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Home My WebLink About7407_Pitt_C&DLandfillInc_CDLF_Phase1_Phase2_Dec2020GW_FID1819172_20231016DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 DENR USE ONLY ❑Paper Report [:]Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Smith Gardner, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Joan A. Smvth. P.G. E-mail: joan@smithgardnerinc.com Phone: 919-828-0577 x 221 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) C&D Disposal, Inc. 802 Recycling Lane. Greenville, NC 29-06 .0500 December 1-8, 2020 27834 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Joan A. Smyth, P.G. Senior Hydrogeologist 919-828-0577 x 221 F�cl?R""�nhtative Name (Print) Title (Area Code) Telephone Number ,,,� 10/3/2023 Affix NC Licensed/ Professional Geologist Seal S�jZft�BA711 F488... 14 N. Boylan Ave. Raleigh, NC 27603 Facility Representative Address F-1370 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Date CAR` OQ. EN FpIle IV 7 SEAL 10/ 1369 ud A. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 December 2020 Groundwater Monitoring Report COD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-20016 7407- CDLF- 2009 Prepared for: CGD Disposal, Inc. 802 Recycling Lane Greenville, North Carolina 27834 September 2021 Prepared by: NCLIC.N0.E1370 (ENGINEERING) SMITH- GARDNER 14 N. Boylan Avenue, Raleigh NC 27603 1 919.828.0577 PRINTED ON IHI RECYCLED PAPER O 2021 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 December 2020 Groundwater Monitoring Report Egg Disposal, Inc. NC Solid Waste Permit 7407-CDLF-2001 6 7407- CDLF- 2009 Prepared For: EGO Disposal, Inc. Greenville, North Carolina S+G Project No. EJERECYCLING-20-1 ^\ D o c u S i g n e d�j/bb y: 4?tV ' e.i V owuL ,,,tl .0 5DD73DOAFAR2442. Daniel J. Pantaleo Staff Environmental Technician , A EN L Signed by: I\� `N a SEA � 10/ /2 Joan A, Smyth, P.G. 3t�9 Senior Hydrogeologist 'p°F—LO A. September 2021 NCLIC.NU1370 (ENGINEERING) SMITH,-GARDNER 14 N. Boylan Avenue, Raleigh NC 2?603 1919.828.057? DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 CSD Disposal, Inc. NC Solid Waste Permit No. 7407- CDLF- 2001 & 7407- CDLF- 2009 December 2020 Groundwater Monitoring Report Table of Contents Paqe 1.0 INTRODUCTION......................................................................................................... 1 2.0 SITE GEOLOGY........................................................................................................... 1 3.0 SAMPLING LOCATIONS.............................................................................................. 1 4.0 SAMPLING PROCEDURES.......................................................................................... 2 5.0 FIELD & LABORATORY RESULTS............................................................................... 2 5.1 Field Results........................................................................................................... 2 5.2 Laboratory Analysis................................................................................................ 2 5.3 Laboratory Results................................................................................................. 2 5.3.1 Inorganic Constituents................................................................................ 3 5.3.2 Organic Constituents.................................................................................. 3 5.3.3 Surface Water Results................................................................................ 4 6.0 GROUNDWATER CHARACTERIZATION....................................................................... 4 7.0 CONCLUSIONS...........................................................................................................4 FIGURE Figure 1 Groundwater Potentiometric Map Figure 2 Concentration Map TABLES Table 1 Groundwater Elevation Table 2 Field Parameters Table 3 Detected Inorganic Constituents Table 4 Detected Organic Constituents Table 5 MNA Parameters Table 6 Velocity and Conductivity Data APPENDICES Appendix A Well Logs Appendix B Laboratory Analytical Report Appendix C Time Vs. Concentration Graphs MD Disposal, Inc. December 2020 Groundwater Monitoring Report September 2021 Table of Contents Page i DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 1.0 INTRODUCTION C&D Disposal, Inc., located at 802 Recycling Lane, Greenville, North Carolina, operates a C&D Landfill under Solid Waste Permit #7407- CDLF- 2001 and #7407- CDLF- 2009. The site is currently required to submit semi-annual groundwater monitoring reports to NCDEQ. The facility contains two active, unlined construction & demolition (C&D) landfill units. The Facility was developed in two non-contiguous footprints, Phases 1 and 2 approximately midway between US 264, i.e., a localized topographic divide, and Grindle Creek. The phases became operational in May 2001 and August 2009, respectively. Phase 1 was the regional repository for flood -damage debris after Hurricane Floyd in 1999. Phase 2 was a staging area, where flood -debris was stored temporarily. Both areas were used for agriculture, and a former railroad corridor traverses the site, including the Phase 2 footprint. This report presents the results from the semi-annual monitoring event conducted December 1- 8, 2020 and includes a field procedure summary, laboratory analyses, summary tables and groundwater characterization. 2.0 SITE GEOLOGY Historical literature and available geologic maps indicate that C&D Landfill, Inc. sits within the NC Coastal Plain. The coastal plain is characterized as an eastward thickening wedge of sedimentary layers that alternate between sandy aquifers an aquitards. Information taken from The Geologic Map of North Carolina, 1985 shows that the C&D landfill is underlain bythe Yorktown Formation, which is described as "fossillifferous clay with varying amounts of fine-grained sand, silty sand, sandy silt, silty clay, and blueish gray shell material" Groundwater in the upper -most aquifer generally flows through unconsolidated sediments. Recharge occurs generally in the northern portion of the site and is limited on slopes. Groundwater flows generally south where it discharges into tributaries of Grindle Creek. The groundwater potentiometric surface generally reflects a subdued expression of the surface topography. Local conditions are considered typical for the coastal plain region. Ground water depths generally range from 3 ft to 12 ft below ground surface (bgs) across the facility. There are minor seasonal variations in the flow pattern, but overall flow direction is consistent. 3.0 SAMPLING LOCATIONS The ground water monitoring network consists of eighteen shallow and four deep wells totaling (22) groundwater monitoring wells. MW-IS (upgradient of phase 1); MW-ID, MW-2D, MW-2S, MW-3D, MW-3S and MW-3A, MW-4, MW-5, MW-6, MW-7, and MW-8 (downgradient of phase 1); MW-9A, MW-16, and MW-17 (upgradient of phase 11); MW-10, MW-11, MW-12S, MW-13, MW-14D, MW-14S, and MW-15 (downgradient of phase II); the network also includes four surface water Locations (SW-1, SW-2, SW-3, and SW-4). CGD Disposal, Inc. December 2020 Groundwater Monitoring Report September 2021 Page 1 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Figure 1 illustrates sampling locations. Available well logs forth e groundwater monitoring wells are included in Appendix A. 4.0 SAMPLING PROCEDURES Environment 1 personnel conducted the monitoring network sampling event December 1-8, 2020. Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (DENR, DWM) and the approved site Water Quality Monitoring Plan'. Each well was gauged to determine groundwater depth and then purged three well volumes or until dry. Groundwater depth from this event, as well as other well details are presented in Table 1. Samples were collected by Environment 1, Inc. in laboratory prepared containers for the specified analytical procedures. Groundwater samples and quality control blanks, were properly preserved, placed on ice and transported to the laboratory facility within the specified hold times for each analysis. 5.0 FIELD 6 LABORATORY RESULTS 5.1 Field Results Temperature, pH, turbidity, specific conductance, ORP, and dissolved oxygen were measured in the field at the time of sampling via direct read instruments. Field results from this sampling event are presented in Table 2. 5.2 Laboratory Analysis Ground and surface water samples were transported to Environment 1, Inc., a North Carolina certified laboratory for metals and Appendix 11 VOC analysis. Samples were also analyzed for additional C&D inorganics, alkalinity, sulfide, chloride, total dissolved solids and tetrahydrofuran. The laboratory report including the full list of analytes tested for is presented as Appendix B. 5.3 Laboratory Results Analytical results were compared to Rule 15A NCAC 2L.0200 (21- Standard) and/or the NC Groundwater Interim Maximum Allowable Concentration. Surface water results were compared with the NCAC 213 Standard for Class C waters (213 Standards). 1 Water Quality Monitoring Plan Amendment, C&D Landfill, Inc., CDLF (Phases 1 and 2) prepared for C&D Landfill, Inc., by David Garrett and Associates, Revised May 2008. CGD Disposal, Inc. December 2020 Groundwater Monitoring Report September 2021 Page 2 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Most constituent concentrations were either below the method detection limit (MDL) or were reported as "J-values". J-values are identified by the laboratory as "estimated values between the MDL and the MRL". 5.3.1 Inor0anic Constituents Five inorganic constituents were reported at concentrations above their 2L Standard this event. • Arsenic (MW-3A, MW-3S, and MW-12S); and • Barium (MW-3S); and • Chromium (MW-3A, MW-3S, MW-10, MW-12S, and MW-14S) • Iron (MW-1D, MW-1S, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW-7, MW- 8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-15, MW-16, and MW-17); and • Manganese (MW-1 D, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW-7, MW-8, MW-10, MW-11, MW-12S, MW-14S, MW-15, MW-16, and MW-17). Three inorganic constituents were reported at concentrations above their GWP standard this event. • Cobalt (MW-2S, MW-3A, MW-3S, MW-7, MW-8, MW-12S, and MW-14S); and • Thallium (MW-1D, MW-IS, and MW-9A); and • Vanadium (MW-1D, MW-1S, MW-2D, MW-2S, MW-3A, MW-3S, MW-4, MW- 5, MW-6, MW-7, MW-8, MW-10, MW-11, MW-125, MW-13, MW-14S, MW- 15, MW-16, and MW-17). As MW-IS and 1 D are upgradient of Phase 1 and MW-16 is upgradient of Phase 2, exceedances in these wells indicate that detected constituents may be due to naturally occurring conditions. Inorganic detections are summarized in Table 3. 5.3.2 Oroanic Constituents Three organic constituents were detected above their 2L Standards during this sampling event. • 1,4-Dioxane (MW-2S, MW-3A, MW-3S, MW-5, MW-8, MW-10, MW-11, MW- 12S, and MW-14S); and • Benzene (MW-125, and MW-14S); and • Vinyl Chloride (MW-11, MW-12S, MW-13, and MW-14S). Organic detections are provided on Table 4. CGD Disposal, Inc. December 2020 Groundwater Monitoring Report September 2021 Page 3 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 5.3.3 Surface Water Results No inorganic or organic constituents were detected above their NC213 standards in surface water samples collected this event. Surface water detections are provided on Table 3. 6.0 GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater data from the most recent sampling event. The data indicates that groundwater is flowing generally south towards tributaries of Grindle Creek. This is consistent with groundwater flow patterns previously reported for the site. The potentiometric surface map is included as Figure 1. Groundwater flow velocities during the sampling event were calculated using the equation: V = Ki/n where: K = hydraulic conductivity i = groundwater gradient n = porosity Calculated groundwater velocities ranged from 0.00068 ft/day (MW-11) to 0.14591 ft/day (MW- 3A) averaging 0.06166 ft/day. Flow velocities and calculated gradients are included in Table 6. 7.0 CONCLUSIONS Analytical results are generally consistent with past sampling events. Iron, manganese, and vanadium were detected in most samples collected this event above their respective NC2L and NCGWP standards. All wells this event, with the exception of MW-7, had turbidities <10NTUs. Due to this, and the exceedances noted in upgradient wells, it is likelythat some of these inorganic exceedances can be attributed to naturally occurring metals in the soil. 1,4-Dioxane, benzene, and vinyl chloride were detected in multiple monitoring wells above their NC21- standards this sampling event. Although not exceeding regulatory limits, 1,2-Dichloroethane and Tetrahydrofuran were also present in multiple wells this event. The presence of these organochlorides as well as vinyl chloride provide some evidence that reductive dichlorination and natural attenuation may be occurring onsite. A corrective action plan is currently being drafted to further address these exceedances and will be submitted under a separate cover. The next groundwater monitoring event is scheduled for Spring 2021. A report with laboratory analysis will be submitted to NCDEQ in accordance with 15A NCAC 13B .0544. CGD Disposal, Inc. December 2020 Groundwater Monitoring Report September 2021 Page 4 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 FIGURES December 2020 Groundwater Monitoring Report EBB Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 11 MW- �' TOC 6 t i ' ❑TW %` ft*lk* 1 A 74 7.1 = 13.60 s f �• �}. ••► ,! LEGEND NOTES '` «. •!►+- "., 1. GROUNDWATER DATA COLLECTED BY ENVIRONMENT 1, INC. -950 EXISTING 10' CONTOUR (SEE REFERENCE 2) DECEMBER 1-8, 2020. 6-9A TOC= 20.58 DTW= 5.54 ' i• Pil GWE= 15.04 EXIS77NG 2' CONTOUR (SEE REFERENCE 2) APPROXIMATE PROPERTY LINE (SEE REFERENCE 1) FLOOD HAZARD AREAS ZONE AE ' (SEE REFERENCE 3) �• APPROXIMATE GROUNDWATER SURFACE CONTOUR . SW-1 SURFACEWATER MONITORING LOCATION MW-8* INDICATES ELEVATON NOT USED FOR CONTOURING MW-1A GROUNDWATER MONITORING WELL TOC TOP OF CASING ELEVATION ! t_ . \ DTW DEPTH TO WATER % 3 ' GWE GROUNDWATER ELEVAIION TO MW 119.1 »_ ', � MW-10 TOC= 20.91 �MW-15 TOC= 16.61 M 1D DTW7.00 D'fW= 7.02 TOC= 19.67 DTW= 3./0 . - - .. i CC- 1.14 �» - GWE= 12.14 `. , DTW= 6.34 GWF-_ 13.21 D ='.62 GWE= 13.91 WE5 13.33 E= 13.5;L MW-14D �r MW-14S III TOC- 17.45 MW- I I TOC= 16.60 DTW= 5.18 TOC= 14.49 * ' DTW= 5.85 GWE= 12.0; DTW= 3.40 *.' ,• GWE= 10.75 GWE- 11 0Q l , r MW-8* oA r - 4 SW-4 - J' L L S © 2021 Smith Gardn Inc. TOC= 21.2' . y D W= 5.70 OW 15.51 i MW-12S +_ TOC= 16.18 ' DTW= 4.84 W-13� GWE= 11.34 MW-3S TOC= 23.02 20.69 DTW= 11.92 9.16 ' - GWE= 11.10 � 1.53 $W-3 c - .•,4% MW-5 ' VMV,'-3D TOC= 17.90 TOC= 22.81 DTW= 5.4 -DTW= 19.80 TOC--'2"3- :WF--- lU15 GWE= 11.03 DTW= 10.64 GWE= 11.29 G fi' REFERENCES 1. PARCEL BOUNDARIES FROM PITT COUNTY GIS DEPARTMENT. 2. FLOOD HAZARD INFORMATION FROM NORTH CAROLINA FLOODPLAIN MAPPING PROGRAM, FEMA FIRM MAP NO. 3720562800L, EFFECTIVE DATE JUNE 19, 2020. 3. AERIAL IMAGERY DATED 2016 FROM PITT COUNTY GIS DEPARTMENT 0 200' 400' -4 TOC= 18.42 ; ` DTW= 6 75 ' GWE= 1 1.67 , SW-1 ' TOC= 40 / DT - 7.50 ., y r - '46 I IW-6 7OC= 20.03 . TW= 8.89 i ,GWE= 11.14 M - MW-2S SW-2 ® = 1.ee ME 11.43 TW= 10.20 WE= 10.37 G = 11.24 \ z w W 0 0 J� z� Q o CM - U o U - c U en m z J N o L Y o m w w < LU _ Z w z w J o cn J J Q ON n o W z � W J w o J G N 0 N = Q a Q C-3 L7 Z C-3 W M C N Z O c CV J J Z LV G W_ W C W m J ,W, W G CO ME C7 W I--- W C C- 0 z 0 CM DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 TABLES December 2020 Groundwater Monitoring Report EBB Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER E�.W [ate 7/ 252T' :.• • .: V • D. . Well Well Installation Date Well Diameter (inches) Total Well Depth (ft Ground Surface Elevation (ft TOC Elevation (ft amsl) Depth to Water (ft) Water Table Elevation Screen Interval (feet bgs) M W-1 D 10/ 13/ 2000 2 33.75 17.4 21.14 7.62 13.52 40- 50 M W-1 S 5/ 2/ 2001 2 17.21 17.59 20.91 7 13.91 3-13 MW-2D 10/11/2000 2 38.17 17.97 21.8 11.43 10.37 39-49 MW-2S 5/3/2001 2 16.57 18.45 21.44 10.2 11.24 3-13 M W- 3A 8/ 10/ 2009 2 23.44 19.13 21.93 10.64 11.29 5- 20 M W- 3D 10/ 13/ 2000 2 52.3 19.37 22.83 11.8 11.03 40- 50 MW-3S 8/6/2007 2 22.24 19.37 23.02 11.92 11.10 8-18 M W- 4 5/ 3/ 2001 2 15.98 14.83 18.42 6.75 11.67 3-13 MW-5 11/19/2002 2 9.5 14.8 17.9 5.4 12.50 3-18 M W- 6 5/ 3/ 2001 2 16.65 16.87 20.03 8.89 11.14 3-13 M W- 7 5/ 3/ 2001 2 16.33 16.03 19.4 7.5 11.90 3-13 MW-8 11/5/2002 2 20.26 18.3 21.21 5.7 15.51 3-18 M W- 9A 8/7/2009 2 23.17 17.64 20.58 5.54 15.04 5- 20 M W-10 8/ 6/ 2009 2 22.73 14.16 16.61 3.4 13.21 5- 20 M W--11 8/ 6/ 2009 2 23.84 11.60 14.49 3.4 11.09 5- 20 MW-12S 8/7/2009 2 22.93 13.72 16.18 4.84 11.34 5-20 MW-13 8/7/2009 2 20.68 18.12 20.69 9.16 11.53 5-20 MW-14D 12/17/2002 2 41.92 14.54 17.45 5.38 12.07 35-40 M W-14S 12/ 18/ 2002 2 23.12 13.9 16.6 5.85 10.75 5- 20 M W-15 12/ 18/ 2002 2 22.14 13.9 19.67 6.34 13.33 5- 20 MW-16 6/16/2017 2 22.73 NA 19.16 7.02 12.14 NA M W-17 12/ 9/ 2002 2 22.25 18.18 20.74 7.14 13.60 5- 20 Note: 1. Well installation, depth, elevations, and screened interval from David Garrett Boring Logs M Rgatsl Gzni%daNkritc inj,2GardAdErNt ntairgRpp s1 EERL)dirr, 2 tr2M C-cc20M EffbydirgTaJEs DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Bf.W [)te7/ W 2T' Well ID pH (SU) Temperature ('Celsius) Specific Conductivity (uMhos/cm) ORP (mv) Dissolved Oxygen Turbidity (NTU) M W-1 D 7.3 19 393 14 210 8.77 M W-1 S 6.5 18 452 12 600 8.88 MW-2D 7.5 17 460 82 410 2.92 MW-2S 6.6 17 1206 79 910 4.4 M W- 3A 6.8 16 2017 -18 430 6.87 MW-3D 7.9 17 539 -1 1 410 1.17 MW-3S 6.9 19 3768 -54 910 3.13 MW-4 6.5 16 364 86 1310 9.7 M W- 5 6.9 15 644 88 580 6.42 M W- 6 6.6 17 390 85 610 8.43 M W- 7 6.7 16 890 112 650 21.9 M W- 8 6.8 18 1527 113 490 7.03 M W- 9A 7.3 18 579 58 200 3.4 M W-10 6.4 14 1440 122 1000 2.57 M W-11 7.1 13 1008 94 200 8.22 MW-12S 6.9 15 2567 136 300 5.24 M W-13 6.6 20 560 56 300 3.69 MW-14D 7.6 17 543 43 1130 1.21 MW-14S 6.7 18 2428 77 1 2320 9.67 M W-15 5.9 18 536 96 1150 7.4 M W-16 6 20 985 112 1690 7.64 M W-17 5.6 18 587 86 1260 6.01 SW-1 6.9 9 370 105 4550 11 SW-2 7.2 6 206 98 9150 2.8 SW-3 6.8 6 277 106 9030 13.3 SW-4 6.4 7 136 118 8650 13 Note: 1. Field Parameters measured by Environment 1 on 12/1/2020 - 12/8/2020. 3. Bold indicates a turbidity exceeding 10 NTU. :\. [C.Ti 77MR-11 a uMtT,T. AWN 010� C:a�i \�.:CTlli�ya�n�ii 4f/.1\�?�:1"/.17�.:CTIlii 90-M DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welled Irurga icGxistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W tote 7i 27/22 Well ID Parameter Standard Limit Result MW-11D Antimony NCGWP 1 0.12 J Arsenic NC21- 10 1.6 J Barium NC21- 700 24.4 Cobalt NCGWP 1 0.12 J Copper NC21- 1000 0.45 J Iron N C2L 300 1984 Lead NC21- 15 0.09 J Manganese NC21- 50 123 Nickel NC21- 100 0.35 J Selenium NC21- 20 0.19 J Thallium NCGWP 0.2 0.5 J Total Chromium NC21- 10 0.36 J Vanadium NCGWP 0.3 0.51 J Zinc NC21- 1000 2.4 J MW-1S Antimony NCGWP 1 0.12 J Arsenic NC21- 10 1.5 J Barium NC21- 700 34.3 Beryllium NCGWP 4 0.05J Cadmium NC21- 2 0.05 J Cobalt NCGWP 1 0.42 J Copper NC21- 1000 0.88 J Iron NC21- 300 1914 Lead NC21- 15 0.82 J Manganese NC2L 50 15 Nickel NC21- 100 0.45 J Selenium NC21- 20 0.16 J Thallium NCGWP 0.2 0.2 J Ti n NCGWP 2000 0.05 J Total Chromium NC21- 10 0.46 J Vanadium NCGWP 0.3 2.1 Zinc NC21- 1000 1.7 J MW-21D Antimony NCGWP 1 0.14 J Arsenic NC21- 10 0.89 J Barium NC21- 700 16 Cobalt NCGWP 1 0.19 J Copper NC21- 1000 0.45 J Iron N C2L 300 424 Lead NC21- 15 0.12 J Manganese NC21- 50 16 Nickel NC21- 100 0.5 J Selenium NC21- 20 0.14 J Thallium NCGWP 0.2 0.12 J Ti n N CGWP 2000 0.19 J Total Chromium NC21- 10 0.46 J Vanadium NCGWP 0.3 0.34 J I:\a9 o• R«cii'ii, AMMYN� a 14MCM166rr.'t" KI e, �• DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W Dte7i27/22 Well ID Parameter Standard Limit Result Zinc NC21- 1000 16 MW-2S Antimony NCGWP 1 0.2 J Arsenic NC21- 10 3.4 J Barium NC21- 700 118 Cobal t NCGWP 1 1.34 Copper NC21- 1000 0.811 Iron NC21- 300 4101 Lead NC21- 15 0.29 J Manganese NC21- 50 219 Nickel NC2L 100 11 Selenium NC2L 20 0.51 J Thallium NCGWP 0.2 0.14 J Ti n NCGWP 2000 0.2 J Total Chromium NC2L 10 2.7 J Vanadium NCGWP 0.3 0.88 J Zinc NC21- 1000 1.6 J MW-3A Antimony NCGWP 1 0.16 J Arsenic NC2L 10 20 Barium NC2L 700 253 Beryllium NCGWP 4 0.05J Cobal t NCGWP 1 5 Copper NC21- 1000 0.15 J Iron NC2L 300 17644 Lead NC21- 15 0.11 J Manganese NC2L 50 643 Nickel NC21- 100 2.1 J Selenium NC21- 20 0.4 J Thallium NCGWP 0.2 0.05 J Ti In NCGWP 2000 0.25 J Total Chromium NC2L 10 11 Vanadium NCGWP 0.3 3.7 Zinc NC21- 1000 1.2 J MW-31D Antimony NCGWP 1 0.15 J Arsenic NC21- 10 0.41 J Barium NC2L 700 10 Cobalt NCGWP 1 0.06 J Copper NC2L 1000 0.18 J Iron NC2L 300 81 Manganese NC2L 50 3 J Nickel NC2L 100 0.21 J Selenium NC2L 20 0.21 J Ti n NCGWP 2000 0.28 J Vanadium NCGWP 0.3 0.15 J Zinc NC21- 1000 1.3 J Antimony NCGWP 1 0.21 J I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ill�rii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W tote 7i 27/22 Well ID Parameter Standard Limit Result M W- 3S Arsenic NC21- 10 23 Barium N C2L 700 834 Beryllium NCGWP 4 0.04 J Cobal t NCGWP 1 4.9 Copper NC21- 1000 0.21 J Iron N C2L 300 18867 Lead NC21- 15 0.1 J Manganese NC21- 50 988 Nickel NC21- 100 2.4 J Selenium NC21- 20 1.6 J Total Chromium NC21- 10 26 Vanadium NCGWP 0.3 7.1 Zinc NC21- 1000 1.4 J MW-4 Antimony NCGWP 1 0.09 J Arsenic NC21- 10 0.98 J Barium NC21- 700 67.6 Beryllium NCGWP 4 0.12 J Cobalt NCGWP 1 0.4 J Copper NC21- 1000 0.19 J Iron N C2L 300 2149 Lead NC21- 15 0.38 J Manganese NC21- 50 53 Nickel NC21- 100 0.34 J Selenium NC21- 20 0.49 J Thallium NCGWP 0.2 0.04 J Ti n NCGWP 2000 0.2 J Total Chromium NC21- 10 2 J Vanadium NCGWP 0.3 2.9 Zinc NC21- 1000 1.3 J MW-5 Antimony NCGWP 1 0.34 J Arsenic NC21- 10 1.6 J Barium NC21- 700 81.8 Beryllium NCGWP 4 0.04 J Cobalt NCGWP 1 0.76 J Copper NC21- 1000 1.2 J Iron N C2L 300 3153 Lead NC21- 15 0.2 J Manganese NC21- 50 127 Nickel NC21- 100 0.89 J Selenium NC21- 20 0.24 J Thallium NCGWP 0.2 0.04 J Ti In N CGWP 2000 0.21 J Total Chromium NC21- 10 2.4 J Vanadium NCGWP 0.3 1.4 Zinc NC21- 1000 2.2 J I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ill�rii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W Dte7i27/22 Well ID Parameter Standard Limit Result MW-6 Antimony NCGWP 1 0.09 J Arsenic NC21- 10 0.44 J Barium NC21- 700 103 Beryllium NCGWP 4 0.02 J Cobalt NCGWP 1 0.4 J Copper NC21- 1000 0.69 J Iron N C2L 300 278 Lead NC21- 15 0.14 J Manganese NC21- 50 40 Nickel NC21- 100 0.39 J Selenium NC21- 20 0.15 J Thallium NCGWP 0.2 0.04 J Total Chromium NC21- 10 11 Vanadium NCGWP 0.3 1.5 Zinc NC21- 1000 0.68 J MW-7 Antimony NCGWP 1 0.111 Arsenic NC21- 10 0.96 J Barium NC21- 700 134 Beryllium NCGWP 4 0.04 J Cobal t NCGWP 1 1.7 Copper NC21- 1000 1.8 J Iron NC21- 300 1015 Lead NC21- 15 0.38 J Manganese NC21- 50 115 Nickel NC21- 100 0.99 J Selenium NC21- 20 0.41 J Thallium NCGWP 0.2 0.06 J Total Chromium NC21- 10 5.3 Vanadium NCGWP 0.3 2 Zinc NC21- 1000 1.7 J MW-8 Antimony NCGWP 1 0.12 J Arsenic NC21- 10 9.1 Barium NC21- 700 164 Cobal t NCGWP 1 1.4 Copper NC21- 1000 0.4 J Iron N C2L 300 13448 Lead NC21- 15 0.11 J Manganese NC21- 50 670 Nickel NC21- 100 1.1 J Selenium NC21- 20 0.28 J Ti In N CGWP 2000 0.24 J Total Chromium NC21- 10 9.4 Vanadium NCGWP 0.3 1.6 Zinc NC21- 1000 1.2 J Antimony NCGWP 1 0.11 I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ilhrii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W tote 7i 27/22 Well ID Parameter Standard Limit Result MW-9A Arsenic NC2L 10 0.22 J Barium NC2L 700 45 Cobalt NCGWP 1 0.02 J Copper NC2L 1000 0.31 J Iron NC2L 300 523 Manganese NC2L 50 47 Nickel NC2L 100 0.19 J Thallium NCGWP 0.2 0.29 J Total Chromium NC2L 10 0.12 J Vanadium NCGWP 0.3 0.26 J Zinc NC2L 1000 0.72 J MW-10 Antimony NCGWP 1 0.19 J Arsenic NC2L 10 2.9 J Barium NC2L 700 160 Cobalt NCGWP 1 0.66 J Copper NC2L 1000 0.28 J Iron NC2L 300 1390 Manganese NC21- 50 276 Nickel NC2L 100 1.8 J Selenium NC2L 20 0.84 J Ti In N CGWP 2000 0.06 J Total Chromium NC21- 10 12 Vanadium NCGWP 0.3 6.9 Zinc NC21- 1000 0.59 J MW-11 Antimony NCGWP 1 0.08 J Arsenic NC21- 10 5.3 Barium NC21- 700 89 Cobalt NCGWP 1 0.9 J Copper NC21- 1000 0.1 J Iron NC2L 300 16358 Lead NC21- 15 0.04 J Manganese NC21- 50 293 Nickel NC21- 100 0.98 J Selenium NC21- 20 0.48 J Ti In N CGWP 2000 0.25 J Total Chromium NC21- 10 2.4 J Vanadium NCGWP 0.3 1.5 Zinc NC2L 1000 0.6 J MW-12S Antimony NCGWP 1 0.19 J Arsenic NC21- 10 20 Barium NC2L 700 451 Cobal t NCGWP 1 2 Copper NC2L 1 1000 0.11 Iron NC2L 300 1650 Manganese NC21- 50 755 I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ilhrii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W tote 727/22 Well ID Parameter Standard Limit Result Nickel NC21- 100 2.6 J Selenium NC21- 20 1.7 J Total Chromium NC21- 10 31 Vanadium NCGWP 0.3 20 Zinc NC21- 1000 0.45 J MW-13 Antimony NCGWP 1 0.111 Arsenic NC21- 10 2.6 J Barium NC21- 700 73 Cobalt NCGWP 1 0.36 J Copper NC21- 1000 0.5 J Iron NC21- 300 3118 Lead NC21- 15 0.05 J Manganese NC21- 50 37 Nickel NC21- 100 0.64 J Selenium NC21- 20 0.56 J Thallium NCGWP 0.2 0.04 J Ti n NCGWP 2000 0.24 J Total Chromium NC21- 10 0.84 J Vanadium NCGWP 0.3 1.8 Zinc NC21- 1000 2.2 J MW-14D Antimony NCGWP 1 0.11 J Arsenic NC21- 10 0.4 J Barium NC21- 700 11 Copper NC21- 1000 0.39 J Iron NC21- 300 36 J Manganese NC21- 50 3 J Nickel NC21- 100 0.22 J Thallium NCGWP 0.2 0.02 J Total Chromium NC21- 10 0.18 J Vanadium NCGWP 0.3 0.22 J Zinc NC21- 1000 4.7 J MW-14S Antimony NCGWP 1 0.19 J Arsenic NC21- 10 3.8 J Barium N C2L 700 384 Beryllium NCGWP 4 0.051 Cobal t NCGWP 1 1.8 Copper NC21- 1000 0.22 J Iron N C2L 300 8689 Lead NC21- 15 0.22 J Manganese NC21- 50 1104 Nickel NC21- 100 1.6 J Selenium NC21- 20 0.84 J Thallium NCGWP 0.2 0.05 J Total Chromium NC21- 10 16 Vanadium NCGWP 0.3 5.8 I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ill�rii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W Dte7i27/22 Well ID Parameter Standard Limit Result Zinc NC21- 1000 1.4 J MW-15 Arsenic NC21- 10 0.89 J Barium NC21- 700 150 Beryllium NCGWP 4 0.2 J Cobalt NCGWP 1 0.2 J Copper NC21- 1000 0.11 Iron N C2L 300 9748 Lead NC21- 15 0.11 Manganese NC21- 50 124 Nickel NC21- 100 0.32 J Selenium NC21- 20 1.3 J Thallium NCGWP 0.2 0.02 J Ti n NCGWP 2000 0.09 J Total Chromium NC21- 10 1.5 J Vanadium NCGWP 0.3 6.9 Zinc NC21- 1000 9.6 J MW-16 Arsenic NC21- 10 5.4 Barium N C2L 700 207 Beryllium NCGWP 4 0.05J Cobalt NCGWP 1 0.81 J Copper NC21- 1000 0.09 J Iron N C2L 300 60200 Manganese NC2L 50 310 Nickel NC21- 100 0.42 J Selenium NC21- 20 0.86 J Thallium NCGWP 0.2 0.02 J Ti In NCGWP 2000 0.15 J Total Chromium NC21- 10 2.9 J Vanadium NCGWP 0.3 7 Zinc NC21- 1000 0.56 J MW-17 Antimony NCGWP 1 0.12 J Arsenic NC21- 10 0.43 J Barium NC21- 700 71 Beryllium NCGWP 4 0.091 Cobalt NCGWP 1 0.15 J Copper NC21- 1000 0.16 J Iron N C2L 300 2940 Lead NC21- 15 0.12 J Manganese NC21- 50 271 Nickel NC21- 100 0.38 J Selenium NC21- 20 0.29 J Ti In NCGWP 2000 0.18 J Total Chromium NC21- 10 1.7 J Vanadium NCGWP 0.3 2.8 Zinc NC21- 1000 1.8 J I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ill�rii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe3 Welded Irurga ici3xistituats EEFb,ydirgLa-d11 Dmwbff 1-8, 220 Bf.W tote 7i 27/22 Well ID Parameter Standard Limit Result SW-1 Antimony NC213 protect 5300 0.11 J Arsenic NC2113 150 1.5 J Barium NC213 protect 21000 74.6 Beryllium NC2113 6.5 0.08 J Cobalt NC213 protect 4 0.6 J Copper NC2113 3.1 1.2 J Lead N C2B 25 1.5 J Nickel NC2113 88 0.74 J Selenium NC2113 5 0.35 J Thallium NC2113 0.47 0.02 J Total Chromium NC2113 NE 4.2 J Vanadium NC2113 NE 4.6 Zinc NC26 81 5.8 J SW-2 Antimony NC213 protect 5300 0.05 J Arsenic NC26 150 0.48 J Barium NC213 protect 21000 52.9 Beryllium NC26 6.5 0.02 J Cobalt NC213 protect 4 0.24 J Copper NC26 3.1 0.19 J Lead NC26 25 0.16 J Nickel NC26 88 0.25 J Selenium NC2113 5 0.14 J Total Chromium NC2113 NE 0.71 J Vanadium NC2113 NE 0.38 J Zinc NC2B 81 1.4 J SW-3 Antimony NC213 protect 5300 0.06 J Arsenic NC2B 150 0.79 J Barium NC213 protect 21000 93.4 Beryllium NC2B 6.5 0.091 Cobalt NC213 protect 4 0.9 J Copper NC2B 3.1 0.42 J Lead NC2B 25 0.34 J Nickel NC2B 88 0.68 J Selenium NC2B 5 0.34 J Thallium NC2113 0.47 0.04 J Total Chromium NC2113 NE 1.4 J Vanadium NC2113 NE 1.2 Zinc NC2113 81 4.1 J SW-4 Antimony NC213 protect 5300 0.05 J Arsenic NC2113 150 0.41 J Barium NC213 protect 21000 90 Beryllium NC2113 6.5 0.14 J Cobalt NC213 protect 1 4 0.74 J Copper NC2113 3.1 0.44 J Lead NC2113 25 0.49 J I:\a�:•�«T,Tr.'�'i�� •��IfT.6rrt"if•�� IPe�i.1L1.1�x�i.1LIi�,:C�ilhrii� DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNER Table3 Lheded Irug1cQnslItI,ErtS FyCilrgLa-dll DbOBT bEr 1-a 20M E�.Ut Cite 7/27122 Well ID Parameter Standard Limit Result Nickel NC213 88 0.49 J Selenium NC213 5 0.19 J Thallium NC213 0.47 0.08 J Total Chromium NC213 NE 1 J Vanadium NC213 NE 1.4 Zinc NC213 81 3.4 J Note: Table Data is presented in ug/I. NC21- - North Carolina groundwater standards per 15A NCA 0 2L.0202 NC2B - NCAC 2E Standard for Class C waters Bold - Concetration exceeding 2L or GWP Standard j - Aconcentration detected by the laboratory above the method detection limit, but below the reporting limit; therefore, result is estimated concentration. NE- Standard not established. 1:�1a0 P at 1111046'ii0 T.R't'if•r� a �� ::��i>1 .:::►Tfli��.>I� �%1►"1.1� �%1►"1]�.::iTj T1 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 SMITH GARDNER Tabe4 D8tectedCg3icGxE;titt 31S Bf.MI [ate 7/27/22 Well ID Parameter Standard Standard Limit Result MW-11D Tetrahydrofuran NCGWP 2000 135 MW-2S 1,4-Dioxane NC2L 3 11.3 Tetrahydrofuran NCGWP 2000 4.05 MW-3A 1,2-Dichloroethane NC2L 0.4 0.03 J 1,4-Dioxane NC21L 3 73.1 2,4,5-TP NC2L 50 0.51 J Acenaphthene NC2L 80 4.99 J Benzene NC2L 1 0.82 J Naphthalene NC2L 6 0.77 J Tetrahydrofuran NCGWP 2000 16.5 Tol uene NC2L 600 0.72 J MW-3S 1,2-Dichloroethane NC2L 0.4 0.05 J 1,4-Dioxane NC21L 3 158 Acenaphthene NC2L 80 5.46 J Benzene NC2L 1 0.46 J Tetrahydrofuran NCGWP 2000 25.6 MW-5 1,4-Dioxane NC2L 3 7.22 Tetrahydrofuran NCGWP 2000 1.05 MW-7 Tetrahydrofuran NCGWP 2000 3.23 MW-8 1,4-Dioxane NC2L 3 36.5 Tetrahydrofuran NCGWP 2000 7.94 MW-10 1,2-Dichloroethane NC2L 0.4 0.04 J 1,4-Dioxane NC21L 3 7.14 Tetrahydrofuran N CGWP 2000 6.24 MW-11 1,2-Dichloroethane NC2L 0.4 0.05 J 1,2-Dichloropropane NC2L 0.6 0.04 J 1,4-Dioxane NC2L 3 6.7 Benzene NC2L 1 0.62 J Tetrahydrofuran NCGWP 2000 5.16 Vinyl Chloride NC21L 0.03 0.14 J MW-12S 1,2-Dichloroethane NC2L 0.4 0.06 J 1,2-Dichloropropane NC2L 0.6 0.06 J 1,4-Dioxane NC21L 3 14.1 Benzene NC21L 1 1.37 Carbon Disulfide NC2L 700 0.34J Naphthalene NC2L 6 2.7 J Tetrahydrofuran NCGWP 2000 29 Tol uene NC2L 600 0.35 J Vinyl Chloride NC2L 0.03 0.73 MW-13 Cis- 1,2-Dichloroethene NC2L 70 0.6 J Tetrahydrofuran NCGWP 2000 2.65 Vinyl Chloride NC21L 0.03 0.24 RA\A/ 1^QI 1,2-Dichloroethane NC2L 0.4 0.06 J 1,2-Dichloropropane NC2L 0.6 0.04 J 1,4-Dioxane NC21L 3 9.63 Z\Rge3s\GardAEtErNtntcircjGarxlAAEr ntcnngFgats\IVtrtin(iut�8.NItV20'5,GpjcfN43V15NtrtingN-Wdes DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNER Table4 atectedoocaj-ISitt.BIS 037 yl irgLa-dll DboaTbEr 1$, = W.M1 Cite 7/27/202' Well ID Parameter Standard Standard Limit Result IVI°°- 1Y`' Benzene NC2L 1 1.37 Tetrahydrofuran NCGWP 2000 18.3 Vinyl Chloride NC2L 0.03 1.96 MW-16 1,2-Dichloroethane NC2L 0.4 0.111 1,2-Dichloropropane NC21- 0.6 0.05 J Note: Table Data is presented in ug/I. NC21- - North Carolina groundwater standards per 15A NCA 0 2L.0202 NC2B - NCAC 2E Standard for Class C waters Bold - Concetration exceeding 2L or GWP Standard J - Aconcentration detected bythe laboratoryabove the method detection limit, but below the reporting limit; therefore, result is estimated concentration. NE- Standard not established ZRgeds\C3anJAdaK,tntairr,GaridndErMntairgFgats\WinQLrti 8.W2T&GbpycfW15WingvTdJe= DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNERTed e5 lta7, M Well ID Parameter Method Detection Limit Standard Limit Result Alkalinity (to pH 4.5) 770 NE 179000 Chloride 350 250000 13000 MW-1D Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 U Sulfide 100 NE U Total Dissolved Residue NE 500000 234000 Alkalinity (to pH 4.5) 770 NE 159000 Chloride 350 250000 10000 MW-is Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 79900 Sulfide 100 NE U Total Dissolved Residue NE 500000 346000 Alkalinity (to pH 4.5) 770 NE 181000 Chloride 350 250000 13000 MW-2D Nitrate -Nitrite as N 40 10000 220 Sulfate 5000 250000 24400 Sulfide 100 NE U Total Dissolved Residue NE 500000 271000 Alkalinity (to pH 4.5) 770 NE 304000 Chloride 350 250000 50000 MW-2S Nitrate -Nitrite as N 40 10000 1550 Sulfate 5000 250000 185000 Sulfide 100 NE U Total Dissolved Residue NE 500000 727000 MW-3A Alkalinity (to pH 4.5) 770 NE 810000 Chloride 350 250000 112000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 46700 Sulfide 100 NE U Total Dissolved Residue NE 500000 1080000 MW-3D Alkalinity (to pH 4.5) 770 NE 222000 Chloride 350 250000 21000 Nitrate -Nitrite as N 40 10000 270 Sulfate 5000 250000 5800 Sulfide 100 NE U Total Dissolved Residue NE 500000 320000 MW-3S Alkalinity (to pH 4.5) 770 NE 1580000 Chloride 350 250000 213000 Nitrate -Nitrite as N 40 10000 370 Sulfate 5000 250000 70900 Sulfide 100 NE U Total Dissolved Residue NE 500000 1960000 MW-4 Alkalinity (to pH 4.5) 770 NE 126000 Chloride 350 250000 11000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 28300 Sulfide 100 NE U Total Dissolved Residue NE 500000 231000 MW-5 Alkalinity (to pH 4.5) 770 NE 254000 Chloride 350 250000 17000 Nitrate -Nitrite as N 40 10000 1950 Sulfate 5000 250000 57200 Sulfide 100 NE U Z\F?OectsiOaxr xdErKb tairzrj3a dAdErKtntairgFttsiWhQxty 8N42M(tprdNbj15Nkting/vIdEs DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNERTed e5 lha7, M Well ID Parameter Method Detection Limit Standard Limit Result Total Dissolved Residue NE 500000 408000 Alkalinity (to pH 4.5) 770 NE 205000 Chloride 350 250000 8000 Nitrate -Nitrite as N 40 10000 1590 MW-6 Sulfate 5000 250000 21100 Sulfide 100 NE U Total Dissolved Residue NE 500000 262000 Alkalinity (to pH 4.5) 770 NE 370000 Chloride 350 250000 23000 Nitrate -Nitrite as N 40 10000 1970 MW 7 Sulfate 5000 250000 40800 Sulfide 100 NE U Total Dissolved Residue NE 500000 479000 Z\F?OectsiOaxrLxdaMritairzrjC3a dAdErKtitargPtjutsiWinQuV8K42DSQwcfN415Udinq/vTEd#s DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNERTed e5 lta7, M Well ID Parameter Method Detection Limit Standard Limit Result Alkalinity (to pH 4.5) 770 NE 620000 Chloride 350 250000 55000 MW 8 Nitrate -Nitrite as N 40 10000 690 Sulfate 5000 250000 90600 Sulfide NE U Total Dissolved Residue NE 500000 836000 Alkalinity (to pH 4.5) 770 NE 210000 Chloride 350 250000 10000 MW-9A Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 72300 Sulfide 100 NE U Total Dissolved Residue NE 500000 347000 Alkalinity (to pH 4.5) 770 NE 455000 Chloride 350 250000 82000 MW-10 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 330000 Sulfide 100 NE 599 J Total Dissolved Residue NE 500000 1010000 MW-11 Alkalinity (to pH 4.5 770 NE 433000 Chloride 350 250000 18000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 214000 Sulfide 100 NE U Total Dissolved Residue NE 500000 754000 MW-12S Alkalinity (to pH 4.5) 770 NE 990000 Chloride 350 250000 119000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 173000 Sulfide 100 NE U Total Dissolved Residue NE 500000 926000 MW-13 Alkalinity (to pH 4.5) 770 NE 280000 Chloride 350 250000 11000 Nitrate -Nitrite as N 40 10000 270 Sulfate 5000 250000 98800 Sulfide 100 NE 409 J Total Dissolved Residue NE 500000 0 Alkalinity (to pH 4.5) 770 NE 250000 Chloride 350 250000 15000 Nitrate -Nitrite as N 40 10000 230 MW-14D Sulfate 5000 250000 U Sulfide 100 NE U Total Dissolved Residue NE 500000 314000 MW-14S Alkalinity (to pH 4.5) 770 NE 1180000 Chloride 350 250000 77000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 29800 Sulfide 100 NE U Total Dissolved Residue NE 500000 1450000 MW-15 Alkalinity (to pH 4.5) 770 NE 76000 Chloride 350 250000 18000 Nitrate -Nitrite as N 40 10000 U Sulfate 5000 250000 147000 Sulfide 100 NE U Z\F?OedsiGardAdErUflairzJC3a dAdErKtitargPtjutsiWhQxty8N429SQwcfN415Udinq/vTad#s DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNERTed e5 lha7, M Well ID Parameter Method Detection Limit Standard Limit Result Total Dissolved Residue NE 500000 361000 Alkalinity (to pH 4.5) 770 NE 124000 Chloride 350 250000 25000 Nitrate -Nitrite as N 40 10000 U MW-16 Sulfate 5000 250000 348000 Sulfide 100 NE U Total Dissolved Residue NE 500000 691000 Alkalinity (to pH 4.5) 770 NE 24000 Chloride 350 250000 18000 Nitrate -Nitrite as N 40 10000 U MW-17 Sulfate 5000 250000 165000 Sulfide 100 NE 397 J Total Dissolved Residue NE 500000 422000 Note: Table Data is presented in ug/I. NC21L - North Carolina groundwater standards per 15A NCAO 2L.0202 NC2B - NCAC 2E Standard for Class C waters Bold - Concetration exceeding 2L or GWP Standard J Aconcentration detected bythe laboratory above the method detection limit, but below the reoortina limit: therefore, result is estimated concentration. NE- Standard not established Z\F?OedsiGardmiEr trflairzrjC3a JAdErKtitargPtjutsiWhQxty8N429SQwcfN415UdingNTad#s DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 SMITH GARDNER 01, -. f. •1111 o o•. Hydraulic Hydraulic Velocity Effective Wel I Conductivity K Gradient v Porosity n (feet/day) i (feet/day) MW-3A 0.805 0.08 0.015 0.14591 MW-10 0.116 0.05 0.004 0.00882 M W-11 0.009 0.04 0.003 0.00068 MW-12S 0.322 0.06 0.017 0.09123 Note: 1. Hydrau I ic conductivity and effective porosity values from historical Wood Inc. groundwater monitoring reports 2. Velocity calculated based on the modified Darcy equation: v=(KI)/n W.M1 Cite 813YZZ MRgEds\Oaxd. daWtoinj2Oar aNtntaiMRperts\EERL�dirr,2Cm2M[x2MEEPa,ydingTaHEs DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 AppendixA Well Logs December 2020 Groundwater Monitoring Report EBB Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. AlfW-I d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.40 �t Equipment CME 750 Drilling Method 3-114" Hollow AugeisNater Level, TOB NA sz Date Started iom2100 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 Comments Plowed field. cool sunny weather Total Depth mo Date of Observation 1omwoo Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Medium dense buff -white, slightly silty, I I I I I I I I I I I I I I I moist 16,00 I I I I I I I I I I I I - - 14.00 I I I I I I I I 1 I I l I I I - - - 3.5 3 i i I i I i S i I 4.0 SAND: Loose, green -gray, silty and clayey, wet 4 SM 5 I I I I I I I I I I -- - 12.00 t I I I I I I I I i S t I I I I I I I I I 7.5 - - 10.00 ' I I ' ' ' —Y SILT: Medium stiff, gray -green, fine sandy and clayey, with heavy shell hash (turritellas) wet, 8.5 2 i i i i ; —_ medium plasticity 1 SM 8.00 i i i i i — 1 I I— I I I I I i I I I I — 6.00 4WV I I I I I I I I I I I S ! S 5 t I I I I I I I I I I — - — 4.00 1 I I I I I I I I t I I I 1 1 I I I I I I — 13.5 3 — I I I I — 4 s I I I I — M L- 1 I I 1 I C L 2,00 1 I I I I — — 0.00 3 I S I I I I 1 I 1 I I I I I I I I I I I I I I I — — — — I I I I 1 I I I I I I 18.5 — 18,5 4 ♦ CLAY: Medium stiff, gray -green, plastic gumbo -2.00 4 clay, moist CL 6 I I I I 1 I I I I I I I I I I I I I I I 4 00 I I I I I I I 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I 1 I I I I I I I I I I 1 I 23.5 4 I I I 5 I I ' I I ' I CL 7 I I I I I I I I DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. A4W--1 d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project CSD Landfill, Inc. (Pitt County) Ground Elevation 17.40 Equipment CME 750 Drilling Method 3-114" Hollow AugelhlVater Level, TOB NA Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 r.nmmPntG Pinwed field- cool sunnv weather Total DeDth sox Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction -8.00 i i ; i CLAY: Medium stiff, gray -green, plastic gumbo 'ANNULUS GROUTED i f S I I I I I I I 1 I I I I I day, moist -10.00 I I I I I I 1 1 I I I I I I I I I I I I I I I I I I 28.5 3CL I I I I I I I I I I 1 3 -12.00 I I I I 1 I I I I I I I 1 I I I I I I I I 1 I I I 31.5 -14.00 SILTYSAND: Dense, partly cemented, black- - ' ' green speckled, variably clayey, silty, moist, hard — ' layer at 36 to 38 feet, very hard below 45 feet -16.00 I 1 I I I I s -7. -• 33.5 6 22 I I I I ! — SM Bentonite 18 I I I r I I Seal -18.00 I I I 7 I I I I I I I ! t S I I I I I 1 1 I I I I I - - -20.00 3 I 1 f t I I I I I I I I I I I I I I I 1 I I I I I I I I I I I - - 38.5 31 I I I 1 I I I 15 I - SM -22.00 I - 24 I I I I I I I I I I I I I I I 1 I - -24.007. I I I I I I I I I I 1 I - I I I I I I I I 1 1 I l I I I I - Sand Pack I - SM -26.00 1 43.5 501.1— I I ! I I I - I I 1 I I 1 I I I I I 1 I I I 77 0.010" 28.00 i i i i i Slotted I I I 7 I I I I I I Screen -30.00 .JII W I I I i ! I I I I I I I I I I t 48.5 50115 I I I I I I I I I S 7. SM -32.00 — ' I I I ' I t Boring Terminated at 50 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. MW-1 s Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C8D Landfill, Inc. (Pitt County) Ground Elevation 17.59 Equipment CME 75 Drilling Method 4.11NO ID HSA Water Level, TOB NA sz Date Started 05102/01 Date Ended 05/02/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 5.59 s Comments Lockino cover with 3.32' stickup Total Depth 13.0 Date of Observation 5/116/01 Elev. SPT Data and Strata Depths. Lithology Description and USCS Code Piez. Construction 1 I I I ! SILTY SAND: Loose, tan -brown, moist [ I I , - Concrete I i I I I pad 16.00 I t I I I • I I I I I SM Bentonite I I I I 1 - Seal 14.00 I I I I I I I I I I I I I I f I I I I I ] i I 1 I - - 12.00— I I I I I I I l } ! I I I I I I I • = - I I I I I I I 3 ! S I I I I I I - - 10.00 I I I I 1 I 8.0 - 0.010" . • . SAND: Loose, tan, fine to medium Slotted 1 Screen I I ! ! $W g.00 ! I 3 I I I I 1 I ! I ! - 6.00 3 5 ! I I I I 1 1 I 1 I I I I I I I I I I I I I I 1 I I I 1 I I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 3 Client and Project C&D Landfill, inc. (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-718" rotary -mud Water Level, TOB 6.6 a Date Started 1019100 Date Ended 10111100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Degth 70.o Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction F I I I I . ' . • - SAND: Loose, tan -yellow, variably silty sand 16.00 { I I I I I I 1 1 I I I I I I I I I I I I I I I I - I I I I I I I I I I 1 3.5 14.00 3.5 16 ' ' CLAY: Medium stiff, tan range, very sandy, silty, e ; slightly plastic, moist, crumbly CL 8 I i I I i I I i 1 I i I I i I I SM 12.00 I I I l I I I ' I I I I I I I 1 1 I I I I I I I i I 75 i D.00 ' SAND: Medium dense, tan, subangular, f - c well ; graded (boring collapsed at 13.6 feet when casing Bentonite- 8.5 5 i pulled, redrilled with 41l4" hollow stem auger) Cement 6 I f I I I � $p- Grout 8 SM 8.00 I I 1 ! I I I I I I - 6.00 I I I I I I 1 I I I I I I I I I I I I I I I S F E 12.5 - �- -, CLAYEY SILT: Medium stiff, gray -green, fine — sandy, with heavy shell hash (whole turritellas), 13.5 3 — moist, moderately plastic 4 00 3 � I I r I I �— CL- 4 I I I I I ML I I I I 1 t I I I I \— I I I I { I I I I I \- 2.00 I I 1 I \ I I ! I I \ — I I I I I 0.00 i I r I I I I I I 1 1 t I I I \— I I I 1 I 16.5 2 a I I 1 I 2 , I i I i I i I i \— iiL- ML -2.00 3 , I I I I I \— I I 1 I I I I I I I \— I I 1 1 I I I I I I �— I I 1 I I I I I I I \ µ -4.00 I 1 I I I 22.5 CLAY: Medium stiff, gray -green, plastic gumbo I I I I I I I I I I clay, moist 23.5 2 -6.00 2 ' I ' I I I I CL 4 I I I I I DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 3 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.97 n Equipment CME 750 Drilling Method 3-7/8" rotarrmud Water Level, TOB 6.6 a Date Started 1o/woo Date Ended 10/11/00 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Depth 70A Date of Observation 1of16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code PEez. Construction 1 I I I CLAY: Medium stiff, gray -green, plastic gumbo i f i i i day, moist -8.00 I I I I i I I I I I I I I I I I I I I I -10.00 I I I I I I I I I I I I I I I I f 7 f f 1 28.5 2 I I I I l I I ' I I 2 , I I 1 I I CL 3 I I I I I I I I -12.00 I I I I I I 1 I [ I I I I I I I I I I I I I I l ? i i I I I I I I I I -14.00 I I I I l S i I I I I I I I I I I E S I I I I I I 33.5 _ 1B 04 33•5 1 I ' I 1 I I SILT: Stiff, gray -green, fine sandy, clayey, fi I I I I — - interlayered with sand SM 8 I I I I I — I _- Bentonite — Seal -18.00 7 I I I I I I I I I I - - i 37.0 _ 1 I I I I I , Sand Pack = — SILT: Hard, black -green speckled, clayey, fine ' — sandy, moist, moderately plastic, scattered -20.00 ; I i I i I i I i I — - pelecypod shell hash 38.5 5 ' — ' ' ' — 4 I 1 I I I ML 29 -22.00 I I I I I I I 1 I I I I I I I I 1 I I I - - - - -24 00 I I I I I I I I I I I I I I I I 1 - - = I I I I I 1 - o.o1a, - Slotted Screen MIL 43.5 10 28.00 20- 27 I I I I I I I I 1 1 — - -28 00 I I I I I I I I 1 I I I I I I I I I I I I I I I 1 I - = - -30.00 I I I I I I I I I I I I I I I I I I I I 1 I 1 I I _- - — - - 48.5 22 I I I I I I I I I 1 49.038 - 5M Bentonite SAND: Very dense (partly cemented), black -green 501.2 i i i i i speckled, clayey, silty, fine glauconite nodules Seal DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 3 of 3 Client and Project C&D Landfill, Inc, (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-7/8" rotary -mud Water Level, TOB 6.6 Date Started iomoo Date Ended 10/11100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 7.9 z Comments Plowed field. cool sunny weather Total Depth 70.o Date of Observation 10M6100 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Very dense (partly cemented), black -green 1 I I I I I E I I I I - speckled, clayey, silty, fine glauconite nodules -3-4.00 I 1 I I I I I I I I 53.5 50/ t I i 36.00 i I i - SM -38.00 I I ! I I I - I I I I I I I I I I I I I I I I I r I 1 57.4 - - ' SAND: Medium dense, green -black speckled, 40.00 i i i i i silty, clayey, fine grained, wet 58.5 6 I I I I I I I I F 7 I I I i 8C 7 42.00 I I I I I I I I Boring .• collapsed below50 I r I 61.5 , ' . feet CLAY: Medium stiff to very hard, gray -green, fine -44.00 i i i I I I I I I I r i ! I I I I I I I sandy, silty, moderately plastic 63.5 5 I I I I I I r s I I I I I -46.00 6 I I I ° I I I CL 5 I I I I I I i l I I I I I i I -48 00 I I I I I I I I I I I I I 7 r r ! F I I I I I I i I I i I I -_^•� I I I I I I I I I I I l k t ! I I I 1 I I I I I I 68.5 40 38 ; CL -s7 nn 501.5 I I t r I I Boring Terminated at 70 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. MW-2s Engineering and Geology Depths in feet, referenced 6.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 1 s.45 Equipment CME 75 Drilling Method 4114" ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Finn Bore & core Logged by David Garrett Stabilized Level 7.91 Comments Locking cover with 2.99' stickup Total Depth 13.o Date of Observation 5116101 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 i i i i i - • - SILTY SAND. Loose, tan -brown, moist Concrete I I i I I I I I I I Prdut l I I I I ! I I I I t — SM Bentonite 16.00 I I I ' I I ' ! I I 1 I I .. - Sea[ 14.00 l 3 I I I I 1 I I I I I 1 I I I I I I 1 - 12.00 I I I I I I I I I I I I ' 1 t I - I I I I I I I I I I 7.0 - SAND: Loose, tan, fine to medium, wet I I 1 I I I I 1 i I . ' 0.019, 10.00 I I Slotted 1 I I I I I I ! 1 I I I SVV Screen 6 W00 V 1 t I I I t I I I ! I I I I I I I I I I I I I I I I I I I [ • 6'00 I I I I i i Boring Terminated at 131eet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. M 3d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-1v4" Hollow AugaiNater Level, TOB 3.0 Q Date Started 10112l00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Comments Plowed field. cool sunnv weather Total Depth 50.0 Date of Observation 10/16/00 Elev, SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I I r I CLAY: Stiff, bright yellow -orange, fine sandy, silty, 1 I I I S I moist I I I S I 18.00 I 1 I I I I I I I 1 I I I I I I I I I I I i ! i I I I I i I I I I I I I Caved 16.00 3.5 4 + I i i i 4.0 SAND: Medium dense, tan -yellow, silty, trace of 4 I i I i I i I i I CL M 6 I I I I I f day, moist 14.00 I I I I I I I I f i I I I I I I I I 1 i 7.0 ' 12 00 I I SAND: Medium dense, tan -buff, well graded fine I to coarse, wet I I I I 4 S I I I 6.5 4 I I I I I I 10.00 5 * I i I i I i I i SW I I i 3 I I I I I I I I I I 1 1 I I I I 8.00 1 I ! ! I I I I I I I I I I I I I I I I 6.00 I I I 1 I 1 I I I I I I I I I 13.5 2 ' ' 14.0 - I I I I SILT: Stiff, gray -green, fine sandy and clayey, with 4 I M L- 4 I i i I i i — - rr heavy shell hash (tuitellas) wet, medium plastic CL 4.00 I I I I I I I I I I I I I I I I 1 1 1 1 — - - 2,00 I I I I I I I I I I I I I I I I I 1 I I I i 16.5 2 I I I I I 1 I I I I - 0•DD 2 CL 4 I I I I I I 1 I I I I I I I I — - - - -2.00 I I I I I I I I I I I I I 1 I I 1 1 I 1 I I I I r I I I I I I I I I - - - - - -4.00 I i I i 1 i I i I i 23.5 — CLAY: Medium stiff, gray -green, plastic gumbo 23.5 2 5 Gay, moist CL 7 I I I I 1 1 I I I I I DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. MW-3d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 r `1 Equipment CME 750 Drilling Method 4-114" Hollow AugekWater Level, TOB 3.0 a Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Y Comments Plowed field, cool sunny weather Total Depth 50.0 Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez, Construction _g 00 ' CLAY: Medium stiff, gray -green, plastic gumbo Bentonite- : day, moist Cement I I I I I r i I I I I I Grout -8.00 I I I I I I ! I I I I 27.5 - - SILTYSAND: Medium dense to dense, partly .. cemented, black -green speckled, variably clayey, 28.5 3 - silty, moist, very hard drilling (cemented) below 38 6 * i i i i feet, glauconitic SM -10.00 5 ! 3 1 I I I I I I I I I -- 12.00 F I I I I I 1 I I 1 I I I I I I I I I I I I I I I 77 - - -14.00 I I I I I I I I I I I I I I I I I I I I I I 33.5 5 I I I I I 18 I I I I I I SM 20 I I I ' - - _18.00 I I I I I _ Bentonite I I I I I I I I I I I I I I I I I I I I - Seal -18.00 I I I I I I I I I I I I 1 I 1 I I I I I I I I I I 38.5 15 I I I I I I I 1 1 1 I I 1 I I I - -20.00 501.3 i I I i I I i 1 1 i l r i I I _ - - SM I I I 1 s f I I - .. -22.00 I I I s I I I 1 I l I I - - Sand Pack -24.00 I I 1 I I 1 1 3 F I SM 43.5 501.5 I 1 I I 1 I f 1 I I -28.00 I 1 1 I I I I I 1 ! ! I I I 0.010" I I I I I Slotted 1 1 1 I r I 1 ! 1 1 I I - -- - Screen V W 1 1 I I I I I I I I 3 f I I I I - - 48,gyp .5 2943 1 I 1 I r I I I I 1 1 1 I I I -30.00 1 ! SM 501.5 Boring Terminated at 50 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. MW-3s Engineering and Geology Depths in feet, referenced b.g.s- Page 1 of 1 Client and Project CAD Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-11,V Hollow AugeliNater Level, TOB 3.9 s Date Started 815107 Date Ended 815107 Water Level, 24 Hr. NA Drilling Firm Bore A Core Logged by Aaron Hill Stabilized Level NA Comments Renlaces former MW-9s Total Depth 20.o Date of Observation NA Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I t ' SILTY CLAY: St'df, bright yellow -orange, fine 1 I I I 1.2 sandy, silty. moist 18.00 1.0 12 + Bentonite- — 16 i i i i — SILTY SAND: Med. dense, brown w! orange ML_ Cement I .. mottle, fine -medium texture CL Grout 21 I I I I I - I I I I I I 33 — Bentonite 16.00 3.5 14 ' i ' i ' i i ' i SAND: Tan, silty, fine texture, moist Seal 11 i i i i i SM- 11 I I I I 1 ML 14.00 I I I I I - 6.0 7 I I i I i I i I i • Sand Pack 11 i i i i 7.1 SM 12.00 11 ; SAND: Medium dense, tan -gray, well graded fine ' to medium texture, wet '• 0.010" 8.5 4 Slotted 4 SW Screen 10.00 4 I I i ! I i I I i I I i I t sM 8 00 I I I 1 1 I I I I I I I I I 7 ! I - I I I I I I I I I I I I r t S 12.9 - I I i I i I i t i CLAYEY SILT: Stiff, gray -green, fine sandy and 6.00 13.5 2 1 _ _ clayey, with heavy shell hash (turritellas) wet, 3 medium plasticity SM 3 I I I S I I 4.00 I I I I I I I I I I \ W I I E I I I I I i I I I I I I I I i t I 2.00 I I I I I \- I I 5 I I 18.5 4 I I ! I I — 5 I \ CL_ 0.� 5 I I F I I I _ Boring Terminated at 20 feet MIL r-111 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/10/09 Date Ended 08/10/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 21.93 Total Depth 20.0 Boring No. MW-3A Page 1 of 1 Ground Elevation 19.13 Water Level, TOB 5.9 Water Level, 24 Hr. NA Stabilized Level 11.4 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 Eli] -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF CLAYEY SAND: Topsoil with roots Bentonite- 1.0 3 1.6 Cement Grout 5 SM 0 - 3' SILTY SAND: Loose orange sli. clayey, fine - medium, trace of roots, sli. moist 3.5 4 - Bentonite Seal 4 -_ sM 3-4' 5 SZ 6.0 7 SM 7 8.5 SAND: Medium dense, tan -buff, 8.5 5 s well graded fine to coarse, SW moist -wet Sand Pack 4-20' 12.9 :. . — �- SILTY CLAY: Stiff, gray -green, 13.5 3 fine sandy, with heavy shell \- hash (turritellas) wet, medium ML- 4 plasticity CL 0.010" Slotted Screen 5 - 20' �- 18.5 2 \- M L- 2 — �— Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. MW-4 Engineering and Geology Depths in feet, referenced b.g.s. Page i of i Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 14.83 Equipment CME 75 Drilling Method 4-114~ ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 3.35 Comments leckinn cover with 3.59'stickuo Total Der)th 13.o Date of Observation wiwo1 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction _ .. - SILTY SAND: Loose, tan -brown, moist Concrete I I I I I .. Pad 14.00 ' ' ' ' ' — I I I I I I I Grout I I 1 I I I - — SM Bentonite I Seal 12.00 I I .. I I I I I I I I 1 I I l I I I — 10.00 I I I I I I I I I 1 1 1 I I I l I I I I — I I I I I I I I 1 I I 6.0 — SAND: Loose, tan, fine to medium, wet i i $.00 I 1 I I I I I ! f I I - - 1 t I 1 t I I 1 I I I 0.010" Slotted 6.00 W Screen I I I i i I I I I I I I I I I • SW 4.00 I I I I I I I I I I I I ! I I - 2.00 I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. MW-5 Engineering and Geology Depths in feet, referenced b.g.s_ Page 1 of 1 Client and Project C&D Landfill, Inc. (Phase 1) Ground Elevation 14,.80 Equipment Mobile 6-53 ATUrilling Method 4-1147 Hollow AugeidVater Level, TOB 3.6 Date Started 11M9102 Date Ended 11/19/02 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 3.9 Comments wooded area, cool sunny weatherTotal Depth 20.o Date of Observation 11/27/02 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Loose, tan, silty, fine to medium, dry ` Bentonite- I Cement 14.00 i ; i i Grout 1.0 4 4 i i i i SM 6 S I I I I I I Bentonite 2.9 Seal 12.00 i i i i i SAND: Medium dense, tan -buff, medium to 3.5 9 I I I 1 coarse, wet (fluvial) 3V ' I � 14 i i i i SW 10.00 16 I I I I I I I I I I S I 5.6 ' SAND: Loose to medium dense, tan -buff, fine to 6.1) 9 coarse, wet, trace of silt (fluvial) $.00 9 i i i i sM 4 I k I I I I I 3 t I I I I I I 8.1 Sand Pack I CLAYEY SAND: Loose, green -gray, silty, wet, 6.00 8.5 4 3 I . � sampled as distinct sand layers with plastic clay lenses (channel or near -shore deposits) SC 4 I \- I I ! I I \ \- I �- 4'00\- 0.01 a, \- ••• Slotted l I I I I Screen 2•00 3 I I I I 1 13.5 3 I i i i ....... .\- 4 i i i i \-\- SC 0.00 4\-\- i-- * Locking steel cover w! 3 foot \- •\ stickup �, -2.00 I I I I I I I I 1 I \- I I 1 I I I I I I I 18.4 Deep SILTY CLAY: Stiff, gray -green, var. sandy, shell 4.00 18.5 3 i i i i i marine 4 1 i i i i hash, moist, plastic ** CL_ deposits (Yorktown 6 i i i Boring Termat 20 feet CHinated Grp.) DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring No. MW-6 Engineering and Geology Depths in feet, referenced b.g-s. Page 1 of 1 Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16"87 Equipment CME 75 Drilling Method 411,C ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 6.68 Comments Lockina cover with 3.16" stickup Total Depth 13.o Date of Observation 5116/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I SILTY SAND: Loose, tan, moist Concrete pad 16.00 I — I I ! I I I - - Grout I I f I I SM Bentonite — Seal 14.00 I l f I I I I I I I 1 I I I I - 12.00 3 1 I I I I ! I I I . . — I I 1 ! I I I I I 1 6.0 - SAND: Loose, tan, fine to medium, wet I I I I I i 0.00 I I I I I 1 I I ! I • I I I I I 1 I I I I • 0.010" ' Slotted 8.00 i i i r i Screen I 1 1 I I I I I I I F I 1 I I I - SVj b 00 I I I I I I I - 1 I l I I I I I I I - 1 1 I I I I - Boring Terminated at 13 feet 4.00 - DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P.G., P.E. Boring No. AM-7 Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16.03 Equipment CME 75 Drilling Method 4-1►47 ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 5.29 ('nmmAntS Lne-kinn cover with 3.37' stickup Total Depth 13.o Date of Observation 5/16/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SILTY SAND: Loose, tan, moist Concrete I I I I I •• P I I I I I — Grout 14.00 1 ; r ; I ; I ; I ;77 SM Bentonfte I I I E I I I I I i Seal 12.00 I I I I I I I I I I I I I I I I S 5 1 i - I I I I ! I I I I 5.0 - - I SAND: Loose, tan, fine to medium, wot 10.00 I I S ! t I I I I I I 1 I I I I I 1 I I I I I I I I I 1 I I I I I I I 0.010" I I I I 1 Slotted Screen I SW 6.00 I 1 I I 1 I I 4D0 I 1 I I I I 1 i I I Boring Terminated at 13 feet DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett, P. G., P.E. Boring .No. AM-8 Engineering and Geology Depths in feet, referenced b-g.s. Page 1 of 1 Client and Project CSD Landfill, Inc. (Phase 1) Ground Elevation 18.30 Equipment Mobile 13-53 ATDrilling Method 4-114" Hollow AugeliJVater Level, TOB 7.3 s Date Started 11/18/02 Date Ended 11/18/02 Water Level, 24 Hr. 7.3 Drilling Firm Bore S Core Logged by David Garrett Stabilized Level 7.3 ('OMMentS wooded area- cool sunny weatherTotal ❑eoth 20.o Date of Observation 11/27/02 Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 SAND: Loose, tan, slightly silty, fine to medium, ` Bentonite- ' dry Cement Grout - 2 i i r i SW 16.00 3 I , I I , f I I , I I , I I , I - Bentonite Seal 3.5 3 I s I I I I 14.00 3 i i i i t - SW 4 I I I I I I I I I I I I I 1 f - I I I I I 6.3 ' 12.00 6.0 4 �' 4 SAND: Medium dense, tan -buff, medium to SW 4 I I I I f I I I :. coarse, wet 10.00 i ! i I i I i I i I 8 4 Sand Pack _ . • SAND: Loose to medium dense, tan -buff, fine to 8.5 7 8 I I i I i I i I , ' ' coarse, wet, trace of slit Sw 8.00 I 1 I I I - I I I I I Slotted I I I I 1 Screen W 6.00 I I I I I I I I I I I I 1 1 1 • 13.5 4 I I I 1 I I I - 4.00 4 I i i i i SW 4 I I 1 I I I Locking I , , , , • steel cover _ wl 3 foot 2.00 I I I : = I stickup I i I I i I 1 i I I s i I i I 17.6 ." SILTY CLAY: Mod. stiff, gray -green, var. sandy, 0.00 i i i heavy shell hash (turritellas) moist, plastic '• CL- " Deep 18.5 3 l• ; I i I i I i I CH marine deposits 4 I I 1 I I 1 I (Ye rkiown 6 Boring Terminated at 20 feet Fm.) DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.58 Total Depth 20.0 Boring No. MW-9A Page 1 of 1 Ground Elevation 17.64 Water Level, TOB 3.1 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -16 -14 -12 -10 -8 -6 -4 -2 -0 -2 N = 0 20 40 60 80 100 BPF 77 SILTY SAND: FILL with brick 1.0 3 77 and concrete fragments Bentonite- Cement Grout 4 2.1 SM 0-3' 5 XX CLAY: Med. stiff, orange -tan - gray (mottled), fine sandy, very 3.5 10 moist Bentonite Seal 12 CL 3-4' 13 5.9 SAND: Medium dense, light 6.0 5 ♦ 5 gray -buff, sli. silty, well graded SW- 6 fine to medium, wet SM 85 4 5 SW- 5 SM Sand Pack 4-20' 13.5 4 13.7 _ 4 — SILTY CLAY: Med. stiff, gray- ML- 5 green, sli. fine sandy, with CL �- heavy shell hash (turritellas) 0.010" Slotted — wet, medium plasticity Screen 5 - 20' �- Artesian water press. at 12 feet 18.5 2 \- M L- 2 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.61 Total Depth 20.0 Boring No. MW-10 Page 1 of 1 Ground Elevation 14.16 Water Level, TOB 2.7 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 W -0 -2 -4 N = 0 20 40 60 80 100 BPF SILT: Soft, dark brown, fine 1 sandy, organic, very moist Bentonite- 1.0 Cement Grout 1 2.1 ML 0-3' 5 SAND: Med. dense, tan -buff, uniform fine grained, wet t t 3.5 9 Bentonite Seal 13 SP 3-4' 12 Ir 6.0 9 12 7.1 SW 2 8.0 SAND: Loose, tan -buff, sli. silty —_ SILTY CLAY: Soft, gray -green, 8.5 3 sli. fine sandy, with heavy shell 2ML- \ hash (turritellas) wet, distict CL sand and clay layers Sand Pack 4-20' 13.5 3 �- 2 — M L- 3 CL \- 0.010" Slotted Screen 5 - 20' �- 18.5 3 \- M L- 3 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 14.49 Total Depth 20.0 Boring No. MW-11 Page 1 of 1 Ground Elevation 11.60 Water Level, TOB 6.1 Water Level, 24 Hr. NA Stabilized Level 3.1 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data M -8 -6 -4 -2 -o -2 -4 -6 -8 N = 0 20 40 60 80 100 BPF SAND: Loose, dark brown, silty, 2 fine - medium, tr. clay, moist Bentonite- 1.0 Cement Grout 2 SM >0-3' 3 2.9 CLAY: Very soft, green -gray, 3.5 1 silty, fine sandy, w/ turritella Bentonite Seal shell hash, wet ��- 3 - 4' o 5.5 CLAY: Soft - med. stiff, gray- 6.0 2 Sz 3 green, fine sandy, very silty, ML- 2 with shell hash (turritellas) wet, CL very sandy layer w/ large shell fragments at 9.5 - 10 feet 8.5 4 5 SC- 6 CL Sand Pack 4-20' 13.5 5 5 14.5 MH- $ SILTY CLAY: Med. stiff, gray- CH — green, sli. fine sandy, wet, very 0.010" Slotted plastic Screen 5 - 20' 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.18 Total Depth 20.0 Boring No. MW-12S Page 1 of 1 Ground Elevation 13.72 Water Level, TOB 2.1 Water Level, 24 Hr. NA Stabilized Level 5.3 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 z. N = 0 20 40 60 80 100 BPF SAND: FILL, Loose, brown, 1.0 1 silty, moist (drilling pad) Bentonite- Cement Grout 2 2 0 SM sz 0 - 3' SAND: Loose, tan -gray. sli. 5 silty, fine -medium, black 3.5 10 decayed organic debris, wet Bentonite Seal 12 SW- 3-4' 13 SM 7W 6.0 5 9 SW 10 SM 8.5 5 Loose, white, clean "sugar sand" 7 9.5 SP 3 10.0 �- SILTY CLAY: Med. stiff, gray- Sand Pack green, sli. fine sandy, moist, w/ 4 - 20' _— shells, very plastic 13.5 3 5 CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.69 Total Depth 20.0 Boring No. MW-13 Page 1 of 1 Ground Elevation 18.12 Water Level, TOB 5.1 Water Level, 24 Hr. NA Stabilized Level 8.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 -10 -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF SILTY SAND: Loose, brown, 1.0 2 fine -medium, w/ clay, roots, dry Bentonite- 3 (perimeter embankment fill) gW_ Cement Grout0 - 3' 3 - SM 3.5 3 4.0 Bentonite Seal CLAYEY SAND: Loose, tan, SC 3 - 4' 5 fine -medium, w/ wood, moist 5.7 - SILTY SAND: Very loose, tan- 6.0 1 1 brown, w/ tr. clay, wood SM 1 _ 8.1 �_ SILTY CLAY: Stiff, green -gray, 8.5 7 9 _— sli. fine sand w/wood Y, ML- 10 C L \_ Sand Pack — 4-20' 12.5 �- �- SILTY CLAY: Stiff, gray -green, 13.5 5 sli. fine sandy, w/ heavy shell 6 — hash (turritellas), moist, very MH- 6 plastic CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 4 \- M H- 5 Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 1 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 -2 -0 W -4 -6 -8 -10 N = 0 20 40 60 80 100 BPF . SILTY SAND: Medium dense 1.0 ♦ tan -brown, fine to medium Convertedfrom 5 SM piezometer 5 B-23d 3.1 3.5 6 SAND: Medium dense, tan, 10 medium to coarse SP 9 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 • dense, dark gray 3 _I SC 5 12.7 Bentonite- Cement Grout �- SILTY CLAY: Stiff, dark gray, 13.5 4 l \- fine sand layers, shell layers, 0-32' 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL 18.5 4 * �_ 6 CH 23.5 5 CH 6 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 2 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -14 -16 -18 - 20 - 22 - 24 N = 0 20 40 60 80 100 BPF \- SILTY CLAY: Stiff, dark gray, fine sand layers, shell layers, becomes sandy with shell hash below 28.4 feet 28.5 21 : \- 16 CL Bentonite Seal 32-33' 32.8 �- SAND: Very dense, dark gray, 33.5 50/A silty, glauconitic, shell hash SM Sand Pack 33-40' 0.0101, Slotted Screen 35-40' 29 38.5 50/.5 Boring Terminated at 40.0 feet SM DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/18/02 Date Ended 12/18/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 16.60 Total Depth 20.0 Boring No. MW-14S Page 1 of 1 Ground Elevation 13.90 Water Level, TOB 3.0 Water Level, 24 Hr. 2.2 Stabilized Level 2.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 -6 N = 0 20 40 60 80 100 BPF SILTY SAND: Medium dense Convertedfrom 1.0 tan -brown, fine to medium piezometer B-23s 5 SM 5 Bentonite- 3.1 _ sz Cement Grout SAND: Medium dense, tan, 3.5 6 0-1' 10 medium to coarse SP Bentonite Seal 9 1-3' 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 dense, dark gray 3 Sc 5 12.7 Sand Pack 3-20' -- SILTY CLAY: Stiff, dark gray, 13.5 4 l \— fine sand layers, shell layers, 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL \- 0.010" Slotted Screen 5-20' 18.5 4 \— s ? Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 David Garrett, P.G., P.E. MW-15s (OLD B-23s) Engineering and Geology Page 1 of 1 Client and Project CAD Landfill, Inc. (Phase 2) Ground Elevation 13.90 Equipment Detrich 0-10 Drilling Method 3-114" HSA Water Level, TOB 3.0 Date Started 12/18/02 Date Ended 12 I8102 Water Level, 24 Hr. 2.2 Drilling Firm Bare & care, inc. Logged by David Garrett Stabilized Level 1.4 Comments Lagged area, cool sunny weather Total Depth 20.0 Date of Observation 1116103 All deaths are given in feet and referenced b.a.s. Depth and Elev. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data -0 - 2 12.00 - 4 10.00 - g 8.00 - 8 6.00 - 10 4.00 - 12 2.00 - 14 0.00 - 16 -2.00 - 18 -4.00 — 20 -6.00 i I l i i i i + � I i i I i i i i i BLANK: No samples taken - please see log fpr &23d sz Bentonite- Cement Grout Bentonite Seal ' i I I i i Sand Pack 3 ' 0.0101, (} t E F e ! i i Slotted Screen DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 David Garrett, P.G., P.E. MW-17 (OLD B-20) M I I I Engineering and Geology Page I of 1 Client and Project C&D Landfill, Inc. (Phase 2) Ground Elevation 18.18 Equipment Detrich D•10 Drilling Method 3-1/4" NSA Water Level, TOB 3.7" Date Started 12/09/02 Date Ended 12109/02 Water Level, 24 Hr. 3.9 Drilling Firm sore & Core, Inc. Logged by David Garrett Stabilized Level 4.1 Comments Logged area, cool Manny weather Total Depth 20.0 Date of Observation 1115103 All depths are given in feet and referenced b.g.s. Depth and Elev.1. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data - a 1 B_oa — 16.00 — 14.00 — 6 12.00 — 8 10.00 — 10 8.00 — 12 6.00 — 14 4.00 — 16 2.00 = 18 0.00 - 20 .. SILTY SAND: Medium Sentonite- ; i dense, dark brown, fine Cement Grout 3 grained SM 5 1 — Bentonite Seal � SAND: Medium dense to dense, tan -brown, SW 19 I i fine to medium 8 14 0i ! i i ! SW 21 ! I 9 12 SW 14 I f � I i Sand Pack 3 SW SAND: Medium dense, [ fine to medium, trace of i { silt E f f� �{ 0.01 01, I I i Slotted Screen 3 a E f ! ! SILTY CLAY: Medium 5 I stiff, trace of shells ML-CL DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 D SOIL CLASSIFICATION P .AND REMARKS T H SEE KEY SYMBOL SHEET FOR EXPLANATION OF (ft) SYMBOLS AND ABBREVIATIONS BELOW. 0 Sandy topsoilirootmat ndfil--- l-debris/gravel - and san----- d --------� La _ _ _ COASTAL PLAIN: Orange -tan -to gray__, dry to moist_, clayey and silty SAND (SM) COAST -AT --1-Tan--a-a-nd -wh-t-m-ist-to-sa-tur-ate-d- L E SAMPLES PL (%) NM.(%) LL (%) E L I (Rec") G E D T N-COUNT ♦ FINES (%) E V E Y or N N P Rcc%MQD% 0 SPT (bpf) D (ft) T E 6"- 6"- 6"- 6" 10 20 30 40 50 60 70 80 90 100 15.0 5 slightly silty, tine to coarse SAND (SP) with trace rounded 10.0 fine gravel 1 . 10 5.0 15 YORKTOWN FORMATION: Dark gray to gray -green, 0.0 saturated, silty, fine to medium SAND (SM) with thin (0,1-0.2) lenses and layers of dark gray -green, fat CLAY (CH) 20 Boring terminated at 20.0 feet. -5.0 G n :7 a 3 25 0.0 d .a a a a n 30 15.0 35 -1 1 �- -20.0 40 -1 1 F- -25.0 45 -30.0 CONTRACTOR: Regional Probing Services -Larry Opper LOGGED BY: M. Lear EQUIPMENT: Geoprobe 5410 DRILL METHOD: Direct Push HOLE DIAMETER: 4" WELL: Stickup 2.9' Size 2" CLOSURE METHOD: Installed Monitering Well MW-16. REMARKS: Well developed by purging approximately 3 well volumes via bailer and pump. Static water level measured at 7,45 ft below TOC. 0 10 20 30 40 50 60 70 80 90 100 GEOTECHNICAL BORING RECORD BORING NO.: MW-16 PROJECT: EJE Recycling LOCATION: Greenville, NC DRILLED: June 16, 2017 PROJECT NO.: 6468-17-7070 PAGE 1 OF 1 IEWED BY: amec faster wheeler ► DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 David Garrett, P.G., P.E. Engineering and Geology .,Client and Project C&D Landfill, Inc. (phases 3 and 4) Equipment CIVIE 450 Drilling Method 4 1vvv H$A Date Started 12114101 Date Ended 12/14/01 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments :.iamg2u aiea5 cioal rarliny weather Total Depth 15.0 All dent :- are ,;:al: ,l__� _s_..__i.td r � � �kl iT.CI pelf l�if�rl'�.��YV`ii N.w.sx OLD B-Is (BG) Page 1 of 1 Ground Elevation 17.19 Water Level, TOE 1.5 Water Level, 24 Hr. 1.4 Stabilized Level 1.6 Date of Observation 12/27/01 Depth and Elegy. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezom2ter Constuction Data 0 r 16.00 2 14.00 4 12.00 6 10.00 8 8.00 10 6.00 12 4.00 14 SAND: Loose, gray- 2 I I I - brown, variably silty, 3 4 moist, trace of clay and a i ! . organics SM I Bentonite- 3 6 ' SP- Cement Grout 7 i I SM 2 SILT: Soft, dark bra.,.n, 2 clayey, decayed 2 — organics (channel Bentonite Seal -= deposits) 2 I — 1 I i ML 2 — Sand Pack 0.0101, 2 i I i i - - — ML Slotted Screen DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Appendix Laboratory Analytical Report December 2020 Groundwater Monitoring Report CRD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EIMONEMM Ala h�@rpmw 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 ID#: 6003 Drinking Water ID: 37715 Wastewater 3D: 1.0 - PHONE (252) 756-6208 FAX (252) 756-0633 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE DATE COLLECTED: 12/02/20 GREENVILLE, NC 27834 DATE REPORTED : 05/24/21 REVIEWED BY: MW-4 MW-5 MW-6 MW-1 MW-8 Analysis Method PARAMETERS MDL MRL Date Analyst Code PH (field measurement), Units 6.5 6.9 6.6 6.7 6.8 12/02/20 SEB 4500HB-11 Nitrate+Nitrite as N. mg/1 0.04 0.04 --- U 1.95 1.59 1.97 0,69 12/03/20 DTL 353.2 R2-9 Alkalinity (to pH 4.5), mg CaCO3/1 1.0 1.0 126 254 205 370 620 12/07/20 JMS 2320E-11 Chloride, mg/1 5.0 5.0 11 17 8 23 55 12/07/20 TMR 4500C1,B-11 Cyanide, ug/1 5.0 5.0 --- t7 --- U --- U --- U --- U 12/10/20 Sea 450OCNR-11 Total Dissolved Residue, mg/1 1.0 10 231 408 262 479 836 12/03/20 JMS 2540C-11 Sulfate, mg/1 5.0 5.0 28.3 57.2 21.1 4018 90.6 12/03/20 SEJ 4500SO42BI Antimony, ug/1 0.03 1.0 0.09 J 0.34 J 0.09 J 0.11 J 0.12 J 12/07/20 HMM EPA200.8 Arsenic, ug/1 0.08 5.0 0.98 J 1.6 J 0.44 J 0.96 J 9.1 12/07/20 HMM EPA200.8 Barium, ug/1 0.04 10.0 67.6 81.8 103 134 164 12/07/20 HMM EPA200.8 Beryllium, ug/1 0.02 1.0 0,12 J 0.04 J 0.02 J 0.04 J --- U 12/07/20 HMM EPA200.8 Cadmium, ug/l 0.04 1,0 --- U --- U --- U --- U --- U 12/07/20 HMM EPA200.8 Cobalt, ug/1 0.02 1.0 0.40 J 0.76 J 0.40 J 1.7 1.4 12/07/20 HMM EPA200.8 Total Chromium, ug/1 0.12 5.0 2.0 J 2,4 J 1.0 J 5.3 9.4 12/14/20 HMM EPA200.8 Copper, ug/1 0.04 10.0 0.19 J 1.2J 0.69J 1.817 0.40 J 12/07/20 HMM EPA200.8 Iron, ug/1 4.96 50.0 2149 3153 278 1015 13448 12/21/20 LFJ EPA200.7 Manganese, ug/1 0.31 10.0 53 127 40 115 670 12/21/20 LFJ EPA200.7 Lead, 0.03 5.0 0.38 J 0.20 J 0.14 J 0,30 J 0,11 J 12/07/20 HMM EPA200.8 ug/1 Mercury, ug/1 0.05 0.20 --- U --- U --- U --- U 12/09/20 MTM 245.1 R3-9 Mercury, ug/1 0.05 0,20 --- V 12/22/20 MTM 245.1 R3-9 Nickel, ug/1 0.03 10.0 0.34 J 0.89 J 0.39 J 0.99 J 1.1 J 12/07/20 HMM EPA200.8 Selenium, ug/l 0.05 10.0 0.49 J 0.24 J 0.15J 0.41 J 0.28 J 12/07/20 HMM EPA200.8 Silver, ug/l 0.22 5.0 --- U --- U --- U --- U --- U 12/07/20 HMM EPA200.8 Thallium, u9/1 0.02 1,0 0.04 J 0.04 J 0.04 J 0.06 J --- U 12/07/20 HMM EPA200.8 Tin, ug/1 0.05 100.0 0.20 J 0.21 J --- U --- U 0.24 J 12/07/20 HMM EPA200.8 Vanadium, ug/1 0.04 1.0 2.9 1.4 1.5 2.0 1.6 12/14/20 HMM EPA200.8 Zinc, ug/1 0.17 10.0 1,3 J 2.2 J 0.68 J 1.7 J 1.2 J 12/07/20 HMM EPA200.8 Sulfide, ug/1 100 1000 --- U --- U --- U --- U --- U 12/05/20 LFJ 4500S2D-11 Conductivity (at 25c), uMhos/cm 1.0 1.0 364 644 390 890 1527 12/02/20 PJC 25105-11 Dissolved Oxygen, mg/1 0.1 0.1 1.31 0.58 0.61 0,65 0.49 12/02/20 PJC 45000G-11 °C 16 15 17 16 18 12/02/20 PJC 2550E-10 Temperature, Static Water Level, feet 6.75 5.40 8.89 7.50 5.70 12/02/20 PJC well Depth, feet 15.98 9.50 16.65 16.33 20.26 12/02/20 PJC +86 +88 +85 +112 +113 12/02/20 PJC 2580E-11 GRP, my Turbidity (Field), NTU 1.0 1.0 9.70 6.42 8.43 21.90 7.03 12/02/20 PJC 2130E-11 J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 [ �dopb[fln MM % a[N�@TpooQa�c�d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: _' V PESTICIDES AND PCB'S EPA METHOD 8081B R2(07) CLIENT ID: Drinking Water ID: 37715 Wastewater ID.: 10 �.mimr PHONE (252) 756-6208 FAX (252) 756-0633 6003 ANALYST: HIC DATE COLLECTED: 12/02/20 DATE EXTRACTED: 12/04/20 DATE ANALYZED: 12/16/20 DATE REPORTED: 05/24/21 MW-4 MW-5 MW-6 MW-7 MW-8 PARAMETERS, u911 MDL MRL 1. Aldrin 0.029 0.050 --- U --- U --- V --- U --- U 2. Alpha-BHC 0.032 0.050 --- U --- U --- U --- U ""- U 3. Seta-BHC 0,031 0.050 --- U --- U -"- U --- U --- U 4. Delta-BHC 0.030 0.050 --- U --- U -'" U --- U U 5. Qamma-BHC (Lindane) 0.032 0.050 --- U --- U --- U --- u --- U 6. Chlordane 0.320 0.500 --- U --- U --- U --- V ""- U 7. 4,4-ADD 0,051 0.100 --- U --- U --- U --- U --- U 8, 4,4-DDE 0.049 0,100 --- U --- U --- U --- U --- U 9. 4,4-DDT 0.052 0.100 --- U --- U "-- U --- V --- U 10. Dieldrin 0.042 0.075 --- U --- V --- Ti --- U --- U 11. Endoeulfan I 0,056 0.100 --- U --- U --- U --- U --- V 12. Endoeulfan 11 0.046 0.100 --- U --- U --- U --- U --- U 13. Endoeulfan Sulfate 0.072 0.100 --- U --- U --- U --- U --- U 14. Endrin 0.053 0.100 --- U --- U --- U --- U --- U 15. Endrin Aldehyde 0.068 0.100 --- U --- U --- U "-- U -" U 16. Heptachlor 0.039 0.050 --- U --- U --- U --- U --- U 17, Heptachlor Epoxide 0.042 0.075 --- U --- U --- U --- U U 18. Methoxychler 0,530 1.000 --- U --- U --- U --- U --- U 19, Pcb-e (Aroclors) 0.500 2,000 --- U --- V --- U --- U --- U 20. Toxaphene 0,690 1.500 --- V --- U -"" U --- U - U J < Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 E HT(M[Nngfl� % �flriz�®Tp@�N%d Drinking Water ID; 37715 Wamtew4Lter IDa 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; LANDFILL APPENDIX II EPA METHOD 8151A R1(96) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: HIC DATE COLLECTED: 12/02/20 DATE EXTRACTED: 12/08/20 DATE ANALYZED: 12/10/20 DATE REPORTED: 05/24/21 MW-4 MW-5 MW-6 MW-7 MW-8 PARAMETERS, ug/l MDL MRL 1. 2,4-D 0.36 2.000 --- U --- U --- U --- U --- u 2. Dinoeeb 0.54 1.000 --- U --- U --- U --- U »-- U 3. 2,4,5-TP 0.42 2.000 --- U --- V --- U --- U --- U 4, 2,4,5-T 0.47 2.000 --- U --- U --- V --- U --- U a - Estimated value between the MDL and MRL, U a Below ALL 4uantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Nim,mmumA Flo RumpumUd Drinking Water ID; 37715 Wa:otawater :LDI ZB• 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 1 DATE EXTRACTED: 12/03/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/29/20 MW-4 12/31/20 NW-5 12/29/20 MW-6 12/29/20 MW-7 12/29/20 MW-B 1, Acenaphthene 2166 10.000 --- U --- U --- U --- U --- U 2, Acenaphthylene 2.60 10,000 --- U --- U --- U --- U --- U 3, Anthracene 2.97 10.000 --- U --- U --- U --- U --- U 4, Benzo[a]antrhacene 4.16 10,000 --- U »-- U --- U --- U --- U 5. Benzo[b]fluoranthene 3.32 10.000 --- U --- U --- U --- U --- U 6. Benzo[klfluoranthene 4.23 10.000 --- U --- U --- U --- U --- U 7. Benzo[g,h,i]perylene 2.61 10,000 --- U --- V --- U --- U --- U 8. Benzo(alpyrene 3.27 10.000 --- U --- U --- U --- U --- U 9. 4-Bromophenyl Phenyl Ether 2,63 10,c00 --- U --- U --- U --- U --- V 10. Butyl Banzyl Phthalate 5.78 10.000 --- U --- U --- V --- U --- V 11, Bis(2-Chloroethoxy) Methane 3.14 I0.000 --- U --- U --- U --- U --- U 12. Bis(2»Chloroethyl) Ether 2.59 10.000 --- U --- U --- U --- U --- U 13. Bis(2-Chloro-l-methylethyl) Ether 2.58 10.000 --- U --- U --- U --- U --- U 14, 2-Chloronaphthalene 2.17 10.000 --- U --- U --- U --- U --- U 15. 4-Chlorophenyl Phenyl Ether 2.42 10,000 --- U --- U --- U --- U --- U 16, Chrymene 4.04 10,000 --- U --- U --- U --- U --- U 17. Dibenzo[a,h]anthracene 2.78 10.000 --- U --- U --- U --- U --- U 18. ❑i-N-Butyl Phthalate 3.09 10.000 --- U --- U --- U --- U --- U 19. Dimethyl Phthalata 3.78 10,000 --- U --- U --- U --- U -" U 20. Diethyl Phthalate 3.92 10.000 --- U --- U --- V --- U --- U 21. 2,4-Dinitrotoluene 3.95 10,000 --- U --- U --- U --- U --- U 22. 2,6-trinitrotoluene 3.88 10.000 »-- U --- U --- U --- U --- U 23. Di-N-Octyl Phthalate 2.01 10.000 --- U --- U --- U --- U --- U 24. Bis-(2-Ethylhexyl) Phthalate 9.97 15.000 --- U --- U --- U --- U --- V 25, Fluoranthene 3.92 10.000 --- U --- U --- U --- U --- V 26. nluorene 2.95 10.000 --- U --- U --- U --- U --- V 27, Hexachlorobenzene 2.61 10.000 --- U --- U --- U --- U --- U 26. Hexachlorocyclopentadiene 4.16 10.000 --- U --- U --- U --- U --- U 29. Indeno[1,2,3-Cd]pyrene 2.91 10.000 --- U --- U --- U --- U --- U 30. Isophorone 3.74 10.000 --- U --- U --- U --- U --- U 31. Nitrobenzene 2.85 10.000 --- U --- U --- U --- U --- U 32, N-Nitrosodimethylamine 4.25 10.000 --- U --- U --- U --- U --- U 33. N-Nitrosodiphenylamine 3.95 10.000 --- U --- U --- U --- V --- U 34, N-Nitrosodi-N-Propylamine 4.06 10.000 --- U --- U --- U --- U --- U 35. Phenanthrene 3.24 10.000 --- U --- U --- U --- U --- U 36. Pyrene 3.63 10.000 --- U --- U --- U --- U --- U 37. 4-Chloro-3-Methylphenol 3.79 20.000 --- U --- U --- U --- U --- U 3B, 2-Chlorophenol 2175 10.000 --- U --- U --- U --- U --- U 39. O-Cresol 3.68 10.000 --- U --- U --- U --- U --- U 40. P-Cresol 4.12 10.000 --- U --- U --- U --- U --- U 91. 2,4-Dichlorophenol 5.19 10.000 --- U --- U --- U --- U --- U 42. 2,6-Dichlorophenol 4.89 10.000 --- U --- U --- U --- U --- U 43. 2,4-Dimethylphenol 3.21 10.000 --- U --- U --- U --- U --- U 44. 4.6-Dinitro-2-Methylphenol 9.77 SO.DDO --- u --- U --- U --- U --- U 45. 2,4-Dinitrophenol 4.37 50.000 --- U --- U --- U --- U --- U 46, Ethyl Methanesulfonate 5,26 20.000 --- U --- U --- U --- U --- U 47. Methyl Methanesulfonate 4.92 10.000 --- U --- U --- U --- U --- U J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limita, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EmW'0r@Efl(@M % hcarpumbd Drinking Water ID; 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: �✓ + ` SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 DATE EXTRACTED: 12/03/20 DATE REPORTED: 05/24/21 Page: 2 PARAMETERS, ug/l Date MDL Analyzed MRL 12/29/20 MW-4 12/31/20 KW-5 12/29/20 MW-6 12/29/20 MW-7 12/29/20 MW-8 48. 2-Nitrophenol 3.64 10.000 --- U --- U --- U --- U --- U 49. 4-Nitrophenol 3.17 50.000 --- U --- U --- U --- U --- U 50. Pentachlorophenol 5.33 25.000 --- U --- U --- U --- U --- U 51. Phenol 1.86 10A 00 --- U --- U --- U --- U --- U 52. 2,3,4,6-Tetrachlorophenol 3.12 10,000 --- U --- U --- U --- U --- U 53. 2,4,5-Trichlorophenol 4.17 10.000 --- U --- U --- U --- U --- U 54. 2,4,6-Trichlorophenol 3.84 10.000 --- U --- V --- U --- U --- U 55. Acetophenone 2.89 10.000 --- U --- U --- U --- U --- U 56. 2-Acetylaminofluarene 3.98 20.000 --- U --- U --- U --- U --- U 57, 4-Aminobiphenyl 4.12 20.000 --- U --- U --- U --- U --- U 50. Benzyl Alcohol 4.47 20.000 --- U --- U --- U --- U --- U 59. 4-Chloroaniline 3.36 20,000 --- U --- U --- U --- U --- U 60, Chlorobenzilate 5.12 10.000 --- V --- U --- U --- U --- U 61. Diallate 2.90 10.000 --- U --- U --- U --- U --- U 62. Dibenzofuran 4.20 10.000 --- U --- U --- U --- U --- U 63, 3,31-Dichlorobenzidine 4.22 20.000 --- U --- U --- U --- U --- U 64. ❑imethoate 3.98 20,000 --- U --- U --- U --- U --- U 65, P-Dimethylaminoazobenzene 2.99 10.000 --- U --- U --- U --- U --^ U 66. 7,12-Dimethylbenz[a]anthracene 5.26 10.000 --- U --- U --- V --- U --- U 67, 3,3-Dimethylbenzidine 3.21 10.000 --- U --- U --- U --- U --- V 68. 1,3-Dinitrobenzene 2.89 20.000 --- U --- U --- U --- U --- U 69. Diphenylamine 5.10 10.000 --- U -»- U --- U --- U --- U 70. Disulfoton 4.28 10.000 --- U --- U --- U --- U --- U 71. Famphur 3.98 20A 00 --- U --- U --- U --- U --- V 72. Hexachloropropene 4.31 10.000 --- U --- U --- U --- U --- V 73. Isosafrole 2.98 10A 00 --- U --- U --- U --- U --- 11 74. Kepone 2.78 20.000 --- U --- U --- U --- U --- U 75. Methapyrilene 3.54 100.000 --- U --- U --- U --- U --- U 76. 3-Metbylcholanthrene 4.21 10,000 --- U --- U --- V --- U --- U T7. 2-Methylnaphthalene 3.79 10,000 --- U --- U --- U --- U --- U 78. Methyl Parathion 4.32 10.000 --- U --- U --- U --- U --- U 79. m-Cresol 3Al 10.000 --- U --- U --- U --- U --- U 80. 1,4-Naphthoquinone 4.00 10.000 --- U --- U --- U --- U --- U 81. 1-Naphthylamine 5.61 10.000 --- U --- U --- U --- U ..._ U 82, 2»Naphthylamine 4.62 10,000 --- U --- U --- U --- U --- U 83. 2-Nitroaniline 3.61 50.000 --- U --- U --- U --- U --- U 84. 3-Nitroaniline 4,81 50.000 --- U --- U --» U --- U --- U 85. 4-Nitroaniline 4.22 20,000 --- U --- U --- U --- U --- U 86. 5-Nitro-D-Toluldine 4.01 10.000 --- U --- U --- U --- U --- U 87. N-Nitrosodi-n-butylamine 3.63 10,000 --- U --- U --- U --- U --- U 08. N-Nitrosodiethylamine 3.83 20.000 --- U --- U --- U --- U --- U 89. N-Nitrosomethylethylamine 3.83 10.000 --- o --- U --- U --- U --- U 90. N-Nitrosopiperidine 5.19 20.000 --- U --- U --- U --- U _-- U 91. N-Nitrosopyrrolidine 2.69 10.000 --- U --- iJ --- U --- U --- U 92. Parathion 3.12 10.000 --- U --- U --- U --- U --- U 93. Pentachlorobenzene 3.92 10.000 --- U --- U --- U --- U --- U 94. Pentachloronitrobenzene 3.71 20,000 --- U --- U --- V --- U --- U J - estimated value between the MDL and MRL, U = Below ALL Uuantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EflwkwuobM % Ngwpo © mhd Drinking Water ID; 37715 Wastewater IM 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: /�/ ` PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT,' ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 3 DATE EXTRACTED: 12/03/20 DATE REPORTED: 05/24/21 SEMI -VOLATILE ORGANICS PPA MF.Twnn A27OR R6 (18) Date Analyzed PARAMETERS, ug/l MDL MRL 12/29/20 MW-4 12/31/20 14W-5 12/29/20 MW-6 12/29/20 MW-7 12/29/20 MW-8 95, Phenacetin 4.41 20.000 --- U --- U --- U --- Ti --- U 96, 1,4-Benzenediamine 2.99 10.000 --- U --- U --- U --- U --- U 97. Phorate 3.86 10.000 --- U --- U --- U --- V --- U 98. Pronamide 3.69 10,000 --- U --- U --- U --- U --- U 99. Safrole 4.12 10.000 --- U --- U --- U --- U --- U 100. 1,2,4,5-Tetrachlorobenzene 5.01 10.000 --- U --- U -"" U --- U "-- U 101. Thionazin 4.62 20.000 --- U --- U --- V --- U --- U 102. O-Toluidine 4.11 10.000 --- U --- U --- U --- U --- U 103. 1,3,5-Trinitrobenzene 3.90 10.000 --- U --- U --- U --- U --- ll 104. 0,0,0-Triethyl PhosQhorothioate 3.61 10.000 --- U --- U --- U --- U --- U 105. Hexachloroethane 1.49 10.000 --- U --- U --- U --- U --- U 106. loodrin 3.21 20.000 --- U --- U --- U --- V --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. NOTE: EPA METHOD 8270E R6 (18): M W-8: One of sir Internal Standards exceeded lower recovery limit. No analytes detected above MDL. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID: 37715 W.jWr*gwi ;- iD:l. 10. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: /' ✓ `✓ �/ �' LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 1 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/11/20 MW-4 12/11/20 MW-5 12/11/20 MW-6 12/11/20 MW-7 12/12/20 MW-6 1. chlaromethane 0.77 3,000 --- U --- U --- U --- U _-- U 2, vinyl Chloride 0.12 0.200 --- U --- U --- V --- U --- U 3. BrDmomethane 0.67 10.000 --- U --- U --- U --- U --- U 4. Chloroethane 0.48 10.000 --- U --- U --- U --- U --- U 5. Trichlorofluoromethane 0.24 1.000 --- U --- U --- U --- U --- U 6. 1,1-Dichloroethene 0.17 5.000 --- U --- V --- U --- U --- U 7. Acetone 9.06 100.000 --- U --_ U --- V --- U --- U 8, Iodomethane 0.26 10.000 --- U --- U --- U --- U --- U 9. Carbon DisulEide 0.23 100.000 --- U --- U --- U --- U --- U 10. Methylene Chloride 0,64 1.000 --- U --- U --- U --- U --- V 11. tram -1,2-Dichloroethene 0.23 5.000 --- U --- U --- U --- U --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U --- U --- U 13. vinyl Acetate 0.20 50.000 --- U --- U --- U --- U "- U 14. Cie-1,2-Dichloxoethane 0.25 5.000 --- U --- U --- U --- U --- U 15, 2-Butanone 2.21 100.000 --- U --- U --- V --- U --- U 16. Bromochloromethane 0.27 3.000 --- U --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U --- U --- U IS, 1,1,1-Trichloroethane 0.19 1.000 --- U --- U --- D --- U --- U 19. Carbon Tetrachloride 0.04 0.200 -_- U ___ V ___ a --- U --- U 20. Benzene 0.24 1.000 --- U --- U --- U --- U --- U 21. 1,2-Dichloroethane 0.02 0.200 --- U --- U --- U --- U --- U 22, Trichloroethane 0,23 1.000 --- U --- U --- U --- V --- U 23. 1,2-nichloropropane 0.04 0.200 --- U --- V __- U ___ U ___ U 24. Bromodichloromethene 0.04 0,200 --- U --- U --- U --- U --- U 25. Cis-1,3-nichloropropene 0.06 0.200 --- U --- U --- U --- U --- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U --- U --- U --- U --- U 27. Toluene 0.23 1.000 --- U --- U --- U --- U --- U 28. trans-1,3-nichloropropene 0.04 0.200 --- U --- U --- U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0.200 --- U --- U U --- U --- U 30. Tetrachloroethene 0.10 0.200 --- U --- U --- U --- U --- U 31. 2-Hexanone 1.57 50.000 --- U --- U --- U --- U --- U 32. Dibromochloromethane 0,03 0.200 --- U --- U --- V --- U --- U 33. 1,2-Dibromoethane 0.03 0.200 --- U --- U --- U --- U --- U 34. Chlorobenzone 0.30 3.000 --- U --- U --- U --- U --- V 35. 1,1,1,2-Tetrach1oroethane 0.22 1.000 --- U --- U --- U --- U --- U 36. Ethylbenzene 0121 1.000 --- U --- U --- U --- U --- U 37. Xylenes 0.68 5.000 --- U --- U --- U --- U --- U 38. Dibromomethane 0.29 10.000 --- U --- U --- U --- U --- U 39. Styrene 0.19 1,p00 --- U --- U --- U --- U --- U 40. Bromoform 0.20 3.000 --- U --- U --- U --- U --- U 41, 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- U --- V --- U 42. 1,2,3-Trichloropropane 0.09 0.200 --- U --- U --- U --- U --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U --- U --- U --- U --- U 44. 1,2-Dichlorobenzene 0.32 5.000 --- U --- U --- U --- U --- U 45, 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- U --- U --- U --- U --- U 46. Acrylonitrile 2,72 200.000 --- U --- U --- U --- U --- U 47. trans-1,4-1)ichloro-2-Butene 0.42 100.000 --- U --- U --- U --- U --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EIMOT(hin@10 I hrLL-MTP(wdbd Drinking Water ID: 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC, MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED; 12/02/20 Page: 2 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 Date MDL Analyzed MRL 12/11/20 KW-4 12/21/20 14w-5 12/11/20 MW-6 12/11/20 MW-7 12/12/20 MW-a 48. Acrolein 1,97 4.000 --- U --- U --- U --- U --- U 49. Allyl Chloride 0.20 10.000 --- U --- V --- U --- U --- U 50. Chloroprone 0.21 20.000 --- U --- V --- U --- U --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U --- U »-- U --- U --- U 52, Dichlorodifluoromethane 0,51 5.000 --- U --- U --- U --- U --- U 53, 1,3-Dichloroprapane 0.26 1.000 --- U --- U --- U --- U --- U 54, 2,2-Dichloropropane 0.17 15.000 --- U --- U --- U --- U --- U 55. 1,1-Dichloropropene 0.22 5.000 --- U --- U --- U --- U --- U 56, Ethyl Methacrylate 0.16 10,000 --- U --- U --- U --- U --- U 57. Hexachlorobutadiene 0.10 0.200 --- U --- U --- U --- U --- U 58. Isobutyl Alcohol 12.80 100.000 --- U --- U --- U --- U --- U 59, Methacrylonitrile 1.93 100.000 --- U --- U --- U --- U --- U 60. Methyl Methacrylate 0.25 30.090 --- U --- U --- U --- U --- U 61. Naphthalene 0.47 6.000 --- U --- U --- U --- U --- U 62. Propionitrile 3.26 150.000 --- U --- U --- U --- U --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U _-- U --- U --- U --- U 64, Acetanitrile 36.29 55.000 --- U --- U --- U --- U --- U 65, Tetrahydroturan 0.39 1.000 --- U 1.05 --- U 3.23 7.94 66. 1,4-Dioxane 2.71 3.000 --- U 7.22 --- U --- U 36.50 ,7 = Estimated value between the MDL and MRL, U - Below ALL 4uantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID; 37715 Wag.tewgter SDI 10: 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: v LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 3 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/11/20 Trip Blank 1. Chloromethane 0.77 3.000 --- U 2, Vinyl Chloride 0.12 0.200 --- U 3. Bromomethane 0.67 10.000 --- U 4. Chloroetbane. 0.48 10.000 --- Ti 5. Trichlorofluoromethane 0.24 1.000 --- U 6. 1,1-Dichloroethene 0.17 5.000 --- U 7. Acetone 9.06 100.000 --- U S. iodomethane 0.26 10.000 --- U 9, Carbon Disulfide 0.23 100.000 --- V 10, Methylene Chloride 0.64 1.000 --- U 11. trane-1,2-Dichloroethene 0.23 5.000 --- U 12. 1,1-Dichloreethane 0.20 5.000 --- U 13. Vinyl Acetate 0,20 50.000 --- U 14. Cie-1,2-Dichloroethene 0.25 5.000 --- U 15. 2-Butanone 2.21 100.000 --- U 16. Bromochloromethane 0.27 3.000 --- U 17. Chloroform 0.25 5.000 --- U 18. 1,1,1-Trichloroethane 0.19 1,000 --- U 19. Carbon Tetrachloride 0.04 0.200 --- U 20. Benzene 0.24 1.000 --- V 21. 1,2-Dichloroethene 0.02 0.200 0.05 d 22. Trichloreethene 0.23 1,000 --- U 23. 1,2-Dichloropropane 0.04 0.200 0.06 J 24. Bromodichloromethane 0.04 0.200 0.06 J 25. Cie-1,3-Dichloropropene 0.06 0.200 --- U 26, 4-Methyl-2-Pentanone 1,19 100.000 --- U 27. Toluene 0.23 1.000 --- U 28. trane-1,3-Dichloropropene 0.04 0.200 --- U 29. 1,1,2-Trichloroethane 0.03 0.200 0.04 J 30. Tetrachloroethene 0.10 0.200 --- U 31, 2-Hexanone 1.57 50.000 --- U 32, Dibromochloromethane 0.03 0.200 0.05 J 33. 1,2-Dibromoethane 0.03 0.200 0.03 17 34. Chlorobenzene 0.30 3.000 --- U 35. 1,1,1,2-Tetrachlorcethane 0.22 1.000 --- U 36, Ethylbenzene 0,21 1.000 --- U 37. Xylenes 0.68 5.000 --- U 38. Dibromomethane 0.28 10,000 --- U 39, Styrene 0.19 1.000 --- U 40. Bromoform 0.20 3.000 --- V 41. 1,1,2,2-Tetrachloroethane 0,03 0.200 --- U 42, 1,2,3-Trichloropropane 0.09 0.200 --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U 44. 1,2-Dichlorobenzene 0.32 5.000 --- U 45, 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- U 46. Acrylonitrile 2.72 200.000 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.000 --- U S = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EflAmuffmW % kwumUd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking Water IDi 37715 A-_ - PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 4 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/11/20 Trip Blank 48. Acrolein 1.97 4.000 --- U 49. Allyl Chloride 0.20 10.000 --- U 50. Chloroprene 0.21 20.000 --- Ti 51. 1,3-Dichlorobenzene 0.41 5.000 --- U 52, Dichlorodifluoromethane 0.51 5.000 --- U 53. 1,3-Dichloropropane 0.20 1.000 --- U 54. 2,2-Dichloropropane 0,17 15.000 --- U 55. 1,1-Dichloropropene 0.22 5.000 --- U 56. Ethyl Methacrylate 0.16 10.000 --- U 57. Hexachlerabutadiene 0.10 0.200 --- U 58, laobutyl Alcohol 12.80 100,000 --- U 59, Methaerylonitrile 1.93 100.000 --- U 60. Methyl Methacrylate 0.25 30.000 --- U 61. Naphthalene 0.47 6,000 --- U 62. Propionitrile 3.26 150.000 --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U 64, Acetanitrile 36,29 55.000 --- U 65. Tetrahydrofuran 0.39 1.000 --- U 66, 1,4-Dioxane 2,71 3.000 --- U J = Estimated value between the MDT, and MRL, U = Below ALL Quantitation Limita. DocuSi 0 N 4 3 0 m CD C cb CD co C rn � w w � c C C)m m cr 0 6 m _ cr o 0 0 m � 0 0 N y n f° =r w w 3 ;v m � o m CD w 0 G) c m C o. V. W co IV O gn tnveiope w: I -ICI <D C z z Iz a zi rA r Q F w �0 a< n� O D td oA �t C z l�7 C �n� m m C i y ,-,0 �" CC"1 0' 4, 8 l� to, z� v rn e w O G7 GG) L V' N C Fi yd N � J o J r m m m z w ➢� 6J c m ro TOTAL CHLORINE, mg/l q j� U L m 0 n OR ugll AT COLLECTION v, 8 m m o — - — TEMPERATURE, °C E� J U� AT COLLECTION r S) Gl S7 z z A o a o 00 # OF CONTAINERS r Field pH ti r; ¢,..; Nitrate -Nitrite -0; Alkalinity > Chloride Y "d Cyanide y m m TDS Y ro m Sulfate > ro 3 ..,: <<> Metals Y �o m Sulfide d Conductivity DC ro 'Temperature r; >: Field Parameter EPA 8276E > 8270E Dup. 1 :a EPA 808113 G) PARAMETERS/TESTS Fn o z 'D j� j� 0 L L L m �? m a c� z = O z i fie' � 8 �r o y = z �r o m rn x m m C f I,/111 ? O m CC C o C z � G� „ m o �_ G) 0 z r, z— crn y c' N n z F c m C m� � > Q mq z < D > O � m o 0 Do74. DOCUSi 0 m n m m m cn r_a 0 0 C iv CD CD � w s F r-5 w 0 a- o n CD o o -o 0 ro cn w � w w � w � 3 (D m o � w m G C CD CD C1 O fV O C) gn tYC1T�veiope IU: bS).Jt)bt5A-/U.St-4r-UZ-y4AZ5-"ly4yyUbb-ittS"1 •' O C rp z z t z 0 0C=l� y a o �rti rrz �R , r. o W ` t-jr �Q Cl CA A � y • m n y tv � N y-a O O n ry b p n N o m- m r c � m �t m m rn TOTAL CHLORINE, mg/l C7 m mbo m OR ug/l AT COLLECTION C C C O C TEMPERATURE,°C �, J AT COLLECTION t O i a A ago 00 o �# OF CONTAINERS z 8081B Duplicate Ga 8260D App. II G� 8260D App. II 2 M q� �N 1 8260D App. 113 4� 8260D App. II 4 til 0 N J t� 8151A Landfill G� t� m m rn...... uJ 8151A Duplicate ORP m m S� G C w c Z � `1 p, m u n zU-) PARAMETERS/TESTS z 2 m O _ r0 to '> M C) m n n n m C7 ao m 0 Ri �o T n 2 Z r Cn m m� T m m mP` � m C ,/L`��Jco O z tyn O <O m m -u 9 m ilf S q 4 = Q ern/ 0 (n m C7 M yy Z O � n r� W m� Z = m � n n m r�r g o 0 n m t+ C O mm m O O � a = 00 N N 0 n92?!Z T DocuS 0 M �C", w 3 o- � w m N (ri (D CD n_ 0 0 C5 w - w o 0 n m o0 0 m n W CD U) w w � CD CD 0 CD w 10 lull LI vu—pG m m m JY JJVVU I H I cn Vy ^ �1 ,�1 p e n o D v p --� ru C) n O0 L�7 ` D i l' _ �, n \0 P� a r �a P Qz y cv a 0 prp t. v 0 �o cn L l E C a H r M O Y n 1J N u N th M 73 Y rn 3-) O w J I G M TOTAL CHLORINE, mg/l p n m n OR ug/I AT COLLECTION 0 © 0 z [ n o C r — TEMPERATURE, °C < m _ C ATCOLLECTION m O -En- c5 [n E5 [n O z A CD# OF CONTAINERS Field pH b Nitrate_Nitrite n ''� Alkalinity 9 + Chloride ti Cyanide C d no i� n 9j TDS m M m Sulfate o Metals ro Sulfide m Conductivity > DO �- Temperature ti Field Parameter U <. .. EPA 8270E Y 0 r a 8270E Dup. 1 0 EPA 8081B +n 0 2: Cn a PARAMETERS/TESTS (D n 2 _ r m cr)R h m CD�? Lj Lj W a n n 0z C7 Or �° z' z z a rn pcl m m cn �' C y O O z m M M Q 3 n-o z —tenCD M „ m o '� C v a r Z rI iTt m m cn n y z N x z > m yr j Z m y r�r o p O c) a z o M oa Do z O 0 o k T m N D- M z _< z v' n m m 9 Un 0 0 n O z DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499 m t:r: m 4t c_- C7 cn m 0 Ua M 0 U3 M 0 In G) m M131 EB1 m cn a b 21 00 z (0 d = r" 0 �3 0 t�) x E� > 4 2 J'J 00 -4 00 cn c T ri P 0 Ro >1 C CD —" tA ;7j 0 F- r- �j 71 0 uj m mM) m m TOTAL CHLORINE, mg/1 0 OR ug/I AT COLLECTION m < m m m ED m 0 TEMPERATURE,C 0 U0 0 co < UD ATCOLLECTION z P P P AOFCONTAINERS t z 8081B Duplicate 8260D App. II G� Cis . .. ...... 8260D App. 112 CN 8260D App. 113 01 0 8260D App. 114 m . ...... m m 81SIA La,dfiu x 8 51A Duplicate 0 ORP m PARAMETERS/TESTS 7L 0 CT m cn CD m x m m m EO F-i CCD1 cl) 0 0 t7l m x m m 0 < m -n �)TC r- 2S -n M m -rn m 0 --a CD m tD co 75 m t 0 N m w UP Up CD �::: m co z �D- 0 :� a: > z m Ez m FD CO C-) 0 < M < 0 rn z m > 0 z n 0 i� M DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 LINWH'T ammd % h(-rU--,-wP0wO gd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS CLIENT ID ANALYST: DATE COLLECTED: DATE ANALYZED: DATE REPORTED: PHONE (252) 756-6208 FAX (252) 756-0633 6003 JP 12/02/20 12/11/20 - 12/12/20 05/24/21 PARAMETERS, ug/1 HDL MRL Concentration 1. Chloromethane 0.77 3.00 --- U 2. Vinyl Chloride 0.12 0.20 --- U 3. Bromomethane 0.67 10.00 --- U 4. Chloroethane 0.48 10.00 --- U 5, Trichlorofluoromethane 0.24 1.00 --- U 6. 1,1-Dichloroethene 0.17 5.00 --- U 7. Acetone 9.06 100.00 --- U 8. Iodomethane 0.26 10.00 --- U 9. Carbon Disulfide 0.23 100.00 --- U 10, Methylene Chloride 0.64 1.00 --- U 11. trans-1,2-Dichloroethene 0.23 5.00 --- U 12. 1,1-Dichloroethane 0.20 5.00 --- U 13. Vinyl Acetate 0.20 50.00 --- U 14. cis-1,2--Dichloroethene 0.25 5.00 --- U 15. 2-Butanone 2.21 100.00 --- U 16. Bromochloromethane 0.27 3.00 --- U 17. Chloroform 0.25 5.00 --- U 18. 1,1,1-Trichloroethane 0.19 1.00 --- U 19. Carbon Tetrachloride 0.04 0.20 --- U 20. Benzene 0.24 1.00 ---- U 21. 1,2-Dichloroethane 0.02 0.20 --- U 22. Trichloraethene 0.23 1.00 --- U 23. 1,2-Dichloropropane 0.04 0.20 --- U 24. Bromodichloromethane 0.04 0.20 ---- U 25. cis-1,3-Dichloropropene 0.06 0.20 --- U 26. 4-methyl-2-Pentanone 1.19 100.00 --- U 27. Toluene 0.23 1.00 ---- U 28. trans-1,3-Dichloropropene 0.04 0.20 --- U 29. 1,1,2-Trichloroethane 0.03 0.20 ---- U 30. Tetrachloroethene 0.10 0.20 --- U 31. 2-Hexanone 1.57 40.00 --- U 32. Dibromochloromethane 0.03 0.20 --- U 33. 1,2-Dibromoethane 0.03 0.20 --- U 34. Chlorobenzene 0.30 3.00 --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.00 --- U 36. Ethylbenzene 0.21 1.00 --- U 37. Xylenes 0.68 5.00 ---- U 38. Dibromomethane 0.28 10.00 --- U 39, Styrene 0.19 1.00 --- U 40. Bromo£orm 0.20 3.00 --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.20 --- U 42. 1,2,3-Trichloropropane 0.09 0.20 --- U 43. 1,4-Dichlorobenzene 0.39 1.00 --- U 44. 1,2-Dichlorobenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- U 46. Acrylonitrile 2.72 200.00 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.00 --- U 48. Acrolein 1.97 4.00 --- U 49. Allyl Chloride 0.20 10.00 ---- U 50. Chloroprene 1 0.21 20.00 --- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EINWT@Rflffl0� % a�c�or�p@F0%4 114 OAKMON7 DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/02/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PARAMETERS, ug/1 MDL MRL Concentration 51. 1,3-Dichlorobenzene 0.41 5.00 --- U 52. Dichlorodifluoromethane 0.51 5.00 --- U 53. 1,3-Dichloropropane 0.28 1.00 --- U 54. 2,2-Dichloropropane 0.17 15.00 --- U 55. 1,1-Dichloropropene 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 --- U 57. Hexachlorobutadiene 0.10 0.20 --- U 58. Isobutyl Alcohol 12.80 100.00 --- U 59. Methacrylonitrile 1.93 100.00 --- U 60. Methyl Methacrylate 0.25 30.00 --- U 61. Naphthalene 0.47 6.00 --- U 62. Propionitrile 3.26 150.00 --- U 63. 1,2,4-Trichlorobenzene 0.50 10.00 --- U 64. Acetonitrile 36.29 55.00 --- U 65. Tetrahydrofuran 0.39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 -- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC, MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JP DATE COLLECTED: 12/02/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits ($ recovery) 1,2-DCA-d4 recovery) Toluene-d8 (% recovery) 4-EPB {$ recovery) Continuing Calibration std. 70-130 100 101 102 Method Blank 70-130 98.3 97.6 97.4 MW-4 70-130 104 102 101 MW-5 70-130 103 102 99.4 MW-6 70-130 101 99.9 97.1 MW-7 70-130 101 101 98.5 MW-8 70-130 99.3 99.4 97.5 Trip blank 70-130 102 100 98.2 6003 MW-4 M.S. 70-130 104 103 100 6003 MW-4 M.S.D. 70-130 104 102 100 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JP DATE COLLECTED: 12/02/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 r REVIEWE❑ BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPACE/MATRIX SPIKE DUPLICATE RESULTS Sample Spiked: (6003) MW-4 Spike Amount Ug/1 Sample Result Ug/1 Spike Result Ug/1 Spike Recovery (70-130%) Spike Dup. Result Ug/1 Spike Dup. Recovery (70-130%) MS/MSD RPD (2096) 1,1-Dichloroethene 20.0 --- U 23.38 117 22.4E 112 3.9 Benzene 20.0 --- U 22.93 115 21.43 107 6.8 Trichloroethene 20.0 --- U 22.59 113 21.46 107 5.1 Toluene 20.0 U 1 21.77 109 20.82 104 4.5 Chlorobenzene 20.0 --- U I 21.98 110 1 20.77 1 104 5.7 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount Ug/l Spike Result Ug/1 Spike Recovery (70--130%) 1,1-Dichloroethene 20.00 20.07 100 Benzene 20.00 20.06 100 Trichloroethene 20.00 20.16 101 Toluene 20.00 19.96 100 Chlorobenzene 20.00 20.11 101 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMON7 DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking Water ID: 31715 aatewater IDi 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 A DATE COLLECTED: 12/01/20 DATE REPORTED : 05/24/21 REVIEWED BY: MW-is MW-17i MW-28 MW-2D MW-39 Analysis Method PARAMETERS MDL MRL Date Analyst Code PH (field measurement), Unite 6.5 7.3 6.6 7.5 6.9 12/01/20 PJC 4500HB-11 Nitrate+Nitrite as N, mg/l 0,04 0.04 --- U --- U 1.55 0.22 0.37 12/02/20 KES 353,2 R2-9 Alkalinity (to pH 4.5), mg CaCO3/1 1.0 1.0 159 179 304 181 1580 12/07/20 JMS 2320E-11 Chloride, mg/1 5.0 5.0 10 13 50 13 213 12/07/20 TMR 4500CLB-11 Cyanide, u9/1 5.0 5.0 --- U --- U --- U --- U --- U 12/10/20 SECT 450OCNE-11 Total Dissolved Residue, mg/1 1.0 10 346 234 727 271 12/03/20 JMS 2540C-11 Total Dissolved Residue, mg/1 1.0 10 1960 12/08/20 HJO 254OC-11 Sulfate, mg/l 5.0 5.0 79.9 --- U 185 24.4 70.9 12/03/20 SEJ 4500SO42B1 Antimony, ug/l 0.03 1.0 0.12 J 0.12 J 0.20 J 0.14 J 0.21 J 12/07/20 HMM EPA200,8 Arsenic, ug/1 0.09 5.0 1.5 J 1.6 J 3.4 J 0,89 J 23 12/07/20 HMM EPA200.8 Barium, ug/1 0,04 10.0 34.3 24,4 116 16.0 034 12/07/20 HMM EPA200.8 Beryllium, ug/l 0.02 1.0 0.05 J --- U --- U --- U 0.04 J 12/07/20 HMM EPA200.8 Cadmium, ug/1 0.04 1.0 0.05 J --- U --- U --- U --- U 12/07/20 HMM EPA200.8 Cobalt, ug/1 0.02 1.0 0.42 J 0.12 J 1.34 0.19 J 4.9 12/07/20 HMM EPA200.8 Total Chromium, ug/1 0.12 5.0 0.46 J 0.36 J 2.7 J 0.46 J 26 12/14/20 HMM EPA200.8 Copper, ug/l 0.04 10,0 0.80 J 0.45 J 0.81 J 0,45 J 0.21 J 12/07/20 HMM EPA200.8 Iron, ug/1 4.96 50.0 1914 1984 4101 424 12/03/20 LFJ EPA200.7 Iron, ug/1 4.96 50.0 16867 12/21/20 LFd EPA200.7 Manganese, ug/1 0,31 10.0 15 123 219 16 12/03/20 LFJ EPA200.7 Manganese, ug/1 0.31 10.0 Res 12/21/20 LFJ EPA200.7 Lead, ug/1 0.03 5.0 0.82 J 0.09 J 0.29 J 0.12 J 0.10 J 12/07/20 HMM EPA200.8 Mercury, ug/l 0.05 0.20 --- U --- U --- U --- U --- U 12/09/20 MTM 245.1 R3-9 Nickel, ug/l 0.03 10.0 0.45 J 0.35 J 1.0 J 0.50 J 2.4 J 12/07/20 HMM EPA200.8 Selenium, ug/l 0.05 10.0 0.16 J 0.19 J 0.51 J 0.14 J 1,6 J 12/07/20 HMM EPA200.6 Silver, ug/l 0.22 5.0 --- U --- U --- U --- U --- U 12/07/20 HMM EPA200.8 Thallium, ug/l 0.02 1.0 0.20 J 0.50 J 0.14 J 0.12J --- U 12/07/20 HMM EPA200.8 Tin, ug/1 0.05 100.0 0.05 J --- U 0.20 J 0.19 J --- U 12/07/20 HUM EPA200.8 vanadium, ug/l 0.04 1.0 2.1 0.51 J Glee J 0.34 J 7.1 12/14/20 HMM EPA200.8 Zinc, ug/1 0.17 10.0 1.7 J 2.4 J 1.6 J 16 1.4 J 12/07/20 HMM EPA200.8 Sulfide, ug/1 100 1000 --- U --- U --- U --- U --- U 12/D5/20 LFJ 4500S2D-11 Conductivity (at 25c), uMhos/cm 1.0 1.0 452 393 1206 460 3768 12/01/20 PJC 2510E-11 Dissolved Oxygen, mg/1 0.1 0.1 0.60 0.21 0.91 0.41 0.91 12/01/20 PJC 450DOG-11 Temperature, °C Is 19 17 17 19 12/01/20 PJC 2550E-10 Static Water Level, feet 7.00 7.62 10.20 11.43 11.92 12/01/20 PJC Well Depth, feet 17.21 33.75 16.57 39.17 22.24 12/01/20 PJC ORP, my +12 +14 +79 +82 -54 12/01/20 PJC 25BOB-11 Turbidity (Field), NTU 1.0 1.0 8.88 8.77 4.40 2.92 3.13 12/01/20 PJC 2130E-11 J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ERAWOMM@10 % kwPumbd Drinking Water ID: 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 ID#: 6003 A PHONE (252) 756-6208 FAX (252) 756-0633 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE DATE COLLECTED: 12/01/20 GREENVILLE, NC 27834 DATE REPORTED : 05/24/21 REVIEWED BY: MW-3D MW-3A Trip Analysis Method PARAMETERS MDL MRL Blank Date Analyst Code PH (field measurement), Units 7.9 6.8 12/01/20 PJC 4500HB-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 0.27 --- U 12/02/20 KES 353.2 R2-93 Alkalinity (to pH 4.5), mg CaCO3/1 1.0 1.0 222 810 12/07/20 JMS 2320E-11 Chloride, mg/1 5.0 5,0 21 112 12/07/20 TMR 4500CLB-11 Cyanide, ug/l 5.0 5.0 --- U --- U 12/10/20 SEJ 450OCNE-ll Total Dissolved Residue, mg/1 1.0 10 320 1000 12/03/20 JMS 254OC-21 Sulfate, mg/l 5.0 5.0 5.8 46.7 12/03/20 SE,7 45008042EII Antimony, ug/l 0.03 1.0 0.15 J 0.16 J 12/07/20 HMM EPA200.8 Arsenic, ug/1 0.08 5.0 0.41 J 20 12/07/20 HUM EPA200.8 Barium, ug/l 0.04 10.0 10.0 253 12/07/20 HUM EPA200.8 Beryllium, ug/l 0.02 1.0 --- U 0.05 J 12/07/20 HMM EPA200.8 Cadmium, ug/l 0.04 1.0 --- U --- U 12/07/20 HMM EPA200.8 Cobalt, ug/l 0.02 1.0 0.06 J 5.0 12/07/20 HMM EPA200.8 Total Chromium, ug/1 0.12 5.0 --- U 11 12/14/20 HMM EPA200.8 Copper, ug/1 0.04 10.0 0.18J 0.15 J 12/07/20 HMM EPA200,8 Iron, ug/1 4.96 50.0 8 J 17644 12/21/20 LFJ EPA200,7 Manganese, ug/l 0.31 10.0 3 J 643 12/21/20 LFJ EPA200.7 Lead, ug/l 0.03 5.0 --- U 0.1117 12/07/20 HMM EPA200.8 Mercury, ug/l 0.05 0.20 --- U --- U 12/09/20 MTM 245.1 R3-94 Nickel, ug/l 0.03 10.0 0.21 J 2.1 J 12/07/20 HMM EPA200.8 Selenium, ug/l 0.05 1010 0.21 J 0.40 J 12/07/20 HMM EPA200.8 Silver, ug/l 0.22 5.0 --- U --- U 12/07/20 HMM EPA200.8 Thallium, ug/1 0.02 1.0 --- U 0.05 J 12/07/20 HMM EPA200.0 Tin, ug/l 0.05 100.0 0.29 J 0.25 J 12/07/20 HMM EPA200.8 vanadium, ug/l 0.04 1.0 0.15J 3.7 12/14/20 HMM EPA200.8 Zinc, ug/1 0.17 10.0 1.3 J 1.2 J 12/07/20 HMM EPA200.8 Sulfide, ug/l 100 1000 --- U --- U 12/05/20 LFJ 450OS21)-11 Conductivity (at 25c), uMhas/cm 1.0 1.0 539 2017 12/01/20 PJC 251OB-11 Dissolved Oxygen, mg/l 0.1 0.1 0.41 0.43 12/01/20 PJC 45000G-11 Temperature, °C 17 16 12/01/20 PJC 2550B-10 Static Water Level, feet 11.80 10.64 12/01/20 PJC Well Depth, feet 52.30 23.44 12/01/20 PJC ORP, my -1 -18 12/01/20 PJC 2580E-11 Turbidity (Field), NTU 1.0 1,0 1.17 6.07 12/01/20 PJC 2130E-11 J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ✓� ` PESTICIDES AND PCB'S EPA METHOD 8081B R2(07) Drinking Water ID: 37715 e tewater ID-t 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: HIC DATE COLLECTED: 12/01/20 Page: 1 DATE EXTRACTED: 12/04/20 DATE REPORTED: 05/24/21 Date Analyzed 12/15/20 12/15/20 12/15/20 12/15/20 12/16/20 KW -IS MW-ID MW-2S MW-2D KW-3S PARAMETERS, ug/1 45DL HRL 1. Aldrin 0.029 0.050 --- U --- V --- U --- U U 2. Alpha-BHC 0.032 0,050 --- U --- V "-- U _- 3. Beta-BHC 0.031 0.050 --- U --- U 4, Delta-BHC 0,030 0.050 --- U -"- U --- U U U 5, Gamma"BHC (Lindane) 0.032 0.050 --- U --- U --- U "-- 6. chlordane 0.320 0.500 --- U '-" U --- U --- U 7. 4,4-DDD 0.051 0.100 --- U --- U --- --- U U --- ❑ U S. 4,4-DDE 0.049 0.100 --- U --- U U -- U 9, 4,4-DDT 0.052 0,100 _-- V --- V--- U - U -- - U 10, Dieldrin 0.042 0.075 --- U --- U --- U --- --- U 11, sndosulfan I 0.056 0.100 --- U --- U --- U --- U 12. sndosulfan II 0.046 0.100 --- U --- U --- U --- U --- --- U V 13. sndoaulfan Sulfate 0.072 0.100 --- U --- V --- U --- U U 14. sndrin 0.053 0.100 --- U --- U --- U --- U --- 15, Endrin Aldehyde 0.066 0.100 --- V --- U --- U --- U U 16, Heptachlor 0.039 0.050 --- U --- U --- U =-- - U V --- U 17. Heptachlor Epoxide 0.042 0.075 --- U --- V --- U 0.530 1.000 --- U --- U --- U - - U -- U 10, 19. Methoxychlor Pcb's (Aroclors) 0.500 2.000 --- U --- V --^ U - - U _ ___ V 20. Toxaphene 0.690 1,500 -__ U ___ U ___ U ___ U J = Eatimated value between the MDL and MRL, U - Below ALL Quantitation Limita. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Em,nim(M Ala RM(C'mummUd Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PESTICIDES AND PCB'S EPA METHOD 8081E R2(07) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: HIC DATE COLLECTED: 12/01/20 Page: 2 DATE EXTRACTED: 12/04/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/15/20 MW-31) 12/15/20 MW-3A 1. Aldrin 0.029 0.050 --- U --- U 2. Alpha-BHC 0.032 0.050 --- U --- U 3. Beta-BHC 0.031 0.050 --- U --- U 4. Delta-BHC 0.030 0.050 --- U --- U 5. Gamma-BHC (Lindane) 0.032 0.050 --- U --- U 6. Chlordane 0.320 0.500 --- U --- U 7. 4,4-DDD 0.051 0.100 --- U --- U U. 4,4-DDE 0.049 0.100 --- U --- U 9. 4,4-DDT 0.052 0.100 --- U --- U 10. Dieldrin 0.042 0.075 --- U --- U 11. Endoeulfan 1 0.056 0.100 --- D --- U 12. Endoeulfan II 0.046 0.100 --- U --- U 13. Endoeulfan Sulfate 0.072 0.100 --- U --- U 14, Endrin 0.053 0.100 --- U --- U 15. Endrin Aldehyde 0.068 0.100 --- U --- U 16. Heptachlor 0.039 0.050 --- U --- U 17. Heptachlor Epoxide 0.042 0.075 --- U --- U 18. Methoxychlor 0.530 1.000 --- U --- U 19. Pcb's (Aroclore) 0.500 2.000 --- U --- U 20. Toxaphene 0.690 1.500 --- U --- U d = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Rad'ToRmid Ala hcupwNgdo Drinking Water IDi 37715 Wastewater IDi 10 114 OAKMON7 DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8151A R1(96) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: HIC DATE COLLECTED: 12/01/20 Page: 1 DATE EXTRACTED: 12/08/20 DATE ANALYZED: 12/10/20 DATE REPORTED: 05/24/21 MW-is MW-1D MW-2S MW-2D MW-35 PARAMETERS, ug/1 MDL MRL 1. 2,4-D 0.36 2.000 --- u --- u --- u --- u --- u 2. Dinoseb 0.54 1.000 --- a --- a --- u --- 17 --- U 3. 2,4,5-TP 0.42 2.000 --- u --- u --- u --- u --- u 4. 2,4,5-T 0.47 2.000 --- u --- u --- u --- u --- u d � Estimated value between the MDL and MRL, U t BeloW ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 h9oQp®�a�c�d Drinking Water ID: 37715 Waatewater IM 10 PHONE (252) 756-6208 FAX {252) 756-0633 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT In: 6003 A CLIENT; C & A DISPOSAL, INC. MR. JUDSON WHITEHURST ANALYST: RTC 802 RECYCLING LANE DATE COLLECTED: 12/01/20 Page: 2 GREENVILLE, NC 27834 DATE EXTRACTED: 12/08/20 DATE ANALYZED: 12/10/20 DATE REPORTED: 05/24/21 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8151A R1(96) MW-3D KW-3A MDL MRL PARAMETERS, ug/l -'- 0.36 2.000 _ _ U U- U 1. 2,4-D 0,54 1,000 --- U -- 2. Dinoaeb 0.42 2.000 --- U 0.51 S _-- u 3. 2,4,5-TP 0.47 2.000 -- U 4, 2,4,5-T J Eatlmated value between the MDL and MRL, U = Se1OW ALL Ruantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 DT@Uon [N� % �UgnQp@Tgftd........... 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, ITC 27834 REVIEWED BY: ✓,� SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Drinking Water ID: 37715 WAA "watex iDs. IA PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Page: 1 DATE EXTRACTED: 12/03/20 DATE ANALYZED: 12/29/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL MW-ls MW-lD MW-26 MW-2D MW-3s 1, Acenaphthene 2.66 10.000 --- U --- U --- U --- U 5.46 ,7 2. Acenaphthylene 2,60 10.000 --- U --- U --- U --- U --- U 3, Anthracene 2.91 10.000 --- U --- U --- U --- U --- U 4. Benzo[a)antrhacene 4.16 10.000 --- U --- U --- U --- U --- U 5. Benzo[b]fluoranthene 3.32 10.000 --- U --- U --- U --- U --- U 6, Benzo[k]fluoranthene 4.23 10.000 --- U --- U --- U --- U --- U 7. Benzo[g,h,i)perylene 2.61 10.000 --- U --- U --- U --- U --- U 8, Benzo[a]pyrena 3.27 10.000 --- U --- U --- U --- U --- U 9. 4-Bromophenyl Phenyl Ether 2.63 10.000 --- U --- U --- Ti --- U --- U 10, Butyl Benzyl Phthalate 5.78 10.000 --- U --- U --- V --- U --- U 11. Bis(2-Chloraethoxy) Methane 3.14 10.000 --- U --- U --- U --- U --- U 12. Bis(2-Chloroethyl) Ether 2.58 10.000 --- U --- U --- U --- U --- V 13. Bis(2-Chloro-l-methylethyl) Ether 2.58 10.000 --- U --- U --- U --- U --- U 14, 2-Chlaronaphthalene 2.17 10.000 --- U --- U --- U --- U --- U 15, 4-Chlorophenyl Phenyl Ether 2.42 10.000 --- U --- U --- Ti --- U --- U 16. Chrysene 4.04 10.000 --- U --- U --- U --- U --- U 17. Dibenzo[a,h]anthracene 2.78 10.000 --- U --- U --- U --- U --- U 18. Di-N-Butyl Phthalate 3.09 10.000 --- U --- U --- U --- U --- V 19. Dimethyl Phthalate 3.78 10.000 --» U --- U --- U --- U --- U 20. Diethyl Phthalate 3.92 10.000 --- U --- U --- U --- U --- U 21. 2,4-Dinitrotoluene 3.95 10,000 -»- U --- U --- U --- U --- V 22. 2,6-Dinitrotoluene 3.08 10.000 --- U --- U --- U --- U --- U 23. Di-N-Octyl Phthalate 2.81 10.000 --- U --- U --- U --- U --- U 24. Bis-(2-Ethylhexyl) Phthalate 9.97 15.000 --- U --- U --- U --- U --- U 25, Fluoranthene 2.92 10.000 --- U --- U --- U --- U --- V 26. Pluorene 2.95 10.000 --- U --- U --- U --- U --- U 27. Hexachlorobenzene 2.61 10.000 --- U --- U --- U --- U --- U 28. Hexachlorocyclopentadiene 4.16 10.000 --- U --- U --- U --- U --- U 29. Indeno[1,2,3-Cd]pyrene 2.91 10.000 --- U --- U --- V --- U --- U 30. Isophorone 3.74 10.000 --- U --- U --- V --- U --- U 31. Nitrobenzene 2.85 10.000 --- U --- U --- U --- U --- U 32. N-Nitrosadimethylamine 4.25 10.000 --- U --- U --- U --- U --- U 33. N-Nitrosodiphenylamine 3.95 10.000 --- U --- U --- U --- U --- U 34. N-Nitrosodi-N-Propylamine 4.06 10.000 »-- U --- U --- U --- U --- U 35. Phenanthrene 3.24 10.000 --- U --- U --- U --- U »-- U 36. Pyrene 3.6-1 101000 --- U --- U --- U --- U --- U 37. 4-Chloro-3-Methylphenol 3.79 20.000 --- U --- U --- U --- U --- U 38. 2-Chlorophenol 2.75 10.000 --- U --- U --- U --- U --- U 39, 0-Cresol 3.6B 10.000 --- U --- U --- U --- U --- U 40. P-Cresol 4.12 10.000 --- U --- U --- U --- U --- U 41. 2,4-Dichlorophenal 5.19 10.000 --- U --- U --- U --- U --- U 42. 2,6-nichlorophenol 4.89 10.000 --- U --- U --- U --- U --- U 43. 2,4-Dimethylphenal 3.21 10.000 --- U --- U --- U --- U --- U 44. 4,6-Dinitro-2-Mathylphenol 4,77 50.000 --- Ti --- U --- U --- U --- U 45. 2,4-Dinitrophenol 4,37 50.000 --- U --- U --- U --- U --- U 46. Ethyl Methaneeulfonate 5.26 20.000 --- U --- U --- U --- U --- U 47. Methyl Methaneaulfonate 4.92 10.000 --- U --- U --- U --- U --- U 49. 2-Nitrophenol 3.64 10.000 --- U --- U --- U --- U --- U .7 = Estimated value between the MDL and MRL, U = Below ALL Ouantitation Limita. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Emw'k nommid t hcmo NOW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID: Drinking Water ID: 31715 Wa8tewater ID; 10 PHONE (252) 756-6208 FAX (252) 756-0633 6003 A ANALYST: UAP DATE COLLECTED: 12/01/20 DATE EXTRACTED: 12/03/20 DATE ANALYZED: 12/29/20 DATE REPORTED: 05/24/21 SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Page: 2 MW-15 NW-1D MW-23 MW-2D MW-3B PARANUTER8, ug/1 MDL NRL - " U -- - U --- U --- U --- U 49. 4-Nitrophenol 3.17 50.000 U --- U --- U __ _ U 50, Pentachlorophenol 5.33 25.OD0 -- _ U -__ „ - U - U --- U ___ U 1.56 10.000 --- U --- V ,._ - U 51, Phenol 52. 2,3,4.6-Tetrachlorophenol 3.12 10.000 --_ U ___ U ..__ U --^ U --- U --- u --- U 53. 2,4,5-Trichlorophenol 4.17 10,000 -"_ U - - U 54. 2,4,6-Trichlorophenol 3.04 10.000 --- U U ___ U --- - U -__ "__ U "__ U 55. Acetophenone =_ U - „ U - - U 56. 2-Acetylaminafluorene 3.98 3,98 20.000 20.000 __ - U ___ U --- U _ - U 5T. 9-Aminobiphenyl 4.12 20.000 --- U _„_ U --- U --- U --- U 50. Denzyl Alcohol 4.47 20.000 -- U -- - --" U 59. 4-Chloroaniline 20.000 --- U --- U --- U --- U 60. Chlorobenzilate 5.12 10.000 -" - U - U U _„_ U --.. U 2.98 2.98 10,000 --' U --- U __ - U 61, Diallate 10.000 -" - U --- U --- U 62. Dibenzofuran 4.26 " U - U -- _ U - - U _"_ U 63. 3,3'-Dichlorobenzidine 9.22 20.000 - --- U --- U --- U __ - 3,98 20,000 --- U - " V -U 64, nimethoate -- _ U ___ U --- U 65. P-Dimethylaminoazobenzene 2.89 10.000 -- - U -- - U ___ U ___ U 66. 7,12-Dimathylbenz[a]anthracene 5.26 10.000 „-- U U __- U___ U 67. 3,3-Dimethylbenzidine 10.000 -- - U _- __ - ___ U ___ U 68. 1,3-Dinitrobenzene 2.89 __- U ___ U --- U - 69. Diphenylamine 5.10 10.000 --' U --- U --- U --- U __ - U 10.000 -_ U -8 --- U ___ U 70. Disulfoton --_ U ___ U ___ U 71. Famphur 3.98 20.000 ___ U "-- U ___ U U 4.31 10,000 -' - U U --- U 72. jaxachloropropene -- - U --- U --- U --- 73. ieosafrole 2.88 10,0D0 - U - - U --- U ___ U 2.78 20,000 --- U --- U __- U 74. xepone 3.54 100.000 --- U --- U --- U ___ U 75. Methapyrilene - V -- - U -- U --- U 76. 3-Methy lcholanthrene 4.21 10.000 - U -- 77. 2-Methyinaphthalena 3.79 10.000 --- U --- U --- U --- U 78. Methyl Parathion32 U ___ U --- U ` 79. m-Cresol 3.81 10.000 --- U -- - U ___ V ___ U --- U --- U 80, 1,4-Naphthoquinone 4.00 10.00D - U __ U - - U -_„ U 81. 1-Naphthylamine 5.61 10.000 -- .. U --- U --- V -'- U --- U 82, 2-Naphthylamine 4.62 10.000 -- - U _ - U U - - - U ..._ U 83. 2-Nitroaniline 3.61 50.000 - _ U --- U ___ U --- U - 89. 3-Nitroaniline 9,81 50.00D --- U -__ U .,__ U --- U - V 85, 9-Nitroaniline 4.22 20.000 --- U ___ U --- U --- U --- U 96. 5-Nitro-O-Toluidine 4.01 10.000 -- U --- U --- U -- U U 87. N-Nitrosodi-n-butylamine 3.63 10,000 --- U _-„ U --- U --^ U 88. N-Nitrosodiethylamine 3.83 20.000 -- - U --- U--- u 69. N-Nitrosomethylethylamine 3,83 50,000 -- - U _ U _ U _ U U 90. N-Nitrosopiperidine 5.19 20,000 -- " U --- U --- U --- U --- U 91. N-Nitrosopyrrolidine 2.89 10.000 -- - U - U U 92. Parathion 3.12 10.000 --- U -- - U U --- U --' V __ - U 93. Pentachlorobenzene 3.71 -- - U --- U --- U --- U --- U 94. Pentachloronitrobenzene .0,000 20.000 21 ___ U - U -_ - U ___ U 95. Phenacetin 4 .4 20.000 -- - U U ___ U 96. 1,4-Benzenediamine 2.99 10.000 --- U between the MDL and NRL, U = Below ALL Quantitation Limits. a = 6atimated value DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 h k _U7oUp©Taqgi Drinking Water ID: 37715 Wastewater IDs 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. jUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: c7AP DATE COLLECTED: 12/01/20 Page: 3 DATE EXTRACTED: 12/03/20 ED• 12/29/20 DATE ANALYZ �.� DATE REPORTED: 05/24/21 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) MW-1S MW-ID MW-20 MW-2D KW-38 PARAMETERS, u9/1 MDL MRL -- - U U --- U --- U --- U 97. Phorate 3.86 10.000 --D _-- D 99. Pronamide 3.69 10.000 --- U --- U --- V --- U 4.12 i0.000 '- - U --- U U 99. Satrole 5.01 10.000 -- - V --- U --- U 100. 1,2,4,5-Tetraahlorobenzene __' ll -- - - U - U __- U 101. Thionazin 4.62 20.000 - -- U --- U --- V --- U -„-U 102. 0-Toluidine 4,11 10.000 --- V -- _ U --- U 103. 1,3,5-Trinitrobenzeno 3,98 10.000 --- U --- U ___ U --- U „'- U 104. 0,0,0-Triethyl Phoaphorothioate 3.61 10.000 -' _ U -_ . v -_ - u -- ___ U u 1o5. rrexachloroethane 1.49 10.000 --- U U --- U 3.11 20.000 --- U -"- 106. Iaodrin J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. NOTE: EPA METHOD 8270E R6 (18): MW-3S: One of six internal Standards exceeded lower recovery limit. One or six Surrogate Standards exceeded upper recovery Iimit. No analytes detected above MDL. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Em'UmOHM % hP_L9@TP@TmW Drinking Water ID: 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: !✓�✓ ' ,u SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Page: 4 DATE EXTRACTED: 12/03/20 DATE ANALYZED: 12/29/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL MW-3D MW-3A 1, Acenaphthene 2.66 10.000 --- u 4.99 .1 2. Acenaphthylene 2.60 10.000 --- u --- u 3. Anthracene 2.97 10.000 --- u --- u 4. Benzo[a)antrhacene 4,16 10.000 --- u --- u 5. Senzo(b)fluoranthene 3.32 10.000 --- u --- u 6. Benzo[k]fluoranthene 4.23 10.000 --- V --- u 7. 9enzo[g,h,i1perylene 2.61 10,000 --- u --- V 8, Benzo[a]pyrene 3.27 10.000 --- u --- U 9. 4-Bromophenyl Phenyl Ether 2.63 10.000 --- u --- u 10. Butyl Benzyl Phthalate 5.70 10.000 --- u --- u 11. Bis(2-Chlarocthoxy) Methane 3.14 10.000 --- u --- u 12. Bis(2-Chloroethyl) Ether 2.58 10.000 --- u --- u 13. Bis(2-Chloro-l-methylethyl) Ether 2.58 10.000 --- 11 --- u 14. 2-Chloronaphthalene 2.17 10.000 --- a --- Ti 15. 4-Chlorophenyl Phenyl Ether 2,42 10.000 --- u --- u 16. Chryaene 4.04 10.000 --- u --- V 17, Dibenzo{a,hjanthracene 2.78 10,000 --- u --- u 18. Di-N-Butyl Phthalate 3.09 10.000 --- u --- u 19, Dimethyl Phthalate 3,78 10.000 --- u --- u 20. Diethyl Phthalate 3.92 10.000 --- u --- V 21. 2,4-Dinitrotoluene 3.95 10,000 --- u --- u 22. 2,6-Dinitrotoluene 3.88 10.000 --- u --- u 23, Di-N-Octyl Phthalate 2,81 10.000 --- u .._ V 24. sis-(2-Ethylhexyl) Phthalate 9.97 15.000 --- u --- u 25, sluoranthene 3.92 10.000 --- u --- u 26. Pluorene 2.95 10.000 --- u --- u 27. Hexachlorobenzene 2.61 10.000 --- u --- u 28, Nexachlorocyclopentadiene 4.16 101000 --- u --- u 29. Indeno(1,2,3-Cd)pyrene 2.91 10.000 --- u --- u 30, laophorone 3.74 10.000 --- a --- O 31. Nitrobenzene 2.85 10.000 --- V --- V 32. N-Nitrosadimethylamine 4.25 10.000 --- u --- V 33. N-Nitrosodiphenylamine 3.95 10.000 --- V --- V 34, N-Nitrosodi-N-Propylamine 4,06 10.000 --- a --- V 35. Phenanthrene 3.24 10.000 --- a --- u 36. Pyrene 3163 10.000 --- u --- u 37. 4-Chloro-3-Methylphenol 3.79 20.000 --- u --- u 38. 2-Chlorophenol 2.75 10.000 --- u --- u 39, O-Cresol 3.68 10.000 --- u --- u 40. P-Cresol 4.12 10.000 --- u --- u 41. 2,4-Dichlorophenol 5.19 10.000 --- u --- u 42. 2,6-Dichlorophenol 4.89 10.000 --- u --- u 43. 2,4-Dimethylphenol 3.21 10.000 --- u --- u 44, 4,6-Dinitro-2-Methylphenol 4.77 50.000 --- u --- u 45. 2,4-Dinitrophenal 4.37 50.000 --- O --- u 46. Ethyl Methaneeulfonate 5.26 20.000 --- u --- u 47. Methyl Methaneeulfonate 4.92 10,000 --- u --- u 40. 2-Nitrophenol 3.64 10.000 --- U --- u .l - Estimated value between the MDL and MRL, u = below ALL Quantitation Limita. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID: 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Page: 5 DATE EXTRACTED: 12/03/20 DATE ANALYZED: 12/29/20 DATE REPORTED: 05/24/21 SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PARAMETERS, uq/l MDL MRL MW-3D KW-3A 49. 4-Nitrophenol 3.17 50.000 --- U --- U 50. Pentachlorophenol 5.33 25.000 --- U --- U 51. Phenol 1.86 10.000 --- U --- U 52. 2,3,4,6-Tetrachlcrophenol 3.12 10.000 --- U --- U 53. 2,4,5-Trichlorophenol 4,17 10.000 --- U --- V 54, 2,4,6-Trichlorophenol 3.84 10.000 --- U --- U 55. Acetophenone 2.89 10.000 --- U --- U 56. 2-Acetylaminofluorene 3.96 20.000 --- U --- U 57. 4-Aminobiphenyl 4.12 20.000 --- U --- U 58. Benzyl Alcohol 4.47 20.000 --- U --- U 59. 4-Chlorcaniline 3.36 20.000 --- U --- U 60. Chlorobenzilate 5.12 10.000 --- U --- U 61. Dial late 2.90 10,000 --- U --- U 62. Dibenzofuran 4,26 10.000 --- U --- U 63, 3,31-Dichlorobenzidine 4.22 20.000 --- V --- U 64. Dimethoate 3,98 20.000 --- V --- V 65. P-Dimethylaminoazobenzene 2.89 10.000 --- U --- U 66. 7,12-Dimethylbenz[a]anthracene 5,26 10.000 --- U --- U 67. 3,3-Dimethylbenzidine 3.21 10.000 --- U --' U 68. 1,3-Dinitrobenzene 2.99 20.000 --•• U --- U 69, Diphenylamine 5.10 10.000 --- U -'- U 70. Disulroton 4,28 10.000 --- D --- U 71. Famphur 3.98 20.000 --- U --- U 72. Hexachloropropene 4.31 10,000 --- U --- U 73. Isosafrole 2.88 10,000 --- U --- U 74, Kepone 2.78 20.000 --- U --- U 75. Methapyrilene 3.54 100,000 --- U --- V 76. 3-Methylcholanthrene 4.21 10.000 --- U --- U 77. 2-Methylnaphthalene 3.79 10,000 --- U --- U 70. Methyl Parathion 4.32 10.000 --- V --- U 79. m-Cresol 3.01 10.000 --- U --- U BO, 1,4-Naphthcquinone 4.00 10.000 --- U --- U 81. 1-Naphthylamine 5.61 101000 --- U --- U 82. 2-Naphthylamine 4.62 10,000 --- U --- U 83. 2-Nitroaniline 3.61 50,000 --- U --- U 84. 3-Nitroaniline 4.81 50.000 --- U --. U 85. 4-Nitroaniline 4.22 20.000 --- U --- U 86. 5-Nitro-O-Toluidine 4.01 10.000 --- U --- U 87. N-Nitrosodi-n-butylamine 3.63 10.000 --- U --- U 88. N-Nitroeodiethylamine 3.83 20.000 --- U --- U 89. N-Nitrosomethylethylamine 3.83 10,000 --- U --- U 90. N-Nitrosopiperidine 5.19 20.000 --- U --- U 91. N-Nitrosopyrrolidine 2.89 10.000 --- U --- U 92. Parathion 3.12 10.000 --- U --- U 93, Pentachlorobenzene 3.92 10.000 --- U --- U 94. Pentachloronitrobenzene 3.71 20.000 --- U --- U 95. Phenacetin 4.41 20.000 --- V --- U 96. 1,4-Benzenediamine 2.99 10.000 --- U --- U J a Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ERW'0F(@RH(@M Ala hko-RunnUd Drinking Water ID: 37715 Wastawaker ID: 1.0 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ��/'✓/� SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Page: 6 DATE EXTRACTED: 12/03/20 DATE ANALYZED: 12/29/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL MW-3D MW-3A 97. Phorate 3.86 10.000 --- U --- U 98. Pronamide 3.69 10.000 --- U --- U 99. Safrole 4.12 10.000 --- U --- U 100. 1,2,4,5-Tetrachlorobenzene 5.01 10,000 --- V --- U 101. Thionaxin 4.62 20,000 --- U --- U 102, 0-Toluidine 4.11 10.000 --- U --- U 103. 1,3,5-Trinitrobenzene 3.98 10.000 - U --- U 104. 0,0,0-Triethyl Phosphorothioate 3,61 10.000 --- U --- U 105. Sexachloroethane 1.49 10.000 --- U --- U 106, isodrin 3.11 20.000 --- U --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DE occcuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-j19499C6B1 EB1 �lYl0 © MEgMI�A��O�o��Drinking water ID; 37715 LLLJJILLLJJJ 41 LLIILL!! U4LlJIIII��IILJJI �' Wastewater IDr 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 2785E FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/01/20 Page: 1 DATE REPORTED: 05/24/21 REVIEWED BY: ` LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Date Analyzed 12/11/20 12/11/20 12/11/20 12/11/20 12/12/20 MW"1S MW-1D MW-2S MW-2D MW-3S PARAMETERS, ug/l MDL MRL 1. Chloromethane 0.77 3.000 --- U --- U " ' U --- U - U 2. Vinyl Chloride 0.12 0.200 --- U --- U --- U --- U --- ll 3, Bromomethane 0.67 10.000 --- U --- U --- U --- U "' U 4. Chloroethane 0.48 10.000 --- U --- U --- U --- U --- U 5. Trichlorofluoromethane 0.24 1.000 --- U --- U --- U --- U --- U 6. 1,1-Dichloroethene 0.17 5.000 --- U --- U --- U --- U -- U 7. Acetone 9.06 100.000 --- U --' U --- U --- V - U 8. Iodomethane 0.26 10.000 --- U --- U --- U --- U -"- U 9. Carbon Disulfide 0.23 100.000 --- U `^' U '-" U - U - U 10, Methylene Chloride 0.64 1.000 --- U --- U --- U --- U --- U 11. trans-1,2-Dichloroethene 0.23 5.000 --- U --- U --- U --- U --- V 12, 1,1-Dichloroethane 0.20 5,000 --- U --- U "' U --- U --- U 13, Vinyl Acetate 0.20 50.000 --- U --- U "' V ""- U --- U 14. Cia-1,2-Dichloroethene 0.25 5.000 --- U --- U --- U --- U - U 15. 2-Butanons 2.21 100.000 --- U --- U --- U ""- U - U 16, Bromochloromethane 0,27 3.000 --- U --- U --- U --- U --- U 17. Chloroform 0,25 5.000 --- U --- U --- U --- U U 18. 1,1,1-Trichloroethane 0.19 1.000 --- U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U --- U --- U 20. Benzene 0.24 1,000 --- U --- U --- U --- U 0.46 .7 21, 1,2-Dichloroethane 0.02 0.200 --- U --- U --- U --- U 0.05 J 22, Trichleroethene 0.23 1.000 --- U --- U --- U --- U --- U 23. 1,2-Dichloropropane 0.04 0.200 --- U --- V --- U --- U --- U 24. Bromodichloromethane 0.04 0.200 --- U --- U --- U --- U --- U 25. Cis-1,3-nichloropropene 0.06 0.200 --- U --- U --- U _-- U --- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U --- U --- U --- U --- U 27. Toluene 0.23 1.000 --- U --- U --- U --- U --- U 28. trans-1,3-Dichloropropene 0.04 0.200 --- U --- U --' U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0.200 --- U --- U --- V --- U --- U 30. Tetrachloreethene 0.10 0.200 --- U _-- U '-' U --- V --- U 31. 2-Hexanone 1.57 50.000 --- U --- U --- U --- U --- U 32. Dibromochloromethane 0.03 0.200 --- U --- U --- U --- u --- U 33, 1,2-Dibromoethane 0.03 0.200 --- U --- U --- U --- U U 34, Chlorobanzene 0,30 3.000 --- U --- U --- U --- U - U 35, 1,1,1,2-Tetrachloroethane 0.22 1,000 --- U --- U --- U --- U --- U 36. Ethylbenzene 0.21 1.000 --- U --- U "" U --- U - U 37. Xylenes 0.68 5.000 --- U --- U --- U --- U '-' U 38. Dibromomethane 0.28 10.000 --- U --- U --- U --- U --- U 39. Styrene 0.19 1.000 --- U --- U --- V --- U --- U 40. Bromoform 0.20 3,000 --- U --- U --- U "-- U --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- U --- V --- U 42, 1,2,3-Trichlaropropane 0.09 0.200 --- U --- U --- U --- U "-- V 43. 1,4-Dichlorobenzene 0.39 1.000 --- U --- U --- U --- U --- V 44. 1,2-Dichlorobenzene 0.32 5.000 --- U --- U --- U --- U --- U 45, 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- U --- U --- U --- U --- U 46, Acrylonitrile 2.72 200.000 --- U --- U -'" U --- U --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.000 --- U --- U -'- U --- U --- U j = Estimated value between the ML and MRL, U = Below ALL 4uantitaticn Limits, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EAHromIN % kul9ownbo 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 i~/ l 0 REVIEWED BY: ' LANDFILL APPENDIX II EPA METHOD 8260D R4 (18) Drinking Water ID: 37715 Wastewater IDi 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Wage: 2 DATE REPORTED: 05/24/21 Date Analyzed 12/11/20 12/11/20 12/11/20 12/11/20 12/12/20 MW-lS MW-ID MW-20 MW-2D MW-3S PARAMETERS, Ug/1 MDL MRL 48. Acrolein 1.97 4.000 --- U __- U ___ U ___ U --- U 49, Allyl chloride 0.20 10.000 --- U --- U --- U --- U --- U 50. Chloroprene 0.21 20.000 --- U _-.. U --- U --- U --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U --- U --- U --- U --- U 52. Dichlorodifluoromethane 0.51 5.000 --- U --- U --" U --- U --- U 53. 1,3-Dichloropropane 0.28 1.000 --- U --- U --- U --- a --- U 54. 2,2-Dichloropropane 0,17 15.000 --- U --- U --- U --- U --- U 55. 1,1-Dichloropropene 0.22 5.000 --- U --- U --- U --- U --- U 56. Ethyl Methacrylate 0,16 10.000 --- U --- U --- U --- U --- U 57, Hexachlorobutadiene 0.10 0,200 --- U --- U --- U --- U --- U 58, Iaobutyl Alcohol 12.90 100.000 --- U --- U --- U --- U --- U 59. Methacrylonitxile 1.93 100.600 --- U --- U --- U --- U --- U 60, Methyl Methacrylate 0.25 30.000 --- U --- U --- U --- U --- U 61. Naphthalene 0.47 6.000 --- U --- U --- U --- U --- U 62. 9ropionitrile 3.26 150.000 --- U --- U --- U --- U --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U --- U --- U --- U --- U 64. Acetonitrile 36.29 55.000 --- U --- U --- U --- U - U 65. Tetrahydrofuran 0.39 1.000 --- U 135.00 4.05 --- U 25.60 66, 1,4-Dioxane 2.71 3.000 --- U --- U 11.30 --- U 150.00 a = Estimated value between the MDL and MRL, U = Below ALL Ruantitation Limits. NOTE: EPA METHOD 8260D R4 (18): MW-ID: Tetrahydrofuran result exceeded instrument calibration range and could not be reanalyzed within holding time. MW-3S: sample received at pH >2 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 E�]dOQ®��c�� ln �[Mk-tjrannTpo@TM�&d7 114 OAKMONT DRIVE GREENVILLF, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ✓ f'' v LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking Water ID: 37715 stewater iDi 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANA'LY ST : JAP DATE COLLECTED: 12/01/20 Page: 3 DATE REPORTED: 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/11/20 MW-3D 12/12/20 MW-3A 12/11/20 Trip Blank 1. Chloromethane 0.77 3.000 --- U --- U --- U 2. Vinyl Chloride 0.12 0.200 --- V --- U --- U 3. Bromomethane 0.67 10.000 --- U --- U --- U 4. Chloroethane 0.45 10.000 --- U --- U --- U 5. Trichlorofluoromethane 0.24 1.000 --- U --- U --- U 6, 1,1-Dichlorcethane 0.17 5.000 --- U --- V --- U 7. Acetone 9.06 100.000 --- U --- U --- U 8, lodomethane 0.26 10.000 --- U --- U --- U 9. Carbon Dieulfide 0.23 100.000 --- U --- a --- U 10. Methylene Chloride 0.64 1.000 --- U --- U --- U 11. trans-1,2-Dichloroethane 0,23 5.000 --- U --- U --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U 13, Vinyl Acetate 0.20 50.000 --- U --- U --- U 14, Cie-1,2-Dichloroethene 0.25 5.000 --- U --- U --- U 15. 2-Butanone 2.21 100.000 --- U --- V --- U 16. Bromochloromethane 0.27 3.000 --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U 18. 1,1,1-Trichloroethane 0.19 1.000 --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U 20, Benzene 0.24 1.000 --- U 0.02 J --- U 21. 1,2-Dichloroethane 0.02 0.200 --- U 0,03 J --- U 22, Trichloroethene 0.23 1,000 --- U --- U --- U 23. 1,2-Dichloropropane 0.04 0.200 --- U --- U --- U 24. Bromodichloromethane 0.04 0.200 --- U --- V --- U 25, Cie-1,3-➢ichloropropens 0.06 0.200 --- U --- U -"- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U --- U --- U 27. Toluene 0.23 1.000 --- U 0.72 J --- U 28. tran8-1,3-Dichloropropene 0.04 0.200 --- U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0.200 --- U --- U --- U 30. Tetrachloroethene 0.10 0.200 --- V --- U --- U 31, 2-Hexanone 1.57 50.000 --- U --- U --- U 32. Dibromochloromethane 0.03 0.200 --- U --- U '-- U 33. 1,2-Dibromoethane 0.03 0.200 --- U --- U "-- U 34. Chlorobenzene 0.30 3.000 --- U --- U "- U 35, 1,1,1,2-Tetrachloroethane 0.22 1.000 --- U --- U --- U 36. Ethylbenzene 0.21 1.000 --- U --- U --- U 37, Xylenea 0.68 5.000 --- U --- U --- U 38. Dibromomethane 0.28 10.000 --- U --- U --- U 39. Styrene 0.19 1.000 --- U --- V --- U 40. Bromoform 0.20 3,000 --- U --- U --- V 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- V 42, 1,2,3-Trichloropropane 0.09 0.200 --- U --- U --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U --- U --» U 44. 1,2-Dichlorobenzene 0.32 5.000 --- U --- U --- U 45, 1,2-Dibroma-3-Chloropropane 0.07 0.200 --- U --- U --- U 46, Acrylonitrile 2.72 200.000 --- U --- U --- U 47. trane-1,4-17ichloro-2-Butene 0.42 100.000 --- U --- U -'- U J = Eatimated value between the MDL and MRL, U = Below ALL Ruantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID: 37715 S?%.st4w4tsr-,ID,, 1.0 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/01/20 Page: 4 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 ❑ate MDL Analyzed MRL 12/11/20 MW-3➢ 12/12/20 MW-3A 12/11/20 Trip Blank 48. Acrolein 1.97 4.000 --- U --- U --- U 49. Allyl Chloride 0,20 10.000 --- U --- U --- U 50. Chloroprene 0.21 20,000 --- U --- U --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U --- U --- U 52. DichlorodiEluoromathane 0.51 5.000 --- U --- U --- U 53. 1,3-Dichloropropane 0.28 1.000 --- U --- U --- U 54. 2,2-Dichloropropane 0.17 15.000 --- U --- U --- Ti 55. 1,1-Dichloropropene 0.22 5.000 --- U --- U --- V 56. Ethyl Methacrylate 0.16 10.000 --- U --- U --- U 57. Hexachlorobutadiene 0.10 0.200 --- U --- U --- U 58, Isobutyl Alcohol 12.80 100.000 --- U --- U --- U 59. Methacrylonitrile 1.93 100.000 --- U --- U --- U 60. Methyl Methacrylate 0.25 30,000 --- U --- U --- U 61. Naphthalene 0.47 6.000 --- U 0.77 U --- U 62. Propionitrile 3.26 150,000 --- U --- V --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U --- U --- U 64. Acetonitrile 36.29 55.000 --- U --- U --- U 65. Tetrahydrofuran 0.39 1.000 --- U 16.50 --- U 66, 1,4-Dioxane 2,71 3.000 --- U 73.10 --- U J = Eetimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 0 U 0 0 C CD LO C: CD 7 3 FIT M m cr w 0 0 Cj v ~ w 0 c , 0 0 t° 3 o� lV w =CD ID U) CD w w � CD 0 CD m � � c o ro a CD n O GJ c� CA CD PT104y rn r m ~ 7 N A 6 n I..f uj CO co 0 Q 0 fJ W W li1 N N �-+ Fn C 7 CA an_ U) C7 � C C t" n Z v, m rm' mx t+ Cr] f) a _<cz� V 00 C m IT] C� 13 y y erg' w m m m ra Ur N s Cjj a z m m m TOTAL CHLORINE, mgll C7 m m m OR ugll AT COLLECTION 1..r� 1� r-n o a 5mE [[ o C n 0 S? TEMPERATURE, °C E J s' - J L)0 ATCOLLECTION G7 P a o ; o 0 00 c 4 OF CONTAINERS to z0 z Field H p ro Nitrate -Nitrite n ro Alkalutit Y _. :•' Chloride y b Cyanide 'b TDS > m m m m m m [v Sulfate b .J c� Metals m Sulfide "� u <' s>' Conductivit Y a 'b DO Temperature J Field Parameter :: 01. :.::: EPA 8270E .... :::::•+: .... .... .... .n. 8270E ID p. I h EPA 8081E G� cn = PARAMETER5/TESTS 2 0 _ -am �r n Mo c� m n n n m m r 0 ao „ z n � z z 0 -0 m m m z m C.j m O g y nr� A� m m m m n S = o G�i c�r� cn n m o m m r rTi o W a z r, = z > G7 z n [�n Oz C.)O r z 00 n m Z o m A 0 m o `u � �z n o mm 0 z ti N n z DocuSi( 0 E C. co CD C rn w cn Q m G)W Q � w co � C fb � m w 10 � do an tnveiope iu: iy4"uot5 ices i W N mDo m m wj �C��Z z z z 'o v 2 CD T p 2 to b d CA ray No lip GLA cl Qn W �i a- co O z rj o 6 n �r�� 6100 uj � IJ Q a n ya n O O � � 71 �` 9L3 CS C3 J p t" w w m m m �1f u� UI rn z m mm TOTAL CHLORINE, rngll m m m OR ugll AT COLLECTION 0 0 0 O C n J TEMPERATURE,°C In m J `t AT COLLECTION t7r7 O n th 0 00 -4 o 00 0 0 N OF CONTAINERS <? 8081B Dn 1 icate p G� 8260D A pp.II 8260D A pp .II2 l� G� ?: 8260D App. II 3 4� 8151A Landfill G� n N 8151A Duplicate ORP > b 0 m in Cj S C� w _� � v PARAMETERSfTESTS n a = n Fo co A � rn o z M m n m n y > = t3 SJ 7° n -n z� = z o - m PP z m r rvcn � o n o m m c m A d CD z co m m z rlt t�ti m -En- n �y n -n m o N v N q m y 0Uj C.) r O z0 Q ` - oa m o m 37 z p b "t O mm c A 2 m 2 m o O nCD 2 N DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 / / 1 REVIEWED BY: ✓/(�, \ VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS CLIENT ID: ANALYST: DATE COLLECTED: DATE ANALYZED: DATE REPORTED: PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 12/01/20 12/11/20 - 12/12/20 05/24/21 PARAMETERS, ug/l HDL MRL Concentration 1. Chloromethane 0.77 3.00 --- u 2. Vinyl Chloride 0.12 0.20 --- U 3. Sromomethane 0.67 10.00 --- V 4. Chloroethane 0.48 10.00 --- V S. TrichloroPluoromethane 0.24 1.00 --- u 6. 1,1-Dichloroethene 0.17 5.00 --- u 7. Acetone 9.06 100.00 --- U 8. Iodomethane 0.26 10.00 --- V 9. Carbon Disulfide 0.23 100.00 --- u 10. Methylene Chloride 0.64 1.00 --- u 11. trans-1,2-Dichloroethene 0.23 5.00 --^ V 12. 1,1-Dichloroethane 0.20 5.00 --- V 13. Vinyl Acetate 0.20 50.00 --- u 14. cis-1,2-Dichloroethene 0.25 5.00 --- u 15. 2--Butanone 2.21 100.00 --- u 16. Bromochloromethane 0.27 3.00 ---- u 17. Chloroform 0.25 5.00 --- u 18. 1,1,1-Trichloroethane 0.19 1.00 --- U 19. Carbon Tetrachloride 0.04 0.20 --- u 20. Benzene 0.24 1.00 --- U 21. 1,2-Dichloroethane 0.02 0.20 --- u 22. T.richloroethene 0.23 1.00 --- u 23. 1,2-Dichloropropane 0.04 0.20 --- V 24. Bromodichloromethane 0.04 0.20 --- u 25. cis-1,3-Dichloropropene 0.06 0.20 --- u 26. 4-methyl-2-Pentanone 1.19 100.00 ^-- u 27. Toluene 0.23 1.00 ---- u 2B. trans-1,3-Dichloropropene 0.04 0.20 --- u 29. 1,1,2-Trichloroethane 0.03 0.20 --- u 30. Tetrachloroethene 0.10 0.20 --- u 31. 2-Hexanone 1.57 40.00 --- V 32. Dibromochloromethane 0.03 0.20 ---- U 33. 1,2-Dibromosthane 0.03 0.20 --- u 34. Chl.orobenzene 0.30 3.00 --- V 35. 1,1,1,2-Tetrachloroethane 0.22 1.00 --- u 36. Ethylbenzene 0.21 1.00 --- U 37. xylenes 0.68 5.00 --- V 38. Dibromomethane 0.28 10.00 --- V 39. Styrene 0.19 1.00 --- u 40. Bromo£orm 0.20 3.00 --^ V 41. 1,1,2,2-Tetrachloroethane 0.03 0.20 --- u 42. 1,2,3-Trichloropropane 0.09 0.20 --- u 43. 1,4-Dichlorobenzone 0.39 1.00 ^-^ u 44. 1,2-Dichlorobenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- V 46. Acryloni.trile 2.72 200.00 --- u 47. trans-1,4-Dichloro-2-Butene 0.42 100.00 --- u 48. Acrolein 1.97 4.00 --- u 49. Ally1 Chloride 0.20 10.00 ---- V 50. Chloroprene 0.21 20.00 --- u DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 &AMER&M Ala hko-tATPumd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. CLIENT ID: MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED: DATE ANALYZED: DATE REPORTED: REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 12/01/20 12/11/20 - 12/12/20 05/24/21 PARAMETERS, ug/1 MDL MRL Concentration 51. 1,3-Dichlorobenzene 0.41 5.00 --- U 52. DichlorodiEluoromethane 0.51 5.60 --- U 53, 1,3-Dichloropropane 0.28 1.00 --- U 54. 2,2-Dichloropropane 0.17 15.00 --- U 55. 1,1-Dichloropropene 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 --- U 57. Hexachlorobutadiene 0,10 0.20 --- U 58, Isobutyl Alcohol 12.80 100.00 --- U 59. Methacrylonitrile 1.93 100.00 --- U 60. Methyl Methacrylate 0.25 30.00 --- U 61. Naphthalene 0.47 6.00 --- U 62, Propionitrile 3.26 150.00 --- U 63. 1,2,4-Trichlorobenzene 0.50 10.00 --- U 64. Acetonitrile 36.29 55.00 --- U 65. Tetrahydro£uran 0,39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 --- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/01/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 REVIEWED BY: ✓/✓ 1�/ VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits (� recovery) 1,2-DCA-d4 recovery) Toluene-d8 (% recovery) 4-BFB (% recovery) Continuing Calibration std. 70-130 100 101 102 Method Blank 70-130 98.3 97.6 97.4 MW-lS 70-130 100 99.5 98.3 MW-1D 70-130 99.5 96.8 97.0 MW-2S 70-130 101 99.3 97.7 MW-2D 70-130 1 103 102 99.1 MR-3S 70-130 103 104 101 MR-3D 70-130 98.4 97.9 98.0 MW-3A 70-130 96.4 96.3 94.5 Trip blank 70-130 104 103 98.9 6003 MW-4 M.S. 70-130 104 103 100 6003 M-4 M.S.D. 70-130 1 104 102 100 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 hakoffmW % ho-LIMpT80d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CSD DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID: ANALYST: DATE COLLECTED: DATE ANALYZED: DATE REPORTED VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 12/01/20 12/11/20 - 12/12/20 05/24/21 Sample Spiked: (6003) NW-4 Spike Amount Ug/1 Sample Result Ug/1 Spike Result Ug/l Spike Recovery (70-130%) Spike Dup. Result Ug/l Spike Dup. Recovery (70-13094) MS/MSD RPD (20%) 1,1-Dichloroethene 20.0 --- U 23.38 117 22.48 112 3.9 Benzene 20.0 --- U 22.93 115 21.43 107 6.8 Trichloroethene 20.0 --- U 22.59 113 21.46 107 5.1 Toluene 20.0 --- U 21.77 109 20.82 104 4.5 Chlorobenzene 20.0 --- U 21.98 110 20.77 1 104 5.7 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount Ug/l Spike Result Ug/l Spike Recovery (70-130%) 1,1-Dichloroethene 20.00 20.07 100 Benzene 20.00 20.06 100 Trichloroethene 20.00 20.16 101 Toluene 20.00 19.96 100 Chlorobenzene 1 20.00 1 20.11 1 101 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ENW,ummug1@2 1, hk(-iU;*TQ0 OT cW Drinking Water IDo 37715 in 1P.1 IQ 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST $02 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 XD##: 6003 B DATE COLLECTED: 12/03/20 DATE REPORTED : 05/24/21 REVIEWED BY: MW-9A MW-10 MW-11 MW-13 MW-12s Analysis Method PARAMETERS MDL MRL Date Analyst Code PH (field measurement), Unite 7.3 6.4 7.1 6.6 6.9 12/03/20 SEB 4500HB-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 --- U --- U --- U 0.27 --- U 12/07/20 TLH 353.2 R2-9 Alkalinity (to pH 4,5), mg CaCO3/1 1.0 1.0 210 455 433 280 590 12/07/20 JMS 2320E-11 Chloride, mg/1 5.0 5.0 10 82 18 11 119 12/07/20 TMR 4500CLB-11 Cyanide, 09/1 5.0 5.0 --- U --- U --- U --- U --- U 12/10/20 SEJ 450OCNE-11 Total Dissolved Residue, mg/1 1.0 10 347 1010 754 D 395 926 12/08/20 HJO 2540C-11 Sulfate, mg/1 5.0 5,0 72.3 330 214 98.8 173 12/09/20 SEJ 450OR042SI Antimony, ug/l 0.03 1.0 0.10 J 0.19J 0.08 J 0,11J 0.19J 12/14/20 HMM EPA200.8 Arsenic, ug/1 0.08 5.0 0.22 J 2.9J 5.3 2.6J 20 12/22/20 HMM EPA200.8 Barium, ug/1 0.04 10.0 45 09 12/14/20 HMM EPA200.B Barium, ug/1 0.04 10.0 160 73 451 12/21/20 HMM EPA200,8 Beryllium, ug/1 0.02 1.0 --- U --- U --- U --- U --- U 12/14/20 HMM EPA200,0 Cadmium, ug/1 0,04 1.0 --- U --- U --- U --- U --- U 12/14/20 HMM EPA200.8 Cobalt, ug/1 0.02 1.0 0.02 J 0.66 J 0.90 J 0.36 J 2.0 12/14/20 HMM EPA200.8 Total Chromium, ug/1 0.12 5.0 0.12 J 12 2.4J 0.84 J 31 12/14/20 HMM HPA200.8 Copper, ug/l 0.04 10.0 0.31 J 0.28 J 0.10 J 0.50 J 0.10 J 12/14/20 HMM EPA200.8 Iron, ug/l 4.96 50.0 523 1390 16358 3118 1650 12/10/20 LFJ EPA200.7 Manganese, ug/1 0.31 10.0 47 276 291 37 755 12/10/20 LFJ EPA200.7 Lead, ug/1 0.03 5.0 --- U --- U 0.04 J 0.05J --- U 12/21/20 HMM EPA200.8 Mercury, ug/1 0.05 0.20 --- U --- U --- U --- U --- U 12/09/20 MTM 245.1 R3-9 Nickel, ug/1 0.03 10.0 0.19 J 1.8 J 0.98 J 0,64 J 2.6 J 12/14/20 HMM EPA200.8 Selenium, ug/1 0.05 10.0 --- U 0.84 J 0,48 J 0.56J 1.7 J 12/22/20 HMM EPA200.8 Silver, ug/1 0.22 5.0 --- U --- U --- U --- U --- U 12/14/20 HMM EPA200.8 Thallium, ug/1 0.02 1.0 0.29J --- U --- U 0.04 J --- U 12/14/20 HMM $PA200•e Tin, ug/1 0.05 100.0 --- U 0.06 J 0.25 J 0.24 J --- U 12/28/20 HMM EPA200.0 Vanadium, ug/1 0.04 1.0 0.26 J 6.9 1.5 1.8 2B 12/14/20 HMM EPA200.8 Zinc, ug/1 0.17 10.0 0.72 J 0.59 J 0.60 J 2.2J 0.45 J 12/14/20 HMM EPA200.8 Sulfide, u9/1 100 1000 --- U 599 J --- U 409 J --- U 12/05/20 LFJ 450052D-11 Conductivity (at 25c), uMhos/cm 1.0 1.0 579 1440 1008 560 2567 12/03/20 SEB 2510E-11 Dissolved Oxygen, mg/1 0.1 0.1 0.2 1.0 0.2 0.3 0.3 12/03/20 SEB 45000G-11 Temperature, 'C 18 14 13 20 15 12/03/20 SEB 255013-10 Static water Level, feet 5.54 3.40 3.40 9.16 4.84 12/03/20 SEB Well Depth, feet 23.17 22.73 23.B4 20.68 22.93 12/03/20 SEB ORP, my +58 +122 +94 +56 +136 12/03/20 SEB 25SOB-11 Turbidity (Field), NTU 1.0 1.0 3.40 2.57 8.22 3.69 5.24 12/03/20 SEB 213OB-11 All QC requirements were not met: D Duplicate data not within established limits, J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ERAT(buon(W % hmpumbd Drinking Water ID! 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PESTICIDES AND PCB'S EPA METHOD 8081B R2(07) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: HIC DATE COLLECTED: 12/03/20 DATE EXTRACTED: 12/04/20 DATE ANALYZED: 12/16/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL MW-9A MW-10 MW-11 MW-13 MW-12a 1. Aldrin 0.029 0.050 --- U --- U --- U --- U --- U 2. Alpha-BHC 0.032 0.050 --- U --- U --- U »-- U --- U 3. Beta-BHC 0.031 0,050 --- U --- U --- U --- it --- U 4. Delta-BHC 0.030 0.050 --- U --- U --- U --- U --- U 5. Gamma-BHC {Lindane) 0.032 0.050 --- U --- U --- U --- U --- U 6. Chlordane 0.320 0.500 --- U --- U --- U --- U --- U 7. 4,4-DDD 0.051 0.100 --- U --- U --- U --- U --- u S. 4,4-DDE 0,049 0.100 --- U --- U --- U --- U --- U 9. 4,4-DDT 0,052 0.100 U --- U --- U --- U --- U 10. Dieldrin 0.042 0.075 --- U --- U --- U --- U --- U 11. EndosulEan I 0.056 0.100 --- U --- U --- U --- U --- U 12. Endoeulfan II 0.046 0.100 --- U --- U --- V --- U --- U 13. Endoeulfan Sulfate 0.072 0.100 --- U --- U --- U --- U --- U 14. Endrin 0.053 0.100 --- U --- U --- V --- U --- U 15, Endrin Aldehyde 0.068 0.100 --- U --- U --- U --- U --- U 16. Heptachlor 0.039 0.050 --- U --- U --- U --- U --- U 17. Heptachlor Epoxide 0.042 0.075 --- U _-- U --- V --- U --- U 18. Methoxychlor 0.530 1.000 --- U --- U --- U --- U --- U 19. Peb's (Aroc}ore) 0.500 2.000 --- U --- U --- U --- U --- U 20, Toxaphene 0.690 1.500 --- U --- U --- U --- U --- V J = Estimated value between the MDL and MRL, U - Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ElflAmMEW Ala Nar,-,*TP@TmW Drinking Water ID: 37715 114 OAKMONT DRIVE GREENVILLE, N,C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: �✓ /�/C�` LANDFILL APPENDIX II EPA METHOD 8151A R1(96) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 8 ANALYST: HIC DATE COLLECTED: 12/03/20 DATE EXTRACTED: 12/08/20 DATE REPORTED: 05/24/21 Date Analyzed 12/10/20 12/14/20 12/10/20 12/10/20 12/10/20 MW-9A MW-10 MW-11 MW-13 MW-128 PARAMETERS, ug/l MDL, MRL 1. 2,4-D 0.36 2.000 --- U --- U --- U --- U --- U 2, Dines" 0.54 1.000 --- U --- U --- U --- U --- U 3. 2,4,5-TP 0.42 2.000 --- U --- U --- U --- U --- U 4, 2,4,5-T 0.47 2.DOD --- n --- U --- ❑ --- U --- U J = Eatimated value between the MDL and MRL, V = Below ALL Quantitation Limita. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EnAmmW % h(_iUj;*TPvmftd Drinking Water IDe 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ` SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page: I DATE EXTRACTED: 12/07/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 Date MDL Analyzed MRL 12/30/20 MW-9A 01/05/21 MW-10 12/30/20 MW-11 12/30/20 MW-13 12/30/20 MW-12s 1, Acenaphthene 2.66 10,000 --- U --- U --- U --- U --- U 2, Acenaphthylene 2.60 10.000 --- U --- U --- U --- U --- U 3, Anthracene 2.97 10.000 --- U --- U --- U --- U --- U 4, Benzo[a]antrhacene 4,16 10,000 --- U --- U --- U --- U --- U 5. Benzo[b]fluoranthene 3.32 10.000 --- U --- U --- U --- U --- U 6. Benzo[k]fluoranthene 4.23 10.000 --- U --- U --- U --- U .._ U 7. Benzo[g,h,i]perylene 2.61 10.000 --- U --- U --- U --- U --- U 8. Benzo[a]pyrene 3.27 10.000 --- U --- U --- U --- U --- U 9. 4-Bromophenyl Phenyl Either 2.63 10,000 --- U --- U --- U --- U --- U 10. Butyl Benzyl Phthalate 5.78 10.000 --- U --- U --- U --- U --- U 11. Bis(2-Chloroethoxy) Methane 3.14 10.000 --- U --- U --- U --- U --- U 12. Bis(2-Chloroethyl) Ether 2.58 10.000 --- U --- U --- U --- U --- U 13. Bis(2-Chloxo-l-methylethyl) Ether 2158 10,000 --- U --- U --- U --- U --- U 14. 2-Chloronaphthalene 2.17 10,0D0 --- U --- U --- U --- U --- U 15, 4-Chlorophenyl Phenyl Ether 2.42 1D.000 --- U --- U --- U --- U --- U 16. Chrysene 4.04 10.000 --- U --- U --- U --- U --- U 17, Dibenzo[a,h]anthracene 2.78 10100D --- U --- U --- U --- U --- U 18. Di-N-Butyl Phthalate 3.09 10,D00 --- U --- U --- U --- U --- U 19, Dimethyl Phthalate 3,78 10.000 --- U --- U --- U --- U --- U 20. Diethyl Phthalate 3.92 10,D00 --- U --- U --- U --- U --- U 21. 2,4-Dinitrotoluene 3,95 10.000 --- U --- U --- U --- U --- U 22. 2,6-Dinitrotoluene 3.88 10.000 --- U --- U --- U --- U --- U 23. Di-N-Octyl Phthalate 2.81 10.000 --- U --- U --- U --- U --- U 24. Bis-(2-Ethylhexyl) Phthalate 9.97 15.000 --- U --- U --- U --- U --- U 25. Fluoranthene 3.92 10.000 --- U --- U --- U --- U --- U 26. Fluorene 2.95 10.000 --- U --- U --- U --- U --- U 27. Hexachlorobenzene 2.61 10.000 --- U --- U --- U --- U --- U 28. Hexachloracyclopentadiene 4.16 10,000 --- U --- U --- U --- U --- U 29. Indeno[1,2,3-Cd]pyrene 2.91 10.000 --- U --- U --- ❑ --- U --- U 30. Isophorone 3.74 10,000 --- U --- U --- U --- U --- U 31, Nitrobenzene 2.85 10.000 --- U --- U --- U --- U --- U 32. N-Nitrosodimethylamine 4.25 10.000 --- U --- U --- U --- U --- U 33. N-Nitrosodiphenylamine 3.95 10,000 --- U --- U --- U --- U --- U 34. N-Nitroeodi-N-Propylamine 4.06 10,000 --- U --- U --- U --- U --- U 35. Phenanthrene 3.24 10.000 --- U --- U --- U --- U --- U 36. Pyrene 3.63 10.000 --- U --- U --- U --- U --- U 37. 4-Chloro-3-Methylphenol 3.79 20.000 --- U --- U --- U --- U --- U 38. 2-Chlorophenol 2.75 10.000 --- U --- U --- U --- U --- U 39. O-Cresol 3.68 10,000 --- U --- U --- U --- U --- U 40. P-Cresol 4.12 10.000 --- U --- U --- U --- U --- U 41, 2,4-Dichlorophenol 5.19 10.000 --- U --- U --- U --- U - U 42, 2,6-Dichlorophenol 4.89 10,000 --- U --- U --- U --- U --- U 43. 2,4-Dimethylphenol 3.21 10.000 --- U --- U --- U --- U --- U 44, 4,6-Dtnitro-2-Methylphenol 4.77 50.000 --- V --- U --- U --- U --- U 45. 2,4-Dinitrophenol 4,37 50.000 --- V --- U --- U --- U --- U 46. Ethyl MethanesulEonate 5.26 20.000 --- Ti --- U --- U --- U --- U 47. Methyl Methanesulfonate 4.92 10,000 --- U --- U --- U --- U --- V J = Estimated value between the MDL and MRL, U = Below ALA Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID! 37715 WdaC.awat.vr 11)z 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page; 2 DATE EXTRACTED: 12/07/20 DATE REPORTED; 05/24/21 PARAMETERS, ug/l Date MDL Analyzed MRL 12/30/20 MW-9A 01/05/21 MW-10 12/30/20 MW-11 12/30/20 MW-13 12/30/20 MW-12s 48. 2-Nitrophenol 3.64 10.000 --- U --- U --- U --- U --- U 49. 4-Nitrophenol 3.17 50.000 -»- U --- U --- U --- U --- U 50. Pentachlorophenol 5.33 25,000 --- U --- V --- U --- U --- U 51. Phenol 1.86 10.000 --- U --- V --- U --- U --- U 52, 2,3,4,6-Tetrachlorophenol 3.12 10.000 --- U --- V --- U --- U --- U 53. 2,4,5-Trichlorophenol 4.17 10.000 --- U --- U --- U --- U --- U 54. 2,4,6-Trichlorophenol 3.84 10.000 --- U --- U --- U --- U --- V 55. Acetophenone 2.89 10,000 --- U --- U --- U --- U --- V 56, 2»Acetylaminofluarene 3.90 20.000 --- U --- U --- U --- U --- U 57. 4-Aminobiphenyl 4.12 20.000 --- U --- U --- U --- V --- U 58. Benzyl Alcohol 4.47 20.000 --- U --- U --- U --- U --- U 59. 4-Chloroaniline 3.36 20.000 --- U --- U --- U --- U --- U 60. Chlorobenzilate 5.12 10.000 --- U --- U --- U --- U --- V 61. Diallate 2.98 10.000 --- U --- U --- U --- U --- U 62. Dibenzofuran 4.28 10.000 --- U --- U --- U --- U --- U 63. 3,31-Dichlorobenzidine 4.22 20.000 --- U --- U --- U --- U --- U 64. Dimethoate 3.98 20.000 --- U --- U --- U --- U --- U 65. P-Dimethylaminoazobenzene 2.89 10.000 --- U --- U --- U --- U --- U 66. 7,12-Dimethylbenz[a]anthracene 5,26 20.000 --- U --- U --- U --- U --- U 67. 3,3-Dimethylbenzidine 3.21 10.000 --- U --- U --- U --- U --- U 68. 1,3-Dinitrobenzene 2,89 20.000 --- U --- U --- U --- U --- U 69. Diphenylamine 5.10 10.000 --- U --- U --- U --- U ..._ U 70. Disulfoton 4.28 10.000 --- U --- U --- U --- U --- U 71. tamphur 3.98 20.000 --- U --- U --- U --- U --- U 72, Hexachloropropene 4.31 10.000 --- U --- U --- U --- U --- U 73. Isoaafrole 2.88 10.000 --- U --- U --- U --- U --- U 74. Kopone 2.78 20.000 --- U --- U --- U --- U --- U 75. Methapyrilene 3.54 100.000 --- U --- U --- U --- U --- U 76. 3-Methylcholanthrene 4.21 10.000 --- U --- U --- U --- U --- U 77. 2-Methylnaphthalene 3.79 10.000 --- U --- U --- U --- U --- U 78. Methyl Parathion 4.32 10.000 --- U --- U --- U --- U --- U 79. m-Cresol 3.81 10.000 --- U --- U --- U --- U --- U 00. 1,4-Naphthoquinone 4.00 I0.000 --- U --- U --- U --- U --- U 81. 1-Naphthylamine 5.61 10,000 --- U --- U --- U --- U --- U 82. 2-Naphthylamine 4.62 10.000 --- U --- U --- U --- U --- U 03, 2-Nitroaniline 3.61 50.000 --- U --- U --- U --- U --- U 94. 3-Nitroaniline 4.81 50.000 --- U --- U --- U --- U --- U 85. 4-Nitroaniline 4.22 20.000 --- U --- U --- U --- U --- U B6. 5-Nitro-O-Toluidine 4,01 10.000 --- U --- U --- U --- U --- U 87. N-Nitroaodi-n-butylamine 3.63 10.000 --- U --- U --- U --- U --- U 88. N-Nitroeodiethylamine 3.83 20.000 --- U --- U --- U --- U --- U 89. N-Nitrosomethylethylamine 3.83 10.000 --- U --- U --- U --- U --- U 90. N-Nitrosopiperidine 5.19 20.000 --- U --- U --- U --- U --- U 91. N-Nitroeopyrrolidine 2.89 10.000 --- U --- U --- U --- U --- U 92. Parathion 3.12 10.000 --- V --- U --- U --- U --- U 93. Pentachlorobenzene 3.92 10.000 --- U --- U --- U --- U --- U 94. Pentachloronitrobenzene 3.71 20.000 --- U --- U --- U --- U --- U a = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Drinking Water ID; 37715 Wastewater IDF 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page: 3 DATE EXTRACTED: 12/07/20 DATE REPORTED: 05/24/21 Date Analyzed PARAMETERS, ug/l MDL MRL 12/30/20 MW-9A 01/05/21 KW-10 12/30/20 MW-11 12/30/20 MW-13 12/30/20 MW-12s 95. Phenacetin 4.41 20.000 --- U --- U --- V --- U --- U 96. 1,4-Benzenediamine 2.99 10.000 --- U --- U --- V --- U --- U 97. Phnrate 3.06 10.000 --- U --- V --- U --- U --- U 90. Pronamide 3.69 10.000 --- U --- V --- U --- U --- U 99, Sarrole 4,12 10.000 --- U --- V --- U --- U --- V 100. 1,2,4,5-Tetranhlorobenzene 5.01 10.000 --- U --- U --- U --- U --- U 101. Thionazin 4.62 20.000 --- U --- V --- U --- U --- U 102. O-Toluidine 4.11 10.000 --- U --- U --- U --- V --- U 103. 1,3,5-Trinitrobenzene 3.95 10.000 --- U --- U --- U --- V --- U 104, 0,0,0-Triethyl Phoephorothioate 3.61 10,000 --- U --- U --- U --- V --- U 105. Hexachloroethane 1.49 10.000 --- U --- U --- U --- U --- U 106. Iaodrin 3.11 20.000 --- U --- U --- U --- V --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. NOTE: EPA METHOD 8276E R6 (18): MW-12S: One of six Internal Standards exceeded lower recovery limit. One of six Surrogate Standards exceeded upper recovery limit. No analytes detected above MDL. DocuSSign Envelope ID: 8935BE5A-77D3E-4FC2-94A8-19499C6B1 EB1 MWkOMEM lJfl hmpumNo Drinking Water ID: 37715 Waatawat.es.IPI 10 114 OAKMONT DRIVE GREENVILLE, N.C, 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page: 1 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 PARAMETERS, uy/l MDL MRL MW-9A MW-10 MW-11 NW-13 MW-128 1. Chloromethane 0.77 3.000 --- U --- U --- U --- U --- U 2. Vinyl Chloride 0.12 0.200 --- U --- U 0.14 J 0.24 0.73 3. Bromomethane 0.67 10.000 --- U --- U --- U --- U --- U 4. Chloroethane 0.48 10.000 --- U --- U --- U --- U --- U 5. Trichlorofluoromethane 0,24 1.000 --- U --- U --- U --- U --- U 6. 1,1-Dichlaroethene 0.17 5.000 --- U --- U --- U --- U --- U 7. Acetone 9.06 100,000 --- U --- U --- U --- U --- U 8. Iodomethane 0.26 10.000 --- U --- U --- U --- U --- U R. Carbon Disulfide 0.23 100.000 --- U --- U --- U --- U 0.34 J 10. Methylene Chloride 0.64 1.000 --- U --- U --- U --- U --- U 11. trana-1,2-Dichloroethene 0,23 5.000 --- U --- U --- U --- U --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U --- U --- U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- U --- U --- U 14. Cis-1,2-Dichloroethene 0.25 5.000 --- U --- U --- U 0.60 J --- U 1-9. 2-Butanane 2.21 100.000 --- U --- U --- U --- U --- U 16. Bromochloromethane 0,27 3.000 --- U --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U --- U --- U 18. 1,1,1-Trichloroethane 0.19 1.000 --- U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U --- U --- U 20. Benzene 0.24 1.000 --- U --- U 0.62 J --- U 1.37 21. 1,2-Dichloroethane 0.02 0.200 --- U 0.04 J 0.05 J --- U 0.06 J 22. Trichloroethene 0.23 1.000 --- U --- U --- U --- U --- U 23. 1,2-Dichloropropene 0.04 0.200 --- U --- U 0.04 J --- U 0.06 J 24. Bromodichloromethane 0.04 0.200 --- U --- U --- V --- U --- U 25. Cis-1,3-Dichloropropene 0.06 0.200 --- U --- U --- U --- U --- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U --- U --- U --- U --- U 27. Toluene 0.23 1.000 --- U --- U --- U --- U 0.35 J 28. trans-1,3-Dichloropropene 0.04 0.200 --- U --- U --- U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0,200 --- U --- U --- U --- U --- U 30. Tetrachloroethane 0.10 0,200 --- U --- U --- U --- U --- U 31. 2-Hexanone 1.57 50.000 --- U --- U --- U --- U --- U 32. Dibromochlaromethane 0.03 0.200 --- U --- U --- U --- U --- U 33. 1,2-Dibromoethane 0.03 0,200 --- U --- U --- U --- U --- ❑ 14, Chlorobenzene 0.30 3.000 --- U --- U --- U --- U --- V 35. 1,1,1,2-Tetrachloroethane 0.22 1.000 --- U --- U --- U --- U --- U 36, Ethylbenzene 0.21 1.000 --- U --- U --- U --- U --- U 37, Rylenes 0.68 5.000 --- U --- U --- U --- U --- U 38. Dibromomethane 0.28 10.000 --- U --- U --- ❑ --- U --- U 39. Styrene 0.19 1.000 --- U --- U --- U --- U --- U 40. Bromoform 0.20 3.000 --- U --- U --- U --- U --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- U --- U --- U 42. 1,2,3-Trichloropropane 0.09 0.200 --- U --- U --- U --- U --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U --- U --- U --- U --- U 44. 1,2-Dichlorobenzene 0.32 S.000 --- U --- U --- U --- U --- U 45, 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- U --- U --- U --- U --- U 46. Acrylonitrile 2.72 200.000 --- U --- U --- U --- U --- U 47, trans-1,4-Dichloro-2-Butene 0.42 100.000 --- U --- U --- U --- U --- U 4B. Acralein 1.97 4.000 --- U --- U --- U --- U --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water In; 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 �� ; y REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: .TAP DATE COLLECTED: 12/03/20 Page: 2 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL MW-9A MW-10 MW-11 MW-13 MW-128 49. Allyl Chloride 0.20 10.000 --- U --- U --- U --- U --- U 50, Chloroprene 0.21 20.000 --- U --- U --- U --- U --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U --- a --- U --- U --- U 52. Dichlorodifluoromethane 0.51 5.000 --- U --- U --- U --- U --- U 53. 1,3-Dichloropropane 0.28 1.000 --- U --- U --- U --- U --- U 54. 2,2-Dichloropropane 0.17 15.000 --- U --- U --- U --- U --- U 55. 1,1-Dichloropropene 0.22 5.000 --- U --- U --- U --- U »-» U 56. Ethyl Methacrylate 0.16 10.0u0 --- 11 --- U --- U --- U --- U 57, Hexachlerebutadiene 0.10 0.200 --- U --- U --- U --- U --- U 58. Isobutyl Alcohol 12.80 100.000 _-- U --- U --- U --- U --- U 59. Methacrylonitrile 1.93 100.000 --- U --- U --- U --- U --- U 60. Methyl Methacrylate 0,25 30,000 --- U --- U --- U --- U --- U 61. Naphthalene 0.47 6.000 --- U --- U --- U --- U 2.70 J 62. Propionitrile 3.26 150.000 --- U --- U --- V --- U --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U --- U --- Ti --- U --- U 64. Acetanitrile 36.29 55.000 --- U --- U --- V --- U --- U 65. Tetrahydrofuran 0.39 1.000 --- U 6.24 5.16 2.65 29.00 66. 1,4-Dioxane 2.71 3.000 --- U 7.14 6.70 --- U 14.10 J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Eadhwg[W% hicupmUd Drinking Water 11); 37715 Wast®W$tB:t I'D�S 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LAME GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page: 3 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRI, Trip Blank 1. Chloromethane 0.77 3.000 --- U 2. Vinyl Chloride 0.12 0,200 --- U 3. Bromomethane 0.67 10.000 --- U 4. Chloroethane 0.48 10.000 --- ❑ 5. Trichlorofluoromethane 0.24 1.000 --- Ti 6. 1,1-Dichloroethene 0.17 5.000 --- V 7. Acetone 9.06 100.000 --- U B. iodomethane 0.26 10.000 --- U 9. Carbon, Disulfide 0.23 100,000 --- U 10. Methylene Chloride 0.64 1.000 --- U 11, trans-1,2-Dichloroethene 0.23 5.000 --- U 12. 1,1-Diehloroethane 0.20 5.000 --- Ti 13. Vinyl Acetate 0.20 50.000 --- U 14. Cie-1,2-Dichloroethene 0.25 5.000 --- Ti 15. 2-Butanone 2.21 100.000 --- V 16. Bromochloromethane 0.27 3.000 --- V 17. Chloroform 0.25 5.000 --- V 18. l,l,l-Trichloroethane 0.19 1.000 --- V 19. Carbon Tetrachloride 0.04 0.200 --- V 20, Benzene 0.24 11000 --- U 21, 1,2-Diehloroethane 0.02 0.200 --- U 22. Trichloroethene 0,23 1.000 --- U 23. 1,2-Dichloropropane 0.04 0.200 --- U 24, Bromodichloromethane 0.04 0.200 --- U 25. Cie-1,3-Dichloropropene 0.06 0.200 --- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U 27. Toluene 0.23 1.000 --- U 20. trans-1,3-Dichloropropene 0.04 0.200 --- U 29. 1,1,2-Trichloroethane 0.03 0.200 --- U 30. Tetrachloroethene 0.10 0,200 --- U 31. 2-Hexanone 1.57 50.000 --- U 32. DibromochlorUmethane 0.03 0.200 --- V 33. 1,2-Dibromoethane 0.03 0.200 --- U 34. Chlorobenzene 0.30 3.000 --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.000 --- U 36. Ethylbenzene 0.21 1.000 --- U 37. %ylenes 0.68 5.000 --- U 38. DibrDMOmethane 0.28 10.000 --- U 39. Styrene 0.19 1.000 --- U 40. Bromoform 0.20 3.000 --- U 41, 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U 42. 1,2,3-Trichloropropane 0.09 0,200 --- U 43. 1,4-Dichlorabenzene 0.39 1.000 --- U 44, 1,2-Dichlorobenzene 0.32 51000 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.200 --- U 46. Acrylonitrile 2.72 200.000 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100,000 --- U 48. Acrolein 1.97 4.000 --- U U a Estimated value between the MDL and MRL, U = Below ALL QUantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 ElMomminvU % bo-NuuMd Drinking Water IDz 37715 wastewater ID; .10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY. LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST: JAP DATE COLLECTED: 12/03/20 Page: 4 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/l MDL MRL Trip Blank 49. Allyl Chloride 0.20 10,000 --- V 50. Chloroprene 0.21 20.000 --- V 51. 1,3-Dichlorobenzene 0.41 5.000 --- U 52, Dichlorodifluoromethane 0.51 5.000 --- U 53. 1,3-Dichloropropane 0.28 1.000 --- U 54. 2,2-Dichloropropane 0.17 15.000 --- U 55. 1,1-Dichloropropane 0.22 5.000 --- U 56. Ethyl Methacrylate 0.16 10.000 --- U 57. Eexachlorobutadiene 0.10 0,200 --- U 58. ieobutyl Alcohol 12.80 100.000 --- U 59, Methacrylonitrile 1.93 100,000 --- U 60. Methyl Methacrylate 0.25 30.000 --- U 61. Naphthalene 0.47 6.000 --- U 62. Propionitrile 3.26 150.000 --- U 63. 1,2,4-Trichlorobenzene 0.50 10.000 --- U 64. Acetonitrile 36,29 55,000 --- U 65. Tetrahydrofuran 0.39 1.000 --- U 66. 1,4-Dioxane 2.71 3.000 --- U .l � Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits. ;A C)92?!:1 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 O 3 m m CJJ m m n 0 C o' cn 0 0 0 0 =r C CD CD C CO w CD U) i? CD 5 n m m C� 0 7 n U) m o m o o0 0 CD n � w m 3 co d (D Cu rR z 0 -0 z P 0 Q rA a Qz O s7jG] '`'ire] W �O ? �0} G -. LJ LA 1 fsJ 'S1 on F kJ c-A m I m m m J (11 9� trl z w ✓ m n n DZI TOTAL CHLORINE, mg/l L L L L - m m m OR ug/l AT COLLECTION �r� v� C o C © C o C TEMPERATURE,°C LIP, AT COLLECTION 0 #OFCONTAINERS m z Field PH "4 >` ' nv:;:: Nitrate -Nitrite ?C> Alkalinity 'b Chloride > '0 s'': Cyanide � 'd N a a a > TDS m m m Sulfate $r. Metals N ri }'^}'• C on ductivify DO Temperature '= Field Parameter EPA 8270E 3 < . 8270E Dup. 1 > 0 EPA 80818 � 4� n = PARAMETERsrrESTS C� j F C O m CS D7 3> C7 O C am r 0 m z t- = z Z Cm") m m o 'v1{ {ham- � C cn [n O a O m -V z m Z 5� b j I*> m � I C C Mm n O b n O m s T mr � C 0 o0 ) C n rl 2f z U? n -ni [, z z O 0 0 0 Cl v m C 'tz �. z- 00 4�. 0 � A r O t7 z DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 o G] c rr_urrt� of N C3 n b !ti l�1 3J m C i� CA r. F7n 0, fl o ron � � c Cr"tn)"C� r� y��•a� Z P c Un0 r- E5 U5 G7 N i^ y W � h �1 -• V w y 0 cc m m C) T1 Q ?° G p W o m m m ✓ - 9 O w m 3 -0 TOTAL CHLORINE, mg/I cQ m m m OR ug/I AT COLLECTION in e M m , TEMPERATURE,°C Q o AT COLLECTION p 3 in � rn a 00 00 00 o #OFCONTAINERS CD 808IB Duplicate > 0 �} C..... ..... ..... ..:J:p: ..... ': co 0 26 r� r 8D App.II PP 8260D A . II 2 G} � 8260D App. II 3 4� 8151A Landfill � 4� m m LAm .. .... 8151A Duplicate 4� O ORP v d c co v El m n CD v w 0 y C5 b J w o 2 o m 0 0 � CD � m v � o G�cnPARAMETERS/TESTS C, Q b mV � Pz N o lY C�i� c O L u L n m n 5 m a m.' z c cn = z zo Z I n� j O Z Do m C r C7 Q � z Cnn w 93 Q to O m in � cam* Z �n L7 " rp 0 W ^ W Rn' a n N n O N T CD o cn O c7 z O C y D m r�r m Z Z U) > Do CY) C G > o 0 z DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 brom (0irm d 114 OAKMONT DRIVE GREENVILLE, N C 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 k \ REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS CLIENT ID: ANALYST: DATE COLLECTED DATE ANALYZED: DATE REPORTED: PHONE (252) 756-6208 FAX (252) 756-0633 6003 B. JP 12/03/20 12/17/20 05/24/21 PARAMETERS, ug/l MDL MRL Concentration 1. Chloromethane 0.77 3.00 --- U 2. Vinyl Chloride 0.12 0.20 --- U 3. Bromomethane 0.67 10.00 --- U 4. Chloroethans 0.4B 10.00 --- U S. Trichloro€luoromethane 0.24 1.00 --- U 6. 1,1-Dichloroethene 0.17 5.00 --- U 7. Acetone 9.06 100.00 --- U 8. Iodomethane 0.26 10.00 --- U 9. Carbon Disulfide 0.23 100.00 --- U 10. Methylene Chloride 0.64 1.00 --- U 11. trans-1,2-Dichloroethene 0.23 5.00 --- U 12. 1,1-Dichloroethane 0.20 5.00 --- U 13. Vinyl Acetate 0.20 50.00 --- U 14. cis-1,2-Dichloroethene 0.25 5.00 --- U 15. 2-Butanone 2.21 100.00 --- U 16. Bxomochloromethane 0.27 3.00 --- U 17. Chloroform 0.25 5.00 1 --- U 10. 1,1,1-Trichloroethane 0.19 1.00 --- U 19. Carbon Tetrachloride 0.04 0.20 --- U 20. Benzene 0.24 1.00 --- U 21. 1,2-Dichloroethane 0.02 0.20 --- U 22. Trichloroethane 0.23 1.00 --- U 23, 1,2-Dichloropropane 0.04 0.20 --- U 24, Bromodichloromethane 0.04 0.20 --- U 25. cis-1,3-Dichloropropene 0.06 0.20 --- u 26. 4-methyl-2-Pentanone 1.19 100.00 --- U 27. Toluene 0.23 1.00 --- U 28. trans-1,3-Dichloropropene 0.04 0.20 --- u 29. 1,1,2-Trichloroethane 0.03 0.20 U 30. Tetrachloroethene 0.10 0.20 --- U 31. 2-Hexanone 1.57 40.00 --- U 32. Dibromochloromethane 0,03 0.20 --- T7 33. 1,2-Dibromoethane 0.03 0.20 --- U 34. Chlorobenzene 0.30 3.00 --- U 35, 1,1,1,2-Tetrachloroethane 0.22 1.00 --- U 36. Ethylbenzene 0.21 1.00 --- U 37. Xylenes 0.68 5.00 --- U 38, Dibromomethane 0.2B 10.00 --- U 39. Styrene 0,19 1.00 --- u 40. Bromoform 0.20 3.00 --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.20 --- U 42. 1,2,3-Trichloropropane 0.09 0.20 --- U 43, 1,4-Dichlorobenzene 0.39 1.00 --- Ti 44. 1,2-Dichlorobenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- U 46. Acrylonitrile 2.72 200.00 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.00 --- u 4B. Acrolein 1.97 4.00 --- U 49. Allyl Chloride 0.20 10.00 --- U 50. Chloroprene 0.21 20.00 ^- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Enw,nimmm % hwPOMW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. CLIENT ID: MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED DATE ANALYZED: DATE REPORTED: REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 B JP 12/03/20 12/17/20 05/24/21 PARAMETERS, ug/1 MDL MRL Concentration 51, 1,3-Dichlorobenzene 0.41 5.00 --- U 52. Dichlorodifluoromethane 0.51 5.00 --- U 53. 1,3-Dichloropropane 0.28 1.00 --- U 54, 2,2-Dichloropropane 0.17 15.00 --- U 55. 1,1-Dichloropropene 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 --- U 57. Hexachlorobutadiene 0.10 0.20 --- U 58. Isobutyl Alcohol 12.80 100.00 --- U 59. Methac:rylonitrile 1.93 100.00 --- U 60. Methyl Methacrylate 0.25 30.00 --- U 61. Naphthalene 0.47 6.00 --- U 62. Propionitrile 3.26 150.00 --- U 63. 1,2,4-Trichlorobenzene 0,50 10.00 --- U 64. Acetonitrile 36.29 55.00 --- U 65. Tetrahydrofuran 0.39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 --- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 I 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/03/20 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits (� recovery) 1,2-DCA-d4 ($ recovery) Toluene-d8 (% recovery) 4-BFB recovery) Continuing Calibration std. 70-130 104 93.6 97.5 Method Blank 70-130 102 101 104 MW-9A 70-130 99.5 97.7 99.3 MW-10 70-130 99.8 96.0 98.6 MW-11 70-130 99.1 95.7 97.9 MW-13 70-130 97.5 95.1 98.6 Trip blank 70-130 99.3 95.4 98.0 6003D MW-15 M.S. 70-130 99.7 97.1 100 6003D MW-15 M.S.D. 70-130 97.9 96.9 99.8 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/03/20 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS Sample Spiked: (6003D) MW-15 Spike Amount Ug/l Sample Result Ug/l Spike Result Ug/l Spike Recovery (70-130%) Spike Dup. Result Ug/l Spike Dup. Recovery (70-130%) MS/MSD RPD (20%) 1,1-Dichloroethene 20.0 --- UI 23.12 116 21.83 109 5.7 Benzene 20.0 --- U 22.24 ill 20.59 103 7.7 Trichloroethene 20.0 --- U 22.13 111 20.80 104 6.2 Toluene 20.0 --- U 22.39 112 20.56 103 8.5 Chlorobenzene 20.0 --- U 21.84 1 103 1 20.05 100 1 8.4 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount Ug/1 Spike Result Ug/1 Spike Recovery (70-130%) 1,1-Dichloroethene 20.00 19.41 97.1 Benzene 20.00 19.66 9B.3 Trichloroethene 20.00 19.60 98.0 Toluene 20.00 19.40 97.0 Chlorobenzene 1 20.00 19.24 1 96.2 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water 1D! 37715 Waet.swat.e.r IP4 I.O. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. MM SON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 C DATE COLLECTED: 12/02/20 DATE REPORTED : 05/24/21 �v REVIEWED BY:\� SW -I SW-2 SW-3 SW-4 Trip Analysis Method PARAMETERS MDL MRL Blank Date Analyst Code PH (field measurement), Units 6.9 7.2 6.8 6.4 12/02/20 SEB 4500HE-11 Antimony, ug/1 0.03 1.0 0,11 J 0.05 J 0.06 J 0.05 J 12/07/20 HMM EPA200.8 Arsenic, ug/1 0.08 5.0 1.5J 0.48 J 0.79 J 0.41 J 12/07/20 HMM EPA200.8 Barium, ug/l 0.04 10.0 74.6 52.9 93.4 90.0 12/07/20 HMM SPA200.8 Beryllium, ug/1 0.02 1.0 0.0B J 0.02 J 0,09 J 0.14 J 12/07/20 HMM EPA200.8 Cadmium, ug/1 0.04 1.0 --- U --- U --- U --- U 12/07/20 HMM EPA200.6 Cobalt, ug/l 0.02 1.0 0.60 J 0.24 J 0.90 J 0.74 J 12/07/20 HMN EPA200.8 Total Chromium, ug/1 0.12 5.0 4.2J 0.71J 1.4J 1.0J 12/14/20 HMM EPA200.6 Copper. ug/l 0.04 10.0 1.2J 0.19J 0,42 J 0.44 J 12/07/20 HUM EPA200.8 Lead, ug/1 0.03 5.0 1.5J 0,16 J 0.34 J 0.49J 12/07/20 HMM EPA200.8 Nickel, ug/l 0,03 10.0 0.74 J 0.25 J 0.60 J 0.49J 12/D7/20 HMM EPA200.8 Selenium, ug/l 0.05 10.0 0.35J 0.14 J 0.34 J 0.19J 12/07/20 HMM EPA200.8 Silver, ug/1 0.22 5.0 --- U --- U --- U 12/07/20 HMM EPA2D0.8 Silver, ug/1 0.22 5.0 --- U 12/14/20 HMM EPA200.8 Thallium, ug/l 0.02 1.0 0.02 .3 --- U 0.04 J 0.08 J 12/07/20 HMM EPA20D.B Vanadium, ug/1 0,04 1.0 4.6 0.38 J 1.2 1.4 12/14/20 HMM EPA200.8 Zinc, ug/l 0.17 10.0 5.8J 1.4J 4.1J 3.4J 12/07/20 HMM EPA200,0 Conductivity (at 25c), uMhos/cm 1.0 1.0 370 266 277 136 12/02/20 PJC 2510B-11 Dissolved Oxygen, mg/l 0.1 O.1 4.55 9.15 9.03 8.65 12/02/20 PJC 45000G-11 °C 9 6 6 7 12/02/20 PJC 255OB-10 Temperature, +105 +98 +106 +118 22/02/20 PJC 2580E-11 ORP, my Turbidity (Field), NTU 1.0 1.0 11.00 2.80 13,30 13.00 12/02/20 PJC 213DB-11 All QC requirements were not met: D Duplicate data not within established limits. J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 C ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 1 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 Date MDL Analyzed MRL 12/11/20 SW-1 12/11/20 SW-2 12/11/20 SW-3 12/11/20 SW-4 12/12/20 Trip Blank 1, Chloromethane 0.77 3.000 --- U --- U --- V --" U --- U 2. Vinyl Chloride 0.12 0.200 --- U --- U --- U --- U --- U 3. Bromomethane 0.67 10.000 --- U --- U --- U --- U --- U 4, Chloroethane 0.48 10.000 --- U --- U --- U --- U --- U 5, Trichlorofluoromethane 0.24 1.000 --- U --- U --- U --- U --- U 6. 1,1-Dichloroethene 0.17 5,000 --- U --- U --- U --- U --- U 7. Acetone 9.06 100.000 --- U --- U --- U --- U --- U 8. Iodomethane 0.26 10.000 --- U --- U --- U --- U -`- U 9. Carbon DisulEide 0.23 100.000 --- U --- U --- U --- U --- U 10. Methylene Chloride 0.64 1.000 --- U --- U --- U --- U --- U 11. trans-1,2-Dichloroethene 0.23 5.000 --- U --- U --- U --- U --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U --- U --- U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- U --- U --- U 14. Cis-1,2-Dichloroethene 0.25 5.000 --- U --- U --- U --- U --- U 15. 2-Butanone 2.21 100.000 --- U --- U --` U --- U --- U 16, Bromochloromethane 0.27 3.000 --- U --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U --- U --- U 18. 1,1,1-Trichloroethane 0119 1.000 --- U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U -"- U --- U --- U 20. Benzene 0,24 1.000 --- U --- U -'- U --- U --- U 21. 1,2-Dichloroethane 0.02 0,200 --- U --- U --- U --- U 0.03 J 22. Trichloroethane 0.23 1.000 --- U --- U --- U --- U -"" U 23. 1,2-Dichloropropane 0.04 0.200 --- U --- U --- U --- U --- U 24. Bromodichloromethane 0.04 0,200 --- U --- U --- U --- U U 25. Cis-1,3-Dichloropropene 0.06 0.200 --- U --- V --- U --- U --- U 26, 4-Methyl-2-Pentanone 1,19 100.000 --- U --- U --- U --- U --- U 27. Toluene 0.23 1.000 --- U --- U --- U --- U --- U 28, trans-1,3-Dichloropropene 0.04 0,200 --- U --- U --- U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0,200 --- U --- U --- U --- U 0.03 J 30. Tatrachloroethene 0.10 0.200 --- U _-- U --- U --- U --- U 31. 2-Hexanone 1.57 50.000 --- U --- U --- U "-- U --- U 32. Dibromochloromethane 0,03 0.200 --- U --- U --- U --- U 0.03 J 33. 1,2-Dibromoethane 0.03 0.200 --- U --- U --- U --- U 0.03 J 34, Chlorobenzene 0,30 3.000 --- U --- U --- U --- U --- U 35. 1,1,1,2-Tatrachloroethane 0.22 1.000 --- U --- U --- U --- U "-- U 36. Ethylbenzene 0.21 1.000 --- U --- V --- U --- U --- U 37. Xylenee 0.68 5.000 --- U --- U --- U --- U --- V 38, Dibromomethane 0.28 10.000 --- U --- U --- U "-- U --- V 39. Styrene 0.19 1.000 --- U --- U --- U 40. Bromoform 0.20 3.000 --- U --- U --- U --- U - U 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- U --- U 0.03 J 42, 1,2,3-Trichloropropane 0.09 0.200 _-- U --- U --- U --- U --- U 43, 1,4-Dichlorobenzene 0.39 1,000 --- U --- U --- V --- U -"" U 44. 1,2-Dichlorobenzene 0.32 5.000 --- U --- U --- U --- U --- U 45. 1,2-Dibroma-3-Chloropropane 0.07 0.200 --- U --- U --- U --- U - U 46. Acrylenitrile 2.72 200.000 --- U --- U --- U --- U --- U 47. trans-1,4-Dichloro-2-Butene 0,42 100.000 --- U --- U --- U --- U --- U J = Batimated value between the MDL and MRL, U = Below ALL 4uantitation Limite. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID; 37715 wastewater IDa 7..0. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 C ANALYST: JAP DATE COLLECTED: 12/02/20 Page: 2 DATE REPORTED: 05/24/21 Pate Analyzed 12/11/20 12/11/20 12/11/20 12/11/20 12/12/20 SW-1 SW-2 SW-3 SW-4 Trip PARAMETERS, ug/1 MDL MRL Blank 48. Acrolein 1,97 4.000 --- D --- U --- u --- V --- U 49. Allyl Chloride 0.20 10.000 --- u --- U --- u --- u --- U 50. Chloroprene 0.21 20.000 --- u --- u --- U --- U ""- u 51. 1,3-Dichlorobenzene 0.41 5,000 --- u --- U --- U --- U --- U 52. DichiorodiEluornmethane 0.51 5.000 --- U --" u --- V --- V --- u 53. 1,3-Dichloropropane 0.28 1.000 --- u --- U '-- V -"" u -'- U 54. 2,2-Dichloropropane 0.17 15.000 --- u --- u --- V --- U _-- u 55. 1,1-Dichloropropene 0.22 5.000 --- V --- u --- u --- V --- u 56. Ethyl Methacrylate 0.16 10.000 --- u --- u --- u --- u »-- V 57. [iexachlorobutadiene 0.10 0.200 --- V --- U --- V --- u --- u 58. Isobutyl Alcohol 12.80 100.000 --- u --- U --- U --- u --- u 59. Mothacrylonitrile 1.93 100.000 --- u --- u --- u --- u --- u 60. Methyl Methacrylate 0.25 30.000 --- u --- V »-- u --- u --- V 61, Naphthalene 0.47 6.000 --- U --- V --- Ti --- u --- U 62, Proptnnitrile 3.26 150.000 --- u --- V --- V --- V --- U 63. 1,2,4-TriChlOrobenzene 0.5o 10.000 --- u --- u --- V --- U --- u 64, Acetonitrile 36.29 55,000 --- V --- V --- D --- u --- V 65. Tetrahydrofuran 0.39 1.000 --- V --- u 0.45 J --- u --- u 66. 1,4-Dioxane 2.71 3.000 --- U --- u --- U --- u --- u a = Estimated value between the MDL and MRL, V = Below ALL QuantitatiOn Limits. DocuSi EF 0 0 CID Q CD Z)-0 Er FT CD � 0 0 ci � - fl) _ w 0 < O (D 3- 0 (D n � w 3 0 CD CD w a gn tnveiope iu: ov,5ottzwA-/USt-4rl L-y4H21-ly4"uot 1ttSl w7� p @ N 7� A z � v� cn rn cn �y � o7 < 00 �S D C �] c p C tomt is w N •- d cr o ' ~�Z Z N 3 m o f� m o o r�Z '� v m m CD CD U)ON W 0 v Fn (] •r1 NAo1i 9 -p Cr" .r m m _, m dQ .f O t� 'k Z w vA 't m m m 33 TOTAL CHLORINE, mg/l 0 vi m OR ug/I AT COLLECTION a 0 0 J Q. � � TEMPERATURE,°C O ATCOLLECTION O m ul u7 # OF CONTAINERS z Field pH -G Metals y Conductivity DO > rb. " V _., Temperature Y b n n a n 8260 Dap. I `V m m m 8260 Dup. 2 8260 Dup. 3 c� c m "'"': 8260 Dup. 4 G] n.: 8260 D App. II N 8260D App. II 2 M 0 � 4{A{ 8260D App. II 3 Field Parameter Z V co =p cn c� n PARAMETERSITESTS n n n p Fn `% 7/:0 C CD C) fld 0 O In p -n T z Z it Z m C> "I Z m m r In �� ' o m m m m 0 c� 3 z o °-< 0 2�° 2S u' �", z m G7 ?+ m o m ii z a D ED InT. n c) n n o s7 [t I s z cn on y = z n 0 r �7 z n n ` m n CVm/i r� T7 n N ry o n0 z n d DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EINAmina(M Ala kwymmUd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 C MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/02/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 IN REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS PARAMETERS, ug/l NDL MRL Concentration 1. Chloromethane 0.77 3.00 --- U 2. Vinyl Chloride 0.12 0.20 --- U 3. Bromomethane 0.67 10.00 --- U 4. Chloroethane 0.48 10.00 --- U S. Trichloro£luoromethane 0.24 1.00 --- U 6. 1,1-Dichloroethene 0.17 5.00 --- U 7. Acetone 9.06 100.00 --- U B. lodomethane 0.26 10.00 --- U 9. Carbon Disulfide 0.23 100.00 --- U 10. Methylene Chloride 0.64 1.00 --- U 11. trans-1,2-Dichloroethene 0.23 5.00 --- U 12. 1,1-Dichloroethane 0.20 5.00 --- U 13. Vinyl Acetate 0.20 50.00 --- U 14. cis-1,2-Dichloroethene 0.25 5.00 --- U 15. 2-Butanone 2.21 100.00 --- U 16. Bromochloromethane 0.27 3.00 --- U 17. Chloroform 0.25 5.00 --- U 18. 1,1,1-Txichloroethane 0.19 1.00 --- U 19. Carbon Tetrachloride 0.04 0.20 --- U 20. Benzene 0.24 1.00 --- U 21. 1,2-Dichloroethane 0.02 0.20 --- U 22. Trichloroethene 0.23 1.00 --- U 23. 1,2-Dichloropropane 0.04 0.20 --- U 24. Bromodichloromethane 0.04 0.20 --- U 25. cis-1,3-Dichloropropene 0.06 0.20 --- U 26. 4-methyl-2-Pentanone 1.19 100.00 --- U 27. Toluene 0.23 1.00 --- U 28. trans-1,3-Dichloropropene 0.04 0.20 --- U 29. 1,1,2-Trichloroethane 0.03 0.20 --- U 30. Tetrachloroethene 0.10 0.20 --- U 31. 2-Hexanone 1.57 40.00 --- U 32. Dibromochloromethane 0.03 0.20 --- U 33. 1,2-Dibromoethane 0.03 0.20 --- U 34. Chlorobenzene 0.30 3.00 --- U 35, 1,1,1,2-Tetrachloroethane 0.22 1.00 ---- U 36. Ethylbenzene 0.21 1.00 --- U 37. Xylenes 0.68 5.00 --- U 38. Dibromomethane 0.28 10.00 --- U 39. Styrene 0.19 1.00 --- U 40. Bromoform 0.20 3.00 --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.20 --- U 42. 1,2,3-Trichloropropane 0.09 0.20 --- U 43. 1,4-Dichlorobenzene 0.39 1.00 --- U 44. 1,2-Dichlorobenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- U 46. Acrylonitrile 2.72 200.00 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.00 --- U 411 Acrolein 1.97 4.00 --- U 49. Allyl Chloride 0.20 10.00 --- U 50. Chloroprene 0.21 20.00 -- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 CLIENT ID: ANALYST: DATE COLLECTED DATE ANALYZED: DATE REPORTED: REVIEWED BY: / ✓ -y VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 C JP 12/02/20 12/11/20 - 12/12/20 05/24/21 PARAMETERS, ug/1 HDL MRL Concentration 51. 1,3-Dichlorobenzene 0.41 5.00 --- U 52. Dichlorodifluoromethane 0.51 5.00 --- U 53. 1,3-Dichloropropane 0.28 1.00 --- U 54. 2,2-Dichloropropane 0.17 15.00 --- U 55, 1,1-Dichloropropene 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 --- U 57. Hexachlorobutadiene 0.10 0.20 --- U 58, Isobutyl Alcohol 12.80 100.00 --- U 59. Methacrylonitrile 1.93 100.00 --- U 60. Methyl Methacrylate 0.25 30.00 --- U 61. Naphthalene 0.47 6.00 --- U 62. Propionitrile 3.26 150.00 --- U 63. 1,2,4-Trichlorobenzene 0.50 1 10.00 --- U 64. Acatonitrile 36.29 55.00 --- U 65. Tetrahydrofuran 0.39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 --- U L DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EuwkmuM Ala ku-Numbd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: '4/'' `� \ PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 C ANALYST: JP DATE COLLECTED: 12/02/20 DATE ANALYZED: 12/11/20 - 12/12/20 DATE REPORTED: 05/24/21 VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits (% recovery) 1,2-DCA-d4 ( recovery) Toluene-d8 (% recovery) 4-BFB (% recovery) Continuing Calibration std. 70-130 100 101 102 Method Blank 70-130 98.3 97.6 97.4 Sw-1 70-130 104 102 99.6 Sw-2 70-130 101 100 98.5 SW-3 70-130 101 100 98.4 sw-4 70-130 101 101 99.7 Trip Blank 70-130 98.5 97.6 94.7 6003 MW-4 M.S. 70-130 104 103 100 6003 Mw-4 M.S.D. 70-130 104 102 100 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 % hmpumbd r - 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID: ANALYST: DATE COLLECTED DATE ANALYZED: DATE REPORTED: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 C JP 12/02/20 12/11/20 - 12/12/20 05/24/21 Sample Spiked: (6003) MW-4 Spike Amount Ug/l Sample Result Ug/1 Spike Result Ug/l Spike Recovery (70-130%) Spike Dup. Result Ug/l Spike Dup. Recovery (70-130%) MS/MSD RPD (20%) 1,1-Dichloroethene 20.0 --- U 23.38 117 22.48 112 3.9 Benzene 20.0 --- U 22.93 115 21.43 107 6.B Trichloroethene 20.0 --- U 22.59 113 21.46 107 5.1 Toluene 20.0 --- U 21.77 109 20.82 104 4.5 Chlorobenzene 20.0 - - U 21.98 1 110 20.77 104 5.7 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount Ug/l Spike Result Ug/1 Spike Recovery (70-130%) 1,1-Dichloroethene 20.00 20.07 100 Benzene 20.00 20.06 100 Trichloroethene 20.00 20.16 101 Toluene 20.00 19.96 100 Chlorobenzene 1 20.00 1 20.11 1 101. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Fli'"n[d % h�o�� Drinking Water ID: 37715 -Wavtv'wa,t.ai4 �D:. 10. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR, J7UDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 D DATE COLLECTED: 12/08/20 DATE REPORTED : 05/24/21 ✓ �✓ `--' REVIEWED BY: - ✓ �/ MW-15 MW-16 MW-17 MW-14S MW-14D Analysis Method PARAMETERS MDL MRL Date Analyst Code PH (field measurement), unite 5,9 6.0 5.6 6.7 7.6 12/00/20 SEB 4500HB-11 Nitrate+Nitrite as N, mg/l 0.04 0.04 --- U --- U --- U --- U 0.23 12/09/20 AES 353.2 R2-9 Alkalinity Ito pH 4.5), mg CaCO3/1 1.0 1.0 76 124 24 1180 250 12/14/20 TMR 2320E-11 Chloride, mg/1 5.0 5.0 18 25 18 77 15 12/14/20 KbS 4500CLB-ll Cyanide, ug/1 5.0 5,0 --- U --- U --- U --- U --- U 12/10/20 SEJ 450OCNE-11 Total Dissolved Residue, mg/1 1.0 10 361 691 422 1450 314 12/10/20 TMR 2540C-11 Sulfate, mg/l 5.0 5.0 147 348 165 29,8 --- U 12/09/20 SEJ 4500SO42E1 Antimony, ug/1 0.03 1.0 --- U --- U 0.12 J 0.19 J 0.11 J 12/14/20 HMM EPA200.8 Arsenic, ug/1 0.08 5.0 0.89 J 5.4 0.43 J 3.8J 0.40 J 12/22/20 HMM EPA200.8 Barium, ug/l 0.04 10.0 150 207 384 12/21/20 HMM EPA200.8 Barium, ug/l 0.04 10.0 71 11 12/14/20 HMM EPA200.8 Beryllium, ug/l 0.02 1.0 0.20 J 0.05 J 0.09 J 0.05 J --- U 12/14/20 HMM SPA200,8 Cadmium, ug/l 0.04 1.0 --- U --- U --- U --- U --- U 12/14/20 HMM EPA200.8 Cobalt, ug/1 0.02 1.0 0.20J 0.B1 J 0.15 J 1.8 --- U 12/14/20 HMM EPA200.8 Total Chromium, ug/1 0.12 5.0 1.5 J 2.9 J 1.7 J 16 0.18 J 12/14/20 HMM EPA200.6 Copper, ug/l 0.04 10.0 0.10 J 0.09 J 0.16 J 0.22 J 0.39 J 12/14/20 HMM EPA200.8 Iron, ug/l 4.96 50.0 974E 60200 2940 8689 36 J 12/21/20 LFJ EPA200.7 Manganese, ug/1 0.31 10.0 124 310 271 1104 3 J 12/21/20 LFJ EPA200.7 Lead, ug/l 0.03 5.0 0.10 J _-- U 0.12 J 0.22 J --- U 12/21/20 HMM EPA200.8 Mercury, ug/l 0.05 0.20 --- U --- U --- U --- U --- U 12/09/20 MTM 245.1 R3-9 Nickel, ug/l 0.03 10.0 0.32 J 0.42 J 0.38 J 1.6 J 0.22 J 12/14/20 HMM EPA200.8 Selenium, ug/l 0.05 10.0 1.3 J 0.86 J 0,29 J 0.84 J --- U 12/22/20 HMM EPA200.8 Silver, ug/l 0.22 5.0 --- U --- U --- U --- U --- U 12/14/20 HMM EPA200.8 Thallium, ug/l 0.02 1.0 0,02J 0.02 J --- U 0.05J 0.02 J 12/14/20 HMM EPA200.8 Tin, ug/l 0.05 100.0 0.09 J 0.15 J 0.18 J --- U --- U 12/29/20 HMM EPA200.8 Vanadium, ug/1 0.04 1.0 6.9 7.0 2.8 5.6 0.22 J 12/14/20 HMM EPA200.8 Zinc, ug/l 0,17 10.0 9.6 J 0.56 J 1.B J 1.4 J 4,7 J 12/14/20 HUM EPA200.8 Sulfide, ug/1 100 1000 --- U --- U 397 J --- U --- U 12/11/20 LFJ 450082D-11 Conductivity tat 25c), uMhoa/cm 1.0 1.0 536 905 587 2420 543 12/08/20 SEB 251OB-11 Dissolved Oxygen, mg/l 0.1 0.1 1.15 1.69 1.26 2.32 1.13 12/08/20 SEB 450000-11 Temperature, °C lB 20 18 18 17 12/08/20 SEE 2550E-10 Static Water Level, feet 6.34 7.02 7.14 5.85 5.30 12/00/20 SEB Well Depth, feet 22.14 22.73 22.25 23.12 41,92 12/09/20 SEB ORP, my +96 +112 +06 +77 +43 12/08/20 SEB 25BOB-11 Turbidity (Field), NT❑ 1.0 110 7.40 7.64 6.01 9.67 1,21 12/08/20 SRB 2130E-11 All QC requirements were not mete D Duplicate data not within established limits. J = Estimated value between the MDL and MRL, U = Below ALL Ouantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID% 37715 Wastewater ID-., 10, 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHIfi EHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ��/�✓'�� PESTICIDES AND PCB'S EPA METHOD 8081B R2(07) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: HIC DATE COLLECTED: 12/08/20 DATE EXTRACTED: 12/09/20 DATE REPORTED: 05/24/21 Date Analysed 12/16/20 12/28/20 12/28/20 12/16/20 12/16/20 MW-15 MW-16 NW-17 MW-14S MW-14D PARAMETERS, ug/1 MDL MRL 1. Aidrin 0.029 0.050 --- U --- U --- U --- U --- U 2, Alpha-BHC 0.032 0.050 --- U --- U --- U --- U '-- U 3. Beta-BHC 0.031 0.050 --- U --- U --- U --- U --- U 4. Delta -BBC 0.030 0.050 --- U --- U --- U --- U --- U 5. Gamma-BHC (Lindane) 0.032 0.050 --- U --- U --- U --- U --- U 6. Chlordane 0.320 0.500 --- U --- U --- U --- U --- V 7. 4,4-DDD 0.051 0.100 --- U --- U --- U --- U --- U 8, 4,4-DDE 0.049 01100 --- U --- U -_- U --- U --- U 9, 4,4-DDT 0.052 0.100 --- D --- U --- U --- U --- U 10, ❑ieldrin 0.042 0.075 --- U --- U --- U --- U --- U 11. Endoaulfan 1 0.056 0.100 --- U --- U --- U --- U "-- U 12. Endoeulfan I1 0.046 0.100 --- U --- U --- D --- U --- U 13. Endaaulfan Sulfate 0.072 0.100 --- U --- U --- U --- U --- U 14. Endrin 0.053 0.100 --- U --- U --- U --- U --- U 15. Endrin Aldehyde 0,068 0.100 --- U --- U --- U --- U - U 16. Heptachlor 0.039 01050 --- U --- U --- U --- U --- U 17. Heptachlor Epoxide 0,042 0.075 --- U --- U --- U --- U --- U 19. Methoxychlor 0.530 1,000 --- U --- U --- U --- U --- U 19, keb's (Aroolors) 0.500 2.000 --- U --- U --- U --- U --- U 20. Toxaphene 0.690 1.500 --- U --- U --- U --- U -"' U a = Estimated value between the MDL and MRL, V = Below ALL Quantitation Limits, DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EINAmm@10 % hmpughd Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEH'URST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: �� v LANDFILL APPENDIX II EPA METHOD 8151A R1(96) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: HIC DATE COLLECTED: 12/08/20 DATE EXTRACTED: 12/10/20 DATE REPORTED: 05/24/21 Date Analyzed 12/12/20 12/12/20 12/12/20 12/12/20 12/11/20 MW-15 Mw»16 MW-17 MW-14S MW-14D PARAMETERS, u9/1 MDL MRL 1. 2,4-D 0.36 2.000 --- U --- U --- U --- U --- U 2. ❑inoeeb 0.54 1.000 --- U --- U --- U --- U __- U 3. 2,4,5-TP 0.42 2.000 --- U _-- U --- U --- U --- U 4, 2,4,5-T 0,47 2.000 --- U --- U --- U --- U ».._ U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EmAnnimM % hc)mFumbdo Drinking Water ID; 37715 --WaBtewat.ar ZDa..LO_ 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/08/20 Page: 1 DATE EXTRACTED: 12/14/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 Date MDL Analyzed MRL 12/30/20 MW-15 12/31/20 MW-16 01/05/21 MW-17 01/05/21 MW-149 01/05/21 MW-14D 1. Acenaphthene 2.66 10.000 --- U --- U --- U »-- U --- U 2. Acenaphthylene 2.60 10.000 --- U --- U --- U --- U --- U 3. Anthracene 2.97 10.000 --- U --- U --- U --- U '-- U 4. Benzo[a]antrhacene 4.16 10,000 --- U --- U --- U --- U --- U 5. Benzo[b]fluoranthene 3.32 10.000 --- U --- V --- U --- U --- U 6, Benzo[klfluoranthene 4.23 10,000 --- Ti --- U --- U --- Ti --- U 7. Benzo[g,h,i]perylene 2.61 10.000 --- U --- U --- U --- U --- U 0, Benzo[a]pyrene 3.27 10.000 --- U --- U --- U --- U --- U 9. 4-Bromophenyl Phenyl ether 2.63 10.000 --- U "-- U --- U --- U --- U 10. Butyl Benzyl Phthalate 5.78 10.000 --- U --- U --- U --- U --- U 11. Bls(2-Chloroethoxy) Methane 3.14 10.000 --- U --- U --- U -'" U -"' U 12, Bia(2-Chloroethyl) Ether 2.5H 10.000 --- U --- U --- V -»» U --- U 13. Bis(2-Chloro-l-methylethyl) Ether 2.58 10,000 --- U --- U --- U --- U --- U 14. 2-Chlaronaphthalene 2,17 10.000 --- U --- V --- U --- U --- U 15. 4-Chlorophenyl Phenyl Ether 2.42 10,000 --- U --- U --- U --- V --- U 16. Chryeene 4.04 10.000 --- U --- U --- U --- U --- U 17. ❑ibenzo[a,h]anthracene 2.78 10.000 --- ❑ --- U --- U --- U --- U 18. Di-N-Butyl Phthalate 3.09 10.000 --- U --- U --- U --- U --- U 19. Dimethyl Phthalate 3.78 10.000 --- U --- U --- U --- U --- U 20. Diethyl Phthalate 3.92 10.000 --- V --- U --- U --- U U 21. 2,4-Dinitrotoluene 3.95 10.000 --- U --- U --- U --- U --- U 22. 2,6-Dinitrotoluene 3.08 10.000 --- U --- U --- U --- U --" U 23. Di-N-Octyl Phthalate 2.81 10.000 --- U --- U --- U --- V --- U 24. Bis-(2-Ethylhexyl) Phthalate 9.97 15.000 --- U --- U --- U --- U --- U 25, Fluoranthene 3.92 10.000 --- U --- U --- U --" U --- U 26. FluOrene 2.95 10,000 --- U --- U --- U --- U --- U 27, Hexachlorobenzene 2.61 10.000 _-- U --- U --- U --- U --- V 28. Hexachlorocyclopentadiene 4.16 10.000 --- U --- U --- U --- U --- U 29, Indeno(1,2,3-Cd)pyrene 2.91 10.000 --- U --- U --- U --- U --» U 30. lsophorone 3.74 10.000 --- U --- U --- U --- V "'- U 31, Nitrobenzene 2.85 10.000 --- U --- U --- U --- U --- U 32, N-Nitroaodimethylamine 4.25 10.000 --- U --- U --- a --- U --- U 33. N-Nitrosodiphenylamine 3.95 10.000 --- U --- U --- U --- U --- U 34, N-Nitrosodi-N-Propylamine 4.06 10.000 --- U --- U --- U --- U --- V 35. Phenanthrene 3.24 10.000 --- U --- U --" U --- U --- V 36. Pyrene 3.63 10.000 --- U --- U --- U --- U --- U 37. 4-Chloro-3-Methylphenol 3.79 20,000 --- U --- U --- U --- U --- U 38. 2-Chlorophen0l 2.75 10,000 --- V --- U --- U --- U --- U 39, O-Cresol 3.68 10.000 --- V --- U --- U --- U --- U 40, P-Cresol 4.12 10.000 --- U --- U --- U --- U --- U 41. 2,4"Dichlorophen0l 5.19 10.000 --- U --- U --- U --- U -"" U 42. 2,6-Dichlorophenol 4.89 10.000 --- U --- U --- Ti --- U --- U 43. 2,4-Dimethylphen0l 3.21 10.000 --- U --- U --- U --- U --- U 44. 4,6-Dinitro-2-Methylphenol 4.77 50.000 --- U --- U --- U --- U --- U 45. 2,4-Dinitrophenol 4.31 50.000 --- U --- V --- U --- V --- U 46. Ethyl Methanesulfonate 5.26 20.000 --- V --- U --- U --- U "-- U 47, Methyl Methanesulfonate 4.92 10.000 --- U --- U --- U --- U --- U J = Eatimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking water ID: 37715 Wastewater IDS 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ✓�� t/y SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/08/20 DATE EXTRACTED: 12/14/20 DATE REPORTED: 05/24/21 Page: 2 PARAMETERS, ug/l Date Analyzed MDL MRL 12/30/20 MW-15 12/31/20 MW-16 01/05/21 MW-17 01/05/21 MW-14S 01/05/21 MW-14D 4B. 2-Nitrophenol 3.64 10.000 --- U --- U --- U --- U -`- U 49. 4-Nitrophenol 3.17 50,000 --- U --- U --- U --» 11 --- U 50. Pentachlorophenol 5.33 25.000 --- U --- U --- U --- U --- U 51. Phenol 1.86 10.000 --- U --- U --- U --- U --- U 52. 2,3,4,6-Tetrachlorophenol 3.12 10.000 --- U --- U --- U --- U --- U 53, 2,4,5-Trichlorophenol 4.17 10,000 --- U --- U --- U --- U --- U 54, 2,4,6-Trichlorophenol 3.84 10.000 --- U --- U --- U --- U --- U 55. Acetophenone 2.89 10.000 --- U --- V '-- U --- U --" U 56. 2-Acetylaminofluorcne 3.98 20.000 --- U --- U --- U --- U --- U 57. 4-Aminobiphenyl 4.12 20.000 --- U --- U --- U --- U --- lJ 50, Benzyl Alcohol 4.47 20.000 --- U --- U --- U --- U --- U 59. 4-Chloroaniline 3.36 20.000 --- U --- U --- V --- U --- U 60. Chlorobenzilate 5.12 10.000 --- U --- U --- V --- U --- U 61. Diallate 2.96 10.000 --- U --- U --- U --- U --- U 62, Dibenzcfuran 4.20 10.000 --- U --- U --- U •-- U --- U 63. 3,31-Dichlorobenzidlne 4.22 20.000 --- U --- U --- U --- U --- U 64, Dimethoate 3.98 20.000 --- U --- U --- U --- U --- U 65. P-Dimethylaminoazobenzene 2.89 10.000 --- U --- U --- U --- U --- U 66, 7,12-Dimethylbenz[a]anthracene 5.26 10,000 --- U --- U --- U --- U --- U 67. 3,3-Dimethylbenzidine 3.21 10.000 --- U --- U "-- U --- U - U 68. 1,3-Dinitrobenzene 2.89 20.000 --- U --- U --- U --- U --- U 69, Diphenylamine 5.10 10.000 --- U --- U --- U --- U --- U 70. DlaulfOtOn 4.28 10.000 --- U --- U --- U --- U --- U 71. Famphur 3.90 20.000 --- U --- U --- U --- U --- U 72, Hexachloropropene 4.31 10.000 --- U --- U --- U --- U --- U 73, Isosafrole 2.08 10.000 --- U --- U --- U --- U -" U 74, Kepone 2.78 20.000 --- U --- U --- U --- U U 75. Methapyrilene 3.54 100.000 --- U --- U --- V --- U --- U 76. 3-Methylcholanthrene 4.21 10.000 --- U --- U --- U --- U --- U 77. 2-Methylnaphthalene 3.79 10.000 --- U -'- U --- U --- U --- U 78. Methyl Parathion 4.32 10.000 --- U --- U --- U --- U - U 79. m-Cresol 3.81 10.000 --- U -'- V '-- U --- U --- U 80, 1,4-Naphthoquinone 4.00 10.000 --- U --- U "-- U --- U --- U 01. 1-Naphthylamine 5.61 10,000 --- U --- U --- U --- U --- V 82. 2-Naphthylamine 4,62 10.000 --- U --- U --- U --- U --- U 03. 2-Nitroaniline 3.61 50.000 --- U --- U --- U --- U - U 84. 3-Nitroaniline 4.81 50.000 --- U --- U --- U --- U --- U 85. 4-Nitroaniline 4.22 20.000 --- U --- U --- U --- U --- U 86. 5-Nitro-D-Toluidine 4.01 10.000 --- U --- U --- U --- U --" U 87. N-Nitrosodl-n-butylamine 3.63 10.000 --- U --- U --- U --- U --- U 80, N-Nitroeodiethylamine 3.83 20,000 --- U --- U --- U --- U - U $9, N-Nitrosomethylethylamine 3.83 10.000 --- U --- U --- U --- U --- U 90, N-Nitrosopiperldine 5.19 20.000 --- U --- U --- U --- U - U 91. N-Nitrosopyrrolidine 2.09 10.000 --- U --- U --- U --- U - U 92. Parathion 3.12 10.o00 --- U --- U --- U --- U --- U 93. Pentachlorobenzene 3.92 10,000 --- U U -" U --" U --- U 94. Pentachloronitrobenzene 3.71 20.000 --- U '-- U --- U --- U --- U J - Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 E�]d��0�[C@l�l� Drinking Water ID: 37715 Wastewater I➢: 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/20 Page: 3 DATE EXTRACTED: 12/14/20 DATE REPORTED: 05/24/21 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Date Analyzed PARAMETERS, ug/l MDL MRL 12/30/20 MW-15 12/31/20 MW-16 01/05/21 MW-17 01/05/21 MW-14S 01/05/21 MW-14D 95. Phenacetin 4.41 20.000 --- U --- V --- U --- U --- U 96. 1,4-Benzenediamine 2.99 10.000 --- U --- U --- U --- U --- U 97. Phorate 3.86 10.000 --- U --- U --- U --- U --- U 98. Pronamide 3.69 10,000 --- U --- U --- U --- U --- U 99. Safrole 4.12 10.000 --- U --- U --- U --- U ---- U 100, 1,2,4,5-Tetrachlorobenzene 5.01 10.000 --- U --- U --- U --- U --- U 101, Thionazin 4.62 20.000 --- U --- U --- U --- U --- U 102. 0-Toluidine 4,11 10,000 --- U --- U --- U --- U --- U 103. 1,3,5-Trinitrobenzene 3.98 10.000 --- U --- U --- U --- U --- U 104. 0,0,0-Triethyl PhDephorothioate 3.61 10.000 --- U --- U --- U --- U --- V 105. Hexachloroethane 1.49 10,000 --- U --- U --- U --- U --- U 106. Ieodrin 3.11 20.000 --- U --- U --- U --- U -"" U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 NEW'numM alp hCorlowpoo�od _ -- . 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Drinking water Im 37715 AL PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/08/20 Page: 1 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 MW-15 edw-16 MW-17 MW-14S MW-14D PARAMETERS, ug/1 MDL MRL 1, Chloromethane 0.77 3.000 --- U --- U --- U --- U --- U 2, Vinyl Chloride 0,12 0.200 --- U --- U --- U 1.96 --- U 3. Bromomethane 0,67 10.000 --- U --- U --- U --- U --- U 4, Chioroethane 0.49 10.000 --- U --- U --- U I --- U _d_ U 5. Trichlorofluoromethane 0.24 1,000 --- U --- U --- U --- U --- U 6, 1,1-Dichloroethene 0.17 5.000 --- U --- U --- U --- U """ U 7. Acetone 9.06 100.000 --- U --- U --- U --- U --- U S. iodomethane 0.26 10.000 --- U --- U --- V --- U --- U 9. Carbon Disulfide 0.23 100,000 --- U --- U --- U --- U --- U 10, Methylene Chloride 0.64 1.000 --- U --- U --- U --- U --- U 11. trans-1,2-Dichloroethene 0.23 5.000 --- U --- V --- U --- U --- U 12, 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U --- U --- U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- U --- U --- U 14. Cis-1,2-Dichloroethene 0.25 5,000 --- U --- U --- U --- U --- U 15. 2-Butanone 2.21 100.000 --- U --- U --- U --- U --- U 16. Bromoohloromathane 0.27 3.000 --- U --- U --- U --- U --- U 17. Chloroform 0.25 5.000 --- U --" U --- U --- U "-- U 18. 1,1,1-Trichloroethane 0.19 1.000 --- U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U --- U --- U 20. Benzene 0.24 1.000 --- Ti --- U --- U 1.37 --- U 21. 1,2-Dichloroethane 0,02 0,200 --- U 0.11 .T --- U 0.06 J --- U 22. Trichloroethene 0.23 1,o00 --- U --- U --- U --- U --- U 23. 1,2-Dichloropropane 0.04 0.200 --- U 0.05 J --- U 0.04 J --- U 24. Bromodichlaromethane 0.04 0,200 --- U --- U --- V --- U --- V 25. Cis-1,3-Dichloropropene 0.06 0.200 --- U --- U --- V --- U --- U 26. 4-Methyl-2-Pentanone 1.19 100,000 --- U --- U --- U --- U --- U 27, Toluene 0.23 1.000 --- U "-^ U --- U --- U --- U 28. trans-2,3-Dichloropropene 0.04 0.200 --- U --- U --- U --- U --- U 29. 1,1,2-Trichloroethane 0.03 0.200 --- U --- V --- U --- U --- U 30. Tetrachloroethane 0.10 0.200 --- U --- U --- U --- U --- U 31. 2-Hexanone 1.57 50.000 --- V --- U --- U --- U --- U 32. Dibromochloromethane 0.03 0,200 --- U --- U --- U --- U "-- U 33. 1,2-Dibromoethane 0.03 0,200 --- U --- U »-- U --- U --- V 34. Chlorobenzene 0.30 3.000 --- U --- U --- U --- U --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.000 --- U --- U --- U --- U --- U 36. Ethylbenzene 0.21 1.000 --- U --- U --- U --- U --- U 37. Xylenes 0.60 5.000 --- U --- U --- U --- U --- U 38. Dibromomethane 0.28 10.000 --- U --- U --- U --- U --- U 39. Styrene 0.19 1.000 --- U --- V --- U --- U »"- U 40. Bromoform 0.20 3.000 --- U --- U --- U --- U --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- U --- U --- U --- U --- U 42, 1,2,3-Trichlorapropane 0.09 0.200 --- U --- U --- U --- U --' U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U --- U --- U --- U --- U 44. 1,2-Dichlorobenzene 0.32 5.000 --- U --- U --- U --- U _-- U 45. 1,2-Dibromo-3-chloropropane 0.07 0.200 --- U --- U --- U --- U --- U 46. Acrylonitrile 2.72 290.000 --- U --- U --- U --- U --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.000 --- U --- U --- U --- U --- 11 48. Acrolein 1.97 4.000 --- U --- U --- U --- U --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 REW'UnNUM % kgommUd Drinking Water ID! 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/08/20 Page: 2 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 MW-15 MN-16 MW-17 MW-14S MW-14D PARAMETERS, ug/l MDT, MRL 49, Ailyl Chloride 0.20 10.000 --- U --- U --- U --- U --- U 50. chloroprene 0.21 20,000 --- U --- V --- U --- U --- U 51, 1,3-Dichlorobenzene 0.41 5.000 --- U --- U --- U --- U "-- U 52. DiahlorodiPluoromethane 0.51 5.000 --- u --- U --- U --- U --- U 53, 1,3-Dichloropropane 0.28 1.000 --- U --- U --- U --- U 54. 2,2-Dichloropropane 0.17 15,000 --- U --- U --- U --- U --- U 55, 1,1-➢ichloropropene 0.22 5.000 --- U --^ U --- U --- V --- U 56. Ethyl Methacrylate 0.16 10.000 --- U --- U --- U --- U --- U 57. Hexachlorobutadiene 0.10 0.200 --- U --^ U --- U --- U --- U 58, I80butyl Alcohol 12.80 100.000 --- U --- U --- U --- U --- U 59. Methacrylonitrile 1.93 100.000 --- U --- V --- U --- U --- U 60. Methyl Methacrylate 0.25 30.000 --- U --- U --- U --- U --- U 61. Naphthalene 0.47 6.000 --- U --- U -"" U --- ❑ u 62. Propionitrile 3.26 150.000 --- U --- U '-- U --- U --- U $3. 1,2,4-Trichlorobenzene 0.50 10.000 --- U U U --- U --- U 64, Acetonitrile 36.29 55.000 --- U U --- U --- V --- U 65. Tetrahydroeuran 0.39 1.000 --- U --- U --- U 18.30 --- U 66. 1,4-Dioxane 2.71 3.000 --- U --- U --- U 9.63 --- U .7 = Estimated value between the MDL and MRL, V = Below ALL 4uantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 E T0000� % �fi(jr:6rn)QPoTM%o Drinking Water IDs 37715 Waatewa"r ID i 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR, JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/20 Page: 3 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 REVIEWED BY; ✓/�J LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PARAMETERS, ug/l MDL MRL Trip Blank 1. Chloromethane 0.77 3.000 --- U 2. Vinyl Chloride 0.12 0.200 --- U 3. Bromomethane 0.67 10.000 --- U 4. Chloroethane 0.40 10.000 --- U 5. Trichlorofluoromethane 0.24 1.000 --- U 6. 1,1-Dichloroethene 0.17 5.000 --- U 7. Acetone 9.06 100.000 --- U S. Iodomethane 0.26 10.000 --- U 9. Carbon Disulfide 0.23 100.000 --- U 10, Methylene Chloride 0.64 1.000 --- U 11. trana-1,2-Dichloroethene 0.23 5.000 --- U 12. 1,1-Dichloroethane 0.20 5.000 --- U 13. Vinyl Acetate 0.20 50.000 --- U 14, Cie-1,2-Dichloroethene 0.25 5.000 --- U 15. 2-Butanone 2.21 100.000 --- U 16. bromochloromethane 0.27 3.000 --- U 17, Chloroform 0.25 5.000 --- U 10. 1,1,1-Trichlarcethane 0.19 1.000 --- U 19. Carbon Tetrachloride 0.04 0.200 --- U 20. benzene 0.24 1.000 --- U 21, 1,2-Dichloroethane 0.02 0.200 --- U 22. Trichloroethene 0.23 1.000 --- U 23, 1,2-Dichloropropane 0.04 0.200 --- U 24, Bromodichloromethane 0.04 0.200 --- U 25. Cie-1,3-Dichloropropene 0.06 0.200 --- U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U 27. Toluene 0.23 1.000 --- U 26, trans-1,3-Dichloropropene 0.04 0.200 --- U 29. 1,1,2-Trichloroethana 0.03 0.200 --- V 30, Tetrachloroethene 0.10 0,200 --- U 31. 2-Hexanone 1.57 50.000 --- U 32, Dibromochloromethane 0.03 0.200 --- U 33. 1,2-Dibromoethane 0.03 0.200 --- U 34, Chlorobenzene 0.30 3.000 --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1,000 --- U 36. Bthylbenzene U.21 1.000 --- U 37. %ylenes 0.69 5.000 --- U 36. Dibromomethane 0.20 10.000 --- U 39. Styrene 0,19 1.000 --- U 40. Bromoform 0.20 3,000 --- U 41. 1,1,2,2-Tetrachloroethane 0,03 0.200 --- U 42. 1,2,3-Trichloropropane 0.09 0.200 --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U 44, 1,2-Dichlorobenzene 0.32 5.000 --- U 45. 1,2-Dibromo-3-Chlaropropane 0.07 0.200 --- U 46. Acrylonitrile 2.72 200.000 --- U 47, trans-1,4-Dichloro-2-Butene 0,42 100.000 --- U 40. Acrolein 1.97 4.000 --- U J = Estimated value between the MDL and MRL, ❑ = Below ALL ouantitation Limits. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Drinking Water ID; 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 I REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/08/20 Page: 4 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 PARAMETERS, ug/1 MDL MRL Trip Blank 49. Allyl Chloride 0.20 10.000 --- U 50. Chloroprene 0.21 20.000 --- U 51. 1,3-Dichlorobenzene 0.41 5.000 --- U 52, Dichloredifluoromethane 0,51 5.000 --- U 53. 1,3-Dichloropropane 0.28 1.000 --- U 54, 2,2-Dichloropropane 0.17 15,000 --- U 55, 1,1-1)ichloropropene 0.22 5.000 --- U 56. Ethyl Methacrylate 0.16 1D.000 --- U 57. Hexachlorobutadiene 0.10 0.200 --- U 59. Isobutyl Alcohol 12.80 100.000 --^ U 59. Methacrylonitrile 1.93 100.000 --- U 60. Methyl Methacrylate 0.25 30.000 --- U 61, Naphthalene 0.47 6.000 --- U 62. Propionitrile 3.26 150.000 --- U 63. 1,2,4-Trichlorobenzene 0.50 10,000 --- U 64. Acetonitrile 36.29 55.000 --- U 65, Tetrahydrofuran 0.39 1.000 --- U 66. 1,4-Dicxane 2.71 3.000 --- U J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits. h m t/ 4 DocuSI( IT m 6 O c cn m o a , 0 0 cn o -C3 0 CD N cl). Sr.cn m -a [D � m v 10 w CD In tnve10pe IU: 3J bS),Jt)btOA-/U.St-4r-UZ-y4AZ5-"11)4yyUbb-ittS"1 N C7 1 p ; rn Z Z M Z 'C+ CCCyyy I"•t• i pWp 0CD 0 m M' M X rro y N x o Z G Q Gi L7 G� a *H tv N O ya � n rp n y i4 N Ln Fn 9'N 0 O i ?a w o w m m .: m O W Cr{ CN J � z w v'1 � y m m m TOTAL CHLORINE, mg/1 G m m OR ug/I AT COLLECTION 06 0 [[ o C n o TEMPERATURE,°C < v VP D ATCOUCTION y in _ - p OF CONTAINERS Field pH Nitrate -Nitrite n "b ti"� ::G•}:Li:: Alkalinity y� V E Chloride Cyanide tv 'd V TDS m m m ..{ Sulfate Metals b C '`` ....: 'fir. Sulfide cn Conductivity ti DO > G Temperature Field Parameter a 8260 Dup. 2 e EPA 8270E G� 8 70E Dup.1 a G� n PARAMETERS/TESTS i o = _ g m Q� c M m a n z a J m m m yy �� 0 0 � c7 z rnn [ten o z `� w m (mr, m 0 vI S rC�i� Q 0 T 0 m m O M M n 17 b n C j 0 r �T> m a �� o o 0 M� rn Z n z = D m n a �' � E o m > O O � o z n z Docu& 0 Cn v w 6 v�. cu w -0 C ro Cn c o ro CD a 10 W t,U C� W n c0 gn r_nveiope iu: miootst5H-1 ia4"uiob i Lts i N ( 0 +v m 65 m z m z H Cn a '� r o Q YY Q h+ N n Z p m f=il m L ,Li. �1 91 to 03 .6 zz 'n in in O z f] ON n a G7 G� G� Jr C N O � C7 rl H t+C n c') + + CD u m m o r Uj m J JI .1 � m m , m TOTAL CHLORINE, mg/l U L l7 �J �,;;� m m OR ug/I AT COLLECTION v� Q mD m 0 < x -� �1 TEMPERATURE, °C w M d � ATCOLLECTION p 0 0 a o 00 0 # OF CONTAINERS EPA 8081B 0 8081H Duplicate Y G� #: 8260D App. II G] ?:::>: 8260D App. II 2 G� . _ _ 8260D App. II 3% 4� 8260D App.114 z m m m .. 8151A Landfill G� 8151A Duplicate G] O:nS OIZI' "G l J n .. 6 a = PARAMETERS/TESTS in n CD m c� as a n n m C7 �n 2 z r m 7z m m C�' n' CCn —i O a��o r X N2 O O m � m m m r1 f n �IN m 2 CD mCG z Cnn �j Cn z T Cr, m " m rn m Z f- �/1' W m C/7 (./3 '� n Z N S Z G7 C a n 3 � o � o z _ > t m r m A z 0 p � C d W < > � z m o 0 = O z DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 u 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. CLIENT ID: MR, JUDSON WHITEHURST 602 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED DATE ANALYZED: DATE REPORTED: REVIEWEb BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 D JP 12/08/20 12/17/20 05/24/21 PARAMETERS, ug/1 MDL MRL Concentration 1. Chloromethane 0,77 3.00 --- U 2. vinyl Chloride 0.12 0.20 U 3. Bromomethane 0.67 10.00 --- U 4. Chloroethane 0.48 10.00 --- U 5. Trichlorofluoromethane 0.24 1.00 --- U 6. 1,1-Dichloroethene 0.17 5.00 --- U 7. Acetone 9.06 100.00 --- U 8. Iodomethane 0.26 10.00 --- U 9. Carbon Disulfide 0.23 100.00 --- U 10. Methylene Chloride 0.64 1.00-- U 11. trans-1,2-Dichloroethene 0.23 5.00 --- U 12. 1,1-Dichloroethane 0.20 5.00 --- U 13. vinyl Acetate 0,20 1 50.00 --- U 14. cis-1,2-Dichloroethene 0,25 5.00 --- U 15. 2-Butanone 2.21 100.00 --- U 16. Bromochloromethane 0.27 3.00 --- U 17. Chloroform 0.25 5.00 - - U 18. 1,1,1-Trichloroethane 0.19 1.00 --- U 19. Carbon Tetrachloride 0.04 0.20 --- U 20, Benzene 0.24 1,00 --- U 21. 1,2-Dichloroethene 0.02 0.20 --- U 22. Trichloroethene 0.23 1.00 ---- U 23. 1,2-Dichloropropene 0.04 0.20 --- U 24. Bromodichloromethane 0.04 0.20 --- U 25. cis-1,3-Dichloropropene 0.06 0.20 --- U 26. 4-methyl-2-Pentanone 1.19 100.00 --- U 27. Toluene 0.23 1.00 --- U 28. trans-1,3-Dichloropropene 0.04 0.20 --- U 29, 1,1,2-Triehloroethane 0.03 0.20 --- U 30. Tetrachloroethene 0.10 0.20 --- U 31. 2-Hexanone 1.57 40.00 -- U 32. Dibromochloromethane 0.03 0.20 --- U 33. 1,2--Dibromoethane 0.03 0.20 --- U 34. Chlorobenxene 0.30 3.00 --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.00 --- U 36. Ethylbenzene 0.21 1.00 --- U 37. Xylenes 0.68 5.00 --- U 38. Dibromomethane 0.28 10.00 --- U 39. Styrene 0.19 1.00 --- U 40. Bromoform 0.20 3.00 --- U 41. 1,1,2,2-Tetrachloroethane 0.03 0.20 --- U 42. 1,2,3-Trichloropropane 0.09 0.20 --- U 43, 1,4-Dichlorobenzene 0.39 1.00 --- U 44, 1,2-Dichlorobenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- U 46. Acrylonitrile 2.72 200.00 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.00 --- U 48. Acroiein 1 1.97 1 4.00 --- U 49. Allyl Chloride 1 0.20 1 10.00 --- U 50. Chloroprene 1 0.21 1 20.00 --- U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC. CLIENT ID: 6003 D MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/20 DATE ANALYZED: 12/17/20 \ DATE REPORTED: 05/24/21 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PARAMETERS, ug/1 MDL MRL Concentration 51. 1,3-Dichlorobenzene 0.41 5.00 --- U 52. Dichlorodi£luoromethane 0.51 5.00 --- U 53. 1,3-Dichloropropane 0.28 1.00 --- U 54. 2,2-Dichloropropane 0.17 15.00 --- U 55. 1,1-Dichloropropene 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 --- U 57. Hexachlorobutadiene 0.10 0.20 --- U 58. Isobutyl Alcohol 12.80 100.00 --- U 59. Methacrylonitrile 1.93 100.00 --- U 60. Methyl Methacrylate 0.25 30.00 --- U 61. Naphthalene 0.47 6.00 --- U 62. Propionitrile 3.26 150.00 --- U 63. 1,2,4-Trichlorobenzene 0.50 10.00 --- U 64. Acetonitrile 1 36.29 55.00 --- U 65. Tetrahydrofuran 0.39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 1 U DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 aRk1-16171®Fp®QM�@d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JP DATE COLLECTED: 12/08/20 DATE ANALYZED: 12/17/20 DATE REPORTED: 05/24/21 VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits ($ recovery) 1,2-DCA-d4 recovery) Toluene-d8 (96 recovery) 4-BFB ('k recovery) Continuing Calibration std. 70-130 104 93.6 97.5 Method Blank 70-130 102 101 104 MW-15 70-130 100 95.9 99.3 MW-16 70-130 99.8 94.6 98.4 MW-17 70-130 99.6 96.3 97.5 MW-14S 70-130 99.0 96.7 1 99.3 MW-141D 70-130 99.1 94.8 9B.7 Trip Blank 70-130 99.1 97.0 96.3 6003D MW-15 M.S. 70-130 99.7 97.1 100 6003D MW-15 M.S.D. 70-130 97.9 96.9 99.8 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. CLIENT ID: MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED DATE ANALYZED: DATE REPORTED: REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 D JP 12/08/20 12/17/20 05/24/21 Sample Spiked: (6003D) MW-15 Spike Amount Ug/1 Sample Result Ug/1 Spike Result Ug/1 Spike Recovery (70-13016) Spike Dup. Result Ug/l Spike Dup. Recovery (70-130%) MS/MSD RPD (20%) 1,1-Dichloroethene 20.0 --- U 23.12 116 21.83 109 5.7 Benzene 20.0 --- U 22.24 ill 20.59 103 7.7 Trichloroethene 20.0 --- U 22.13 ill 20.80 104 6.2 Toluene 20.0 --- U 22.39 112 20.56 103 8.5 Chlorobenzene 20.0 --- U 1 21.80 1 103 1 20.05 100 8.4 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount Ug/1 Spike Result Ug/1 Spike Recovery (70-130$) 1,1-Dichloroethene 20.00 19.41 97.1 Benzene 20.00 19.66 98.3 Trichloroethene 20.00 19.60 98.0 Toluene 20.00 19.40 97.0 Chlorobenzene 20.00 19.24 96.2 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 Appendix C Time vs. Concentration Graphs December 2020 Groundwater Monitoring Report EBB Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 This page intentionally left blank. DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 BE MW-3A Organochlorides -21 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 3 2.5 2 0 0 u 1 0.5 0 Jul-09 Nov-10 Apr-12 Aug-1 tTetrachloroethene (CAS 127-18-4) BE MW-3S Organochlorides 3 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 t Trichloroethene(CA579-01-6) +1,2-Dichloroethane tcis-1,2-Dichloroethene --*--Vinyl chloride DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 1.6 1.4 1.2 1 0 u 0.6 0.4 0.2 0 f Jul-09 Nov-10 BE MW-8 Organochlorides Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 tTetrachloroethene (CAS 127-18-4) tTrichloroethene(CAS 79-01-6) t 1,2-Dichloroethane cis-1,2-Dichloroethene Vinyl chloride DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1EB1 EJE MW-10 Organochlorides Oct-21 DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EJE MW-11 Organochlorides 0.8 0.7 0.6 0.5 c 0 0 +� 0.4 w 0 0.3 u 0.2 0.1 01 • • • • • • • • 6 • i 6 • • • r • r 0 it • Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 t Tetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) t 1,2-Dichloroethane +cis-1,2-Dichloroethene +Vinyl chloride DocuSign Envelope ID: 8935BE5A-7D3E-4FC2-94A8-19499C6B1 EB1 EJE MW-12S Organochlorides 9 — 8 — 7 — 6 — c — 6 — c 0 w 4 — u 3 • / \ 2 0 Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 t Tetrachloroethene(CAS 127-18-4) tTrichloroethene(CAS 79-01-6) t1,2-Dichloroethane tcis-1,2-Dichloroethene +Vinyl chloride