7407_Pitt_C&DLandfillInc_CDLF_Phase1_Phase2_Dec2022GW_FID1818848_20231005

ELM Site Solutions, Inc.
P. O. Box 97607
Raleigh, North Carolina 27624
Phone: [phone]
October 5, 2023
submitted via electronic mail
Ms. Jaclynne Drummond
Hydrogeologist
Solid Waste Section
Division of Waste Management
North Carolina Department of Environmental Quality
217 West Jones Street
Raleigh, North Carolina 27603
RE: December 2022 Assessment Monitoring Report
C&D Landfill, Inc.
Permit #: 7407-CDLF-2001/2009
Dear Ms. Drummond:
On behalf of C&D Landfill, Inc., ELM Site Solutions herein submits the attached Compliance
Monitoring Report for the above -referenced facility. Also attached is the Environmental Monitoring
Report Form and laboratory EDD. This report includes groundwater, surface water and landfill gas
sampling results from activities completed during the reporting period.
Please contact us if you have any questions or if additional information is required.
Sincerely,
ELM Site Solutions, Inc.
sr
Rusty Norris, PE, PLS, RSM
Senior Engineer
c Judson Whitehurst

R USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reaortina Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitorinq Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
ELM Site Solutions, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Roland B. Norris II, PE Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
r
Landfill, Inc. 802 Recycling Lane, Greenville, NC 27834 4-07 .0500 December 12 to 19, 2022
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Surface water monitorinq data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
® No. No groundwater or surface water standards were exceeded.
Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Roland B. Norris Il, PE Senior Engineer 919-792-3733
Facility Representative Name (Print) Title (Area Code) Telephone Number
Affix NC Licensed/ FIrofessional Geologist Seal
Signature
P.O. Box 97607, Raleigh, NC 27624
Facility Representative Address
C-3141
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
Date

Semi -Annual Compliance
Monitoring Report
December 2022 Semi -Annual Monitoring Event
C&D Landfill, Inc. Construction and Demolition Debris Landfill
Pitt County, North Carolina
North Carolina Solid Waste Permit No. 74-07
Prepared for:
C&D Landfill, Inc.
802 Recycling Lane
Greenville, North Carolina 27834
Prepared by:
ELM Site Solutions, Inc.
P.O. Box 97607
Raleigh, North Carolina 27624
919-792-3733
October 2023

ziemi-Aranuai uompliance
! on"Itoring Repoft
, P 'w-
.ceimber 2029 Ser-ni-Annual I'Milonitoring Event
Landfill, Inc. Construction and Demolition Debris Landfill
Pitt County, North Carolina
North Carolina Solid Waste Permit No. 74-0-17
Prepared for
C&D Landfill, Inc.
802 Recycling Lane
Greenville, North Carolina 27834
Prepared by:
ELM Site Solutions, Inc.
P.O. Box 97607
Raleigh, North Carolina 27624
919-792-3733
UAL
Thomas V. Taylc
Senior Geologist
October 2023
�eland B. 0ris ll,ILI�F �-!,Z5, R
Senior Engineer

TABLE OF CONTENTS
1.0
Introduction
4
2.0
Geology and Hydrogeology
4
3.0
Field Methods
5
3.1 Groundwater and Surface Water Monitoring
5
3.2 Landfill Gas Monitoring
7
4.0
Field and Analytical Results
8
4.1 Groundwater Results
8
4.2 Surface Water Results
10
4.3 Landfill Gas Results
10
5.0
Groundwater Characterization
10
6.0
Summary and Conclusions
11
Tables
1 Monitoring Well Construction and Groundwater Elevations — December 12 to 19, 2022
2 Stabilized Groundwater Field Parameter Measurements — December 2022
3 Summary of Groundwater Analytical Results — December 2022
4 Summary of MNA Analytical Results — December 2022
5 Summary of Surface Water Analytical Results — December 2022
6 Groundwater Velocity Data — December 2022
Figures
1 Water Table Contour Map — December 2022
Appendices
Appendix A Field Sample Collection Records
Appendix B Landfill Gas Monitoring Data Forms (June and September 2022)
Appendix C Laboratory Analytical Reports
C&D Landfill, Inc. 3 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

1.0 Introduction
Groundwater and surface water compliance monitoring was completed between December 12
and 19, 2022, at the C&D Landfill, Inc. Construction and Demolition Debris Landfill (C&D
Landfill) near Greenville, North Carolina. The field monitoring event was completed by
Environment 1, Inc. of Greenville, North Carolina. This monitoring event satisfies requirements
of the compliance monitoring program under Solid Waste Permit No. 74-07 and Solid Waste
Regulations 15A NCAC 13B .0544, with the current monitoring network configuration meeting
requirements of 15A NCAC 13B .0546. The following report summarizes sampling procedures,
field and laboratory results, and groundwater characterization as required by North Carolina
Department of Environmental Quality (NCDEQ), Division of Waste Management (DWM), Solid
Waste Section (SWS) Regulations. The NCDEQ Environmental Monitoring Reporting Form is
included with this report.
In addition to groundwater and surface water sampling, 19 landfill gas monitoring wells were
monitored in June and September 2022 by C&D Landfill personnel to satisfy requirements
provided in the facility's Solid Waste Permit. Landfill gas monitoring results are also
summarized herein.
The facility contains two unlined construction and demolition (C&D) debris landfill units. Phase
2 is currently active. Phase 1 ceased accepting waste and entered final closure in late 2022.
The Facility was developed in two non-contiguous footprints (i.e., Phases 1 and 2) located
approximately midway between US 264, a localized topographic divide, and Grindle Creek. The
phases became operational in May 2001 and August 2009, respectively. Phase 1 was the
regional repository for flood -damage debris after Hurricane Floyd in 1999. Phase 2 was initially
a staging area, where flood -debris was stored temporarily. Both areas were previously used for
agricultural purposes. A former railroad corridor traverses the site, including beneath a portion
of the Phase 2 footprint.
2.0 Geology and Hydrogeology
Historical literature and available geologic maps indicate that C&D Landfill is located within the
NC Coastal Plain Physiographic Province. The Coastal Plain is characterized as an eastward
C&D Landfill, Inc. 4 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

thickening wedge of sedimentary units that alternate between sandy aquifers and clayey
aquitards. Information taken from The Geologic Map of North Carolina, 1985, shows that the
C&D landfill is underlain by the Yorktown Formation, which is described as "fossiliferous clay
with varying amounts of fine-grained sand, silty sand, sandy silt, silty clay, and blueish gray shell
material".
Groundwater in the uppermost aquifer generally flows through unconsolidated sediments. Re-
charge occurs generally in the northern portion of the site. Groundwater flows generally south
and southwest where it discharges into tributaries of Grindle Creek. The groundwater
potentiometric surface generally reflects surface topography, and groundwater mounding is
present beneath the Phase 1 and 2 landfill footprints. Local conditions are considered typical
for the Coastal Plain region. Groundwater depths generally range from three to 12 feet below
ground surface (bgs) across the facility. There are minor seasonal and intermittent variations in
the flow pattern, but overall, the flow direction is consistent.
3.0 Field Methods
3.1 Groundwater and Surface Water Monitoring
The current groundwater monitoring network consists of the following 16 shallow and four deep
groundwater monitoring wells: MW-1 S and MW-1 D (upgradient of Phase 1); MW-2S; MW-2D;
MW-3D; MW-3A; MW-4; MW-5; MW-6; MW-7 and MW-8 (downgradient of closed Phase 1);
MW-9A and MW-17 (upgradient of active Phase 2); MW-10; MW-11; MW-12S; MW-13; MW-
14S; MW-14D and MW-15 (downgradient of Phase 2). In addition, piezometers PZ-10 and PZ-
11 (downgradient of future Phase 3) were also sampled as outlined in the approved site Water
Quality Monitoring Plan, Phases 1, 2 and 3, C&D Landfill, Inc., Greenville, North Carolina (Smith
Gardner, March 2022). The plan provides that these piezometers require addition to the site's
monitoring network upon approval of the Phase 3 Permit to Construct which was approved on
October 24, 2022. The monitoring network also includes four surface water locations (SW-1,
SW-2, SW-3, and SW-4). It should be noted that SW-1 and SW-2 were unable to be sampled
by Environment 1 personnel during this sampling event due to the locations being dry.
Sampling locations are shown on Figure 1.
C&D Landfill, Inc. 5 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring
Guidance Document for Solid Waste Facilities (NCDEQ, DWM, SWS) and the aforementioned
approved site water quality monitoring plan. Prior to sample collection, each well was gauged to
determine the depth to groundwater and then purged approximately one well volume or until
dry. Groundwater depths and elevations from this monitoring event, as well as well construction
details are presented in Table 1.
Groundwater samples were collected by Environment 1 using low -flow purge methods with a
peristaltic pump and new polyethylene tubing. Samples were collected in laboratory prepared
containers for the specified analytical parameters discussed below. Groundwater samples and
quality control samples were properly preserved, placed on ice and transported to the laboratory
within the specified hold times for each analysis.
Field water quality parameters were measured in the field using a calibrated direct -read YSI
instrument including temperature, pH, specific conductivity, turbidity, dissolved oxygen (DO),
and oxidation-reduction potential (ORP)
Surface water samples were collected from locations SW-3 and SW-4 using a field
decontaminated long -handle dipper that was used to transfer water directly into laboratory
prepared sample containers.
Groundwater samples were collected in laboratory containers provided by Environment 1, a
North Carolina certified laboratory. Groundwater samples, except PZ-10 and PZ-11, were
analyzed for the following in accordance with triennial sampling table listed in the site's
groundwater monitoring plan:
• Appendix II volatile organic compounds (VOCs), plus tetrahydrofuran and 1,4-dioxane,
by EPA Method 8260D;
• Appendix II semi -volatile organic compounds (SVOCs) by EPA Method 8270E;
• Appendix II pesticides and PCBs by EPA Method 8081 B;
• Appendix II chlorinated herbicides by EPA Method 8151A;
• Appendix II metals, plus iron and manganese, by EPA Method 200.8;
• Mercury by EPA Method 245.1; and
C&D Landfill, Inc. 6 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

Landfill specific parameters including: nitrate+nitrite as N, chloride, sulfate, sulfide,
alkalinity to pH 4.5, total dissolved solids (TDS), and cyanide.
Groundwater samples MW-1 S, MW-1 D, MW-2D, MW-3A, MW-3D, MW-6, MW-8, MW-9A, MW-
10, MW-11, MW-12S, and MW-14D were also analyzed for the following in accordance with
triennial sampling table listed in the site's groundwater monitoring plan:
• Monitored natural attenuation (MNA) parameters including: biological oxygen demand
(BOD), chemical oxygen demand (COD), total organic carbon (TOC), total hardness,
carbon dioxide (CO2), lower -level volatile fatty acids (LLVFA); methane, ethane, ethene
(MEE); and hydrogen (1­112).
Surface water samples SW-3 and SW-4, and groundwater samples PZ-10 and PZ-11 were
analyzed for the following in accordance with semi-annual sampling table listed in the site's
groundwater monitoring plan:
• Appendix II VOCs, plus tetrahydrofuran and 1,4-dioxane, by EPA Method 8260D;
• Appendix I metals, plus iron and manganese, by EPA Method 200.8; and
• General chemistry analytes including: chloride, sulfate, sulfide, alkalinity to pH 4.5, and
TDS.
Groundwater samples were transported to the laboratory on ice under chain -of -custody
protocols. The analytical results were compared to the 15A NCAC 02L .0202 Groundwater
Quality Standards or Interim Maximum Allowable Concentrations (hereinafter referred to as the
`2L Standards'). Surface water analytical results were compared to the 15A NCAC 02B Surface
Water Quality Standards (hereinafter referred to as the '213 Standards'). Field data sheets are
provided in Appendix A.
3.2 Landfill Gas Monitoring
Nineteen landfill gas monitoring locations (GP-1 through GP-5, GP-10, GP-11, SG-6, SG-7, SG-
8, SG-12 through SG-20) were monitored quarterly by C&D Landfill personnel in June and
September 2022. It should be noted that the current approved Landfill Gas Monitoring Plan
C&D Landfill, Inc. 7 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

(March 2022) has reduced the number of monitoring locations to six (GP-1 through GP-4, GP-
10, and GP-11). Landfill gas monitoring locations are shown on Figure 1.
Landfill gas quarterly monitoring events were conducted on June 22, 2022, and September 23,
2022, during this reporting period. Percent lower explosive limit (% LEL), % methane (CH4) by
volume, % oxygen (02), % carbon dioxide (CO2), and % hydrogen sulfide (H2S) were measured
and recorded at the landfill gas monitoring locations using a calibrated QRAE II gas monitoring
instrument. DWM Landfill Gas Monitoring Data Forms for the reporting period are provided in
Appendix B.
4.0 Field and Analytical Results
4.1 Groundwater Results
As stated in Section 3.1 above, field water quality parameters including temperature, pH,
specific conductivity, turbidity, DO, and ORP were measured and recorded during well purging
activities. Water quality parameter measurements are provided in Table 2 along with the
approximate total volume of water purged from each well. It must be noted that turbidity
measurements exceeded 10 nephelometric turbidity units (NTUs) in samples collected from
wells MW-4, MW-11, MW-13, MW-14S, PZ-10, and PZ-11 during this monitoring event.
Organic compounds detected above their respective 2L Standard, followed by the well(s) where
the compound was detected above the standard, are listed as follows:
Benzene: MW-3A, MW-12S, and MW-14S.
1,2-Dibromomethane (EDB): MW-8 (J qualified).
Vinyl Chloride: MW-10 (J qualified), MW-11 (J qualified), MW-12S, and MW-14S.
1,4-Dioxane: MW-1S, MW-2S, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-10, MW-11,
MW-12S, and MW-14S.
"J" qualified detections indicate an estimated value that is less than the Method Reporting Limit
(MRL) and greater than or equal to the Method Detection Limit (MDL). Based on historical data,
C&D Landfill, Inc. 8 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

the organic compound exceedances of benzene, vinyl chloride and 1,4-dioxane are considered
the primary Site constituents of concern (COCs).
Inorganics compounds detected above their respective 2L Standard, followed by the well(s)
where the compound was detected above the standard, are listed as follows:
Antimony: MW-14S.
Arsenic: MW-3A, MW-7, MW-8, MW-10, MW-12S, and MW-14S.
Total Chromium: MW-3A, MW-8, MW-10, MW-12S, and MW-14S.
Cobalt: MW-3A, MW-5, MW-6, MW-7, MW-8, MW-10, MW-11, MW-12S, MW-14S, PZ-
10, and PZ-11.
Iron: MW-1 D, MW-21D, MW-3A, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-11,
MW-12S, MW-13, MW-14S, MW-15, MW-17, PZ-10, and PZ-11.
Manganese: MW-1 D, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11,
MW-12S, MW-14S, MW-15, MW-17, PZ-10, and PZ-11.
Vanadium: MW-3A, MW-6, MW-10, MW-12S, MW-14S, PZ-10, and PZ-11.
Chloride: MW-3A and MW-14S.
Sulfate: MW-1 S, MW-11, MW-15, and MW-17.
TDS: MW-1 S, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S,
MW-14S, and MW-15.
Underlined sample results identified above indicate locations where the turbidity exceeded 10
NTUs suggesting the result may be biased high for the indicated metals and attributable to
natural/background conditions.
MNA results indicated an exceedance of the 2L Standard for acetic acid at monitoring wells
MW-8, MW-10, and MW-12S.
No additional inorganic target compounds were detected in the groundwater samples that
exceeded their respective 2L Standard. Groundwater analytical results are summarized in
Table 3 and MNA analytical results are summarized in Table 4. The laboratory analytical
reports are provided in Appendix C.
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Greenville, North Carolina October 2023

For quality assurance/quality control (QA/QC) seven trip blanks were submitted during the
sampling event for VOC analysis. No VOCs were detected at or above the MDL in the trip
blanks.
4.2 Surface Water Results
Surface water organic analytical results indicated the presence of tetrahydrofuran and 1,4-
dioxane in sample SW-3. The concentrations of these two compounds are well below their
respective 2B Standards.
The only inorganics that were detected above their respective 2B Standard include iron and
total alkalinity detected in sample SW-3. It must be noted that these exceedances are based on
recommended water quality criteria.
No other analytes were detected in surface water samples that exceeded their respective 2B
Standard. Surface water analytical results are summarized in Table 5 and the laboratory
analytical report is provided in Appendix C.
4.3 Landfill Gas Results
As noted in Section 3.2, quarterly landfill gas monitoring events were conducted on June 22,
2022, and September 23, 2022. Landfill gas was measured at 19 landfill gas monitoring
locations during the monitoring events.
All monitoring locations exhibited 0% LEL during the reporting period. Hydrogen sulfide gas
was also not detected at any location. DWM Landfill Gas Monitoring Data Forms for the
reporting period are provided in Appendix B.
5.0 Groundwater Characterization
A water table contour map was prepared from the well gauging measurements collected in
December 2022 as shown on Figure 1. As noted on the figure, shallow groundwater flows
generally south and southwest toward tributaries of Grindle Creek as historically observed.
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Greenville, North Carolina October 2023

Horizontal groundwater flow velocities were calculated using the equation V = KI/ ne where:
V = estimated horizontal velocity,
K = hydraulic conductivity (from historical monitoring reports),
I = estimated shallow hydraulic gradient,
ne = estimated effective porosity (from historical monitoring reports).
Calculated estimated shallow groundwater velocities ranged from 0.00095 ft/day at MW-11 to
0.014 ft/day at MW-3A as shown on Table 6.
6.0 Summary and Conclusions
The following is a summary of current site conditions and conclusions based on results of the
December 2022 monitoring event:
Groundwater organic compounds detected above their respective 2L Standard included the
following:
Benzene: MW-3A, MW-12S, and MW-14S.
1,2-Dibromomethane (EDB): MW-8 (J qualified).
Vinyl Chloride: MW-10 (J qualified), MW-11 (J qualified), MW-12S, and MW-14S.
1,4-Dioxane: MW-1 S, MW-2S, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-10, MW-11,
MW-12S, and MW-14S.
Groundwater inorganics compounds detected above their respective 2L Standard included the
following:
Antimony: MW-14S.
Arsenic: MW-3A, MW-7, MW-8, MW-10, MW-12S, and MW-14S.
Total Chromium: MW-3A, MW-8, MW-10, MW-12S, and MW-14S.
Cobalt: MW-3A, MW-5, MW-6, MW-7, MW-8, MW-10, MW-11, MW-12S, MW-14S, PZ-
10, and PZ-11.
Iron: MW-1 D, MW-2D, MW-3A, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-11,
MW-12S, MW-13, MW-14S, MW-15, MW-17, PZ-10, and PZ-11.
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Manganese: MW-1 D, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11,
MW-12S, MW-14S, MW-15, MW-17, PZ-10, and PZ-11.
Vanadium: MW-3A, MW-6, MW-10, MW-12S, MW-14S, PZ-10, and PZ-11.
Chloride: MW-3A and MW-14S.
Sulfate: MW-1 S, MW-11, MW-15, and MW-17.
TDS: MW-1 S, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S,
MW-14S, and MW-15.
Analytical results are generally consistent with past sampling events. Organic compound (non -
qualified) exceedances included benzene, vinyl chloride and 1,4-dioxane, which are considered
the site COCs. Detections were on the same order of magnitude as previous events indicating
minimal additional source contribution during the reporting period. A review of historical data
indicates the presence of organochlorides, and in addition to continued detection of vinyl
chloride, indicates that reductive dichlorination via natural attenuation may be occurring at the
Site.
Seven inorganic elements (metals) exceeded their respective 2L Standard, with two (iron and
manganese) detected in upgradient/background wells above their respective 2L Standards.
Each of the seven metals detected above their respective 2L Standard had some detections
that were likely influenced by elevated NTU (turbidity) values, indicating that the source may be
attributed to naturally occurring and/or background conditions.
No organic compounds were detected in surface water samples above 2B Standards.
Inorganics detected above their respective 2B Standard included iron and total alkalinity
detected in sample SW-3. These detections only exceeded recommended water quality criteria.
Additional water quality parameters (chloride, sulfate and TDS) were detected above their
respective 2L standard. Sulfate and TDS were detected in upgradient/background wells
indicating possible natural occurrence and/or background conditions.
All landfill gas monitoring locations exhibited 0% LEL during the reporting period. Hydrogen
sulfide gas was also not detected at any location.
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Greenville, North Carolina October 2023

C&D Landfill personnel will continue with quarterly landfill gas monitoring at the site with the
next two events scheduled for March and June 2023. It was reported by C&D Landfill personnel
that the December 2022 landfill gas monitoring event did not occur due to a malfunctioning
landfill gas meter.
Semi-annual groundwater and surface water monitoring will continue at the site with the next
event scheduled for June 2023.
C&D Landfill, Inc. 13 Semi -Annual Compliance Monitoring Report
Greenville, North Carolina October 2023

TABLES

Table 1
Monitoring Well Construction and Groundwater Elevations - December 12 to 19, 2022
C&D Landfill, Inc. Construction and Demolition Debris Landfill
Greenville, North Carolina
Well ID
Date
Constructed
Screen
Interval
(ft BGS)
Measured
Total Depth
(ft BTOC)
Well Diameter
and Material
Ground
Surface
Elevation
ft MSL
Top of
Casing
Elevation
ft MSL
Depth to
Water
(ft BTOC)
Water Level
Elevation
(ft MSL)
MW-1 S
05/02/01
3 - 13
17.2
2" PVC
17.59
20.91
8.80
12.11
MW-1 D
10/13/00
40 - 50
33.8
2" PVC
17.40
21.14
9.48
11.66
MW-2S
05/03/01
3 - 13
16.6
2" PVC
18.45
21.44
13.21
8.23
MW-2D
10/11/00
39 - 49
38.2
2" PVC
17.97
21.80
13.26
8.54
MW-3A
08/10/09
5 - 20
23.4
2" PVC
19.13
21.93
12.11
9.82
MW-3D
10/13/00
40 - 50
52.3
2" PVC
19.37
22.83
13.52
9.31
MW-4
05/03/01
3 - 13
15.5
2" PVC
14.83
18.42
7.20
11.22
MW-5
11/19/02
3 - 18
9.5
2" PVC
14.80
17.90
6.70
11.20
MW-6
05/03/01
3 - 13
16.7
2" PVC
16.87
20.03
10.24
9.79
MW-7
05/03/01
3 - 13
16.3
2" PVC
16.03
19.40
9.03
10.37
MW-8
11/05/02
3 - 18
20.3
2" PVC
18.30
21.21
10.21
11.00
MW-9A
08/07/09
5 - 20
23.2
2" PVC
17.64
20.58
6.30
14.28
MW-10
08/06/09
5 - 20
22.7
2" PVC
14.16
16.61
4.11
12.50
MW-11
08/06/09
5 - 20
23.8
2" PVC
11.60
14.49
4.50
9.99
MW-12S
08/07/09
5 - 20
22.9
2" PVC
13.72
16.81
12.70*
4.11
MW-13
08/07/09
5 - 20
20.7
2" PVC
18.12
20.69
10.00
10.69
MW-14S
12/18/02
5 - 20
23.1
2" PVC
13.90
16.60
5.69
10.91
MW-14D
12/17/02
35 - 40
41.9
2" PVC
14.54
17.45
6.84
10.61
MW-15
12/18/02
5 - 20
14.6
2" PVC
13.90
19.67
7.00
12.67
MW-17
12/09/02
5 - 20
1 13.3
1 2" PVC
1 18.18
1 20.74
8.03
1 12.71
Notes:
Field data collected by Environment 1, Greenville, NC.
ft BGS - Feet below ground surface.
ft BTOC - Feet below top of casing.
ft MSL - Feet above mean sea level.

Table 2
Groundwater Field Parameter Measurements - December 2022
C&D Landfill, Inc. Construction and Demolition Debris Landfill
Greenville, North Carolina
Sample ID
Volume
Purged
(Gallons)
Temperature
(degrees C)
pH (SU)
Specific
Conductivity
(US/cm)
Turbidity
(NTU)
Dissolved
Oxygen
(mg/L)
Oxidation
Reduction
Potential (mV)
MW-1 S
1.5
15
6.9
1386
3.0
1.18
113
MW-1 D
4.0
12
7.4
370
2.1
1.82
91
MW-2S
0.5
16
9.1
332
0.9
3.14
90
MW-2D
4.0
14
8.7
447
3.9
1.08
118
MW-3A
2.0
15
6.9
3765
4.8
1.47
142
MW-3D
6.5
16
8.4
556
0.9
2.37
116
MW-4
1.5
15
7.7
502
17.2
2.23
167
MW-5
0.5
14
7.5
1680
2.3
5.67
117
MW-6
1.0
15
7.1
1723
6.8
3.36
134
MW-7
1.5
16
6.9
2582
9.7
3.37
137
MW-8
2.0
18
6.9
2963
3.1
2.81
158
MW-9A
3.0
15
7.7
1040
8.6
7.85
149
MW-10
3.5
15
6.7
2461
2.9
2.66
159
MW-11
3.5
14
7.3
1507
18.9
3.36
146
MW-12S
2.0
17
6.9
3093
2.7
0.98
161
MW-13
2.0
15
7.2
624
21.3
4.87
92
MW-14S
3.0
18
6.8
4065
97.2
1.97
167
MW-14D
6.0
19
7.2
532
0.6
3.47
127
MW-15
1.5
17
6.5
1240
7.8
2.79
113
MW-17
1.0
17
6.6
660
2.4
2.46
84
PZ-10
2.0
13
6.4
70
570
1.22
106
PZ-11
1 2.5
1 13
1 6.1
1 234
1 260
1 2.81
1 103
Notes:
Field data collected by Environment 1, Greenville, NC.
C = Degrees celsius.
SU = Standard units.
uS/cm = Microsiemens per centimeter.
NTU = Nephelometric Turbidity Units.
mg/L = Milligrams per liter.
my = Millivolts.

Table 4
Summary of MNA Analytical Results - December 2022
C and D Landfill, Inc. Construction and Demolition Landfill
Greenville, North Carolina
Analyte
NC 2L
Groundwater
Standard or
IMAC
Units
AMIR-
MWAS
MWAD
MW-2D
MW-3A
MW-3D
MW-6
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-14D
12/14/2022
12/14/2022
12/14/2022
12/14/2022
12/14/2022
12/14/2022
12/15/2022
12/15/2022
12/15/2022
12/15/2022
12/15/2022
12/15/2022
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Result Q
Hach IR-1
Ferrous Iron NS ug/L <50 350 <50 5000 <50 3500 9500 10,000 200.0 9000 5000 <50
MNA Parameters
Biological Oxygen Demand
NS
mg/L
<2.0
U
4.1
R
<2.0
U
11
R
<2.0
U
3.2
R
10
R
<2.0
U
11
R
3.4
R
22
<2.0
U
Chemical Oxygen Demand
NS
mg/L
80
29
<0.840
U
742
<0.840
U
279
393
36
531
150
603
<0.840
U
Total Organic Carbon
NS
mg/L
12.95
8.62
2.71
30.99
3.44
47.68
36.95
10.96
42.80
36.48
37.72
3.35
Total Hardness
NS
mg/L
488
92
128
740
88
690
760
400
680
880
720
154.00
Carbon Dioxide
NS
mg/L
127
16
7
320
10
250
324
132
504
212
420
18.00
Volatile Fatty Acids by Method AM23
Acetic Acid
5
mg/L
4.5
J
0.70
J
0.58
J
4.8
J
0.65
J
4.7
J
0.62
6.5
0.67
S&0.62
Butyric Acid
NS
mg/L
<0.58
U
<0.12
U
<0.12
U
1.3
J
<0.12
U
1.4
J
<0.58
U
<0.058
U
0.96
J
0.063
J
0.75
J
<0.058
U
Hexanoic Acid
NS
mg/L
0.91
J
<0.12
U
<0.12
U
0.96
J
<0.12
U
0.85
J
0.72
J
0.099
J
0.86
J
0.12
J
1.0
J
<0.058
U
Lactic Acid
NS
mg/L
1.3
J
18
11
3.4
J
15
3.3
J
2.2
J
1.0
<0.53
U
1.4
1.5
J
9.4
Propionic Acid
NS
mg/L
<0.53
U
<0.11
U
<0.11
U
0.66
J
<0.11
U
<0.53
U
0.62
J
0.070
J
0.75
J
<0.053
U
0.71
J
<0.053
U
Hydrogen by Method AM20GAX
Hydrogen NS nM 1.7 J 2.0 0.63 J 1.1 J <0.49 U 0.88 J 1.1 J 0.69 J <0.49 U 0.78 J 0.71 J 0.96 J
MEE by EPA Method RSK175
Methane
NS
ug/L
13.8
2200
80.7
2390
8.74
915
1320
101
2940
151
1960
39.2
Ethane
NS
ug/L
<0.172
U
1.49
<0.172
U
<0.172
U
<0.172
U
<0.172
U
<0.172
U
0.449
J
<0.172
U
<0.172
U
<0.172
U
<0.172
U
Ethene
NS
ug/L
<0.241
U
<0.241
U
0.861
J
<0.241
U
<0.241
U
<0.241
U
<0.241
U
<0.241
U
1 <0.241
U
<0.241
U
<0.241
U
<0.241
U
Notes:
Wells sampled by Environment 1, Greenville, NC.
MNA - Monitored Natural Attenuation.
NC 2L Groundwater Standard or IMAC - 15A NCAC 02L Groundwater Quality Standards (April 1, 2022); NC Interim Maximum Allowable Concentrations (IMACs) (June 30, 2021).
NA - Not Analyzed.
NS - Not Specified.
Bold - Detected Constituent.
U - Not detected. The associated value indicates approximate sample concentration necessary to be detected.
J - Estimated value > or = the Method Detection Limit (MDL) and < the Method Reporting Limit (MRL).
R - Replicate varied by more than 30 % .
Green highlighted cell indicates the value is greater than the NC 2L Groundwater Standard or IMAC.
1 of

Table 5
Summary of Surface Water Analytical Results - December 2022
C10/3/2023 Landfill, Inc. Construction and Demolition Landfill
Greenville, North Carolina
Analyte
NC 213
Standards Acute
Toxicity - Class
C
NC 2B Standards
Chronic Toxicity -
Class C
NC 2B Surface
Water
Standards -
Class C
Units
SW-3
SW-4
12/19/2022
12/19/2022
Result
Q
Result
Q
VOCs by EPA Method 8260D
Tetrahydrofuran
NA
NA
110,000a
ug/L
2.98
<0.39
U
1,4-Dioxane
NA
NA
80a
ug/L
5.61
<2.71
U
Metals by EPA Method 200.8
Arsenic
340
150
NS
ug/L
2.3
J
0.41
J
Barium
NS
NS
21'000a
ug/L
105
66.9
Beryllium
65
6.5
NS
ug/L
<0.10
J
0.12
J
Total Chromium
183.07
23.81
NS
ug/L
3.3
J
1.0
J
Cobalt
16a
1.6a
NS
ug/L
0.58
J
0.61
J
Copper
3.64
2.74
NS
ug/L
0.54
J
0.50
J
Iron
NS
NS
10006
ug/L
1763
597
Lead
13.88
0.54
NS
ug/L
0.25
J
0.50
J
Manganese
NS
NS
NS
ug/L
82
10
Nickel
144.92
16.10
NS
ug/L
0.84
J
0.9
J
Vanadium
NS
NS
NS
ug/L
1
1
Zinc
36.20
36.50
NS
ug/L
5.3
J
6.5
J
General Chemistry
Chloride
NA
NA
230
mg/L
35
15
Sulfate
NA
NA
250
mg/L
71.9
40.2
Sulfide
NA
NA
NS
mg/L
<0.10
U
<0.10
U
Alkalinity to pH 4.5
NA
NA
20b
mg/L
128
14
Total Dissolved Solids
NA
NA
NS
mg/L
260
110
Notes:
Samples collected by Environment 1, Greenville, NC.
NC 213 Surface Water Standards - 15A NCAC 02B Surface Water Quality Standards (July 26, 2021).
a - NC In -stream Target Values.
b - EPA National Recommended Water Quality Criteria.
NA - Not Applicable.
NS - Not Specified.
Bold - Detected Constituent.
U - Not detected. The associated number indicates approximate sample concentration necessary to be detected.
J - Estimated value > or = the Method Detection Limit (MDL) and < the Method Reporting Limit (MRL).
Green highlighted cell indicates the value exceeds the NC 213 Standard.

Table 6
Groundwater Velocity Data - December 2022
C&D Landfill, Inc. Constructon and Demolition Debris Landfill
Greenville, North Carolina
Hydraulic
Effective
Hydraulic
Well ID
Conductivity
Porosity
Gradient (1)
Velocity (V)
(K) (ft/day)
(ne)
(ft/ft)
(ft/day)
MW-3A
0.805
0.08
0.0014
0.014
MW-10
0.116
0.05
0.005
0.012
MW-11
0.009
0.04
0.0042
0.00095
Notes:
Velocity calculated based on the modified Darcy equation: V = KI/n.
Hydraulic conductivity and effective porosity values from historical Wood, Inc. groundwater
monitoring reports.

FIGURES

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1) BASE MAPPING INCLUDING GROUNDWATER MONITORING WELL LOCATIONS PROVIDED IN
DIGITAL CAD FORMAT BY SMITH GARDNER & ASSOC. FEBRUARY, 2025
2) AERIAL ORTHOPHOTOGRAPHY AND TOPOGRAPHIC CONTOURS PROVIDED BY PITT
COUNTY GIS (NC ONE MAPS).
3) TOPOGRAPHIC CONTOURS OF TOP PORTION OF PHASE I LANDFILL PROVIDED BY SMITH
GARNDER & ASSOC. FEBRUARY, 2023.
4) GAS WELL LOCATIONS VISUALLY FIELD VERIFIED MAY , 2025.
5) 100 YEAR FLOOD ZONES PROVIDED BY NC ONE MAPS.
LEGEND
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or in part. It is only to be used for the project and
site specifically identified herein and is not to be
used on any other project. It is to be returned
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APPENDICES

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APPENDIX B
LANDFILL GAS MONITORING DATA
FORMS
(JUNE and SEPTEMBER 2022)

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: Thisform and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by arty person upon request. (IVC General Statute 132-6).
FacilityName: 60 L&nok;Y Permit Number: FYOIL—(0`F- A009
Sampling Date: G X-X/A2 NC Landfill Rule (.0500 or.1600): , 0"0
Sample Collector Name & Position: Ake, I✓a r P Gn
Gas Meter Type & Serial Number: g99. 4 ,0 i i Gas Meter Calibration Date: &AZ1s 2-
Field Calibration Date & Time: (//"/�Z
Field Calibration Gas Type (15115 or 35/50): /Slp i— Field Calibration Gas Canister Expiration Date: (O Z•ZA z
Gas Meter Pump Rate: f V1 /),-
Ambient Air Temperature: Barometric Pressure (in. or min Hg): Weather Conditions:
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CH4 (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (H2S) gas monitoring may be required for Construction & Demolition Landfills (CDLFs). See individual
permit conditions and/or Facility LFG monitoring plan.
Location or
FG Well ID
Sample
Tube
Purge
Time of
Day
Time
pumped
(sec)
Initial
�/a LEL
Stabilized
% LEL
% CH4
(volume)NOTES
% 02
(volume)[(volume)
% CO2
% H2S*
(volume)?
n
Q': oo
s
o
6
A
30
ff: og'
Ns
0
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0
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30
9:
ys'
o
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A I, s'
1 r 7
0
NOTE: tf needed, attach additional data forms to include additional LFG monitoring data locations for• the facility.
ACTION LEVELS: Methane: >1.25% by volume (inside structures) AND >5% by volume (at facility boundary)
Hydrogen Sulfide: >1 % by volume (inside structures) AND >4% by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. I am aware that there are significant penalties for making any false statement, representation,
or certification including the possibility of a line and imprisonment.
r
SIGNATURE TIf LE
Revised — February 4, 2020

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by arty person upon request (NC General Statute 132-6).
FacilityName: L 8- D Lw wdC,1 f Permit Number:
Sampling Date: 4/i/2Al,eL NC Landfill Rule (.0500 or.1600): . OSOG
Sample Collector Name & Position: jj, ke- b/a,we^
Gas Meter Type & Serial Number: d QA Z' i. Gas Meter Calibration Date: 4/JLZ,4& 2_
Field Calibration Date & Time: z
Field Calibration Gas Type (15115 or 35/50): /sOS' Field Calibration Gas Canister Expiration Date:
Gas Meter Pump Rate: */ -
Ambient Air Temperature: Barometric Pressure (in. or mm Hg): Weather Conditions:
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CH4 (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (H2S) gas monitoring may he required for Construction & Demolition Landf lls (CDLFs). See individual
permit conditions and/or Facility LFG monitoring plan.
Location or
LFG Well ID
Sample
Tube
Purge
Time of
Day
Time
Pumped
(sec)
Tnitial
n
/o LEL
Stabilized
a
/o LEL
% CH4
(volume)
0
/0 02
(volume)
0
/e Cr
(volume)
0 �
/a H S
(volume)
NOTES
S
30
C- Jo
s
v
i
O,
o
S
4:11—
s—
to
ZD. '
0,4
07
17
30
er.w
Yjr
0&
v-
S
30
4 s xv
7
.70
q:,Yo
C9 t
3o
4:7f-
O
at,
NOTE: If needed, attach additional data forms to include additional LFG monitoring data locations for thelacility.
ACTION LEVELS: Methane: >1.25% by volume (inside structures) AND >5% by volume (at facility boundary)
Hydrogen Sulfide: >1 % by volume (inside structures) AND >40/., by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. I am aware that there are significant penalties for making any false statement, representation,
or certificica�tiioon/including the possibility of a fine and imprisonment. SIGNATURE TI LF
Revised — February 4, 2020

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: 77iis form and any injormalion attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by airy person upon request (NC General .Stalule 132-6).
FacilityName: GeF-D La i« Tne. Permit Number: Y C407 — C Qiir— - 2al l
Sampling Date: q&:FZZ 2 NC Landfill Rule (.0500 or.1600): 10"42
Sample Collector Name & Position: 41t Ke k1af-An" (1l�traitiovtS /riw.na.. er
Gas Meter Type & Serial Number: a Q A I7 � t Gas Meter Calibration Date: V2412. A
Field Calibration Date & Time: Ct ATA2 I -
Field Calibration Gas Type (15115 or 35/50): / S'-�l s` Field Calibration Gas Canister Expiration Date: '—
Gas Meter Pump Rate: 4�IA
Ambient Air Temperature: Barometric Pressure (in. or mm Hg): Weather Conditions: Gifu
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CH4 (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (H2S) gas monitoring may be required for Construction & Demolition Landfills (CDLFs). See individual
permit conditions and/or Facility LFG monitoring plan.
Location or
LFG Well ID
Sample
Tube
Purge
Time of
Day
Time
Pumped
(sec)
initial
o
/o LEL
Stabilized
o
/o LEL
% CH4
(volume)
0
/0 02
(volume)
0
/o CO2
(volume)
0 , r
/a Fi.,S
(volume)
NOTES
o
Z. d.r-
67 s
z1
0.7
20
1.0
5 7
30
9,10
0
0
1.0
30
--f , s-a
d0
0
1 .1-
d
NOTE: If needed, attach additional data forms to include additional LFG monitoring data locations for the facility.
ACTION LEVELS: Methane: >1.25% by volume (inside structures) AND >5% by volume (at facility boundary)
Hydrogen Sulfide: >1 % by volume (inside structures) AND >4"/o by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. I am aware that there are significant penalties for making any false statement, representation,
or certification including the possibility of a tine and imprisonment.
�iar�4�ib,� g /'%anaQer
SIGNATURE TITLE T�
Revised — February 4, 2020

NC Division of Waste Management - Solid Waste Section
Landfill Gas Monitoring Data Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
FacilityName:_C,.d--n Ga .ill Permit Number: ?-q0 7--CL2.F-,xdO-i
Sampling Date: 912112.2 NC Landfill Rule (.0500 or.1600): . os_"
Sample Collector Name & Position: /y; �Ce b/a►e�re.� DAts eah'ens A'Isr a.�
Gas Meter Type & Serial Number: 0PAC ;; Gas Meter Calibration Date:
Field Calibration Date & Time: 9AT/aLZ
Field Calibration Gas Type (15/15 or 35/50): /S'�/S�Field Calibration Gas Canister Expiration Date: ^`
Gas Meter Pump Rate: AA -
Ambient Air Temperature: Barometric Pressure (in. or min Hg): Weather Conditions: i�!'�►r'
Instructions: Under "Location or LFG Well", list monitoring well # or describe monitoring location (e.g., inside field office).
Attach a test location map or drawing. Report methane readings as both % LEL and % CH4 by volume.
Convert % CH4 (by volume) to % LEL as follows: % methane (by volume) x 20 = % LEL.
*Hydrogen Sulfide (H2S) gas monitoring may be required for Construction & Demolition Landfills (CDLFs). See individual
permit conditions and/or Facility LFG monitoring plan.
Location or
LFG Well ID
S ample
Tube
purge
Time of
Day
Time
Pumped
(sec)
Initial
% LEL
Stabilized
% LEL
% CH4
(volume)
ova 02
(volume)
% CO2
(volume)
% H2S*
(volume)
NOTES
6- )
3
D
O
IM 2
I
39
2(�2
, i
3
30
s'
s6
V
10
Zos-
e.4
3
3
v-
a
6
!q. Y
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330
y.
e_
6
8
0
1.1.4-
l .
53o>s
: Ys
At sue'
a
0
0
20
C2 S"
S
0
Y'
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o
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5 20
o
y: 00
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d
0
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11
o
p%r-
(r Iv
P
4 : to
s'
b
.z
o,
0
NOTE: ]jneeded, attach additional data forms to include additional LFG monitoring data locations for the facility.
ACTION LEVELS: Methane: >1.25% by volume (inside structures) AND >5% by volume (at facility boundary)
Hydrogen Sulfide: >1 % by volume (inside structures) AND >40/,, by volume (at facility boundary)
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments
are true and correct. I am aware that there are significant penalties for making any false statement, representation,
or certification * eluding the possibility of a fine and imprisonment.
SIGNATURE TIfFLE
Revised — February 4, 2020

APPENDIX C
LABORATORY ANALYTICAL
REPORTS

ElMommid Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
PARAMETERS MDL
PH (field measurement), Unite
Nitrate+Nitrite as N, mg/l
0.04
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
Chloride, mg/l
1.0
Cyanide, ug/1
5.0
Total Dissolved Residue, mg/l
10
Total Dissolved Residue, mg/l
10
Sulfate, mg/1
5.0
Antimony, ug/1
0.30
Arsenic, ug/l
0.13
Barium, ug/1
0.14
Beryllium, ug/1
0.10
Cadmium, ug/l
0.19
Cobalt, ug/l
0.10
Total Chromium, ug/l
0.19
Copper, ug/1
0.26
Iron, ug/1
12.20
Manganese, ug/1
2.70
Lead, ug/l
0.09
Mercury, ug/l
0.08
Nickel, ug/1
0.13
Selenium, ug/l
0.43
Silver, ug/l
0.14
Thallium, ug/1
0.13
Tin, ug/l
0.36
Vanadium, ug/1
0.14
Zinc, ug/l
0.34
Sulfide, ug/1
100
Conductivity (at 25c), uMhos/cm
1.0
Dissolved Oxygen, mg/1
0.1
Temperature, °C
Static Water Level, feet
Well Depth, feet
ORP, my
Turbidity (Field), NTU
1.0
PHONE [phone]
FAX [phone]
ID#: 6003
DATE COLLECTED: 12/12/22
DATE REPORTED : 03/29/23
REVIEWED BY:
MW-4 MW-5 MW-7
MRL
7.7
0.04 --- U
1.0 90
1.0 21
5.0 --- U
10 270
10
5.0 111
1.0 --- U
5.0 0.68 J
10.0 49.6
1.0 0.12 J
1.0 --- U
1.0 0.24 J
5.0 2.6 J
10.0 0.32 J
50.0 3143
10.0 45
5.0 0.64 J
0.20 --- U
10.0 0.86 J
10.0 0.46 J
5.0 --- U
1.0 --- U
100.0 0.39 J
1.0 3
10.0 5.0 J
1000 TESTED
1.0 502
0.1 2.23
15
7.20
15.48
+167
1.0 17.20
7.5
--- U
443
76
--- U
830
224
--- U
5.6
132
U
U
2.1
4.0 J
0.30 J
14435
571
0.18 J
--- U
1.8 J
0.49 J
-- U
- U
0.46 J
1
0.61 J
TESTED
1680
5.67
14
6.70
9.50
+117
2.26
6.9
2.06
1360
82
--- U
1400
108
--- U
18
420
U
U
11
9.0
0.45 J
25865
756
U
U
2.1J
1.0 J
--- U
0.49 J
U
1
--- U
TESTED
2582
3.37
16
9.03
16.33
+137
9.73
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Trip Analysis Method
Blank Date Analyst Code
12/12/22 JWT 4500HB-11
12/14/22 TRJ 353.2 R2-93
12/16/22 JDJ 2320B-11
12/20/22 BLV 4500CLB-11
12/14/22 HMM 450OCNE-16
12/13/22 JDJ D5907-13
12/15/22 BNC D5907-13
12/14/22 DRC 4500SO42E11
12/20/22 NAB EPA200.8
12/16/22 NAB BPA200.8
12/16/22 NAB EPA200.8
12/19/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/14/22 MTM EPA200.7
12/14/22 MTM EPA200.7
12/16/22 NAB EPA200.8
12/27/22 DRC 245.1 R3-94
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/21/22 NAB EPA200.8
12/16/22 NAB EPA200.8
12/20/22 NAB EPA200.8
12/12/22 JWT 2510E-11
12/12/22 PJC 45000G-16
12/12/22 PJC 2550B-10
12/12/22 JWT
12/12/22 JWT
12/12/22 JWT 2580B-11
12/12/22 JWT 2130E-11
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

Enwkmug[W Flo hmpuMd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PESTICIDES AND PCB'S
Fva MRTRnn SOS1B R2 (07)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/15/22
DATE ANALYZED: 12/28/22
DATE REPORTED: 03/29/23
PARAMETERS, ug/l
MDL
MRL
MW-4
MW-5
MW-7
1.
Aldrin
0.029
0.050
---
U
---
U
---
U
2.
Alpha-BHC
0.032
0.050
---
U
---
U
---
U
3.
Beta-BHC
0.031
0.050
---
U
---
U
---
U
4.
Delta-BHC
0.030
0.050
---
U
---
U
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
---
U
---
U
6.
Chlordane
0.320
0.500
---
U
---
U
---
U
7.
4,4-DDD
0.051
0.100
---
U
---
U
---
U
S.
4,4-DDE
0.049
0.100
---
U
---
U
---
U
9.
4,4-DDT
0,052
0.100
---
U
---
U
---
U
10.
Dieldrin
0.042
0.075
---
U
---
U
---
U
11.
Endosulfan I
0.056
0.100
---
U
---
U
---
U
12.
Endosulfan II
0.046
0.100
---
U
---
U
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
---
U
---
U
14.
Endrin
0.053
0.100
---
U
---
U
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
---
U
---
U
16.
Heptachlor
0.039
0.050
---
U
---
U
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
---
U
---
U
18.
Methoxychlor
0.530
1.000
---
U
---
U
---
U
19.
Pcb-s (Aroclors)
0.500
2.000
---
U
---
U
---
U
20.
Toxaphene
0.690
1.500
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Flo hmpughd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/14/22
DATE REPORTED: 03/29/23
Date Analyzed:
12/15/22
12/15/22
12/16/22
MW-4
MW-5
MW-7
PARAMETERS, ug/1
MDL MRL
1.
2,4-D
0.36
2.000
--- U
--- U
--- U
2.
Dinoseb
0.54
1.000
--- U
--- U
--- U
3.
2,4,5-TP
0.42
2.000
--- U
--- U
--- U
4.
2,4,5-T
0.47
2.000
--- U
--- U
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

�IIII1Yl�ll O�Illlu��� �� ���O��IJ�OpO ��i Drinking Water ID: 37715
LLL���LLLIIIIIIJJJ 1:J LI LLLIIILLLIIILILI �' 4laata`uaYwr TOe 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
1
REVIEWED BY: _//„///
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 1
DATE EXTRACTED: 12/13/22
DATE REPORTED: 03/29/23
SEMI -VOLATILE ORGANICS
FDa MF.Twnn R270E R6 (18)
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/16/22
MW-4
12/16/22
MW-5
01/04/23
MW-7
1.
Acenaphthene
2.66
10.000
---
U
---
U
---
U
2.
Acenaphthylene
2.60
10.000
---
U
---
U
---
U
3.
Anthracene
2.97
10,000
---
U
---
U
---
U
4.
Benzo[a]antrhacene
4.16
10.000
---
U
---
U
---
U
5.
Benzo[b)fluoranthene
3.32
10.000
---
U
---
U
---
U
6.
Benzo[k)fluoranthene
4.23
10.000
---
U
---
U
---
U
7.
Benzo[g,h,i)perylene
2.61
10.000
---
U
---
U
---
U
B.
Benzo[a)pyrene
3.27
10.000
---
U
---
U
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10.000
---
U
---
U
---
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
---
U
---
U
11.
Bis(2-Chloroethoxy) Methane
3.14
10.000
---
U
---
U
---
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
---
U
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
---
U
---
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
---
U
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
---
U
---
U
16.
Chrysene
4.04
10.000
---
U
---
U
---
U
17.
Dibenzo[a,h)anthracene
2.78
10.000
---
U
---
U
--
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
---
U
---
U
19.
Dimethyl Phthalate
3.78
10.000
---
U
---
U
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
---
U
---
U
21.
2,4-Dinitrotolvene
3.95
10.000
---
U
---
U
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
---
U
---
U
23,
Di-N-Octyl Phthalate
2.81
10.000
---
U
---
U
---
U
24.
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
---
U
--
U
25.
Fluoranthene
3.92
10.000
---
U
---
U
---
U
26.
Fluorene
2.95
10.000
---
U
---
U
---
U
27.
Hexachlorobenzene
2.61
10.000
---
U
---
U
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
---
U
---
U
29.
Indeno[1,2,3-Cd)pyrene
2.91
10.000
---
U
---
U
---
U
30.
isophorone
3.74
10.000
---
U
---
U
---
U
31.
Nitrobenzene
2.85
10.000
---
U
---
U
___
U
32.
N-Nitrosodimethylamine
4.25
10.000
---
U
---
U
-__
U
33.
N-Nitrosodiphenylamine
3.95
10.000
---
U
---
U
---
U
34.
N-Nitroeodi-N-Propylamine
4.06
10.000
---
U
---
U
U
35,
Phenanthrene
3.24
10.000
---
U
---
U
---
U
36.
Pyrene
3.63
10.000
---
U
---
U
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
---
U
---
U
38.
2-Chlorophenol
2.75
10. 000
---
U
---
U
---
U
39.
O-Cresol
3.68
10.000
---
U
---
U
-__
U
40.
P-Cresol
4.12
10.000
---
U
---
U
- __
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
---
U
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
---
U
-- _
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
---
U
U
44,
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
---
U
--
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
---
U
--
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
---
U
-
U
47.
Methyl Methaneeulfonate
4.92
1 10.000
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ERW'Unmu(M Flo hCupamho
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
CLIENT ID:
PHONE [phone]
FAX [phone]
6003
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/13/22
/j DATE REPORTED: 03/29/23
REVIEWED BY: ✓�/� .�J
SEMI -VOLATILE ORGANICS
F.PA MRTwon 8270E R6(18)
PARAMETERS, Ug/l
Date Analyzed:
MDL MRL
12/16/22
MW-4
12/16/22
MW-5
01/04/23
MW-7
48.
2-Nitrophenol
3.64
10.000
---
U
---
U
---
U
49.
4-Nitrophenol
3.17
50.000
---
U
---
U
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
---
U
---
U
51.
Phenol
1.86
10.000
---
U
---
U
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
---
U
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
---
U
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
---
U
-"-
U
55.
Acetophenone
2.89
10.000
---
U
---
U
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
---
U
"-"
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
---
U
"--
U
58.
Benzyl Alcohol
4.47
20.000
---
U
---
U
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
---
U
---
U
60.
chlorobenzilate
5.12
10.000
---
U
---
U
-"-
U
61.
Diallate
2.98
10.000
---
U
---
U
---
U
62.
Dibenzofuran
4.28
10.000
---
U
---
U
---
U
63.
3,31-Dichlorobenzidine
4.22
20.000
---
U
---
U
---
U
64.
Dimethoate
3.98
20.000
---
U
---
U
---
U
65,
P-Dimethylaminoazobenzene
2.89
10.000
---
U
---
U
--"
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
---
U
"--
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
---
U
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
---
U
"--
U
69.
Diphenylamine
5.10
10.000
---
U
---
U
-"
U
70.
Disulfoton
4.28
10.000
---
U
---
U
---
U
71.
Famphur
3.98
20.000
---
U
---
U
U
72.
Hexachloropropene
4.31
10.000
---
U
---
U
---
U
73.
Isoeafrole
2.88
10.000
---
U
---
U
---
U
2.78
20.000
---
U
---
U
---
U
74.
Kepone
U
---
U
75.
Methapyrilene
3.54
100.000
---
U
---
76.
3-Methylcholanthrene
4.21
10.000
---
U
---
U
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
---
U
---
U
78.
Methyl Parathion
4.32
10.000
---
U
---
U
---
U
79.
m-Cresol
3.81
10.000
---
U
---
U
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
---
U
---
U
81.
1-Naphthylamine
5.61
10.000
---
U
---
U
-""
U
82.
2-Naphthylamine
4.62
10.000
---
U
---
U
---
U
83.
2-Nitroaniline
3.61
50.000
---
U
---
U
"--
U
84.
3-Nitroaniline
4.81
50.000
---
U
---
U
"--
U
85.
4-Nitroaniline
4.22
20.000
---
U
---
U
---
U
86.
5-Nitro-O-Toluidine
4.01
10. 000
---
U
---
U
"--
U
87.
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
---
U
--_
U
88.
N-Nitrosodiethylamine
3.83
20.000
---
U
---
U
---
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
---
U
--_
U
90.
N-Nitroeopiperidine
5.19
20.000
---
U
---
U
---
U
91.
N-Nitroeopyrrolidine
2.89
10.0 00
---
U
---
U
---
U
92.
Parathion
3.12
10.000
---
U
---
U
___
U
93.
Pentachlorobenzene
3.92
10.000
---
U
---
U
___
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 2

Enwk(DRE&W Flo
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PHONE [phone]
FAX [phone]
CLIENT: C &
D DISPOSAL, INC.
CLIENT ID:
6003
MR.
JUDSON WHITEHURST
802
RECYCLING LANE
ANALYST:
HIC
GREENVILLE, NC 27834
DATE COLLECTED:
12/12/22 Page: 3
DATE EXTRACTED:
12/13/22
v
DATE REPORTED:
03/29/23
REVIEWED BY:
.
SEMI -VOLATILE
ORGANICS
wnm TAWTUnn R97nR R6 (18)
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/16/22
MW-4
12/16/22
MW-5
01/04/23
MW-7
95.
Phenacetin
4.41
20.000
---
U
--"
U
--
U
96.
1,4-Benzenediamine
2.99
10.000
---
U
---
U
---
U
3.86
10.000
---
U
---
U
- __
U
97.
Phorate
---
U
--_
U
98.
Pronamide
3.69
10.000
---
U
99.
Saf role
4.12
10.000
---
U
---
U
U
100.
1,2,4,5-Tetrachlorobenzene
5.01
10.000
---
U
---
U
-_ -
U
101.
Thionazin
4.62
20.000
---
U
---
U
---
U
102.
O-Toluidine
4.11
10.000
---
U
---
U
___
U
103.
1,3,5-Trinitrobenzene
3.98
10.000
---
U
---
U
___
U
104.
0,0,0-Triethyl Phosphorothioate
3.61
10.000
---
U
---
U
U
105.
Hexachloroethane
1.49
10.000
---
U
---
U
U
106.
Ieodrin
3.11
1 20.000
---
U
"--
U
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

��1Y/��OIIIIIIIIII�UII� �0 ���OP���OP p���� Drinking Water ID: 37715
LLL���LLLIIILLLJII 1J IIIJJJ LJIJLLIIUUIIJJ lJ IIISSS u' Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
vva ivmsrmunn R26nn R4 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 1
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/29/23
PARAMETERS, ug/l
MDL
MRL
MW-4
MW-5
MW-7
Trip
Blank
1.
Chloromethane
0.77
3.000
---
U
---
U
---
U
'--
U
2.
Vinyl Chloride
0.12
0.200
---
U
---
U
---
U
---
U
3.
Bromomethane
0.67
10.000
---
U
---
U
---
U
---
U
4.
Chloroethane
0.48
10.000
---
U
---
U
---
U
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
_--
U
---
U
--'
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
---
U
---
U
---
U
7.
Acetone
9.06
100.000
---
U
---
U
---
U
---
U
U
S.
Iodomethane
0.26
10.000
---
U
---
U
---
U
---
9.
Carbon Disulfide
0.23
100.000
---
U
---
U
---
U
---
U
10.
Methylene Chloride
0.64
1.000
---
U
---
U
---
U
---
U
11.
trans-1,2-Dichloroethene
023 ..
5 000
---
U
---
U
---
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
---
U
---
U
13.
Vinyl Acetate
0,20
50.000
---
U
---
U
---
U
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
---
U
---
U
---
U
15.
2-Butanone
2.21
100.000
---
U
U
---
U
---
U
U
16.
Bromochloromethane
0.27
3.000
---
U
---
U
---
U
---
17.
Chloroform
0.25
5.000
---
U
---
U
---
U
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
---
U
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
---
U
---
U
---
U
0.24
1.000
---
U
---
U
---
U
-__
U
20.
Benzene
---
U
---
U
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
U
U
22.
Trichloroethene
0.23
1.000
---
U
---
U
---
U
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
___
U
-__
U
___
U
24.
Bromodichloromethane
0.04
0.200
---
U
---
U
---
U
---
25.
Cis-1,3-Dichloropropene
0.06
0.200
---
U
---
U
---
U
---
U
U
26.
4-Methyl-2-Pentanone
1,19
100.000
---
U
---
U
---
U
---
U
27.
Toluene
0.23
1.000
---
U
U
---
U
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
---
U
---
U
---
U
29,
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
---
U
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
U
---
U
---
U
31.
2-Hexanone
1.57
50.000
---
U
---
U
---
U
U
---
___
U
32,
Dibromochloromethane
0.03
0.200
---
U
---
U
---
U
33.
1,2-Dibromoethane
0.03
0.200
---
U
---
U
---
U
___
U
34.
Chlorobenzene
0.30
3.000
---
U
---
U
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
___
U
___
U
___
U
36.
Ethylbenzene
0.21
1.000
---
U
---
U
---
U
---
U
37.
Xylenee
0.68
5.000
---
U
---
U
___
U
-__
U
38.
Dibromomethane
0.28
10.000
---
U
---
U
---
U
---
U
0.19
1.000
---
U
---
U
---
U
=_-
39,
Styrene
---
U
---
U
-
U
40.
Bromoform
0.20
3.000
---
U
U
41.
1, 1,2,2-Tetrachloroethane
0.03
0.200
---
U
'--
U
---
U
-'-
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
---
U
---
U
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
---
U
---
---
U
U
---
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
---
U
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
---
U
---
U
2.72
200.000
---
U
---
U
-_-
U
-
46.
47.
Acrylonitrile
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
--
U
U
---
U
U
1.97
4.000
---
U
---
U
---
U
48.
Acrolein
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Eimwkwu(W Flo lumpudid
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: ,-
LANDFILL APPENDIX II
was MPTWnn R260n R4 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/12/22
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/29/23
PARAMETERS, ug/l
MDL
MRL
MW-4
MW-5
MW-7
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
---
U
---
U
---
U
U
50.
Chloroprene
0.21
20.000
---
U
---
U
---
U
-
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5,000
---
U
---
U
---
U
---
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
U
---
U
U
54.
2,2-Dichloropropane
0.17
000 15
.
U
---
U
-- _
U
U
55.
1,1-Dichloropropene
2
0.2.
5000
U
U
---
U
---
U
56,
Ethyl Methacrylate
0.16
10.000
---
U
---
U
---
U
___
-
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
---
U
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
---
U
---
U
U
59.
Meth acrylonitrile
1.93
100.000
---
U
---
U
---
U
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
---
U
---
U
---
---
U
61.
Naphthalene
0.47
6.000
---
U
---
U
---
U
U
62.
Propionitrile
3.26
150.000
---
U
---
U
---
U
---
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
---
U
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
---
U
---
-
U
0.39
1.000
---
U
4.62
12.00
__
65.
Tetrahydrofuran
29.20
11.20
__ -
U
66.
1,4-Dioxane
2.71
3.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 2

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EmwkwEW % hmpudid
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
PHONE [phone]
FAX [phone]
ID#: 6003 B
DATE COLLECTED: 12/12/22
DATE REPORTED : 03/17/23
REVIEWED BY:
MW-13 Trip
Analysis
Method
MDL
MRL
Blank
Date Analyst
Code
PARAMETERS
7 2
12/12/22 JWT
4500HB-11
PH (field measurement), Unite
7.76
12/14/22 TRJ
353.2 R2-93
Nitrate+Nitrite as N, mg/l
0.04
0.04
166
12/16/22 JDJ
2320B-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
11
12/20/22 BLV
4500CLB-11
Chloride, mg/l
1.0
1.0
U
12/14/22 HMM
4500CNS-16
Cyanide, ug/1
50
.
5.0
---
370
12/13/22 JDJ
D5907-13
Total Dissolved Residue, mg/l
10
10
106
12/14/22 DRC
45005042E11
Sulfate, mg/l
5 0
5.0
U
12/20/22 NAB
BPA200.8
Antimony, ug/l
0.30
1.0
5.0
__
1.8 J
12/16/22 NAB
EPA200.8
Arsenic, ug/l
0.13
88.6
12/16/22 NAB
EPA200.8
Barium, ug/1
0.14
10.0
U
12/19/22 NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
U
12/16/22 NAB
EPA200.8
Cadmium, ug/1
0. 19
1.0
---
0.25 J
12/16/22 NAB
SPA200.8
Cobalt, ug/l
0.10
1.0
0.58 J
12/16/22 NAB
EPA200.8
Total Chromium, ug/l
0.19
5.0
0.76 J
12/16/22 NAB
EPA200.8
Copper, ug/1
0.26
10.0
4076
12/14/22 MTM
EPA200.7
Iron, ug/1
12.20
50.0
20
12/14/22 MTM
EPA200.7
Manganese, ug/l
2.70
10.0
5.0
0.25 J
12/16/22 NAB
EPA200.8
Lead, ug/1
0.09
U
12/27/22 DRC
245.1 R3-94
Mercury, ug/1
008
.
0.20
---
0.79 J
12/16/22 NAB
EPA200.8
Nickel, ug/1
0.13
10.0
0.66 J
12/16/22 NAB
EPA200.8
Selenium, ug/l
0.43
10.0
U
12/16/22 NAB
EPA200.8
Silver, ug/1
0.14
5.0
U
12/16/22 NAB
EPA200.8
Thallium, ug/1
0.13
1.0
---
U
12/21/22 NAB
EPA200.8
Tin, ug/l
0.36
100.0
---
4
12/16/22 NAB
SPA200.8
Vanadium, ug/1
0.14
1.0
2.9J
12/20/22 NAB
EPA200.8
Zinc, ug/l
0.34
10.0
Sulfide, ug/l
100
1000
TESTED
624
12/12/22 JWT
2510B-11
Conductivity (at 25c), uMhos/cm
1.0
1.0
12/12/22 Pic
45000G-16
Dissolved Oxygen, mg/l
0.1
0.1
4.87
15
12/12/22 PJC
255OB-10
Temperature, °C
10.00
12/12/22 JWT
Static Water Level, feet
20.68
12/12/22 JWT
Well Depth, feet
+92
12/12/22 JWT
2580B-11
ORP, my
1.0
1.0
21.30
12/12/22 JWT
2130E-11
Turbidity (Field), NTU
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

Endonfin(M Flo hmpudbd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JiMSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
JJ
REVIEWED BY:
PESTICIDES AND PCB'S
ccn mumunn RnRlB R2 (07)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/15/22
DATE ANALYZED: 12/28/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
�MW-13
1.
Aldrin
0.029
0.050
---
U
2.
Alpha-BHC
0.032
0.050
---
U
3.
Beta-BHC
0.031
0.050
---
U
4.
Delta-BHC
0.030
0.050
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
6.
Chlordane
0.320
0.500
---
U
0.051
0.100
---
U
7.
4,4-DDD
0.049
0.100
---
U
B.
4,4-DDE
0.052
0.100
---
U
9,
4,4-DDT
10.
Dieldrin
0.042
0.075
---
U
11.
Endosulfan I
0.056
0.100
---
U
12.
Endosulfan iI
0.046
0.100
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
14.
Endrin
0.053
0.100
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
16.
Heptachlor
0.039
0.050
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
18.
Methoxychlor
0.530
1.000
---
U
19.
Pcb's (Aroclore)
0.500
2.000
---
U
20.
Toxaphene
0.690
1.500
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EWOTOREW Flo hmpo mW
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: ✓ J
LANDFILL APPENDIX II
vva MF.THnn 8151A R1(96)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/14/22
DATE ANALYZED: 12/23/22
DATE REPORTED: 03/17/23
MW-13
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
2. Dinoseb
0.54
1.000
--- U
0.42
2.000
0.615 J
3. 2,4,5-TP
4. 2,4,5-T
0.47
2.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
Wastewater ID: 10
ERWITuME&W Flo hmpudid
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: C &
D DISPOSAL, INC.
CLIENT ID:
6003 B
MR.
JUDSON WHITEHURST
802
RECYCLING LANE
ANALYST:
HIC
12/12/22
GREENVILLE, NC 27834
DATE COLLECTED:
DATE EXTRACTED:
12/13/22
DATE ANALYZED:
12/16/22
l/��
DATE REPORTED:
03/17/23
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
MW-13
PARAMETERS, ug/1 MDL MRL
1. ACenaphthene
2.66
10.000
--- U
2. Acenaphthylene
2.60
10.000
--- U
2.97
10,000
--- U
3. Anthracene
--- U
4. Benzo[alantrhacene
4.16
10.000
5. Benzo[b]fluoranthene
3.32
10.000
--- U
6. Benzo[klfluoranthene
4.23
10.000
--- U
7. Benzo[g,h,ilperylene
2.61
10.000
--- U
3.27
10.000
--- U
B. Benzo[alpyrene
9. 4-Bromophenyl Phenyl Ether
2.63
10.000
--- U
10. Butyl Henzyl Phthalate
5.78
10.000
--- U
11. Bis(2-Chloroethoxy) Methane
3.14
10.000
--- U
12, Bie(2-Chloroethyl) Ether
2.58
10.000
--- U
13. Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
--- U
14. 2-Chloronaphthalene
2.17
10.000
--- U
15. 4-Chlorophenyl Phenyl Ether
2.42
10.000
--- U
4.04
10.000
--- U
16. Chry sane
--- U
17. Dibenzo[a,hlanthracene
2.78
10.000
18. Di-N-Butyl Phthalate
3.09
10.000
--- U
19, Dimethyl Phthalate
3.78
10.000
--- U
20. Diethyl Phthalate
3.92
10.000
--- U
21. 2,9-Dinitrotoluene
3.95
10.000
--- U
22. 2,6-Dinitrotoluene
3.88
10.000
--- U
23. Di-N-Octyl Phthalate
2.81
10.000
--- U
24. Hie-(2-Ethylhexyl) Phthalate
9.97
15.000
--- U
3.92
10.000
--- U
25. Fluoranthene
--- U
26. Fluorene
2.95
10.000
U
27. Hexachlorobenzene
2.61
10.000
---
28. Hexachlorocyclopentadiene
4.16
10.000
--- U
29, indeno[1,2,3-Cdlpyrene
2.91
10.000
--- U
3.74
10.000
--- U
30. Isophorone
--- U
31. Nitrobenzene
2.85
10.000
U
32. N-Nitrosodimethylamine
4.25
10.000
---
33. N-Nitrosodiphenylamine
3.95
10.000
--- U
34. N-Nitrosodi-N-Propylamine
4.06
10.000
--- U
3.24
10.000
--- U
35. Phenanthrene
--- U
36. Pyrene
3.63
3.79
10.000
20.000
--- U
37. 4-Chloro-3-Methylphenol
38. 2-Chlorophenol
2.75
10.000
--- U
3.68
10.000
--- U
39. 0-Cresol
--- U
40. P-Cresol
4.12
10.000
U
41. 2,4-Dichlorophenol
5.19
10.000
---
42. 2,6-Dichlorophenol
4.89
10.000
--- U
43. 2,4-Dimethylphenol
3.21
10.000
--- U
44. 4,6-Dinitro-2-Methylphenol
4.77
50.000
--- U
45. 2,4-Dinitrophenol
4.37
50.000
--- U
46, Ethyl Methanesulfonate
5.26
20.000
--- U
47. Methyl Methaneeulfonate
4.92
10.000
--- U
3.64
10.000
--- U
48. 2-Nitrophenol
,7 = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 1

EADmE[i (W Flo hmpudid
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
J
REVIEWED BY: ....///���-
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 2
DATE EXTRACTED: 12/13/22
DATE ANALYZED: 12/16/22
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
Fva mwTwnn 8270E R6 (18)
PARAMETERS, Ug/l MDL MRL
MW-13
49. 4-Nitrophenol
3.17
50.000
--- U
50. Pentachlorophenol
5.33
25.000
--- U
51. Phenol
1.86
10.000
--- U
52. 2,3,4,6-Tetrachlorophenol
3.12
10.000
--- U
53. 2,4,5-Trichlorophenol
4.17
10.000
--- U
54. 2,4,6-Trichlorophenol
3.84
10.000
--- U
55. Acetophenone
2.89
10.000
--- U
56. 2-Acetylaminofluorene
3.98
20.000
--- U
57. 4-Aminobiphenyl
4.12
20.000
--- U
58. Benzyl Alcohol
4.47
20.000
--- U
59. 4-Chloroaniline
3.36
20.000
--- U
60. Chlorobenzilate
5.12
10.000
--- U
61. Diallate
2.98
10.000
--- U
62. Dibenzofuran
4.28
10.000
--- U
63. 3,31-Dichlorobenzidine
4.22
20.000
--- U
64. Dimethoate
3.98
20.000
--- U
65. P-Dimethylaminoazobenzene
2.89
10.000
--- U
66. 7,12-Dimethylbenz[a]anthracene
5.26
10.000
--- U
67. 3,3-Dimethylbenzidine
3.21
10.000
--- U
68. 1,3-Dinitrobenzene
2.89
20.000
--- U
69. Diphenylamine
5.10
10.000
--- U
70. Disulfoton
4.28
10.000
--- U
71. Famphur
3.98
20.000
--- U
72, Hexachloropropene
4.31
10.000
--- U
73. Isosafrole
2.88
10.000
--- U
2.79
20.000
--- U
74. Repone
75. Methapyrilene
3.54
100.000
--- U
76. 3-Methylcholanthrene
4.21
10.000
--- U
77. 2-Methylnaphthalene
3.79
10.000
--- U
78. Methyl Parathion
4.32
10.000
--- U
79. m-Cresol
3.81
10.000
--- U
80. 1,4-Naphthoquinone
4.00
10.000
--- U
81. 1-Naphthylamine
5.61
10.000
--- U
82. 2-Naphthylamine
4.62
10.000
--- U
83, 2-Nitroaniline
3.61
50.000
--- U
84. 3-Nitroaniline
4.81
50.000
--- U
85. 4-Nitroaniline
4.22
20.000
--- U
86. 5-Nitro-O-Toluidine
4.01
10.000
--- U
87. N-Nitrosodi-n-butylamine
3.63
10.000
--- U
88. N-Nitrosodiethylamine
3.83
20.000
--- U
89. N-Nitrosomethylethylamine
3.83
10.000
--- U
90. N-Nitrosopiperidine
5.19
20.000
--- U
91, N-Nitrosopyrrolidine
2.89
10.000
--- U
92. Parathion
3.12
10.000
--- U
93, Pentachlorobenzene
3.92
10.000
--- U
94. Pentachloronitrobenzene
3.71
20.000
--- U
95, Phenacetin
4.41
20.000
--- U
96. 1,4-Benzenediamine
2.99
10.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

kn w'n �nrnurP-n� � - inn (ono �nnr n. �a A
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 3
DATE EXTRACTED: 12/13/22
DATE ANALYZED: 12/16/22
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
FPA METHOD 8270E R6(18)
PARAMETERS, ug/l MDL MRL
MW-13
97. Phorate
3.86
10.000
--- U
98. Pronamide
3.69
10.000
--- U
99. Safrole
4.12
10.000
--- U
100. 1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
101. Thionazin
4.62
20.000
--- U
102. 0-Toluidine
4.11
10.000
--- U
103. 1,3,5-Trinitrobenzene
3.98
10.000
--- U
104. 0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
105. Hexachloroethane
1.49
10.000
--- U
106. Isodrin
3.11
20.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ElMomfiHM alp hwPuMd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR.. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
coa mpTunn R26nD R4(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 1
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/1 MDL MRL
MW-13
Trip
Blank
1. Chloromethane
0.77
3.000
--- U
--- U
2. Vinyl Chloride
0.12
0,200
--- U
--- U
3. Bromome thane
0.67
10.000
--- U
- U
4. Chloroethane
0.48
10.000
--- U
--- U
5. Trichlorofluoromethane
0.24
1.000
--- U
--- U
6. 1,1-Dichloroethene
0.17
5.000
--- U
--- U
9.06
100.000
--- U
--- U
7. Acetone
U
--- U
8. Iodomethane
0.26
10.000
---
9. Carbon Disulfide
0.23
100.000
--- U
--- U
10, Methylene Chloride
0.64
1.000
--- U
--- U
11. trans-1,2-Dichloroethene
0.23
5.000
--- U
--- U
12. 1,1-Dichloroethane
0.20
5.000
--- U
--- U
13. Vinyl Acetate
0.20
50.000
--- U
--- U
14. Cie-1,2-Dichloroethene
0.25
5.000
--- U
--- U
2.21
100.000
--- U
--- U
15. 2-Butanone
--- U
16. Bromochloromethane
0.27
3.000
--- U
17. Chloroform
0.25
5.000
--- U
--- U
18. 1,1,1-Trichloroethane
0.19
1.000
--- U
--- U
19. Carbon Tetrachloride
0.04
0.200
--- U
--- U
0.24
1.000
--- U
--- U
20. Benzene
--- U
--- U
21. 1,2-Dichloroethane
0.02
0.200
22. Trichloroethene
0.23
1.000
--- U
--- U
23, 1,2-Dichloropropane
0.04
0.200
--- U
--- U
24. Bromodichloromethane
0.04
0.200
--- U
--- U
25. Cie-1,3-Dichloropropene
0.06
0.200
--- U
--- U
26. 4-Methyl-2-Pentanone
1.19
100.000
--- U
--- U
27. Toluene
0.23
1.000
--- U
--- U
28. trans-1,3-Dichloropropene
0.04
0.200
--- U
--- U
29. 1,1,2-Trichloroethane
0.03
0.200
--- U
--- U
30. Tetrachloroethene
0.10
0.200
--- U
--- U
1.57
50.000
--- U
--- U
31. 2-Hexanone
--- U
32. Dibromochloromethane
0.03
0.200
--- U
33. 1,2-Dibromoethane
0.03
0.200
--- U
--- U
34. Chlorobenzene
0.30
3.000
--- U
--- U
35. 1,1,1,2-Tetrachloroethane
0.22
1.000
--- U
--- U
36. Ethylbenzene
0.21
1.000
--- U
--- U
37. Xylenes
0.68
5.000
--- U
--- U
38, Dibromomethane
0.28
10.000
--- U
- U
0.19
1,000
--- U
-_- U
39. Styrene
U
- U
40. Bromoform
0.20
3.000
---
41. 1,1,2,2-Tetrachloroethane
0.03
0.200
--- U
--- U
42. 1,2,3-Trichloropropane
0.09
0.200
--- U
--- U
43. 1,4-Dichlorobenzene
0.39
1.000
--- U
--- U
44. 1,2-Dichlorobenzene
0.32
5.000
--- U
--- U
45. 1,2-Dibromo-3-Chloropropane
0.07
0.200
--- U
--- U
46, Acrylonitrile
2.72
200.000
--- U
--- U
47. trans-1,4-Dichloro-2-Butene
0.42
100.000
--- U
- U
48. Acrolein
1.97
4.000
--- U
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enw,umEgM Flo DEwpwm%d
Drinking Water ID: 37715
W-tnwatar ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: z�-
LANDFILL APPENDIX II
wma mwTunn R260n R4 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 2
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-13
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
---
U
50.
Chloroprene
0.21
20.000
---
U
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
53.
1,3-Dichloropropane
0.26
1.000
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
---
U
59,
Methacrylonitrile
1.93
100.000
---
U
---
U
60,
Methyl Methacrylate
0.25
30.000
---
U
---
U
61.
Naphthalene
0.47
6.000
---
U
---
U
62,
Propionitrile
3.26
150.000
---
U
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
65.
Tetrahydrofuran
0.39
1.000
---
U
---
U
66.
1,4-Dioxane
2.71
3.000
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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EmwkwuM Flo ��c�or�poQ���d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
Drinking Water ID: 37715
Wastewater ID: 1.0
PHONE [phone]
FAX [phone]
ID#: 6003 A
DATE COLLECTED: 12/12/22
DATE REPORTED : 03/17/23
REVIEWED BY:
MW-2S
MW-38 Trip
Analysis
Method
Blank
Date Analyst
Code
PARAMETERS
MDL
MRL
9.1
MISSING
12/12/22 JWT
4500HB-11
PH (field measurement), Units
12/14/22 TRJ
353.2 R2-93
Nitrate+Nitrite as N, mg/1
0.04
0.04
0.52
MISSING
12/14/22 JDJ
2320B-11
2320H-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
25
MISSING
12/16/22 BLV
Chloride, mg/1
1.0
1.0
31
MISSING
12/20/22 HMV
4500CLB-11
450OCNE-
Cyanide, ug/l
5.0
5.0
--- U
MISSING
12/14/22 JDJ
907-13
Total Dissolved Residue, mg/1
10
10
180
MISSING
12/14/22 DRC
4500SO42Ell
Sulfate, mg/1
5.0
5.0
60.2
MISSING
12/20/22 NAB
EPA200.8
Antimony, ug/l
0.30
1.0
--- U
MISSING
12/16/22 NAB
EPA200.8
Arsenic, ug/1
0.13
5.0
0.38 J
MISSING
12/16/22 NAB
EPA200.8
Barium, ug/1
0.14
10.0
3.9J
MISSING
12/19/22 NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
--- U
MISSING
12/16/22 NAB
EPA200.8
Cadmium, ug/1
0.19
1.0
--- U
MISSING
12/16/22 NAB
EPA200.8
Cobalt, ug/l
0.19
--- U
MISSING0
12/16/22 NAB
EPA200.8
Total Chromium, ug/1
0.1
5.0
5.
--- U
MISSING
12/16/22 NAB
EPA200.8
Copper, ug/l
0.26
10.0
--- U
MISSING
12/14/22 MTM
SPA200.7
Iron, ug/1
12.20
--- U
MISSING
12/14/22 MTM
EPA200.7
Manganese, ug/l
2.09
10.0
15.0
--- U
MISSING
12/16/22 NAB
EPA200.8
Lead, ug/l
0.08
5.0
--- U
MISSING
12/27/22 DRC
245.1 R3-94
Mercury, ug/l
0.13
U
MISSING
MISSING
12/16/22 NAB
EPA200.8
Nickel, ug/l
0.43
10.0
10.0
.8 J
12/16/22 NAB
EPA200.8
Selenium, ug/l
0.14
15.0
---
--- U
MISSING
12/16/22 NAB
EPA200.8
Silver, ug/l
0.14
5.0
--- U
MISSING
MISSING
12/16/22 NAB
EPA200.8
Thallium, ug/l
0.
.0
--- U
U
MISSING
12/21/22 NAB
EPA200.8
Tin, ug/1
0. 36
100.0
---
4
MISSING
12/16/22 NAB
EPA200.8
Vanadium, ug/1
14
0.14
1
1.0
U
MISSING
12/20/22 NAB
SPA200.8
Zinc, ug/1
0.34
10.0
---
4500S2D-11
Sulfide, ug/l
100
1.0
TESTED
MISSING0
12/12/22 JWT
2510E-11
Conductivity (at 25c), uMhos/cm
1.0
1
1.
332
MISSING
12/12/22 PJC
45000G-16
Dissolved Oxygen, mg/1
0.1
0.1
3.14
MISSING
12/12/22 PJC
2550E-10
Temperature, °C
16
13.21
MISSING
MISSING
12/12/22 JWT
Static Water Level, feet
16.57
MISSING
12/12/22 JWT
Well Depth, feet
MISSING
Method 8270E (duplicate)
MISSING
EPA Method 8081E (duplicate)
MISSING
82II (duplicate)
MISSING
82II (duplicate)
MISSING
SPA 8151A Duplicate (Landfill List)
MISSING
12/12/22 JWT
2580B-11
ORP, my
U
MISSING
12/12/22 JWT
2130B-11
Turbidity (Field), NTU
1.0
1.0
---
J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding results) are attached.

Enw,unflopid Flo hmpmUd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PESTICIDES AND PCB'S
EPA METHOD 8081B R2(07)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/15/22
DATE ANALYZED: 12/28/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-2S
1.
Aldrin
0.029
0.050
---
U
2.
Alpha-BHC
0.032
0.050
---
U
3.
Beta-BHC
0.031
0.050
---
U
4.
Delta-BHC
0.030
0.050
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
6.
Chlordane
0.320
0.500
---
U
7.
4,4-DDD
0.051
0.100
---
U
8.
4,4-DDE
0.049
0.100
---
U
9.
4,4-DDT
0.052
0.100
---
U
10.
Dieldrin
0.042
0.075
---
U
11.
Endosulfan I
0.056
0.100
---
U
12.
Endosulfan II
0.046
0.100
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
14.
Endrin
0.053
0.100
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
16.
Heptachlor
0.039
0,050
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
18.
Methoxychlor
0.530
1.000
---
U
19.
Pcb's (Aroclors)
0.500
2.000
---
U
20.
Toxaphene
0.690
1.500
---
U
a = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EmAmIMMEM Flo himpuMd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/14/22
DATE ANALYZED: 12/15/22
DATE REPORTED: 03/17/23
MW-2S
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
2. Dinoseb
0.54
1.000
--- U
3. 2,4,5-TP
0.42
2.000
--- U
4. 2,4,5-T
0.47
2.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

NnAnIME&M Flo hcupw0d
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
J
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 1
DATE EXTRACTED: 12/13/22
DATE ANALYZED: 12/16/22
DATE REPORTED: 03/17/23
PARAMETERS, Ug/l
MDL
MRL
MW-2S
1.
Acenaphthene
2.66
10.000
---
U
2.
Acenaphthylene
2.60
10.000
---
U
3.
Anthracene
2.97
10.000
---
U
4.
Benzo[a)antrhacene
4.16
10.000
---
U
5.
Benzo[b)fluoranthene
3.32
10.000
---
U
6.
Benzo[k)fluoranthene
4.23
10.000
---
U
7.
Benzo[g,h,i)perylene
2.61
10,000
---
U
8.
Benzo[a)pyrene
3.27
10.000
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10.000
---
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
11.
Bis(2-Chloroethoxy) Methane
3.14
10.000
---
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
16.
Chrysene
4.04
10.000
---
U
17.
Dibenzo[a,h]anthracene
2.78
10.000
---
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
19.
Dimethyl Phthalate
3.78
10.000
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
21.
2,4-Dinitrotoluene
3.95
10.000
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
23.
Di-N-Octyl Phthalate
2.81
10.000
---
U
24.
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
25.
Fluoranthene
3.92
10.000
---
U
26,
Fluorene
2.95
10.000
---
U
27.
Hexachlorobenzene
2.61
10.000
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
29.
Indeno[1,2,3-Cd)pyrene
2.91
10.000
---
U
30.
Isophorone
3.74
10.000
---
U
31.
Nitrobenzene
2.85
10.000
---
U
32,
N-Nitrosodimethylamine
4.25
10.000
---
U
33.
N-Nitrosodiphenylamine
3.95
10.000
---
U
34.
N-Nitrosodi-N-Propylamine
4.06
10.000
---
U
35.
Phenanthrene
3.24
10.000
---
U
36.
Pyrene
3.63
10.000
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
38.
2-Chlorophenol
2.75
10.000
---
U
39.
0-Cresol
3.68
10.000
---
U
40.
P-Cresol
4.12
10.000
---
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
44.
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
47.
Methyl Methanesulfonate
4.92
10.000
---
U
48.
2-Nitrophenol
3.64
10.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 2
DATE EXTRACTED: 12/13/22
DATE ANALYZED: 12/16/22
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/1
MDL
MRL
MW-2S
49.
4-Nitrophenol
3.17
50.000
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
51.
Phenol
1.86
10.000
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
55.
Acetophenone
2.89
10.000
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
60.
Chlorobenzilate
5.12
10.000
---
U
61.
Diallate
2.98
10.000
---
U
62.
Dibenzofuran
4.28
10.000
---
U
63.
3,31-Dichlorobenzidine
4.22
20.000
---
U
64.
Dimethoate
3.98
20.000
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
69.
Diphenylamine
5.10
10.000
---
U
70.
Disulfoton
4.28
10.000
---
U
71.
Famphur
3.98
20.000
---
U
72.
Hexachloropropene
4.31
10.000
---
U
73.
Isosafrole
2.88
10.000
---
U
74.
Kepone
2.78
20.000
---
U
75.
Methapyrilene
3.54
100.000
---
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
78.
Methyl Parathion
4.32
10.000
---
U
79.
m-Cresol
3.81
10.000
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
81,
1-Naphthylamine
5.61
10.000
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
83.
2-Nitroaniline
3.61
50.000
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
87.
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
88.
N-Nitrosodiethylamine
3.83
20.000
---
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
91.
N-Nitrosopyrrolidine
2.89
10.000
---
U
92.
Parathion
3.12
10.000
---
U
93.
Pentachlorobenzene
3.92
10.000
---
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
95.
Phenacetin
4.41
20.000
---
U
96.
1,4-Benzenediamine
2.99
10.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ERW'DT0[MflW % haboo umbd
Drinking Water ID: 37715
Hastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
MR. JUDSON WHITEHURST
802 RECYCLING LANE ANALYST: HIC
GREENVILLE, NC 27834 DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/13/22
DATE ANALYZED: 12/16/22
REVIEWED BY: DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l
MDL
MRL
MW-2S
97.
Phorate
3.86
10.000
--- U
98.
Pronamide
3.69
10.000
--- U
99.
Safrole
4.12
10.000
--- U
100.
1,2,4,5-Tetrachlorobenzene
5.01
10,000
--- U
101.
Thionazin
4.62
20.000
--- U
102.
O-Toluidine
4.11
10.000
--- U
103.
1,3,5-Trinitrobenzene
3.98
10.000
--- U
104.
0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
105.
Hexachloroethane
1.49
10.000
--- U
106.
Isodrin
3.11
20.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 3

[��doQo��c��� Flo D�c�oQpor���c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
Drinking Water ID: 37715
Wastewater IDS 10
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: JAP
DATE COLLECTED: 12/12/22
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-2S
Trip
Blank
1.
Chloromethane
0.77
3.000
---
U
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
---
U
3.
Bromomethane
0.67
10.000
---
U
---
U
4.
Chloroethane
0.48
10.000
---
U
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
---
U
7.
Acetone
9.06
100.000
---
U
---
U
8.
Iodomethane
0.26
10.000
---
U
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
---
U
10.
Methylene Chloride
0.64
1.000
---
U
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
13,
Vinyl Acetate
0.20
50.000
---
U
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
---
U
15.
2-Butanone
2.21
100.000
---
U
---
U
16.
Bromochloromethane
0.27
3.000
---
U
---
U
17.
Chloroform
0.25
5.000
---
U
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
---
U
20.
Benzene
0.24
1.000
---
U
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
U
---
U
22.
Trichloroethene
0.23
1.000
---
U
---
U
23.
1,2-Dichloropropane
0.04
0,200
---
U
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
---
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
---
U
27.
Toluene
0.23
1.000
---
U
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
---
U
31.
2-Hexanone
1.57
50.000
---
U
---
U
32.
Dibromochloromethane
0.03
0.200
---
U
---
U
33.
1,2-Dibromoethane
0.03
0.200
---
U
---
U
34.
Chlorobenzene
0.30
3.000
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
36.
Ethylbenzene
0.21
1.000
---
U
---
U
37.
Xylenes
0.68
5.000
---
U
---
U
38,
Dibromomethane
0.28
10.000
---
U
---
U
39.
Styrene
0.19
1.000
---
U
---
U
40.
Bromoform
0.20
3,000
---
U
---
U
41.
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
---
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
---
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
---
U
46.
Acrylonitrile
2.72
200.000
---
U
---
U
47.
trans-1,4-Dichloro-2-Butene
0,42
100.000
---
U
---
U
48.
Acrolein
1.97
4.000
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 1

EmAmmid % hrmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. =SON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: i��✓ J
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
Drinking Water ID: 37715
Wastewater III: 10
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 2
DATE ANALYZED: 12/20/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-2S
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
---
U
50.
Chloroprene
0.21
20.000
---
U
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
---
U
61.
Naphthalene
0.47
6.000
---
U
---
U
62.
Propionitrile
3.26
150.000
---
U
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
65.
Tetrahydrofuran
0.39
1.000
---
U
---
U
66.
1,4-Dioxane
2.71
3.000
4.01
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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ERW,0T@flE(bM Flo hmpumbd
Drinking Water IDo 37715
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 D
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE DATE COLLECTED: 12/12/22
GREENVILLE, NC 27834 DATE REPORTED : 03/23/23
REVIEWED BY:
MW-15
MW-16
MW-17
MW-14S
Trip Analysis
Method
PARAMETERS
MDL
MRL
Blank Date Analyst
Code
PH (field measurement), Unite
6.5
MISSING
6.6
6.8
12/12/22
JWT
4500HB-11
Nitrate+Nitrite as N, mg/l
0.04
0.04
5.41
MISSING
0.06
--- U
12/14/22
TRJ
353.2 R2-
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
76
MISSING
85
1700
12/16/22
JDJ
2320E-11
Chloride, mg/1
1.0
1.0
26
MISSING
19
361
12/20/22
BLV
4500CLB-1
Cyanide, ug/1
5.0
5.0
--- U
MISSING
--- U
6
12/14/22
HMM
450OCNE-1
Total Dissolved Residue, mg/l
10
10
590
MISSING
460
12/13/22
JDJ
D5907-13
Total Dissolved Residue, mg/l
10
10
2400
12/15/22
BNC
D5907-13
Sulfate, mg/1
5.0
5.0
265
MISSING
254
27.2
12/14/22
DEC
4500SO42E
Antimony, ug/l
0.30
1.0
0.44 J
MISSING
--- U
1.1
12/20/22
NAB
EPA200.8
Arsenic, ug/l
0.13
5.0
2.3 J
MISSING
1.0 J
64
12/16/22
NAB
EPA200.8
Barium, ug/1
0.14
10.0
153
MISSING
46.4
384
12/16/22
NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
0.32 J
MISSING
--- U
0.11 J
12/19/22
NAB
EPA200.8
Cadmium, ug/l
0.19
1.0
0.30 J
MISSING
--- U
--- U
12/16/22
NAB
EPA200.8
Cobalt, ug/l
0.10
1.0
0.92 J
MISSING
0.11 J
3.6
12/16/22
NAB
EPA200.8
Total Chromium, ug/1
0.19
5.0
3.8 J
MISSING
2.0 J
62
12/16/22
NAB
EPA200.8
Copper, ug/l
0.26
10.0
1 J
MISSING
0.39 J
0.35 J
12/16/22
NAB
EPA200.8
Iron, ug/1
12.20
50.0
1198
MISSING
577
1950
12/14/22
MTM
EPA200.7
Manganese, ug/l
2.70
10.0
189
MISSING
171
558
12/14/22
MTM
EPA200.7
Lead, ug/l
0.09
5.0
0.70 J
MISSING
--- U
0.34 J
12/16/22
NAB
BPA200.8
Mercury, ug/l
0.08
0.20
--- U
MISSING
--- U
--- U
12/27/22
DRC
245.1 R3-
Nickel, ug/l
0.13
10.0
1.6 J
MISSING
0.41 J
6.1 J
12/16/22
NAB
EPA200.8
Selenium, ug/l
0.43
10.0
1.0 J
MISSING
--- U
3.4 J
12/16/22
NAB
EPA200.8
Silver, ug/1
0.14
5.0
--- U
MISSING
12/16/22
NAB
EPA200.8
Silver, ug/1
0.14
5.0
--- U
--- U
12/19/22
NAB
EPA200.8
Thallium, ug/1
0.13
1.0
0.20 J
MISSING
--- U
12/16/22
NAB
EPA200.8
Thallium, ug/1
0.13
1.0
--- U
12/19/22
NAB
EPA200.8
Tin, ug/1
0.36
100.0
--- U
MISSING
--- U
0.96 J
12/21/22
NAB
EPA200.8
Vanadium, ug/l
0.14
1.0
3
MISSING
2
23
12/16/22
NAB
EPA200.8
Zinc, ug/l
0.34
10.0
69
MISSING
0.50 J
1.3 J
12/20/22
NAB
EPA200.8
Sulfide, ug/1
100
1000
TESTED
MISSING
TESTED
TESTED
4500S2D-1
Conductivity (at 25c), uMhos/cm
1.0
1.0
1240
MISSING
660
4065
12/12/22
JWT
251OB-11
Dissolved Oxygen, mg/1
0.1
0.1
2.79
MISSING
2.46
1.97
12/12/22
PJC
45000G-16
°C
17
MISSING
17
18
12/12/22
PJC
2550B-10
Temperature,
Static Water Level, feet
7.00
MISSING
8.03
5.69
12/12/22
JWT
Well Depth, feet
14.61
MISSING
13.27
23.12
12/12/22
JWT
Method 8270E (duplicate)
MISSING
EPA Method 8081B (duplicate)
MISSING
82II (duplicate)
MISSING
82II (duplicate)
MISSING
EPA 8151A Duplicate (Landfill List)
MISSING
+113
MISSING
+84
+167
12/12/22
JWT
2580E-11
ORP, my
Turbidity (Field), NTU
1.0
1.0
7.75
MISSING
2.43
97.20
12/12/22
JWT
213OB-11
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any results) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

ElMonflumsM Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: X� \u
PESTICIDES AND PCB'S
PDA MF.TUnfl AnAIR R2 (07)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/15/22
DATE ANALYZED: 12/28/22
DATE REPORTED: 03/23/23
PARAMETERS, ug/l
MDL
MRL
MW-15
MW-17
MW-14S
1.
Aldrin
0.029
0.050
---
U
---
U
-"
U
2.
Alpha-BHC
0.032
0.050
---
U
---
U
---
U
3.
Beta-BHC
0.031
0.050
---
U
---
U
---
U
4.
Delta-BHC
0.030
0.050
---
U
---
U
0.036
J
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
---
U
---
U
6.
Chlordane
1 0.320
0.500
---
U
---
U
--"
U
7.
4,4-DDD
0.051
0.100
---
U
---
U
---
U
8.
4,4-DDE
0.049
0.100
---
U
---
U
"--
U
9,
4,4-DDT
0.052
0.100
---
U
---
U
---
U
10.
Dieldrin
0.042
0.075
---
U
---
U
-"-
U
11.
Endosulfan I
0.056
0.100
---
U
---
U
--"
U
12.
Endosulfan II
0.046
0.100
---
U
---
U
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
---
U
"--
U
14.
Endrin
0.053
0.100
---
U
---
U
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
---
U
-"-
U
16.
Heptachlor
0.039
0.050
---
U
---
U
--"
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
---
U
""-
U
IS.
Methoxychlor
0.530
1.000
---
U
---
U
-"-
U
19.
Pcb's (AroclorS)
0.500
2.000
---
U
---
U
---
U
20.
Toxaphene
0.690
1.500
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ERW'nEH(@0 Flo Numpumho
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
R.PA MRTHnn 8151A R1(96)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/12/22
DATE EXTRACTED: 12/14/22
DATE ANALYZED: 12/16/22
DATE REPORTED: 03/23/23
MW-15
MW-17
MW-14S
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
--- U
--- U
2. Dinoseb
0.54
1.000
--- U
--- U
--- U
3. 2,4,5-TP
0.42
2.000
--- U
--- U
--- U
4. 2,4,5-T
0.47
2.000
--- U
'-- U
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

MWOmMEW Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: -"4
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 1
DATE EXTRACTED: 12/13/22
DATE REPORTED: 03/23/23
SEMI -VOLATILE ORGANICS
Fpa MFTunn 8270E R6(18)
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/16/22
MW-15
01/04/23
MW-17
01/04/23
MW-14S
1.
Acenaphthene
2.66
10.000
---
U
4.81
J
---
U
2.
Acenaphthylene
2.60
10.000
---
U
---
U
---
U
3.
Anthracene
2.97
10.000
---
U
---
U
---
U
4.
Benzo(a)antrhacene
4.16
10.000
---
U
---
U
---
U
5.
Benzo[b)fluoranthene
3.32
10.000
---
U
---
U
---
U
6.
Benzo[k1fluoranthene
4.23
10.000
---
U
---
U
-"-
U
7.
Benzo[g,h,i)perylene
2.61
10.000
---
U
---
U
---
U
8.
Benzo[a]pyrene
3.27
10.000
---
U
---
U
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10,000
---
U
---
U
-"-
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
---
U
--"
U
11.
Bis(2-Chloroethoxy) Methane
3,14
10.000
---
U
---
U
-""
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
---
U
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
---
U
"--
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
---
U
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
---
U
---
U
16.
Chrysene
4.04
10.000
---
U
---
U
---
U
17.
Dibenzo[a,h)anthracene
2.78
10,000
---
U
---
U
---
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
---
U
---
U
19.
Dimethyl Phthalate
3.78
10.000
---
U
---
U
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
---
U
---
U
21.
2,4-Dinitrotoluene
3.95
10.000
---
U
---
U
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
---
U
---
U
23.
Di-N-Octyl Phthalate
2.81
10.000
---
U
---
U
--"
U
24.
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
---
U
"--
U
25.
Fluoranthene
3.92
10.000
---
U
---
U
---
U
26.
Fluorene
2.95
10.000
---
U
---
U
--"
U
27.
Hexachlorobenzene
2.61
10.000
---
U
---
U
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
---
U
---
U
29.
Indeno[1,2,3-Cd)pyrene
2.91
10.000
---
U
---
U
""-
U
30.
Isophorone
3.74
10.000
---
U
---
U
--
U
31.
Nitrobenzene
2.85
10.000
---
U
---
U
U
32.
N-Nitrosodimethylamine
4.25
10.000
---
U
---
U
---
U
33.
N-Nitrosodipeehylamine
3.95
10.000
---
U
---
U
---
U
34.
N-Nitrosodi-N-Propylamine
4.06
10.000
---
U
---
U
""-
U
35.
Phenanthrene
3.24
10.000
---
U
---
U
---
U
36.
Pyrene
3.63
10.000
---
U
---
U
"--
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
---
U
---
U
38.
2-Chlorophenol
2.75
10.000
---
U
---
U
---
U
39.
O-Cresol
3.68
10.000
---
U
---
U
---
U
40.
P-Cresol
4.12
10.000
---
U
---
U
---
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
---
U
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
---
U
---
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
---
U
"--
U
44,
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
---
U
---
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
---
U
-"-
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
---
U
---
U
47.
Methyl Methanesulfonate
4.92
10.000
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits.

EflAmNEW Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: /JJ
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 2
DATE EXTRACTED: 12/13/22
DATE REPORTED: 03/23/23
SEMI -VOLATILE ORGANICS
Fva mwTunn R27nE R6 (18)
PARAMETERS, ug/1
Date Analyzed:
MDL MRL
12/16/22
MW-15
01/04/23
MW-17
01/04/23
MW-14S
48.
2-Nitrophenol
3.64
10.000
---
U
---
U
---
U
49.
4-Nitrophenol
3.17
50.000
---
U
---
U
"--
U
50.
Pentachlorophenol
5.33
25.000
---
U
---
U
---
U
51.
Phenol
1.86
10.000
---
U
---
U
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
---
U
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
---
U
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
---
U
---
U
55.
Acetophenone
2.89
10.000
---
U
---
U
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
---
U
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
---
U
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
---
U
---
U
59.
4-Chloroaniline
3.36
20,000
---
U
---
U
---
U
60.
Chlorobenzilate
5.12
10.000
---
U
---
U
---
U
61,
Diallate
2.98
10.000
---
U
---
U
---
U
62.
Dibenzofuran
4.28
10.000
---
U
---
U
---
U
63.
3,31-Dichlorobenzidine
4.22
20.000
---
U
---
U
---
U
64.
Dimethoate
3.98
20.000
---
U
---
U
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
---
U
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
---
U
"-"
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
---
U
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
---
U
---
U
69.
Diphenylamine
5.10
10,000
---
U
---
U
---
U
70.
Disulfoton
4.28
10.000
---
U
---
U
---
U
71.
Famphur
3.98
20.000
---
U
---
U
---
U
72.
Hexachloropropene
4.31
10.000
---
U
---
U
---
U
73.
Isosafrole
2.88
10.000
---
U
---
U
---
U
74,
Kepone
2.78
20.000
---
U
---
U
"--
U
75.
Methapyrilene
3.54
100.000
---
U
---
U
-""
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
---
U
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
---
U
"--
U
78.
Methyl Parathion
4.32
10.000
---
U
---
U
---
U
79.
m-Cresol
3.81
10.000
---
U
---
U
--"
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
---
U
---
U
81.
1-Naphthylamine
5.61
10,000
---
U
---
U
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
---
U
---
U
83.
2-Nitroaniline
3.61
50.000
---
U
---
U
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
---
U
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
---
U
"--
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
---
U
U
87,
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
---
U
---
U
88.
N-Nitrosodiethylamine
3.83
20.000
---
U
---
U
---
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
---
U
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
---
U
---
U
91.
N-Nitroeopyrrolidine
2.89
10.00 0
---
U
---
U
---
U
92.
Parathion
3.12
10.000
---
U
---
U
-"_
U
93.
Pentachlorobenzene
3.92
10.000
---
U
---
U
-"_
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enw,numW Flo hcupumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/12/22 Page: 3
DATE EXTRACTED: 12/13/22
DATE REPORTED: 03/23/23
SEMI -VOLATILE ORGANICS
PDA MF.TUnn 8270E R6 (18)
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/16/22
MW-15
01/04/23
MW-17
01/04/23
MW-14S
95.
Phenacetin
4.41
20.000
---
U
---
U
---
U
96.
1,4-Benzenediamine
2.99
10.000
---
U
---
U
---
U
97.
Phorate
3.86
10.000
---
U
---
U
---
U
98.
Pronamide
3.69
10.000
---
U
---
U
---
U
99.
Safrole
4.12
10.000
---
U
---
U
---
U
100.
1,2,4,5-Tetrachlorobenzene
5.01
10.000
---
U
---
U
---
U
101.
Thionazin
4.62
20.000
---
U
---
U
---
U
102.
0-Toluidine
4.11
10.000
---
U
---
U
---
U
103.
1,3,5-Trinitrobenzene
3.98
10.000
---
U
---
U
---
U
104.
0,0,0-Triethyl Phosphorothioate
3.61
10.000
---
U
---
U
---
U
105.
Hexachloroethane
1.49
10.000
---
U
---
U
---
U
106.
Isodrin
3.11
20.000
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EflW'0T@RH(@1W Flo hC@TP@T@%4
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
j REVIEWED BY:
LANDFILL APPENDIX II
vva mwTunn 9190n R4 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 1
DATE REPORTED: 03/23/23
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/20/22
MW-15
12/21/22
MW-17
12/21/22
MW-14S
12/20/22
Trip
Blank
1.
Chloromethane
0.77
3.000
---
U
---
U
---
U
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
---
U
0.82
---
U
3.
Bromomethane
0.67
10.000
---
U
---
U
---
U
---
U
4.
Chloroethane
0.48
10.000
---
U
---
U
---
U
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
---
U
---
U
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
---
U
---
U
---
U
7.
Acetone
9.06
100.000
---
U
---
U
48.10
J
---
U
8.
Iodomethane
0.26
10.000
---
U
---
U
---
U
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
---
U
1.27
J
U
10.
Methylene Chloride
0.64
1.000
---
U
---
U
---
U
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
---
U
---
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
---
U
---
U
13.
Vinyl Acetate
0.20
50.000
---
U
---
U
---
U
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
---
U
---
U
---
U
15.
2-Butanone
2.21
100.000
---
U
---
U
2.B1
J
---
U
16.
Hromochloromethane
027
.
3000
.
- - -
U
---
U
---
U
---
U
17.
Chloroform
0.25
5.000
---
U
---
U
---
U
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
---
U
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
---
U
---
U
---
U
0.24
1.000
---
U
---
U
1.57
___U
20,
Benzene
U
---
U
0.11
J
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
22.
Trichloroethene
0.23
1.000
---
U
---
U
---
U
___
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
---
U
0.05
J
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
---
U
---
U
---
U
25,
Cie-1,3-Dichloropropene
0.06
0.200
---
U
---
U
---
U
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
---
U
---
U
"'-
U
27.
Toluene
0.23
1.000
---
U
---
U
1.81
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
---
U
---
U
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
---
U
___
U
30.
Tetrachloroethene
0.10
0.200
---
U
---
U
---
U
---
U
31.
2-Hex anone
1.57
50.000
---
U
---
U
---
U
---
U
U
32.
Dibromochloromethane
0,03
0.200
---
U
---
U
---
U
---
33.
1,2-Dibromoethane
0.03
0.200
---
U
---
U
---
U
---
U
34.
Chlorobenzene
0.30
3.000
---
U
---
U
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
---
U
---
U
36.
Ethylbenzene
0.21
1.000
---
U
---
U
0.59
J
=_-
U
0.68
5.000
---
U
---
U
1.53
J
-
U
37.
Xylenes
---
U
---
U
-
U
38.
Dibromomethane
0.28
10.000
---
U
U
0.19
1.000
---
U
---
U
---
U
---
39.
Styrene
U
---
U
---
U
40.
Bromoform
0.20
3.000
---
U
U
41,
1, 1,2,2-Tetrachloroethane
0.03
0.200
---
U
___
U
___
U
___
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
---
U
---
U
---
-
U
43.
1,4-Dichlorobenzene
0.39
1,000
---
U
---
U
---
U
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
---
U
---
U
---
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
---
U
---
U
---
U
2.72
200.000
---
U
---
U
---
U
---
46.
47.
Acrylonitrile
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

E[Mumn(IM Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
cna mwTvnn RiAnn R4 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: JAP
DATE COLLECTED: 12/12/22 Page: 2
DATE REPORTED: 03/23/23
PARAMETERS, ug/l
Date Analyzed:
MDL MRL
12/20/22
MW-15
12/21/22
MW-17
12/21/22
MW-14S
12/20/22
Trip
Blank
48.
Acrolein
1.97
4.000
---
U
---
U
---
U
---
U
49.
Allyl Chloride
0.20
10.000
---
U
---
U
---
U
---
U
50.
Chloroprene
0.21
20.000
---
U
---
U
---
U
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
---
U
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
---
U
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
---
U
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
---
U
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
---
U
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
---
U
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
---
U
---
U
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
---
U
---
U
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
---
U
---
U
---
U
61.
Naphthalene
0.47
6.000
---
U
---
U
5.19
J
---
U
62.
Propionitrile
3.26
150.000
---
U
---
U
---
U
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
---
U
---
U
64.
Acetonitrile
36.29
55,000
---
U
---
U
---
U
---
U
65.
Tetrahydrofuran
0.39
1.000
---
U
---
U
78.40
---
U
66.
1,4-Dioxane
2.71
3.000
---
U
---
U
53.30
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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= (� Z
D
D
-{
®
m
< D
Dic-)
m
O
c�
Or
m Z
m
Z (n
TI -D{
m m
m
D
m
0
o
O
0
N

Enwkmm(110 Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 A
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE DATE COLLECTED: 12/14/22
GREENVILLE, NC 27834 DATE REPORTED : 03/23/23
REVIEWED BY: �� �✓ Lam,
MW-is
MW-lD
MW-2D
MW-3D
MW-3A
Analysis
Method
PARAMETERS
MDL
MRL
Date Analyst
Code
PH (field measurement), Units
BOD, mg/l
COD, mg/l
Nitrate+Nitrite as N, mg/l
Total Organic Carbon, mg/l
Total Organic Carbon, mg/l
Alkalinity (to pH 4.5), mg CaCO3/1
Chloride, mg/l
Cyanide, ug/1
Total Hardness, mg/l
Total Dissolved Residue, mg/1
Sulfate, mg/l
Antimony, ug/1
Arsenic, ug/l
Barium, ug/l
Barium, ug/l
Beryllium, ug/l
Beryllium, ug/l
Cadmium, ug/l
Cobalt, ug/1
Total Chromium, ug/l
Copper, ug/l
Iron, ug/l
Manganese, ug/1
Lead, ug/l
Lead, ug/1
Mercury, ug/1
Nickel, ug/1
Selenium, ug/l
Silver, ug/l
Thallium, ug/1
Tin, ug/1
Vanadium, ug/l
Zinc, ug/l
Sulfide, ug/1
Conductivity (at 25c), uMhos/cm
Dissolved Oxygen, mg/l
Temperature, °C
Iron (Ferrous), ug/l
Static Water Level, feet
Well Depth, feet
Carbon Dioxide, mg/l
2.0
0.840
0.04
0.129
0.129
1.0
1.0
5.0
10
5.0
0.30
0.13
0.14
0.14
0.10
0.10
0.19
0.10
0.19
0.26
12.20
2.70
0.09
0.09
0.08
0.13
0.43
0.14
0.13
0.36
0.14
0.34
100
1.0
0.1
50.00
1.0
2.0
20.0
0.04
1.0
1.0
1.0
1.0
5.0
10
5.0
1.0
5.0
10.0
10.0
1.0
1.0
1.0
1.0
5.0
10.0
50.0
10.0
5.0
5.0
0.20
10.0
10.0
5.0
1.0
100.0
1.0
10.0
1000
1.0
0.1
100.0
1.0
6.9
--- U
80
4.25
12.95
226
74
--- U
488
880
302
0.49 J
0.80 J
114
--- U
0.28 J
0.18 J
1.6 J
2 J
124
36
0.36 J
--- U
1.2 J
0.84 J
--- U
--- U
--- U
2
--- U
TESTED
1386
1.18
15
--- U
8.80
17.21
127
7.4
r 4.1
29
0.07
8.62
170
15
--- U
92
220
--- U
--- U
1.4 J
27.5
--- U
--- U
--- U
0.26 J
--- U
2488
56
--- U
--- U
0.20 J
--- U
--- U
--- U
--- U
0.71 J
--- U
TESTED
370
1.82
12
350
9.48
33.75
16
8.7
--- U
--- U
--- U
2.71
192
13
--- U
128
260
24.6
--- U
1.3 J
15.4
--- U
--- U
--- U
--- U
--- U
856
25
--- U
--- U
0.18 J
--- U
--- U
--- U
--- U
0.18 J
1.4 J
TESTED
447
1.08
14
--- U
13.26
38.17
7
8.4
--- U
--- U
--- U
3.44
242
23
--- U
88
150
--- U
--- U
0.35 J
11.7
--- U
--- U
--- U
--- U
--- U
86
3 J
--- U
--- U
0.35 J
--- U
--- U
--- U
--- U
--- U
8.6 J
TESTED
556
2.37
16
--- U
13.52
92.30
10
6.9
r 11
742
0.05
30.99
1730
256
5
740
2100
71.3
0.43 J
45
628
--- U
--- U
7.0
23
--- U
21314
1050
--- U
--- U
5.0 J
1.4 J
--- U
--- U
--- U
9
0.99 J
TESTED
3765
1.47
15
5000
12.11
23.44
320
12/14/22
12/15/22
12/16/22
12/15/22
12/16/22
12/15/22
12/19/22
12/20/22
12/22/22
12/19/22
12/15/22
12/16/22
12/20/22
12/16/22
12/20/22
12/16/22
12/19/22
12/20/22
12/16/22
12/16/22
12/16/22
12/16/22
12/16/22
12/16/22
12/16/22
12/19/22
12/27/22
12/16/22
12/16/22
12/19/22
12/19/22
12/22/22
12/16/22
12/20/22
12/14/22
12/14/22
12/14/22
12/14/22
12/14/22
12/14/22
12/14/22
JWT
HMM
HMM
KES
HMM
HMM
BNC
BLV
HMM
HMV
BNC
DRC
NAB
NAB
NAB
NAB
NAB
NAB
NAB
NAB
NAB
NAB
MTM
MTM
NAB
NAB
DRC
NAB
NAB
NAB
NAB
NAB
NAB
NAB
JWT
JWT
JWT
HMM
JWT
JWT
JMS
4500HB-11
521OB-16
H8000-79
353.2 R2-
531OC-14
531OC-14
2320B-11
4500CLB-1
45000NE-1
2340C-11
D5907-13
4500SO42E
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.7
EPA200.7
EPA200.8
EPA200.8
245.1 R3-
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
EPA200.8
2510E-11
45000G-16
2550E-10
HACH IR-1
450oCO2C-
All QC requirements were not met: r Replicate varied by more than 30%.
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

ERW'0T@[@HW % hwPuMd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
PARAMETERS
ORP, my
Turbidity (Field), NTU
MW-lS MW-lD MW-2D
MDL MRL
+113 +91 +118
1.0 1.0 2.95 2.08 3.93
All QC requirements were not met: r Replicate varied by more than 30%.
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 6003 A
DATE COLLECTED: 12/14/22
DATE REPORTED : 03/23/23
�� v
REVIEWED BY:
MW-3D MW-3A Analysis
Method
Date Analyst
Code
+116 +142 12/14/22 JWT
258OB-11
--- U 4.79 12/14/22 JWT
213OB-11

Enw,omflHOM % kwpmbd
Drinking Water ID: 37715
maatam t— ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
Trip Analysis Method
PARAMETERS MDL MRL Blank Date Analyst Code
All QC requirements were not met: r Replicate varied by more than 30%.
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
ID#: 6003 A
DATE COLLECTED: 12/14/22
DATE REPORTED : 03/23/23
REVIEWED BY:

ERAmMEW % hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
1 v
REVIEWED BY:
PARAMETERS, ug/l
1. Aldrin
2. Alpha-BHC
3. Beta-BHC
4. Delta-BHC
5. Gamma-BHC (Lindane)
6. Chlordane
7. 4,4-DDD
8. 4,4-DDE
9. 4,4-DDT
10. Dieldrin
11. Endosulfan I
12. Endosulfan II
13. Endosulfan Sulfate
14. Endrin
15. Endrin Aldehyde
16. Heptachlor
17. Heptachlor Epoxide
18, Methoxychlor
19. Pcb's (Aroclors)
20. Toxaphene
CLIENT ID:
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
6003 A
ANALYST: HIC
DATE COLLECTED: 12/14/22
DATE EXTRACTED: 12/15/22
DATE REPORTED: 03/23/23
PESTICIDES AND PCB'S
-� ,A"N
Date Analyzed:
MDL MRL
01/20/23
MW-1S
12/29/22
MW-ID
01/20/23
MW-2D
01/20/23
MW-3D
01/20/23
MW-3A
0.029
0.050
---
U
--"
U
___
U
0.032
0.050
---
U
---
U
---
U
U
U
0,031
0.050
---
U
---
U
---
U
---
U
---
U
0.030
0.050
---
U
---
U
_--
U
___
U
0.045
J
0.032
0.050
---
U
--"
U
U
0.320
0.500
---
U
---
U
U
0.051
0.100
---
U
---
U
---
U
0.049
0.100
---
U
---
U
___
U
0.052
0.100
---
U
-"-
U
U
0.042
0.075
---
U
-"-
U
U
0.056
0.100
---
U
---
U
-
U
---
U
---
U
0.046
0.100
---
U
---
U
---
U
---
U
---
U
0.072
0.100
---
U
---
U
U
0.053
0.100
---
U
---
U
---
U
0.068
0.100
---
U
-
U
U
---
U
---
U
0.039
0.050
---
U
---
U
---
U
0.042
0.075
---
U
--
U
-
U
---
U
---
i7
0.530
1.000
---
U
--
U
U
0.500
2.000
---
U
___
U
__
U
---
U
---
U
0.690
1.500
---
U
_-
U
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enw,unnEW % hcupumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
wrn+mvnrC 1 CZ 1 n "D 1 1 Q Ai 1
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/14/22
DATE EXTRACTED: 12/21/22
DATE REPORTED: 03/23/23
Date Analyzed:=12/23/2212/23/22
12/23/22
12/23/22
12/27/22
MW-ID
MW-2D
MW-3D
MW-3A
PARAMETERS, ug/1 MDL MRL
--- U
--- U
--' U
0.36 2.000
1. 2,4-D
U
--- U
--' U
--- U
--- U
2. Dinoseb 0.54 1.000
---
U
--- U
0.486 J
3. 2,4,5-TP 0.42 2.000
---
U
--- U
--- U
0.47 2.000
--- U
--- U
---
4. 2,4,5-T
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 1
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/23/23
SEMI -VOLATILE ORGANICS
•rnr OnnAV D%/iA]
MW-1S
MW-1D
MW-2D
MW-3D
MW-3A
PARAMETERS, ug/l
MDL
MRL
U
---
U
---
U
---
U
6.69
J
1. Acenaphthene
2.66
10.000
---
U
V
U
2. Acenaphthylene
2.60
10.000
---
U
-"-
U
__-
-
U
U
u
2.97
10.000
---
U
---
v
3. Anthracene
---
U
___
U
V
___
U
4. Benzo[a]antrhacene
4.16
10.000
---
U
U
---
U
---
U
5. Benzo[b]fluoranthene
3.32
10.000
---
U
---
U
---
---
U
6. Henzo[kJfluoranthene
4.23
10.000
---
U
---
U
U
U
---
U
2.61
10.000
---
U
---
U
'--
U
7. Benzo[g,h,i]perylene
3.27
10.000
---
U
---
U
---
U
---
U
---
8, Benzo[a]pyrene
U
--_
u
9. 4-Hromophenyl Phenyl Ether
2.63
10.000
---
U
---
V
U
10. Butyl Benzyl Phthalate
5.78
10.000
---
U
--"
U
---
U
---
U
---
U
11. Hie(2-Chloroethoxy) Methane
3.14
10.000
---
U
---
U
12. Bie(2-Chloroethyl) Ether
2.58
10.000
---
U
---
U
---
U
V
u
13. Bis(2-Chloro-i-methylethyl) Ether
2.58
10.000
---
U
---
U
14. 2-Chloronaphthalene
2.17
10.000
---
U
---
U
---
U
U
___
U
---
U
15. 4-Chlorophenyl Phenyl Ether
2.42
10.000
'_
U
---
U
U
---
U
---
U
16. Chryeene
4.04
10.000
---
U
---
__ -
U
U
---
___
U
---
U
---
U
17. Dibenzo[a,h]anthracene
2.78
10.000
---
U
U
---
U
---
U
18. Di-N-Butyl Phthalate
3.09
10.000
---
U
---
U
---
v
---
U
19. Dimethyl Phthalate
3.78
10.000
---
U
---
U
U
---
U
---
20. Diethyl Phthalate
3.92
10.000
---
U
---
U
---
u
21. 2,4-Dinitrotoluene
3.95
10.000
---
U
---
U
U
---
U
---
U
22, 2,6-Dinitrotoluene
3.88
10.000
---
U
---
U
---
U
---
U
---
U
23. Di-N-Octyl Phthalate
2.81
10.000
---
U
_-"
u
---
U
___
U
---
U
24. Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
"--
U
_-_
U
---
U
_-_
U
25. Fluoranthene
3.92
10.000
---
U
-"-
U
---
---
u
2.95
10.000
---
U
---
U
U
26. Fluorene
---
U
---
U
___
U
---
U
---
27. Hexachlorobenzene
2.61
10.000
---
U
U
---
U
28. Hexachlorocyclopentadiene
4.16
10.000
---
U
U
---
U
---
U
29. Indeno[1,2,3-Cd]pyrene
2.91
10.000
---
U
--"
U
---
---
U
---
U
---
30. Isophorone
3.74
10.000
---
U
---
_
U
U
___
U
___
U
---
U
31. Nitrobenzene
2.85
10.000
---
U
-'
-- -
U
___
U
___
U
---
U
32. N-Nitrosodimethylamine
10.000
---
U
- _
U
_ _
V
__
U
33. N-Nitrosodiphenylamine
3.95
3.06
10.000
-- _
U
_" _
U
U
_--
U
'--
U
34. N-Nitrosodi-N-Propylamine
4.06
10.000
-- _
U
--_
U
'--
U
-'-
U
---
U
35. Phenanthrene
3.24
10.000
-- -
U
---
U
U
---
--'
U
'-'
U
---
U
3.63
10.000
-- _
U
-'-
--_
U
36. Pyrene
---
U
-
U
-
u
-_ -
U
37. 4-Chloro-3-Methylphenol
3.79
20.000
---
U
---
U
---
U
38. 2-Chlorophenol
2.75
10.000
---
U
---
U
U
---
U
---
U
---
U
39. O-Cresol
3.68
10.000
---
U
---
U
--�
U
---
U
---
U
40, P-Cresol
4.12
10.000
---
U
---
U
-__
U
___
U
---
U
41. 2,4-Dichlorophenol
10.000
---
U
--_
U
-
U
_
U
__
U
42. 2,6-Dichlorophenol
4.8
.89
10000
.
---
U
_9
--
---
U
---
U
---
U
-'-
U
43. 2,4-Dimethylphenol
3.21
10.000
-- -
U
U
---
U
---
U
44. 4,6-Dinitro-2-Methylphenol
4.77
50.000
-- -
U
---
U
-'-
'--
v
--- U
---
U
45. 2,4-Dinitrophenol
4,37
50.000
-- -
U
---
U
-'-
U
---
U
---
U
46. Ethyl Methaneeulfonate
5.26
20.000
-- -
U
--- U
U
--'
U
47. Methyl Methaneeulfonate
4.92
10.000
-- -
U
---
U
---
U
___ U
---
U
48, 2-Nitrophenol
3.64
10.000
---
U
---
J = Estimated value between the MDL and MRL, u = aeiow nLL yua++����•--�•• __...___.

ElMommu Flo hmpumud
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
SEMI -VOLATILE ORGANICS
F.PA MRTWon 8270E R6(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 2
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/23/23
PARAMETERS, Ug/1
MDL
MRL
MW-1S
MW-1D
MW-2D
MW-3D
MW-3A
49.
4-Nitrophenol
3.17
50.000
---
U
---
U
---
U
---
U
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
---
U
---
U
---
U
---
U
51.
Phenol
1.86
10.000
---
U
---
U
---
U
---
U
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
---
U
---
U
---
U
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
---
U
---
U
---
U
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
---
U
---
U
---
U
---
U
55.
Acetophenone
2.89
10.000
---
U
---
U
---
U
---
U
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
---
U
---
U
---
U
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
---
U
---
U
---
U
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
---
U
---
U
---
U
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
---
U
---
U
---
U
---
U
60.
Chlorobenzilate
5.12
10.000
---
U
---
U
---
U
---
U
---
U
61.
Diallate
2.98
10.000
---
U
---
U
---
U
---
U
---
U
62.
Dibenzofuran
4.28
10.000
---
U
---
U
---
U
---
U
---
U
63,
3,31-Dichlorobenzidine
4.22
20.000
---
U
---
U
---
U
---
U
---
U
64.
Dimethoate
3.98
20.000
---
U
---
U
---
U
---
U
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
---
U
---
U
---
U
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
---
U
---
U
---
U
---
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
---
U
---
U
---
U
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
---
U
---
U
---
U
---
U
69,
Diphenylamine
5.10
10.000
---
U
---
U
---
U
---
U
---
U
70.
DisUlfoton
4.28
10,000
---
U
---
U
---
U
---
U
---
U
71.
Famphur
3.98
20.000
---
U
---
U
---
U
---
U
---
U
72.
Hexachloropropene
4.31
10.000
---
U
---
U
---
U
---
U
---
U
73.
Isosafrole
2.88
10.000
---
U
---
U
---
U
---
U
---
U
74.
Kepone
2.78
20.000
---
U
---
U
---
U
---
U
---
U
75.
Methapyrilene
3.54
100.000
---
U
---
U
---
U
---
U
---
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
---
U
---
U
---
U
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
---
U
---
U
---
U
---
U
78.
Methyl Parathion
4.32
10.000
---
U
---
U
---
U
---
U
---
U
79.
m-Cresol
3.81
10.000
---
U
---
U
---
U
---
U
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
---
U
---
U
---
U
---
U
81.
1-Naphthylamine
5.61
10.000
---
U
---
U
---
i7
---
U
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
---
U
---
U
---
U
---
U
83.
2-Nitroaniline
3.61
50.000
---
U
---
U
---
U
---
U
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
---
U
---
U
---
U
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
---
U
---
U
---
U
---
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
---
U
---
U
---
U
U
87.
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
---
U
---
U
---
U
---
U
80.
N-Nitrosodiethylamine
3.83
20.000
---
U
---
U
---
U
---
U
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
---
U
---
U
---
U
---
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
---
U
---
U
---
U
---
U
91.
N-Nitrosopyrrolidine
2.89
10.000
---
U
---
U
---
U
---
U
U
92.
Parathion
3.12
10.000
---
U
---
U
---
U
---
U
---
U
93.
Pentachlorobenzene
3.92
10.000
---
U
---
U
---
U
---
U
---
U
94.
Pentachloronitrobenzene
3.71
20,000
---
U
---
U
---
U
---
U
---
U
95,
Phenacetin
4.41
20.000
---
U
---
U
---
U
---
U
U
96.
1,4-Benzenediamine
2.99
10.000
---
U
---
U
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enw,unflEW Flo lompmUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 3
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/23/23
SEMI -VOLATILE ORGANICS
c- "WMW^n 077nw Ri, (1 Al
ug/l MDL MRL]
MW-1S
MW-1D
E
14W-2D
MW-3D
-
qAPARAMETERS,
10.000
--- U
U
---U--U98.
97. Phorate3.86
U
--- U
--- U
Pronamide3.69
10.000
--- U
---
99. 9afrole
4.12
10.000
--- U
U
--- U
--- U
U
--- U
100. 1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
-"- U
'-- U
---
U
101. Thionazin
4.62
20.000
--- U
U
--- U
U
U
102. 0-Toluidine
4.11
10.000
--- U
U
--- U
___ U
103. 1,3,5-Trinitrobenzene
3.98
10.000
--- U
--- U
--- U
--- U
104. 0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
--"
U
105. Hexachloroethane
1.49
10.000
--- U
--- U
--- U
U
106. Ieodrin
3.11
20.000
--- U
--- U
--- U
--- U
_
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
-R Mwnr% 001Znn Ad (9 Al
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST: JAP
DATE COLLECTED: 12/14/22
DATE ANALYZED: 12/21/22
DATE REPORTED: 03/23/23
Page: 1
PARAMETERS, ug/l
MDL
MRL
MW-lS
MW-ID
MW-2D
MW-3D
MW-3A
1.
Chloromethane
0.77
3.000
---
U
U
---
U
---
U
U
2.
Vinyl Chloride
12
200
0.200
---
U
---
U
---
U
U
---
U
3.
Hromomethane
0.67
10.000
---
U
U
---
U
---
U
U
---
_
U
4.
Chloroethane
0..
48
10000
---
U
---
U
- __
U
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
U
---
U
---
U
-
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
_--
U
U
___
U
U
___
15.90
J
7.
Acetone
9.06
100.000
---
U
---
U
---
U
---
U
U
B.
iodomethane
0.26
10.000
---
U
---
U
---
U
___
U
-_
U
9.
Carbon Disulfide
0.23
100.000
---
U
---
U
---
U
---
U
10.
Methylene Chloride
0.64
1.000
---
U
""
U
___
U
_
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
---
U
---
U
-_ _
U
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
U
---
U
_
U
13.
Vinyl Acetate
0.20
50.000
---
U
---
U
___
U
_"
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
---
U
---
U
U
U
221
100000
---
U
---
U
---
U
___
15.
2-Hutanone
..
---
U
---
U
_ _
U
-- -
U
16.
Bromochloromethane
0.27
3.000
---
U
___
U
_
U
17.
Chloroform
0.25
5.000
---
U
U
---
U
---
U
10.
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
---
U
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
---
U
---
U
---
U
1.32
0.24
1.000
---
U
__
U
_
20.
Benzene
-- _
_--
U
___
U
.32
J
21.
1,2-Dichloroethane
0.02
0.200
---
U
U
---
U
22.
Trichloroethene
0.23
1.000
---
U
---
U
---
U
---
U
0.04
J
23.
1,2-Dichloropropane
0.04
0.200
---
U
U
---
U
V
---
---
U
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
---
U
---
U
---
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
---
U
---
U
U
---
U
U
26.
4-Methyl-2-Pentanone
1,19
100.000
---
U
---
U
---
U
0.24
JU
0.23
1.000
---
U
'--
U
---
U
27.
Toluene
---
U
20.
trans-1,3-Dichloropropene
0.04
0.200
---
U
U
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
---
U
---
U
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
---
U
_--
U
---
---
U
---
U
1.57
50.000
---
U
---
U
---
U
31.
2-Hexanone
---
U
---
U
---
U
---
32.
Dibromochloromethane
0.03
0.200
---
U
---
U
---
U
0.03
0.200
---
U
---
U
---
U
33.
1,2-Dibromoethane
---
U
---
U
---
U
---
U
---
U
34.
Chlorobenzene
0.30
3.000
U
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
---
U
0.21
1.000
---
U
---
U
---
U
---
36.
Ethylbenzene
U
---
U
---
U
---
U
37.
Xylenes
0.68
5.000
-- -
U
---
U
U
38.
Dibromomethane
0.28
10.000
---
U
""
U
U
U
39,
Styrene
0.19
1.000
---
U
'-
U
U
U
40.
Bromoform
0.20
3.000
---
U
---
U
-_
41.
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
---
U
---
---
U
---
U
---
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
---
U
---
U
---
U
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
---
U
U
---
U
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
"--
U
---
U
---
U
___
U
---
U
45.
1,2-Dibromo-3-Chloropropane
.
0.200
"-'
U
--_
II
__-
U
---
U
U
46,
Acrylonitrile
2 .72 72
2
200.000
---
U
'"-
U
---
___
U
___
U
---
U
47.
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
-
U
U
___
U
---
U
1.97
4.000
---
U
"-"
U
__-
48,
Acrolein
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enwkmmid Flo hmpumW
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
WnA 7AWMunn 079nn Rd (1 A)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 A
ANALYST: JAP
DATE COLLECTED: 12/14/22 Page: 2
DATE ANALYZED: 12/21/22
DATE REPORTED: 03/23/23
PARAMETERS, ug/l
MDL
MRL
MW-IS
MW-1D
MW-2D
MW-3D
MW-3A
49.
Allyl Chloride
0.20
10.000
---
U
---
U
---
U
-
U
U
50.
Chloroprene
0.21
20.000
---
U
---
U
---
U
U
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
---
U
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
---
U
U
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
---
U
---
U
U
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
---
U
U
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
---
U
U
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
---
U
---
U
U
U
57,
Hexachlorobutadiene
0.10
0.200
---
U
---
U
---
U
U
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
---
U
---
U
---
U
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
---
U
---
U
U
U
60.
Methyl Methacrylate
0.25
30.000
---
U
---
U
---
U
U
1.54
U
J
61.
Naphthalene
0.47
6.000
---
U
---
U
---
U
---
U
U
62.
Propionitrile
3.26
150.000
---
U
---
U
---
U
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
---
U
---
U
---
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
---
U
U
30.60
U
65.
Tetrahydrofuran
0.39
1.000
---
U
35.70
---
U
---
U
135.00
66.
1,4-Dioxane
2.71
3.000
19.30
---
U
---
U
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
LL��LJLII/ LLII LILILILILI�JL1LIlS �' waera.•,arar rn• in
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST: JAP
DATE COLLECTED: 12/14/22
DATE ANALYZED: 12/21/22
DATE REPORTED: 03/23/23
PARAMETERS, ug/l
MDL
MRL
Trip
Blank
1.
Chloromethane
0.77
3.000
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
3.
Bromomethane
0.67
10.000
---
U
4.
Chloroethane
0.48
10,000
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
7.
Acetone
9.06
100.000
---
U
8.
Iodomethane
0.26
10.000
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
10.
Methylene Chloride
0.64
1.000
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
13.
Vinyl Acetate
0.20
50.000
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
15,
2-Butanone
2.21
100.000
---
U
16,
Bromochloromethane
0.27
3.000
---
U
17.
Chloroform
0.25
5.000
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
20.
Benzene
0.24
1.000
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
U
22,
Trichloroethene
0.23
1.000
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
27.
Toluene
0.23
1.000
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
31.
2-Hexanone
1.57
50.000
---
U
32.
Dibromochloromethane
0.03
0.200
---
U
33.
1,2-Dibromoethane
0.03
0.200
---
U
34.
Chlorobenzene
0.30
3.000
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
36.
Ethylbenzene
0.21
1.000
---
U
37.
Xylenes
0.68
5.000
---
U
38.
Dibromomethane
0.28
10.000
---
U
39.
Styrene
0.19
1.000
---
U
40.
Bromoform
0.20
3.000
---
U
41,
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
46,
Acrylonitrile
2.72
200.000
---
U
47.
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
48.
Acrolein
1.97
4.000
---
U
U = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 3

Enw,ningid Flo hmpumW
Drinking Water ID: 37715
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A
MR. JUDSON WHITEHURST
802 RECYCLING LANE ANALYST: JAP
GREENVILLE, NC 27834 DATE COLLECTED: 12/14/22 Page: 4
DATE ANALYZED: 12/21/22
� DATE REPORTED: 03/23/23
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
PARAMETERS, ug/l
MDL
MRL
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
50.
Chloroprene
0.21
20.000
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
61.
Naphthalene
0.47
6.000
---
U
62.
Propionitrile
3.26
150.000
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
64.
Acetonitrile
36.29
55.000
---
U
65.
Tetrahydrofuran
0.39
1.000
---
U
66.
1,4-Dioxane
2.71
3.000
---
U
J = Estimated value between the MDL and MRL, U - Below ALL Quantitation Limits.

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Elmwkmmomalp hmpuMd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. =SON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
Drinking Water ID: 37715
-jw iiiiiiiiiiiiiiiiiiiiiiiift
PHONE [phone]
FAX [phone]
ID#: 6003
DATE COLLECTED: 12/14/22
DATE REPORTED : 03/17/23
REVIEWED BY:
MW-6
Analysis
Method
PARAMETERS
MDL
MRL
Date Analyst
Code
PH (field measurement), Units
7.1
12/14/22
JWT
4500HB-11
BOD, mg/l
2.0
2.0
r 3.2
12/15/22
HMM
521OB-16
COD, mg/l
0.840
20.0
279
12/16/22
HMM
H8000-79
Nitrate+Nitrite as N, mg/l
0.04
0.04
2.06
12/15/22
KES
353.2 R2-93
Total Organic Carbon, mg/l
0.129
1.0
47.68
12/16/22
HMM
531OC-14
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
975
12/19/22
BNC
2320B-11
Chloride, mg/l
1.0
1.0
43
12/20/22
BLV
4500CLB-11
Cyanide, ug/l
5.0
5.0
--- U
12/22/22
HMM
450OCNE-16
Total Hardness, mg/l
690
12/19/22
HMV
2340C-11
Total Dissolved Residue, mg/1
10
10
1400
12/15/22
BNC
D5907-13
Sulfate, mg/l
5.0
5.0
139
12/16/22
DRC
4500SO42Ell
Antimony, ug/l
0.30
1.0
--- U
12/20/22
NAB
EPA200.8
Arsenic, ug/l
0.13
5.0
10
12/16/22
NAB
BPA200.8
Barium, ug/l
0.14
10.0
527
12/16/22
NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
--- U
12/19/22
NAB
BPA200.8
Cadmium, ug/l
0.19
1.0
--- U
12/16/22
NAB
EPA200.8
Cobalt, ug/l
0.10
1.0
2.4
12/16/22
NAB
EPA200.8
Total Chromium, ug/l
0.19
5.0
7.8
12/16/22
NAB
EPA200.8
Copper, ug/l
0.26
10.0
0.74J
12/16/22
NAB
EPA200.8
Iron, ug/l
12.20
50.0
11698
12/16/22
MTM
EPA200.7
Manganese, ug/l
2.70
10.0
878
12/16/22
MTM
EPA200.7
Lead, ug/l
0.09
5.0
0.11 J
12/16/22
NAB
EPA200.8
Mercury, ug/1
0.08
0.20
--- U
12/27/22
DRC
245.1 R3-94
Nickel, ug/l
0.13
10.0
2.0J
12/16/22
NAB
EPA200.8
Selenium, ug/l
0.43
10.0
0.92 J
12/16/22
NAB
EPA200.8
Silver, ug/1
0.14
5.0
--- U
12/19/22
NAB
EPA200.8
Thallium, ug/l
0.13
1.0
--- U
12/19/22
NAB
EPA200.8
Tin, ug/l
0.36
100.0
--- U
12/22/22
NAB
EPA200.8
Vanadium, ug/l
0.14
1.0
9
12/16/22
NAB
EPA200.8
Zinc, ug/l
0.34
10.0
--- U
12/20/22
NAB
EPA200.8
Sulfide, ug/l
100
1000
TESTED
Conductivity (at 25c), uMhos/cm
1.0
1.0
1723
12/14/22
JWT
251OB-11
Dissolved Oxygen, mg/l
0.1
0.1
3.36
12/14/22
JWT
45000G-16
Temperature, °C
15
12/14/22
JWT
255OB-10
Iron (Ferrous), ug/1
50.00
100.0
3500
12/14/22
HMM
HACH IR-18C
Static Water Level, feet
10.24
12/14/22
JWT
Well Depth, feet
16.65
12/14/22
JWT
Carbon Dioxide, mg/l
1.0
1.0
250
12/14/22
JMS
45000O2C-11
+134
12/14/22
JWT
258OB-11
ORP, my
Turbidity (Field), NTU
1.0
1.0
6.76
12/14/22
JWT
213OB-11
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

EflwkuflaW Flo D�c�oQpor�a�c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: 1' J
PESTICIDES AND PCB'S
EPA METHOD 8081B R2(07)
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/14/22
DATE EXTRACTED: 12/15/22
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-6
1.
Aldrin
0.029
0.050
---
U
2.
Alpha-BHC
0.032
0.050
---
U
3.
Beta-BHC
0.031
0.050
---
U
4.
Delta-BHC
0.030
0.050
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
6.
Chlordane
0.320
0.500
---
U
7.
4,4-DDD
0.051
0.100
---
U
8.
4,4-DDE
0.049
0.100
---
U
9.
4,4-DDT
0.052
0.100
---
U
10.
Dieldrin
0.042
0.075
---
U
11.
Endosulfan I
0.056
0.100
---
U
12.
Endosulfan II
0,046
0.100
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
14.
Endrin
0.053
0.100
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
16.
Heptachlor
0.039
0.050
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
18.
Methoxychlor
0.530
1.000
---
U
19.
Pcb-s (Aroclors)
0.500
2.000
---
U
20.
Toxaphene
0.690
1.500
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ENW,ummid % kccTp@TM4
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
^J
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
Drinking Water ID; 37715
Wastewater ID:: 10.
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/14/22
DATE EXTRACTED: 12/21/22
DATE ANALYZED: 12/23/22
DATE REPORTED: 03/17/23
MW-6
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
2. Dinoseb
0.54
1.000
--- U
3. 2,4,5-TP
0.42
2.000
--- U
4. 2,4,5-T
0.47
2.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
1� I REVIEWED BY: z \
Drinking Water ID: 37715
N � T -
W­t­t am
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 1
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
RPA METHOD 8270E R6(18)
PARAMETERS, ug/1
MDL
MRL
MW-6
1.
Acenaphthene
2.66
10.000
3.40
J
2.
Acenaphthylene
2.60
10.000
---
U
3.
Anthracene
2.97
10.000
---
U
4.
Benzo[a3antrhacene
4.16
10.000
---
U
5,
Benzo[b)fluoranthene
3.32
10.000
---
U
6.
Benzo[k)fluoranthene
4.23
10.000
---
U
7.
Benzo[g,h,i3perylene
2.61
10.000
---
U
S.
Benzo[a3pyrene
3.27
10.000
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10.000
---
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
11.
Bis(2-Chloroethoxy) Methane
3.14
10.000
---
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
16.
Chrysene
4.04
10.000
---
U
17.
Dibenzo[a,h)anthracene
2.78
10.000
---
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
19.
Dimethyl Phthalate
3.78
10.000
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
21.
2,4-Dinitrotoluene
3.95
10.000
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
23,
Di-N-Octyl Phthalate
2.81
10.000
---
U
24.
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
25.
Fluoranthene
3.92
10.000
---
U
26.
Fluorene
2.95
10.000
---
U
27.
Hexachlorobenzene
2.61
10.000
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
29.
Indeno[1,2,3-Cd3pyrene
2.91
10.000
---
U
30.
Isophorone
3.74
10.000
---
U
31.
Nitrobenzene
2.85
10.000
---
U
32.
N-Nitrosodimethylamine
4.25
10.000
---
U
33.
N-Nitrosodiphenylamine
3.95
10.000
---
U
34.
N-Nitroeodi-N-Propylamine
4.06
10.000
---
U
35.
Phenanthrene
3.24
10.000
---
U
36.
Pyrene
3.63
10.000
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
38.
2-Chlorophenol
2.75
10.000
---
U
39.
O-Cresol
3.68
10.000
---
U
40.
P-Cresol
4.12
10.000
---
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
44.
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
47.
Methyl Methanesulfonate
4.92
10.000
---
U
48,
2-Nitrophenol
3.64
10.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 2
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l
MDL
MRL
MW-6
49.
4-Nitrophenol
3.17
50.000
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
51.
Phenol
1.86
10.000
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
55.
Acetophenone
2.89
10.000
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
60.
Chlorobenzilate
5.12
10.000
---
U
61.
Diallate
2.98
10.000
---
U
62.
Dibenzofuran
4.28
10.000
---
U
63.
3,3,-Dichlorobenzidine
4.22
20.000
---
U
64.
Dimethoate
3.98
20.000
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
69,
Diphenylamine
5.10
10.000
---
U
70,
Disulfoton
4.28
10.000
---
U
71.
Famphur
3.98
20.000
---
U
72.
Hexachloropropene
4.31
10.000
---
U
73.
Isosafrole
2.88
10.000
---
U
74.
Kepone
2.78
20.000
---
U
75,
Methapyrilene
3.54
100.000
---
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
78,
Methyl Parathion
4.32
10.000
---
U
79.
m-Cresol
3.81
10.000
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
81.
1-Naphthylamine
5.61
10.000
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
83,
2-Nitroaniline
3.61
50.000
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
87.
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
88.
N-Nitrosodiethylamine
3.83
20,000
---
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
91.
N-Nitrosopyrrolidine
2.89
10.000
---
U
92.
Parathion
3.12
10.000
---
U
93.
Pentachlorobenzene
3.92
10.000
---
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
95.
Phenacetin
4.41
20.000
---
U
96.
1,4-Benzenediamine
2.99
10.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits.

[��dor�o����� Flo D��oQpoQa�c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. =SON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/14/22 Page: 3
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l MDL MRL
MW-6
97. Phorate
3.86
10.000
--- U
98. Pronamide
3.69
10.000
--- U
99. Safrole
4.12
10.000
--- U
100. 1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
101. Thionazin
4.62
20.000
--- U
102. O-Toluidine
4.11
10.000
--- U
103. 1,3,5-Trinitrobenzene
3.98
10.000
--- U
104, 0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
105. Hexachloroethane
1.49
10.000
--- U
106. Isodrin
3.11
20.000
--- U
U = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Elu'ronflM Flo hmpmUd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. =SON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/14/22 Page: 1
DATE ANALYZED: 12/21/22
DATE REPORTED: 03/17/23
PARAMETERS, ng/l
MDL
MRL
MW-6
1.
Chloromethane
0.77
3.000
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
3.
Bromomethane
0.67
10.000
---
U
4.
Chloroethane
0.48
10.000
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
7.
Acetone
9.06
100.000
---
U
S.
Iodomethane
0.26
10.000
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
10.
Methylene Chloride
0.64
1.000
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
13.
Vinyl Acetate
0.20
50.000
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
15.
2-Butanone
2.21
100.000
---
U
16.
Bromochloromethane
0.27
3.000
---
U
17.
Chloroform
0.25
5.000
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
20.
Benzene
0.24
1.000
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
U
22.
Trichloroethene
0.23
1.000
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
25.
Cis-1,3-Dichloropropene
0.06
0.200
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
27.
Toluene
0.23
1.000
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
31.
2-Hexanone
1.57
50.000
---
U
32.
Dibromochloromethane
0.03
0.200
---
U
33.
1,2-Dibromoethane
0.03
0.200
---
U
34.
Chlorobenzene
0.30
3.000
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
36.
Ethylbenzene
0.21
1.000
---
U
37.
Xylenes
0.68
5.000
---
U
38.
Dibromomethane
0.28
10.000
---
U
39.
Styrene
0.19
1.000
---
U
40.
Bromoform
0.20
3.000
---
U
41.
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
42.
1,2,3-Trichloropropane
0.09
0,200
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
46.
Acrylonitrile
2.72
200.000
---
U
47.
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
48.
Acrolein
1.97
4,000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
LLL��� ILLJII LLLJII l:/ llll LLLIII LLLIII LLLIII Ll LJ lS u-'
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. =SON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC/27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/14/22 Page: 2
DATE ANALYZED: 12/21/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-6
49.
Allyl Chloride
0.20
10.000
---
U
50.
Chloroprene
0.21
20.000
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
61.
Naphthalene
0.47
6.000
---
U
62.
Propionitrile
3.26
150.000
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
64.
Acetonitrile
36.29
55.000
---
U
65.
Tetrahydrofuran
0.39
1.000
6.85
66.
1,4-Dioxane
2.71
3.000
15.10
J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits.

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EEW'OnERM Flo hC@qwM%4
Drinking Water ID: 37715
mser o..,w r.er ID! 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 D
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
8p2 RECYCLING LANE DATE COLLECTED: 12/15/22
DATE REPORTED 03/17/23
GREENVILLE, NC 27834
REVIEWED BY: �� \
MW-14D Trip
Analysis
Method
MDL
MRL
Blank
Date Analyst
Code
PARAMETERS
7.2
12/15/22 PJC
4500HB-11
PH (field measurement), Unite
12/15/22 HMM
521OB-16
BOD, mg/1
2.0
2.0
--- U
U
12/16/22 HMM
H8000 -79
COD, mg/l
0.840
20.0
---
0.07
12/20/22 KES
353.2 R2-93
Nitrate+Nitrite as N, mg/1
0.04
0.04
12/16/22 HMM
531OC-14
Total Organic Carbon, mg/l
0.129
1.0
3.35
12/16/22 JDJ
2320E-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
246
12/20/22 BLV
4500CLH-11
Chloride, mg/l
.0
.0
15
12/22/22 HMM
4500CNE-16
Cyanide, ug/l
5
5.0
5.0
5
--- U
154
12/27/22 ADR
2340C-11
Total Hardness, mg/l
300
12/20/22 BNC
D5907-13
Total Dissolved Residue, mg/1
10
10
12/19/22 DRC
4500SO42E11
Sulfate, mg/l
5.0
5.0
--- U
U
12/22/22 NAB
EPA200.8
Antimony, ug/1
0.30
1.0
---
J
12/22/22 NAB
EPA200.8
Arsenic, ug/1
0.13
.0
10.0
10.0
12/22/22 NAB
EPA200.8
Barium, ug/1
0.14
1.0
0
U
01/04/23 NAB
EPA200.8
Beryllium, ug/1
0.10
1
1.0
---
U
12/22/22 NAB
EPA200.8
Cadmium, ug/l
0.19
1.0
---
U
12/22/22 NAB
EPA200.8
Cobalt, ug/1
0.10
1.0
---
U
12/22/22 NAB
EPA200.8
Total Chromium, ug/l
0.19
5.0
---
12/22/22 NAB
EPA200.8
Copper, ug/1
0.26
10.0
--- U
18 J
12/16/22 MTM
EPA200.7
Iron, ug/l
12.20
50.0
10
12/MTM
EPA200.7
Manganese, ug/l
2.70
10.0
U
12/2222/22 /22 NAB
EPA200.8
Lead, ug/1
009
.
5.0
---
U
12/27/22 DRC
245.1 R3-94
Mercury, ug/1
0.08
0.20
__ -
J
12/22/22 NAB
EPA200.8
Nickel, ug/l
0.3
10.0
U
12/22/22 NAB
EPA200.8
Selenium, ug/1
0.43
10.0
- --
U
12/22/22 NAB
EPA200.8
Silver, ug/1
0.1
5.0
---
U
12/22/22 NAB
EPA200.8
Thallium, ug/1
0.13
1.0
---
U
12/22/22 NAB
EPA200.8
Tin, Ug/
0.36
100.0
1.0
---
0.15 J
12/22/22 NAB
EPA200.8
Vanadium, ug/1
0.14
0.78 J
12/22/22 NAB
EPA200.8
Zinc, ug/1
0.34
10.0
Sulfide, ug/l
100
1000
TESTED
12/15/23 PJC
2510B-11
Conductivity (at 25c), uMhos/cm
1.0
1.0
532
12/15/22 PJC
45000G-16
Dissolved Oxygen, mg/1
0.1
0.1
3.47
19
12/15/22 PJC
255OB-10
Temperature, °C
U
12/15/22 BLV
HACH IR-18C
Iron (Ferrous), ug/1
50.00
100.0
---
6.84
12/15/22 PJC
Static Water Level, feet
41.92
12/15/22 PJC
Well Depth, feet
18
12/15/22 HMM
45000O2C-11
Carbon Dioxide, mg/1
1.0
1.0
+127
12/15/22 PJC
2580B-11
ORP, my
1'0
__ U
12/15/22 PJC
213OB-11
Turbidity (Field), NTU
1.0
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

Enwkma@W Flo kwpTOW
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
I �
REVIEWED BY:
PESTICIDES AND PCB'S
teen mpTwnn 8081B R2 (07)
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/19/22
DATE ANALYZED: 01/20/23
DATE REPORTED: 03/17/23
PARAMETERS, ug/1
MDL
MRL
MW-14D
1.
Aldrin
0.029
0.050
---
U
2.
Alpha-BHC
0.032
0.050
---
U
3.
Beta-BHC
0.031
0.050
---
U
4.
Delta-BHC
0.030
0.050
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
6.
Chlordane
0.320
0.500
---
U
7.
4,4-DDD
0.051
0.100
---
U
B.
4,4-DDE
0.049
0.100
---
U
9.
4,4-DDT
0.052
0.100
---
U
10.
Dieldrin
0.042
0.075
---
U
11.
Endoeulfan I
0.056
0.100
---
U
12.
Endosulfan II
0.046
0.100
---
U
13.
Endoeulfan Sulfate
0.072
0.100
---
U
14.
Endrin
0.053
0.100
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
16.
Heptachlor
0.039
0.050
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
18.
Methoxychlor
0,530
1.000
---
U
19.
Pcb-s (Aroclors)
0.500
2.000
---
U
20.
Toxaphene
0.690
1.500
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EAnIMEW Flo hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
Wnr ?jwmunn R1glA R1(96)
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/21/22
DATE ANALYZED: 12/23/22
DATE REPORTED: 03/17/23
MW-14D
PARAMETERS, ug/1 MDL MRL
0.36
2.000
--- U
1. 2,4-D
0.54
1.000
--- U
2, Dinoseb
0.42
2.000
--- U
3. 2,4,5-TP
0.47
2.000
--- U
4. 2,4,5-T
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EflW'0T@EHW % kwPuMd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
J-.
REVIEWED BY: l
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 1
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/24/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
F.PA MF.Twon 8270E R6 (18)
PARAMETERS, ug/1
MDL
MRL
MW-14D
1.
Acenaphthene
2.66
10.000
---
U
2.
Acenaphthylene
2.60
10.000
---
U
3.
Anthracene
2.97
10.000
---
U
4.
Benzo[a]antrhacene
4.16
10.000
---
U
5.
Benzo[b)fluoranthene
3.32
10.000
---
U
6.
Benzo[k]fluoranthene
4.23
10.000
---
U
7.
Benzo[g,h,i)perylene
2.61
10.000
---
U
8.
Benzo[a)pyrene
3.27
10.000
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10.000
---
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
11.
Bis(2-Chloroethoxy) Methane
3.14
10.000
---
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
16.
Chrysene
4.04
10.000
---
U
17.
Dibenzo[a,h]anthracene
2.78
10.000
---
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
19.
Dimethyl Phthalate
3.78
10.000
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
21.
2,4-Dinitrotoluene
3.95
10.000
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
23.
Di-N-Octyl Phthalate
2.81
10.000
---
U
24,
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
25.
Fluoranthene
3.92
10.000
---
U
26.
Fluorene
2.95
10.000
---
U
27.
Hexachlorobenzene
2.61
10.000
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
29.
Indeno[1,2,3-Cd)pyrene
2.91
10.000
---
U
30.
Isophorone
3.74
10.000
---
U
31.
Nitrobenzene
2.85
10.000
---
U
32.
N-Nitrosodimethylamine
4.25
10.000
---
U
33.
N-Nitrosodiphenylamine
3.95
10.000
---
U
34.
N-Nitrosodi-N-Propylamine
4.06
10.000
---
U
35.
Phenanthrene
3.24
10.000
---
U
36.
Pyrene
3.63
10.000
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
38.
2-Chlorophenol
2.75
10.000
---
U
39.
O-Cresol
3.68
10.000
---
U
40.
P-Cresol
4.12
10.000
---
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
44.
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
47.
Methyl Methanesulfonate
4.92
10.000
---
U
48.
2-Nitrophenol
3.64
10.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ElMon[MR&O Flo hmpumUd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 2
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/24/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
FAA MRTHnn R270E R6(18)
PARAMETERS, ug/1
MDL
MRL
MW-14D
49.
4-Nitrophenol
3.17
50.000
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
51.
Phenol
1.86
10.000
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
55.
Acetophenone
2.89
10.000
---
U
56.
2-Acetylaminofluorene
3.98
20.000
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
60.
Chlorobenzilate
5.12
10.000
---
U
61.
Diallate
2.98
10.000
---
U
62.
Dibenzofuran
4.28
10,000
---
U
63.
3,31-Dichlorobenzidine
4.22
20.000
---
U
64.
Dimethoate
3.98
20.000
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10,000
---
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
69.
Diphenylamine
5.10
10.000
---
U
70.
Disulfoton
4.28
10.000
---
U
71.
Famphur
3.98
20.000
---
U
72.
Hexachloropropene
4.31
10.000
---
U
73.
Isosafrole
2.88
10.000
---
U
74.
Kepone
2.78
20.000
---
U
75.
Methapyrilene
3.54
100.000
---
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
77.
2-Methylnaphthalene
3.79
10.000
---
U
78.
Methyl Parathion
4.32
10.000
---
U
79.
m-Cresol
3.81
10.000
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
81.
1-Naphthylamine
5.61
10.000
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
83.
2-Nitroaniline
3.61
50,000
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
86,
5-Nitro-O-TOluidine
4.01
10.000
---
U
87,
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
88.
N-Nitrosodiethylamine
3.83
20.000
---
U
89.
N-Nitrosomethylethylamine
3.83
10.000
---
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
91.
N-Nitrosopyrrolidine
2.89
10.000
---
U
92.
Parathion
3.12
10.000
---
U
93.
Pentachlorobenzene
3.92
10.000
---
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
95.
Phenacetin
4.41
20.000
--- U
96.
1,4-Benzenediamine
2.99
10.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

f nnY'wnnnun(pan � i hnanonnom,M l
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 D
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 3
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/24/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
vna m munn R270R R6(18)
PARAMETERS, ug/1 MDL MRL
MW-14D
3.86
10.000
--- U
97. Phorate
98. Pronamide
3.69
10.000
--- U
99. Safrole
4.12
10.000
--- U
100. 1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
101. Thionazin
4.62
20.000
--- U
102. 0-Toluidine
4.11
10,000
--- U
103, 1,3,5-Trinitrobenzene
3.98
10.000
--- U
104. 0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
105. Hexachloroethane
1.49
10.000
--- U
106. Isodrin
3.11
20.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

f nnAnn nn nanny i No2no ono,, Wo
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
wma mvmunn R26nn R4(18)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 D
ANALYST: JAP
DATE COLLECTED: 12/15/22
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
:::L]
MW-141)
Trip
Blank
1.
Chloromethane
_
0.77
3.000
---
U
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
---
U
3.
Bromomethane
0.67
10.000
---
U
---
U
4.
Chloroethane
0.48
10.000
---
U
---
U
5,
Trichlorofluoromethane
0.24
1.000
---
U
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
---
U
7.
Acetone
9.06
100.000
---
U
---
U
8.
Iodomethane
0.26
10.000
---
U
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
---
U
10.
Methylene Chloride
0.64
1.000
---
U
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
13.
Vinyl Acetate
0.20
50.000
---
U
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
---
U
15.
2-Butanone
2.21
100.000
---
U
---
U
16.
BrOMOchloromethane
0.27
3.000
---
U
---
U
17.
Chloroform
0.25
5.000
---
U
---
U
18,
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
---
U
20.
Benzene
0.24
1.000
---
U
---
U
21.
1,2-Dichloroethane
0.02
0.200
---
U
---
U
22.
Trichloroethene
0.23
1.000
---
U
---
U
23.
1,2-Dichloropropene
0.04
0.200
---
U
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
---
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
---
U
27.
Toluene
0.23
1.000
---
U
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
---
U
31.
2-Hexanone
1.57
50.000
---
U
---
U
32.
Dibromochloromethane
0.03
0.200
---
U
---
U
33.
1,2-Dibromoethane
0.03
0.200
---
U
---
U
34.
Chlorobenzene
0.30
3.000
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
36.
Ethylbenzene
0.21
1.000
---
U
---
U
37.
Xylenes
0.68
5.000
---
U
---
U
38.
Dibromomethane
0.28
10.000
---
U
---
U
39.
Styrene
0.19
1.000
---
U
---
U
40.
Bromoform
0.20
3.000
---
U
---
U
41.
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
---
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
---
U
45.
1,2-Dibromo-3-Chlor0propane
0.07
0.200
---
U
--- U
46.
Acrylonitrile
2.72
200.000
---
U
--- U
47.
trans-1,4-Dichloro-2-Butene
0.42
100,000
---
U
--- U
48.
Acrolein
1.97
1
4.000
--- U
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 1

EIMUnNEW Flo kwpmbd
Drinking Water ID: 37715
PHONE [phone]
114 OAKMONT DRIVE
FAX [phone]
GREENVILLE, N.C. 27858
CLIENT: C &
D DISPOSAL, INC.
CLIENT ID:
6003 D
MR.
=SON WHITEHURST
802
NE
RECYCLING LANE
ANALYST:
JAP
GREENVILLE, NC
DATE COLLECTED:
12/15/22 Page: 2
DATE ANALYZED:
12/29/22
`
DATE REPORTED:
03/17/23
REVIEWED BY:
LANDFILL
APPENDIX II
cva mwTunn
R260n R4(18)
PARAMETERS, ug/1
MDL
MRL
MW-14D
Trip
Blank
49,
Allyl Chloride
0.20
10.000
---
U
---
U
0.21
20.000
---
U
---
U
50.
Chloroprene
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
56,
Ethyl Methacrylate
0.16
10.000
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
58.
Isobutyl Alcohol
12,80
100.000
---
U
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
---
U
60,
Methyl Methacrylate
0.25
30.000
---
U
---
U
61,
Naphthalene
0.47
6.000
---
U
---
U
62,
Propionitrile
3.26
150.000
---
U
---
U
63,
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
65.
Tetrahydrofuran
0.39
1.000
---
U
---
U
66,
1,4-Dioxane
2.71
3.000
---
U
-- =
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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��doQo��c��� Flo D�c�oQpoQa�c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
Drinking Water ID: 37715
Wastewater ID: 10dA
PHONE [phone]
FAX [phone]
ID#: 6003
DATE COLLECTED: 12/15/22
DATE REPORTED : 03/17/23
�v
REVIEWED BY:
MW-8
Analysis
Method
PARAMETERS
MDL
MRL
Date Analyst
Code
PH (field measurement), Units
6.9
12/15/22
PJC
4500HB-11
BOD, mg/l
2.0
2.0
r 10
12/15/22
HMM
5210E-16
COD, mg/l
0.840
20.0
393
12/16/22
HMM
H8000-79
Nitrate+Nitrite as N, mg/l
0.04
0.04
--- U
12/20/22
KES
353.2 R2-93
Total Organic Carbon, mg/l
0.129
1.0
36.95
12/16/22
HMM
531OC-14
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
1280
12/19/22
BNC
2320B-11
Chloride, mg/l
1.0
1.0
117
12/20/22
BLV
4500CLB-11
Cyanide, ug/1
5.0
5.0
--- U
12/22/22
HMM
4500CNE-16
Total Hardness, mg/l
760
12/19/22
HMV
2340C-11
Total Dissolved Residue, mg/l
10
10
1600
12/20/22
BNC
D5907-13
Sulfate, mg/l
5.0
5.0
226
12/19/22
DRC
4500SO42HII
Antimony, ug/l
0.30
1.0
--- U
12/22/22
NAB
EPA200.8
Arsenic, ug/1
0.13
5.0
30
12/22/22
NAB
EPA200.8
Barium, ug/l
0.14
10.0
487
12/22/22
NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
--- U
12/22/22
NAB
EPA200.8
Cadmium, ug/1
0.19
1.0
--- U
12/22/22
NAB
EPA200.8
Cobalt, ug/l
0.10
1.0
2.2
12/22/22
NAB
EPA200.8
Total Chromium, ug/l
0.19
5.0
23
12/22/22
NAB
EPA200.8
Copper, ug/l
0.26
10.0
--- U
12/22/22
NAB
EPA200.8
Iron, ug/l
12.20
50.0
27189
12/16/22
MTM
EPA200.7
Manganese, ug/l
2.70
10.0
840
12/16/22
MTM
EPA200.7
Lead, ug/l
0.09
5.0
0.25 J
12/22/22
NAB
EPA200.8
Mercury, ug/l
0.08
0.20
--- U
12/27/22
DRC
245.1 R3-94
Nickel, ug/l
0.13
10.0
1.8 J
12/22/22
NAB
EPA200.8
Selenium, ug/1
0.43
10.0
0.84 J
12/22/22
NAB
EPA200.8
Silver, ug/l
0.14
5.0
--- U
12/22/22
NAB
EPA200.8
Thallium, ug/l
0.13
1.0
0,14 J
12/22/22
NAB
EPA200.8
Tin, ug/l
0.36
100.0
--- U
12/22/22
NAB
EPA200.8
Vanadium, ug/l
0.14
1.0
4
12/22/22
NAB
EPA200.8
Zinc, ug/l
0.34
10.0
0.44 J
12/22/22
NAB
BPA200.8
Sulfide, ug/l
100
1000
TESTED
Conductivity (at 25c), uMhos/cm
1.0
1.0
2963
12/15/23
PJC
251OB-11
Dissolved Oxygen, mg/l
0.1
0.1
2.81
12/15/22
PJC
45000G-16
Temperature, °C
18
12/15/22
PJC
2550E-10
Iron (Ferrous), ug/l
50.00
100.0
9500
12/15/22
BLV
HACH IR-18C
Static Water Level, feet
10.21
12/15/22
PJC
Well Depth, feet
20.26
12/15/22
PJC
Carbon Dioxide, mg/l
1.0
1.0
324
12/15/22
HMM
45000O2C-11
+158
12/15/22
PJC
2580E-11
ORP, my
Turbidity (Field), NTU
1.0
1.0
3.17
12/15/22
PJC
213OB-11
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

ENAUTmEW alp hcupaTmUd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PESTICIDES AND PCB'S
EPA METHOD 8081B R2(07)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/19/22
DATE ANALYZED: 01/20/23
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-8
1.
Aldrin
0.029
0.050
---
U
2.
Alpha-BHC
0.032
0.050
---
U
3.
Beta-BHC
0.031
0.050
---
U
4.
Delta-BHC
0.030
0.050
0.056
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
6.
Chlordane
0.320
0.500
---
U
7.
4,4-DDD
0.051
0.100
---
U
8.
4,4-DDE
0.049
0.100
---
U
9.
4,4-DDT
0.052
0.100
---
U
10.
Dieldrin
0.042
0.075
---
U
11.
Endosulfan I
0.056
0.100
---
U
12.
Endosulfan II
0.046
0.100
---
U
13.
Endosulfan Sulfate
0.072
0.100
---
U
14,
Endrin
0.053
0.100
---
U
15.
Endrin Aldehyde
0.068
0.100
---
U
16.
Heptachlor
0.039
0.050
---
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
18.
Methoxychlor
0.530
1.000
---
U
19.
Pcb's (Aroclors)
0.500
2.000
---
U
20,
Toxaphene
0.690
1.500
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EfiW'0T@RHQM Flo kc@Tp@TMUd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: ����
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/21/22
DATE ANALYZED: 12/23/22
DATE REPORTED: 03/17/23
MW-S
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
2. Dinoseb
0.54
1.000
--- U
3. 2,4,5-TP
0.42
2.000
--- U
4. 2,4,5-T
0.47
2.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
Drinking Water ID: 37715
r ID: 1
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 1
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l
MDL
MRL
MW-8
1.
Acenaphthene
2.66
10.000
---
U
2.
Acenaphthylene
2.60
10.000
---
U
3.
Anthracene
2.97
10.000
---
U
4.
Benzo[a)antrhacene
4.16
10.000
---
U
5.
Benzo[b)fluoranthene
3.32
10.000
---
U
6.
Benzo[k)fluoranthene
4.23
10.000
---
U
7.
Benzo[g,h,i)perylene
2.61
10.000
---
U
8.
Benzo[a)pyrene
3.27
10.000
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10.000
---
U
10.
Butyl Benzyl Phthalate
5.78
10.000
---
U
11.
Bis(2-Chloroethoxy) Methane
3.14
10.000
---
U
12.
Bis(2-Chloroethyl) Ether
2.58
10.000
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
---
U
14.
2-Chloronaphthalene
2.17
10.000
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10.000
---
U
16.
Chrysene
4.04
10.000
---
U
17.
Dibenzo[a,h)anthracene
2.78
10.000
---
U
18.
Di-N-Butyl Phthalate
3.09
10.000
---
U
19,
Dimethyl Phthalate
3.7B
10.000
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
21,
2,4-Dinitrotoluene
3.95
10.000
---
U
22.
2,6-Dinitrotoluene
3.88
10.000
---
U
23.
Di-N-Octyl Phthalate
2.81
10.000
---
U
24.
Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
---
U
25.
Fluoranthene
3.92
10.000
---
U
26.
Fluorene
2.95
10.000
---
U
27.
Hexachlorobenzene
2.61
10.000
---
U
28.
Hexachlorocyclopentadiene
4.16
10.000
---
U
29.
Indeno[l,2,3-Cd)pyrene
2.91
10.000
---
U
30.
Isophorone
3.74
10.000
---
U
31.
Nitrobenzene
2.85
10.000
---
U
32.
N-Nitrosodimethylamine
4.25
10.000
---
U
33.
N-Nitrosodiphenylamine
3.95
10.000
---
U
34.
N-Nitrosodi-N-Propylamine
4.06
10.000
---
U
35.
Phenanthrene
3.24
10.000
---
U
36.
Pyrene
3.63
10.000
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.000
---
U
38.
2-Chlorophenol
2.75
10.000
---
U
39.
O-Cresol
3.68
10.000
---
U
40.
P-Cresol
4.12
10.000
---
U
41.
2,4-Dichlorophenol
5.19
10.000
---
U
42.
2,6-Dichlorophenol
4.89
10.000
---
U
43.
2,4-Dimethylphenol
3.21
10.000
---
U
44.
4,6-Dinitro-2-Methylphenol
4.77
50.000
---
U
45.
2,4-Dinitrophenol
4.37
50.000
---
U
46.
Ethyl Methanesulfonate
5.26
20.000
---
U
47.
Methyl Methanesulfonate
4.92
10.000
--- U
48.
2-Nitrophenol
3.64
10.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL 4uantitation Limits.

EMW'0T@MH(M Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: _J
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 2
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l
MDL
MRL
MW-8
49.
4-Nitrophenol
3.17
50.000
---
U
50.
Pentachlorophenol
5.33
25.000
---
U
51.
Phenol
1.86
10.000
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
U
53.
2,4,5-Trichlorophenol
4.17
10.000
---
U
54.
2,4,6-Trichlorophenol
3.84
10.000
---
U
55.
Acetophenone
2.89
10.000
---
U
56.
2-Acetylaminofluorene
3.98
20,000
---
U
57.
4-Aminobiphenyl
4.12
20.000
---
U
58.
Benzyl Alcohol
4.47
20.000
---
U
59.
4-Chloroaniline
3.36
20.000
---
U
60.
chlorobenzilate
5.12
10.000
---
U
61.
Diallate
2.98
10.000
---
U
62.
Dibenzofuran
4.28
10.000
---
U
63.
3,31-Dichlorobenzidine
4.22
20.000
---
U
64.
Dimethoate
3.98
20.000
---
U
65.
P-Dimethylaminoazobenzene
2.89
10.000
---
U
66.
7,12-Dimethylbenz[a]anthracene
5.26
10.000
---
U
67.
3,3-Dimethylbenzidine
3.21
10.000
---
U
68.
1,3-Dinitrobenzene
2.89
20.000
---
U
69,
Diphenylamine
5.10
10.000
---
U
70.
Disulfoton
4.28
10.000
---
U
71.
Famphur
3.98
20.000
---
U
72.
Hexachloropropene
4.31
10.000
---
U
73.
Isosafrole
2.88
10.000
---
U
74.
Kepone
2.78
20.000
---
U
75.
Methapyrilene
3.54
100.000
---
U
76.
3-Methylcholanthrene
4.21
10.000
---
U
77,
2-Methylnaphthalene
3.79
10.000
---
U
78.
Methyl Parathion
4.32
10.000
---
U
79.
m-Cresol
3.81
10,000
---
U
80.
1,4-Naphthoquinone
4.00
10.000
---
U
81,
1-Naphthylamine
5.61
10.000
---
U
82.
2-Naphthylamine
4.62
10.000
---
U
83.
2-Nitroaniline
3.61
50.000
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
85.
4-Nitroaniline
4.22
20.000
---
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
87.
N-Nitrosodi-n-butylamine
3.63
10.000
---
U
88.
N-Nitrosodiethylamine
3.83
20.000
---
U
89.
N-Nitrosomethylethylamine
3.83
10,000
---
U
90.
N-Nitrosopiperidine
5.19
20.000
---
U
91.
N-Nitrosopyrrolidine
2.89
10.000
---
U
92.
Parathion
3.12
10.000
---
U
93.
Pentachlorobenzene
3.92
10.000
---
U
94.
Pentachloronitrobenzene
3.71
20.000
---
U
95.
Phenacetin
4.41
20.000
--- U
96.
1,4-Benzenediamine
2.99
10.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

MAUTuDE(M % hmpumbd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 3
DATE EXTRACTED: 12/16/22
DATE ANALYZED: 01/04/23
DATE REPORTED: 03/17/23
SEMI -VOLATILE ORGANICS
EPA METHOD 8270E R6(18)
PARAMETERS, ug/l
MDL
MRL
MW-8
97.
Phorate
3.86
10.000
--- U
98.
Pronamide
3.69
10.000
--- U
99.
Safrole
4.12
10.000
--- U
100.
1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
101.
Thionazin
4.62
20.000
--- U
102.
0-Toluidine
4.11
10.000
--- U
103.
1,3,5-Trinitrobenzene
3.98
10.000
--- U
104.
0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
105.
Hexachloroethane
1.49
10.000
--- U
106.
Isodrin
3.11
20.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Drinking Water ID: 37715
In. in
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: ��✓ �`
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/15/22 Page: 1
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/1
MDL
MRL
MW-8
1.
Chloromethane
0.77
3.000
---
U
2.
Vinyl Chloride
0.12
0.200
---
U
3.
Bromomethane
0.67
10.000
---
U
4.
Chloroethane
0.48
10.000
---
U
5.
Trichlorofluoromethane
0.24
1.000
---
U
6.
1,1-Dichloroethene
0.17
5.000
---
U
7.
Acetone
9.06
100.000
17.30
J
8.
Iodomethane
0.26
10.000
---
U
9.
Carbon Disulfide
0.23
100.000
---
U
10.
Methylene Chloride
0.64
1.000
---
U
11.
trans-1,2-Dichloroethene
0.23
5.000
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
13.
Vinyl Acetate
0.20
50.000
---
U
14.
Cie-1,2-Dichloroethene
0.25
5.000
---
U
15.
2-Butanone
2.21
100.000
---
U
16.
Bromochloromethane
0.27
3.000
---
U
17.
Chloroform
0.25
5.000
---
U
18.
1,1,1-Trichloroethane
0.19
1.000
---
U
19.
Carbon Tetrachloride
0.04
0.200
---
U
20.
Benzene
0.24
1.000
---
U
21.
1,2-Dichloroethane
0.02
0.200
0.03
J
22.
Trichloroethene
0.23
1.000
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
24.
Bromodichloromethane
0.04
0.200
---
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
26.
4-Methyl-2-Pentanone
1.19
100.000
---
U
27.
Toluene
0.23
1.000
---
U
28.
trans-1,3-Dichloropropene
0.04
0.200
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
30.
Tetrachloroethene
0.10
0.200
---
U
31.
2-Hexanone
1.57
50.000
---
U
32.
Dibromochloromethane
0.03
0.200
---
U
33.
1,2-Dibromoethane
0.03
0.200
0.04
J
34.
Chlorobenzene
0.30
3.000
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
36.
Ethylbenzene
0.21
1.000
---
U
37.
Xylenes
0.68
5.000
---
U
38.
Dibromomethane
0.28
10.000
---
U
39.
Styrene
0.19
1.000
---
U
40.
Bromoform
0.20
3.000
---
U
41.
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
42.
1,2,3-Trichloropropane
0.09
0.200
---
U
43.
1,4-Dichlorobenzene
0.39
1.000
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
45.
1,2-Dibromo-3-Chloropropane
0.07
0.200
---
U
46.
Acrylonitrile
2.72
200.000
---
U
47.
trans-1,4-Dichloro-2-Butene
0.42
100.000
---
U
48.
Acrolein
1.97
4.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ERADTaIREGM Flo hwPoTmUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260D R4(18)
Drinking Water ID: 37715
Wastewater IDs 10
...._�T..w., ._,. ....
PHONE [phone]
FAX [phone]
CLIENT ID: 6003
ANALYST: JAP
DATE COLLECTED: 12/15/22 Page: 2
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-8
49.
Allyl Chloride
0.20
10.000
---
U
50.
Chloroprene
0.21
20.000
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
58.
Isobutyl Alcohol
12.80
100.000
---
U
59.
Methacrylonitrile
1.93
100.000
---
U
60.
Methyl Methacrylate
0.25
30.000
---
U
61.
Naphthalene
0.47
6.000
---
U
62.
Propionitrile
3.26
150.000
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
64.
Acetonitrile
36.29
55.000
---
U
65.
Tetrahydrofuran
0.39
1.000
14.50
66.
1,4-Dioxane
2.71
3.000
74.80
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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TOTAL CHLORINE, mg/I
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m
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<
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TEMPERATURE,°C
<
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so SIB Dnplivate
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ENW,Dmmmn� % hmpumUd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 B
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE DATE COLLECTED: 12/15/22
DATE REPORTED 03/17/23
GREENVILLE, NC 27834
REVIEWED BY:
MW-9A
MW-10
MW-11 MW-12s Trip
Analysis
Method
Blank
Date Analyst
Code
PARAMETERS
MDL
MRL
6.7
7.3
6.9
12/15/22 PJC
4500HB-11
PH (field measurement), Units
7.7
3.4
22
12/15/22 HMM
521OB-16
BOD, mg/l
2.0
2.0
--- U
r it
r
150
603
12/16/22 HMM
H8000-79
COD, mg/l
0.840
20.0
36
531
U
12/20/22 KES
353.2 R2-93
Nitrate+Nitrite as N, mg/1
0.04
0.04
--- V
'-- U
--- U
36.48
---
37.72
HMM
12/1166320B-1
5 310C-1 4
Total Organic Carbon, mg/l
0.129
1.0
10.96
42.80
1285
12//22
/22 HNC
2320CL8-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
274
950
620
206
12/9/22 BLV
Chloride, mg/l
1.0
1.0
11
190
60
6
12/22/22 HMM
450OCNE-16
Cyanide, ug/1
5.0
5.0
--- U
--- U
--- U
12//22 HMV
2340C-11
Total Hardness, mg/l
400
680
880
720
12/2727/22 ADR
2340C-11
Total Hardness, mg/1
1500
1200
1600
12/20/22 BNC
D5907-13
Total Dissolved Residue, mg/l
10
10
530
377
12/19/22 DRC
4500SO42EII
Sulfate, mg/1
5.0
5.0
154
30.3
--- U
52
052 J
12/22/22 NAB
EPA200.8
Antimony, ug/1
0.30
1.0
--- U
--- U
9
.
45
12/22/22 NAB
EPA200.8
Arsenic, ug/1
0.13
5.0
0.84 J
12
12/22/22 NAB
EPA200.8
Barium, ug/1
0.14
10.0
112
316
135
460
12/28/22 NAB
SPA200.8
Barium, ug/l
0.14
10.0
U
12/22/22 NAB
EPA200.8
Beryllium, ug/1
0.10
1.0
--- U
0.11 J
__-
- _ j7
01/04/23 NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
U
___ U
12/22/22 NAB
EPA200.8
Cadmium, ug/l
0.19
1.0
--- U
--- U
---
1.7
3'3
12/22/22 NAB
EPA200.8
Cobalt, ug/1
0.10
1.0
0.76 J
2.7
12/22/22 NAB
EPA200.8
Total Chromium, ug/l
0.19
5.0
0.40 J
41
5.8
0.30 J
-48
- U
12/22/22 NAB
EPA200.8
Copper, ug/l
0.26
10.0
--- U
--- U
187
25535
1298
12/16/22 MTM
EPA200.7
Iron, ug/1
12.20
50.0
16071
343
632
12/16/22 MTM
EPA200.7
Manganese, ug/l
2.70
10.0
873
329
V
12/16/22 NAB
EPA200.8
Lead, ug/ly,u
0.08
5.0
--- U
"-_
U
--- U
12/27/22 DRC
245.1 R3-94
Mercury, ug/1
0.13
U
-" U
3.6 J
---
1.9 J
3.6 J
12/22/22 NAB
EPA200.8
Nickel, ug/1
0.13
10.0
10.0
.2
0.29 J
0.71 J
2.3 J
12/22/22 NAB
EPA200.8
Selenium, ug/l
0.43
10.0
--- U
2.1 J
___ U
- U
12/22/22 NAB
EPA200.8
Silver, ug/1
0.14
.0
U
-" _ U
_
12/22/22 NAB
EPA200.8
Thallium, ug/1
0.13
1
1.0
0.38 J
--- U
U
_-- U
12/22/22 NAB
EPA200.8
Tin, ug/1
0.14
101.0
U
- U
""
__-
2
36
12/22/22 NAB
EPA200.8
Vanadium, ug/1
0.14
1.0
0.90 J
.9
20
1.1 J
1.8 J
12/22/22 NAB
EPA200.8
Zinc, ug/1
0.34
10.0
1000
1.2 J
TESTED
1.4 J
TESTED
TESTED
TESTED
Sulfide, ug/1
100
2461
1507
3093
12/15/23 PJC
2510E-11
Conductivity (at 25c), uMhoe/cm
1.0
1.0
1040
3.36
0 98
12/15/22 PJC
45000G-16
Dissolved Oxygen, mg/1
0.1
0.1
7.85
2.66
14
17
12/15/22 PJC
2550A-10
Temperature, °C
15
15
200
9000
5000
12/15/22 BLV
HACH IR-18C
Iron (Ferrous), ug/l
50.00
100.0
10000
4.50
12.70
12/15/22 PJC
Static Water Level, feet
6.30
4.11
22.73
23.84
22.93
12/15/22 PJC
Well Depth, feet
23.17
504
212
420
12/15/22 HMM
45000O2C-11
Carbon Dioxide, mg/l
1.0
1.0
132
+161
12/15/22 PJC
258OB-11
+149
+159
+146
ORP, my
All QC requirements were not met: r Replicate varied by more than 30%.
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
NOTE: Any result(s) listed above as "TESTED" were subcontracted to another laboratory. The corresponding result(s) are attached.

��doQor��c�r�� Flo D�c�oQpor���c�d
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
MW-9A
PARAMETERS MDL MRL
Turbidity (Field), NTU 1.0 1.0 8.58
PHONE [phone]
FAX [phone]
ID#: 6003 B
DATE COLLECTED: 12/15/22
DATE REPORTED : 03/17/23
REVIEWED BY:
MW-10 MW-11 MW-128 Trip Analysis Method
Blank Date Analyst Code
2.85 18.90 2.68 12/15/22 PJC 2130E-11
,7 = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

ERW'0T@[MH(@V Flo hmpumW
Drinking Water ID: 37715
W- tewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
PESTICIDES AND PCB'S
nnA TRc'munn RnAlR R7 (n7)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/19/22
DATE ANALYZED: 01/20/23
DATE REPORTED: 03/17/23
PARAMETERS, ug/l
MDL
MRL
MW-9A
MW-10
MW-11
MW-12s
1.
Aldrin
0.029
0.050
---
U
---
U
---
U
'--
U
2.
Alpha-BHC
0.032
0.050
---
U
---
U
---
U
---
U
U
3.
Beta-HHC
0.031
0.050
---
U
---
U
---
---
U
U
'--
0.04B
J
4.
Delta-BHC
0.030
0,050
---
U
---
U
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
---
U
---
U
U
6.
Chlordane
..
0320
0 500
---
U
---
U
---
U
---
U
7,
4,4-DDD
0.051
0.100
---
U
---
U
---
U
---
U
B.
4,4-DDE
0.049
0.100
---
U
---
U
---
U
---
---
U
9.
4,4-DDT
0.052
0.100
---
U
---
U
---
U
U
10.
Dieldrin
0.042
0.075
---
U
---
U
---
U
---
U
11,
Endoaulfan I
0.056
0.100
---
U
---
U
---
U
---
---
U
12.
Sndosulf an ZI
46
0.0.
0100
---
U
---
U
---
U
---
U
13.
Endoaulfan Sulfate
0.072
0.100
---
U
---
U
---
U
__
U
14.
Sndrin
0.053
0.100
---
U
U
__ -
U
15.
Sndrin Aldehyde
0.068
0.100
---
U
---
U
---
U
---
U
16.
Heptachlor
0.039
0.050
---
U
---
U
---
U
U
17.
Heptachlor Epoxide
0.042
0.075
---
U
---
U
---
U
=_-
-
U
18.
Methoxychlor
0.530
1.000
---
U
---
U
---
U
U
19.
Pcb's (Aroclors)
0.500
2.000
---
U
---
U
---
U
---
0690
1..500
-
U
---
U
---
U
---
U
20.
Toxaphene
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

rp
own[MR&W % hmpudid
Drinking Water ID: 37715
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: ��✓/ U
LANDFILL APPENDIX II
ana mWMWnn Al 51 A Rl (96)
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/21/22
DATE REPORTED: 03/17/23
Date
Analyzed
12/23/22
12/27/22
12/23/22
12/27/22
MW-9A
MW-10
MW-11
MW-12s
PARAMETERS, Ug/l
MDL
MRL
0.36
2.000
--- U
0.763 J
--- U
1.00 J
1.
2,4-D
U
--- U
--- U
- U
2.
Dinoeeb
0.54
1.000
---
3.
2,4,5-TP
0.42
2.000
--- U
--- U
--- U
U
4.
2,4,5-T
0.47
2.000
--- U
--- U
--- U
---
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

RMOTmEW Flo hmpumbd
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: \v
SEMI -VOLATILE ORGANICS
wnT ?Avmvnn A77nR R6 (18)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/15/22 Page: 1
DATE EXTRACTED: 12/16/22
DATE REPORTED: 03/17/23
Date Analyzed
PARAMETERS, ug/l MDL MRL
01/04/23
MW_9A
01/24/23
MW-10
01/24/23
MW-11
01/24/23
MW-12s
1. Acenaphthene
2.66
10.000
--- U
--- U
--- U
--- U
U
2. Acenaphthylene
2.60
10.000
--- U
--- U
--- U
=--
- U
3. Anthrac ens
2.97
10.000
--- U
--- U
--- U
- U
4. Benzo[a]antrhacene
4.16
10.000
- U
-"- U
__ - U
U
5. Benzo[b]fluoranthene
3.32
10.000
--- U
--- U
--- U
---
--- U
6. Benzo[k]fluoranthene
4.23
10.000
--- U
--- U
--- U
--- U
7. Benzo[g,h,i]perylene
2.61
10.000
--- U
--- U
--- U
8. Benzo[a]pyrene
3.27
10.000
--_ U
-"- U
U
- U
9. 4-Bromophenyl Phenyl Ether
2.63
10.000
--- U
--- U
-" U
_-
--- U
10. Butyl Benzyl Phthalate
5.78
10.000
--- U
--- U
--- U
11. Bis(2-Chloroethoxy) Methane
3.14
10.000
--- U
___ U
___ U
--- U
12. Bis(2-Chloroethyl) Ether
2.58
10.000
--- U
___ U
--- U
--- U
13. Bis(2-Chloro-l-methylethyl) Ether
2.58
10.000
--- U
--- U
--- U
14. 2-Chloronaphthalene
2.17
10.000
--- U
--- U
--- U
- U
15. 4-Chlorophenyl Phenyl Ether
2.42
10.000
___ U
___ U
___ U
4.04
10,000
--- U
--- U
--- U
16. Chrysene
--- U
--- U
- U
17. Dibenzo[a,h]anthracene
. 278
10000
.
- U
U
18. Di-N-Butyl Phthalate
3.09
10.000
--- U
--- U
--- U
---
--- U
19. Dimethyl Phthalate
3.78
10.000
--- U
--- U
--- U
U
20. Diethyl Phthalate
3.92
10.000
--- U
--- U
--- U
---
--- U
21. 2,4-Dinitrotoluene
3.95
10.000
--- U
--- U
--- U
--- U
22. 2,6-Dinitrotoluene
3.88
10.000
--- U
--- U
--- U
--- U
23, Di-N-Octyl Phthalate
2.81
10.000
--- U
--- U
--- U
U
24. Bis-(2-Ethylhexyl) Phthalate
9.97
15.000
--- U
--- U
--- U
=--
- U
25. Fluoranthene
3.92
10.000
--- U
--- U
--- U
U
26. Fluorene
2.95
10.000
--- U
U
--- U
---
__ - U
27. Hexachlorobenzene
2.61
10.000
--- U
--- U
--- U
28. Hexachlorocyclopentadiene
4.16
10.000
--- U
-- U
--- U
29, Indeno[1,2,3-Cd]pyrene
2.91
10.000
--- U
--- U
--- U
--- U
3.74
10.000
--- U
--- U
--- U
30. Isophorone
--- U
--- U
U
31, Nitrobenzene
2.85
10.000
--- U
=--
- U
32. N-Nitroeodimethylamine
4.25
10.000
--- U
--- U
--- U
U
33, N-Nitrosodiphenylamine
3.95
10.000
--- U
--- U
--- U
---
U
34. N-Nitrosodi-N-Propylamine
4.06
10.000
--- U
--- U
--- U
---
35. Phenanthrene
3.24
10.000
--- U
--- U
--- U
--- U
- U
3.63
10.000
--- U
--- U
36. Pyrene
--- U
--- U
--- U
37. 4-Chloro-3-Methylphenol
3.79
20.000
--- U
U
2.75
10.000
--- U
--- U
--- U
---
38. 2-Chlorophenol
--- U
--- U
--- U
--- U
39, 0-Cresol
3.68
10.000
U
--- U
40. P-Cresol
4.12
10.000
--- U
--- U
---
- U
41. 2,4-Dichlorophenol
5.19
10.000
--- U
--- U
__
--- U
42. 2,6-Dichlorophenol
4.89
10.000
--- U
--- U
--- U
--- U
43. 2,4-Dimethylphenol
3.21
10.000
--- U
--- U
--- U
--- U
44. 4,6-Dinitro-2-Methylphenol
4.77
50.000
--- U
--- U
--- U
--- U
45. 2,4-Dinitrophenol
4.37
50.000
--- U
--- U
--- U
--- U
46. Ethyl Methaneeulfonate
5.26
20.000
--- U
--- U
--- U
--- U
--- U
47, Methyl Methaneeulfonate
4.92
10.000
--- U
-" U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

E[Mumfln(M Flo hCopumbd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
PHONE [phone]
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: C &
D DISPOSAL, INC.
CLIENT ID:
6003 B
MR.
JUDSON WHITEHURST
802
NE
RECYCLING LANE
ANALYST:
HIC
GREENVILLE,
NC
DATE COLLECTED:
12/15/22 Page: 2
DATE EXTRACTED:
12/16/22
BY:
DATE REPORTED:
03/17/23
REVIEWED
SEMI -VOLATILE
ORGANICS
vvn mwTwnn R270E R6 (18)
Date Analyzed
PARAMETERS, ug/l MDL MRL
01/04/23
MW-9A
01/24/23
MW-10
01/24/23
MW-11
01/24/23
MW-12s
48. 2-Nitrophenol
3.64
10.000
--- U
--- U
--- U
--- U
--- U
--- U
49. 4-Nitrophenol
3.17
50.000
--- U
--- U
U
--- U
50, Pentachlorophenol
5.33
25.000
--- U
--- U
---
U
51. Phenol
1.86
10.000
--- U
- U
- U
52. 2,3,4,6-Tetrachlorophenol
3.12
10.000
--- U
--- U
--
U
--- U
53. 2,4,5-Trichlorophenol
4.17
10.000
--- U
--- U
---
--- U
--- U
54. 2,4,6-Trichlorophenol
3.84
10.000
--- U
--- U
U
--- U
55. Acetophenone
2.89
10.000
--- U
--- U
---
U
--- U
56. 2-Acetylaminofluorene
3.98
20.000
--- U
--- U
---
--- U
--- U
57. 4-Aminobiphenyl
4.12
20.000
--- U
--- U
U
--- U
58. Benzyl Alcohol
4.47
20.000
--- U
--- U
---
--- U
--- U
59. 4-Chloroaniline
3.36
20.000
--- U
--- U
U
--- U
60. Chlorobenzilate
5.12
10.000
--- U
--- U
---
U
___ U
61. Diallate
2.98
10.000
-_- U
--- U
---
U
- U
62. Dibenzofuran
4.28
10.000
--- U
U
U
_ - U
63. 3,3'-Dichlorobenzidine
4.22
20.000
--- U
--- U
---
--- U
--- U
64. Dimethoate
3.98
20.000
--- U
--- U
U
--- U
--- U
65. P-Dimethylaminoazobenzene
2.89
10.000
--- U
_""
-'- U
66. 7,12-Dimethylbenz[a]anthracene
5.26
10.000
--- U
--- U
--- U
--- U
67. 3,3-Dimethylbenzidine
3.21
10.000
--- U
--- U
U
--- U
68. 1,3-Dinitrobenzene
2.89
20.000
--- U
--- U
--- U
---
--- U
--- U
69. Diphenylamine
5.10
10.000
--- U
U
--- U
70, Disulfoton
4.28
10.000
--- U
--- U
--- U
---
--- U
--- U
71. Famphur
3.98
20.000
--- U
__ - U
U
--- U
72. Hexachloropropene
4.31
10.000
--- U
--- U
--- U
--- U
73, Isosafrole
2.88
10.000
--- U
-"" U
--- U
--- U
�74. Kepone
2.78
20.000
--- U
--- U
___ U
--- U
75. Methapyrilene
3.54
100.000
--- U
U
--- U
76. 3-Methylcholanthrene
4.21
10.000
--- U
--- U
---
--- U
--- U
77. 2-Methylnaphthalene
3.79
10.000
--- U
--- U
U
--- U
78. Methyl Parathion
4.32
10.000
--- U
--- U
--- U
---
--- U
--- U
79. m-Cresol
3.81
10.000
--- U
--- U
___ U
--- U
4.00
10.000
--- U
80. 1,4-Naphthoquinone
--- U
--- U
--- U
--- U
81. 1-Naphthylamine
5.61
10.000
U
--- U
82. 2-Naphthylamine
4.62
10.000
--- U
--- U
---
U
--- U
83. 2-Nitroaniline
3.61
50.000
--- U
--- U
---
U
--- U
84. 3-Nitroaniline
4.81
50.000
--- U
--- U
---
U
--- U
85. 4-Nitroaniline
4.22
20.000
--- U
--- U
---
--- U
--- U
86. 5-Nitro-O-Toluidine
4.01
10.000
--- U
--- U
--- U
--- U
87. N-Nitrosodi-n-butylamine
3.63
10.000
--- U
--- U
--- U
--- U
88. N-Nitroeodiethylamine
3.83
20.000
--- U
--- U
--- U
--- U
89. N-Nitroaomethylethylamine
3.83
10.000
--- U
--- U
--- U
--- U
90. N-Nitrosopiperidine
5.19
20.000
--- U
--- U
V
91, N-Nitrosopyrrolidine
2.89
10.000
--- U
__ _ U
___
U
___ U
92. Parathion
3.12
10.000
--- U
U
-
- - U
- U
93. Pentachlorobenzene
3.92
10.000
--- U
--- U
94. Pentachloronitrobenzene
3.71
20.000
--- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Ein'UnHH&M Flo hmpumUd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: HIC
DATE COLLECTED: 12/15/22
DATE EXTRACTED: 12/16/22
��. DATE REPORTED: 03/17/23
REVIEWED BY:
SEMI -VOLATILE ORGANICS
swa mmmunn R270E R6 (18)
Date Analyzed
PARAMETERS, ug/l MDL MRL
01/04/23
MW-9A
01/24/23
MW-10
01/24/23
MW-11
01/24/23
MW-129
4.41
20.000
--- U
--- U
--- U
--- U
95. Phenacetin
--- U
--- U
--- U
96. 1,4-Benzenediamine
2.99
10.000
--- U
--- U
--- U
3.86
10.000
--- U
--- U
97. Phorate
--- U
--- U
--- U
98. Pronamide
3.69
10.000
--- U
--- U
--- U
99. Saf role
4.12
10.000
--- U
--- U
- U
U
100, 1,2,4,5-Tetrachlorobenzene
5.01
10.000
--- U
--- U
__
--- U
--- U
101. Thionazin
4.62
20.000
--- U
--- U
--- U
--- U
--- p
102. 0-Toluidine
4.11
10.000
--- U
--- U
--- U
103. 1,3,5-Trinitrobenzene
3.98
10.000
--- U
--- U
--- U
--- U
104. 0,0,0-Triethyl Phosphorothioate
3.61
10.000
--- U
--' U
U
--- U
105. Hexachloroethane
1.49
10.000
--- U
--- U
---
U
--- U
106. Isodrin
3.11
20.000
--- U
--- U
---
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.
Page: 3

��IY/�II OIIIIIIIIII��� I1� �IIu�O�I�JIOP�p ��� Drinking Water ID: 37715
LLL���LLLIIILLLJJI l:J LI LILILILILI LILIIllSS7 IJ U �! ILII-� Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
.,r ,x mvnn R79nn R4 (l R)
PHONE [phone]
FAX [phone]
CLIENT ID: 60Q3 B
ANALYST: JAP
DATE COLLECTED: 12/15/22 Page: 1
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
MDL MRL
PARAMETERS, ug/1
MW-9A
MW-10
MW-11
MW-12s
Trip
Blank
0.77
3.000
--- U
--- U
--- U
--- U
--- U
1. Chloromethane
0.17 J
0.12 J
1--
-- - U
2. Vinyl Chloride
0.12
0.200
--- U
_ U
- V
U
3. Bromomethane
0.67
10.000
--- U
--" U
--- U
--- U
--- U
4. Chloroethane
0.48
10.000
--- U
--- U
U
--- U
--- V
5. Trichlorofluoromethane
0.24
1.000
--- U
--- U
---
--- U
--- U
6.
0.17
5.000
--- U
--- U
--- U
9.99 J
25.20 J
__ V
Acetone
7. Acetone
9.06
100.000
--- U
--- U
- U
--
8, Iodomethane
0.26
10.000
--- U
--- U
U
0.48 J
1.21 J
--- U
9. Carbon Disulfide
0.23
100.000
--- U
---
--- U
--- U
--- U
10. Methylene Chloride
0.64
1.000
--- U
--- U
--- U
--- U
11. trans-1,2-Dichloroethene
0.23
5.000
--- U
--- U
--- U
--- U
--- U
--- U
12. 1,1-Dichloroethane
0,20
5.000
--- U
--- U
_ U
13. Vinyl Acetate
0.20
50.000
--- U
--- U
=_
- U
0.36 J
- U
14. Cis-1,2-Dichloroethene
0.25
5.000
--- U
--- U
--- U
2.30 J
--- U
15. 2-Butanone
2.21
100.000
--- U
--- U
U
--- U
--- U
---
16. Bromochloromethane
0.27
3.000
--- U
---
--- U
--- U
--- U
0.25
5.000
--- U
--- U
17. Chloroform
--- U
--- U
--- U
---
18. 1,1,1-Trichloroethane
0.19
1.000
--- U
_ U
19. Carbon Tetrachloride
0.04
0.200
--- U
--- U
--
0.73 J
1.88
_ U
0.24
1.000
--- U
0.62 J
--- U
20. Benzene
--- U
0--- J
0--- J
0--- J
21. 1,2-Dichloroethane
0.23
U
- U
" U
22. Trichloroethene
0.23
1.200
1.000
--- U
--- U
U
---
0--- J
0--- J
---
23. 1,2-Dichloropropane
0.04
0.200
--- U
---
--- U
- V
- - U
24. Bromodichloromethane
0.04
0.200
--- U
--- U
--- U
___ U
--- U
25. Cie-1,3-Dichloropropene
0.06
0.200
--- V
--- U
__- U
___ U
--- U
26, 4-Methyl-2-Pentanone
1.19
100.000
--- V
--- U
--- U
--- U
---
27. Toluene
0.04
-- _ V
__-
- U
U
U
--- U
28. trans-1,3-Dichloropropene
0.04
0.200
0.200
-- U
V
- - - U
- U
- D
29. 1,1,2-Trichloroethane
0.
0.200
-- - U
___ U
U
--- U
--- U
30. Tetrachloroethene
10
0.00
-- - U
--- U
---
V
--- U
--- V
31. 2-Hexanone
.57
1.57
50.000
--- U
--- U
--- U
---
U
--- U
32. Dibromochloromethane
0.03
0.200
--- U
___ U
--- U
--- U
33. 1,2-Dibromoethane
0.03
0.200
--- U
--- U
t7
___ U
--- U
34. Chlorobenzene
0.30
3.000
--- U
--- U
___
U
___ V
--- U
35. 1,1,1,2-Tetrachloroethane
0.22
1.000
--- U
--- U
___
U
--- U
--- U
0.68
--- U
0--- J
__-
36. Ethylbenzene
-- U
--- U
--- U
--- U
37, Xylenes
0.68
5.000
5.000
-- - U
_-- U
--- U
--- U
--- U
38. Dibromomethane
0.28
10.000
--- U
_ U
0..000
-- - U
--- U
--- U
39. Styrene
--- U
--- U
--- U
--- U
40. BroM0form
0.20 20
3.000
U
___ U
--- U
--- U
41. 1,1,2,2-Tetrachloroethane
0.03
0.200
--- U
---
U
--- U
--- U
42. 1,2,3-Trichloropropane
0.09
0.200
--- U
--- U
--- U
---
--- U
--- U
--- U
43. 1,4-Dichlorobenzene
0.39
1.000
--- U
--- U
--- U
--- U
--- U
44. 1,2-Dichlorobenzene
0.32
5.000
--- U
U
U
--- U
45. 1,2-Dibromo-3-Chloropropane
.
0.200
--- U
U
---
--- V
-- _ U
-_ _ U
46, Acrylonitrile
2 .72
200.000
- - U
-- U
-- U
--- U
--- U
--- U
47, trans-1,4-Dichloro-2-Butene
0.42
100.000
-- - U
"
- U
--- U
--- V
48. Acrolein
1.97
4.000
--' U
- -- U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

��dor�o��c��� Flo D�c�oQpoQ��c�d
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY:
LANDFILL APPENDIX II
-R Mwr%" 017Gf)n Rd fl Rl
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 B
ANALYST: JAP
DATE COLLECTED: 12/15/22 Page: 2
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/1
MDL
MRL
MW-9A
MW-10
MW-11
MW-12s
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
---
U
---
U
U
---
---
U
U
---
---
V
U
0.21
20.000
---
U
---
U
---
50.
Chloroprene
---
U
---
U
---
U
---
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
U
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
---
---
U
---
V
0.28
1.000
---
U
---
U
---
U
53.
1,3-Dichloropropane
---
U
---
U
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
U
__-
U
_-_
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
---
U
---
U
---
U
56.
Ethyl Methacrylate
0.16
10.000
---
U
---
U
---
---
U
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
U
58.
Isobutyl Alcohol
..
1280
100000
-
U
- --
U
---
1.93
100.000
---
U
---
U
__ _
U
U
59.
61.
Methacrylonitrile
Methyl Methacrylate
0.25
30.000
---
U
---
U
---
U
U
---
1.42
V
J
---
---
V
0.47
6.000
---
U
2.12
J
--_
61.
Naphthalene
---
U
_
U
V
U
62.
Propionitrile
3.26
150.000
---
U
U
---
U
---
U
63,
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
---
-
U
64.
Acetonitrile
36.29
55.000
---
U
---
22.10
U
__
20.40
34.00
---
U
65,
Tetrahydrofuran
0.39
1.000
---
U
29.80
22.40
31.10
-
U
66.
1,4-Dioxane
2.71
3.000
---
U
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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Emwkwm[W Flo hmpumbd
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
PARAMETERS MDL
PH (field measurement), Units
Alkalinity (to pH 4.5), mg CaCO3/1 1.0
Chloride, mg/l
1.0
Chloride, mg/l
1.0
Total Dissolved Residue, mg/l
10
Sulfate, mg/l
5.0
Antimony, ug/l
0.30
Arsenic, ug/l
0.13
Barium, ug/l
0.14
Beryllium, ug/l
0.10
Cadmium, ug/l
0.19
Cobalt, ug/l
0.10
Total Chromium, ug/1
0.19
Copper, ug/l
0.26
Iron, ug/1
12.20
Manganese, ug/1
2.70
Lead, ug/1
0.09
Nickel, ug/1
0.13
Selenium, ug/l
0.43
Silver, ug/l
0.14
Thallium, ug/l
0.13
Vanadium, ug/l
0.14
Zinc, ug/l
0.34
Sulfide, ug/l
100
Conductivity (at 25c), uMhos/cm
1.0
Dissolved Oxygen, mg/1
0.1
Temperature, °C
8260 (duplicate)
8260 (duplicate)
ORP, my
Turbidity (Field), NTU
1.0
SW-1 SW-2 SW-3
MRL
MISSING
1.0 MISSING
1.0 MISSING
1.0
10 MISSING
5.0 MISSING
1.0 MISSING
5.0 MISSING
10.0 MISSING
1.0 MISSING
1.0 MISSING
1.0 MISSING
5.0 MISSING
10.0 MISSING
50.0 MISSING
10.0 MISSING
5.0 MISSING
10.0 MISSING
10.0 MISSING
5.0 MISSING
1.0 MISSING
1.0 MISSING
10.0 MISSING
1000 MISSING
1.0 MISSING
0.1 MISSING
MISSING
MISSING
MISSING
MISSING
1.0 MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
MISSING
All QC requirements were not met: r Replicate varied by more than 30%.
PHONE [phone]
FAX [phone]
ID#: 6003 C
DATE COLLECTED: 12/19/22
DATE REPORTED : 03/17/23
I
REVIEWED BY:
7.7
128
35
260
71.9
--- U
2.3 J
105
- U
U
0.58 J
3.3 J
0.54 J
1763
82
0.25 J
0.84 J
- U
U
U
1
5.3 J
--- U
1093
7.45
6
+159
9.62
SW-4 Piezometer
Analysis
Method
#10
Date Analyst
Code
8.0
6.4
12/19/22
PJC
4500HB-11
14
13
12/27/22
BNC
2320E-11
15
12/20/22
BLV
4500CLB-11
5
12/27/22
JDJ
4500CLB-11
110
190
12/20/22
HNC
D5907-13
40.2
116
12/29/22
DRC
4500SO42Ell
___ U
--- U
12/22/22
NAB
EPA200.8
0.41 J
5.4
12/22/22
NAB
EPA200.8
66.9
119
12/22/22
NAB
EPA200.8
0.12 J
2
01/04/23
NAB
EPA200.8
___ U
--- U
12/22/22
NAB
EPA200.8
0.61 J
8.4
12/22/22
NAB
EPA200.8
1.0 J
31
12/22/22
NAB
EPA200.8
0.50 J
5 J
12/22/22
NAB
EPA200.8
597
17894
12/22/22
MTM
EPA200.7
10
54
12/22/22
MTM
EPA200.7
0.50 J
15
12/22/22
NAB
EPA200.8
0.91 J
9.8 J
12/22/22
NAB
EPA200.8
___ U
1.2 J
12/22/22
NAB
EPA200.8
U
--- U
12/22/22
NAB
EPA200.8
--- U
0.25 J
12/22/22
NAB
EPA200.8
1
40
12/22/22
NAB
EPA200.8
6.5 J
38
12/22/22
NAB
EPA200.8
--- U
256 J
12/21/22
HMM
4500S2D-11
224
70
12/19/22
PJC
251OB-11
11.43
1.22
12/19/22
PJC
45000G-16
5
13
12/19/22
PJC
255OB-10
+130
+106
12/19/22
PJC
258OB-11
7.51
570
12/19/22
PJC
213OB-11
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

Enw,unREM Flo hCwP@TM%d
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 C
C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE DATE COLLECTED: 12/19/22
DATE REPORTED 03/17/23
GREENVILLE, NC 27834
REVIEWED BY: ✓/J/`�/ L
Piezometer Trip
Piezometer Analysis
Method
PARAMETERS
MDL
MRL
#11 Blank
#11D Date Analyst
Code
6.1
12/19/22
PJC
4500HB-11
PH (field measurement),
Units
12/27/22
BNC
2320B-11
Alkalinity (to pH 4.5),
mg CaCO3/1
1.0
1.0
14
12/20/22
BLV
4500CLB-11
Chloride, mg/1
1.0
1.0
6
6
12/20/22
BNC
D5907-13
Total Dissolved Residue,
mg/l
10
10
160
12/29/22
DRC
4500SO42EII
Sulfate, mg/l
5.0
5.0
112
12/22/22
NAB
EPA200.8
Antimony, ug/l
0.30
1.0
--- U
12/22/22
NAB
EPA200.8
Arsenic, ug/1
0.13
5.0
2.8 J
12/28/22
NAB
EPA200.8
Barium, ug/1
0.14
10.0
161
01/04/23
NAB
EPA200.8
Beryllium, ug/l
0.10
1.0
2
12/22/22
NAB
RPA200.8
Cadmium, ug/l
0.19
1.0
--- U
12/22/22
NAB
EPA200.8
Cobalt, ug/l
0.10
1.0
3.5
12/22/22
NAB
EPA200.8
Total Chromium, ug/1
0.19
5.0
6.5
12/22/22
NAB
EPA200.8
Copper, ug/1
0.26
10.0
1 J
12/22/22
MTM
EPA200.7
Iron, ug/1
12.20
50.0
12832
12/22/22
MTM
EPA200.7
Manganese, ug/l
2.70
10.0
78
12/22/22
NAB
EPA200.8
Lead, ug/l
0.09
5.0
1.8 J
12/22/22
NAB
EPA200.8
Nickel, ug/l
0.13
10.0
5.2 J
12/22/22
NAB
HPA200.8
Selenium, ug/l
0.43
10.0
1.2 J
12/22/22
NAB
EPA200.8
Silver, ug/1
0.14
5.0
--- U
12/22/22
NAB
EPA200.8
Thallium, ug/l
0.13
1.0
--- U
12/22/22
NAB
EPA200.8
Vanadium, ug/1
0.14
1.0
9
12/22/22
NAB
EPA200.8
Zinc, ug/l
0.34
10.0
32
12/21/22
HMM
4500S2D-11
Sulfide, ug/1
100
1000
--- U
12/19/22
PJC
2510E-11
Conductivity (at 25c),
uMhoe/cm
1.0
1.0
234
12/19/22
PJC
45000G-16
Dissolved Oxygen, mg/1
0.1
0.1
2.81
12/19/22
PJC
2550B-10
Temperature, °C
13
51.85 12/19/22
PJC
Well Depth, feet
+103
12/19/22
PJC
2580B-11
ORP, my
1.0
260
12/19/22
PJC
2130H-11
Turbidity (Field), NTU
1.0
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

EADmEaM alp hmpumW
Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: C & D DISPOSAL, INC.
MR. JUDSON WHITEHURST
802 RECYCLING LANE
GREENVILLE, NC 27834
REVIEWED BY: 11 '�v
LANDFILL APPENDIX II
--MWnn 079znn T?d (1 R)
PHONE [phone]
FAX [phone]
CLIENT ID: 6003 C
ANALYST: JAP
DATE COLLECTED: 12/19/22 Page: 1
DATE ANALYZED: 12/29/22
DATE REPORTED: 03/17/23
PARAMETERS, ug/1 MDL MRL
SW-3
SW-4
Piezometer
#10
Piezometer
#11
Trip
Blank
1. Chloromethane
0.77
3,000
--- U
--- U
--- U
--- V
--- U
--- V
--- V
2. Vinyl Chloride
0.12
0.200
--- U
--- U
-'- U
3. Bromomethane
0.67
10.000
--- U
--- U
--- U
--- U
--- U
4. Chloroethane
0.48
10.000
--- U
--- U
--- U
--- U
--- U
5. Trichlorofluoromethane
0.24
1.000
--- U
--- U
--- U
--- U
--- V
0.17
5.000
--- U
--- U
--- U
6. 1,1-Dichloroethene
9.06
100.000
--- U
--- U
__ - U
7. Acetone
--- U
--- U
- U
8. Iodomethane
0.26
10.000
--- U
- U
U
V
9. Carbon Disulfide
0.23
100.000
--- U
-"- U
--- U
--- U
--- U
10. Methylene Chloride
0.64
1.000
--- U
--- U
--- U
11. trans-1,2-Dichloroethene
0.23
5.000
--- U
--- U
--- U
--- U
--- U
12. 1,1-Dichloroethane
0.20
5.000
--- U
--- U
- U
13. Vinyl Acetate
0.20
50.000
--- U
--" U
__
--- U
--- U
--- U
14. Cie-1,2-Dichloroethene
0.25
5.000
--- U
--- U
2.21
100.000
--- U
--- U
--- U
15. 2-Butanone
--- U
--- U
--- U
---
16. Bromochloromethane
0.27
3.000
--- U
--- U
--- U
--- U
17. Chloroform
0.25
5.000
--- U
--- U
U
--- U
--- V
18. 1,1,1-Trichloroethane
0.19
1.000
--- U
--- U
---
19. Carbon Tetrachloride
0.04
0.200
--- U
--- U
--' U
--- U
--- U
0.24
1.000
--- U
--- U
--- U
20. Benzene
U
--- U
--- U
--- U
---
21. 1,2-Dichloroethane
0.02
0.200
---
--- U
--- V
22. Trichloroethene
0.23
1.000
--- U
--- U
'-- U
--- U
--- U
--- U
23, 1,2-Dichloropropane
0.04
0.200
--- U
--- U
U
--- U
--- V
24. Bromodichloromethane
0.04
0.200
--- U
--- U
---
25. Cie-1,3-Dichloropropene
0.06
0.200
--- U
--- U
--- U
--- U
--- U
--- U
26, 4-Methyl-2-Pentanone
1.19
100.000
--- U
--- U
U
--- U
--- V
0.23
1.000
--- U
--- U
-'-
27. Toluene
--- U
--- U
__
--
28. trans-1,3-Dichloropropene
0.04
0.200
--- U
--- U
--- V
29. 1,1,2-Trichloroethane
0.03
0.200
--- U
--- U
'-- U
U
--- U
30. Tetrachloroethene
0.10
0.200
--- U
--- U
--- U
--- U
---
31. 2-Hexanone
1.57
50.000
--- U
--- U
--- U
--- U
--- U
---
32. Dibromochloromethane
0.03
0.200
--- U
U
33. 1,2-Dibromoethane
0.03
0.200
--- U
--- U
---
34. Chlorobenzene
0.30
3.000
--- U
--- U
--- U
--- U
--- U
--- U
35. 1,1,1,2-Tetrachloroethane
0.22
1.000
--- U
--- U
--- U
--- U
0.21
1.000
--- U
--- U
'-- U
36. Ethylbenzene
--- U
--- U
--- V
-'- V
37. Xylenes
0.68
5.000
-- - U
- U
_ U
38. Dibromomethane
0.28
10,000
--- U
_
VU
-
0.19
1.000
--- U
--- U
___
39. Styrene
--- U
U
V
40. Bromoform
0.20
3.000
--- U
U
--- U
41. 1,1,2,2-Tetrachloroethane
0.03
0.200
--- U
---
--- U
--- U
--- V
42. 1,2,3-Trichloropropane
0.09
0.200
- - U
--- U
--- U
--- U
--- V
43. 1,4-Dichlorobenzene
0.39
1.000
--- U
--- U
U
--- U
--- U
44. 1,2-Dichlorobenzene
0.32
5.000
--- U
--- U
---
V
--- U
--- V
45. 1,2-Dibromo-3-Chloropropane
0.07
0.200
--- U
--- U
---
U
--- U
--- V
47, Acrylonitrile
2.72
200.000
--- U
--- U
---
U
--- U
--- V
4trans-1,4-Dichloro-2-Butene
0.42
100.000
--- V
--- U
---
--- U
1.97
4.000
U
--- U
48. Acrolein
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

RMOnNEW % hmpumbd
Drinking Water ID: 37715
wastewater ID: 10
114 OAKMONT DRIVE
PHONE [phone]
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: C &
D DISPOSAL, INC.
CLIENT ID:
6003 C
MR.
JUDSON WHITEHURST
802
NE
RECYCLING LANE
ANALYST:
JAP
GREENVILLE,
NC
DATE COLLECTED:
12/19/22 Page: 2
DATE ANALYZED:
12/29/22
DATE REPORTED:
03/17/23
REVIEWED BY:
LANDFILL APPENDIX II
�nr wRcmvnn A7s;nn R4 (1 R)
PARAMETERS, ug/l
MDL
MRL
SW-3
SW-4
��"
Trip
Blank
49.
Allyl Chloride
0.20
10.000
---
U
---
U
---
U
20.000
---
U
---
U
50.
Chloroprene0.21
---
U
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
---
U
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
U
---
U
53.
1,3-Dichloropropane
0.28
1.000
---
U
---
U
---
---
U
U
---
---
U
---
U
54.
2,2-Dichloropropane
0.17
15.000
---
U
---
U
U
---
U
---
U
55.
1,1-Dichloropropene
0.22
5.000
---
U
---
U
___
__ -
U
56,
Ethyl Methacrylate
0.16
10.000
---
U
-"-
U
U
---
U
---
U
57.
Hexachlorobutadiene
0.10
0.200
---
U
---
U
---
__
U
U
58.
Zsobutyl Alcohol
12.80
100.000
---
U
-"-
U
__ _
U
1.93
100.000
---
U
--"
U
__ -
U
59.
60.
Methacrylonitrile
Methyl Methacrylate
0.25
30.000
---
U
---
U
---
U
---
U
---
U
0.47
6.000
---
U
---
U
---
U
61.
Naphthalene
U
---
U
---
U
---
U
62.
Propionitrile
3.26
150.000
---
U
---
U
---
U
---
U
63.
1,2,4-Trichlorobenzene
0.50
10.000
---
U
---
U
---
U
---
U
64.
Acetonitrile
36.29
55.000
---
U
---
U
---
U
U
---
U
---
U
65.
Tetrahydrofuran
0.39
1.000
2.98
---
U
U
D
_"
U
2.71
3.000
5.61
---
U
---
66.
1,4-Dioxane
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits.

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�nviroclae 1
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 910,392.0223 Lab @ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info(i ienvironmentalchemists.com
Environment -1 Date of Report: Dec 21, 2022
Post Office Box 7085 Customer PO M HJ0600312162022
Greenville NC 27858 Customer ID: 08100051
Attention: Report #: 2022-25092
Project ID: C&D Disposal, Inc
Lab ID Sample ID: E-1 Collect DaterTime Matrix Sampled by
22-61696 Site: MW-6 12/14/2022 2:34 PM Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DatelTime
Matrix Sampled by
22-61701
Site: MW-4
12/12/2022 11:00 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DaterTime
Matrix Sampled by
22-61702
Site: MW-5
12/12/2022 1:14 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.07 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61703
Site: MW-7
12/12/2022 11:38 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.06 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61704
Site: MW-2S
12/12/2022 12:16 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg1L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61705
Site: MWAS
12/14/2022 9:16 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Report #:: 2022-25092 Pagel of 4

Environment -1
Date of Report: Dec 21, 2022
Post Office Box 7085
Customer PO #: HJ0600312162022
Greenville
NC 27858
Customer ID: 08100051
Attention:
Report #: 2022-25092
Project ID: C&D Disposal, Inc
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61706
Site: MWAD
12/14/2022 10:08 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.11 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61707
Site: MW-2D
12/14/2022 1:30 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DatelTime
Matrix Sampled by
22-61708
Site: MW-3D
12/14/2022 12:28 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DatelTime
Matrix Sampled by
22-61709
Site: MW-3A
12/14/2022 11:24 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.08 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61710
Site: MW-13
12/12/2022 1:53 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 s D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DatelTime
Matrix Sampled by
22-61711
Site: MW-15
12/12/2022 3:06 PM
Water Client
Test Method Results Date Analyzed
Sulfide SM 4500 S D-2011 0.05 mg/L 12/19/2022
Report #:: 2022-25092 Page 2 of 4

Environment -1 Date of Report: Dec 21, 2022
Post Office Box 7085 Customer PO #: HJ0600312162022
Greenville NC 27858 Customer ID: 08100051
Attention: Report #: 2022-25092
Project ID: C&D Disposal, Inc
Lab ID Sample ID: E-1 Collect DatelTime Matrix Sampled by
22-61712 Site: MW-17 12/12/2022 3:38 PM Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.49 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61713
Site: MW-14S
12/12/2022 2:33 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
5.10 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61714
Site: MW-8
12/15/2022 1:46 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
0.11 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect DatefTime
Matrix Sampled by
22-61715
Site: MW-14D
12/15/2022 1:15 PM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61716
Site: MW-9A
12/15/2022 9:46 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
<0.05 mg/L 12/19/2022
Lab ID
Sample ID: E-1
Collect Date/Time
Matrix Sampled by
22-61717
Site: MW-10
12/15/2022 10:40 AM
Water Client
Test
Method
Results Date Analyzed
Sulfide
SM 4500 S D-2011
3.12 mg/L 12/1912022
Report #.: 2022-25092 Page 3 of 4

Environment - I Date of Report: Dec 21, 2022
Post Office Box 7085 Customer PO #: HJ0600312162022
Greenville NC 27858 Customer ID: 08100051
Attention: Report #: 2022-25092
Project ID: C&D Disposal, Inc
Lab ID Sample ID: E-1 Collect DatelTime Matrix Sampled by
22-61718 Site: MW-11
12/15/2022 11:31 AM Water Client
Test Method Results Date Analyzed
Sulfide
Lab ID Sample ID: E-1
22-61728 Site: MW-12S
Test
Sulfide
Comment:
Reviewed by: f
SM 4500 S D-2011
Collect Date/Time Matrix
12/15/2022 12:20 PM Water
Method
SM 4500 S D-2011
0.10 mg/L 12/19/2022
Sampled by
Client
Results Date Analyzed
0.90 mg/L 12/19/2022
Report #:: 2022-25092 Page 4 of 4

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:rz \i. 1 — Date: 2.Z Report Number: _ 2022- nC
Receipt of sample: ,ECHEM Pickup ❑ Client Deliveryfpq JUPS ❑ FeclEx ❑ Other ❑
❑ YES
❑ NO
N/A
11. Were custody seals present on the cooler?
❑ YES
10 NO
NjA
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank X9 Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
A. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
1�( YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
YES
❑ NO
12, Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15, Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18, Were orthophosphate samples filtered in the field within 15 minutes?
'1OC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H,SOa HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and time: _
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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aceAna lytical
Deliver To
Mark Oliveira
LELAP Certificate Number: 01955
A2LA Accredited (DoD ELAP-QSM 5.4) Certificate Number: 6429.01
ANALYTICAL RESULTS
•:I
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 02/01/2023
Report Y 222121722
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project C&D Disposal 7407
Samples Collected 12/14/22 - 12/15/22
Environment 1, Inc
114 Oakmont Drive
Greenville, NC 27835
[phone]
Additional Recipients
NONE
CCCR
CERT # 6429.01
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 1 of 23

Report#: 222121722
aceAnarytical
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
" Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
CA P__L
dle_l
Authorized Signature
Pace Gulf Coast Report 222121722
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Report#: 222121722
Project ID: C&D Disposal 7407
Certifications
Report Date: 02/01/2023
Certification
Certification Number
A2LA Accredited DoD ELAP-QSM 5.4
6429.01
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
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Report#: 222121722
aceAnarytical
Project ID: C&D Disposal 7407 Report Date: 02/01/2023
Case Narrative
Client: Environment 1, Inc. Report: 222121722
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
GENERAL CHEMISTRY
In method AM23G, sample was run outside of recognized holding time.
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 4 of 23

aceAnarytical
Report#: 222121722
Project ID: C&D Disposal 7407
Report Date:
02/01/2023
Sample Summary
Lab ID
Client ID
Matrix
Collect Date
Receive Date
22212172201
MW-1S
Water
12/14/22 09:16
12/16/22 12:30
22212172202
MW-1 D
Water
12/14/22 10:08
12/16/22 12:30
22212172203
MW-2D
Water
12/14/2213:30
12/16/22 12:30
22212172204
MW-3A
Water
12/14/2211:24
12/16/22 12:30
22212172205
MW-3D
Water
12/14/2212:28
12/16/22 12:30
22212172206
MW-6
Water
12/14/2214:34
12/16/22 12:30
22212172207
MW-8
Water
12/15/2213:46
12/16/22 12:30
22212172208
MW-9A
Water
12/15/22 09:46
12/16/22 12:30
22212172209
MW-10
Water
12/15/2210:40
12/16/22 12:30
22212172210
MW-11
Water
12/15/2211:31
12/16/22 12:30
22212172211
MW-12S
Water
12/15/22 12:20
12/16/22 12:30
22212172212
MW-14D
Water
12/15/2213:15
12/16/22 12:30
22212172213
MW-1 S
Bubble Strip
12/14/22 09:16
12/16/22 12:30
22212172214
MW-1 D
Bubble Strip
12/14/22 10:08
12/16/22 12:30
22212172215
MW-2D
Bubble Strip
12/14/22 13:30
12/16/22 12:30
22212172216
MW-3D
Bubble Strip
12/14/22 12:28
12/16/22 12:30
22212172217
MW-6
Bubble Strip
12/14/22 14:34
12/16/22 12:30
22212172218
MW-8
Bubble Strip
12/15/22 13:46
12/16/22 12:30
22212172219
MW-9A
Bubble Strip
12/15/22 09:46
12/16/22 12:30
22212172220
MW-10
Bubble Strip
12/15/22 10:40
12/16/22 12:30
22212172221
MW-11
Bubble Strip
12/15/22 11:31
12/16/22 12:30
22212172222
MW-12S
Bubble Strip
12/15/22 12:20
12/16/22 12:30
22212172223
MW-14D
Bubble Strip
12/15/22 13:15
12/16/22 12:30
22212172224
MW-3A
Bubble Strip
12/14/22 11:24
12/16/22 12:30
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 5 of 23

Report#: 222121722
aceAnarytical
Project ID: C&D Disposal 7407
Report Date:
02/01/2023
Detect Summary
Results and Detection Limits
are adjusted for dilution and moisture when applicable
AM23G
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22212172201
MW-1 S
Acetic Acid
mg/L
4.5J
10
NA
22212172201
MW-1S
Hexanoic Acid
mg/L
0.911
10
NA
22212172201
MW-1 S
Lactic Acid
mg/L
1.3J
10
NA
22212172202
MW-1 D
Acetic Acid
mg/L
0.70J
2
NA
22212172202
MW-1 D
Lactic Acid
mg/L
18
2
NA
22212172203
MW-2D
Acetic Acid
mg/L
0.58J
2
NA
22212172203
MW-2D
Lactic Acid
mg/L
11
2
NA
22212172204
MW-3A
Acetic Acid
mg/L
4.8J
10
NA
22212172204
MW-3A
Butyric Acid
mg/L
1.3J
10
NA
22212172204
MW-3A
Hexanoic Acid
mg/L
0.96J
10
NA
22212172204
MW-3A
Lactic Acid
mg/L
3.4J
10
NA
22212172204
MW-3A
Propionic Acid
mg/L
0.66J
10
NA
22212172205
MW-3D
Acetic Acid
mg/L
0.65J
2
NA
22212172205
MW-3D
Lactic Acid
mg/L
15
2
NA
22212172206
MW-6
Acetic Acid
mg/L
4.7J
10
NA
22212172206
MW-6
Butyric Acid
mg/L
1.4J
10
NA
22212172206
MW-6
Hexanoic Acid
mg/L
0.85J
10
NA
22212172206
MW-6
Lactic Acid
mg/L
3.3J
10
NA
22212172207
MW-8
Acetic Acid
mg/L
6.5
10
NA
22212172207
MW-8
Hexanoic Acid
mg/L
0.72J
10
NA
22212172207
MW-8
Lactic Acid
mg/L
2.2J
10
NA
22212172207
MW-8
Propionic Acid
mg/L
0.62J
10
NA
22212172208
MW-9A
Acetic Acid
mg/L
0.62
1
NA
22212172208
MW-9A
Hexanoic Acid
mg/L
0.0991
1
NA
22212172208
MW-9A
Lactic Acid
mg/L
1.0
1
NA
22212172208
MW-9A
Propionic Acid
mg/L
0.070J
1
NA
22212172209
MW-10
Acetic Acid
mg/L
6.5
10
NA
22212172209
MW-10
Butyric Acid
mg/L
0.96J
10
NA
22212172209
MW-10
Hexanoic Acid
mg/L
0.86J
10
NA
22212172209
MW-10
Propionic Acid
mg/L
0.75J
10
NA
22212172210
MW-11
Acetic Acid
mg/L
0.67
1
NA
22212172210
MW-11
Butyric Acid
mg/L
0.063J
1
NA
22212172210
MW-11
Hexanoic Acid
mg/L
0.12J
1
NA
22212172210
MW-11
Lactic Acid
mg/L
1.4
1
NA
22212172211
MW-12S
Acetic Acid
mg/L
6.8
10
NA
22212172211
MW-12S
Butyric Acid
mg/L
0.75J
10
NA
22212172211
MW-12S
Hexanoic Acid
mg/L
1.01
10
NA
22212172211
MW-12S
Lactic Acid
mg/L
1.51
10
NA
22212172211
MW-12S
Propionic Acid
mg/L
0.71J
10
NA
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 6 of 23

Report#: 222121722
aceAnarytical
Project ID: C&D Disposal 7407
Report Date:
02/01/2023
Detect Summary (Continued)
Results and Detection Limits are adjusted for
dilution and moisture when applicable
AM23G
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22212172212
MW-14D
Acetic Acid
mg/L
0.62
1
NA
22212172212
MW-14D
Lactic Acid
mg/L
9.4
1
NA
AM20GAX
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22212172213
MW-is
Hydrogen
nM
1.7J
1
NA
22212172214
MW-1 D
Hydrogen
nM
2.0
1
NA
22212172215
MW-21D
Hydrogen
nM
0.63J
1
NA
22212172217
MW-6
Hydrogen
nM
0.88J
1
NA
22212172218
MW-8
Hydrogen
nM
1.11
1
NA
22212172219
MW-9A
Hydrogen
nM
0.69J
1
NA
22212172221
MW-11
Hydrogen
nM
0.78J
1
NA
22212172222
MW-12S
Hydrogen
nM
0.71J
1
NA
22212172223
MW-14D
Hydrogen
nM
0.96J
1
NA
22212172224
MW-3A
Hydrogen
nM
1.11
1
NA
EPA RSK175
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22212172201
MW-is
Methane
ug/L
13.8
1
NA
22212172202
MW-1 D
Ethane
ug/L
1.49
1
NA
22212172202
MW-1 D
Methane
ug/L
2200
1
NA
22212172203
MW-21D
Ethene
ug/L
0.861J
1
NA
22212172203
MW-21D
Methane
ug/L
80.7
1
NA
22212172204
MW-3A
Methane
ug/L
2390
1
NA
22212172205
MW-31D
Methane
ug/L
8.74
1
NA
22212172206
MW-6
Methane
ug/L
915
1
NA
22212172207
MW-8
Methane
ug/L
1320
1
NA
22212172208
MW-9A
Ethane
ug/L
0.449J
1
NA
22212172208
MW-9A
Methane
ug/L
101
1
NA
22212172209
MW-10
Methane
ug/L
2940
1
NA
22212172210
MW-11
Methane
ug/L
151
1
NA
22212172211
MW-12S
Methane
ug/L
1960
1
NA
22212172212
MW-14D
Methane
ug/L
39.2
1
NA
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 7 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-1 c Collect Date 12/14/2022 09:16 Lab ID 22212172201
•7 Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/27/2310:16 758357 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.5J
1.2
5.0
mg/L
107-92-6 Butyric Acid
0.58U
0.58
5.0
mg/L
142-62-1 Hexanoic Acid
0.911
0.58
5.0
mg/L
646-07-1 i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2 i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5 Lactic Acid
1.3J
0.53
5.0
mg/L
109-52-4 Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4 Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3 Pyruvic Acid
0.60U
0.60
5.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2211:44 756714 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
13.8
1.98
5.00
ug/L
MW-1 D Collect Date 12/14/2022 10:08 Lab ID 22212172202
Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 2 01/27/2310:48 758357 LHM NA
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
0.70J
0.25
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
18
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 8 of 23

aceAnalytica! Report#: 222121722
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-1 D Collect Date 12/14/2022 10:08 Lab ID 22212172202
Receive Date 12/16/2022 12:30 Matrix Water
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2211:59 756714 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
1.49
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
2200
1.98
5.00
ug/L
Collect Date 12/14/2022 13:30 Lab ID 22212172203
MW�ZD Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 2 01/27/2311:20 758357 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
0.58J
0.25
1.0
mg/L
107-92-6 Butyric Acid
0.12U
0.12
1.0
mg/L
142-62-1 Hexanoic Acid
0.12U
0.12
1.0
mg/L
646-07-1 i-Hexanoic Acid
0.11 U
0.11
1.0
mg/L
503-74-2 i-Pentanoic Acid
0.12U
0.12
1.0
mg/L
50-21-5 Lactic Acid
11
0.11
1.0
mg/L
109-52-4 Pentanoic Acid
0.11 U
0.11
1.0
mg/L
79-09-4 Propionic Acid
0.11 U
0.11
1.0
mg/L
127-17-3 Pyruvic Acid
0.12U
0.12
1.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2212:15 756714 LMB NA
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
0.172U
0.172
1.00
0.861 J
0.241
1.00
80.7
1.98
5.00
Units
ug/L
ug/L
ug/L
Pace Gulf Coast Report#: 222121722 02/01/2023 10:27 Page 9 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-3A Collect Date 12/14/2022 11:24 Lab ID 22212172204
Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/27/2311:51 758357 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.8J
1.2
5.0
mg/L
107-92-6 Butyric Acid
1.3J
0.58
5.0
mg/L
142-62-1 Hexanoic Acid
0.96J
0.58
5.0
mg/L
646-07-1 i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2 i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5 Lactic Acid
3.4J
0.53
5.0
mg/L
109-52-4 Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4 Propionic Acid
0.66J
0.53
5.0
mg/L
127-17-3 Pyruvic Acid
0.60U
0.60
5.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2212:31 756714 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
2390
1.98
5.00
ug/L
MW-3D Collect Date 12/14/2022 12:28 Lab ID 22212172205
Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 2 01/27/2312:23 758357 LHM NA
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
0.65J
0.25
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.12U
0.12
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
15
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.11 U
0.11
1.0
mg/L
0.12U
0.12
1.0
mg/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 10 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-3D Collect Date 12/14/2022 12:28 Lab ID 22212172205
Receive Date 12/16/2022 12:30 Matrix Water
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2212:47 756714 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
8.74
1.98
5.00
ug/L
c Collect Date 12/14/2022 14:34 Lab ID 22212172206
MW-V Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/27/2312:54 758357 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
4.7J
1.2
5.0
mg/L
107-92-6 Butyric Acid
1.4J
0.58
5.0
mg/L
142-62-1 Hexanoic Acid
0.85J
0.58
5.0
mg/L
646-07-1 i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2 i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5 Lactic Acid
3.3J
0.53
5.0
mg/L
109-52-4 Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4 Propionic Acid
0.53U
0.53
5.0
mg/L
127-17-3 Pyruvic Acid
0.60U
0.60
5.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2213:03 756714 LMB NA
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
0.172U
0.172
1.00
0.241 U
0.241
1.00
915
1.98
5.00
Units
ug/L
ug/L
ug/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 11 of 23

aceAnalytica! Report#: 222121722
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-8 Collect Date 12/15/2022 13:46 Lab ID 22212172207
Receive Date 12/16/2022 12:30 Matrix Water
AM23G "Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/11/23 06:28 757731 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
6.5
1.2
5.0
mg/L
107-92-6 Butyric Acid
0.58U
0.58
5.0
mg/L
142-62-1 Hexanoic Acid
0.72J
0.58
5.0
mg/L
646-07-1 i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2 i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5 Lactic Acid
2.2J
0.53
5.0
mg/L
109-52-4 Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4 Propionic Acid
0.62J
0.53
5.0
mg/L
127-17-3 Pyruvic Acid
0.60U
0.60
5.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/22/2213:18 756714 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
1320
1.98
5.00
ug/L
MW-9A Collect Date 12/15/2022 09:46 Lab ID 22212172208
Receive Date 12/16/2022 12:30 Matrix Water
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 01/11/23 07:00 757731 LHM NA
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.62
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
142-62-1
Hexanoic Acid
0.0991
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
1.0
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.070J
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 12 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-9A Collect Date 12/15/2022 09:46 Lab ID 22212172208
Receive Date 12/16/2022 12:30 Matrix Water
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/29/2211:27 757043 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.449J
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
101
1.98
5.00
ug/L
Collect Date 12/15/2022 10:40 Lab ID 22212172209
MW-1 0 Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/11/23 07:31 757731 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
6.5
1.2
5.0
mg/L
107-92-6 Butyric Acid
0.96J
0.58
5.0
mg/L
142-62-1 Hexanoic Acid
0.86J
0.58
5.0
mg/L
646-07-1 i-Hexanoic Acid
0.56U
0.56
5.0
mg/L
503-74-2 i-Pentanoic Acid
0.61 U
0.61
5.0
mg/L
50-21-5 Lactic Acid
0.53U
0.53
5.0
mg/L
109-52-4 Pentanoic Acid
0.56U
0.56
5.0
mg/L
79-09-4 Propionic Acid
0.75J
0.53
5.0
mg/L
127-17-3 Pyruvic Acid
0.60U
0.60
5.0
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/29/2211:43 757043 LMB NA
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
0.172U
0.172
1.00
0.241 U
0.241
1.00
2940
1.98
5.00
Units
ug/L
ug/L
ug/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 13 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-1 1 Collect Date 12/15/2022 11:31 Lab ID 22212172210
Receive Date 12/16/2022 12:30 Matrix Water
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 01/11/23 08:03 757731 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
0.67
0.12
0.50
mg/L
107-92-6 Butyric Acid
0.063J
0.058
0.50
mg/L
142-62-1 Hexanoic Acid
0.12J
0.058
0.50
mg/L
646-07-1 i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2 i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5 Lactic Acid
1.4
0.053
0.50
mg/L
109-52-4 Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4 Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3 Pyruvic Acid
0.060U
0.060
0.50
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/29/2211:59 757043 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
151
1.98
5.00
ug/L
MW-12S Collect Date 12/15/2022 12:20 Lab ID 22212172211
Receive Date 12/16/2022 12:30 Matrix Water
AM23G *Results and limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 01/11/23 08:34 757731 LHM NA
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
6.8
1.2
5.0
mg/L
0.75J
0.58
5.0
mg/L
1.01
0.58
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.61 U
0.61
5.0
mg/L
1.5J
0.53
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.71J
0.53
5.0
mg/L
0.60U
0.60
5.0
mg/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 14 of 23

aceAnalytica! Report#: 222121722
Project ID: C&D Disposal 7407 Report Date: 02/O1/2023
Sample Results
MW-12S Collect Date 12/15/2022 12:20 Lab ID 22212172211
Receive Date 12/16/2022 12:30 Matrix Water
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/29/2212:15 757043 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.172U
0.172
1.00
ug/L
74-85-1
Ethene
0.241 U
0.241
1.00
ug/L
74-82-8
Methane
1960
1.98
5.00
ug/L
Collect Date 12/15/2022 13:15 Lab ID 22212172212
MW-14D Receive Date 12/16/2022 12:30 Matrix Water
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 01/11/23 09:06 757731 LHM NA
CAS# Parameter
Result
DL
LOQ
Units
64-19-7 Acetic Acid
0.62
0.12
0.50
mg/L
107-92-6 Butyric Acid
0.058U
0.058
0.50
mg/L
142-62-1 Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1 i-Hexanoic Acid
0.0561J
0.056
0.50
mg/L
503-74-2 i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5 Lactic Acid
9.4
0.053
0.50
mg/L
109-52-4 Pentanoic Acid
0.0561J
0.056
0.50
mg/L
79-09-4 Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3 Pyruvic Acid
0.060U
0.060
0.50
mg/L
EPA RSK175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/29/2212:30 757043 LMB NA
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
0.172U
0.172
1.00
0.241 U
0.241
1.00
39.2
1.98
5.00
Units
ug/L
ug/L
ug/L
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 15 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/01/2023
Sample Results
MW-1 c Collect Date 12/14/2022 09:16 Lab ID 22212172213
•7 Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2210:04 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.7J
0.49
1.9
nM
MW-1 D Collect Date 12/14/2022 10:08 Lab ID 22212172214
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2210:17 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
2.0
0.49
1.9
nM
Collect Date 12/14/2022 13:30 Lab ID 22212172215
MW�ZD Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2210:29 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.63J
0.49
1.9
nM
Collect Date 12/14/2022 12:28 Lab ID 22212172216
MW�3D Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2210:42 756435 LMB NA
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
0.49U
0.49
1.9
nM
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 16 of 23

aceAnalytica! Report#: 222121722
Project ID: C&D Disposal 7407 Report Date: 02/01/2023
Sample Results
MW-6 Collect Date 12/14/2022 14:34 Lab ID 22212172217
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2210:54 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.881
0.49
1.9
nM
MW-8 Collect Date 12/15/2022 13:46 Lab ID 22212172218
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2211:08 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.11
0.49
1.9
nM
Collect Date 12/15/2022 09:46 Lab ID 22212172219
MW�9A Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2211:24 756435 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.69J
0.49
1.9
nM
MW-1 O Collect Date 12/15/2022 10:40 Lab ID 22212172220
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/19/2211:37 756435 LMB NA
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
0.49U
0.49
1.9
nM
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 17 of 23

Report#: 222121722
aceAr�alytrca!
Project ID: C&D Disposal 7407 Report Date: 02/01/2023
Sample Results
MW-1 1 Collect Date 12/15/2022 11:31 Lab ID 22212172221
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/20/22 06:58 756483 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.78J
0.49
1.9
nM
MW-12S Collect Date 12/15/2022 12:20 Lab ID 22212172222
Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/20/22 07:10 756483 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.71J
0.49
1.9
nM
Collect Date 12/15/2022 13:15 Lab ID 22212172223
MW-14D Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/20/22 07:22 756483 LMB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.96J
0.49
1.9
nM
Collect Date 12/14/2022 11:24 Lab ID 22212172224
MW-3A Receive Date 12/16/2022 12:30 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/20/22 07:35 756483 LMB NA
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
1.11
0.49
1.9
nM
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 18 of 23

1 21'Analytical
Report#: 222121722
Project ID: C&D Disposal 7407
General Chemistry QC Summary
Report Date: 02/01/2023
Analytical Batch Client ID
MB757731
LCS757731
LCSD757731
757731 Lab ID
2440077
2440078
2440079
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
01/11/23 03:50
01/11/23 03:19
01/11/23 19:32
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
2.3
116
70 - 130
2.0
2.2
109
6
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.7
86
70 - 130
2.0
1.4
72
18
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.9
95
70 - 130
2.0
2.2
108
13
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
1.9
96
70 - 130
2.0
2.1
106
10
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
1.7
87
70 - 130
2.0
1.9
97
11
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.0
102
70 - 130
2.0
1.8
90
12
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
1.8
91
70 - 130
2.0
2.2
108
18
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
1.9
96
70 - 130
2.0
1.7
83
14
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.7
83
70 - 130
2.0
2.0
100
19
20
Analytical Batch Client ID
MB758357
LCS758357
LCSD758357
758357 Lab ID
2444004
2444005
2444006
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
01/27/23 02:23
01/27/23 01:20
01/27/23 15:32
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
2.5
125
70 - 130
2.0
2.4
118
6
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
2.2
110
70 - 130
2.0
2.0
102
8
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
2.3
113
70 - 130
2.0
2.2
108
4
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.0
99
70 - 130
2.0
2.3
113
13
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
2.0
102
70 - 130
2.0
2.0
99
3
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.4
118
70 - 130
2.0
2.2
111
6
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
2.3
114
70 - 130
2.0
2.2
110
3
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
2.4
119
70 - 130
2.0
2.3
113
5
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
2.1
107
70 - 130
2.0
1.9
97
9
20
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 19 of 23

1 21'Analytical
Report#: 222121722
Project ID: C&D Disposal 7407
General Chromatography QC Summary
Report Date: 02/01/2023
Analytical Batch Client ID
MB756435
LCS756435
LCSD756435
756435 Lab ID
2434354
2434355
2434356
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
12/19/22 06:38
12/19/22 06:13
12/19/22 06:25
Matrix
Bubble Strip
Bubble Strip
Bubble Strip
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Hydrogen 1333-74-0
0.49U
0.49
12
13
107
70 - 130
12
12
105
1
20
Analytical Batch Client ID
MB756483
LCS756483
LCSD756483
756483 Lab ID
2434601
2434602
2434603
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
12/20/22 06:45
12/20/22 06:20
12/20/22 06:32
Matrix
Bubble Strip
Bubble Strip
Bubble Strip
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DLI
Added
Limits%R
1 Added
Limit
Hydrogen 1333-74-0
0.49U
1 0.491
121
12
11051
70 - 130
1 121
1211051
0
1 20
Analytical Batch
Client ID
MB756714
LCS756714
LCSD756714
756714
Lab ID
2435562
2435563
2435564
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
12/22/22 07:51
12/22/22 06:20
12/22/22 06:36
Matrix
Water
Water
Water
EPA RSK175
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPDT30
Result
DL
Added
Limits%R
Added
Ethane
74-84-0
0.172U
0.172
97.1
90.7
93
70-1 30
97.1
85.2
88
6
Ethene
74-85 1
0.241U
0.241
119
109
92
70 130
119
104
88
5
Methane
74-82-8
1.98U
1.98
378
380
101
70-130
378
358
95
6
Analytical Batch
Client ID
MB757043
LCS757043
LCSD757043
757043
Lab ID
2437088
2437089
2437090
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
12/29/22 08:34
12/29/22 06:34
12/29/22 06:50
Matrix
Water
Water
Water
EPA RSK175
Units
ug/L
Spike
I Result
%R
Control
Spike
Result
%R
RPDT30
Result
DL
Added
Limits%R
Added
Ethane
74-84-0
0.172U
0.172
97.1
92.9
96
70-1 30
97.1
94.5
97
2
Ethene
74-85-1
0.241U
0.241
119
112
94
70-130
119
115
97
3
Methane
74-82-8
1.98U
1.98
378
392
104
70-130
378
394
104
1
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 20 of 23

CHAIN -OF -CUSTODY Analytical Request Document
LAB USE ONLY -Affix Wor'
-/IePaceAnalyfical'
C!'ent!D: F1 - Environment 1 Inc.
Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields
'
ALL SHAC SDG: 222121722
iveT ContainerPreservatPM: RWe
•• Preservative Types: (1) nitric acid, (2) suit......._..., ,_, ...... __......._ ...,.., , ., ........................... .... ....,..,.."..,.,
Company:
nwronm - � �n�,
Billing Information: f- /enMt�� SnL,
(ttt Aw-^o\' ,wt,
&Ceen�ille,� WC, 2RSSg
Address: IN ooktoon+ prl-a-
_l IS
Report To:
(�'
Email To: AA
/� of I JG t rv�® eAVi fonMZ(� �Tr�
�/ n,,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (8) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Copy To:
Site Collection Info/Address:
Lab Profile/Line:
CustomerAnalyses
Project Name/Number:
O D 1spoSo�` ', �(
State: County/City: Time Zone Collected:
Lab sample Receipt checklist:
L D 07
Ob / I ] PT [ ] MT [ ] CT Pq ET
Custody Seals Present/Intact Y N NA
custody Signatures Present Y N NA
Phone:7,52- 756 tog
Site/Facility ID #:
Compliance Monitoring?
Email:
O�
[ ] Yes [ ] No
Collector Signature Present Y N NA
Bottles Intact Y N NA
correct Bottles Y N NA
Collected By (print):
Purchase Order #:
DW PWS ID #:
RkkTh,4[ J, Nelo
Quote If:
DW Location Code:
Sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA - Headspace Acceptable Y N NA
Collect})ed/I- By (signature):
Turnaround Date Required:
Immediately Packed on Ice:
Yes [ ] No
S
USDA Regulated Soils Y N NA
Samples in Holding Time Y N NA
Residual chlorine Present Y N NA
Sample Disposal:
Rush:
Field Filtered (if applicable):
[ ] Dispose as appropriate [ I Return
[ ] Same Day [ ] Next Day
( ] Yes [ ] No
Cl Strips:
[ ] Archive:
[ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day
Sample pH Acceptable Y N NA
[ IHold:
(Expedite Charges Apply)
Analysis:
01
C
Q
pH Strips:
Sulfide Present Y N NA
Lead Acetate strips:
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), Vapor (V), Other (OT)
o
L-
17)
LAB USE ONLY:
*
Comp /
Collected (or
Composite End
Res
# of
Lab Sample # / Comments:
Customer Sample ID
Matrix
Grab
Composite Start)
CI
Ctns
L
Date
Time
Date
Time
6,-ab
*W u
1.16A
13
M W- 1 D
I
I
WOW
4 a
AW-2P
1
i 30
5
vf- 3A
:z4A
ew- 3dT
2:zg
I(v 5
hl-
:3N
Mu- C&
I' 6
$ -7
w - I A
q: Y6A
Mw- 10
to:gOA
6
MW- l
t(:_1A
ID
Customer Remarks/ Special Conditions/ Possible Hazards:
Type of Ice Used: Wet Blue Dry None
SHORT HOLDS PRESENT (<72 hours):
Y N N/A
Lab Sample Temperature Info:
�AGIa f r -TP- I `0
Temp Blank Received: Y N NA
Therm ID#:
Packing Material Used:
Lab Tracking #: 2 O 3 3 n 5 1
Q c
Cooler 1 Temp Upon Receipt: oC
Radchem sample(s) screened (<500 cpm): Y N NA
Samples received via:
Cooler 1 Therm Corr. Factor: oC
FEDEX UPS Client Courier Pace Courier
Cooler 1 Corrected Temp: oC
Comments:
1.43t
Reli uished by/Company: (Signature)
/
Date/Time:
Received by/Company: (Signature)
Date/Time:
MT1L LAB USE ONLY
Table #:
n✓i(Jn(nILJ Tit,
,Z1�, 7-/L(x)0]r(1
Acctnum:
Relinquished by/Company: Si nature
q (Signature) )
Date
Date/Time:
Received by mpany: nature)
Date/Time: 2 30
p
Up �
�a� ,���
Template:
P
Trip Blank Received: Y N NA
HCL McOH TSP Other
` -1
d
Prelogin:
PM:
Relinquished by/Company: (Signature)
Date/Time:
Recei by/Compan : ignature)
Date/Time:
Non Conformance(s):
Page:
PB:
YES / NO
of:
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 21 of 23

CHAIN -OF -CUSTODY Analytical Request Document
- aceAnalyl'ical'
Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields
LAB USE ONLY -Affix Wei
v!g;;;m; F1 _ Fnyirnnmon4 1 Ind
ALL SHA[ SDG: 222121722
Container Preservative PM: RWe
** Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Company:
Billing Information: �nV)r
Address:
1I4 ouJcr✓lon� D(;��
Report To:
k I U o.
Email To: t ,
M DI tJ�i rqQ Cnv:ronMe nt tA, C&^A
Copy To:
Site Collection Info/Address:
Analyses
Lab Profile/Line:
Gusto e�r)Project Name/Numb : 1 7
6ST) PiS .-I"It 7`4 (
State: Count /City: Time Zone Collected:
I��i / Fip ( ]PT[ ]MT[ ]CT [>dET
`
^'
S
t
S
Q
Lab sample Receipt Checklist:
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
Correct Bottles Y N NA
Sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA - Headspace Acceptable Y N NA
USDA Regulated Soils Y N NA
Samples in Holding Time Y N NA
Residual chlorine Present Y N NA
Cl Strip :
s
Sle H Acceptable Y N NA
am P P P
pH Strips:
Sulfide Present Y N NA
Lead Acetate Strips:
LAB USE ONLY:
Lab Sample # / Comments:
Phone: L5Z,- 7J56 -i ZOE
Email:
Site/Facility ID #:
7 lu Q l
Compliance Monitoring?
[ ] Yes ( ] No
Collected By (print):
PTf IGk J �h(it •/
Purchase Order #:
Quote #:
DW PWS ID #:
DW Location Code:
Collected By (signature):
QWha
Turnaround Date Required:
Immediately Packed on Ice:
] Yes [ ] No
ample Disposal:
[ J Dispose as appropriate [ ]Return
[ ] Archive:
[ ] Hold:
Rush:
Same Day Next Da
[ 1 y
[ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day
(Expedite Charges Apply)
Field Filtered (if applicable):
]Yes ] No
[ [
Analysis:
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
P
Matrix *
Comp /
Grab
Collected (or
Composite Start)
Composite End
Res
Cl
# of
Ctns
Date
Time
Date
Time
MW 12S
Gw
6rz In
(7,-15-t7-
is'-2op
Mw-i4D
Z
v
115
v
Customer Remarks / Special Conditions / Possible Hazards:
7L{ l7 �
Type of Ice Used: Wet Blue Dry None
SHORT HOLDS PRESENT (<72 hours): Y N N/A
Lab Sample Temperature Info:
Temp Blank Received: Y N NA
Therm ID#:
Cooler 1 Temp Upon Receipt: OC
Cooler 1 Therm Corr. Factor: oC
Cooler 1 Corrected Temp: oC
Comments:
Packing Material Used:
Lab Tracking #:
2833252
Radchem sample(s) screened (<500 cpm): Y N NA
Samples received via:
FEDEX UPS Client Courier Pace Courier
RelinnQuished by/Comps : (Si nature) _� y A
/ 01virw lfid J �'t
Date/Time: 'r
(2 )Cl'7i2 t�OD('
Received by/Company: (Signature)
Date/Time:
MTJL LAB USE ONLY
Table #:
Acctnum:
Template:
Prelogin:
PM:
pB:
Relinquished by/Company: (Signature)
V )
Date/Time: l M
I° —1 ( � " I /t�
Received / ompature)
an . ign
Date/Time: U
' 1
/ Z
Tri Blank Received: Y N NA
P
HCL McOH TSP Other
Relinquished by/Company: (Signature)
Date/Time:
Receive y Compan (Sig
Date/Time:
Non Conformance(s):
YES / NO
Page: L
of:
Pace Gulf Coast Report#: 222121722 02/01 /2023 10:27 Page 22 of 23

(��-aceAnalyfical'SAMPLE RECEIVING CHECKLIST IIIIIIIIYIII III
SAMPLE DELIVERY GROUP
222121722
CHECKLIST
YES
NO
Client PM RIUe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
E1 - Environrrent 1, Inc.
UPS
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
304439
N/bOune, DDdie K
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
*❑
0
❑
❑
Line Item(s)
Receive Date(s)
1 - IVEELLVFA
12/16/22
2- hydrogen
Preservative added to any containers?
❑
*❑
If received, was headspace for VOC water containers < 6mm?
*❑
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID: E38
Temp °C
None
None
1.2
NOTES
Revision 1.6
Page 1 of 1
Pace Gulf Coast Report#: 222121722
02/01 /2023 10:27
Page 23 of 23