1Dibenz(a,h)anthracene ND
9.71 1.84 ug/L 07/07/22 11:34 07/08/22 00:36 1DibenzofuranND
9.71 2.14 ug/L 07/07/22 11:34 07/08/22 00:36 1Diethyl phthalate 9.33 J
9.71 2.04 ug/L 07/07/22 11:34 07/08/22 00:36 1Dimethyl phthalate ND
9.71 2.23 ug/L 07/07/22 11:34 07/08/22 00:36 1Di-n-butyl phthalate ND
9.71 2.72 ug/L 07/07/22 11:34 07/08/22 00:36 1Di-n-octyl phthalate ND
9.71 1.55 ug/L 07/07/22 11:34 07/08/22 00:36 1FluorantheneND
9.71 3.30 ug/L 07/07/22 11:34 07/08/22 00:36 1FluoreneND
9.71 1.55 ug/L 07/07/22 11:34 07/08/22 00:36 1HexachlorobenzeneND
9.71 3.88 ug/L 07/07/22 11:34 07/08/22 00:36 1HexachlorobutadieneND
9.71 3.40 ug/L 07/07/22 11:34 07/08/22 00:36 1HexachlorocyclopentadieneND
9.71 3.50 ug/L 07/07/22 11:34 07/08/22 00:36 1HexachloroethaneND
9.71 4.17 ug/L 07/07/22 11:34 07/08/22 00:36 1Indeno[1,2,3-cd]pyrene ND
9.71 1.94 ug/L 07/07/22 11:34 07/08/22 00:36 1IsophoroneND
9.71 3.40 ug/L 07/07/22 11:34 07/08/22 00:36 1Naphthalene24.4
9.71 3.40 ug/L 07/07/22 11:34 07/08/22 00:36 1NitrobenzeneND
9.71 2.33 ug/L 07/07/22 11:34 07/08/22 00:36 1N-Nitrosodi-n-propylamine ND
9.71 2.82 ug/L 07/07/22 11:34 07/08/22 00:36 1N-Nitrosodiphenylamine ND
48.5 9.61 ug/L 07/07/22 11:34 07/08/22 00:36 1PentachlorophenolND
9.71 4.17 ug/L 07/07/22 11:34 07/08/22 00:36 1PhenanthreneND
9.71 1.46 ug/L 07/07/22 11:34 07/08/22 00:36 1PhenolND
9.71 3.59 ug/L 07/07/22 11:34 07/08/22 00:36 1PyreneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-3Client Sample ID: GW-2
Matrix: WaterDate Collected: 06/30/22 16:20
Date Received: 07/01/22 11:00
2,4,6-Tribromophenol (Surr)108 30-130 07/07/22 11:34 07/08/22 00:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)60 07/07/22 11:34 07/08/22 00:36 125-130
2-Fluorophenol (Surr)36 07/07/22 11:34 07/08/22 00:36 110-130
Nitrobenzene-d5 (Surr)56 07/07/22 11:34 07/08/22 00:36 130-130
Phenol-d5 (Surr)26 07/07/22 11:34 07/08/22 00:36 110-130
Terphenyl-d14 (Surr)83 07/07/22 11:34 07/08/22 00:36 135-131
Method: 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 22:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00500 0.000890 mg/L 07/05/22 17:15 07/06/22 22:23 1Barium0.288
0.000500 0.0000780 mg/L 07/05/22 17:15 07/06/22 22:23 1CadmiumND
0.00500 0.00260 mg/L 07/05/22 17:15 07/06/22 22:23 1ChromiumND
0.00250 0.000340 mg/L 07/05/22 17:15 07/06/22 22:23 1Lead0.000580 J
0.00250 0.00120 mg/L 07/05/22 17:15 07/06/22 22:23 1SeleniumND
0.00100 0.000390 mg/L 07/05/22 17:15 07/06/22 22:23 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-4Client Sample ID: GW-1
Matrix: WaterDate Collected: 06/30/22 17:25
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 5.00 1.80 ug/L 07/08/22 21:19 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.00 1.05 ug/L 07/08/22 21:19 51,1,1-Trichloroethane ND
5.00 2.00 ug/L 07/08/22 21:19 51,1,2,2-Tetrachloroethane ND
5.00 1.15 ug/L 07/08/22 21:19 51,1,2-Trichloro-1,2,2-trifluoroethane ND
5.00 1.60 ug/L 07/08/22 21:19 51,1,2-Trichloroethane ND
5.00 1.65 ug/L 07/08/22 21:19 51,1-Dichloroethane ND
5.00 1.65 ug/L 07/08/22 21:19 51,1-Dichloroethene ND
5.00 1.40 ug/L 07/08/22 21:19 51,1-Dichloropropene ND
25.0 4.05 ug/L 07/08/22 21:19 51,2,3-Trichlorobenzene ND
5.00 2.40 ug/L 07/08/22 21:19 51,2,3-Trichloropropane ND
25.0 2.65 ug/L 07/08/22 21:19 51,2,4-Trichlorobenzene ND
5.00 2.15 ug/L 07/08/22 21:19 51,2,4-Trimethylbenzene 58.1
25.0 9.00 ug/L 07/08/22 21:19 51,2-Dibromo-3-Chloropropane ND
5.00 1.55 ug/L 07/08/22 21:19 51,2-Dichlorobenzene ND
5.00 1.25 ug/L 07/08/22 21:19 51,2-Dichloroethane 6.49
5.00 1.10 ug/L 07/08/22 21:19 51,2-Dichloropropane ND
5.00 1.40 ug/L 07/08/22 21:19 51,3,5-Trimethylbenzene 9.78
5.00 1.55 ug/L 07/08/22 21:19 51,3-Dichlorobenzene ND
5.00 1.80 ug/L 07/08/22 21:19 51,3-Dichloropropane ND
5.00 1.55 ug/L 07/08/22 21:19 51,4-Dichlorobenzene ND
5.00 1.75 ug/L 07/08/22 21:19 52,2-Dichloropropane ND
50.0 32.0 ug/L 07/08/22 21:19 52-Butanone (MEK)ND
5.00 1.25 ug/L 07/08/22 21:19 52-Chlorotoluene ND
50.0 16.0 ug/L 07/08/22 21:19 52-Hexanone ND
5.00 2.05 ug/L 07/08/22 21:19 54-Chlorotoluene ND
5.00 2.20 ug/L 07/08/22 21:19 54-Isopropyltoluene ND
50.0 13.5 ug/L 07/08/22 21:19 54-Methyl-2-pentanone (MIBK)17.6 J
50.0 18.5 ug/L 07/08/22 21:19 5AcetoneND
5.00 1.35 ug/L 07/08/22 21:19 5Benzene229
5.00 1.20 ug/L 07/08/22 21:19 5BromobenzeneND
5.00 2.95 ug/L 07/08/22 21:19 5BromoformND
25.0 18.5 ug/L 07/08/22 21:19 5BromomethaneND*+
10.0 2.15 ug/L 07/08/22 21:19 5Carbon disulfide ND
5.00 1.50 ug/L 07/08/22 21:19 5Carbon tetrachloride ND
5.00 0.750 ug/L 07/08/22 21:19 5ChlorobenzeneND
5.00 1.70 ug/L 07/08/22 21:19 5ChlorobromomethaneND
5.00 1.95 ug/L 07/08/22 21:19 5ChlorodibromomethaneND
25.0 23.0 ug/L 07/08/22 21:19 5ChloroethaneND*+
5.00 1.35 ug/L 07/08/22 21:19 5ChloroformND
5.00 2.70 ug/L 07/08/22 21:19 5ChloromethaneND
5.00 1.25 ug/L 07/08/22 21:19 5cis-1,2-Dichloroethene ND
5.00 1.30 ug/L 07/08/22 21:19 5cis-1,3-Dichloropropene ND
5.00 1.70 ug/L 07/08/22 21:19 5DibromomethaneND
5.00 1.25 ug/L 07/08/22 21:19 5DichlorobromomethaneND
5.00 1.80 ug/L 07/08/22 21:19 5DichlorodifluoromethaneND
50.0 25.0 ug/L 07/08/22 21:19 5Ethyl acetate ND
5.00 1.00 ug/L 07/08/22 21:19 5Ethylbenzene232
5.00 1.65 ug/L 07/08/22 21:19 5Ethylene Dibromide ND
25.0 1.10 ug/L 07/08/22 21:19 5HexachlorobutadieneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-4Client Sample ID: GW-1
Matrix: WaterDate Collected: 06/30/22 17:25
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane 51.2 25.0 3.25 ug/L 07/08/22 21:19 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
50.0 19.5 ug/L 07/08/22 21:19 5IodomethaneND*+
50.0 3.50 ug/L 07/08/22 21:19 5Isopropyl ether 18.9 J
5.00 1.30 ug/L 07/08/22 21:19 5Isopropylbenzene15.9
5.00 2.45 ug/L 07/08/22 21:19 5m,p-Xylene 42.7
25.0 4.05 ug/L 07/08/22 21:19 5Methyl tert-butyl ether ND
25.0 16.0 ug/L 07/08/22 21:19 5Methylene Chloride ND
25.0 12.0 ug/L 07/08/22 21:19 5Naphthalene358
5.00 2.60 ug/L 07/08/22 21:19 5n-Butylbenzene 8.39
5.00 2.15 ug/L 07/08/22 21:19 5n-Heptane 3.11 J *+
5.00 2.05 ug/L 07/08/22 21:19 5N-Propylbenzene 30.5
5.00 1.30 ug/L 07/08/22 21:19 5o-Xylene 51.4
5.00 2.65 ug/L 07/08/22 21:19 5sec-Butylbenzene ND
5.00 1.35 ug/L 07/08/22 21:19 5Styrene12.6
5.00 2.15 ug/L 07/08/22 21:19 5tert-Butylbenzene ND
2.50 1.75 ug/L 07/08/22 21:19 5TetrachloroetheneND
5.00 1.25 ug/L 07/08/22 21:19 5Toluene31.4
5.00 1.70 ug/L 07/08/22 21:19 5trans-1,2-Dichloroethene ND
5.00 1.15 ug/L 07/08/22 21:19 5trans-1,3-Dichloropropene ND
10.0 6.25 ug/L 07/08/22 21:19 5trans-1,4-Dichloro-2-butene ND
5.00 1.00 ug/L 07/08/22 21:19 5TrichloroetheneND
5.00 1.65 ug/L 07/08/22 21:19 5TrichlorofluoromethaneND
10.0 3.45 ug/L 07/08/22 21:19 5Vinyl acetate ND *+
5.00 2.00 ug/L 07/08/22 21:19 5Vinyl chloride ND
5.00 1.15 ug/L 07/08/22 21:19 5Xylenes, Total 94.1
1,2-Dichloroethane-d4 (Surr)84 60-124 07/08/22 21:19 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 07/08/22 21:19 570-130
Dibromofluoromethane (Surr)95 07/08/22 21:19 570-130
Toluene-d8 (Surr)104 07/08/22 21:19 570-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 9.30 4.28 ug/L 07/07/22 11:34 07/08/22 01:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.30 3.07 ug/L 07/07/22 11:34 07/08/22 01:01 12,4,5-Trichlorophenol ND
9.30 2.05 ug/L 07/07/22 11:34 07/08/22 01:01 12,4,6-Trichlorophenol ND
9.30 3.44 ug/L 07/07/22 11:34 07/08/22 01:01 12,4-Dichlorophenol ND
9.30 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 12,4-Dimethylphenol ND
46.5 14.9 ug/L 07/07/22 11:34 07/08/22 01:01 12,4-Dinitrophenol ND
9.30 2.14 ug/L 07/07/22 11:34 07/08/22 01:01 12,4-Dinitrotoluene ND
9.30 2.60 ug/L 07/07/22 11:34 07/08/22 01:01 12,6-Dinitrotoluene ND
9.30 4.46 ug/L 07/07/22 11:34 07/08/22 01:01 12-Chloronaphthalene ND
9.30 2.98 ug/L 07/07/22 11:34 07/08/22 01:01 12-Chlorophenol ND
9.30 4.28 ug/L 07/07/22 11:34 07/08/22 01:01 12-Methylnaphthalene 44.7
9.30 1.67 ug/L 07/07/22 11:34 07/08/22 01:01 12-Methylphenol ND
46.5 2.70 ug/L 07/07/22 11:34 07/08/22 01:01 12-Nitroaniline ND
9.30 3.63 ug/L 07/07/22 11:34 07/08/22 01:01 12-Nitrophenol ND
9.30 1.30 ug/L 07/07/22 11:34 07/08/22 01:01 13 & 4 Methylphenol ND
55.8 9.30 ug/L 07/07/22 11:34 07/08/22 01:01 13,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-4Client Sample ID: GW-1
Matrix: WaterDate Collected: 06/30/22 17:25
Date Received: 07/01/22 11:00
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 46.5 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
46.5 4.93 ug/L 07/07/22 11:34 07/08/22 01:01 14,6-Dinitro-2-methylphenol ND
9.30 4.37 ug/L 07/07/22 11:34 07/08/22 01:01 14-Bromophenyl phenyl ether ND
9.30 2.33 ug/L 07/07/22 11:34 07/08/22 01:01 14-Chloro-3-methylphenol ND
18.6 0.930 ug/L 07/07/22 11:34 07/08/22 01:01 14-Chloroaniline ND
9.30 4.93 ug/L 07/07/22 11:34 07/08/22 01:01 14-Chlorophenyl phenyl ether ND
46.5 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 14-Nitroaniline ND
46.5 7.53 ug/L 07/07/22 11:34 07/08/22 01:01 14-Nitrophenol ND
9.30 4.09 ug/L 07/07/22 11:34 07/08/22 01:01 1AcenaphtheneND
9.30 3.35 ug/L 07/07/22 11:34 07/08/22 01:01 1AcenaphthyleneND
9.30 2.05 ug/L 07/07/22 11:34 07/08/22 01:01 1AcetophenoneND
9.30 3.35 ug/L 07/07/22 11:34 07/08/22 01:01 1AnthraceneND
9.30 2.05 ug/L 07/07/22 11:34 07/08/22 01:01 1AtrazineND
9.30 4.46 ug/L 07/07/22 11:34 07/08/22 01:01 1BenzaldehydeND
9.30 3.91 ug/L 07/07/22 11:34 07/08/22 01:01 1Benzo[a]anthracene ND
9.30 2.60 ug/L 07/07/22 11:34 07/08/22 01:01 1Benzo[a]pyrene ND
9.30 2.88 ug/L 07/07/22 11:34 07/08/22 01:01 1Benzo[b]fluoranthene ND
9.30 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 1Benzo[g,h,i]perylene ND
9.30 2.70 ug/L 07/07/22 11:34 07/08/22 01:01 1Benzo[k]fluoranthene ND
9.30 2.88 ug/L 07/07/22 11:34 07/08/22 01:01 1bis (2-chloroisopropyl) ether ND
9.30 1.67 ug/L 07/07/22 11:34 07/08/22 01:01 1Bis(2-chloroethoxy)methane ND
9.30 3.35 ug/L 07/07/22 11:34 07/08/22 01:01 1Bis(2-chloroethyl)ether ND
9.30 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 1Bis(2-ethylhexyl) phthalate ND
9.30 2.60 ug/L 07/07/22 11:34 07/08/22 01:01 1Butyl benzyl phthalate ND
9.30 2.60 ug/L 07/07/22 11:34 07/08/22 01:01 1CaprolactamND
9.30 1.67 ug/L 07/07/22 11:34 07/08/22 01:01 1CarbazoleND
9.30 3.53 ug/L 07/07/22 11:34 07/08/22 01:01 1ChryseneND
9.30 2.79 ug/L 07/07/22 11:34 07/08/22 01:01 1Dibenz(a,h)anthracene ND
9.30 1.77 ug/L 07/07/22 11:34 07/08/22 01:01 1DibenzofuranND
9.30 2.05 ug/L 07/07/22 11:34 07/08/22 01:01 1Diethyl phthalate 8.03 J
9.30 1.95 ug/L 07/07/22 11:34 07/08/22 01:01 1Dimethyl phthalate ND
9.30 2.14 ug/L 07/07/22 11:34 07/08/22 01:01 1Di-n-butyl phthalate ND
9.30 2.60 ug/L 07/07/22 11:34 07/08/22 01:01 1Di-n-octyl phthalate ND
9.30 1.49 ug/L 07/07/22 11:34 07/08/22 01:01 1FluorantheneND
9.30 3.16 ug/L 07/07/22 11:34 07/08/22 01:01 1FluoreneND
9.30 1.49 ug/L 07/07/22 11:34 07/08/22 01:01 1HexachlorobenzeneND
9.30 3.72 ug/L 07/07/22 11:34 07/08/22 01:01 1HexachlorobutadieneND
9.30 3.26 ug/L 07/07/22 11:34 07/08/22 01:01 1HexachlorocyclopentadieneND
9.30 3.35 ug/L 07/07/22 11:34 07/08/22 01:01 1HexachloroethaneND
9.30 4.00 ug/L 07/07/22 11:34 07/08/22 01:01 1Indeno[1,2,3-cd]pyrene ND
9.30 1.86 ug/L 07/07/22 11:34 07/08/22 01:01 1IsophoroneND
9.30 3.26 ug/L 07/07/22 11:34 07/08/22 01:01 1Naphthalene153
9.30 3.26 ug/L 07/07/22 11:34 07/08/22 01:01 1NitrobenzeneND
9.30 2.23 ug/L 07/07/22 11:34 07/08/22 01:01 1N-Nitrosodi-n-propylamine ND
9.30 2.70 ug/L 07/07/22 11:34 07/08/22 01:01 1N-Nitrosodiphenylamine ND
46.5 9.21 ug/L 07/07/22 11:34 07/08/22 01:01 1PentachlorophenolND
9.30 4.00 ug/L 07/07/22 11:34 07/08/22 01:01 1PhenanthreneND
9.30 1.40 ug/L 07/07/22 11:34 07/08/22 01:01 1PhenolND
9.30 3.44 ug/L 07/07/22 11:34 07/08/22 01:01 1PyreneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-4Client Sample ID: GW-1
Matrix: WaterDate Collected: 06/30/22 17:25
Date Received: 07/01/22 11:00
2,4,6-Tribromophenol (Surr)100 30-130 07/07/22 11:34 07/08/22 01:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)49 07/07/22 11:34 07/08/22 01:01 125-130
2-Fluorophenol (Surr)32 07/07/22 11:34 07/08/22 01:01 110-130
Nitrobenzene-d5 (Surr)55 07/07/22 11:34 07/08/22 01:01 130-130
Phenol-d5 (Surr)23 07/07/22 11:34 07/08/22 01:01 110-130
Terphenyl-d14 (Surr)72 07/07/22 11:34 07/08/22 01:01 135-131
Method: 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 22:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00500 0.000890 mg/L 07/05/22 17:15 07/06/22 22:25 1Barium0.500
0.000500 0.0000780 mg/L 07/05/22 17:15 07/06/22 22:25 1Cadmium0.000105 J
0.00500 0.00260 mg/L 07/05/22 17:15 07/06/22 22:25 1ChromiumND
0.00250 0.000340 mg/L 07/05/22 17:15 07/06/22 22:25 1Lead0.000625 J
0.00250 0.00120 mg/L 07/05/22 17:15 07/06/22 22:25 1SeleniumND
0.00100 0.000390 mg/L 07/05/22 17:15 07/06/22 22:25 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 15:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-5Client Sample ID: Duplicate
Matrix: WaterDate Collected: 06/30/22 00:00
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS
RL MDL
1,1,1,2-Tetrachloroethane ND 5.00 1.80 ug/L 07/08/22 21:38 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.00 1.05 ug/L 07/08/22 21:38 51,1,1-Trichloroethane ND
5.00 2.00 ug/L 07/08/22 21:38 51,1,2,2-Tetrachloroethane ND
5.00 1.15 ug/L 07/08/22 21:38 51,1,2-Trichloro-1,2,2-trifluoroethane ND
5.00 1.60 ug/L 07/08/22 21:38 51,1,2-Trichloroethane ND
5.00 1.65 ug/L 07/08/22 21:38 51,1-Dichloroethane ND
5.00 1.65 ug/L 07/08/22 21:38 51,1-Dichloroethene ND
5.00 1.40 ug/L 07/08/22 21:38 51,1-Dichloropropene ND
25.0 4.05 ug/L 07/08/22 21:38 51,2,3-Trichlorobenzene ND
5.00 2.40 ug/L 07/08/22 21:38 51,2,3-Trichloropropane ND
25.0 2.65 ug/L 07/08/22 21:38 51,2,4-Trichlorobenzene ND
5.00 2.15 ug/L 07/08/22 21:38 51,2,4-Trimethylbenzene 81.1
25.0 9.00 ug/L 07/08/22 21:38 51,2-Dibromo-3-Chloropropane ND
5.00 1.55 ug/L 07/08/22 21:38 51,2-Dichlorobenzene ND
5.00 1.25 ug/L 07/08/22 21:38 51,2-Dichloroethane 5.57
5.00 1.10 ug/L 07/08/22 21:38 51,2-Dichloropropane ND
5.00 1.40 ug/L 07/08/22 21:38 51,3,5-Trimethylbenzene 12.4
5.00 1.55 ug/L 07/08/22 21:38 51,3-Dichlorobenzene ND
5.00 1.80 ug/L 07/08/22 21:38 51,3-Dichloropropane ND
5.00 1.55 ug/L 07/08/22 21:38 51,4-Dichlorobenzene ND
5.00 1.75 ug/L 07/08/22 21:38 52,2-Dichloropropane ND
50.0 32.0 ug/L 07/08/22 21:38 52-Butanone (MEK)ND
5.00 1.25 ug/L 07/08/22 21:38 52-Chlorotoluene ND
50.0 16.0 ug/L 07/08/22 21:38 52-Hexanone ND
5.00 2.05 ug/L 07/08/22 21:38 54-Chlorotoluene ND
5.00 2.20 ug/L 07/08/22 21:38 54-Isopropyltoluene ND
50.0 13.5 ug/L 07/08/22 21:38 54-Methyl-2-pentanone (MIBK)17.0 J
50.0 18.5 ug/L 07/08/22 21:38 5AcetoneND
5.00 1.35 ug/L 07/08/22 21:38 5Benzene229
5.00 1.20 ug/L 07/08/22 21:38 5BromobenzeneND
5.00 2.95 ug/L 07/08/22 21:38 5BromoformND
25.0 18.5 ug/L 07/08/22 21:38 5BromomethaneND*+
10.0 2.15 ug/L 07/08/22 21:38 5Carbon disulfide ND
5.00 1.50 ug/L 07/08/22 21:38 5Carbon tetrachloride ND
5.00 0.750 ug/L 07/08/22 21:38 5ChlorobenzeneND
5.00 1.70 ug/L 07/08/22 21:38 5ChlorobromomethaneND
5.00 1.95 ug/L 07/08/22 21:38 5ChlorodibromomethaneND
25.0 23.0 ug/L 07/08/22 21:38 5ChloroethaneND*+
5.00 1.35 ug/L 07/08/22 21:38 5ChloroformND
5.00 2.70 ug/L 07/08/22 21:38 5ChloromethaneND
5.00 1.25 ug/L 07/08/22 21:38 5cis-1,2-Dichloroethene ND
5.00 1.30 ug/L 07/08/22 21:38 5cis-1,3-Dichloropropene ND
5.00 1.70 ug/L 07/08/22 21:38 5DibromomethaneND
5.00 1.25 ug/L 07/08/22 21:38 5DichlorobromomethaneND
5.00 1.80 ug/L 07/08/22 21:38 5DichlorodifluoromethaneND
50.0 25.0 ug/L 07/08/22 21:38 5Ethyl acetate ND
5.00 1.00 ug/L 07/08/22 21:38 5Ethylbenzene263
5.00 1.65 ug/L 07/08/22 21:38 5Ethylene Dibromide ND
25.0 1.10 ug/L 07/08/22 21:38 5HexachlorobutadieneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-5Client Sample ID: Duplicate
Matrix: WaterDate Collected: 06/30/22 00:00
Date Received: 07/01/22 11:00
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
Hexane 51.6 25.0 3.25 ug/L 07/08/22 21:38 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
50.0 19.5 ug/L 07/08/22 21:38 5IodomethaneND*+
50.0 3.50 ug/L 07/08/22 21:38 5Isopropyl ether 18.7 J
5.00 1.30 ug/L 07/08/22 21:38 5Isopropylbenzene17.8
5.00 2.45 ug/L 07/08/22 21:38 5m,p-Xylene 53.9
25.0 4.05 ug/L 07/08/22 21:38 5Methyl tert-butyl ether ND
25.0 16.0 ug/L 07/08/22 21:38 5Methylene Chloride ND
25.0 12.0 ug/L 07/08/22 21:38 5Naphthalene388
5.00 2.60 ug/L 07/08/22 21:38 5n-Butylbenzene 9.78
5.00 2.15 ug/L 07/08/22 21:38 5n-Heptane 4.43 J *+
5.00 2.05 ug/L 07/08/22 21:38 5N-Propylbenzene 35.6
5.00 1.30 ug/L 07/08/22 21:38 5o-Xylene 64.6
5.00 2.65 ug/L 07/08/22 21:38 5sec-Butylbenzene ND
5.00 1.35 ug/L 07/08/22 21:38 5Styrene13.5
5.00 2.15 ug/L 07/08/22 21:38 5tert-Butylbenzene ND
2.50 1.75 ug/L 07/08/22 21:38 5TetrachloroetheneND
5.00 1.25 ug/L 07/08/22 21:38 5Toluene34.3
5.00 1.70 ug/L 07/08/22 21:38 5trans-1,2-Dichloroethene ND
5.00 1.15 ug/L 07/08/22 21:38 5trans-1,3-Dichloropropene ND
10.0 6.25 ug/L 07/08/22 21:38 5trans-1,4-Dichloro-2-butene ND
5.00 1.00 ug/L 07/08/22 21:38 5TrichloroetheneND
5.00 1.65 ug/L 07/08/22 21:38 5TrichlorofluoromethaneND
10.0 3.45 ug/L 07/08/22 21:38 5Vinyl acetate ND *+
5.00 2.00 ug/L 07/08/22 21:38 5Vinyl chloride ND
5.00 1.15 ug/L 07/08/22 21:38 5Xylenes, Total 119
1,2-Dichloroethane-d4 (Surr)82 60-124 07/08/22 21:38 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 07/08/22 21:38 570-130
Dibromofluoromethane (Surr)95 07/08/22 21:38 570-130
Toluene-d8 (Surr)104 07/08/22 21:38 570-130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
1,1'-Biphenyl ND 9.23 4.24 ug/L 07/07/22 11:34 07/08/22 01:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
9.23 3.04 ug/L 07/07/22 11:34 07/08/22 01:25 12,4,5-Trichlorophenol ND
9.23 2.03 ug/L 07/07/22 11:34 07/08/22 01:25 12,4,6-Trichlorophenol ND
9.23 3.41 ug/L 07/07/22 11:34 07/08/22 01:25 12,4-Dichlorophenol ND
9.23 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 12,4-Dimethylphenol ND
46.1 14.8 ug/L 07/07/22 11:34 07/08/22 01:25 12,4-Dinitrophenol ND
9.23 2.12 ug/L 07/07/22 11:34 07/08/22 01:25 12,4-Dinitrotoluene ND
9.23 2.58 ug/L 07/07/22 11:34 07/08/22 01:25 12,6-Dinitrotoluene ND
9.23 4.43 ug/L 07/07/22 11:34 07/08/22 01:25 12-Chloronaphthalene ND
9.23 2.95 ug/L 07/07/22 11:34 07/08/22 01:25 12-Chlorophenol ND
9.23 4.24 ug/L 07/07/22 11:34 07/08/22 01:25 12-Methylnaphthalene 57.9
9.23 1.66 ug/L 07/07/22 11:34 07/08/22 01:25 12-Methylphenol ND
46.1 2.68 ug/L 07/07/22 11:34 07/08/22 01:25 12-Nitroaniline ND
9.23 3.60 ug/L 07/07/22 11:34 07/08/22 01:25 12-Nitrophenol ND
9.23 1.29 ug/L 07/07/22 11:34 07/08/22 01:25 13 & 4 Methylphenol ND
55.4 9.23 ug/L 07/07/22 11:34 07/08/22 01:25 13,3'-Dichlorobenzidine ND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-5Client Sample ID: Duplicate
Matrix: WaterDate Collected: 06/30/22 00:00
Date Received: 07/01/22 11:00
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3-Nitroaniline ND 46.1 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
46.1 4.89 ug/L 07/07/22 11:34 07/08/22 01:25 14,6-Dinitro-2-methylphenol ND
9.23 4.34 ug/L 07/07/22 11:34 07/08/22 01:25 14-Bromophenyl phenyl ether ND
9.23 2.31 ug/L 07/07/22 11:34 07/08/22 01:25 14-Chloro-3-methylphenol ND
18.5 0.923 ug/L 07/07/22 11:34 07/08/22 01:25 14-Chloroaniline ND
9.23 4.89 ug/L 07/07/22 11:34 07/08/22 01:25 14-Chlorophenyl phenyl ether ND
46.1 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 14-Nitroaniline ND
46.1 7.47 ug/L 07/07/22 11:34 07/08/22 01:25 14-Nitrophenol ND
9.23 4.06 ug/L 07/07/22 11:34 07/08/22 01:25 1AcenaphtheneND
9.23 3.32 ug/L 07/07/22 11:34 07/08/22 01:25 1AcenaphthyleneND
9.23 2.03 ug/L 07/07/22 11:34 07/08/22 01:25 1AcetophenoneND
9.23 3.32 ug/L 07/07/22 11:34 07/08/22 01:25 1AnthraceneND
9.23 2.03 ug/L 07/07/22 11:34 07/08/22 01:25 1AtrazineND
9.23 4.43 ug/L 07/07/22 11:34 07/08/22 01:25 1BenzaldehydeND
9.23 3.87 ug/L 07/07/22 11:34 07/08/22 01:25 1Benzo[a]anthracene ND
9.23 2.58 ug/L 07/07/22 11:34 07/08/22 01:25 1Benzo[a]pyrene ND
9.23 2.86 ug/L 07/07/22 11:34 07/08/22 01:25 1Benzo[b]fluoranthene ND
9.23 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 1Benzo[g,h,i]perylene ND
9.23 2.68 ug/L 07/07/22 11:34 07/08/22 01:25 1Benzo[k]fluoranthene ND
9.23 2.86 ug/L 07/07/22 11:34 07/08/22 01:25 1bis (2-chloroisopropyl) ether ND
9.23 1.66 ug/L 07/07/22 11:34 07/08/22 01:25 1Bis(2-chloroethoxy)methane ND
9.23 3.32 ug/L 07/07/22 11:34 07/08/22 01:25 1Bis(2-chloroethyl)ether ND
9.23 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 1Bis(2-ethylhexyl) phthalate ND
9.23 2.58 ug/L 07/07/22 11:34 07/08/22 01:25 1Butyl benzyl phthalate ND
9.23 2.58 ug/L 07/07/22 11:34 07/08/22 01:25 1CaprolactamND
9.23 1.66 ug/L 07/07/22 11:34 07/08/22 01:25 1CarbazoleND
9.23 3.51 ug/L 07/07/22 11:34 07/08/22 01:25 1ChryseneND
9.23 2.77 ug/L 07/07/22 11:34 07/08/22 01:25 1Dibenz(a,h)anthracene ND
9.23 1.75 ug/L 07/07/22 11:34 07/08/22 01:25 1DibenzofuranND
9.23 2.03 ug/L 07/07/22 11:34 07/08/22 01:25 1Diethyl phthalate 7.57 J
9.23 1.94 ug/L 07/07/22 11:34 07/08/22 01:25 1Dimethyl phthalate ND
9.23 2.12 ug/L 07/07/22 11:34 07/08/22 01:25 1Di-n-butyl phthalate ND
9.23 2.58 ug/L 07/07/22 11:34 07/08/22 01:25 1Di-n-octyl phthalate ND
9.23 1.48 ug/L 07/07/22 11:34 07/08/22 01:25 1FluorantheneND
9.23 3.14 ug/L 07/07/22 11:34 07/08/22 01:25 1FluoreneND
9.23 1.48 ug/L 07/07/22 11:34 07/08/22 01:25 1HexachlorobenzeneND
9.23 3.69 ug/L 07/07/22 11:34 07/08/22 01:25 1HexachlorobutadieneND
9.23 3.23 ug/L 07/07/22 11:34 07/08/22 01:25 1HexachlorocyclopentadieneND
9.23 3.32 ug/L 07/07/22 11:34 07/08/22 01:25 1HexachloroethaneND
9.23 3.97 ug/L 07/07/22 11:34 07/08/22 01:25 1Indeno[1,2,3-cd]pyrene ND
9.23 1.85 ug/L 07/07/22 11:34 07/08/22 01:25 1IsophoroneND
9.23 3.23 ug/L 07/07/22 11:34 07/08/22 01:25 1Naphthalene184
9.23 3.23 ug/L 07/07/22 11:34 07/08/22 01:25 1NitrobenzeneND
9.23 2.21 ug/L 07/07/22 11:34 07/08/22 01:25 1N-Nitrosodi-n-propylamine ND
9.23 2.68 ug/L 07/07/22 11:34 07/08/22 01:25 1N-Nitrosodiphenylamine ND
46.1 9.13 ug/L 07/07/22 11:34 07/08/22 01:25 1PentachlorophenolND
9.23 3.97 ug/L 07/07/22 11:34 07/08/22 01:25 1PhenanthreneND
9.23 1.38 ug/L 07/07/22 11:34 07/08/22 01:25 1PhenolND
9.23 3.41 ug/L 07/07/22 11:34 07/08/22 01:25 1PyreneND
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Client Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Lab Sample ID: 680-217736-5Client Sample ID: Duplicate
Matrix: WaterDate Collected: 06/30/22 00:00
Date Received: 07/01/22 11:00
2,4,6-Tribromophenol (Surr)110 30-130 07/07/22 11:34 07/08/22 01:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)52 07/07/22 11:34 07/08/22 01:25 125-130
2-Fluorophenol (Surr)32 07/07/22 11:34 07/08/22 01:25 110-130
Nitrobenzene-d5 (Surr)56 07/07/22 11:34 07/08/22 01:25 130-130
Phenol-d5 (Surr)23 07/07/22 11:34 07/08/22 01:25 110-130
Terphenyl-d14 (Surr)80 07/07/22 11:34 07/08/22 01:25 135-131
Method: 6020B - Metals (ICP/MS) - Total Recoverable
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 22:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00500 0.000890 mg/L 07/05/22 17:15 07/06/22 22:28 1Barium0.511
0.000500 0.0000780 mg/L 07/05/22 17:15 07/06/22 22:28 1Cadmium0.000115 J
0.00500 0.00260 mg/L 07/05/22 17:15 07/06/22 22:28 1ChromiumND
0.00250 0.000340 mg/L 07/05/22 17:15 07/06/22 22:28 1Lead0.000630 J
0.00250 0.00120 mg/L 07/05/22 17:15 07/06/22 22:28 1SeleniumND
0.00100 0.000390 mg/L 07/05/22 17:15 07/06/22 22:28 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 680-729670/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 0.360 ug/L 07/08/22 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.2101.00 ug/L 07/08/22 15:35 11,1,1-Trichloroethane
ND 0.4001.00 ug/L 07/08/22 15:35 11,1,2,2-Tetrachloroethane
ND 0.2301.00 ug/L 07/08/22 15:35 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.3201.00 ug/L 07/08/22 15:35 11,1,2-Trichloroethane
ND 0.3301.00 ug/L 07/08/22 15:35 11,1-Dichloroethane
ND 0.3301.00 ug/L 07/08/22 15:35 11,1-Dichloroethene
ND 0.2801.00 ug/L 07/08/22 15:35 11,1-Dichloropropene
ND 0.8105.00 ug/L 07/08/22 15:35 11,2,3-Trichlorobenzene
ND 0.4801.00 ug/L 07/08/22 15:35 11,2,3-Trichloropropane
ND 0.5305.00 ug/L 07/08/22 15:35 11,2,4-Trichlorobenzene
ND 0.4301.00 ug/L 07/08/22 15:35 11,2,4-Trimethylbenzene
ND 1.805.00 ug/L 07/08/22 15:35 11,2-Dibromo-3-Chloropropane
ND 0.3101.00 ug/L 07/08/22 15:35 11,2-Dichlorobenzene
ND 0.2501.00 ug/L 07/08/22 15:35 11,2-Dichloroethane
ND 0.2201.00 ug/L 07/08/22 15:35 11,2-Dichloropropane
ND 0.2801.00 ug/L 07/08/22 15:35 11,3,5-Trimethylbenzene
ND 0.3101.00 ug/L 07/08/22 15:35 11,3-Dichlorobenzene
ND 0.3601.00 ug/L 07/08/22 15:35 11,3-Dichloropropane
ND 0.3101.00 ug/L 07/08/22 15:35 11,4-Dichlorobenzene
ND 0.3501.00 ug/L 07/08/22 15:35 12,2-Dichloropropane
ND 6.4010.0 ug/L 07/08/22 15:35 12-Butanone (MEK)
ND 0.2501.00 ug/L 07/08/22 15:35 12-Chlorotoluene
ND 3.2010.0 ug/L 07/08/22 15:35 12-Hexanone
ND 0.4101.00 ug/L 07/08/22 15:35 14-Chlorotoluene
ND 0.4401.00 ug/L 07/08/22 15:35 14-Isopropyltoluene
ND 2.7010.0 ug/L 07/08/22 15:35 14-Methyl-2-pentanone (MIBK)
ND 3.7010.0 ug/L 07/08/22 15:35 1Acetone
ND 0.2701.00 ug/L 07/08/22 15:35 1Benzene
ND 0.2401.00 ug/L 07/08/22 15:35 1Bromobenzene
ND 0.5901.00 ug/L 07/08/22 15:35 1Bromoform
ND 3.705.00 ug/L 07/08/22 15:35 1Bromomethane
ND 0.4302.00 ug/L 07/08/22 15:35 1Carbon disulfide
ND 0.3001.00 ug/L 07/08/22 15:35 1Carbon tetrachloride
ND 0.1501.00 ug/L 07/08/22 15:35 1Chlorobenzene
ND 0.3401.00 ug/L 07/08/22 15:35 1Chlorobromomethane
ND 0.3901.00 ug/L 07/08/22 15:35 1Chlorodibromomethane
ND 4.605.00 ug/L 07/08/22 15:35 1Chloroethane
ND 0.2701.00 ug/L 07/08/22 15:35 1Chloroform
ND 0.5401.00 ug/L 07/08/22 15:35 1Chloromethane
ND 0.2501.00 ug/L 07/08/22 15:35 1cis-1,2-Dichloroethene
ND 0.2601.00 ug/L 07/08/22 15:35 1cis-1,3-Dichloropropene
ND 0.3401.00 ug/L 07/08/22 15:35 1Dibromomethane
ND 0.2501.00 ug/L 07/08/22 15:35 1Dichlorobromomethane
ND 0.3601.00 ug/L 07/08/22 15:35 1Dichlorodifluoromethane
ND 5.0010.0 ug/L 07/08/22 15:35 1Ethyl acetate
ND 0.2001.00 ug/L 07/08/22 15:35 1Ethylbenzene
ND 0.3301.00 ug/L 07/08/22 15:35 1Ethylene Dibromide
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-729670/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
RL MDL
Hexachlorobutadiene ND 5.00 0.220 ug/L 07/08/22 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.6505.00 ug/L 07/08/22 15:35 1Hexane
ND 3.9010.0 ug/L 07/08/22 15:35 1Iodomethane
ND 0.70010.0 ug/L 07/08/22 15:35 1Isopropyl ether
ND 0.2601.00 ug/L 07/08/22 15:35 1Isopropylbenzene
ND 0.4901.00 ug/L 07/08/22 15:35 1m,p-Xylene
ND 0.8105.00 ug/L 07/08/22 15:35 1Methyl tert-butyl ether
ND 3.205.00 ug/L 07/08/22 15:35 1Methylene Chloride
ND 2.405.00 ug/L 07/08/22 15:35 1Naphthalene
ND 0.5201.00 ug/L 07/08/22 15:35 1n-Butylbenzene
ND 0.4301.00 ug/L 07/08/22 15:35 1n-Heptane
ND 0.4101.00 ug/L 07/08/22 15:35 1N-Propylbenzene
ND 0.2601.00 ug/L 07/08/22 15:35 1o-Xylene
ND 0.5301.00 ug/L 07/08/22 15:35 1sec-Butylbenzene
ND 0.2701.00 ug/L 07/08/22 15:35 1Styrene
ND 0.4301.00 ug/L 07/08/22 15:35 1tert-Butylbenzene
ND 0.3500.500 ug/L 07/08/22 15:35 1Tetrachloroethene
ND 0.2501.00 ug/L 07/08/22 15:35 1Toluene
ND 0.3401.00 ug/L 07/08/22 15:35 1trans-1,2-Dichloroethene
ND 0.2301.00 ug/L 07/08/22 15:35 1trans-1,3-Dichloropropene
ND 1.252.00 ug/L 07/08/22 15:35 1trans-1,4-Dichloro-2-butene
ND 0.2001.00 ug/L 07/08/22 15:35 1Trichloroethene
ND 0.3301.00 ug/L 07/08/22 15:35 1Trichlorofluoromethane
ND 0.6902.00 ug/L 07/08/22 15:35 1Vinyl acetate
ND 0.4001.00 ug/L 07/08/22 15:35 1Vinyl chloride
ND 0.2301.00 ug/L 07/08/22 15:35 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)81 60-124 07/08/22 15:35 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
105 07/08/22 15:35 14-Bromofluorobenzene (Surr)70-130
93 07/08/22 15:35 1Dibromofluoromethane (Surr)70-130
105 07/08/22 15:35 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729670/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
1,1,1,2-Tetrachloroethane 50.0 54.68 ug/L 109 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 46.82 ug/L 94 70 -130
1,1,2,2-Tetrachloroethane 50.0 55.65 ug/L 111 70 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 47.28 ug/L 95 63 -141
1,1,2-Trichloroethane 50.0 52.77 ug/L 106 70 -130
1,1-Dichloroethane 50.0 50.55 ug/L 101 70 -130
1,1-Dichloroethene 50.0 45.65 ug/L 91 70 -130
1,1-Dichloropropene 50.0 54.35 ug/L 109 70 -130
1,2,3-Trichlorobenzene 50.0 49.47 ug/L 99 61 -141
1,2,3-Trichloropropane 50.0 49.57 ug/L 99 70 -130
Eurofins Savannah
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729670/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
1,2,4-Trichlorobenzene 50.0 48.71 ug/L 97 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2,4-Trimethylbenzene 50.0 52.25 ug/L 104 70 -130
1,2-Dibromo-3-Chloropropane 50.0 49.29 ug/L 99 70 -130
1,2-Dichlorobenzene 50.0 50.01 ug/L 100 70 -130
1,2-Dichloroethane 50.0 43.98 ug/L 88 70 -130
1,2-Dichloropropane 50.0 54.76 ug/L 110 70 -130
1,3,5-Trimethylbenzene 50.0 51.70 ug/L 103 70 -130
1,3-Dichlorobenzene 50.0 52.34 ug/L 105 70 -130
1,3-Dichloropropane 50.0 50.77 ug/L 102 70 -130
1,4-Dichlorobenzene 50.0 50.32 ug/L 101 70 -130
2,2-Dichloropropane 50.0 49.09 ug/L 98 70 -130
2-Butanone (MEK)250 242.3 ug/L 97 69 -120
2-Chlorotoluene 50.0 50.40 ug/L 101 70 -130
2-Hexanone 250 286.2 ug/L 114 70 -130
4-Chlorotoluene 50.0 50.79 ug/L 102 70 -130
4-Isopropyltoluene 50.0 55.96 ug/L 112 70 -130
4-Methyl-2-pentanone (MIBK)250 287.9 ug/L 115 68 -120
Acetone 250 242.0 ug/L 97 67 -120
Benzene 50.0 53.70 ug/L 107 70 -130
Bromobenzene 50.0 48.48 ug/L 97 70 -130
Bromoform 50.0 46.27 ug/L 93 69 -129
Bromomethane 50.0 155.7 *+ug/L 311 28 -192
Carbon disulfide 50.0 48.77 ug/L 98 70 -130
Carbon tetrachloride 50.0 44.79 ug/L 90 70 -130
Chlorobenzene 50.0 49.95 ug/L 100 70 -130
Chlorobromomethane 50.0 45.98 ug/L 92 70 -130
Chlorodibromomethane 50.0 47.74 ug/L 95 70 -130
Chloroethane 50.0 118.1 E *+ug/L 236 31 -213
Chloroform 50.0 45.92 ug/L 92 70 -130
Chloromethane 50.0 43.58 ug/L 87 59 -127
cis-1,2-Dichloroethene 50.0 47.72 ug/L 95 70 -130
cis-1,3-Dichloropropene 50.0 54.06 ug/L 108 70 -130
Dibromomethane 50.0 47.17 ug/L 94 70 -130
Dichlorobromomethane 50.0 49.14 ug/L 98 70 -130
Dichlorodifluoromethane 50.0 43.38 ug/L 87 70 -130
Ethylbenzene 50.0 54.41 ug/L 109 70 -130
Ethylene Dibromide 50.0 50.37 ug/L 101 70 -130
Hexachlorobutadiene 50.0 45.74 ug/L 91 70 -130
Hexane 50.0 61.46 ug/L 123 70 -130
Iodomethane 50.0 83.49 *+ug/L 167 52 -129
Isopropylbenzene 50.0 54.28 ug/L 109 70 -130
m,p-Xylene 50.0 51.67 ug/L 103 70 -130
Methyl tert-butyl ether 50.0 48.08 ug/L 96 70 -130
Methylene Chloride 50.0 46.08 ug/L 92 70 -130
Naphthalene 50.0 47.90 ug/L 96 57 -149
n-Butylbenzene 50.0 57.91 ug/L 116 70 -130
n-Heptane 50.0 66.09 *+ug/L 132 65 -120
N-Propylbenzene 50.0 54.80 ug/L 110 70 -130
o-Xylene 50.0 52.27 ug/L 105 70 -130
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729670/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
sec-Butylbenzene 50.0 54.50 ug/L 109 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Styrene 50.0 56.44 ug/L 113 70 -130
tert-Butylbenzene 50.0 51.44 ug/L 103 70 -130
Tetrachloroethene 50.0 47.22 ug/L 94 70 -130
Toluene 50.0 50.85 ug/L 102 70 -130
trans-1,2-Dichloroethene 50.0 46.49 ug/L 93 70 -130
trans-1,3-Dichloropropene 50.0 54.11 ug/L 108 70 -130
trans-1,4-Dichloro-2-butene 50.0 55.06 ug/L 110 67 -120
Trichloroethene 50.0 47.71 ug/L 95 70 -130
Trichlorofluoromethane 50.0 69.14 ug/L 138 63 -142
Vinyl acetate 100 134.9 ug/L 135 67 -135
Vinyl chloride 50.0 54.90 ug/L 110 66 -129
Xylenes, Total 100 103.9 ug/L 104 70 -130
1,2-Dichloroethane-d4 (Surr)60 -124
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)70 -130
92Dibromofluoromethane (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-729670/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
1,1,1,2-Tetrachloroethane 50.0 57.67 ug/L 115 70 -130 5 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 46.84 ug/L 94 70 -130 0 30
1,1,2,2-Tetrachloroethane 50.0 59.15 ug/L 118 70 -130 6 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 45.25 ug/L 91 63 -141 4 30
1,1,2-Trichloroethane 50.0 53.71 ug/L 107 70 -130 2 30
1,1-Dichloroethane 50.0 50.89 ug/L 102 70 -130 1 30
1,1-Dichloroethene 50.0 46.43 ug/L 93 70 -130 2 20
1,1-Dichloropropene 50.0 52.52 ug/L 105 70 -130 3 20
1,2,3-Trichlorobenzene 50.0 49.50 ug/L 99 61 -141 0 30
1,2,3-Trichloropropane 50.0 50.19 ug/L 100 70 -130 1 30
1,2,4-Trichlorobenzene 50.0 48.69 ug/L 97 70 -130 0 30
1,2,4-Trimethylbenzene 50.0 52.71 ug/L 105 70 -130 1 30
1,2-Dibromo-3-Chloropropane 50.0 50.65 ug/L 101 70 -130 3 30
1,2-Dichlorobenzene 50.0 49.98 ug/L 100 70 -130 0 30
1,2-Dichloroethane 50.0 45.44 ug/L 91 70 -130 3 50
1,2-Dichloropropane 50.0 56.49 ug/L 113 70 -130 3 20
1,3,5-Trimethylbenzene 50.0 52.25 ug/L 104 70 -130 1 30
1,3-Dichlorobenzene 50.0 52.90 ug/L 106 70 -130 1 30
1,3-Dichloropropane 50.0 53.51 ug/L 107 70 -130 5 20
1,4-Dichlorobenzene 50.0 49.54 ug/L 99 70 -130 2 30
2,2-Dichloropropane 50.0 48.46 ug/L 97 70 -130 1 20
2-Butanone (MEK)250 261.6 ug/L 105 69 -120 8 30
2-Chlorotoluene 50.0 50.76 ug/L 102 70 -130 1 30
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-729670/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729670
2-Hexanone 250 304.2 ug/L 122 70 -130 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Chlorotoluene 50.0 52.31 ug/L 105 70 -130 3 30
4-Isopropyltoluene 50.0 53.94 ug/L 108 70 -130 4 30
4-Methyl-2-pentanone (MIBK)250 300.9 ug/L 120 68 -120 4 30
Acetone 250 243.0 ug/L 97 67 -120 0 30
Benzene 50.0 53.69 ug/L 107 70 -130 0 30
Bromobenzene 50.0 49.78 ug/L 100 70 -130 3 30
Bromoform 50.0 47.34 ug/L 95 69 -129 2 30
Bromomethane 50.0 156.7 *+ug/L 313 28 -192 1 30
Carbon disulfide 50.0 47.84 ug/L 96 70 -130 2 30
Carbon tetrachloride 50.0 45.89 ug/L 92 70 -130 2 30
Chlorobenzene 50.0 51.45 ug/L 103 70 -130 3 30
Chlorobromomethane 50.0 46.71 ug/L 93 70 -130 2 30
Chlorodibromomethane 50.0 49.75 ug/L 100 70 -130 4 30
Chloroethane 50.0 118.7 E *+ug/L 237 31 -213 0 30
Chloroform 50.0 46.64 ug/L 93 70 -130 2 30
Chloromethane 50.0 43.81 ug/L 88 59 -127 1 30
cis-1,2-Dichloroethene 50.0 48.85 ug/L 98 70 -130 2 30
cis-1,3-Dichloropropene 50.0 55.92 ug/L 112 70 -130 3 20
Dibromomethane 50.0 47.98 ug/L 96 70 -130 2 30
Dichlorobromomethane 50.0 49.99 ug/L 100 70 -130 2 30
Dichlorodifluoromethane 50.0 41.80 ug/L 84 70 -130 4 40
Ethylbenzene 50.0 55.58 ug/L 111 70 -130 2 20
Ethylene Dibromide 50.0 52.14 ug/L 104 70 -130 3 30
Hexachlorobutadiene 50.0 45.76 ug/L 92 70 -130 0 20
Hexane 50.0 59.91 ug/L 120 70 -130 3 30
Iodomethane 50.0 82.76 *+ug/L 166 52 -129 1 30
Isopropylbenzene 50.0 54.78 ug/L 110 70 -130 1 30
m,p-Xylene 50.0 52.26 ug/L 105 70 -130 1 30
Methyl tert-butyl ether 50.0 50.10 ug/L 100 70 -130 4 30
Methylene Chloride 50.0 47.04 ug/L 94 70 -130 2 30
Naphthalene 50.0 48.73 ug/L 97 57 -149 2 30
n-Butylbenzene 50.0 56.63 ug/L 113 70 -130 2 30
n-Heptane 50.0 65.02 *+ug/L 130 65 -120 2 30
N-Propylbenzene 50.0 56.29 ug/L 113 70 -130 3 30
o-Xylene 50.0 53.05 ug/L 106 70 -130 1 30
sec-Butylbenzene 50.0 55.15 ug/L 110 70 -130 1 30
Styrene 50.0 56.00 ug/L 112 70 -130 1 30
tert-Butylbenzene 50.0 52.69 ug/L 105 70 -130 2 30
Tetrachloroethene 50.0 48.48 ug/L 97 70 -130 3 30
Toluene 50.0 51.19 ug/L 102 70 -130 1 30
trans-1,2-Dichloroethene 50.0 45.77 ug/L 92 70 -130 2 30
trans-1,3-Dichloropropene 50.0 55.68 ug/L 111 70 -130 3 30
trans-1,4-Dichloro-2-butene 50.0 58.92 ug/L 118 67 -120 7 30
Trichloroethene 50.0 47.95 ug/L 96 70 -130 1 30
Trichlorofluoromethane 50.0 69.31 ug/L 139 63 -142 0 30
Vinyl acetate 100 140.7 *+ug/L 141 67 -135 4 30
Vinyl chloride 50.0 55.44 ug/L 111 66 -129 1 30
Xylenes, Total 100 105.3 ug/L 105 70 -130 1 30
Eurofins Savannah
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
1,2-Dichloroethane-d4 (Surr)60 -124
Surrogate
92
LCSD LCSD
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)70 -130
92Dibromofluoromethane (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 680-730068/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 0.360 ug/L 07/11/22 16:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.2101.00 ug/L 07/11/22 16:35 11,1,1-Trichloroethane
ND 0.4001.00 ug/L 07/11/22 16:35 11,1,2,2-Tetrachloroethane
ND 0.2301.00 ug/L 07/11/22 16:35 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.3201.00 ug/L 07/11/22 16:35 11,1,2-Trichloroethane
ND 0.3301.00 ug/L 07/11/22 16:35 11,1-Dichloroethane
ND 0.3301.00 ug/L 07/11/22 16:35 11,1-Dichloroethene
ND 0.2801.00 ug/L 07/11/22 16:35 11,1-Dichloropropene
ND 0.8105.00 ug/L 07/11/22 16:35 11,2,3-Trichlorobenzene
ND 0.4801.00 ug/L 07/11/22 16:35 11,2,3-Trichloropropane
ND 0.5305.00 ug/L 07/11/22 16:35 11,2,4-Trichlorobenzene
ND 0.4301.00 ug/L 07/11/22 16:35 11,2,4-Trimethylbenzene
ND 1.805.00 ug/L 07/11/22 16:35 11,2-Dibromo-3-Chloropropane
ND 0.3101.00 ug/L 07/11/22 16:35 11,2-Dichlorobenzene
ND 0.2501.00 ug/L 07/11/22 16:35 11,2-Dichloroethane
ND 0.2201.00 ug/L 07/11/22 16:35 11,2-Dichloropropane
ND 0.2801.00 ug/L 07/11/22 16:35 11,3,5-Trimethylbenzene
ND 0.3101.00 ug/L 07/11/22 16:35 11,3-Dichlorobenzene
ND 0.3601.00 ug/L 07/11/22 16:35 11,3-Dichloropropane
ND 0.3101.00 ug/L 07/11/22 16:35 11,4-Dichlorobenzene
ND 0.3501.00 ug/L 07/11/22 16:35 12,2-Dichloropropane
ND 6.4010.0 ug/L 07/11/22 16:35 12-Butanone (MEK)
ND 0.2501.00 ug/L 07/11/22 16:35 12-Chlorotoluene
ND 3.2010.0 ug/L 07/11/22 16:35 12-Hexanone
ND 0.4101.00 ug/L 07/11/22 16:35 14-Chlorotoluene
ND 0.4401.00 ug/L 07/11/22 16:35 14-Isopropyltoluene
ND 2.7010.0 ug/L 07/11/22 16:35 14-Methyl-2-pentanone (MIBK)
ND 3.7010.0 ug/L 07/11/22 16:35 1Acetone
ND 0.2701.00 ug/L 07/11/22 16:35 1Benzene
ND 0.2401.00 ug/L 07/11/22 16:35 1Bromobenzene
ND 0.5901.00 ug/L 07/11/22 16:35 1Bromoform
ND 3.705.00 ug/L 07/11/22 16:35 1Bromomethane
ND 0.4302.00 ug/L 07/11/22 16:35 1Carbon disulfide
ND 0.3001.00 ug/L 07/11/22 16:35 1Carbon tetrachloride
ND 0.1501.00 ug/L 07/11/22 16:35 1Chlorobenzene
ND 0.3401.00 ug/L 07/11/22 16:35 1Chlorobromomethane
ND 0.3901.00 ug/L 07/11/22 16:35 1Chlorodibromomethane
ND 4.605.00 ug/L 07/11/22 16:35 1Chloroethane
ND 0.2701.00 ug/L 07/11/22 16:35 1Chloroform
ND 0.5401.00 ug/L 07/11/22 16:35 1Chloromethane
ND 0.2501.00 ug/L 07/11/22 16:35 1cis-1,2-Dichloroethene
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-730068/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
RL MDL
cis-1,3-Dichloropropene ND 1.00 0.260 ug/L 07/11/22 16:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.3401.00 ug/L 07/11/22 16:35 1Dibromomethane
ND 0.2501.00 ug/L 07/11/22 16:35 1Dichlorobromomethane
ND 0.3601.00 ug/L 07/11/22 16:35 1Dichlorodifluoromethane
ND 5.0010.0 ug/L 07/11/22 16:35 1Ethyl acetate
ND 0.2001.00 ug/L 07/11/22 16:35 1Ethylbenzene
ND 0.3301.00 ug/L 07/11/22 16:35 1Ethylene Dibromide
ND 0.2205.00 ug/L 07/11/22 16:35 1Hexachlorobutadiene
ND 0.6505.00 ug/L 07/11/22 16:35 1Hexane
ND 3.9010.0 ug/L 07/11/22 16:35 1Iodomethane
ND 0.70010.0 ug/L 07/11/22 16:35 1Isopropyl ether
ND 0.2601.00 ug/L 07/11/22 16:35 1Isopropylbenzene
ND 0.4901.00 ug/L 07/11/22 16:35 1m,p-Xylene
ND 0.8105.00 ug/L 07/11/22 16:35 1Methyl tert-butyl ether
ND 3.205.00 ug/L 07/11/22 16:35 1Methylene Chloride
ND 2.405.00 ug/L 07/11/22 16:35 1Naphthalene
ND 0.5201.00 ug/L 07/11/22 16:35 1n-Butylbenzene
ND 0.4301.00 ug/L 07/11/22 16:35 1n-Heptane
ND 0.4101.00 ug/L 07/11/22 16:35 1N-Propylbenzene
ND 0.2601.00 ug/L 07/11/22 16:35 1o-Xylene
ND 0.5301.00 ug/L 07/11/22 16:35 1sec-Butylbenzene
ND 0.2701.00 ug/L 07/11/22 16:35 1Styrene
ND 0.4301.00 ug/L 07/11/22 16:35 1tert-Butylbenzene
ND 0.3500.500 ug/L 07/11/22 16:35 1Tetrachloroethene
ND 0.2501.00 ug/L 07/11/22 16:35 1Toluene
ND 0.3401.00 ug/L 07/11/22 16:35 1trans-1,2-Dichloroethene
ND 0.2301.00 ug/L 07/11/22 16:35 1trans-1,3-Dichloropropene
ND 1.252.00 ug/L 07/11/22 16:35 1trans-1,4-Dichloro-2-butene
ND 0.2001.00 ug/L 07/11/22 16:35 1Trichloroethene
ND 0.3301.00 ug/L 07/11/22 16:35 1Trichlorofluoromethane
ND 0.6902.00 ug/L 07/11/22 16:35 1Vinyl acetate
ND 0.4001.00 ug/L 07/11/22 16:35 1Vinyl chloride
ND 0.2301.00 ug/L 07/11/22 16:35 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)91 60-124 07/11/22 16:35 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 07/11/22 16:35 14-Bromofluorobenzene (Surr)70-130
102 07/11/22 16:35 1Dibromofluoromethane (Surr)70-130
104 07/11/22 16:35 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730068/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
1,1,1,2-Tetrachloroethane 50.0 56.19 ug/L 112 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 47.21 ug/L 94 70 -130
1,1,2,2-Tetrachloroethane 50.0 57.12 ug/L 114 70 -130
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730068/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 53.36 ug/L 107 63 -141
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2-Trichloroethane 50.0 52.90 ug/L 106 70 -130
1,1-Dichloroethane 50.0 49.55 ug/L 99 70 -130
1,1-Dichloroethene 50.0 46.30 ug/L 93 70 -130
1,1-Dichloropropene 50.0 47.27 ug/L 95 70 -130
1,2,3-Trichlorobenzene 50.0 55.47 ug/L 111 61 -141
1,2,3-Trichloropropane 50.0 54.65 ug/L 109 70 -130
1,2,4-Trichlorobenzene 50.0 56.73 ug/L 113 70 -130
1,2,4-Trimethylbenzene 50.0 55.32 ug/L 111 70 -130
1,2-Dibromo-3-Chloropropane 50.0 55.89 ug/L 112 70 -130
1,2-Dichlorobenzene 50.0 52.30 ug/L 105 70 -130
1,2-Dichloroethane 50.0 48.94 ug/L 98 70 -130
1,2-Dichloropropane 50.0 49.60 ug/L 99 70 -130
1,3,5-Trimethylbenzene 50.0 53.88 ug/L 108 70 -130
1,3-Dichlorobenzene 50.0 52.54 ug/L 105 70 -130
1,3-Dichloropropane 50.0 52.69 ug/L 105 70 -130
1,4-Dichlorobenzene 50.0 52.29 ug/L 105 70 -130
2,2-Dichloropropane 50.0 44.14 ug/L 88 70 -130
2-Butanone (MEK)250 252.4 ug/L 101 69 -120
2-Chlorotoluene 50.0 51.21 ug/L 102 70 -130
2-Hexanone 250 259.0 ug/L 104 70 -130
4-Chlorotoluene 50.0 51.45 ug/L 103 70 -130
4-Isopropyltoluene 50.0 51.54 ug/L 103 70 -130
4-Methyl-2-pentanone (MIBK)250 255.6 ug/L 102 68 -120
Acetone 250 264.1 ug/L 106 67 -120
Benzene 50.0 49.60 ug/L 99 70 -130
Bromobenzene 50.0 57.98 ug/L 116 70 -130
Bromoform 50.0 63.52 ug/L 127 69 -129
Bromomethane 50.0 59.35 ug/L 119 28 -192
Carbon disulfide 50.0 45.94 ug/L 92 70 -130
Carbon tetrachloride 50.0 49.40 ug/L 99 70 -130
Chlorobenzene 50.0 53.92 ug/L 108 70 -130
Chlorobromomethane 50.0 52.54 ug/L 105 70 -130
Chlorodibromomethane 50.0 56.69 ug/L 113 70 -130
Chloroethane 50.0 60.24 ug/L 120 31 -213
Chloroform 50.0 48.67 ug/L 97 70 -130
Chloromethane 50.0 41.55 ug/L 83 59 -127
cis-1,2-Dichloroethene 50.0 48.24 ug/L 96 70 -130
cis-1,3-Dichloropropene 50.0 52.70 ug/L 105 70 -130
Dibromomethane 50.0 53.53 ug/L 107 70 -130
Dichlorobromomethane 50.0 51.44 ug/L 103 70 -130
Dichlorodifluoromethane 50.0 35.01 ug/L 70 70 -130
Ethylbenzene 50.0 53.60 ug/L 107 70 -130
Ethylene Dibromide 50.0 53.45 ug/L 107 70 -130
Hexachlorobutadiene 50.0 48.01 ug/L 96 70 -130
Hexane 50.0 39.58 ug/L 79 70 -130
Iodomethane 50.0 55.45 ug/L 111 52 -129
Isopropylbenzene 50.0 52.97 ug/L 106 70 -130
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-730068/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
m,p-Xylene 50.0 52.01 ug/L 104 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Methyl tert-butyl ether 50.0 49.59 ug/L 99 70 -130
Methylene Chloride 50.0 50.65 ug/L 101 70 -130
Naphthalene 50.0 54.57 ug/L 109 57 -149
n-Butylbenzene 50.0 48.89 ug/L 98 70 -130
n-Heptane 50.0 36.35 ug/L 73 65 -120
N-Propylbenzene 50.0 53.78 ug/L 108 70 -130
o-Xylene 50.0 52.83 ug/L 106 70 -130
sec-Butylbenzene 50.0 54.04 ug/L 108 70 -130
Styrene 50.0 56.71 ug/L 113 70 -130
tert-Butylbenzene 50.0 52.74 ug/L 105 70 -130
Tetrachloroethene 50.0 50.64 ug/L 101 70 -130
Toluene 50.0 51.89 ug/L 104 70 -130
trans-1,2-Dichloroethene 50.0 52.46 ug/L 105 70 -130
trans-1,3-Dichloropropene 50.0 52.61 ug/L 105 70 -130
trans-1,4-Dichloro-2-butene 50.0 54.72 ug/L 109 67 -120
Trichloroethene 50.0 51.09 ug/L 102 70 -130
Trichlorofluoromethane 50.0 50.87 ug/L 102 63 -142
Vinyl acetate 100 191.5 *+ug/L 191 67 -135
Vinyl chloride 50.0 38.75 ug/L 78 66 -129
Xylenes, Total 100 104.8 ug/L 105 70 -130
1,2-Dichloroethane-d4 (Surr)60 -124
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)70 -130
105Dibromofluoromethane (Surr)70 -130
108Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730068/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
1,1,1,2-Tetrachloroethane 50.0 57.78 ug/L 116 70 -130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,1-Trichloroethane 50.0 47.30 ug/L 95 70 -130 0 30
1,1,2,2-Tetrachloroethane 50.0 57.79 ug/L 116 70 -130 1 30
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 52.27 ug/L 105 63 -141 2 30
1,1,2-Trichloroethane 50.0 53.30 ug/L 107 70 -130 1 30
1,1-Dichloroethane 50.0 48.61 ug/L 97 70 -130 2 30
1,1-Dichloroethene 50.0 47.18 ug/L 94 70 -130 2 20
1,1-Dichloropropene 50.0 46.44 ug/L 93 70 -130 2 20
1,2,3-Trichlorobenzene 50.0 55.10 ug/L 110 61 -141 1 30
1,2,3-Trichloropropane 50.0 57.23 ug/L 114 70 -130 5 30
1,2,4-Trichlorobenzene 50.0 57.42 ug/L 115 70 -130 1 30
1,2,4-Trimethylbenzene 50.0 56.58 ug/L 113 70 -130 2 30
1,2-Dibromo-3-Chloropropane 50.0 57.89 ug/L 116 70 -130 4 30
1,2-Dichlorobenzene 50.0 51.50 ug/L 103 70 -130 2 30
1,2-Dichloroethane 50.0 48.34 ug/L 97 70 -130 1 50
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730068/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
1,2-Dichloropropane 50.0 50.72 ug/L 101 70 -130 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,3,5-Trimethylbenzene 50.0 53.74 ug/L 107 70 -130 0 30
1,3-Dichlorobenzene 50.0 51.05 ug/L 102 70 -130 3 30
1,3-Dichloropropane 50.0 53.52 ug/L 107 70 -130 2 20
1,4-Dichlorobenzene 50.0 50.11 ug/L 100 70 -130 4 30
2,2-Dichloropropane 50.0 44.45 ug/L 89 70 -130 1 20
2-Butanone (MEK)250 264.0 ug/L 106 69 -120 5 30
2-Chlorotoluene 50.0 52.08 ug/L 104 70 -130 2 30
2-Hexanone 250 267.9 ug/L 107 70 -130 3 20
4-Chlorotoluene 50.0 53.41 ug/L 107 70 -130 4 30
4-Isopropyltoluene 50.0 48.65 ug/L 97 70 -130 6 30
4-Methyl-2-pentanone (MIBK)250 265.5 ug/L 106 68 -120 4 30
Acetone 250 261.4 ug/L 105 67 -120 1 30
Benzene 50.0 49.50 ug/L 99 70 -130 0 30
Bromobenzene 50.0 58.01 ug/L 116 70 -130 0 30
Bromoform 50.0 66.52 *+ug/L 133 69 -129 5 30
Bromomethane 50.0 60.67 ug/L 121 28 -192 2 30
Carbon disulfide 50.0 45.67 ug/L 91 70 -130 1 30
Carbon tetrachloride 50.0 48.84 ug/L 98 70 -130 1 30
Chlorobenzene 50.0 53.90 ug/L 108 70 -130 0 30
Chlorobromomethane 50.0 54.55 ug/L 109 70 -130 4 30
Chlorodibromomethane 50.0 58.32 ug/L 117 70 -130 3 30
Chloroethane 50.0 55.12 ug/L 110 31 -213 9 30
Chloroform 50.0 50.09 ug/L 100 70 -130 3 30
Chloromethane 50.0 40.37 ug/L 81 59 -127 3 30
cis-1,2-Dichloroethene 50.0 47.24 ug/L 94 70 -130 2 30
cis-1,3-Dichloropropene 50.0 53.77 ug/L 108 70 -130 2 20
Dibromomethane 50.0 53.11 ug/L 106 70 -130 1 30
Dichlorobromomethane 50.0 51.10 ug/L 102 70 -130 1 30
Dichlorodifluoromethane 50.0 34.38 *-ug/L 69 70 -130 2 40
Ethylbenzene 50.0 52.51 ug/L 105 70 -130 2 20
Ethylene Dibromide 50.0 55.89 ug/L 112 70 -130 4 30
Hexachlorobutadiene 50.0 45.32 ug/L 91 70 -130 6 20
Hexane 50.0 38.50 ug/L 77 70 -130 3 30
Iodomethane 50.0 54.25 ug/L 108 52 -129 2 30
Isopropylbenzene 50.0 52.72 ug/L 105 70 -130 0 30
m,p-Xylene 50.0 51.38 ug/L 103 70 -130 1 30
Methyl tert-butyl ether 50.0 51.46 ug/L 103 70 -130 4 30
Methylene Chloride 50.0 51.30 ug/L 103 70 -130 1 30
Naphthalene 50.0 54.58 ug/L 109 57 -149 0 30
n-Butylbenzene 50.0 46.92 ug/L 94 70 -130 4 30
n-Heptane 50.0 35.21 ug/L 70 65 -120 3 30
N-Propylbenzene 50.0 52.65 ug/L 105 70 -130 2 30
o-Xylene 50.0 52.80 ug/L 106 70 -130 0 30
sec-Butylbenzene 50.0 53.37 ug/L 107 70 -130 1 30
Styrene 50.0 56.71 ug/L 113 70 -130 0 30
tert-Butylbenzene 50.0 53.07 ug/L 106 70 -130 1 30
Tetrachloroethene 50.0 51.09 ug/L 102 70 -130 1 30
Toluene 50.0 52.04 ug/L 104 70 -130 0 30
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-730068/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 730068
trans-1,2-Dichloroethene 50.0 52.47 ug/L 105 70 -130 0 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
trans-1,3-Dichloropropene 50.0 53.56 ug/L 107 70 -130 2 30
trans-1,4-Dichloro-2-butene 50.0 55.19 ug/L 110 67 -120 1 30
Trichloroethene 50.0 51.89 ug/L 104 70 -130 2 30
Trichlorofluoromethane 50.0 50.06 ug/L 100 63 -142 2 30
Vinyl acetate 100 199.4 *+ug/L 199 67 -135 4 30
Vinyl chloride 50.0 37.93 ug/L 76 66 -129 2 30
Xylenes, Total 100 104.2 ug/L 104 70 -130 1 30
1,2-Dichloroethane-d4 (Surr)60 -124
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr)70 -130
107Dibromofluoromethane (Surr)70 -130
109Toluene-d8 (Surr)70 -130
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-729541/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729586 Prep Batch: 729541
RL MDL
1,1'-Biphenyl ND 10.0 4.60 ug/L 07/07/22 11:34 07/07/22 18:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 3.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4,5-Trichlorophenol
ND 2.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4,6-Trichlorophenol
ND 3.7010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4-Dichlorophenol
ND 3.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4-Dimethylphenol
ND 16.050.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4-Dinitrophenol
ND 2.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,4-Dinitrotoluene
ND 2.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12,6-Dinitrotoluene
ND 4.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Chloronaphthalene
ND 3.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Chlorophenol
ND 4.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Methylnaphthalene
ND 1.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Methylphenol
ND 2.9050.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Nitroaniline
ND 3.9010.0 ug/L 07/07/22 11:34 07/07/22 18:50 12-Nitrophenol
ND 1.4010.0 ug/L 07/07/22 11:34 07/07/22 18:50 13 & 4 Methylphenol
ND 10.060.0 ug/L 07/07/22 11:34 07/07/22 18:50 13,3'-Dichlorobenzidine
ND 3.0050.0 ug/L 07/07/22 11:34 07/07/22 18:50 13-Nitroaniline
ND 5.3050.0 ug/L 07/07/22 11:34 07/07/22 18:50 14,6-Dinitro-2-methylphenol
ND 4.7010.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Bromophenyl phenyl ether
ND 2.5010.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Chloro-3-methylphenol
ND 1.0020.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Chloroaniline
ND 5.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Chlorophenyl phenyl ether
ND 3.0050.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Nitroaniline
ND 8.1050.0 ug/L 07/07/22 11:34 07/07/22 18:50 14-Nitrophenol
ND 4.4010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Acenaphthene
ND 3.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Acenaphthylene
ND 2.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Acetophenone
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-729541/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729586 Prep Batch: 729541
RL MDL
Anthracene ND 10.0 3.60 ug/L 07/07/22 11:34 07/07/22 18:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 2.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Atrazine
ND 4.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzaldehyde
ND 4.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzo[a]anthracene
ND 2.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzo[a]pyrene
ND 3.1010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzo[b]fluoranthene
ND 3.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzo[g,h,i]perylene
ND 2.9010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Benzo[k]fluoranthene
ND 3.1010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1bis (2-chloroisopropyl) ether
ND 1.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Bis(2-chloroethoxy)methane
ND 3.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Bis(2-chloroethyl)ether
ND 3.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Bis(2-ethylhexyl) phthalate
ND 2.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Butyl benzyl phthalate
ND 2.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Caprolactam
ND 1.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Carbazole
ND 3.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Chrysene
ND 3.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Dibenz(a,h)anthracene
ND 1.9010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Dibenzofuran
ND 2.2010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Diethyl phthalate
ND 2.1010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Dimethyl phthalate
ND 2.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Di-n-butyl phthalate
ND 2.8010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Di-n-octyl phthalate
ND 1.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Fluoranthene
ND 3.4010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Fluorene
ND 1.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Hexachlorobenzene
ND 4.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Hexachlorobutadiene
ND 3.5010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Hexachlorocyclopentadiene
ND 3.6010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Hexachloroethane
ND 4.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Indeno[1,2,3-cd]pyrene
ND 2.0010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Isophorone
ND 3.5010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Naphthalene
ND 3.5010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Nitrobenzene
ND 2.4010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1N-Nitrosodi-n-propylamine
ND 2.9010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1N-Nitrosodiphenylamine
ND 9.9050.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Pentachlorophenol
ND 4.3010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Phenanthrene
ND 1.5010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Phenol
ND 3.7010.0 ug/L 07/07/22 11:34 07/07/22 18:50 1Pyrene
2,4,6-Tribromophenol (Surr)106 30-130 07/07/22 18:50 1
MB MB
Surrogate
07/07/22 11:34
Dil FacPreparedAnalyzedQualifierLimits%Recovery
59 07/07/22 11:34 07/07/22 18:50 12-Fluorobiphenyl (Surr)25-130
33 07/07/22 11:34 07/07/22 18:50 12-Fluorophenol (Surr)10-130
60 07/07/22 11:34 07/07/22 18:50 1Nitrobenzene-d5 (Surr)30-130
22 07/07/22 11:34 07/07/22 18:50 1Phenol-d5 (Surr)10-130
77 07/07/22 11:34 07/07/22 18:50 1Terphenyl-d14 (Surr)35-131
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729541/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729586 Prep Batch: 729541
1,1'-Biphenyl 200 122.5 ug/L 61 26 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4,5-Trichlorophenol 200 159.2 ug/L 80 26 -130
2,4,6-Trichlorophenol 200 156.1 ug/L 78 28 -130
2,4-Dichlorophenol 200 148.4 ug/L 74 27 -130
2,4-Dimethylphenol 200 135.7 ug/L 68 26 -130
2,4-Dinitrophenol 400 383.2 ug/L 96 23 -130
2,4-Dinitrotoluene 200 175.4 ug/L 88 37 -130
2,6-Dinitrotoluene 200 164.0 ug/L 82 35 -130
2-Chloronaphthalene 200 128.4 ug/L 64 25 -130
2-Chlorophenol 200 118.8 ug/L 59 24 -130
2-Methylnaphthalene 200 126.6 ug/L 63 22 -130
2-Methylphenol 200 116.2 ug/L 58 21 -130
2-Nitroaniline 200 165.9 ug/L 83 36 -130
2-Nitrophenol 200 148.8 ug/L 74 27 -130
3 & 4 Methylphenol 200 113.8 ug/L 57 19 -130
3,3'-Dichlorobenzidine 200 203.6 ug/L 102 35 -130
3-Nitroaniline 200 149.9 ug/L 75 14 -130
4,6-Dinitro-2-methylphenol 400 379.1 ug/L 95 38 -130
4-Bromophenyl phenyl ether 200 164.3 ug/L 82 34 -130
4-Chloro-3-methylphenol 200 171.7 ug/L 86 28 -130
4-Chloroaniline 200 135.2 ug/L 68 10 -130
4-Chlorophenyl phenyl ether 200 153.3 ug/L 77 31 -130
4-Nitroaniline 200 152.0 ug/L 76 36 -130
4-Nitrophenol 400 130.1 ug/L 33 10 -130
Acenaphthene 200 119.9 ug/L 60 28 -130
Acenaphthylene 200 135.7 ug/L 68 31 -130
Acetophenone 200 127.5 ug/L 64 28 -130
Anthracene 200 140.0 ug/L 70 36 -130
Atrazine 200 150.6 ug/L 75 10 -142
Benzaldehyde 200 118.6 ug/L 59 22 -130
Benzo[a]anthracene 200 154.6 ug/L 77 34 -130
Benzo[a]pyrene 200 146.3 ug/L 73 36 -130
Benzo[b]fluoranthene 200 140.0 ug/L 70 35 -130
Benzo[g,h,i]perylene 200 152.7 ug/L 76 35 -130
Benzo[k]fluoranthene 200 138.7 ug/L 69 34 -130
bis (2-chloroisopropyl) ether 200 141.7 ug/L 71 33 -130
Bis(2-chloroethoxy)methane 200 130.4 ug/L 65 31 -130
Bis(2-chloroethyl)ether 200 129.7 ug/L 65 30 -130
Bis(2-ethylhexyl) phthalate 200 132.0 ug/L 66 33 -138
Butyl benzyl phthalate 200 150.1 ug/L 75 35 -135
Caprolactam 200 64.41 ug/L 32 10 -130
Carbazole 200 144.4 ug/L 72 36 -130
Chrysene 200 154.3 ug/L 77 33 -130
Dibenz(a,h)anthracene 200 154.3 ug/L 77 35 -130
Dibenzofuran 200 136.6 ug/L 68 31 -130
Diethyl phthalate 200 138.1 ug/L 69 36 -130
Dimethyl phthalate 200 148.3 ug/L 74 34 -130
Di-n-butyl phthalate 200 145.2 ug/L 73 35 -130
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729541/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729586 Prep Batch: 729541
Di-n-octyl phthalate 200 164.5 ug/L 82 34 -139
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Fluoranthene 200 160.9 ug/L 80 35 -130
Fluorene 200 138.4 ug/L 69 33 -130
Hexachlorobenzene 200 175.9 ug/L 88 30 -130
Hexachlorobutadiene 200 138.0 ug/L 69 12 -130
Hexachlorocyclopentadiene 200 139.9 ug/L 70 15 -130
Hexachloroethane 200 111.2 ug/L 56 12 -130
Indeno[1,2,3-cd]pyrene 200 192.6 ug/L 96 34 -130
Isophorone 200 144.6 ug/L 72 27 -130
Naphthalene 200 122.9 ug/L 61 19 -130
Nitrobenzene 200 134.7 ug/L 67 32 -130
N-Nitrosodi-n-propylamine 200 148.3 ug/L 74 33 -130
N-Nitrosodiphenylamine 200 134.5 ug/L 67 35 -130
Pentachlorophenol 400 355.6 ug/L 89 24 -130
Phenanthrene 200 134.1 ug/L 67 36 -130
Phenol 200 55.33 ug/L 28 10 -130
Pyrene 200 140.5 ug/L 70 33 -130
2,4,6-Tribromophenol (Surr)30 -130
Surrogate
114
LCS LCS
Qualifier Limits%Recovery
612-Fluorobiphenyl (Surr)25 -130
362-Fluorophenol (Surr)10 -130
65Nitrobenzene-d5 (Surr)30 -130
27Phenol-d5 (Surr)10 -130
81Terphenyl-d14 (Surr)35 -131
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-729181/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 729491 Prep Batch: 729181
RL MDL
Arsenic ND 0.00300 0.000860 mg/L 07/05/22 17:15 07/06/22 21:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0008900.00500 mg/L 07/05/22 17:15 07/06/22 21:41 1Barium
ND 0.00007800.000500 mg/L 07/05/22 17:15 07/06/22 21:41 1Cadmium
ND 0.002600.00500 mg/L 07/05/22 17:15 07/06/22 21:41 1Chromium
ND 0.0003400.00250 mg/L 07/05/22 17:15 07/06/22 21:41 1Lead
ND 0.001200.00250 mg/L 07/05/22 17:15 07/06/22 21:41 1Selenium
ND 0.0003900.00100 mg/L 07/05/22 17:15 07/06/22 21:41 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729181/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 729491 Prep Batch: 729181
Arsenic 0.100 0.1009 mg/L 101 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Barium 0.100 0.1002 mg/L 100 80 -120
Cadmium 0.0500 0.04968 mg/L 99 80 -120
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QC Sample Results
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729181/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 729491 Prep Batch: 729181
Chromium 0.100 0.1023 mg/L 102 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Lead 0.505 0.4952 mg/L 98 80 -120
Selenium 0.100 0.09967 mg/L 99 80 -120
Silver 0.0500 0.05094 mg/L 102 80 -120
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-729248/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729366 Prep Batch: 729248
RL MDL
Mercury ND 0.000200 0.0000800 mg/L 07/06/22 09:06 07/06/22 14:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-729248/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729366 Prep Batch: 729248
Mercury 0.00250 0.002272 mg/L 91 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Savannah
Page 39 of 70 7/12/2022
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QC Association Summary
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
GC/MS VOA
Analysis Batch: 729670
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-217736-1 GW-4 Total/NA
Water 8260D680-217736-3 GW-2 Total/NA
Water 8260D680-217736-4 GW-1 Total/NA
Water 8260D680-217736-5 Duplicate Total/NA
Water 8260DMB 680-729670/14 Method Blank Total/NA
Water 8260DLCS 680-729670/9 Lab Control Sample Total/NA
Water 8260DLCSD 680-729670/10 Lab Control Sample Dup Total/NA
Analysis Batch: 730068
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260D680-217736-2 GW-3 Total/NA
Water 8260DMB 680-730068/9 Method Blank Total/NA
Water 8260DLCS 680-730068/5 Lab Control Sample Total/NA
Water 8260DLCSD 680-730068/6 Lab Control Sample Dup Total/NA
GC/MS Semi VOA
Prep Batch: 729541
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C680-217736-1 GW-4 Total/NA
Water 3510C680-217736-2 GW-3 Total/NA
Water 3510C680-217736-3 GW-2 Total/NA
Water 3510C680-217736-4 GW-1 Total/NA
Water 3510C680-217736-5 Duplicate Total/NA
Water 3510CMB 680-729541/1-A Method Blank Total/NA
Water 3510CLCS 680-729541/2-A Lab Control Sample Total/NA
Analysis Batch: 729586
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270E 729541680-217736-1 GW-4 Total/NA
Water 8270E 729541680-217736-2 GW-3 Total/NA
Water 8270E 729541680-217736-3 GW-2 Total/NA
Water 8270E 729541680-217736-4 GW-1 Total/NA
Water 8270E 729541680-217736-5 Duplicate Total/NA
Water 8270E 729541MB 680-729541/1-A Method Blank Total/NA
Water 8270E 729541LCS 680-729541/2-A Lab Control Sample Total/NA
Metals
Prep Batch: 729181
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A680-217736-1 GW-4 Total Recoverable
Water 3005A680-217736-2 GW-3 Total Recoverable
Water 3005A680-217736-3 GW-2 Total Recoverable
Water 3005A680-217736-4 GW-1 Total Recoverable
Water 3005A680-217736-5 Duplicate Total Recoverable
Water 3005AMB 680-729181/1-A Method Blank Total Recoverable
Water 3005ALCS 680-729181/2-A Lab Control Sample Total Recoverable
Prep Batch: 729248
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A680-217736-1 GW-4 Total/NA
Eurofins Savannah
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QC Association Summary
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Metals (Continued)
Prep Batch: 729248 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A680-217736-2 GW-3 Total/NA
Water 7470A680-217736-3 GW-2 Total/NA
Water 7470A680-217736-4 GW-1 Total/NA
Water 7470A680-217736-5 Duplicate Total/NA
Water 7470AMB 680-729248/1-A Method Blank Total/NA
Water 7470ALCS 680-729248/2-A Lab Control Sample Total/NA
Analysis Batch: 729366
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 729248680-217736-1 GW-4 Total/NA
Water 7470A 729248680-217736-2 GW-3 Total/NA
Water 7470A 729248680-217736-3 GW-2 Total/NA
Water 7470A 729248680-217736-4 GW-1 Total/NA
Water 7470A 729248680-217736-5 Duplicate Total/NA
Water 7470A 729248MB 680-729248/1-A Method Blank Total/NA
Water 7470A 729248LCS 680-729248/2-A Lab Control Sample Total/NA
Analysis Batch: 729491
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 729181680-217736-1 GW-4 Total Recoverable
Water 6020B 729181680-217736-2 GW-3 Total Recoverable
Water 6020B 729181680-217736-3 GW-2 Total Recoverable
Water 6020B 729181680-217736-4 GW-1 Total Recoverable
Water 6020B 729181680-217736-5 Duplicate Total Recoverable
Water 6020B 729181MB 680-729181/1-A Method Blank Total Recoverable
Water 6020B 729181LCS 680-729181/2-A Lab Control Sample Total Recoverable
Eurofins Savannah
Page 41 of 70 7/12/2022
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217736-1
Project/Site: Greenhouse Project
Client Sample ID: GW-4 Lab Sample ID: 680-217736-1
Matrix: WaterDate Collected: 06/30/22 14:10
Date Received: 07/01/22 11:00
Analysis 8260D SMP07/08/22 19:241 TAL SAV729670
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 729541 07/07/22 11:34 MR TAL SAVTotal/NA 537 mL 1 mL
Analysis 8270E 1 729586 07/07/22 23:47 T1C TAL SAVTotal/NA
CMSNInstrument ID:
Prep 3005A 729181 07/05/22 17:15 JE TAL SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 729491 07/06/22 22:18 BWR TAL SAVTotal Recoverable
ICPMSDInstrument ID:
Prep 7470A 729248 07/06/22 09:06 JKL TAL SAVTotal/NA 50 mL 50 mL
Analysis 7470A 1 729366 07/06/22 14:59 JKL TAL SAVTotal/NA
QuickTrace2Instrument ID:
Client Sample ID: GW-3 Lab Sample ID: 680-217736-2
Matrix: WaterDate Collected: 06/30/22 15:15
Date Received: 07/01/22 11:00
Analysis 8260D P1C07/12/22 00:181 TAL SAV730068
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSU
Prep 3510C 729541 07/07/22 11:34 MR TAL SAVTotal/NA 544.8 mL 1 mL
Analysis 8270E 1 729586 07/08/22 00:11 T1C TAL SAVTotal/NA
CMSNInstrument ID:
Prep 3005A 729181 07/05/22 17:15 JE TAL SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 729491 07/06/22 22:20 BWR TAL SAVTotal Recoverable
ICPMSDInstrument ID:
Prep 7470A 729248 07/06/22 09:06 JKL TAL SAVTotal/NA 50 mL 50 mL
Analysis 7470A 1 729366 07/06/22 15:02 JKL TAL SAVTotal/NA
QuickTrace2Instrument ID:
Client Sample ID: GW-2 Lab Sample ID: 680-217736-3
Matrix: WaterDate Collected: 06/30/22 16:20
Date Received: 07/01/22 11:00
Analysis 8260D SMP07/08/22 21:0010 TAL SAV729670
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 729541 07/07/22 11:34 MR TAL SAVTotal/NA 515 mL 1 mL
Analysis 8270E 1 729586 07/08/22 00:36 T1C TAL SAVTotal/NA
CMSNInstrument ID:
Prep 3005A 729181 07/05/22 17:15 JE TAL SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 729491 07/06/22 22:23 BWR TAL SAVTotal Recoverable
ICPMSDInstrument ID:
Prep 7470A 729248 07/06/22 09:06 JKL TAL SAVTotal/NA 50 mL 50 mL
Analysis 7470A 1 729366 07/06/22 15:04 JKL TAL SAVTotal/NA
QuickTrace2Instrument ID:
Eurofins Savannah
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Lab Chronicle
Client: S&ME, Inc.Job ID: 680-217736-1
Project/Site: Greenhouse Project
Client Sample ID: GW-1 Lab Sample ID: 680-217736-4
Matrix: WaterDate Collected: 06/30/22 17:25
Date Received: 07/01/22 11:00
Analysis 8260D SMP07/08/22 21:195 TAL SAV729670
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 729541 07/07/22 11:34 MR TAL SAVTotal/NA 537.6 mL 1 mL
Analysis 8270E 1 729586 07/08/22 01:01 T1C TAL SAVTotal/NA
CMSNInstrument ID:
Prep 3005A 729181 07/05/22 17:15 JE TAL SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 729491 07/06/22 22:25 BWR TAL SAVTotal Recoverable
ICPMSDInstrument ID:
Prep 7470A 729248 07/06/22 09:06 JKL TAL SAVTotal/NA 50 mL 50 mL
Analysis 7470A 1 729366 07/06/22 15:07 JKL TAL SAVTotal/NA
QuickTrace2Instrument ID:
Client Sample ID: Duplicate Lab Sample ID: 680-217736-5
Matrix: WaterDate Collected: 06/30/22 00:00
Date Received: 07/01/22 11:00
Analysis 8260D SMP07/08/22 21:385 TAL SAV729670
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSC
Prep 3510C 729541 07/07/22 11:34 MR TAL SAVTotal/NA 542 mL 1 mL
Analysis 8270E 1 729586 07/08/22 01:25 T1C TAL SAVTotal/NA
CMSNInstrument ID:
Prep 3005A 729181 07/05/22 17:15 JE TAL SAVTotal Recoverable 50 mL 250 mL
Analysis 6020B 1 729491 07/06/22 22:28 BWR TAL SAVTotal Recoverable
ICPMSDInstrument ID:
Prep 7470A 729248 07/06/22 09:06 JKL TAL SAVTotal/NA 50 mL 50 mL
Analysis 7470A 1 729366 07/06/22 15:09 JKL TAL SAVTotal/NA
QuickTrace2Instrument ID:
Laboratory References:
Rochester = Rochester, NY, 1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: S&ME, Inc.Job ID: 680-217736-1
Project/Site: Greenhouse Project
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 269 12-31-22
Eurofins Savannah
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Method Summary
Job ID: 680-217736-1Client: S&ME, Inc.
Project/Site: Greenhouse Project
Method Method Description LaboratoryProtocol
SW8468260DVolatile Organic Compounds by GC/MS TAL SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)TAL SAV
SW8466020BMetals (ICP/MS)TAL SAV
SW8467470AMercury (CVAA)TAL SAV
NoneSubcontractGeneral Subcontract Method Rochester
SW8463005APreparation, Total Recoverable or Dissolved Metals TAL SAV
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)TAL SAV
SW8465030BPurge and Trap TAL SAV
SW8467470APreparation, Mercury TAL SAV
Protocol References:
None = None
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
Rochester = Rochester, NY, 1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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July 08, 2022 Service Request No:R2206035
John Andros
Eurofins ET NW (formerly TestAmerica)
Savannah, GA 31404
All testing was performed according to our laboratory’s quality assurance program and met the
requirements of the TNI standards except as noted in the case narrative report. Any testing not
included in the lab's accreditation is identified on a Non-Certified Analytes report. All results are
intended to be considered in their entirety. ALS Environmental is not responsible for use of less than
the complete report. Results apply only to the individual samples submitted to the lab for analysis, as
listed in the report. The measurement uncertainty of the results included in this report is within that
expected when using the prescribed method(s), and represented by Laboratory Control Sample
control limits. Any events, such as QC failures or Holding Time exceedances, which may add to the
uncertainty are explained in the report narrative or are flagged with qualifiers. The flags are explained
in the Report Qualifiers and Definitions page of this report.
For your reference, these analyses have been assigned our service request number
Enclosed are the results of the sample(s) submitted to our laboratory
Laboratory Results for:Greenhouse Project, Mangum St. Brownfield
Dear John,
July 01, 2022
R2206035.
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Nicole Mansen
Project Manager
dba ALS Environmental
ALS Group USA, Corp.
ADDRESS
FAXPHONE
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
[phone]+1 585 288 5380 |
Page 1 of 23Page 46 of 70 7/12/2022
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Narrative Documents
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 2 of 23Page 47 of 70 7/12/2022
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CASE NARRATIVE
Client:
Project:
Sample Matrix:
Service Request:
Date Received:
Eurofins ET NW (formerly TestAmerica)
Greenhouse Project, Mangum St. Brownfield
Water
R2206035
07/01/2022
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains
analytical results for samples for the Tier II level requested by the client.
Sample Receipt:
Five water samples were received for analysis at ALS Environmental on 07/01/2022. Any discrepancies upon initial sample
inspection are annotated on the sample receipt and preservation form included within this report. The samples were stored at
minimum in accordance with the analytical method requirements.
General Chemistry:
No significant anomalies were noted with this analysis.
1565 Jefferson Rd, Building 300, Rochester, NY 14623 | 585-288-5380 | www.alsglobal.com
Approved by Date 07/08/2022
Page 3 of 23Page 48 of 70 7/12/2022
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Sample Receipt Information
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 4 of 23Page 49 of 70 7/12/2022
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GW-4R2206035-001 6/30/2022 1410
GW-3R2206035-002 6/30/2022 1515
GW-2R2206035-003 6/30/2022 1620
GW-1R2206035-004 6/30/2022 1725
DuplicateR2206035-005 6/30/2022
Client:Eurofins ET NW (formerly TestAmerica)Service Request:R2206035
Project:Greenhouse Project, Mangum St. Brownfield/68027092
SAMPLE CROSS-REFERENCE
SAMPLE #CLIENT SAMPLE ID DATE TIME
Printed 7/8/2022 2:27:33 PM Sample Summary
Page 5 of 23Page 50 of 70 7/12/2022
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Eurofins TestAmerica,Savannah
5102 laRoche Avenue
Savannah,GA 31404
Phon.[phone] Fax [phone]
Chain of Custody Record ::~eurofins I Em1ronntent TestTnx
Afnl!l'lca
Samp\tlr:LftbPM:C8rIietT~No(a):cae No:
Cllenllnfonnallon James Waters John Andros
C1ilmIContllCl:Phone:E-Mttl:State of Orlgln:Pogo,
Shipping J ReceMng iohn.androg@et evrofinsus com North Carolina Page of
Compony.IPWS1D:Jobtl:
ALS Laboratory Group Anal sis Re UeSled
Address:DuctDltft RtqUe1I~:Preservation Codes:
1565 Jefferson Rd .•B1d9.300.St•.360 A.HCl M.HexztncCity.TAT Requested (days):0:B.NereH N."""Rochester
~
c.zn Acetllte Q-AlNa02
State.ZIp:D.NlIrlcAdd P.Na204S
NY 14623 Comp(lance Project •••••No E.NaHS04 0-ND2S03;;;F-McOH R-No2S203Phono,PO#:a G.Amchlor S.H2SO<0-••H-Aacof1llcAcId T •TSPDodecehyclrate
Ernell:0#:Z :>,...u.Aoetono~I !!!.~J-OIWnle1 V.MCAA
ProjoctNamlt:EurofrnsProjectiii:l ~g;.~K.EOTA W-pH4.5~l.EOA z.other(apecffy)Greenhouse Projed 66027092 {:••iSit,,:SSOWIiI:~~~u Othor.
Mangum St.Brownfield E 1;
~~~
Sample Matrix ~!(--.~'"E
Type n "~.-.u zsample(C""""""-.~;;
SamDle Identification SamDle Dnte TIme G-.reb)1TJon..••••_d::.'"{?SoeclallnstructionslNote:
Preservation Code:X I X
GW-4 6130/22 1410 G W X
GW-3 6130/22 1515 G W X
GW.2 6130/22 1620 G W X
GW.1 6130/22 1725 G W X
DUPLICATE 6130/22 NlA G W X
PossIble Hazard Identfflcatlon sad'e Disposal (A foo may be assassed "samples are retained longer than 1month)
oNon~8Z8rd 0 Flammable oSkin Irritant o Poison B CJ Unknown o Redioloolcsl Retum ToClient 0 DiSDOSSl8v Lsb 0 Archive For Months
Deliverable Requested:I,II,III,IV,Other (speclfy)Special InstrudlonsJOC RequIrements:
Empty Kit Relinquished by:IDa'.:ITlme:1M•••••of""'''''''''''
""."""""by/-J..A.A-r 11.-/J,DatefTJme:/130 Com R~~~"",/°7l7'J ..u q :l/i)I~~6/3,!/:;J -ETtif
Relinquishedby:Date1Tlrne:Com,.",RecelYedby.-DateITlmo'r......-nvR22060355 ,
1
Relinquishedby:DatelTIme:Com,.",Reootveclby.0"''''Euro1In.ETNW (formtl'ty TlltAm.rtCil IGrunhoullProJ.d,M.nllum at.Brownfl.ld
Custody Seals Intact:ICustodY Seal No.:CooterT~ratuTll(lI).C find OtherRelNlrb:l 11111111111111111111111111111111111111111111111111 I/J.Yes A No -~----"------Ver:"UI1101:lVI":IPage 6 of 23Page 51 of 70 7/12/2022
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--
Y N
Y N
Sample Bottle
Y'NYN
VELOCITY CLIENT
From:T
Y N
Y N
ups
Y N
Y N
Perchlorate samples have required headspace?
Did VOA vials,Alk,or Sulfide have sig~bubbles?
Where did the bottlesoriginate?ALSIROC
Soil VOA received as:Bulk Encore'
5a
Y N
Y N
COURIER:ALS
Y N
Y N
5b
6
Y N 7
Time:q:~G
Folder NumberJJ\}'\by:
Y
R2206035 5EUroflnlETNW(formerly T••tAm.rlcl'Gr••nhou ••Project,Mlngum st.8rownn,td
Cooler Receipt and Preservation Check Fo """1111"""""1""""11111"""'"11"'".I..••••~----..-/
~\"ins:;Jif-,...--
Were Custody seals on outside of cooler?
Observed Temp (0C)
Within 0-6°C?
If <O°C,were samples frozen?
2 Custody papers properly completed (ink,signed)
3 Did allbo 've in good condition (unbroke ?
4 Circle:et Icel Dry Ice Gel packs
Project/Client
Cooler received on
8.Temperature Readings
If out of Temperature,note packing/ice condition:Ice melted Poorly Packed (described below)Same Day Rule
&Client Approval to Run Samples:Standing Approval Client aware at drop-off Client notified by:_
All samples held in storage location:.~by .on 7J I '1.at LD ',to
5035 samples placed m storage locatIOn:by on at within 48 hours of sampling?Y N
OIS <;W-3j bur he bol"'1t£hu5 <::t lo(,ah~YJti~
tiS ~W-3.J\1;«1'.fJ.e bcNie \.tU7 tit joccr/'/C(J V1ti~
•
HPROD BULK
HTR FLDT
SUB HGFB
AlS ll3541
f3ZfGjS)by:
..m-.~~NO ~12.Were 5035 vials acceptable (no extra labels,not leaking)?YES NO <N/A-J
13.Air Samoles:Cassettes I Tubes Intact YIN with MS YIN Canisters Pressurized Tedlar<iilBa",Int1ated~
pH Lot oftest Reagent Preserved?Lot Received Exp Sample ID Vol.Lot Added Final
paper Ves No Adjusted Added pH
>12 NaOH
$2 HNO,
$2 H2SO4
<4 NaHS04
5-9 Fo,608pest NlFNotiry fo,3day
Residual ForCN,If +.contact PM to add
Chlorine Phenol,625,N",S,O,(625.608.
(-)6080est 522 eN),ascorbic (phenol).
Na2S20,
ZnAcetate --••VOAs and 1664 Not to be tested before analysis.
HCI ••••Otherwise,all bottles orall samples with chemical preservatives
are checked (not iust reoresentativesl.C {-(va-BMU%Bottle lotnumbers._
Explain all Discrepancies!Other Comments:J.LOu 0001:'C06 \Nfnt£~~5(;-3
Loc 003 t C06 \rJY,-r-kt10+5G-J
Cooler BreakdownlPreservation Cheek ••:Date:7 Time:
---'9.Were all bottle labels complete (i.e.analysis,preservation,etc.)?
10.Did all bottle labels and tags agree with custody papers?
11 Were correct containers used for the tests indicated?
Labels secondary reviewed by:
PC Secondary Review:_
P:\INTRANET\QAQC\Forms Controlled\Cooler Receiptrl9.doc
'significant air bubbles:VOA >5-6 mm :WC >I in.diameter
03/021202\
Page 7 of 23Page 52 of 70 7/12/2022
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Miscellaneous Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 8 of 23Page 53 of 70 7/12/2022
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RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\QUALIF_routine rev 6.doc 9/30/21
REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
J Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
DoD: concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
“Notes” column of the Form I, this qualifier
denotes analysis was performed out of
Holding Time.
H Analysis was performed out of hold time for
tests that have an “immediate” hold time
criteria.
# Spike was diluted out.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post-Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% difference between the two
GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesticide/Aroclor is not
confirmed (≥100% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value derived
from a study designed to provide the lowest
concentration that will be detected 99% of the time.
Values between the MDL and MRL are estimated
(see J qualifier).
LOD Limit of Detection. A value at or above the MDL
which has been verified to be detectable.
ND Non-Detect. Analyte was not detected at the
concentration listed. Same as U qualifier.

Rochester Lab ID # for State Accreditations¹

¹ Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements of the current NELAP/TNI standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited. For a specific list of accredited analytes, contact the laboratory or go to
https://www.alsglobal.com/locations/americas/north-america/usa/new-york/rochester-environmental

NELAP States
Florida ID # E87674
New Hampshire ID # 2941
New York ID # 10145
Pennsylvania ID# 68-786
Virginia #460167
Non-NELAP States
Connecticut ID #PH0556
Delaware Approved
Maine ID #NY01587
North Carolina #36701
North Carolina #676
Rhode Island LAO00333
Page 9 of 23Page 54 of 70 7/12/2022
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ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources Board
CAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental Quality
DHS Department of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation Program
GC Gas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LUFT Leaking Underground Fuel Tank
M Modified
MCL Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable Number
MRL Method Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not Detected
NIOSH National Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum Hydrocarbons
tr Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
Acronyms
ALS Laboratory Group
Page 10 of 23Page 55 of 70 7/12/2022
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07/1/22Date Received:
Date Collected:
WaterSample Matrix:
06/30/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-4Sample Name:
Lab Code:R2206035-001
7199 KWONG
07/1/22Date Received:
Date Collected:
WaterSample Matrix:
06/30/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-3Sample Name:
Lab Code:R2206035-002
7199 KWONG
07/1/22Date Received:
Date Collected:
WaterSample Matrix:
06/30/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-2Sample Name:
Lab Code:R2206035-003
7199 KWONG
07/1/22Date Received:
Date Collected:
WaterSample Matrix:
06/30/22
Extracted/Digested ByAnalysis Method Analyzed By
GW-1Sample Name:
Lab Code:R2206035-004
7199 KWONG
07/1/22Date Received:
Date Collected:
WaterSample Matrix:
06/30/22
Extracted/Digested ByAnalysis Method Analyzed By
DuplicateSample Name:
Lab Code:R2206035-005
7199 KWONG
Analyst Summary report
ALS Group USA, Corp.
dba ALS Environmental
Client:Service Request:
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Project:
R2206035
Printed 7/8/2022 2:27:34 PM 22-0000632555 rev 00Superset Reference:
Page 11 of 23Page 56 of 70 7/12/2022
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RIGHT SOLUTIONS | RIGHT PARTNER
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev 2.doc 12/20/19

INORGANIC PREPARATION METHODS
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.

Water/Liquid Matrix Solid/Soil/Non-Aqueous Matrix

Analytical Method Preparation Method Analytical Method Preparation
Method
200.7 200.2 6010C 3050B
200.8 200.2 6020A 3050B
6010C 3005A/3010A 6010C TCLP (1311)
extract
3005A/3010A
6020A ILM05.3 6010 SPLP (1312) extract 3005A/3010A
9034 Sulfide Acid Soluble 9030B 7199 3060A
SM 4500-CN-E Residual
Cyanide
SM 4500-CN-G 300.0 Anions/ 350.1/
353.2/ SM 2320B/ SM
5210B/ 9056A Anions
DI extraction
SM 4500-CN-E WAD
Cyanide
SM 4500-CN-I For analytical methods not listed, the preparation
method is the same as the analytical method reference.

Page 12 of 23Page 57 of 70 7/12/2022
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Sample Results
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 13 of 23Page 58 of 70 7/12/2022
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General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 14 of 23Page 59 of 70 7/12/2022
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Client:
07/01/22 09:40
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/30/22 14:10
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:GW-4
Lab Code:R2206035-001
Chromium, Hexavalent 07/01/22 11:3310.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:34 PM 22-0000632555 rev 00Superset Reference:
Page 15 of 23Page 60 of 70 7/12/2022
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Client:
07/01/22 09:40
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/30/22 15:15
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:GW-3
Lab Code:R2206035-002
Chromium, Hexavalent 07/01/22 11:4810.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:34 PM 22-0000632555 rev 00Superset Reference:
Page 16 of 23Page 61 of 70 7/12/2022
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Client:
07/01/22 09:40
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/30/22 16:20
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:GW-2
Lab Code:R2206035-003
Chromium, Hexavalent 07/01/22 12:0310.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:34 PM 22-0000632555 rev 00Superset Reference:
Page 17 of 23Page 62 of 70 7/12/2022
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Client:
07/01/22 09:40
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/30/22 17:25
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:GW-1
Lab Code:R2206035-004
Chromium, Hexavalent 07/01/22 12:1910.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:35 PM 22-0000632555 rev 00Superset Reference:
Page 18 of 23Page 63 of 70 7/12/2022
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Client:
07/01/22 09:40
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:06/30/22
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:Duplicate
Lab Code:R2206035-005
Chromium, Hexavalent 07/01/22 12:3410.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:35 PM 22-0000632555 rev 00Superset Reference:
Page 19 of 23Page 64 of 70 7/12/2022
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QC Summary Forms
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 20 of 23Page 65 of 70 7/12/2022
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General Chemistry
ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
Page 21 of 23Page 66 of 70 7/12/2022
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Client:
NA
R2206035
Date Received:
Date Collected:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name QDate AnalyzedDil.MDLMRLResultUnits
Sample Name:Method Blank
Lab Code:R2206035-MB
Chromium, Hexavalent 07/01/22 08:4710.0020.010 UND7199 mg/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 7/8/2022 2:27:35 PM 22-0000632555 rev 00Superset Reference:
Page 22 of 23Page 67 of 70 7/12/2022
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Analyte Name
R2206035
Date Analyzed:
Service Request:
Water
Greenhouse Project, Mangum St. Brownfield/68027092
Eurofins ET NW (formerly TestAmerica)
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
General Chemistry Parameters
NA
mg/L
Basis:
Units:
Lab Control Sample
R2206035-LCS
07/01/22
Spike AmountResult % Rec % Rec LimitsAnalytical Method
dba ALS EnvironmentalALS Group USA, Corp.
QA/QC Report
Chromium, Hexavalent 85-115101 0.2000.201 7199
22-0000632555 rev 00Superset Reference:Printed 7/8/2022 2:27:35 PM
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Page 69 of 70 7/12/2022
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Login Sample Receipt Checklist
Client: S&ME, Inc.Job Number: 680-217736-1
Login Number: 217736
Question Answer Comment
Creator: Watters, David
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
Page 70 of 70 7/12/2022
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Appendix VI – NCDEQ Risk Calculator Output

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Mangum Street, Durham, NC
North Carolina Department of Environmental Quality
Risk Calculator
N. MANGUM ST. PROERTIES II
601 SOUTH MANGUM STREET
BROWNFIELDS
20593-21-032
July 2022
May 2022 EPA RSL Table
10/5/2022
Prepared By:Ben Kelly, S&ME, Inc.
Tom Raymond, S&ME, Inc. 11/3/2022
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
0.31 67-64-1 Acetone mg/kg
4.26 7440-38-2 Arsenic, Inorganic mg/kg
215 7440-39-3 Barium mg/kg
3.38 71-43-2 Benzene mg/kg
1.17 104-51-8 Butylbenzene, n-mg/kg
0.00467 135-98-8 Butylbenzene, sec-mg/kg
0.105 7440-43-9 Cadmium (Diet)mg/kg
215 16065-83-1 Chromium(III), Insoluble Salts mg/kg
3.45 18540-29-9 Chromium(VI)mg/kg
0.389 98-82-8 Cumene mg/kg
5.35 100-41-4 Ethylbenzene mg/kg
11.1 142-82-5 Heptane, N-mg/kg
13.9 110-54-3 Hexane, N-mg/kg
63.2 7439-92-1 ~Lead and Compounds mg/kg
0.149 7439-97-6 ~Mercury (elemental)mg/kg
0.176 108-95-2 Phenol mg/kg
0.0901 117-81-7 ~Bis(2-ethylhexyl)phthalate mg/kg
0.0405 56-55-3 ~Benz[a]anthracene mg/kg
0.0484 205-99-2 ~Benzo[b]fluoranthene mg/kg
0.0336 218-01-9 ~Chrysene mg/kg
0.0616 206-44-0 ~Fluoranthene mg/kg
2.42 91-57-6 ~Methylnaphthalene, 2-mg/kg
3.49 91-20-3 ~Naphthalene mg/kg
0.0595 129-00-0 ~Pyrene mg/kg
1.43 103-65-1 Propyl benzene mg/kg
3.97 7782-49-2 Selenium mg/kg
0.0805 7440-22-4 Silver mg/kg
9.86 95-63-6 Trimethylbenzene, 1,2,4-mg/kg
3.5 108-67-8 Trimethylbenzene, 1,3,5-mg/kg
21.1 1330-20-7 Xylenes mg/kg
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Description of Exposure Point Concentration Selection:
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(ug/L)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.511 7440-39-3 Barium ug/L GW-DUP
284 71-43-2 Benzene ug/L GW-2
9.78 104-51-8 Butylbenzene, n-ug/L
0.000115 7440-43-9 Cadmium (Diet)ug/L GW-DUP
0.867 67-66-3 Chloroform ug/L
18.7 98-82-8 Cumene ug/L
6.49 107-06-2 Dichloroethane, 1,2-ug/L
246 108-20-3 Diisopropyl Ether ug/L
4.43 142-82-5 Heptane, N-ug/L
51.6 110-54-3 Hexane, N-ug/L
0.0058 7439-92-1 ~Lead and Compounds ug/L
17.6 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/L
57.9 91-57-6 ~Methylnaphthalene, 2-ug/L
388 91-20-3 ~Naphthalene ug/L
35.6 103-65-1 Propyl benzene ug/L
13.5 100-42-5 Styrene ug/L
36.2 108-88-3 Toluene ug/L
81.1 95-63-6 Trimethylbenzene, 1,2,4-ug/L
12.4 108-67-8 Trimethylbenzene, 1,3,5-ug/L
119 1330-20-7 Xylenes ug/L
Input Form 2B
Groundwater Exposure Point Concentration Table
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/m3)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
270 67-64-1 Acetone ug/m3 SG-5
54 71-43-2 Benzene ug/m3 SG-DUP
61 75-15-0 Carbon Disulfide ug/m3 SG-6
19 98-82-8 Cumene ug/m3 SG-2
2900 110-82-7 Cyclohexane ug/m3 SG-2
110 100-41-4 Ethylbenzene ug/m3 SG-1
170 142-82-5 Heptane, N-ug/m3 SG-2
2200 110-54-3 Hexane, N-ug/m3 SG-2
36 67-63-0 Isopropanol ug/m3 SG-1
20 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 SG-1
29 91-20-3 ~Naphthalene ug/m3 SG-1
61 103-65-1 Propyl benzene ug/m3 SG-2
31 127-18-4 Tetrachloroethylene ug/m3 SG-3
97 108-88-3 Toluene ug/m3 SG-2
28 79-01-6 Trichloroethylene ug/m3 SG-2
130 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 SG-1
100 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 SG-2
99 1330-20-7 Xylenes ug/m3 SG-1
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 2.3E-05 8.3E-01 NO
Groundwater Use*4.0E-03 7.8E+01 YES
Soil 3.2E-06 8.1E-02 NO
Groundwater Use*1.0E-03 1.8E+01 YES
Construction Worker Soil 1.4E-06 2.3E-01 NO
Soil 1.1E-05 3.9E-01 NO
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 2.7E-04 1.1E+01 YES
Soil Gas to Indoor Air 2.0E-05 1.0E+00 YES
Indoor Air 0.0E+00 0.0E+00 NO
Groundwater to Indoor Air 6.1E-05 2.7E+00 YES
Soil Gas to Indoor Air 1.5E-06 8.1E-02 NO
Indoor Air 0.0E+00 0.0E+00 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC
2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Sitewide Risk Output Form 1B
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
Receptor Pathway
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Check box to include in site-wide risk calculations
Carcinogenic Risk Hazard Index
Soil 2.3E-05 8.3E-01 NM NM
Groundwater Use*4.0E-03 7.8E+01 NM NM
Soil 3.2E-06 8.1E-02 NM NM
Groundwater Use*1.0E-03 1.8E+01 NM NM
Construction Worker Soil 1.4E-06 2.3E-01
Soil 1.1E-05 3.9E-01
Surface Water Use*NM NM
Groundwater to Indoor Air 2.7E-04 1.1E+01 NM NM
Soil Gas to Indoor Air NM NM NM NM
Indoor Air NM NM NM NM
Groundwater to Indoor Air 6.1E-05 2.7E+00 NM NM
Soil Gas to Indoor Air NM NM NM NM
Indoor Air NM NM NM NM
4.3E-03 9.0E+01 0.0E+00 0.0E+00 1.1E-03 2.1E+01 0.0E+00 0.0E+00 1.4E-06 2.3E-01 1.1E-05 3.9E-01
3. NM = Not Modeled
4. NC = Pathway not calculated
Resident
Non-Residential Worker
Recreator/Trespasser
VAPOR INTRUSION CALCULATORS
DIRECT CONTACT SOIL AND WATER CALCULATORS
Non-Residential Worker - Future Scenario Construction Worker Recreator/TrespasserResident - Current Scenario Resident - Future Scenario Non-Residential Worker - Current Scenario
TOTAL SITEWIDE RISK FOR EACH RECEPTOR
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure.
Resident
Non-Residential Worker
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient67-64-1 Acetone 0.31 0.31 0.31 4.4E-06 4.4E-06
7440-38-2 Arsenic, Inorganic 4.26 4.26 4.26 5.5E-06 7.8E-07 1.1E-10 6.3E-06 1.1E-01 1.3E-02 4.6E-06 1.2E-01
7440-39-3 Barium 215 215 215 1.4E-02 7.0E-06 1.4E-0271-43-2 Benzene 3.38 3.38 3.38 2.7E-07 2.5E-06 2.8E-06 1.1E-02 2.9E-02 3.9E-02
104-51-8 Butylbenzene, n-1.17 1.17 1.17 3.0E-04 3.0E-04
135-98-8 Butylbenzene, sec-0.00467 0.00467 0.00467 6.0E-07 6.0E-07
7440-43-9 Cadmium (Diet)0.105 0.105 0.105 1.1E-12 1.1E-12 1.3E-02 1.3E-03 1.7E-07 1.5E-02
16065-83-1 Chromium(III), Insoluble Salts 215 215 215 1.8E-03 1.8E-03
18540-29-9 Chromium(VI)3.45 3.45 3.45 1.1E-05 4.8E-09 1.1E-05 1.5E-02 5.6E-07 1.5E-02
98-82-8 Cumene 0.389 0.389 0.389 5.0E-05 1.4E-04 1.9E-04
100-41-4 Ethylbenzene 5.35 5.35 5.35 8.5E-08 7.9E-07 8.7E-07 1.4E-03 8.5E-04 2.2E-03142-82-5 Heptane, N-11.1 11.1 11.1 4.7E-01 8.5E-03 4.8E-01
110-54-3 Hexane, N-13.9 13.9 13.9 6.1E-03 6.1E-03
7439-92-1 ~Lead and Compounds 63.2 63.2 63.2 <SL**<SL**<SL**7439-97-6 ~Mercury (elemental)0.149 0.149 0.149 1.3E-02 1.3E-02
108-95-2 Phenol 0.176 0.176 0.176 7.5E-06 1.8E-06 1.4E-11 9.3E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0901 0.0901 0.0901 1.8E-09 5.1E-10 1.3E-15 2.3E-09 5.8E-05 1.4E-05 7.1E-0556-55-3 ~Benz[a]anthracene 0.0405 0.0405 0.0405 2.6E-08 8.8E-09 5.1E-10 3.6E-08
205-99-2 ~Benzo[b]fluoranthene 0.0484 0.0484 0.0484 3.2E-08 1.1E-08 4.8E-14 4.2E-08
218-01-9 ~Chrysene 0.0336 0.0336 0.0336 2.2E-10 7.3E-11 3.4E-16 2.9E-10
206-44-0 ~Fluoranthene 0.0616 0.0616 0.0616 2.0E-05 6.1E-06 2.6E-05
91-57-6 ~Methylnaphthalene, 2-2.42 2.42 2.42 7.7E-03 2.4E-03 1.0E-02
91-20-3 ~Naphthalene 3.49 3.49 3.49 6.0E-07 2.2E-07 8.6E-07 1.7E-06 2.2E-03 6.9E-04 2.3E-02 2.6E-02
129-00-0 ~Pyrene 0.0595 0.0595 0.0595 2.5E-05 7.8E-06 3.3E-05
103-65-1 Propyl benzene 1.43 1.43 1.43 1.8E-04 1.8E-04 3.7E-047782-49-2 Selenium 3.97 3.97 3.97 1.0E-02 3.2E-09 1.0E-02
7440-22-4 Silver 0.0805 0.0805 0.0805 2.1E-04 2.1E-04
95-63-6 Trimethylbenzene, 1,2,4-9.86 9.86 9.86 1.3E-02 1.9E-02 3.1E-02108-67-8 Trimethylbenzene, 1,3,5-3.5 3.5 3.5 4.5E-03 7.9E-03 1.2E-02
1330-20-7 Xylenes 21.1 21.1 21.1 1.3E-03 3.3E-02 3.4E-02
Cumulative:2.3E-05 8.3E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Groundwater Use
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to inhalation associated with tapwater use, not inhalation associated with vapor intrusion from subsurface groundwater sources.
CAS #Chemical Name:
Ingestion
Concentration
(ug/L)
Dermal
Concentration
(ug/L)
Inhalation
Concentration
(ug/L)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-39-3 Barium 0.511 0.511 0.511 1.3E-04 8.0E-06 1.4E-04
71-43-2 Benzene 284 284 284 2.0E-04 2.9E-05 3.9E-04 6.2E-04 3.5E+00 4.7E-01 4.5E+00 8.5E+00104-51-8 Butylbenzene, n-9.78 9.78 9.78 9.8E-03 9.8E-03
7440-43-9 Cadmium (Diet)0.000115 0.000115 0.000115 5.7E-05 5.7E-05
67-66-3 Chloroform 0.867 0.867 0.867 3.4E-07 3.0E-08 3.6E-06 3.9E-06 4.3E-03 3.4E-04 4.2E-03 8.9E-0398-82-8 Cumene 18.7 18.7 18.7 9.3E-03 9.8E-03 2.2E-02 4.1E-02
107-06-2 Dichloroethane, 1,2-6.49 6.49 6.49 7.6E-06 3.5E-07 3.0E-05 3.8E-05 5.4E-02 2.3E-03 4.4E-01 5.0E-01108-20-3 Diisopropyl Ether 246 246 246 1.7E-01 1.7E-01
142-82-5 Heptane, N-4.43 4.43 4.43 7.4E-01 5.3E-03 7.4E-01
110-54-3 Hexane, N-51.6 51.6 51.6 3.5E-02 3.5E-02
7439-92-1 ~Lead and Compounds 0.0058 0.0058 0.0058 <SL**<SL**<SL**
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)17.6 17.6 17.6 2.8E-03 2.8E-03
91-57-6 ~Methylnaphthalene, 2-57.9 57.9 57.9 7.2E-01 8.9E-01 1.6E+00
91-20-3 ~Naphthalene 388 388 388 6.0E-04 3.7E-04 2.3E-03 3.3E-03 9.7E-01 5.5E-01 6.2E+01 6.4E+01
103-65-1 Propyl benzene 35.6 35.6 35.6 1.8E-02 1.9E-02 1.7E-02 5.4E-02100-42-5 Styrene 13.5 13.5 13.5 3.4E-03 1.3E-03 6.5E-03 1.1E-02
108-88-3 Toluene 36.2 36.2 36.2 2.3E-02 6.8E-03 3.5E-03 3.3E-02
95-63-6 Trimethylbenzene, 1,2,4-81.1 81.1 81.1 4.0E-01 4.0E-01 6.5E-01 1.5E+00
108-67-8 Trimethylbenzene, 1,3,5-12.4 12.4 12.4 6.2E-02 4.5E-02 9.9E-02 2.1E-01
1330-20-7 Xylenes 119 119 119 3.0E-02 1.6E-02 5.7E-01 6.2E-01
Cumulative:4.0E-03 7.8E+01
Output Form 2B
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA Action Level of
15 μg/L.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Groundwater Use
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to inhalation associated with tapwater use, not inhalation associated with vapor intrusion from subsurface groundwater sources.
CAS #Chemical Name:Ingestion Concentration
(ug/L)
Dermal Concentration
(ug/L)
Inhalation Concentration
(ug/L)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-39-3 Barium 0.511 0.511 0.511 1.8E-05 4.1E-06 2.2E-05
71-43-2 Benzene 284 284 284 4.0E-05 1.7E-05 9.0E-05 1.5E-04 5.0E-01 2.2E-01 1.1E+00 1.8E+00
104-51-8 Butylbenzene, n-9.78 9.78 9.78 1.4E-03 1.4E-03
7440-43-9 Cadmium (Diet)0.000115 0.000115 0.000115 8.2E-06 8.2E-06
67-66-3 Chloroform 0.867 0.867 0.867 6.8E-08 1.7E-08 8.1E-07 9.0E-07 6.2E-04 1.6E-04 1.0E-03 1.8E-03
98-82-8 Cumene 18.7 18.7 18.7 1.3E-03 4.5E-03 5.3E-03 1.1E-02
107-06-2 Dichloroethane, 1,2-6.49 6.49 6.49 1.5E-06 2.1E-07 6.9E-06 8.6E-06 7.7E-03 1.1E-03 1.1E-01 1.1E-01
108-20-3 Diisopropyl Ether 246 246 246 4.0E-02 4.0E-02
142-82-5 Heptane, N-4.43 4.43 4.43 1.0E-01 1.3E-03 1.1E-01
110-54-3 Hexane, N-51.6 51.6 51.6 8.4E-03 8.4E-03
7439-92-1 ~Lead and Compounds 0.0058 0.0058 0.0058 <SL**<SL**<SL**
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)17.6 17.6 17.6 6.7E-04 6.7E-04
91-57-6 ~Methylnaphthalene, 2-57.9 57.9 57.9 1.0E-01 4.1E-01 5.1E-01
91-20-3 ~Naphthalene 388 388 388 1.2E-04 2.2E-04 5.4E-04 8.7E-04 1.4E-01 2.6E-01 1.5E+01 1.5E+01
103-65-1 Propyl benzene 35.6 35.6 35.6 2.5E-03 9.0E-03 4.1E-03 1.6E-02
100-42-5 Styrene 13.5 13.5 13.5 4.8E-04 6.1E-04 1.5E-03 2.6E-03
108-88-3 Toluene 36.2 36.2 36.2 3.2E-03 3.1E-03 8.3E-04 7.2E-03
95-63-6 Trimethylbenzene, 1,2,4-81.1 81.1 81.1 5.8E-02 1.9E-01 1.5E-01 4.0E-01
108-67-8 Trimethylbenzene, 1,3,5-12.4 12.4 12.4 8.8E-03 2.1E-02 2.4E-02 5.3E-02
1330-20-7 Xylenes 119 119 119 4.2E-03 7.3E-03 1.4E-01 1.5E-01
Cumulative:1.0E-03 1.8E+01
Output Form 2D
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA Action Level of 15 μg/L.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.31 0.31 0.31 2.9E-07 2.9E-07
7440-38-2 Arsenic, Inorganic 4.26 4.26 4.26 1.2E-06 2.5E-07 2.5E-11 1.4E-06 7.3E-03 1.5E-03 1.1E-06 8.8E-03
7440-39-3 Barium 215 215 215 9.2E-04 1.7E-06 9.2E-04
71-43-2 Benzene 3.38 3.38 3.38 5.7E-08 5.7E-07 6.3E-07 7.2E-04 6.8E-03 7.6E-03
104-51-8 Butylbenzene, n-1.17 1.17 1.17 2.0E-05 2.0E-05
135-98-8 Butylbenzene, sec-0.00467 0.00467 0.00467 4.0E-08 4.0E-08
7440-43-9 Cadmium (Diet)0.105 0.105 0.105 2.6E-13 2.6E-13 9.0E-04 1.5E-04 4.0E-08 1.1E-03
16065-83-1 Chromium(III), Insoluble Salts 215 215 215 1.2E-04 1.2E-04
18540-29-9 Chromium(VI)3.45 3.45 3.45 5.3E-07 4.0E-10 5.3E-07 9.8E-04 1.3E-07 9.8E-04
98-82-8 Cumene 0.389 0.389 0.389 3.3E-06 3.4E-05 3.7E-05
100-41-4 Ethylbenzene 5.35 5.35 5.35 1.8E-08 1.8E-07 2.0E-07 9.2E-05 2.0E-04 2.9E-04
142-82-5 Heptane, N-11.1 11.1 11.1 3.2E-02 2.0E-03 3.4E-02
110-54-3 Hexane, N-13.9 13.9 13.9 1.4E-03 1.4E-03
7439-92-1 ~Lead and Compounds 63.2 63.2 63.2 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.149 0.149 0.149 3.1E-03 3.1E-03
108-95-2 Phenol 0.176 0.176 0.176 5.0E-07 2.1E-07 3.4E-12 7.1E-07
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0901 0.0901 0.0901 3.9E-10 1.6E-10 3.0E-16 5.5E-10 3.9E-06 1.6E-06 5.5E-06
56-55-3 ~Benz[a]anthracene 0.0405 0.0405 0.0405 1.2E-09 6.8E-10 4.2E-11 2.0E-09
205-99-2 ~Benzo[b]fluoranthene 0.0484 0.0484 0.0484 1.5E-09 8.1E-10 4.0E-15 2.3E-09
218-01-9 ~Chrysene 0.0336 0.0336 0.0336 1.0E-11 5.7E-12 2.8E-17 1.6E-11
206-44-0 ~Fluoranthene 0.0616 0.0616 0.0616 1.3E-06 7.3E-07 2.0E-06
91-57-6 ~Methylnaphthalene, 2-2.42 2.42 2.42 5.2E-04 2.8E-04 8.0E-04
91-20-3 ~Naphthalene 3.49 3.49 3.49 1.3E-07 7.0E-08 2.0E-07 3.9E-07 1.5E-04 8.2E-05 5.4E-03 5.6E-03
129-00-0 ~Pyrene 0.0595 0.0595 0.0595 1.7E-06 9.3E-07 2.6E-06
103-65-1 Propyl benzene 1.43 1.43 1.43 1.2E-05 4.4E-05 5.6E-05
7782-49-2 Selenium 3.97 3.97 3.97 6.8E-04 7.6E-10 6.8E-04
7440-22-4 Silver 0.0805 0.0805 0.0805 1.4E-05 1.4E-05
95-63-6 Trimethylbenzene, 1,2,4-9.86 9.86 9.86 8.4E-04 4.5E-03 5.3E-03
108-67-8 Trimethylbenzene, 1,3,5-3.5 3.5 3.5 3.0E-04 1.9E-03 2.2E-03
1330-20-7 Xylenes 21.1 21.1 21.1 9.0E-05 7.9E-03 8.0E-03
Cumulative:3.2E-06 8.1E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.31 0.31 0.31 9.1E-07 9.1E-07
7440-38-2 Arsenic, Inorganic 4.26 4.26 4.26 1.5E-07 2.5E-08 5.6E-08 2.4E-07 2.5E-02 4.0E-03 6.4E-02 9.3E-02
7440-39-3 Barium 215 215 215 3.2E-03 9.7E-03 1.3E-02
71-43-2 Benzene 3.38 3.38 3.38 7.5E-09 1.1E-07 1.2E-07 1.0E-03 1.3E-02 1.4E-02
104-51-8 Butylbenzene, n-1.17 1.17 1.17 3.4E-05 3.4E-05
135-98-8 Butylbenzene, sec-0.00467 0.00467 0.00467 1.4E-07 1.4E-07
7440-43-9 Cadmium (Diet)0.105 0.105 0.105 5.8E-10 5.8E-10 6.2E-04 7.9E-05 2.4E-03 3.1E-03
16065-83-1 Chromium(III), Insoluble Salts 215 215 215 4.2E-04 9.7E-03 1.0E-02
18540-29-9 Chromium(VI)3.45 3.45 3.45 7.0E-08 8.9E-07 9.6E-07 2.0E-03 2.6E-03 4.6E-03
98-82-8 Cumene 0.389 0.389 0.389 2.9E-06 7.4E-04 7.4E-04
100-41-4 Ethylbenzene 5.35 5.35 5.35 2.4E-09 3.4E-08 3.7E-08 3.2E-04 1.1E-04 4.3E-04
142-82-5 Heptane, N-11.1 11.1 11.1 1.1E-02 3.3E-03 1.4E-02
110-54-3 Hexane, N-13.9 13.9 13.9 1.4E-04 8.9E-03 9.1E-03
7439-92-1 ~Lead and Compounds 63.2 63.2 63.2 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.149 0.149 0.149 1.5E-02 1.5E-02
108-95-2 Phenol 0.176 0.176 0.176 8.6E-07 2.8E-07 2.0E-07 1.3E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0901 0.0901 0.0901 5.1E-11 1.6E-11 6.7E-13 6.8E-11 1.3E-05 4.3E-06 1.8E-05
56-55-3 ~Benz[a]anthracene 0.0405 0.0405 0.0405 1.6E-10 6.8E-11 1.5E-11 2.5E-10
205-99-2 ~Benzo[b]fluoranthene 0.0484 0.0484 0.0484 2.0E-10 8.1E-11 8.9E-12 2.9E-10
218-01-9 ~Chrysene 0.0336 0.0336 0.0336 1.4E-12 5.7E-13 6.2E-14 2.0E-12
206-44-0 ~Fluoranthene 0.0616 0.0616 0.0616 1.8E-06 7.6E-07 2.6E-06
91-57-6 ~Methylnaphthalene, 2-2.42 2.42 2.42 1.8E-03 7.4E-04 2.5E-03
91-20-3 ~Naphthalene 3.49 3.49 3.49 1.7E-08 7.0E-09 3.8E-08 6.1E-08 1.7E-05 7.1E-06 2.7E-02 2.7E-02
129-00-0 ~Pyrene 0.0595 0.0595 0.0595 5.8E-07 2.4E-07 8.3E-07
103-65-1 Propyl benzene 1.43 1.43 1.43 4.2E-05 2.2E-04 2.6E-04
7782-49-2 Selenium 3.97 3.97 3.97 2.3E-03 4.5E-05 2.4E-03
7440-22-4 Silver 0.0805 0.0805 0.0805 4.7E-05 4.7E-05
95-63-6 Trimethylbenzene, 1,2,4-9.86 9.86 9.86 7.3E-04 6.6E-03 7.3E-03
108-67-8 Trimethylbenzene, 1,3,5-3.5 3.5 3.5 2.6E-04 2.8E-03 3.1E-03
1330-20-7 Xylenes 21.1 21.1 21.1 1.6E-04 9.8E-03 9.9E-03
Cumulative:1.4E-06 2.3E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.31 0.31 0.31 9.1E-07 9.1E-07
7440-38-2 Arsenic, Inorganic 4.26 4.26 4.26 1.5E-07 2.5E-08 5.6E-08 2.4E-07 2.5E-02 4.0E-03 6.4E-02 9.3E-02
7440-39-3 Barium 215 215 215 3.2E-03 9.7E-03 1.3E-02
71-43-2 Benzene 3.38 3.38 3.38 7.5E-09 1.1E-07 1.2E-07 1.0E-03 1.3E-02 1.4E-02
104-51-8 Butylbenzene, n-1.17 1.17 1.17 3.4E-05 3.4E-05
135-98-8 Butylbenzene, sec-0.00467 0.00467 0.00467 1.4E-07 1.4E-07
7440-43-9 Cadmium (Diet)0.105 0.105 0.105 5.8E-10 5.8E-10 6.2E-04 7.9E-05 2.4E-03 3.1E-03
16065-83-1 Chromium(III), Insoluble Salts 215 215 215 4.2E-04 9.7E-03 1.0E-02
18540-29-9 Chromium(VI)3.45 3.45 3.45 7.0E-08 8.9E-07 9.6E-07 2.0E-03 2.6E-03 4.6E-03
98-82-8 Cumene 0.389 0.389 0.389 2.9E-06 7.4E-04 7.4E-04
100-41-4 Ethylbenzene 5.35 5.35 5.35 2.4E-09 3.4E-08 3.7E-08 3.2E-04 1.1E-04 4.3E-04
142-82-5 Heptane, N-11.1 11.1 11.1 1.1E-02 3.3E-03 1.4E-02
110-54-3 Hexane, N-13.9 13.9 13.9 1.4E-04 8.9E-03 9.1E-03
7439-92-1 ~Lead and Compounds 63.2 63.2 63.2 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.149 0.149 0.149 1.5E-02 1.5E-02
108-95-2 Phenol 0.176 0.176 0.176 8.6E-07 2.8E-07 2.0E-07 1.3E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0901 0.0901 0.0901 5.1E-11 1.6E-11 6.7E-13 6.8E-11 1.3E-05 4.3E-06 1.8E-05
56-55-3 ~Benz[a]anthracene 0.0405 0.0405 0.0405 1.6E-10 6.8E-11 1.5E-11 2.5E-10
205-99-2 ~Benzo[b]fluoranthene 0.0484 0.0484 0.0484 2.0E-10 8.1E-11 8.9E-12 2.9E-10
218-01-9 ~Chrysene 0.0336 0.0336 0.0336 1.4E-12 5.7E-13 6.2E-14 2.0E-12
206-44-0 ~Fluoranthene 0.0616 0.0616 0.0616 1.8E-06 7.6E-07 2.6E-06
91-57-6 ~Methylnaphthalene, 2-2.42 2.42 2.42 1.8E-03 7.4E-04 2.5E-03
91-20-3 ~Naphthalene 3.49 3.49 3.49 1.7E-08 7.0E-09 3.8E-08 6.1E-08 1.7E-05 7.1E-06 2.7E-02 2.7E-02
129-00-0 ~Pyrene 0.0595 0.0595 0.0595 5.8E-07 2.4E-07 8.3E-07
103-65-1 Propyl benzene 1.43 1.43 1.43 4.2E-05 2.2E-04 2.6E-04
7782-49-2 Selenium 3.97 3.97 3.97 2.3E-03 4.5E-05 2.4E-03
7440-22-4 Silver 0.0805 0.0805 0.0805 4.7E-05 4.7E-05
95-63-6 Trimethylbenzene, 1,2,4-9.86 9.86 9.86 7.3E-04 6.6E-03 7.3E-03
108-67-8 Trimethylbenzene, 1,3,5-3.5 3.5 3.5 2.6E-04 2.8E-03 3.1E-03
1330-20-7 Xylenes 21.1 21.1 21.1 1.6E-04 9.8E-03 9.9E-03
Cumulative:1.4E-06 2.3E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Recreator/Trespasser Soil Output Form 2F
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
Receptor Type:
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.31 0.31 0.31 2.5E-06 2.5E-06
7440-38-2 Arsenic, Inorganic 4.26 4.26 4.26 3.1E-06 4.3E-07 5.1E-12 3.5E-06 6.1E-02 7.2E-03 2.1E-07 6.8E-02
7440-39-3 Barium 215 215 215 7.7E-03 3.2E-07 7.7E-03
71-43-2 Benzene 3.38 3.38 3.38 1.5E-07 1.2E-07 2.6E-07 6.0E-03 1.3E-03 7.4E-03104-51-8 Butylbenzene, n-1.17 1.17 1.17 1.7E-04 1.7E-04135-98-8 Butylbenzene, sec-0.00467 0.00467 0.00467 3.3E-07 3.3E-07
7440-43-9 Cadmium (Diet)0.105 0.105 0.105 5.3E-14 5.3E-14 7.5E-03 7.1E-04 7.9E-09 8.2E-03
16065-83-1 Chromium(III), Insoluble Salts 215 215 215 1.0E-03 1.0E-03
18540-29-9 Chromium(VI)3.45 3.45 3.45 6.3E-06 2.2E-10 6.3E-06 8.2E-03 2.6E-08 8.2E-03
98-82-8 Cumene 0.389 0.389 0.389 2.8E-05 6.6E-06 3.4E-05
100-41-4 Ethylbenzene 5.35 5.35 5.35 4.7E-08 3.7E-08 8.4E-08 7.6E-04 3.9E-05 8.0E-04
142-82-5 Heptane, N-11.1 11.1 11.1 2.6E-01 3.9E-04 2.6E-01110-54-3 Hexane, N-13.9 13.9 13.9 2.8E-04 2.8E-047439-92-1 ~Lead and Compounds 63.2 63.2 63.2 <SL**<SL**<SL**7439-97-6 ~Mercury (elemental)0.149 0.149 0.149 6.0E-04 6.0E-04
108-95-2 Phenol 0.176 0.176 0.176 4.2E-06 9.9E-07 6.6E-13 5.2E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0901 0.0901 0.0901 1.0E-09 2.8E-10 6.0E-17 1.3E-09 3.2E-05 7.6E-06 4.0E-05
56-55-3 ~Benz[a]anthracene 0.0405 0.0405 0.0405 1.5E-08 4.9E-09 2.4E-11 2.0E-08
205-99-2 ~Benzo[b]fluoranthene 0.0484 0.0484 0.0484 1.8E-08 5.9E-09 2.2E-15 2.3E-08
218-01-9 ~Chrysene 0.0336 0.0336 0.0336 1.2E-10 4.1E-11 1.6E-17 1.6E-10
206-44-0 ~Fluoranthene 0.0616 0.0616 0.0616 1.1E-05 3.4E-06 1.4E-0591-57-6 ~Methylnaphthalene, 2-2.42 2.42 2.42 4.3E-03 1.3E-03 5.6E-0391-20-3 ~Naphthalene 3.49 3.49 3.49 3.4E-07 1.2E-07 4.0E-08 5.0E-07 1.2E-03 3.8E-04 1.0E-03 2.7E-03
129-00-0 ~Pyrene 0.0595 0.0595 0.0595 1.4E-05 4.4E-06 1.8E-05
103-65-1 Propyl benzene 1.43 1.43 1.43 1.0E-04 8.5E-06 1.1E-04
7782-49-2 Selenium 3.97 3.97 3.97 5.7E-03 1.5E-10 5.7E-03
7440-22-4 Silver 0.0805 0.0805 0.0805 1.1E-04 1.1E-04
95-63-6 Trimethylbenzene, 1,2,4-9.86 9.86 9.86 7.0E-03 8.7E-04 7.9E-03
108-67-8 Trimethylbenzene, 1,3,5-3.5 3.5 3.5 2.5E-03 3.7E-04 2.9E-031330-20-7 Xylenes 21.1 21.1 21.1 7.5E-04 1.5E-03 2.3E-03
Cumulative:1.1E-05 3.9E-01
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400
mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Groundwater to Indoor Air
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
CAS #Chemical Name:
Groundwater
Concentration
(ug/L)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-39-3 Barium 0.511 -1.0E-01
71-43-2 Benzene 284 3.6E-01 6.3E+00 1.8E-04 2.1E+00
104-51-8 Butylbenzene, n-9.78 --
7440-43-9 Cadmium (Diet)0.000115 1.6E-03 2.1E-03
67-66-3 Chloroform 0.867 1.2E-01 2.0E+01 1.1E-06 1.3E-03
98-82-8 Cumene 18.7 -8.3E+01 2.1E-02
107-06-2 Dichloroethane, 1,2-6.49 1.1E-01 1.5E+00 2.9E-06 4.3E-02
108-20-3 Diisopropyl Ether 246 -1.5E+02 3.5E-02
142-82-5 Heptane, N-4.43 -8.3E+01 8.7E-01
110-54-3 Hexane, N-51.6 -1.5E+02 5.2E+00
7439-92-1 ~Lead and Compounds 0.0058 --
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)17.6 -6.3E+02 3.2E-05
91-57-6 ~Methylnaphthalene, 2-57.9 --
91-20-3 ~Naphthalene 388 8.3E-02 6.3E-01 8.5E-05 2.2E+00
103-65-1 Propyl benzene 35.6 -2.1E+02 1.5E-02
100-42-5 Styrene 13.5 -2.1E+02 1.5E-03
108-88-3 Toluene 36.2 -1.0E+03 1.9E-03
95-63-6 Trimethylbenzene, 1,2,4-81.1 -1.3E+01 3.3E-01
108-67-8 Trimethylbenzene, 1,3,5-12.4 -1.3E+01 7.1E-02
1330-20-7 Xylenes 119 -2.1E+01 3.1E-01
Cumulative:2.7E-04 1.1E+01
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor
intrusion risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 270 8.1 --
71-43-2 Benzene 54 1.62 3.6E-01 6.3E+00 4.5E-06 5.2E-02
75-15-0 Carbon Disulfide 61 1.83 -1.5E+02 2.5E-03
98-82-8 Cumene 19 0.57 -8.3E+01 1.4E-03
110-82-7 Cyclohexane 2900 87 -1.3E+03 1.4E-02
100-41-4 Ethylbenzene 110 3.3 1.1E+00 2.1E+02 2.9E-06 3.2E-03
142-82-5 Heptane, N-170 5.1 -8.3E+01 1.2E-02
110-54-3 Hexane, N-2200 66 -1.5E+02 9.0E-02
67-63-0 Isopropanol 36 1.08 -4.2E+01 5.2E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)20 0.6 -1.0E+03 1.2E-04
91-20-3 ~Naphthalene 29 0.87 8.3E-02 6.3E-01 1.1E-05 2.8E-01
103-65-1 Propyl benzene 61 1.83 -2.1E+02 1.8E-03
127-18-4 Tetrachloroethylene 31 0.93 1.1E+01 8.3E+00 8.6E-08 2.2E-02
108-88-3 Toluene 97 2.91 -1.0E+03 5.6E-04
79-01-6 Trichloroethylene 28 0.84 4.8E-01 4.2E-01 1.8E-06 4.0E-01
95-63-6 Trimethylbenzene, 1,2,4-130 3.9 -1.3E+01 6.2E-02
108-67-8 Trimethylbenzene, 1,3,5-100 3 -1.3E+01 4.8E-02
1330-20-7 Xylenes 99 2.97 -2.1E+01 2.8E-02
Cumulative:2.0E-05 1.0E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Groundwater to Indoor Air
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
CAS #Chemical Name:
Groundwater
Concentration
(ug/L)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-39-3 Barium 0.511 -4.4E-01
71-43-2 Benzene 284 64.43990188 1.6E+00 2.6E+01 4.1E-05 4.9E-01
104-51-8 Butylbenzene, n-9.78 6.357399836 --
7440-43-9 Cadmium (Diet)0.000115 6.8E-03 8.8E-03
67-66-3 Chloroform 0.867 0.130085446 5.3E-01 8.6E+01 2.4E-07 3.0E-04
98-82-8 Cumene 18.7 8.791905151 -3.5E+02 5.0E-03
107-06-2 Dichloroethane, 1,2-6.49 0.31309076 4.7E-01 6.1E+00 6.6E-07 1.0E-02
108-20-3 Diisopropyl Ether 246 25.74652494 -6.1E+02 8.4E-03
142-82-5 Heptane, N-4.43 362.2240392 -3.5E+02 2.1E-01
110-54-3 Hexane, N-51.6 3797.219951 -6.1E+02 1.2E+00
7439-92-1 ~Lead and Compounds 0.0058 --
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)17.6 0.099296811 -2.6E+03 7.6E-06
91-57-6 ~Methylnaphthalene, 2-57.9 1.226173344 --
91-20-3 ~Naphthalene 388 6.979558463 3.6E-01 2.6E+00 1.9E-05 5.3E-01
103-65-1 Propyl benzene 35.6 15.28209321 -8.8E+02 3.5E-03
100-42-5 Styrene 13.5 1.517784137 -8.8E+02 3.5E-04
108-88-3 Toluene 36.2 9.826982829 -4.4E+03 4.5E-04
95-63-6 Trimethylbenzene, 1,2,4-81.1 20.42420278 -5.3E+01 7.8E-02
108-67-8 Trimethylbenzene, 1,3,5-12.4 4.445952576 -5.3E+01 1.7E-02
1330-20-7 Xylenes 119 32.25551922 -8.8E+01 7.4E-02
Cumulative:6.1E-05 2.7E+00
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3D
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 20593-21-032
Exposure Unit ID: Mangum Street, Durham, NC
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 270 2.7 --
71-43-2 Benzene 54 0.54 1.6E+00 2.6E+01 3.4E-07 4.1E-03
75-15-0 Carbon Disulfide 61 0.61 -6.1E+02 2.0E-04
98-82-8 Cumene 19 0.19 -3.5E+02 1.1E-04
110-82-7 Cyclohexane 2900 29 -5.3E+03 1.1E-03
100-41-4 Ethylbenzene 110 1.1 4.9E+00 8.8E+02 2.2E-07 2.5E-04
142-82-5 Heptane, N-170 1.7 -3.5E+02 9.7E-04
110-54-3 Hexane, N-2200 22 -6.1E+02 7.2E-03
67-63-0 Isopropanol 36 0.36 -1.8E+02 4.1E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)20 0.2 -4.4E+03 9.1E-06
91-20-3 ~Naphthalene 29 0.29 3.6E-01 2.6E+00 8.0E-07 2.2E-02
103-65-1 Propyl benzene 61 0.61 -8.8E+02 1.4E-04
127-18-4 Tetrachloroethylene 31 0.31 4.7E+01 3.5E+01 6.6E-09 1.8E-03
108-88-3 Toluene 97 0.97 -4.4E+03 4.4E-05
79-01-6 Trichloroethylene 28 0.28 3.0E+00 1.8E+00 9.4E-08 3.2E-02
95-63-6 Trimethylbenzene, 1,2,4-130 1.3 -5.3E+01 4.9E-03
108-67-8 Trimethylbenzene, 1,3,5-100 1 -5.3E+01 3.8E-03
1330-20-7 Xylenes 99 0.99 -8.8E+01 2.3E-03
Cumulative:1.5E-06 8.1E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator