22042_Matheson AVE_Final Grade Sampling Rpt_Compliance Letter_20231012

October 13, 2023 Sent Via Email Mr. Dan Fitzpatrick
BP NODA, LLC and BP Trail, LLC 3328 Peachtree Rd, NE, Suite 100 Atlanta, GA 30032 [e-mail] Subject: Final Grade Sampling Compliance Review Matheson Ave Brownfields Properties Charlotte, Mecklenburg County Brownfields Project Number: 22042-18-060 and 23015-19-060 Dear Mr. Fitzpatrick: The North Carolina Department of Environmental Quality (DEQ) Brownfields Redevelopment Section received and reviewed the Final Grade Sampling Report (Report) dated October 6, 2023, for Matheson Ave II (22042-18-060) and Matheson Ave Creek (23015-19-060) (collectively, Matheson Ave) Brownfields Properties. This report was submitted on your behalf by Mr. Eric Wysong of Apex Engineering, LLC (Apex) and includes the edits from the previous version dated June 8, 2022. DEQ understands the
redevelopment on the Matheson Ave Brownfields Properties was done jointly under the DEQ-approved Environmental Management Plan (EMP) dated November 26, 2019. DEQ Brownfields has reviewed the Report and evaluated the analytical data using the DEQ Risk Calculator. The results of this evaluation for soil were below the DEQ thresholds for residential use. DEQ Brownfields has found this Report to be in compliance with the EMP. Please be advised that this compliance review from DEQ Brownfields does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have any questions, please contact me at (704) 661-10330, or via e-mail at [e-mail].
Sincerely, Carolyn Minnich Project Manager ec: Brownfields Property Management Unit Eric Wysong [e-mail] Stephen A. McCullers [e-mail]

Apex Companies, LLC  5900-O Northwoods Business Parkway  Charlotte, NC 28269  T 704.799.6390  F 704.799.6395  apexcos.com
October 6, 2023
Ms. Carolyn Minnich Brownfields Project Manager North Carolina Department of Environmental Quality
Division of Waste Management 217 West Jones Street Raleigh, North Carolina 27699
Re: Final Grade Sampling Report Matheson Ave II and Matheson Ave Creek Brownfields Projects Chick Godley Road and 255 Matheson Avenue Brownfields Project No. 22042-18-060 and 23015-19-060 Dear Ms. Minnich: On behalf of BP NODA, LLC and BP Trail, LLC, Apex Companies, LLC (Apex) is pleased to submit the results of the Final Grade Sampling for the Matheson Ave II and Matheson Ave
Creek properties (Brownfields Project Numbers 22042-18-060 and 23015-19-060) located in Charlotte, Mecklenburg County, North Carolina. This report has been updated from the initial report submitted on June 8, 2022, to address comments received from the North Carolina
Department of Environmental Quality. Site redevelopment activities performed under the approved Environmental Management Plan
(EMP) signed November 27, 2019 have been completed. This Final Grade Sampling Report documents the final requirement of the redevelopment under this EMP as well as Land Use Restriction 15.k in the recorded Notice of Brownfield Property.
It has been a pleasure working with you on this project; thank you for your continued support. Please do not hesitate to call if you have any questions or require additional information.
Sincerely, Apex Companies, LLC
Eric Wysong, LG Project Manager

Attachment:
Brownfields Final Grade Sampling Report October 6, 2023 Matheson Ave II and Matheson Ave Creek Sites Page i

TABLE OF CONTENTS Section Page
1.0 INTRODUCTION ............................................................................................................... 1
2.0 SOIL SAMPLING ACTIVITIES ......................................................................................... 1
2.1 Utility Clearance .................................................................................................... 2
2.2 Soil Sampling ........................................................................................................ 2
2.2 Analytical Results .................................................................................................. 3
2.3 Risk Calculation ..................................................................................................... 6
3.0 DISCUSSION .................................................................................................................... 6
4.0 CONCLUSIONS ................................................................................................................ 7
FIGURES Figure 1 Site Location Map Figure 2 Site Development Features Figure 3 Final Grade Sample Location Map TABLES Table 1 Summary of VOC Soil Analytical Detections Table 2 Summary of SVOC and Metals Analytical Detections
APPENDICES Appendix A Laboratory Analytical Reports Appendix B NCDEQ Risk Calculator Output Sheet
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 1

1.0 INTRODUCTION
Maryland Apex Engineering, PC (Apex), a North Carolina licensed business entity of Apex
Companies, LLC, has prepared this Brownfields Final Grade Sampling Report for the
development associated with the Matheson Ave II and Matheson Avenue Creek Brownfield sites
(Brownfields Project No. 22042-18-060 and 23015-19-060) located at 2710 Chick Godley Road
and 255 Matheson Avenue in Charlotte, North Carolina (the “site”) (Figure 1). This report
documents sampling activities conducted during the completion of construction activities. All soil
sampling activities were conducted in general accordance with the Final Grade Sampling Work
Plan dated May 20, 2022 (Work Plan), which was approved by the North Carolina Department of
Environmental Quality (NCDEQ) in a letter dated May 20, 2022. Methods stated in the Work Plan
are in accordance with the NCDEQ approved Environmental Management Plan (EMP) prepared
for the site by Apex, dated November 27, 2019. This work was performed on behalf of the
Brownfields Prospective Developers (PD), BP NODA, LLC and BP Trail, LLC.
The site totals approximately 14.44 acres and contains three multi-story, high density residential
structures, a leasing and amenity center, a pool, and a pool cabana. The remainder of the site
consists of landscape features and paved drive lanes and parking areas. The central portion of
the site, primarily comprised of the Matheson Ave Creek Brownfields project, remains
undeveloped and contains a fenced barrier blocking access and separating it from the
residentially developed portions of the site. The redevelopment activities have been conducted in
accordance with the approved NCDEQ Notice of Brownfields Properties for two properties,
Brownfields Project Numbers 22042-18-060 and 23015-19-060, recorded February 4, 2019 and
July 12, 2019, respectively, and the approved EMP. See attached Figure 2 describing general
site development features.
2.0 SOIL SAMPLING ACTIVITIES
On May 26, 2022, Apex conducted soil sampling activities in accordance with the NCDEQ
approved Work Plan. The methodology and results are summarized in the following sections.
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 2

2.1 Utility Clearance
Prior to conducting onsite sampling activities, Apex contacted North Carolina 811 to mark
subsurface utilities on the Site. Apex also coordinated with the site contractors to verify that all
underground utilities were properly identified near the proposed boring locations.
2.2 Soil Sampling
On May 26, 2022, Apex advanced shallow soil borings in areas on the Brownfields site not
covered by building foundations, sidewalks, and driveways for collection of final grade soil
samples. The soil borings were advanced to a depth of zero to two feet below ground surface
from five designated composite sample areas (areas A through E) on the Brownfields site (see
Figure 3). Each area included five soil borings per composite sample area (e.g., A-1 through A-5)
for a total of twenty-five soil borings on the Brownfields site (see Figure 3). The Work Plan
indicated soil boring locations would be recorded with a handheld GPS. Due to interference from
onsite structure and powerlines, accuracy from the handheld GPS was low and the borings were
more accurately located based on their position relative to onsite developed features such as
landscaped islands, developed buildings, walkways, and roadways. Due to the abundance of
developed features, soil borings were able to be accurately placed in the locations proposed in
the work plan without any conflicts.
The shallow soil borings were advanced using a decontaminated hand auger and the soil from
the borings was field screened for the presence of odor, staining, and elevated volatile organic
compound (VOC) readings using a hand-held photoionization detector (PID). Grab samples were
collected from zero to one foot below ground surface (bgs) and one foot to two feet bgs at each
soil boring location. The material was observed to consist primarily of silty red clay, with significant
amounts of gravel. No distinctive odors of an environmental concern were noted, such as
petroleum or solvent odors, and no staining was observed.
The highest PID detection was recorded at D-4 from the depth interval of one to two feet bgs at a
concentration of 6.0 parts per million (ppm). A VOC sample was collected from this interval for
laboratory analysis. The remainder of the PID readings ranged from non-detect to 0.2 ppm. Due
to insignificant PID readings, the VOC samples collected in composite areas A, B, C, and E were
selected from the boring closest to the center of each individual area at a depth between one and
two feet bgs in accordance with the Work Plan. After collection, the samples were labeled and
placed in a laboratory-supplied cooler with ice. The samples were then hand delivered to Pace
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 3

Analytical in Huntersville, North Carolina under standard chain-of-custody protocol for analysis of
VOCs by EPA Method 8260D, preparation Method 5035.
After the selected VOC soil sample from each of the areas was collected and prepared, the ten
grab soil samples from each area were combined into one composite soil sample per composite
area using a decontaminated stainless-steel bowl and spoon. The five composite soil samples
were placed in laboratory-supplied sample containers, labeled, and placed in a laboratory
supplied cooler with ice. The samples were then hand delivered to Pace Analytical in Huntersville,
North Carolina under standard chain-of-custody protocol for analysis of semi-volatile organic
compounds (SVOCs) by EPA Method 8270E, metals (arsenic, barium, cadmium, total chromium,
lead, manganese, selenium, and silver) by EPA Method 6010D, and mercury by EPA Method
7471B. Splits of the composite soil samples were handled in accordance with the aforementioned
handling and chain-of-custody procedures, but delivered via FedEx overnight shipping to Eurofins
Lancaster Laboratories Environment Testing, LLC in Lancaster, Pennsylvania for analysis of
hexavalent chromium by EPA Method 7199.
As an added quality control measure, one duplicate soil sample (DUP-1) was collected from the
D composite area and analyzed for the same parameters as the parent sample. Additionally, one
equipment blank (EB-1) was created by pouring deionized water over the decontaminated auger
bucket and submitted for analysis of each method for which the soil was sampled. Finally, one
trip blank was prepared by the laboratory, included with the sample bottle shipment, and
accompanied the samples throughout the entire process. The trip blank was submitted for
analysis of total VOCs by USEPA method 8260.
2.2 Analytical Results
The soil sample results were compared to the January 2022 NCDEQ Preliminary Soil
Remediation Goals for Residential Health-Based Direct Contact (Residential PSRGs). The
analytical detections are shown in the attached Table 1 and Table 2, and summarized as follows:
VOCs
Laboratory analytical detections of VOCs are summarized as follows:
• Naphthalene, toluene, and 1,2,4-trimethylbenzene were detected in the sample collected
from A-3 (1-2)’ at concentrations below Residential PSRGs. No other VOCs were detected
in A-3 (1-2)’.
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 4

• P-isopropyltoluene, naphthalene, toluene, 1,2,4-trimethylbenzene, m&p-xylenes, o-
xylenes, and total xylenes were detected in the sample collected from B-3 (1-2)’ at
concentrations below Residential PSRGs. No other VOCs were detected in B-3 (1-2)’.
• No VOCs were detected in the sample collected from C-3 (1-2)’.
• Ethylbenzene, p-isopropyltoluene, toluene, and styrene were detected in the sample
collected from D-4 (1-2)’ at concentrations below Residential PSRGs. No other VOCs
were detected in D-4 (1-2)’.
• Tetrachloroethene and toluene were detected in the sample collected from E-3 (1-2)’ at
concentrations below Residential PSRGs. No other VOCs were detected in E-3 (1-2)’.
• Ethylbenzene, p-isopropyltoluene, and styrene were detected in the duplicate sample
(DUP-1) collected from D-4 (1-2)’ at concentrations below Residential PSRGs. No other
VOCs were detected in DUP-1.
SVOCs
Laboratory analytical detections of SVOCs are summarized as follows:
• No SVOCs were detected in the area A-, C-, D-, or E-Composite samples.
• Anthracene, benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(g,h,i)perylene, benzo(k)fluoranthene, chrysene, fluoranthene, indeno(1,2,3-
cd)pyrene, phenanthrene, and pyrene were detected in the sample collected from the
B-Composite area. All detected concentrations were below Residential PSRGs except for
benzo(a)pyrene detected at an estimated concentration of 0.327 milligrams per kilogram
(mg/kg), which exceeds its applicable Residential PSRG of 0.11 mg/kg. The
benzo(a)pyrene result is considered estimated because it is a J-flagged result, which is
below the laboratory reporting limit but above the laboratory method detection limit. No
other SVOCs were detected in the B-Composite sample.
• Benzo(a)anthracene, benzo(b)fluoranthene, chrysene, fluoranthene, phenanthrene, and
pyrene were detected in the duplicate sample (DUP-1) collected from the D-Composite
area. All of the detected concentrations were below Residential PSRGs and detected at
J-flagged concentrations, which are regarded as estimated concentrations. No other
SVOCs were detected in DUP-1.
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 5

Metals
Laboratory analytical results did not identify detectable concentrations of arsenic, cadmium,
selenium, or silver in any of the five composite samples or the duplicate sample. Several metals
were detected in each of the samples, summarized as follows:
• Barium concentrations ranged from 71.9 mg/kg in the DUP-1 sample collected from D-
Composite to 157 mg/kg in the sample collected from C-Composite. All detected
concentrations of barium were below the Residential PSRG;
• Chromium III concentrations ranged from 22 mg/kg in the sample collected from C-
Composite to 52.5 mg/kg in the sample collected from D-Composite. All detected
concentrations of barium were below the Residential PSRG;
• Hexavalent chromium concentrations ranged from 0.517 mg/kg in the sample collected
from the B-Composite to 2.78 mg/kg in the sample collected from the C-Composite. All
Hexavalent chromium concentrations exceeded the Residential PSRG;
• Lead concentrations ranged from 11.1 mg/kg in the sample collected from E-Composite
to 33.9 mg/kg in the sample collected from D-Composite. All detected concentrations of
lead were below the Residential PSRG;
• Manganese concentrations ranged from 373 mg/kg in the sample collected from C-
Composite to 1,030 mg/kg in the sample collected from D-Composite. The detected
concentrations of manganese exceeded the Residential PSRG in the A, B, D, and E-
Composite samples and DUP-1, but were below the Residential PSRG in the C-
Composite sample;
• Mercury concentrations ranged from non-detect in the C- and E-Composite samples, to
an estimated J-flag concentration of 0.044 mg/kg in the B-Composite sample. All detected
concentrations of mercury were below the Residential PSRG;
Quality Assurance / Quality Control (QA/QC)
Laboratory analytical detections of QA/QC samples are summarized as follows:
• No VOCs or SVOCs were detected in the equipment blank sample (EB-1).
• Arsenic was detected in EB-1 at an estimated J-flag concentration of 3.0 µg/L; no other
metals were detected in the EB-1 sample. The low arsenic concentration in EB1 is not a
significant concern due to the low concentration detected and the lack of detected
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 6

concentrations of arsenic in any of the soil samples collected during the final grade
sampling event.
• Methylene chloride was detected in the Trip Blank sample at an estimated J-flagged
concentration of 0.002 micrograms per liter (µg/L). The result was also flagged by the
laboratory as being confirmed by a second analysis and as a possible laboratory
contaminant; it was reportedly not detected in the method blank. Methylene chloride was
not detected in any of the samples collected at the site, including the equipment blank,
and is therefore considered to be a laboratory contaminant and not an environmental
concern related to the site. No other VOCs were detected in the Trip Blank.

The soil sampling locations are depicted on Figure 3 and the complete laboratory analytical
reports are included as Appendix A.
2.3 Risk Calculation
The analytical results were further evaluated using the NCDEQ Risk Calculator (January 2022
version) to evaluate the risk associated with the remaining soil on the site. The risk calculator
was used to evaluate the carcinogenic and non-carcinogenic risks for residential direct contact by
entering the highest concentrations of each VOC, SVOC, and metal detected in the May 2022
final grade sampling event into the calculator. The results of the risk calculator indicate the
following:
• Residential direct contact with soil:
o Cumulative carcinogenic risk of 1.3 x 10-5
o Cumulative hazard index of 5.9 x 10-1
The output sheet from the NCDEQ Risk Calculator is included as Appendix B.
3.0 DISCUSSION
The site has been developed with minimal areas that have not been covered with pavement or
building footprints. Final grade sampling was conducted in areas of potential soil exposure, which
are limited to landscaping and manicured lawn around the buildings, along the site perimeter,
adjacent to walkways, and in a small dog park. Several VOCs, SVOCs, and metals were detected
in the final grade soil samples, which were evaluated using the NCDEQ Risk Calculator based on
the highest concentrations of each detected analyte. The results of the risk calculations indicate
Brownfields Final Grade Sampling Report June 8, 2022 Matheson Ave II and Matheson Ave Creek Sites Page 7

a site wide cumulative carcinogenic risk of 1.3 x 10-5 and a cumulative hazard index of 5.9 x 10-1,
which are below the NCDEQ acceptable threshold for cumulative carcinogenic risk of 1.0 x 10-4
and the acceptable threshold for cumulative non-carcinogenic hazard of 1.0.
Although site wide cumulative carcinogenic risk and cumulative hazard index does not exceed
applicable NCDEQ thresholds for residential use, the site wide cumulative hazard for construction
worker is 4.8, which exceeds the applicable NCDEQ threshold of 1.0. This exceedance is driven
by concentrations of manganese in soil, which are generally within the range of manganese
naturally found in soils of this region. Based on these results, construction workers exposed to
soil at the site should exercise caution to minimize contact and potential inhalation or ingestion of
soil. The construction worker pathway is calculated in the NCDEQ Risk Calculator using default
assumptions that are conservative and may not be appropriate in all circumstances. As such,
proper exposure protections must be considered on a case-by-case basis dependent upon the
location and type of work being performed. The risk of construction worker exposure at the site
is mitigated by the recorded land use restrictions, which prohibit activity that disturbs soil on the
site without prior written approval from NCDEQ, with the exception of landscaping activities
restricted to depths not exceeding 24 inches.
4.0 CONCLUSIONS
Apex has completed final grade sampling activities at the Matheson Ave II and Matheson Avenue
Creek Brownfield sites (Brownfields Project No. 22042-18-060 and 23015-19-060) located at
2710 Chick Godley Road and 255 Matheson Avenue in Charlotte, North Carolina. Based on the
results of the risk calculations, the cumulative carcinogenic and non-carcinogenic risk were
determined to be below the limits for direct contact soil exposure in a residential scenario. Most
of the site is covered with paved areas and buildings. There are no playgrounds or significant
recreational fields and potential soil exposure is limited to minimal grassy areas along the site
perimeter, around buildings, adjacent to roads and pathways, and in a small dog park.
Undeveloped portions of the site are located along the Little Sugar Creek corridor, which is
separated from the developed portions of the site by a continuous fence. Based on the results of
final grade sampling at the site, the soil at the site presents no unacceptable risk for the proposed
residential site use and no further investigation is warranted.

FIGURES
USGS The National Map: National Boundaries Dataset, 3D Elevation Program,
Geographic Names Information System, National Hydrography Dataset,
National Land Cover Database, National Structures Dataset, and National
Transportation Dataset; U.S. Census Bureau - TIGER/Line
CHECK BY: EW
DRAWN BY: SP
DATE: 11/30/17
SCALE: AS SHOWN
CAD NO.: 510
PRJ NO.: 510
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SITE LOCATION
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N Project No. 510621-001E:\Apex\Phase 1 Figures\Client\BP Noda\Figure 2 - BP NODA - Overview.mxd Modified 3/31/2022 by Cole.Wilkinson NAD 1983 StatePlane North Carolina FIPS 3200 Feet Coordinate System LEGEND:&AAREA A&AAREA B&AAREA C&AAREA D&AAREA ENHD STREAMPAVED PARKING AND DRIVELANESBUILDING OUTLINES050100 1 " = 100 'FIGURE 2SITE DEVELOPMENT FEATURESService Layer Credits:City of Charlotte, INSERT AERIAL DATE/QUADRANGLE NAME, ETC.Matheson Ave II and Matheson Ave Creek2710 Chick Godley Roadand 255 Matheson AvenueCharlotte, North Carolina 28206A-1 = Composite Area Location and Sample NumberApex Companies, LLC10610 Metromont Pkwy., Suite 206Charlotte, North Carolina 28269Phone: [phone]www.apexcos.comNorth Carolina5900 Northwoods Business Pkwy,Ste 5900-OCharlotte, NC 28269Fence around residential developed area restricting access to Matheson Ave Creek side of projectPaved trail/greenwayNarrow strip of landscaping (about 36 inches wide) between concrete paved path and paved drive lanes planted with ornamental grasses separated by sections of lawn grassPaved parking extends to barrier fence with thin strip between parking and fence planted with row of arborvitaeFence around residential developed area restricting access to Matheson Ave Creek side of projectStructural retaining wallsStructural retaining wallsLandscaping with row of arborvitae
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TABLES
TABLE 1
Summary of VOC Analytical Detections
Final Grade Sampling - June 2022
Brownfields Project Numbers 22042-18-060 23015-19-060
255 Matheson Avenue
Charlotte, North Carolina
A-3 (1-2)'B-3(1-2)'C-3 (1-2)'D-4 (1-2)'DUP-1
(D-4 (1-2)')E-3 (1-2)'
Ethylbenzene <0.0066 <0.0067 <0.0071 0.0147 0.0311 <0.007 6.1
P-Isopropyltoluene <0.0066 0.0049J <0.0071 0.117 0.157 <0.007 NE
Naphthalene 0.0144 0.0328 <0.0071 <0.0082 <0.0079 <0.007 2.1
Tetrachloroethene <0.0066 <0.0067 <0.0071 <0.0082 <0.0079 0.0193 17
Toluene 0.0061J 0.0171 <0.0071 0.0055J <0.0079 0.0038J 990
1,2,4-Trimethylbenzene 0.0039J 0.0106 <0.0071 <0.0082 <0.0079 <0.007 63
Styrene <0.0066 <0.0067 <0.0071 0.0797 0.231 <0.007 1,200
m&p-Xylene <0.0133 0.0236 <0.0141 <0.0165 <0.0159 <0.0141 120
o-Xylene <0.0066 0.0133 <0.0071 <0.0082 <0.0079 <0.007 140
Xylene (Total)<0.0133 0.0370 <0.0141 <0.0165 <0.0159 <0.0141 120
Notes:
mg/kg = milligrams per kilogram
NCDEQ = North Carolina Department of Environmental Quality
PSRG = Preliminary Soil Remediation Goals
IHSB Standards = Inactive Hazardous Sites Branch PSRG for residential health (January 2022)
VOCs = Volatile Organic Compounds
NE = PSRG not established
< = Result below laboratory method detection limit
J = Result is below laboratory reporting limit but above laboratory detection limit; considered to be an estimated concentration
DUP = Blind field soil duplicate (collected from D-4 (1-2)')
IHSB Residential
PSRG StandardsAnalyte
VOCs by USEPA Method 8260 (mg/kg)
SAMPLE ANALYTICAL RESULTS
TABLE 2
Summary of SVOC and Metals Analytical Detections
Final Grade Sampling - June 2022
Brownfields Project Numbers 22042-18-060 23015-19-060
255 Matheson Avenue
Charlotte, North Carolina
A-Composite B-Composite C-Composite D-Composite DUP-1
(D-Composite)E-Composite
Anthracene <1.960 0.233J <0.411 <0.473 <0.417 <0.388 3,600
Benzo(a)anthracene <1.960 0.440 <0.411 <0.473 0.139J <0.388 1.1
Benzo(a)pyrene <1.960 0.327J <0.411 <0.473 <0.417 <0.388 0.11
Benzo(b)fluoranthene <1.960 0.429 <0.411 <0.473 0.163J <0.388 1.1
Benzo(g,h,i)perylene <1.960 0.194J <0.411 <0.473 <0.417 <0.388 NE
Benzo(k)fluroanthene <1.960 0.210J <0.411 <0.473 <0.417 <0.388 11
Chrysene <1.960 0.482 <0.411 <0.473 0.171J <0.388 110
Fluoranthene <1.960 0.858 <0.411 <0.473 0.268J <0.388 480
Indeno(1,2,3-cd)pyrene <1.960 0.176J <0.411 <0.473 <0.417 <0.388 1.1
Phenanthrene <1.960 0.715 <0.411 <0.473 0.195J <0.388 NE
Pyrene <1.960 0.654 <0.411 <0.473 0.219J <0.388 360
Barium 115 121 157 124 71.9 112 3,100
Chromium (III)46.5 37.1 22.0 52.5 39.5 39.4 23,000
Chromium (VI)0.528 0.517 2.78 0.820 0.924 0.528J 0.31
Lead 22.5 27.2 16.4 33.9 18.6 11.1 400
Manganese 701 575 373 1,030 530 627 380
Mercury 0.018J 0.044J <0.30 0.032J 0.025J <0.26 4.7
Notes:
mg/kg = milligrams per kilogram
NCDEQ = North Carolina Department of Environmental Quality
PSRG = Preliminary Soil Remediation Goals
IHSB Standards = Inactive Hazardous Sites Branch PSRG for residential health (January 2022)
SVOCs = Semi-Volatile Organic Compounds
Bold/Underlined concentrations exceed the Residential PSRG
NE = PSRG not established
< = Result below laboratory method detection limit
J = Result is below laboratory reporting limit but above laboratory detection limit; considered to be an estimated concentration
DUP-1 = Blind field soil duplicate (collected from D-Composite)
Analyte
SAMPLE ANALYTICAL RESULTS
SVOCs by USEPA Method 8270 (mg/kg)
Metals by USEPA Method 6010/7471/7199 (mg/kg)
IHSB Residential
PSRG Standards

APPENDIX A Laboratory Analytical Report
#=CL#
June 07, 2022
LIMS USE: FR - ERIC WYSONG
LIMS OBJECT ID: 92606758
92606758
Project:
Pace Project No.:
RE:
Eric Wysong
Apex Companies
5900-O Northwoods Business
Parkway
Charlotte, NC 28269
510621-001
Dear Eric Wysong:
Enclosed are the analytical results for sample(s) received by the laboratory on May 27, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 78
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92606758
510621-001
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 78
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92606758
510621-001
Lab ID Sample ID Matrix Date Collected Date Received
92606758001 A-3 (1-2)'Solid 05/26/22 18:45 05/27/22 09:05
92606758002 B-3 (1-2)'Solid 05/26/22 17:00 05/27/22 09:05
92606758003 C-3 (1-2)'Solid 05/26/22 14:50 05/27/22 09:05
92606758004 D-4 (1-2)'Solid 05/26/22 10:10 05/27/22 09:05
92606758005 E-3 (1-2)'Solid 05/26/22 13:05 05/27/22 09:05
92606758006 A-COMPOSITE Solid 05/26/22 18:50 05/27/22 09:05
92606758007 B-COMPOSITE Solid 05/26/22 17:10 05/27/22 09:05
92606758008 C-COMPOSITE Solid 05/26/22 14:55 05/27/22 09:05
92606758009 D-COMPOSITE Solid 05/26/22 10:15 05/27/22 09:05
92606758010 E-COMPOSITE Solid 05/26/22 13:15 05/27/22 09:05
92606758011 DUP-1 Solid 05/26/22 00:00 05/27/22 09:05
92606758012 EB-1 Water 05/26/22 18:55 05/27/22 09:05
92606758013 TRIP BLANK Water 05/26/22 00:00 05/27/22 09:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 78
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92606758
510621-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92606758001 A-3 (1-2)'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758002 B-3 (1-2)'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758003 C-3 (1-2)'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758004 D-4 (1-2)'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758005 E-3 (1-2)'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758006 A-COMPOSITE EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92606758007 B-COMPOSITE EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92606758008 C-COMPOSITE EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92606758009 D-COMPOSITE EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92606758010 E-COMPOSITE EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92606758011 DUP-1 EPA 6010D 8 PASI-GADRB
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92606758012 EB-1 EPA 6020B 8 PASI-GACW1
EPA 7470A 1 PASI-GAVB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 78
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92606758
510621-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92606758013 TRIP BLANK EPA 8260D 63 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: A-3 (1-2)'Lab ID: 92606758001 Collected: 05/26/22 18:45 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 02:22 67-64-105/27/22 15:53133 42.6 1
Benzene ND ug/kg 06/01/22 02:22 71-43-2 M105/27/22 15:536.6 2.6 1
Bromobenzene ND ug/kg 06/01/22 02:22 108-86-1 M105/27/22 15:536.6 2.2 1
Bromochloromethane ND ug/kg 06/01/22 02:22 74-97-5 M105/27/22 15:536.6 2.0 1
Bromodichloromethane ND ug/kg 06/01/22 02:22 75-27-4 M105/27/22 15:536.6 2.6 1
Bromoform ND ug/kg 06/01/22 02:22 75-25-2 M105/27/22 15:536.6 2.3 1
Bromomethane ND ug/kg 06/01/22 02:22 74-83-905/27/22 15:5313.3 10.5 1
2-Butanone (MEK)ND ug/kg 06/01/22 02:22 78-93-305/27/22 15:53133 31.8 1
n-Butylbenzene ND ug/kg 06/01/22 02:22 104-51-8 M105/27/22 15:536.6 3.1 1
sec-Butylbenzene ND ug/kg 06/01/22 02:22 135-98-8 M105/27/22 15:536.6 2.9 1
tert-Butylbenzene ND ug/kg 06/01/22 02:22 98-06-6 M105/27/22 15:536.6 2.4 1
Carbon tetrachloride ND ug/kg 06/01/22 02:22 56-23-505/27/22 15:536.6 2.5 1
Chlorobenzene ND ug/kg 06/01/22 02:22 108-90-7 M105/27/22 15:536.6 1.3 1
Chloroethane ND ug/kg 06/01/22 02:22 75-00-305/27/22 15:5313.3 5.1 1
Chloroform ND ug/kg 06/01/22 02:22 67-66-3 M105/27/22 15:536.6 4.0 1
Chloromethane ND ug/kg 06/01/22 02:22 74-87-305/27/22 15:5313.3 5.6 1
2-Chlorotoluene ND ug/kg 06/01/22 02:22 95-49-8 M105/27/22 15:536.6 2.3 1
4-Chlorotoluene ND ug/kg 06/01/22 02:22 106-43-4 M105/27/22 15:536.6 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 02:22 96-12-805/27/22 15:536.6 2.6 1
Dibromochloromethane ND ug/kg 06/01/22 02:22 124-48-1 M105/27/22 15:536.6 3.7 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 02:22 106-93-4 M105/27/22 15:536.6 2.9 1
Dibromomethane ND ug/kg 06/01/22 02:22 74-95-3 M105/27/22 15:536.6 1.4 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 02:22 95-50-1 M105/27/22 15:536.6 2.4 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 02:22 541-73-1 M105/27/22 15:536.6 2.1 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 02:22 106-46-7 M105/27/22 15:536.6 1.7 1
Dichlorodifluoromethane ND ug/kg 06/01/22 02:22 75-71-8 v105/27/22 15:5313.3 2.9 1
1,1-Dichloroethane ND ug/kg 06/01/22 02:22 75-34-3 M105/27/22 15:536.6 2.7 1
1,2-Dichloroethane ND ug/kg 06/01/22 02:22 107-06-2 M105/27/22 15:536.6 4.4 1
1,1-Dichloroethene ND ug/kg 06/01/22 02:22 75-35-405/27/22 15:536.6 2.7 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 02:22 156-59-2 M105/27/22 15:536.6 2.3 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 02:22 156-60-5 M105/27/22 15:536.6 2.3 1
1,2-Dichloropropane ND ug/kg 06/01/22 02:22 78-87-5 M105/27/22 15:536.6 2.0 1
1,3-Dichloropropane ND ug/kg 06/01/22 02:22 142-28-9 M105/27/22 15:536.6 2.1 1
2,2-Dichloropropane ND ug/kg 06/01/22 02:22 594-20-705/27/22 15:536.6 2.2 1
1,1-Dichloropropene ND ug/kg 06/01/22 02:22 563-58-6 M105/27/22 15:536.6 3.2 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 02:22 10061-01-5 M105/27/22 15:536.6 1.8 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 02:22 10061-02-6 M105/27/22 15:536.6 2.3 1
Diisopropyl ether ND ug/kg 06/01/22 02:22 108-20-3 M105/27/22 15:536.6 1.8 1
Ethylbenzene ND ug/kg 06/01/22 02:22 100-41-4 M105/27/22 15:536.6 3.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 02:22 87-68-305/27/22 15:5313.3 10.8 1
2-Hexanone ND ug/kg 06/01/22 02:22 591-78-605/27/22 15:5366.3 6.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 02:22 98-82-8 M105/27/22 15:536.6 2.3 1
p-Isopropyltoluene ND ug/kg 06/01/22 02:22 99-87-605/27/22 15:536.6 3.3 1
Methylene Chloride ND ug/kg 06/01/22 02:22 75-09-2 M105/27/22 15:5326.5 18.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: A-3 (1-2)'Lab ID: 92606758001 Collected: 05/26/22 18:45 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 02:22 108-10-105/27/22 15:5366.3 6.4 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 02:22 1634-04-4 M105/27/22 15:536.6 2.5 1
Naphthalene 14.4 ug/kg 06/01/22 02:22 91-20-305/27/22 15:536.6 3.5 1
n-Propylbenzene ND ug/kg 06/01/22 02:22 103-65-1 M105/27/22 15:536.6 2.4 1
Styrene ND ug/kg 06/01/22 02:22 100-42-5 M105/27/22 15:536.6 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 02:22 630-20-6 M105/27/22 15:536.6 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 02:22 79-34-5 M105/27/22 15:536.6 1.8 1
Tetrachloroethene ND ug/kg 06/01/22 02:22 127-18-4 M105/27/22 15:536.6 2.1 1
Toluene 6.1J ug/kg 06/01/22 02:22 108-88-3 M105/27/22 15:536.6 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 02:22 87-61-605/27/22 15:536.6 5.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 02:22 120-82-105/27/22 15:536.6 5.6 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 02:22 71-55-6 M105/27/22 15:536.6 3.4 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 02:22 79-00-5 M105/27/22 15:536.6 2.2 1
Trichloroethene ND ug/kg 06/01/22 02:22 79-01-6 M105/27/22 15:536.6 1.7 1
Trichlorofluoromethane ND ug/kg 06/01/22 02:22 75-69-405/27/22 15:536.6 3.6 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 02:22 96-18-4 M105/27/22 15:536.6 3.4 1
1,2,4-Trimethylbenzene 3.9J ug/kg 06/01/22 02:22 95-63-6 M105/27/22 15:536.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 02:22 108-67-8 M105/27/22 15:536.6 2.2 1
Vinyl acetate ND ug/kg 06/01/22 02:22 108-05-4 M105/27/22 15:5366.3 4.8 1
Vinyl chloride ND ug/kg 06/01/22 02:22 75-01-405/27/22 15:5313.3 3.4 1
Xylene (Total)ND ug/kg 06/01/22 02:22 1330-20-7 MS05/27/22 15:5313.3 3.8 1
m&p-Xylene ND ug/kg 06/01/22 02:22 179601-23-105/27/22 15:5313.3 4.5 1
o-Xylene ND ug/kg 06/01/22 02:22 95-47-6 M105/27/22 15:536.6 2.9 1
Surrogates
Toluene-d8 (S)100 %06/01/22 02:22 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)102 %06/01/22 02:22 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)104 %06/01/22 02:22 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.7 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: B-3 (1-2)'Lab ID: 92606758002 Collected: 05/26/22 17:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 02:40 67-64-105/27/22 15:53134 43.1 1
Benzene ND ug/kg 06/01/22 02:40 71-43-205/27/22 15:536.7 2.7 1
Bromobenzene ND ug/kg 06/01/22 02:40 108-86-105/27/22 15:536.7 2.2 1
Bromochloromethane ND ug/kg 06/01/22 02:40 74-97-505/27/22 15:536.7 2.0 1
Bromodichloromethane ND ug/kg 06/01/22 02:40 75-27-405/27/22 15:536.7 2.6 1
Bromoform ND ug/kg 06/01/22 02:40 75-25-205/27/22 15:536.7 2.4 1
Bromomethane ND ug/kg 06/01/22 02:40 74-83-905/27/22 15:5313.4 10.6 1
2-Butanone (MEK)ND ug/kg 06/01/22 02:40 78-93-305/27/22 15:53134 32.2 1
n-Butylbenzene ND ug/kg 06/01/22 02:40 104-51-805/27/22 15:536.7 3.2 1
sec-Butylbenzene ND ug/kg 06/01/22 02:40 135-98-805/27/22 15:536.7 3.0 1
tert-Butylbenzene ND ug/kg 06/01/22 02:40 98-06-605/27/22 15:536.7 2.4 1
Carbon tetrachloride ND ug/kg 06/01/22 02:40 56-23-505/27/22 15:536.7 2.5 1
Chlorobenzene ND ug/kg 06/01/22 02:40 108-90-705/27/22 15:536.7 1.3 1
Chloroethane ND ug/kg 06/01/22 02:40 75-00-305/27/22 15:5313.4 5.2 1
Chloroform ND ug/kg 06/01/22 02:40 67-66-305/27/22 15:536.7 4.1 1
Chloromethane ND ug/kg 06/01/22 02:40 74-87-305/27/22 15:5313.4 5.6 1
2-Chlorotoluene ND ug/kg 06/01/22 02:40 95-49-805/27/22 15:536.7 2.4 1
4-Chlorotoluene ND ug/kg 06/01/22 02:40 106-43-405/27/22 15:536.7 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 02:40 96-12-805/27/22 15:536.7 2.6 1
Dibromochloromethane ND ug/kg 06/01/22 02:40 124-48-105/27/22 15:536.7 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 02:40 106-93-405/27/22 15:536.7 3.0 1
Dibromomethane ND ug/kg 06/01/22 02:40 74-95-305/27/22 15:536.7 1.4 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 02:40 95-50-105/27/22 15:536.7 2.4 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 02:40 541-73-105/27/22 15:536.7 2.1 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 02:40 106-46-705/27/22 15:536.7 1.7 1
Dichlorodifluoromethane ND ug/kg 06/01/22 02:40 75-71-8 v105/27/22 15:5313.4 2.9 1
1,1-Dichloroethane ND ug/kg 06/01/22 02:40 75-34-305/27/22 15:536.7 2.8 1
1,2-Dichloroethane ND ug/kg 06/01/22 02:40 107-06-205/27/22 15:536.7 4.4 1
1,1-Dichloroethene ND ug/kg 06/01/22 02:40 75-35-405/27/22 15:536.7 2.8 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 02:40 156-59-205/27/22 15:536.7 2.3 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 02:40 156-60-505/27/22 15:536.7 2.4 1
1,2-Dichloropropane ND ug/kg 06/01/22 02:40 78-87-505/27/22 15:536.7 2.0 1
1,3-Dichloropropane ND ug/kg 06/01/22 02:40 142-28-905/27/22 15:536.7 2.1 1
2,2-Dichloropropane ND ug/kg 06/01/22 02:40 594-20-705/27/22 15:536.7 2.2 1
1,1-Dichloropropene ND ug/kg 06/01/22 02:40 563-58-605/27/22 15:536.7 3.2 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 02:40 10061-01-505/27/22 15:536.7 1.8 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 02:40 10061-02-605/27/22 15:536.7 2.3 1
Diisopropyl ether ND ug/kg 06/01/22 02:40 108-20-305/27/22 15:536.7 1.8 1
Ethylbenzene ND ug/kg 06/01/22 02:40 100-41-405/27/22 15:536.7 3.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 02:40 87-68-305/27/22 15:5313.4 11.0 1
2-Hexanone ND ug/kg 06/01/22 02:40 591-78-605/27/22 15:5367.2 6.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 02:40 98-82-805/27/22 15:536.7 2.3 1
p-Isopropyltoluene 4.9J ug/kg 06/01/22 02:40 99-87-605/27/22 15:536.7 3.3 1
Methylene Chloride ND ug/kg 06/01/22 02:40 75-09-205/27/22 15:5326.9 18.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: B-3 (1-2)'Lab ID: 92606758002 Collected: 05/26/22 17:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 02:40 108-10-105/27/22 15:5367.2 6.5 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 02:40 1634-04-405/27/22 15:536.7 2.5 1
Naphthalene 32.8 ug/kg 06/01/22 02:40 91-20-305/27/22 15:536.7 3.5 1
n-Propylbenzene ND ug/kg 06/01/22 02:40 103-65-105/27/22 15:536.7 2.4 1
Styrene ND ug/kg 06/01/22 02:40 100-42-505/27/22 15:536.7 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 02:40 630-20-605/27/22 15:536.7 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 02:40 79-34-505/27/22 15:536.7 1.8 1
Tetrachloroethene ND ug/kg 06/01/22 02:40 127-18-405/27/22 15:536.7 2.1 1
Toluene 17.1 ug/kg 06/01/22 02:40 108-88-305/27/22 15:536.7 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 02:40 87-61-605/27/22 15:536.7 5.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 02:40 120-82-105/27/22 15:536.7 5.6 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 02:40 71-55-605/27/22 15:536.7 3.5 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 02:40 79-00-505/27/22 15:536.7 2.2 1
Trichloroethene ND ug/kg 06/01/22 02:40 79-01-605/27/22 15:536.7 1.7 1
Trichlorofluoromethane ND ug/kg 06/01/22 02:40 75-69-405/27/22 15:536.7 3.7 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 02:40 96-18-405/27/22 15:536.7 3.4 1
1,2,4-Trimethylbenzene 10.6 ug/kg 06/01/22 02:40 95-63-605/27/22 15:536.7 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 02:40 108-67-805/27/22 15:536.7 2.3 1
Vinyl acetate ND ug/kg 06/01/22 02:40 108-05-405/27/22 15:5367.2 4.9 1
Vinyl chloride ND ug/kg 06/01/22 02:40 75-01-405/27/22 15:5313.4 3.4 1
Xylene (Total)37.0 ug/kg 06/01/22 02:40 1330-20-705/27/22 15:5313.4 3.8 1
m&p-Xylene 23.6 ug/kg 06/01/22 02:40 179601-23-105/27/22 15:5313.4 4.6 1
o-Xylene 13.3 ug/kg 06/01/22 02:40 95-47-605/27/22 15:536.7 3.0 1
Surrogates
Toluene-d8 (S)102 %06/01/22 02:40 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)102 %06/01/22 02:40 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)105 %06/01/22 02:40 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.4 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: C-3 (1-2)'Lab ID: 92606758003 Collected: 05/26/22 14:50 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 03:18 67-64-105/27/22 15:53141 45.3 1
Benzene ND ug/kg 06/01/22 03:18 71-43-205/27/22 15:537.1 2.8 1
Bromobenzene ND ug/kg 06/01/22 03:18 108-86-105/27/22 15:537.1 2.3 1
Bromochloromethane ND ug/kg 06/01/22 03:18 74-97-505/27/22 15:537.1 2.1 1
Bromodichloromethane ND ug/kg 06/01/22 03:18 75-27-405/27/22 15:537.1 2.7 1
Bromoform ND ug/kg 06/01/22 03:18 75-25-205/27/22 15:537.1 2.5 1
Bromomethane ND ug/kg 06/01/22 03:18 74-83-905/27/22 15:5314.1 11.2 1
2-Butanone (MEK)ND ug/kg 06/01/22 03:18 78-93-305/27/22 15:53141 33.9 1
n-Butylbenzene ND ug/kg 06/01/22 03:18 104-51-805/27/22 15:537.1 3.3 1
sec-Butylbenzene ND ug/kg 06/01/22 03:18 135-98-805/27/22 15:537.1 3.1 1
tert-Butylbenzene ND ug/kg 06/01/22 03:18 98-06-605/27/22 15:537.1 2.5 1
Carbon tetrachloride ND ug/kg 06/01/22 03:18 56-23-505/27/22 15:537.1 2.6 1
Chlorobenzene ND ug/kg 06/01/22 03:18 108-90-705/27/22 15:537.1 1.4 1
Chloroethane ND ug/kg 06/01/22 03:18 75-00-305/27/22 15:5314.1 5.5 1
Chloroform ND ug/kg 06/01/22 03:18 67-66-305/27/22 15:537.1 4.3 1
Chloromethane ND ug/kg 06/01/22 03:18 74-87-305/27/22 15:5314.1 5.9 1
2-Chlorotoluene ND ug/kg 06/01/22 03:18 95-49-805/27/22 15:537.1 2.5 1
4-Chlorotoluene ND ug/kg 06/01/22 03:18 106-43-405/27/22 15:537.1 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 03:18 96-12-805/27/22 15:537.1 2.7 1
Dibromochloromethane ND ug/kg 06/01/22 03:18 124-48-105/27/22 15:537.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 03:18 106-93-405/27/22 15:537.1 3.1 1
Dibromomethane ND ug/kg 06/01/22 03:18 74-95-305/27/22 15:537.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 03:18 95-50-105/27/22 15:537.1 2.5 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 03:18 541-73-105/27/22 15:537.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 03:18 106-46-705/27/22 15:537.1 1.8 1
Dichlorodifluoromethane ND ug/kg 06/01/22 03:18 75-71-8 v105/27/22 15:5314.1 3.1 1
1,1-Dichloroethane ND ug/kg 06/01/22 03:18 75-34-305/27/22 15:537.1 2.9 1
1,2-Dichloroethane ND ug/kg 06/01/22 03:18 107-06-205/27/22 15:537.1 4.7 1
1,1-Dichloroethene ND ug/kg 06/01/22 03:18 75-35-405/27/22 15:537.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 03:18 156-59-205/27/22 15:537.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 03:18 156-60-505/27/22 15:537.1 2.5 1
1,2-Dichloropropane ND ug/kg 06/01/22 03:18 78-87-505/27/22 15:537.1 2.1 1
1,3-Dichloropropane ND ug/kg 06/01/22 03:18 142-28-905/27/22 15:537.1 2.2 1
2,2-Dichloropropane ND ug/kg 06/01/22 03:18 594-20-705/27/22 15:537.1 2.3 1
1,1-Dichloropropene ND ug/kg 06/01/22 03:18 563-58-605/27/22 15:537.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 03:18 10061-01-505/27/22 15:537.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 03:18 10061-02-605/27/22 15:537.1 2.4 1
Diisopropyl ether ND ug/kg 06/01/22 03:18 108-20-305/27/22 15:537.1 1.9 1
Ethylbenzene ND ug/kg 06/01/22 03:18 100-41-405/27/22 15:537.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 03:18 87-68-305/27/22 15:5314.1 11.5 1
2-Hexanone ND ug/kg 06/01/22 03:18 591-78-605/27/22 15:5370.6 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 03:18 98-82-805/27/22 15:537.1 2.4 1
p-Isopropyltoluene ND ug/kg 06/01/22 03:18 99-87-605/27/22 15:537.1 3.5 1
Methylene Chloride ND ug/kg 06/01/22 03:18 75-09-205/27/22 15:5328.2 19.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: C-3 (1-2)'Lab ID: 92606758003 Collected: 05/26/22 14:50 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 03:18 108-10-105/27/22 15:5370.6 6.8 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 03:18 1634-04-405/27/22 15:537.1 2.6 1
Naphthalene ND ug/kg 06/01/22 03:18 91-20-305/27/22 15:537.1 3.7 1
n-Propylbenzene ND ug/kg 06/01/22 03:18 103-65-105/27/22 15:537.1 2.5 1
Styrene ND ug/kg 06/01/22 03:18 100-42-505/27/22 15:537.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 03:18 630-20-605/27/22 15:537.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 03:18 79-34-505/27/22 15:537.1 1.9 1
Tetrachloroethene ND ug/kg 06/01/22 03:18 127-18-405/27/22 15:537.1 2.2 1
Toluene ND ug/kg 06/01/22 03:18 108-88-305/27/22 15:537.1 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 03:18 87-61-605/27/22 15:537.1 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 03:18 120-82-105/27/22 15:537.1 5.9 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 03:18 71-55-605/27/22 15:537.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 03:18 79-00-505/27/22 15:537.1 2.3 1
Trichloroethene ND ug/kg 06/01/22 03:18 79-01-605/27/22 15:537.1 1.8 1
Trichlorofluoromethane ND ug/kg 06/01/22 03:18 75-69-405/27/22 15:537.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 03:18 96-18-405/27/22 15:537.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/01/22 03:18 95-63-605/27/22 15:537.1 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 03:18 108-67-805/27/22 15:537.1 2.4 1
Vinyl acetate ND ug/kg 06/01/22 03:18 108-05-405/27/22 15:5370.6 5.1 1
Vinyl chloride ND ug/kg 06/01/22 03:18 75-01-405/27/22 15:5314.1 3.6 1
Xylene (Total)ND ug/kg 06/01/22 03:18 1330-20-705/27/22 15:5314.1 4.0 1
m&p-Xylene ND ug/kg 06/01/22 03:18 179601-23-105/27/22 15:5314.1 4.8 1
o-Xylene ND ug/kg 06/01/22 03:18 95-47-605/27/22 15:537.1 3.1 1
Surrogates
Toluene-d8 (S)100 %06/01/22 03:18 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)101 %06/01/22 03:18 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)101 %06/01/22 03:18 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.7 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: D-4 (1-2)'Lab ID: 92606758004 Collected: 05/26/22 10:10 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 03:36 67-64-105/27/22 15:53165 53.0 1
Benzene ND ug/kg 06/01/22 03:36 71-43-205/27/22 15:538.2 3.3 1
Bromobenzene ND ug/kg 06/01/22 03:36 108-86-105/27/22 15:538.2 2.7 1
Bromochloromethane ND ug/kg 06/01/22 03:36 74-97-505/27/22 15:538.2 2.4 1
Bromodichloromethane ND ug/kg 06/01/22 03:36 75-27-405/27/22 15:538.2 3.2 1
Bromoform ND ug/kg 06/01/22 03:36 75-25-205/27/22 15:538.2 2.9 1
Bromomethane ND ug/kg 06/01/22 03:36 74-83-905/27/22 15:5316.5 13.0 1
2-Butanone (MEK)ND ug/kg 06/01/22 03:36 78-93-305/27/22 15:53165 39.6 1
n-Butylbenzene ND ug/kg 06/01/22 03:36 104-51-805/27/22 15:538.2 3.9 1
sec-Butylbenzene ND ug/kg 06/01/22 03:36 135-98-805/27/22 15:538.2 3.6 1
tert-Butylbenzene ND ug/kg 06/01/22 03:36 98-06-605/27/22 15:538.2 2.9 1
Carbon tetrachloride ND ug/kg 06/01/22 03:36 56-23-505/27/22 15:538.2 3.1 1
Chlorobenzene ND ug/kg 06/01/22 03:36 108-90-705/27/22 15:538.2 1.6 1
Chloroethane ND ug/kg 06/01/22 03:36 75-00-305/27/22 15:5316.5 6.4 1
Chloroform ND ug/kg 06/01/22 03:36 67-66-305/27/22 15:538.2 5.0 1
Chloromethane ND ug/kg 06/01/22 03:36 74-87-305/27/22 15:5316.5 6.9 1
2-Chlorotoluene ND ug/kg 06/01/22 03:36 95-49-805/27/22 15:538.2 2.9 1
4-Chlorotoluene ND ug/kg 06/01/22 03:36 106-43-405/27/22 15:538.2 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 03:36 96-12-805/27/22 15:538.2 3.2 1
Dibromochloromethane ND ug/kg 06/01/22 03:36 124-48-105/27/22 15:538.2 4.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 03:36 106-93-405/27/22 15:538.2 3.6 1
Dibromomethane ND ug/kg 06/01/22 03:36 74-95-305/27/22 15:538.2 1.8 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 03:36 95-50-105/27/22 15:538.2 3.0 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 03:36 541-73-105/27/22 15:538.2 2.6 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 03:36 106-46-705/27/22 15:538.2 2.1 1
Dichlorodifluoromethane ND ug/kg 06/01/22 03:36 75-71-8 v105/27/22 15:5316.5 3.6 1
1,1-Dichloroethane ND ug/kg 06/01/22 03:36 75-34-305/27/22 15:538.2 3.4 1
1,2-Dichloroethane ND ug/kg 06/01/22 03:36 107-06-205/27/22 15:538.2 5.5 1
1,1-Dichloroethene ND ug/kg 06/01/22 03:36 75-35-405/27/22 15:538.2 3.4 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 03:36 156-59-205/27/22 15:538.2 2.8 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 03:36 156-60-505/27/22 15:538.2 2.9 1
1,2-Dichloropropane ND ug/kg 06/01/22 03:36 78-87-505/27/22 15:538.2 2.5 1
1,3-Dichloropropane ND ug/kg 06/01/22 03:36 142-28-905/27/22 15:538.2 2.6 1
2,2-Dichloropropane ND ug/kg 06/01/22 03:36 594-20-705/27/22 15:538.2 2.7 1
1,1-Dichloropropene ND ug/kg 06/01/22 03:36 563-58-605/27/22 15:538.2 4.0 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 03:36 10061-01-505/27/22 15:538.2 2.2 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 03:36 10061-02-605/27/22 15:538.2 2.8 1
Diisopropyl ether ND ug/kg 06/01/22 03:36 108-20-305/27/22 15:538.2 2.2 1
Ethylbenzene 14.7 ug/kg 06/01/22 03:36 100-41-405/27/22 15:538.2 3.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 03:36 87-68-305/27/22 15:5316.5 13.5 1
2-Hexanone ND ug/kg 06/01/22 03:36 591-78-605/27/22 15:5382.5 8.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 03:36 98-82-805/27/22 15:538.2 2.8 1
p-Isopropyltoluene 117 ug/kg 06/01/22 03:36 99-87-605/27/22 15:538.2 4.1 1
Methylene Chloride ND ug/kg 06/01/22 03:36 75-09-205/27/22 15:5333.0 22.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: D-4 (1-2)'Lab ID: 92606758004 Collected: 05/26/22 10:10 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 03:36 108-10-105/27/22 15:5382.5 8.0 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 03:36 1634-04-405/27/22 15:538.2 3.1 1
Naphthalene ND ug/kg 06/01/22 03:36 91-20-305/27/22 15:538.2 4.3 1
n-Propylbenzene ND ug/kg 06/01/22 03:36 103-65-105/27/22 15:538.2 2.9 1
Styrene 79.7 ug/kg 06/01/22 03:36 100-42-505/27/22 15:538.2 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 03:36 630-20-605/27/22 15:538.2 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 03:36 79-34-505/27/22 15:538.2 2.2 1
Tetrachloroethene ND ug/kg 06/01/22 03:36 127-18-405/27/22 15:538.2 2.6 1
Toluene 5.5J ug/kg 06/01/22 03:36 108-88-305/27/22 15:538.2 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 03:36 87-61-605/27/22 15:538.2 6.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 03:36 120-82-105/27/22 15:538.2 6.9 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 03:36 71-55-605/27/22 15:538.2 4.3 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 03:36 79-00-505/27/22 15:538.2 2.7 1
Trichloroethene ND ug/kg 06/01/22 03:36 79-01-605/27/22 15:538.2 2.1 1
Trichlorofluoromethane ND ug/kg 06/01/22 03:36 75-69-405/27/22 15:538.2 4.5 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 03:36 96-18-405/27/22 15:538.2 4.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/01/22 03:36 95-63-605/27/22 15:538.2 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 03:36 108-67-805/27/22 15:538.2 2.8 1
Vinyl acetate ND ug/kg 06/01/22 03:36 108-05-405/27/22 15:5382.5 6.0 1
Vinyl chloride ND ug/kg 06/01/22 03:36 75-01-405/27/22 15:5316.5 4.2 1
Xylene (Total)ND ug/kg 06/01/22 03:36 1330-20-705/27/22 15:5316.5 4.7 1
m&p-Xylene ND ug/kg 06/01/22 03:36 179601-23-105/27/22 15:5316.5 5.6 1
o-Xylene ND ug/kg 06/01/22 03:36 95-47-605/27/22 15:538.2 3.6 1
Surrogates
Toluene-d8 (S)101 %06/01/22 03:36 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)101 %06/01/22 03:36 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)103 %06/01/22 03:36 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.5 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: E-3 (1-2)'Lab ID: 92606758005 Collected: 05/26/22 13:05 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 03:55 67-64-105/27/22 15:53141 45.2 1
Benzene ND ug/kg 06/01/22 03:55 71-43-205/27/22 15:537.0 2.8 1
Bromobenzene ND ug/kg 06/01/22 03:55 108-86-105/27/22 15:537.0 2.3 1
Bromochloromethane ND ug/kg 06/01/22 03:55 74-97-505/27/22 15:537.0 2.1 1
Bromodichloromethane ND ug/kg 06/01/22 03:55 75-27-405/27/22 15:537.0 2.7 1
Bromoform ND ug/kg 06/01/22 03:55 75-25-205/27/22 15:537.0 2.5 1
Bromomethane ND ug/kg 06/01/22 03:55 74-83-905/27/22 15:5314.1 11.1 1
2-Butanone (MEK)ND ug/kg 06/01/22 03:55 78-93-305/27/22 15:53141 33.8 1
n-Butylbenzene ND ug/kg 06/01/22 03:55 104-51-805/27/22 15:537.0 3.3 1
sec-Butylbenzene ND ug/kg 06/01/22 03:55 135-98-805/27/22 15:537.0 3.1 1
tert-Butylbenzene ND ug/kg 06/01/22 03:55 98-06-605/27/22 15:537.0 2.5 1
Carbon tetrachloride ND ug/kg 06/01/22 03:55 56-23-505/27/22 15:537.0 2.6 1
Chlorobenzene ND ug/kg 06/01/22 03:55 108-90-705/27/22 15:537.0 1.4 1
Chloroethane ND ug/kg 06/01/22 03:55 75-00-305/27/22 15:5314.1 5.4 1
Chloroform ND ug/kg 06/01/22 03:55 67-66-305/27/22 15:537.0 4.3 1
Chloromethane ND ug/kg 06/01/22 03:55 74-87-305/27/22 15:5314.1 5.9 1
2-Chlorotoluene ND ug/kg 06/01/22 03:55 95-49-805/27/22 15:537.0 2.5 1
4-Chlorotoluene ND ug/kg 06/01/22 03:55 106-43-405/27/22 15:537.0 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 03:55 96-12-805/27/22 15:537.0 2.7 1
Dibromochloromethane ND ug/kg 06/01/22 03:55 124-48-105/27/22 15:537.0 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 03:55 106-93-405/27/22 15:537.0 3.1 1
Dibromomethane ND ug/kg 06/01/22 03:55 74-95-305/27/22 15:537.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 03:55 95-50-105/27/22 15:537.0 2.5 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 03:55 541-73-105/27/22 15:537.0 2.2 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 03:55 106-46-705/27/22 15:537.0 1.8 1
Dichlorodifluoromethane ND ug/kg 06/01/22 03:55 75-71-8 v105/27/22 15:5314.1 3.1 1
1,1-Dichloroethane ND ug/kg 06/01/22 03:55 75-34-305/27/22 15:537.0 2.9 1
1,2-Dichloroethane ND ug/kg 06/01/22 03:55 107-06-205/27/22 15:537.0 4.7 1
1,1-Dichloroethene ND ug/kg 06/01/22 03:55 75-35-405/27/22 15:537.0 2.9 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 03:55 156-59-205/27/22 15:537.0 2.4 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 03:55 156-60-505/27/22 15:537.0 2.5 1
1,2-Dichloropropane ND ug/kg 06/01/22 03:55 78-87-505/27/22 15:537.0 2.1 1
1,3-Dichloropropane ND ug/kg 06/01/22 03:55 142-28-905/27/22 15:537.0 2.2 1
2,2-Dichloropropane ND ug/kg 06/01/22 03:55 594-20-705/27/22 15:537.0 2.3 1
1,1-Dichloropropene ND ug/kg 06/01/22 03:55 563-58-605/27/22 15:537.0 3.4 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 03:55 10061-01-505/27/22 15:537.0 1.9 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 03:55 10061-02-605/27/22 15:537.0 2.4 1
Diisopropyl ether ND ug/kg 06/01/22 03:55 108-20-305/27/22 15:537.0 1.9 1
Ethylbenzene ND ug/kg 06/01/22 03:55 100-41-405/27/22 15:537.0 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 03:55 87-68-305/27/22 15:5314.1 11.5 1
2-Hexanone ND ug/kg 06/01/22 03:55 591-78-605/27/22 15:5370.3 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 03:55 98-82-805/27/22 15:537.0 2.4 1
p-Isopropyltoluene ND ug/kg 06/01/22 03:55 99-87-605/27/22 15:537.0 3.5 1
Methylene Chloride ND ug/kg 06/01/22 03:55 75-09-205/27/22 15:5328.1 19.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: E-3 (1-2)'Lab ID: 92606758005 Collected: 05/26/22 13:05 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 03:55 108-10-105/27/22 15:5370.3 6.8 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 03:55 1634-04-405/27/22 15:537.0 2.6 1
Naphthalene ND ug/kg 06/01/22 03:55 91-20-305/27/22 15:537.0 3.7 1
n-Propylbenzene ND ug/kg 06/01/22 03:55 103-65-105/27/22 15:537.0 2.5 1
Styrene ND ug/kg 06/01/22 03:55 100-42-505/27/22 15:537.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 03:55 630-20-605/27/22 15:537.0 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 03:55 79-34-505/27/22 15:537.0 1.9 1
Tetrachloroethene 19.3 ug/kg 06/01/22 03:55 127-18-405/27/22 15:537.0 2.2 1
Toluene 3.8J ug/kg 06/01/22 03:55 108-88-305/27/22 15:537.0 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 03:55 87-61-605/27/22 15:537.0 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 03:55 120-82-105/27/22 15:537.0 5.9 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 03:55 71-55-605/27/22 15:537.0 3.7 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 03:55 79-00-505/27/22 15:537.0 2.3 1
Trichloroethene ND ug/kg 06/01/22 03:55 79-01-605/27/22 15:537.0 1.8 1
Trichlorofluoromethane ND ug/kg 06/01/22 03:55 75-69-405/27/22 15:537.0 3.9 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 03:55 96-18-405/27/22 15:537.0 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/01/22 03:55 95-63-605/27/22 15:537.0 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 03:55 108-67-805/27/22 15:537.0 2.4 1
Vinyl acetate ND ug/kg 06/01/22 03:55 108-05-405/27/22 15:5370.3 5.1 1
Vinyl chloride ND ug/kg 06/01/22 03:55 75-01-405/27/22 15:5314.1 3.6 1
Xylene (Total)ND ug/kg 06/01/22 03:55 1330-20-705/27/22 15:5314.1 4.0 1
m&p-Xylene ND ug/kg 06/01/22 03:55 179601-23-105/27/22 15:5314.1 4.8 1
o-Xylene ND ug/kg 06/01/22 03:55 95-47-605/27/22 15:537.0 3.1 1
Surrogates
Toluene-d8 (S)99 %06/01/22 03:55 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)100 %06/01/22 03:55 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)99 %06/01/22 03:55 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.8 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: A-COMPOSITE Lab ID: 92606758006 Collected: 05/26/22 18:50 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 16:46 7440-38-205/31/22 15:533.6 2.5 1
Barium 115 mg/kg 06/01/22 16:46 7440-39-305/31/22 15:531.2 0.49 1
Cadmium ND mg/kg 06/01/22 16:46 7440-43-905/31/22 15:531.2 0.35 1
Chromium 46.5 mg/kg 06/01/22 16:46 7440-47-305/31/22 15:531.2 1.1 1
Lead 22.5 mg/kg 06/01/22 16:46 7439-92-105/31/22 15:533.0 1.8 1
Manganese 701 mg/kg 06/01/22 16:46 7439-96-505/31/22 15:534.8 0.89 1
Selenium ND mg/kg 06/02/22 17:52 7782-49-2 D305/31/22 15:5329.7 25.7 5
Silver ND mg/kg 06/01/22 16:46 7440-22-405/31/22 15:531.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.018J mg/kg 06/01/22 08:52 7439-97-605/31/22 17:000.28 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 13:13 83-32-906/01/22 17:261960 688 5
Acenaphthylene ND ug/kg 06/02/22 13:13 208-96-806/01/22 17:261960 688 5
Aniline ND ug/kg 06/02/22 13:13 62-53-306/01/22 17:261960 765 5
Anthracene ND ug/kg 06/02/22 13:13 120-12-706/01/22 17:261960 640 5
Benzo(a)anthracene ND ug/kg 06/02/22 13:13 56-55-306/01/22 17:261960 652 5
Benzo(a)pyrene ND ug/kg 06/02/22 13:13 50-32-806/01/22 17:261960 676 5
Benzo(b)fluoranthene ND ug/kg 06/02/22 13:13 205-99-206/01/22 17:261960 652 5
Benzo(g,h,i)perylene ND ug/kg 06/02/22 13:13 191-24-206/01/22 17:261960 759 5
Benzo(k)fluoranthene ND ug/kg 06/02/22 13:13 207-08-906/01/22 17:261960 688 5
Benzoic Acid ND ug/kg 06/02/22 13:13 65-85-006/01/22 17:269780 4200 5
Benzyl alcohol ND ug/kg 06/02/22 13:13 100-51-606/01/22 17:263910 1480 5
4-Bromophenylphenyl ether ND ug/kg 06/02/22 13:13 101-55-306/01/22 17:261960 753 5
Butylbenzylphthalate ND ug/kg 06/02/22 13:13 85-68-706/01/22 17:261960 824 5
4-Chloro-3-methylphenol ND ug/kg 06/02/22 13:13 59-50-706/01/22 17:263910 1380 5
4-Chloroaniline ND ug/kg 06/02/22 13:13 106-47-8 IL06/01/22 17:263910 1540 5
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 13:13 111-91-106/01/22 17:261960 812 5
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 13:13 111-44-406/01/22 17:261960 735 5
2-Chloronaphthalene ND ug/kg 06/02/22 13:13 91-58-706/01/22 17:261960 777 5
2-Chlorophenol ND ug/kg 06/02/22 13:13 95-57-806/01/22 17:261960 735 5
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 13:13 7005-72-306/01/22 17:261960 729 5
Chrysene ND ug/kg 06/02/22 13:13 218-01-906/01/22 17:261960 712 5
Dibenz(a,h)anthracene ND ug/kg 06/02/22 13:13 53-70-306/01/22 17:261960 753 5
Dibenzofuran ND ug/kg 06/02/22 13:13 132-64-906/01/22 17:261960 706 5
1,2-Dichlorobenzene ND ug/kg 06/02/22 13:13 95-50-106/01/22 17:261960 706 5
1,3-Dichlorobenzene ND ug/kg 06/02/22 13:13 541-73-106/01/22 17:261960 694 5
1,4-Dichlorobenzene ND ug/kg 06/02/22 13:13 106-46-706/01/22 17:261960 747 5
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 13:13 91-94-1 IL06/01/22 17:263910 1320 5
2,4-Dichlorophenol ND ug/kg 06/02/22 13:13 120-83-206/01/22 17:261960 765 5
Diethylphthalate ND ug/kg 06/02/22 13:13 84-66-2 v106/01/22 17:261960 718 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: A-COMPOSITE Lab ID: 92606758006 Collected: 05/26/22 18:50 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 13:13 105-67-906/01/22 17:261960 812 5
Dimethylphthalate ND ug/kg 06/02/22 13:13 131-11-306/01/22 17:261960 712 5
Di-n-butylphthalate ND ug/kg 06/02/22 13:13 84-74-206/01/22 17:261960 658 5
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 13:13 534-52-106/01/22 17:263910 1830 5
2,4-Dinitrophenol ND ug/kg 06/02/22 13:13 51-28-506/01/22 17:269780 6050 5
2,4-Dinitrotoluene ND ug/kg 06/02/22 13:13 121-14-206/01/22 17:261960 753 5
2,6-Dinitrotoluene ND ug/kg 06/02/22 13:13 606-20-206/01/22 17:261960 718 5
Di-n-octylphthalate ND ug/kg 06/02/22 13:13 117-84-0 v106/01/22 17:261960 771 5
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 13:13 117-81-706/01/22 17:261960 759 5
Fluoranthene ND ug/kg 06/02/22 13:13 206-44-006/01/22 17:261960 670 5
Fluorene ND ug/kg 06/02/22 13:13 86-73-706/01/22 17:261960 688 5
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 13:13 87-68-306/01/22 17:261960 848 5
Hexachlorobenzene ND ug/kg 06/02/22 13:13 118-74-106/01/22 17:261960 765 5
Hexachlorocyclopentadiene ND ug/kg 06/02/22 13:13 77-47-4 v206/01/22 17:261960 1120 5
Hexachloroethane ND ug/kg 06/02/22 13:13 67-72-106/01/22 17:261960 747 5
Indeno(1,2,3-cd)pyrene ND ug/kg 06/02/22 13:13 193-39-506/01/22 17:261960 771 5
Isophorone ND ug/kg 06/02/22 13:13 78-59-106/01/22 17:261960 872 5
1-Methylnaphthalene ND ug/kg 06/02/22 13:13 90-12-006/01/22 17:261960 688 5
2-Methylnaphthalene ND ug/kg 06/02/22 13:13 91-57-606/01/22 17:261960 783 5
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 13:13 95-48-706/01/22 17:261960 801 5
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 13:13 15831-10-406/01/22 17:261960 789 5
Naphthalene ND ug/kg 06/02/22 13:13 91-20-306/01/22 17:261960 664 5
2-Nitroaniline ND ug/kg 06/02/22 13:13 88-74-406/01/22 17:269780 1600 5
3-Nitroaniline ND ug/kg 06/02/22 13:13 99-09-2 IL06/01/22 17:269780 1540 5
4-Nitroaniline ND ug/kg 06/02/22 13:13 100-01-606/01/22 17:263910 1490 5
Nitrobenzene ND ug/kg 06/02/22 13:13 98-95-306/01/22 17:261960 907 5
2-Nitrophenol ND ug/kg 06/02/22 13:13 88-75-5 v106/01/22 17:261960 848 5
4-Nitrophenol ND ug/kg 06/02/22 13:13 100-02-706/01/22 17:269780 3780 5
N-Nitrosodimethylamine ND ug/kg 06/02/22 13:13 62-75-906/01/22 17:261960 658 5
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 13:13 621-64-706/01/22 17:261960 735 5
N-Nitrosodiphenylamine ND ug/kg 06/02/22 13:13 86-30-606/01/22 17:261960 694 5
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 13:13 108-60-106/01/22 17:261960 931 5
Pentachlorophenol ND ug/kg 06/02/22 13:13 87-86-506/01/22 17:263910 1920 5
Phenanthrene ND ug/kg 06/02/22 13:13 85-01-806/01/22 17:261960 640 5
Phenol ND ug/kg 06/02/22 13:13 108-95-206/01/22 17:261960 872 5
Pyrene ND ug/kg 06/02/22 13:13 129-00-006/01/22 17:261960 795 5
Pyridine ND ug/kg 06/02/22 13:13 110-86-106/01/22 17:261960 617 5
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 13:13 120-82-106/01/22 17:261960 771 5
2,4,5-Trichlorophenol ND ug/kg 06/02/22 13:13 95-95-406/01/22 17:261960 895 5
2,4,6-Trichlorophenol ND ug/kg 06/02/22 13:13 88-06-206/01/22 17:261960 806 5
Surrogates
Nitrobenzene-d5 (S)73 %06/02/22 13:13 4165-60-006/01/22 17:2621-130 5
2-Fluorobiphenyl (S)75 %06/02/22 13:13 321-60-806/01/22 17:2619-130 5
Terphenyl-d14 (S)94 %06/02/22 13:13 1718-51-006/01/22 17:2615-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: A-COMPOSITE Lab ID: 92606758006 Collected: 05/26/22 18:50 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)79 %06/02/22 13:13 13127-88-306/01/22 17:2618-130 5
2-Fluorophenol (S)64 %06/02/22 13:13 367-12-406/01/22 17:2618-130 5
2,4,6-Tribromophenol (S)88 %06/02/22 13:13 118-79-606/01/22 17:2618-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.0 %05/27/22 17:57 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: B-COMPOSITE Lab ID: 92606758007 Collected: 05/26/22 17:10 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 16:51 7440-38-205/31/22 15:533.5 2.5 1
Barium 121 mg/kg 06/01/22 16:51 7440-39-305/31/22 15:531.2 0.48 1
Cadmium ND mg/kg 06/01/22 16:51 7440-43-905/31/22 15:531.2 0.34 1
Chromium 37.1 mg/kg 06/01/22 16:51 7440-47-305/31/22 15:531.2 1.1 1
Lead 27.2 mg/kg 06/01/22 16:51 7439-92-105/31/22 15:532.9 1.8 1
Manganese 575 mg/kg 06/01/22 16:51 7439-96-505/31/22 15:534.6 0.87 1
Selenium ND mg/kg 06/02/22 17:57 7782-49-2 D305/31/22 15:5329.0 25.1 5
Silver ND mg/kg 06/01/22 16:51 7440-22-405/31/22 15:531.2 0.48 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.044J mg/kg 06/01/22 08:55 7439-97-605/31/22 17:000.29 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 12:18 83-32-906/01/22 17:26420 148 1
Acenaphthylene ND ug/kg 06/02/22 12:18 208-96-806/01/22 17:26420 148 1
Aniline ND ug/kg 06/02/22 12:18 62-53-306/01/22 17:26420 164 1
Anthracene 233J ug/kg 06/02/22 12:18 120-12-706/01/22 17:26420 138 1
Benzo(a)anthracene 440 ug/kg 06/02/22 12:18 56-55-306/01/22 17:26420 140 1
Benzo(a)pyrene 327J ug/kg 06/02/22 12:18 50-32-806/01/22 17:26420 145 1
Benzo(b)fluoranthene 429 ug/kg 06/02/22 12:18 205-99-206/01/22 17:26420 140 1
Benzo(g,h,i)perylene 194J ug/kg 06/02/22 12:18 191-24-206/01/22 17:26420 163 1
Benzo(k)fluoranthene 210J ug/kg 06/02/22 12:18 207-08-906/01/22 17:26420 148 1
Benzoic Acid ND ug/kg 06/02/22 12:18 65-85-006/01/22 17:262100 903 1
Benzyl alcohol ND ug/kg 06/02/22 12:18 100-51-606/01/22 17:26840 318 1
4-Bromophenylphenyl ether ND ug/kg 06/02/22 12:18 101-55-306/01/22 17:26420 162 1
Butylbenzylphthalate ND ug/kg 06/02/22 12:18 85-68-706/01/22 17:26420 177 1
4-Chloro-3-methylphenol ND ug/kg 06/02/22 12:18 59-50-706/01/22 17:26840 295 1
4-Chloroaniline ND ug/kg 06/02/22 12:18 106-47-806/01/22 17:26840 330 1
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 12:18 111-91-106/01/22 17:26420 174 1
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 12:18 111-44-406/01/22 17:26420 158 1
2-Chloronaphthalene ND ug/kg 06/02/22 12:18 91-58-706/01/22 17:26420 167 1
2-Chlorophenol ND ug/kg 06/02/22 12:18 95-57-806/01/22 17:26420 158 1
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 12:18 7005-72-306/01/22 17:26420 157 1
Chrysene 482 ug/kg 06/02/22 12:18 218-01-906/01/22 17:26420 153 1
Dibenz(a,h)anthracene ND ug/kg 06/02/22 12:18 53-70-306/01/22 17:26420 162 1
Dibenzofuran ND ug/kg 06/02/22 12:18 132-64-906/01/22 17:26420 152 1
1,2-Dichlorobenzene ND ug/kg 06/02/22 12:18 95-50-106/01/22 17:26420 152 1
1,3-Dichlorobenzene ND ug/kg 06/02/22 12:18 541-73-106/01/22 17:26420 149 1
1,4-Dichlorobenzene ND ug/kg 06/02/22 12:18 106-46-706/01/22 17:26420 160 1
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 12:18 91-94-1 IL06/01/22 17:26840 284 1
2,4-Dichlorophenol ND ug/kg 06/02/22 12:18 120-83-206/01/22 17:26420 164 1
Diethylphthalate ND ug/kg 06/02/22 12:18 84-66-2 v106/01/22 17:26420 154 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: B-COMPOSITE Lab ID: 92606758007 Collected: 05/26/22 17:10 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 12:18 105-67-906/01/22 17:26420 174 1
Dimethylphthalate ND ug/kg 06/02/22 12:18 131-11-306/01/22 17:26420 153 1
Di-n-butylphthalate ND ug/kg 06/02/22 12:18 84-74-206/01/22 17:26420 141 1
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 12:18 534-52-106/01/22 17:26840 392 1
2,4-Dinitrophenol ND ug/kg 06/02/22 12:18 51-28-506/01/22 17:262100 1300 1
2,4-Dinitrotoluene ND ug/kg 06/02/22 12:18 121-14-206/01/22 17:26420 162 1
2,6-Dinitrotoluene ND ug/kg 06/02/22 12:18 606-20-206/01/22 17:26420 154 1
Di-n-octylphthalate ND ug/kg 06/02/22 12:18 117-84-006/01/22 17:26420 166 1
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 12:18 117-81-706/01/22 17:26420 163 1
Fluoranthene 858 ug/kg 06/02/22 12:18 206-44-006/01/22 17:26420 144 1
Fluorene ND ug/kg 06/02/22 12:18 86-73-706/01/22 17:26420 148 1
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 12:18 87-68-306/01/22 17:26420 182 1
Hexachlorobenzene ND ug/kg 06/02/22 12:18 118-74-106/01/22 17:26420 164 1
Hexachlorocyclopentadiene ND ug/kg 06/02/22 12:18 77-47-406/01/22 17:26420 241 1
Hexachloroethane ND ug/kg 06/02/22 12:18 67-72-106/01/22 17:26420 160 1
Indeno(1,2,3-cd)pyrene 176J ug/kg 06/02/22 12:18 193-39-506/01/22 17:26420 166 1
Isophorone ND ug/kg 06/02/22 12:18 78-59-106/01/22 17:26420 187 1
1-Methylnaphthalene ND ug/kg 06/02/22 12:18 90-12-006/01/22 17:26420 148 1
2-Methylnaphthalene ND ug/kg 06/02/22 12:18 91-57-606/01/22 17:26420 168 1
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 12:18 95-48-706/01/22 17:26420 172 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 12:18 15831-10-4 v206/01/22 17:26420 169 1
Naphthalene ND ug/kg 06/02/22 12:18 91-20-306/01/22 17:26420 143 1
2-Nitroaniline ND ug/kg 06/02/22 12:18 88-74-406/01/22 17:262100 344 1
3-Nitroaniline ND ug/kg 06/02/22 12:18 99-09-206/01/22 17:262100 330 1
4-Nitroaniline ND ug/kg 06/02/22 12:18 100-01-606/01/22 17:26840 320 1
Nitrobenzene ND ug/kg 06/02/22 12:18 98-95-306/01/22 17:26420 195 1
2-Nitrophenol ND ug/kg 06/02/22 12:18 88-75-506/01/22 17:26420 182 1
4-Nitrophenol ND ug/kg 06/02/22 12:18 100-02-706/01/22 17:262100 812 1
N-Nitrosodimethylamine ND ug/kg 06/02/22 12:18 62-75-906/01/22 17:26420 141 1
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 12:18 621-64-706/01/22 17:26420 158 1
N-Nitrosodiphenylamine ND ug/kg 06/02/22 12:18 86-30-606/01/22 17:26420 149 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 12:18 108-60-106/01/22 17:26420 200 1
Pentachlorophenol ND ug/kg 06/02/22 12:18 87-86-506/01/22 17:26840 411 1
Phenanthrene 715 ug/kg 06/02/22 12:18 85-01-806/01/22 17:26420 138 1
Phenol ND ug/kg 06/02/22 12:18 108-95-206/01/22 17:26420 187 1
Pyrene 654 ug/kg 06/02/22 12:18 129-00-006/01/22 17:26420 171 1
Pyridine ND ug/kg 06/02/22 12:18 110-86-106/01/22 17:26420 132 1
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 12:18 120-82-106/01/22 17:26420 166 1
2,4,5-Trichlorophenol ND ug/kg 06/02/22 12:18 95-95-406/01/22 17:26420 192 1
2,4,6-Trichlorophenol ND ug/kg 06/02/22 12:18 88-06-206/01/22 17:26420 173 1
Surrogates
Nitrobenzene-d5 (S)64 %06/02/22 12:18 4165-60-006/01/22 17:2621-130 1
2-Fluorobiphenyl (S)73 %06/02/22 12:18 321-60-806/01/22 17:2619-130 1
Terphenyl-d14 (S)77 %06/02/22 12:18 1718-51-006/01/22 17:2615-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: B-COMPOSITE Lab ID: 92606758007 Collected: 05/26/22 17:10 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)60 %06/02/22 12:18 13127-88-306/01/22 17:2618-130 1
2-Fluorophenol (S)54 %06/02/22 12:18 367-12-406/01/22 17:2618-130 1
2,4,6-Tribromophenol (S)79 %06/02/22 12:18 118-79-606/01/22 17:2618-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.7 %05/27/22 17:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: C-COMPOSITE Lab ID: 92606758008 Collected: 05/26/22 14:55 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 16:55 7440-38-205/31/22 15:533.6 2.5 1
Barium 157 mg/kg 06/01/22 16:55 7440-39-305/31/22 15:531.2 0.49 1
Cadmium ND mg/kg 06/01/22 16:55 7440-43-905/31/22 15:531.2 0.35 1
Chromium 22.0 mg/kg 06/01/22 16:55 7440-47-305/31/22 15:531.2 1.1 1
Lead 16.4 mg/kg 06/01/22 16:55 7439-92-105/31/22 15:533.0 1.9 1
Manganese 373 mg/kg 06/01/22 16:55 7439-96-505/31/22 15:534.8 0.89 1
Selenium ND mg/kg 06/02/22 18:01 7782-49-2 D305/31/22 15:5329.8 25.8 5
Silver ND mg/kg 06/01/22 16:55 7440-22-405/31/22 15:531.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/01/22 09:03 7439-97-605/31/22 17:000.30 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 12:46 83-32-906/01/22 17:26411 144 1
Acenaphthylene ND ug/kg 06/02/22 12:46 208-96-806/01/22 17:26411 144 1
Aniline ND ug/kg 06/02/22 12:46 62-53-306/01/22 17:26411 161 1
Anthracene ND ug/kg 06/02/22 12:46 120-12-706/01/22 17:26411 134 1
Benzo(a)anthracene ND ug/kg 06/02/22 12:46 56-55-306/01/22 17:26411 137 1
Benzo(a)pyrene ND ug/kg 06/02/22 12:46 50-32-806/01/22 17:26411 142 1
Benzo(b)fluoranthene ND ug/kg 06/02/22 12:46 205-99-206/01/22 17:26411 137 1
Benzo(g,h,i)perylene ND ug/kg 06/02/22 12:46 191-24-206/01/22 17:26411 159 1
Benzo(k)fluoranthene ND ug/kg 06/02/22 12:46 207-08-906/01/22 17:26411 144 1
Benzoic Acid ND ug/kg 06/02/22 12:46 65-85-006/01/22 17:262050 882 1
Benzyl alcohol ND ug/kg 06/02/22 12:46 100-51-606/01/22 17:26821 311 1
4-Bromophenylphenyl ether ND ug/kg 06/02/22 12:46 101-55-306/01/22 17:26411 158 1
Butylbenzylphthalate ND ug/kg 06/02/22 12:46 85-68-706/01/22 17:26411 173 1
4-Chloro-3-methylphenol ND ug/kg 06/02/22 12:46 59-50-706/01/22 17:26821 289 1
4-Chloroaniline ND ug/kg 06/02/22 12:46 106-47-806/01/22 17:26821 322 1
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 12:46 111-91-106/01/22 17:26411 170 1
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 12:46 111-44-406/01/22 17:26411 154 1
2-Chloronaphthalene ND ug/kg 06/02/22 12:46 91-58-706/01/22 17:26411 163 1
2-Chlorophenol ND ug/kg 06/02/22 12:46 95-57-806/01/22 17:26411 154 1
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 12:46 7005-72-306/01/22 17:26411 153 1
Chrysene ND ug/kg 06/02/22 12:46 218-01-906/01/22 17:26411 149 1
Dibenz(a,h)anthracene ND ug/kg 06/02/22 12:46 53-70-306/01/22 17:26411 158 1
Dibenzofuran ND ug/kg 06/02/22 12:46 132-64-906/01/22 17:26411 148 1
1,2-Dichlorobenzene ND ug/kg 06/02/22 12:46 95-50-106/01/22 17:26411 148 1
1,3-Dichlorobenzene ND ug/kg 06/02/22 12:46 541-73-106/01/22 17:26411 146 1
1,4-Dichlorobenzene ND ug/kg 06/02/22 12:46 106-46-706/01/22 17:26411 157 1
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 12:46 91-94-1 IL06/01/22 17:26821 277 1
2,4-Dichlorophenol ND ug/kg 06/02/22 12:46 120-83-206/01/22 17:26411 161 1
Diethylphthalate ND ug/kg 06/02/22 12:46 84-66-2 v106/01/22 17:26411 151 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: C-COMPOSITE Lab ID: 92606758008 Collected: 05/26/22 14:55 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 12:46 105-67-906/01/22 17:26411 170 1
Dimethylphthalate ND ug/kg 06/02/22 12:46 131-11-306/01/22 17:26411 149 1
Di-n-butylphthalate ND ug/kg 06/02/22 12:46 84-74-206/01/22 17:26411 138 1
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 12:46 534-52-106/01/22 17:26821 383 1
2,4-Dinitrophenol ND ug/kg 06/02/22 12:46 51-28-506/01/22 17:262050 1270 1
2,4-Dinitrotoluene ND ug/kg 06/02/22 12:46 121-14-206/01/22 17:26411 158 1
2,6-Dinitrotoluene ND ug/kg 06/02/22 12:46 606-20-206/01/22 17:26411 151 1
Di-n-octylphthalate ND ug/kg 06/02/22 12:46 117-84-006/01/22 17:26411 162 1
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 12:46 117-81-706/01/22 17:26411 159 1
Fluoranthene ND ug/kg 06/02/22 12:46 206-44-006/01/22 17:26411 141 1
Fluorene ND ug/kg 06/02/22 12:46 86-73-706/01/22 17:26411 144 1
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 12:46 87-68-306/01/22 17:26411 178 1
Hexachlorobenzene ND ug/kg 06/02/22 12:46 118-74-106/01/22 17:26411 161 1
Hexachlorocyclopentadiene ND ug/kg 06/02/22 12:46 77-47-406/01/22 17:26411 235 1
Hexachloroethane ND ug/kg 06/02/22 12:46 67-72-106/01/22 17:26411 157 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/02/22 12:46 193-39-506/01/22 17:26411 162 1
Isophorone ND ug/kg 06/02/22 12:46 78-59-106/01/22 17:26411 183 1
1-Methylnaphthalene ND ug/kg 06/02/22 12:46 90-12-006/01/22 17:26411 144 1
2-Methylnaphthalene ND ug/kg 06/02/22 12:46 91-57-606/01/22 17:26411 164 1
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 12:46 95-48-706/01/22 17:26411 168 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 12:46 15831-10-4 v206/01/22 17:26411 165 1
Naphthalene ND ug/kg 06/02/22 12:46 91-20-306/01/22 17:26411 139 1
2-Nitroaniline ND ug/kg 06/02/22 12:46 88-74-406/01/22 17:262050 336 1
3-Nitroaniline ND ug/kg 06/02/22 12:46 99-09-206/01/22 17:262050 322 1
4-Nitroaniline ND ug/kg 06/02/22 12:46 100-01-606/01/22 17:26821 312 1
Nitrobenzene ND ug/kg 06/02/22 12:46 98-95-306/01/22 17:26411 190 1
2-Nitrophenol ND ug/kg 06/02/22 12:46 88-75-506/01/22 17:26411 178 1
4-Nitrophenol ND ug/kg 06/02/22 12:46 100-02-706/01/22 17:262050 794 1
N-Nitrosodimethylamine ND ug/kg 06/02/22 12:46 62-75-906/01/22 17:26411 138 1
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 12:46 621-64-706/01/22 17:26411 154 1
N-Nitrosodiphenylamine ND ug/kg 06/02/22 12:46 86-30-606/01/22 17:26411 146 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 12:46 108-60-106/01/22 17:26411 195 1
Pentachlorophenol ND ug/kg 06/02/22 12:46 87-86-506/01/22 17:26821 402 1
Phenanthrene ND ug/kg 06/02/22 12:46 85-01-806/01/22 17:26411 134 1
Phenol ND ug/kg 06/02/22 12:46 108-95-206/01/22 17:26411 183 1
Pyrene ND ug/kg 06/02/22 12:46 129-00-006/01/22 17:26411 167 1
Pyridine ND ug/kg 06/02/22 12:46 110-86-106/01/22 17:26411 129 1
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 12:46 120-82-106/01/22 17:26411 162 1
2,4,5-Trichlorophenol ND ug/kg 06/02/22 12:46 95-95-406/01/22 17:26411 188 1
2,4,6-Trichlorophenol ND ug/kg 06/02/22 12:46 88-06-206/01/22 17:26411 169 1
Surrogates
Nitrobenzene-d5 (S)70 %06/02/22 12:46 4165-60-006/01/22 17:2621-130 1
2-Fluorobiphenyl (S)73 %06/02/22 12:46 321-60-806/01/22 17:2619-130 1
Terphenyl-d14 (S)80 %06/02/22 12:46 1718-51-006/01/22 17:2615-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: C-COMPOSITE Lab ID: 92606758008 Collected: 05/26/22 14:55 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)64 %06/02/22 12:46 13127-88-306/01/22 17:2618-130 1
2-Fluorophenol (S)60 %06/02/22 12:46 367-12-406/01/22 17:2618-130 1
2,4,6-Tribromophenol (S)78 %06/02/22 12:46 118-79-606/01/22 17:2618-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.0 %05/27/22 17:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: D-COMPOSITE Lab ID: 92606758009 Collected: 05/26/22 10:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 17:12 7440-38-205/31/22 15:533.9 2.8 1
Barium 124 mg/kg 06/01/22 17:12 7440-39-305/31/22 15:531.3 0.54 1
Cadmium ND mg/kg 06/01/22 17:12 7440-43-905/31/22 15:531.3 0.39 1
Chromium 52.5 mg/kg 06/01/22 17:12 7440-47-305/31/22 15:531.3 1.2 1
Lead 33.9 mg/kg 06/01/22 17:12 7439-92-105/31/22 15:533.3 2.0 1
Manganese 1030 mg/kg 06/01/22 17:12 7439-96-505/31/22 15:535.3 0.98 1
Selenium ND mg/kg 06/02/22 18:06 7782-49-2 D305/31/22 15:5332.8 28.4 5
Silver ND mg/kg 06/01/22 17:12 7440-22-405/31/22 15:531.3 0.54 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.032J mg/kg 06/01/22 09:05 7439-97-605/31/22 17:000.33 0.014 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 13:15 83-32-906/01/22 17:26473 166 1
Acenaphthylene ND ug/kg 06/02/22 13:15 208-96-806/01/22 17:26473 166 1
Aniline ND ug/kg 06/02/22 13:15 62-53-306/01/22 17:26473 185 1
Anthracene ND ug/kg 06/02/22 13:15 120-12-706/01/22 17:26473 155 1
Benzo(a)anthracene ND ug/kg 06/02/22 13:15 56-55-306/01/22 17:26473 158 1
Benzo(a)pyrene ND ug/kg 06/02/22 13:15 50-32-806/01/22 17:26473 163 1
Benzo(b)fluoranthene ND ug/kg 06/02/22 13:15 205-99-206/01/22 17:26473 158 1
Benzo(g,h,i)perylene ND ug/kg 06/02/22 13:15 191-24-206/01/22 17:26473 183 1
Benzo(k)fluoranthene ND ug/kg 06/02/22 13:15 207-08-906/01/22 17:26473 166 1
Benzoic Acid ND ug/kg 06/02/22 13:15 65-85-006/01/22 17:262360 1020 1
Benzyl alcohol ND ug/kg 06/02/22 13:15 100-51-606/01/22 17:26946 358 1
4-Bromophenylphenyl ether ND ug/kg 06/02/22 13:15 101-55-306/01/22 17:26473 182 1
Butylbenzylphthalate ND ug/kg 06/02/22 13:15 85-68-706/01/22 17:26473 199 1
4-Chloro-3-methylphenol ND ug/kg 06/02/22 13:15 59-50-706/01/22 17:26946 332 1
4-Chloroaniline ND ug/kg 06/02/22 13:15 106-47-806/01/22 17:26946 371 1
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 13:15 111-91-106/01/22 17:26473 196 1
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 13:15 111-44-406/01/22 17:26473 178 1
2-Chloronaphthalene ND ug/kg 06/02/22 13:15 91-58-706/01/22 17:26473 188 1
2-Chlorophenol ND ug/kg 06/02/22 13:15 95-57-806/01/22 17:26473 178 1
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 13:15 7005-72-306/01/22 17:26473 176 1
Chrysene ND ug/kg 06/02/22 13:15 218-01-906/01/22 17:26473 172 1
Dibenz(a,h)anthracene ND ug/kg 06/02/22 13:15 53-70-306/01/22 17:26473 182 1
Dibenzofuran ND ug/kg 06/02/22 13:15 132-64-906/01/22 17:26473 171 1
1,2-Dichlorobenzene ND ug/kg 06/02/22 13:15 95-50-106/01/22 17:26473 171 1
1,3-Dichlorobenzene ND ug/kg 06/02/22 13:15 541-73-106/01/22 17:26473 168 1
1,4-Dichlorobenzene ND ug/kg 06/02/22 13:15 106-46-706/01/22 17:26473 181 1
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 13:15 91-94-1 IL06/01/22 17:26946 320 1
2,4-Dichlorophenol ND ug/kg 06/02/22 13:15 120-83-206/01/22 17:26473 185 1
Diethylphthalate ND ug/kg 06/02/22 13:15 84-66-2 v106/01/22 17:26473 173 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: D-COMPOSITE Lab ID: 92606758009 Collected: 05/26/22 10:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 13:15 105-67-906/01/22 17:26473 196 1
Dimethylphthalate ND ug/kg 06/02/22 13:15 131-11-306/01/22 17:26473 172 1
Di-n-butylphthalate ND ug/kg 06/02/22 13:15 84-74-206/01/22 17:26473 159 1
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 13:15 534-52-106/01/22 17:26946 441 1
2,4-Dinitrophenol ND ug/kg 06/02/22 13:15 51-28-506/01/22 17:262360 1460 1
2,4-Dinitrotoluene ND ug/kg 06/02/22 13:15 121-14-206/01/22 17:26473 182 1
2,6-Dinitrotoluene ND ug/kg 06/02/22 13:15 606-20-206/01/22 17:26473 173 1
Di-n-octylphthalate ND ug/kg 06/02/22 13:15 117-84-006/01/22 17:26473 186 1
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 13:15 117-81-706/01/22 17:26473 183 1
Fluoranthene ND ug/kg 06/02/22 13:15 206-44-006/01/22 17:26473 162 1
Fluorene ND ug/kg 06/02/22 13:15 86-73-706/01/22 17:26473 166 1
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 13:15 87-68-306/01/22 17:26473 205 1
Hexachlorobenzene ND ug/kg 06/02/22 13:15 118-74-106/01/22 17:26473 185 1
Hexachlorocyclopentadiene ND ug/kg 06/02/22 13:15 77-47-406/01/22 17:26473 271 1
Hexachloroethane ND ug/kg 06/02/22 13:15 67-72-106/01/22 17:26473 181 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/02/22 13:15 193-39-506/01/22 17:26473 186 1
Isophorone ND ug/kg 06/02/22 13:15 78-59-106/01/22 17:26473 211 1
1-Methylnaphthalene ND ug/kg 06/02/22 13:15 90-12-006/01/22 17:26473 166 1
2-Methylnaphthalene ND ug/kg 06/02/22 13:15 91-57-606/01/22 17:26473 189 1
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 13:15 95-48-706/01/22 17:26473 193 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 13:15 15831-10-4 v206/01/22 17:26473 191 1
Naphthalene ND ug/kg 06/02/22 13:15 91-20-306/01/22 17:26473 160 1
2-Nitroaniline ND ug/kg 06/02/22 13:15 88-74-406/01/22 17:262360 387 1
3-Nitroaniline ND ug/kg 06/02/22 13:15 99-09-206/01/22 17:262360 371 1
4-Nitroaniline ND ug/kg 06/02/22 13:15 100-01-606/01/22 17:26946 360 1
Nitrobenzene ND ug/kg 06/02/22 13:15 98-95-306/01/22 17:26473 219 1
2-Nitrophenol ND ug/kg 06/02/22 13:15 88-75-506/01/22 17:26473 205 1
4-Nitrophenol ND ug/kg 06/02/22 13:15 100-02-706/01/22 17:262360 914 1
N-Nitrosodimethylamine ND ug/kg 06/02/22 13:15 62-75-906/01/22 17:26473 159 1
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 13:15 621-64-706/01/22 17:26473 178 1
N-Nitrosodiphenylamine ND ug/kg 06/02/22 13:15 86-30-606/01/22 17:26473 168 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 13:15 108-60-106/01/22 17:26473 225 1
Pentachlorophenol ND ug/kg 06/02/22 13:15 87-86-506/01/22 17:26946 463 1
Phenanthrene ND ug/kg 06/02/22 13:15 85-01-806/01/22 17:26473 155 1
Phenol ND ug/kg 06/02/22 13:15 108-95-206/01/22 17:26473 211 1
Pyrene ND ug/kg 06/02/22 13:15 129-00-006/01/22 17:26473 192 1
Pyridine ND ug/kg 06/02/22 13:15 110-86-106/01/22 17:26473 149 1
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 13:15 120-82-106/01/22 17:26473 186 1
2,4,5-Trichlorophenol ND ug/kg 06/02/22 13:15 95-95-406/01/22 17:26473 216 1
2,4,6-Trichlorophenol ND ug/kg 06/02/22 13:15 88-06-206/01/22 17:26473 195 1
Surrogates
Nitrobenzene-d5 (S)68 %06/02/22 13:15 4165-60-006/01/22 17:2621-130 1
2-Fluorobiphenyl (S)65 %06/02/22 13:15 321-60-806/01/22 17:2619-130 1
Terphenyl-d14 (S)61 %06/02/22 13:15 1718-51-006/01/22 17:2615-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: D-COMPOSITE Lab ID: 92606758009 Collected: 05/26/22 10:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)57 %06/02/22 13:15 13127-88-306/01/22 17:2618-130 1
2-Fluorophenol (S)26 %06/02/22 13:15 367-12-406/01/22 17:2618-130 1
2,4,6-Tribromophenol (S)30 %06/02/22 13:15 118-79-606/01/22 17:2618-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.5 %05/27/22 17:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: E-COMPOSITE Lab ID: 92606758010 Collected: 05/26/22 13:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 17:17 7440-38-205/31/22 15:533.3 2.4 1
Barium 112 mg/kg 06/01/22 17:17 7440-39-305/31/22 15:531.1 0.46 1
Cadmium ND mg/kg 06/01/22 17:17 7440-43-905/31/22 15:531.1 0.33 1
Chromium 39.4 mg/kg 06/01/22 17:17 7440-47-305/31/22 15:531.1 1.0 1
Lead 11.1 mg/kg 06/01/22 17:17 7439-92-105/31/22 15:532.8 1.7 1
Manganese 627 mg/kg 06/01/22 17:17 7439-96-505/31/22 15:534.5 0.83 1
Selenium ND mg/kg 06/02/22 18:24 7782-49-2 D305/31/22 15:5327.8 24.1 5
Silver ND mg/kg 06/01/22 17:17 7440-22-405/31/22 15:531.1 0.46 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/01/22 09:08 7439-97-605/31/22 17:000.26 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 13:43 83-32-906/01/22 17:26388 136 1
Acenaphthylene ND ug/kg 06/02/22 13:43 208-96-806/01/22 17:26388 136 1
Aniline ND ug/kg 06/02/22 13:43 62-53-306/01/22 17:26388 152 1
Anthracene ND ug/kg 06/02/22 13:43 120-12-706/01/22 17:26388 127 1
Benzo(a)anthracene ND ug/kg 06/02/22 13:43 56-55-306/01/22 17:26388 129 1
Benzo(a)pyrene ND ug/kg 06/02/22 13:43 50-32-806/01/22 17:26388 134 1
Benzo(b)fluoranthene ND ug/kg 06/02/22 13:43 205-99-206/01/22 17:26388 129 1
Benzo(g,h,i)perylene ND ug/kg 06/02/22 13:43 191-24-206/01/22 17:26388 151 1
Benzo(k)fluoranthene ND ug/kg 06/02/22 13:43 207-08-906/01/22 17:26388 136 1
Benzoic Acid ND ug/kg 06/02/22 13:43 65-85-006/01/22 17:261940 834 1
Benzyl alcohol ND ug/kg 06/02/22 13:43 100-51-606/01/22 17:26776 294 1
4-Bromophenylphenyl ether ND ug/kg 06/02/22 13:43 101-55-306/01/22 17:26388 149 1
Butylbenzylphthalate ND ug/kg 06/02/22 13:43 85-68-706/01/22 17:26388 163 1
4-Chloro-3-methylphenol ND ug/kg 06/02/22 13:43 59-50-706/01/22 17:26776 273 1
4-Chloroaniline ND ug/kg 06/02/22 13:43 106-47-806/01/22 17:26776 305 1
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 13:43 111-91-106/01/22 17:26388 161 1
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 13:43 111-44-406/01/22 17:26388 146 1
2-Chloronaphthalene ND ug/kg 06/02/22 13:43 91-58-706/01/22 17:26388 154 1
2-Chlorophenol ND ug/kg 06/02/22 13:43 95-57-806/01/22 17:26388 146 1
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 13:43 7005-72-306/01/22 17:26388 145 1
Chrysene ND ug/kg 06/02/22 13:43 218-01-906/01/22 17:26388 141 1
Dibenz(a,h)anthracene ND ug/kg 06/02/22 13:43 53-70-306/01/22 17:26388 149 1
Dibenzofuran ND ug/kg 06/02/22 13:43 132-64-906/01/22 17:26388 140 1
1,2-Dichlorobenzene ND ug/kg 06/02/22 13:43 95-50-106/01/22 17:26388 140 1
1,3-Dichlorobenzene ND ug/kg 06/02/22 13:43 541-73-106/01/22 17:26388 138 1
1,4-Dichlorobenzene ND ug/kg 06/02/22 13:43 106-46-706/01/22 17:26388 148 1
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 13:43 91-94-1 IL06/01/22 17:26776 262 1
2,4-Dichlorophenol ND ug/kg 06/02/22 13:43 120-83-206/01/22 17:26388 152 1
Diethylphthalate ND ug/kg 06/02/22 13:43 84-66-2 v106/01/22 17:26388 142 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: E-COMPOSITE Lab ID: 92606758010 Collected: 05/26/22 13:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 13:43 105-67-906/01/22 17:26388 161 1
Dimethylphthalate ND ug/kg 06/02/22 13:43 131-11-306/01/22 17:26388 141 1
Di-n-butylphthalate ND ug/kg 06/02/22 13:43 84-74-206/01/22 17:26388 131 1
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 13:43 534-52-106/01/22 17:26776 362 1
2,4-Dinitrophenol ND ug/kg 06/02/22 13:43 51-28-506/01/22 17:261940 1200 1
2,4-Dinitrotoluene ND ug/kg 06/02/22 13:43 121-14-206/01/22 17:26388 149 1
2,6-Dinitrotoluene ND ug/kg 06/02/22 13:43 606-20-206/01/22 17:26388 142 1
Di-n-octylphthalate ND ug/kg 06/02/22 13:43 117-84-006/01/22 17:26388 153 1
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 13:43 117-81-706/01/22 17:26388 151 1
Fluoranthene ND ug/kg 06/02/22 13:43 206-44-006/01/22 17:26388 133 1
Fluorene ND ug/kg 06/02/22 13:43 86-73-706/01/22 17:26388 136 1
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 13:43 87-68-306/01/22 17:26388 168 1
Hexachlorobenzene ND ug/kg 06/02/22 13:43 118-74-106/01/22 17:26388 152 1
Hexachlorocyclopentadiene ND ug/kg 06/02/22 13:43 77-47-406/01/22 17:26388 222 1
Hexachloroethane ND ug/kg 06/02/22 13:43 67-72-106/01/22 17:26388 148 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/02/22 13:43 193-39-506/01/22 17:26388 153 1
Isophorone ND ug/kg 06/02/22 13:43 78-59-106/01/22 17:26388 173 1
1-Methylnaphthalene ND ug/kg 06/02/22 13:43 90-12-006/01/22 17:26388 136 1
2-Methylnaphthalene ND ug/kg 06/02/22 13:43 91-57-606/01/22 17:26388 155 1
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 13:43 95-48-706/01/22 17:26388 159 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 13:43 15831-10-4 v206/01/22 17:26388 156 1
Naphthalene ND ug/kg 06/02/22 13:43 91-20-306/01/22 17:26388 132 1
2-Nitroaniline ND ug/kg 06/02/22 13:43 88-74-406/01/22 17:261940 318 1
3-Nitroaniline ND ug/kg 06/02/22 13:43 99-09-206/01/22 17:261940 305 1
4-Nitroaniline ND ug/kg 06/02/22 13:43 100-01-606/01/22 17:26776 295 1
Nitrobenzene ND ug/kg 06/02/22 13:43 98-95-306/01/22 17:26388 180 1
2-Nitrophenol ND ug/kg 06/02/22 13:43 88-75-506/01/22 17:26388 168 1
4-Nitrophenol ND ug/kg 06/02/22 13:43 100-02-706/01/22 17:261940 750 1
N-Nitrosodimethylamine ND ug/kg 06/02/22 13:43 62-75-906/01/22 17:26388 131 1
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 13:43 621-64-706/01/22 17:26388 146 1
N-Nitrosodiphenylamine ND ug/kg 06/02/22 13:43 86-30-606/01/22 17:26388 138 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 13:43 108-60-106/01/22 17:26388 185 1
Pentachlorophenol ND ug/kg 06/02/22 13:43 87-86-506/01/22 17:26776 380 1
Phenanthrene ND ug/kg 06/02/22 13:43 85-01-806/01/22 17:26388 127 1
Phenol ND ug/kg 06/02/22 13:43 108-95-206/01/22 17:26388 173 1
Pyrene ND ug/kg 06/02/22 13:43 129-00-006/01/22 17:26388 158 1
Pyridine ND ug/kg 06/02/22 13:43 110-86-106/01/22 17:26388 122 1
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 13:43 120-82-106/01/22 17:26388 153 1
2,4,5-Trichlorophenol ND ug/kg 06/02/22 13:43 95-95-406/01/22 17:26388 178 1
2,4,6-Trichlorophenol ND ug/kg 06/02/22 13:43 88-06-206/01/22 17:26388 160 1
Surrogates
Nitrobenzene-d5 (S)60 %06/02/22 13:43 4165-60-006/01/22 17:2621-130 1
2-Fluorobiphenyl (S)69 %06/02/22 13:43 321-60-806/01/22 17:2619-130 1
Terphenyl-d14 (S)71 %06/02/22 13:43 1718-51-006/01/22 17:2615-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: E-COMPOSITE Lab ID: 92606758010 Collected: 05/26/22 13:15 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)58 %06/02/22 13:43 13127-88-306/01/22 17:2618-130 1
2-Fluorophenol (S)55 %06/02/22 13:43 367-12-406/01/22 17:2618-130 1
2,4,6-Tribromophenol (S)74 %06/02/22 13:43 118-79-606/01/22 17:2618-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.3 %05/27/22 17:58 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: DUP-1 Lab ID: 92606758011 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/01/22 17:22 7440-38-205/31/22 15:533.7 2.6 1
Barium 71.9 mg/kg 06/01/22 17:22 7440-39-305/31/22 15:531.2 0.51 1
Cadmium ND mg/kg 06/01/22 17:22 7440-43-905/31/22 15:531.2 0.36 1
Chromium 39.5 mg/kg 06/01/22 17:22 7440-47-305/31/22 15:531.2 1.1 1
Lead 18.6 mg/kg 06/01/22 17:22 7439-92-105/31/22 15:533.1 1.9 1
Manganese 530 mg/kg 06/01/22 17:22 7439-96-505/31/22 15:534.9 0.92 1
Selenium ND mg/kg 06/01/22 17:22 7782-49-205/31/22 15:536.1 5.3 1
Silver ND mg/kg 06/01/22 17:22 7440-22-405/31/22 15:531.2 0.50 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.025J mg/kg 06/01/22 09:11 7439-97-605/31/22 17:000.30 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/02/22 14:12 83-32-906/01/22 17:26417 146 1
Acenaphthylene ND ug/kg 06/02/22 14:12 208-96-806/01/22 17:26417 146 1
Aniline ND ug/kg 06/02/22 14:12 62-53-306/01/22 17:26417 163 1
Anthracene ND ug/kg 06/02/22 14:12 120-12-706/01/22 17:26417 136 1
Benzo(a)anthracene 139J ug/kg 06/02/22 14:12 56-55-306/01/22 17:26417 139 1
Benzo(a)pyrene ND ug/kg 06/02/22 14:12 50-32-806/01/22 17:26417 144 1
Benzo(b)fluoranthene 163J ug/kg 06/02/22 14:12 205-99-206/01/22 17:26417 139 1
Benzo(g,h,i)perylene ND ug/kg 06/02/22 14:12 191-24-206/01/22 17:26417 162 1
Benzo(k)fluoranthene ND ug/kg 06/02/22 14:12 207-08-906/01/22 17:26417 146 1
Benzoic Acid ND ug/kg 06/02/22 14:12 65-85-006/01/22 17:262080 895 1
Benzyl alcohol ND ug/kg 06/02/22 14:12 100-51-606/01/22 17:26834 316 1
4-Bromophenylphenyl ether ND ug/kg 06/02/22 14:12 101-55-306/01/22 17:26417 160 1
Butylbenzylphthalate ND ug/kg 06/02/22 14:12 85-68-706/01/22 17:26417 176 1
4-Chloro-3-methylphenol ND ug/kg 06/02/22 14:12 59-50-706/01/22 17:26834 293 1
4-Chloroaniline ND ug/kg 06/02/22 14:12 106-47-806/01/22 17:26834 327 1
bis(2-Chloroethoxy)methane ND ug/kg 06/02/22 14:12 111-91-106/01/22 17:26417 173 1
bis(2-Chloroethyl) ether ND ug/kg 06/02/22 14:12 111-44-406/01/22 17:26417 157 1
2-Chloronaphthalene ND ug/kg 06/02/22 14:12 91-58-706/01/22 17:26417 165 1
2-Chlorophenol ND ug/kg 06/02/22 14:12 95-57-806/01/22 17:26417 157 1
4-Chlorophenylphenyl ether ND ug/kg 06/02/22 14:12 7005-72-306/01/22 17:26417 155 1
Chrysene 171J ug/kg 06/02/22 14:12 218-01-906/01/22 17:26417 152 1
Dibenz(a,h)anthracene ND ug/kg 06/02/22 14:12 53-70-306/01/22 17:26417 160 1
Dibenzofuran ND ug/kg 06/02/22 14:12 132-64-906/01/22 17:26417 150 1
1,2-Dichlorobenzene ND ug/kg 06/02/22 14:12 95-50-106/01/22 17:26417 150 1
1,3-Dichlorobenzene ND ug/kg 06/02/22 14:12 541-73-106/01/22 17:26417 148 1
1,4-Dichlorobenzene ND ug/kg 06/02/22 14:12 106-46-706/01/22 17:26417 159 1
3,3'-Dichlorobenzidine ND ug/kg 06/02/22 14:12 91-94-1 IL06/01/22 17:26834 282 1
2,4-Dichlorophenol ND ug/kg 06/02/22 14:12 120-83-206/01/22 17:26417 163 1
Diethylphthalate ND ug/kg 06/02/22 14:12 84-66-2 v106/01/22 17:26417 153 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: DUP-1 Lab ID: 92606758011 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4-Dimethylphenol ND ug/kg 06/02/22 14:12 105-67-906/01/22 17:26417 173 1
Dimethylphthalate ND ug/kg 06/02/22 14:12 131-11-306/01/22 17:26417 152 1
Di-n-butylphthalate ND ug/kg 06/02/22 14:12 84-74-206/01/22 17:26417 140 1
4,6-Dinitro-2-methylphenol ND ug/kg 06/02/22 14:12 534-52-106/01/22 17:26834 389 1
2,4-Dinitrophenol ND ug/kg 06/02/22 14:12 51-28-506/01/22 17:262080 1290 1
2,4-Dinitrotoluene ND ug/kg 06/02/22 14:12 121-14-206/01/22 17:26417 160 1
2,6-Dinitrotoluene ND ug/kg 06/02/22 14:12 606-20-206/01/22 17:26417 153 1
Di-n-octylphthalate ND ug/kg 06/02/22 14:12 117-84-006/01/22 17:26417 164 1
bis(2-Ethylhexyl)phthalate ND ug/kg 06/02/22 14:12 117-81-706/01/22 17:26417 162 1
Fluoranthene 268J ug/kg 06/02/22 14:12 206-44-006/01/22 17:26417 143 1
Fluorene ND ug/kg 06/02/22 14:12 86-73-706/01/22 17:26417 146 1
Hexachloro-1,3-butadiene ND ug/kg 06/02/22 14:12 87-68-306/01/22 17:26417 181 1
Hexachlorobenzene ND ug/kg 06/02/22 14:12 118-74-106/01/22 17:26417 163 1
Hexachlorocyclopentadiene ND ug/kg 06/02/22 14:12 77-47-406/01/22 17:26417 239 1
Hexachloroethane ND ug/kg 06/02/22 14:12 67-72-106/01/22 17:26417 159 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/02/22 14:12 193-39-506/01/22 17:26417 164 1
Isophorone ND ug/kg 06/02/22 14:12 78-59-106/01/22 17:26417 186 1
1-Methylnaphthalene ND ug/kg 06/02/22 14:12 90-12-006/01/22 17:26417 146 1
2-Methylnaphthalene ND ug/kg 06/02/22 14:12 91-57-606/01/22 17:26417 167 1
2-Methylphenol(o-Cresol)ND ug/kg 06/02/22 14:12 95-48-706/01/22 17:26417 170 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/02/22 14:12 15831-10-4 v206/01/22 17:26417 168 1
Naphthalene ND ug/kg 06/02/22 14:12 91-20-306/01/22 17:26417 141 1
2-Nitroaniline ND ug/kg 06/02/22 14:12 88-74-406/01/22 17:262080 341 1
3-Nitroaniline ND ug/kg 06/02/22 14:12 99-09-206/01/22 17:262080 327 1
4-Nitroaniline ND ug/kg 06/02/22 14:12 100-01-606/01/22 17:26834 317 1
Nitrobenzene ND ug/kg 06/02/22 14:12 98-95-306/01/22 17:26417 193 1
2-Nitrophenol ND ug/kg 06/02/22 14:12 88-75-506/01/22 17:26417 181 1
4-Nitrophenol ND ug/kg 06/02/22 14:12 100-02-706/01/22 17:262080 806 1
N-Nitrosodimethylamine ND ug/kg 06/02/22 14:12 62-75-906/01/22 17:26417 140 1
N-Nitroso-di-n-propylamine ND ug/kg 06/02/22 14:12 621-64-706/01/22 17:26417 157 1
N-Nitrosodiphenylamine ND ug/kg 06/02/22 14:12 86-30-606/01/22 17:26417 148 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/02/22 14:12 108-60-106/01/22 17:26417 198 1
Pentachlorophenol ND ug/kg 06/02/22 14:12 87-86-506/01/22 17:26834 408 1
Phenanthrene 195J ug/kg 06/02/22 14:12 85-01-806/01/22 17:26417 136 1
Phenol ND ug/kg 06/02/22 14:12 108-95-206/01/22 17:26417 186 1
Pyrene 219J ug/kg 06/02/22 14:12 129-00-006/01/22 17:26417 169 1
Pyridine ND ug/kg 06/02/22 14:12 110-86-106/01/22 17:26417 131 1
1,2,4-Trichlorobenzene ND ug/kg 06/02/22 14:12 120-82-106/01/22 17:26417 164 1
2,4,5-Trichlorophenol ND ug/kg 06/02/22 14:12 95-95-406/01/22 17:26417 191 1
2,4,6-Trichlorophenol ND ug/kg 06/02/22 14:12 88-06-206/01/22 17:26417 172 1
Surrogates
Nitrobenzene-d5 (S)62 %06/02/22 14:12 4165-60-006/01/22 17:2621-130 1
2-Fluorobiphenyl (S)71 %06/02/22 14:12 321-60-806/01/22 17:2619-130 1
Terphenyl-d14 (S)69 %06/02/22 14:12 1718-51-006/01/22 17:2615-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: DUP-1 Lab ID: 92606758011 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Phenol-d6 (S)50 %06/02/22 14:12 13127-88-306/01/22 17:2618-130 1
2-Fluorophenol (S)26 %06/02/22 14:12 367-12-406/01/22 17:2618-130 1
2,4,6-Tribromophenol (S)20 %06/02/22 14:12 118-79-606/01/22 17:2618-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/01/22 04:14 67-64-105/27/22 15:53159 50.9 1
Benzene ND ug/kg 06/01/22 04:14 71-43-205/27/22 15:537.9 3.2 1
Bromobenzene ND ug/kg 06/01/22 04:14 108-86-105/27/22 15:537.9 2.6 1
Bromochloromethane ND ug/kg 06/01/22 04:14 74-97-505/27/22 15:537.9 2.3 1
Bromodichloromethane ND ug/kg 06/01/22 04:14 75-27-405/27/22 15:537.9 3.1 1
Bromoform ND ug/kg 06/01/22 04:14 75-25-205/27/22 15:537.9 2.8 1
Bromomethane ND ug/kg 06/01/22 04:14 74-83-905/27/22 15:5315.9 12.5 1
2-Butanone (MEK)ND ug/kg 06/01/22 04:14 78-93-305/27/22 15:53159 38.1 1
n-Butylbenzene ND ug/kg 06/01/22 04:14 104-51-805/27/22 15:537.9 3.7 1
sec-Butylbenzene ND ug/kg 06/01/22 04:14 135-98-805/27/22 15:537.9 3.5 1
tert-Butylbenzene ND ug/kg 06/01/22 04:14 98-06-605/27/22 15:537.9 2.8 1
Carbon tetrachloride ND ug/kg 06/01/22 04:14 56-23-505/27/22 15:537.9 3.0 1
Chlorobenzene ND ug/kg 06/01/22 04:14 108-90-705/27/22 15:537.9 1.5 1
Chloroethane ND ug/kg 06/01/22 04:14 75-00-305/27/22 15:5315.9 6.1 1
Chloroform ND ug/kg 06/01/22 04:14 67-66-305/27/22 15:537.9 4.8 1
Chloromethane ND ug/kg 06/01/22 04:14 74-87-305/27/22 15:5315.9 6.7 1
2-Chlorotoluene ND ug/kg 06/01/22 04:14 95-49-805/27/22 15:537.9 2.8 1
4-Chlorotoluene ND ug/kg 06/01/22 04:14 106-43-405/27/22 15:537.9 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/01/22 04:14 96-12-805/27/22 15:537.9 3.1 1
Dibromochloromethane ND ug/kg 06/01/22 04:14 124-48-105/27/22 15:537.9 4.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/01/22 04:14 106-93-405/27/22 15:537.9 3.5 1
Dibromomethane ND ug/kg 06/01/22 04:14 74-95-305/27/22 15:537.9 1.7 1
1,2-Dichlorobenzene ND ug/kg 06/01/22 04:14 95-50-105/27/22 15:537.9 2.9 1
1,3-Dichlorobenzene ND ug/kg 06/01/22 04:14 541-73-105/27/22 15:537.9 2.5 1
1,4-Dichlorobenzene ND ug/kg 06/01/22 04:14 106-46-705/27/22 15:537.9 2.1 1
Dichlorodifluoromethane ND ug/kg 06/01/22 04:14 75-71-8 v105/27/22 15:5315.9 3.4 1
1,1-Dichloroethane ND ug/kg 06/01/22 04:14 75-34-305/27/22 15:537.9 3.3 1
1,2-Dichloroethane ND ug/kg 06/01/22 04:14 107-06-205/27/22 15:537.9 5.2 1
1,1-Dichloroethene ND ug/kg 06/01/22 04:14 75-35-405/27/22 15:537.9 3.3 1
cis-1,2-Dichloroethene ND ug/kg 06/01/22 04:14 156-59-205/27/22 15:537.9 2.7 1
trans-1,2-Dichloroethene ND ug/kg 06/01/22 04:14 156-60-505/27/22 15:537.9 2.8 1
1,2-Dichloropropane ND ug/kg 06/01/22 04:14 78-87-505/27/22 15:537.9 2.4 1
1,3-Dichloropropane ND ug/kg 06/01/22 04:14 142-28-905/27/22 15:537.9 2.5 1
2,2-Dichloropropane ND ug/kg 06/01/22 04:14 594-20-705/27/22 15:537.9 2.6 1
1,1-Dichloropropene ND ug/kg 06/01/22 04:14 563-58-605/27/22 15:537.9 3.8 1
cis-1,3-Dichloropropene ND ug/kg 06/01/22 04:14 10061-01-505/27/22 15:537.9 2.2 1
trans-1,3-Dichloropropene ND ug/kg 06/01/22 04:14 10061-02-605/27/22 15:537.9 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: DUP-1 Lab ID: 92606758011 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Diisopropyl ether ND ug/kg 06/01/22 04:14 108-20-305/27/22 15:537.9 2.1 1
Ethylbenzene 31.1 ug/kg 06/01/22 04:14 100-41-405/27/22 15:537.9 3.7 1
Hexachloro-1,3-butadiene ND ug/kg 06/01/22 04:14 87-68-305/27/22 15:5315.9 13.0 1
2-Hexanone ND ug/kg 06/01/22 04:14 591-78-605/27/22 15:5379.3 7.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/01/22 04:14 98-82-805/27/22 15:537.9 2.7 1
p-Isopropyltoluene 157 ug/kg 06/01/22 04:14 99-87-605/27/22 15:537.9 3.9 1
Methylene Chloride ND ug/kg 06/01/22 04:14 75-09-205/27/22 15:5331.7 21.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/01/22 04:14 108-10-105/27/22 15:5379.3 7.6 1
Methyl-tert-butyl ether ND ug/kg 06/01/22 04:14 1634-04-405/27/22 15:537.9 3.0 1
Naphthalene ND ug/kg 06/01/22 04:14 91-20-305/27/22 15:537.9 4.2 1
n-Propylbenzene ND ug/kg 06/01/22 04:14 103-65-105/27/22 15:537.9 2.8 1
Styrene 231 ug/kg 06/01/22 04:14 100-42-505/27/22 15:537.9 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/01/22 04:14 630-20-605/27/22 15:537.9 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/01/22 04:14 79-34-505/27/22 15:537.9 2.1 1
Tetrachloroethene ND ug/kg 06/01/22 04:14 127-18-405/27/22 15:537.9 2.5 1
Toluene ND ug/kg 06/01/22 04:14 108-88-305/27/22 15:537.9 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/01/22 04:14 87-61-605/27/22 15:537.9 6.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/01/22 04:14 120-82-105/27/22 15:537.9 6.7 1
1,1,1-Trichloroethane ND ug/kg 06/01/22 04:14 71-55-605/27/22 15:537.9 4.1 1
1,1,2-Trichloroethane ND ug/kg 06/01/22 04:14 79-00-505/27/22 15:537.9 2.6 1
Trichloroethene ND ug/kg 06/01/22 04:14 79-01-605/27/22 15:537.9 2.0 1
Trichlorofluoromethane ND ug/kg 06/01/22 04:14 75-69-405/27/22 15:537.9 4.4 1
1,2,3-Trichloropropane ND ug/kg 06/01/22 04:14 96-18-405/27/22 15:537.9 4.0 1
1,2,4-Trimethylbenzene ND ug/kg 06/01/22 04:14 95-63-605/27/22 15:537.9 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/01/22 04:14 108-67-805/27/22 15:537.9 2.7 1
Vinyl acetate ND ug/kg 06/01/22 04:14 108-05-405/27/22 15:5379.3 5.8 1
Vinyl chloride ND ug/kg 06/01/22 04:14 75-01-405/27/22 15:5315.9 4.0 1
Xylene (Total)ND ug/kg 06/01/22 04:14 1330-20-705/27/22 15:5315.9 4.5 1
m&p-Xylene ND ug/kg 06/01/22 04:14 179601-23-105/27/22 15:5315.9 5.4 1
o-Xylene ND ug/kg 06/01/22 04:14 95-47-605/27/22 15:537.9 3.5 1
Surrogates
Toluene-d8 (S)101 %06/01/22 04:14 2037-26-505/27/22 15:5370-130 1
4-Bromofluorobenzene (S)102 %06/01/22 04:14 460-00-405/27/22 15:5369-134 1
1,2-Dichloroethane-d4 (S)104 %06/01/22 04:14 17060-07-005/27/22 15:5370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.3 %05/27/22 15:39 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: EB-1 Lab ID: 92606758012 Collected: 05/26/22 18:55 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Arsenic 3.0J ug/L 06/01/22 20:05 7440-38-205/31/22 13:075.0 2.2 1
Barium ND ug/L 06/01/22 20:05 7440-39-305/31/22 13:075.0 0.67 1
Cadmium ND ug/L 06/01/22 20:05 7440-43-905/31/22 13:070.50 0.11 1
Chromium ND ug/L 06/01/22 20:05 7440-47-305/31/22 13:075.0 1.1 1
Lead ND ug/L 06/01/22 20:05 7439-92-105/31/22 13:071.0 0.89 1
Manganese ND ug/L 06/01/22 20:05 7439-96-505/31/22 13:0710.0 1.1 1
Selenium ND ug/L 06/01/22 20:05 7782-49-205/31/22 13:075.0 1.4 1
Silver ND ug/L 06/01/22 20:05 7440-22-405/31/22 13:075.0 0.44 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 06/06/22 15:19 7439-97-606/06/22 11:050.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 05/31/22 15:59 83-32-905/31/22 05:278.3 1.7 1
Acenaphthylene ND ug/L 05/31/22 15:59 208-96-805/31/22 05:278.3 1.6 1
Aniline ND ug/L 05/31/22 15:59 62-53-305/31/22 05:278.3 1.4 1
Anthracene ND ug/L 05/31/22 15:59 120-12-705/31/22 05:278.3 1.9 1
Benzo(a)anthracene ND ug/L 05/31/22 15:59 56-55-305/31/22 05:278.3 2.2 1
Benzo(a)pyrene ND ug/L 05/31/22 15:59 50-32-805/31/22 05:278.3 2.3 1
Benzo(b)fluoranthene ND ug/L 05/31/22 15:59 205-99-205/31/22 05:278.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 05/31/22 15:59 191-24-205/31/22 05:278.3 2.4 1
Benzo(k)fluoranthene ND ug/L 05/31/22 15:59 207-08-905/31/22 05:278.3 2.3 1
Benzoic Acid ND ug/L 05/31/22 15:59 65-85-005/31/22 05:2741.7 18.3 1
Benzyl alcohol ND ug/L 05/31/22 15:59 100-51-605/31/22 05:2716.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 05/31/22 15:59 101-55-305/31/22 05:278.3 1.5 1
Butylbenzylphthalate ND ug/L 05/31/22 15:59 85-68-705/31/22 05:278.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 05/31/22 15:59 59-50-705/31/22 05:278.3 2.8 1
4-Chloroaniline ND ug/L 05/31/22 15:59 106-47-805/31/22 05:2716.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/31/22 15:59 111-91-105/31/22 05:278.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 05/31/22 15:59 111-44-405/31/22 05:278.3 1.6 1
2-Chloronaphthalene ND ug/L 05/31/22 15:59 91-58-705/31/22 05:278.3 1.4 1
2-Chlorophenol ND ug/L 05/31/22 15:59 95-57-805/31/22 05:278.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 05/31/22 15:59 7005-72-305/31/22 05:278.3 1.7 1
Chrysene ND ug/L 05/31/22 15:59 218-01-905/31/22 05:278.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 05/31/22 15:59 53-70-305/31/22 05:278.3 2.5 1
Dibenzofuran ND ug/L 05/31/22 15:59 132-64-905/31/22 05:278.3 1.8 1
1,2-Dichlorobenzene ND ug/L 05/31/22 15:59 95-50-105/31/22 05:278.3 1.5 1
1,3-Dichlorobenzene ND ug/L 05/31/22 15:59 541-73-105/31/22 05:278.3 1.3 1
1,4-Dichlorobenzene ND ug/L 05/31/22 15:59 106-46-705/31/22 05:278.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 05/31/22 15:59 91-94-105/31/22 05:2716.7 6.8 1
2,4-Dichlorophenol ND ug/L 05/31/22 15:59 120-83-205/31/22 05:278.3 1.2 1
Diethylphthalate ND ug/L 05/31/22 15:59 84-66-205/31/22 05:278.3 1.7 1
2,4-Dimethylphenol ND ug/L 05/31/22 15:59 105-67-905/31/22 05:278.3 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: EB-1 Lab ID: 92606758012 Collected: 05/26/22 18:55 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Dimethylphthalate ND ug/L 05/31/22 15:59 131-11-305/31/22 05:278.3 1.8 1
Di-n-butylphthalate ND ug/L 05/31/22 15:59 84-74-205/31/22 05:278.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 05/31/22 15:59 534-52-105/31/22 05:2716.7 6.5 1
2,4-Dinitrophenol ND ug/L 05/31/22 15:59 51-28-505/31/22 05:2741.7 21.7 1
2,4-Dinitrotoluene ND ug/L 05/31/22 15:59 121-14-205/31/22 05:278.3 1.4 1
2,6-Dinitrotoluene ND ug/L 05/31/22 15:59 606-20-205/31/22 05:278.3 1.4 1
Di-n-octylphthalate ND ug/L 05/31/22 15:59 117-84-005/31/22 05:278.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/31/22 15:59 117-81-705/31/22 05:275.0 3.1 1
Fluoranthene ND ug/L 05/31/22 15:59 206-44-005/31/22 05:278.3 1.8 1
Fluorene ND ug/L 05/31/22 15:59 86-73-705/31/22 05:278.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 05/31/22 15:59 87-68-305/31/22 05:278.3 1.5 1
Hexachlorobenzene ND ug/L 05/31/22 15:59 118-74-105/31/22 05:278.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 05/31/22 15:59 77-47-405/31/22 05:278.3 1.3 1
Hexachloroethane ND ug/L 05/31/22 15:59 67-72-105/31/22 05:278.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/31/22 15:59 193-39-505/31/22 05:278.3 2.4 1
Isophorone ND ug/L 05/31/22 15:59 78-59-105/31/22 05:278.3 1.4 1
1-Methylnaphthalene ND ug/L 05/31/22 15:59 90-12-005/31/22 05:278.3 1.7 1
2-Methylnaphthalene ND ug/L 05/31/22 15:59 91-57-605/31/22 05:278.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 05/31/22 15:59 95-48-705/31/22 05:278.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/31/22 15:59 15831-10-405/31/22 05:278.3 1.0 1
Naphthalene ND ug/L 05/31/22 15:59 91-20-305/31/22 05:278.3 1.7 1
2-Nitroaniline ND ug/L 05/31/22 15:59 88-74-405/31/22 05:2716.7 2.5 1
3-Nitroaniline ND ug/L 05/31/22 15:59 99-09-205/31/22 05:2716.7 3.1 1
4-Nitroaniline ND ug/L 05/31/22 15:59 100-01-605/31/22 05:2716.7 4.2 1
Nitrobenzene ND ug/L 05/31/22 15:59 98-95-305/31/22 05:278.3 1.6 1
2-Nitrophenol ND ug/L 05/31/22 15:59 88-75-505/31/22 05:278.3 1.2 1
4-Nitrophenol ND ug/L 05/31/22 15:59 100-02-705/31/22 05:2741.7 5.5 1
N-Nitrosodimethylamine ND ug/L 05/31/22 15:59 62-75-905/31/22 05:278.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 05/31/22 15:59 621-64-705/31/22 05:278.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 05/31/22 15:59 86-30-605/31/22 05:278.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 05/31/22 15:59 108-60-105/31/22 05:278.3 0.96 1
Pentachlorophenol ND ug/L 05/31/22 15:59 87-86-5 v205/31/22 05:2716.7 3.1 1
Phenanthrene ND ug/L 05/31/22 15:59 85-01-805/31/22 05:278.3 1.7 1
Phenol ND ug/L 05/31/22 15:59 108-95-205/31/22 05:278.3 1.1 1
Pyrene ND ug/L 05/31/22 15:59 129-00-005/31/22 05:278.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 05/31/22 15:59 120-82-105/31/22 05:278.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 05/31/22 15:59 95-95-405/31/22 05:278.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 05/31/22 15:59 88-06-205/31/22 05:278.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)49 %05/31/22 15:59 4165-60-005/31/22 05:2710-144 1
2-Fluorobiphenyl (S)44 %05/31/22 15:59 321-60-805/31/22 05:2710-130 1
Terphenyl-d14 (S)149 %05/31/22 15:59 1718-51-005/31/22 05:2734-163 1
Phenol-d6 (S)26 %05/31/22 15:59 13127-88-305/31/22 05:2710-130 1
2-Fluorophenol (S)33 %05/31/22 15:59 367-12-405/31/22 05:2710-130 1
2,4,6-Tribromophenol (S)84 %05/31/22 15:59 118-79-605/31/22 05:2710-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: EB-1 Lab ID: 92606758012 Collected: 05/26/22 18:55 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 05/31/22 14:22 67-64-125.0 5.1 1
Benzene ND ug/L 05/31/22 14:22 71-43-21.0 0.34 1
Bromobenzene ND ug/L 05/31/22 14:22 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 05/31/22 14:22 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 05/31/22 14:22 75-27-41.0 0.31 1
Bromoform ND ug/L 05/31/22 14:22 75-25-21.0 0.34 1
Bromomethane ND ug/L 05/31/22 14:22 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 05/31/22 14:22 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 05/31/22 14:22 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 05/31/22 14:22 108-90-71.0 0.28 1
Chloroethane ND ug/L 05/31/22 14:22 75-00-31.0 0.65 1
Chloroform ND ug/L 05/31/22 14:22 67-66-31.0 0.43 1
Chloromethane ND ug/L 05/31/22 14:22 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 05/31/22 14:22 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 05/31/22 14:22 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/22 14:22 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 05/31/22 14:22 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/22 14:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/22 14:22 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 05/31/22 14:22 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 05/31/22 14:22 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 05/31/22 14:22 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 05/31/22 14:22 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 05/31/22 14:22 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 05/31/22 14:22 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 05/31/22 14:22 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 05/31/22 14:22 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 05/31/22 14:22 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 05/31/22 14:22 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 05/31/22 14:22 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/31/22 14:22 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 05/31/22 14:22 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 05/31/22 14:22 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 05/31/22 14:22 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 05/31/22 14:22 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 05/31/22 14:22 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/31/22 14:22 87-68-32.0 1.5 1
2-Hexanone ND ug/L 05/31/22 14:22 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 05/31/22 14:22 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 05/31/22 14:22 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/22 14:22 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 05/31/22 14:22 1634-04-41.0 0.42 1
Naphthalene ND ug/L 05/31/22 14:22 91-20-31.0 0.64 1
Styrene ND ug/L 05/31/22 14:22 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/22 14:22 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: EB-1 Lab ID: 92606758012 Collected: 05/26/22 18:55 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 05/31/22 14:22 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 05/31/22 14:22 127-18-41.0 0.29 1
Toluene ND ug/L 05/31/22 14:22 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 05/31/22 14:22 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 05/31/22 14:22 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 05/31/22 14:22 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 05/31/22 14:22 79-00-51.0 0.32 1
Trichloroethene ND ug/L 05/31/22 14:22 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 05/31/22 14:22 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 05/31/22 14:22 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 05/31/22 14:22 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 05/31/22 14:22 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 05/31/22 14:22 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 05/31/22 14:22 179601-23-12.0 0.71 1
o-Xylene ND ug/L 05/31/22 14:22 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %05/31/22 14:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %05/31/22 14:22 17060-07-070-130 1
Toluene-d8 (S)100 %05/31/22 14:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: TRIP BLANK Lab ID: 92606758013 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 05/31/22 14:40 67-64-125.0 5.1 1
Benzene ND ug/L 05/31/22 14:40 71-43-21.0 0.34 1
Bromobenzene ND ug/L 05/31/22 14:40 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 05/31/22 14:40 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 05/31/22 14:40 75-27-41.0 0.31 1
Bromoform ND ug/L 05/31/22 14:40 75-25-21.0 0.34 1
Bromomethane ND ug/L 05/31/22 14:40 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 05/31/22 14:40 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 05/31/22 14:40 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 05/31/22 14:40 108-90-71.0 0.28 1
Chloroethane ND ug/L 05/31/22 14:40 75-00-31.0 0.65 1
Chloroform ND ug/L 05/31/22 14:40 67-66-31.0 0.43 1
Chloromethane ND ug/L 05/31/22 14:40 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 05/31/22 14:40 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 05/31/22 14:40 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/22 14:40 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 05/31/22 14:40 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/22 14:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/22 14:40 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 05/31/22 14:40 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 05/31/22 14:40 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 05/31/22 14:40 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 05/31/22 14:40 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 05/31/22 14:40 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 05/31/22 14:40 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 05/31/22 14:40 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 05/31/22 14:40 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 05/31/22 14:40 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 05/31/22 14:40 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 05/31/22 14:40 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/31/22 14:40 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 05/31/22 14:40 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 05/31/22 14:40 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 05/31/22 14:40 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 05/31/22 14:40 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 05/31/22 14:40 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/31/22 14:40 87-68-32.0 1.5 1
2-Hexanone ND ug/L 05/31/22 14:40 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 05/31/22 14:40 99-87-61.0 0.41 1
Methylene Chloride 2.0J ug/L 05/31/22 14:40 75-09-2 C0,C75.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/22 14:40 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 05/31/22 14:40 1634-04-41.0 0.42 1
Naphthalene ND ug/L 05/31/22 14:40 91-20-31.0 0.64 1
Styrene ND ug/L 05/31/22 14:40 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/22 14:40 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 78
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92606758
510621-001
Sample: TRIP BLANK Lab ID: 92606758013 Collected: 05/26/22 00:00 Received: 05/27/22 09:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 05/31/22 14:40 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 05/31/22 14:40 127-18-41.0 0.29 1
Toluene ND ug/L 05/31/22 14:40 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 05/31/22 14:40 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 05/31/22 14:40 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 05/31/22 14:40 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 05/31/22 14:40 79-00-51.0 0.32 1
Trichloroethene ND ug/L 05/31/22 14:40 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 05/31/22 14:40 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 05/31/22 14:40 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 05/31/22 14:40 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 05/31/22 14:40 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 05/31/22 14:40 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 05/31/22 14:40 179601-23-12.0 0.71 1
o-Xylene ND ug/L 05/31/22 14:40 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)104 %05/31/22 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %05/31/22 14:40 17060-07-070-130 1
Toluene-d8 (S)101 %05/31/22 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701326
EPA 3050B
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660542
Associated Lab Samples:92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 3.0 06/01/22 15:542.1
Barium mg/kg ND 1.0 06/01/22 15:540.41
Cadmium mg/kg ND 1.0 06/01/22 15:540.30
Chromium mg/kg ND 1.0 06/01/22 15:540.91
Lead mg/kg ND 2.5 06/01/22 15:541.6
Manganese mg/kg ND 4.0 06/01/22 15:540.75
Selenium mg/kg ND 5.0 06/01/22 15:544.3
Silver mg/kg ND 1.0 06/01/22 15:540.41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660543LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 98.0100 98 80-120
Barium mg/kg 102100 102 80-120
Cadmium mg/kg 104100 104 80-120
Chromium mg/kg 105100 105 80-120
Lead mg/kg 101100 101 80-120
Manganese mg/kg 104100 104 80-120
Selenium mg/kg 94.1100 94 80-120
Silver mg/kg 97.8100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660544MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606747001
3660545
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 125 82 75-12580 3 20133ND103 107
Barium mg/kg 125 105 75-125101 2 2013325.8 157 160
Cadmium mg/kg 125 104 75-12599 0 20133ND131 131
Chromium mg/kg 125 102 75-125100 3 2013336.0 164 169
Lead mg/kg 125 124 75-125116 1 2013338.8 194 193
Manganese mg/kg 125 105 75-125103 2 20133182314 319
Selenium mg/kg M1,R11255075-12559 21 20133ND63.2 77.8
Silver mg/kg 125 98 75-12595 2 20133ND123 126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701327
EPA 3005A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92606758012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660556
Associated Lab Samples:92606758012
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 5.0 06/01/22 19:232.2
Barium ug/L ND 5.0 06/01/22 19:230.67
Cadmium ug/L ND 0.50 06/01/22 19:230.11
Chromium ug/L ND 5.0 06/01/22 19:231.1
Lead ug/L ND 1.0 06/01/22 19:230.89
Manganese ug/L ND 10.0 06/01/22 19:231.1
Selenium ug/L ND 5.0 06/01/22 19:231.4
Silver ug/L ND 5.0 06/01/22 19:230.44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660557LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 97.4100 97 80-120
Barium ug/L 96.6100 97 80-120
Cadmium ug/L 96.6100 97 80-120
Chromium ug/L 91.0100 91 80-120
Lead ug/L 96.3100 96 80-120
Manganese ug/L 93.3100 93 80-120
Selenium ug/L 97.4100 97 80-120
Silver ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606541003
3660559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 100 102 75-12598 3 20100ND105 101
Barium ug/L 100 98 75-12589 4 20100119217 208
Cadmium ug/L 100 100 75-12595 5 20100ND100 94.8
Chromium ug/L 100 107 75-125100 7 20100ND108 101
Lead ug/L 100 102 75-12595 6 20100ND103 96.9
Manganese ug/L 100 109 75-12597 6 2010087.8 197 185
Selenium ug/L 100 97 75-12595 3 20100ND97.9 95.3
Silver ug/L 100 103 75-12599 4 20100ND103 99.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702443
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92606758012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3665839
Associated Lab Samples:92606758012
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/06/22 14:280.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665840LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3665841MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605559002
3665842
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 94 75-12595 1 202.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701357
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660700
Associated Lab Samples:92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.23 06/01/22 07:530.0096
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660701LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.260.32 82 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660702MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605803001
3660703
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.32 115 75-12570 200.34ND 0.38 0.25J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701051
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758001, 92606758002, 92606758003, 92606758004, 92606758005, 92606758011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3659413
Associated Lab Samples:92606758001, 92606758002, 92606758003, 92606758004, 92606758005, 92606758011
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/01/22 02:031.9
1,1,1-Trichloroethane ug/kg ND 5.0 06/01/22 02:032.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/01/22 02:031.3
1,1,2-Trichloroethane ug/kg ND 5.0 06/01/22 02:031.7
1,1-Dichloroethane ug/kg ND 5.0 06/01/22 02:032.1
1,1-Dichloroethene ug/kg ND 5.0 06/01/22 02:032.1
1,1-Dichloropropene ug/kg ND 5.0 06/01/22 02:032.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/01/22 02:034.0
1,2,3-Trichloropropane ug/kg ND 5.0 06/01/22 02:032.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/01/22 02:034.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/01/22 02:031.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/01/22 02:031.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/01/22 02:032.2
1,2-Dichlorobenzene ug/kg ND 5.0 06/01/22 02:031.8
1,2-Dichloroethane ug/kg ND 5.0 06/01/22 02:033.3
1,2-Dichloropropane ug/kg ND 5.0 06/01/22 02:031.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/01/22 02:031.7
1,3-Dichlorobenzene ug/kg ND 5.0 06/01/22 02:031.6
1,3-Dichloropropane ug/kg ND 5.0 06/01/22 02:031.6
1,4-Dichlorobenzene ug/kg ND 5.0 06/01/22 02:031.3
2,2-Dichloropropane ug/kg ND 5.0 06/01/22 02:031.6
2-Butanone (MEK)ug/kg ND 100 06/01/22 02:0324.0
2-Chlorotoluene ug/kg ND 5.0 06/01/22 02:031.8
2-Hexanone ug/kg ND 50.0 06/01/22 02:034.8
4-Chlorotoluene ug/kg ND 5.0 06/01/22 02:030.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/01/22 02:034.8
Acetone ug/kg ND 100 06/01/22 02:0332.1
Benzene ug/kg ND 5.0 06/01/22 02:032.0
Bromobenzene ug/kg ND 5.0 06/01/22 02:031.6
Bromochloromethane ug/kg ND 5.0 06/01/22 02:031.5
Bromodichloromethane ug/kg ND 5.0 06/01/22 02:031.9
Bromoform ug/kg ND 5.0 06/01/22 02:031.8
Bromomethane ug/kg ND 10.0 06/01/22 02:037.9
Carbon tetrachloride ug/kg ND 5.0 06/01/22 02:031.9
Chlorobenzene ug/kg ND 5.0 06/01/22 02:030.96
Chloroethane ug/kg ND 10.0 06/01/22 02:033.9
Chloroform ug/kg ND 5.0 06/01/22 02:033.0
Chloromethane ug/kg ND 10.0 06/01/22 02:034.2
cis-1,2-Dichloroethene ug/kg ND 5.0 06/01/22 02:031.7
cis-1,3-Dichloropropene ug/kg ND 5.0 06/01/22 02:031.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3659413
Associated Lab Samples:92606758001, 92606758002, 92606758003, 92606758004, 92606758005, 92606758011
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 06/01/22 02:032.8
Dibromomethane ug/kg ND 5.0 06/01/22 02:031.1
Dichlorodifluoromethane ug/kg ND 10.0 v106/01/22 02:032.2
Diisopropyl ether ug/kg ND 5.0 06/01/22 02:031.4
Ethylbenzene ug/kg ND 5.0 06/01/22 02:032.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/01/22 02:038.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/01/22 02:031.7
m&p-Xylene ug/kg ND 10.0 06/01/22 02:033.4
Methyl-tert-butyl ether ug/kg ND 5.0 06/01/22 02:031.9
Methylene Chloride ug/kg ND 20.0 06/01/22 02:0313.7
n-Butylbenzene ug/kg ND 5.0 06/01/22 02:032.4
n-Propylbenzene ug/kg ND 5.0 06/01/22 02:031.8
Naphthalene ug/kg ND 5.0 06/01/22 02:032.6
o-Xylene ug/kg ND 5.0 06/01/22 02:032.2
p-Isopropyltoluene ug/kg ND 5.0 06/01/22 02:032.5
sec-Butylbenzene ug/kg ND 5.0 06/01/22 02:032.2
Styrene ug/kg ND 5.0 06/01/22 02:031.3
tert-Butylbenzene ug/kg ND 5.0 06/01/22 02:031.8
Tetrachloroethene ug/kg ND 5.0 06/01/22 02:031.6
Toluene ug/kg ND 5.0 06/01/22 02:031.4
trans-1,2-Dichloroethene ug/kg ND 5.0 06/01/22 02:031.8
trans-1,3-Dichloropropene ug/kg ND 5.0 06/01/22 02:031.7
Trichloroethene ug/kg ND 5.0 06/01/22 02:031.3
Trichlorofluoromethane ug/kg ND 5.0 06/01/22 02:032.8
Vinyl acetate ug/kg ND 50.0 06/01/22 02:033.6
Vinyl chloride ug/kg ND 10.0 06/01/22 02:032.5
Xylene (Total)ug/kg ND 10.0 06/01/22 02:032.8
1,2-Dichloroethane-d4 (S)%112 70-130 06/01/22 02:03
4-Bromofluorobenzene (S)%99 69-134 06/01/22 02:03
Toluene-d8 (S)%100 70-130 06/01/22 02:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3659414LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12701250 102 70-130
1,1,1-Trichloroethane ug/kg 12901250 103 70-130
1,1,2,2-Tetrachloroethane ug/kg 12201250 98 70-130
1,1,2-Trichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethane ug/kg 12301250 99 70-130
1,1-Dichloroethene ug/kg 13401250 107 70-130
1,1-Dichloropropene ug/kg 13401250 108 70-130
1,2,3-Trichlorobenzene ug/kg 13301250 107 65-130
1,2,3-Trichloropropane ug/kg 11701250 94 70-130
1,2,4-Trichlorobenzene ug/kg 12901250 103 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3659414LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13501250 108 70-130
1,2-Dibromo-3-chloropropane ug/kg 12501250 100 70-130
1,2-Dibromoethane (EDB)ug/kg 12301250 99 70-130
1,2-Dichlorobenzene ug/kg 12901250 103 70-130
1,2-Dichloroethane ug/kg 12001250 96 63-130
1,2-Dichloropropane ug/kg 12701250 102 70-130
1,3,5-Trimethylbenzene ug/kg 13701250 110 70-130
1,3-Dichlorobenzene ug/kg 12401250 99 70-130
1,3-Dichloropropane ug/kg 12201250 98 70-130
1,4-Dichlorobenzene ug/kg 12201250 98 70-130
2,2-Dichloropropane ug/kg 12001250 96 66-130
2-Butanone (MEK)ug/kg 24402500 98 70-130
2-Chlorotoluene ug/kg 12901250 103 70-130
2-Hexanone ug/kg 25102500 101 70-130
4-Chlorotoluene ug/kg 12801250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25602500 102 70-130
Acetone ug/kg 23702500 95 69-130
Benzene ug/kg 11901250 95 70-130
Bromobenzene ug/kg 12901250 103 70-130
Bromochloromethane ug/kg 12501250 100 70-130
Bromodichloromethane ug/kg 11101250 89 69-130
Bromoform ug/kg 13701250 110 70-130
Bromomethane ug/kg 14801250 118 52-130
Carbon tetrachloride ug/kg 13101250 105 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 14401250 115 65-130
Chloroform ug/kg 12401250 99 70-130
Chloromethane ug/kg 14701250 117 55-130
cis-1,2-Dichloroethene ug/kg 13201250 105 70-130
cis-1,3-Dichloropropene ug/kg 12901250 103 70-130
Dibromochloromethane ug/kg 12801250 103 70-130
Dibromomethane ug/kg 12801250 102 70-130
Dichlorodifluoromethane ug/kg 1610 v11250129 45-156
Diisopropyl ether ug/kg 13101250 104 70-130
Ethylbenzene ug/kg 11801250 95 70-130
Hexachloro-1,3-butadiene ug/kg 12701250 101 66-130
Isopropylbenzene (Cumene)ug/kg 13101250 104 70-130
m&p-Xylene ug/kg 25602500 102 70-130
Methyl-tert-butyl ether ug/kg 12001250 96 70-130
Methylene Chloride ug/kg 12201250 97 65-130
n-Butylbenzene ug/kg 13301250 106 67-130
n-Propylbenzene ug/kg 12701250 102 70-130
Naphthalene ug/kg 13301250 106 70-130
o-Xylene ug/kg 13501250 108 70-130
p-Isopropyltoluene ug/kg 13501250 108 67-130
sec-Butylbenzene ug/kg 13401250 107 69-130
Styrene ug/kg 14101250 113 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3659414LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13001250 104 67-130
Tetrachloroethene ug/kg 12901250 103 70-130
Toluene ug/kg 11901250 95 70-130
trans-1,2-Dichloroethene ug/kg 13301250 106 70-130
trans-1,3-Dichloropropene ug/kg 12901250 103 68-130
Trichloroethene ug/kg 13101250 105 70-130
Trichlorofluoromethane ug/kg 13001250 104 70-130
Vinyl acetate ug/kg 26302500 105 70-130
Vinyl chloride ug/kg 14801250 119 61-130
Xylene (Total)ug/kg 39003750 104 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3659415MATRIX SPIKE SAMPLE:
MSSpike
Result
92606758001
1,1,1,2-Tetrachloroethane ug/kg 408 M166461 70-131ND
1,1,1-Trichloroethane ug/kg 415 M166463 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 382 M166458 66-130ND
1,1,2-Trichloroethane ug/kg 372 M166456 66-133ND
1,1-Dichloroethane ug/kg 383 M166458 65-130ND
1,1-Dichloroethene ug/kg 418664 63 10-158ND
1,1-Dichloropropene ug/kg 434 M166465 68-133ND
1,2,3-Trichlorobenzene ug/kg 411664 62 27-138ND
1,2,3-Trichloropropane ug/kg 348 M166453 67-130ND
1,2,4-Trichlorobenzene ug/kg 411664 62 51-134ND
1,2,4-Trimethylbenzene ug/kg 406 M166461 63-1363.9J
1,2-Dibromo-3-chloropropane ug/kg 327664 49 32-130ND
1,2-Dibromoethane (EDB)ug/kg 384 M166458 70-130ND
1,2-Dichlorobenzene ug/kg 410 M166462 69-130ND
1,2-Dichloroethane ug/kg 368 M166455 59-130ND
1,2-Dichloropropane ug/kg 405 M166461 70-130ND
1,3,5-Trimethylbenzene ug/kg 404 M166461 65-137ND
1,3-Dichlorobenzene ug/kg 400 M166460 70-130ND
1,3-Dichloropropane ug/kg 386 M166458 70-130ND
1,4-Dichlorobenzene ug/kg 370 M166456 68-130ND
2,2-Dichloropropane ug/kg 344664 52 32-130ND
2-Butanone (MEK)ug/kg 5881320 44 10-136ND
2-Chlorotoluene ug/kg 392 M166459 69-141ND
2-Hexanone ug/kg 6771320 51 10-144ND
4-Chlorotoluene ug/kg 387 M166458 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 6781320 51 25-143ND
Acetone ug/kg 4631320 35 10-130ND
Benzene ug/kg 400 M166460 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3659415MATRIX SPIKE SAMPLE:
MSSpike
Result
92606758001
Bromobenzene ug/kg 403 M166461 70-130ND
Bromochloromethane ug/kg 358 M166454 69-134ND
Bromodichloromethane ug/kg 337 M166451 64-130ND
Bromoform ug/kg 381 M166457 62-130ND
Bromomethane ug/kg 239664 36 20-176ND
Carbon tetrachloride ug/kg 437664 66 65-140ND
Chlorobenzene ug/kg 407 M166461 70-130ND
Chloroethane ug/kg 123664 19 10-130ND
Chloroform ug/kg 371 M166456 63-130ND
Chloromethane ug/kg 498664 75 58-130ND
cis-1,2-Dichloroethene ug/kg 416 M166463 66-130ND
cis-1,3-Dichloropropene ug/kg 375 M166457 67-130ND
Dibromochloromethane ug/kg 367 M166455 67-130ND
Dibromomethane ug/kg 389 M166459 63-131ND
Dichlorodifluoromethane ug/kg 584 v166488 44-180ND
Diisopropyl ether ug/kg 399 M166460 63-130ND
Ethylbenzene ug/kg 383 M166458 66-130ND
Hexachloro-1,3-butadiene ug/kg 440664 66 64-150ND
Isopropylbenzene (Cumene)ug/kg 408 M166461 69-135ND
m&p-Xylene ug/kg 8211320 62 60-133ND
Methyl-tert-butyl ether ug/kg 344 M166452 65-130ND
Methylene Chloride ug/kg 327 M166449 61-130ND
n-Butylbenzene ug/kg 386 M166458 65-140ND
n-Propylbenzene ug/kg 379 M166457 67-140ND
Naphthalene ug/kg 389664 56 15-14514.4
o-Xylene ug/kg 424 M166464 66-133ND
p-Isopropyltoluene ug/kg 400664 60 56-147ND
sec-Butylbenzene ug/kg 414 M166462 65-139ND
Styrene ug/kg 407 M166461 70-132ND
tert-Butylbenzene ug/kg 391 M166459 62-135ND
Tetrachloroethene ug/kg 408 M166461 70-135ND
Toluene ug/kg 389 M166458 67-1306.1J
trans-1,2-Dichloroethene ug/kg 410 M166462 69-130ND
trans-1,3-Dichloropropene ug/kg 361 M166454 62-130ND
Trichloroethene ug/kg 438 M166466 70-135ND
Trichlorofluoromethane ug/kg 158664 24 10-130ND
Vinyl acetate ug/kg 675 M1132051 53-130ND
Vinyl chloride ug/kg 453664 68 61-148ND
Xylene (Total)ug/kg 1250 MS199063 63-132ND
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606758002
3659416SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 11.1 4 3010.6
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 6.1J 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606758002
3659416SAMPLE DUPLICATE:
m&p-Xylene ug/kg 25.0 5 3023.6
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 37.1 12 3032.8
o-Xylene ug/kg 14.9 11 3013.3
p-Isopropyltoluene ug/kg ND 304.9J
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 18.1 6 3017.1
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 39.8 7 3037.0
1,2-Dichloroethane-d4 (S)%100105
4-Bromofluorobenzene (S)%102102
Toluene-d8 (S)%100102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701304
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758012, 92606758013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660444
Associated Lab Samples:92606758012, 92606758013
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/31/22 14:030.31
1,1,1-Trichloroethane ug/L ND 1.0 05/31/22 14:030.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/31/22 14:030.22
1,1,2-Trichloroethane ug/L ND 1.0 05/31/22 14:030.32
1,1-Dichloroethane ug/L ND 1.0 05/31/22 14:030.37
1,1-Dichloroethene ug/L ND 1.0 05/31/22 14:030.35
1,1-Dichloropropene ug/L ND 1.0 05/31/22 14:030.43
1,2,3-Trichlorobenzene ug/L ND 1.0 05/31/22 14:030.81
1,2,3-Trichloropropane ug/L ND 1.0 05/31/22 14:030.26
1,2,4-Trichlorobenzene ug/L ND 1.0 05/31/22 14:030.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/31/22 14:030.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/31/22 14:030.27
1,2-Dichlorobenzene ug/L ND 1.0 05/31/22 14:030.34
1,2-Dichloroethane ug/L ND 1.0 05/31/22 14:030.32
1,2-Dichloropropane ug/L ND 1.0 05/31/22 14:030.36
1,3-Dichlorobenzene ug/L ND 1.0 05/31/22 14:030.34
1,3-Dichloropropane ug/L ND 1.0 05/31/22 14:030.28
1,4-Dichlorobenzene ug/L ND 1.0 05/31/22 14:030.33
2,2-Dichloropropane ug/L ND 1.0 05/31/22 14:030.39
2-Butanone (MEK)ug/L ND 5.0 05/31/22 14:034.0
2-Chlorotoluene ug/L ND 1.0 05/31/22 14:030.32
2-Hexanone ug/L ND 5.0 05/31/22 14:030.48
4-Chlorotoluene ug/L ND 1.0 05/31/22 14:030.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/31/22 14:032.7
Acetone ug/L ND 25.0 05/31/22 14:035.1
Benzene ug/L ND 1.0 05/31/22 14:030.34
Bromobenzene ug/L ND 1.0 05/31/22 14:030.29
Bromochloromethane ug/L ND 1.0 05/31/22 14:030.47
Bromodichloromethane ug/L ND 1.0 05/31/22 14:030.31
Bromoform ug/L ND 1.0 05/31/22 14:030.34
Bromomethane ug/L ND 2.0 05/31/22 14:031.7
Carbon tetrachloride ug/L ND 1.0 05/31/22 14:030.33
Chlorobenzene ug/L ND 1.0 05/31/22 14:030.28
Chloroethane ug/L ND 1.0 05/31/22 14:030.65
Chloroform ug/L 3.0 1.0 05/31/22 14:030.43
Chloromethane ug/L ND 1.0 05/31/22 14:030.54
cis-1,2-Dichloroethene ug/L ND 1.0 05/31/22 14:030.38
cis-1,3-Dichloropropene ug/L ND 1.0 05/31/22 14:030.36
Dibromochloromethane ug/L ND 1.0 05/31/22 14:030.36
Dibromomethane ug/L ND 1.0 05/31/22 14:030.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660444
Associated Lab Samples:92606758012, 92606758013
Matrix: Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 05/31/22 14:030.35
Diisopropyl ether ug/L ND 1.0 05/31/22 14:030.31
Ethylbenzene ug/L ND 1.0 05/31/22 14:030.30
Hexachloro-1,3-butadiene ug/L ND 2.0 05/31/22 14:031.5
m&p-Xylene ug/L ND 2.0 05/31/22 14:030.71
Methyl-tert-butyl ether ug/L ND 1.0 05/31/22 14:030.42
Methylene Chloride ug/L ND 5.0 05/31/22 14:032.0
Naphthalene ug/L ND 1.0 05/31/22 14:030.64
o-Xylene ug/L ND 1.0 05/31/22 14:030.34
p-Isopropyltoluene ug/L ND 1.0 05/31/22 14:030.41
Styrene ug/L ND 1.0 05/31/22 14:030.29
Tetrachloroethene ug/L ND 1.0 05/31/22 14:030.29
Toluene ug/L ND 1.0 05/31/22 14:030.48
trans-1,2-Dichloroethene ug/L ND 1.0 05/31/22 14:030.40
trans-1,3-Dichloropropene ug/L ND 1.0 05/31/22 14:030.36
Trichloroethene ug/L ND 1.0 05/31/22 14:030.38
Trichlorofluoromethane ug/L ND 1.0 05/31/22 14:030.30
Vinyl acetate ug/L ND 2.0 05/31/22 14:031.3
Vinyl chloride ug/L ND 1.0 05/31/22 14:030.39
Xylene (Total)ug/L ND 1.0 05/31/22 14:030.34
1,2-Dichloroethane-d4 (S)%109 70-130 05/31/22 14:03
4-Bromofluorobenzene (S)%100 70-130 05/31/22 14:03
Toluene-d8 (S)%100 70-130 05/31/22 14:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660445LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.350 95 70-130
1,1,1-Trichloroethane ug/L 49.950 100 70-130
1,1,2,2-Tetrachloroethane ug/L 45.450 91 70-130
1,1,2-Trichloroethane ug/L 46.650 93 70-130
1,1-Dichloroethane ug/L 47.150 94 70-130
1,1-Dichloroethene ug/L 50.950 102 70-132
1,1-Dichloropropene ug/L 48.850 98 70-131
1,2,3-Trichlorobenzene ug/L 45.750 91 70-134
1,2,3-Trichloropropane ug/L 44.750 89 70-130
1,2,4-Trichlorobenzene ug/L 46.350 93 70-130
1,2-Dibromo-3-chloropropane ug/L 45.050 90 70-132
1,2-Dibromoethane (EDB)ug/L 48.350 97 70-130
1,2-Dichlorobenzene ug/L 44.550 89 70-130
1,2-Dichloroethane ug/L 49.350 99 70-130
1,2-Dichloropropane ug/L 46.950 94 70-130
1,3-Dichlorobenzene ug/L 44.750 89 70-130
1,3-Dichloropropane ug/L 44.850 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660445LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 43.750 87 70-130
2,2-Dichloropropane ug/L 48.950 98 70-130
2-Butanone (MEK)ug/L 102100 102 70-133
2-Chlorotoluene ug/L 43.850 88 70-130
2-Hexanone ug/L 98.3100 98 70-130
4-Chlorotoluene ug/L 44.450 89 70-130
4-Methyl-2-pentanone (MIBK)ug/L 96.2100 96 70-130
Acetone ug/L 99.3100 99 70-144
Benzene ug/L 42.750 85 70-130
Bromobenzene ug/L 44.850 90 70-130
Bromochloromethane ug/L 46.350 93 70-130
Bromodichloromethane ug/L 49.050 98 70-130
Bromoform ug/L 49.550 99 70-131
Bromomethane ug/L 50.250 100 30-177
Carbon tetrachloride ug/L 47.250 94 70-130
Chlorobenzene ug/L 46.450 93 70-130
Chloroethane ug/L 55.150 110 46-131
Chloroform ug/L 47.650 95 70-130
Chloromethane ug/L 56.950 114 49-130
cis-1,2-Dichloroethene ug/L 48.350 97 70-130
cis-1,3-Dichloropropene ug/L 48.250 96 70-130
Dibromochloromethane ug/L 49.250 98 70-130
Dibromomethane ug/L 48.450 97 70-130
Dichlorodifluoromethane ug/L 52.850 106 52-134
Diisopropyl ether ug/L 49.650 99 70-131
Ethylbenzene ug/L 46.150 92 70-130
Hexachloro-1,3-butadiene ug/L 49.850 100 70-131
m&p-Xylene ug/L 93.0100 93 70-130
Methyl-tert-butyl ether ug/L 47.950 96 70-130
Methylene Chloride ug/L 51.850 104 68-130
Naphthalene ug/L 45.950 92 70-133
o-Xylene ug/L 46.350 93 70-130
p-Isopropyltoluene ug/L 45.850 92 70-130
Styrene ug/L 47.750 95 70-130
Tetrachloroethene ug/L 47.850 96 70-130
Toluene ug/L 44.850 90 70-130
trans-1,2-Dichloroethene ug/L 49.050 98 70-130
trans-1,3-Dichloropropene ug/L 48.450 97 70-130
Trichloroethene ug/L 47.850 96 70-130
Trichlorofluoromethane ug/L 45.350 91 61-130
Vinyl acetate ug/L 104100 104 70-140
Vinyl chloride ug/L 51.550 103 59-142
Xylene (Total)ug/L 139150 93 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3660447MATRIX SPIKE SAMPLE:
MSSpike
Result
92606804002
1,1,1,2-Tetrachloroethane ug/L 21.620 108 70-135ND
1,1,1-Trichloroethane ug/L 22.720 113 70-148ND
1,1,2,2-Tetrachloroethane ug/L 20.420 102 70-131ND
1,1,2-Trichloroethane ug/L 21.420 107 70-136ND
1,1-Dichloroethane ug/L 21.520 107 70-147ND
1,1-Dichloroethene ug/L 22.920 114 70-158ND
1,1-Dichloropropene ug/L 23.520 118 70-149ND
1,2,3-Trichlorobenzene ug/L 19.620 98 68-140ND
1,2,3-Trichloropropane ug/L 19.820 99 67-137ND
1,2,4-Trichlorobenzene ug/L 20.220 101 70-139ND
1,2-Dibromo-3-chloropropane ug/L 20.020 100 69-136ND
1,2-Dibromoethane (EDB)ug/L 20.920 105 70-137ND
1,2-Dichlorobenzene ug/L 20.720 103 70-133ND
1,2-Dichloroethane ug/L 21.420 107 67-138ND
1,2-Dichloropropane ug/L 21.520 108 70-138ND
1,3-Dichlorobenzene ug/L 20.920 104 70-133ND
1,3-Dichloropropane ug/L 21.320 107 70-136ND
1,4-Dichlorobenzene ug/L 21.320 106 70-133ND
2,2-Dichloropropane ug/L 22.820 114 52-155ND
2-Butanone (MEK)ug/L 44.740 112 61-147ND
2-Chlorotoluene ug/L 21.920 110 70-141ND
2-Hexanone ug/L 44.140 110 67-139ND
4-Chlorotoluene ug/L 21.920 109 70-135ND
4-Methyl-2-pentanone (MIBK)ug/L 44.840 112 67-136ND
Acetone ug/L 42.540 106 55-159ND
Benzene ug/L 21.220 106 67-150ND
Bromobenzene ug/L 21.320 106 70-134ND
Bromochloromethane ug/L 20.720 103 70-146ND
Bromodichloromethane ug/L 21.720 108 70-138ND
Bromoform ug/L 20.720 103 57-138ND
Bromomethane ug/L 20.1 v320101 10-200ND
Carbon tetrachloride ug/L 22.920 115 70-147ND
Chlorobenzene ug/L 21.720 108 70-137ND
Chloroethane ug/L 25.220 126 51-166ND
Chloroform ug/L 22.420 112 70-144ND
Chloromethane ug/L 23.7 v320119 24-161ND
cis-1,2-Dichloroethene ug/L 22.420 112 67-148ND
cis-1,3-Dichloropropene ug/L 21.920 110 70-142ND
Dibromochloromethane ug/L 20.620 103 68-138ND
Dibromomethane ug/L 20.020 100 70-134ND
Dichlorodifluoromethane ug/L 24.3 v320121 43-155ND
Diisopropyl ether ug/L 22.220 111 65-146ND
Ethylbenzene ug/L 21.720 108 68-143ND
Hexachloro-1,3-butadiene ug/L 21.020 105 62-151ND
m&p-Xylene ug/L 44.140 110 53-157ND
Methyl-tert-butyl ether ug/L 19.720 98 59-156ND
Methylene Chloride ug/L 19.420 97 64-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3660447MATRIX SPIKE SAMPLE:
MSSpike
Result
92606804002
Naphthalene ug/L 20.420 102 57-150ND
o-Xylene ug/L 21.520 107 68-143ND
p-Isopropyltoluene ug/L 22.720 113 70-141ND
Styrene ug/L 21.920 110 70-136ND
Tetrachloroethene ug/L 23.020 115 70-139ND
Toluene ug/L 21.520 108 47-157ND
trans-1,2-Dichloroethene ug/L 23.320 117 70-149ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-138ND
Trichloroethene ug/L 21.520 108 70-149ND
Trichlorofluoromethane ug/L 21.320 106 61-154ND
Vinyl acetate ug/L 45.540 114 48-156ND
Vinyl chloride ug/L 23.620 118 55-172ND
Xylene (Total)ug/L 65.560 109 66-145ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606804001
3660446SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606804001
3660446SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND v230ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND v230ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%100110
4-Bromofluorobenzene (S)%100100
Toluene-d8 (S)%10199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701229
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660129
Associated Lab Samples:92606758012
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 05/31/22 13:271.7
1,2-Dichlorobenzene ug/L ND 10.0 05/31/22 13:271.8
1,3-Dichlorobenzene ug/L ND 10.0 05/31/22 13:271.6
1,4-Dichlorobenzene ug/L ND 10.0 05/31/22 13:271.7
1-Methylnaphthalene ug/L ND 10.0 05/31/22 13:272.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 05/31/22 13:271.2
2,4,5-Trichlorophenol ug/L ND 10.0 05/31/22 13:271.4
2,4,6-Trichlorophenol ug/L ND 10.0 05/31/22 13:271.6
2,4-Dichlorophenol ug/L ND 10.0 05/31/22 13:271.4
2,4-Dimethylphenol ug/L ND 10.0 05/31/22 13:271.7
2,4-Dinitrophenol ug/L ND 50.0 05/31/22 13:2726.0
2,4-Dinitrotoluene ug/L ND 10.0 05/31/22 13:271.6
2,6-Dinitrotoluene ug/L ND 10.0 05/31/22 13:271.7
2-Chloronaphthalene ug/L ND 10.0 05/31/22 13:271.7
2-Chlorophenol ug/L ND 10.0 05/31/22 13:271.2
2-Methylnaphthalene ug/L ND 10.0 05/31/22 13:271.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 05/31/22 13:271.9
2-Nitroaniline ug/L ND 20.0 05/31/22 13:273.0
2-Nitrophenol ug/L ND 10.0 05/31/22 13:271.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 05/31/22 13:271.2
3,3'-Dichlorobenzidine ug/L ND 20.0 05/31/22 13:278.1
3-Nitroaniline ug/L ND 20.0 05/31/22 13:273.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/31/22 13:277.8
4-Bromophenylphenyl ether ug/L ND 10.0 05/31/22 13:271.8
4-Chloro-3-methylphenol ug/L ND 10.0 05/31/22 13:273.3
4-Chloroaniline ug/L ND 20.0 05/31/22 13:273.6
4-Chlorophenylphenyl ether ug/L ND 10.0 05/31/22 13:272.0
4-Nitroaniline ug/L ND 20.0 05/31/22 13:275.1
4-Nitrophenol ug/L ND 50.0 05/31/22 13:276.6
Acenaphthene ug/L ND 10.0 05/31/22 13:272.0
Acenaphthylene ug/L ND 10.0 05/31/22 13:272.0
Aniline ug/L ND 10.0 05/31/22 13:271.6
Anthracene ug/L ND 10.0 05/31/22 13:272.3
Benzo(a)anthracene ug/L ND 10.0 05/31/22 13:272.7
Benzo(a)pyrene ug/L ND 10.0 05/31/22 13:272.8
Benzo(b)fluoranthene ug/L ND 10.0 05/31/22 13:272.6
Benzo(g,h,i)perylene ug/L ND 10.0 05/31/22 13:272.8
Benzo(k)fluoranthene ug/L ND 10.0 05/31/22 13:272.7
Benzoic Acid ug/L ND 50.0 05/31/22 13:2722.0
Benzyl alcohol ug/L ND 20.0 05/31/22 13:272.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3660129
Associated Lab Samples:92606758012
Matrix: Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/31/22 13:271.8
bis(2-Chloroethyl) ether ug/L ND 10.0 05/31/22 13:271.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 05/31/22 13:273.7
Butylbenzylphthalate ug/L ND 10.0 05/31/22 13:273.1
Chrysene ug/L ND 10.0 05/31/22 13:272.8
Di-n-butylphthalate ug/L ND 10.0 05/31/22 13:272.2
Di-n-octylphthalate ug/L ND 10.0 05/31/22 13:273.9
Dibenz(a,h)anthracene ug/L ND 10.0 05/31/22 13:273.0
Dibenzofuran ug/L ND 10.0 05/31/22 13:272.1
Diethylphthalate ug/L ND 10.0 05/31/22 13:272.0
Dimethylphthalate ug/L ND 10.0 05/31/22 13:272.1
Fluoranthene ug/L ND 10.0 05/31/22 13:272.2
Fluorene ug/L ND 10.0 05/31/22 13:272.1
Hexachloro-1,3-butadiene ug/L ND 10.0 05/31/22 13:271.8
Hexachlorobenzene ug/L ND 10.0 05/31/22 13:272.2
Hexachlorocyclopentadiene ug/L ND 10.0 05/31/22 13:271.6
Hexachloroethane ug/L ND 10.0 05/31/22 13:271.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 05/31/22 13:272.9
Isophorone ug/L ND 10.0 05/31/22 13:271.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 05/31/22 13:271.3
N-Nitrosodimethylamine ug/L ND 10.0 05/31/22 13:271.9
N-Nitrosodiphenylamine ug/L ND 10.0 05/31/22 13:273.0
Naphthalene ug/L ND 10.0 05/31/22 13:272.1
Nitrobenzene ug/L ND 10.0 05/31/22 13:271.9
Pentachlorophenol ug/L ND 20.0 v205/31/22 13:273.8
Phenanthrene ug/L ND 10.0 05/31/22 13:272.0
Phenol ug/L ND 10.0 05/31/22 13:271.4
Pyrene ug/L ND 10.0 05/31/22 13:272.2
2,4,6-Tribromophenol (S)%102 10-144 05/31/22 13:27
2-Fluorobiphenyl (S)%89 10-130 05/31/22 13:27
2-Fluorophenol (S)%73 10-130 05/31/22 13:27
Nitrobenzene-d5 (S)%111 10-144 05/31/22 13:27
Phenol-d6 (S)%57 10-130 05/31/22 13:27
Terphenyl-d14 (S)%142 34-163 05/31/22 13:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660130LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 31.950 64 18-130
1,2-Dichlorobenzene ug/L 31.950 64 20-130
1,3-Dichlorobenzene ug/L 31.350 63 18-130
1,4-Dichlorobenzene ug/L 32.050 64 18-130
1-Methylnaphthalene ug/L 39.750 79 29-130
2,2'-Oxybis(1-chloropropane)ug/L 41.750 83 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660130LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 53.650 107 35-130
2,4,6-Trichlorophenol ug/L 48.250 96 31-130
2,4-Dichlorophenol ug/L 57.650 115 35-130
2,4-Dimethylphenol ug/L 56.150 112 34-130
2,4-Dinitrophenol ug/L 295250 118 10-153
2,4-Dinitrotoluene ug/L 64.650 129 37-136
2,6-Dinitrotoluene ug/L 61.750 123 33-136
2-Chloronaphthalene ug/L 44.950 90 26-130
2-Chlorophenol ug/L 47.150 94 37-130
2-Methylnaphthalene ug/L 41.250 82 29-130
2-Methylphenol(o-Cresol)ug/L 49.550 99 35-130
2-Nitroaniline ug/L 116100 116 37-130
2-Nitrophenol ug/L 53.550 107 32-130
3&4-Methylphenol(m&p Cresol)ug/L 43.850 88 34-130
3,3'-Dichlorobenzidine ug/L 99.5100 100 34-136
3-Nitroaniline ug/L 107100 107 37-138
4,6-Dinitro-2-methylphenol ug/L 107100 107 21-157
4-Bromophenylphenyl ether ug/L 52.450 105 38-130
4-Chloro-3-methylphenol ug/L 114100 114 37-130
4-Chloroaniline ug/L 96.5100 97 38-130
4-Chlorophenylphenyl ether ug/L 52.150 104 33-130
4-Nitroaniline ug/L 115100 115 42-137
4-Nitrophenol ug/L 160250 64 10-130
Acenaphthene ug/L 46.350 93 33-130
Acenaphthylene ug/L 48.050 96 35-130
Aniline ug/L 44.950 90 22-130
Anthracene ug/L 47.050 94 48-130
Benzo(a)anthracene ug/L 54.550 109 48-137
Benzo(a)pyrene ug/L 62.650 125 49-138
Benzo(b)fluoranthene ug/L 60.650 121 52-138
Benzo(g,h,i)perylene ug/L 58.250 116 48-140
Benzo(k)fluoranthene ug/L 59.150 118 48-139
Benzoic Acid ug/L 129250 51 10-130
Benzyl alcohol ug/L 94.3100 94 35-130
bis(2-Chloroethoxy)methane ug/L 56.750 113 34-130
bis(2-Chloroethyl) ether ug/L 50.150 100 36-130
bis(2-Ethylhexyl)phthalate ug/L 62.250 124 32-165
Butylbenzylphthalate ug/L 60.750 121 34-161
Chrysene ug/L 51.150 102 47-131
Di-n-butylphthalate ug/L 57.350 115 39-144
Di-n-octylphthalate ug/L 53.050 106 30-170
Dibenz(a,h)anthracene ug/L 63.850 128 49-138
Dibenzofuran ug/L 51.750 103 33-130
Diethylphthalate ug/L 56.650 113 38-131
Dimethylphthalate ug/L 55.250 110 37-130
Fluoranthene ug/L 54.850 110 46-137
Fluorene ug/L 52.650 105 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3660130LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 26.850 54 11-130
Hexachlorobenzene ug/L 49.050 98 38-130
Hexachlorocyclopentadiene ug/L 31.350 63 10-130
Hexachloroethane ug/L 28.950 58 14-130
Indeno(1,2,3-cd)pyrene ug/L 60.950 122 41-130
Isophorone ug/L 47.050 94 33-130
N-Nitroso-di-n-propylamine ug/L 57.050 114 36-130
N-Nitrosodimethylamine ug/L 40.050 80 34-130
N-Nitrosodiphenylamine ug/L 50.950 102 37-130
Naphthalene ug/L 37.150 74 30-130
Nitrobenzene ug/L 53.250 106 36-130
Pentachlorophenol ug/L 82.6 v310083 23-149
Phenanthrene ug/L 51.750 103 44-130
Phenol ug/L 33.150 66 18-130
Pyrene ug/L 54.450 109 47-134
2,4,6-Tribromophenol (S)%125 10-144
2-Fluorobiphenyl (S)%105 10-130
2-Fluorophenol (S)%85 10-130
Nitrobenzene-d5 (S)%122 10-144
Phenol-d6 (S)%77 10-130
Terphenyl-d14 (S)%143 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660131MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605187011
3660132
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 47 10-13044 7 3050ND23.4 21.9
1,2-Dichlorobenzene ug/L 50 38 10-13045 17 3050ND18.8 22.4
1,3-Dichlorobenzene ug/L 50 34 10-13043 23 3050ND17.0 21.3
1,4-Dichlorobenzene ug/L 50 37 10-13044 18 3050ND18.3 21.9
1-Methylnaphthalene ug/L 50 64 10-13062 4 3050ND32.1 30.9
2,2'-Oxybis(1-chloropropane)ug/L 50 59 12-14258 2 3050ND29.7 29.1
2,4,5-Trichlorophenol ug/L 50 18 10-14319 3050ND9.2J 9.5J
2,4,6-Trichlorophenol ug/L M1501110-1479 3050ND5.3J 4.7J
2,4-Dichlorophenol ug/L 50 44 10-13847 7 3050ND22.0 23.7
2,4-Dimethylphenol ug/L 50 83 25-13088 6 3050ND41.3 44.1
2,4-Dinitrophenol ug/L M1250810-1657 30250NDND ND
2,4-Dinitrotoluene ug/L 50 108 29-148113 5 3050ND54.2 56.7
2,6-Dinitrotoluene ug/L 50 108 26-146116 7 3050ND54.1 57.9
2-Chloronaphthalene ug/L 50 74 11-13071 3 3050ND37.0 35.7
2-Chlorophenol ug/L 50 40 10-13337 7 3050ND19.9 18.5
2-Methylnaphthalene ug/L 50 64 13-13063 3 3050ND32.2 31.3
2-Methylphenol(o-Cresol) ug/L 50 74 20-13075 1 3050ND37.0 37.5
2-Nitroaniline ug/L 100 99 24-136103 3 30100ND99.4 103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660131MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605187011
3660132
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 50 42 10-15343 1 3050ND21.1 21.4
3&4-Methylphenol(m&p
Cresol)ug/L 50 65 16-13066 1 3050ND32.5 32.8
3,3'-Dichlorobenzidine ug/L 100 88 10-15393 5 30100ND88.5 92.7
3-Nitroaniline ug/L 100 97 22-151103 6 30100ND96.9 103
4,6-Dinitro-2-methylphenol ug/L 100 30 10-18030 2 30100ND30.1 29.6
4-Bromophenylphenyl ether ug/L 50 95 25-130102 7 3050ND47.6 51.1
4-Chloro-3-methylphenol ug/L 100 96 25-133102 6 30100ND95.7 102
4-Chloroaniline ug/L 100 73 14-13277 5 30100ND73.3 76.8
4-Chlorophenylphenyl ether ug/L 50 90 19-13091 1 3050ND45.1 45.7
4-Nitroaniline ug/L 100 100 29-150110 10 30100ND99.8 110
4-Nitrophenol ug/L M1250010-1300 30250NDND ND
Acenaphthene ug/L 50 76 16-13079 3 3050ND38.2 39.6
Acenaphthylene ug/L 50 79 15-13779 1 3050ND39.7 39.5
Aniline ug/L 50 63 10-13060 6 3050ND31.7 30.0
Anthracene ug/L 50 86 37-13690 5 3050ND42.8 45.0
Benzo(a)anthracene ug/L 50 100 40-145111 11 3050ND49.9 55.7
Benzo(a)pyrene ug/L 50 115 41-146127 10 3050ND57.6 63.7
Benzo(b)fluoranthene ug/L 50 113 39-151124 9 3050ND56.5 62.0
Benzo(g,h,i)perylene ug/L 50 110 40-147119 8 3050ND55.1 59.4
Benzo(k)fluoranthene ug/L 50 103 40-146115 11 3050ND51.6 57.7
Benzoic Acid ug/L M1250010-1300 30250NDND ND
Benzyl alcohol ug/L 100 68 25-13069 0 30100ND68.3 68.5
bis(2-Chloroethoxy)methane ug/L 50 76 23-13077 2 3050ND38.0 38.6
bis(2-Chloroethyl) ether ug/L 50 69 25-13066 6 3050ND34.7 32.9
bis(2-Ethylhexyl)phthalate ug/L 50 117 28-166129 10 3050ND58.3 64.4
Butylbenzylphthalate ug/L 50 119 33-165132 11 3050ND59.5 66.2
Chrysene ug/L 50 95 38-141101 6 3050ND47.5 50.5
Di-n-butylphthalate ug/L 50 108 32-153116 8 3050ND54.0 58.2
Di-n-octylphthalate ug/L 50 101 30-175112 10 3050ND50.3 55.8
Dibenz(a,h)anthracene ug/L 50 116 39-148128 10 3050ND57.8 64.1
Dibenzofuran ug/L 50 86 20-13089 3 3050ND43.0 44.5
Diethylphthalate ug/L 50 105 28-142110 5 3050ND52.5 55.1
Dimethylphthalate ug/L 50 96 26-13698 3 3050ND47.8 49.0
Fluoranthene ug/L 50 105 39-143110 5 3050ND52.4 54.9
Fluorene ug/L 50 89 24-13292 3 3050ND44.7 45.9
Hexachloro-1,3-butadiene ug/L 50 34 10-13033 4 3050ND17.2 16.6
Hexachlorobenzene ug/L 50 86 29-13093 7 3050ND43.1 46.3
Hexachlorocyclopentadiene ug/L 50 51 10-13044 15 3050ND25.6 22.1
Hexachloroethane ug/L 50 30 10-13037 20 3050ND15.2 18.6
Indeno(1,2,3-cd)pyrene ug/L 50 112 39-148122 9 3050ND55.9 61.1
Isophorone ug/L 50 65 23-13066 2 3050ND32.3 32.9
N-Nitroso-di-n-propylamine ug/L 50 81 25-13077 5 3050ND40.3 38.5
N-Nitrosodimethylamine ug/L 50 59 22-13053 12 3050ND29.7 26.3
N-Nitrosodiphenylamine ug/L 50 93 26-13499 6 3050ND46.5 49.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3660131MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92605187011
3660132
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 50 54 14-13053 2 3050ND26.8 26.3
Nitrobenzene ug/L 50 78 25-13075 4 3050ND38.8 37.4
Pentachlorophenol ug/L M1,v2100010-1750 30100NDND ND
Phenanthrene ug/L 50 92 36-13398 5 3050ND46.2 48.8
Phenol ug/L 50 40 10-13036 9 3050ND19.8 18.1
Pyrene ug/L 50 101 40-143109 8 3050ND50.5 54.6
2,4,6-Tribromophenol (S) %14 10-14416
2-Fluorobiphenyl (S)%74 10-13077
2-Fluorophenol (S)%19 10-13013
Nitrobenzene-d5 (S)%82 10-14477
Phenol-d6 (S)%44 10-13038
Terphenyl-d14 (S)%128 34-163141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701616
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3662011
Associated Lab Samples:92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 06/02/22 10:18128
1,2-Dichlorobenzene ug/kg ND 326 06/02/22 10:18117
1,3-Dichlorobenzene ug/kg ND 326 06/02/22 10:18115
1,4-Dichlorobenzene ug/kg ND 326 06/02/22 10:18124
1-Methylnaphthalene ug/kg ND 326 06/02/22 10:18114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 v106/02/22 10:18155
2,4,5-Trichlorophenol ug/kg ND 326 06/02/22 10:18149
2,4,6-Trichlorophenol ug/kg ND 326 06/02/22 10:18134
2,4-Dichlorophenol ug/kg ND 326 06/02/22 10:18127
2,4-Dimethylphenol ug/kg ND 326 06/02/22 10:18135
2,4-Dinitrophenol ug/kg ND 1630 06/02/22 10:181010
2,4-Dinitrotoluene ug/kg ND 326 06/02/22 10:18125
2,6-Dinitrotoluene ug/kg ND 326 06/02/22 10:18119
2-Chloronaphthalene ug/kg ND 326 06/02/22 10:18129
2-Chlorophenol ug/kg ND 326 06/02/22 10:18122
2-Methylnaphthalene ug/kg ND 326 06/02/22 10:18130
2-Methylphenol(o-Cresol)ug/kg ND 326 06/02/22 10:18133
2-Nitroaniline ug/kg ND 1630 06/02/22 10:18266
2-Nitrophenol ug/kg ND 326 06/02/22 10:18141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 06/02/22 10:18131
3,3'-Dichlorobenzidine ug/kg ND 651 IL06/02/22 10:18220
3-Nitroaniline ug/kg ND 1630 IL06/02/22 10:18256
4,6-Dinitro-2-methylphenol ug/kg ND 651 06/02/22 10:18304
4-Bromophenylphenyl ether ug/kg ND 326 06/02/22 10:18125
4-Chloro-3-methylphenol ug/kg ND 651 06/02/22 10:18229
4-Chloroaniline ug/kg ND 651 06/02/22 10:18256
4-Chlorophenylphenyl ether ug/kg ND 326 06/02/22 10:18121
4-Nitroaniline ug/kg ND 651 IL06/02/22 10:18248
4-Nitrophenol ug/kg ND 1630 06/02/22 10:18630
Acenaphthene ug/kg ND 326 06/02/22 10:18114
Acenaphthylene ug/kg ND 326 06/02/22 10:18114
Aniline ug/kg ND 326 06/02/22 10:18127
Anthracene ug/kg ND 326 06/02/22 10:18107
Benzo(a)anthracene ug/kg ND 326 06/02/22 10:18109
Benzo(a)pyrene ug/kg ND 326 06/02/22 10:18112
Benzo(b)fluoranthene ug/kg ND 326 06/02/22 10:18109
Benzo(g,h,i)perylene ug/kg ND 326 06/02/22 10:18126
Benzo(k)fluoranthene ug/kg ND 326 06/02/22 10:18114
Benzoic Acid ug/kg ND 1630 06/02/22 10:18700
Benzyl alcohol ug/kg ND 651 06/02/22 10:18247
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 78
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3662011
Associated Lab Samples:92606758006, 92606758007, 92606758008, 92606758009, 92606758010, 92606758011
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 326 06/02/22 10:18135
bis(2-Chloroethyl) ether ug/kg ND 326 06/02/22 10:18122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 06/02/22 10:18126
Butylbenzylphthalate ug/kg ND 326 06/02/22 10:18137
Chrysene ug/kg ND 326 06/02/22 10:18118
Di-n-butylphthalate ug/kg ND 326 06/02/22 10:18110
Di-n-octylphthalate ug/kg ND 326 06/02/22 10:18128
Dibenz(a,h)anthracene ug/kg ND 326 06/02/22 10:18125
Dibenzofuran ug/kg ND 326 06/02/22 10:18117
Diethylphthalate ug/kg ND 326 06/02/22 10:18119
Dimethylphthalate ug/kg ND 326 06/02/22 10:18118
Fluoranthene ug/kg ND 326 06/02/22 10:18112
Fluorene ug/kg ND 326 06/02/22 10:18114
Hexachloro-1,3-butadiene ug/kg ND 326 06/02/22 10:18141
Hexachlorobenzene ug/kg ND 326 06/02/22 10:18127
Hexachlorocyclopentadiene ug/kg ND 326 06/02/22 10:18187
Hexachloroethane ug/kg ND 326 06/02/22 10:18124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 06/02/22 10:18128
Isophorone ug/kg ND 326 06/02/22 10:18145
N-Nitroso-di-n-propylamine ug/kg ND 326 06/02/22 10:18122
N-Nitrosodimethylamine ug/kg ND 326 06/02/22 10:18110
N-Nitrosodiphenylamine ug/kg ND 326 06/02/22 10:18115
Naphthalene ug/kg ND 326 06/02/22 10:18111
Nitrobenzene ug/kg ND 326 06/02/22 10:18151
Pentachlorophenol ug/kg ND 651 06/02/22 10:18319
Phenanthrene ug/kg ND 326 06/02/22 10:18107
Phenol ug/kg ND 326 06/02/22 10:18145
Pyrene ug/kg ND 326 06/02/22 10:18132
Pyridine ug/kg ND 326 06/02/22 10:18103
2,4,6-Tribromophenol (S)%73 18-130 06/02/22 10:18
2-Fluorobiphenyl (S)%51 19-130 06/02/22 10:18
2-Fluorophenol (S)%47 18-130 06/02/22 10:18
Nitrobenzene-d5 (S)%50 21-130 06/02/22 10:18
Phenol-d6 (S)%50 18-130 06/02/22 10:18
Terphenyl-d14 (S)%89 15-130 06/02/22 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3662012LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13201670 79 47-130
1,2-Dichlorobenzene ug/kg 12901670 77 49-130
1,3-Dichlorobenzene ug/kg 13101670 79 48-130
1,4-Dichlorobenzene ug/kg 13001670 78 49-130
1-Methylnaphthalene ug/kg 13801670 83 54-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3662012LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 1620 v1167097 38-130
2,4,5-Trichlorophenol ug/kg 14601670 88 49-130
2,4,6-Trichlorophenol ug/kg 14201670 85 50-130
2,4-Dichlorophenol ug/kg 14501670 87 51-130
2,4-Dimethylphenol ug/kg 13801670 83 53-130
2,4-Dinitrophenol ug/kg 78208330 94 39-130
2,4-Dinitrotoluene ug/kg 16201670 97 53-130
2,6-Dinitrotoluene ug/kg 17301670 104 55-130
2-Chloronaphthalene ug/kg 14401670 86 48-130
2-Chlorophenol ug/kg 13401670 80 54-130
2-Methylnaphthalene ug/kg 14101670 84 57-130
2-Methylphenol(o-Cresol)ug/kg 13201670 79 50-130
2-Nitroaniline ug/kg 28903330 87 49-130
2-Nitrophenol ug/kg 16501670 99 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 12101670 73 50-130
3,3'-Dichlorobenzidine ug/kg 2400 IL333072 47-130
3-Nitroaniline ug/kg 3570 IL3330107 45-130
4,6-Dinitro-2-methylphenol ug/kg 32203330 97 50-142
4-Bromophenylphenyl ether ug/kg 15701670 94 55-130
4-Chloro-3-methylphenol ug/kg 27703330 83 52-130
4-Chloroaniline ug/kg 25303330 76 49-130
4-Chlorophenylphenyl ether ug/kg 14001670 84 53-130
4-Nitroaniline ug/kg 2800 IL333084 51-130
4-Nitrophenol ug/kg 67608330 81 40-130
Acenaphthene ug/kg 14601670 88 56-130
Acenaphthylene ug/kg 14301670 86 58-130
Aniline ug/kg 11601670 70 44-130
Anthracene ug/kg 14001670 84 60-130
Benzo(a)anthracene ug/kg 15201670 91 59-130
Benzo(a)pyrene ug/kg 15301670 92 57-130
Benzo(b)fluoranthene ug/kg 14901670 89 54-130
Benzo(g,h,i)perylene ug/kg 13701670 82 59-130
Benzo(k)fluoranthene ug/kg 15401670 93 54-130
Benzoic Acid ug/kg 61208330 73 19-130
Benzyl alcohol ug/kg 24903330 75 50-130
bis(2-Chloroethoxy)methane ug/kg 13201670 79 55-130
bis(2-Chloroethyl) ether ug/kg 12301670 74 53-130
bis(2-Ethylhexyl)phthalate ug/kg 15301670 92 58-130
Butylbenzylphthalate ug/kg 17101670 103 46-138
Chrysene ug/kg 14701670 88 57-130
Di-n-butylphthalate ug/kg 15401670 93 57-130
Di-n-octylphthalate ug/kg 17501670 105 57-130
Dibenz(a,h)anthracene ug/kg 14701670 88 60-130
Dibenzofuran ug/kg 14801670 89 54-130
Diethylphthalate ug/kg 15401670 92 55-130
Dimethylphthalate ug/kg 15001670 90 57-130
Fluoranthene ug/kg 15501670 93 57-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3662012LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13501670 81 56-130
Hexachloro-1,3-butadiene ug/kg 13301670 80 41-130
Hexachlorobenzene ug/kg 15401670 92 53-130
Hexachlorocyclopentadiene ug/kg 11601670 69 23-130
Hexachloroethane ug/kg 12401670 74 48-130
Indeno(1,2,3-cd)pyrene ug/kg 14101670 85 61-130
Isophorone ug/kg 13301670 80 49-130
N-Nitroso-di-n-propylamine ug/kg 12301670 74 52-130
N-Nitrosodimethylamine ug/kg 11601670 69 45-130
N-Nitrosodiphenylamine ug/kg 15301670 92 56-130
Naphthalene ug/kg 13401670 80 56-130
Nitrobenzene ug/kg 13501670 81 50-130
Pentachlorophenol ug/kg 28003330 84 33-130
Phenanthrene ug/kg 15701670 94 60-130
Phenol ug/kg 14001670 84 54-130
Pyrene ug/kg 16401670 98 61-130
Pyridine ug/kg 9881670 59 35-130
2,4,6-Tribromophenol (S)%109 18-130
2-Fluorobiphenyl (S)%82 19-130
2-Fluorophenol (S)%76 18-130
Nitrobenzene-d5 (S)%82 21-130
Phenol-d6 (S)%83 18-130
Terphenyl-d14 (S)%96 15-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3662013MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606203003
3662014
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1880 74 22-13077 3 301860ND1390 1430
1,2-Dichlorobenzene ug/kg 1880 71 23-13072 1 301860ND1330 1340
1,3-Dichlorobenzene ug/kg 1880 72 26-13073 1 301860ND1350 1360
1,4-Dichlorobenzene ug/kg 1880 71 27-13072 2 301860ND1320 1340
1-Methylnaphthalene ug/kg 1880 75 30-13080 7 301860ND1400 1500
2,2'-Oxybis(1-
chloropropane)ug/kg 1880 67 30-13067 0 301860ND1250 1240
2,4,5-Trichlorophenol ug/kg 1880 87 26-13086 2 301860ND1630 1600
2,4,6-Trichlorophenol ug/kg 1880 86 23-13088 1 301860ND1610 1630
2,4-Dichlorophenol ug/kg 1880 81 29-13083 3 301860ND1510 1550
2,4-Dimethylphenol ug/kg 1880 80 13-13084 4 301860ND1510 1560
2,4-Dinitrophenol ug/kg 9360 36 10-13160 48 309320ND3400 5570
2,4-Dinitrotoluene ug/kg 1880 89 28-13093 4 301860ND1660 1740
2,6-Dinitrotoluene ug/kg 1880 91 36-13094 3 301860ND1700 1750
2-Chloronaphthalene ug/kg 1880 77 27-13077 1 301860ND1440 1430
2-Chlorophenol ug/kg 1880 75 29-13075 0 301860ND1400 1400
2-Methylnaphthalene ug/kg 1880 75 29-13079 4 301860ND1410 1470
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3662013MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606203003
3662014
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol) ug/kg 1880 75 20-13076 1 301860ND1400 1420
2-Nitroaniline ug/kg 3740 74 29-13076 3 303730ND2770 2850
2-Nitrophenol ug/kg v118809726-13099 2 301860ND1820 1850
3&4-Methylphenol(m&p
Cresol)ug/kg 1880 75 10-17678 3 301860ND1410 1460
3,3'-Dichlorobenzidine ug/kg IL37408615-13089 3 303730ND3210 3310
3-Nitroaniline ug/kg IL37408028-13082 3 303730ND2980 3060
4,6-Dinitro-2-methylphenol ug/kg 3740 68 15-13280 15 303730ND2560 2980
4-Bromophenylphenyl ether ug/kg 1880 86 35-13092 7 301860ND1600 1720
4-Chloro-3-methylphenol ug/kg 3740 84 30-13089 6 303730ND3150 3330
4-Chloroaniline ug/kg IL37407228-13075 4 303730ND2680 2790
4-Chlorophenylphenyl ether ug/kg 1880 79 32-13085 7 301860ND1480 1580
4-Nitroaniline ug/kg 3740 78 30-13081 3 303730ND2910 3010
4-Nitrophenol ug/kg 9360 70 17-13079 13 309320ND6520 7390
Acenaphthene ug/kg 1880 74 29-13077 3 301860ND1390 1440
Acenaphthylene ug/kg 1880 79 31-13081 1 301860ND1480 1500
Aniline ug/kg 1880 65 10-13066 2 301860ND1220 1240
Anthracene ug/kg 1880 67 33-13072 8 301860ND1250 1350
Benzo(a)anthracene ug/kg 1880 80 32-13089 11 301860ND1490 1660
Benzo(a)pyrene ug/kg 1880 74 32-13082 11 301860ND1380 1540
Benzo(b)fluoranthene ug/kg 1880 70 33-13081 14 301860ND1310 1510
Benzo(g,h,i)perylene ug/kg 1880 82 28-13090 9 301860ND1540 1670
Benzo(k)fluoranthene ug/kg 1880 68 31-13077 12 301860ND1280 1440
Benzoic Acid ug/kg 9360 10 10-13016 309320ND946J 1510J
Benzyl alcohol ug/kg 3740 73 31-13076 3 303730ND2750 2820
bis(2-
Chloroethoxy)methane ug/kg 1880 72 30-13075 4 301860ND1340 1390
bis(2-Chloroethyl) ether ug/kg 1880 67 68-13070 3 301860ND1260 1300
bis(2-Ethylhexyl)phthalate ug/kg 1880 80 40-13093 15 301860ND1490 1730
Butylbenzylphthalate ug/kg 1880 81 40-13094 14 301860ND1520 1750
Chrysene ug/kg 1880 76 30-13083 9 301860ND1420 1550
Di-n-butylphthalate ug/kg 1880 76 41-13087 13 301860ND1430 1620
Di-n-octylphthalate ug/kg v118809742-130109 12 301860ND1820 2040
Dibenz(a,h)anthracene ug/kg 1880 85 27-13093 8 301860ND1600 1730
Dibenzofuran ug/kg 1880 77 32-13081 5 301860ND1440 1510
Diethylphthalate ug/kg v118808240-13085 3 301860ND1530 1590
Dimethylphthalate ug/kg 1880 84 37-13086 2 301860ND1570 1600
Fluoranthene ug/kg 1880 81 26-13091 11 301860ND1510 1690
Fluorene ug/kg 1880 76 31-13081 5 301860ND1430 1510
Hexachloro-1,3-butadiene ug/kg 1880 78 20-13081 4 301860ND1450 1510
Hexachlorobenzene ug/kg 1880 88 29-13095 8 301860ND1640 1780
Hexachlorocyclopentadiene ug/kg v318804810-13048 1 301860ND905 893
Hexachloroethane ug/kg 1880 71 21-13071 0 301860ND1320 1330
Indeno(1,2,3-cd)pyrene ug/kg 1880 83 28-13091 9 301860ND1540 1690
Isophorone ug/kg 1880 71 32-13074 4 301860ND1320 1380
N-Nitroso-di-n-propylamine ug/kg 1880 70 31-13071 1 301860ND1310 1320
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/07/2022 05:37 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3662013MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606203003
3662014
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 1880 66 20-13069 5 301860ND1230 1290
N-Nitrosodiphenylamine ug/kg 1880 73 32-13075 2 301860ND1370 1390
Naphthalene ug/kg 1880 74 30-13076 2 301860ND1390 1410
Nitrobenzene ug/kg 1880 75 25-13076 1 301860ND1410 1420
Pentachlorophenol ug/kg 3740 72 10-13076 5 303730ND2710 2840
Phenanthrene ug/kg 1880 75 34-13080 7 301860ND1400 1490
Phenol ug/kg 1880 81 14-13079 2 301860ND1630 1590
Pyrene ug/kg 1880 79 31-13087 9 301860ND1490 1620
Pyridine ug/kg 1880 59 10-13061 2 301860ND1110 1140
2,4,6-Tribromophenol (S) %89 18-13061
2-Fluorobiphenyl (S)%68 19-13043
2-Fluorophenol (S)%73 18-13046
Nitrobenzene-d5 (S)%70 21-13048
Phenol-d6 (S)%73 18-13047
Terphenyl-d14 (S)%82 15-13057
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701044
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758001, 92606758002, 92606758003, 92606758004, 92606758005, 92606758011
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606526001
3659378SAMPLE DUPLICATE:
Percent Moisture %98.5 N212597.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606758011
3659379SAMPLE DUPLICATE:
Percent Moisture %23.9 N2112521.3
REPORT OF LABORATORY ANALYSIS
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92606758
510621-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
701078
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92606758006, 92606758007, 92606758008, 92606758009, 92606758010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606608001
3659665SAMPLE DUPLICATE:
Percent Moisture %21.6 N232521.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92606583002
3659666SAMPLE DUPLICATE:
Percent Moisture %41.6 N2112546.3
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92606758
510621-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Result confirmed by second analysis.C0
Analyte is a possible laboratory contaminant (not present in method blank).C7
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 72 of 78
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92606758
510621-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92606758006 701326 701441A-COMPOSITE EPA 3050B EPA 6010D
92606758007 701326 701441B-COMPOSITE EPA 3050B EPA 6010D
92606758008 701326 701441C-COMPOSITE EPA 3050B EPA 6010D
92606758009 701326 701441D-COMPOSITE EPA 3050B EPA 6010D
92606758010 701326 701441E-COMPOSITE EPA 3050B EPA 6010D
92606758011 701326 701441DUP-1 EPA 3050B EPA 6010D
92606758012 701327 701422EB-1 EPA 3005A EPA 6020B
92606758012 702443 702488EB-1 EPA 7470A EPA 7470A
92606758006 701357 701443A-COMPOSITE EPA 7471B EPA 7471B
92606758007 701357 701443B-COMPOSITE EPA 7471B EPA 7471B
92606758008 701357 701443C-COMPOSITE EPA 7471B EPA 7471B
92606758009 701357 701443D-COMPOSITE EPA 7471B EPA 7471B
92606758010 701357 701443E-COMPOSITE EPA 7471B EPA 7471B
92606758011 701357 701443DUP-1 EPA 7471B EPA 7471B
92606758012 701229 701368EB-1 EPA 3510C EPA 8270E
92606758006 701616 701912A-COMPOSITE EPA 3546 EPA 8270E
92606758007 701616 701912B-COMPOSITE EPA 3546 EPA 8270E
92606758008 701616 701912C-COMPOSITE EPA 3546 EPA 8270E
92606758009 701616 701912D-COMPOSITE EPA 3546 EPA 8270E
92606758010 701616 701912E-COMPOSITE EPA 3546 EPA 8270E
92606758011 701616 701912DUP-1 EPA 3546 EPA 8270E
92606758001 701051 701341A-3 (1-2)'EPA 5035A/5030B EPA 8260D
92606758002 701051 701341B-3 (1-2)'EPA 5035A/5030B EPA 8260D
92606758003 701051 701341C-3 (1-2)'EPA 5035A/5030B EPA 8260D
92606758004 701051 701341D-4 (1-2)'EPA 5035A/5030B EPA 8260D
92606758005 701051 701341E-3 (1-2)'EPA 5035A/5030B EPA 8260D
92606758011 701051 701341DUP-1 EPA 5035A/5030B EPA 8260D
92606758012 701304EB-1 EPA 8260D
92606758013 701304TRIP BLANK EPA 8260D
92606758001 701044A-3 (1-2)'SW-846
92606758002 701044B-3 (1-2)'SW-846
92606758003 701044C-3 (1-2)'SW-846
92606758004 701044D-4 (1-2)'SW-846
92606758005 701044E-3 (1-2)'SW-846
92606758006 701078A-COMPOSITE SW-846
92606758007 701078B-COMPOSITE SW-846
92606758008 701078C-COMPOSITE SW-846
92606758009 701078D-COMPOSITE SW-846
92606758010 701078E-COMPOSITE SW-846
92606758011 701044DUP-1 SW-846
REPORT OF LABORATORY ANALYSIS
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Page 75 of 78
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Page 78 of 78
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-216125-1
Client Project/Site: 510621-001
For:
Apex Companies LLC
5900 Northwoods Business Pkwy
Suite 5900-O
Charlotte, North Carolina 28269
Attn: Mr. Eric Wysong
Authorized for release by:
6/2/2022 12:28:59 PM
David Fuller, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
Definitions/Glossary
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Qualifiers
HPLC/IC
Qualifier Description
F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL, and the absolute difference between results is <
the upper reporting limits for both.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Sample Summary
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Lab Sample ID Client Sample ID Matrix Collected Received
680-216125-1 A-Composite Solid 05/26/22 18:50 05/27/22 12:23
680-216125-2 B-Composite Solid 05/26/22 17:10 05/27/22 12:23
680-216125-3 C-Composite Solid 05/26/22 14:55 05/27/22 12:23
680-216125-4 D-Composite Solid 05/26/22 10:15 05/27/22 12:23
680-216125-5 E-Composite Solid 05/26/22 13:15 05/27/22 12:23
680-216125-6 DUP-1 Solid 05/26/22 00:00 05/27/22 12:23
680-216125-7 EB-1 Water 05/26/22 18:55 05/27/22 12:23
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Case Narrative
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Job ID: 680-216125-1
Laboratory: Eurofins Savannah
Narrative
Receipt
The samples were received on 5/27/2022 11:01 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.1º C.
HPLC/IC
Per method requirements, Hexavalent Chromium soil samples are run in duplicate. The higher result is considered the primary result and
the lower result is secondary.
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Client Sample Results
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Lab Sample ID: 680-216125-1Client Sample ID: A-Composite
Matrix: SolidDate Collected: 05/26/22 18:50
Percent Solids: 83.0Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)0.528 0.498 0.174 mg/Kg ☼05/31/22 13:26 05/31/22 19:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.498 0.174 mg/Kg 05/31/22 13:26 05/31/22 19:52 1☼Hexavalent Chromium (CrVI)0.439 J
Lab Sample ID: 680-216125-2Client Sample ID: B-Composite
Matrix: SolidDate Collected: 05/26/22 17:10
Percent Solids: 79.5Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)0.517 0.487 0.171 mg/Kg ☼05/31/22 13:26 05/31/22 20:49 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.487 0.171 mg/Kg 05/31/22 13:26 05/31/22 20:56 1☼Hexavalent Chromium (CrVI)0.503
Lab Sample ID: 680-216125-3Client Sample ID: C-Composite
Matrix: SolidDate Collected: 05/26/22 14:55
Percent Solids: 73.3Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)2.78 0.535 0.187 mg/Kg ☼05/31/22 13:26 05/31/22 21:15 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.535 0.187 mg/Kg 05/31/22 13:26 05/31/22 21:22 1☼Hexavalent Chromium (CrVI)2.31
Lab Sample ID: 680-216125-4Client Sample ID: D-Composite
Matrix: SolidDate Collected: 05/26/22 10:15
Percent Solids: 79.5Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)0.797 0.524 0.184 mg/Kg ☼05/31/22 13:26 05/31/22 21:28 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.524 0.184 mg/Kg 05/31/22 13:26 05/31/22 21:34 1☼Hexavalent Chromium (CrVI)0.820
Lab Sample ID: 680-216125-5Client Sample ID: E-Composite
Matrix: SolidDate Collected: 05/26/22 13:15
Percent Solids: 74.9Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)0.528 J 0.530 0.185 mg/Kg ☼05/31/22 13:26 05/31/22 21:41 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.530 0.185 mg/Kg 05/31/22 13:26 05/31/22 21:47 1☼Hexavalent Chromium (CrVI)0.474 J
Lab Sample ID: 680-216125-6Client Sample ID: DUP-1
Matrix: SolidDate Collected: 05/26/22 00:00
Percent Solids: 60.7Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Hexavalent Chromium (CrVI)0.924 0.649 0.227 mg/Kg ☼05/31/22 13:26 05/31/22 21:54 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
0.649 0.227 mg/Kg 05/31/22 13:26 05/31/22 22:00 1☼Hexavalent Chromium (CrVI)0.918
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Client Sample Results
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Lab Sample ID: 680-216125-7Client Sample ID: EB-1
Matrix: WaterDate Collected: 05/26/22 18:55
Date Received: 05/27/22 12:23
Method: 7199 - Chromium, Hexavalent (IC) - Dissolved
RL MDL
Hexavalent chromium ND 10.0 5.00 ug/L 05/27/22 14:45 1
Analyte Dil FacAnalyzedPreparedUnitDResult Qualifier
10.0 5.00 ug/L 05/27/22 14:52 1Hexavalent chromium ND
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QC Sample Results
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.439 J 980 847.2 mg/Kg 86 75 -125☼
Analyte
MSI MSI
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.528 980 849.4 mg/Kg 87 75 -125☼
Analyte
MSI MSI
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.439 J 49.8 46.90 mg/Kg 93 75 -125☼
Analyte
MSS MSS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.528 49.8 46.52 mg/Kg 92 75 -125☼
Analyte
MSS MSS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.439 J 0.6191 F5 mg/Kg 34 20☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: A-CompositeLab Sample ID: 680-216125-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 260870 Prep Batch: 260469
Hexavalent Chromium (CrVI)0.528 0.6052 mg/Kg 14 20☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 410-260860/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 260860
RL MDL
Hexavalent chromium ND 10.0 5.00 ug/L 05/27/22 14:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Method BlankLab Sample ID: MB 410-260860/12
Matrix: Water Prep Type: Total/NA
Analysis Batch: 260860
RL MDL
Hexavalent chromium ND 10.0 5.00 ug/L 05/27/22 14:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Eurofins Savannah
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QC Sample Results
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-260860/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 260860
Hexavalent chromium 100 100.9 ug/L 101 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-260860/13
Matrix: Water Prep Type: Total/NA
Analysis Batch: 260860
Hexavalent chromium 100 103.3 ug/L 103 90 -110 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-260860/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 260860
Hexavalent chromium 100 102.9 ug/L 103 90 -110 2 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
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QC Association Summary
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
HPLC/IC
Prep Batch: 260469
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A680-216125-1 A-Composite Total/NA
Solid 3060A680-216125-2 B-Composite Total/NA
Solid 3060A680-216125-3 C-Composite Total/NA
Solid 3060A680-216125-4 D-Composite Total/NA
Solid 3060A680-216125-5 E-Composite Total/NA
Solid 3060A680-216125-6 DUP-1 Total/NA
Solid 3060A680-216125-1 MSI A-Composite Total/NA
Solid 3060A680-216125-1 MSS A-Composite Total/NA
Solid 3060A680-216125-1 DU A-Composite Total/NA
Analysis Batch: 260860
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7199680-216125-7 EB-1 Dissolved
Water 7199680-216125-7 EB-1 Dissolved
Water 7199MB 410-260860/10 Method Blank Total/NA
Water 7199MB 410-260860/12 Method Blank Total/NA
Water 7199LCS 410-260860/11 Lab Control Sample Total/NA
Water 7199LCSD 410-260860/13 Lab Control Sample Dup Total/NA
Water 7199LCSD 410-260860/14 Lab Control Sample Dup Total/NA
Analysis Batch: 260870
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 260469680-216125-1 A-Composite Total/NA
Solid 7199 260469680-216125-1 A-Composite Total/NA
Solid 7199 260469680-216125-2 B-Composite Total/NA
Solid 7199 260469680-216125-2 B-Composite Total/NA
Solid 7199 260469680-216125-3 C-Composite Total/NA
Solid 7199 260469680-216125-3 C-Composite Total/NA
Solid 7199 260469680-216125-4 D-Composite Total/NA
Solid 7199 260469680-216125-4 D-Composite Total/NA
Solid 7199 260469680-216125-5 E-Composite Total/NA
Solid 7199 260469680-216125-5 E-Composite Total/NA
Solid 7199 260469680-216125-6 DUP-1 Total/NA
Solid 7199 260469680-216125-6 DUP-1 Total/NA
Solid 7199 260469680-216125-1 MSI A-Composite Total/NA
Solid 7199 260469680-216125-1 MSI A-Composite Total/NA
Solid 7199 260469680-216125-1 MSS A-Composite Total/NA
Solid 7199 260469680-216125-1 MSS A-Composite Total/NA
Solid 7199 260469680-216125-1 DU A-Composite Total/NA
Solid 7199 260469680-216125-1 DU A-Composite Total/NA
General Chemistry
Analysis Batch: 260908
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-216125-1 A-Composite Total/NA
Solid Moisture680-216125-2 B-Composite Total/NA
Solid Moisture680-216125-3 C-Composite Total/NA
Solid Moisture680-216125-4 D-Composite Total/NA
Solid Moisture680-216125-5 E-Composite Total/NA
Solid Moisture680-216125-6 DUP-1 Total/NA
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Lab Chronicle
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Client Sample ID: A-Composite Lab Sample ID: 680-216125-1
Matrix: SolidDate Collected: 05/26/22 18:50
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: A-Composite Lab Sample ID: 680-216125-1
Matrix: SolidDate Collected: 05/26/22 18:50
Percent Solids: 83.0Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.42 g 100 mL
Analysis 7199 1 260870 05/31/22 19:45 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.42 g 100 mL
Analysis 7199 1 260870 05/31/22 19:52 Z7CH ELLETotal/NA
26790Instrument ID:
Client Sample ID: B-Composite Lab Sample ID: 680-216125-2
Matrix: SolidDate Collected: 05/26/22 17:10
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: B-Composite Lab Sample ID: 680-216125-2
Matrix: SolidDate Collected: 05/26/22 17:10
Percent Solids: 79.5Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.58 g 100 mL
Analysis 7199 1 260870 05/31/22 20:49 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.58 g 100 mL
Analysis 7199 1 260870 05/31/22 20:56 Z7CH ELLETotal/NA
26790Instrument ID:
Client Sample ID: C-Composite Lab Sample ID: 680-216125-3
Matrix: SolidDate Collected: 05/26/22 14:55
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
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Lab Chronicle
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Client Sample ID: C-Composite Lab Sample ID: 680-216125-3
Matrix: SolidDate Collected: 05/26/22 14:55
Percent Solids: 73.3Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.55 g 100 mL
Analysis 7199 1 260870 05/31/22 21:15 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.55 g 100 mL
Analysis 7199 1 260870 05/31/22 21:22 Z7CH ELLETotal/NA
26790Instrument ID:
Client Sample ID: D-Composite Lab Sample ID: 680-216125-4
Matrix: SolidDate Collected: 05/26/22 10:15
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: D-Composite Lab Sample ID: 680-216125-4
Matrix: SolidDate Collected: 05/26/22 10:15
Percent Solids: 79.5Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.40 g 100 mL
Analysis 7199 1 260870 05/31/22 21:28 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.40 g 100 mL
Analysis 7199 1 260870 05/31/22 21:34 Z7CH ELLETotal/NA
26790Instrument ID:
Client Sample ID: E-Composite Lab Sample ID: 680-216125-5
Matrix: SolidDate Collected: 05/26/22 13:15
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: E-Composite Lab Sample ID: 680-216125-5
Matrix: SolidDate Collected: 05/26/22 13:15
Percent Solids: 74.9Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.52 g 100 mL
Analysis 7199 1 260870 05/31/22 21:41 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.52 g 100 mL
Analysis 7199 1 260870 05/31/22 21:47 Z7CH ELLETotal/NA
26790Instrument ID:
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Lab Chronicle
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Client Sample ID: DUP-1 Lab Sample ID: 680-216125-6
Matrix: SolidDate Collected: 05/26/22 00:00
Date Received: 05/27/22 12:23
Analysis Moisture UGCW06/01/22 11:421 ELLE260908
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: DUP-1 Lab Sample ID: 680-216125-6
Matrix: SolidDate Collected: 05/26/22 00:00
Percent Solids: 60.7Date Received: 05/27/22 12:23
Prep 3060A Z7CH05/31/22 13:26 ELLE260469
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 2.54 g 100 mL
Analysis 7199 1 260870 05/31/22 21:54 Z7CH ELLETotal/NA
26790Instrument ID:
Prep 3060A 260469 05/31/22 13:26 Z7CH ELLETotal/NA 2.54 g 100 mL
Analysis 7199 1 260870 05/31/22 22:00 Z7CH ELLETotal/NA
26790Instrument ID:
Client Sample ID: EB-1 Lab Sample ID: 680-216125-7
Matrix: WaterDate Collected: 05/26/22 18:55
Date Received: 05/27/22 12:23
Analysis 7199 Z7CH05/27/22 14:451 ELLE260860
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Dissolved
Instrument ID: 26790
Analysis 7199 1 260860 05/27/22 14:52 Z7CH ELLEDissolved
26790Instrument ID:
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: Apex Companies LLC Job ID: 680-216125-1
Project/Site: 510621-001
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-22
Eurofins Savannah
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Method Summary
Job ID: 680-216125-1Client: Apex Companies LLC
Project/Site: 510621-001
Method Method Description LaboratoryProtocol
SW8467199Chromium, Hexavalent (IC)ELLE
EPAMoisturePercent Moisture ELLE
SW8463060AAlkaline Digestion (Chromium, Hexavalent)ELLE
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Environment Testing, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Apex Companies LLC Job Number: 680-216125-1
Login Number: 216125
Question Answer Comment
Creator: Foreman, Leah M
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 05/27/22 12:32 PMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
Eurofins Savannah
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APPENDIX B
NCDEQ Risk Calculator Output Sheet
DEQ Risk Calculator - Direct Contact - Resident SoilVersion Date: January 2022Basis: November 2021 EPA RSL TableSite ID: Matheson Ave Brownfields SiteExposure Unit ID: Final Grade Sampling* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.CAS #Chemical Name:Ingestion Concentration (mg/kg)Dermal Concentration (mg/kg)Inhalation Concentration (mg/kg)*Ingestion Carcinogenic RiskDermal Carcinogenic RiskInhalation Carcinogenic Risk*Calculated Carcinogenic RiskIngestion Hazard QuotientDermal Hazard QuotientInhalation Hazard Quotient*Calculated Non-Carcinogenic Hazard Quotient7440-39-3Barium157 157 1571.0E-025.1E-06 1.0E-0216065-83-1 Chromium(III), Insoluble Salts52.5 52.5 52.54.5E-044.5E-0418540-29-9Chromium(VI)2.78 2.78 2.789.1E-063.9E-09 9.1E-06 1.2E-024.5E-07 1.2E-02100-41-4Ethylbenzene0.0311 0.0311 0.0311 4.9E-104.6E-09 5.1E-09 8.0E-064.9E-06 1.3E-057439-92-1~Lead and Compounds33.9 33.9 33.9<SL** <SL** <SL**7439-96-5Manganese (Non-diet)1030 1030 10305.5E-013.3E-045.5E-017487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.044 0.044 0.0441.9E-032.4E-09 1.9E-03120-12-7~Anthracene0.233 0.233 0.2339.9E-06 3.1E-061.3E-0556-55-3~Benz[a]anthracene0.44 0.44 0.44 2.9E-07 9.6E-08 5.6E-09 3.9E-0750-32-8~Benzo[a]pyrene0.327 0.327 0.3272.1E-067.1E-07 3.3E-12 2.8E-06 1.4E-02 4.3E-03 2.6E-06 1.8E-02205-99-2~Benzo[b]fluoranthene0.429 0.429 0.429 2.8E-07 9.3E-08 4.3E-13 3.7E-07207-08-9~Benzo[k]fluoranthene0.21 0.21 0.21 1.4E-08 4.6E-09 2.1E-14 1.8E-08218-01-9~Chrysene0.482 0.482 0.482 3.1E-09 1.1E-09 4.8E-15 4.2E-09206-44-0~Fluoranthene0.858 0.858 0.8582.7E-04 8.5E-053.6E-04193-39-5~Indeno[1,2,3-cd]pyrene0.176 0.176 0.176 1.1E-07 3.8E-08 1.8E-13 1.5E-0791-20-3~Naphthalene0.0328 0.0328 0.0328 5.7E-09 2.1E-09 8.0E-09 1.6E-08 2.1E-05 6.5E-06 2.1E-04 2.4E-04129-00-0~Pyrene0.654 0.654 0.6542.8E-04 8.6E-053.6E-04100-42-5Styrene0.231 0.231 0.2311.5E-052.2E-05 3.7E-05127-18-4Tetrachloroethylene0.0193 0.0193 0.0193 5.8E-115.7E-10 6.3E-10 4.1E-051.5E-04 1.9E-04108-88-3Toluene0.0171 0.0171 0.01712.7E-067.2E-07 3.5E-0695-63-6Trimethylbenzene, 1,2,4-0.0106 0.0106 0.01061.4E-052.0E-05 3.4E-051330-20-7Xylenes0.037 0.037 0.0372.4E-065.8E-05 6.0E-05Cumulative:1.3E-055.9E-01Output Form 2A** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Matheson Ave Brownfields Site
Exposure Unit ID: Final Grade Sampling
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-39-3 Barium 157 157 157 2.3E-03 7.1E-03 9.4E-03
16065-83-1 Chromium(III), Insoluble Salts 52.5 52.5 52.5 1.0E-04 2.4E-03 2.5E-03
18540-29-9 Chromium(VI) 2.78 2.78 2.78 5.6E-08 7.2E-07 7.7E-07 1.6E-03 2.1E-03 3.7E-03
100-41-4 Ethylbenzene 0.0311 0.0311 0.0311 1.4E-11 2.0E-10 2.1E-10 1.8E-06 6.5E-07 2.5E-06
7439-92-1 ~Lead and Compounds 33.9 33.9 33.9 <SL** <SL** <SL**
7439-96-5 Manganese (Non-diet) 1030 1030 1030 1.3E-01 4.6E+00 4.8E+00
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.044 0.044 0.044 6.5E-05 3.3E-05 9.8E-05
120-12-7 ~Anthracene 0.233 0.233 0.233 6.9E-07 2.9E-07 9.7E-07
56-55-3 ~Benz[a]anthracene 0.44 0.44 0.44 1.8E-09 7.4E-10 1.7E-10 2.7E-09
50-32-8 ~Benzo[a]pyrene 0.327 0.327 0.327 1.3E-08 5.5E-09 6.0E-10 1.9E-08 3.2E-03 1.3E-03 3.7E-02 4.1E-02
205-99-2 ~Benzo[b]fluoranthene 0.429 0.429 0.429 1.7E-09 7.2E-10 7.9E-11 2.5E-09
207-08-9 ~Benzo[k]fluoranthene 0.21 0.21 0.21 8.5E-11 3.5E-11 3.9E-12 1.2E-10
218-01-9 ~Chrysene 0.482 0.482 0.482 1.9E-11 8.1E-12 8.9E-13 2.8E-11
206-44-0 ~Fluoranthene 0.858 0.858 0.858 2.5E-05 1.1E-05 3.6E-05
193-39-5 ~Indeno[1,2,3-cd]pyrene 0.176 0.176 0.176 7.1E-10 3.0E-10 3.2E-11 1.0E-09
91-20-3 ~Naphthalene 0.0328 0.0328 0.0328 1.6E-10 6.6E-11 3.5E-10 5.8E-10 1.6E-07 6.7E-08 2.5E-04 2.5E-04
129-00-0 ~Pyrene 0.654 0.654 0.654 6.4E-06 2.7E-06 9.1E-06
100-42-5 Styrene 0.231 0.231 0.231 3.4E-06 8.7E-06 1.2E-05
127-18-4 Tetrachloroethylene 0.0193 0.0193 0.0193 1.6E-12 3.1E-11 3.3E-11 7.1E-06 2.1E-04 2.2E-04
108-88-3 Toluene 0.0171 0.0171 0.0171 6.3E-08 8.5E-07 9.1E-07
95-63-6 Trimethylbenzene, 1,2,4- 0.0106 0.0106 0.0106 7.8E-07 7.1E-06 7.9E-06
1330-20-7 Xylenes 0.037 0.037 0.037 2.7E-07 1.7E-05 1.7E-05
Cumulative: 8.0E-07 4.8E+00
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator