Loading...
HomeMy WebLinkAbout25052_450 Polo Road_Brownfields Assessment Report_20230324 PREPARED FOR: 450 POLO, LLC 675 SEMINOLE AVENUE, NE, SUITE B1 ATLANTA, GA 29601 PREPARED BY: EAS PROFESSIONALS, INC. 9 PILGRIM ROAD GREENVILLE, SC 29607 BROWNFIELDS ASSESSMENT REPORT FOR 450 POLO ROAD PROPERTY WINSTON-SALEM, NORTH CAROLINA EAS PROJECT NO. 225234 MARCH 24, 2023 Geotechnical, Environmental, Construction Materials and Forensic Engineering Construction Materials Testing | Laboratory Testing | Land Surveying | Specialty Inspections March 24, 2023 NCDEQ – Division of Waste Management Brownfields Program 1646 Mail Service Center Raleigh, NC 27699-1646 Attention: Mr. Seth A. Titley Reference: Brownfields Assessment Report 450 Polo Road Property Winston-Salem, Forsyth County, North Carolina Brownfield Project No. 25052-21-034 EAS Project No.: 225234 Dear Mr. Titley: Engineering and Surveying Professionals Inc. (EAS) is pleased to provide this Brownfields Assessment Report (BAR) for the 450 Polo Road Property located in Winston-Salem, Forsyth County, North Carolina. This BAR has been prepared in accordance with the Assessment Work Plan (AWP) prepared by EAS and approved by you on October 19, 2022. If you have any questions regarding this report do not hesitate to contact Derek M. Ross at 828.382.8319. Respectfully Submitted, EAS PROFESSIONALS, INC. Derek M. Ross J. Ashley Brown, PE Environmental Services Manager Senior Environmental Engineer NC License Number 023160 Brownfields Assessment Report PAGE i EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 BROWNFIELDS ASSESSMENT REPORT 450 Polo Road Property Winston-Salem, Forsyth County, North Carolina Brownfield Project No. 25052-21-034 March 24, 2023 DISTRIBUTION LIST NCDEQ EAS Professionals Inc. Brownfields Program 9 Pilgrim Road 217 West Jones Street Greenville, SC 29607 Raleigh, NC 27699-1646 Phone: (919) 707-8200 Phone: (828) 676-2050 Contact: Ms. Tracy Wahl Contact: Derek M. Ross Email: tracy.wahl@ncdenr.gov Email: dross@eas-pro.com NCDEQ Brownfields Program 450 West Hanes Mill Road Suite 300 Winston Salem, NC 27105 Phone: (336)-776-9800 office Contact: Mr. Seth A. Titley Email: seth.titley@ncdenr.gov 450 Polo, LLC c/o Jeff Koon 675 Seminole Avenue NE, Suite B1 Atlanta, GA 30307 Phone: (404)-618-0726 Contact: Mr. Jeff Koon Email: jeffkoon@stratuspropertygroup.com Roberts & Stevens, P.A. City Centre Building 301 College Street, Suite 400 Asheville, NC 28801 Phone: (828) 252-6600 Contact: Mr. William Clarke Email: bclarke@roberts-stevens.com Brownfields Assessment Report PAGE ii EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 450 Polo Road Winston-Salem, Forsyth County, North Carolina Brownfield Project No. 25052-21-034 March 24, 2022 Certification: I, J. Ashley Brown, a Professional Engineer for EAS Professionals, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. EAS Professionals, Inc. is licensed to practice engineering in North Carolina. The certification number of the company is C-3066. J. Ashley Brown, P.E. Senior Environmental Engineer NC License No. 023160 3/24/23 Brownfields Assessment Report PAGE iii EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 TABLE OF CONTENTS 1.0 INTRODUCTION ............................................................................................................. 1 1.1 BACKGROUND ............................................................................................................... 1 1.2 PROPERTY AND SURROUNDING AREA DESCRIPTION ............................................. 3 1.3 REGULATORY BACKGROUND ..................................................................................... 4 2.0 SCOPE OF WORK .......................................................................................................... 5 2.1 PROJECT ORGANIZATION ............................................................................................ 5 2.2 SPECIAL TRAINING REQUIREMENTS AND CERTIFICATION ..................................... 5 2.3 SAMPLE PROCEDURES, MEDIA, LOCATIONS AND ANALYTICAL PARAMETERS .... 6 2.4 SAMPLE LOCATIONS PROCEDURES, AND ANALYTICAL PARAMETERS ............... 11 2.4.1 General Sampling Procedures ..............................................................................11 2.4.2 Soil Sampling Procedures.....................................................................................12 2.4.3 Groundwater Sampling Procedures ......................................................................13 2.4.4 Soil Gas Sampling Procedures .............................................................................15 2.4.5 Documentation .....................................................................................................17 2.5 RECEPTOR SURVEY ................................................................................................... 19 3.0 QUALITY ASSURANCE PROJECT PLAN .................................................................... 20 3.1 INTRODUCTION ........................................................................................................... 20 3.2 DATA QUALITY OBJECTIVES (DQOS) ........................................................................ 20 3.3 DATA QUALITY OBJECTIVES – SEVEN STEP PROCESS ......................................... 20 3.0 FINDINGS ..................................................................................................................... 23 3.1 SOIL SAMPLING RESULTS ......................................................................................... 23 3.2 GROUNDWATER SAMPLING RESULTS ..................................................................... 24 3.3 SOIL GAS SAMPLING RESULTS ................................................................................. 25 4.0 MANAGEMENT OF INVESTIGATION DERIVED WASTES .......................................... 25 5.0 SUMMARY AND CONCLUSIONS ................................................................................. 26 5.1 SOIL SAMPLING ........................................................................................................... 26 5.2 SOIL GAS SAMPLING .................................................................................................. 27 5.3 GROUNDWATER SAMPLING ...................................................................................... 27 Brownfields Assessment Report PAGE iv EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 ATTACHMENT A: FIGURES Figure 1: Sample Location Map Figure 2: Site Location Map Figure 3: Groundwater Potentiometric Map Figure 4: Cut Soil Sample Location Map Figure 5: Receptor Survey Site Vicinity Map Figure 6: Public Water Sources Map Attachment B: Laboratory Results Tables Attachment C: Risk Calculator Results Attachment D: Site Plat Showing Oil/Water Separator provided by Stratus Development Group Attachment E: Boring Logs Attachment F: Well Construction Records Attachment G: Receptor Survey Attachment H: Laboratory Data Sheets, Table 2 Brownfields Assessment Report EAS No. 22-5234 450 Polo road Winston Salem, NC March 24, 2023 BROWNFIELDS ASSESSMENT REPORT 450 POLO ROAD 1.0 INTRODUCTION 1.1 Background The 450 Polo Road Property is located at 450 Polo Road, Winston-Salem, Forsyth County, North Carolina (the Property). It is identified by Forsyth County as Parcel Identification Number (PIN) 6827-72-3724.000. The Property includes approximately 3.95-acres and is bounded generally to the north by Polo Road, with the NCDOT Location and Surveys Unit to the northwest, the NCDOT Roadside Environmental Unit to the north, and a commercial building occupied by La Oficina, Alexa & Jonathan Hair Designers, La Loteria (Mexican convenience store), L&C Appliances, La Victoria (Mexican grocery store), and Polo Laundry to the northeast. The property is bounded to the east by Calvary Chapel Fellowship (church), beyond which lies residential development, and to the south by McCanless Street with residential development, with additional residential development further south. Adjacent to the west is cleared land, with commercial development and wooded land further west. The subject site is in the northwestern area of the city of Winston Salem, approximately 300 feet southeast of the intersection of Polo Road and N. Cherry Street. The surrounding area is generally occupied by wooded land and commercial and residential development. Environmental Corporation of America (ECA) completed Phase I Environmental Site Assessment (ESA) of the Property dated January 8, 2021. According to the Phase I ESA, the Property was formerly cleared and/or agricultural land from at least 1940 until sometime between 1950 and 1961, when the present-day parking area on its northern end was constructed. The Property has consisted of wooded land and a parking area from at least 1961 until the present day. The Gwyn Commercial Property (Salem Uniform Service) facility addressed as 4015 North Cherry Street and adjoining the Property to the west was identified on the SHWS (EPAID NONCD0002438), LUST, INST CONTROL, VCP, BROWNFIELDS (Project ID 07011-03-34), IMD, UST, and RCRA- QG databases. This facility was formerly utilized as a drycleaner. According to EDR, an 8,000-gallon fuel oil UST on the Salem Uniform site was reported as temporarily closed. A 1,000-gallon gasoline UST and a 2,000-gallon gasoline UST were reportedly removed from the ground in 1994. A release associated with these USTs was reported in 1994 which impacted both soil and groundwater and the case is listed as closed in 2019. According to a plat provided by Mr. Jeff Koon of Stratus Development Group, LLC, the 1,000-gallon and 2,000-gallon closed USTs at the Salem Uniform Service property were formerly located approximately 90 feet from the Property. The plat also depicts a former oil-water separator on the southern portion of the Salem Uniform Service property. This plat is included as Attachment D. Brownfields Assessment Report PAGE 2 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 ECA’s review of a Limited Site Assessment Report of the Salem Uniform Service property prepared by ENSR Consulting and Engineering, Inc. (ENSR) and dated June 2003 identified tetrachloroethylene (PCE) in two of the three soil samples collected at concentrations (27.5 mg/kg and 0.903 mg/kg) exceeding the US EPA soil-to- groundwater maximum soil contaminant concentration (MSCC) of 0.0007 mg/kg. The 2003 ENSR report indicated Ethylbenzene, 1,3,5-trimethylbenzene, PCE, trichloroethene (TCE), and cis-1,2-dichloroethene were detected in a groundwater sample collected at concentrations of exceeding these compounds’ respective 15A North Carolina Administrative Code (NCAC) 2L Groundwater Quality Standards. PCE was also detected above the gross contaminant level (GCL) of 0.7 mg/L. A copy of this report will be submitted to NCDEQ, separately. ECA also reviewed a Notice of Brownfields Property for the Salem Uniform Service property dated August 11, 2006, which restricted the use of that adjoining property to warehousing, retail, office, or parking purposes. The use of surface water, groundwater, and soil, and the construction of a new structure was also prohibited without written notice to NCDENR. ECA’s review of a Groundwater and Air Monitoring Report for the April 2019 Sampling Event of the Salem Uniform Service property dated August 2019 conducted by AECOM Technical Services of North Carolina, Inc. (AECOM) identified PCE at concentrations above the 2L Standard in 22 monitoring well samples. TCE was detected at concentrations above the 2L Standard in 10 monitoring well samples. Additionally, the PCE breakdown products cis-1,2-dichloroethylene (DCE), and vinyl chloride as well as benzene and 1,2-dichloroethane (DCA, a tetrachloroethane breakdown product) were detected at concentrations above the 2L Standard in several samples. Per the 2019 AECOM report historical trends reportedly showed that PCE in most site monitoring wells had generally either decreased or remained stable since 2004 with the exception of fluctuations observed in most intermediate-depth onsite monitoring wells. ECA was also provided with groundwater isoconcentration maps that indicate that shallow groundwater beneath the western portion of the Property has been adversely impacted by the PCE contamination plume migrating from the Salem Uniform property. This report was submitted to the NCDEQ, separately. Based on the information reviewed, along with the previous Phase I and Phase II Environmental Site Assessments discussed in section 5.4.7 of this previous Phase I ESA, ECA considered the PCE groundwater contamination associated with the Salem Uniform Service property to represent a recognized environmental condition (REC) for the Property. ECA was also provided with a previous Phase I Environmental Site Assessment (ESA) report of the Property conducted by Terraquest Environmental Consultants, P.C. (Terraquest) and dated July 8, 2016. Terraquest identified the Property as undeveloped with the exception of the construction of the asphalt paved parking lot prior to 1951. Terraquest identified one historical recognized environmental condition Brownfields Assessment Report PAGE 3 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 in association with the former Pilot Freight Carriers (JSGO) facility located at 4103 Cherry Street immediately north of the Property. According to Terraquest, a release was reported during the closure of USTs, “T1” and “T2” but soils were remediated to below North Carolina Department of Environmental Quality (NCDEQ) Department of Waste Management (DWM)-UST soil and groundwater cleanup standards, so this off- site release was not considered a recognized environmental condition by Terraquest. A copy of this report will be submitted to the NCDEQ, separately. Terraquest also identified two offsite facilities that in their opinion constituted RECs during the course of their 2016 Phase I ESA of the Property, which included a chlorinated solvent release from the upgradient western adjoining property, Salem Uniform Services Facility/Gwyn Commercial Property, and a former upgradient gasoline station release at Pace Gas & Car Wash addressed as 335 Polo Road, identified to the northeast during the city directory review and site reconnaissance. Additionally, in the 2016 Phase I report Terraquest discussed a release from a 1,000- gallon and a 2,000-gallon steel gasoline USTs on the Salem Uniform Services Facility but determined this release was not a recognized environmental condition, since it was identified as low risk by the NCDEQ based on analytical results of the ongoing assessments at this facility showing no elevated petroleum-related contamination in the monitoring wells sampled. ECA was also provided with a previous Phase II ESA for the Property by Terraquest and dated January 24, 2017 that was conducted as a result of the findings in their earlier Phase I ESA. The Phase II ESA included both soil and groundwater sampling. Soil contaminants detected did not exceed the NCDWM soil to groundwater MSCCs. Groundwater analytical results of the northwestern groundwater sample (Well TQMW1) indicated the presence of benzene and PCE at levels that exceeded the 2L Standard which were likely associated with the petroleum and chlorinated solvent releases that occurred on the adjoining former Salem Uniform Services facility. Analysis of the northeastern groundwater sample (Well TQMW2) revealed numerous petroleum-based contaminant concentrations in excess of the 2L Standard along with a detection of PCE exceeding the 2L Standard. Terraquest noted that the petroleum contamination present in the sample from Well TQMW2 was likely from the Pace Gas & Car Wash facility and the PCE potentially migrated from the Polo Laundry facility located at 325 Polo Road to the northeast of the Property. Based on this information, the petroleum and solvent releases identified in the groundwater at the Property were considered a REC in the January 8, 2021, ECA Phase I ESA Report. Based on the information summarized above, this assessment is attempting to fill data gaps with respect to potential soil, groundwater and soil vapor impacts beneath areas of the Property not assessed in previous investigations. 1.2 Property and Surrounding Area Description The 450 Polo Road Property is adjoined to the north by Polo Road, with the NCDOT Brownfields Assessment Report PAGE 4 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Location and Surveys Unit to the northwest, the NCDOT Roadside Environmental Unit to the north, and a commercial building occupied by La Oficina, Alexa & Jonathan Hair Designers, La Loteria (Mexican convenience store), L&C Appliances, La Victoria (Mexican grocery store), and Polo Laundry to the northeast. The property is bounded to the east by Calvary Chapel Fellowship (church), beyond which lies residential development, and to the south by McCanless Street with residential development, with additional residential development further south. Adjacent to the west is cleared land (Former Salem Uniform Service site), with commercial development and wooded land further west. The surrounding area is generally occupied by wooded land and commercial and residential development. The Property includes approximately 3.95- acres and is bounded generally to the north by Polo Road. 1.3 Regulatory Background Based on the findings of ECA’s Phase I ESA dated January 8, 2021, the Limited Site Assessment Report conducted by ENSR dated June 2003, the Notice of Brownfields Property dated August 11, 2006, the Brownfields Site Inspection Report dated August 13, 2008, the Groundwater and Air Monitoring Report for the April 2019 Sampling Event dated August 2019 conducted by AECOM, the Phase I Environmental Site Assessment (ESA) conducted by Terraquest dated July 8, 2016, and the Phase II Environmental Site Assessment conducted by Terraquest dated January 24, 2017, it was recommended by the NCDEQ, that Stratus Development Group, LLC be entered into a Brownfields Agreement (25052-21-034) for the Property identified by Forsyth County as PIN 6827-72-3724.000, herein referred to as the Property. As a result, Stratus Development Group, LLC, on behalf of 450 Polo LLC submitted to NC DEQ Brownfields Program an application as a Prospective Developer seeking a Brownfields Agreement. Subsequently, a Letter of Eligibility (LOE) for the property was awarded on December 3, 2021. Per the language in LOE prepared by NCDEQ, “The North Carolina Department of Environmental Quality (DEQ) has received and reviewed your July 14, 2021 Brownfields Property Application (BPA) and revised application and affidavit (received November 15, 2021) submitted on behalf of 450 Polo, LLC as a Prospective Developer seeking a Brownfields Agreement regarding the Brownfields Property. Upon review of the BPA with respect to the requirements of the Brownfields Property Reuse Act of 1997, DEQ has determined that this project is eligible for entry into the North Carolina Brownfields Program (NCBP) and for continued evaluation for a Brownfields Agreement (BFA).” On October 19, 2022, EAS submitted to Mr. Seth Titley of the DEQ Brownfields Program an Assessment Work Plan (AWP) for the Property to identify and determine the source, nature and extent of contamination in specific areas of the Property that has not been previously assessed. This AWP was prepared to meet the requirements prescribed in the DEQ guidance, THE MINIMUM REQUIREMENTS CHECKLIST FOR SITE ASSESSMENT WORK PLANS AND REPORTS dated February 2022. This document was also developed to serve as the QA/QC document for all soil and Brownfields Assessment Report PAGE 5 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 groundwater assessment activities to be conducted at this specific site. the AWP was approved by Mr. Titley in an October 21, 2022 letter to Mr. Jeff Koon of 450 Polo, LLC. This BAR describes the field and laboratory methods used to collect and analyze soil, soil vapor, and groundwater samples to allow characterization of environmental impacts on the site. The approved methods and laboratory quality control procedures employed have been strictly followed to ensure that the data are reliable and defensible. This BAR describes sample locations, analytical parameters, standard procedures for sample collection, sample container and preservation requirements, equipment decontamination procedures, documentation requirements, and the number and types of field and laboratory quality control samples used. 2.0 SCOPE OF WORK 2.1 Project Organization The Project Manager (PM) for this project is Mr. Derek M. Ross. Decisions regarding project scope, sampling locations, collection equipment, or other project related issues will be made by the PM in consultation with team members and the NCDEQ Project Manager. Mr. J. Ashley Brown, P.E. has acted as the project Field Operations Manager (FOM) and Senior Reviewer for the project. Ms. Heather J. Wagner with Pace Analytical is the Subcontract Laboratory Manager for this project. The Subcontract Laboratory Manager is the point of contact for all laboratory-related issues for this project. The subcontract Laboratory Manager has conducted second-tier reviews of all analytical data prior to submission to EAS and has maintained communication with the EAS Project Manager during this review. Pace Analytical National Center for Testing & Innovation 12065 Lebanon Rd. Mt. Juliet, TN 37122 615-773-9686 2.2 Special Training Requirements and Certification All site personnel for the project had completed the Occupational Safety and Health Administration (OSHA) basic 40-hour health and safety training course, Hazardous Waste Operations and Emergency Response (HAZWOPER), including annual refreshers. All drilling was performed by a licensed North Carolina Well Drilling Contractor, who is experienced in the collection of soil and groundwater samples. Drilling activities were supervised by a North Carolina registered Professional Engineer (P.E.). All soil borings and groundwater monitoring wells were installed and will be abandoned by a North Carolina licensed well driller in accordance with 15A NCAC 2C .0108. Standards of Construction: Wells Other Than Water Supply. Brownfields Assessment Report PAGE 6 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 2.3 Sample Procedures, Media, Locations and Analytical Parameters Laboratory clean sampling containers appropriate for the analytical methods were used to collect all samples along with clean storage containers capable of holding the sample containers and ice necessary to appropriately preserve the samples collected. Those collecting the samples had training appropriate to the task, including an awareness of the need to avoid cross contamination of samples through measures such as the use of clean gloves for the collection of each sample. All sampling implements such scoops, hand augers etc. used were laboratory clean stainless steel. In addition, the following additional sampling protocols were followed: Samples were collected, properly labeled, secured, and immediately preserved by placing them on ice. Each sample container was tightly sealed and placed in a clean zip lock bag. A laboratory Chain of Custody (COC) Form was completed that included relevant information for all samples including unique identification codes for each sample, date of collection, time of collection, and a description of the container sizes and types. After the collection of all samples and the completed COC form were placed in a waterproof container (zip lock bag) with the samples and shipped overnight to the State of North Carolina-approved laboratory (Pace) for the analyses specified in Table 1. The shipping containers had signed and dated custody seals and enough ice to properly preserve the samples during transit. Soils – There are plans to construct eight (8) buildings on eight (8) building pads on the Property. Six (6) of these buildings will be constructed on or in the vicinity of the documented groundwater impacts. Consequently, EAS collected thirty-one (31) soil samples in the vicinity of the proposed eight (8) building footprints and associated improvements as shown in Figures 1 and 4. In each soil boring for the proposed structures, one “surface” sample was collected from 0-1’ below ground surface (bgs) i.e. SS-1 and one “subsurface” sample i.e. SS-1-a was collected from 4-5’ below existing grade from each of the eight (8) locations. Four (4) of these soil samples were collected in the area of two proposed building footprints in the southwestern portion of the Property (SS-1, SS-1-a, SS-2, and SS-2-a). Four (4) soil samples were collected in the vicinity of the two proposed building footprints in the northwestern portion of the Property (SS-3, SS-3-a, SS-4 and SS-4-a). Four (4) soil samples were collected in the vicinity of two proposed building footprints in the northeastern portion of the Property (SS-5, SS-5-a, SS-6 and SS-6-a) and four (4) soil samples were collected in the vicinity of the proposed two building footprints in the southeastern area of the Property (SS-7, SS-7-a, SS-8 and SS-8-a). In addition to the structure sampling, NCDEQ indicated it was necessary to sample and analyze soil samples from grading “cut” areas on site to determine if those cut soils will be suitable for use as onsite fill, or in the case of soils from proposed utility trench cuts, if soils in the areas of those cuts will need to be taken out before site grading begins. The site grading plan suggests one mass grading cut area of two (2) feet in depth in the southeastern corner of the site. Across the remainder of the site, site grading will involve fills ranging from less than one foot to nine (9) feet in depth. Brownfields Assessment Report PAGE 7 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Seven (7) utility trench cut samples (CS-1 through CS-7) were collected from the areas shown on Figure 4 from the depths indicated in Table 1 (due to proposed utility depths, samples at two (2) intervals were collected for the three (3) deeper samples). One soil sample from one (1) to two (2) feet bgs was collected in the single cut area in the southeastern corner of the site (CS-8 on Table 1 and Figure 4). The sampling locations, depth intervals, source areas and analyses performed are summarized in Table 1. In addition to the soil samples described above, consistent with NCDEQ requirements, one duplicate sample was collected for at least every 20 samples collected, with a total of five (5) duplicate samples collected (one at each depth at two building pad locations during the soil sampling event and one duplicate sample during the cut soil sampling event). All of the soil samples were analyzed for volatile organic compounds (VOCs) by Environmental Protection Agency (EPA) Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270 and RCRA Metals by EPA Method 6020. See Table 1 Soil Sample Summary below. See the attached Figures 1 and 4 for the approximate soil sample locations and Table 1 below for a breakdown of the number of samples and proposed collection depths. Table 1 Soil Sampling Summary Property Location/Potential Source Soil Sample ID Soil Sample Depth (Feet bgs) Analyses Building 1 SS-1 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 1 SS-1-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 2 SS-2 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 2 SS-2-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 3 SS-3 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals Brownfields Assessment Report PAGE 8 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Property Location/Potential Source Soil Sample ID Soil Sample Depth (Feet bgs) Analyses 6020 Building 3 SS-3-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 4 SS-4 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 4 SS-4-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 5 SS-5 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 5 SS-5-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 6 SS-6 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 6 SS-6-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 7 SS-7 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 7 SS-7-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 8 SS-8 0-1’ VOCs 8260, Brownfields Assessment Report PAGE 9 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Property Location/Potential Source Soil Sample ID Soil Sample Depth (Feet bgs) Analyses SVOCs 8270, RCRA Metals 6020 Building 8 SS-8-a 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 2 SS-2 (DUP) 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 2 SS-2-a (DUP) 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 3 SS-3 (DUP) 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Building 3 SS-3-a (DUP) 4-5’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Two (2) Foot Deep Utility Trenching East of Building 1 CS-1 0-2’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Two (2) Foot Deep Utility Trenching North of Building 2 CS-2 0-2’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Two (2) Foot Deep Utility Trenching South of Buildings 3 & 4 CS-3 0-2’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Seven (7) Foot Deep Utility Trenching East of Building 4 CS-4 (originally designated CS-4-a 2-3’ VOCs 8260, SVOCs 8270, RCRA Metals Brownfields Assessment Report PAGE 10 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Property Location/Potential Source Soil Sample ID Soil Sample Depth (Feet bgs) Analyses on Table 1 of the AWP) 6020 CS-4-a (originally designated CS-4-b on Table 1 of the AWP) 6-7’ Six (6) Foot Deep Utility Trenching South of Building 5 CS-5 (originally designated CS-5-a on Table 1 of the AWP) Auger refusal encountered at 1’. Unable to collect planned sample from 1-3’. Sample collected from 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 CS-5-a (originally designated CS-5-b on Table 1 of the AWP) 5-6’ (Unable to collect due to auger refusal) CS-5 (DUP) 0-1’ Seven (7) Foot Deep Utility Trenching South of Building 6 CS-6 (originally designated CS-6-a on Table 1 of the AWP) Auger refusal encountered at 2.5’. Unable to collect planned sample from 2-3’. Sample collected from 0-1’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 CS-6-a (originally designated CS-6-b on Table 1 of the AWP) Unable to collect planned sample from 6-7’ due to auger refusal. Sample collected from 1-2.5’ Two (2) Foot Deep Utility Trenching West of Building 7 CS-7 0-2’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 Two (2) Foot Deep Mass Grading Cut East of Building 8 CS-8 0-2’ VOCs 8260, SVOCs 8270, RCRA Metals 6020 TOTAL 31 Brownfields Assessment Report PAGE 11 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Soil Gas – Twelve (12) soil gas samples were collected across site in accordance with the requirements of the NC Brownfields program. Due to the degraded condition of the asphalt-paved area in the northern part of the site it was not be possible to collect sub- slab soil gas samples. Exterior soil gas samples (SG-1 through SG-8) were collected at a depth of approximately five (5) feet bgs within the footprints of the proposed building pads. Exterior soil gas samples SG-9 and SG-10 were collected at a depth of approximately five (5) feet bgs along the western property boundary. Of the twelve (12) soil gas samples collected, two (2) duplicate samples were collected, one at the time if each of the two soil gas sampling events. See the attached Figure 1 for the approximate soil gas sample locations. Surface Water – Surface water features are not currently present on the Property. Therefore, surface water samples were not collected during the course of this assessment. Groundwater – Earlier studies by others have identified VOC groundwater impacts in the northwestern and northeastern areas of the Property. However, groundwater assessment activities have not been conducted on the southeastern portion of the Property. Based on this information coupled with the proposed building locations on these areas of the Property, groundwater in the shallow (unconfined) aquifer was evaluated by constructing six monitoring wells (MWs) with a minimum of 15’ of 2” diameter PVC riser attached to 15 feet of 2” diameter PVC screen with a 0.010” slot size for total well depths of 30’ to 40’ feet bgs. The wells were installed in the vicinities of the proposed eight (8) building footprints as follows: one (1) in between buildings 1 and 2, one (1) between buildings 3 and 4, one (1) between buildings 5 and 6, one (1) in the building 7 footprint one (1) in the building 8 footprint and one (1) on the western property boundary adjacent to the west of the proposed building 2. See the attached Figure 1 for the approximate monitoring well locations. Boring logs for all sample locations are included in Attachment E. 2.4 Sample Locations Procedures, and Analytical Parameters 2.4.1 General Sampling Procedures Laboratory clean sampling containers appropriate for the analytical methods were used along with clean storage containers capable of holding the sample containers and ice necessary to appropriately preserve the samples collected. Those collecting the samples had training appropriate to the task, including an awareness of the need to avoid cross contamination of samples through measures such as the use of clean gloves for the collection of each sample. Required sampling implements such scoops, hand augers etc. were laboratory clean stainless steel. In addition, the following additional sampling protocols were followed: Soil and groundwater samples were collected, properly labeled, secured, and Brownfields Assessment Report PAGE 12 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 immediately preserved by placing them on ice. Each sample container was tightly sealed and placed in a clean zip lock bag. A laboratory Chain of Custody (COC) Form was completed that included relevant information for all samples including unique identification codes for each sample, date of collection, time of collection, and a description of the container sizes and types. After the collection of all samples the completed COC form was placed in a waterproof container (zip lock bag) with the samples and shipped overnight to the State of North Carolina-approved, National Voluntary Laboratory Accreditation Program (NVLAP) laboratory (Pace) for the analyses specified in this AWP in Tables 2 and 3 below. The shipping containers had signed and dated custody seals and enough ice to properly preserve the samples during transit. Soil gas samples were collected using laboratory clean Summa Canisters and regulators. Following sample collection Summa cannisters containing the soil gas samples were appropriately labeled with a unique identifier and dated, and COC forms were completed for all samples, which included beginning, final and lab-received vacuum/pressure readings. The Summa cannisters were shipped to H&P Mobile Geochemistry in Carlsbad, California for analysis of the full list of US EPA Method TO- 15 VOCs. Soil gas samples collected on December 21, 2022 were received by the laboratory on December 28, 2022. Soil gas samples collected on January 27, 2023 were received by the laboratory on January 30, 2023. H&P has the following accreditations: • United States Department of Defense, Environmental Laboratory Accreditation Program (ISO/IEC 17025:2005 and DoD-ELAP) - PJLA Accreditation No. 69070 (Methods: H&P 8260SV; EPA 8260B; EPA TO15) - TNI National Environmental Field Activities Program (NEFAP) • California Department of Public Health, Environmental Laboratory Accreditation Program, (ELAP) Certificate No. 2741; and Mobile Laboratory Certificate No. 2740 • National Environmental Laboratory Accreditation Program (NELAP) through the State of Louisiana, Department of Environmental Quality, Certificate No. 04138 2.4.2 Soil Sampling Procedures On November 10 and 14, 2022 EAS collected a total of thirty-one (31) soil samples from the proposed location of eight (8) structures and other locations (2 at each building footprint, 5 associated duplicate samples and 10 cut soil samples). Samples were collected using either an appropriately decontaminated direct push drilling rig Macrocore Soil Sampler or stainless-steel hand augers. Soil samples designated “Surface” were collected from surface to approximately one foot below grade (0-1’). Soil samples designated “Subsurface” were collected from approximately four feet (4) to five (5) feet below existing grade. Cut soil samples were collected from the ground Brownfields Assessment Report PAGE 13 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 surface up to approximately seven (7) feet below grade. Refer to Table 1 for specific sample depths. Soil samples were screened at one-foot intervals with a 10.6 eV MiniRAE photoionization detector (PID) and were also screened for visual and olfactory indicators. All sampling equipment was thoroughly cleaned between sampling locations using an Alconox solution for wash, followed by a clean water rinse and a final deionized water rinse. Samplers used clean nitrile or latex gloves between each sampling location. The soil sampling locations, depth intervals, source areas and proposed analyses are summarized in Table 1. In addition, at least one (1) duplicate sample was collected for at least every twenty (20) samples collected, as required by NCDEQ guidance. A total of five (5) duplicate soil samples were collected. These duplicate samples were collected at the locations of proposed Buildings 2 and 3 (two depths per location) and cut soil location CS-5. Each soil sample and duplicate sample was analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270 and RCRA Metals by EPA Method 6020. All soil cut samples were analyzed for these same parameters. All laboratory analytical detections were compared to the most recent (January 2023) NCDEQ Preliminary Soil Remediation Goals (PSRGs). In addition, all metals detections were compared to published naturally occurring regional background metals concentrations. These detections are shown on Tables 1A, 1B(a), and 1B(b) in Attachment B. 2.4.3 Groundwater Sampling Procedures Earlier groundwater investigations conducted on the site and adjacent properties by others indicated monitoring wells were set at a total depth of approximately 40 feet below grade. This information helped guide the installation of six (6), two-inch, Type II Monitoring wells on the site using an appropriately decontaminated hollow solid-stem auger drilling rig at the locations shown on Figure 1. The wells were installed in the shallow (unconfined) aquifer with a minimum of fifteen (15) feet of 2” diameter PVC riser attached to 15 feet of 2” diameter PVC screen with a 0.010” slot size at depths where the groundwater level at the time of drilling would be approximately in the middle of the screen. This resulted in wells of depths of 30 to 40 feet bgs. All wells were finished with the appropriate sand pack, screened interval isolation seal and grout to the surface. A groundwater monitoring well summary is provided in Table 2 below. Table 2 Groundwater Monitoring Well Summary Monitoring Well ID Total Well Depth (feet) Ground Elevation (feet above msl) Groundwater Elevation (feet above msl) Depth to Groundwater (feet) MW-1 30 963.3 954.1 9.2 MW-2 40 982.6 955.3 27.3 MW-3 40 979.9 956.6 23.3 Brownfields Assessment Report PAGE 14 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 MW-4 30 968.2 955.9 12.3 MW-5 30 971.3 953.4 17.9 MW-6 30 968.9 953.4 15.5 Following installation of the wells, the water levels in them were allowed to stabilize at least 48-hours and their water levels were measured relative to the top of the well casings. They were then developed by surging and pumping to reduce turbidity to the greatest extent possible. All purge waters were collected in appropriately labeled 55- gallon drums. Well construction records are provided in Attachment F. Groundwater samples were collected from all six (6) monitoring wells on December 12 ,2022. Prior to collecting samples from the wells, during the later phases of the well purging process, EAS measured the following parameters with appropriately calibrated field meters: temperature, pH, turbidity, and specific conductance until all parameters had stabilized to within 5% of the previous reading. The wells were then sampled. Groundwater sampling was conducted in accordance with the EPA Region 4 Science and Ecosystem Support Division (SESD) Groundwater Sampling Operating Procedure documented dated April 20, 2017. Groundwater samples from each well were analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA metals by EPA Method 6020, unfiltered. In addition, the following quality control samples were also be submitted and analyzed for VOCs: one trip blank and at least one duplicate sample per sampling round (VOCs, SVOCs and RCRA metals, unfiltered). The planned field blank was not submitted to the laboratory due to miscommunication. All field instruments and sampling equipment were decontaminated between wells by use of an Alconox soap solution, clean water rinse, followed by a deionized water rinse. All field data was recorded in field logs and Well Development Forms. EAS field technicians measured water levels in each well relative to the top of casing at least 24 hours after sampling was complete and elevations of each top of casing were determined by surveying methods. These water level and top of casing measurements were used to develop a groundwater potentiometric surface map with a graphic scale and north arrow which is included as Figure 3. All groundwater sample analytical results have been compared to the 15A North Carolina Administrative Code (NCAC) 02L.0202 Groundwater Standards (2L Standards) dated April 1, 2022. Results are shown in attached Tables 1C and 1D in Attachment B. Brownfields Assessment Report PAGE 15 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Table 3 Groundwater Sample Analytical Procedures Property Location/Potential Source Sample ID Analyses Between Buildings 1 and 2 MW-1 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Between Buildings 2 and 3 MW-2 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Between Buildings 5 and 6 MW-3 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Building 7 MW-4 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Building 8 MW-5 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Western Property Boundary MW-6 VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered Duplicate Sample Dup-1 (MW-3) VOCs 8260, SVOCs 8270, RCRA Metals 6020, Unfiltered 2.4.4 Soil Gas Sampling Procedures Soil gas samples were collected at each proposed structure location and at two locations along the western boundary of the property where historical data suggest possible migration of subsurface impacts from the former Salem Uniform facility. This included eight (8) buildings, two (2) locations along the western boundary, as well as two (2) duplicate samples for a total of twelve (12) soil gas samples as summarized in Table 4. All soil vapor samples were collected from a depth of five (5) feet below existing grade. See Figure 1 for approximate soil gas sample locations. Soil vapor samples were collected using a vapor point implant system set within a sand pack within the sampling interval which was isolated by hydrated bentonite chip seal. Soil gas sampling followed modified US EPA Region 4 Laboratory Services and Applied Science Division (LSASD) Procedure 307-R4. The steps followed are summarized as follows. 1. An appropriately sized sampling hole was drilled at each sampling location using either a Geoprobe® drilling rig or a properly decontaminated stainless steel hand auger. Sampling depths were five (5) feet from existing grade. After the hole was created the work area was covered with a sheet of clean plastic sheeting. The sampler(s) then donned a pair of clean powder free rubber gloves. 2. Drilling tooling was extracted from the borehole to facilitate installation in the open borehole. Brownfields Assessment Report PAGE 16 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 3. A properly decontaminated water level sounder was used to verify groundwater was not present in the bottom of the boring. 4. A 2-3 inch lift of clean sand was placed at the terminus of the borehole. 5. A new single-use vapor implant was connected to sample tubing and the vapor implant was lowered down the borehole to the top of sand via the sample tubing. 6. Clean sand was then slowly introduced into the boring until there was approximately six inches of sand above the soil vapor implant. Care was taken to ensure no bridging of the sand. 7. The remaining borehole was then backfilled with bentonite crumbles to the ground surface. Potable water was used to hydrate the bentonite in intervals after the first 6-inches of bentonite had been placed. 8. After installation, the system was purged and a leak check performed. Purging was performed using a peristaltic pump and three-way valve to evacuate air from the annular space below the sample point and sample tubing. 9. A leak check was conducted by placing a shroud over the sample point and saturating the air within the shroud with helium gas to a concentration between approximately 70% and 80%. A helium gas detector was used to determine the concentration of helium within the shroud. Once concentrations in the shroud had reached an acceptable level, the sample point was purged into a Tedlar® bag. The helium detector was then used to screen the contents of the Tedlar® bag to confirm it did not contain a helium concentration greater than 5% of that detected in the shroud. Sample points had to successfully pass the leak check criteria prior to sampling. The leak check was documented on the sampling QA/QC field form. 10. Following a successful leak check, laboratory-supplied, individually certified 1- liter Summa canisters were connected to each of the sampling points via the Teflon® tubing. Flow regulators on the Summa canisters were set to collect the samples at a flow rate of approximately 100 mL/min. After the samples were collected, the canisters were immediately shipped under chain-of-custody protocol to H&P Mobile Geochemistry in Carlsbad, California for analysis of the full list of US EPA Method TO-15 VOCs including Naphthalene. Following the Chain of custody forms for soil gas samples is a table (Table 2) of Summa cannister vacuum pressure readings showing values for the laboratory out, beginning of sample collection, end of sample collection and laboratory- received vacuum pressure readings. Brownfields Assessment Report PAGE 17 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Table 4 Soil Gas Samples Sample ID Location Depth at Existing Grade (feet) Analysis* SG-1 Building 1 5’ Full TO-15 VOCs SG-2 Building 2 5’ Full TO-15 VOCs SG-3 Building 3 5’ Full TO-15 VOCs SG-4 Building 4 5’ Full TO-15 VOCs SG-5 Building 5 5’ Full TO-15 VOCs SG-6 Building 6 5’ Full TO-15 VOCs SG-7 Building 7 5’ Full TO-15 VOCs SG-8 Building 8 5’ Full TO-15 VOCs SG-9 Western property boundary 5’ Full TO-15 VOCs SG-10 Western property boundary 5’ Full TO-15 VOCs SG-Duplicate From SG-7 5’ Full TO-15 VOCs Duplicate-2 From SG-10 5’ Full TO-15 VOCs * Analysis was the TO-15 Extended 8260 list which includes Naphthalene and other compounds 2.4.5 Documentation Sample Labeling After samples were collected, they were placed into certified laboratory clean containers supplied by the laboratory. Each sample container had a sample label generated by the sampling personnel. Each sample container label had, at a minimum, the following information: • Sample identification. • Analysis requested. • Project Number. • Date and Time of Collection. Soil and Groundwater Sample Packaging and Shipping After the sample labels were placed on each sample container, the outside of each container was then wiped clean. As necessary, a strip of clear tape was applied on the label to ensure the ink did not smear. Each sample was then be packaged and shipped in the following manner: • Checked lid/cap to ensure proper closure to eliminate leaks. • Checked to ensure each label is intact and legible. • Placed each labeled sample container in a sealed clear plastic zip bag. • Placed the samples in a large zip tied plastic bag with ice and placed that bag in a clean waterproof shipping container (i.e. a cooler). • Placed a temperature blank (40 ml vial filled with water) in the container with the Brownfields Assessment Report PAGE 18 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 samples. • Labeled and placed the trip blank in the container with the samples. • Packed the shipping container with noncombustible packing material such as bubble wrap to prevent container breakage. • Enclosed a copy of the chain-of-custody in a clear plastic bag taped to the underside of the shipping container lid. • Taped the cooler shut using strapping tape over the hinges. • Placed custody seals that had been signed and dated across the top and sides of the cooler so that when they were broken at the signature section of the seal when the shipping container was opened. • Placed return address label clearly on the outside of the shipping container. • If more than one shipping container was being sent to the laboratory, each shipping container was labeled as 1 of 2, 2 of 2, etc. • Shipped by overnight delivery through a commercial carrier. • The air bill for the laboratory was completed so the samples were received the next calendar day. Address the recipient as “sample custodian.” Soil Gas Summa Canisters Shipping Summa cannisters containing soil vapor samples were checked to ensure they were tightly secured, and dust caps were attached as applicable. Labels were then verified, and they were shipped in laboratory supplied protective containers, overnight under proper chain of custody to the laboratory. Shipping containers were sealed with Custody Seals. Custody Seals Each sample shipping container was sealed with strapping tape and with at least two custody seals. The custody seals were placed so that they were broken at the signature section of the seal when the shipping chest was opened. Each custody seal included the following information: • Date of sample shipment (release of custody). • Signature of individual releasing custody. Chain-of-Custody (COC) COC forms accompanied the samples collected. The COC form sent to the laboratory included the following information: • Printed name and signature of sampler. • Date and time relinquished. • Project number. • Sample numbers or identifications. • Sample matrix (i.e. soil, groundwater). • Type of sample (all should be discrete or grab). • Analyses requested/turnaround time. • Preservative information. • Date and time of sample collection. • Designation of laboratory QC samples. • Date shipped/method of shipment/air bill number/laboratory address. Brownfields Assessment Report PAGE 19 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Each chain-of-custody form was distributed as follows: • The original laboratory copy was placed in a zip lock bag, which was sealed and placed into the shipping container and shipped with the samples to the laboratory • A copy was placed in the Job Folder Field Documentation A field logbook was maintained that document field activities. Criteria for the documentation include: • Bound logbook. • Indelible ink used for entries. • Entries should be factual, detailed, and objective. • Date and time of all entries. Information recorded the field logbook included the following as well as other information: • Date and time of entry. • Purpose of sampling. • Name and affiliation of personnel performing sampling. • Type of sample, e.g.: soil, groundwater. • Description of samples (color, texture, etc.). • Analysis requested. • Description and location of the sampling point. • Date and time of sample collection. • Difficulties experienced in obtaining sample if applicable. • Visual references, such as maps or photographs of the sampling site. • Field observation, such as weather conditions during sampling periods. • Whether chain-of-custody forms have been filled out for the samples. • Laboratory name, address, and date shipped. 2.5 RECEPTOR SURVEY EAS performed a receptor survey in accordance with Program guidelines to determine land use, public and private water supply wells, and underground utilities within the vicinity of the subject property. On December 21, 2022, EAS’s representative performed a windshield receptor survey within 1,500 feet of the property boundaries to determine if water supply or irrigation wells were present. Nineteen (19) receptors (private water supply wells) were observed within 1,500 feet of the property boundaries. The results are the receptor survey and supporting documentation/research are attached (see Attachment G and Figures 5 and 6). Brownfields Assessment Report PAGE 20 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 3.0 QUALITY ASSURANCE PROJECT PLAN 3.1 Introduction The AWP was developed and implemented in accordance with the technical intent of the National Contingency Plan. All drilling, soil and groundwater sampling, well installation, and decontamination activities will be performed in accordance with the US EPA Region 4 Field Branches Quality System and Technical Procedures. The AWP is designed to characterize potentially impacted soil, soil gas and groundwater on the 450 Polo Road Property with regard to possible exposure risks to those impacted media under residential land use. The primary objective of this AWP is to collect soil, soil gas and groundwater samples that will allow measurement of chemical properties of these media that are both accurate and precise. If the measured values are found to be sufficiently accurate and precise, they will be considered reliable measurements of the chemical properties of the sampled soil, soil gas and groundwater. 3.2 Data Quality Objectives (DQOs) Data collected from suspect soils during the field sampling activities will be of a quality such that it can be screened and compared to the NCDEQ-PSRGs. Soil gas samples will be screened and compared to the NCDEQ-Residential Vapor Intrusion Screening Levels. In the case of groundwater samples, laboratory analytical results will be compared to the 15A NCAC 2L Standards. If an analyte is not listed in these documents, it will be compared to their respective EPA Regional Screening levels (RSLs). All laboratory data will be reported under a minimum of Level II QA/QC protocols. Laboratory analysis will include the sample method detection limits meeting applicable screening values and J-Flags will be reported for respective media. All soil and groundwater samples will be analyzed by a State of North Carolina-certified and NVLAP certified laboratory using promulgated US EPA methodology such as those listed in Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW-846, 3rd Edition (SW- 846). The laboratory that will be performing the TO-15 analysis in accordance with SW -846 has the certifications listed in Section 2.5.2 above. These methodologies specify Quality Assurance and Quality Control (QA/QC) procedures at are to be implemented by the approved laboratory performing the analyses. The methods also provide guidelines regarding detection capabilities and limits of sample quantification. If for any reason the sample quantitation limit cannot meet the de minimis standard given in the guidance cited above, either due to technological limitations of the method or sample matrix interference, the sample method detection limit and J-Flags will be reported. 3.3 Data Quality Objectives – Seven Step Process This DQO process was developed within the framework of the Guidance on Systematic Brownfields Assessment Report PAGE 21 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 Planning Using the Data Quality Objectives Process EPA QA/G-4, and Section 3 of Quality Assurance Guidance for Conducting Brownfields Site Assessment. DQOs for this project are outlined in the following seven steps: 1: State the Problem A Groundwater and Air Monitoring Report for an April 2019 Sampling Event dated August 2019 conducted by AECOM detected PCE in groundwater at concentrations above the 2L Standard of 0.7 ug/L in 22 monitoring well samples. Detected concentrations of PCE exceeding the 2L Standard ranged from an estimated concentration of 0.703 ug/L to 50,100 ug/L. Trichloroethene (TCE) was detected at concentrations above the 2L Standard of 3 ug/L in 10 monitoring well samples. Detected concentrations of TCE exceeding the 2L Standard ranged from an estimated concentration of 3.68 ug/L to 684 ug/L. Additionally, cis-1,2-Dichloroethylene (DCE), 1,2-dichloroethane (DCA), benzene, and vinyl chloride were detected at concentrations above the 2L Standard in several samples. Groundwater isoconcentration maps indicated that shallow groundwater beneath the western portion of the Property has been adversely impacted by the PCE contamination plume migrating from this facility. A previous Phase II Environmental Site Assessment conducted by Terraquest and dated January 24, 2017 identified groundwater impacted with benzene and PCE at levels that exceeded the 2L Standard benzene beneath the northwestern portion of the Property; and elevated benzene, toluene, ethylbenzene, xylenes (BTEX), naphthalene, 1,2-dibromoethane (EDB), 1, 2-dichloroethane (DCA), 1,2,4- trimethylbenzene, 2-hexanone and PCE concentrations were detected beneath the northeastern portion of the Property. Soil gas was not previously assessed in these earlier studies by others and the extent of the impacts in soil and groundwater throughout the areas of the Property proposed to be improved were not defined. A more comprehensive study is needed to better assess potential risks to human health and the environment with regard to the future residential land use on the Property. 2: Identify the Goals of the Study The goals of this study are to determine if impacts exist in other areas of the Property where they were not identified in the previous assessments, and to determine the extent of environmental impacts where they were found to exist in this earlier study. Additional goals of the study will be to determine what risks any measured impacts may pose to human health and if additional assessment and/or remediation of the site is needed. Brownfields Assessment Report PAGE 22 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 3: Identify Information Inputs Soil, soil vapor and groundwater samples will be collected and analyzed from suspect areas of the Property. Data obtained from these analyses will be used to characterize the extent of environmental impacts on the Property, what, if any, risks these impacts may pose to human health and the environment, and if any additional assessment may be necessary. Soil and Groundwater samples will be collected and analyzed as described in Section 2.4 of this AWP. 4: Define the Boundaries of the Study The proposed study described in this AWP is limited to the geographic boundaries of the 450 Polo Road Property. Regarding temporal limits, no regulatory time limits have been indicated. It is, however, the goal of the owners of the 450 Polo Road Property to have all work required in this first phase of the Brownfields project complete, a report of findings of the study to NCDEQ, and response received from NCDEQ as soon as possible. 5: Develop the Analytical Approach Parameters of interest in this study have been indicated by information obtained during the aforementioned previous assessments. Findings of this study will be used to determine what additional actions may be needed to accommodate planned residential development of the site. 6: Specify Performance or Acceptance Criteria Laboratory analytical data obtained in the course of this study will be used to determine if contaminants exist on the Property in excess of the criteria given in Section 3.2 of this AWP. Historical research, earlier sampling data from the Property and the NCDEQ AWP Checklist have helped guide the analytical parameters and sample locations chosen. EPA-mandated laboratory procedures and protocols should help ensure performance criteria are met. Some of these procedures and protocols include the use of equipment and various sample blanks, duplicate samples, and evaluation of analyte recoveries. If one or more of these protocols do not meet acceptance criteria, the data will be evaluated in detail and if necessary, re-analysis or re-sampling conducted. 7: Develop the Plan for Obtaining Data Design optimization to meet project goals within the project boundaries has been the guiding force in the development of this AWP. In the course of evaluating the history of potential source areas and exposure pathways, sampling locations and parameters have been refined and adjusted. Analytical parameters and spatial distribution of sampling locations have been developed to identify and characterize a wide range of potential impacts across the entire Property, even at locations where available historical information suggests a low probability of impacts. Brownfields Assessment Report PAGE 23 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 3.0 FINDINGS 3.1 Soil Sampling Results RCRA Metals Thirty-one (31) surface and subsurface soil samples were analyzed for the eight (8) Resource Conservation and Recovery Act (RCRA) metals using EPA Method 6020B except for Mercury which was analyzed using EPA Method 7471B. Results are summarized in Table 1A in Attachment B. All detections were compared to the NCDEQ’s Industrial/Commercial, Residential and Protection of Groundwater Heath Based Preliminary Soil Remediation Goals (PSRGs) (January 2023), as well as to published naturally occurring regional background metals concentrations. The only PSRG exceedances were for arsenic and chromium. arsenic was detected in all soil samples at concentration ranging from 1.05 mg/kg (with “J” qualifier) to 10.8 mg/kg. Of these detections, fourteen (14) exceeded the Industrial PSRG for arsenic and seventeen (17) exceeded both the Residential and Protection of Groundwater PSRGs. chromium was also detected in all thirty-one (31) soil samples with twenty- seven (27) exceeding the Industrial PSGR, three (3) exceeding both the Residential and Protection of Groundwater PSRGs and one (1) exceeding the Residential PSRG only. All metals detections were compared to published regional naturally occurring background levels and in all cases were found to be consistent with naturally occurring levels and are considered representative of background conditions. Semi-Volatile Organic Compounds (SVOCs) Thirty-one (31) surface and subsurface soil samples were analyzed for SVOCs by EPA Method 8270E. Results are summarized in Table 1B(a) in Attachment B. The polynuclear aromatic hydrocarbon (PNA) benzo(a)anthracene was detected in thirteen (13) samples at concentrations ranging from 0.00791 mg/kg (with “J” qualifier) to 3.77 mg/kg. Two (2) of these detections exceeded the Protection of Groundwater PSRG, and two (2) of these detections exceeded the Residential and Protection of Groundwater PSRGs for this compound. The PNA benzo(b)fluoranthene was detected in fourteen (14) samples at concentrations ranging from 0.0155 mg/kg (with “J” qualifier) to 6.95 mg/kg. Three (3) of these detections exceeded the Protection of Groundwater and Residential PSRGs for this compound. The PNA benzo(a)pyrene was detected in fourteen (14) samples at concentrations ranging from 0.0106 mg/kg (with “J” qualifier) to 5.12 mg/kg. Two (2) of these detections exceeded the Industrial/Commercial PSRG, and three (3) of these detections exceeded the Residential and Protection of Groundwater PSRGs for this compound. Brownfields Assessment Report PAGE 24 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 The PNA dibenz(a,h)anthracene was detected in five (5) samples at concentrations ranging from 0.0315 mg/kg (with “J” qualifier) to 0.604 mg/kg. One (1) of these detections exceeded the Protection of Groundwater and Residential PSRGs for this compound, and three (3) of these detections exceeded the Residential PSRG. The PNA indeno(1,2,3-cd)pyrene was detected in eight (8) samples at concentrations ranging from 0.0278 mg/kg (with “J” qualifier) to 2.36 mg/kg. The highest detection (2.36 mg/kg) only exceeded the Residential PSRG for this compound. Volatile Organic Compounds (VOCs) Thirty-one (31) surface and subsurface soil samples were analyzed for VOCs by EPA Method 8260B. Results are summarized in Table 1B(b) in Attachment B. The following VOCs were detected at concentrations below all PSRGs: acetone (2 samples), benzene (1 sample), sec-butylbenzene (2 samples), chloroform (11 samples), 1,4-dichlorobenzene (1 sample), ethylbenzene (2 samples), isopropylbenzene (cumene, 8 samples), p-Isopropyltoluene (9 samples), 4-methyl-2- pentanone (MIBK) (2 samples), napthalene (1 sample), styrene (2 samples), tetrachloroethene (11 samples), toluene (10 samples), 1,2,4-trimethylbenzene (1 sample) and total xylenes (12 samples). The VOC tetrachloroethene was detection at 0.00855 mg/kg, which is above the Protection of Groundwater PSRG for this compound. This concentration does not exceed other PSRGs. 3.2 Groundwater Sampling Results RCRA Metals Seven (7) groundwater samples were collected from six (6) groundwater monitoring wells recently constructed in the shallow (unconfined) aquifer (six [6] wells sampled and one [1] duplicate) after proper well development. All samples were analyzed for the eight RCRA metals using EPA Method 6020B except for Mercury which was analyzed using EPA Method 7470A. All detections were compared to the 15A North Carolina Administrative Code (NCAC) 02L.0202 Groundwater Standards (2L Standards) (April 1, 2022). The arsenic 2L standard was exceeded in three (3) wells, the barium 2L standard was exceeded in two (2) wells, the chromium 2L standard was exceeded in three (3) wells, the lead 2L standard was exceeded in five (5) wells, and the mercury 2L standard was exceeded in in two (2) wells. Results are summarized in Table 1C in Attachment B. Semi-Volatile Organic Compounds (SVOCs) Seven (7) groundwater samples were collected from six (6) groundwater monitoring Brownfields Assessment Report PAGE 25 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 wells recently constructed in the shallow (unconfined) aquifer (six [6] wells sampled and one [1] duplicate) after proper well development. All samples were analyzed for SVOCs using EPA Method 8270E. The only SVOC detected above the 2L standard was naphthalene in one monitoring well (MW-3). This compound was detected in both the SVOC analysis using Method 8270E and the VOC analysis using Method 8260D. However, the Method 8260B result had a “J3” qualifier indicating the result was outside the acceptable precision range while the Method 8270E result had no qualifiers. For this reason, the 8270E result is considered the acceptable one. Results are summarized in Table 1D in Attachment B. Volatile Organic Compounds (VOCs) Seven (7) groundwater samples were collected from six (6) groundwater monitoring wells recently constructed in the shallow (unconfined) aquifer (six [6] wells sampled and one [1] duplicate) after proper well development. All samples were analyzed for VOCs using EPA Method 8260D. The VOCs benzene, 1,2-dibromoethane, 1,2-dichloroethane, toluene, and total xylenes exceeded their respective 2L limits in one (1) well (MW-3). The 2L Standard for tetrachloroethene was exceeded in two (2) wells (MW-3 and MW-6). Results are summarized in Table 1D in Attachment B. 3.3 Soil Gas Sampling Results Soil gas samples were collected at each proposed structure location and at two locations along the western boundary of the property where historical data suggest possible migration of subsurface impacts from the former Salem Uniform facility. This included eight (8) buildings, two (2) locations along the western boundary, as well as two (2) duplicate samples for a total of twelve (12) soil gas samples as summarized in Table 1E. All soil vapor samples were collected from a depth of five (5) feet below existing grade and were analyzed for the extended list of EPA Method VOCs. Thirty-two (32) different VOCs were detected in the soil vapor points sampled. The VOCs benzene, ethylbenzene, and tetrachloroethene exceeded their respective NCDEQ Vapor Intrusion Sub-Slab and Exterior Soil Gas Screening Levels (July 2022) in soil gas samples SG-10 and Duplicate-2 (the duplicate sample from vapor well SG- 10.) The soil gas screening levels for chloroform and m,p-xylene were exceeded in soil gas sample Duplicate-2 from vapor well SG-10. Tetrachloroethene exceeded the screening level in the soil gas sample collected from vapor well SG-3. 4.0 MANAGEMENT OF INVESTIGATION DERIVED WASTES The investigation derived wastes (IDW) associated with the performance of this sampling plan have been containerized and characterized in accordance with 15A NCAC 02T.1503 (https://deq.nc.gov/media/14220/download) and 15A NCAC 02H. Brownfields Assessment Report PAGE 26 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 0106 (https://files.nc.gov/ncdeq/DENR/documents/HPAI/Appendix%202%20Decontaminati on.pdf) IDW include the following: • Drilling cuttings from the construction of monitoring wells • Soils remaining from soil and soil vapor sample collection • Monitoring well purge waters • Wash waters derived from decontamination of equipment All drilling cuttings obtained from the construction of monitoring and vapor monitoring wells, as well as any soils remaining from the collection of soil and soil vapor samples, monitoring well purge waters, and collected equipment decontamination waters, have been collected in sealed in 55-gallon drums and are being stored in a designated location onsite. Laboratory analytical data for soil and groundwater samples collected and analyzed during this investigation will be used to characterize these soils and waters for disposal. Following waste profiling these soils and waters will be properly disposed and documentation of their disposal obtained. 5.0 SUMMARY AND CONCLUSIONS EAS has completed a Brownfields assessment of the 3.927-acre undeveloped property at 450 Polo Road in Winston-Salem, North Carolina. These activities were completed in accordance with the Brownfields Site Assessment Work Plan prepared by EAS and approved by the NCDEQ Brownfields Program on October 21, 2022. Sampling activities included the collection and analysis of soil, groundwater and soil vapor samples from across the site with the goal of determining potential risks that may be presented for residential site development. The following is a summary of assessment activities and findings. 5.1 Soil Sampling Thirty-one (31) surface and subsurface soil samples were analyzed for the eight (8) RCRA metals using EPA Method 6020B except for Mercury which was analyzed using EPA Method 7471B. These same thirty-one (31) samples were also analyzed for VOCs using EPA Method 8260D and for SVOC using EPA Method 8270E. Results are summarized in Tables 1A, 1B(a) and 1B(b) in Attachment B. All detections were compared to the NCDEQ’s Industrial/Commercial, Residential and Protection of Groundwater (PSRGs) (January 2023). The highest analyte concentrations detected in any of the soil samples collected were subsequently used in the NCDEQ Risk Calculator (January 2023) to model a Site-wide “worst-case” scenario for soil exposure in the proposed residential land use scenario. The Risk Calculator results are provided in Attachment C. Results of the Site-wide worst-case soil exposure calculation for residential land use indicate a Lifetime Incremental Cancer Risk (LICR) of 4.7 x 10-4 which exceeds the Brownfields Assessment Report PAGE 27 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 target LICR of 1 x 10-4. In addition, the Residential Soil Exposure Hazard Index (HI) was calculated to be 1.1 which exceeds the target HI of 1.0. 5.2 Soil Gas Sampling Soil gas samples were collected at each proposed structure location and at two locations along the western boundary of the property where historical data suggest possible migration of subsurface impacts from the former Salem Uniform facility. This included eight (8) buildings, two (2) locations along the western boundary, as well as two (2) duplicate samples for a total of twelve (12) soil gas samples as summarized in Table 1E in Attachment B. All soil vapor samples were collected from a depth of five (5) feet below existing grade and were analyzed for the extended list of EPA Method VOCs. Thirty-two (32) different VOCs were detected in the soil vapor points sampled. The highest VOC concentration of each compound detected in any of the soil vapor points was used to model a hypothetical Site-wide worst-case vapor exposure scenario for residential development. The results of the Site-wide worst-case soil gas exposure model found a LICR of 1.7 x 10-5 which is below the LICR target value of 1 x 10-4. In addition, result of the worst- case calculation for residential HI is 0.97, which is the below the HI target value of 1.0. 5.3 Groundwater Sampling Seven (7) groundwater samples were collected from six (6) groundwater monitoring wells recently constructed in the shallow (unconfined) aquifer (six [6] wells sampled and one [1] duplicate) after proper well development. All samples were analyzed for the eight RCRA metals using EPA Method 6020B except for Mercury which was analyzed using EPA Method 7470A. These same seven (7) samples were also analyzed for VOCs using EPA Method 8260D and for SVOCs using EPA Method 8270E. Results are summarized in Tables 1C and 1D in Attachment B. All detections were compared to the 15A North Carolina Administrative Code (NCAC) 02L.0202 Groundwater Standards (2L Standards) (April 1, 2022). The arsenic 2L standard was exceeded in three (3) wells, the barium 2L standard was exceeded in two (2) wells, the chromium 2L standard was exceeded in three (3) wells, the lead 2L standard was exceeded in five (5) wells, and the mercury 2L standard was exceeded in in two (2) wells. The only SVOC detected above the 2L standard was naphthalene in one monitoring well (MW-3). The VOCs benzene, 1,2-dibromoethane, 1,2- dichloroethane, toluene, and total xylenes exceeded their respective 2L limits in one (1) well (MW-3). The 2L Standard for tetrachloroethene was exceeded in two (2) wells (MW-3 and MW-6). Site development plans call for the use of municipal water for all site improvements. As site development as planned does not result in a completed groundwater exposure Brownfields Assessment Report PAGE 28 EAS No. 225234 450 Polo road Winston Salem, NC March 24, 2023 pathway, a potential exposure model for groundwater was not performed. Brownfields Assessment Report EAS No. 22-5234 450 Polo road Winston Salem, NC March 24, 2023 ATTACHMENT A FIGURES Figure 1: Sample Location Map Figure 2: Site Location Map Figure 3: Groundwater Potentiometric Map Figure 4: Cut Soil Sample Location Map Figure 5: Receptor Survey Site Vicinity Map Figure 6: Public Water Sources Map Sample Location Map Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:Stimmel Date:March 2023 Scale: NTS Figure 1 Project Site Proposed Monitoring Well (MW) Locations SS-1/SS-1-a/SG-1 SS-2/SS-2-a/SG-2 SS-3/SS-3-a/SG-3 SS-4/SS-4-a/SG-4 SS-5/SS-5-a/SG-5 SS-6/SS-6-a/SG-6 SS-7/SS-7-a/SG-7 SS-8/SS-8-a/SG-8 SG-9 SG-10 MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 North Building 1 Building 2 Building 3 Building 4 Building 5 Building 6 Building 7 Building 8 Proposed Soil Sample (SS) and Soil Gas (SG) Sampling Locations Site Location Map North Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:USGS Rural Hall, NC 2022 Date:March 2023 Scale: As Shown Figure 2 Groundwater Potentiometric Map North As Shown Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:Client/EAS Date:March 2023 Scale: As Shown Figure 3With Paper Size: 36.00 x 24.00 inches Cut Soil Sample Location Map North Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:Stimmel 2020 Date:March 2023 Scale: As Shown Figure 4 0.0 Trench Utility Cuts Depths Variable ~2-8 feet into undisturbed soil 0.0 0.0 +2.5 0.0 0.0 0.0 +2.0 +2.5 +2.0 +2.0 +2.0 +2.0 +2.0 +2.0 +4.0 +5.0 +3.0 +3.0 +1.0 +4.0 0.0 +1.0 -2.0 +6.0 +6.5 +6.5 +6.0 +2.0 +7.5 +7.5 +7.5 +9.0 0.0 Projected Cut/Fill Depths; + values fill, - values cut +6.0 CS-1 CS-2 CS-4/CS-4-a CS-3 CS-5/CS-5-a’ CS-6/SC-6-a CS-7 CS-8 Cut Soil (CS) Sample Receptor Survey Site Vicinity Map North Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:EAS/Forsyth County GIS Date:March 2023 Scale: As Shown Figure 5 Zoning Boundaries: RS/RSQ/RM/RMU-Residential; LI-Limited Industrial; HB-Highway Business; LB-Limited Business; MH-Manufactured Housing; GI-General Industrial; GB-General Business; PB-Pedestrian Business; LO-Limited Office; NO-Neighborhood Office Water Supply Well See Table 3 of Brownfield Assessment Report for Surrounding Property Owners PW2 PW3 PW4 PW5 PW6 PW8 PW9 PW10 PW11 PW12 PW13 PW14 PW15 PW16 PW17 1,500 ft. PW7 PW1 PW18 PW19 Public Water Sources Map North Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:SWAPInfo 2.0 Date:March 2023 Scale: NTS Figure 6 No surface water sources, groundwater sources, or wellhead protection areas within a 1-mile radius of the property 1 mi. Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT B Laboratory Results Tables Soil IDDepth (Ft)Date SampledArsenicBariumCadmiumChromiumLeadSeleniumSilverMercurySS-1 0-1'11/10/22 3.15 15.0 <0.105 8.82 17.2 0.249 <0.107 0.0502 SS-1-a 4-5'11/10/22 1.74 41.2 <0.0982 5.51J 7.45 0.235J <0.0993 <0.0207 SS-2 0-1'11/10/22 1.77 20.8 0.129J 6.25J 30.7 <0.246 <0.118 0.0467J SS-2 (DUP) 0-1'11/10/22 4.04 27.3 <0.113 11.5 19.5 1.15J <0.114 0.0582 SS-2-a 4-5'11/10/22 5.43 21.2 <0.111 17.5 9.53 0.496J <0.113 0.165 SS-2-a (DUP) 4-5'11/10/22 6.88 36.7 <0.111 23.2 11.6 1.11J <0.113 0.180 SS-3 0-1'11/10/22 3.41 13.3 <0.104 13.1 6.52 0.220J <0.105 0.0289J SS-3 (DUP) 0-1'11/10/22 5.02 22.5 <0.129 19.8 8.12 0.801J <0.131 0.0310J SS-3-a 4-5'11/10/22 1.61 6.41 <0.0946 5.97 3.81 <0.199 <0.0957 <0.0199 SS-3-a (DUP) 4-5'11/10/22 4.24 15.7 <0.128 17.5 7.34 0.936J <0.129 <0.0269 SS-4 0-1'11/10/22 7.86 18.8 <0.119 33.4 10.1 0.645J <0.121 0.0775 SS-4-a 4-5'11/10/22 1.05J 8.03 <0.144 8.42 8.90 <0.302 <0.145 <0.0302 SS-5 0-1'11/10/22 8.68 10.1 <0.126 21.6 9.78 <0.265 <0.127 0.0805 SS-5-a 4-5'11/10/22 10.8 26.6 <0.114 39.2 22.7 0.595J <0.115 0.163 SS-6 0-1'11/10/22 15.3 25.1 <0.125 34.5 11.9 1.12J <0.126 0.0849 SS-6-a 4-5'11/10/22 11.4 37.2 <0.103 38.3 12.6 1.42J <0.104 0.143 SS-7 0-1'11/10/22 4.82 33.8 0.905J 12.3 56.9 0.827J <0.110 0.0513 SS-7-a 4-5'11/10/22 5.30 43.7 <0.106 16.7 12.0 0.773J <0.107 0.0637 SS-8 0-1'11/10/22 6.94 22.1 <0.118 12.4 18.7 1.03J <0.119 0.0564 SS-8-a 4-5'11/10/22 5.38 21.7 <0.0971 8.56 27.5 0.788J <0.0982 0.0210J CS-1 0-2'11/14/22 6.26 48.7 0.962J 78.4 94.8 0.986J <0.126 0.0589 CS-2 0-2'11/14/22 4.54 27.5 <0.108 12.4 11.0 0.774J <0.109 0.0364J CS-3 0-2'11/14/22 3.68 30.0 0.178J 11.0 73.6 0.550J <0.105 <0.0219 CS-4 2-3'11/14/22 7.87 32.4 <0.108 28.4 14.8 0.817J <0.109 0.0668 CS-4-a 6-7'11/14/22 1.25J 21.0 <0.129 1.84J 22.9 0.330B J <0.131 <0.0272 CS-5 0-1'11/14/22 4.60 39.5 0.506J 30.9 61.1 0.785J <0.116 0.0731 CS-5 (DUP) 0-1'11/14/22 5.90 44.0 0.380J 31.5 67.3 0.704J <0.103 0.0502 CS-6 0-1'11/14/22 7.69 33.2 <0.106 26.6 46.8 0.827J <0.108 0.0638 CS-6-a 1-2.5'11/14/22 10.7 46.8 <0.102 37.0 46.9 0.882J <0.103 0.0669 CS-7 0-2'11/14/22 4.51 39.6 0.709J 15.2 52.8 0.607J <0.106 0.0390J CS-8 0-2'11/14/22 5.57 37.8 <0.101 13.1 15.8 0.876J <0.102 0.0458J 3 47,000 20 6.5 800 1,200 1,200 70 0.68 3,100 1.4 0.31 250 78 78 4.7 5.8 580 3 3.8 270 2.1 3.4 NL Units in milligrams per kilogram (mg/kg) <X.X = Less than the Method Detection Limit (MDL) shown NL = Not listed, No PSRG established RHB-PSRG = NCDEQ Residential Health Based PSRGs (January 2023) PG-PSRG = NCDEQ Protection of Groundwater PSRGs (January 2023) Pink shading indicates exceedance of Industrial/Commercial PSRG Orange shading indicates exceedance of Residential PSRG, but not the Industrial PSRG Yellow shading indicates exceedance of Protection of Groundwater PSRG Qualifiers B = The same analyte is found in the associate blank J = The indentification of the analyte is acceptable; the reported value is an estimate I/CHB-PSRG = NCDEQ Industrial/Commercial Health Based Preliminary Soil Remediation Goals (PSRGs) (January 2023) RHB-PSRG I/CHB-PSRG PG-PSRG Table 1A Soil Metal Detections (mg/kg) 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 Soil IDDepth (Ft)Date SampledAcenaphtheneAcenaphthyleneAnthraceneBenzidineBenzo(a)anthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(g,h,i)peryleneBenzo(a)pyreneChryseneDibenz(a,h)anthracene1,2-Dichlorobenzene3,3-DichlorobenzidineFluorantheneFluoreneHexachlorocyclopentadieneIndeno(1,2,3-cd)pyreneNaphthalenen-NitrosodimethylaminePhenanthreneBis(2-ethylhexyl)phthalateDi-n-butyl phthalatePyrene2,4-DimethylphenolSS-1 0-1'11/10/22 <0.00664 <0.00578 <0.00731 <0.0771C3 0.00876J 0.0185J <0.00729 0.00929J 0.0139J 0.0128J <0.0114 <0.0122 <0.0152 0.0191J <0.00668 <0.0216 <0.0116 <0.0103 <0.0609 0.0101J <0.0520 <0.0140 0.0182J <0.0107 SS-1-a 4-5'11/10/22 <0.00619 <0.00538 <0.00681 <0.0719C3 <0.00674 <0.00713 <0.00680 <0.00699 <0.00711 <0.00760 <0.0106 <0.0113 <0.0141 <0.00690 <0.00622 <0.0135 <0.0108 <0.00960 <0.0567 <0.00759 <0.0484 <0.0131 <0.00744 <0.00999SS-2 0-1'11/10/22 <0.00738 <0.00642 <0.00812 <0.0857C3 <0.00803 0.0155J <0.00810 <0.00834 0.0106J 0.0118J <0.0126 <0.0135 <0.0168 0.0175J <0.00742 <0.0240 <0.0129 0.0840 <0.0676 0.0133J <0.0578 <0.0156 0.0162J <0.0119SS-2 (DUP)0-1'11/10/22 <0.00712 <0.00619 <0.00783 <0.0827C3 0.00791J 0.0161J <0.00782 <0.00804 0.0111J 0.0112J <0.0122 <0.0130 <0.0162 0.0178J <0.00716 <0.0231 <0.0124 <0.0110 <0.0653 0.00910J <0.0557 <0.0151 0.0162J <0.0115SS-2-a 4-5'11/10/22 <0.00705 <0.00614 <0.00776 <0.0819C3 <0.00768 <0.00812 <0.00775 <0.00797 <0.00810 <0.00866 <0.0121 <0.0129 <0.0161 <0.00786 <0.00709 <0.0229 <0.0123 <0.0109 <0.0646 <0.00865 <0.0552 <0.0149 <0.00848 <0.0114 SS-2-a (DUP)4-5'11/10/22 <0.00702 <0.00611 <0.00773 <0.0816C3 J6 <0.00765 <0.00809 <0.00771 <0.00794 <0.00807 <0.00863 <0.0120 <0.0129 <0.0160 <0.00783 <0.00706 <0.0228 <0.0123 <0.0109 <0.0644 <0.00861 <0.0550 <0.0149 <0.00844 <0.0113 SS-3 0-1'11/10/22 <0.00656 <0.00571 <0.00721 <0.0762C3 <0.00714 <0.00756 <0.00720 <0.00741 <0.00753 <0.00805 <0.0112 <0.0120 <0.0150 <0.00731 <0.00659 <0.0213 <0.0114 <0.0102 <0.0601 <0.00804 0.0811J <0.0139 <0.00788 <0.0106 SS-3 (DUP)0-1'11/10/22 <0.00815 <0.00709 <0.00897 <0.0947C3 <0.00888 <0.00939 <0.00895 <0.00921 <0.00936 <0.0100 <0.0140 <0.0149 <0.0186 <0.00909 <0.00820 <0.0265 <0.0142 <0.0126 <0.0747 <0.0100 <0.0638 <0.0172 <0.00980 <0.0132SS-3-a 4-5'11/10/22 <0.00596 <0.00519 <0.00656 <0.0693C3 <0.00649 <0.00687 <0.00655 <0.00674 <0.00685 <0.00732 <0.0102 <0.0109 <0.0136 <0.00665 <0.00600 <0.0194 <0.0104 <0.00925 <0.0546 <0.00731 0.0481J <0.0126 <0.00717 <0.00962SS-3-a (DUP)4-5'11/10/22 <0.00804 <0.00700 <0.00885 <0.0934C3 <0.00876 <0.00927 <0.00883 <0.00909 <0.00924 <0.00988 <0.0138 0.0273J <0.0184 <0.00897 <0.00809 <0.0261 <0.0140 <0.0125 <0.0737 <0.00986 <0.0630 <0.0170 <0.00967 <0.0130SS-4 0-1'11/10/22 <0.00753 <0.00655 <0.00828 <0.0874C3 <0.00820 <0.00867 <0.00827 <0.00850 <0.00864 <0.00924 <0.0129 <0.0138 <0.0172 <0.00839 <0.00757 <0.0244 <0.0131 <0.0117 <0.0690 <0.00923 <0.0589 <0.0159 <0.00905 <0.0121SS-4-a 4-5'11/10/22 <0.00905 <0.00788 <0.00996 <0.105C3 <0.00986 <0.0104 <0.00994 <0.0102 <0.0104 <0.0111 <0.0155 <0.0166 <0.0207 <0.0101 <0.00910 <0.0294 <0.0158 <0.0140 <0.0830 <0.0111 <0.0709 <0.0191 <0.0109 <0.0146 SS-5 0-1'11/10/22 <0.00794 <0.00691 <0.00873 <0.0922C3 <0.00864 <0.00915 <0.00872 <0.00897 <0.00912 <0.00975 <0.0136 <0.0145 <0.0181 <0.00885 <0.00798 <0.0258 <0.0139 <0.0123 <0.0728 <0.00973 <0.0621 <0.0168 <0.00954 <0.0128 SS-5-a 4-5'11/10/22 0.00759J <0.00624 <0.00789 <0.0832C3 <0.00781 <0.00826 <0.00787 <0.00810 <0.00823 <0.00880 <0.0123 <0.0131 <0.0164 <0.00799 0.00812J <0.0233 <0.0125 0.0863 <0.0657 0.0146J <0.0561 <0.0152 <0.00862 <0.0116 SS-6 0-1'11/10/22 <0.00788 <0.00686 <0.00867 <0.0915C3 <0.00858 <0.00908 <0.00866 <0.00891 <0.00905 <0.00968 <0.0135 <0.0144 <0.0180 <0.00879 <0.00793 <0.0256 <0.0138 <0.0122 <0.0722 <0.00967 <0.0617 <0.0167 <0.00948 <0.0127SS-6-a 4-5'11/10/22 <0.00650 <0.00565 <0.00715 <0.0755C3 <0.00707 <0.00748 <0.00714 <0.00734 <0.00746 <0.00798 <0.0111 <0.0119 <0.0148 <0.00724 <0.00653 <0.0211 <0.0113 <0.0101 <0.0595 <0.00797 <0.0509 <0.0137 <0.00781 <0.0105SS-7 0-1'11/10/22 0.971 0.0445 1.51 <0.0794C3 3.77 4.54 0.888 0.768 3.31 3.30 0.238 <0.0125 <0.0156 9.40 0.774 <0.0222 1.01 0.416 <0.0626 8.08 <0.0535 <0.0145 6.59 <0.0110SS-7-a 4-5'11/10/22 <0.00667 <0.00581 <0.00734 <0.0775C3 <0.00727 <0.00769 <0.00733 <0.00754 <0.00766 <0.00820 <0.0114 <0.0122 <0.0152 <0.00744 <0.00671 <0.0217 <0.0117 <0.0104 <0.0612 <0.00818 <0.0522 <0.0141 <0.00802 <0.0108 SS-8 0-1'11/10/22 <0.00744 <0.00648 <0.00819 <0.0865C3 0.00977J 0.0225J <0.00818 0.0111J 0.0138J 0.0142J <0.0127 <0.0136 <0.0170 0.0246J <0.00749 <0.0242 <0.0130 <0.0115 <0.0682 0.0101J <0.0583 <0.0157 0.0227J <0.0120 SS-8-a 4-5'11/10/22 <0.00612 <0.00533 <0.00673 <0.0711C3 <0.00667 <0.00705 <0.00672 <0.00692 <0.00703 <0.00752 <0.0105 <0.0112 <0.0140 <0.00682 <0.00615 <0.0199 <0.0107 <0.00949 <0.0561 <0.00751 <0.0479 <0.0129 <0.00736 <0.00988 CS-1 0-2'11/14/22 <0.00783 <0.00681 <0.00861 <0.0909C3 0.00894J 0.0170J <0.00859 <0.00884 0.00968J <0.00961 <0.0134 <0.0143 <0.0179 0.0190J <0.00787 <0.0254 <0.0137 <0.0121 <0.0717C3 0.0132J <0.0613 0.0189J 0.0179J <0.0126C3CS-2 0-2'11/14/22 <0.00678 <0.00590 <0.00746 <0.0787 0.00951J 0.0184J <0.00744 <0.00766 0.0136J 0.0110J <0.0116 <0.0124 <0.0155 0.0205J <0.00682 <0.0220 <0.0118 <0.0105 <0.0621 0.0111J <0.0531 <0.0143 0.0200J <0.0109 CS-3 0-2'11/14/22 <0.00656 0.0105J <0.00722 <0.0762 0.0241J 0.0488 0.0156J 0.0293J 0.0353J 0.0319J <0.0112 <0.0120 <0.0150 0.0548 <0.00660 <0.0213 0.0312J <0.0102 <0.0601 0.0313J <0.0514 0.0173J 0.0469 <0.0106 CS-4 2-3'11/14/22 <0.00679 <0.00591 <0.00748 <0.0789 <0.00740 <0.00783 <0.00746 <0.00768 <0.00780 <0.00835 <0.0116 <0.0124 <0.0155 <0.00758 <0.00683 <0.0221 <0.0119 <0.0105 <0.0623 <0.00833 <0.0532 <0.0144 <0.00817 <0.0110 CS-4-a 6-7'11/14/22 <0.00814 <0.00709 <0.00896 <0.0946 <0.00887 <0.00938 <0.00895 <0.00920 <0.00935 <0.0100 <0.0139 <0.0149 <0.0186 <0.00908 <0.00819 <0.0264 <0.0142 <0.0126 <0.0746 <0.00999 <0.0638 <0.0172 <0.00979 <0.0131 CS-5 0-1'11/14/22 0.103 2.07 0.629 <0.167 1.75 6.95 1.46 1.84 5.12 2.04 0.604 <0.0263 <0.0329 2.16 0.152 <0.0468 2.36 0.220 <0.132 0.757 <0.113 <0.0305 2.63 <0.0232 CS-5 (DUP)0-1'11/14/22 0.0512J 0.0677J 0.105 <0.150 0.280 0.390 0.127 0.101 0.286 0.291 0.0315J <0.0236 <0.0294 0.581 0.0434J <0.0419 0.122 0.0230J <0.118 0.416 <0.101 <0.0273 0.484 <0.0208 CS-6 0-1'11/14/22 0.0644J 0.496 0.340 <0.156J6 1.09J6 1.73J6 0.494 0.831J3 J6 1.53J6 1.32J6 0.243 <0.0245 <0.0306J3 1.47J6 0.189 <0.0436J6 0.882J6 0.167 <0.123 1.54J6 <0.105 <0.0284 1.94J6 <0.0217 CS-6-a 1-2.5'11/14/22 0.0200J 0.252 0.135 <0.149 0.519 0.789 0.274 0.313 0.711 0.645 0.0937 <0.0235 <0.0293 0.771 0.0612J <0.0417 0.346 0.0361J <0.118 0.606 <0.100 <0.0271 0.981 <0.0207 CS-7 0-2'11/14/22 <0.00658 0.00917J <0.00724 <0.0764 0.0354J 0.0580 0.0186J 0.0297J 0.0408 0.0446 <0.0113 <0.0121 <0.0150 0.0708 <0.00662 <0.0214 0.0286J <0.0102 <0.0603 0.0379J <0.0515 <0.0139 0.0624 <0.0106 CS-8 0-2'11/14/22 <0.00636 0.0114J <0.00699 <0.0738 0.0202J 0.0493 0.0143J 0.0269J 0.0304J 0.0269J <0.0109 <0.0116 <0.0145 0.0525 <0.00639 <0.0206 0.0278J <0.00986 <0.0583 0.0213J <0.0498 <0.0134 0.0479 <0.0103 9,000 NL 45,000 0.01 21 21 210 NL 2.1 2,100 2.1 2,000 5.1 6,000 6,000 1.60 21 8.8 0.035 NL 160 16000 4,500 3,300 720 NL 3,600 0.00053 1.1 1.1 11 NL 0.11 110 0.11 380 1.2 480 480 0.38 1.1 2.1 0.002 NL 39 1300 360 250 16 NL 1,300 0.0000079 0.35 1.2 12 NL 0.12 36 0.38 0.39 0.01 670 110 2.6 3.9 0.39 0.0000034 NL 14 35 440 2.4Units in milligrams per kilogram (mg/kg) <X.X = Less than the Method Detection Limit (MDL) shownNL= Not listed, No PSRG established I/CHB-PSRG = NCDEQ Industrial/Commercial Health Based Preliminary Soil Remediation Goals (PSRGs) (January 2023) RHB-PSRG = NCDEQ Residential Health Based PSRGs (January 2023) PG-PSRG = NCDEQ Protection of Groundwater PSRGs (January 2023) Pink shading indicates exceedance of Industrial/Commercial PSRG Orange shading indicates exceedance of Residential PSRG, but not the Industrial PSRGYellow shading indicates exceedance of Protection of Groundwater PSRG QualifiersC3 = The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptableJ = The indentification of the analyte is acceptable; the reported value is an estimate J3 = The associated batch QC was outside the established quality control range for precisionJ6 = The sample matrix interfered with the ability to make any accurate determination; spike value is low PG-PSRG I/CHB-PSRG RHB-PSRG SVOCs Table 1B(a) Soil Organic Detections (SVOCs) mg/kg 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 Soil IDDepth (Ft)Date SampledAcetoneAcrylonitrileBenzeneBromodichloromethaneBromomethanesec-Butylbenzenetert-ButylbenzeneChlorodibromomethaneChloroethaneChloroformChloromethane4-Chlorotoluene1,2-Dibromo-3-ChloropropaneDibromomethane1,4-DichlorobenzeneDichlorodifluoromethanecis-1,3-Dichloropropene2,2-DichloropropaneEthylbenzeneIsopropylbenzene (Cumene)p-Isopropyltoluene4-Methyl-2-pentanone (MIBK)Naphthalenen-PropylbenzeneStyrene1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-TrichloroethaneTrichlorofluoromethane1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneVinyl chlorideXylenes, TotalSS-1 0-1'11/10/22 <0.0588 <0.00581 <0.000752 <0.00117 <0.00318 <0.00465 <0.00314C3 <0.000338 <0.00273 <0.00165 <0.00701 <0.000725 <0.00629C3 <0.00121 <0.00113 <0.00259 <0.00122J4 <0.00223 <0.00119 <0.000685 <0.00411 <0.00367 <0.00787 <0.00152 <0.000368 <0.00112 0.00608 0.00757J <0.0118 <0.00709 <0.00148 <0.00133 <0.00255 <0.00322 <0.00187 0.00613B JSS-1-a 4-5'11/10/22 <0.0478 <0.00473 <0.000611 <0.000949 <0.00258 <0.00377 <0.00255C3 <0.000801 <0.00223 <0.00135 <0.00570 <0.000589 <0.00511C3 <0.000982 <0.000917 <0.00211 <0.000991J4 <0.00181 <0.000965 <0.000556 0.00831 <0.00299 <0.00639 <0.00124 <0.000300 <0.000910 0.00329 <0.00170 <0.00960 <0.00576 <0.00121 <0.00108 <0.00207 <0.00262 <0.00152 <0.00115 SS-2 0-1'11/10/22 <0.0646 <0.00639 <0.000826 <0.00128 <0.00348 <0.00509 <0.00345C3 <0.00108 <0.00301 <0.00182 <0.00770 <0.000796 <0.00690C3 <0.00133 <0.00124 <0.00285 <0.00134J4 <0.00244 0.00200B J <0.000752 0.00716J <0.00403 <0.00863 <0.00168 <0.000405 <0.00123 <0.00159 <0.00230 <0.0130 <0.00778 <0.00163 <0.00146 <0.00279 <0.00354 <0.00205 0.00188B JSS-2 (DUP)0-1'11/10/22 <0.0607J3 J4 <0.00600J3 <0.000776 <0.00120 <0.00327 <0.00479 <0.00324 <0.00102C3 <0.00283 <0.00171 <0.00723 <0.000748 <0.00648J3 <0.00125 <0.00116 <0.00268 <0.00126 <0.00229 <0.00122 <0.000706 0.00789J <0.00379 <0.00811J3 <0.00158 <0.000381 <0.00116C3 <0.00149 <0.00216 <0.0122C4 <0.00731J3 <0.00153 <0.00137 <0.00263 <0.00332 <0.00193 <0.00146 SS-2-a 4-5'11/10/22 <0.0652 <0.00645 <0.000835 <0.00130 <0.00353 <0.00514 <0.00348 <0.00109 <0.00304 <0.00183 <0.00778 <0.000805 <0.00697C3 <0.00134 <0.00125 <0.00288 <0.00135J4 <0.00247 <0.00132 <0.000759 <0.00455 <0.00408 <0.00871 <0.00169 <0.000410 <0.00124 0.00558 <0.00232 <0.0131 <0.00786 <0.00164 <0.00148 <0.00283 <0.00357 <0.00207 <0.00157 SS-2-a (DUP)4-5'11/10/22 <0.0606J3 J4 <0.00598J3 <0.000775 <0.00120 <0.00327 <0.00478 <0.00324 <0.00101C3 <0.00282 <0.00171 <0.00721 <0.000746 <0.00647J3 <0.00124 <0.00116 <0.00266 <0.00125 <0.00230 <0.00122 <0.000705 <0.00422 <0.00378 <0.00810J3 <0.00157 <0.000379 <0.00115C3 <0.00149 <0.00215 <0.0121C4 <0.00730J3 <0.00153 <0.00137 <0.00261 <0.00332 <0.00193 <0.00146 SS-3 0-1'11/10/22 <0.0528 <0.00522 <0.000675 <0.00105 <0.00285 <0.00416 <0.00282C3 <0.000885 <0.00246 <0.00149 <0.00629 <0.000651 <0.00564C3 <0.00108 <0.00101 <0.00233 <0.00109J4 <0.00199 <0.00107 <0.000614 0.00704J <0.00330 <0.00705 <0.00137 <0.000331 <0.00100 0.00422 <0.00188 <0.0106 <0.00636 <0.00133 <0.00120 <0.00228 <0.00289 <0.00168 <0.00127 SS-3 (DUP)0-1'11/10/22 <0.0745J3 J4 <0.00737J3 <0.000953 <0.00148 <0.00402 <0.00587 <0.00398 <0.00125C3 <0.00347 <0.00210 <0.00886 <0.000918 <0.00795J3 <0.00153 <0.00143 <0.00329 <0.00154 <0.00281 <0.00150 <0.000866 <0.00521 <0.00464 <0.00995J3 <0.00194 <0.000466 <0.00142 C3 <0.00183 <0.00264 <0.0149C4 <0.00896J3 <0.00188 <0.00169 <0.00323 <0.00408 <0.00236 <0.00179 SS-3-a 4-5'11/10/22 <0.0523 <0.00517 <0.000669 <0.00104 <0.00282 <0.00413 <0.00280C3 <0.000877 <0.00244 <0.00148 <0.00624 <0.000645 <0.00559C3 <0.00108 <0.00100 <0.00231 <0.00108J4 <0.00198 <0.00106 0.00086J 0.00724 <0.00327 <0.00700 <0.00136 <0.000329 <0.000996 0.00484 <0.00186 <0.0105 <0.00631 <0.00133 <0.00119 <0.00227 <0.00287 <0.00166 <0.00127 SS-3-a (DUP)4-5'11/10/22 <0.0727J3 J4 <0.00719J3 <0.000930 <0.00144 <0.00392 <0.00574 <0.00388 <0.00122C3 <0.00339 <0.00205 <0.00866 <0.000896 <0.00777J3 <0.00149 <0.00139 <0.00321 <0.00151 <0.00275 <0.00147 0.000928J <0.00508 <0.00454 <0.00972J3 <0.00189 <0.000456 <0.00138C3 <0.00178 <0.00259 <0.0146C4 <0.00876J3 <0.00184 <0.00165 <0.00315 <0.00398 <0.00231 <0.00175 SS-4 0-1'11/10/22 <0.0686 <0.00679 <0.000877 <0.00136 <0.00370 0.00583B J <0.00367C3 <0.00115 <0.00319 <0.00193 <0.00817 <0.000845 <0.00732C3 <0.00141 <0.00131 <0.00303 <0.00142J4 <0.00259 <0.00138 0.000939J <0.00478 <0.00429 <0.00916 <0.00179 <0.000431 <0.00131 0.00446J <0.00245 <0.0138 <0.00826 <0.00173 <0.00155 <0.00296 <0.00376 <0.00218 <0.00165 SS-4-a 4-5'11/10/22 <0.0872 <0.00862 <0.00112 <0.00173 <0.00471 <0.00689 <0.00466 <0.00146 <0.00405 <0.00246 <0.0104 <0.00108 <0.00933C3 <0.00179 <0.00167 <0.00384 <0.00181J4 <0.00330 <0.00176 <0.00101 <0.00609 <0.00546 <0.0117 <0.00227 <0.000548 <0.00166 0.00855 0.00377J <0.0175 <0.0105 <0.00221 <0.00198 <0.00377 <0.00478 <0.00277 <0.00210 SS-5 0-1'11/10/22 <0.0730 <0.00722 <0.000934 <0.00145 <0.00394 <0.00576 <0.00390C3 <0.00122 <0.00340 <0.00206 <0.00870 <0.000900 <0.00780C3 <0.00150 <0.00140 <0.00322 <0.00151J4 <0.00276 <0.00147 0.00135J 0.00518J <0.00456 <0.00976 <0.00190 <0.000458 <0.00139 0.00526 <0.00260 <0.0147 <0.00880 <0.00185 <0.00165 <0.00316 <0.00400 <0.00232 <0.00176 SS-5-a 4-5'11/10/22 <0.0612 <0.00605 <0.000783 <0.00121 <0.00330 <0.00483 <0.00327C3 <0.00103 <0.00285 <0.00173 <0.00729 <0.000754 <0.00654C3 <0.00126 <0.00117 <0.00270 <0.00127J4 <0.00231 <0.00124 0.00127J <0.00427 <0.00382 <0.00818 <0.00159 <0.000384 <0.00116 0.00414J <0.00218 <0.0123 <0.00737 <0.00155 <0.00139 <0.00265 <0.00335 <0.00194 <0.00147 SS-6 0-1'11/10/22 <0.0734 <0.00726 <0.000940 <0.00146 <0.00396 <0.00580 <0.00392C3 <0.00123 <0.00342 <0.00207 <0.00875 <0.000905 <0.00785C3 <0.00151 <0.00141 <0.00324 <0.00152J4 <0.00278 <0.00148 <0.000855 <0.00513 <0.00459 <0.00982 <0.00191 <0.000461 <0.00140 0.00384J <0.00262 <0.0147 <0.00885 <0.00186 <0.00166 <0.00318 <0.00402 <0.00233 <0.00177 SS-6-a 4-5'11/10/22 <0.0524 <0.00519 <0.000671 <0.00104 <0.00283 <0.00414 <0.00280C3 <0.000879 <0.00244 <0.00148 <0.00625 <0.000646 <0.00560C3 <0.00108 <0.00101 <0.00231 <0.00109J4 <0.00198 <0.00106 <0.000611 0.00460J <0.00328 <0.00701 <0.00136 <0.000329 <0.000998 0.00521 <0.00187 <0.0105 <0.00632 <0.00133 <0.00119 <0.00227 <0.00287 <0.00167 <0.00126 SS-7 0-1'11/10/22 <0.0572 <0.00566 <0.000732 <0.00114 <0.00309 0.00477B J <0.00306C3 <0.000959 <0.00266 <0.00161 <0.00682 <0.000705 <0.00611C3 <0.00118 <0.00110 <0.00252 <0.00119J4 <0.00216 <0.00116 <0.000666 0.00547J <0.00357 <0.00765 <0.00149 <0.000359 <0.00109 <0.00140 0.00215J <0.0115 <0.00690 <0.00145 <0.00130 <0.00248 <0.00314 <0.00182 <0.00138 SS-7-a 4-5'11/10/22 <0.0562J3 J4 <0.00566J3 <0.000719 <0.00112 <0.00303 <0.00443 <0.00300 <0.000942C3 <0.00262 <0.00159 <0.00670 <0.000693 <0.00600J3 <0.00115 <0.00108 <0.00248 <0.00117 <0.00212 <0.00113 <0.000654 <0.00393 <0.00351 <0.00751J3 <0.00146 <0.000353 <0.00107C3 <0.00138 <0.00200 <0.0113C4 <0.00677J3 <0.00142 <0.00127 <0.00243 <0.00308 <0.00179 <0.00135 SS-8 0-1'11/10/22 0.123C5 J3 J4 <0.00745J3 <0.000965 <0.00150 <0.00406 <0.00594 <0.00403 <0.00126C3 <0.00350 <0.00213 <0.00899 <0.000930 <0.00806J3 <0.00155 <0.00145 <0.00332 <0.00156 <0.00284 <0.00152 <0.000879 <0.00527 0.00527J <0.0101J3 <0.00196 <0.000472 <0.00144C3 <0.00185 <0.00269 <0.0151C4 <0.00909J3 <0.00191 <0.00171 <0.00327 <0.00413 <0.00240 0.00181JSS-8-a 4-5'11/10/22 <0.0509J3 J4 <0.00504J3 <0.000651 <0.00101 <0.00275 <0.00402 <0.00272 <0.000854C3 <0.00238 <0.00143 <0.00607 <0.000629 <0.00544J3 <0.00105 <0.000977 <0.00225 <0.00106 <0.00192 <0.00103 <0.000593 <0.00356 <0.00318 <0.00681J3 <0.00132 <0.000319 <0.000969C3 <0.00125 <0.00181 <0.0102C4 <0.00614J3 <0.00128 <0.00115 <0.00220 <0.00279 <0.00162 <0.00123 CS-1 0-2'11/14/22 <0.0827 <0.00818 0.00296 <0.00164J4 <0.00446 <0.00653J4 <0.00443 <0.00139 <0.00385 0.00760 <0.00987 <0.00102J4 <0.00885 <0.00170J40.00221B J <0.00365 <0.00114 <0.00314 <0.00167 0.00113B J J4 0.0170 <0.00517 <0.0111 <0.00216J4 0.00192B J <0.00158 <0.00203 0.0229 <0.0166C4 <0.00998 <0.00209J4 <0.00187 0.00403J <0.00454J4 <0.00263 0.0158CS-2 0-2'11/14/22 <0.0562 <0.00556 <0.000719 <0.00112 <0.00303C3 <0.00444 <0.00300 <0.000942 <0.00261C3 J4 0.00400 <0.00670C3 <0.000693 <0.00601 <0.00116 <0.00108 <0.00248C3 <0.00117 <0.00213C3 <0.00114 <0.000654 <0.00393 <0.00352 <0.00752 <0.00146 <0.000353 <0.00107 <0.00138 <0.00201 <0.0113 <0.00678J4 <0.00142 <0.00127C3 <0.00243 <0.00308 <0.00178C3 J4 0.00139JCS-3 0-2'11/14/22 <0.0537 <0.00532 <0.000687 <0.00107 <0.00290C3 <0.00424 <0.00287 <0.000900 <0.00250C3 J4 0.00357J <0.00640C3 <0.000663 <0.00575 <0.00110 <0.00103 <0.00237C3 <0.00111 <0.00203C3 <0.00108 <0.000626 <0.00376 <0.00336 <0.00719 <0.00140 <0.000337 <0.00102 <0.00132 <0.00192 <0.0108 <0.00647J4 <0.00136 <0.00122C3 <0.00233 <0.00294 <0.00170C3 J4 0.00180JCS-4 2-3'11/14/22 <0.0562 <0.00556 <0.000719 <0.00112 <0.00303C3 <0.00443 <0.00300 <0.000942 <0.00262C3 J4 0.00416 <0.00670C3 <0.000693 <0.00600 <0.00115 <0.00108 <0.00248C3 <0.00117 <0.00212C3 <0.00113 <0.000654 <0.00393 <0.00351 <0.00751 <0.00146 <0.000352 <0.00107 <0.00138 <0.00200 <0.0113 <0.00677J4 <0.00142 <0.00127C3 <0.00243 <0.00308 <0.00179C3 J4 0.00369JCS-4-a 6-7'11/14/22 <0.0740 <0.00732 <0.000946 <0.00147 <0.00399C3 <0.00584 <0.00395 <0.00124 <0.00344C3 J4 0.00496J <0.00881C3 <0.000912 <0.00790 <0.00152 <0.00142 <0.00326C3 <0.00153 <0.00280C3 <0.00149 <0.000861 <0.00517 <0.00462 <0.00989 <0.00193 <0.000464 <0.00141 <0.00182 0.00306J <0.0149 <0.00892J4 <0.00187 <0.00168C3 <0.00320 <0.00405 <0.00235C3 J4 <0.00178CS-5 0-1'11/14/22 <0.0645 <0.00637 <0.000825 <0.00128 <0.00348C3 <0.00508 <0.00345 <0.00108 <0.00300C3 J4 0.00459 <0.00767C3 <0.000793 <0.00688 <0.00132 <0.00124 <0.00284C3 <0.00134 <0.00244C3 <0.00130 0.000838J <0.00450 <0.00402 <0.00861 <0.00168 <0.000404 <0.00123 <0.00158 0.00261J <0.0129 <0.00777J4 <0.00163 <0.00146C3 <0.00279 <0.00353 <0.00205C3 J4 0.00238JCS-5 (DUP)0-1'11/14/22 <0.0509 <0.00504 <0.000651 <0.00101 <0.00275C3 <0.00402 <0.00272 <0.000854 <0.00237C3 J4 0.00321J <0.00607C3 <0.000628 <0.00544 <0.00105 <0.000976 <0.00225C3 0.00106 <0.00192C3 <0.00103 <0.000593 <0.00356 <0.00318 <0.00681 <0.00133 <0.000319 <0.000969 <0.00125 0.00232J <0.0102 <0.00614J4 <0.00129 <0.00115C3 <0.00220 <0.00279 <0.00162C3 J4 0.00487JCS-6 0-1'11/14/22 <0.0559 <0.00553 <0.000716 <0.00111 <0.00302C3 <0.00441 <0.00299 <0.000938 <0.00260C3 J4 0.00332J <0.00667C3 <0.000689 <0.00598 <0.00115 <0.00107 <0.00247C3 <0.00112 <0.00211C3 <0.00113 <0.000651 <0.00391 <0.00349 0.00834J <0.00146 <0.000351 <0.00106 <0.00137 0.00277J <0.0112 <0.00674J4 <0.00141 <0.00127C3 <0.00242 <0.00306 <0.00178C3 J4 0.00218JCS-6-a 1-2.5'11/14/22 0.154 <0.00509 <0.000659 <0.00102 <0.00278C3 <0.00406 <0.00275 <0.000863 <0.00240C3 J4 0.00346J <0.00614C3 <0.000635 <0.00550 <0.00106 <0.000988 <0.00227C3 <0.00104 <0.00195C3 0.00133J <0.000600 <0.00360 <0.00322 <0.00688 <0.00134 <0.000323 <0.000980 <0.00126 0.00219J <0.0103 <0.00621J4 <0.00130 <0.00117C3 <0.00223 <0.00282 <0.00164C3 J4 0.00161JCS-7 0-2'11/14/22 <0.0533 <0.00527 <0.000682 <0.00106 <0.00288C3 <0.00420 <0.00285 <0.000894 <0.00248C3 J4 0.00387 <0.00635C3 <0.000657 <0.00569 <0.00109 <0.00102 <0.00235C3 <0.00111 <0.00201C3 <0.00108 <0.000620 <0.00372 <0.00333 <0.00712 <0.00139 <0.000334 <0.00101 <0.00131 0.00274J <0.0107 <0.00642J4 <0.00135 <0.00121C3 <0.00231 <0.00292 <0.00169C3 J4 0.00206JCS-8 0-2'11/14/22 <0.0496 <0.00490 <0.000634 <0.000985 <0.00268C3 <0.00391 <0.00265 <0.000832 <0.00231C3 J4 0.00435 <0.00591C3 <0.000611 <0.00530 <0.00102 <0.000951<0.00219C3 <0.00103 <0.00187C3 <0.00100 0.000679J <0.00346 <0.00310 <0.00663 <0.00129 0.000781B J <0.000944 <0.00122 <0.00177 <0.00996 <0.00598J4 <0.00125 <0.00112C3 <0.00215 <0.00272 <0.00158C3 J4 <0.00120210,000 1.2 5.4 1.4 6.4 23,000 23,000 39 4,800 1.5 99 4,700 0.068 21 12 78 8.6 NL 27 2,100 NL 30,000 8.8 5,100 7,300 2.8 82 9,700 190 55 7,600 70,000 370 320 1.7 530 14,000 0.27 1.2 0.31 1.4 1,600 1,600 8.3 1,100 0.34 23 310 0.0056 5 2.8 18 1.9 NL 6.1 410 NL 7,000 2.1 780 1,200 0.64 17 990 13 12 1,700 4,700 63 56 0.061 12025 0.00028 0.01 0.0033 0.05 4.1 3.1 0.0021 17 0.39 0.015 0.46 0.00035 0.34 0.12 30 0.0029 NL 13 2.3 NL 0.45 0.39 2.6 1.5 0.0016 0.0063 8.3 0.33 4.1 1.4 25 12 11 0.00021 9.9Units in milligrams per kilogram (mg/kg)<X.X = Less than the Method Detection Limit (MDL) shownNL= Not listed, No PSRG established I/CHB-PSRG = NCDEQ Industrial/Commercial Health Based Preliminary Soil Remediation Goals (PSRGs) (January 2023)RHB-PSRG = NCDEQ Residential Health Based PSRGs (January 2023)PG-PSRG = NCDEQ Protection of Groundwater PSRGs (January 2023)Yellow shading indicates exceedance of Protection of Groundwater PSRG QualifiersB = The same analyte is found in the associate blankC3 = The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptableC4 = The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Data is likely to show a low bias concerning the result C5 = The reported concentration is an estimate. The continuing calibration standard with this data responded high. Data is likely to how a high bias concerning the result.J = The indentification of the analyte is acceptable; the reported value is an estimateJ3 = The associated batch QC was outside the established quality control range for precisionJ4 = The associated batch QC was outside the established quality control range for precision PG-PSRG Table 1B(b)Soil Organic Detections (VOCs) mg/kg 450 POLO ROAD PROPERTY, WINSTON-SALEM, NCBROWNFIELDS PROJECT NO. 25052-21-034 VOCs I/CHB-PSRG RHB-PSRG Sample IDDate SampledArsenicBariumCadmiumChromiumLeadSeleniumSilverMercuryMW-1 12/12/22 0.656B J 94.7 <0.150 <1.24 2.58 1.74B J <0.0700 <0.100 MW-2 12/13/22 2.11 127 <0.150 13.4 38.8 <0.300 <0.0700 1.29 MW-3 12/13/22 22.8 420 0.271J 19.3 239 3.32 0.109J 1.67 Dup-1 (MW-3)12/13/22 13.7 201 0.211J 12.6 119 1.66J 0.0957J 0.86 MW-4 12/13/22 14.1 854 0.427J 18.8 91.8 7.71 0.116J <0.100 MW-5 12/13/22 12.1 746 0.272J 7.57J 65.3 7.71 <0.0700 <0.100 MW-6 12/13/22 8.99J 224 0.265J 8.55J 40.5 5.22 <0.0700 <0.100 10 700 2 10 15 20 20 1 Units in micrograms per liter (µg/L) <X.X = Less than the Method Detection Limit (MDL) shown NL= Not listed, No Standard established Pink shading indicates exceedance of 2L Standard Qualifiers B = The same analyte is found in the associate blank J = The indentification of the analyte is acceptable; the reported value is an estimate 15A NCAC 2L Standard = 15A North Carolina Administrative Code (NCAC) 02L.0202 Groundwater Standards (2L Standards) (April 1, 2022) 15A NCAC 2L Standard Table 1C Groundwater Metal Detections (µg/L) 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 Soil IDDate SampledBenzidineNaphthalenen-NitrosodiphenylaminePhenanthrene2,4-Dimethylphenol4-NitrophenolAcetoneAcroleinBenzenen-Butylbenzenesec-Butylbenzene2-Chloroethyl vinyl etherChloroform1,2-Dibromoethane1,2-Dichloroethanecis-1,2-DichloroetheneDi-isopropyl etherEthylbenzeneHexachloro-1,3-butadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanone (MIBK)Methyl tert-butyl etherNaphthalenen-PropylbenzeneTetrachloroetheneToluene1,2,3-Trichlorobenzene1,2,4-TrichlorobenzeneTrichloroethene1,2,3-Trimethylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes, TotalMW-1 12/12/22 <3.74J4 0.373J <2.37 <0.112 <0.0636 <0.143J4 <11.3 <2.54C3 <0.0941 <0.157 <0.125 <0.575 <0.111 <0.126 <0.0819 <0.126 <0.105 <0.137 <0.337C3 <0.105 <0.120 <0.478 <0.101 <1.00C3 <0.0993 <0.300 <0.278 <0.230 <0.481C3 <0.190 <0.104 <0.322 <0.104 <0.174 MW-2 12/13/22 <3.74J4 <0.159 <2.37 <0.112 <0.0636 <0.143 <11.3J3 <2.54 0.205J <0.157 <0.125 <0.575 0.825J <0.126 0.21J <0.126 0.125J 0.187J <0.337J3 <0.105 <0.120 <0.478 <0.101 <1.00J3 0.133J 0.409J 0.852J <0.230J3 <0.481J3 0.241J 0.285J < 0.322 0.251J 0.661J MW-3 12/13/22 <3.74J4 11.9 <2.37 0.117J 0.881J <0.143 15.8J J3 <2.54 772 2.48 2.31 0.667J <0.111 29.4 97.1 0.186J 15.5 304 <0.337J3 15.7 1.15 8.15J <0.101 40.7J3 34.5 20.6 2330 <0.230J3 <0.481J3 <0.190 91.9 224 74.3 1110 Dup-1 (MW-3) 12/13/22 <3.74J4 15.5 <2.37 <0.112 <0.0636 <0.143 <11.3J3 <2.54 1300 2.26 2.07 0.894J <0.111 28.4 88.4 0.24J 14.4 297 <0.337J3 14.4 0.995J 7.68J <0.101 39.8J3 30.4 21.8 2160 <0.230J3 <0.481J3 <0.190 81.6 215 65.2 1040 MW-4 12/13/22 <3.74J4 <0.159 <2.37J4 <0.112 <0.0636 <0.143 <11.3J3 <2.54 <0.0941 <0.157 <0.125 <0.575 <0.111 <0.126 <0.0819 <0.126 <0.105 <0.137 <0.337J3 <0.105 <0.120 <0.478 <0.101 <1.00J3 <0.0993 <0.300 <0.278 <0.230J3 <0.481J3 <0.190 <0.104 <0.322 <0.104 <0.174 MW-5 12/13/22 <3.74J4 <0.159 <2.37J4 <0.112 <0.0636 <0.143 <11.3 <2.54C3 <0.0941 <0.157 <0.125 <0.575 <0.111 <0.126 <0.0819 <0.126 <0.105 <0.137 <0.337C3 <0.105 <0.120 <0.478 <0.101 <1.00C3 <0.0993 <0.300 <0.278 <0.230 <0.481C3 <0.190 <0.104 <0.322 <0.104 <0.174 MW-6 12/13/22 <3.74J4 <0.159 <2.37 <0.112 <0.0636 <0.143 <11.3J3 <2.54 0.145J <0.157 <0.125 <0.575 0.283J <0.126 0.143J <0.126 0.688J <0.137 <0.337J3 <0.105 <0.120 <0.478 0.238J <1.00J3 <0.0993 25.8 0.526J <0.230J3 <0.481J3 <0.190 <0.104 <0.322 <0.104 0.373JNL 6 NL 200 100 NL 6,000 NL 1 70 70 NL 70 0.02 0.4 70 70 600 0.4 70 25 100 20 6 70 0.7 600 NL 70 3 NL 400 400 500 Units in micrograms per liter (µg/L) <X.X = Less than the Method Detection Limit (MDL) shown NL= Not listed, No Standard established 15A NCAC 2L Standard = 15A North Carolina Administrative Code (NCAC) 02L.0202 Groundwater Standards (2L Standards) (April 1, 2022) Pink shading indicates exceedance of 2L Standard Qualifiers C3 = The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptableJ = The indentification of the analyte is acceptable; the reported value is an estimateJ3 = The associated batch QC was outside the established quality control range for precision J4 = The associated batch QC was outside the established quality control range for precision 15A NCAC 2L Standard VOCsSVOCs Table 1D Groundwater Organic Detections (SVOCs and VOCs) µg/L 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 Sample IDDate SampledAcetoneBenzene2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroformChloromethaneCyclohexaneDichlorodifluoromethane (F12)EthanolEthylbenzene4-Ethyltoluenen-Heptanen-HexaneIsopropylbenzene (Cumene)p-IsopropyltolueneNaphthalenePropenen-PropylbenzeneStyreneTetrachloroetheneTolueneTrichloroetheneTrichlorofluoromethane (F11)1,1,2-Trichlorotrifluoroethane (F113)1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2,2,4-Trimethylpentanem,p-Xyleneo-XyleneSG-1 12/21/22 2.3J 0.2J <0.3 1.4J <0.2 0.3J <0.3 <0.2 <0.1 <0.3 1.5J <1.2 2.1 1.0J 1.2J <0.2 0.2J 1.2J 1.0J 1.5 2.0 <0.2 <0.3 10 <0.3 1.1J <0.3 5.3 1.4J <0.2 10 <0.2 SG-2 12/21/22 31 0.1J <0.3 7.2 1.6J 0.4J <0.3 <0.2 0.9 2.2J 1.4J <1.2 2.0 3.9 <0.2 <0.2 0.8J 4.0 0.7J 4.0 1.6J 0.7J 2.4J 3.1 <0.3 <0.2 <0.3 18 5.4 2.5 9.8 4.6 SG-3 12/21/22 14 0.5J 1.7J <0.2 <0.2 0.4J 1.0J 1.5 <0.1 <0.3 1.3J <1.2 0.7J 1.2J <0.2 <0.2 0.2J 0.7J 0.7J 1.6 <0.2 <0.2 410 4.4 <0.3 <0.2 <0.3 4.9 1.3J <0.2 5.0 2.8 SG-4 12/21/22 13 0.3J <0.3 <0.2 <0.2 1.1J 1.7 1.7 <0.1 2.0J 1.3J <1.2 1.1J 1.0J 1.0J <0.2 <0.2 0.8J 0.5J 0.9J 0.4J <0.2 54 21 <0.3 1.4J <0.3 3.9 1.0J 0.4J 6.3 2.9 SG-5 12/21/22 <0.5 0.2J <0.3 <0.2 <0.2 0.6J <0.3 <0.2 <0.1 1.9J 1.6J <1.2 0.3J 0.3J <0.2 <0.2 <0.2 0.4J <0.2 1.5 <0.2 <0.2 37 7.8 <0.3 <0.2 <0.3 1.2J 0.3J <0.2 1.3J 0.7J SG-6 12/21/22 <0.5 0.3J <0.3 <0.2 <0.2 0.7J <0.3 <0.2 <0.1 2.0J <0.4 <1.2 0.4J <0.2 <0.2 <0.2 <0.2 0.4J <0.2 1.7 <0.2 <0.2 4.5 14 <0.3 <0.2 <0.3 1.0J 0.2J <0.2 1.2J 0.7J SG-7 12/21/22 4.5J 0.4J <0.3 0.5J <0.2 0.3J <0.3 <0.2 <0.1 0.9J 1.6J <1.2 0.9J 0.5J 0.7J <0.2 <0.2 0.4J <0.2 2.0 <0.2 <0.2 0.8J 9.0 <0.3 1.1J <0.3 2.1 0.5J <0.2 3.0 4.0 SG-8 12/21/22 <0.5 0.3J <0.3 0.7J <0.2 0.5J <0.3 0.6J <0.1 2.7J 1.6J <1.2 1.4J 0.6J <0.2 <0.2 <0.2 6.8 0.6J 1.9 0.2J <0.2 0.5J 12 <0.3 <0.2 <0.3 4.4 0.9J <0.2 6.8 3.5 SG-9 12/21/22 7.0 0.2J <0.3 <0.2 <0.2 3.6 <0.3 2.5 <0.1 1.2J 1.7J <1.2 0.7J <0.2 <0.2 <0.2 <0.2 12 0.6J <0.1 <0.2 <0.2 250 3.5 <0.3 2.0J 0.5J <0.2 <0.2 <0.2 1.5J 5.2 SG-10 1/27/23 350 100 <0.3 <0.2 <0.2 6.6 <0.3 4.1 <0.1 53 25 190 89 <0.2 70 230 <0.2 <0.2 <0.2 <0.1 <0.2 1,300 560 940 <0.3 13 <0.3 <0.2 <0.2 230 390 230 SG-Duplicate 12/21/22 1.8J 0.3J <0.3 0.3J <0.2 0.2J <0.3 0.9J <0.1 1.4J 1.4J <1.2 0.4J 0.3J <0.2 <0.2 <0.2 0.3J <0.2 <0.1 <0.2 <0.2 4.7 5.9 1.7J 1.1J <0.3 1.4J 0.4J <0.2 1.7J 0.8J Duplicate-2 1/27/22 380 120 <0.3 <0.2 <0.2 6.7 <0.3 4.7 <0.1 69 28 240 150 <0.2 83 260 <0.2 <0.2 <0.2 <0.1 <0.2 1,400 590 1,100 <0.3 8.9 <0.3 <0.2 <0.2 250 760 300 NL 12 35,000 NL NL 4,900 16 4.1 630 42,000 700 NL 37 NL 2,800 4,900 2,800 NL NL 21,000 7,000 7,000 280 35,000 14 NL NL 420 420 NL 700 700 NL 160 440,000 NL NL 61,000 200 53 7,900 88,000 8,800 NL 490 NL 35,000 61,000 35,000 NL NL 260,000 88,000 88,000 3,500 440,000 180 NL NL 5,300 5,300 NL 8,800 8,800 Units in micrograms per cubic meter (µg/m3) <X.X = Less than the Method Detection Limit (MDL) shown NL= Not listed, No Standard established SGSL = Soil Gas Screening Level Pink shading indicates exceedance of Residential SGSL Qualifiers J = Detected but below the RL; therefore, result is an estimated concentration. (1) NCDEQ Vapor Intrusion Sub-Slab and Exterior Soil Gas Screening Levels (January 2023) Residential SGSL(1) Non-Residential SGSL(1) Table 1E Soil Gas Detections (µg/m3) 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC VOCs (TO-15) BROWNFIELDS PROJECT NO. 25052-21-034 Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT C Risk Calculator Results Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Prepared By:EAS Professionals, Inc. Site Wide - Hypothetical Worst Case North Carolina Department of Environmental Quality Risk Calculator 450 Polo Road 450 Polo Road, Winston-Salem, NC Division of Waste Management - Brownfields Program 25052-21-034 January 2023 November 2022 EPA RSL Table North Carolina DEQ Risk Calculator Table of Contents Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case Form No. Input Form 1A Complete Exposure Pathways Input Form 1B Exposure Factors and Target Risks Input Form 1C Contaminant Migration Parameters Input Form 1D Sample Statistics Input Form 2A Soil Exposure Point Concentration Table Input Form 2B Groundwater Exposure Point Concentration Table Input Form 2C Surface Water Exposure Point Concentration Table Input Form 2D Soil Gas Exposure Point Concentration Table Input Form 2E Indoor Air Exposure Point Concentration Table Output Form 1A Risk for Individual Pathways Output Form 1B Sitewide Risk Output Form 2A Resident Soil Output Form 2B Resident Groundwater Use Output Form 2C Non-Residential Worker Soil Output Form 2D Non-Residential Worker Groundwater Use Output Form 2E Construction Worker Soil Output Form 2F Recreator/Trespasser Soil Output Form 2G Recreator/Trespasser Surface Water Output Form 3A Resident Groundwater to Indoor Air Output Form 3B Resident Soil Gas to Indoor Air Output Form 3C Resident Indoor Air Output Form 3D Non-Residential Worker Groundwater to Indoor Air Output Form 3E Non-Residential Worker Soil Gas to Indoor Air Output Form 3F Non-Residential Worker Indoor Air Output Form 4A Soil to Groundwater - Forward Mode Output Form 4B Groundwater to Groundwater - Forward Mode Output Form 4C Soil to Surface Water - Forward Mode Output Form 4D Groundwater to Surface Water - Forward Mode Output Form 4E Soil to Groundwater - Backward Mode Output Form 4F Groundwater to Groundwater - Backward Mode Output Form 4G Soil to Surface Water - Backward Mode Output Form 4H Groundwater to Surface Water - Backward Mode Output Section 4 - Contaminant Migration Worksheets Output Section 3 - Vapor Intrusion Calculators TOC Description DATA INPUT SHEETS Check box if included Input Section 1 - Exposure Pathways & Parameters Input Section 2 - Exposure Point Concentrations DATA OUTPUT SHEETS Output Section 1 - Summary Output for All Calculators Output Section 2 - Direct Contact Soil and Groundwater Calculators North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations Exposure Point Concentration (mg/kg) Notes:CAS Number Chemical For the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main Menu Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 0.154 67-64-1 Acetone mg/kg 15.3 7440-38-2 Arsenic, Inorganic mg/kg 48.7 7440-39-3 Barium mg/kg 0.00296 71-43-2 Benzene mg/kg 0.167 RL (MDL) is greater than Residential PSRG 92-87-5 Benzidine mg/kg 0.00583 135-98-8 Butylbenzene, sec-mg/kg 0.962 7440-43-9 Cadmium (Diet)mg/kg 0.0076 67-66-3 Chloroform mg/kg 78.4 Reported value is within the naturally occurring background metals range of 7-300 mg/kg for North Carolina or Southeastern soils based on Elements in North American Soils by Dragun and Chekiri, 2005 16065-83-1 Chromium(III), Insoluble Salts mg/kg 0.00135 Isopropylbenzene 98-82-8 Cumene mg/kg 0.00933 RL (MDL) is greater than Residential PSRG 96-12-8 Dibromo-3-chloropropane, 1,2-mg/kg 0.0273 95-50-1 Dichlorobenzene, 1,2-mg/kg 0.00221 106-46-7 Dichlorobenzene, 1,4-mg/kg 0.00106 542-75-6 Dichloropropene, 1,3-mg/kg 0.002 100-41-4 Ethylbenzene mg/kg 94.8 7439-92-1 ~Lead and Compounds mg/kg 0.18 7439-97-6 ~Mercury (elemental)mg/kg 0.00527 MIBK, laboratory reported value included a "J" qualifier 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)mg/kg 0.132 RL (MDL) is greater than Residential PSRG 62-75-9 Nitrosodimethylamine, N-mg/kg 0.0811 117-81-7 ~Bis(2-ethylhexyl)phthalate mg/kg 0.0189 84-74-2 ~Dibutyl Phthalate mg/kg 0.971 83-32-9 ~Acenaphthene mg/kg 1.51 120-12-7 ~Anthracene mg/kg 3.77 56-55-3 ~Benz[a]anthracene mg/kg 5.12 50-32-8 ~Benzo[a]pyrene mg/kg 6.95 205-99-2 ~Benzo[b]fluoranthene mg/kg 1.46 207-08-9 ~Benzo[k]fluoranthene mg/kg 3.3 218-01-9 ~Chrysene mg/kg 0.604 53-70-3 ~Dibenz[a,h]anthracene mg/kg 9.4 206-44-0 ~Fluoranthene mg/kg 0.774 86-73-7 ~Fluorene mg/kg 2.36 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg 0.416 Result from SVOC analysis 91-20-3 ~Naphthalene mg/kg 6.59 129-00-0 ~Pyrene mg/kg 1.42 7782-49-2 Selenium mg/kg 0.00192 100-42-5 Styrene mg/kg 0.00855 127-18-4 Tetrachloroethylene mg/kg 0.0229 108-88-3 Toluene mg/kg 0.00403 95-63-6 Trimethylbenzene, 1,2,4-mg/kg 0.0158 1330-20-7 Xylenes mg/kg Input Form 2A Soil Exposure Point Concentration Table Description of Exposure Point Concentration Selection: North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case Description of Exposure Point Concentration Selection: NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations Exposure Point Concentration (ug/L) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 15.8 67-64-1 Acetone ug/L 22.8 7440-38-2 Arsenic, Inorganic ug/L 854 7440-39-3 Barium ug/L 1300 71-43-2 Benzene ug/L 2.48 104-51-8 Butylbenzene, n-ug/L 2.31 135-98-8 Butylbenzene, sec-ug/L 0.427 7440-43-9 Cadmium (Water)ug/L 0.825 67-66-3 Chloroform ug/L 19.3 16065-83-1 Chromium(III), Insoluble Salts ug/L 15.7 Isopropylbenzene 98-82-8 Cumene ug/L 29.4 106-93-4 Dibromoethane, 1,2-ug/L 97.1 107-06-2 Dichloroethane, 1,2-ug/L 0.24 156-59-2 Dichloroethylene, cis-1,2-ug/L 15.5 108-20-3 Diisopropyl Ether ug/L 0.881 105-67-9 Dimethylphenol, 2,4-ug/L 304 100-41-4 Ethylbenzene ug/L 239 7439-92-1 ~Lead and Compounds ug/L 1.67 7439-97-6 ~Mercury (elemental)ug/L 8.15 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/L 0.238 1634-04-4 Methyl tert-Butyl Ether (MTBE)ug/L 15.5 91-20-3 ~Naphthalene ug/L 34.5 103-65-1 Propyl benzene ug/L 7.71 7782-49-2 Selenium ug/L 0.116 7440-22-4 Silver ug/L 25.8 127-18-4 Tetrachloroethylene ug/L 2330 108-88-3 Toluene ug/L 0.241 79-01-6 Trichloroethylene ug/L 91.9 526-73-8 Trimethylbenzene, 1,2,3-ug/L 224 95-63-6 Trimethylbenzene, 1,2,4-ug/L 74.3 108-67-8 Trimethylbenzene, 1,3,5-ug/L 1110 1330-20-7 Xylenes ug/L Input Form 2B Groundwater Exposure Point Concentration Table North Carolina DEQ Risk Calculator Exposure Point Concentrations Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case Description of Exposure Point Concentration Selection: Exposure Point Concentration (ug/m3) Notes:CAS Number Chemical Minimum Concentration (Qualifier) Maximum Concentration (Qualifier) Units Location of Maximum Concentration Detection Frequency Range of Detection Limits Concentration Used for Screening Background Value Screening Toxicity Value (Screening Level) (n/c) Potential ARAR/TBC Value Potential ARAR/TBC Source COPC Flag (Y/N) Rationale for Selection or Deletion 380 67-64-1 Acetone ug/m3 120 71-43-2 Benzene ug/m3 7.2 104-51-8 Butylbenzene, n-ug/m3 1.6 135-98-8 Butylbenzene, sec-ug/m3 6.7 75-15-0 Carbon Disulfide ug/m3 1.7 56-23-5 Carbon Tetrachloride ug/m3 4.7 67-66-3 Chloroform ug/m3 0.9 74-87-3 Chloromethane ug/m3 0.8 98-82-8 Cumene ug/m3 69 110-82-7 Cyclohexane ug/m3 28 75-71-8 Dichlorodifluoromethane ug/m3 150 100-41-4 Ethylbenzene ug/m3 83 142-82-5 Heptane, N-ug/m3 260 110-54-3 Hexane, N-ug/m3 1.7 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3 1 91-20-3 ~Naphthalene ug/m3 2 103-65-1 Propyl benzene ug/m3 4 115-07-1 Propylene ug/m3 1,400 100-42-5 Styrene ug/m3 590 127-18-4 Tetrachloroethylene ug/m3 1,100 108-88-3 Toluene ug/m3 1.7 79-01-6 Trichloroethylene ug/m3 13 75-69-4 Trichlorofluoromethane ug/m3 18 95-63-6 Trimethylbenzene, 1,2,4-ug/m3 5.4 108-67-8 Trimethylbenzene, 1,3,5-ug/m3 250 25167-70-8 Trimethylpentene, 2,4,4-ug/m3 1060 1330-20-7 Xylenes ug/m3 Input Form 2D Soil Gas Exposure Point Concentration Table Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations North Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil 4.7E-04 1.1E+00 YES Groundwater Use*NC NC NC Soil 2.9E-05 9.3E-02 NO Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 1.7E-05 9.7E-01 NO Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: North Carolina DEQ Risk Calculator DEQ Risk Calculator - Direct Contact - Resident Soil Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case * - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion. CAS # Chemical Name: Ingestion Concentration (mg/kg) Dermal Concentration (mg/kg) Inhalation Concentration (mg/kg)* Ingestion Carcinogenic Risk Dermal Carcinogenic Risk Inhalation Carcinogenic Risk* Calculated Carcinogenic Risk Ingestion Hazard Quotient Dermal Hazard Quotient Inhalation Hazard Quotient* Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 0.154 0.154 0.154 2.2E-06 2.2E-06 7440-38-2 Arsenic, Inorganic 15.3 15.3 15.3 2.0E-05 2.8E-06 3.9E-10 2.3E-05 3.9E-01 4.6E-02 1.6E-05 4.4E-01 7440-39-3 Barium 48.7 48.7 48.7 3.1E-03 1.6E-06 3.1E-03 71-43-2 Benzene 0.00296 0.00296 0.00296 2.3E-10 2.2E-09 2.4E-09 9.5E-06 2.5E-05 3.5E-05 92-87-5 Benzidine 0.167 0.167 0.167 2.5E-04 6.4E-05 1.9E-10 3.2E-04 7.1E-04 1.7E-04 8.8E-04 135-98-8 Butylbenzene, sec-0.00583 0.00583 0.00583 7.5E-07 7.5E-07 7440-43-9 Cadmium (Diet)0.962 0.962 0.962 1.0E-11 1.0E-11 1.2E-01 1.2E-02 1.6E-06 1.3E-01 67-66-3 Chloroform 0.0076 0.0076 0.0076 3.4E-10 2.0E-08 2.0E-08 9.7E-06 2.4E-05 3.3E-05 16065-83-1 Chromium(III), Insoluble Salts 78.4 78.4 78.4 6.7E-04 6.7E-04 98-82-8 Cumene 0.00135 0.00135 0.00135 1.7E-07 4.9E-07 6.6E-07 96-12-8 Dibromo-3-chloropropane, 1,2-0.00933 0.00933 0.00933 4.9E-08 1.6E-06 1.7E-06 6.0E-04 1.3E-03 1.9E-03 95-50-1 Dichlorobenzene, 1,2-0.0273 0.0273 0.0273 3.9E-06 1.1E-05 1.4E-05 106-46-7 Dichlorobenzene, 1,4-0.00221 0.00221 0.00221 1.7E-11 7.8E-10 8.0E-10 4.0E-07 2.4E-07 6.4E-07 542-75-6 Dichloropropene, 1,3-0.00106 0.00106 0.00106 1.5E-10 4.0E-10 5.5E-10 4.5E-07 1.3E-05 1.4E-05 100-41-4 Ethylbenzene 0.002 0.002 0.002 3.2E-11 3.0E-10 3.3E-10 5.1E-07 3.2E-07 8.3E-07 7439-92-1 ~Lead and Compounds 94.8 94.8 94.8 <SL**<SL**<SL**7439-97-6 ~Mercury (elemental)0.18 0.18 0.18 1.6E-02 1.6E-02 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 0.00527 0.00527 0.00527 1.5E-07 1.5E-07 62-75-9 Nitrosodimethylamine, N-0.132 0.132 0.132 4.4E-05 2.1E-05 6.5E-05 2.1E-01 3.6E-02 2.5E-01 117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0811 0.0811 0.0811 1.6E-09 4.6E-10 1.2E-15 2.1E-09 5.2E-05 1.2E-05 6.4E-05 84-74-2 ~Dibutyl Phthalate 0.0189 0.0189 0.0189 2.4E-06 5.7E-07 3.0E-06 83-32-9 ~Acenaphthene 0.971 0.971 0.971 2.1E-04 6.4E-05 2.7E-04 120-12-7 ~Anthracene 1.51 1.51 1.51 6.4E-05 2.0E-05 8.4E-05 56-55-3 ~Benz[a]anthracene 3.77 3.77 3.77 2.5E-06 8.2E-07 4.8E-08 3.3E-06 50-32-8 ~Benzo[a]pyrene 5.12 5.12 5.12 3.3E-05 1.1E-05 5.1E-11 4.5E-05 2.2E-01 6.7E-02 4.1E-05 2.9E-01 205-99-2 ~Benzo[b]fluoranthene 6.95 6.95 6.95 4.5E-06 1.5E-06 6.9E-12 6.1E-06 207-08-9 ~Benzo[k]fluoranthene 1.46 1.46 1.46 9.5E-08 3.2E-08 1.5E-13 1.3E-07 218-01-9 ~Chrysene 3.3 3.3 3.3 2.2E-08 7.2E-09 3.3E-14 2.9E-08 53-70-3 ~Dibenz[a,h]anthracene 0.604 0.604 0.604 3.9E-06 1.3E-06 6.0E-12 5.3E-06 206-44-0 ~Fluoranthene 9.4 9.4 9.4 3.0E-03 9.3E-04 3.9E-03 86-73-7 ~Fluorene 0.774 0.774 0.774 2.5E-04 7.6E-05 3.2E-04 193-39-5 ~Indeno[1,2,3-cd]pyrene 2.36 2.36 2.36 1.5E-06 5.1E-07 2.4E-12 2.1E-06 91-20-3 ~Naphthalene 0.416 0.416 0.416 7.2E-08 2.6E-08 1.0E-07 2.0E-07 2.7E-04 8.2E-05 2.7E-03 3.0E-03 129-00-0 ~Pyrene 6.59 6.59 6.59 2.8E-03 8.7E-04 3.7E-03 7782-49-2 Selenium 1.42 1.42 1.42 3.6E-03 1.1E-09 3.6E-03 100-42-5 Styrene 0.00192 0.00192 0.00192 1.2E-07 1.8E-07 3.1E-07 127-18-4 Tetrachloroethylene 0.00855 0.00855 0.00855 2.6E-11 2.5E-10 2.8E-10 1.8E-05 6.5E-05 8.3E-05 108-88-3 Toluene 0.0229 0.0229 0.0229 3.7E-06 9.6E-07 4.6E-06 95-63-6 Trimethylbenzene, 1,2,4-0.00403 0.00403 0.00403 5.2E-06 7.6E-06 1.3E-05 1330-20-7 Xylenes 0.0158 0.0158 0.0158 1.0E-06 2.5E-05 2.6E-05 Cumulative:4.7E-04 1.1E+00 Output Form 2A ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case * - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion. CAS # Chemical Name: Ingestion Concentration (mg/kg) Dermal Concentration (mg/kg) Inhalation Concentration (mg/kg)* Ingestion Carcinogenic Risk Dermal Carcinogenic Risk Inhalation Carcinogenic Risk Calculated Carcinogenic Risk Ingestion Hazard Quotient Dermal Hazard Quotient Inhalation Hazard Quotient Calculated Non- Carcinogenic Hazard Quotient67-64-1 Acetone 0.154 0.154 0.154 1.5E-07 1.5E-077440-38-2 Arsenic, Inorganic 15.3 15.3 15.3 4.2E-06 8.9E-07 9.0E-11 5.1E-06 2.6E-02 5.5E-03 3.9E-06 3.2E-02 7440-39-3 Barium 48.7 48.7 48.7 2.1E-04 3.7E-07 2.1E-04 71-43-2 Benzene 0.00296 0.00296 0.00296 5.0E-11 5.0E-10 5.5E-10 6.3E-07 6.0E-06 6.6E-06 92-87-5 Benzidine 0.167 0.167 0.167 1.2E-05 5.0E-06 1.5E-11 1.7E-05 4.8E-05 2.0E-05 6.8E-05135-98-8 Butylbenzene, sec-0.00583 0.00583 0.00583 5.0E-08 5.0E-08 7440-43-9 Cadmium (Diet)0.962 0.962 0.962 2.4E-12 2.4E-12 8.2E-03 1.4E-03 3.7E-07 9.6E-03 67-66-3 Chloroform 0.0076 0.0076 0.0076 7.2E-11 4.5E-09 4.6E-09 6.5E-07 5.6E-06 6.3E-06 16065-83-1 Chromium(III), Insoluble Salts 78.4 78.4 78.4 4.5E-05 4.5E-05 98-82-8 Cumene 0.00135 0.00135 0.00135 1.2E-08 1.2E-07 1.3E-07 96-12-8 Dibromo-3-chloropropane, 1,2-0.00933 0.00933 0.00933 2.3E-09 1.3E-07 1.4E-07 4.0E-05 3.1E-04 3.5E-04 95-50-1 Dichlorobenzene, 1,2-0.0273 0.0273 0.0273 2.6E-07 2.5E-06 2.8E-06 106-46-7 Dichlorobenzene, 1,4-0.00221 0.00221 0.00221 3.6E-12 1.8E-10 1.8E-10 2.7E-08 5.7E-08 8.4E-08 542-75-6 Dichloropropene, 1,3-0.00106 0.00106 0.00106 3.2E-11 9.1E-11 1.2E-10 3.0E-08 3.2E-06 3.2E-06 100-41-4 Ethylbenzene 0.002 0.002 0.002 6.7E-12 6.8E-11 7.4E-11 3.4E-08 7.6E-08 1.1E-07 7439-92-1 ~Lead and Compounds 94.8 94.8 94.8 <SL**<SL**<SL** 7439-97-6 ~Mercury (elemental)0.18 0.18 0.18 3.7E-03 3.7E-03 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 0.00527 0.00527 0.00527 3.6E-08 3.6E-08 62-75-9 Nitrosodimethylamine, N-0.132 0.132 0.132 2.1E-06 1.7E-06 3.8E-06 1.4E-02 8.6E-03 2.3E-02 117-81-7 ~Bis(2-ethylhexyl)phthalate 0.0811 0.0811 0.0811 3.5E-10 1.5E-10 2.7E-16 4.9E-10 3.5E-06 1.5E-06 4.9E-06 84-74-2 ~Dibutyl Phthalate 0.0189 0.0189 0.0189 1.6E-07 6.8E-08 2.3E-0783-32-9 ~Acenaphthene 0.971 0.971 0.971 1.4E-05 7.6E-06 2.1E-05 120-12-7 ~Anthracene 1.51 1.51 1.51 4.3E-06 2.4E-06 6.7E-06 56-55-3 ~Benz[a]anthracene 3.77 3.77 3.77 1.2E-07 6.3E-08 3.9E-09 1.8E-07 50-32-8 ~Benzo[a]pyrene 5.12 5.12 5.12 1.6E-06 8.6E-07 4.2E-12 2.4E-06 1.5E-02 8.0E-03 9.9E-06 2.3E-02205-99-2 ~Benzo[b]fluoranthene 6.95 6.95 6.95 2.1E-07 1.2E-07 5.7E-13 3.3E-07 207-08-9 ~Benzo[k]fluoranthene 1.46 1.46 1.46 4.5E-09 2.5E-09 1.2E-14 6.9E-09 218-01-9 ~Chrysene 3.3 3.3 3.3 1.0E-09 5.6E-10 2.7E-15 1.6E-09 53-70-3 ~Dibenz[a,h]anthracene 0.604 0.604 0.604 1.8E-07 1.0E-07 5.0E-13 2.9E-07206-44-0 ~Fluoranthene 9.4 9.4 9.4 2.0E-04 1.1E-04 3.1E-04 86-73-7 ~Fluorene 0.774 0.774 0.774 1.7E-05 9.1E-06 2.6E-05 193-39-5 ~Indeno[1,2,3-cd]pyrene 2.36 2.36 2.36 7.2E-08 4.0E-08 1.9E-13 1.1E-07 91-20-3 ~Naphthalene 0.416 0.416 0.416 1.5E-08 8.4E-09 2.3E-08 4.7E-08 1.8E-05 9.8E-06 6.4E-04 6.7E-04 129-00-0 ~Pyrene 6.59 6.59 6.59 1.9E-04 1.0E-04 2.9E-04 7782-49-2 Selenium 1.42 1.42 1.42 2.4E-04 2.7E-10 2.4E-04 100-42-5 Styrene 0.00192 0.00192 0.00192 8.2E-09 4.4E-08 5.2E-08 127-18-4 Tetrachloroethylene 0.00855 0.00855 0.00855 5.5E-12 5.8E-11 6.3E-11 1.2E-06 1.6E-05 1.7E-05 108-88-3 Toluene 0.0229 0.0229 0.0229 2.5E-07 2.3E-07 4.7E-07 95-63-6 Trimethylbenzene, 1,2,4-0.00403 0.00403 0.00403 3.5E-07 1.8E-06 2.2E-06 1330-20-7 Xylenes 0.0158 0.0158 0.0158 6.8E-08 5.9E-06 6.0E-06 Cumulative: 2.9E-05 9.3E-02 Output Form 2C ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg for commercial/industrial soil. North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 25052-21-034 Exposure Unit ID: Site Wide - Hypothetical Worst Case CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 380 11.4 -- 71-43-2 Benzene 120 3.6 3.6E-01 6.3E+00 1.0E-05 1.2E-01 104-51-8 Butylbenzene, n-7.2 0.216 -- 135-98-8 Butylbenzene, sec-1.6 0.048 -- 75-15-0 Carbon Disulfide 6.7 0.201 -1.5E+02 2.8E-04 56-23-5 Carbon Tetrachloride 1.7 0.051 4.7E-01 2.1E+01 1.1E-07 4.9E-04 67-66-3 Chloroform 4.7 0.141 1.2E-01 2.0E+01 1.2E-06 1.4E-03 74-87-3 Chloromethane 0.9 0.027 -1.9E+01 2.9E-04 98-82-8 Cumene 0.8 0.024 -8.3E+01 5.8E-05 110-82-7 Cyclohexane 69 2.07 -1.3E+03 3.3E-04 75-71-8 Dichlorodifluoromethane 28 0.84 -2.1E+01 8.1E-03 100-41-4 Ethylbenzene 150 4.5 1.1E+00 2.1E+02 4.0E-06 4.3E-03 142-82-5 Heptane, N-83 2.49 -8.3E+01 6.0E-03 110-54-3 Hexane, N-260 7.8 -1.5E+02 1.1E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone)1.7 0.051 -1.0E+03 9.8E-06 91-20-3 ~Naphthalene 1 0.03 8.3E-02 6.3E-01 3.6E-07 9.6E-03 103-65-1 Propyl benzene 2 0.06 -2.1E+02 5.8E-05 115-07-1 Propylene 4 0.12 -6.3E+02 3.8E-05 100-42-5 Styrene 1400 42 -2.1E+02 4.0E-02 127-18-4 Tetrachloroethylene 590 17.7 1.1E+01 8.3E+00 1.6E-06 4.2E-01 108-88-3 Toluene 1100 33 -1.0E+03 6.3E-03 79-01-6 Trichloroethylene 1.7 0.051 4.8E-01 4.2E-01 1.1E-07 2.4E-02 75-69-4 Trichlorofluoromethane 13 0.39 -- 95-63-6 Trimethylbenzene, 1,2,4-18 0.54 -1.3E+01 8.6E-03 108-67-8 Trimethylbenzene, 1,3,5-5.4 0.162 -1.3E+01 2.6E-03 25167-70-8 Trimethylpentene, 2,4,4-250 7.5 -- 1330-20-7 Xylenes 1060 31.8 -2.1E+01 3.0E-01 Cumulative: 1.7E-05 9.7E-01 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT D Site Plat Showing Oil/Water Separator provided by Stratus Development Group Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT E Boring Logs SURFICIAL ORGANIC LADENTOPSOIL: 2 inches RESIDUAL Brown, sandy siltyCLAY (CL) Sample CS-1 collected from thisrange Boring terminated at a depth of2 feet. Groundwater was notencountered during sampling. 0.2 2.0 Boring No.: CS-1 Type of Boring:Hand Auger Total Depth: 2.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 2 inches RESIDUAL Brown, sandy siltyCLAY (CL) Sample CS-2 collected from thisrange Boring terminated at a depth of2 feet. Groundwater was notencountered during sampling. 0.2 2.0 Boring No.: CS-2 Type of Boring:Hand Auger Total Depth: 2.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 2 inches FILL Reddish brown, sandy SILT(ML) Sample CS-3 collected from thisrange Boring terminated at a depth of2 feet. Groundwater was notencountered during sampling. 0.2 2.0 Boring No.: CS-3 Type of Boring:Hand Auger Total Depth: 2.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Brown, clayey SILT (ML) Reddish brown and tan, sandySILT (ML) Sample CS-4 collected from thisrange GRAVEL RESIDUAL Reddish brown, siltySAND (SM) Tan and orangish brown, siltySAND (SM) Sample CS-4-a collected fromthis range Boring terminated at a depth of7 feet. Groundwater was notencountered during sampling. 0.20.4 1.0 4.04.3 6.0 7.0 Boring No.: CS-4 Type of Boring:Direct Push Total Depth: 7.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 1 inch FILL Reddish brown and brown,clayey sandy SILT (ML) withgravel Sample CS-5 collected from thisrange Boring terminated at a depth of1 foot due to hand augerrefusal. Two offset boringswere performed with similarrefusal depths. Sample CS-5-awas not collected due to handauger refusal. Groundwaterwas not encountered duringsampling. 0.1 1.0 Boring No.: CS-5 Type of Boring:Hand Auger Total Depth: 1.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 1 inch FILL Reddish brown, sandy siltyCLAY (CL) with gravel Sample CS-6 collected from thisrange Reddish brown, sandy clayeySILT (ML) with gravel Sample CS-6-a collected fromthis range Boring terminated at a depth of2.5 feet due to hand augerrefusal. Groundwater was notencountered during sampling. 0.1 1.0 2.5 Boring No.: CS-6 Type of Boring:Hand Auger Total Depth: 2.5 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 1 inch FILL Reddish brown, sandy siltyCLAY (CL) with gravel Sample CS-7 collected from thisrange Reddish brown, sandy clayeySILT (ML) with gravel Sample CS-7 collected from thisrange Boring terminated at a depth of2.5 feet. Groundwater was notencountered during sampling. 0.1 1.0 2.5 Boring No.: CS-7 Type of Boring:Hand Auger Total Depth: 2.0 feet Elevation: Date Drilled: 11/14/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 5 inches RESIDUAL Brown, silty SAND(SM) Sample CS-8 collected from thisrange (0-2 feet bgs) Reddish brown, silty SAND (SM) Sample CS-8 collected from thisrange (0-2 feet bgs) Boring terminated at a depth of2 feet. Groundwater was notencountered during sampling. 0.4 1.0 2.0 Boring No.: CS-8 Type of Boring:Hand Auger Total Depth: 2.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 4 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 4 inches RESIDUAL Brown, sandy SILT(ML) with trace clay Reddish brown, sandy SILT (ML)with trace clay Brown, silty SAND (SM) Brown and tan, silty SAND (SM)with trace gravel 0.3 1.0 2.0 4.0 963.0 962.3 961.3 959.3 Boring No.: MW-1 (1 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 963.3± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of30 feet. Stabilized groundwaterwas observed at a depth of 9.2feet bgs. 30.0 933.3 Boring No.: MW-1 (2 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 963.3± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) RESIDUAL Red, clayey SILT (ML)with little sand Red, sandy SILT (ML) 0.20.4 1.0 3.0 982.4982.2 981.6 979.6 Boring No.: MW-2 (1 of 2) Total Depth: 40.0 feet Type of Boring:Hollow Stem Auger Elevation: 982.6± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of40 feet. Stabilized groundwaterwas observed at a depth of 27.3feet bgs. 40.0 942.6 Boring No.: MW-2 (2 of 2) Total Depth: 40.0 feet Type of Boring:Hollow Stem Auger Elevation: 982.6± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) Red, clayey SILT (ML) with littlesand RESIDUAL Red, sandy SILT (ML) 0.20.4 1.0 3.0 979.7979.5 978.9 976.9 Boring No.: MW-3 (1 of 2) Total Depth: 40.0 feet Type of Boring:Hollow Stem Auger Elevation: 979.9± feet Date Drilled: 11/9/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of40 feet. Stabilized groundwaterwas observed at a depth of 23.3feet bgs. 40.0 939.9 Boring No.: MW-3 (2 of 2) Total Depth: 40.0 feet Type of Boring:Hollow Stem Auger Elevation: 979.9± feet Date Drilled: 11/9/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 3 inches FILL Brown and dark brown,clayey SILT (ML) with sand Light brown, sandy clayey SILT(ML) RESIDUAL Light reddish brown,sandy silty CLAY (CL) 0.3 2.0 4.0 968.0 966.2 964.2 Boring No.: MW-4 (1 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 968.2± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of30 feet. Stabilized groundwaterwas observed at a depth of 12.3feet bgs. 30.0 938.2 Boring No.: MW-4 (2 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 968.2± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 1 inch RESIDUAL Reddish brown, siltySAND (SM) Light reddish brown, silty SAND(SM) 0.1 2.0 971.2 969.3 Boring No.: MW-5 (1 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 971.3± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of30 feet. Stabilized groundwaterwas observed at a depth of 17.9feet bgs. 30.0 941.3 Boring No.: MW-5 (2 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 971.3± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 4 inches RESIDUAL Brown, silty CLAY (CL) Light reddish brown, clayeysandy SILT (ML) Tan and brown, sandy SILT (ML)with clay and trace gravel 0.3 1.0 4.0 968.6 967.9 964.9 Boring No.: MW-6 (1 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 968.9± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) continued on next page Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Boring terminated at a depth of30 feet. Stabilized groundwaterwas observed at a depth of 15.5feet bgs. 30.0 938.9 Boring No.: MW-6 (2 of 2) Total Depth: 30.0 feet Type of Boring:Hollow Stem Auger Elevation: 968.9± feet Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 4 inches RESIDUAL Brown, sandy SILT(ML) with trace clay Sample SS-1 collected from thisrange Reddish brown, sandy SILT (ML)with trace clay Brown, silty SAND (SM) Brown and tan, silty SAND (SM)with trace gravel Sample SS-1-a collected fromthis range.Sample SG-1 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.3 1.0 2.0 4.0 5.0 Boring No.: SS-1/SG-1 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 4 inches RESIDUAL Brown, silty CLAY (CL) Sample SS-2/SS-2 (DUP)collected from this range Light reddish brown, clayeysandy SILT (ML) Tan and brown, sandy SILT (ML)with clay and trace gravel Sample SS-2-a/SS-2 (DUP)collected from this range.Sample SG-2 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.3 1.0 4.0 5.0 Boring No.: SS-2/SG-2 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) Sample SS-3/SS-3 (DUP)collected from this range RESIDUAL Red, clayey SILT (ML)with little sand Red, sandy SILT (ML) Sample SS-3-a/SS-3-a (DUP)collected from this range.Sample SG-3 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.20.4 1.0 3.0 5.0 Boring No.: SS-3/SG-3 Type of Boring:Direct Push Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) Sample SS-4 collected from thisrange Red, clayey SILT (ML) with littlesand RESIDUAL Red, sandy SILT (ML) Sample SS-4-a collected fromthis range.Sample SG-4 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.20.4 1.0 3.0 5.0 Boring No.: SS-4/SG-4 Type of Boring:Direct Push Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) Sample SS-5 collected from thisrange. Red, clayey SILT (ML) with littlesand RESIDUAL Red, sandy SILT (ML) Sample SS-5 collected from thisrange.Sample SG-5 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.20.4 1.0 3.0 5.0 Boring No.: SS-5/SG-5 Type of Boring:Direct Push Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 ASPHALT 2 inches AGGREGATE BASE COURSE5 inches FILL Tan and red, silty CLAY (CL) Sample SS-6 collected from thisrange Red, clayey SILT (ML) with littlesand RESIDUAL Red, sandy SILT (ML) Sample SS-6-a collected fromthis range.Sample SG-6 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.20.4 1.0 3.0 5.0 Boring No.: SS-6/SG-6 Type of Boring:Direct Push Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 3 inches FILL Brown and dark brown,clayey SILT (ML) with sand Sample SS-7 collected from thisrange Light brown, sandy clayey SILT(ML) RESIDUAL Light reddish brown,sandy silty CLAY (CL) Sample SS-7-a collected fromthis range.Sample SG-7 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.3 2.0 4.0 5.0 Boring No.: SS-7/SG-7 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 1 inch RESIDUAL Reddish brown, siltySAND (SM) Sample SS-8 collected from thisrange Light reddish brown, silty SAND(SM) Sample SS-8-a collected fromthis range.Sample SG-8 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater was notencountered during sampling. 0.1 2.0 5.0 Boring No.: SS-8/SG-8 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 2 inches RESIDUAL Brown, sandy siltyCLAY (CL) Light reddish brown, clayeysandy SILT (ML) Sample SG-9 collected from 5feet bgs. Boring terminated at a depth of5 feet. Groundwater/perchedgroundwater was purged fromthe soil gas well prior tosampling. 0.2 2.0 5.0 Boring No.: SG-9 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 SURFICIAL ORGANIC LADENTOPSOIL: 2 inches RESIDUAL Reddish brown,sandy SILT (ML) Sample SG-10 collected from 5feet bgs. Boring terminated at a depth of2 feet. Groundwater was notencountered during sampling. 0.2 5.0 Boring No.: SG-10 Type of Boring:Hand Auger Total Depth: 5.0 feet Elevation: Date Drilled: 11/10/22 Depth(feet)USCS SampleDepth(feet)"N"Value10 20 30 40 50 60 70 80 90 GroundWaterDepth Location: See Attachment A, Figure 1 Driller: EDPS EAS Project No.: EAS-225234 Client:450 Polo, LLC SampleBlows*Samp. Loc.Elevation(feet) BORING LOG *Number of blows required for a 140-pound hammer dropping 30 inches to drive a 2-inch outside diameter (1.375-inch inside diameter) sampler a total of 18 inches inthree 6-inch increments. The sum of the last two increments of penetration is termed the Standard Penetration Resistance ("N"). Project:450 Polo Road Property, Winston-Salem, North Carolina SPT Resistance (blows per foot)Description of Materials(Classification) Date: February 2023 9 Pilgrim Road Greenville, SC 29607 Phone (864) 234-7368 Fax (864) 234-7369 Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT F Well Construction Records Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT G Receptor Survey North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Site: Address: City: County: Brownfields Project Number: Date Property and Building Characteristics a. Provide occupancy and use information. c. Describe the foundation construction. Include details on type, floor construction, and depth below grade. e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details. If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed. b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height (number of stories). % of property that is covered by buildings BROWNFIELDS PROPERTY RECEPTOR SURVEY This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager (PM). Current Usage Proposed UsageSurface Conditions % of property that is grassed areas % of property that is agricultural crops % of property that is paved NASize of Property (acres) % of property that is wooded/brush d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g. positive pressure?). Rev. 02/2019 Page 1 of 3 450 Polo Road Property 450 Polo Rd, Winston-Salem, NC 27105 Winston-Salem Forsyth 25052-21-034 1/12/2023 +/- 3.927 75 25 0 0 0 NA NA NA NA Residential NA NA NA NA NA North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Surrounding Property Land Use North South East West Utilities Is there a septic system on-site? (Y or N) _________ Please provide the utility providers for the subject property a. Natural Gas ___________________________ b. Sewer ___________________________ c. Electricity ___________________________ d. Other __________________________ For surrounding properties, please complete the following table with available information. Is there a basement within 1,000 ft of the Property Is there a residence within 1,000 ft of the Property? Utility/Potential Receptor Is a buried electrical cable main within 100 ft of Property boundary? Is a storm water pipe within 100 ft of the Property boundary? Is a sanitary sewer within 100 ft of the Property boundary? * If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property. Is a water line main within 100 ft of Property boundary? Is a natural gas line main within 100 ft of the Property boundary? Is a buried telephone/ cable main within 100 ft of the Property boundary? Is a septic system leach field within 500 ft of the Property boundary? Direction For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is required, the public utility locators should be contacted. This information can then be added to a site map. Y/N * Is a school or daycare center within 1,000 ft of the P? Specific Land Uses of Interest Y/N * * If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses. Distance (ft) DirectionDistance (ft)Address Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are present, please provide addresses of the facilities. Zoning/Land Use Proposed Usage Current Use/Occupant Rev. 02/2019 Page 2 of 3 State of NC - DOT Single Family Residential Homes Church - Calvary Chapel Fellowship Vacant NA NA NA Retail/Mixed-use Y 886 West 600 Polo Rd. Y 10 East 411 McCanless St., et al. 4001 Cherry St.260 WestY N Piedmont Natural Gas Winston-Salem/Forsyth County Utilities Duke Energy NA Y 0 N & S Y 13 North Unknown Unknown Unknown Unknown Y 35 North North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Water Supply What is the potable water supply for the property? Public ______ Private ______ Surface Water & Wetlands b. List the uses of the water body. c. What is the source of the water for the water body? d. What is the nature of the bottom of the water body (e.g., rocky or concrete bottom, drainage ways or impoundments) If no on-site surface water features, what is the nearest surface water body? Are there any wetlands present on the property? If no wetlands on-site, are wetlands suspected on adjoining properties? Is a public water supply well within 1 mile of the Property boundary? Is a private water supply well within 1,500 ft of the Property bd?Is an irrigation well within 1,500 ft of the Property boundary? Response/Comments The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property. If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name. The purpose of this section is to provide information on the water supply for the site and surrounding areas. a. Is the water body naturally developed or man-made? Y/NWater Supply Wells Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed. Are there surface water features on the property? (If yes, please complete a. to d.) Provide Information regarding Surface Water and Wetlands Distance (ft)Direction Address Rev. 02/2019 Page 3 of 3 X Winston-Salem/Forsyth County Utilities N NA NA NA Y see map/Figure 5VariousVariousVarious N NA NA NA Yes, seasonal drainage ditch Man-made Not used (ditch at outfall of on-site stormwater pipe) Surface runoff and on-site stormwater pipe Sandy bottom drainage way NA No, and not suspected on adjoining properties Receptor Survey Site Vicinity Map North Project:450 Polo Road Property Location:450 Polo Road Winston Salem, NC EAS Project No.:225234 Source:EAS/Forsyth County GIS Date:March 2023 Scale: As Shown Figure 5 Zoning Boundaries: RS/RSQ/RM/RMU-Residential; LI-Limited Industrial; HB-Highway Business; LB-Limited Business; MH-Manufactured Housing; GI-General Industrial; GB-General Business; PB-Pedestrian Business; LO-Limited Office; NO-Neighborhood Office Water Supply Well See Table 3 of Brownfield Assessment Report for Surrounding Property Owners PW2 PW3 PW4 PW5 PW6 PW8 PW9 PW10 PW11 PW12 PW13 PW14 PW15 PW16 PW17 1,500 ft. PW7 PW1 PW18 PW19 Well ID No. Well Owner/Address Well Address Well Use Well Depth (feet BGS)Type of Well Casing Depth (feet BGS) Screen Interval (feet BGS)Distance from Property Boundary (feet) PW1 Robert J. Hill 801 Delmonte Dr. Winston-Salem, NC 27106 801 Delmonte Dr. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 1,475 PW2 Carolina College, Inc. 4209 Indiana Ave.Winston-Salem, NC 27105 619 Polo Rd. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 1,315 PW3 Blue Ridge Real Estate Devel. 2299 Cloverdale Ave. Winston-Salem, NC 27103 537 Polo Rd. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 833 PW4 Blue Ridge Real Estate Devel. 2299 Cloverdale Ave. Winston-Salem, NC 27103 531 Polo Rd. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 762 PW5 John Dominic Storch 108 Brandon Pl.Winston-Salem, NC 27104 527 Polo Rd. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 695 PW6 Campus Capital Partners, LLC 1231 Polo Rd. Winston-Salem, NC 27106 526 Polo Rd. Winston-Salem, NC 27106 unknown unknown unknown unknown unknown 672 PW7 Orfilio Vasques Benitez 4004 Cherry St. Winston-Salem, NC 27105 4004 Cherry St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 513 PW8 412 McCanless Street, LLC 2420 Sattsgate Dr. Lewisville, NC 27023 412 McCanless St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 78 PW9 Calvary Chapel Fellowship of Winston-Salem 3975 Philpark Dr. Winston-Salem, NC 27106 402 Polo Rd. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 100 PW10 Stephen A. Meadows 102 Meta Ct. King, NC 27021 4018 Dalton St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 410 PW11 L & O Maintenance 3950 Philpark Dr. Winston-Salem, NC 27106 4015 Dalton St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 520 PW12 Jeffrey Scott Furr 1115 Foothills Dr. Pinnacle, NC 27043 4022 Reich St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 760 PW13 Lucy Vasquez PO Box 12367 Wilmington, NC 28405 4030 Reich St.Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 755 PW14 Luis Cortes Ambrosio 4112 Reich St Winston-Salem, NC 27105 4112 Reich St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 655 PW15 Jerry S. Furr 106 Windermere Way King, NC 27021 4114 Reich St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 655 PW16 Yeimy Noyola Leiva 4115 Reich St. Winston-Salem, NC 27105 4115 Reich St. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 790 PW17 Tawana J. Mciver 301 Polo Rd. Winston-Salem, NC 27105 301 Polo Rd. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 618 PW18 James R. Harrington 217 Polo Rd. Winston-Salem, NC 27105 217 Polo Rd. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 1,183 PW19 Edsel L. Spainhour 223 Craft Dr. Winston-Salem, NC 27105 223 Craft Dr. Winston-Salem, NC 27105 unknown unknown unknown unknown unknown 1,278 BGS = Below Ground SurfaceWell ID numbers are displayed on Figure 5 Table 2 Water Supply Well Information 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034   RECORD OF COMMUNICATION EAS PROJECT NO. 225234 Project Name: Brownfields Assessment Report, 450 Polo Road Property, Winston-Salem, NC Location: 450 Polo Road, Winston-Salem, NC Communication with: Ms. Sandy (last name withheld), Supervisor of City Link for Winston-Salem Of: City of Winston-Salem Phone: 336-727-8000 Communication via: (X) Telephone ( ) Discussion during site inspection ( ) Email ( ) Office visit/meeting at ( ) Letter Recorded by: W. Godfrey Time: 3:10 pm Date: 1-12-2023 Subject: Water Provider Summary of Communication: EAS spoke with Ms. Sandy (last name withheld), Supervisor with City Link for Winston-Salem, who stated that municipal water in the subject property area is provided by Winston-Salem/Forsyth County Utilities.   RECORD OF COMMUNICATION EAS PROJECT NO. 225234 Project Name: Brownfields Assessment Report, 450 Polo Road Property, Winston-Salem, NC Location: 450 Polo Road, Winston-Salem, NC Communication with: Ms. Nancy Schuh, Senior Office Assistant Of: Forsyth County Division of Environmental Health Phone: 336-703-3225 Communication via: (X) Telephone ( ) Discussion during site inspection ( ) Email ( ) Office visit/meeting at ( ) Letter Recorded by: W. Godfrey Time: 2:41 pm Date: 12-20-2022 Subject: Private Wells Summary of Communication: EAS spoke with Ms. Nancy Schuh, Senior Office Assistant with Forsyth County’s Division of Environmental Health, who stated that they have no records of private wells (irrigation or drinking) for the subject property. She stated that the county does not have a GIS/mapping tool that shows private wells. Brownfields Assessment Report 450 Polo road Winston Salem, NC EAS No. 22-5234 March 2023 ATTACHMENT H Laboratory Data Sheets ANALYTICAL REPORT November 30, 2022 EAS Professionals, Inc. Sample Delivery Group:L1557235 Samples Received:11/12/2022 Project Number:EAS-225234 Description:450 Polo Road Report To:Derek Ross 9 Pilgrim Road Greenville, SC 29607 Entire Report Reviewed By: November 30, 2022 [Preliminary Report] Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 1 of 96 November 30, 2022 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 1 of 96 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 7 Sr: Sample Results 8 SS-1 L1557235-01 8 SS-1-A L1557235-02 11 SS-2 L1557235-03 14 SS-2-A L1557235-04 17 SS-3 L1557235-05 20 SS-3-A L1557235-06 23 SS-4 L1557235-07 26 SS-4-A L1557235-08 29 SS-5 L1557235-09 32 SS-5-A L1557235-10 35 SS-6 L1557235-11 38 SS-6-A L1557235-12 41 SS-7 L1557235-13 44 SS-7-A L1557235-14 47 SS-8 L1557235-15 50 SS-8-A L1557235-16 53 SS-2 (DUP) L1557235-17 56 SS-2-A (DUP) L1557235-18 59 SS-3 (DUP) L1557235-19 62 SS-3-A (DUP) L1557235-20 65 Qc: Quality Control Summary 68 Total Solids by Method 2540 G-2011 68 Mercury by Method 7471B 70 Metals (ICPMS) by Method 6020B 73 Volatile Organic Compounds (GC/MS) by Method 8260D 75 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 84 Gl: Glossary of Terms 90 Al: Accreditations & Locations 92 Sc: Sample Chain of Custody 93 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 2 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 2 of 96 SAMPLE SUMMARY Collected by Collected date/time Received date/time SS-1 L1557235-01 Solid Westley Godfrey 11/10/22 12:15 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:12 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:08 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1.12 11/10/22 12:15 11/17/22 15:52 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1.12 11/10/22 12:15 11/23/22 14:33 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 22:24 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-1-A L1557235-02 Solid Westley Godfrey 11/10/22 12:25 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:14 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:25 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 12:25 11/17/22 16:12 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 12:25 11/23/22 14:52 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 21:03 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-2 L1557235-03 Solid Westley Godfrey 11/10/22 11:30 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:16 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:28 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 11:30 11/17/22 16:34 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 11:30 11/23/22 15:11 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 22:44 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-2-A L1557235-04 Solid Westley Godfrey 11/10/22 11:40 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:19 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:32 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1.13 11/10/22 11:40 11/17/22 16:55 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1.13 11/10/22 11:40 11/23/22 16:27 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 19:22 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-3 L1557235-05 Solid Westley Godfrey 11/10/22 15:15 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:21 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:42 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:15 11/17/22 17:16 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 15:15 11/23/22 16:46 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 21:23 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 3 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 3 of 96 SAMPLE SUMMARY Collected by Collected date/time Received date/time SS-3-A L1557235-06 Solid Westley Godfrey 11/10/22 15:15 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:23 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:45 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1.2 11/10/22 15:15 11/17/22 17:38 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1.2 11/10/22 15:15 11/23/22 17:05 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 21:43 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-4 L1557235-07 Solid Westley Godfrey 11/10/22 15:25 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:26 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:48 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1.06 11/10/22 15:25 11/17/22 17:59 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1.06 11/10/22 15:25 11/23/22 17:24 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 22:04 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-4-A L1557235-08 Solid Westley Godfrey 11/10/22 15:25 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:28 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:52 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1.02 11/10/22 15:25 11/17/22 18:20 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1.02 11/10/22 15:25 11/23/22 18:13 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 20:23 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-5 L1557235-09 Solid Westley Godfrey 11/10/22 15:40 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:35 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:55 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:40 11/17/22 18:41 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 15:40 11/23/22 18:32 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 18:21 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-5-A L1557235-10 Solid Westley Godfrey 11/10/22 15:40 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959829 1 11/16/22 08:04 11/16/22 08:20 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960559 1 11/16/22 11:11 11/17/22 13:38 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1966023 5 11/28/22 16:36 11/28/22 20:58 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:40 11/17/22 19:03 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 15:40 11/23/22 18:51 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 19:42 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 4 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 4 of 96 SAMPLE SUMMARY Collected by Collected date/time Received date/time SS-6 L1557235-11 Solid Westley Godfrey 11/10/22 15:55 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960561 1 11/16/22 11:09 11/17/22 14:29 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:30 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:55 11/17/22 19:24 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 15:55 11/23/22 19:10 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 19:02 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-6-A L1557235-12 Solid Westley Godfrey 11/10/22 15:55 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960561 1 11/16/22 11:09 11/17/22 14:32 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:33 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:55 11/17/22 19:45 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1963991 1 11/10/22 15:55 11/23/22 19:29 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 20:02 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-7 L1557235-13 Solid Westley Godfrey 11/10/22 15:45 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960561 1 11/16/22 11:09 11/17/22 14:34 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:36 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961410 1 11/10/22 15:45 11/17/22 20:06 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 23:24 JRM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 5 11/18/22 05:50 11/22/22 20:28 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-7-A L1557235-14 Solid Westley Godfrey 11/10/22 15:55 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960561 1 11/16/22 11:09 11/17/22 14:37 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:48 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1 11/10/22 15:55 11/18/22 05:51 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 18:42 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-8 L1557235-15 Solid Westley Godfrey 11/10/22 14:50 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 15:43 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:52 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1.22 11/10/22 14:50 11/18/22 06:10 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 20:43 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 5 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 5 of 96 SAMPLE SUMMARY Collected by Collected date/time Received date/time SS-8-A L1557235-16 Solid Westley Godfrey 11/10/22 15:00 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 15:45 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:55 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1.11 11/10/22 15:00 11/18/22 06:28 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 18:01 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-2 (DUP) L1557235-17 Solid Westley Godfrey 11/10/22 11:30 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 16:23 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 20:58 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1 11/10/22 11:30 11/18/22 06:47 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 23:04 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-2-A (DUP) L1557235-18 Solid Westley Godfrey 11/10/22 11:40 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 16:26 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 21:02 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1.04 11/10/22 11:40 11/18/22 07:06 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 17:00 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-3 (DUP) L1557235-19 Solid Westley Godfrey 11/10/22 15:15 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 16:28 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 21:05 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1.01 11/10/22 15:15 11/18/22 07:25 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 16:20 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time SS-3-A (DUP) L1557235-20 Solid Westley Godfrey 11/10/22 15:15 11/12/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1959833 1 11/16/22 09:11 11/16/22 09:28 CMK Mt. Juliet, TN Mercury by Method 7471B WG1960568 1 11/16/22 11:07 11/17/22 16:31 SRT Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961432 5 11/28/22 17:46 11/29/22 21:08 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1961734 1 11/10/22 15:15 11/18/22 07:44 ACG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1960983 1 11/18/22 05:50 11/18/22 16:40 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 6 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 6 of 96 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Heather J Wagner Project Manager 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 7 of 96 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 7 of 96 SAMPLE RESULTS - 01 L1557235 SS-1 Collected date/time: 11/10/22 12:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 81.2 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0502 0.0222 0.0493 1 11/17/2022 13:12 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 3.15 0.123 1.23 5 11/28/2022 20:08 WG1966023 Barium 15.0 0.187 3.08 5 11/28/2022 20:08 WG1966023 Cadmium U 0.105 1.23 5 11/28/2022 20:08 WG1966023 Chromium 8.82 0.365 6.16 5 11/28/2022 20:08 WG1966023 Lead 17.2 0.122 2.46 5 11/28/2022 20:08 WG1966023 Selenium 0.249 J 0.222 3.08 5 11/28/2022 20:08 WG1966023 Silver U 0.107 0.616 5 11/28/2022 20:08 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0588 0.0806 1.12 11/17/2022 15:52 WG1961410 Acrylonitrile U 0.00581 0.0201 1.12 11/17/2022 15:52 WG1961410 Benzene U 0.000752 0.00161 1.12 11/17/2022 15:52 WG1961410 Bromobenzene U 0.00145 0.0201 1.12 11/17/2022 15:52 WG1961410 Bromodichloromethane U 0.00117 0.00403 1.12 11/17/2022 15:52 WG1961410 Bromoform U 0.00188 0.0403 1.12 11/17/2022 15:52 WG1961410 Bromomethane U 0.00318 0.0201 1.12 11/17/2022 15:52 WG1961410 n-Butylbenzene U 0.00846 0.0201 1.12 11/17/2022 15:52 WG1961410 sec-Butylbenzene U 0.00465 0.0201 1.12 11/17/2022 15:52 WG1961410 tert-Butylbenzene U C3 0.00314 0.00806 1.12 11/17/2022 15:52 WG1961410 Carbon tetrachloride U 0.00145 0.00806 1.12 11/17/2022 15:52 WG1961410 Chlorobenzene U 0.000338 0.00403 1.12 11/17/2022 15:52 WG1961410 Chlorodibromomethane U 0.000985 0.00403 1.12 11/17/2022 15:52 WG1961410 Chloroethane U 0.00273 0.00806 1.12 11/17/2022 15:52 WG1961410 Chloroform U 0.00165 0.00403 1.12 11/17/2022 15:52 WG1961410 Chloromethane U 0.00701 0.0201 1.12 11/17/2022 15:52 WG1961410 2-Chlorotoluene U 0.00139 0.00403 1.12 11/17/2022 15:52 WG1961410 4-Chlorotoluene U 0.000725 0.00806 1.12 11/17/2022 15:52 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00629 0.0403 1.12 11/17/2022 15:52 WG1961410 1,2-Dibromoethane U 0.00104 0.00403 1.12 11/17/2022 15:52 WG1961410 Dibromomethane U 0.00121 0.00806 1.12 11/17/2022 15:52 WG1961410 1,2-Dichlorobenzene U 0.000685 0.00806 1.12 11/17/2022 15:52 WG1961410 1,3-Dichlorobenzene U 0.000967 0.00806 1.12 11/17/2022 15:52 WG1961410 1,4-Dichlorobenzene U 0.00113 0.00806 1.12 11/17/2022 15:52 WG1961410 Dichlorodifluoromethane U 0.00259 0.00403 1.12 11/17/2022 15:52 WG1961410 1,1-Dichloroethane U 0.000791 0.00403 1.12 11/17/2022 15:52 WG1961410 1,2-Dichloroethane U 0.00105 0.00403 1.12 11/17/2022 15:52 WG1961410 1,1-Dichloroethene U 0.000977 0.00403 1.12 11/17/2022 15:52 WG1961410 cis-1,2-Dichloroethene U 0.00118 0.00403 1.12 11/17/2022 15:52 WG1961410 trans-1,2-Dichloroethene U 0.00167 0.00806 1.12 11/17/2022 15:52 WG1961410 1,2-Dichloropropane U 0.00229 0.00806 1.12 11/17/2022 15:52 WG1961410 1,1-Dichloropropene U 0.00130 0.00403 1.12 11/17/2022 15:52 WG1961410 1,3-Dichloropropane U 0.000807 0.00806 1.12 11/17/2022 15:52 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 8 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 8 of 96 SAMPLE RESULTS - 01 L1557235 SS-1 Collected date/time: 11/10/22 12:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00122 0.00403 1.12 11/17/2022 15:52 WG1961410 trans-1,3-Dichloropropene U 0.00184 0.00806 1.12 11/17/2022 15:52 WG1961410 2,2-Dichloropropane U 0.00223 0.00403 1.12 11/17/2022 15:52 WG1961410 Di-isopropyl ether U 0.000660 0.00161 1.12 11/17/2022 15:52 WG1961410 Ethylbenzene U 0.00119 0.00403 1.12 11/17/2022 15:52 WG1961410 Hexachloro-1,3-butadiene U 0.00967 0.0403 1.12 11/17/2022 15:52 WG1961410 Isopropylbenzene U 0.000685 0.00403 1.12 11/17/2022 15:52 WG1961410 p-Isopropyltoluene U 0.00411 0.00806 1.12 11/17/2022 15:52 WG1961410 2-Butanone (MEK)U 0.102 0.161 1.12 11/17/2022 15:52 WG1961410 Methylene Chloride U 0.0107 0.0403 1.12 11/17/2022 15:52 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00367 0.0403 1.12 11/17/2022 15:52 WG1961410 Methyl tert-butyl ether U 0.000564 0.00161 1.12 11/17/2022 15:52 WG1961410 Naphthalene U 0.00787 0.0201 1.12 11/17/2022 15:52 WG1961410 n-Propylbenzene U 0.00152 0.00806 1.12 11/23/2022 14:33 WG1963991 Styrene U 0.000368 0.0201 1.12 11/17/2022 15:52 WG1961410 1,1,1,2-Tetrachloroethane U 0.00152 0.00403 1.12 11/17/2022 15:52 WG1961410 1,1,2,2-Tetrachloroethane U 0.00112 0.00403 1.12 11/17/2022 15:52 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00121 0.00403 1.12 11/17/2022 15:52 WG1961410 Tetrachloroethene 0.00608 0.00144 0.00403 1.12 11/23/2022 14:33 WG1963991 Toluene 0.00757 J 0.00210 0.00806 1.12 11/17/2022 15:52 WG1961410 1,2,3-Trichlorobenzene U 0.0118 0.0201 1.12 11/17/2022 15:52 WG1961410 1,2,4-Trichlorobenzene U 0.00709 0.0201 1.12 11/17/2022 15:52 WG1961410 1,1,1-Trichloroethane U 0.00148 0.00403 1.12 11/17/2022 15:52 WG1961410 1,1,2-Trichloroethane U 0.000962 0.00403 1.12 11/17/2022 15:52 WG1961410 Trichloroethene U 0.000941 0.00161 1.12 11/17/2022 15:52 WG1961410 Trichlorofluoromethane U 0.00133 0.00403 1.12 11/17/2022 15:52 WG1961410 1,2,3-Trichloropropane U 0.00260 0.0201 1.12 11/17/2022 15:52 WG1961410 1,2,4-Trimethylbenzene U 0.00255 0.00806 1.12 11/17/2022 15:52 WG1961410 1,2,3-Trimethylbenzene U 0.00255 0.00806 1.12 11/17/2022 15:52 WG1961410 1,3,5-Trimethylbenzene U 0.00322 0.00806 1.12 11/17/2022 15:52 WG1961410 Vinyl chloride U 0.00187 0.00403 1.12 11/17/2022 15:52 WG1961410 Xylenes, Total 0.00613 B J 0.00142 0.0105 1.12 11/17/2022 15:52 WG1961410 (S) Toluene-d8 116 75.0-131 11/17/2022 15:52 WG1961410 (S) Toluene-d8 104 75.0-131 11/23/2022 14:33 WG1963991 (S) 4-Bromofluorobenzene 107 67.0-138 11/17/2022 15:52 WG1961410 (S) 4-Bromofluorobenzene 101 67.0-138 11/23/2022 14:33 WG1963991 (S) 1,2-Dichloroethane-d4 83.9 70.0-130 11/17/2022 15:52 WG1961410 (S) 1,2-Dichloroethane-d4 83.8 70.0-130 11/23/2022 14:33 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00664 0.0410 1 11/18/2022 22:24 WG1960983 Acenaphthylene U 0.00578 0.0410 1 11/18/2022 22:24 WG1960983 Anthracene U 0.00731 0.0410 1 11/18/2022 22:24 WG1960983 Benzidine U C3 0.0771 2.06 1 11/18/2022 22:24 WG1960983 Benzo(a)anthracene 0.00876 J 0.00723 0.0410 1 11/18/2022 22:24 WG1960983 Benzo(b)fluoranthene 0.0185 J 0.00765 0.0410 1 11/18/2022 22:24 WG1960983 Benzo(k)fluoranthene U 0.00729 0.0410 1 11/18/2022 22:24 WG1960983 Benzo(g,h,i)perylene 0.00929 J 0.00750 0.0410 1 11/18/2022 22:24 WG1960983 Benzo(a)pyrene 0.0139 J 0.00763 0.0410 1 11/18/2022 22:24 WG1960983 Bis(2-chlorethoxy)methane U 0.0123 0.410 1 11/18/2022 22:24 WG1960983 Bis(2-chloroethyl)ether U 0.0136 0.410 1 11/18/2022 22:24 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0177 0.410 1 11/18/2022 22:24 WG1960983 4-Bromophenyl-phenylether U 0.0144 0.410 1 11/18/2022 22:24 WG1960983 2-Chloronaphthalene U 0.00721 0.0410 1 11/18/2022 22:24 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 9 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 9 of 96 SAMPLE RESULTS - 01 L1557235 SS-1 Collected date/time: 11/10/22 12:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0143 0.410 1 11/18/2022 22:24 WG1960983 Chrysene 0.0128 J 0.00816 0.0410 1 11/18/2022 22:24 WG1960983 Dibenz(a,h)anthracene U 0.0114 0.0410 1 11/18/2022 22:24 WG1960983 1,2-Dichlorobenzene U 0.0122 0.410 1 11/18/2022 22:24 WG1960983 1,3-Dichlorobenzene U 0.0124 0.410 1 11/18/2022 22:24 WG1960983 1,4-Dichlorobenzene U 0.0122 0.410 1 11/18/2022 22:24 WG1960983 3,3-Dichlorobenzidine U 0.0152 0.410 1 11/18/2022 22:24 WG1960983 2,4-Dinitrotoluene U 0.0118 0.410 1 11/18/2022 22:24 WG1960983 2,6-Dinitrotoluene U 0.0134 0.410 1 11/18/2022 22:24 WG1960983 Fluoranthene 0.0191 J 0.00741 0.0410 1 11/18/2022 22:24 WG1960983 Fluorene U 0.00668 0.0410 1 11/18/2022 22:24 WG1960983 Hexachlorobenzene U 0.0145 0.410 1 11/18/2022 22:24 WG1960983 Hexachloro-1,3-butadiene U 0.0138 0.410 1 11/18/2022 22:24 WG1960983 Hexachlorocyclopentadiene U 0.0216 0.410 1 11/18/2022 22:24 WG1960983 Hexachloroethane U 0.0161 0.410 1 11/18/2022 22:24 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0116 0.0410 1 11/18/2022 22:24 WG1960983 Isophorone U 0.0126 0.410 1 11/18/2022 22:24 WG1960983 Naphthalene U 0.0103 0.0410 1 11/18/2022 22:24 WG1960983 Nitrobenzene U 0.0143 0.410 1 11/18/2022 22:24 WG1960983 n-Nitrosodimethylamine U 0.0609 0.410 1 11/18/2022 22:24 WG1960983 n-Nitrosodiphenylamine U 0.0310 0.410 1 11/18/2022 22:24 WG1960983 n-Nitrosodi-n-propylamine U 0.0137 0.410 1 11/18/2022 22:24 WG1960983 Phenanthrene 0.0101 J 0.00814 0.0410 1 11/18/2022 22:24 WG1960983 Benzylbutyl phthalate U 0.0128 0.410 1 11/18/2022 22:24 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0520 0.410 1 11/18/2022 22:24 WG1960983 Di-n-butyl phthalate U 0.0140 0.410 1 11/18/2022 22:24 WG1960983 Diethyl phthalate U 0.0136 0.410 1 11/18/2022 22:24 WG1960983 Dimethyl phthalate U 0.0870 0.410 1 11/18/2022 22:24 WG1960983 Di-n-octyl phthalate U 0.0277 0.410 1 11/18/2022 22:24 WG1960983 Pyrene 0.0182 J 0.00798 0.0410 1 11/18/2022 22:24 WG1960983 1,2,4-Trichlorobenzene U 0.0128 0.410 1 11/18/2022 22:24 WG1960983 4-Chloro-3-methylphenol U 0.0133 0.410 1 11/18/2022 22:24 WG1960983 2-Chlorophenol U 0.0136 0.410 1 11/18/2022 22:24 WG1960983 2,4-Dichlorophenol U 0.0120 0.410 1 11/18/2022 22:24 WG1960983 2,4-Dimethylphenol U 0.0107 0.410 1 11/18/2022 22:24 WG1960983 4,6-Dinitro-2-methylphenol U 0.0930 0.410 1 11/18/2022 22:24 WG1960983 2,4-Dinitrophenol U 0.0960 0.410 1 11/18/2022 22:24 WG1960983 2-Nitrophenol U 0.0147 0.410 1 11/18/2022 22:24 WG1960983 4-Nitrophenol U 0.0128 0.410 1 11/18/2022 22:24 WG1960983 Pentachlorophenol U 0.0110 0.410 1 11/18/2022 22:24 WG1960983 Phenol U 0.0165 0.410 1 11/18/2022 22:24 WG1960983 2,4,6-Trichlorophenol U 0.0132 0.410 1 11/18/2022 22:24 WG1960983 (S) 2-Fluorophenol 33.2 12.0-120 11/18/2022 22:24 WG1960983 (S) Phenol-d5 30.8 10.0-120 11/18/2022 22:24 WG1960983 (S) Nitrobenzene-d5 30.1 10.0-122 11/18/2022 22:24 WG1960983 (S) 2-Fluorobiphenyl 28.3 15.0-120 11/18/2022 22:24 WG1960983 (S) 2,4,6-Tribromophenol 40.3 10.0-127 11/18/2022 22:24 WG1960983 (S) p-Terphenyl-d14 33.5 10.0-120 11/18/2022 22:24 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 10 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 10 of 96 SAMPLE RESULTS - 02 L1557235 SS-1-A Collected date/time: 11/10/22 12:25 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 87.1 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0207 0.0459 1 11/17/2022 13:14 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.74 0.115 1.15 5 11/28/2022 20:25 WG1966023 Barium 41.2 0.175 2.87 5 11/28/2022 20:25 WG1966023 Cadmium U 0.0982 1.15 5 11/28/2022 20:25 WG1966023 Chromium 5.51 J 0.340 5.74 5 11/28/2022 20:25 WG1966023 Lead 7.45 0.114 2.30 5 11/28/2022 20:25 WG1966023 Selenium 0.235 J 0.207 2.87 5 11/28/2022 20:25 WG1966023 Silver U 0.0993 0.574 5 11/28/2022 20:25 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0478 0.0655 1 11/17/2022 16:12 WG1961410 Acrylonitrile U 0.00473 0.0164 1 11/17/2022 16:12 WG1961410 Benzene U 0.000611 0.00131 1 11/17/2022 16:12 WG1961410 Bromobenzene U 0.00118 0.0164 1 11/17/2022 16:12 WG1961410 Bromodichloromethane U 0.000949 0.00327 1 11/17/2022 16:12 WG1961410 Bromoform U 0.00153 0.0327 1 11/17/2022 16:12 WG1961410 Bromomethane U 0.00258 0.0164 1 11/17/2022 16:12 WG1961410 n-Butylbenzene U 0.00687 0.0164 1 11/17/2022 16:12 WG1961410 sec-Butylbenzene U 0.00377 0.0164 1 11/17/2022 16:12 WG1961410 tert-Butylbenzene U C3 0.00255 0.00655 1 11/17/2022 16:12 WG1961410 Carbon tetrachloride U 0.00118 0.00655 1 11/17/2022 16:12 WG1961410 Chlorobenzene U 0.000275 0.00327 1 11/17/2022 16:12 WG1961410 Chlorodibromomethane U 0.000801 0.00327 1 11/17/2022 16:12 WG1961410 Chloroethane U 0.00223 0.00655 1 11/17/2022 16:12 WG1961410 Chloroform U 0.00135 0.00327 1 11/17/2022 16:12 WG1961410 Chloromethane U 0.00570 0.0164 1 11/17/2022 16:12 WG1961410 2-Chlorotoluene U 0.00113 0.00327 1 11/17/2022 16:12 WG1961410 4-Chlorotoluene U 0.000589 0.00655 1 11/17/2022 16:12 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00511 0.0327 1 11/17/2022 16:12 WG1961410 1,2-Dibromoethane U 0.000848 0.00327 1 11/17/2022 16:12 WG1961410 Dibromomethane U 0.000982 0.00655 1 11/17/2022 16:12 WG1961410 1,2-Dichlorobenzene U 0.000556 0.00655 1 11/17/2022 16:12 WG1961410 1,3-Dichlorobenzene U 0.000786 0.00655 1 11/17/2022 16:12 WG1961410 1,4-Dichlorobenzene U 0.000917 0.00655 1 11/17/2022 16:12 WG1961410 Dichlorodifluoromethane U 0.00211 0.00327 1 11/17/2022 16:12 WG1961410 1,1-Dichloroethane U 0.000643 0.00327 1 11/17/2022 16:12 WG1961410 1,2-Dichloroethane U 0.000850 0.00327 1 11/17/2022 16:12 WG1961410 1,1-Dichloroethene U 0.000793 0.00327 1 11/17/2022 16:12 WG1961410 cis-1,2-Dichloroethene U 0.000961 0.00327 1 11/17/2022 16:12 WG1961410 trans-1,2-Dichloroethene U 0.00136 0.00655 1 11/17/2022 16:12 WG1961410 1,2-Dichloropropane U 0.00186 0.00655 1 11/17/2022 16:12 WG1961410 1,1-Dichloropropene U 0.00106 0.00327 1 11/17/2022 16:12 WG1961410 1,3-Dichloropropane U 0.000656 0.00655 1 11/17/2022 16:12 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 11 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 11 of 96 SAMPLE RESULTS - 02 L1557235 SS-1-A Collected date/time: 11/10/22 12:25 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.000991 0.00327 1 11/17/2022 16:12 WG1961410 trans-1,3-Dichloropropene U 0.00149 0.00655 1 11/17/2022 16:12 WG1961410 2,2-Dichloropropane U 0.00181 0.00327 1 11/17/2022 16:12 WG1961410 Di-isopropyl ether U 0.000537 0.00131 1 11/17/2022 16:12 WG1961410 Ethylbenzene U 0.000965 0.00327 1 11/17/2022 16:12 WG1961410 Hexachloro-1,3-butadiene U 0.00786 0.0327 1 11/17/2022 16:12 WG1961410 Isopropylbenzene U 0.000556 0.00327 1 11/17/2022 16:12 WG1961410 p-Isopropyltoluene 0.00831 0.00334 0.00655 1 11/17/2022 16:12 WG1961410 2-Butanone (MEK)U 0.0831 0.131 1 11/17/2022 16:12 WG1961410 Methylene Chloride U 0.00869 0.0327 1 11/17/2022 16:12 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00299 0.0327 1 11/17/2022 16:12 WG1961410 Methyl tert-butyl ether U 0.000458 0.00131 1 11/17/2022 16:12 WG1961410 Naphthalene U 0.00639 0.0164 1 11/17/2022 16:12 WG1961410 n-Propylbenzene U 0.00124 0.00655 1 11/23/2022 14:52 WG1963991 Styrene U 0.000300 0.0164 1 11/17/2022 16:12 WG1961410 1,1,1,2-Tetrachloroethane U 0.00124 0.00327 1 11/17/2022 16:12 WG1961410 1,1,2,2-Tetrachloroethane U 0.000910 0.00327 1 11/17/2022 16:12 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.000987 0.00327 1 11/17/2022 16:12 WG1961410 Tetrachloroethene 0.00329 0.00117 0.00327 1 11/23/2022 14:52 WG1963991 Toluene U 0.00170 0.00655 1 11/17/2022 16:12 WG1961410 1,2,3-Trichlorobenzene U 0.00960 0.0164 1 11/17/2022 16:12 WG1961410 1,2,4-Trichlorobenzene U 0.00576 0.0164 1 11/17/2022 16:12 WG1961410 1,1,1-Trichloroethane U 0.00121 0.00327 1 11/17/2022 16:12 WG1961410 1,1,2-Trichloroethane U 0.000782 0.00327 1 11/17/2022 16:12 WG1961410 Trichloroethene U 0.000765 0.00131 1 11/17/2022 16:12 WG1961410 Trichlorofluoromethane U 0.00108 0.00327 1 11/17/2022 16:12 WG1961410 1,2,3-Trichloropropane U 0.00212 0.0164 1 11/17/2022 16:12 WG1961410 1,2,4-Trimethylbenzene U 0.00207 0.00655 1 11/17/2022 16:12 WG1961410 1,2,3-Trimethylbenzene U 0.00207 0.00655 1 11/17/2022 16:12 WG1961410 1,3,5-Trimethylbenzene U 0.00262 0.00655 1 11/17/2022 16:12 WG1961410 Vinyl chloride U 0.00152 0.00327 1 11/17/2022 16:12 WG1961410 Xylenes, Total U 0.00115 0.00851 1 11/17/2022 16:12 WG1961410 (S) Toluene-d8 122 75.0-131 11/17/2022 16:12 WG1961410 (S) Toluene-d8 104 75.0-131 11/23/2022 14:52 WG1963991 (S) 4-Bromofluorobenzene 103 67.0-138 11/17/2022 16:12 WG1961410 (S) 4-Bromofluorobenzene 98.6 67.0-138 11/23/2022 14:52 WG1963991 (S) 1,2-Dichloroethane-d4 81.4 70.0-130 11/17/2022 16:12 WG1961410 (S) 1,2-Dichloroethane-d4 82.4 70.0-130 11/23/2022 14:52 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00619 0.0382 1 11/18/2022 21:03 WG1960983 Acenaphthylene U 0.00538 0.0382 1 11/18/2022 21:03 WG1960983 Anthracene U 0.00681 0.0382 1 11/18/2022 21:03 WG1960983 Benzidine U C3 0.0719 1.92 1 11/18/2022 21:03 WG1960983 Benzo(a)anthracene U 0.00674 0.0382 1 11/18/2022 21:03 WG1960983 Benzo(b)fluoranthene U 0.00713 0.0382 1 11/18/2022 21:03 WG1960983 Benzo(k)fluoranthene U 0.00680 0.0382 1 11/18/2022 21:03 WG1960983 Benzo(g,h,i)perylene U 0.00699 0.0382 1 11/18/2022 21:03 WG1960983 Benzo(a)pyrene U 0.00711 0.0382 1 11/18/2022 21:03 WG1960983 Bis(2-chlorethoxy)methane U 0.0115 0.382 1 11/18/2022 21:03 WG1960983 Bis(2-chloroethyl)ether U 0.0126 0.382 1 11/18/2022 21:03 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0165 0.382 1 11/18/2022 21:03 WG1960983 4-Bromophenyl-phenylether U 0.0134 0.382 1 11/18/2022 21:03 WG1960983 2-Chloronaphthalene U 0.00672 0.0382 1 11/18/2022 21:03 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 12 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 12 of 96 SAMPLE RESULTS - 02 L1557235 SS-1-A Collected date/time: 11/10/22 12:25 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0133 0.382 1 11/18/2022 21:03 WG1960983 Chrysene U 0.00760 0.0382 1 11/18/2022 21:03 WG1960983 Dibenz(a,h)anthracene U 0.0106 0.0382 1 11/18/2022 21:03 WG1960983 1,2-Dichlorobenzene U 0.0113 0.382 1 11/18/2022 21:03 WG1960983 1,3-Dichlorobenzene U 0.0116 0.382 1 11/18/2022 21:03 WG1960983 1,4-Dichlorobenzene U 0.0114 0.382 1 11/18/2022 21:03 WG1960983 3,3-Dichlorobenzidine U 0.0141 0.382 1 11/18/2022 21:03 WG1960983 2,4-Dinitrotoluene U 0.0110 0.382 1 11/18/2022 21:03 WG1960983 2,6-Dinitrotoluene U 0.0125 0.382 1 11/18/2022 21:03 WG1960983 Fluoranthene U 0.00690 0.0382 1 11/18/2022 21:03 WG1960983 Fluorene U 0.00622 0.0382 1 11/18/2022 21:03 WG1960983 Hexachlorobenzene U 0.0135 0.382 1 11/18/2022 21:03 WG1960983 Hexachloro-1,3-butadiene U 0.0129 0.382 1 11/18/2022 21:03 WG1960983 Hexachlorocyclopentadiene U 0.0201 0.382 1 11/18/2022 21:03 WG1960983 Hexachloroethane U 0.0150 0.382 1 11/18/2022 21:03 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0108 0.0382 1 11/18/2022 21:03 WG1960983 Isophorone U 0.0117 0.382 1 11/18/2022 21:03 WG1960983 Naphthalene U 0.00960 0.0382 1 11/18/2022 21:03 WG1960983 Nitrobenzene U 0.0133 0.382 1 11/18/2022 21:03 WG1960983 n-Nitrosodimethylamine U 0.0567 0.382 1 11/18/2022 21:03 WG1960983 n-Nitrosodiphenylamine U 0.0289 0.382 1 11/18/2022 21:03 WG1960983 n-Nitrosodi-n-propylamine U 0.0127 0.382 1 11/18/2022 21:03 WG1960983 Phenanthrene U 0.00759 0.0382 1 11/18/2022 21:03 WG1960983 Benzylbutyl phthalate U 0.0119 0.382 1 11/18/2022 21:03 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0484 0.382 1 11/18/2022 21:03 WG1960983 Di-n-butyl phthalate U 0.0131 0.382 1 11/18/2022 21:03 WG1960983 Diethyl phthalate U 0.0126 0.382 1 11/18/2022 21:03 WG1960983 Dimethyl phthalate U 0.0811 0.382 1 11/18/2022 21:03 WG1960983 Di-n-octyl phthalate U 0.0258 0.382 1 11/18/2022 21:03 WG1960983 Pyrene U 0.00744 0.0382 1 11/18/2022 21:03 WG1960983 1,2,4-Trichlorobenzene U 0.0119 0.382 1 11/18/2022 21:03 WG1960983 4-Chloro-3-methylphenol U 0.0124 0.382 1 11/18/2022 21:03 WG1960983 2-Chlorophenol U 0.0126 0.382 1 11/18/2022 21:03 WG1960983 2,4-Dichlorophenol U 0.0111 0.382 1 11/18/2022 21:03 WG1960983 2,4-Dimethylphenol U 0.00999 0.382 1 11/18/2022 21:03 WG1960983 4,6-Dinitro-2-methylphenol U 0.0867 0.382 1 11/18/2022 21:03 WG1960983 2,4-Dinitrophenol U 0.0894 0.382 1 11/18/2022 21:03 WG1960983 2-Nitrophenol U 0.0137 0.382 1 11/18/2022 21:03 WG1960983 4-Nitrophenol U 0.0119 0.382 1 11/18/2022 21:03 WG1960983 Pentachlorophenol U 0.0103 0.382 1 11/18/2022 21:03 WG1960983 Phenol U 0.0154 0.382 1 11/18/2022 21:03 WG1960983 2,4,6-Trichlorophenol U 0.0123 0.382 1 11/18/2022 21:03 WG1960983 (S) 2-Fluorophenol 53.6 12.0-120 11/18/2022 21:03 WG1960983 (S) Phenol-d5 50.5 10.0-120 11/18/2022 21:03 WG1960983 (S) Nitrobenzene-d5 48.6 10.0-122 11/18/2022 21:03 WG1960983 (S) 2-Fluorobiphenyl 46.1 15.0-120 11/18/2022 21:03 WG1960983 (S) 2,4,6-Tribromophenol 66.0 10.0-127 11/18/2022 21:03 WG1960983 (S) p-Terphenyl-d14 54.8 10.0-120 11/18/2022 21:03 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 13 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 13 of 96 SAMPLE RESULTS - 03 L1557235 SS-2 Collected date/time: 11/10/22 11:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 73.1 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0467 J 0.0246 0.0548 1 11/17/2022 13:16 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.77 0.137 1.37 5 11/28/2022 20:28 WG1966023 Barium 20.8 0.208 3.42 5 11/28/2022 20:28 WG1966023 Cadmium 0.129 J 0.117 1.37 5 11/28/2022 20:28 WG1966023 Chromium 6.25 J 0.405 6.84 5 11/28/2022 20:28 WG1966023 Lead 30.7 0.136 2.74 5 11/28/2022 20:28 WG1966023 Selenium U 0.246 3.42 5 11/28/2022 20:28 WG1966023 Silver U 0.118 0.684 5 11/28/2022 20:28 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0646 0.0884 1 11/17/2022 16:34 WG1961410 Acrylonitrile U 0.00639 0.0221 1 11/17/2022 16:34 WG1961410 Benzene U 0.000826 0.00177 1 11/17/2022 16:34 WG1961410 Bromobenzene U 0.00159 0.0221 1 11/17/2022 16:34 WG1961410 Bromodichloromethane U 0.00128 0.00442 1 11/17/2022 16:34 WG1961410 Bromoform U 0.00207 0.0442 1 11/17/2022 16:34 WG1961410 Bromomethane U 0.00348 0.0221 1 11/17/2022 16:34 WG1961410 n-Butylbenzene U 0.00929 0.0221 1 11/17/2022 16:34 WG1961410 sec-Butylbenzene U 0.00509 0.0221 1 11/17/2022 16:34 WG1961410 tert-Butylbenzene U C3 0.00345 0.00884 1 11/17/2022 16:34 WG1961410 Carbon tetrachloride U 0.00159 0.00884 1 11/17/2022 16:34 WG1961410 Chlorobenzene U 0.000371 0.00442 1 11/17/2022 16:34 WG1961410 Chlorodibromomethane U 0.00108 0.00442 1 11/17/2022 16:34 WG1961410 Chloroethane U 0.00301 0.00884 1 11/17/2022 16:34 WG1961410 Chloroform U 0.00182 0.00442 1 11/17/2022 16:34 WG1961410 Chloromethane U 0.00770 0.0221 1 11/17/2022 16:34 WG1961410 2-Chlorotoluene U 0.00153 0.00442 1 11/17/2022 16:34 WG1961410 4-Chlorotoluene U 0.000796 0.00884 1 11/17/2022 16:34 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00690 0.0442 1 11/17/2022 16:34 WG1961410 1,2-Dibromoethane U 0.00115 0.00442 1 11/17/2022 16:34 WG1961410 Dibromomethane U 0.00133 0.00884 1 11/17/2022 16:34 WG1961410 1,2-Dichlorobenzene U 0.000752 0.00884 1 11/17/2022 16:34 WG1961410 1,3-Dichlorobenzene U 0.00106 0.00884 1 11/17/2022 16:34 WG1961410 1,4-Dichlorobenzene U 0.00124 0.00884 1 11/17/2022 16:34 WG1961410 Dichlorodifluoromethane U 0.00285 0.00442 1 11/17/2022 16:34 WG1961410 1,1-Dichloroethane U 0.000869 0.00442 1 11/17/2022 16:34 WG1961410 1,2-Dichloroethane U 0.00115 0.00442 1 11/17/2022 16:34 WG1961410 1,1-Dichloroethene U 0.00107 0.00442 1 11/17/2022 16:34 WG1961410 cis-1,2-Dichloroethene U 0.00130 0.00442 1 11/17/2022 16:34 WG1961410 trans-1,2-Dichloroethene U 0.00184 0.00884 1 11/17/2022 16:34 WG1961410 1,2-Dichloropropane U 0.00251 0.00884 1 11/17/2022 16:34 WG1961410 1,1-Dichloropropene U 0.00143 0.00442 1 11/17/2022 16:34 WG1961410 1,3-Dichloropropane U 0.000886 0.00884 1 11/17/2022 16:34 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 14 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 14 of 96 SAMPLE RESULTS - 03 L1557235 SS-2 Collected date/time: 11/10/22 11:30 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00134 0.00442 1 11/17/2022 16:34 WG1961410 trans-1,3-Dichloropropene U 0.00202 0.00884 1 11/17/2022 16:34 WG1961410 2,2-Dichloropropane U 0.00244 0.00442 1 11/17/2022 16:34 WG1961410 Di-isopropyl ether U 0.000725 0.00177 1 11/17/2022 16:34 WG1961410 Ethylbenzene 0.00200 B J 0.00130 0.00442 1 11/17/2022 16:34 WG1961410 Hexachloro-1,3-butadiene U 0.0106 0.0442 1 11/17/2022 16:34 WG1961410 Isopropylbenzene U 0.000752 0.00442 1 11/17/2022 16:34 WG1961410 p-Isopropyltoluene 0.00716 J 0.00451 0.00884 1 11/17/2022 16:34 WG1961410 2-Butanone (MEK)U 0.112 0.177 1 11/17/2022 16:34 WG1961410 Methylene Chloride U 0.0117 0.0442 1 11/17/2022 16:34 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00403 0.0442 1 11/17/2022 16:34 WG1961410 Methyl tert-butyl ether U 0.000619 0.00177 1 11/17/2022 16:34 WG1961410 Naphthalene U 0.00863 0.0221 1 11/17/2022 16:34 WG1961410 n-Propylbenzene U 0.00168 0.00884 1 11/23/2022 15:11 WG1963991 Styrene U 0.000405 0.0221 1 11/17/2022 16:34 WG1961410 1,1,1,2-Tetrachloroethane U 0.00168 0.00442 1 11/17/2022 16:34 WG1961410 1,1,2,2-Tetrachloroethane U 0.00123 0.00442 1 11/17/2022 16:34 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00133 0.00442 1 11/17/2022 16:34 WG1961410 Tetrachloroethene U 0.00159 0.00442 1 11/17/2022 16:34 WG1961410 Toluene U 0.00230 0.00884 1 11/17/2022 16:34 WG1961410 1,2,3-Trichlorobenzene U 0.0130 0.0221 1 11/17/2022 16:34 WG1961410 1,2,4-Trichlorobenzene U 0.00778 0.0221 1 11/17/2022 16:34 WG1961410 1,1,1-Trichloroethane U 0.00163 0.00442 1 11/17/2022 16:34 WG1961410 1,1,2-Trichloroethane U 0.00106 0.00442 1 11/17/2022 16:34 WG1961410 Trichloroethene U 0.00103 0.00177 1 11/17/2022 16:34 WG1961410 Trichlorofluoromethane U 0.00146 0.00442 1 11/17/2022 16:34 WG1961410 1,2,3-Trichloropropane U 0.00287 0.0221 1 11/17/2022 16:34 WG1961410 1,2,4-Trimethylbenzene U 0.00279 0.00884 1 11/17/2022 16:34 WG1961410 1,2,3-Trimethylbenzene U 0.00279 0.00884 1 11/17/2022 16:34 WG1961410 1,3,5-Trimethylbenzene U 0.00354 0.00884 1 11/17/2022 16:34 WG1961410 Vinyl chloride U 0.00205 0.00442 1 11/17/2022 16:34 WG1961410 Xylenes, Total 0.00188 B J 0.00156 0.0115 1 11/17/2022 16:34 WG1961410 (S) Toluene-d8 118 75.0-131 11/17/2022 16:34 WG1961410 (S) Toluene-d8 104 75.0-131 11/23/2022 15:11 WG1963991 (S) 4-Bromofluorobenzene 104 67.0-138 11/17/2022 16:34 WG1961410 (S) 4-Bromofluorobenzene 97.5 67.0-138 11/23/2022 15:11 WG1963991 (S) 1,2-Dichloroethane-d4 80.6 70.0-130 11/17/2022 16:34 WG1961410 (S) 1,2-Dichloroethane-d4 81.3 70.0-130 11/23/2022 15:11 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00738 0.0456 1 11/18/2022 22:44 WG1960983 Acenaphthylene U 0.00642 0.0456 1 11/18/2022 22:44 WG1960983 Anthracene U 0.00812 0.0456 1 11/18/2022 22:44 WG1960983 Benzidine U C3 0.0857 2.29 1 11/18/2022 22:44 WG1960983 Benzo(a)anthracene U 0.00803 0.0456 1 11/18/2022 22:44 WG1960983 Benzo(b)fluoranthene 0.0155 J 0.00850 0.0456 1 11/18/2022 22:44 WG1960983 Benzo(k)fluoranthene U 0.00810 0.0456 1 11/18/2022 22:44 WG1960983 Benzo(g,h,i)perylene U 0.00834 0.0456 1 11/18/2022 22:44 WG1960983 Benzo(a)pyrene 0.0106 J 0.00847 0.0456 1 11/18/2022 22:44 WG1960983 Bis(2-chlorethoxy)methane U 0.0137 0.456 1 11/18/2022 22:44 WG1960983 Bis(2-chloroethyl)ether U 0.0151 0.456 1 11/18/2022 22:44 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0197 0.456 1 11/18/2022 22:44 WG1960983 4-Bromophenyl-phenylether U 0.0160 0.456 1 11/18/2022 22:44 WG1960983 2-Chloronaphthalene U 0.00801 0.0456 1 11/18/2022 22:44 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 15 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 15 of 96 SAMPLE RESULTS - 03 L1557235 SS-2 Collected date/time: 11/10/22 11:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0159 0.456 1 11/18/2022 22:44 WG1960983 Chrysene 0.0118 J 0.00906 0.0456 1 11/18/2022 22:44 WG1960983 Dibenz(a,h)anthracene U 0.0126 0.0456 1 11/18/2022 22:44 WG1960983 1,2-Dichlorobenzene U 0.0135 0.456 1 11/18/2022 22:44 WG1960983 1,3-Dichlorobenzene U 0.0138 0.456 1 11/18/2022 22:44 WG1960983 1,4-Dichlorobenzene U 0.0136 0.456 1 11/18/2022 22:44 WG1960983 3,3-Dichlorobenzidine U 0.0168 0.456 1 11/18/2022 22:44 WG1960983 2,4-Dinitrotoluene U 0.0131 0.456 1 11/18/2022 22:44 WG1960983 2,6-Dinitrotoluene U 0.0149 0.456 1 11/18/2022 22:44 WG1960983 Fluoranthene 0.0175 J 0.00823 0.0456 1 11/18/2022 22:44 WG1960983 Fluorene U 0.00742 0.0456 1 11/18/2022 22:44 WG1960983 Hexachlorobenzene U 0.0162 0.456 1 11/18/2022 22:44 WG1960983 Hexachloro-1,3-butadiene U 0.0153 0.456 1 11/18/2022 22:44 WG1960983 Hexachlorocyclopentadiene U 0.0240 0.456 1 11/18/2022 22:44 WG1960983 Hexachloroethane U 0.0179 0.456 1 11/18/2022 22:44 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0129 0.0456 1 11/18/2022 22:44 WG1960983 Isophorone U 0.0140 0.456 1 11/18/2022 22:44 WG1960983 Naphthalene 0.0840 0.0114 0.0456 1 11/18/2022 22:44 WG1960983 Nitrobenzene U 0.0159 0.456 1 11/18/2022 22:44 WG1960983 n-Nitrosodimethylamine U 0.0676 0.456 1 11/18/2022 22:44 WG1960983 n-Nitrosodiphenylamine U 0.0345 0.456 1 11/18/2022 22:44 WG1960983 n-Nitrosodi-n-propylamine U 0.0152 0.456 1 11/18/2022 22:44 WG1960983 Phenanthrene 0.0133 J 0.00905 0.0456 1 11/18/2022 22:44 WG1960983 Benzylbutyl phthalate U 0.0142 0.456 1 11/18/2022 22:44 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0578 0.456 1 11/18/2022 22:44 WG1960983 Di-n-butyl phthalate U 0.0156 0.456 1 11/18/2022 22:44 WG1960983 Diethyl phthalate U 0.0151 0.456 1 11/18/2022 22:44 WG1960983 Dimethyl phthalate U 0.0966 0.456 1 11/18/2022 22:44 WG1960983 Di-n-octyl phthalate U 0.0308 0.456 1 11/18/2022 22:44 WG1960983 Pyrene 0.0162 J 0.00887 0.0456 1 11/18/2022 22:44 WG1960983 1,2,4-Trichlorobenzene U 0.0142 0.456 1 11/18/2022 22:44 WG1960983 4-Chloro-3-methylphenol U 0.0148 0.456 1 11/18/2022 22:44 WG1960983 2-Chlorophenol U 0.0151 0.456 1 11/18/2022 22:44 WG1960983 2,4-Dichlorophenol U 0.0133 0.456 1 11/18/2022 22:44 WG1960983 2,4-Dimethylphenol U 0.0119 0.456 1 11/18/2022 22:44 WG1960983 4,6-Dinitro-2-methylphenol U 0.103 0.456 1 11/18/2022 22:44 WG1960983 2,4-Dinitrophenol U 0.107 0.456 1 11/18/2022 22:44 WG1960983 2-Nitrophenol U 0.0163 0.456 1 11/18/2022 22:44 WG1960983 4-Nitrophenol U 0.0142 0.456 1 11/18/2022 22:44 WG1960983 Pentachlorophenol U 0.0123 0.456 1 11/18/2022 22:44 WG1960983 Phenol U 0.0183 0.456 1 11/18/2022 22:44 WG1960983 2,4,6-Trichlorophenol U 0.0146 0.456 1 11/18/2022 22:44 WG1960983 (S) 2-Fluorophenol 46.8 12.0-120 11/18/2022 22:44 WG1960983 (S) Phenol-d5 43.9 10.0-120 11/18/2022 22:44 WG1960983 (S) Nitrobenzene-d5 40.9 10.0-122 11/18/2022 22:44 WG1960983 (S) 2-Fluorobiphenyl 40.9 15.0-120 11/18/2022 22:44 WG1960983 (S) 2,4,6-Tribromophenol 58.3 10.0-127 11/18/2022 22:44 WG1960983 (S) p-Terphenyl-d14 47.3 10.0-120 11/18/2022 22:44 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 16 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 16 of 96 SAMPLE RESULTS - 04 L1557235 SS-2-A Collected date/time: 11/10/22 11:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 76.4 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.165 0.0236 0.0523 1 11/17/2022 13:19 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.43 0.131 1.31 5 11/28/2022 20:32 WG1966023 Barium 21.2 0.199 3.27 5 11/28/2022 20:32 WG1966023 Cadmium U 0.112 1.31 5 11/28/2022 20:32 WG1966023 Chromium 17.5 0.387 6.54 5 11/28/2022 20:32 WG1966023 Lead 9.53 0.130 2.62 5 11/28/2022 20:32 WG1966023 Selenium 0.496 J 0.236 3.27 5 11/28/2022 20:32 WG1966023 Silver U 0.113 0.654 5 11/28/2022 20:32 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0652 0.0894 1.13 11/17/2022 16:55 WG1961410 Acrylonitrile U 0.00645 0.0223 1.13 11/17/2022 16:55 WG1961410 Benzene U 0.000835 0.00179 1.13 11/17/2022 16:55 WG1961410 Bromobenzene U 0.00161 0.0223 1.13 11/17/2022 16:55 WG1961410 Bromodichloromethane U 0.00130 0.00448 1.13 11/17/2022 16:55 WG1961410 Bromoform U 0.00209 0.0448 1.13 11/17/2022 16:55 WG1961410 Bromomethane U 0.00353 0.0223 1.13 11/17/2022 16:55 WG1961410 n-Butylbenzene U 0.00938 0.0223 1.13 11/17/2022 16:55 WG1961410 sec-Butylbenzene U 0.00514 0.0223 1.13 11/17/2022 16:55 WG1961410 tert-Butylbenzene U 0.00348 0.00894 1.13 11/23/2022 16:27 WG1963991 Carbon tetrachloride U 0.00160 0.00894 1.13 11/17/2022 16:55 WG1961410 Chlorobenzene U 0.000375 0.00448 1.13 11/17/2022 16:55 WG1961410 Chlorodibromomethane U 0.00109 0.00448 1.13 11/17/2022 16:55 WG1961410 Chloroethane U 0.00304 0.00894 1.13 11/17/2022 16:55 WG1961410 Chloroform U 0.00183 0.00448 1.13 11/17/2022 16:55 WG1961410 Chloromethane U 0.00778 0.0223 1.13 11/17/2022 16:55 WG1961410 2-Chlorotoluene U 0.00155 0.00448 1.13 11/17/2022 16:55 WG1961410 4-Chlorotoluene U 0.000805 0.00894 1.13 11/17/2022 16:55 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00697 0.0448 1.13 11/17/2022 16:55 WG1961410 1,2-Dibromoethane U 0.00116 0.00448 1.13 11/17/2022 16:55 WG1961410 Dibromomethane U 0.00134 0.00894 1.13 11/17/2022 16:55 WG1961410 1,2-Dichlorobenzene U 0.000759 0.00894 1.13 11/17/2022 16:55 WG1961410 1,3-Dichlorobenzene U 0.00107 0.00894 1.13 11/17/2022 16:55 WG1961410 1,4-Dichlorobenzene U 0.00125 0.00894 1.13 11/17/2022 16:55 WG1961410 Dichlorodifluoromethane U 0.00288 0.00448 1.13 11/17/2022 16:55 WG1961410 1,1-Dichloroethane U 0.000878 0.00448 1.13 11/17/2022 16:55 WG1961410 1,2-Dichloroethane U 0.00116 0.00448 1.13 11/17/2022 16:55 WG1961410 1,1-Dichloroethene U 0.00108 0.00448 1.13 11/17/2022 16:55 WG1961410 cis-1,2-Dichloroethene U 0.00131 0.00448 1.13 11/17/2022 16:55 WG1961410 trans-1,2-Dichloroethene U 0.00187 0.00894 1.13 11/17/2022 16:55 WG1961410 1,2-Dichloropropane U 0.00253 0.00894 1.13 11/17/2022 16:55 WG1961410 1,1-Dichloropropene U 0.00145 0.00448 1.13 11/17/2022 16:55 WG1961410 1,3-Dichloropropane U 0.000895 0.00894 1.13 11/17/2022 16:55 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 17 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 17 of 96 SAMPLE RESULTS - 04 L1557235 SS-2-A Collected date/time: 11/10/22 11:40 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00135 0.00448 1.13 11/17/2022 16:55 WG1961410 trans-1,3-Dichloropropene U 0.00204 0.00894 1.13 11/17/2022 16:55 WG1961410 2,2-Dichloropropane U 0.00247 0.00448 1.13 11/17/2022 16:55 WG1961410 Di-isopropyl ether U 0.000732 0.00179 1.13 11/17/2022 16:55 WG1961410 Ethylbenzene U 0.00132 0.00448 1.13 11/17/2022 16:55 WG1961410 Hexachloro-1,3-butadiene U 0.0107 0.0448 1.13 11/17/2022 16:55 WG1961410 Isopropylbenzene U 0.000759 0.00448 1.13 11/17/2022 16:55 WG1961410 p-Isopropyltoluene U 0.00455 0.00894 1.13 11/17/2022 16:55 WG1961410 2-Butanone (MEK)U 0.114 0.179 1.13 11/17/2022 16:55 WG1961410 Methylene Chloride U 0.0119 0.0448 1.13 11/17/2022 16:55 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00408 0.0448 1.13 11/17/2022 16:55 WG1961410 Methyl tert-butyl ether U 0.000626 0.00179 1.13 11/17/2022 16:55 WG1961410 Naphthalene U 0.00871 0.0223 1.13 11/17/2022 16:55 WG1961410 n-Propylbenzene U 0.00169 0.00894 1.13 11/17/2022 16:55 WG1961410 Styrene U 0.000410 0.0223 1.13 11/17/2022 16:55 WG1961410 1,1,1,2-Tetrachloroethane U 0.00169 0.00448 1.13 11/17/2022 16:55 WG1961410 1,1,2,2-Tetrachloroethane U 0.00124 0.00448 1.13 11/17/2022 16:55 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00135 0.00448 1.13 11/17/2022 16:55 WG1961410 Tetrachloroethene 0.00558 0.00160 0.00448 1.13 11/23/2022 16:27 WG1963991 Toluene U 0.00232 0.00894 1.13 11/17/2022 16:55 WG1961410 1,2,3-Trichlorobenzene U 0.0131 0.0223 1.13 11/17/2022 16:55 WG1961410 1,2,4-Trichlorobenzene U 0.00786 0.0223 1.13 11/17/2022 16:55 WG1961410 1,1,1-Trichloroethane U 0.00164 0.00448 1.13 11/17/2022 16:55 WG1961410 1,1,2-Trichloroethane U 0.00107 0.00448 1.13 11/17/2022 16:55 WG1961410 Trichloroethene U 0.00104 0.00179 1.13 11/17/2022 16:55 WG1961410 Trichlorofluoromethane U 0.00148 0.00448 1.13 11/17/2022 16:55 WG1961410 1,2,3-Trichloropropane U 0.00289 0.0223 1.13 11/17/2022 16:55 WG1961410 1,2,4-Trimethylbenzene U 0.00283 0.00894 1.13 11/17/2022 16:55 WG1961410 1,2,3-Trimethylbenzene U 0.00283 0.00894 1.13 11/17/2022 16:55 WG1961410 1,3,5-Trimethylbenzene U 0.00357 0.00894 1.13 11/17/2022 16:55 WG1961410 Vinyl chloride U 0.00207 0.00448 1.13 11/17/2022 16:55 WG1961410 Xylenes, Total U 0.00157 0.0116 1.13 11/17/2022 16:55 WG1961410 (S) Toluene-d8 115 75.0-131 11/17/2022 16:55 WG1961410 (S) Toluene-d8 103 75.0-131 11/23/2022 16:27 WG1963991 (S) 4-Bromofluorobenzene 102 67.0-138 11/17/2022 16:55 WG1961410 (S) 4-Bromofluorobenzene 96.8 67.0-138 11/23/2022 16:27 WG1963991 (S) 1,2-Dichloroethane-d4 81.0 70.0-130 11/17/2022 16:55 WG1961410 (S) 1,2-Dichloroethane-d4 82.4 70.0-130 11/23/2022 16:27 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00705 0.0436 1 11/18/2022 19:22 WG1960983 Acenaphthylene U 0.00614 0.0436 1 11/18/2022 19:22 WG1960983 Anthracene U 0.00776 0.0436 1 11/18/2022 19:22 WG1960983 Benzidine U C3 0.0819 2.18 1 11/18/2022 19:22 WG1960983 Benzo(a)anthracene U 0.00768 0.0436 1 11/18/2022 19:22 WG1960983 Benzo(b)fluoranthene U 0.00812 0.0436 1 11/18/2022 19:22 WG1960983 Benzo(k)fluoranthene U 0.00775 0.0436 1 11/18/2022 19:22 WG1960983 Benzo(g,h,i)perylene U 0.00797 0.0436 1 11/18/2022 19:22 WG1960983 Benzo(a)pyrene U 0.00810 0.0436 1 11/18/2022 19:22 WG1960983 Bis(2-chlorethoxy)methane U 0.0131 0.436 1 11/18/2022 19:22 WG1960983 Bis(2-chloroethyl)ether U 0.0144 0.436 1 11/18/2022 19:22 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0188 0.436 1 11/18/2022 19:22 WG1960983 4-Bromophenyl-phenylether U 0.0153 0.436 1 11/18/2022 19:22 WG1960983 2-Chloronaphthalene U 0.00765 0.0436 1 11/18/2022 19:22 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 18 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 18 of 96 SAMPLE RESULTS - 04 L1557235 SS-2-A Collected date/time: 11/10/22 11:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0152 0.436 1 11/18/2022 19:22 WG1960983 Chrysene U 0.00866 0.0436 1 11/18/2022 19:22 WG1960983 Dibenz(a,h)anthracene U 0.0121 0.0436 1 11/18/2022 19:22 WG1960983 1,2-Dichlorobenzene U 0.0129 0.436 1 11/18/2022 19:22 WG1960983 1,3-Dichlorobenzene U 0.0132 0.436 1 11/18/2022 19:22 WG1960983 1,4-Dichlorobenzene U 0.0130 0.436 1 11/18/2022 19:22 WG1960983 3,3-Dichlorobenzidine U 0.0161 0.436 1 11/18/2022 19:22 WG1960983 2,4-Dinitrotoluene U 0.0125 0.436 1 11/18/2022 19:22 WG1960983 2,6-Dinitrotoluene U 0.0143 0.436 1 11/18/2022 19:22 WG1960983 Fluoranthene U 0.00786 0.0436 1 11/18/2022 19:22 WG1960983 Fluorene U 0.00709 0.0436 1 11/18/2022 19:22 WG1960983 Hexachlorobenzene U 0.0154 0.436 1 11/18/2022 19:22 WG1960983 Hexachloro-1,3-butadiene U 0.0147 0.436 1 11/18/2022 19:22 WG1960983 Hexachlorocyclopentadiene U 0.0229 0.436 1 11/18/2022 19:22 WG1960983 Hexachloroethane U 0.0171 0.436 1 11/18/2022 19:22 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0123 0.0436 1 11/18/2022 19:22 WG1960983 Isophorone U 0.0133 0.436 1 11/18/2022 19:22 WG1960983 Naphthalene U 0.0109 0.0436 1 11/18/2022 19:22 WG1960983 Nitrobenzene U 0.0152 0.436 1 11/18/2022 19:22 WG1960983 n-Nitrosodimethylamine U 0.0646 0.436 1 11/18/2022 19:22 WG1960983 n-Nitrosodiphenylamine U 0.0330 0.436 1 11/18/2022 19:22 WG1960983 n-Nitrosodi-n-propylamine U 0.0145 0.436 1 11/18/2022 19:22 WG1960983 Phenanthrene U 0.00865 0.0436 1 11/18/2022 19:22 WG1960983 Benzylbutyl phthalate U 0.0136 0.436 1 11/18/2022 19:22 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0552 0.436 1 11/18/2022 19:22 WG1960983 Di-n-butyl phthalate U 0.0149 0.436 1 11/18/2022 19:22 WG1960983 Diethyl phthalate U 0.0144 0.436 1 11/18/2022 19:22 WG1960983 Dimethyl phthalate U 0.0924 0.436 1 11/18/2022 19:22 WG1960983 Di-n-octyl phthalate U 0.0294 0.436 1 11/18/2022 19:22 WG1960983 Pyrene U 0.00848 0.0436 1 11/18/2022 19:22 WG1960983 1,2,4-Trichlorobenzene U 0.0136 0.436 1 11/18/2022 19:22 WG1960983 4-Chloro-3-methylphenol U 0.0141 0.436 1 11/18/2022 19:22 WG1960983 2-Chlorophenol U 0.0144 0.436 1 11/18/2022 19:22 WG1960983 2,4-Dichlorophenol U 0.0127 0.436 1 11/18/2022 19:22 WG1960983 2,4-Dimethylphenol U 0.0114 0.436 1 11/18/2022 19:22 WG1960983 4,6-Dinitro-2-methylphenol U 0.0988 0.436 1 11/18/2022 19:22 WG1960983 2,4-Dinitrophenol U 0.102 0.436 1 11/18/2022 19:22 WG1960983 2-Nitrophenol U 0.0156 0.436 1 11/18/2022 19:22 WG1960983 4-Nitrophenol U 0.0136 0.436 1 11/18/2022 19:22 WG1960983 Pentachlorophenol U 0.0117 0.436 1 11/18/2022 19:22 WG1960983 Phenol U 0.0175 0.436 1 11/18/2022 19:22 WG1960983 2,4,6-Trichlorophenol U 0.0140 0.436 1 11/18/2022 19:22 WG1960983 (S) 2-Fluorophenol 60.6 12.0-120 11/18/2022 19:22 WG1960983 (S) Phenol-d5 56.9 10.0-120 11/18/2022 19:22 WG1960983 (S) Nitrobenzene-d5 54.1 10.0-122 11/18/2022 19:22 WG1960983 (S) 2-Fluorobiphenyl 51.1 15.0-120 11/18/2022 19:22 WG1960983 (S) 2,4,6-Tribromophenol 69.7 10.0-127 11/18/2022 19:22 WG1960983 (S) p-Terphenyl-d14 61.5 10.0-120 11/18/2022 19:22 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 19 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 19 of 96 SAMPLE RESULTS - 05 L1557235 SS-3 Collected date/time: 11/10/22 15:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 82.2 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0289 J 0.0219 0.0487 1 11/17/2022 13:21 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 3.41 0.122 1.22 5 11/28/2022 20:42 WG1966023 Barium 13.3 0.185 3.04 5 11/28/2022 20:42 WG1966023 Cadmium U 0.104 1.22 5 11/28/2022 20:42 WG1966023 Chromium 13.1 0.360 6.08 5 11/28/2022 20:42 WG1966023 Lead 6.52 0.120 2.43 5 11/28/2022 20:42 WG1966023 Selenium 0.220 J 0.219 3.04 5 11/28/2022 20:42 WG1966023 Silver U 0.105 0.608 5 11/28/2022 20:42 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0528 0.0723 1 11/17/2022 17:16 WG1961410 Acrylonitrile U 0.00522 0.0181 1 11/17/2022 17:16 WG1961410 Benzene U 0.000675 0.00145 1 11/17/2022 17:16 WG1961410 Bromobenzene U 0.00130 0.0181 1 11/17/2022 17:16 WG1961410 Bromodichloromethane U 0.00105 0.00361 1 11/17/2022 17:16 WG1961410 Bromoform U 0.00169 0.0361 1 11/17/2022 17:16 WG1961410 Bromomethane U 0.00285 0.0181 1 11/17/2022 17:16 WG1961410 n-Butylbenzene U 0.00759 0.0181 1 11/17/2022 17:16 WG1961410 sec-Butylbenzene U 0.00416 0.0181 1 11/17/2022 17:16 WG1961410 tert-Butylbenzene U C3 0.00282 0.00723 1 11/17/2022 17:16 WG1961410 Carbon tetrachloride U 0.00130 0.00723 1 11/17/2022 17:16 WG1961410 Chlorobenzene U 0.000304 0.00361 1 11/17/2022 17:16 WG1961410 Chlorodibromomethane U 0.000885 0.00361 1 11/17/2022 17:16 WG1961410 Chloroethane U 0.00246 0.00723 1 11/17/2022 17:16 WG1961410 Chloroform U 0.00149 0.00361 1 11/17/2022 17:16 WG1961410 Chloromethane U 0.00629 0.0181 1 11/17/2022 17:16 WG1961410 2-Chlorotoluene U 0.00125 0.00361 1 11/17/2022 17:16 WG1961410 4-Chlorotoluene U 0.000651 0.00723 1 11/17/2022 17:16 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00564 0.0361 1 11/17/2022 17:16 WG1961410 1,2-Dibromoethane U 0.000937 0.00361 1 11/17/2022 17:16 WG1961410 Dibromomethane U 0.00108 0.00723 1 11/17/2022 17:16 WG1961410 1,2-Dichlorobenzene U 0.000614 0.00723 1 11/17/2022 17:16 WG1961410 1,3-Dichlorobenzene U 0.000867 0.00723 1 11/17/2022 17:16 WG1961410 1,4-Dichlorobenzene U 0.00101 0.00723 1 11/17/2022 17:16 WG1961410 Dichlorodifluoromethane U 0.00233 0.00361 1 11/17/2022 17:16 WG1961410 1,1-Dichloroethane U 0.000710 0.00361 1 11/17/2022 17:16 WG1961410 1,2-Dichloroethane U 0.000938 0.00361 1 11/17/2022 17:16 WG1961410 1,1-Dichloroethene U 0.000876 0.00361 1 11/17/2022 17:16 WG1961410 cis-1,2-Dichloroethene U 0.00106 0.00361 1 11/17/2022 17:16 WG1961410 trans-1,2-Dichloroethene U 0.00150 0.00723 1 11/17/2022 17:16 WG1961410 1,2-Dichloropropane U 0.00205 0.00723 1 11/17/2022 17:16 WG1961410 1,1-Dichloropropene U 0.00117 0.00361 1 11/17/2022 17:16 WG1961410 1,3-Dichloropropane U 0.000724 0.00723 1 11/17/2022 17:16 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 20 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 20 of 96 SAMPLE RESULTS - 05 L1557235 SS-3 Collected date/time: 11/10/22 15:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00109 0.00361 1 11/17/2022 17:16 WG1961410 trans-1,3-Dichloropropene U 0.00165 0.00723 1 11/17/2022 17:16 WG1961410 2,2-Dichloropropane U 0.00199 0.00361 1 11/17/2022 17:16 WG1961410 Di-isopropyl ether U 0.000593 0.00145 1 11/17/2022 17:16 WG1961410 Ethylbenzene U 0.00107 0.00361 1 11/17/2022 17:16 WG1961410 Hexachloro-1,3-butadiene U 0.00867 0.0361 1 11/17/2022 17:16 WG1961410 Isopropylbenzene U 0.000614 0.00361 1 11/17/2022 17:16 WG1961410 p-Isopropyltoluene 0.00704 J 0.00369 0.00723 1 11/17/2022 17:16 WG1961410 2-Butanone (MEK)U 0.0918 0.145 1 11/17/2022 17:16 WG1961410 Methylene Chloride U 0.00960 0.0361 1 11/17/2022 17:16 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00330 0.0361 1 11/17/2022 17:16 WG1961410 Methyl tert-butyl ether U 0.000506 0.00145 1 11/17/2022 17:16 WG1961410 Naphthalene U 0.00705 0.0181 1 11/17/2022 17:16 WG1961410 n-Propylbenzene U 0.00137 0.00723 1 11/17/2022 17:16 WG1961410 Styrene U 0.000331 0.0181 1 11/17/2022 17:16 WG1961410 1,1,1,2-Tetrachloroethane U 0.00137 0.00361 1 11/17/2022 17:16 WG1961410 1,1,2,2-Tetrachloroethane U 0.00100 0.00361 1 11/17/2022 17:16 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00109 0.00361 1 11/17/2022 17:16 WG1961410 Tetrachloroethene 0.00422 0.00130 0.00361 1 11/23/2022 16:46 WG1963991 Toluene U 0.00188 0.00723 1 11/17/2022 17:16 WG1961410 1,2,3-Trichlorobenzene U 0.0106 0.0181 1 11/17/2022 17:16 WG1961410 1,2,4-Trichlorobenzene U 0.00636 0.0181 1 11/17/2022 17:16 WG1961410 1,1,1-Trichloroethane U 0.00133 0.00361 1 11/17/2022 17:16 WG1961410 1,1,2-Trichloroethane U 0.000863 0.00361 1 11/17/2022 17:16 WG1961410 Trichloroethene U 0.000844 0.00145 1 11/17/2022 17:16 WG1961410 Trichlorofluoromethane U 0.00120 0.00361 1 11/17/2022 17:16 WG1961410 1,2,3-Trichloropropane U 0.00234 0.0181 1 11/17/2022 17:16 WG1961410 1,2,4-Trimethylbenzene U 0.00228 0.00723 1 11/17/2022 17:16 WG1961410 1,2,3-Trimethylbenzene U 0.00228 0.00723 1 11/17/2022 17:16 WG1961410 1,3,5-Trimethylbenzene U 0.00289 0.00723 1 11/17/2022 17:16 WG1961410 Vinyl chloride U 0.00168 0.00361 1 11/17/2022 17:16 WG1961410 Xylenes, Total U 0.00127 0.00940 1 11/17/2022 17:16 WG1961410 (S) Toluene-d8 117 75.0-131 11/17/2022 17:16 WG1961410 (S) Toluene-d8 103 75.0-131 11/23/2022 16:46 WG1963991 (S) 4-Bromofluorobenzene 105 67.0-138 11/17/2022 17:16 WG1961410 (S) 4-Bromofluorobenzene 103 67.0-138 11/23/2022 16:46 WG1963991 (S) 1,2-Dichloroethane-d4 81.8 70.0-130 11/17/2022 17:16 WG1961410 (S) 1,2-Dichloroethane-d4 82.1 70.0-130 11/23/2022 16:46 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00656 0.0405 1 11/18/2022 21:23 WG1960983 Acenaphthylene U 0.00571 0.0405 1 11/18/2022 21:23 WG1960983 Anthracene U 0.00721 0.0405 1 11/18/2022 21:23 WG1960983 Benzidine U C3 0.0762 2.03 1 11/18/2022 21:23 WG1960983 Benzo(a)anthracene U 0.00714 0.0405 1 11/18/2022 21:23 WG1960983 Benzo(b)fluoranthene U 0.00756 0.0405 1 11/18/2022 21:23 WG1960983 Benzo(k)fluoranthene U 0.00720 0.0405 1 11/18/2022 21:23 WG1960983 Benzo(g,h,i)perylene U 0.00741 0.0405 1 11/18/2022 21:23 WG1960983 Benzo(a)pyrene U 0.00753 0.0405 1 11/18/2022 21:23 WG1960983 Bis(2-chlorethoxy)methane U 0.0122 0.405 1 11/18/2022 21:23 WG1960983 Bis(2-chloroethyl)ether U 0.0134 0.405 1 11/18/2022 21:23 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0175 0.405 1 11/18/2022 21:23 WG1960983 4-Bromophenyl-phenylether U 0.0142 0.405 1 11/18/2022 21:23 WG1960983 2-Chloronaphthalene U 0.00712 0.0405 1 11/18/2022 21:23 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 21 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 21 of 96 SAMPLE RESULTS - 05 L1557235 SS-3 Collected date/time: 11/10/22 15:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0141 0.405 1 11/18/2022 21:23 WG1960983 Chrysene U 0.00805 0.0405 1 11/18/2022 21:23 WG1960983 Dibenz(a,h)anthracene U 0.0112 0.0405 1 11/18/2022 21:23 WG1960983 1,2-Dichlorobenzene U 0.0120 0.405 1 11/18/2022 21:23 WG1960983 1,3-Dichlorobenzene U 0.0123 0.405 1 11/18/2022 21:23 WG1960983 1,4-Dichlorobenzene U 0.0121 0.405 1 11/18/2022 21:23 WG1960983 3,3-Dichlorobenzidine U 0.0150 0.405 1 11/18/2022 21:23 WG1960983 2,4-Dinitrotoluene U 0.0116 0.405 1 11/18/2022 21:23 WG1960983 2,6-Dinitrotoluene U 0.0133 0.405 1 11/18/2022 21:23 WG1960983 Fluoranthene U 0.00731 0.0405 1 11/18/2022 21:23 WG1960983 Fluorene U 0.00659 0.0405 1 11/18/2022 21:23 WG1960983 Hexachlorobenzene U 0.0144 0.405 1 11/18/2022 21:23 WG1960983 Hexachloro-1,3-butadiene U 0.0136 0.405 1 11/18/2022 21:23 WG1960983 Hexachlorocyclopentadiene U 0.0213 0.405 1 11/18/2022 21:23 WG1960983 Hexachloroethane U 0.0159 0.405 1 11/18/2022 21:23 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0114 0.0405 1 11/18/2022 21:23 WG1960983 Isophorone U 0.0124 0.405 1 11/18/2022 21:23 WG1960983 Naphthalene U 0.0102 0.0405 1 11/18/2022 21:23 WG1960983 Nitrobenzene U 0.0141 0.405 1 11/18/2022 21:23 WG1960983 n-Nitrosodimethylamine U 0.0601 0.405 1 11/18/2022 21:23 WG1960983 n-Nitrosodiphenylamine U 0.0307 0.405 1 11/18/2022 21:23 WG1960983 n-Nitrosodi-n-propylamine U 0.0135 0.405 1 11/18/2022 21:23 WG1960983 Phenanthrene U 0.00804 0.0405 1 11/18/2022 21:23 WG1960983 Benzylbutyl phthalate U 0.0127 0.405 1 11/18/2022 21:23 WG1960983 Bis(2-ethylhexyl)phthalate 0.0811 J 0.0513 0.405 1 11/18/2022 21:23 WG1960983 Di-n-butyl phthalate U 0.0139 0.405 1 11/18/2022 21:23 WG1960983 Diethyl phthalate U 0.0134 0.405 1 11/18/2022 21:23 WG1960983 Dimethyl phthalate U 0.0859 0.405 1 11/18/2022 21:23 WG1960983 Di-n-octyl phthalate U 0.0274 0.405 1 11/18/2022 21:23 WG1960983 Pyrene U 0.00788 0.0405 1 11/18/2022 21:23 WG1960983 1,2,4-Trichlorobenzene U 0.0127 0.405 1 11/18/2022 21:23 WG1960983 4-Chloro-3-methylphenol U 0.0131 0.405 1 11/18/2022 21:23 WG1960983 2-Chlorophenol U 0.0134 0.405 1 11/18/2022 21:23 WG1960983 2,4-Dichlorophenol U 0.0118 0.405 1 11/18/2022 21:23 WG1960983 2,4-Dimethylphenol U 0.0106 0.405 1 11/18/2022 21:23 WG1960983 4,6-Dinitro-2-methylphenol U 0.0919 0.405 1 11/18/2022 21:23 WG1960983 2,4-Dinitrophenol U 0.0948 0.405 1 11/18/2022 21:23 WG1960983 2-Nitrophenol U 0.0145 0.405 1 11/18/2022 21:23 WG1960983 4-Nitrophenol U 0.0127 0.405 1 11/18/2022 21:23 WG1960983 Pentachlorophenol U 0.0109 0.405 1 11/18/2022 21:23 WG1960983 Phenol U 0.0163 0.405 1 11/18/2022 21:23 WG1960983 2,4,6-Trichlorophenol U 0.0130 0.405 1 11/18/2022 21:23 WG1960983 (S) 2-Fluorophenol 55.3 12.0-120 11/18/2022 21:23 WG1960983 (S) Phenol-d5 51.5 10.0-120 11/18/2022 21:23 WG1960983 (S) Nitrobenzene-d5 51.2 10.0-122 11/18/2022 21:23 WG1960983 (S) 2-Fluorobiphenyl 47.3 15.0-120 11/18/2022 21:23 WG1960983 (S) 2,4,6-Tribromophenol 71.1 10.0-127 11/18/2022 21:23 WG1960983 (S) p-Terphenyl-d14 57.6 10.0-120 11/18/2022 21:23 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 22 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 22 of 96 SAMPLE RESULTS - 06 L1557235 SS-3-A Collected date/time: 11/10/22 15:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 90.4 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0199 0.0442 1 11/17/2022 13:23 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.61 0.111 1.11 5 11/28/2022 20:45 WG1966023 Barium 6.41 0.168 2.77 5 11/28/2022 20:45 WG1966023 Cadmium U 0.0946 1.11 5 11/28/2022 20:45 WG1966023 Chromium 5.97 0.327 5.53 5 11/28/2022 20:45 WG1966023 Lead 3.81 0.110 2.21 5 11/28/2022 20:45 WG1966023 Selenium U 0.199 2.77 5 11/28/2022 20:45 WG1966023 Silver U 0.0957 0.553 5 11/28/2022 20:45 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0523 0.0717 1.2 11/17/2022 17:38 WG1961410 Acrylonitrile U 0.00517 0.0179 1.2 11/17/2022 17:38 WG1961410 Benzene U 0.000669 0.00143 1.2 11/17/2022 17:38 WG1961410 Bromobenzene U 0.00129 0.0179 1.2 11/17/2022 17:38 WG1961410 Bromodichloromethane U 0.00104 0.00358 1.2 11/17/2022 17:38 WG1961410 Bromoform U 0.00167 0.0358 1.2 11/17/2022 17:38 WG1961410 Bromomethane U 0.00282 0.0179 1.2 11/17/2022 17:38 WG1961410 n-Butylbenzene U 0.00753 0.0179 1.2 11/17/2022 17:38 WG1961410 sec-Butylbenzene U 0.00413 0.0179 1.2 11/17/2022 17:38 WG1961410 tert-Butylbenzene U C3 0.00280 0.00717 1.2 11/17/2022 17:38 WG1961410 Carbon tetrachloride U 0.00129 0.00717 1.2 11/17/2022 17:38 WG1961410 Chlorobenzene U 0.000301 0.00358 1.2 11/17/2022 17:38 WG1961410 Chlorodibromomethane U 0.000877 0.00358 1.2 11/17/2022 17:38 WG1961410 Chloroethane U 0.00244 0.00717 1.2 11/17/2022 17:38 WG1961410 Chloroform U 0.00148 0.00358 1.2 11/17/2022 17:38 WG1961410 Chloromethane U 0.00624 0.0179 1.2 11/17/2022 17:38 WG1961410 2-Chlorotoluene U 0.00124 0.00358 1.2 11/17/2022 17:38 WG1961410 4-Chlorotoluene U 0.000645 0.00717 1.2 11/17/2022 17:38 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00559 0.0358 1.2 11/17/2022 17:38 WG1961410 1,2-Dibromoethane U 0.000929 0.00358 1.2 11/17/2022 17:38 WG1961410 Dibromomethane U 0.00108 0.00717 1.2 11/17/2022 17:38 WG1961410 1,2-Dichlorobenzene U 0.000609 0.00717 1.2 11/17/2022 17:38 WG1961410 1,3-Dichlorobenzene U 0.000860 0.00717 1.2 11/17/2022 17:38 WG1961410 1,4-Dichlorobenzene U 0.00100 0.00717 1.2 11/17/2022 17:38 WG1961410 Dichlorodifluoromethane U 0.00231 0.00358 1.2 11/17/2022 17:38 WG1961410 1,1-Dichloroethane U 0.000704 0.00358 1.2 11/17/2022 17:38 WG1961410 1,2-Dichloroethane U 0.000931 0.00358 1.2 11/17/2022 17:38 WG1961410 1,1-Dichloroethene U 0.000869 0.00358 1.2 11/17/2022 17:38 WG1961410 cis-1,2-Dichloroethene U 0.00105 0.00358 1.2 11/17/2022 17:38 WG1961410 trans-1,2-Dichloroethene U 0.00149 0.00717 1.2 11/17/2022 17:38 WG1961410 1,2-Dichloropropane U 0.00203 0.00717 1.2 11/17/2022 17:38 WG1961410 1,1-Dichloropropene U 0.00116 0.00358 1.2 11/17/2022 17:38 WG1961410 1,3-Dichloropropane U 0.000718 0.00717 1.2 11/17/2022 17:38 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 23 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 23 of 96 SAMPLE RESULTS - 06 L1557235 SS-3-A Collected date/time: 11/10/22 15:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00108 0.00358 1.2 11/17/2022 17:38 WG1961410 trans-1,3-Dichloropropene U 0.00164 0.00717 1.2 11/17/2022 17:38 WG1961410 2,2-Dichloropropane U 0.00198 0.00358 1.2 11/17/2022 17:38 WG1961410 Di-isopropyl ether U 0.000588 0.00143 1.2 11/17/2022 17:38 WG1961410 Ethylbenzene U 0.00106 0.00358 1.2 11/17/2022 17:38 WG1961410 Hexachloro-1,3-butadiene U 0.00860 0.0358 1.2 11/17/2022 17:38 WG1961410 Isopropylbenzene 0.000860 J 0.000609 0.00358 1.2 11/17/2022 17:38 WG1961410 p-Isopropyltoluene 0.00724 0.00366 0.00717 1.2 11/17/2022 17:38 WG1961410 2-Butanone (MEK)U 0.0910 0.143 1.2 11/17/2022 17:38 WG1961410 Methylene Chloride U 0.00952 0.0358 1.2 11/17/2022 17:38 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00327 0.0358 1.2 11/17/2022 17:38 WG1961410 Methyl tert-butyl ether U 0.000502 0.00143 1.2 11/17/2022 17:38 WG1961410 Naphthalene U 0.00700 0.0179 1.2 11/17/2022 17:38 WG1961410 n-Propylbenzene U 0.00136 0.00717 1.2 11/17/2022 17:38 WG1961410 Styrene U 0.000329 0.0179 1.2 11/17/2022 17:38 WG1961410 1,1,1,2-Tetrachloroethane U 0.00136 0.00358 1.2 11/17/2022 17:38 WG1961410 1,1,2,2-Tetrachloroethane U 0.000996 0.00358 1.2 11/17/2022 17:38 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00108 0.00358 1.2 11/17/2022 17:38 WG1961410 Tetrachloroethene 0.00484 0.00129 0.00358 1.2 11/23/2022 17:05 WG1963991 Toluene U 0.00186 0.00717 1.2 11/17/2022 17:38 WG1961410 1,2,3-Trichlorobenzene U 0.0105 0.0179 1.2 11/17/2022 17:38 WG1961410 1,2,4-Trichlorobenzene U 0.00631 0.0179 1.2 11/17/2022 17:38 WG1961410 1,1,1-Trichloroethane U 0.00133 0.00358 1.2 11/17/2022 17:38 WG1961410 1,1,2-Trichloroethane U 0.000855 0.00358 1.2 11/17/2022 17:38 WG1961410 Trichloroethene U 0.000837 0.00143 1.2 11/17/2022 17:38 WG1961410 Trichlorofluoromethane U 0.00119 0.00358 1.2 11/17/2022 17:38 WG1961410 1,2,3-Trichloropropane U 0.00232 0.0179 1.2 11/17/2022 17:38 WG1961410 1,2,4-Trimethylbenzene U 0.00227 0.00717 1.2 11/17/2022 17:38 WG1961410 1,2,3-Trimethylbenzene U 0.00227 0.00717 1.2 11/17/2022 17:38 WG1961410 1,3,5-Trimethylbenzene U 0.00287 0.00717 1.2 11/17/2022 17:38 WG1961410 Vinyl chloride U 0.00166 0.00358 1.2 11/17/2022 17:38 WG1961410 Xylenes, Total U 0.00127 0.00932 1.2 11/17/2022 17:38 WG1961410 (S) Toluene-d8 116 75.0-131 11/17/2022 17:38 WG1961410 (S) Toluene-d8 101 75.0-131 11/23/2022 17:05 WG1963991 (S) 4-Bromofluorobenzene 103 67.0-138 11/17/2022 17:38 WG1961410 (S) 4-Bromofluorobenzene 104 67.0-138 11/23/2022 17:05 WG1963991 (S) 1,2-Dichloroethane-d4 79.8 70.0-130 11/17/2022 17:38 WG1961410 (S) 1,2-Dichloroethane-d4 79.1 70.0-130 11/23/2022 17:05 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00596 0.0368 1 11/18/2022 21:43 WG1960983 Acenaphthylene U 0.00519 0.0368 1 11/18/2022 21:43 WG1960983 Anthracene U 0.00656 0.0368 1 11/18/2022 21:43 WG1960983 Benzidine U C3 0.0693 1.85 1 11/18/2022 21:43 WG1960983 Benzo(a)anthracene U 0.00649 0.0368 1 11/18/2022 21:43 WG1960983 Benzo(b)fluoranthene U 0.00687 0.0368 1 11/18/2022 21:43 WG1960983 Benzo(k)fluoranthene U 0.00655 0.0368 1 11/18/2022 21:43 WG1960983 Benzo(g,h,i)perylene U 0.00674 0.0368 1 11/18/2022 21:43 WG1960983 Benzo(a)pyrene U 0.00685 0.0368 1 11/18/2022 21:43 WG1960983 Bis(2-chlorethoxy)methane U 0.0111 0.368 1 11/18/2022 21:43 WG1960983 Bis(2-chloroethyl)ether U 0.0122 0.368 1 11/18/2022 21:43 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0159 0.368 1 11/18/2022 21:43 WG1960983 4-Bromophenyl-phenylether U 0.0129 0.368 1 11/18/2022 21:43 WG1960983 2-Chloronaphthalene U 0.00647 0.0368 1 11/18/2022 21:43 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 24 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 24 of 96 SAMPLE RESULTS - 06 L1557235 SS-3-A Collected date/time: 11/10/22 15:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0128 0.368 1 11/18/2022 21:43 WG1960983 Chrysene U 0.00732 0.0368 1 11/18/2022 21:43 WG1960983 Dibenz(a,h)anthracene U 0.0102 0.0368 1 11/18/2022 21:43 WG1960983 1,2-Dichlorobenzene U 0.0109 0.368 1 11/18/2022 21:43 WG1960983 1,3-Dichlorobenzene U 0.0112 0.368 1 11/18/2022 21:43 WG1960983 1,4-Dichlorobenzene U 0.0110 0.368 1 11/18/2022 21:43 WG1960983 3,3-Dichlorobenzidine U 0.0136 0.368 1 11/18/2022 21:43 WG1960983 2,4-Dinitrotoluene U 0.0106 0.368 1 11/18/2022 21:43 WG1960983 2,6-Dinitrotoluene U 0.0121 0.368 1 11/18/2022 21:43 WG1960983 Fluoranthene U 0.00665 0.0368 1 11/18/2022 21:43 WG1960983 Fluorene U 0.00600 0.0368 1 11/18/2022 21:43 WG1960983 Hexachlorobenzene U 0.0131 0.368 1 11/18/2022 21:43 WG1960983 Hexachloro-1,3-butadiene U 0.0124 0.368 1 11/18/2022 21:43 WG1960983 Hexachlorocyclopentadiene U 0.0194 0.368 1 11/18/2022 21:43 WG1960983 Hexachloroethane U 0.0145 0.368 1 11/18/2022 21:43 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0104 0.0368 1 11/18/2022 21:43 WG1960983 Isophorone U 0.0113 0.368 1 11/18/2022 21:43 WG1960983 Naphthalene U 0.00925 0.0368 1 11/18/2022 21:43 WG1960983 Nitrobenzene U 0.0128 0.368 1 11/18/2022 21:43 WG1960983 n-Nitrosodimethylamine U 0.0546 0.368 1 11/18/2022 21:43 WG1960983 n-Nitrosodiphenylamine U 0.0279 0.368 1 11/18/2022 21:43 WG1960983 n-Nitrosodi-n-propylamine U 0.0123 0.368 1 11/18/2022 21:43 WG1960983 Phenanthrene U 0.00731 0.0368 1 11/18/2022 21:43 WG1960983 Benzylbutyl phthalate U 0.0115 0.368 1 11/18/2022 21:43 WG1960983 Bis(2-ethylhexyl)phthalate 0.0481 J 0.0467 0.368 1 11/18/2022 21:43 WG1960983 Di-n-butyl phthalate U 0.0126 0.368 1 11/18/2022 21:43 WG1960983 Diethyl phthalate U 0.0122 0.368 1 11/18/2022 21:43 WG1960983 Dimethyl phthalate U 0.0781 0.368 1 11/18/2022 21:43 WG1960983 Di-n-octyl phthalate U 0.0249 0.368 1 11/18/2022 21:43 WG1960983 Pyrene U 0.00717 0.0368 1 11/18/2022 21:43 WG1960983 1,2,4-Trichlorobenzene U 0.0115 0.368 1 11/18/2022 21:43 WG1960983 4-Chloro-3-methylphenol U 0.0119 0.368 1 11/18/2022 21:43 WG1960983 2-Chlorophenol U 0.0122 0.368 1 11/18/2022 21:43 WG1960983 2,4-Dichlorophenol U 0.0107 0.368 1 11/18/2022 21:43 WG1960983 2,4-Dimethylphenol U 0.00962 0.368 1 11/18/2022 21:43 WG1960983 4,6-Dinitro-2-methylphenol U 0.0835 0.368 1 11/18/2022 21:43 WG1960983 2,4-Dinitrophenol U 0.0862 0.368 1 11/18/2022 21:43 WG1960983 2-Nitrophenol U 0.0132 0.368 1 11/18/2022 21:43 WG1960983 4-Nitrophenol U 0.0115 0.368 1 11/18/2022 21:43 WG1960983 Pentachlorophenol U 0.00991 0.368 1 11/18/2022 21:43 WG1960983 Phenol U 0.0148 0.368 1 11/18/2022 21:43 WG1960983 2,4,6-Trichlorophenol U 0.0118 0.368 1 11/18/2022 21:43 WG1960983 (S) 2-Fluorophenol 57.4 12.0-120 11/18/2022 21:43 WG1960983 (S) Phenol-d5 52.5 10.0-120 11/18/2022 21:43 WG1960983 (S) Nitrobenzene-d5 50.5 10.0-122 11/18/2022 21:43 WG1960983 (S) 2-Fluorobiphenyl 48.6 15.0-120 11/18/2022 21:43 WG1960983 (S) 2,4,6-Tribromophenol 72.0 10.0-127 11/18/2022 21:43 WG1960983 (S) p-Terphenyl-d14 59.1 10.0-120 11/18/2022 21:43 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 25 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 25 of 96 SAMPLE RESULTS - 07 L1557235 SS-4 Collected date/time: 11/10/22 15:25 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 71.6 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0775 0.0251 0.0559 1 11/17/2022 13:26 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 7.86 0.140 1.40 5 11/28/2022 20:48 WG1966023 Barium 18.8 0.212 3.49 5 11/28/2022 20:48 WG1966023 Cadmium U 0.119 1.40 5 11/28/2022 20:48 WG1966023 Chromium 33.4 0.413 6.98 5 11/28/2022 20:48 WG1966023 Lead 10.1 0.138 2.79 5 11/28/2022 20:48 WG1966023 Selenium 0.645 J 0.251 3.49 5 11/28/2022 20:48 WG1966023 Silver U 0.121 0.698 5 11/28/2022 20:48 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0686 0.0939 1.06 11/17/2022 17:59 WG1961410 Acrylonitrile U 0.00679 0.0236 1.06 11/17/2022 17:59 WG1961410 Benzene U 0.000877 0.00188 1.06 11/17/2022 17:59 WG1961410 Bromobenzene U 0.00169 0.0236 1.06 11/17/2022 17:59 WG1961410 Bromodichloromethane U 0.00136 0.00470 1.06 11/17/2022 17:59 WG1961410 Bromoform U 0.00220 0.0470 1.06 11/17/2022 17:59 WG1961410 Bromomethane U 0.00370 0.0236 1.06 11/17/2022 17:59 WG1961410 n-Butylbenzene U 0.00985 0.0236 1.06 11/17/2022 17:59 WG1961410 sec-Butylbenzene 0.00583 B J 0.00540 0.0236 1.06 11/17/2022 17:59 WG1961410 tert-Butylbenzene U C3 0.00367 0.00939 1.06 11/17/2022 17:59 WG1961410 Carbon tetrachloride U 0.00169 0.00939 1.06 11/17/2022 17:59 WG1961410 Chlorobenzene U 0.000395 0.00470 1.06 11/17/2022 17:59 WG1961410 Chlorodibromomethane U 0.00115 0.00470 1.06 11/17/2022 17:59 WG1961410 Chloroethane U 0.00319 0.00939 1.06 11/17/2022 17:59 WG1961410 Chloroform U 0.00193 0.00470 1.06 11/17/2022 17:59 WG1961410 Chloromethane U 0.00817 0.0236 1.06 11/17/2022 17:59 WG1961410 2-Chlorotoluene U 0.00162 0.00470 1.06 11/17/2022 17:59 WG1961410 4-Chlorotoluene U 0.000845 0.00939 1.06 11/17/2022 17:59 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00732 0.0470 1.06 11/17/2022 17:59 WG1961410 1,2-Dibromoethane U 0.00122 0.00470 1.06 11/17/2022 17:59 WG1961410 Dibromomethane U 0.00141 0.00939 1.06 11/17/2022 17:59 WG1961410 1,2-Dichlorobenzene U 0.000799 0.00939 1.06 11/17/2022 17:59 WG1961410 1,3-Dichlorobenzene U 0.00113 0.00939 1.06 11/17/2022 17:59 WG1961410 1,4-Dichlorobenzene U 0.00131 0.00939 1.06 11/17/2022 17:59 WG1961410 Dichlorodifluoromethane U 0.00303 0.00470 1.06 11/17/2022 17:59 WG1961410 1,1-Dichloroethane U 0.000921 0.00470 1.06 11/17/2022 17:59 WG1961410 1,2-Dichloroethane U 0.00122 0.00470 1.06 11/17/2022 17:59 WG1961410 1,1-Dichloroethene U 0.00114 0.00470 1.06 11/17/2022 17:59 WG1961410 cis-1,2-Dichloroethene U 0.00138 0.00470 1.06 11/17/2022 17:59 WG1961410 trans-1,2-Dichloroethene U 0.00195 0.00939 1.06 11/17/2022 17:59 WG1961410 1,2-Dichloropropane U 0.00268 0.00939 1.06 11/17/2022 17:59 WG1961410 1,1-Dichloropropene U 0.00152 0.00470 1.06 11/17/2022 17:59 WG1961410 1,3-Dichloropropane U 0.000941 0.00939 1.06 11/17/2022 17:59 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 26 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 26 of 96 SAMPLE RESULTS - 07 L1557235 SS-4 Collected date/time: 11/10/22 15:25 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00142 0.00470 1.06 11/17/2022 17:59 WG1961410 trans-1,3-Dichloropropene U 0.00214 0.00939 1.06 11/17/2022 17:59 WG1961410 2,2-Dichloropropane U 0.00259 0.00470 1.06 11/17/2022 17:59 WG1961410 Di-isopropyl ether U 0.000771 0.00188 1.06 11/17/2022 17:59 WG1961410 Ethylbenzene U 0.00138 0.00470 1.06 11/17/2022 17:59 WG1961410 Hexachloro-1,3-butadiene U 0.0113 0.0470 1.06 11/17/2022 17:59 WG1961410 Isopropylbenzene 0.000939 J 0.000799 0.00470 1.06 11/17/2022 17:59 WG1961410 p-Isopropyltoluene U 0.00478 0.00939 1.06 11/17/2022 17:59 WG1961410 2-Butanone (MEK)U 0.119 0.188 1.06 11/17/2022 17:59 WG1961410 Methylene Chloride U 0.0125 0.0470 1.06 11/17/2022 17:59 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00429 0.0470 1.06 11/17/2022 17:59 WG1961410 Methyl tert-butyl ether U 0.000657 0.00188 1.06 11/17/2022 17:59 WG1961410 Naphthalene U 0.00916 0.0236 1.06 11/17/2022 17:59 WG1961410 n-Propylbenzene U 0.00179 0.00939 1.06 11/17/2022 17:59 WG1961410 Styrene U 0.000431 0.0236 1.06 11/17/2022 17:59 WG1961410 1,1,1,2-Tetrachloroethane U 0.00177 0.00470 1.06 11/17/2022 17:59 WG1961410 1,1,2,2-Tetrachloroethane U 0.00131 0.00470 1.06 11/17/2022 17:59 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00142 0.00470 1.06 11/17/2022 17:59 WG1961410 Tetrachloroethene 0.00446 J 0.00168 0.00470 1.06 11/23/2022 17:24 WG1963991 Toluene U 0.00245 0.00939 1.06 11/17/2022 17:59 WG1961410 1,2,3-Trichlorobenzene U 0.0138 0.0236 1.06 11/17/2022 17:59 WG1961410 1,2,4-Trichlorobenzene U 0.00826 0.0236 1.06 11/17/2022 17:59 WG1961410 1,1,1-Trichloroethane U 0.00173 0.00470 1.06 11/17/2022 17:59 WG1961410 1,1,2-Trichloroethane U 0.00112 0.00470 1.06 11/17/2022 17:59 WG1961410 Trichloroethene U 0.00110 0.00188 1.06 11/17/2022 17:59 WG1961410 Trichlorofluoromethane U 0.00155 0.00470 1.06 11/17/2022 17:59 WG1961410 1,2,3-Trichloropropane U 0.00305 0.0236 1.06 11/17/2022 17:59 WG1961410 1,2,4-Trimethylbenzene U 0.00296 0.00939 1.06 11/17/2022 17:59 WG1961410 1,2,3-Trimethylbenzene U 0.00296 0.00939 1.06 11/17/2022 17:59 WG1961410 1,3,5-Trimethylbenzene U 0.00376 0.00939 1.06 11/17/2022 17:59 WG1961410 Vinyl chloride U 0.00218 0.00470 1.06 11/17/2022 17:59 WG1961410 Xylenes, Total U 0.00165 0.0122 1.06 11/17/2022 17:59 WG1961410 (S) Toluene-d8 114 75.0-131 11/17/2022 17:59 WG1961410 (S) Toluene-d8 102 75.0-131 11/23/2022 17:24 WG1963991 (S) 4-Bromofluorobenzene 106 67.0-138 11/17/2022 17:59 WG1961410 (S) 4-Bromofluorobenzene 100 67.0-138 11/23/2022 17:24 WG1963991 (S) 1,2-Dichloroethane-d4 83.8 70.0-130 11/17/2022 17:59 WG1961410 (S) 1,2-Dichloroethane-d4 84.3 70.0-130 11/23/2022 17:24 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00753 0.0465 1 11/18/2022 22:04 WG1960983 Acenaphthylene U 0.00655 0.0465 1 11/18/2022 22:04 WG1960983 Anthracene U 0.00828 0.0465 1 11/18/2022 22:04 WG1960983 Benzidine U C3 0.0874 2.33 1 11/18/2022 22:04 WG1960983 Benzo(a)anthracene U 0.00820 0.0465 1 11/18/2022 22:04 WG1960983 Benzo(b)fluoranthene U 0.00867 0.0465 1 11/18/2022 22:04 WG1960983 Benzo(k)fluoranthene U 0.00827 0.0465 1 11/18/2022 22:04 WG1960983 Benzo(g,h,i)perylene U 0.00850 0.0465 1 11/18/2022 22:04 WG1960983 Benzo(a)pyrene U 0.00864 0.0465 1 11/18/2022 22:04 WG1960983 Bis(2-chlorethoxy)methane U 0.0140 0.465 1 11/18/2022 22:04 WG1960983 Bis(2-chloroethyl)ether U 0.0154 0.465 1 11/18/2022 22:04 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0201 0.465 1 11/18/2022 22:04 WG1960983 4-Bromophenyl-phenylether U 0.0163 0.465 1 11/18/2022 22:04 WG1960983 2-Chloronaphthalene U 0.00817 0.0465 1 11/18/2022 22:04 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 27 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 27 of 96 SAMPLE RESULTS - 07 L1557235 SS-4 Collected date/time: 11/10/22 15:25 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0162 0.465 1 11/18/2022 22:04 WG1960983 Chrysene U 0.00924 0.0465 1 11/18/2022 22:04 WG1960983 Dibenz(a,h)anthracene U 0.0129 0.0465 1 11/18/2022 22:04 WG1960983 1,2-Dichlorobenzene U 0.0138 0.465 1 11/18/2022 22:04 WG1960983 1,3-Dichlorobenzene U 0.0141 0.465 1 11/18/2022 22:04 WG1960983 1,4-Dichlorobenzene U 0.0138 0.465 1 11/18/2022 22:04 WG1960983 3,3-Dichlorobenzidine U 0.0172 0.465 1 11/18/2022 22:04 WG1960983 2,4-Dinitrotoluene U 0.0133 0.465 1 11/18/2022 22:04 WG1960983 2,6-Dinitrotoluene U 0.0152 0.465 1 11/18/2022 22:04 WG1960983 Fluoranthene U 0.00839 0.0465 1 11/18/2022 22:04 WG1960983 Fluorene U 0.00757 0.0465 1 11/18/2022 22:04 WG1960983 Hexachlorobenzene U 0.0165 0.465 1 11/18/2022 22:04 WG1960983 Hexachloro-1,3-butadiene U 0.0156 0.465 1 11/18/2022 22:04 WG1960983 Hexachlorocyclopentadiene U 0.0244 0.465 1 11/18/2022 22:04 WG1960983 Hexachloroethane U 0.0183 0.465 1 11/18/2022 22:04 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0131 0.0465 1 11/18/2022 22:04 WG1960983 Isophorone U 0.0142 0.465 1 11/18/2022 22:04 WG1960983 Naphthalene U 0.0117 0.0465 1 11/18/2022 22:04 WG1960983 Nitrobenzene U 0.0162 0.465 1 11/18/2022 22:04 WG1960983 n-Nitrosodimethylamine U 0.0690 0.465 1 11/18/2022 22:04 WG1960983 n-Nitrosodiphenylamine U 0.0352 0.465 1 11/18/2022 22:04 WG1960983 n-Nitrosodi-n-propylamine U 0.0155 0.465 1 11/18/2022 22:04 WG1960983 Phenanthrene U 0.00923 0.0465 1 11/18/2022 22:04 WG1960983 Benzylbutyl phthalate U 0.0145 0.465 1 11/18/2022 22:04 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0589 0.465 1 11/18/2022 22:04 WG1960983 Di-n-butyl phthalate U 0.0159 0.465 1 11/18/2022 22:04 WG1960983 Diethyl phthalate U 0.0154 0.465 1 11/18/2022 22:04 WG1960983 Dimethyl phthalate U 0.0986 0.465 1 11/18/2022 22:04 WG1960983 Di-n-octyl phthalate U 0.0314 0.465 1 11/18/2022 22:04 WG1960983 Pyrene U 0.00905 0.0465 1 11/18/2022 22:04 WG1960983 1,2,4-Trichlorobenzene U 0.0145 0.465 1 11/18/2022 22:04 WG1960983 4-Chloro-3-methylphenol U 0.0151 0.465 1 11/18/2022 22:04 WG1960983 2-Chlorophenol U 0.0154 0.465 1 11/18/2022 22:04 WG1960983 2,4-Dichlorophenol U 0.0135 0.465 1 11/18/2022 22:04 WG1960983 2,4-Dimethylphenol U 0.0121 0.465 1 11/18/2022 22:04 WG1960983 4,6-Dinitro-2-methylphenol U 0.105 0.465 1 11/18/2022 22:04 WG1960983 2,4-Dinitrophenol U 0.109 0.465 1 11/18/2022 22:04 WG1960983 2-Nitrophenol U 0.0166 0.465 1 11/18/2022 22:04 WG1960983 4-Nitrophenol U 0.0145 0.465 1 11/18/2022 22:04 WG1960983 Pentachlorophenol U 0.0125 0.465 1 11/18/2022 22:04 WG1960983 Phenol U 0.0187 0.465 1 11/18/2022 22:04 WG1960983 2,4,6-Trichlorophenol U 0.0149 0.465 1 11/18/2022 22:04 WG1960983 (S) 2-Fluorophenol 65.1 12.0-120 11/18/2022 22:04 WG1960983 (S) Phenol-d5 60.9 10.0-120 11/18/2022 22:04 WG1960983 (S) Nitrobenzene-d5 56.3 10.0-122 11/18/2022 22:04 WG1960983 (S) 2-Fluorobiphenyl 55.4 15.0-120 11/18/2022 22:04 WG1960983 (S) 2,4,6-Tribromophenol 78.9 10.0-127 11/18/2022 22:04 WG1960983 (S) p-Terphenyl-d14 66.4 10.0-120 11/18/2022 22:04 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 28 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 28 of 96 SAMPLE RESULTS - 08 L1557235 SS-4-A Collected date/time: 11/10/22 15:25 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 59.5 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0302 0.0672 1 11/17/2022 13:28 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.05 J 0.168 1.68 5 11/28/2022 20:52 WG1966023 Barium 8.03 0.255 4.20 5 11/28/2022 20:52 WG1966023 Cadmium U 0.144 1.68 5 11/28/2022 20:52 WG1966023 Chromium 8.42 0.497 8.40 5 11/28/2022 20:52 WG1966023 Lead 8.90 0.166 3.36 5 11/28/2022 20:52 WG1966023 Selenium U 0.302 4.20 5 11/28/2022 20:52 WG1966023 Silver U 0.145 0.840 5 11/28/2022 20:52 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0872 0.120 1.02 11/17/2022 18:20 WG1961410 Acrylonitrile U 0.00862 0.0300 1.02 11/17/2022 18:20 WG1961410 Benzene U 0.00112 0.00239 1.02 11/17/2022 18:20 WG1961410 Bromobenzene U 0.00215 0.0300 1.02 11/17/2022 18:20 WG1961410 Bromodichloromethane U 0.00173 0.00598 1.02 11/17/2022 18:20 WG1961410 Bromoform U 0.00279 0.0598 1.02 11/17/2022 18:20 WG1961410 Bromomethane U 0.00471 0.0300 1.02 11/17/2022 18:20 WG1961410 n-Butylbenzene U 0.0125 0.0300 1.02 11/17/2022 18:20 WG1961410 sec-Butylbenzene U 0.00689 0.0300 1.02 11/17/2022 18:20 WG1961410 tert-Butylbenzene U 0.00466 0.0120 1.02 11/23/2022 18:13 WG1963991 Carbon tetrachloride U 0.00215 0.0120 1.02 11/17/2022 18:20 WG1961410 Chlorobenzene U 0.000501 0.00598 1.02 11/17/2022 18:20 WG1961410 Chlorodibromomethane U 0.00146 0.00598 1.02 11/17/2022 18:20 WG1961410 Chloroethane U 0.00405 0.0120 1.02 11/17/2022 18:20 WG1961410 Chloroform U 0.00246 0.00598 1.02 11/17/2022 18:20 WG1961410 Chloromethane U 0.0104 0.0300 1.02 11/17/2022 18:20 WG1961410 2-Chlorotoluene U 0.00207 0.00598 1.02 11/17/2022 18:20 WG1961410 4-Chlorotoluene U 0.00108 0.0120 1.02 11/17/2022 18:20 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00933 0.0598 1.02 11/17/2022 18:20 WG1961410 1,2-Dibromoethane U 0.00155 0.00598 1.02 11/17/2022 18:20 WG1961410 Dibromomethane U 0.00179 0.0120 1.02 11/17/2022 18:20 WG1961410 1,2-Dichlorobenzene U 0.00101 0.0120 1.02 11/17/2022 18:20 WG1961410 1,3-Dichlorobenzene U 0.00143 0.0120 1.02 11/17/2022 18:20 WG1961410 1,4-Dichlorobenzene U 0.00167 0.0120 1.02 11/17/2022 18:20 WG1961410 Dichlorodifluoromethane U 0.00384 0.00598 1.02 11/17/2022 18:20 WG1961410 1,1-Dichloroethane U 0.00117 0.00598 1.02 11/17/2022 18:20 WG1961410 1,2-Dichloroethane U 0.00155 0.00598 1.02 11/17/2022 18:20 WG1961410 1,1-Dichloroethene U 0.00145 0.00598 1.02 11/17/2022 18:20 WG1961410 cis-1,2-Dichloroethene U 0.00176 0.00598 1.02 11/17/2022 18:20 WG1961410 trans-1,2-Dichloroethene U 0.00248 0.0120 1.02 11/17/2022 18:20 WG1961410 1,2-Dichloropropane U 0.00340 0.0120 1.02 11/17/2022 18:20 WG1961410 1,1-Dichloropropene U 0.00193 0.00598 1.02 11/17/2022 18:20 WG1961410 1,3-Dichloropropane U 0.00120 0.0120 1.02 11/17/2022 18:20 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 29 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 29 of 96 SAMPLE RESULTS - 08 L1557235 SS-4-A Collected date/time: 11/10/22 15:25 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00181 0.00598 1.02 11/17/2022 18:20 WG1961410 trans-1,3-Dichloropropene U 0.00272 0.0120 1.02 11/17/2022 18:20 WG1961410 2,2-Dichloropropane U 0.00330 0.00598 1.02 11/17/2022 18:20 WG1961410 Di-isopropyl ether U 0.000979 0.00239 1.02 11/17/2022 18:20 WG1961410 Ethylbenzene U 0.00176 0.00598 1.02 11/17/2022 18:20 WG1961410 Hexachloro-1,3-butadiene U 0.0143 0.0598 1.02 11/17/2022 18:20 WG1961410 Isopropylbenzene U 0.00101 0.00598 1.02 11/17/2022 18:20 WG1961410 p-Isopropyltoluene U 0.00609 0.0120 1.02 11/17/2022 18:20 WG1961410 2-Butanone (MEK)U 0.152 0.239 1.02 11/17/2022 18:20 WG1961410 Methylene Chloride U 0.0159 0.0598 1.02 11/17/2022 18:20 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00546 0.0598 1.02 11/17/2022 18:20 WG1961410 Methyl tert-butyl ether U 0.000837 0.00239 1.02 11/17/2022 18:20 WG1961410 Naphthalene U 0.0117 0.0300 1.02 11/17/2022 18:20 WG1961410 n-Propylbenzene U 0.00227 0.0120 1.02 11/17/2022 18:20 WG1961410 Styrene U 0.000548 0.0300 1.02 11/17/2022 18:20 WG1961410 1,1,1,2-Tetrachloroethane U 0.00227 0.00598 1.02 11/17/2022 18:20 WG1961410 1,1,2,2-Tetrachloroethane U 0.00166 0.00598 1.02 11/17/2022 18:20 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00180 0.00598 1.02 11/17/2022 18:20 WG1961410 Tetrachloroethene 0.00855 0.00214 0.00598 1.02 11/23/2022 18:13 WG1963991 Toluene 0.00377 J 0.00312 0.0120 1.02 11/17/2022 18:20 WG1961410 1,2,3-Trichlorobenzene U 0.0175 0.0300 1.02 11/17/2022 18:20 WG1961410 1,2,4-Trichlorobenzene U 0.0105 0.0300 1.02 11/17/2022 18:20 WG1961410 1,1,1-Trichloroethane U 0.00221 0.00598 1.02 11/17/2022 18:20 WG1961410 1,1,2-Trichloroethane U 0.00143 0.00598 1.02 11/17/2022 18:20 WG1961410 Trichloroethene U 0.00140 0.00239 1.02 11/17/2022 18:20 WG1961410 Trichlorofluoromethane U 0.00198 0.00598 1.02 11/17/2022 18:20 WG1961410 1,2,3-Trichloropropane U 0.00387 0.0300 1.02 11/17/2022 18:20 WG1961410 1,2,4-Trimethylbenzene U 0.00377 0.0120 1.02 11/17/2022 18:20 WG1961410 1,2,3-Trimethylbenzene U 0.00377 0.0120 1.02 11/17/2022 18:20 WG1961410 1,3,5-Trimethylbenzene U 0.00478 0.0120 1.02 11/17/2022 18:20 WG1961410 Vinyl chloride U 0.00277 0.00598 1.02 11/17/2022 18:20 WG1961410 Xylenes, Total U 0.00210 0.0155 1.02 11/17/2022 18:20 WG1961410 (S) Toluene-d8 112 75.0-131 11/17/2022 18:20 WG1961410 (S) Toluene-d8 98.6 75.0-131 11/23/2022 18:13 WG1963991 (S) 4-Bromofluorobenzene 106 67.0-138 11/17/2022 18:20 WG1961410 (S) 4-Bromofluorobenzene 99.9 67.0-138 11/23/2022 18:13 WG1963991 (S) 1,2-Dichloroethane-d4 80.3 70.0-130 11/17/2022 18:20 WG1961410 (S) 1,2-Dichloroethane-d4 81.7 70.0-130 11/23/2022 18:13 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00905 0.0559 1 11/18/2022 20:23 WG1960983 Acenaphthylene U 0.00788 0.0559 1 11/18/2022 20:23 WG1960983 Anthracene U 0.00996 0.0559 1 11/18/2022 20:23 WG1960983 Benzidine U C3 0.105 2.80 1 11/18/2022 20:23 WG1960983 Benzo(a)anthracene U 0.00986 0.0559 1 11/18/2022 20:23 WG1960983 Benzo(b)fluoranthene U 0.0104 0.0559 1 11/18/2022 20:23 WG1960983 Benzo(k)fluoranthene U 0.00994 0.0559 1 11/18/2022 20:23 WG1960983 Benzo(g,h,i)perylene U 0.0102 0.0559 1 11/18/2022 20:23 WG1960983 Benzo(a)pyrene U 0.0104 0.0559 1 11/18/2022 20:23 WG1960983 Bis(2-chlorethoxy)methane U 0.0168 0.559 1 11/18/2022 20:23 WG1960983 Bis(2-chloroethyl)ether U 0.0185 0.559 1 11/18/2022 20:23 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0242 0.559 1 11/18/2022 20:23 WG1960983 4-Bromophenyl-phenylether U 0.0196 0.559 1 11/18/2022 20:23 WG1960983 2-Chloronaphthalene U 0.00982 0.0559 1 11/18/2022 20:23 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 30 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 30 of 96 SAMPLE RESULTS - 08 L1557235 SS-4-A Collected date/time: 11/10/22 15:25 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0195 0.559 1 11/18/2022 20:23 WG1960983 Chrysene U 0.0111 0.0559 1 11/18/2022 20:23 WG1960983 Dibenz(a,h)anthracene U 0.0155 0.0559 1 11/18/2022 20:23 WG1960983 1,2-Dichlorobenzene U 0.0166 0.559 1 11/18/2022 20:23 WG1960983 1,3-Dichlorobenzene U 0.0170 0.559 1 11/18/2022 20:23 WG1960983 1,4-Dichlorobenzene U 0.0166 0.559 1 11/18/2022 20:23 WG1960983 3,3-Dichlorobenzidine U 0.0207 0.559 1 11/18/2022 20:23 WG1960983 2,4-Dinitrotoluene U 0.0160 0.559 1 11/18/2022 20:23 WG1960983 2,6-Dinitrotoluene U 0.0183 0.559 1 11/18/2022 20:23 WG1960983 Fluoranthene U 0.0101 0.0559 1 11/18/2022 20:23 WG1960983 Fluorene U 0.00910 0.0559 1 11/18/2022 20:23 WG1960983 Hexachlorobenzene U 0.0198 0.559 1 11/18/2022 20:23 WG1960983 Hexachloro-1,3-butadiene U 0.0188 0.559 1 11/18/2022 20:23 WG1960983 Hexachlorocyclopentadiene U 0.0294 0.559 1 11/18/2022 20:23 WG1960983 Hexachloroethane U 0.0220 0.559 1 11/18/2022 20:23 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0158 0.0559 1 11/18/2022 20:23 WG1960983 Isophorone U 0.0171 0.559 1 11/18/2022 20:23 WG1960983 Naphthalene U 0.0140 0.0559 1 11/18/2022 20:23 WG1960983 Nitrobenzene U 0.0195 0.559 1 11/18/2022 20:23 WG1960983 n-Nitrosodimethylamine U 0.0830 0.559 1 11/18/2022 20:23 WG1960983 n-Nitrosodiphenylamine U 0.0423 0.559 1 11/18/2022 20:23 WG1960983 n-Nitrosodi-n-propylamine U 0.0186 0.559 1 11/18/2022 20:23 WG1960983 Phenanthrene U 0.0111 0.0559 1 11/18/2022 20:23 WG1960983 Benzylbutyl phthalate U 0.0175 0.559 1 11/18/2022 20:23 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0709 0.559 1 11/18/2022 20:23 WG1960983 Di-n-butyl phthalate U 0.0191 0.559 1 11/18/2022 20:23 WG1960983 Diethyl phthalate U 0.0185 0.559 1 11/18/2022 20:23 WG1960983 Dimethyl phthalate U 0.119 0.559 1 11/18/2022 20:23 WG1960983 Di-n-octyl phthalate U 0.0378 0.559 1 11/18/2022 20:23 WG1960983 Pyrene U 0.0109 0.0559 1 11/18/2022 20:23 WG1960983 1,2,4-Trichlorobenzene U 0.0175 0.559 1 11/18/2022 20:23 WG1960983 4-Chloro-3-methylphenol U 0.0181 0.559 1 11/18/2022 20:23 WG1960983 2-Chlorophenol U 0.0185 0.559 1 11/18/2022 20:23 WG1960983 2,4-Dichlorophenol U 0.0163 0.559 1 11/18/2022 20:23 WG1960983 2,4-Dimethylphenol U 0.0146 0.559 1 11/18/2022 20:23 WG1960983 4,6-Dinitro-2-methylphenol U 0.127 0.559 1 11/18/2022 20:23 WG1960983 2,4-Dinitrophenol U 0.131 0.559 1 11/18/2022 20:23 WG1960983 2-Nitrophenol U 0.0200 0.559 1 11/18/2022 20:23 WG1960983 4-Nitrophenol U 0.0175 0.559 1 11/18/2022 20:23 WG1960983 Pentachlorophenol U 0.0150 0.559 1 11/18/2022 20:23 WG1960983 Phenol U 0.0225 0.559 1 11/18/2022 20:23 WG1960983 2,4,6-Trichlorophenol U 0.0180 0.559 1 11/18/2022 20:23 WG1960983 (S) 2-Fluorophenol 66.2 12.0-120 11/18/2022 20:23 WG1960983 (S) Phenol-d5 60.3 10.0-120 11/18/2022 20:23 WG1960983 (S) Nitrobenzene-d5 57.6 10.0-122 11/18/2022 20:23 WG1960983 (S) 2-Fluorobiphenyl 53.0 15.0-120 11/18/2022 20:23 WG1960983 (S) 2,4,6-Tribromophenol 74.5 10.0-127 11/18/2022 20:23 WG1960983 (S) p-Terphenyl-d14 65.4 10.0-120 11/18/2022 20:23 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 31 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 31 of 96 SAMPLE RESULTS - 09 L1557235 SS-5 Collected date/time: 11/10/22 15:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 67.9 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0805 0.0265 0.0589 1 11/17/2022 13:35 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 8.68 0.147 1.47 5 11/28/2022 20:55 WG1966023 Barium 10.1 0.224 3.68 5 11/28/2022 20:55 WG1966023 Cadmium U 0.126 1.47 5 11/28/2022 20:55 WG1966023 Chromium 21.6 0.436 7.36 5 11/28/2022 20:55 WG1966023 Lead 9.78 0.146 2.95 5 11/28/2022 20:55 WG1966023 Selenium U 0.265 3.68 5 11/28/2022 20:55 WG1966023 Silver U 0.127 0.736 5 11/28/2022 20:55 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0730 0.100 1 11/17/2022 18:41 WG1961410 Acrylonitrile U 0.00722 0.0250 1 11/17/2022 18:41 WG1961410 Benzene U 0.000934 0.00200 1 11/17/2022 18:41 WG1961410 Bromobenzene U 0.00180 0.0250 1 11/17/2022 18:41 WG1961410 Bromodichloromethane U 0.00145 0.00500 1 11/17/2022 18:41 WG1961410 Bromoform U 0.00234 0.0500 1 11/17/2022 18:41 WG1961410 Bromomethane U 0.00394 0.0250 1 11/17/2022 18:41 WG1961410 n-Butylbenzene U 0.0105 0.0250 1 11/17/2022 18:41 WG1961410 sec-Butylbenzene U 0.00576 0.0250 1 11/17/2022 18:41 WG1961410 tert-Butylbenzene U C3 0.00390 0.0100 1 11/17/2022 18:41 WG1961410 Carbon tetrachloride U 0.00180 0.0100 1 11/17/2022 18:41 WG1961410 Chlorobenzene U 0.000420 0.00500 1 11/17/2022 18:41 WG1961410 Chlorodibromomethane U 0.00122 0.00500 1 11/17/2022 18:41 WG1961410 Chloroethane U 0.00340 0.0100 1 11/17/2022 18:41 WG1961410 Chloroform U 0.00206 0.00500 1 11/17/2022 18:41 WG1961410 Chloromethane U 0.00870 0.0250 1 11/17/2022 18:41 WG1961410 2-Chlorotoluene U 0.00173 0.00500 1 11/17/2022 18:41 WG1961410 4-Chlorotoluene U 0.000900 0.0100 1 11/17/2022 18:41 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00780 0.0500 1 11/17/2022 18:41 WG1961410 1,2-Dibromoethane U 0.00130 0.00500 1 11/17/2022 18:41 WG1961410 Dibromomethane U 0.00150 0.0100 1 11/17/2022 18:41 WG1961410 1,2-Dichlorobenzene U 0.000850 0.0100 1 11/17/2022 18:41 WG1961410 1,3-Dichlorobenzene U 0.00120 0.0100 1 11/17/2022 18:41 WG1961410 1,4-Dichlorobenzene U 0.00140 0.0100 1 11/17/2022 18:41 WG1961410 Dichlorodifluoromethane U 0.00322 0.00500 1 11/17/2022 18:41 WG1961410 1,1-Dichloroethane U 0.000982 0.00500 1 11/17/2022 18:41 WG1961410 1,2-Dichloroethane U 0.00130 0.00500 1 11/17/2022 18:41 WG1961410 1,1-Dichloroethene U 0.00121 0.00500 1 11/17/2022 18:41 WG1961410 cis-1,2-Dichloroethene U 0.00147 0.00500 1 11/17/2022 18:41 WG1961410 trans-1,2-Dichloroethene U 0.00208 0.0100 1 11/17/2022 18:41 WG1961410 1,2-Dichloropropane U 0.00284 0.0100 1 11/17/2022 18:41 WG1961410 1,1-Dichloropropene U 0.00162 0.00500 1 11/17/2022 18:41 WG1961410 1,3-Dichloropropane U 0.00100 0.0100 1 11/17/2022 18:41 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 32 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 32 of 96 SAMPLE RESULTS - 09 L1557235 SS-5 Collected date/time: 11/10/22 15:40 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00151 0.00500 1 11/17/2022 18:41 WG1961410 trans-1,3-Dichloropropene U 0.00228 0.0100 1 11/17/2022 18:41 WG1961410 2,2-Dichloropropane U 0.00276 0.00500 1 11/17/2022 18:41 WG1961410 Di-isopropyl ether U 0.000820 0.00200 1 11/17/2022 18:41 WG1961410 Ethylbenzene U 0.00147 0.00500 1 11/17/2022 18:41 WG1961410 Hexachloro-1,3-butadiene U 0.0120 0.0500 1 11/17/2022 18:41 WG1961410 Isopropylbenzene 0.00135 J 0.000850 0.00500 1 11/17/2022 18:41 WG1961410 p-Isopropyltoluene 0.00518 J 0.00510 0.0100 1 11/17/2022 18:41 WG1961410 2-Butanone (MEK)U 0.127 0.200 1 11/17/2022 18:41 WG1961410 Methylene Chloride U 0.0133 0.0500 1 11/17/2022 18:41 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00456 0.0500 1 11/17/2022 18:41 WG1961410 Methyl tert-butyl ether U 0.000700 0.00200 1 11/17/2022 18:41 WG1961410 Naphthalene U 0.00976 0.0250 1 11/17/2022 18:41 WG1961410 n-Propylbenzene U 0.00190 0.0100 1 11/17/2022 18:41 WG1961410 Styrene U 0.000458 0.0250 1 11/17/2022 18:41 WG1961410 1,1,1,2-Tetrachloroethane U 0.00190 0.00500 1 11/17/2022 18:41 WG1961410 1,1,2,2-Tetrachloroethane U 0.00139 0.00500 1 11/17/2022 18:41 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00151 0.00500 1 11/17/2022 18:41 WG1961410 Tetrachloroethene 0.00526 0.00179 0.00500 1 11/23/2022 18:32 WG1963991 Toluene U 0.00260 0.0100 1 11/17/2022 18:41 WG1961410 1,2,3-Trichlorobenzene U 0.0147 0.0250 1 11/17/2022 18:41 WG1961410 1,2,4-Trichlorobenzene U 0.00880 0.0250 1 11/17/2022 18:41 WG1961410 1,1,1-Trichloroethane U 0.00185 0.00500 1 11/17/2022 18:41 WG1961410 1,1,2-Trichloroethane U 0.00119 0.00500 1 11/17/2022 18:41 WG1961410 Trichloroethene U 0.00117 0.00200 1 11/17/2022 18:41 WG1961410 Trichlorofluoromethane U 0.00165 0.00500 1 11/17/2022 18:41 WG1961410 1,2,3-Trichloropropane U 0.00324 0.0250 1 11/17/2022 18:41 WG1961410 1,2,4-Trimethylbenzene U 0.00316 0.0100 1 11/17/2022 18:41 WG1961410 1,2,3-Trimethylbenzene U 0.00316 0.0100 1 11/17/2022 18:41 WG1961410 1,3,5-Trimethylbenzene U 0.00400 0.0100 1 11/17/2022 18:41 WG1961410 Vinyl chloride U 0.00232 0.00500 1 11/17/2022 18:41 WG1961410 Xylenes, Total U 0.00176 0.0130 1 11/17/2022 18:41 WG1961410 (S) Toluene-d8 113 75.0-131 11/17/2022 18:41 WG1961410 (S) Toluene-d8 102 75.0-131 11/23/2022 18:32 WG1963991 (S) 4-Bromofluorobenzene 101 67.0-138 11/17/2022 18:41 WG1961410 (S) 4-Bromofluorobenzene 102 67.0-138 11/23/2022 18:32 WG1963991 (S) 1,2-Dichloroethane-d4 77.8 70.0-130 11/17/2022 18:41 WG1961410 (S) 1,2-Dichloroethane-d4 85.3 70.0-130 11/23/2022 18:32 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00794 0.0490 1 11/18/2022 18:21 WG1960983 Acenaphthylene U 0.00691 0.0490 1 11/18/2022 18:21 WG1960983 Anthracene U 0.00873 0.0490 1 11/18/2022 18:21 WG1960983 Benzidine U C3 0.0922 2.46 1 11/18/2022 18:21 WG1960983 Benzo(a)anthracene U 0.00864 0.0490 1 11/18/2022 18:21 WG1960983 Benzo(b)fluoranthene U 0.00915 0.0490 1 11/18/2022 18:21 WG1960983 Benzo(k)fluoranthene U 0.00872 0.0490 1 11/18/2022 18:21 WG1960983 Benzo(g,h,i)perylene U 0.00897 0.0490 1 11/18/2022 18:21 WG1960983 Benzo(a)pyrene U 0.00912 0.0490 1 11/18/2022 18:21 WG1960983 Bis(2-chlorethoxy)methane U 0.0147 0.490 1 11/18/2022 18:21 WG1960983 Bis(2-chloroethyl)ether U 0.0162 0.490 1 11/18/2022 18:21 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0212 0.490 1 11/18/2022 18:21 WG1960983 4-Bromophenyl-phenylether U 0.0172 0.490 1 11/18/2022 18:21 WG1960983 2-Chloronaphthalene U 0.00862 0.0490 1 11/18/2022 18:21 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 33 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 33 of 96 SAMPLE RESULTS - 09 L1557235 SS-5 Collected date/time: 11/10/22 15:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0171 0.490 1 11/18/2022 18:21 WG1960983 Chrysene U 0.00975 0.0490 1 11/18/2022 18:21 WG1960983 Dibenz(a,h)anthracene U 0.0136 0.0490 1 11/18/2022 18:21 WG1960983 1,2-Dichlorobenzene U 0.0145 0.490 1 11/18/2022 18:21 WG1960983 1,3-Dichlorobenzene U 0.0149 0.490 1 11/18/2022 18:21 WG1960983 1,4-Dichlorobenzene U 0.0146 0.490 1 11/18/2022 18:21 WG1960983 3,3-Dichlorobenzidine U 0.0181 0.490 1 11/18/2022 18:21 WG1960983 2,4-Dinitrotoluene U 0.0141 0.490 1 11/18/2022 18:21 WG1960983 2,6-Dinitrotoluene U 0.0161 0.490 1 11/18/2022 18:21 WG1960983 Fluoranthene U 0.00885 0.0490 1 11/18/2022 18:21 WG1960983 Fluorene U 0.00798 0.0490 1 11/18/2022 18:21 WG1960983 Hexachlorobenzene U 0.0174 0.490 1 11/18/2022 18:21 WG1960983 Hexachloro-1,3-butadiene U 0.0165 0.490 1 11/18/2022 18:21 WG1960983 Hexachlorocyclopentadiene U 0.0258 0.490 1 11/18/2022 18:21 WG1960983 Hexachloroethane U 0.0193 0.490 1 11/18/2022 18:21 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0139 0.0490 1 11/18/2022 18:21 WG1960983 Isophorone U 0.0150 0.490 1 11/18/2022 18:21 WG1960983 Naphthalene U 0.0123 0.0490 1 11/18/2022 18:21 WG1960983 Nitrobenzene U 0.0171 0.490 1 11/18/2022 18:21 WG1960983 n-Nitrosodimethylamine U 0.0728 0.490 1 11/18/2022 18:21 WG1960983 n-Nitrosodiphenylamine U 0.0371 0.490 1 11/18/2022 18:21 WG1960983 n-Nitrosodi-n-propylamine U 0.0163 0.490 1 11/18/2022 18:21 WG1960983 Phenanthrene U 0.00973 0.0490 1 11/18/2022 18:21 WG1960983 Benzylbutyl phthalate U 0.0153 0.490 1 11/18/2022 18:21 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0621 0.490 1 11/18/2022 18:21 WG1960983 Di-n-butyl phthalate U 0.0168 0.490 1 11/18/2022 18:21 WG1960983 Diethyl phthalate U 0.0162 0.490 1 11/18/2022 18:21 WG1960983 Dimethyl phthalate U 0.104 0.490 1 11/18/2022 18:21 WG1960983 Di-n-octyl phthalate U 0.0331 0.490 1 11/18/2022 18:21 WG1960983 Pyrene U 0.00954 0.0490 1 11/18/2022 18:21 WG1960983 1,2,4-Trichlorobenzene U 0.0153 0.490 1 11/18/2022 18:21 WG1960983 4-Chloro-3-methylphenol U 0.0159 0.490 1 11/18/2022 18:21 WG1960983 2-Chlorophenol U 0.0162 0.490 1 11/18/2022 18:21 WG1960983 2,4-Dichlorophenol U 0.0143 0.490 1 11/18/2022 18:21 WG1960983 2,4-Dimethylphenol U 0.0128 0.490 1 11/18/2022 18:21 WG1960983 4,6-Dinitro-2-methylphenol U 0.111 0.490 1 11/18/2022 18:21 WG1960983 2,4-Dinitrophenol U 0.115 0.490 1 11/18/2022 18:21 WG1960983 2-Nitrophenol U 0.0175 0.490 1 11/18/2022 18:21 WG1960983 4-Nitrophenol U 0.0153 0.490 1 11/18/2022 18:21 WG1960983 Pentachlorophenol U 0.0132 0.490 1 11/18/2022 18:21 WG1960983 Phenol U 0.0197 0.490 1 11/18/2022 18:21 WG1960983 2,4,6-Trichlorophenol U 0.0158 0.490 1 11/18/2022 18:21 WG1960983 (S) 2-Fluorophenol 65.4 12.0-120 11/18/2022 18:21 WG1960983 (S) Phenol-d5 58.8 10.0-120 11/18/2022 18:21 WG1960983 (S) Nitrobenzene-d5 55.2 10.0-122 11/18/2022 18:21 WG1960983 (S) 2-Fluorobiphenyl 53.0 15.0-120 11/18/2022 18:21 WG1960983 (S) 2,4,6-Tribromophenol 68.0 10.0-127 11/18/2022 18:21 WG1960983 (S) p-Terphenyl-d14 63.1 10.0-120 11/18/2022 18:21 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 34 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 34 of 96 SAMPLE RESULTS - 10 L1557235 SS-5-A Collected date/time: 11/10/22 15:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 75.2 1 11/16/2022 08:20 WG1959829 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.163 0.0239 0.0532 1 11/17/2022 13:38 WG1960559 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 10.8 0.133 1.33 5 11/28/2022 20:58 WG1966023 Barium 26.6 0.202 3.32 5 11/28/2022 20:58 WG1966023 Cadmium U 0.114 1.33 5 11/28/2022 20:58 WG1966023 Chromium 39.2 0.394 6.65 5 11/28/2022 20:58 WG1966023 Lead 22.7 0.132 2.66 5 11/28/2022 20:58 WG1966023 Selenium 0.595 J 0.239 3.32 5 11/28/2022 20:58 WG1966023 Silver U 0.115 0.665 5 11/28/2022 20:58 WG1966023 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0612 0.0838 1 11/17/2022 19:03 WG1961410 Acrylonitrile U 0.00605 0.0209 1 11/17/2022 19:03 WG1961410 Benzene U 0.000783 0.00168 1 11/17/2022 19:03 WG1961410 Bromobenzene U 0.00151 0.0209 1 11/17/2022 19:03 WG1961410 Bromodichloromethane U 0.00121 0.00419 1 11/17/2022 19:03 WG1961410 Bromoform U 0.00196 0.0419 1 11/17/2022 19:03 WG1961410 Bromomethane U 0.00330 0.0209 1 11/17/2022 19:03 WG1961410 n-Butylbenzene U 0.00880 0.0209 1 11/17/2022 19:03 WG1961410 sec-Butylbenzene U 0.00483 0.0209 1 11/17/2022 19:03 WG1961410 tert-Butylbenzene U C3 0.00327 0.00838 1 11/17/2022 19:03 WG1961410 Carbon tetrachloride U 0.00150 0.00838 1 11/17/2022 19:03 WG1961410 Chlorobenzene U 0.000352 0.00419 1 11/17/2022 19:03 WG1961410 Chlorodibromomethane U 0.00103 0.00419 1 11/17/2022 19:03 WG1961410 Chloroethane U 0.00285 0.00838 1 11/17/2022 19:03 WG1961410 Chloroform U 0.00173 0.00419 1 11/17/2022 19:03 WG1961410 Chloromethane U 0.00729 0.0209 1 11/17/2022 19:03 WG1961410 2-Chlorotoluene U 0.00145 0.00419 1 11/17/2022 19:03 WG1961410 4-Chlorotoluene U 0.000754 0.00838 1 11/17/2022 19:03 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00654 0.0419 1 11/17/2022 19:03 WG1961410 1,2-Dibromoethane U 0.00109 0.00419 1 11/17/2022 19:03 WG1961410 Dibromomethane U 0.00126 0.00838 1 11/17/2022 19:03 WG1961410 1,2-Dichlorobenzene U 0.000712 0.00838 1 11/17/2022 19:03 WG1961410 1,3-Dichlorobenzene U 0.00101 0.00838 1 11/17/2022 19:03 WG1961410 1,4-Dichlorobenzene U 0.00117 0.00838 1 11/17/2022 19:03 WG1961410 Dichlorodifluoromethane U 0.00270 0.00419 1 11/17/2022 19:03 WG1961410 1,1-Dichloroethane U 0.000823 0.00419 1 11/17/2022 19:03 WG1961410 1,2-Dichloroethane U 0.00109 0.00419 1 11/17/2022 19:03 WG1961410 1,1-Dichloroethene U 0.00102 0.00419 1 11/17/2022 19:03 WG1961410 cis-1,2-Dichloroethene U 0.00123 0.00419 1 11/17/2022 19:03 WG1961410 trans-1,2-Dichloroethene U 0.00174 0.00838 1 11/17/2022 19:03 WG1961410 1,2-Dichloropropane U 0.00238 0.00838 1 11/17/2022 19:03 WG1961410 1,1-Dichloropropene U 0.00136 0.00419 1 11/17/2022 19:03 WG1961410 1,3-Dichloropropane U 0.000840 0.00838 1 11/17/2022 19:03 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 35 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 35 of 96 SAMPLE RESULTS - 10 L1557235 SS-5-A Collected date/time: 11/10/22 15:40 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00127 0.00419 1 11/17/2022 19:03 WG1961410 trans-1,3-Dichloropropene U 0.00191 0.00838 1 11/17/2022 19:03 WG1961410 2,2-Dichloropropane U 0.00231 0.00419 1 11/17/2022 19:03 WG1961410 Di-isopropyl ether U 0.000687 0.00168 1 11/17/2022 19:03 WG1961410 Ethylbenzene U 0.00124 0.00419 1 11/17/2022 19:03 WG1961410 Hexachloro-1,3-butadiene U 0.0101 0.0419 1 11/17/2022 19:03 WG1961410 Isopropylbenzene 0.00127 J 0.000712 0.00419 1 11/17/2022 19:03 WG1961410 p-Isopropyltoluene U 0.00427 0.00838 1 11/17/2022 19:03 WG1961410 2-Butanone (MEK)U 0.106 0.168 1 11/17/2022 19:03 WG1961410 Methylene Chloride U 0.0111 0.0419 1 11/17/2022 19:03 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00382 0.0419 1 11/17/2022 19:03 WG1961410 Methyl tert-butyl ether U 0.000587 0.00168 1 11/17/2022 19:03 WG1961410 Naphthalene U 0.00818 0.0209 1 11/17/2022 19:03 WG1961410 n-Propylbenzene U 0.00159 0.00838 1 11/17/2022 19:03 WG1961410 Styrene U 0.000384 0.0209 1 11/17/2022 19:03 WG1961410 1,1,1,2-Tetrachloroethane U 0.00159 0.00419 1 11/17/2022 19:03 WG1961410 1,1,2,2-Tetrachloroethane U 0.00116 0.00419 1 11/17/2022 19:03 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00126 0.00419 1 11/17/2022 19:03 WG1961410 Tetrachloroethene 0.00414 J 0.00150 0.00419 1 11/23/2022 18:51 WG1963991 Toluene U 0.00218 0.00838 1 11/17/2022 19:03 WG1961410 1,2,3-Trichlorobenzene U 0.0123 0.0209 1 11/17/2022 19:03 WG1961410 1,2,4-Trichlorobenzene U 0.00737 0.0209 1 11/17/2022 19:03 WG1961410 1,1,1-Trichloroethane U 0.00155 0.00419 1 11/17/2022 19:03 WG1961410 1,1,2-Trichloroethane U 0.00100 0.00419 1 11/17/2022 19:03 WG1961410 Trichloroethene U 0.000979 0.00168 1 11/17/2022 19:03 WG1961410 Trichlorofluoromethane U 0.00139 0.00419 1 11/17/2022 19:03 WG1961410 1,2,3-Trichloropropane U 0.00271 0.0209 1 11/17/2022 19:03 WG1961410 1,2,4-Trimethylbenzene U 0.00265 0.00838 1 11/17/2022 19:03 WG1961410 1,2,3-Trimethylbenzene U 0.00265 0.00838 1 11/17/2022 19:03 WG1961410 1,3,5-Trimethylbenzene U 0.00335 0.00838 1 11/17/2022 19:03 WG1961410 Vinyl chloride U 0.00194 0.00419 1 11/17/2022 19:03 WG1961410 Xylenes, Total U 0.00147 0.0109 1 11/17/2022 19:03 WG1961410 (S) Toluene-d8 115 75.0-131 11/17/2022 19:03 WG1961410 (S) Toluene-d8 102 75.0-131 11/23/2022 18:51 WG1963991 (S) 4-Bromofluorobenzene 101 67.0-138 11/17/2022 19:03 WG1961410 (S) 4-Bromofluorobenzene 103 67.0-138 11/23/2022 18:51 WG1963991 (S) 1,2-Dichloroethane-d4 78.0 70.0-130 11/17/2022 19:03 WG1961410 (S) 1,2-Dichloroethane-d4 84.8 70.0-130 11/23/2022 18:51 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.00759 J 0.00717 0.0443 1 11/18/2022 19:42 WG1960983 Acenaphthylene U 0.00624 0.0443 1 11/18/2022 19:42 WG1960983 Anthracene U 0.00789 0.0443 1 11/18/2022 19:42 WG1960983 Benzidine U C3 0.0832 2.22 1 11/18/2022 19:42 WG1960983 Benzo(a)anthracene U 0.00781 0.0443 1 11/18/2022 19:42 WG1960983 Benzo(b)fluoranthene U 0.00826 0.0443 1 11/18/2022 19:42 WG1960983 Benzo(k)fluoranthene U 0.00787 0.0443 1 11/18/2022 19:42 WG1960983 Benzo(g,h,i)perylene U 0.00810 0.0443 1 11/18/2022 19:42 WG1960983 Benzo(a)pyrene U 0.00823 0.0443 1 11/18/2022 19:42 WG1960983 Bis(2-chlorethoxy)methane U 0.0133 0.443 1 11/18/2022 19:42 WG1960983 Bis(2-chloroethyl)ether U 0.0146 0.443 1 11/18/2022 19:42 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0191 0.443 1 11/18/2022 19:42 WG1960983 4-Bromophenyl-phenylether U 0.0156 0.443 1 11/18/2022 19:42 WG1960983 2-Chloronaphthalene U 0.00778 0.0443 1 11/18/2022 19:42 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 36 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 36 of 96 SAMPLE RESULTS - 10 L1557235 SS-5-A Collected date/time: 11/10/22 15:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0154 0.443 1 11/18/2022 19:42 WG1960983 Chrysene U 0.00880 0.0443 1 11/18/2022 19:42 WG1960983 Dibenz(a,h)anthracene U 0.0123 0.0443 1 11/18/2022 19:42 WG1960983 1,2-Dichlorobenzene U 0.0131 0.443 1 11/18/2022 19:42 WG1960983 1,3-Dichlorobenzene U 0.0134 0.443 1 11/18/2022 19:42 WG1960983 1,4-Dichlorobenzene U 0.0132 0.443 1 11/18/2022 19:42 WG1960983 3,3-Dichlorobenzidine U 0.0164 0.443 1 11/18/2022 19:42 WG1960983 2,4-Dinitrotoluene U 0.0127 0.443 1 11/18/2022 19:42 WG1960983 2,6-Dinitrotoluene U 0.0145 0.443 1 11/18/2022 19:42 WG1960983 Fluoranthene U 0.00799 0.0443 1 11/18/2022 19:42 WG1960983 Fluorene 0.00812 J 0.00721 0.0443 1 11/18/2022 19:42 WG1960983 Hexachlorobenzene U 0.0157 0.443 1 11/18/2022 19:42 WG1960983 Hexachloro-1,3-butadiene U 0.0149 0.443 1 11/18/2022 19:42 WG1960983 Hexachlorocyclopentadiene U 0.0233 0.443 1 11/18/2022 19:42 WG1960983 Hexachloroethane U 0.0174 0.443 1 11/18/2022 19:42 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0125 0.0443 1 11/18/2022 19:42 WG1960983 Isophorone U 0.0136 0.443 1 11/18/2022 19:42 WG1960983 Naphthalene 0.0863 0.0111 0.0443 1 11/18/2022 19:42 WG1960983 Nitrobenzene U 0.0154 0.443 1 11/18/2022 19:42 WG1960983 n-Nitrosodimethylamine U 0.0657 0.443 1 11/18/2022 19:42 WG1960983 n-Nitrosodiphenylamine U 0.0335 0.443 1 11/18/2022 19:42 WG1960983 n-Nitrosodi-n-propylamine U 0.0148 0.443 1 11/18/2022 19:42 WG1960983 Phenanthrene 0.0146 J 0.00879 0.0443 1 11/18/2022 19:42 WG1960983 Benzylbutyl phthalate U 0.0138 0.443 1 11/18/2022 19:42 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0561 0.443 1 11/18/2022 19:42 WG1960983 Di-n-butyl phthalate U 0.0152 0.443 1 11/18/2022 19:42 WG1960983 Diethyl phthalate U 0.0146 0.443 1 11/18/2022 19:42 WG1960983 Dimethyl phthalate U 0.0939 0.443 1 11/18/2022 19:42 WG1960983 Di-n-octyl phthalate U 0.0299 0.443 1 11/18/2022 19:42 WG1960983 Pyrene U 0.00862 0.0443 1 11/18/2022 19:42 WG1960983 1,2,4-Trichlorobenzene U 0.0138 0.443 1 11/18/2022 19:42 WG1960983 4-Chloro-3-methylphenol U 0.0144 0.443 1 11/18/2022 19:42 WG1960983 2-Chlorophenol U 0.0146 0.443 1 11/18/2022 19:42 WG1960983 2,4-Dichlorophenol U 0.0129 0.443 1 11/18/2022 19:42 WG1960983 2,4-Dimethylphenol U 0.0116 0.443 1 11/18/2022 19:42 WG1960983 4,6-Dinitro-2-methylphenol U 0.100 0.443 1 11/18/2022 19:42 WG1960983 2,4-Dinitrophenol U 0.104 0.443 1 11/18/2022 19:42 WG1960983 2-Nitrophenol U 0.0158 0.443 1 11/18/2022 19:42 WG1960983 4-Nitrophenol U 0.0138 0.443 1 11/18/2022 19:42 WG1960983 Pentachlorophenol U 0.0119 0.443 1 11/18/2022 19:42 WG1960983 Phenol U 0.0178 0.443 1 11/18/2022 19:42 WG1960983 2,4,6-Trichlorophenol U 0.0142 0.443 1 11/18/2022 19:42 WG1960983 (S) 2-Fluorophenol 64.8 12.0-120 11/18/2022 19:42 WG1960983 (S) Phenol-d5 60.2 10.0-120 11/18/2022 19:42 WG1960983 (S) Nitrobenzene-d5 56.5 10.0-122 11/18/2022 19:42 WG1960983 (S) 2-Fluorobiphenyl 54.7 15.0-120 11/18/2022 19:42 WG1960983 (S) 2,4,6-Tribromophenol 73.8 10.0-127 11/18/2022 19:42 WG1960983 (S) p-Terphenyl-d14 64.9 10.0-120 11/18/2022 19:42 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 37 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 37 of 96 SAMPLE RESULTS - 11 L1557235 SS-6 Collected date/time: 11/10/22 15:55 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 68.4 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0849 0.0263 0.0585 1 11/17/2022 14:29 WG1960561 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 15.3 0.146 1.46 5 11/29/2022 20:30 WG1961432 Barium 25.1 0.222 3.66 5 11/29/2022 20:30 WG1961432 Cadmium U 0.125 1.46 5 11/29/2022 20:30 WG1961432 Chromium 34.5 0.433 7.31 5 11/29/2022 20:30 WG1961432 Lead 11.9 0.145 2.92 5 11/29/2022 20:30 WG1961432 Selenium 1.12 J 0.263 3.66 5 11/29/2022 20:30 WG1961432 Silver U 0.126 0.731 5 11/29/2022 20:30 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0734 0.101 1 11/17/2022 19:24 WG1961410 Acrylonitrile U 0.00726 0.0252 1 11/17/2022 19:24 WG1961410 Benzene U 0.000940 0.00201 1 11/17/2022 19:24 WG1961410 Bromobenzene U 0.00181 0.0252 1 11/17/2022 19:24 WG1961410 Bromodichloromethane U 0.00146 0.00503 1 11/17/2022 19:24 WG1961410 Bromoform U 0.00235 0.0503 1 11/17/2022 19:24 WG1961410 Bromomethane U 0.00396 0.0252 1 11/17/2022 19:24 WG1961410 n-Butylbenzene U 0.0106 0.0252 1 11/17/2022 19:24 WG1961410 sec-Butylbenzene U 0.00580 0.0252 1 11/17/2022 19:24 WG1961410 tert-Butylbenzene U C3 0.00392 0.0101 1 11/17/2022 19:24 WG1961410 Carbon tetrachloride U 0.00181 0.0101 1 11/17/2022 19:24 WG1961410 Chlorobenzene U 0.000423 0.00503 1 11/17/2022 19:24 WG1961410 Chlorodibromomethane U 0.00123 0.00503 1 11/17/2022 19:24 WG1961410 Chloroethane U 0.00342 0.0101 1 11/17/2022 19:24 WG1961410 Chloroform U 0.00207 0.00503 1 11/17/2022 19:24 WG1961410 Chloromethane U 0.00875 0.0252 1 11/17/2022 19:24 WG1961410 2-Chlorotoluene U 0.00174 0.00503 1 11/17/2022 19:24 WG1961410 4-Chlorotoluene U 0.000905 0.0101 1 11/17/2022 19:24 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00785 0.0503 1 11/17/2022 19:24 WG1961410 1,2-Dibromoethane U 0.00130 0.00503 1 11/17/2022 19:24 WG1961410 Dibromomethane U 0.00151 0.0101 1 11/17/2022 19:24 WG1961410 1,2-Dichlorobenzene U 0.000855 0.0101 1 11/17/2022 19:24 WG1961410 1,3-Dichlorobenzene U 0.00121 0.0101 1 11/17/2022 19:24 WG1961410 1,4-Dichlorobenzene U 0.00141 0.0101 1 11/17/2022 19:24 WG1961410 Dichlorodifluoromethane U 0.00324 0.00503 1 11/17/2022 19:24 WG1961410 1,1-Dichloroethane U 0.000988 0.00503 1 11/17/2022 19:24 WG1961410 1,2-Dichloroethane U 0.00131 0.00503 1 11/17/2022 19:24 WG1961410 1,1-Dichloroethene U 0.00122 0.00503 1 11/17/2022 19:24 WG1961410 cis-1,2-Dichloroethene U 0.00148 0.00503 1 11/17/2022 19:24 WG1961410 trans-1,2-Dichloroethene U 0.00209 0.0101 1 11/17/2022 19:24 WG1961410 1,2-Dichloropropane U 0.00286 0.0101 1 11/17/2022 19:24 WG1961410 1,1-Dichloropropene U 0.00163 0.00503 1 11/17/2022 19:24 WG1961410 1,3-Dichloropropane U 0.00101 0.0101 1 11/17/2022 19:24 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 38 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 38 of 96 SAMPLE RESULTS - 11 L1557235 SS-6 Collected date/time: 11/10/22 15:55 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00152 0.00503 1 11/17/2022 19:24 WG1961410 trans-1,3-Dichloropropene U 0.00229 0.0101 1 11/17/2022 19:24 WG1961410 2,2-Dichloropropane U 0.00278 0.00503 1 11/17/2022 19:24 WG1961410 Di-isopropyl ether U 0.000825 0.00201 1 11/17/2022 19:24 WG1961410 Ethylbenzene U 0.00148 0.00503 1 11/17/2022 19:24 WG1961410 Hexachloro-1,3-butadiene U 0.0121 0.0503 1 11/17/2022 19:24 WG1961410 Isopropylbenzene U 0.000855 0.00503 1 11/17/2022 19:24 WG1961410 p-Isopropyltoluene U 0.00513 0.0101 1 11/17/2022 19:24 WG1961410 2-Butanone (MEK)U 0.128 0.201 1 11/17/2022 19:24 WG1961410 Methylene Chloride U 0.0134 0.0503 1 11/17/2022 19:24 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00459 0.0503 1 11/17/2022 19:24 WG1961410 Methyl tert-butyl ether U 0.000704 0.00201 1 11/17/2022 19:24 WG1961410 Naphthalene U 0.00982 0.0252 1 11/17/2022 19:24 WG1961410 n-Propylbenzene U 0.00191 0.0101 1 11/17/2022 19:24 WG1961410 Styrene U 0.000461 0.0252 1 11/17/2022 19:24 WG1961410 1,1,1,2-Tetrachloroethane U 0.00191 0.00503 1 11/17/2022 19:24 WG1961410 1,1,2,2-Tetrachloroethane U 0.00140 0.00503 1 11/17/2022 19:24 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00152 0.00503 1 11/17/2022 19:24 WG1961410 Tetrachloroethene 0.00384 J 0.00180 0.00503 1 11/23/2022 19:10 WG1963991 Toluene U 0.00262 0.0101 1 11/17/2022 19:24 WG1961410 1,2,3-Trichlorobenzene U 0.0147 0.0252 1 11/17/2022 19:24 WG1961410 1,2,4-Trichlorobenzene U 0.00885 0.0252 1 11/17/2022 19:24 WG1961410 1,1,1-Trichloroethane U 0.00186 0.00503 1 11/17/2022 19:24 WG1961410 1,1,2-Trichloroethane U 0.00120 0.00503 1 11/17/2022 19:24 WG1961410 Trichloroethene U 0.00118 0.00201 1 11/17/2022 19:24 WG1961410 Trichlorofluoromethane U 0.00166 0.00503 1 11/17/2022 19:24 WG1961410 1,2,3-Trichloropropane U 0.00326 0.0252 1 11/17/2022 19:24 WG1961410 1,2,4-Trimethylbenzene U 0.00318 0.0101 1 11/17/2022 19:24 WG1961410 1,2,3-Trimethylbenzene U 0.00318 0.0101 1 11/17/2022 19:24 WG1961410 1,3,5-Trimethylbenzene U 0.00402 0.0101 1 11/17/2022 19:24 WG1961410 Vinyl chloride U 0.00233 0.00503 1 11/17/2022 19:24 WG1961410 Xylenes, Total U 0.00177 0.0131 1 11/17/2022 19:24 WG1961410 (S) Toluene-d8 114 75.0-131 11/17/2022 19:24 WG1961410 (S) Toluene-d8 102 75.0-131 11/23/2022 19:10 WG1963991 (S) 4-Bromofluorobenzene 104 67.0-138 11/17/2022 19:24 WG1961410 (S) 4-Bromofluorobenzene 102 67.0-138 11/23/2022 19:10 WG1963991 (S) 1,2-Dichloroethane-d4 76.8 70.0-130 11/17/2022 19:24 WG1961410 (S) 1,2-Dichloroethane-d4 84.4 70.0-130 11/23/2022 19:10 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00788 0.0487 1 11/18/2022 19:02 WG1960983 Acenaphthylene U 0.00686 0.0487 1 11/18/2022 19:02 WG1960983 Anthracene U 0.00867 0.0487 1 11/18/2022 19:02 WG1960983 Benzidine U C3 0.0915 2.44 1 11/18/2022 19:02 WG1960983 Benzo(a)anthracene U 0.00858 0.0487 1 11/18/2022 19:02 WG1960983 Benzo(b)fluoranthene U 0.00908 0.0487 1 11/18/2022 19:02 WG1960983 Benzo(k)fluoranthene U 0.00866 0.0487 1 11/18/2022 19:02 WG1960983 Benzo(g,h,i)perylene U 0.00891 0.0487 1 11/18/2022 19:02 WG1960983 Benzo(a)pyrene U 0.00905 0.0487 1 11/18/2022 19:02 WG1960983 Bis(2-chlorethoxy)methane U 0.0146 0.487 1 11/18/2022 19:02 WG1960983 Bis(2-chloroethyl)ether U 0.0161 0.487 1 11/18/2022 19:02 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0211 0.487 1 11/18/2022 19:02 WG1960983 4-Bromophenyl-phenylether U 0.0171 0.487 1 11/18/2022 19:02 WG1960983 2-Chloronaphthalene U 0.00855 0.0487 1 11/18/2022 19:02 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 39 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 39 of 96 SAMPLE RESULTS - 11 L1557235 SS-6 Collected date/time: 11/10/22 15:55 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0170 0.487 1 11/18/2022 19:02 WG1960983 Chrysene U 0.00968 0.0487 1 11/18/2022 19:02 WG1960983 Dibenz(a,h)anthracene U 0.0135 0.0487 1 11/18/2022 19:02 WG1960983 1,2-Dichlorobenzene U 0.0144 0.487 1 11/18/2022 19:02 WG1960983 1,3-Dichlorobenzene U 0.0148 0.487 1 11/18/2022 19:02 WG1960983 1,4-Dichlorobenzene U 0.0145 0.487 1 11/18/2022 19:02 WG1960983 3,3-Dichlorobenzidine U 0.0180 0.487 1 11/18/2022 19:02 WG1960983 2,4-Dinitrotoluene U 0.0140 0.487 1 11/18/2022 19:02 WG1960983 2,6-Dinitrotoluene U 0.0159 0.487 1 11/18/2022 19:02 WG1960983 Fluoranthene U 0.00879 0.0487 1 11/18/2022 19:02 WG1960983 Fluorene U 0.00793 0.0487 1 11/18/2022 19:02 WG1960983 Hexachlorobenzene U 0.0173 0.487 1 11/18/2022 19:02 WG1960983 Hexachloro-1,3-butadiene U 0.0164 0.487 1 11/18/2022 19:02 WG1960983 Hexachlorocyclopentadiene U 0.0256 0.487 1 11/18/2022 19:02 WG1960983 Hexachloroethane U 0.0192 0.487 1 11/18/2022 19:02 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0138 0.0487 1 11/18/2022 19:02 WG1960983 Isophorone U 0.0149 0.487 1 11/18/2022 19:02 WG1960983 Naphthalene U 0.0122 0.0487 1 11/18/2022 19:02 WG1960983 Nitrobenzene U 0.0170 0.487 1 11/18/2022 19:02 WG1960983 n-Nitrosodimethylamine U 0.0722 0.487 1 11/18/2022 19:02 WG1960983 n-Nitrosodiphenylamine U 0.0369 0.487 1 11/18/2022 19:02 WG1960983 n-Nitrosodi-n-propylamine U 0.0162 0.487 1 11/18/2022 19:02 WG1960983 Phenanthrene U 0.00967 0.0487 1 11/18/2022 19:02 WG1960983 Benzylbutyl phthalate U 0.0152 0.487 1 11/18/2022 19:02 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0617 0.487 1 11/18/2022 19:02 WG1960983 Di-n-butyl phthalate U 0.0167 0.487 1 11/18/2022 19:02 WG1960983 Diethyl phthalate U 0.0161 0.487 1 11/18/2022 19:02 WG1960983 Dimethyl phthalate U 0.103 0.487 1 11/18/2022 19:02 WG1960983 Di-n-octyl phthalate U 0.0329 0.487 1 11/18/2022 19:02 WG1960983 Pyrene U 0.00948 0.0487 1 11/18/2022 19:02 WG1960983 1,2,4-Trichlorobenzene U 0.0152 0.487 1 11/18/2022 19:02 WG1960983 4-Chloro-3-methylphenol U 0.0158 0.487 1 11/18/2022 19:02 WG1960983 2-Chlorophenol U 0.0161 0.487 1 11/18/2022 19:02 WG1960983 2,4-Dichlorophenol U 0.0142 0.487 1 11/18/2022 19:02 WG1960983 2,4-Dimethylphenol U 0.0127 0.487 1 11/18/2022 19:02 WG1960983 4,6-Dinitro-2-methylphenol U 0.110 0.487 1 11/18/2022 19:02 WG1960983 2,4-Dinitrophenol U 0.114 0.487 1 11/18/2022 19:02 WG1960983 2-Nitrophenol U 0.0174 0.487 1 11/18/2022 19:02 WG1960983 4-Nitrophenol U 0.0152 0.487 1 11/18/2022 19:02 WG1960983 Pentachlorophenol U 0.0131 0.487 1 11/18/2022 19:02 WG1960983 Phenol U 0.0196 0.487 1 11/18/2022 19:02 WG1960983 2,4,6-Trichlorophenol U 0.0156 0.487 1 11/18/2022 19:02 WG1960983 (S) 2-Fluorophenol 63.6 12.0-120 11/18/2022 19:02 WG1960983 (S) Phenol-d5 58.8 10.0-120 11/18/2022 19:02 WG1960983 (S) Nitrobenzene-d5 54.9 10.0-122 11/18/2022 19:02 WG1960983 (S) 2-Fluorobiphenyl 51.9 15.0-120 11/18/2022 19:02 WG1960983 (S) 2,4,6-Tribromophenol 66.4 10.0-127 11/18/2022 19:02 WG1960983 (S) p-Terphenyl-d14 62.3 10.0-120 11/18/2022 19:02 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 40 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 40 of 96 SAMPLE RESULTS - 12 L1557235 SS-6-A Collected date/time: 11/10/22 15:55 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 83.0 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.143 0.0217 0.0482 1 11/17/2022 14:32 WG1960561 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 11.4 0.121 1.21 5 11/29/2022 20:33 WG1961432 Barium 37.2 0.183 3.01 5 11/29/2022 20:33 WG1961432 Cadmium U 0.103 1.21 5 11/29/2022 20:33 WG1961432 Chromium 38.3 0.357 6.03 5 11/29/2022 20:33 WG1961432 Lead 12.6 0.119 2.41 5 11/29/2022 20:33 WG1961432 Selenium 1.42 J 0.217 3.01 5 11/29/2022 20:33 WG1961432 Silver U 0.104 0.603 5 11/29/2022 20:33 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0524 0.0718 1 11/17/2022 19:45 WG1961410 Acrylonitrile U 0.00519 0.0180 1 11/17/2022 19:45 WG1961410 Benzene U 0.000671 0.00144 1 11/17/2022 19:45 WG1961410 Bromobenzene U 0.00129 0.0180 1 11/17/2022 19:45 WG1961410 Bromodichloromethane U 0.00104 0.00359 1 11/17/2022 19:45 WG1961410 Bromoform U 0.00168 0.0359 1 11/17/2022 19:45 WG1961410 Bromomethane U 0.00283 0.0180 1 11/17/2022 19:45 WG1961410 n-Butylbenzene U 0.00754 0.0180 1 11/17/2022 19:45 WG1961410 sec-Butylbenzene U 0.00414 0.0180 1 11/17/2022 19:45 WG1961410 tert-Butylbenzene U C3 0.00280 0.00718 1 11/17/2022 19:45 WG1961410 Carbon tetrachloride U 0.00129 0.00718 1 11/17/2022 19:45 WG1961410 Chlorobenzene U 0.000302 0.00359 1 11/17/2022 19:45 WG1961410 Chlorodibromomethane U 0.000879 0.00359 1 11/17/2022 19:45 WG1961410 Chloroethane U 0.00244 0.00718 1 11/17/2022 19:45 WG1961410 Chloroform U 0.00148 0.00359 1 11/17/2022 19:45 WG1961410 Chloromethane U 0.00625 0.0180 1 11/17/2022 19:45 WG1961410 2-Chlorotoluene U 0.00124 0.00359 1 11/17/2022 19:45 WG1961410 4-Chlorotoluene U 0.000646 0.00718 1 11/17/2022 19:45 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00560 0.0359 1 11/17/2022 19:45 WG1961410 1,2-Dibromoethane U 0.000931 0.00359 1 11/17/2022 19:45 WG1961410 Dibromomethane U 0.00108 0.00718 1 11/17/2022 19:45 WG1961410 1,2-Dichlorobenzene U 0.000611 0.00718 1 11/17/2022 19:45 WG1961410 1,3-Dichlorobenzene U 0.000862 0.00718 1 11/17/2022 19:45 WG1961410 1,4-Dichlorobenzene U 0.00101 0.00718 1 11/17/2022 19:45 WG1961410 Dichlorodifluoromethane U 0.00231 0.00359 1 11/17/2022 19:45 WG1961410 1,1-Dichloroethane U 0.000705 0.00359 1 11/17/2022 19:45 WG1961410 1,2-Dichloroethane U 0.000932 0.00359 1 11/17/2022 19:45 WG1961410 1,1-Dichloroethene U 0.000871 0.00359 1 11/17/2022 19:45 WG1961410 cis-1,2-Dichloroethene U 0.00105 0.00359 1 11/17/2022 19:45 WG1961410 trans-1,2-Dichloroethene U 0.00149 0.00718 1 11/17/2022 19:45 WG1961410 1,2-Dichloropropane U 0.00204 0.00718 1 11/17/2022 19:45 WG1961410 1,1-Dichloropropene U 0.00116 0.00359 1 11/17/2022 19:45 WG1961410 1,3-Dichloropropane U 0.000720 0.00718 1 11/17/2022 19:45 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 41 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 41 of 96 SAMPLE RESULTS - 12 L1557235 SS-6-A Collected date/time: 11/10/22 15:55 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00109 0.00359 1 11/17/2022 19:45 WG1961410 trans-1,3-Dichloropropene U 0.00164 0.00718 1 11/17/2022 19:45 WG1961410 2,2-Dichloropropane U 0.00198 0.00359 1 11/17/2022 19:45 WG1961410 Di-isopropyl ether U 0.000589 0.00144 1 11/17/2022 19:45 WG1961410 Ethylbenzene U 0.00106 0.00359 1 11/17/2022 19:45 WG1961410 Hexachloro-1,3-butadiene U 0.00862 0.0359 1 11/17/2022 19:45 WG1961410 Isopropylbenzene U 0.000611 0.00359 1 11/17/2022 19:45 WG1961410 p-Isopropyltoluene 0.00460 J 0.00366 0.00718 1 11/17/2022 19:45 WG1961410 2-Butanone (MEK)U 0.0912 0.144 1 11/17/2022 19:45 WG1961410 Methylene Chloride U 0.00954 0.0359 1 11/17/2022 19:45 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00328 0.0359 1 11/17/2022 19:45 WG1961410 Methyl tert-butyl ether U 0.000503 0.00144 1 11/17/2022 19:45 WG1961410 Naphthalene U 0.00701 0.0180 1 11/17/2022 19:45 WG1961410 n-Propylbenzene U 0.00136 0.00718 1 11/17/2022 19:45 WG1961410 Styrene U 0.000329 0.0180 1 11/17/2022 19:45 WG1961410 1,1,1,2-Tetrachloroethane U 0.00136 0.00359 1 11/17/2022 19:45 WG1961410 1,1,2,2-Tetrachloroethane U 0.000998 0.00359 1 11/17/2022 19:45 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00108 0.00359 1 11/17/2022 19:45 WG1961410 Tetrachloroethene 0.00521 0.00129 0.00359 1 11/23/2022 19:29 WG1963991 Toluene U 0.00187 0.00718 1 11/17/2022 19:45 WG1961410 1,2,3-Trichlorobenzene U 0.0105 0.0180 1 11/17/2022 19:45 WG1961410 1,2,4-Trichlorobenzene U 0.00632 0.0180 1 11/17/2022 19:45 WG1961410 1,1,1-Trichloroethane U 0.00133 0.00359 1 11/17/2022 19:45 WG1961410 1,1,2-Trichloroethane U 0.000858 0.00359 1 11/17/2022 19:45 WG1961410 Trichloroethene U 0.000839 0.00144 1 11/17/2022 19:45 WG1961410 Trichlorofluoromethane U 0.00119 0.00359 1 11/17/2022 19:45 WG1961410 1,2,3-Trichloropropane U 0.00233 0.0180 1 11/17/2022 19:45 WG1961410 1,2,4-Trimethylbenzene U 0.00227 0.00718 1 11/17/2022 19:45 WG1961410 1,2,3-Trimethylbenzene U 0.00227 0.00718 1 11/17/2022 19:45 WG1961410 1,3,5-Trimethylbenzene U 0.00287 0.00718 1 11/17/2022 19:45 WG1961410 Vinyl chloride U 0.00167 0.00359 1 11/17/2022 19:45 WG1961410 Xylenes, Total U 0.00126 0.00934 1 11/17/2022 19:45 WG1961410 (S) Toluene-d8 113 75.0-131 11/17/2022 19:45 WG1961410 (S) Toluene-d8 99.7 75.0-131 11/23/2022 19:29 WG1963991 (S) 4-Bromofluorobenzene 101 67.0-138 11/17/2022 19:45 WG1961410 (S) 4-Bromofluorobenzene 99.2 67.0-138 11/23/2022 19:29 WG1963991 (S) 1,2-Dichloroethane-d4 78.2 70.0-130 11/17/2022 19:45 WG1961410 (S) 1,2-Dichloroethane-d4 82.6 70.0-130 11/23/2022 19:29 WG1963991 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00650 0.0401 1 11/18/2022 20:02 WG1960983 Acenaphthylene U 0.00565 0.0401 1 11/18/2022 20:02 WG1960983 Anthracene U 0.00715 0.0401 1 11/18/2022 20:02 WG1960983 Benzidine U C3 0.0755 2.01 1 11/18/2022 20:02 WG1960983 Benzo(a)anthracene U 0.00707 0.0401 1 11/18/2022 20:02 WG1960983 Benzo(b)fluoranthene U 0.00748 0.0401 1 11/18/2022 20:02 WG1960983 Benzo(k)fluoranthene U 0.00714 0.0401 1 11/18/2022 20:02 WG1960983 Benzo(g,h,i)perylene U 0.00734 0.0401 1 11/18/2022 20:02 WG1960983 Benzo(a)pyrene U 0.00746 0.0401 1 11/18/2022 20:02 WG1960983 Bis(2-chlorethoxy)methane U 0.0121 0.401 1 11/18/2022 20:02 WG1960983 Bis(2-chloroethyl)ether U 0.0133 0.401 1 11/18/2022 20:02 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0174 0.401 1 11/18/2022 20:02 WG1960983 4-Bromophenyl-phenylether U 0.0141 0.401 1 11/18/2022 20:02 WG1960983 2-Chloronaphthalene U 0.00705 0.0401 1 11/18/2022 20:02 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 42 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 42 of 96 SAMPLE RESULTS - 12 L1557235 SS-6-A Collected date/time: 11/10/22 15:55 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 4-Chlorophenyl-phenylether U 0.0140 0.401 1 11/18/2022 20:02 WG1960983 Chrysene U 0.00798 0.0401 1 11/18/2022 20:02 WG1960983 Dibenz(a,h)anthracene U 0.0111 0.0401 1 11/18/2022 20:02 WG1960983 1,2-Dichlorobenzene U 0.0119 0.401 1 11/18/2022 20:02 WG1960983 1,3-Dichlorobenzene U 0.0122 0.401 1 11/18/2022 20:02 WG1960983 1,4-Dichlorobenzene U 0.0119 0.401 1 11/18/2022 20:02 WG1960983 3,3-Dichlorobenzidine U 0.0148 0.401 1 11/18/2022 20:02 WG1960983 2,4-Dinitrotoluene U 0.0115 0.401 1 11/18/2022 20:02 WG1960983 2,6-Dinitrotoluene U 0.0131 0.401 1 11/18/2022 20:02 WG1960983 Fluoranthene U 0.00724 0.0401 1 11/18/2022 20:02 WG1960983 Fluorene U 0.00653 0.0401 1 11/18/2022 20:02 WG1960983 Hexachlorobenzene U 0.0142 0.401 1 11/18/2022 20:02 WG1960983 Hexachloro-1,3-butadiene U 0.0135 0.401 1 11/18/2022 20:02 WG1960983 Hexachlorocyclopentadiene U 0.0211 0.401 1 11/18/2022 20:02 WG1960983 Hexachloroethane U 0.0158 0.401 1 11/18/2022 20:02 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0113 0.0401 1 11/18/2022 20:02 WG1960983 Isophorone U 0.0123 0.401 1 11/18/2022 20:02 WG1960983 Naphthalene U 0.0101 0.0401 1 11/18/2022 20:02 WG1960983 Nitrobenzene U 0.0140 0.401 1 11/18/2022 20:02 WG1960983 n-Nitrosodimethylamine U 0.0595 0.401 1 11/18/2022 20:02 WG1960983 n-Nitrosodiphenylamine U 0.0304 0.401 1 11/18/2022 20:02 WG1960983 n-Nitrosodi-n-propylamine U 0.0134 0.401 1 11/18/2022 20:02 WG1960983 Phenanthrene U 0.00797 0.0401 1 11/18/2022 20:02 WG1960983 Benzylbutyl phthalate U 0.0125 0.401 1 11/18/2022 20:02 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0509 0.401 1 11/18/2022 20:02 WG1960983 Di-n-butyl phthalate U 0.0137 0.401 1 11/18/2022 20:02 WG1960983 Diethyl phthalate U 0.0133 0.401 1 11/18/2022 20:02 WG1960983 Dimethyl phthalate U 0.0851 0.401 1 11/18/2022 20:02 WG1960983 Di-n-octyl phthalate U 0.0271 0.401 1 11/18/2022 20:02 WG1960983 Pyrene U 0.00781 0.0401 1 11/18/2022 20:02 WG1960983 1,2,4-Trichlorobenzene U 0.0125 0.401 1 11/18/2022 20:02 WG1960983 4-Chloro-3-methylphenol U 0.0130 0.401 1 11/18/2022 20:02 WG1960983 2-Chlorophenol U 0.0133 0.401 1 11/18/2022 20:02 WG1960983 2,4-Dichlorophenol U 0.0117 0.401 1 11/18/2022 20:02 WG1960983 2,4-Dimethylphenol U 0.0105 0.401 1 11/18/2022 20:02 WG1960983 4,6-Dinitro-2-methylphenol U 0.0910 0.401 1 11/18/2022 20:02 WG1960983 2,4-Dinitrophenol U 0.0939 0.401 1 11/18/2022 20:02 WG1960983 2-Nitrophenol U 0.0143 0.401 1 11/18/2022 20:02 WG1960983 4-Nitrophenol U 0.0125 0.401 1 11/18/2022 20:02 WG1960983 Pentachlorophenol U 0.0108 0.401 1 11/18/2022 20:02 WG1960983 Phenol U 0.0162 0.401 1 11/18/2022 20:02 WG1960983 2,4,6-Trichlorophenol U 0.0129 0.401 1 11/18/2022 20:02 WG1960983 (S) 2-Fluorophenol 57.7 12.0-120 11/18/2022 20:02 WG1960983 (S) Phenol-d5 53.6 10.0-120 11/18/2022 20:02 WG1960983 (S) Nitrobenzene-d5 51.9 10.0-122 11/18/2022 20:02 WG1960983 (S) 2-Fluorobiphenyl 49.4 15.0-120 11/18/2022 20:02 WG1960983 (S) 2,4,6-Tribromophenol 64.4 10.0-127 11/18/2022 20:02 WG1960983 (S) p-Terphenyl-d14 59.1 10.0-120 11/18/2022 20:02 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 43 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 43 of 96 SAMPLE RESULTS - 13 L1557235 SS-7 Collected date/time: 11/10/22 15:45 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 78.9 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0513 0.0228 0.0507 1 11/17/2022 14:34 WG1960561 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.82 0.127 1.27 5 11/29/2022 20:36 WG1961432 Barium 33.8 0.193 3.17 5 11/29/2022 20:36 WG1961432 Cadmium 0.905 J 0.108 1.27 5 11/29/2022 20:36 WG1961432 Chromium 12.3 0.375 6.34 5 11/29/2022 20:36 WG1961432 Lead 56.9 0.126 2.54 5 11/29/2022 20:36 WG1961432 Selenium 0.827 J 0.228 3.17 5 11/29/2022 20:36 WG1961432 Silver U 0.110 0.634 5 11/29/2022 20:36 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0572 0.0784 1 11/17/2022 20:06 WG1961410 Acrylonitrile U 0.00566 0.0196 1 11/17/2022 20:06 WG1961410 Benzene U 0.000732 0.00157 1 11/17/2022 20:06 WG1961410 Bromobenzene U 0.00141 0.0196 1 11/17/2022 20:06 WG1961410 Bromodichloromethane U 0.00114 0.00392 1 11/17/2022 20:06 WG1961410 Bromoform U 0.00183 0.0392 1 11/17/2022 20:06 WG1961410 Bromomethane U 0.00309 0.0196 1 11/17/2022 20:06 WG1961410 n-Butylbenzene U 0.00823 0.0196 1 11/17/2022 20:06 WG1961410 sec-Butylbenzene 0.00477 B J 0.00451 0.0196 1 11/17/2022 20:06 WG1961410 tert-Butylbenzene U C3 0.00306 0.00784 1 11/17/2022 20:06 WG1961410 Carbon tetrachloride U 0.00141 0.00784 1 11/17/2022 20:06 WG1961410 Chlorobenzene U 0.000329 0.00392 1 11/17/2022 20:06 WG1961410 Chlorodibromomethane U 0.000959 0.00392 1 11/17/2022 20:06 WG1961410 Chloroethane U 0.00266 0.00784 1 11/17/2022 20:06 WG1961410 Chloroform U 0.00161 0.00392 1 11/17/2022 20:06 WG1961410 Chloromethane U 0.00682 0.0196 1 11/17/2022 20:06 WG1961410 2-Chlorotoluene U 0.00136 0.00392 1 11/17/2022 20:06 WG1961410 4-Chlorotoluene U 0.000705 0.00784 1 11/17/2022 20:06 WG1961410 1,2-Dibromo-3-Chloropropane U C3 0.00611 0.0392 1 11/17/2022 20:06 WG1961410 1,2-Dibromoethane U 0.00102 0.00392 1 11/17/2022 20:06 WG1961410 Dibromomethane U 0.00118 0.00784 1 11/17/2022 20:06 WG1961410 1,2-Dichlorobenzene U 0.000666 0.00784 1 11/17/2022 20:06 WG1961410 1,3-Dichlorobenzene U 0.000941 0.00784 1 11/17/2022 20:06 WG1961410 1,4-Dichlorobenzene U 0.00110 0.00784 1 11/17/2022 20:06 WG1961410 Dichlorodifluoromethane U 0.00252 0.00392 1 11/17/2022 20:06 WG1961410 1,1-Dichloroethane U 0.000770 0.00392 1 11/17/2022 20:06 WG1961410 1,2-Dichloroethane U 0.00102 0.00392 1 11/17/2022 20:06 WG1961410 1,1-Dichloroethene U 0.000950 0.00392 1 11/17/2022 20:06 WG1961410 cis-1,2-Dichloroethene U 0.00115 0.00392 1 11/17/2022 20:06 WG1961410 trans-1,2-Dichloroethene U 0.00163 0.00784 1 11/17/2022 20:06 WG1961410 1,2-Dichloropropane U 0.00223 0.00784 1 11/17/2022 20:06 WG1961410 1,1-Dichloropropene U 0.00127 0.00392 1 11/17/2022 20:06 WG1961410 1,3-Dichloropropane U 0.000785 0.00784 1 11/17/2022 20:06 WG1961410 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 44 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 44 of 96 SAMPLE RESULTS - 13 L1557235 SS-7 Collected date/time: 11/10/22 15:45 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U J4 0.00119 0.00392 1 11/17/2022 20:06 WG1961410 trans-1,3-Dichloropropene U 0.00179 0.00784 1 11/17/2022 20:06 WG1961410 2,2-Dichloropropane U 0.00216 0.00392 1 11/17/2022 20:06 WG1961410 Di-isopropyl ether U 0.000643 0.00157 1 11/17/2022 20:06 WG1961410 Ethylbenzene U 0.00116 0.00392 1 11/17/2022 20:06 WG1961410 Hexachloro-1,3-butadiene U 0.00941 0.0392 1 11/17/2022 20:06 WG1961410 Isopropylbenzene U 0.000666 0.00392 1 11/17/2022 20:06 WG1961410 p-Isopropyltoluene 0.00547 J 0.00400 0.00784 1 11/17/2022 20:06 WG1961410 2-Butanone (MEK)U 0.0995 0.157 1 11/17/2022 20:06 WG1961410 Methylene Chloride U 0.0104 0.0392 1 11/17/2022 20:06 WG1961410 4-Methyl-2-pentanone (MIBK)U 0.00357 0.0392 1 11/17/2022 20:06 WG1961410 Methyl tert-butyl ether U 0.000549 0.00157 1 11/17/2022 20:06 WG1961410 Naphthalene U 0.00765 0.0196 1 11/17/2022 20:06 WG1961410 n-Propylbenzene U 0.00149 0.00784 1 11/17/2022 20:06 WG1961410 Styrene U 0.000359 0.0196 1 11/17/2022 20:06 WG1961410 1,1,1,2-Tetrachloroethane U 0.00149 0.00392 1 11/17/2022 20:06 WG1961410 1,1,2,2-Tetrachloroethane U 0.00109 0.00392 1 11/17/2022 20:06 WG1961410 1,1,2-Trichlorotrifluoroethane U 0.00118 0.00392 1 11/17/2022 20:06 WG1961410 Tetrachloroethene U 0.00140 0.00392 1 11/17/2022 20:06 WG1961410 Toluene 0.00215 J 0.00204 0.00784 1 11/17/2022 20:06 WG1961410 1,2,3-Trichlorobenzene U 0.0115 0.0196 1 11/17/2022 20:06 WG1961410 1,2,4-Trichlorobenzene U 0.00690 0.0196 1 11/17/2022 20:06 WG1961410 1,1,1-Trichloroethane U 0.00145 0.00392 1 11/17/2022 20:06 WG1961410 1,1,2-Trichloroethane U 0.000936 0.00392 1 11/17/2022 20:06 WG1961410 Trichloroethene U 0.000915 0.00157 1 11/17/2022 20:06 WG1961410 Trichlorofluoromethane U 0.00130 0.00392 1 11/17/2022 20:06 WG1961410 1,2,3-Trichloropropane U 0.00254 0.0196 1 11/17/2022 20:06 WG1961410 1,2,4-Trimethylbenzene U 0.00248 0.00784 1 11/17/2022 20:06 WG1961410 1,2,3-Trimethylbenzene U 0.00248 0.00784 1 11/17/2022 20:06 WG1961410 1,3,5-Trimethylbenzene U 0.00314 0.00784 1 11/17/2022 20:06 WG1961410 Vinyl chloride U 0.00182 0.00392 1 11/17/2022 20:06 WG1961410 Xylenes, Total U 0.00138 0.0102 1 11/17/2022 20:06 WG1961410 (S) Toluene-d8 114 75.0-131 11/17/2022 20:06 WG1961410 (S) 4-Bromofluorobenzene 104 67.0-138 11/17/2022 20:06 WG1961410 (S) 1,2-Dichloroethane-d4 78.8 70.0-130 11/17/2022 20:06 WG1961410 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.971 0.00683 0.0422 1 11/18/2022 23:24 WG1960983 Acenaphthylene 0.0445 0.00595 0.0422 1 11/18/2022 23:24 WG1960983 Anthracene 1.51 0.00752 0.0422 1 11/18/2022 23:24 WG1960983 Benzidine U C3 0.0794 2.12 1 11/18/2022 23:24 WG1960983 Benzo(a)anthracene 3.77 0.0372 0.212 5 11/22/2022 20:28 WG1960983 Benzo(b)fluoranthene 4.54 0.0394 0.212 5 11/22/2022 20:28 WG1960983 Benzo(k)fluoranthene 0.888 0.00751 0.0422 1 11/18/2022 23:24 WG1960983 Benzo(g,h,i)perylene 0.768 0.00772 0.0422 1 11/18/2022 23:24 WG1960983 Benzo(a)pyrene 3.31 0.0392 0.212 5 11/22/2022 20:28 WG1960983 Bis(2-chlorethoxy)methane U 0.0127 0.422 1 11/18/2022 23:24 WG1960983 Bis(2-chloroethyl)ether U 0.0139 0.422 1 11/18/2022 23:24 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0183 0.422 1 11/18/2022 23:24 WG1960983 4-Bromophenyl-phenylether U 0.0148 0.422 1 11/18/2022 23:24 WG1960983 2-Chloronaphthalene U 0.00742 0.0422 1 11/18/2022 23:24 WG1960983 4-Chlorophenyl-phenylether U 0.0147 0.422 1 11/18/2022 23:24 WG1960983 Chrysene 3.30 0.0420 0.212 5 11/22/2022 20:28 WG1960983 Dibenz(a,h)anthracene 0.238 0.0117 0.0422 1 11/18/2022 23:24 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 45 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 45 of 96 SAMPLE RESULTS - 13 L1557235 SS-7 Collected date/time: 11/10/22 15:45 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0125 0.422 1 11/18/2022 23:24 WG1960983 1,3-Dichlorobenzene U 0.0128 0.422 1 11/18/2022 23:24 WG1960983 1,4-Dichlorobenzene U 0.0126 0.422 1 11/18/2022 23:24 WG1960983 3,3-Dichlorobenzidine U 0.0156 0.422 1 11/18/2022 23:24 WG1960983 2,4-Dinitrotoluene U 0.0121 0.422 1 11/18/2022 23:24 WG1960983 2,6-Dinitrotoluene U 0.0138 0.422 1 11/18/2022 23:24 WG1960983 Fluoranthene 9.40 0.0382 0.212 5 11/22/2022 20:28 WG1960983 Fluorene 0.774 0.00687 0.0422 1 11/18/2022 23:24 WG1960983 Hexachlorobenzene U 0.0150 0.422 1 11/18/2022 23:24 WG1960983 Hexachloro-1,3-butadiene U 0.0142 0.422 1 11/18/2022 23:24 WG1960983 Hexachlorocyclopentadiene U 0.0222 0.422 1 11/18/2022 23:24 WG1960983 Hexachloroethane U 0.0166 0.422 1 11/18/2022 23:24 WG1960983 Indeno(1,2,3-cd)pyrene 1.01 0.0119 0.0422 1 11/18/2022 23:24 WG1960983 Isophorone U 0.0129 0.422 1 11/18/2022 23:24 WG1960983 Naphthalene 0.416 0.0106 0.0422 1 11/18/2022 23:24 WG1960983 Nitrobenzene U 0.0147 0.422 1 11/18/2022 23:24 WG1960983 n-Nitrosodimethylamine U 0.0626 0.422 1 11/18/2022 23:24 WG1960983 n-Nitrosodiphenylamine U 0.0320 0.422 1 11/18/2022 23:24 WG1960983 n-Nitrosodi-n-propylamine U 0.0141 0.422 1 11/18/2022 23:24 WG1960983 Phenanthrene 8.08 0.0420 0.212 5 11/22/2022 20:28 WG1960983 Benzylbutyl phthalate U 0.0132 0.422 1 11/18/2022 23:24 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0535 0.422 1 11/18/2022 23:24 WG1960983 Di-n-butyl phthalate U 0.0145 0.422 1 11/18/2022 23:24 WG1960983 Diethyl phthalate U 0.0139 0.422 1 11/18/2022 23:24 WG1960983 Dimethyl phthalate U 0.0895 0.422 1 11/18/2022 23:24 WG1960983 Di-n-octyl phthalate U 0.0285 0.422 1 11/18/2022 23:24 WG1960983 Pyrene 6.59 0.0411 0.212 5 11/22/2022 20:28 WG1960983 1,2,4-Trichlorobenzene U 0.0132 0.422 1 11/18/2022 23:24 WG1960983 4-Chloro-3-methylphenol U 0.0137 0.422 1 11/18/2022 23:24 WG1960983 2-Chlorophenol U 0.0139 0.422 1 11/18/2022 23:24 WG1960983 2,4-Dichlorophenol U 0.0123 0.422 1 11/18/2022 23:24 WG1960983 2,4-Dimethylphenol U 0.0110 0.422 1 11/18/2022 23:24 WG1960983 4,6-Dinitro-2-methylphenol U 0.0957 0.422 1 11/18/2022 23:24 WG1960983 2,4-Dinitrophenol U 0.0988 0.422 1 11/18/2022 23:24 WG1960983 2-Nitrophenol U 0.0151 0.422 1 11/18/2022 23:24 WG1960983 4-Nitrophenol U 0.0132 0.422 1 11/18/2022 23:24 WG1960983 Pentachlorophenol U 0.0114 0.422 1 11/18/2022 23:24 WG1960983 Phenol U 0.0170 0.422 1 11/18/2022 23:24 WG1960983 2,4,6-Trichlorophenol U 0.0136 0.422 1 11/18/2022 23:24 WG1960983 (S) 2-Fluorophenol 45.9 12.0-120 11/18/2022 23:24 WG1960983 (S) 2-Fluorophenol 57.6 12.0-120 11/22/2022 20:28 WG1960983 (S) Phenol-d5 43.2 10.0-120 11/18/2022 23:24 WG1960983 (S) Phenol-d5 51.8 10.0-120 11/22/2022 20:28 WG1960983 (S) Nitrobenzene-d5 40.5 10.0-122 11/18/2022 23:24 WG1960983 (S) Nitrobenzene-d5 47.1 10.0-122 11/22/2022 20:28 WG1960983 (S) 2-Fluorobiphenyl 40.2 15.0-120 11/18/2022 23:24 WG1960983 (S) 2-Fluorobiphenyl 56.5 15.0-120 11/22/2022 20:28 WG1960983 (S) 2,4,6-Tribromophenol 58.6 10.0-127 11/18/2022 23:24 WG1960983 (S) 2,4,6-Tribromophenol 64.4 10.0-127 11/22/2022 20:28 WG1960983 (S) p-Terphenyl-d14 48.3 10.0-120 11/18/2022 23:24 WG1960983 (S) p-Terphenyl-d14 65.3 10.0-120 11/22/2022 20:28 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 46 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 46 of 96 SAMPLE RESULTS - 14 L1557235 SS-7-A Collected date/time: 11/10/22 15:55 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 80.8 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0637 0.0223 0.0495 1 11/17/2022 14:37 WG1960561 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.30 0.124 1.24 5 11/29/2022 20:48 WG1961432 Barium 43.7 0.188 3.10 5 11/29/2022 20:48 WG1961432 Cadmium U 0.106 1.24 5 11/29/2022 20:48 WG1961432 Chromium 16.7 0.366 6.19 5 11/29/2022 20:48 WG1961432 Lead 12.0 0.123 2.48 5 11/29/2022 20:48 WG1961432 Selenium 0.773 J 0.223 3.10 5 11/29/2022 20:48 WG1961432 Silver U 0.107 0.619 5 11/29/2022 20:48 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0562 0.0770 1 11/18/2022 05:51 WG1961734 Acrylonitrile U J3 0.00556 0.0192 1 11/18/2022 05:51 WG1961734 Benzene U 0.000719 0.00154 1 11/18/2022 05:51 WG1961734 Bromobenzene U 0.00139 0.0192 1 11/18/2022 05:51 WG1961734 Bromodichloromethane U 0.00112 0.00385 1 11/18/2022 05:51 WG1961734 Bromoform U 0.00180 0.0385 1 11/18/2022 05:51 WG1961734 Bromomethane U 0.00303 0.0192 1 11/18/2022 05:51 WG1961734 n-Butylbenzene U 0.00808 0.0192 1 11/18/2022 05:51 WG1961734 sec-Butylbenzene U 0.00443 0.0192 1 11/18/2022 05:51 WG1961734 tert-Butylbenzene U 0.00300 0.00770 1 11/18/2022 05:51 WG1961734 Carbon tetrachloride U 0.00138 0.00770 1 11/18/2022 05:51 WG1961734 Chlorobenzene U 0.000323 0.00385 1 11/18/2022 05:51 WG1961734 Chlorodibromomethane U C3 0.000942 0.00385 1 11/18/2022 05:51 WG1961734 Chloroethane U 0.00262 0.00770 1 11/18/2022 05:51 WG1961734 Chloroform U 0.00159 0.00385 1 11/18/2022 05:51 WG1961734 Chloromethane U 0.00670 0.0192 1 11/18/2022 05:51 WG1961734 2-Chlorotoluene U 0.00133 0.00385 1 11/18/2022 05:51 WG1961734 4-Chlorotoluene U 0.000693 0.00770 1 11/18/2022 05:51 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00600 0.0385 1 11/18/2022 05:51 WG1961734 1,2-Dibromoethane U 0.000998 0.00385 1 11/18/2022 05:51 WG1961734 Dibromomethane U 0.00115 0.00770 1 11/18/2022 05:51 WG1961734 1,2-Dichlorobenzene U 0.000654 0.00770 1 11/18/2022 05:51 WG1961734 1,3-Dichlorobenzene U 0.000924 0.00770 1 11/18/2022 05:51 WG1961734 1,4-Dichlorobenzene U 0.00108 0.00770 1 11/18/2022 05:51 WG1961734 Dichlorodifluoromethane U 0.00248 0.00385 1 11/18/2022 05:51 WG1961734 1,1-Dichloroethane U 0.000756 0.00385 1 11/18/2022 05:51 WG1961734 1,2-Dichloroethane U 0.000999 0.00385 1 11/18/2022 05:51 WG1961734 1,1-Dichloroethene U 0.000933 0.00385 1 11/18/2022 05:51 WG1961734 cis-1,2-Dichloroethene U 0.00113 0.00385 1 11/18/2022 05:51 WG1961734 trans-1,2-Dichloroethene U 0.00160 0.00770 1 11/18/2022 05:51 WG1961734 1,2-Dichloropropane U 0.00219 0.00770 1 11/18/2022 05:51 WG1961734 1,1-Dichloropropene U 0.00125 0.00385 1 11/18/2022 05:51 WG1961734 1,3-Dichloropropane U 0.000771 0.00770 1 11/18/2022 05:51 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 47 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 47 of 96 SAMPLE RESULTS - 14 L1557235 SS-7-A Collected date/time: 11/10/22 15:55 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00117 0.00385 1 11/18/2022 05:51 WG1961734 trans-1,3-Dichloropropene U 0.00175 0.00770 1 11/18/2022 05:51 WG1961734 2,2-Dichloropropane U 0.00212 0.00385 1 11/18/2022 05:51 WG1961734 Di-isopropyl ether U 0.000631 0.00154 1 11/18/2022 05:51 WG1961734 Ethylbenzene U 0.00113 0.00385 1 11/18/2022 05:51 WG1961734 Hexachloro-1,3-butadiene U 0.00924 0.0385 1 11/18/2022 05:51 WG1961734 Isopropylbenzene U 0.000654 0.00385 1 11/18/2022 05:51 WG1961734 p-Isopropyltoluene U 0.00393 0.00770 1 11/18/2022 05:51 WG1961734 2-Butanone (MEK)U 0.0977 0.154 1 11/18/2022 05:51 WG1961734 Methylene Chloride U 0.0102 0.0385 1 11/18/2022 05:51 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00351 0.0385 1 11/18/2022 05:51 WG1961734 Methyl tert-butyl ether U 0.000539 0.00154 1 11/18/2022 05:51 WG1961734 Naphthalene U J3 0.00751 0.0192 1 11/18/2022 05:51 WG1961734 n-Propylbenzene U 0.00146 0.00770 1 11/18/2022 05:51 WG1961734 Styrene U 0.000353 0.0192 1 11/18/2022 05:51 WG1961734 1,1,1,2-Tetrachloroethane U 0.00146 0.00385 1 11/18/2022 05:51 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00107 0.00385 1 11/18/2022 05:51 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00116 0.00385 1 11/18/2022 05:51 WG1961734 Tetrachloroethene U 0.00138 0.00385 1 11/18/2022 05:51 WG1961734 Toluene U 0.00200 0.00770 1 11/18/2022 05:51 WG1961734 1,2,3-Trichlorobenzene U C4 0.0113 0.0192 1 11/18/2022 05:51 WG1961734 1,2,4-Trichlorobenzene U J3 0.00677 0.0192 1 11/18/2022 05:51 WG1961734 1,1,1-Trichloroethane U 0.00142 0.00385 1 11/18/2022 05:51 WG1961734 1,1,2-Trichloroethane U 0.000919 0.00385 1 11/18/2022 05:51 WG1961734 Trichloroethene U 0.000899 0.00154 1 11/18/2022 05:51 WG1961734 Trichlorofluoromethane U 0.00127 0.00385 1 11/18/2022 05:51 WG1961734 1,2,3-Trichloropropane U 0.00249 0.0192 1 11/18/2022 05:51 WG1961734 1,2,4-Trimethylbenzene U 0.00243 0.00770 1 11/18/2022 05:51 WG1961734 1,2,3-Trimethylbenzene U 0.00243 0.00770 1 11/18/2022 05:51 WG1961734 1,3,5-Trimethylbenzene U 0.00308 0.00770 1 11/18/2022 05:51 WG1961734 Vinyl chloride U 0.00179 0.00385 1 11/18/2022 05:51 WG1961734 Xylenes, Total U 0.00135 0.0100 1 11/18/2022 05:51 WG1961734 (S) Toluene-d8 101 75.0-131 11/18/2022 05:51 WG1961734 (S) 4-Bromofluorobenzene 98.6 67.0-138 11/18/2022 05:51 WG1961734 (S) 1,2-Dichloroethane-d4 99.7 70.0-130 11/18/2022 05:51 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00667 0.0412 1 11/18/2022 18:42 WG1960983 Acenaphthylene U 0.00581 0.0412 1 11/18/2022 18:42 WG1960983 Anthracene U 0.00734 0.0412 1 11/18/2022 18:42 WG1960983 Benzidine U C3 0.0775 2.07 1 11/18/2022 18:42 WG1960983 Benzo(a)anthracene U 0.00727 0.0412 1 11/18/2022 18:42 WG1960983 Benzo(b)fluoranthene U 0.00769 0.0412 1 11/18/2022 18:42 WG1960983 Benzo(k)fluoranthene U 0.00733 0.0412 1 11/18/2022 18:42 WG1960983 Benzo(g,h,i)perylene U 0.00754 0.0412 1 11/18/2022 18:42 WG1960983 Benzo(a)pyrene U 0.00766 0.0412 1 11/18/2022 18:42 WG1960983 Bis(2-chlorethoxy)methane U 0.0124 0.412 1 11/18/2022 18:42 WG1960983 Bis(2-chloroethyl)ether U 0.0136 0.412 1 11/18/2022 18:42 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0178 0.412 1 11/18/2022 18:42 WG1960983 4-Bromophenyl-phenylether U 0.0145 0.412 1 11/18/2022 18:42 WG1960983 2-Chloronaphthalene U 0.00724 0.0412 1 11/18/2022 18:42 WG1960983 4-Chlorophenyl-phenylether U 0.0144 0.412 1 11/18/2022 18:42 WG1960983 Chrysene U 0.00820 0.0412 1 11/18/2022 18:42 WG1960983 Dibenz(a,h)anthracene U 0.0114 0.0412 1 11/18/2022 18:42 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 48 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 48 of 96 SAMPLE RESULTS - 14 L1557235 SS-7-A Collected date/time: 11/10/22 15:55 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0122 0.412 1 11/18/2022 18:42 WG1960983 1,3-Dichlorobenzene U 0.0125 0.412 1 11/18/2022 18:42 WG1960983 1,4-Dichlorobenzene U 0.0123 0.412 1 11/18/2022 18:42 WG1960983 3,3-Dichlorobenzidine U 0.0152 0.412 1 11/18/2022 18:42 WG1960983 2,4-Dinitrotoluene U 0.0118 0.412 1 11/18/2022 18:42 WG1960983 2,6-Dinitrotoluene U 0.0135 0.412 1 11/18/2022 18:42 WG1960983 Fluoranthene U 0.00744 0.0412 1 11/18/2022 18:42 WG1960983 Fluorene U 0.00671 0.0412 1 11/18/2022 18:42 WG1960983 Hexachlorobenzene U 0.0146 0.412 1 11/18/2022 18:42 WG1960983 Hexachloro-1,3-butadiene U 0.0139 0.412 1 11/18/2022 18:42 WG1960983 Hexachlorocyclopentadiene U 0.0217 0.412 1 11/18/2022 18:42 WG1960983 Hexachloroethane U 0.0162 0.412 1 11/18/2022 18:42 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0117 0.0412 1 11/18/2022 18:42 WG1960983 Isophorone U 0.0126 0.412 1 11/18/2022 18:42 WG1960983 Naphthalene U 0.0104 0.0412 1 11/18/2022 18:42 WG1960983 Nitrobenzene U 0.0144 0.412 1 11/18/2022 18:42 WG1960983 n-Nitrosodimethylamine U 0.0612 0.412 1 11/18/2022 18:42 WG1960983 n-Nitrosodiphenylamine U 0.0312 0.412 1 11/18/2022 18:42 WG1960983 n-Nitrosodi-n-propylamine U 0.0137 0.412 1 11/18/2022 18:42 WG1960983 Phenanthrene U 0.00818 0.0412 1 11/18/2022 18:42 WG1960983 Benzylbutyl phthalate U 0.0129 0.412 1 11/18/2022 18:42 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0522 0.412 1 11/18/2022 18:42 WG1960983 Di-n-butyl phthalate U 0.0141 0.412 1 11/18/2022 18:42 WG1960983 Diethyl phthalate U 0.0136 0.412 1 11/18/2022 18:42 WG1960983 Dimethyl phthalate U 0.0874 0.412 1 11/18/2022 18:42 WG1960983 Di-n-octyl phthalate U 0.0279 0.412 1 11/18/2022 18:42 WG1960983 Pyrene U 0.00802 0.0412 1 11/18/2022 18:42 WG1960983 1,2,4-Trichlorobenzene U 0.0129 0.412 1 11/18/2022 18:42 WG1960983 4-Chloro-3-methylphenol U 0.0134 0.412 1 11/18/2022 18:42 WG1960983 2-Chlorophenol U 0.0136 0.412 1 11/18/2022 18:42 WG1960983 2,4-Dichlorophenol U 0.0120 0.412 1 11/18/2022 18:42 WG1960983 2,4-Dimethylphenol U 0.0108 0.412 1 11/18/2022 18:42 WG1960983 4,6-Dinitro-2-methylphenol U 0.0935 0.412 1 11/18/2022 18:42 WG1960983 2,4-Dinitrophenol U 0.0965 0.412 1 11/18/2022 18:42 WG1960983 2-Nitrophenol U 0.0147 0.412 1 11/18/2022 18:42 WG1960983 4-Nitrophenol U 0.0129 0.412 1 11/18/2022 18:42 WG1960983 Pentachlorophenol U 0.0111 0.412 1 11/18/2022 18:42 WG1960983 Phenol U 0.0166 0.412 1 11/18/2022 18:42 WG1960983 2,4,6-Trichlorophenol U 0.0132 0.412 1 11/18/2022 18:42 WG1960983 (S) 2-Fluorophenol 71.8 12.0-120 11/18/2022 18:42 WG1960983 (S) Phenol-d5 66.8 10.0-120 11/18/2022 18:42 WG1960983 (S) Nitrobenzene-d5 62.8 10.0-122 11/18/2022 18:42 WG1960983 (S) 2-Fluorobiphenyl 59.1 15.0-120 11/18/2022 18:42 WG1960983 (S) 2,4,6-Tribromophenol 74.8 10.0-127 11/18/2022 18:42 WG1960983 (S) p-Terphenyl-d14 70.4 10.0-120 11/18/2022 18:42 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 49 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 49 of 96 SAMPLE RESULTS - 15 L1557235 SS-8 Collected date/time: 11/10/22 14:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 72.4 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0564 0.0249 0.0552 1 11/17/2022 15:43 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 6.94 0.138 1.38 5 11/29/2022 20:52 WG1961432 Barium 22.1 0.210 3.45 5 11/29/2022 20:52 WG1961432 Cadmium U 0.118 1.38 5 11/29/2022 20:52 WG1961432 Chromium 12.4 0.409 6.91 5 11/29/2022 20:52 WG1961432 Lead 18.7 0.137 2.76 5 11/29/2022 20:52 WG1961432 Selenium 1.03 J 0.249 3.45 5 11/29/2022 20:52 WG1961432 Silver U 0.119 0.691 5 11/29/2022 20:52 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.123 C5 J3 J4 0.0753 0.103 1.22 11/18/2022 06:10 WG1961734 Acrylonitrile U J3 0.00745 0.0259 1.22 11/18/2022 06:10 WG1961734 Benzene U 0.000965 0.00207 1.22 11/18/2022 06:10 WG1961734 Bromobenzene U 0.00186 0.0259 1.22 11/18/2022 06:10 WG1961734 Bromodichloromethane U 0.00150 0.00516 1.22 11/18/2022 06:10 WG1961734 Bromoform U 0.00242 0.0516 1.22 11/18/2022 06:10 WG1961734 Bromomethane U 0.00406 0.0259 1.22 11/18/2022 06:10 WG1961734 n-Butylbenzene U 0.0108 0.0259 1.22 11/18/2022 06:10 WG1961734 sec-Butylbenzene U 0.00594 0.0259 1.22 11/18/2022 06:10 WG1961734 tert-Butylbenzene U 0.00403 0.0103 1.22 11/18/2022 06:10 WG1961734 Carbon tetrachloride U 0.00186 0.0103 1.22 11/18/2022 06:10 WG1961734 Chlorobenzene U 0.000433 0.00516 1.22 11/18/2022 06:10 WG1961734 Chlorodibromomethane U C3 0.00126 0.00516 1.22 11/18/2022 06:10 WG1961734 Chloroethane U 0.00350 0.0103 1.22 11/18/2022 06:10 WG1961734 Chloroform U 0.00213 0.00516 1.22 11/18/2022 06:10 WG1961734 Chloromethane U 0.00899 0.0259 1.22 11/18/2022 06:10 WG1961734 2-Chlorotoluene U 0.00179 0.00516 1.22 11/18/2022 06:10 WG1961734 4-Chlorotoluene U 0.000930 0.0103 1.22 11/18/2022 06:10 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00806 0.0516 1.22 11/18/2022 06:10 WG1961734 1,2-Dibromoethane U 0.00134 0.00516 1.22 11/18/2022 06:10 WG1961734 Dibromomethane U 0.00155 0.0103 1.22 11/18/2022 06:10 WG1961734 1,2-Dichlorobenzene U 0.000879 0.0103 1.22 11/18/2022 06:10 WG1961734 1,3-Dichlorobenzene U 0.00124 0.0103 1.22 11/18/2022 06:10 WG1961734 1,4-Dichlorobenzene U 0.00145 0.0103 1.22 11/18/2022 06:10 WG1961734 Dichlorodifluoromethane U 0.00332 0.00516 1.22 11/18/2022 06:10 WG1961734 1,1-Dichloroethane U 0.00101 0.00516 1.22 11/18/2022 06:10 WG1961734 1,2-Dichloroethane U 0.00134 0.00516 1.22 11/18/2022 06:10 WG1961734 1,1-Dichloroethene U 0.00125 0.00516 1.22 11/18/2022 06:10 WG1961734 cis-1,2-Dichloroethene U 0.00152 0.00516 1.22 11/18/2022 06:10 WG1961734 trans-1,2-Dichloroethene U 0.00215 0.0103 1.22 11/18/2022 06:10 WG1961734 1,2-Dichloropropane U 0.00293 0.0103 1.22 11/18/2022 06:10 WG1961734 1,1-Dichloropropene U 0.00167 0.00516 1.22 11/18/2022 06:10 WG1961734 1,3-Dichloropropane U 0.00103 0.0103 1.22 11/18/2022 06:10 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 50 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 50 of 96 SAMPLE RESULTS - 15 L1557235 SS-8 Collected date/time: 11/10/22 14:50 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00156 0.00516 1.22 11/18/2022 06:10 WG1961734 trans-1,3-Dichloropropene U 0.00235 0.0103 1.22 11/18/2022 06:10 WG1961734 2,2-Dichloropropane U 0.00284 0.00516 1.22 11/18/2022 06:10 WG1961734 Di-isopropyl ether U 0.000847 0.00207 1.22 11/18/2022 06:10 WG1961734 Ethylbenzene U 0.00152 0.00516 1.22 11/18/2022 06:10 WG1961734 Hexachloro-1,3-butadiene U 0.0124 0.0516 1.22 11/18/2022 06:10 WG1961734 Isopropylbenzene U 0.000879 0.00516 1.22 11/18/2022 06:10 WG1961734 p-Isopropyltoluene U 0.00527 0.0103 1.22 11/18/2022 06:10 WG1961734 2-Butanone (MEK)U 0.131 0.207 1.22 11/18/2022 06:10 WG1961734 Methylene Chloride U 0.0137 0.0516 1.22 11/18/2022 06:10 WG1961734 4-Methyl-2-pentanone (MIBK)0.00527 J 0.00471 0.0516 1.22 11/18/2022 06:10 WG1961734 Methyl tert-butyl ether U 0.000723 0.00207 1.22 11/18/2022 06:10 WG1961734 Naphthalene U J3 0.0101 0.0259 1.22 11/18/2022 06:10 WG1961734 n-Propylbenzene U 0.00196 0.0103 1.22 11/18/2022 06:10 WG1961734 Styrene U 0.000472 0.0259 1.22 11/18/2022 06:10 WG1961734 1,1,1,2-Tetrachloroethane U 0.00196 0.00516 1.22 11/18/2022 06:10 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00144 0.00516 1.22 11/18/2022 06:10 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00156 0.00516 1.22 11/18/2022 06:10 WG1961734 Tetrachloroethene U 0.00185 0.00516 1.22 11/18/2022 06:10 WG1961734 Toluene U 0.00269 0.0103 1.22 11/18/2022 06:10 WG1961734 1,2,3-Trichlorobenzene U C4 0.0151 0.0259 1.22 11/18/2022 06:10 WG1961734 1,2,4-Trichlorobenzene U J3 0.00909 0.0259 1.22 11/18/2022 06:10 WG1961734 1,1,1-Trichloroethane U 0.00191 0.00516 1.22 11/18/2022 06:10 WG1961734 1,1,2-Trichloroethane U 0.00123 0.00516 1.22 11/18/2022 06:10 WG1961734 Trichloroethene U 0.00121 0.00207 1.22 11/18/2022 06:10 WG1961734 Trichlorofluoromethane U 0.00171 0.00516 1.22 11/18/2022 06:10 WG1961734 1,2,3-Trichloropropane U 0.00335 0.0259 1.22 11/18/2022 06:10 WG1961734 1,2,4-Trimethylbenzene U 0.00327 0.0103 1.22 11/18/2022 06:10 WG1961734 1,2,3-Trimethylbenzene U 0.00327 0.0103 1.22 11/18/2022 06:10 WG1961734 1,3,5-Trimethylbenzene U 0.00413 0.0103 1.22 11/18/2022 06:10 WG1961734 Vinyl chloride U 0.00240 0.00516 1.22 11/18/2022 06:10 WG1961734 Xylenes, Total 0.00181 J 0.00181 0.0134 1.22 11/18/2022 06:10 WG1961734 (S) Toluene-d8 102 75.0-131 11/18/2022 06:10 WG1961734 (S) 4-Bromofluorobenzene 101 67.0-138 11/18/2022 06:10 WG1961734 (S) 1,2-Dichloroethane-d4 98.5 70.0-130 11/18/2022 06:10 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00744 0.0460 1 11/18/2022 20:43 WG1960983 Acenaphthylene U 0.00648 0.0460 1 11/18/2022 20:43 WG1960983 Anthracene U 0.00819 0.0460 1 11/18/2022 20:43 WG1960983 Benzidine U C3 0.0865 2.31 1 11/18/2022 20:43 WG1960983 Benzo(a)anthracene 0.00977 J 0.00811 0.0460 1 11/18/2022 20:43 WG1960983 Benzo(b)fluoranthene 0.0225 J 0.00858 0.0460 1 11/18/2022 20:43 WG1960983 Benzo(k)fluoranthene U 0.00818 0.0460 1 11/18/2022 20:43 WG1960983 Benzo(g,h,i)perylene 0.0111 J 0.00841 0.0460 1 11/18/2022 20:43 WG1960983 Benzo(a)pyrene 0.0138 J 0.00855 0.0460 1 11/18/2022 20:43 WG1960983 Bis(2-chlorethoxy)methane U 0.0138 0.460 1 11/18/2022 20:43 WG1960983 Bis(2-chloroethyl)ether U 0.0152 0.460 1 11/18/2022 20:43 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0199 0.460 1 11/18/2022 20:43 WG1960983 4-Bromophenyl-phenylether U 0.0162 0.460 1 11/18/2022 20:43 WG1960983 2-Chloronaphthalene U 0.00808 0.0460 1 11/18/2022 20:43 WG1960983 4-Chlorophenyl-phenylether U 0.0160 0.460 1 11/18/2022 20:43 WG1960983 Chrysene 0.0142 J 0.00914 0.0460 1 11/18/2022 20:43 WG1960983 Dibenz(a,h)anthracene U 0.0127 0.0460 1 11/18/2022 20:43 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 51 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 51 of 96 SAMPLE RESULTS - 15 L1557235 SS-8 Collected date/time: 11/10/22 14:50 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0136 0.460 1 11/18/2022 20:43 WG1960983 1,3-Dichlorobenzene U 0.0140 0.460 1 11/18/2022 20:43 WG1960983 1,4-Dichlorobenzene U 0.0137 0.460 1 11/18/2022 20:43 WG1960983 3,3-Dichlorobenzidine U 0.0170 0.460 1 11/18/2022 20:43 WG1960983 2,4-Dinitrotoluene U 0.0132 0.460 1 11/18/2022 20:43 WG1960983 2,6-Dinitrotoluene U 0.0151 0.460 1 11/18/2022 20:43 WG1960983 Fluoranthene 0.0246 J 0.00830 0.0460 1 11/18/2022 20:43 WG1960983 Fluorene U 0.00749 0.0460 1 11/18/2022 20:43 WG1960983 Hexachlorobenzene U 0.0163 0.460 1 11/18/2022 20:43 WG1960983 Hexachloro-1,3-butadiene U 0.0155 0.460 1 11/18/2022 20:43 WG1960983 Hexachlorocyclopentadiene U 0.0242 0.460 1 11/18/2022 20:43 WG1960983 Hexachloroethane U 0.0181 0.460 1 11/18/2022 20:43 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0130 0.0460 1 11/18/2022 20:43 WG1960983 Isophorone U 0.0141 0.460 1 11/18/2022 20:43 WG1960983 Naphthalene U 0.0115 0.0460 1 11/18/2022 20:43 WG1960983 Nitrobenzene U 0.0160 0.460 1 11/18/2022 20:43 WG1960983 n-Nitrosodimethylamine U 0.0682 0.460 1 11/18/2022 20:43 WG1960983 n-Nitrosodiphenylamine U 0.0348 0.460 1 11/18/2022 20:43 WG1960983 n-Nitrosodi-n-propylamine U 0.0153 0.460 1 11/18/2022 20:43 WG1960983 Phenanthrene 0.0101 J 0.00913 0.0460 1 11/18/2022 20:43 WG1960983 Benzylbutyl phthalate U 0.0144 0.460 1 11/18/2022 20:43 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0583 0.460 1 11/18/2022 20:43 WG1960983 Di-n-butyl phthalate U 0.0157 0.460 1 11/18/2022 20:43 WG1960983 Diethyl phthalate U 0.0152 0.460 1 11/18/2022 20:43 WG1960983 Dimethyl phthalate U 0.0975 0.460 1 11/18/2022 20:43 WG1960983 Di-n-octyl phthalate U 0.0311 0.460 1 11/18/2022 20:43 WG1960983 Pyrene 0.0227 J 0.00895 0.0460 1 11/18/2022 20:43 WG1960983 1,2,4-Trichlorobenzene U 0.0144 0.460 1 11/18/2022 20:43 WG1960983 4-Chloro-3-methylphenol U 0.0149 0.460 1 11/18/2022 20:43 WG1960983 2-Chlorophenol U 0.0152 0.460 1 11/18/2022 20:43 WG1960983 2,4-Dichlorophenol U 0.0134 0.460 1 11/18/2022 20:43 WG1960983 2,4-Dimethylphenol U 0.0120 0.460 1 11/18/2022 20:43 WG1960983 4,6-Dinitro-2-methylphenol U 0.104 0.460 1 11/18/2022 20:43 WG1960983 2,4-Dinitrophenol U 0.108 0.460 1 11/18/2022 20:43 WG1960983 2-Nitrophenol U 0.0164 0.460 1 11/18/2022 20:43 WG1960983 4-Nitrophenol U 0.0144 0.460 1 11/18/2022 20:43 WG1960983 Pentachlorophenol U 0.0124 0.460 1 11/18/2022 20:43 WG1960983 Phenol U 0.0185 0.460 1 11/18/2022 20:43 WG1960983 2,4,6-Trichlorophenol U 0.0148 0.460 1 11/18/2022 20:43 WG1960983 (S) 2-Fluorophenol 54.2 12.0-120 11/18/2022 20:43 WG1960983 (S) Phenol-d5 50.2 10.0-120 11/18/2022 20:43 WG1960983 (S) Nitrobenzene-d5 47.1 10.0-122 11/18/2022 20:43 WG1960983 (S) 2-Fluorobiphenyl 45.3 15.0-120 11/18/2022 20:43 WG1960983 (S) 2,4,6-Tribromophenol 63.1 10.0-127 11/18/2022 20:43 WG1960983 (S) p-Terphenyl-d14 52.0 10.0-120 11/18/2022 20:43 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 52 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 52 of 96 SAMPLE RESULTS - 16 L1557235 SS-8-A Collected date/time: 11/10/22 15:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 88.1 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0210 J 0.0204 0.0454 1 11/17/2022 15:45 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.38 0.114 1.14 5 11/29/2022 20:55 WG1961432 Barium 21.7 0.173 2.84 5 11/29/2022 20:55 WG1961432 Cadmium U 0.0971 1.14 5 11/29/2022 20:55 WG1961432 Chromium 8.56 0.336 5.68 5 11/29/2022 20:55 WG1961432 Lead 27.5 0.112 2.27 5 11/29/2022 20:55 WG1961432 Selenium 0.788 J 0.204 2.84 5 11/29/2022 20:55 WG1961432 Silver U 0.0982 0.568 5 11/29/2022 20:55 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0509 0.0698 1.11 11/18/2022 06:28 WG1961734 Acrylonitrile U J3 0.00504 0.0175 1.11 11/18/2022 06:28 WG1961734 Benzene U 0.000651 0.00140 1.11 11/18/2022 06:28 WG1961734 Bromobenzene U 0.00126 0.0175 1.11 11/18/2022 06:28 WG1961734 Bromodichloromethane U 0.00101 0.00350 1.11 11/18/2022 06:28 WG1961734 Bromoform U 0.00163 0.0350 1.11 11/18/2022 06:28 WG1961734 Bromomethane U 0.00275 0.0175 1.11 11/18/2022 06:28 WG1961734 n-Butylbenzene U 0.00733 0.0175 1.11 11/18/2022 06:28 WG1961734 sec-Butylbenzene U 0.00402 0.0175 1.11 11/18/2022 06:28 WG1961734 tert-Butylbenzene U 0.00272 0.00698 1.11 11/18/2022 06:28 WG1961734 Carbon tetrachloride U 0.00125 0.00698 1.11 11/18/2022 06:28 WG1961734 Chlorobenzene U 0.000293 0.00350 1.11 11/18/2022 06:28 WG1961734 Chlorodibromomethane U C3 0.000854 0.00350 1.11 11/18/2022 06:28 WG1961734 Chloroethane U 0.00238 0.00698 1.11 11/18/2022 06:28 WG1961734 Chloroform U 0.00143 0.00350 1.11 11/18/2022 06:28 WG1961734 Chloromethane U 0.00607 0.0175 1.11 11/18/2022 06:28 WG1961734 2-Chlorotoluene U 0.00121 0.00350 1.11 11/18/2022 06:28 WG1961734 4-Chlorotoluene U 0.000629 0.00698 1.11 11/18/2022 06:28 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00544 0.0350 1.11 11/18/2022 06:28 WG1961734 1,2-Dibromoethane U 0.000904 0.00350 1.11 11/18/2022 06:28 WG1961734 Dibromomethane U 0.00105 0.00698 1.11 11/18/2022 06:28 WG1961734 1,2-Dichlorobenzene U 0.000593 0.00698 1.11 11/18/2022 06:28 WG1961734 1,3-Dichlorobenzene U 0.000837 0.00698 1.11 11/18/2022 06:28 WG1961734 1,4-Dichlorobenzene U 0.000977 0.00698 1.11 11/18/2022 06:28 WG1961734 Dichlorodifluoromethane U 0.00225 0.00350 1.11 11/18/2022 06:28 WG1961734 1,1-Dichloroethane U 0.000685 0.00350 1.11 11/18/2022 06:28 WG1961734 1,2-Dichloroethane U 0.000905 0.00350 1.11 11/18/2022 06:28 WG1961734 1,1-Dichloroethene U 0.000846 0.00350 1.11 11/18/2022 06:28 WG1961734 cis-1,2-Dichloroethene U 0.00102 0.00350 1.11 11/18/2022 06:28 WG1961734 trans-1,2-Dichloroethene U 0.00145 0.00698 1.11 11/18/2022 06:28 WG1961734 1,2-Dichloropropane U 0.00199 0.00698 1.11 11/18/2022 06:28 WG1961734 1,1-Dichloropropene U 0.00113 0.00350 1.11 11/18/2022 06:28 WG1961734 1,3-Dichloropropane U 0.000699 0.00698 1.11 11/18/2022 06:28 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 53 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 53 of 96 SAMPLE RESULTS - 16 L1557235 SS-8-A Collected date/time: 11/10/22 15:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00106 0.00350 1.11 11/18/2022 06:28 WG1961734 trans-1,3-Dichloropropene U 0.00160 0.00698 1.11 11/18/2022 06:28 WG1961734 2,2-Dichloropropane U 0.00192 0.00350 1.11 11/18/2022 06:28 WG1961734 Di-isopropyl ether U 0.000572 0.00140 1.11 11/18/2022 06:28 WG1961734 Ethylbenzene U 0.00103 0.00350 1.11 11/18/2022 06:28 WG1961734 Hexachloro-1,3-butadiene U 0.00837 0.0350 1.11 11/18/2022 06:28 WG1961734 Isopropylbenzene U 0.000593 0.00350 1.11 11/18/2022 06:28 WG1961734 p-Isopropyltoluene U 0.00356 0.00698 1.11 11/18/2022 06:28 WG1961734 2-Butanone (MEK)U 0.0886 0.140 1.11 11/18/2022 06:28 WG1961734 Methylene Chloride U 0.00927 0.0350 1.11 11/18/2022 06:28 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00318 0.0350 1.11 11/18/2022 06:28 WG1961734 Methyl tert-butyl ether U 0.000489 0.00140 1.11 11/18/2022 06:28 WG1961734 Naphthalene U J3 0.00681 0.0175 1.11 11/18/2022 06:28 WG1961734 n-Propylbenzene U 0.00132 0.00698 1.11 11/18/2022 06:28 WG1961734 Styrene U 0.000319 0.0175 1.11 11/18/2022 06:28 WG1961734 1,1,1,2-Tetrachloroethane U 0.00132 0.00350 1.11 11/18/2022 06:28 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.000969 0.00350 1.11 11/18/2022 06:28 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00105 0.00350 1.11 11/18/2022 06:28 WG1961734 Tetrachloroethene U 0.00125 0.00350 1.11 11/18/2022 06:28 WG1961734 Toluene U 0.00181 0.00698 1.11 11/18/2022 06:28 WG1961734 1,2,3-Trichlorobenzene U C4 0.0102 0.0175 1.11 11/18/2022 06:28 WG1961734 1,2,4-Trichlorobenzene U J3 0.00614 0.0175 1.11 11/18/2022 06:28 WG1961734 1,1,1-Trichloroethane U 0.00128 0.00350 1.11 11/18/2022 06:28 WG1961734 1,1,2-Trichloroethane U 0.000834 0.00350 1.11 11/18/2022 06:28 WG1961734 Trichloroethene U 0.000815 0.00140 1.11 11/18/2022 06:28 WG1961734 Trichlorofluoromethane U 0.00115 0.00350 1.11 11/18/2022 06:28 WG1961734 1,2,3-Trichloropropane U 0.00226 0.0175 1.11 11/18/2022 06:28 WG1961734 1,2,4-Trimethylbenzene U 0.00220 0.00698 1.11 11/18/2022 06:28 WG1961734 1,2,3-Trimethylbenzene U 0.00220 0.00698 1.11 11/18/2022 06:28 WG1961734 1,3,5-Trimethylbenzene U 0.00279 0.00698 1.11 11/18/2022 06:28 WG1961734 Vinyl chloride U 0.00162 0.00350 1.11 11/18/2022 06:28 WG1961734 Xylenes, Total U 0.00123 0.00908 1.11 11/18/2022 06:28 WG1961734 (S) Toluene-d8 103 75.0-131 11/18/2022 06:28 WG1961734 (S) 4-Bromofluorobenzene 100 67.0-138 11/18/2022 06:28 WG1961734 (S) 1,2-Dichloroethane-d4 98.9 70.0-130 11/18/2022 06:28 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00612 0.0378 1 11/18/2022 18:01 WG1960983 Acenaphthylene U 0.00533 0.0378 1 11/18/2022 18:01 WG1960983 Anthracene U 0.00673 0.0378 1 11/18/2022 18:01 WG1960983 Benzidine U C3 0.0711 1.90 1 11/18/2022 18:01 WG1960983 Benzo(a)anthracene U 0.00667 0.0378 1 11/18/2022 18:01 WG1960983 Benzo(b)fluoranthene U 0.00705 0.0378 1 11/18/2022 18:01 WG1960983 Benzo(k)fluoranthene U 0.00672 0.0378 1 11/18/2022 18:01 WG1960983 Benzo(g,h,i)perylene U 0.00692 0.0378 1 11/18/2022 18:01 WG1960983 Benzo(a)pyrene U 0.00703 0.0378 1 11/18/2022 18:01 WG1960983 Bis(2-chlorethoxy)methane U 0.0114 0.378 1 11/18/2022 18:01 WG1960983 Bis(2-chloroethyl)ether U 0.0125 0.378 1 11/18/2022 18:01 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0164 0.378 1 11/18/2022 18:01 WG1960983 4-Bromophenyl-phenylether U 0.0133 0.378 1 11/18/2022 18:01 WG1960983 2-Chloronaphthalene U 0.00664 0.0378 1 11/18/2022 18:01 WG1960983 4-Chlorophenyl-phenylether U 0.0132 0.378 1 11/18/2022 18:01 WG1960983 Chrysene U 0.00752 0.0378 1 11/18/2022 18:01 WG1960983 Dibenz(a,h)anthracene U 0.0105 0.0378 1 11/18/2022 18:01 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 54 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 54 of 96 SAMPLE RESULTS - 16 L1557235 SS-8-A Collected date/time: 11/10/22 15:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0112 0.378 1 11/18/2022 18:01 WG1960983 1,3-Dichlorobenzene U 0.0115 0.378 1 11/18/2022 18:01 WG1960983 1,4-Dichlorobenzene U 0.0113 0.378 1 11/18/2022 18:01 WG1960983 3,3-Dichlorobenzidine U 0.0140 0.378 1 11/18/2022 18:01 WG1960983 2,4-Dinitrotoluene U 0.0108 0.378 1 11/18/2022 18:01 WG1960983 2,6-Dinitrotoluene U 0.0124 0.378 1 11/18/2022 18:01 WG1960983 Fluoranthene U 0.00682 0.0378 1 11/18/2022 18:01 WG1960983 Fluorene U 0.00615 0.0378 1 11/18/2022 18:01 WG1960983 Hexachlorobenzene U 0.0134 0.378 1 11/18/2022 18:01 WG1960983 Hexachloro-1,3-butadiene U 0.0127 0.378 1 11/18/2022 18:01 WG1960983 Hexachlorocyclopentadiene U 0.0199 0.378 1 11/18/2022 18:01 WG1960983 Hexachloroethane U 0.0149 0.378 1 11/18/2022 18:01 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0107 0.0378 1 11/18/2022 18:01 WG1960983 Isophorone U 0.0116 0.378 1 11/18/2022 18:01 WG1960983 Naphthalene U 0.00949 0.0378 1 11/18/2022 18:01 WG1960983 Nitrobenzene U 0.0132 0.378 1 11/18/2022 18:01 WG1960983 n-Nitrosodimethylamine U 0.0561 0.378 1 11/18/2022 18:01 WG1960983 n-Nitrosodiphenylamine U 0.0286 0.378 1 11/18/2022 18:01 WG1960983 n-Nitrosodi-n-propylamine U 0.0126 0.378 1 11/18/2022 18:01 WG1960983 Phenanthrene U 0.00751 0.0378 1 11/18/2022 18:01 WG1960983 Benzylbutyl phthalate U 0.0118 0.378 1 11/18/2022 18:01 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0479 0.378 1 11/18/2022 18:01 WG1960983 Di-n-butyl phthalate U 0.0129 0.378 1 11/18/2022 18:01 WG1960983 Diethyl phthalate U 0.0125 0.378 1 11/18/2022 18:01 WG1960983 Dimethyl phthalate U 0.0802 0.378 1 11/18/2022 18:01 WG1960983 Di-n-octyl phthalate U 0.0256 0.378 1 11/18/2022 18:01 WG1960983 Pyrene U 0.00736 0.0378 1 11/18/2022 18:01 WG1960983 1,2,4-Trichlorobenzene U 0.0118 0.378 1 11/18/2022 18:01 WG1960983 4-Chloro-3-methylphenol U 0.0123 0.378 1 11/18/2022 18:01 WG1960983 2-Chlorophenol U 0.0125 0.378 1 11/18/2022 18:01 WG1960983 2,4-Dichlorophenol U 0.0110 0.378 1 11/18/2022 18:01 WG1960983 2,4-Dimethylphenol U 0.00988 0.378 1 11/18/2022 18:01 WG1960983 4,6-Dinitro-2-methylphenol U 0.0857 0.378 1 11/18/2022 18:01 WG1960983 2,4-Dinitrophenol U 0.0885 0.378 1 11/18/2022 18:01 WG1960983 2-Nitrophenol U 0.0135 0.378 1 11/18/2022 18:01 WG1960983 4-Nitrophenol U 0.0118 0.378 1 11/18/2022 18:01 WG1960983 Pentachlorophenol U 0.0102 0.378 1 11/18/2022 18:01 WG1960983 Phenol U 0.0152 0.378 1 11/18/2022 18:01 WG1960983 2,4,6-Trichlorophenol U 0.0122 0.378 1 11/18/2022 18:01 WG1960983 (S) 2-Fluorophenol 60.2 12.0-120 11/18/2022 18:01 WG1960983 (S) Phenol-d5 54.6 10.0-120 11/18/2022 18:01 WG1960983 (S) Nitrobenzene-d5 51.5 10.0-122 11/18/2022 18:01 WG1960983 (S) 2-Fluorobiphenyl 49.1 15.0-120 11/18/2022 18:01 WG1960983 (S) 2,4,6-Tribromophenol 65.6 10.0-127 11/18/2022 18:01 WG1960983 (S) p-Terphenyl-d14 61.7 10.0-120 11/18/2022 18:01 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 55 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 55 of 96 SAMPLE RESULTS - 17 L1557235 SS-2 (DUP) Collected date/time: 11/10/22 11:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 75.7 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0582 0.0238 0.0528 1 11/17/2022 16:23 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.04 0.132 1.32 5 11/29/2022 20:58 WG1961432 Barium 27.3 0.201 3.30 5 11/29/2022 20:58 WG1961432 Cadmium U 0.113 1.32 5 11/29/2022 20:58 WG1961432 Chromium 11.5 0.391 6.60 5 11/29/2022 20:58 WG1961432 Lead 19.5 0.131 2.64 5 11/29/2022 20:58 WG1961432 Selenium 1.15 J 0.238 3.30 5 11/29/2022 20:58 WG1961432 Silver U 0.114 0.660 5 11/29/2022 20:58 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0607 0.0831 1 11/18/2022 06:47 WG1961734 Acrylonitrile U J3 0.00600 0.0208 1 11/18/2022 06:47 WG1961734 Benzene U 0.000776 0.00166 1 11/18/2022 06:47 WG1961734 Bromobenzene U 0.00150 0.0208 1 11/18/2022 06:47 WG1961734 Bromodichloromethane U 0.00120 0.00415 1 11/18/2022 06:47 WG1961734 Bromoform U 0.00194 0.0415 1 11/18/2022 06:47 WG1961734 Bromomethane U 0.00327 0.0208 1 11/18/2022 06:47 WG1961734 n-Butylbenzene U 0.00873 0.0208 1 11/18/2022 06:47 WG1961734 sec-Butylbenzene U 0.00479 0.0208 1 11/18/2022 06:47 WG1961734 tert-Butylbenzene U 0.00324 0.00831 1 11/18/2022 06:47 WG1961734 Carbon tetrachloride U 0.00149 0.00831 1 11/18/2022 06:47 WG1961734 Chlorobenzene U 0.000349 0.00415 1 11/18/2022 06:47 WG1961734 Chlorodibromomethane U C3 0.00102 0.00415 1 11/18/2022 06:47 WG1961734 Chloroethane U 0.00283 0.00831 1 11/18/2022 06:47 WG1961734 Chloroform U 0.00171 0.00415 1 11/18/2022 06:47 WG1961734 Chloromethane U 0.00723 0.0208 1 11/18/2022 06:47 WG1961734 2-Chlorotoluene U 0.00144 0.00415 1 11/18/2022 06:47 WG1961734 4-Chlorotoluene U 0.000748 0.00831 1 11/18/2022 06:47 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00648 0.0415 1 11/18/2022 06:47 WG1961734 1,2-Dibromoethane U 0.00108 0.00415 1 11/18/2022 06:47 WG1961734 Dibromomethane U 0.00125 0.00831 1 11/18/2022 06:47 WG1961734 1,2-Dichlorobenzene U 0.000706 0.00831 1 11/18/2022 06:47 WG1961734 1,3-Dichlorobenzene U 0.000997 0.00831 1 11/18/2022 06:47 WG1961734 1,4-Dichlorobenzene U 0.00116 0.00831 1 11/18/2022 06:47 WG1961734 Dichlorodifluoromethane U 0.00268 0.00415 1 11/18/2022 06:47 WG1961734 1,1-Dichloroethane U 0.000816 0.00415 1 11/18/2022 06:47 WG1961734 1,2-Dichloroethane U 0.00108 0.00415 1 11/18/2022 06:47 WG1961734 1,1-Dichloroethene U 0.00101 0.00415 1 11/18/2022 06:47 WG1961734 cis-1,2-Dichloroethene U 0.00122 0.00415 1 11/18/2022 06:47 WG1961734 trans-1,2-Dichloroethene U 0.00173 0.00831 1 11/18/2022 06:47 WG1961734 1,2-Dichloropropane U 0.00236 0.00831 1 11/18/2022 06:47 WG1961734 1,1-Dichloropropene U 0.00134 0.00415 1 11/18/2022 06:47 WG1961734 1,3-Dichloropropane U 0.000833 0.00831 1 11/18/2022 06:47 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 56 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 56 of 96 SAMPLE RESULTS - 17 L1557235 SS-2 (DUP) Collected date/time: 11/10/22 11:30 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00126 0.00415 1 11/18/2022 06:47 WG1961734 trans-1,3-Dichloropropene U 0.00189 0.00831 1 11/18/2022 06:47 WG1961734 2,2-Dichloropropane U 0.00229 0.00415 1 11/18/2022 06:47 WG1961734 Di-isopropyl ether U 0.000681 0.00166 1 11/18/2022 06:47 WG1961734 Ethylbenzene U 0.00122 0.00415 1 11/18/2022 06:47 WG1961734 Hexachloro-1,3-butadiene U 0.00997 0.0415 1 11/18/2022 06:47 WG1961734 Isopropylbenzene U 0.000706 0.00415 1 11/18/2022 06:47 WG1961734 p-Isopropyltoluene 0.00789 J 0.00424 0.00831 1 11/18/2022 06:47 WG1961734 2-Butanone (MEK)U 0.106 0.166 1 11/18/2022 06:47 WG1961734 Methylene Chloride U 0.0110 0.0415 1 11/18/2022 06:47 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00379 0.0415 1 11/18/2022 06:47 WG1961734 Methyl tert-butyl ether U 0.000582 0.00166 1 11/18/2022 06:47 WG1961734 Naphthalene U J3 0.00811 0.0208 1 11/18/2022 06:47 WG1961734 n-Propylbenzene U 0.00158 0.00831 1 11/18/2022 06:47 WG1961734 Styrene U 0.000381 0.0208 1 11/18/2022 06:47 WG1961734 1,1,1,2-Tetrachloroethane U 0.00158 0.00415 1 11/18/2022 06:47 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00116 0.00415 1 11/18/2022 06:47 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00125 0.00415 1 11/18/2022 06:47 WG1961734 Tetrachloroethene U 0.00149 0.00415 1 11/18/2022 06:47 WG1961734 Toluene U 0.00216 0.00831 1 11/18/2022 06:47 WG1961734 1,2,3-Trichlorobenzene U C4 0.0122 0.0208 1 11/18/2022 06:47 WG1961734 1,2,4-Trichlorobenzene U J3 0.00731 0.0208 1 11/18/2022 06:47 WG1961734 1,1,1-Trichloroethane U 0.00153 0.00415 1 11/18/2022 06:47 WG1961734 1,1,2-Trichloroethane U 0.000992 0.00415 1 11/18/2022 06:47 WG1961734 Trichloroethene U 0.000971 0.00166 1 11/18/2022 06:47 WG1961734 Trichlorofluoromethane U 0.00137 0.00415 1 11/18/2022 06:47 WG1961734 1,2,3-Trichloropropane U 0.00269 0.0208 1 11/18/2022 06:47 WG1961734 1,2,4-Trimethylbenzene U 0.00263 0.00831 1 11/18/2022 06:47 WG1961734 1,2,3-Trimethylbenzene U 0.00263 0.00831 1 11/18/2022 06:47 WG1961734 1,3,5-Trimethylbenzene U 0.00332 0.00831 1 11/18/2022 06:47 WG1961734 Vinyl chloride U 0.00193 0.00415 1 11/18/2022 06:47 WG1961734 Xylenes, Total U 0.00146 0.0108 1 11/18/2022 06:47 WG1961734 (S) Toluene-d8 106 75.0-131 11/18/2022 06:47 WG1961734 (S) 4-Bromofluorobenzene 98.3 67.0-138 11/18/2022 06:47 WG1961734 (S) 1,2-Dichloroethane-d4 93.3 70.0-130 11/18/2022 06:47 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00712 0.0440 1 11/18/2022 23:04 WG1960983 Acenaphthylene U 0.00619 0.0440 1 11/18/2022 23:04 WG1960983 Anthracene U 0.00783 0.0440 1 11/18/2022 23:04 WG1960983 Benzidine U C3 0.0827 2.21 1 11/18/2022 23:04 WG1960983 Benzo(a)anthracene 0.00791 J 0.00775 0.0440 1 11/18/2022 23:04 WG1960983 Benzo(b)fluoranthene 0.0161 J 0.00820 0.0440 1 11/18/2022 23:04 WG1960983 Benzo(k)fluoranthene U 0.00782 0.0440 1 11/18/2022 23:04 WG1960983 Benzo(g,h,i)perylene U 0.00804 0.0440 1 11/18/2022 23:04 WG1960983 Benzo(a)pyrene 0.0111 J 0.00818 0.0440 1 11/18/2022 23:04 WG1960983 Bis(2-chlorethoxy)methane U 0.0132 0.440 1 11/18/2022 23:04 WG1960983 Bis(2-chloroethyl)ether U 0.0145 0.440 1 11/18/2022 23:04 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0190 0.440 1 11/18/2022 23:04 WG1960983 4-Bromophenyl-phenylether U 0.0155 0.440 1 11/18/2022 23:04 WG1960983 2-Chloronaphthalene U 0.00773 0.0440 1 11/18/2022 23:04 WG1960983 4-Chlorophenyl-phenylether U 0.0153 0.440 1 11/18/2022 23:04 WG1960983 Chrysene 0.0112 J 0.00874 0.0440 1 11/18/2022 23:04 WG1960983 Dibenz(a,h)anthracene U 0.0122 0.0440 1 11/18/2022 23:04 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 57 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 57 of 96 SAMPLE RESULTS - 17 L1557235 SS-2 (DUP) Collected date/time: 11/10/22 11:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0130 0.440 1 11/18/2022 23:04 WG1960983 1,3-Dichlorobenzene U 0.0133 0.440 1 11/18/2022 23:04 WG1960983 1,4-Dichlorobenzene U 0.0131 0.440 1 11/18/2022 23:04 WG1960983 3,3-Dichlorobenzidine U 0.0162 0.440 1 11/18/2022 23:04 WG1960983 2,4-Dinitrotoluene U 0.0126 0.440 1 11/18/2022 23:04 WG1960983 2,6-Dinitrotoluene U 0.0144 0.440 1 11/18/2022 23:04 WG1960983 Fluoranthene 0.0178 J 0.00794 0.0440 1 11/18/2022 23:04 WG1960983 Fluorene U 0.00716 0.0440 1 11/18/2022 23:04 WG1960983 Hexachlorobenzene U 0.0156 0.440 1 11/18/2022 23:04 WG1960983 Hexachloro-1,3-butadiene U 0.0148 0.440 1 11/18/2022 23:04 WG1960983 Hexachlorocyclopentadiene U 0.0231 0.440 1 11/18/2022 23:04 WG1960983 Hexachloroethane U 0.0173 0.440 1 11/18/2022 23:04 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0124 0.0440 1 11/18/2022 23:04 WG1960983 Isophorone U 0.0135 0.440 1 11/18/2022 23:04 WG1960983 Naphthalene U 0.0110 0.0440 1 11/18/2022 23:04 WG1960983 Nitrobenzene U 0.0153 0.440 1 11/18/2022 23:04 WG1960983 n-Nitrosodimethylamine U 0.0653 0.440 1 11/18/2022 23:04 WG1960983 n-Nitrosodiphenylamine U 0.0333 0.440 1 11/18/2022 23:04 WG1960983 n-Nitrosodi-n-propylamine U 0.0147 0.440 1 11/18/2022 23:04 WG1960983 Phenanthrene 0.00910 J 0.00873 0.0440 1 11/18/2022 23:04 WG1960983 Benzylbutyl phthalate U 0.0137 0.440 1 11/18/2022 23:04 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0557 0.440 1 11/18/2022 23:04 WG1960983 Di-n-butyl phthalate U 0.0151 0.440 1 11/18/2022 23:04 WG1960983 Diethyl phthalate U 0.0145 0.440 1 11/18/2022 23:04 WG1960983 Dimethyl phthalate U 0.0933 0.440 1 11/18/2022 23:04 WG1960983 Di-n-octyl phthalate U 0.0297 0.440 1 11/18/2022 23:04 WG1960983 Pyrene 0.0162 J 0.00856 0.0440 1 11/18/2022 23:04 WG1960983 1,2,4-Trichlorobenzene U 0.0137 0.440 1 11/18/2022 23:04 WG1960983 4-Chloro-3-methylphenol U 0.0143 0.440 1 11/18/2022 23:04 WG1960983 2-Chlorophenol U 0.0145 0.440 1 11/18/2022 23:04 WG1960983 2,4-Dichlorophenol U 0.0128 0.440 1 11/18/2022 23:04 WG1960983 2,4-Dimethylphenol U 0.0115 0.440 1 11/18/2022 23:04 WG1960983 4,6-Dinitro-2-methylphenol U 0.0997 0.440 1 11/18/2022 23:04 WG1960983 2,4-Dinitrophenol U 0.103 0.440 1 11/18/2022 23:04 WG1960983 2-Nitrophenol U 0.0157 0.440 1 11/18/2022 23:04 WG1960983 4-Nitrophenol U 0.0137 0.440 1 11/18/2022 23:04 WG1960983 Pentachlorophenol U 0.0118 0.440 1 11/18/2022 23:04 WG1960983 Phenol U 0.0177 0.440 1 11/18/2022 23:04 WG1960983 2,4,6-Trichlorophenol U 0.0141 0.440 1 11/18/2022 23:04 WG1960983 (S) 2-Fluorophenol 61.7 12.0-120 11/18/2022 23:04 WG1960983 (S) Phenol-d5 57.8 10.0-120 11/18/2022 23:04 WG1960983 (S) Nitrobenzene-d5 54.2 10.0-122 11/18/2022 23:04 WG1960983 (S) 2-Fluorobiphenyl 50.8 15.0-120 11/18/2022 23:04 WG1960983 (S) 2,4,6-Tribromophenol 76.2 10.0-127 11/18/2022 23:04 WG1960983 (S) p-Terphenyl-d14 60.3 10.0-120 11/18/2022 23:04 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 58 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 58 of 96 SAMPLE RESULTS - 18 L1557235 SS-2-A (DUP) Collected date/time: 11/10/22 11:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 76.7 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.180 0.0235 0.0521 1 11/17/2022 16:26 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 6.88 0.130 1.30 5 11/29/2022 21:02 WG1961432 Barium 36.7 0.198 3.26 5 11/29/2022 21:02 WG1961432 Cadmium U 0.111 1.30 5 11/29/2022 21:02 WG1961432 Chromium 23.2 0.386 6.52 5 11/29/2022 21:02 WG1961432 Lead 11.6 0.129 2.61 5 11/29/2022 21:02 WG1961432 Selenium 1.11 J 0.235 3.26 5 11/29/2022 21:02 WG1961432 Silver U 0.113 0.652 5 11/29/2022 21:02 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0606 0.0829 1.04 11/18/2022 07:06 WG1961734 Acrylonitrile U J3 0.00598 0.0207 1.04 11/18/2022 07:06 WG1961734 Benzene U 0.000775 0.00166 1.04 11/18/2022 07:06 WG1961734 Bromobenzene U 0.00149 0.0207 1.04 11/18/2022 07:06 WG1961734 Bromodichloromethane U 0.00120 0.00414 1.04 11/18/2022 07:06 WG1961734 Bromoform U 0.00194 0.0414 1.04 11/18/2022 07:06 WG1961734 Bromomethane U 0.00327 0.0207 1.04 11/18/2022 07:06 WG1961734 n-Butylbenzene U 0.00870 0.0207 1.04 11/18/2022 07:06 WG1961734 sec-Butylbenzene U 0.00478 0.0207 1.04 11/18/2022 07:06 WG1961734 tert-Butylbenzene U 0.00324 0.00829 1.04 11/18/2022 07:06 WG1961734 Carbon tetrachloride U 0.00149 0.00829 1.04 11/18/2022 07:06 WG1961734 Chlorobenzene U 0.000348 0.00414 1.04 11/18/2022 07:06 WG1961734 Chlorodibromomethane U C3 0.00101 0.00414 1.04 11/18/2022 07:06 WG1961734 Chloroethane U 0.00282 0.00829 1.04 11/18/2022 07:06 WG1961734 Chloroform U 0.00171 0.00414 1.04 11/18/2022 07:06 WG1961734 Chloromethane U 0.00721 0.0207 1.04 11/18/2022 07:06 WG1961734 2-Chlorotoluene U 0.00143 0.00414 1.04 11/18/2022 07:06 WG1961734 4-Chlorotoluene U 0.000746 0.00829 1.04 11/18/2022 07:06 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00647 0.0414 1.04 11/18/2022 07:06 WG1961734 1,2-Dibromoethane U 0.00107 0.00414 1.04 11/18/2022 07:06 WG1961734 Dibromomethane U 0.00124 0.00829 1.04 11/18/2022 07:06 WG1961734 1,2-Dichlorobenzene U 0.000705 0.00829 1.04 11/18/2022 07:06 WG1961734 1,3-Dichlorobenzene U 0.000995 0.00829 1.04 11/18/2022 07:06 WG1961734 1,4-Dichlorobenzene U 0.00116 0.00829 1.04 11/18/2022 07:06 WG1961734 Dichlorodifluoromethane U 0.00266 0.00414 1.04 11/18/2022 07:06 WG1961734 1,1-Dichloroethane U 0.000815 0.00414 1.04 11/18/2022 07:06 WG1961734 1,2-Dichloroethane U 0.00108 0.00414 1.04 11/18/2022 07:06 WG1961734 1,1-Dichloroethene U 0.00100 0.00414 1.04 11/18/2022 07:06 WG1961734 cis-1,2-Dichloroethene U 0.00122 0.00414 1.04 11/18/2022 07:06 WG1961734 trans-1,2-Dichloroethene U 0.00172 0.00829 1.04 11/18/2022 07:06 WG1961734 1,2-Dichloropropane U 0.00236 0.00829 1.04 11/18/2022 07:06 WG1961734 1,1-Dichloropropene U 0.00134 0.00414 1.04 11/18/2022 07:06 WG1961734 1,3-Dichloropropane U 0.000831 0.00829 1.04 11/18/2022 07:06 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 59 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 59 of 96 SAMPLE RESULTS - 18 L1557235 SS-2-A (DUP) Collected date/time: 11/10/22 11:40 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00125 0.00414 1.04 11/18/2022 07:06 WG1961734 trans-1,3-Dichloropropene U 0.00190 0.00829 1.04 11/18/2022 07:06 WG1961734 2,2-Dichloropropane U 0.00230 0.00414 1.04 11/18/2022 07:06 WG1961734 Di-isopropyl ether U 0.000679 0.00166 1.04 11/18/2022 07:06 WG1961734 Ethylbenzene U 0.00122 0.00414 1.04 11/18/2022 07:06 WG1961734 Hexachloro-1,3-butadiene U 0.00995 0.0414 1.04 11/18/2022 07:06 WG1961734 Isopropylbenzene U 0.000705 0.00414 1.04 11/18/2022 07:06 WG1961734 p-Isopropyltoluene U 0.00422 0.00829 1.04 11/18/2022 07:06 WG1961734 2-Butanone (MEK)U 0.105 0.166 1.04 11/18/2022 07:06 WG1961734 Methylene Chloride U 0.0110 0.0414 1.04 11/18/2022 07:06 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00378 0.0414 1.04 11/18/2022 07:06 WG1961734 Methyl tert-butyl ether U 0.000580 0.00166 1.04 11/18/2022 07:06 WG1961734 Naphthalene U J3 0.00810 0.0207 1.04 11/18/2022 07:06 WG1961734 n-Propylbenzene U 0.00157 0.00829 1.04 11/18/2022 07:06 WG1961734 Styrene U 0.000379 0.0207 1.04 11/18/2022 07:06 WG1961734 1,1,1,2-Tetrachloroethane U 0.00157 0.00414 1.04 11/18/2022 07:06 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00115 0.00414 1.04 11/18/2022 07:06 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00125 0.00414 1.04 11/18/2022 07:06 WG1961734 Tetrachloroethene U 0.00149 0.00414 1.04 11/18/2022 07:06 WG1961734 Toluene U 0.00215 0.00829 1.04 11/18/2022 07:06 WG1961734 1,2,3-Trichlorobenzene U C4 0.0121 0.0207 1.04 11/18/2022 07:06 WG1961734 1,2,4-Trichlorobenzene U J3 0.00730 0.0207 1.04 11/18/2022 07:06 WG1961734 1,1,1-Trichloroethane U 0.00153 0.00414 1.04 11/18/2022 07:06 WG1961734 1,1,2-Trichloroethane U 0.000990 0.00414 1.04 11/18/2022 07:06 WG1961734 Trichloroethene U 0.000968 0.00166 1.04 11/18/2022 07:06 WG1961734 Trichlorofluoromethane U 0.00137 0.00414 1.04 11/18/2022 07:06 WG1961734 1,2,3-Trichloropropane U 0.00268 0.0207 1.04 11/18/2022 07:06 WG1961734 1,2,4-Trimethylbenzene U 0.00261 0.00829 1.04 11/18/2022 07:06 WG1961734 1,2,3-Trimethylbenzene U 0.00261 0.00829 1.04 11/18/2022 07:06 WG1961734 1,3,5-Trimethylbenzene U 0.00332 0.00829 1.04 11/18/2022 07:06 WG1961734 Vinyl chloride U 0.00193 0.00414 1.04 11/18/2022 07:06 WG1961734 Xylenes, Total U 0.00146 0.0108 1.04 11/18/2022 07:06 WG1961734 (S) Toluene-d8 105 75.0-131 11/18/2022 07:06 WG1961734 (S) 4-Bromofluorobenzene 99.1 67.0-138 11/18/2022 07:06 WG1961734 (S) 1,2-Dichloroethane-d4 96.9 70.0-130 11/18/2022 07:06 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00702 0.0434 1 11/18/2022 17:00 WG1960983 Acenaphthylene U 0.00611 0.0434 1 11/18/2022 17:00 WG1960983 Anthracene U 0.00773 0.0434 1 11/18/2022 17:00 WG1960983 Benzidine U C3 J6 0.0816 2.18 1 11/18/2022 17:00 WG1960983 Benzo(a)anthracene U 0.00765 0.0434 1 11/18/2022 17:00 WG1960983 Benzo(b)fluoranthene U 0.00809 0.0434 1 11/18/2022 17:00 WG1960983 Benzo(k)fluoranthene U 0.00771 0.0434 1 11/18/2022 17:00 WG1960983 Benzo(g,h,i)perylene U 0.00794 0.0434 1 11/18/2022 17:00 WG1960983 Benzo(a)pyrene U 0.00807 0.0434 1 11/18/2022 17:00 WG1960983 Bis(2-chlorethoxy)methane U 0.0130 0.434 1 11/18/2022 17:00 WG1960983 Bis(2-chloroethyl)ether U 0.0143 0.434 1 11/18/2022 17:00 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0188 0.434 1 11/18/2022 17:00 WG1960983 4-Bromophenyl-phenylether U 0.0152 0.434 1 11/18/2022 17:00 WG1960983 2-Chloronaphthalene U 0.00762 0.0434 1 11/18/2022 17:00 WG1960983 4-Chlorophenyl-phenylether U 0.0151 0.434 1 11/18/2022 17:00 WG1960983 Chrysene U 0.00863 0.0434 1 11/18/2022 17:00 WG1960983 Dibenz(a,h)anthracene U 0.0120 0.0434 1 11/18/2022 17:00 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 60 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 60 of 96 SAMPLE RESULTS - 18 L1557235 SS-2-A (DUP) Collected date/time: 11/10/22 11:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0129 0.434 1 11/18/2022 17:00 WG1960983 1,3-Dichlorobenzene U 0.0132 0.434 1 11/18/2022 17:00 WG1960983 1,4-Dichlorobenzene U 0.0129 0.434 1 11/18/2022 17:00 WG1960983 3,3-Dichlorobenzidine U 0.0160 0.434 1 11/18/2022 17:00 WG1960983 2,4-Dinitrotoluene U 0.0124 0.434 1 11/18/2022 17:00 WG1960983 2,6-Dinitrotoluene U 0.0142 0.434 1 11/18/2022 17:00 WG1960983 Fluoranthene U 0.00783 0.0434 1 11/18/2022 17:00 WG1960983 Fluorene U 0.00706 0.0434 1 11/18/2022 17:00 WG1960983 Hexachlorobenzene U 0.0154 0.434 1 11/18/2022 17:00 WG1960983 Hexachloro-1,3-butadiene U 0.0146 0.434 1 11/18/2022 17:00 WG1960983 Hexachlorocyclopentadiene U 0.0228 0.434 1 11/18/2022 17:00 WG1960983 Hexachloroethane U 0.0171 0.434 1 11/18/2022 17:00 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0123 0.0434 1 11/18/2022 17:00 WG1960983 Isophorone U 0.0133 0.434 1 11/18/2022 17:00 WG1960983 Naphthalene U 0.0109 0.0434 1 11/18/2022 17:00 WG1960983 Nitrobenzene U 0.0151 0.434 1 11/18/2022 17:00 WG1960983 n-Nitrosodimethylamine U 0.0644 0.434 1 11/18/2022 17:00 WG1960983 n-Nitrosodiphenylamine U 0.0328 0.434 1 11/18/2022 17:00 WG1960983 n-Nitrosodi-n-propylamine U 0.0145 0.434 1 11/18/2022 17:00 WG1960983 Phenanthrene U 0.00861 0.0434 1 11/18/2022 17:00 WG1960983 Benzylbutyl phthalate U 0.0136 0.434 1 11/18/2022 17:00 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0550 0.434 1 11/18/2022 17:00 WG1960983 Di-n-butyl phthalate U 0.0149 0.434 1 11/18/2022 17:00 WG1960983 Diethyl phthalate U 0.0143 0.434 1 11/18/2022 17:00 WG1960983 Dimethyl phthalate U 0.0920 0.434 1 11/18/2022 17:00 WG1960983 Di-n-octyl phthalate U 0.0293 0.434 1 11/18/2022 17:00 WG1960983 Pyrene U 0.00844 0.0434 1 11/18/2022 17:00 WG1960983 1,2,4-Trichlorobenzene U 0.0136 0.434 1 11/18/2022 17:00 WG1960983 4-Chloro-3-methylphenol U 0.0141 0.434 1 11/18/2022 17:00 WG1960983 2-Chlorophenol U 0.0143 0.434 1 11/18/2022 17:00 WG1960983 2,4-Dichlorophenol U 0.0126 0.434 1 11/18/2022 17:00 WG1960983 2,4-Dimethylphenol U 0.0113 0.434 1 11/18/2022 17:00 WG1960983 4,6-Dinitro-2-methylphenol U 0.0984 0.434 1 11/18/2022 17:00 WG1960983 2,4-Dinitrophenol U 0.102 0.434 1 11/18/2022 17:00 WG1960983 2-Nitrophenol U 0.0155 0.434 1 11/18/2022 17:00 WG1960983 4-Nitrophenol U 0.0136 0.434 1 11/18/2022 17:00 WG1960983 Pentachlorophenol U 0.0117 0.434 1 11/18/2022 17:00 WG1960983 Phenol U 0.0175 0.434 1 11/18/2022 17:00 WG1960983 2,4,6-Trichlorophenol U 0.0139 0.434 1 11/18/2022 17:00 WG1960983 (S) 2-Fluorophenol 68.3 12.0-120 11/18/2022 17:00 WG1960983 (S) Phenol-d5 62.4 10.0-120 11/18/2022 17:00 WG1960983 (S) Nitrobenzene-d5 60.6 10.0-122 11/18/2022 17:00 WG1960983 (S) 2-Fluorobiphenyl 57.3 15.0-120 11/18/2022 17:00 WG1960983 (S) 2,4,6-Tribromophenol 69.8 10.0-127 11/18/2022 17:00 WG1960983 (S) p-Terphenyl-d14 64.5 10.0-120 11/18/2022 17:00 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 61 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 61 of 96 SAMPLE RESULTS - 19 L1557235 SS-3 (DUP) Collected date/time: 11/10/22 15:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 66.1 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0310 J 0.0272 0.0605 1 11/17/2022 16:28 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.02 0.151 1.51 5 11/29/2022 21:05 WG1961432 Barium 22.5 0.230 3.78 5 11/29/2022 21:05 WG1961432 Cadmium U 0.129 1.51 5 11/29/2022 21:05 WG1961432 Chromium 19.8 0.448 7.56 5 11/29/2022 21:05 WG1961432 Lead 8.12 0.150 3.03 5 11/29/2022 21:05 WG1961432 Selenium 0.801 J 0.272 3.78 5 11/29/2022 21:05 WG1961432 Silver U 0.131 0.756 5 11/29/2022 21:05 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0745 0.102 1.01 11/18/2022 07:25 WG1961734 Acrylonitrile U J3 0.00737 0.0254 1.01 11/18/2022 07:25 WG1961734 Benzene U 0.000953 0.00204 1.01 11/18/2022 07:25 WG1961734 Bromobenzene U 0.00183 0.0254 1.01 11/18/2022 07:25 WG1961734 Bromodichloromethane U 0.00148 0.00511 1.01 11/18/2022 07:25 WG1961734 Bromoform U 0.00238 0.0511 1.01 11/18/2022 07:25 WG1961734 Bromomethane U 0.00402 0.0254 1.01 11/18/2022 07:25 WG1961734 n-Butylbenzene U 0.0107 0.0254 1.01 11/18/2022 07:25 WG1961734 sec-Butylbenzene U 0.00587 0.0254 1.01 11/18/2022 07:25 WG1961734 tert-Butylbenzene U 0.00398 0.0102 1.01 11/18/2022 07:25 WG1961734 Carbon tetrachloride U 0.00183 0.0102 1.01 11/18/2022 07:25 WG1961734 Chlorobenzene U 0.000428 0.00511 1.01 11/18/2022 07:25 WG1961734 Chlorodibromomethane U C3 0.00125 0.00511 1.01 11/18/2022 07:25 WG1961734 Chloroethane U 0.00347 0.0102 1.01 11/18/2022 07:25 WG1961734 Chloroform U 0.00210 0.00511 1.01 11/18/2022 07:25 WG1961734 Chloromethane U 0.00886 0.0254 1.01 11/18/2022 07:25 WG1961734 2-Chlorotoluene U 0.00176 0.00511 1.01 11/18/2022 07:25 WG1961734 4-Chlorotoluene U 0.000918 0.0102 1.01 11/18/2022 07:25 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00795 0.0511 1.01 11/18/2022 07:25 WG1961734 1,2-Dibromoethane U 0.00132 0.00511 1.01 11/18/2022 07:25 WG1961734 Dibromomethane U 0.00153 0.0102 1.01 11/18/2022 07:25 WG1961734 1,2-Dichlorobenzene U 0.000866 0.0102 1.01 11/18/2022 07:25 WG1961734 1,3-Dichlorobenzene U 0.00122 0.0102 1.01 11/18/2022 07:25 WG1961734 1,4-Dichlorobenzene U 0.00143 0.0102 1.01 11/18/2022 07:25 WG1961734 Dichlorodifluoromethane U 0.00329 0.00511 1.01 11/18/2022 07:25 WG1961734 1,1-Dichloroethane U 0.00100 0.00511 1.01 11/18/2022 07:25 WG1961734 1,2-Dichloroethane U 0.00132 0.00511 1.01 11/18/2022 07:25 WG1961734 1,1-Dichloroethene U 0.00124 0.00511 1.01 11/18/2022 07:25 WG1961734 cis-1,2-Dichloroethene U 0.00150 0.00511 1.01 11/18/2022 07:25 WG1961734 trans-1,2-Dichloroethene U 0.00212 0.0102 1.01 11/18/2022 07:25 WG1961734 1,2-Dichloropropane U 0.00289 0.0102 1.01 11/18/2022 07:25 WG1961734 1,1-Dichloropropene U 0.00165 0.00511 1.01 11/18/2022 07:25 WG1961734 1,3-Dichloropropane U 0.00102 0.0102 1.01 11/18/2022 07:25 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 62 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 62 of 96 SAMPLE RESULTS - 19 L1557235 SS-3 (DUP) Collected date/time: 11/10/22 15:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00154 0.00511 1.01 11/18/2022 07:25 WG1961734 trans-1,3-Dichloropropene U 0.00232 0.0102 1.01 11/18/2022 07:25 WG1961734 2,2-Dichloropropane U 0.00281 0.00511 1.01 11/18/2022 07:25 WG1961734 Di-isopropyl ether U 0.000836 0.00204 1.01 11/18/2022 07:25 WG1961734 Ethylbenzene U 0.00150 0.00511 1.01 11/18/2022 07:25 WG1961734 Hexachloro-1,3-butadiene U 0.0122 0.0511 1.01 11/18/2022 07:25 WG1961734 Isopropylbenzene U 0.000866 0.00511 1.01 11/18/2022 07:25 WG1961734 p-Isopropyltoluene U 0.00521 0.0102 1.01 11/18/2022 07:25 WG1961734 2-Butanone (MEK)U 0.129 0.204 1.01 11/18/2022 07:25 WG1961734 Methylene Chloride U 0.0135 0.0511 1.01 11/18/2022 07:25 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00464 0.0511 1.01 11/18/2022 07:25 WG1961734 Methyl tert-butyl ether U 0.000712 0.00204 1.01 11/18/2022 07:25 WG1961734 Naphthalene U J3 0.00995 0.0254 1.01 11/18/2022 07:25 WG1961734 n-Propylbenzene U 0.00194 0.0102 1.01 11/18/2022 07:25 WG1961734 Styrene U 0.000466 0.0254 1.01 11/18/2022 07:25 WG1961734 1,1,1,2-Tetrachloroethane U 0.00193 0.00511 1.01 11/18/2022 07:25 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00142 0.00511 1.01 11/18/2022 07:25 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00154 0.00511 1.01 11/18/2022 07:25 WG1961734 Tetrachloroethene U 0.00183 0.00511 1.01 11/18/2022 07:25 WG1961734 Toluene U 0.00264 0.0102 1.01 11/18/2022 07:25 WG1961734 1,2,3-Trichlorobenzene U C4 0.0149 0.0254 1.01 11/18/2022 07:25 WG1961734 1,2,4-Trichlorobenzene U J3 0.00896 0.0254 1.01 11/18/2022 07:25 WG1961734 1,1,1-Trichloroethane U 0.00188 0.00511 1.01 11/18/2022 07:25 WG1961734 1,1,2-Trichloroethane U 0.00122 0.00511 1.01 11/18/2022 07:25 WG1961734 Trichloroethene U 0.00119 0.00204 1.01 11/18/2022 07:25 WG1961734 Trichlorofluoromethane U 0.00169 0.00511 1.01 11/18/2022 07:25 WG1961734 1,2,3-Trichloropropane U 0.00331 0.0254 1.01 11/18/2022 07:25 WG1961734 1,2,4-Trimethylbenzene U 0.00323 0.0102 1.01 11/18/2022 07:25 WG1961734 1,2,3-Trimethylbenzene U 0.00323 0.0102 1.01 11/18/2022 07:25 WG1961734 1,3,5-Trimethylbenzene U 0.00408 0.0102 1.01 11/18/2022 07:25 WG1961734 Vinyl chloride U 0.00236 0.00511 1.01 11/18/2022 07:25 WG1961734 Xylenes, Total U 0.00179 0.0132 1.01 11/18/2022 07:25 WG1961734 (S) Toluene-d8 103 75.0-131 11/18/2022 07:25 WG1961734 (S) 4-Bromofluorobenzene 99.7 67.0-138 11/18/2022 07:25 WG1961734 (S) 1,2-Dichloroethane-d4 97.5 70.0-130 11/18/2022 07:25 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00815 0.0504 1 11/18/2022 16:20 WG1960983 Acenaphthylene U 0.00709 0.0504 1 11/18/2022 16:20 WG1960983 Anthracene U 0.00897 0.0504 1 11/18/2022 16:20 WG1960983 Benzidine U C3 0.0947 2.53 1 11/18/2022 16:20 WG1960983 Benzo(a)anthracene U 0.00888 0.0504 1 11/18/2022 16:20 WG1960983 Benzo(b)fluoranthene U 0.00939 0.0504 1 11/18/2022 16:20 WG1960983 Benzo(k)fluoranthene U 0.00895 0.0504 1 11/18/2022 16:20 WG1960983 Benzo(g,h,i)perylene U 0.00921 0.0504 1 11/18/2022 16:20 WG1960983 Benzo(a)pyrene U 0.00936 0.0504 1 11/18/2022 16:20 WG1960983 Bis(2-chlorethoxy)methane U 0.0151 0.504 1 11/18/2022 16:20 WG1960983 Bis(2-chloroethyl)ether U 0.0166 0.504 1 11/18/2022 16:20 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0218 0.504 1 11/18/2022 16:20 WG1960983 4-Bromophenyl-phenylether U 0.0177 0.504 1 11/18/2022 16:20 WG1960983 2-Chloronaphthalene U 0.00885 0.0504 1 11/18/2022 16:20 WG1960983 4-Chlorophenyl-phenylether U 0.0175 0.504 1 11/18/2022 16:20 WG1960983 Chrysene U 0.0100 0.0504 1 11/18/2022 16:20 WG1960983 Dibenz(a,h)anthracene U 0.0140 0.0504 1 11/18/2022 16:20 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 63 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 63 of 96 SAMPLE RESULTS - 19 L1557235 SS-3 (DUP) Collected date/time: 11/10/22 15:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0149 0.504 1 11/18/2022 16:20 WG1960983 1,3-Dichlorobenzene U 0.0153 0.504 1 11/18/2022 16:20 WG1960983 1,4-Dichlorobenzene U 0.0150 0.504 1 11/18/2022 16:20 WG1960983 3,3-Dichlorobenzidine U 0.0186 0.504 1 11/18/2022 16:20 WG1960983 2,4-Dinitrotoluene U 0.0144 0.504 1 11/18/2022 16:20 WG1960983 2,6-Dinitrotoluene U 0.0165 0.504 1 11/18/2022 16:20 WG1960983 Fluoranthene U 0.00909 0.0504 1 11/18/2022 16:20 WG1960983 Fluorene U 0.00820 0.0504 1 11/18/2022 16:20 WG1960983 Hexachlorobenzene U 0.0178 0.504 1 11/18/2022 16:20 WG1960983 Hexachloro-1,3-butadiene U 0.0169 0.504 1 11/18/2022 16:20 WG1960983 Hexachlorocyclopentadiene U 0.0265 0.504 1 11/18/2022 16:20 WG1960983 Hexachloroethane U 0.0198 0.504 1 11/18/2022 16:20 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0142 0.0504 1 11/18/2022 16:20 WG1960983 Isophorone U 0.0154 0.504 1 11/18/2022 16:20 WG1960983 Naphthalene U 0.0126 0.0504 1 11/18/2022 16:20 WG1960983 Nitrobenzene U 0.0175 0.504 1 11/18/2022 16:20 WG1960983 n-Nitrosodimethylamine U 0.0747 0.504 1 11/18/2022 16:20 WG1960983 n-Nitrosodiphenylamine U 0.0381 0.504 1 11/18/2022 16:20 WG1960983 n-Nitrosodi-n-propylamine U 0.0168 0.504 1 11/18/2022 16:20 WG1960983 Phenanthrene U 0.0100 0.0504 1 11/18/2022 16:20 WG1960983 Benzylbutyl phthalate U 0.0157 0.504 1 11/18/2022 16:20 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0638 0.504 1 11/18/2022 16:20 WG1960983 Di-n-butyl phthalate U 0.0172 0.504 1 11/18/2022 16:20 WG1960983 Diethyl phthalate U 0.0166 0.504 1 11/18/2022 16:20 WG1960983 Dimethyl phthalate U 0.107 0.504 1 11/18/2022 16:20 WG1960983 Di-n-octyl phthalate U 0.0340 0.504 1 11/18/2022 16:20 WG1960983 Pyrene U 0.00980 0.0504 1 11/18/2022 16:20 WG1960983 1,2,4-Trichlorobenzene U 0.0157 0.504 1 11/18/2022 16:20 WG1960983 4-Chloro-3-methylphenol U 0.0163 0.504 1 11/18/2022 16:20 WG1960983 2-Chlorophenol U 0.0166 0.504 1 11/18/2022 16:20 WG1960983 2,4-Dichlorophenol U 0.0147 0.504 1 11/18/2022 16:20 WG1960983 2,4-Dimethylphenol U 0.0132 0.504 1 11/18/2022 16:20 WG1960983 4,6-Dinitro-2-methylphenol U 0.114 0.504 1 11/18/2022 16:20 WG1960983 2,4-Dinitrophenol U 0.118 0.504 1 11/18/2022 16:20 WG1960983 2-Nitrophenol U 0.0180 0.504 1 11/18/2022 16:20 WG1960983 4-Nitrophenol U 0.0157 0.504 1 11/18/2022 16:20 WG1960983 Pentachlorophenol U 0.0136 0.504 1 11/18/2022 16:20 WG1960983 Phenol U 0.0203 0.504 1 11/18/2022 16:20 WG1960983 2,4,6-Trichlorophenol U 0.0162 0.504 1 11/18/2022 16:20 WG1960983 (S) 2-Fluorophenol 57.9 12.0-120 11/18/2022 16:20 WG1960983 (S) Phenol-d5 53.4 10.0-120 11/18/2022 16:20 WG1960983 (S) Nitrobenzene-d5 50.9 10.0-122 11/18/2022 16:20 WG1960983 (S) 2-Fluorobiphenyl 48.5 15.0-120 11/18/2022 16:20 WG1960983 (S) 2,4,6-Tribromophenol 58.6 10.0-127 11/18/2022 16:20 WG1960983 (S) p-Terphenyl-d14 56.8 10.0-120 11/18/2022 16:20 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 64 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 64 of 96 SAMPLE RESULTS - 20 L1557235 SS-3-A (DUP) Collected date/time: 11/10/22 15:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 67.0 1 11/16/2022 09:28 WG1959833 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0269 0.0597 1 11/17/2022 16:31 WG1960568 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.24 0.149 1.49 5 11/29/2022 21:08 WG1961432 Barium 15.7 0.227 3.73 5 11/29/2022 21:08 WG1961432 Cadmium U 0.128 1.49 5 11/29/2022 21:08 WG1961432 Chromium 17.5 0.442 7.46 5 11/29/2022 21:08 WG1961432 Lead 7.34 0.148 2.98 5 11/29/2022 21:08 WG1961432 Selenium 0.936 J 0.269 3.73 5 11/29/2022 21:08 WG1961432 Silver U 0.129 0.746 5 11/29/2022 21:08 WG1961432 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U J3 J4 0.0727 0.0996 1 11/18/2022 07:44 WG1961734 Acrylonitrile U J3 0.00719 0.0249 1 11/18/2022 07:44 WG1961734 Benzene U 0.000930 0.00199 1 11/18/2022 07:44 WG1961734 Bromobenzene U 0.00179 0.0249 1 11/18/2022 07:44 WG1961734 Bromodichloromethane U 0.00144 0.00498 1 11/18/2022 07:44 WG1961734 Bromoform U 0.00233 0.0498 1 11/18/2022 07:44 WG1961734 Bromomethane U 0.00392 0.0249 1 11/18/2022 07:44 WG1961734 n-Butylbenzene U 0.0105 0.0249 1 11/18/2022 07:44 WG1961734 sec-Butylbenzene U 0.00574 0.0249 1 11/18/2022 07:44 WG1961734 tert-Butylbenzene U 0.00388 0.00996 1 11/18/2022 07:44 WG1961734 Carbon tetrachloride U 0.00179 0.00996 1 11/18/2022 07:44 WG1961734 Chlorobenzene U 0.000418 0.00498 1 11/18/2022 07:44 WG1961734 Chlorodibromomethane U C3 0.00122 0.00498 1 11/18/2022 07:44 WG1961734 Chloroethane U 0.00339 0.00996 1 11/18/2022 07:44 WG1961734 Chloroform U 0.00205 0.00498 1 11/18/2022 07:44 WG1961734 Chloromethane U 0.00866 0.0249 1 11/18/2022 07:44 WG1961734 2-Chlorotoluene U 0.00172 0.00498 1 11/18/2022 07:44 WG1961734 4-Chlorotoluene U 0.000896 0.00996 1 11/18/2022 07:44 WG1961734 1,2-Dibromo-3-Chloropropane U J3 0.00777 0.0498 1 11/18/2022 07:44 WG1961734 1,2-Dibromoethane U 0.00129 0.00498 1 11/18/2022 07:44 WG1961734 Dibromomethane U 0.00149 0.00996 1 11/18/2022 07:44 WG1961734 1,2-Dichlorobenzene U 0.000847 0.00996 1 11/18/2022 07:44 WG1961734 1,3-Dichlorobenzene U 0.00120 0.00996 1 11/18/2022 07:44 WG1961734 1,4-Dichlorobenzene U 0.00139 0.00996 1 11/18/2022 07:44 WG1961734 Dichlorodifluoromethane U 0.00321 0.00498 1 11/18/2022 07:44 WG1961734 1,1-Dichloroethane U 0.000978 0.00498 1 11/18/2022 07:44 WG1961734 1,2-Dichloroethane U 0.00129 0.00498 1 11/18/2022 07:44 WG1961734 1,1-Dichloroethene U 0.00121 0.00498 1 11/18/2022 07:44 WG1961734 cis-1,2-Dichloroethene U 0.00146 0.00498 1 11/18/2022 07:44 WG1961734 trans-1,2-Dichloroethene U 0.00207 0.00996 1 11/18/2022 07:44 WG1961734 1,2-Dichloropropane U 0.00283 0.00996 1 11/18/2022 07:44 WG1961734 1,1-Dichloropropene U 0.00161 0.00498 1 11/18/2022 07:44 WG1961734 1,3-Dichloropropane U 0.000998 0.00996 1 11/18/2022 07:44 WG1961734 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 65 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 65 of 96 SAMPLE RESULTS - 20 L1557235 SS-3-A (DUP) Collected date/time: 11/10/22 15:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00151 0.00498 1 11/18/2022 07:44 WG1961734 trans-1,3-Dichloropropene U 0.00227 0.00996 1 11/18/2022 07:44 WG1961734 2,2-Dichloropropane U 0.00275 0.00498 1 11/18/2022 07:44 WG1961734 Di-isopropyl ether U 0.000817 0.00199 1 11/18/2022 07:44 WG1961734 Ethylbenzene U 0.00147 0.00498 1 11/18/2022 07:44 WG1961734 Hexachloro-1,3-butadiene U 0.0120 0.0498 1 11/18/2022 07:44 WG1961734 Isopropylbenzene 0.000928 J 0.000847 0.00498 1 11/18/2022 07:44 WG1961734 p-Isopropyltoluene U 0.00508 0.00996 1 11/18/2022 07:44 WG1961734 2-Butanone (MEK)U 0.126 0.199 1 11/18/2022 07:44 WG1961734 Methylene Chloride U 0.0132 0.0498 1 11/18/2022 07:44 WG1961734 4-Methyl-2-pentanone (MIBK)U 0.00454 0.0498 1 11/18/2022 07:44 WG1961734 Methyl tert-butyl ether U 0.000697 0.00199 1 11/18/2022 07:44 WG1961734 Naphthalene U J3 0.00972 0.0249 1 11/18/2022 07:44 WG1961734 n-Propylbenzene U 0.00189 0.00996 1 11/18/2022 07:44 WG1961734 Styrene U 0.000456 0.0249 1 11/18/2022 07:44 WG1961734 1,1,1,2-Tetrachloroethane U 0.00189 0.00498 1 11/18/2022 07:44 WG1961734 1,1,2,2-Tetrachloroethane U C3 0.00138 0.00498 1 11/18/2022 07:44 WG1961734 1,1,2-Trichlorotrifluoroethane U 0.00150 0.00498 1 11/18/2022 07:44 WG1961734 Tetrachloroethene U 0.00178 0.00498 1 11/18/2022 07:44 WG1961734 Toluene U 0.00259 0.00996 1 11/18/2022 07:44 WG1961734 1,2,3-Trichlorobenzene U C4 0.0146 0.0249 1 11/18/2022 07:44 WG1961734 1,2,4-Trichlorobenzene U J3 0.00876 0.0249 1 11/18/2022 07:44 WG1961734 1,1,1-Trichloroethane U 0.00184 0.00498 1 11/18/2022 07:44 WG1961734 1,1,2-Trichloroethane U 0.00119 0.00498 1 11/18/2022 07:44 WG1961734 Trichloroethene U 0.00116 0.00199 1 11/18/2022 07:44 WG1961734 Trichlorofluoromethane U 0.00165 0.00498 1 11/18/2022 07:44 WG1961734 1,2,3-Trichloropropane U 0.00323 0.0249 1 11/18/2022 07:44 WG1961734 1,2,4-Trimethylbenzene U 0.00315 0.00996 1 11/18/2022 07:44 WG1961734 1,2,3-Trimethylbenzene U 0.00315 0.00996 1 11/18/2022 07:44 WG1961734 1,3,5-Trimethylbenzene U 0.00398 0.00996 1 11/18/2022 07:44 WG1961734 Vinyl chloride U 0.00231 0.00498 1 11/18/2022 07:44 WG1961734 Xylenes, Total U 0.00175 0.0129 1 11/18/2022 07:44 WG1961734 (S) Toluene-d8 104 75.0-131 11/18/2022 07:44 WG1961734 (S) 4-Bromofluorobenzene 102 67.0-138 11/18/2022 07:44 WG1961734 (S) 1,2-Dichloroethane-d4 92.9 70.0-130 11/18/2022 07:44 WG1961734 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00804 0.0497 1 11/18/2022 16:40 WG1960983 Acenaphthylene U 0.00700 0.0497 1 11/18/2022 16:40 WG1960983 Anthracene U 0.00885 0.0497 1 11/18/2022 16:40 WG1960983 Benzidine U C3 0.0934 2.49 1 11/18/2022 16:40 WG1960983 Benzo(a)anthracene U 0.00876 0.0497 1 11/18/2022 16:40 WG1960983 Benzo(b)fluoranthene U 0.00927 0.0497 1 11/18/2022 16:40 WG1960983 Benzo(k)fluoranthene U 0.00883 0.0497 1 11/18/2022 16:40 WG1960983 Benzo(g,h,i)perylene U 0.00909 0.0497 1 11/18/2022 16:40 WG1960983 Benzo(a)pyrene U 0.00924 0.0497 1 11/18/2022 16:40 WG1960983 Bis(2-chlorethoxy)methane U 0.0149 0.497 1 11/18/2022 16:40 WG1960983 Bis(2-chloroethyl)ether U 0.0164 0.497 1 11/18/2022 16:40 WG1960983 2,2-Oxybis(1-Chloropropane)U 0.0215 0.497 1 11/18/2022 16:40 WG1960983 4-Bromophenyl-phenylether U 0.0175 0.497 1 11/18/2022 16:40 WG1960983 2-Chloronaphthalene U 0.00873 0.0497 1 11/18/2022 16:40 WG1960983 4-Chlorophenyl-phenylether U 0.0173 0.497 1 11/18/2022 16:40 WG1960983 Chrysene U 0.00988 0.0497 1 11/18/2022 16:40 WG1960983 Dibenz(a,h)anthracene U 0.0138 0.0497 1 11/18/2022 16:40 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 66 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 66 of 96 SAMPLE RESULTS - 20 L1557235 SS-3-A (DUP) Collected date/time: 11/10/22 15:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene 0.0273 J 0.0147 0.497 1 11/18/2022 16:40 WG1960983 1,3-Dichlorobenzene U 0.0151 0.497 1 11/18/2022 16:40 WG1960983 1,4-Dichlorobenzene U 0.0148 0.497 1 11/18/2022 16:40 WG1960983 3,3-Dichlorobenzidine U 0.0184 0.497 1 11/18/2022 16:40 WG1960983 2,4-Dinitrotoluene U 0.0142 0.497 1 11/18/2022 16:40 WG1960983 2,6-Dinitrotoluene U 0.0163 0.497 1 11/18/2022 16:40 WG1960983 Fluoranthene U 0.00897 0.0497 1 11/18/2022 16:40 WG1960983 Fluorene U 0.00809 0.0497 1 11/18/2022 16:40 WG1960983 Hexachlorobenzene U 0.0176 0.497 1 11/18/2022 16:40 WG1960983 Hexachloro-1,3-butadiene U 0.0167 0.497 1 11/18/2022 16:40 WG1960983 Hexachlorocyclopentadiene U 0.0261 0.497 1 11/18/2022 16:40 WG1960983 Hexachloroethane U 0.0195 0.497 1 11/18/2022 16:40 WG1960983 Indeno(1,2,3-cd)pyrene U 0.0140 0.0497 1 11/18/2022 16:40 WG1960983 Isophorone U 0.0152 0.497 1 11/18/2022 16:40 WG1960983 Naphthalene U 0.0125 0.0497 1 11/18/2022 16:40 WG1960983 Nitrobenzene U 0.0173 0.497 1 11/18/2022 16:40 WG1960983 n-Nitrosodimethylamine U 0.0737 0.497 1 11/18/2022 16:40 WG1960983 n-Nitrosodiphenylamine U 0.0376 0.497 1 11/18/2022 16:40 WG1960983 n-Nitrosodi-n-propylamine U 0.0166 0.497 1 11/18/2022 16:40 WG1960983 Phenanthrene U 0.00986 0.0497 1 11/18/2022 16:40 WG1960983 Benzylbutyl phthalate U 0.0155 0.497 1 11/18/2022 16:40 WG1960983 Bis(2-ethylhexyl)phthalate U 0.0630 0.497 1 11/18/2022 16:40 WG1960983 Di-n-butyl phthalate U 0.0170 0.497 1 11/18/2022 16:40 WG1960983 Diethyl phthalate U 0.0164 0.497 1 11/18/2022 16:40 WG1960983 Dimethyl phthalate U 0.105 0.497 1 11/18/2022 16:40 WG1960983 Di-n-octyl phthalate U 0.0336 0.497 1 11/18/2022 16:40 WG1960983 Pyrene U 0.00967 0.0497 1 11/18/2022 16:40 WG1960983 1,2,4-Trichlorobenzene U 0.0155 0.497 1 11/18/2022 16:40 WG1960983 4-Chloro-3-methylphenol U 0.0161 0.497 1 11/18/2022 16:40 WG1960983 2-Chlorophenol U 0.0164 0.497 1 11/18/2022 16:40 WG1960983 2,4-Dichlorophenol U 0.0145 0.497 1 11/18/2022 16:40 WG1960983 2,4-Dimethylphenol U 0.0130 0.497 1 11/18/2022 16:40 WG1960983 4,6-Dinitro-2-methylphenol U 0.113 0.497 1 11/18/2022 16:40 WG1960983 2,4-Dinitrophenol U 0.116 0.497 1 11/18/2022 16:40 WG1960983 2-Nitrophenol U 0.0178 0.497 1 11/18/2022 16:40 WG1960983 4-Nitrophenol U 0.0155 0.497 1 11/18/2022 16:40 WG1960983 Pentachlorophenol U 0.0134 0.497 1 11/18/2022 16:40 WG1960983 Phenol U 0.0200 0.497 1 11/18/2022 16:40 WG1960983 2,4,6-Trichlorophenol U 0.0160 0.497 1 11/18/2022 16:40 WG1960983 (S) 2-Fluorophenol 62.1 12.0-120 11/18/2022 16:40 WG1960983 (S) Phenol-d5 57.4 10.0-120 11/18/2022 16:40 WG1960983 (S) Nitrobenzene-d5 54.3 10.0-122 11/18/2022 16:40 WG1960983 (S) 2-Fluorobiphenyl 52.8 15.0-120 11/18/2022 16:40 WG1960983 (S) 2,4,6-Tribromophenol 65.3 10.0-127 11/18/2022 16:40 WG1960983 (S) p-Terphenyl-d14 63.2 10.0-120 11/18/2022 16:40 WG1960983 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 67 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 67 of 96 QUALITY CONTROL SUMMARYWG1959829 Total Solids by Method 2540 G-2011 L1557235-01,02,03,04,05,06,07,08,09,10 Method Blank (MB) (MB) R3861777-1 11/16/22 08:20 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00300 L1557235-01 Original Sample (OS) • Duplicate (DUP) (OS) L1557235-01 11/16/22 08:20 • (DUP) R3861777-3 11/16/22 08:20 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 81.2 80.2 1 1.23 10 Laboratory Control Sample (LCS) (LCS) R3861777-2 11/16/22 08:20 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85.0-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 68 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 68 of 96 QUALITY CONTROL SUMMARYWG1959833 Total Solids by Method 2540 G-2011 L1557235-11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3861974-1 11/16/22 09:28 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00500 L1557235-11 Original Sample (OS) • Duplicate (DUP) (OS) L1557235-11 11/16/22 09:28 • (DUP) R3861974-3 11/16/22 09:28 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 68.4 69.7 1 1.94 10 Laboratory Control Sample (LCS) (LCS) R3861974-2 11/16/22 09:28 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85.0-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 69 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 69 of 96 QUALITY CONTROL SUMMARYWG1960559 Mercury by Method 7471B L1557235-01,02,03,04,05,06,07,08,09,10 Method Blank (MB) (MB) R3862400-1 11/17/22 12:55 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Mercury U 0.0180 0.0400 Laboratory Control Sample (LCS) (LCS) R3862400-2 11/17/22 12:57 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Mercury 0.500 0.492 98.3 80.0-120 L1557581-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557581-17 11/17/22 13:00 • (MS) R3862400-3 11/17/22 13:07 • (MSD) R3862400-4 11/17/22 13:09 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Mercury 0.500 U 0.466 0.440 93.2 88.0 1 75.0-125 5.78 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 70 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 70 of 96 QUALITY CONTROL SUMMARYWG1960561 Mercury by Method 7471B L1557235-11,12,13,14 Method Blank (MB) (MB) R3862361-1 11/17/22 14:18 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Mercury U 0.0180 0.0400 Laboratory Control Sample (LCS) (LCS) R3862361-2 11/17/22 14:20 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Mercury 0.500 0.483 96.7 80.0-120 L1557408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557408-01 11/17/22 14:22 • (MS) R3862361-3 11/17/22 14:25 • (MSD) R3862361-4 11/17/22 14:27 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Mercury 0.609 0.0299 0.584 0.557 91.0 86.5 1 75.0-125 4.76 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 71 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 71 of 96 QUALITY CONTROL SUMMARYWG1960568 Mercury by Method 7471B L1557235-15,16,17,18,19,20 Method Blank (MB) (MB) R3862415-1 11/17/22 15:24 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Mercury U 0.0180 0.0400 Laboratory Control Sample (LCS) (LCS) R3862415-2 11/17/22 15:26 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Mercury 0.500 0.495 99.0 80.0-120 L1557581-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557581-03 11/17/22 15:29 • (MS) R3862415-3 11/17/22 15:31 • (MSD) R3862415-4 11/17/22 15:34 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Mercury 0.500 U 0.456 0.478 91.2 95.6 1 75.0-125 4.76 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 72 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 72 of 96 QUALITY CONTROL SUMMARYWG1961432 Metals (ICPMS) by Method 6020B L1557235-11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3866304-1 11/29/22 20:07 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.100 1.00 Barium U 0.152 2.50 Cadmium U 0.0855 1.00 Chromium U 0.297 5.00 Lead U 0.0990 2.00 Selenium U 0.180 2.50 Silver U 0.0865 0.500 Laboratory Control Sample (LCS) (LCS) R3866304-2 11/29/22 20:10 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Arsenic 100 100 100 80.0-120 Barium 100 100 100 80.0-120 Cadmium 100 101 101 80.0-120 Chromium 100 101 101 80.0-120 Lead 100 98.5 98.5 80.0-120 Selenium 100 105 105 80.0-120 Silver 20.0 19.9 99.3 80.0-120 L1558011-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558011-08 11/29/22 20:13 • (MS) R3866304-5 11/29/22 20:23 • (MSD) R3866304-6 11/29/22 20:27 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 113 1.93 107 109 93.5 95.3 5 75.0-125 1.89 20 Barium 113 63.0 210 177 130 101 5 75.0-125 E J5 E 16.9 20 Cadmium 113 U 109 113 96.5 100 5 75.0-125 3.58 20 Chromium 113 14.1 119 125 93.0 98.1 5 75.0-125 4.73 20 Lead 113 2.63 110 111 95.1 96.4 5 75.0-125 1.28 20 Selenium 113 0.369 115 120 102 106 5 75.0-125 3.93 20 Silver 22.6 U 21.5 22.2 95.2 98.2 5 75.0-125 3.04 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 73 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 73 of 96 QUALITY CONTROL SUMMARYWG1966023 Metals (ICPMS) by Method 6020B L1557235-01,02,03,04,05,06,07,08,09,10 Method Blank (MB) (MB) R3865820-1 11/28/22 20:02 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.100 1.00 Barium U 0.152 2.50 Cadmium U 0.0855 1.00 Chromium U 0.297 5.00 Lead U 0.0990 2.00 Selenium U 0.180 2.50 Silver U 0.0865 0.500 Laboratory Control Sample (LCS) (LCS) R3865820-2 11/28/22 20:05 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Arsenic 100 94.4 94.4 80.0-120 Barium 100 93.1 93.1 80.0-120 Cadmium 100 99.5 99.5 80.0-120 Chromium 100 97.0 97.0 80.0-120 Lead 100 96.1 96.1 80.0-120 Selenium 100 101 101 80.0-120 Silver 20.0 20.2 101 80.0-120 L1557235-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557235-01 11/28/22 20:08 • (MS) R3865820-5 11/28/22 20:18 • (MSD) R3865820-6 11/28/22 20:22 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 123 3.15 118 121 93.1 95.3 5 75.0-125 2.27 20 Barium 123 15.0 133 128 95.7 91.6 5 75.0-125 3.86 20 Cadmium 123 U 131 122 106 99.1 5 75.0-125 6.78 20 Chromium 123 8.82 136 134 103 101 5 75.0-125 1.72 20 Lead 123 17.2 141 132 100 93.2 5 75.0-125 6.27 20 Selenium 123 0.249 107 117 86.7 95.1 5 75.0-125 9.25 20 Silver 24.6 U 26.1 24.3 106 98.6 5 75.0-125 7.19 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 74 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 74 of 96 QUALITY CONTROL SUMMARYWG1961410 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13 Method Blank (MB) (MB) R3864139-3 11/17/22 12:42 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0365 0.0500 Acrylonitrile U 0.00361 0.0125 Benzene U 0.000467 0.00100 Bromobenzene U 0.000900 0.0125 Bromodichloromethane U 0.000725 0.00250 Bromoform U 0.00117 0.0250 Bromomethane U 0.00197 0.0125 n-Butylbenzene U 0.00525 0.0125 sec-Butylbenzene 0.00320 J 0.00288 0.0125 tert-Butylbenzene U 0.00195 0.00500 Carbon tetrachloride U 0.000898 0.00500 Chlorobenzene U 0.000210 0.00250 Chlorodibromomethane U 0.000612 0.00250 Chloroethane U 0.00170 0.00500 Chloroform U 0.00103 0.00250 Chloromethane U 0.00435 0.0125 2-Chlorotoluene U 0.000865 0.00250 4-Chlorotoluene U 0.000450 0.00500 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1,2-Dibromoethane U 0.000648 0.00250 Dibromomethane U 0.000750 0.00500 1,2-Dichlorobenzene U 0.000425 0.00500 1,3-Dichlorobenzene U 0.000600 0.00500 1,4-Dichlorobenzene U 0.000700 0.00500 Dichlorodifluoromethane U 0.00161 0.00250 1,1-Dichloroethane U 0.000491 0.00250 1,2-Dichloroethane U 0.000649 0.00250 1,1-Dichloroethene U 0.000606 0.00250 cis-1,2-Dichloroethene U 0.000734 0.00250 trans-1,2-Dichloroethene U 0.00104 0.00500 1,2-Dichloropropane U 0.00142 0.00500 1,1-Dichloropropene U 0.000809 0.00250 1,3-Dichloropropane U 0.000501 0.00500 cis-1,3-Dichloropropene U 0.000757 0.00250 trans-1,3-Dichloropropene U 0.00114 0.00500 2,2-Dichloropropane U 0.00138 0.00250 Di-isopropyl ether U 0.000410 0.00100 Ethylbenzene 0.00135 J 0.000737 0.00250 Hexachloro-1,3-butadiene U 0.00600 0.0250 Isopropylbenzene U 0.000425 0.00250 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 75 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 75 of 96 QUALITY CONTROL SUMMARYWG1961410 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13 Method Blank (MB) (MB) R3864139-3 11/17/22 12:42 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.00255 0.00500 2-Butanone (MEK)U 0.0635 0.100 Methylene Chloride U 0.00664 0.0250 4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250 Methyl tert-butyl ether U 0.000350 0.00100 Naphthalene U 0.00488 0.0125 n-Propylbenzene U 0.000950 0.00500 Styrene 0.00983 J 0.000229 0.0125 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 Tetrachloroethene 0.00403 0.000896 0.00250 Toluene U 0.00130 0.00500 1,2,3-Trichlorobenzene U 0.00733 0.0125 1,2,4-Trichlorobenzene U 0.00440 0.0125 1,1,1-Trichloroethane U 0.000923 0.00250 1,1,2-Trichloroethane U 0.000597 0.00250 Trichloroethene U 0.000584 0.00100 Trichlorofluoromethane U 0.000827 0.00250 1,2,3-Trichloropropane U 0.00162 0.0125 1,2,4-Trimethylbenzene U 0.00158 0.00500 1,2,3-Trimethylbenzene U 0.00158 0.00500 1,3,5-Trimethylbenzene U 0.00200 0.00500 Vinyl chloride U 0.00116 0.00250 Xylenes, Total 0.00222 J 0.000880 0.00650 (S) Toluene-d8 106 75.0-131 (S) 4-Bromofluorobenzene 103 67.0-138 (S) 1,2-Dichloroethane-d4 78.8 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864139-1 11/17/22 10:16 • (LCSD) R3864139-2 11/17/22 11:08 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acetone 0.625 0.648 0.647 104 104 10.0-160 0.154 31 Acrylonitrile 0.625 0.710 0.740 114 118 45.0-153 4.14 22 Benzene 0.125 0.116 0.111 92.8 88.8 70.0-123 4.41 20 Bromobenzene 0.125 0.116 0.116 92.8 92.8 73.0-121 0.000 20 Bromodichloromethane 0.125 0.107 0.102 85.6 81.6 73.0-121 4.78 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 76 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 76 of 96 QUALITY CONTROL SUMMARYWG1961410 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864139-1 11/17/22 10:16 • (LCSD) R3864139-2 11/17/22 11:08 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Bromoform 0.125 0.122 0.131 97.6 105 64.0-132 7.11 20 Bromomethane 0.125 0.118 0.116 94.4 92.8 56.0-147 1.71 20 n-Butylbenzene 0.125 0.120 0.117 96.0 93.6 68.0-135 2.53 20 sec-Butylbenzene 0.125 0.111 0.109 88.8 87.2 74.0-130 1.82 20 tert-Butylbenzene 0.125 0.0974 0.0975 77.9 78.0 75.0-127 0.103 20 Carbon tetrachloride 0.125 0.136 0.130 109 104 66.0-128 4.51 20 Chlorobenzene 0.125 0.134 0.131 107 105 76.0-128 2.26 20 Chlorodibromomethane 0.125 0.120 0.121 96.0 96.8 74.0-127 0.830 20 Chloroethane 0.125 0.132 0.125 106 100 61.0-134 5.45 20 Chloroform 0.125 0.127 0.115 102 92.0 72.0-123 9.92 20 Chloromethane 0.125 0.130 0.147 104 118 51.0-138 12.3 20 2-Chlorotoluene 0.125 0.114 0.104 91.2 83.2 75.0-124 9.17 20 4-Chlorotoluene 0.125 0.111 0.119 88.8 95.2 75.0-124 6.96 20 1,2-Dibromo-3-Chloropropane 0.125 0.0943 0.101 75.4 80.8 59.0-130 6.86 20 1,2-Dibromoethane 0.125 0.115 0.118 92.0 94.4 74.0-128 2.58 20 Dibromomethane 0.125 0.110 0.112 88.0 89.6 75.0-122 1.80 20 1,2-Dichlorobenzene 0.125 0.121 0.123 96.8 98.4 76.0-124 1.64 20 1,3-Dichlorobenzene 0.125 0.129 0.131 103 105 76.0-125 1.54 20 1,4-Dichlorobenzene 0.125 0.124 0.124 99.2 99.2 77.0-121 0.000 20 Dichlorodifluoromethane 0.125 0.109 0.111 87.2 88.8 43.0-156 1.82 20 1,1-Dichloroethane 0.125 0.129 0.124 103 99.2 70.0-127 3.95 20 1,2-Dichloroethane 0.125 0.130 0.127 104 102 65.0-131 2.33 20 1,1-Dichloroethene 0.125 0.131 0.125 105 100 65.0-131 4.69 20 cis-1,2-Dichloroethene 0.125 0.122 0.117 97.6 93.6 73.0-125 4.18 20 trans-1,2-Dichloroethene 0.125 0.120 0.112 96.0 89.6 71.0-125 6.90 20 1,2-Dichloropropane 0.125 0.115 0.113 92.0 90.4 74.0-125 1.75 20 1,1-Dichloropropene 0.125 0.119 0.113 95.2 90.4 73.0-125 5.17 20 1,3-Dichloropropane 0.125 0.112 0.107 89.6 85.6 80.0-125 4.57 20 cis-1,3-Dichloropropene 0.125 0.101 0.0940 80.8 75.2 76.0-127 J4 7.18 20 trans-1,3-Dichloropropene 0.125 0.106 0.105 84.8 84.0 73.0-127 0.948 20 2,2-Dichloropropane 0.125 0.121 0.111 96.8 88.8 59.0-135 8.62 20 Di-isopropyl ether 0.125 0.142 0.140 114 112 60.0-136 1.42 20 Ethylbenzene 0.125 0.139 0.130 111 104 74.0-126 6.69 20 Hexachloro-1,3-butadiene 0.125 0.118 0.117 94.4 93.6 57.0-150 0.851 20 Isopropylbenzene 0.125 0.146 0.142 117 114 72.0-127 2.78 20 p-Isopropyltoluene 0.125 0.120 0.116 96.0 92.8 72.0-133 3.39 20 2-Butanone (MEK)0.625 0.612 0.629 97.9 101 30.0-160 2.74 24 Methylene Chloride 0.125 0.116 0.108 92.8 86.4 68.0-123 7.14 20 4-Methyl-2-pentanone (MIBK)0.625 0.625 0.628 100 100 56.0-143 0.479 20 Methyl tert-butyl ether 0.125 0.109 0.105 87.2 84.0 66.0-132 3.74 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 77 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 77 of 96 QUALITY CONTROL SUMMARYWG1961410 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864139-1 11/17/22 10:16 • (LCSD) R3864139-2 11/17/22 11:08 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Naphthalene 0.125 0.115 0.119 92.0 95.2 59.0-130 3.42 20 n-Propylbenzene 0.125 0.122 0.116 97.6 92.8 74.0-126 5.04 20 Styrene 0.125 0.137 0.134 110 107 72.0-127 2.21 20 1,1,1,2-Tetrachloroethane 0.125 0.146 0.139 117 111 74.0-129 4.91 20 1,1,2,2-Tetrachloroethane 0.125 0.107 0.107 85.6 85.6 68.0-128 0.000 20 1,1,2-Trichlorotrifluoroethane 0.125 0.128 0.120 102 96.0 61.0-139 6.45 20 Tetrachloroethene 0.125 0.157 0.147 126 118 70.0-136 6.58 20 Toluene 0.125 0.131 0.126 105 101 75.0-121 3.89 20 1,2,3-Trichlorobenzene 0.125 0.110 0.114 88.0 91.2 59.0-139 3.57 20 1,2,4-Trichlorobenzene 0.125 0.113 0.114 90.4 91.2 62.0-137 0.881 20 1,1,1-Trichloroethane 0.125 0.133 0.130 106 104 69.0-126 2.28 20 1,1,2-Trichloroethane 0.125 0.120 0.117 96.0 93.6 78.0-123 2.53 20 Trichloroethene 0.125 0.138 0.129 110 103 76.0-126 6.74 20 Trichlorofluoromethane 0.125 0.112 0.117 89.6 93.6 61.0-142 4.37 20 1,2,3-Trichloropropane 0.125 0.105 0.102 84.0 81.6 67.0-129 2.90 20 1,2,4-Trimethylbenzene 0.125 0.118 0.115 94.4 92.0 70.0-126 2.58 20 1,2,3-Trimethylbenzene 0.125 0.110 0.109 88.0 87.2 74.0-124 0.913 20 1,3,5-Trimethylbenzene 0.125 0.112 0.109 89.6 87.2 73.0-127 2.71 20 Vinyl chloride 0.125 0.138 0.129 110 103 63.0-134 6.74 20 Xylenes, Total 0.375 0.402 0.388 107 103 72.0-127 3.54 20 (S) Toluene-d8 105 106 75.0-131 (S) 4-Bromofluorobenzene 113 111 67.0-138 (S) 1,2-Dichloroethane-d4 97.6 96.6 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 78 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 78 of 96 QUALITY CONTROL SUMMARYWG1961734 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-14,15,16,17,18,19,20 Method Blank (MB) (MB) R3862572-3 11/18/22 00:04 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0365 0.0500 Acrylonitrile U 0.00361 0.0125 Benzene U 0.000467 0.00100 Bromobenzene U 0.000900 0.0125 Bromodichloromethane U 0.000725 0.00250 Bromoform U 0.00117 0.0250 Bromomethane U 0.00197 0.0125 n-Butylbenzene U 0.00525 0.0125 sec-Butylbenzene U 0.00288 0.0125 tert-Butylbenzene U 0.00195 0.00500 Carbon tetrachloride U 0.000898 0.00500 Chlorobenzene U 0.000210 0.00250 Chlorodibromomethane U 0.000612 0.00250 Chloroethane U 0.00170 0.00500 Chloroform U 0.00103 0.00250 Chloromethane U 0.00435 0.0125 2-Chlorotoluene U 0.000865 0.00250 4-Chlorotoluene U 0.000450 0.00500 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1,2-Dibromoethane U 0.000648 0.00250 Dibromomethane U 0.000750 0.00500 1,2-Dichlorobenzene U 0.000425 0.00500 1,3-Dichlorobenzene U 0.000600 0.00500 1,4-Dichlorobenzene U 0.000700 0.00500 Dichlorodifluoromethane U 0.00161 0.00250 1,1-Dichloroethane U 0.000491 0.00250 1,2-Dichloroethane U 0.000649 0.00250 1,1-Dichloroethene U 0.000606 0.00250 cis-1,2-Dichloroethene U 0.000734 0.00250 trans-1,2-Dichloroethene U 0.00104 0.00500 1,2-Dichloropropane U 0.00142 0.00500 1,1-Dichloropropene U 0.000809 0.00250 1,3-Dichloropropane U 0.000501 0.00500 cis-1,3-Dichloropropene U 0.000757 0.00250 trans-1,3-Dichloropropene U 0.00114 0.00500 2,2-Dichloropropane U 0.00138 0.00250 Di-isopropyl ether U 0.000410 0.00100 Ethylbenzene U 0.000737 0.00250 Hexachloro-1,3-butadiene U 0.00600 0.0250 Isopropylbenzene U 0.000425 0.00250 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 79 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 79 of 96 QUALITY CONTROL SUMMARYWG1961734 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-14,15,16,17,18,19,20 Method Blank (MB) (MB) R3862572-3 11/18/22 00:04 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.00255 0.00500 2-Butanone (MEK)U 0.0635 0.100 Methylene Chloride U 0.00664 0.0250 4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250 Methyl tert-butyl ether U 0.000350 0.00100 Naphthalene U 0.00488 0.0125 n-Propylbenzene U 0.000950 0.00500 Styrene 0.00235 J 0.000229 0.0125 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 Tetrachloroethene U 0.000896 0.00250 Toluene U 0.00130 0.00500 1,2,3-Trichlorobenzene U 0.00733 0.0125 1,2,4-Trichlorobenzene U 0.00440 0.0125 1,1,1-Trichloroethane U 0.000923 0.00250 1,1,2-Trichloroethane U 0.000597 0.00250 Trichloroethene U 0.000584 0.00100 Trichlorofluoromethane U 0.000827 0.00250 1,2,3-Trichloropropane U 0.00162 0.0125 1,2,4-Trimethylbenzene U 0.00158 0.00500 1,2,3-Trimethylbenzene U 0.00158 0.00500 1,3,5-Trimethylbenzene U 0.00200 0.00500 Vinyl chloride U 0.00116 0.00250 Xylenes, Total U 0.000880 0.00650 (S) Toluene-d8 103 75.0-131 (S) 4-Bromofluorobenzene 103 67.0-138 (S) 1,2-Dichloroethane-d4 91.9 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3862572-1 11/17/22 22:48 • (LCSD) R3862572-2 11/17/22 23:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acetone 0.625 1.13 0.699 181 112 10.0-160 J4 J3 47.1 31 Acrylonitrile 0.625 0.911 0.686 146 110 45.0-153 J3 28.2 22 Benzene 0.125 0.129 0.124 103 99.2 70.0-123 3.95 20 Bromobenzene 0.125 0.109 0.119 87.2 95.2 73.0-121 8.77 20 Bromodichloromethane 0.125 0.115 0.113 92.0 90.4 73.0-121 1.75 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 80 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 80 of 96 QUALITY CONTROL SUMMARYWG1961734 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-14,15,16,17,18,19,20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3862572-1 11/17/22 22:48 • (LCSD) R3862572-2 11/17/22 23:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Bromoform 0.125 0.110 0.102 88.0 81.6 64.0-132 7.55 20 Bromomethane 0.125 0.136 0.121 109 96.8 56.0-147 11.7 20 n-Butylbenzene 0.125 0.123 0.113 98.4 90.4 68.0-135 8.47 20 sec-Butylbenzene 0.125 0.106 0.113 84.8 90.4 74.0-130 6.39 20 tert-Butylbenzene 0.125 0.105 0.116 84.0 92.8 75.0-127 9.95 20 Carbon tetrachloride 0.125 0.131 0.126 105 101 66.0-128 3.89 20 Chlorobenzene 0.125 0.119 0.114 95.2 91.2 76.0-128 4.29 20 Chlorodibromomethane 0.125 0.0984 0.0994 78.7 79.5 74.0-127 1.01 20 Chloroethane 0.125 0.156 0.130 125 104 61.0-134 18.2 20 Chloroform 0.125 0.127 0.126 102 101 72.0-123 0.791 20 Chloromethane 0.125 0.125 0.130 100 104 51.0-138 3.92 20 2-Chlorotoluene 0.125 0.107 0.104 85.6 83.2 75.0-124 2.84 20 4-Chlorotoluene 0.125 0.117 0.125 93.6 100 75.0-124 6.61 20 1,2-Dibromo-3-Chloropropane 0.125 0.146 0.118 117 94.4 59.0-130 J3 21.2 20 1,2-Dibromoethane 0.125 0.114 0.110 91.2 88.0 74.0-128 3.57 20 Dibromomethane 0.125 0.136 0.129 109 103 75.0-122 5.28 20 1,2-Dichlorobenzene 0.125 0.127 0.116 102 92.8 76.0-124 9.05 20 1,3-Dichlorobenzene 0.125 0.132 0.120 106 96.0 76.0-125 9.52 20 1,4-Dichlorobenzene 0.125 0.122 0.119 97.6 95.2 77.0-121 2.49 20 Dichlorodifluoromethane 0.125 0.156 0.166 125 133 43.0-156 6.21 20 1,1-Dichloroethane 0.125 0.125 0.126 100 101 70.0-127 0.797 20 1,2-Dichloroethane 0.125 0.124 0.119 99.2 95.2 65.0-131 4.12 20 1,1-Dichloroethene 0.125 0.135 0.135 108 108 65.0-131 0.000 20 cis-1,2-Dichloroethene 0.125 0.126 0.123 101 98.4 73.0-125 2.41 20 trans-1,2-Dichloroethene 0.125 0.129 0.133 103 106 71.0-125 3.05 20 1,2-Dichloropropane 0.125 0.122 0.116 97.6 92.8 74.0-125 5.04 20 1,1-Dichloropropene 0.125 0.129 0.132 103 106 73.0-125 2.30 20 1,3-Dichloropropane 0.125 0.116 0.120 92.8 96.0 80.0-125 3.39 20 cis-1,3-Dichloropropene 0.125 0.119 0.119 95.2 95.2 76.0-127 0.000 20 trans-1,3-Dichloropropene 0.125 0.113 0.115 90.4 92.0 73.0-127 1.75 20 2,2-Dichloropropane 0.125 0.124 0.118 99.2 94.4 59.0-135 4.96 20 Di-isopropyl ether 0.125 0.136 0.133 109 106 60.0-136 2.23 20 Ethylbenzene 0.125 0.121 0.118 96.8 94.4 74.0-126 2.51 20 Hexachloro-1,3-butadiene 0.125 0.138 0.119 110 95.2 57.0-150 14.8 20 Isopropylbenzene 0.125 0.128 0.114 102 91.2 72.0-127 11.6 20 p-Isopropyltoluene 0.125 0.116 0.116 92.8 92.8 72.0-133 0.000 20 2-Butanone (MEK)0.625 0.794 0.632 127 101 30.0-160 22.7 24 Methylene Chloride 0.125 0.127 0.121 102 96.8 68.0-123 4.84 20 4-Methyl-2-pentanone (MIBK)0.625 0.663 0.629 106 101 56.0-143 5.26 20 Methyl tert-butyl ether 0.125 0.127 0.119 102 95.2 66.0-132 6.50 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 81 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 81 of 96 QUALITY CONTROL SUMMARYWG1961734 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-14,15,16,17,18,19,20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3862572-1 11/17/22 22:48 • (LCSD) R3862572-2 11/17/22 23:07 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Naphthalene 0.125 0.158 0.123 126 98.4 59.0-130 J3 24.9 20 n-Propylbenzene 0.125 0.113 0.123 90.4 98.4 74.0-126 8.47 20 Styrene 0.125 0.121 0.109 96.8 87.2 72.0-127 10.4 20 1,1,1,2-Tetrachloroethane 0.125 0.121 0.113 96.8 90.4 74.0-129 6.84 20 1,1,2,2-Tetrachloroethane 0.125 0.0966 0.112 77.3 89.6 68.0-128 14.8 20 1,1,2-Trichlorotrifluoroethane 0.125 0.126 0.120 101 96.0 61.0-139 4.88 20 Tetrachloroethene 0.125 0.117 0.119 93.6 95.2 70.0-136 1.69 20 Toluene 0.125 0.117 0.121 93.6 96.8 75.0-121 3.36 20 1,2,3-Trichlorobenzene 0.125 0.129 0.107 103 85.6 59.0-139 18.6 20 1,2,4-Trichlorobenzene 0.125 0.148 0.112 118 89.6 62.0-137 J3 27.7 20 1,1,1-Trichloroethane 0.125 0.119 0.116 95.2 92.8 69.0-126 2.55 20 1,1,2-Trichloroethane 0.125 0.111 0.110 88.8 88.0 78.0-123 0.905 20 Trichloroethene 0.125 0.133 0.122 106 97.6 76.0-126 8.63 20 Trichlorofluoromethane 0.125 0.124 0.118 99.2 94.4 61.0-142 4.96 20 1,2,3-Trichloropropane 0.125 0.110 0.121 88.0 96.8 67.0-129 9.52 20 1,2,4-Trimethylbenzene 0.125 0.121 0.119 96.8 95.2 70.0-126 1.67 20 1,2,3-Trimethylbenzene 0.125 0.121 0.117 96.8 93.6 74.0-124 3.36 20 1,3,5-Trimethylbenzene 0.125 0.110 0.107 88.0 85.6 73.0-127 2.76 20 Vinyl chloride 0.125 0.122 0.134 97.6 107 63.0-134 9.38 20 Xylenes, Total 0.375 0.367 0.338 97.9 90.1 72.0-127 8.23 20 (S) Toluene-d8 94.3 102 75.0-131 (S) 4-Bromofluorobenzene 108 98.5 67.0-138 (S) 1,2-Dichloroethane-d4 105 107 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 82 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 82 of 96 QUALITY CONTROL SUMMARYWG1963991 Volatile Organic Compounds (GC/MS) by Method 8260D L1557235-01,02,03,04,05,06,07,08,09,10,11,12 Method Blank (MB) (MB) R3864974-3 11/23/22 11:35 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg tert-Butylbenzene U 0.00195 0.00500 n-Propylbenzene U 0.000950 0.00500 Tetrachloroethene U 0.000896 0.00250 (S) Toluene-d8 104 75.0-131 (S) 4-Bromofluorobenzene 104 67.0-138 (S) 1,2-Dichloroethane-d4 78.2 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864974-1 11/23/22 09:44 • (LCSD) R3864974-2 11/23/22 10:03 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% tert-Butylbenzene 0.125 0.131 0.114 105 91.2 75.0-127 13.9 20 n-Propylbenzene 0.125 0.115 0.119 92.0 95.2 74.0-126 3.42 20 Tetrachloroethene 0.125 0.123 0.128 98.4 102 70.0-136 3.98 20 (S) Toluene-d8 100 99.7 75.0-131 (S) 4-Bromofluorobenzene 102 102 67.0-138 (S) 1,2-Dichloroethane-d4 87.6 92.0 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 83 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 83 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3862892-2 11/18/22 14:59 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acenaphthene U 0.00539 0.0333 Acenaphthylene U 0.00469 0.0333 Anthracene U 0.00593 0.0333 Benzidine U 0.0626 1.67 Benzo(a)anthracene U 0.00587 0.0333 Benzo(b)fluoranthene U 0.00621 0.0333 Benzo(k)fluoranthene U 0.00592 0.0333 Benzo(g,h,i)perylene U 0.00609 0.0333 Benzo(a)pyrene U 0.00619 0.0333 Bis(2-chlorethoxy)methane U 0.0100 0.333 Bis(2-chloroethyl)ether U 0.0110 0.333 2,2-Oxybis(1-Chloropropane)U 0.0144 0.333 4-Bromophenyl-phenylether U 0.0117 0.333 2-Chloronaphthalene U 0.00585 0.0333 4-Chlorophenyl-phenylether U 0.0116 0.333 Chrysene U 0.00662 0.0333 Dibenz(a,h)anthracene U 0.00923 0.0333 1,2-Dichlorobenzene U 0.00987 0.333 1,3-Dichlorobenzene U 0.0101 0.333 1,4-Dichlorobenzene U 0.00991 0.333 3,3-Dichlorobenzidine U 0.0123 0.333 2,4-Dinitrotoluene U 0.00955 0.333 2,6-Dinitrotoluene U 0.0109 0.333 Fluoranthene U 0.00601 0.0333 Fluorene U 0.00542 0.0333 Hexachlorobenzene U 0.0118 0.333 Hexachloro-1,3-butadiene U 0.0112 0.333 Hexachlorocyclopentadiene U 0.0175 0.333 Hexachloroethane U 0.0131 0.333 Indeno(1,2,3-cd)pyrene U 0.00941 0.0333 Isophorone U 0.0102 0.333 Naphthalene U 0.00836 0.0333 Nitrobenzene U 0.0116 0.333 n-Nitrosodimethylamine U 0.0494 0.333 n-Nitrosodiphenylamine U 0.0252 0.333 n-Nitrosodi-n-propylamine U 0.0111 0.333 Phenanthrene U 0.00661 0.0333 Benzylbutyl phthalate U 0.0104 0.333 Bis(2-ethylhexyl)phthalate U 0.0422 0.333 Di-n-butyl phthalate U 0.0114 0.333 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 84 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 84 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3862892-2 11/18/22 14:59 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Diethyl phthalate U 0.0110 0.333 Dimethyl phthalate U 0.0706 0.333 Di-n-octyl phthalate U 0.0225 0.333 Pyrene U 0.00648 0.0333 1,2,4-Trichlorobenzene U 0.0104 0.333 4-Chloro-3-methylphenol U 0.0108 0.333 2-Chlorophenol U 0.0110 0.333 2,4-Dichlorophenol U 0.00970 0.333 2,4-Dimethylphenol U 0.00870 0.333 4,6-Dinitro-2-methylphenol U 0.0755 0.333 2,4-Dinitrophenol U 0.0779 0.333 2-Nitrophenol U 0.0119 0.333 4-Nitrophenol U 0.0104 0.333 Pentachlorophenol U 0.00896 0.333 Phenol U 0.0134 0.333 2,4,6-Trichlorophenol U 0.0107 0.333 (S) 2-Fluorophenol 61.0 12.0-120 (S) Phenol-d5 56.2 10.0-120 (S) Nitrobenzene-d5 54.1 10.0-122 (S) 2-Fluorobiphenyl 51.1 15.0-120 (S) 2,4,6-Tribromophenol 54.1 10.0-127 (S) p-Terphenyl-d14 63.1 10.0-120 Laboratory Control Sample (LCS) (LCS) R3862892-1 11/18/22 14:39 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Acenaphthene 0.666 0.539 80.9 38.0-120 Acenaphthylene 0.666 0.541 81.2 40.0-120 Anthracene 0.666 0.536 80.5 42.0-120 Benzidine 1.33 0.198 14.9 10.0-120 Benzo(a)anthracene 0.666 0.576 86.5 44.0-120 Benzo(b)fluoranthene 0.666 0.562 84.4 43.0-120 Benzo(k)fluoranthene 0.666 0.588 88.3 44.0-120 Benzo(g,h,i)perylene 0.666 0.563 84.5 43.0-120 Benzo(a)pyrene 0.666 0.610 91.6 45.0-120 Bis(2-chlorethoxy)methane 0.666 0.414 62.2 20.0-120 Bis(2-chloroethyl)ether 0.666 0.669 100 16.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 85 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 85 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Laboratory Control Sample (LCS) (LCS) R3862892-1 11/18/22 14:39 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2,2-Oxybis(1-Chloropropane)0.666 0.546 82.0 23.0-120 4-Bromophenyl-phenylether 0.666 0.607 91.1 40.0-120 2-Chloronaphthalene 0.666 0.509 76.4 35.0-120 4-Chlorophenyl-phenylether 0.666 0.534 80.2 40.0-120 Chrysene 0.666 0.582 87.4 43.0-120 Dibenz(a,h)anthracene 0.666 0.542 81.4 44.0-120 1,2-Dichlorobenzene 0.666 0.523 78.5 32.0-120 1,3-Dichlorobenzene 0.666 0.513 77.0 30.0-120 1,4-Dichlorobenzene 0.666 0.503 75.5 31.0-120 3,3-Dichlorobenzidine 1.33 0.883 66.4 28.0-120 2,4-Dinitrotoluene 0.666 0.638 95.8 45.0-120 2,6-Dinitrotoluene 0.666 0.613 92.0 42.0-120 Fluoranthene 0.666 0.566 85.0 44.0-120 Fluorene 0.666 0.529 79.4 41.0-120 Hexachlorobenzene 0.666 0.569 85.4 39.0-120 Hexachloro-1,3-butadiene 0.666 0.423 63.5 15.0-120 Hexachlorocyclopentadiene 0.666 0.456 68.5 15.0-120 Hexachloroethane 0.666 0.502 75.4 17.0-120 Indeno(1,2,3-cd)pyrene 0.666 0.502 75.4 45.0-120 Isophorone 0.666 0.408 61.3 23.0-120 Naphthalene 0.666 0.411 61.7 18.0-120 Nitrobenzene 0.666 0.426 64.0 17.0-120 n-Nitrosodimethylamine 0.666 0.517 77.6 10.0-125 n-Nitrosodiphenylamine 0.666 0.477 71.6 40.0-120 n-Nitrosodi-n-propylamine 0.666 0.520 78.1 26.0-120 Phenanthrene 0.666 0.565 84.8 42.0-120 Benzylbutyl phthalate 0.666 0.633 95.0 40.0-120 Bis(2-ethylhexyl)phthalate 0.666 0.634 95.2 41.0-120 Di-n-butyl phthalate 0.666 0.585 87.8 43.0-120 Diethyl phthalate 0.666 0.543 81.5 43.0-120 Dimethyl phthalate 0.666 0.564 84.7 43.0-120 Di-n-octyl phthalate 0.666 0.580 87.1 40.0-120 Pyrene 0.666 0.618 92.8 41.0-120 1,2,4-Trichlorobenzene 0.666 0.414 62.2 17.0-120 4-Chloro-3-methylphenol 0.666 0.463 69.5 28.0-120 2-Chlorophenol 0.666 0.537 80.6 28.0-120 2,4-Dichlorophenol 0.666 0.423 63.5 25.0-120 2,4-Dimethylphenol 0.666 0.426 64.0 15.0-120 4,6-Dinitro-2-methylphenol 0.666 0.598 89.8 16.0-120 2,4-Dinitrophenol 0.666 0.392 58.9 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 86 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 86 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Laboratory Control Sample (LCS) (LCS) R3862892-1 11/18/22 14:39 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2-Nitrophenol 0.666 0.489 73.4 20.0-120 4-Nitrophenol 0.666 0.494 74.2 27.0-120 Pentachlorophenol 0.666 0.477 71.6 29.0-120 Phenol 0.666 0.590 88.6 28.0-120 2,4,6-Trichlorophenol 0.666 0.486 73.0 37.0-120 (S) 2-Fluorophenol 86.5 12.0-120 (S) Phenol-d5 79.9 10.0-120 (S) Nitrobenzene-d5 61.6 10.0-122 (S) 2-Fluorobiphenyl 73.9 15.0-120 (S) 2,4,6-Tribromophenol 94.7 10.0-127 (S) p-Terphenyl-d14 90.1 10.0-120 L1557235-18 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557235-18 11/18/22 17:00 • (MS) R3862892-3 11/18/22 17:21 • (MSD) R3862892-4 11/18/22 17:41 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.857 U 0.439 0.447 51.2 51.7 1 18.0-120 1.76 32 Acenaphthylene 0.857 U 0.448 0.452 52.3 52.3 1 25.0-120 0.868 32 Anthracene 0.857 U 0.418 0.425 48.8 49.1 1 22.0-120 1.55 29 Benzidine 1.72 U U U 0.000 0.000 1 10.0-120 J6 J6 0.000 40 Benzo(a)anthracene 0.857 U 0.442 0.460 51.5 53.2 1 25.0-120 4.05 29 Benzo(b)fluoranthene 0.857 U 0.431 0.438 50.3 50.6 1 19.0-122 1.50 31 Benzo(k)fluoranthene 0.857 U 0.422 0.450 49.2 52.0 1 23.0-120 6.28 30 Benzo(g,h,i)perylene 0.857 U 0.422 0.433 49.2 50.0 1 10.0-120 2.44 33 Benzo(a)pyrene 0.857 U 0.456 0.474 53.2 54.8 1 24.0-120 3.92 30 Bis(2-chlorethoxy)methane 0.857 U 0.352 0.354 41.0 41.0 1 10.0-120 0.738 34 Bis(2-chloroethyl)ether 0.857 U 0.455 0.453 53.0 52.4 1 10.0-120 0.287 40 2,2-Oxybis(1-Chloropropane)0.857 U 0.442 0.443 51.5 51.2 1 10.0-120 0.295 40 4-Bromophenyl-phenylether 0.857 U 0.469 0.481 54.7 55.6 1 27.0-120 2.47 30 2-Chloronaphthalene 0.857 U 0.417 0.426 48.6 49.2 1 20.0-120 2.16 32 4-Chlorophenyl-phenylether 0.857 U 0.437 0.450 50.9 52.0 1 24.0-120 2.94 29 Chrysene 0.857 U 0.443 0.459 51.7 53.0 1 21.0-120 3.47 29 Dibenz(a,h)anthracene 0.857 U 0.403 0.420 47.0 48.5 1 10.0-120 4.12 32 1,2-Dichlorobenzene 0.857 U 0.425 0.425 49.5 49.1 1 10.0-120 0.000 38 1,3-Dichlorobenzene 0.857 U 0.416 0.413 48.5 47.7 1 10.0-120 0.629 40 1,4-Dichlorobenzene 0.857 U 0.414 0.416 48.3 48.0 1 10.0-120 0.314 39 3,3-Dichlorobenzidine 1.72 U 0.551 0.566 32.0 32.6 1 10.0-120 2.57 34 2,4-Dinitrotoluene 0.857 U 0.564 0.577 65.8 66.7 1 30.0-120 2.28 31 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 87 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 87 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 L1557235-18 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557235-18 11/18/22 17:00 • (MS) R3862892-3 11/18/22 17:21 • (MSD) R3862892-4 11/18/22 17:41 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% 2,6-Dinitrotoluene 0.857 U 0.493 0.515 57.4 59.5 1 25.0-120 4.40 31 Fluoranthene 0.857 U 0.443 0.453 51.7 52.4 1 18.0-126 2.33 32 Fluorene 0.857 U 0.431 0.440 50.3 50.9 1 25.0-120 2.09 30 Hexachlorobenzene 0.857 U 0.444 0.460 51.8 53.2 1 27.0-120 3.46 28 Hexachloro-1,3-butadiene 0.857 U 0.367 0.373 42.9 43.1 1 10.0-120 1.41 38 Hexachlorocyclopentadiene 0.857 U 0.383 0.408 44.7 47.1 1 10.0-120 6.26 40 Hexachloroethane 0.857 U 0.412 0.418 48.0 48.3 1 10.0-120 1.57 40 Indeno(1,2,3-cd)pyrene 0.857 U 0.377 0.395 43.9 45.6 1 10.0-120 4.73 32 Isophorone 0.857 U 0.353 0.348 41.2 40.2 1 13.0-120 1.49 34 Naphthalene 0.857 U 0.352 0.356 41.0 41.1 1 10.0-120 1.10 35 Nitrobenzene 0.857 U 0.370 0.370 43.2 42.8 1 10.0-120 0.000 36 n-Nitrosodimethylamine 0.857 U 0.413 0.367 48.2 42.5 1 10.0-127 11.7 40 n-Nitrosodiphenylamine 0.857 U 0.374 0.383 43.6 44.3 1 17.0-120 2.41 29 n-Nitrosodi-n-propylamine 0.857 U 0.429 0.437 50.0 50.5 1 10.0-120 1.81 37 Phenanthrene 0.857 U 0.440 0.459 51.4 53.0 1 17.0-120 4.06 31 Benzylbutyl phthalate 0.857 U 0.504 0.529 58.8 61.1 1 23.0-120 4.79 30 Bis(2-ethylhexyl)phthalate 0.857 U 0.495 0.521 57.8 60.2 1 17.0-126 5.13 30 Di-n-butyl phthalate 0.857 U 0.451 0.472 52.6 54.5 1 30.0-120 4.52 29 Diethyl phthalate 0.857 U 0.442 0.455 51.5 52.6 1 26.0-120 2.91 28 Dimethyl phthalate 0.857 U 0.467 0.468 54.4 54.1 1 25.0-120 0.279 29 Di-n-octyl phthalate 0.857 U 0.485 0.504 56.5 58.3 1 21.0-123 3.95 29 Pyrene 0.857 U 0.468 0.490 54.6 56.6 1 16.0-121 4.63 32 1,2,4-Trichlorobenzene 0.857 U 0.356 0.354 41.5 41.0 1 12.0-120 0.367 37 4-Chloro-3-methylphenol 0.857 U 0.396 0.405 46.2 46.8 1 15.0-120 2.28 30 2-Chlorophenol 0.857 U 0.452 0.452 52.7 52.3 1 15.0-120 0.000 37 2,4-Dichlorophenol 0.857 U 0.378 0.384 44.1 44.4 1 20.0-120 1.71 31 2,4-Dimethylphenol 0.857 U 0.378 0.388 44.1 44.9 1 10.0-120 2.72 33 4,6-Dinitro-2-methylphenol 0.857 U 0.667 0.687 77.8 79.4 1 10.0-120 2.89 39 2,4-Dinitrophenol 0.857 U 0.691 0.713 80.5 82.4 1 10.0-121 3.16 40 2-Nitrophenol 0.857 U 0.439 0.452 51.2 52.3 1 12.0-120 2.92 39 4-Nitrophenol 0.857 U 0.468 0.474 54.6 54.8 1 10.0-137 1.38 32 Pentachlorophenol 0.857 U 0.508 0.543 59.3 62.8 1 10.0-160 6.69 31 Phenol 0.857 U 0.467 0.467 54.4 53.9 1 12.0-120 0.000 38 2,4,6-Trichlorophenol 0.857 U 0.427 0.439 49.8 50.8 1 19.0-120 2.71 32 (S) 2-Fluorophenol 56.2 56.3 12.0-120 (S) Phenol-d5 52.0 52.6 10.0-120 (S) Nitrobenzene-d5 41.3 42.5 10.0-122 (S) 2-Fluorobiphenyl 46.5 47.6 15.0-120 (S) 2,4,6-Tribromophenol 62.8 63.9 10.0-127 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 88 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 88 of 96 QUALITY CONTROL SUMMARYWG1960983 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1557235-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 L1557235-18 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557235-18 11/18/22 17:00 • (MS) R3862892-3 11/18/22 17:21 • (MSD) R3862892-4 11/18/22 17:41 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% (S) p-Terphenyl-d14 53.5 56.3 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 89 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 89 of 96 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions (dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. MDL (dry)Method Detection Limit. RDL Reported Detection Limit. RDL (dry)Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptable. C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Data is likely to show a low bias concerning the result. C5 The reported concentration is an estimate. The continuing calibration standard associated with this data responded high.Data is likely to show a high bias concerning the result. E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 90 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 90 of 96 GLOSSARY OF TERMS Qualifier Description J4 The associated batch QC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 91 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 91 of 96 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:05 92 of 96 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1557235 11/30/22 10:48 92 of 96 ANALYTICAL REPORT December 01, 2022 EAS Professionals, Inc. Sample Delivery Group:L1558771 Samples Received:11/16/2022 Project Number:EAS-225234 Description:450 Polo Road Report To:Derek Ross 9 Pilgrim Road Greenville, SC 29607 Entire Report Reviewed By: December 01, 2022 [Preliminary Report] Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 1 of 70 December 01, 2022 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 1 of 70 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 6 Sr: Sample Results 7 CS-1 L1558771-01 7 CS-2 L1558771-02 10 CS-3 L1558771-03 13 CS-4 L1558771-04 16 CS-4-A L1558771-05 19 CS-5 L1558771-06 22 CS-5 (DUP) L1558771-07 25 CS-6 L1558771-08 28 CS-6-A L1558771-09 31 CS-7 L1558771-10 34 CS-8 L1558771-11 37 Qc: Quality Control Summary 40 Total Solids by Method 2540 G-2011 40 Mercury by Method 7471B 42 Metals (ICPMS) by Method 6020B 43 Volatile Organic Compounds (GC/MS) by Method 8260D 46 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 54 Gl: Glossary of Terms 66 Al: Accreditations & Locations 68 Sc: Sample Chain of Custody 69 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 2 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 2 of 70 SAMPLE SUMMARY Collected by Collected date/time Received date/time CS-1 L1558771-01 Solid Westley Godfrey 11/14/22 12:00 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961475 1 11/18/22 10:18 11/18/22 10:32 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 14:57 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961902 5 11/23/22 13:53 11/25/22 14:10 JPD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962259 1.25 11/14/22 12:00 11/19/22 10:26 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962624 1 11/21/22 09:14 11/22/22 13:42 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-2 L1558771-02 Solid Westley Godfrey 11/14/22 12:15 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961475 1 11/18/22 10:18 11/18/22 10:32 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 14:59 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961902 5 11/23/22 13:53 11/25/22 14:13 JPD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1.02 11/14/22 12:15 11/19/22 12:37 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 10:39 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-3 L1558771-03 Solid Westley Godfrey 11/14/22 12:20 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961475 1 11/18/22 10:18 11/18/22 10:32 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:01 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1961902 5 11/23/22 13:53 11/25/22 14:17 JPD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1.03 11/14/22 12:20 11/19/22 12:56 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 11:39 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-4 L1558771-04 Solid Westley Godfrey 11/14/22 14:45 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:03 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 18:50 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 14:45 11/19/22 13:15 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 11:19 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-4-A L1558771-05 Solid Westley Godfrey 11/14/22 14:45 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:05 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1963015 5 11/28/22 09:37 11/28/22 17:31 JPD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 14:45 11/19/22 13:34 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 10:19 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 3 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 3 of 70 SAMPLE SUMMARY Collected by Collected date/time Received date/time CS-5 L1558771-06 Solid Westley Godfrey 11/14/22 13:00 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:07 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 18:53 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1.07 11/14/22 13:00 11/19/22 13:54 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 10 11/24/22 16:00 11/26/22 17:06 JRM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 2 11/24/22 16:00 11/25/22 14:01 ADF Mt. Juliet, TN Collected by Collected date/time Received date/time CS-5 (DUP) L1558771-07 Solid Westley Godfrey 11/14/22 13:00 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:09 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 18:56 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 13:00 11/19/22 14:12 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 2 11/24/22 16:00 11/25/22 14:21 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-6 L1558771-08 Solid Westley Godfrey 11/14/22 13:15 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:15 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 19:09 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 13:15 11/19/22 14:32 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 2 11/24/22 16:00 11/25/22 12:40 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-6-A L1558771-09 Solid Westley Godfrey 11/14/22 13:15 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:17 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 19:12 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 13:15 11/19/22 14:51 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 2 11/24/22 16:00 11/25/22 13:41 JRM Mt. Juliet, TN Collected by Collected date/time Received date/time CS-7 L1558771-10 Solid Westley Godfrey 11/14/22 12:30 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:19 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 19:15 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 12:30 11/19/22 15:10 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 10:59 JRM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 4 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 4 of 70 SAMPLE SUMMARY Collected by Collected date/time Received date/time CS-8 L1558771-11 Solid Westley Godfrey 11/14/22 13:35 11/16/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Total Solids by Method 2540 G-2011 WG1961476 1 11/18/22 12:38 11/18/22 12:52 KDW Mt. Juliet, TN Mercury by Method 7471B WG1961812 1 11/20/22 09:32 11/21/22 15:21 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1962098 5 11/30/22 16:36 12/01/22 19:19 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1962462 1 11/14/22 13:35 11/19/22 15:29 JHH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1962878 1 11/24/22 16:00 11/25/22 09:58 ADF Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 5 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 5 of 70 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Heather J Wagner Project Manager 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 6 of 70 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 6 of 70 SAMPLE RESULTS - 01 L1558771 CS-1 Collected date/time: 11/14/22 12:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 68.9 1 11/18/2022 10:32 WG1961475 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0589 0.0261 0.0581 1 11/21/2022 14:57 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 6.26 0.145 1.45 5 11/25/2022 14:10 WG1961902 Barium 48.7 0.221 3.63 5 11/25/2022 14:10 WG1961902 Cadmium 0.962 J 0.124 1.45 5 11/25/2022 14:10 WG1961902 Chromium 78.4 0.430 7.26 5 11/25/2022 14:10 WG1961902 Lead 94.8 0.144 2.90 5 11/25/2022 14:10 WG1961902 Selenium 0.986 J 0.261 3.63 5 11/25/2022 14:10 WG1961902 Silver U 0.126 0.726 5 11/25/2022 14:10 WG1961902 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0827 0.113 1.25 11/19/2022 10:26 WG1962259 Acrylonitrile U 0.00818 0.0283 1.25 11/19/2022 10:26 WG1962259 Benzene 0.00296 0.00106 0.00227 1.25 11/19/2022 10:26 WG1962259 Bromobenzene U 0.00205 0.0283 1.25 11/19/2022 10:26 WG1962259 Bromodichloromethane U J4 0.00164 0.00568 1.25 11/19/2022 10:26 WG1962259 Bromoform U 0.00265 0.0568 1.25 11/19/2022 10:26 WG1962259 Bromomethane U 0.00446 0.0283 1.25 11/19/2022 10:26 WG1962259 n-Butylbenzene U 0.0119 0.0283 1.25 11/19/2022 10:26 WG1962259 sec-Butylbenzene U J4 0.00653 0.0283 1.25 11/19/2022 10:26 WG1962259 tert-Butylbenzene U 0.00443 0.0113 1.25 11/19/2022 10:26 WG1962259 Carbon tetrachloride U 0.00203 0.0113 1.25 11/19/2022 10:26 WG1962259 Chlorobenzene U 0.000477 0.00568 1.25 11/19/2022 10:26 WG1962259 Chlorodibromomethane U 0.00139 0.00568 1.25 11/19/2022 10:26 WG1962259 Chloroethane U 0.00385 0.0113 1.25 11/19/2022 10:26 WG1962259 Chloroform 0.00760 0.00234 0.00568 1.25 11/19/2022 10:26 WG1962259 Chloromethane U 0.00987 0.0283 1.25 11/19/2022 10:26 WG1962259 2-Chlorotoluene U 0.00196 0.00568 1.25 11/19/2022 10:26 WG1962259 4-Chlorotoluene U J4 0.00102 0.0113 1.25 11/19/2022 10:26 WG1962259 1,2-Dibromo-3-Chloropropane U 0.00885 0.0568 1.25 11/19/2022 10:26 WG1962259 1,2-Dibromoethane U 0.00147 0.00568 1.25 11/19/2022 10:26 WG1962259 Dibromomethane U J4 0.00170 0.0113 1.25 11/19/2022 10:26 WG1962259 1,2-Dichlorobenzene U 0.000963 0.0113 1.25 11/19/2022 10:26 WG1962259 1,3-Dichlorobenzene U 0.00136 0.0113 1.25 11/19/2022 10:26 WG1962259 1,4-Dichlorobenzene 0.00221 B J 0.00159 0.0113 1.25 11/19/2022 10:26 WG1962259 Dichlorodifluoromethane U 0.00365 0.00568 1.25 11/19/2022 10:26 WG1962259 1,1-Dichloroethane U 0.00111 0.00568 1.25 11/19/2022 10:26 WG1962259 1,2-Dichloroethane U 0.00147 0.00568 1.25 11/19/2022 10:26 WG1962259 1,1-Dichloroethene U 0.00137 0.00568 1.25 11/19/2022 10:26 WG1962259 cis-1,2-Dichloroethene U 0.00167 0.00568 1.25 11/19/2022 10:26 WG1962259 trans-1,2-Dichloroethene U 0.00236 0.0113 1.25 11/19/2022 10:26 WG1962259 1,2-Dichloropropane U 0.00323 0.0113 1.25 11/19/2022 10:26 WG1962259 1,1-Dichloropropene U 0.00183 0.00568 1.25 11/19/2022 10:26 WG1962259 1,3-Dichloropropane U 0.00114 0.0113 1.25 11/19/2022 10:26 WG1962259 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 7 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 7 of 70 SAMPLE RESULTS - 01 L1558771 CS-1 Collected date/time: 11/14/22 12:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00172 0.00568 1.25 11/19/2022 10:26 WG1962259 trans-1,3-Dichloropropene U 0.00259 0.0113 1.25 11/19/2022 10:26 WG1962259 2,2-Dichloropropane U 0.00314 0.00568 1.25 11/19/2022 10:26 WG1962259 Di-isopropyl ether U 0.000931 0.00227 1.25 11/19/2022 10:26 WG1962259 Ethylbenzene U 0.00167 0.00568 1.25 11/19/2022 10:26 WG1962259 Hexachloro-1,3-butadiene U 0.0136 0.0568 1.25 11/19/2022 10:26 WG1962259 Isopropylbenzene 0.00113 B J J4 0.000963 0.00568 1.25 11/19/2022 10:26 WG1962259 p-Isopropyltoluene 0.0170 0.00579 0.0113 1.25 11/19/2022 10:26 WG1962259 2-Butanone (MEK)U 0.144 0.227 1.25 11/19/2022 10:26 WG1962259 Methylene Chloride U 0.0151 0.0568 1.25 11/19/2022 10:26 WG1962259 4-Methyl-2-pentanone (MIBK)U 0.00517 0.0568 1.25 11/19/2022 10:26 WG1962259 Methyl tert-butyl ether U 0.000795 0.00227 1.25 11/19/2022 10:26 WG1962259 Naphthalene U 0.0111 0.0283 1.25 11/19/2022 10:26 WG1962259 n-Propylbenzene U J4 0.00216 0.0113 1.25 11/19/2022 10:26 WG1962259 Styrene 0.00192 B J 0.000519 0.0283 1.25 11/19/2022 10:26 WG1962259 1,1,1,2-Tetrachloroethane U 0.00216 0.00568 1.25 11/19/2022 10:26 WG1962259 1,1,2,2-Tetrachloroethane U 0.00158 0.00568 1.25 11/19/2022 10:26 WG1962259 1,1,2-Trichlorotrifluoroethane U 0.00171 0.00568 1.25 11/19/2022 10:26 WG1962259 Tetrachloroethene U 0.00203 0.00568 1.25 11/19/2022 10:26 WG1962259 Toluene 0.0229 0.00296 0.0113 1.25 11/19/2022 10:26 WG1962259 1,2,3-Trichlorobenzene U C4 0.0166 0.0283 1.25 11/19/2022 10:26 WG1962259 1,2,4-Trichlorobenzene U 0.00998 0.0283 1.25 11/19/2022 10:26 WG1962259 1,1,1-Trichloroethane U J4 0.00209 0.00568 1.25 11/19/2022 10:26 WG1962259 1,1,2-Trichloroethane U 0.00135 0.00568 1.25 11/19/2022 10:26 WG1962259 Trichloroethene U 0.00132 0.00227 1.25 11/19/2022 10:26 WG1962259 Trichlorofluoromethane U 0.00187 0.00568 1.25 11/19/2022 10:26 WG1962259 1,2,3-Trichloropropane U 0.00366 0.0283 1.25 11/19/2022 10:26 WG1962259 1,2,4-Trimethylbenzene 0.00403 J 0.00359 0.0113 1.25 11/19/2022 10:26 WG1962259 1,2,3-Trimethylbenzene U 0.00359 0.0113 1.25 11/19/2022 10:26 WG1962259 1,3,5-Trimethylbenzene U J4 0.00454 0.0113 1.25 11/19/2022 10:26 WG1962259 Vinyl chloride U 0.00263 0.00568 1.25 11/19/2022 10:26 WG1962259 Xylenes, Total 0.0158 0.00200 0.0147 1.25 11/19/2022 10:26 WG1962259 (S) Toluene-d8 111 75.0-131 11/19/2022 10:26 WG1962259 (S) 4-Bromofluorobenzene 99.0 67.0-138 11/19/2022 10:26 WG1962259 (S) 1,2-Dichloroethane-d4 89.9 70.0-130 11/19/2022 10:26 WG1962259 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00783 0.0483 1 11/22/2022 13:42 WG1962624 Acenaphthylene U 0.00681 0.0483 1 11/22/2022 13:42 WG1962624 Anthracene U 0.00861 0.0483 1 11/22/2022 13:42 WG1962624 Benzidine U C3 0.0909 2.42 1 11/22/2022 13:42 WG1962624 Benzo(a)anthracene 0.00894 J 0.00852 0.0483 1 11/22/2022 13:42 WG1962624 Benzo(b)fluoranthene 0.0170 J 0.00902 0.0483 1 11/22/2022 13:42 WG1962624 Benzo(k)fluoranthene U 0.00859 0.0483 1 11/22/2022 13:42 WG1962624 Benzo(g,h,i)perylene U 0.00884 0.0483 1 11/22/2022 13:42 WG1962624 Benzo(a)pyrene 0.00968 J 0.00899 0.0483 1 11/22/2022 13:42 WG1962624 Bis(2-chlorethoxy)methane U 0.0145 0.483 1 11/22/2022 13:42 WG1962624 Bis(2-chloroethyl)ether U 0.0160 0.483 1 11/22/2022 13:42 WG1962624 2,2-Oxybis(1-Chloropropane)U 0.0209 0.483 1 11/22/2022 13:42 WG1962624 4-Bromophenyl-phenylether U 0.0170 0.483 1 11/22/2022 13:42 WG1962624 2-Chloronaphthalene U 0.00849 0.0483 1 11/22/2022 13:42 WG1962624 4-Chlorophenyl-phenylether U 0.0168 0.483 1 11/22/2022 13:42 WG1962624 Chrysene U 0.00961 0.0483 1 11/22/2022 13:42 WG1962624 Dibenz(a,h)anthracene U 0.0134 0.0483 1 11/22/2022 13:42 WG1962624 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 8 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 8 of 70 SAMPLE RESULTS - 01 L1558771 CS-1 Collected date/time: 11/14/22 12:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0143 0.483 1 11/22/2022 13:42 WG1962624 1,3-Dichlorobenzene U 0.0147 0.483 1 11/22/2022 13:42 WG1962624 1,4-Dichlorobenzene U 0.0144 0.483 1 11/22/2022 13:42 WG1962624 3,3-Dichlorobenzidine U 0.0179 0.483 1 11/22/2022 13:42 WG1962624 2,4-Dinitrotoluene U 0.0139 0.483 1 11/22/2022 13:42 WG1962624 2,6-Dinitrotoluene U 0.0158 0.483 1 11/22/2022 13:42 WG1962624 Fluoranthene 0.0190 J 0.00873 0.0483 1 11/22/2022 13:42 WG1962624 Fluorene U 0.00787 0.0483 1 11/22/2022 13:42 WG1962624 Hexachlorobenzene U 0.0171 0.483 1 11/22/2022 13:42 WG1962624 Hexachloro-1,3-butadiene U 0.0163 0.483 1 11/22/2022 13:42 WG1962624 Hexachlorocyclopentadiene U 0.0254 0.483 1 11/22/2022 13:42 WG1962624 Hexachloroethane U 0.0190 0.483 1 11/22/2022 13:42 WG1962624 Indeno(1,2,3-cd)pyrene U 0.0137 0.0483 1 11/22/2022 13:42 WG1962624 Isophorone U 0.0148 0.483 1 11/22/2022 13:42 WG1962624 Naphthalene U 0.0121 0.0483 1 11/22/2022 13:42 WG1962624 Nitrobenzene U 0.0168 0.483 1 11/22/2022 13:42 WG1962624 n-Nitrosodimethylamine U C3 0.0717 0.483 1 11/22/2022 13:42 WG1962624 n-Nitrosodiphenylamine U 0.0366 0.483 1 11/22/2022 13:42 WG1962624 n-Nitrosodi-n-propylamine U 0.0161 0.483 1 11/22/2022 13:42 WG1962624 Phenanthrene 0.0132 J 0.00960 0.0483 1 11/22/2022 13:42 WG1962624 Benzylbutyl phthalate U 0.0151 0.483 1 11/22/2022 13:42 WG1962624 Bis(2-ethylhexyl)phthalate U 0.0613 0.483 1 11/22/2022 13:42 WG1962624 Di-n-butyl phthalate 0.0189 J 0.0166 0.483 1 11/22/2022 13:42 WG1962624 Diethyl phthalate U 0.0160 0.483 1 11/22/2022 13:42 WG1962624 Dimethyl phthalate U 0.103 0.483 1 11/22/2022 13:42 WG1962624 Di-n-octyl phthalate U 0.0327 0.483 1 11/22/2022 13:42 WG1962624 Pyrene 0.0179 J 0.00941 0.0483 1 11/22/2022 13:42 WG1962624 1,2,4-Trichlorobenzene U 0.0151 0.483 1 11/22/2022 13:42 WG1962624 4-Chloro-3-methylphenol U 0.0157 0.483 1 11/22/2022 13:42 WG1962624 2-Chlorophenol U 0.0160 0.483 1 11/22/2022 13:42 WG1962624 2,4-Dichlorophenol U 0.0141 0.483 1 11/22/2022 13:42 WG1962624 2,4-Dimethylphenol U C3 0.0126 0.483 1 11/22/2022 13:42 WG1962624 4,6-Dinitro-2-methylphenol U 0.110 0.483 1 11/22/2022 13:42 WG1962624 2,4-Dinitrophenol U 0.113 0.483 1 11/22/2022 13:42 WG1962624 2-Nitrophenol U 0.0173 0.483 1 11/22/2022 13:42 WG1962624 4-Nitrophenol U 0.0151 0.483 1 11/22/2022 13:42 WG1962624 Pentachlorophenol U 0.0130 0.483 1 11/22/2022 13:42 WG1962624 Phenol U 0.0195 0.483 1 11/22/2022 13:42 WG1962624 2,4,6-Trichlorophenol U 0.0155 0.483 1 11/22/2022 13:42 WG1962624 (S) 2-Fluorophenol 64.8 12.0-120 11/22/2022 13:42 WG1962624 (S) Phenol-d5 60.1 10.0-120 11/22/2022 13:42 WG1962624 (S) Nitrobenzene-d5 54.3 10.0-122 11/22/2022 13:42 WG1962624 (S) 2-Fluorobiphenyl 57.0 15.0-120 11/22/2022 13:42 WG1962624 (S) 2,4,6-Tribromophenol 72.0 10.0-127 11/22/2022 13:42 WG1962624 (S) p-Terphenyl-d14 62.2 10.0-120 11/22/2022 13:42 WG1962624 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 9 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 9 of 70 SAMPLE RESULTS - 02 L1558771 CS-2 Collected date/time: 11/14/22 12:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 79.5 1 11/18/2022 10:32 WG1961475 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0364 J 0.0226 0.0503 1 11/21/2022 14:59 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.54 0.126 1.26 5 11/25/2022 14:13 WG1961902 Barium 27.5 0.191 3.14 5 11/25/2022 14:13 WG1961902 Cadmium U 0.108 1.26 5 11/25/2022 14:13 WG1961902 Chromium 12.4 0.372 6.29 5 11/25/2022 14:13 WG1961902 Lead 11.0 0.124 2.51 5 11/25/2022 14:13 WG1961902 Selenium 0.774 J 0.226 3.14 5 11/25/2022 14:13 WG1961902 Silver U 0.109 0.629 5 11/25/2022 14:13 WG1961902 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0562 0.0770 1.02 11/19/2022 12:37 WG1962462 Acrylonitrile U 0.00556 0.0193 1.02 11/19/2022 12:37 WG1962462 Benzene U 0.000719 0.00154 1.02 11/19/2022 12:37 WG1962462 Bromobenzene U 0.00139 0.0193 1.02 11/19/2022 12:37 WG1962462 Bromodichloromethane U 0.00112 0.00385 1.02 11/19/2022 12:37 WG1962462 Bromoform U 0.00180 0.0385 1.02 11/19/2022 12:37 WG1962462 Bromomethane U C3 0.00303 0.0193 1.02 11/19/2022 12:37 WG1962462 n-Butylbenzene U 0.00808 0.0193 1.02 11/19/2022 12:37 WG1962462 sec-Butylbenzene U 0.00444 0.0193 1.02 11/19/2022 12:37 WG1962462 tert-Butylbenzene U 0.00300 0.00770 1.02 11/19/2022 12:37 WG1962462 Carbon tetrachloride U 0.00138 0.00770 1.02 11/19/2022 12:37 WG1962462 Chlorobenzene U 0.000323 0.00385 1.02 11/19/2022 12:37 WG1962462 Chlorodibromomethane U 0.000942 0.00385 1.02 11/19/2022 12:37 WG1962462 Chloroethane U C3 J4 0.00261 0.00770 1.02 11/19/2022 12:37 WG1962462 Chloroform 0.00400 0.00159 0.00385 1.02 11/19/2022 12:37 WG1962462 Chloromethane U C3 0.00670 0.0193 1.02 11/19/2022 12:37 WG1962462 2-Chlorotoluene U 0.00133 0.00385 1.02 11/19/2022 12:37 WG1962462 4-Chlorotoluene U 0.000693 0.00770 1.02 11/19/2022 12:37 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00601 0.0385 1.02 11/19/2022 12:37 WG1962462 1,2-Dibromoethane U 0.000998 0.00385 1.02 11/19/2022 12:37 WG1962462 Dibromomethane U 0.00116 0.00770 1.02 11/19/2022 12:37 WG1962462 1,2-Dichlorobenzene U 0.000654 0.00770 1.02 11/19/2022 12:37 WG1962462 1,3-Dichlorobenzene U 0.000924 0.00770 1.02 11/19/2022 12:37 WG1962462 1,4-Dichlorobenzene U 0.00108 0.00770 1.02 11/19/2022 12:37 WG1962462 Dichlorodifluoromethane U C3 0.00248 0.00385 1.02 11/19/2022 12:37 WG1962462 1,1-Dichloroethane U 0.000756 0.00385 1.02 11/19/2022 12:37 WG1962462 1,2-Dichloroethane U 0.00100 0.00385 1.02 11/19/2022 12:37 WG1962462 1,1-Dichloroethene U 0.000933 0.00385 1.02 11/19/2022 12:37 WG1962462 cis-1,2-Dichloroethene U 0.00113 0.00385 1.02 11/19/2022 12:37 WG1962462 trans-1,2-Dichloroethene U 0.00160 0.00770 1.02 11/19/2022 12:37 WG1962462 1,2-Dichloropropane U 0.00219 0.00770 1.02 11/19/2022 12:37 WG1962462 1,1-Dichloropropene U 0.00125 0.00385 1.02 11/19/2022 12:37 WG1962462 1,3-Dichloropropane U 0.000772 0.00770 1.02 11/19/2022 12:37 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 10 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 10 of 70 SAMPLE RESULTS - 02 L1558771 CS-2 Collected date/time: 11/14/22 12:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00117 0.00385 1.02 11/19/2022 12:37 WG1962462 trans-1,3-Dichloropropene U 0.00175 0.00770 1.02 11/19/2022 12:37 WG1962462 2,2-Dichloropropane U C3 0.00213 0.00385 1.02 11/19/2022 12:37 WG1962462 Di-isopropyl ether U 0.000631 0.00154 1.02 11/19/2022 12:37 WG1962462 Ethylbenzene U 0.00114 0.00385 1.02 11/19/2022 12:37 WG1962462 Hexachloro-1,3-butadiene U 0.00924 0.0385 1.02 11/19/2022 12:37 WG1962462 Isopropylbenzene U 0.000654 0.00385 1.02 11/19/2022 12:37 WG1962462 p-Isopropyltoluene U 0.00393 0.00770 1.02 11/19/2022 12:37 WG1962462 2-Butanone (MEK)U 0.0978 0.154 1.02 11/19/2022 12:37 WG1962462 Methylene Chloride U 0.0102 0.0385 1.02 11/19/2022 12:37 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00352 0.0385 1.02 11/19/2022 12:37 WG1962462 Methyl tert-butyl ether U 0.000539 0.00154 1.02 11/19/2022 12:37 WG1962462 Naphthalene U 0.00752 0.0193 1.02 11/19/2022 12:37 WG1962462 n-Propylbenzene U 0.00146 0.00770 1.02 11/19/2022 12:37 WG1962462 Styrene U 0.000353 0.0193 1.02 11/19/2022 12:37 WG1962462 1,1,1,2-Tetrachloroethane U 0.00146 0.00385 1.02 11/19/2022 12:37 WG1962462 1,1,2,2-Tetrachloroethane U 0.00107 0.00385 1.02 11/19/2022 12:37 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00116 0.00385 1.02 11/19/2022 12:37 WG1962462 Tetrachloroethene U 0.00138 0.00385 1.02 11/19/2022 12:37 WG1962462 Toluene U 0.00201 0.00770 1.02 11/19/2022 12:37 WG1962462 1,2,3-Trichlorobenzene U 0.0113 0.0193 1.02 11/19/2022 12:37 WG1962462 1,2,4-Trichlorobenzene U J4 0.00678 0.0193 1.02 11/19/2022 12:37 WG1962462 1,1,1-Trichloroethane U 0.00142 0.00385 1.02 11/19/2022 12:37 WG1962462 1,1,2-Trichloroethane U 0.000920 0.00385 1.02 11/19/2022 12:37 WG1962462 Trichloroethene U 0.000900 0.00154 1.02 11/19/2022 12:37 WG1962462 Trichlorofluoromethane U C3 0.00127 0.00385 1.02 11/19/2022 12:37 WG1962462 1,2,3-Trichloropropane U 0.00249 0.0193 1.02 11/19/2022 12:37 WG1962462 1,2,4-Trimethylbenzene U 0.00243 0.00770 1.02 11/19/2022 12:37 WG1962462 1,2,3-Trimethylbenzene U 0.00243 0.00770 1.02 11/19/2022 12:37 WG1962462 1,3,5-Trimethylbenzene U 0.00308 0.00770 1.02 11/19/2022 12:37 WG1962462 Vinyl chloride U C3 J4 0.00178 0.00385 1.02 11/19/2022 12:37 WG1962462 Xylenes, Total 0.00139 J 0.00136 0.0100 1.02 11/19/2022 12:37 WG1962462 (S) Toluene-d8 101 75.0-131 11/19/2022 12:37 WG1962462 (S) 4-Bromofluorobenzene 106 67.0-138 11/19/2022 12:37 WG1962462 (S) 1,2-Dichloroethane-d4 86.3 70.0-130 11/19/2022 12:37 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00678 0.0419 1 11/25/2022 10:39 WG1962878 Acenaphthylene U 0.00590 0.0419 1 11/25/2022 10:39 WG1962878 Anthracene U 0.00746 0.0419 1 11/25/2022 10:39 WG1962878 Benzidine U 0.0787 2.10 1 11/25/2022 10:39 WG1962878 Benzo(a)anthracene 0.00951 J 0.00738 0.0419 1 11/25/2022 10:39 WG1962878 Benzo(b)fluoranthene 0.0184 J 0.00781 0.0419 1 11/25/2022 10:39 WG1962878 Benzo(k)fluoranthene U 0.00744 0.0419 1 11/25/2022 10:39 WG1962878 Benzo(g,h,i)perylene U 0.00766 0.0419 1 11/25/2022 10:39 WG1962878 Benzo(a)pyrene 0.0136 J 0.00778 0.0419 1 11/25/2022 10:39 WG1962878 Bis(2-chlorethoxy)methane U 0.0126 0.419 1 11/25/2022 10:39 WG1962878 Bis(2-chloroethyl)ether U 0.0138 0.419 1 11/25/2022 10:39 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0181 0.419 1 11/25/2022 10:39 WG1962878 4-Bromophenyl-phenylether U 0.0147 0.419 1 11/25/2022 10:39 WG1962878 2-Chloronaphthalene U 0.00736 0.0419 1 11/25/2022 10:39 WG1962878 4-Chlorophenyl-phenylether U 0.0146 0.419 1 11/25/2022 10:39 WG1962878 Chrysene 0.0110 J 0.00832 0.0419 1 11/25/2022 10:39 WG1962878 Dibenz(a,h)anthracene U 0.0116 0.0419 1 11/25/2022 10:39 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 11 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 11 of 70 SAMPLE RESULTS - 02 L1558771 CS-2 Collected date/time: 11/14/22 12:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0124 0.419 1 11/25/2022 10:39 WG1962878 1,3-Dichlorobenzene U 0.0127 0.419 1 11/25/2022 10:39 WG1962878 1,4-Dichlorobenzene U 0.0125 0.419 1 11/25/2022 10:39 WG1962878 3,3-Dichlorobenzidine U 0.0155 0.419 1 11/25/2022 10:39 WG1962878 2,4-Dinitrotoluene U 0.0120 0.419 1 11/25/2022 10:39 WG1962878 2,6-Dinitrotoluene U 0.0137 0.419 1 11/25/2022 10:39 WG1962878 Fluoranthene 0.0205 J 0.00756 0.0419 1 11/25/2022 10:39 WG1962878 Fluorene U 0.00682 0.0419 1 11/25/2022 10:39 WG1962878 Hexachlorobenzene U 0.0148 0.419 1 11/25/2022 10:39 WG1962878 Hexachloro-1,3-butadiene U 0.0141 0.419 1 11/25/2022 10:39 WG1962878 Hexachlorocyclopentadiene U 0.0220 0.419 1 11/25/2022 10:39 WG1962878 Hexachloroethane U 0.0165 0.419 1 11/25/2022 10:39 WG1962878 Indeno(1,2,3-cd)pyrene U 0.0118 0.0419 1 11/25/2022 10:39 WG1962878 Isophorone U 0.0128 0.419 1 11/25/2022 10:39 WG1962878 Naphthalene U 0.0105 0.0419 1 11/25/2022 10:39 WG1962878 Nitrobenzene U 0.0146 0.419 1 11/25/2022 10:39 WG1962878 n-Nitrosodimethylamine U 0.0621 0.419 1 11/25/2022 10:39 WG1962878 n-Nitrosodiphenylamine U 0.0317 0.419 1 11/25/2022 10:39 WG1962878 n-Nitrosodi-n-propylamine U 0.0140 0.419 1 11/25/2022 10:39 WG1962878 Phenanthrene 0.0111 J 0.00831 0.0419 1 11/25/2022 10:39 WG1962878 Benzylbutyl phthalate U 0.0131 0.419 1 11/25/2022 10:39 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0531 0.419 1 11/25/2022 10:39 WG1962878 Di-n-butyl phthalate U 0.0143 0.419 1 11/25/2022 10:39 WG1962878 Diethyl phthalate U 0.0138 0.419 1 11/25/2022 10:39 WG1962878 Dimethyl phthalate U 0.0888 0.419 1 11/25/2022 10:39 WG1962878 Di-n-octyl phthalate U 0.0283 0.419 1 11/25/2022 10:39 WG1962878 Pyrene 0.0200 J 0.00815 0.0419 1 11/25/2022 10:39 WG1962878 1,2,4-Trichlorobenzene U 0.0131 0.419 1 11/25/2022 10:39 WG1962878 4-Chloro-3-methylphenol U 0.0136 0.419 1 11/25/2022 10:39 WG1962878 2-Chlorophenol U 0.0138 0.419 1 11/25/2022 10:39 WG1962878 2,4-Dichlorophenol U 0.0122 0.419 1 11/25/2022 10:39 WG1962878 2,4-Dimethylphenol U 0.0109 0.419 1 11/25/2022 10:39 WG1962878 4,6-Dinitro-2-methylphenol U 0.0949 0.419 1 11/25/2022 10:39 WG1962878 2,4-Dinitrophenol U 0.0980 0.419 1 11/25/2022 10:39 WG1962878 2-Nitrophenol U 0.0150 0.419 1 11/25/2022 10:39 WG1962878 4-Nitrophenol U 0.0131 0.419 1 11/25/2022 10:39 WG1962878 Pentachlorophenol U 0.0113 0.419 1 11/25/2022 10:39 WG1962878 Phenol U 0.0168 0.419 1 11/25/2022 10:39 WG1962878 2,4,6-Trichlorophenol U 0.0135 0.419 1 11/25/2022 10:39 WG1962878 (S) 2-Fluorophenol 69.2 12.0-120 11/25/2022 10:39 WG1962878 (S) Phenol-d5 64.7 10.0-120 11/25/2022 10:39 WG1962878 (S) Nitrobenzene-d5 61.8 10.0-122 11/25/2022 10:39 WG1962878 (S) 2-Fluorobiphenyl 59.7 15.0-120 11/25/2022 10:39 WG1962878 (S) 2,4,6-Tribromophenol 94.8 10.0-127 11/25/2022 10:39 WG1962878 (S) p-Terphenyl-d14 70.0 10.0-120 11/25/2022 10:39 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 12 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 12 of 70 SAMPLE RESULTS - 03 L1558771 CS-3 Collected date/time: 11/14/22 12:20 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 82.1 1 11/18/2022 10:32 WG1961475 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0219 0.0487 1 11/21/2022 15:01 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 3.68 0.122 1.22 5 11/25/2022 14:17 WG1961902 Barium 30.0 0.185 3.04 5 11/25/2022 14:17 WG1961902 Cadmium 0.178 J 0.104 1.22 5 11/25/2022 14:17 WG1961902 Chromium 11.0 0.360 6.09 5 11/25/2022 14:17 WG1961902 Lead 73.6 0.121 2.43 5 11/25/2022 14:17 WG1961902 Selenium 0.550 J 0.219 3.04 5 11/25/2022 14:17 WG1961902 Silver U 0.105 0.609 5 11/25/2022 14:17 WG1961902 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0537 0.0736 1.03 11/19/2022 12:56 WG1962462 Acrylonitrile U 0.00532 0.0184 1.03 11/19/2022 12:56 WG1962462 Benzene U 0.000687 0.00147 1.03 11/19/2022 12:56 WG1962462 Bromobenzene U 0.00132 0.0184 1.03 11/19/2022 12:56 WG1962462 Bromodichloromethane U 0.00107 0.00369 1.03 11/19/2022 12:56 WG1962462 Bromoform U 0.00173 0.0369 1.03 11/19/2022 12:56 WG1962462 Bromomethane U C3 0.00290 0.0184 1.03 11/19/2022 12:56 WG1962462 n-Butylbenzene U 0.00773 0.0184 1.03 11/19/2022 12:56 WG1962462 sec-Butylbenzene U 0.00424 0.0184 1.03 11/19/2022 12:56 WG1962462 tert-Butylbenzene U 0.00287 0.00736 1.03 11/19/2022 12:56 WG1962462 Carbon tetrachloride U 0.00132 0.00736 1.03 11/19/2022 12:56 WG1962462 Chlorobenzene U 0.000309 0.00369 1.03 11/19/2022 12:56 WG1962462 Chlorodibromomethane U 0.000900 0.00369 1.03 11/19/2022 12:56 WG1962462 Chloroethane U C3 J4 0.00250 0.00736 1.03 11/19/2022 12:56 WG1962462 Chloroform 0.00357 J 0.00151 0.00369 1.03 11/19/2022 12:56 WG1962462 Chloromethane U C3 0.00640 0.0184 1.03 11/19/2022 12:56 WG1962462 2-Chlorotoluene U 0.00127 0.00369 1.03 11/19/2022 12:56 WG1962462 4-Chlorotoluene U 0.000663 0.00736 1.03 11/19/2022 12:56 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00575 0.0369 1.03 11/19/2022 12:56 WG1962462 1,2-Dibromoethane U 0.000953 0.00369 1.03 11/19/2022 12:56 WG1962462 Dibromomethane U 0.00110 0.00736 1.03 11/19/2022 12:56 WG1962462 1,2-Dichlorobenzene U 0.000626 0.00736 1.03 11/19/2022 12:56 WG1962462 1,3-Dichlorobenzene U 0.000883 0.00736 1.03 11/19/2022 12:56 WG1962462 1,4-Dichlorobenzene U 0.00103 0.00736 1.03 11/19/2022 12:56 WG1962462 Dichlorodifluoromethane U C3 0.00237 0.00369 1.03 11/19/2022 12:56 WG1962462 1,1-Dichloroethane U 0.000723 0.00369 1.03 11/19/2022 12:56 WG1962462 1,2-Dichloroethane U 0.000955 0.00369 1.03 11/19/2022 12:56 WG1962462 1,1-Dichloroethene U 0.000892 0.00369 1.03 11/19/2022 12:56 WG1962462 cis-1,2-Dichloroethene U 0.00108 0.00369 1.03 11/19/2022 12:56 WG1962462 trans-1,2-Dichloroethene U 0.00153 0.00736 1.03 11/19/2022 12:56 WG1962462 1,2-Dichloropropane U 0.00209 0.00736 1.03 11/19/2022 12:56 WG1962462 1,1-Dichloropropene U 0.00119 0.00369 1.03 11/19/2022 12:56 WG1962462 1,3-Dichloropropane U 0.000737 0.00736 1.03 11/19/2022 12:56 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 13 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 13 of 70 SAMPLE RESULTS - 03 L1558771 CS-3 Collected date/time: 11/14/22 12:20 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00111 0.00369 1.03 11/19/2022 12:56 WG1962462 trans-1,3-Dichloropropene U 0.00167 0.00736 1.03 11/19/2022 12:56 WG1962462 2,2-Dichloropropane U C3 0.00203 0.00369 1.03 11/19/2022 12:56 WG1962462 Di-isopropyl ether U 0.000603 0.00147 1.03 11/19/2022 12:56 WG1962462 Ethylbenzene U 0.00108 0.00369 1.03 11/19/2022 12:56 WG1962462 Hexachloro-1,3-butadiene U 0.00883 0.0369 1.03 11/19/2022 12:56 WG1962462 Isopropylbenzene U 0.000626 0.00369 1.03 11/19/2022 12:56 WG1962462 p-Isopropyltoluene U 0.00376 0.00736 1.03 11/19/2022 12:56 WG1962462 2-Butanone (MEK)U 0.0935 0.147 1.03 11/19/2022 12:56 WG1962462 Methylene Chloride U 0.00978 0.0369 1.03 11/19/2022 12:56 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00336 0.0369 1.03 11/19/2022 12:56 WG1962462 Methyl tert-butyl ether U 0.000516 0.00147 1.03 11/19/2022 12:56 WG1962462 Naphthalene U 0.00719 0.0184 1.03 11/19/2022 12:56 WG1962462 n-Propylbenzene U 0.00140 0.00736 1.03 11/19/2022 12:56 WG1962462 Styrene U 0.000337 0.0184 1.03 11/19/2022 12:56 WG1962462 1,1,1,2-Tetrachloroethane U 0.00139 0.00369 1.03 11/19/2022 12:56 WG1962462 1,1,2,2-Tetrachloroethane U 0.00102 0.00369 1.03 11/19/2022 12:56 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00111 0.00369 1.03 11/19/2022 12:56 WG1962462 Tetrachloroethene U 0.00132 0.00369 1.03 11/19/2022 12:56 WG1962462 Toluene U 0.00192 0.00736 1.03 11/19/2022 12:56 WG1962462 1,2,3-Trichlorobenzene U 0.0108 0.0184 1.03 11/19/2022 12:56 WG1962462 1,2,4-Trichlorobenzene U J4 0.00647 0.0184 1.03 11/19/2022 12:56 WG1962462 1,1,1-Trichloroethane U 0.00136 0.00369 1.03 11/19/2022 12:56 WG1962462 1,1,2-Trichloroethane U 0.000879 0.00369 1.03 11/19/2022 12:56 WG1962462 Trichloroethene U 0.000860 0.00147 1.03 11/19/2022 12:56 WG1962462 Trichlorofluoromethane U C3 0.00122 0.00369 1.03 11/19/2022 12:56 WG1962462 1,2,3-Trichloropropane U 0.00239 0.0184 1.03 11/19/2022 12:56 WG1962462 1,2,4-Trimethylbenzene U 0.00233 0.00736 1.03 11/19/2022 12:56 WG1962462 1,2,3-Trimethylbenzene U 0.00233 0.00736 1.03 11/19/2022 12:56 WG1962462 1,3,5-Trimethylbenzene U 0.00294 0.00736 1.03 11/19/2022 12:56 WG1962462 Vinyl chloride U C3 J4 0.00170 0.00369 1.03 11/19/2022 12:56 WG1962462 Xylenes, Total 0.00180 J 0.00129 0.00958 1.03 11/19/2022 12:56 WG1962462 (S) Toluene-d8 103 75.0-131 11/19/2022 12:56 WG1962462 (S) 4-Bromofluorobenzene 100 67.0-138 11/19/2022 12:56 WG1962462 (S) 1,2-Dichloroethane-d4 82.4 70.0-130 11/19/2022 12:56 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00656 0.0405 1 11/25/2022 11:39 WG1962878 Acenaphthylene 0.0105 J 0.00571 0.0405 1 11/25/2022 11:39 WG1962878 Anthracene U 0.00722 0.0405 1 11/25/2022 11:39 WG1962878 Benzidine U 0.0762 2.03 1 11/25/2022 11:39 WG1962878 Benzo(a)anthracene 0.0241 J 0.00715 0.0405 1 11/25/2022 11:39 WG1962878 Benzo(b)fluoranthene 0.0488 0.00756 0.0405 1 11/25/2022 11:39 WG1962878 Benzo(k)fluoranthene 0.0156 J 0.00721 0.0405 1 11/25/2022 11:39 WG1962878 Benzo(g,h,i)perylene 0.0293 J 0.00741 0.0405 1 11/25/2022 11:39 WG1962878 Benzo(a)pyrene 0.0353 J 0.00754 0.0405 1 11/25/2022 11:39 WG1962878 Bis(2-chlorethoxy)methane U 0.0122 0.405 1 11/25/2022 11:39 WG1962878 Bis(2-chloroethyl)ether U 0.0134 0.405 1 11/25/2022 11:39 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0175 0.405 1 11/25/2022 11:39 WG1962878 4-Bromophenyl-phenylether U 0.0142 0.405 1 11/25/2022 11:39 WG1962878 2-Chloronaphthalene U 0.00712 0.0405 1 11/25/2022 11:39 WG1962878 4-Chlorophenyl-phenylether U 0.0141 0.405 1 11/25/2022 11:39 WG1962878 Chrysene 0.0319 J 0.00806 0.0405 1 11/25/2022 11:39 WG1962878 Dibenz(a,h)anthracene U 0.0112 0.0405 1 11/25/2022 11:39 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 14 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 14 of 70 SAMPLE RESULTS - 03 L1558771 CS-3 Collected date/time: 11/14/22 12:20 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0120 0.405 1 11/25/2022 11:39 WG1962878 1,3-Dichlorobenzene U 0.0123 0.405 1 11/25/2022 11:39 WG1962878 1,4-Dichlorobenzene U 0.0121 0.405 1 11/25/2022 11:39 WG1962878 3,3-Dichlorobenzidine U 0.0150 0.405 1 11/25/2022 11:39 WG1962878 2,4-Dinitrotoluene U 0.0116 0.405 1 11/25/2022 11:39 WG1962878 2,6-Dinitrotoluene U 0.0133 0.405 1 11/25/2022 11:39 WG1962878 Fluoranthene 0.0548 0.00732 0.0405 1 11/25/2022 11:39 WG1962878 Fluorene U 0.00660 0.0405 1 11/25/2022 11:39 WG1962878 Hexachlorobenzene U 0.0144 0.405 1 11/25/2022 11:39 WG1962878 Hexachloro-1,3-butadiene U 0.0136 0.405 1 11/25/2022 11:39 WG1962878 Hexachlorocyclopentadiene U 0.0213 0.405 1 11/25/2022 11:39 WG1962878 Hexachloroethane U 0.0159 0.405 1 11/25/2022 11:39 WG1962878 Indeno(1,2,3-cd)pyrene 0.0312 J 0.0115 0.0405 1 11/25/2022 11:39 WG1962878 Isophorone U 0.0124 0.405 1 11/25/2022 11:39 WG1962878 Naphthalene U 0.0102 0.0405 1 11/25/2022 11:39 WG1962878 Nitrobenzene U 0.0141 0.405 1 11/25/2022 11:39 WG1962878 n-Nitrosodimethylamine U 0.0601 0.405 1 11/25/2022 11:39 WG1962878 n-Nitrosodiphenylamine U 0.0307 0.405 1 11/25/2022 11:39 WG1962878 n-Nitrosodi-n-propylamine U 0.0135 0.405 1 11/25/2022 11:39 WG1962878 Phenanthrene 0.0313 J 0.00805 0.0405 1 11/25/2022 11:39 WG1962878 Benzylbutyl phthalate U 0.0127 0.405 1 11/25/2022 11:39 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0514 0.405 1 11/25/2022 11:39 WG1962878 Di-n-butyl phthalate 0.0173 J 0.0139 0.405 1 11/25/2022 11:39 WG1962878 Diethyl phthalate U 0.0134 0.405 1 11/25/2022 11:39 WG1962878 Dimethyl phthalate U 0.0859 0.405 1 11/25/2022 11:39 WG1962878 Di-n-octyl phthalate U 0.0274 0.405 1 11/25/2022 11:39 WG1962878 Pyrene 0.0469 0.00789 0.0405 1 11/25/2022 11:39 WG1962878 1,2,4-Trichlorobenzene U 0.0127 0.405 1 11/25/2022 11:39 WG1962878 4-Chloro-3-methylphenol U 0.0131 0.405 1 11/25/2022 11:39 WG1962878 2-Chlorophenol U 0.0134 0.405 1 11/25/2022 11:39 WG1962878 2,4-Dichlorophenol U 0.0118 0.405 1 11/25/2022 11:39 WG1962878 2,4-Dimethylphenol U 0.0106 0.405 1 11/25/2022 11:39 WG1962878 4,6-Dinitro-2-methylphenol U 0.0919 0.405 1 11/25/2022 11:39 WG1962878 2,4-Dinitrophenol U 0.0948 0.405 1 11/25/2022 11:39 WG1962878 2-Nitrophenol U 0.0145 0.405 1 11/25/2022 11:39 WG1962878 4-Nitrophenol U 0.0127 0.405 1 11/25/2022 11:39 WG1962878 Pentachlorophenol U 0.0109 0.405 1 11/25/2022 11:39 WG1962878 Phenol U 0.0163 0.405 1 11/25/2022 11:39 WG1962878 2,4,6-Trichlorophenol U 0.0130 0.405 1 11/25/2022 11:39 WG1962878 (S) 2-Fluorophenol 56.8 12.0-120 11/25/2022 11:39 WG1962878 (S) Phenol-d5 54.8 10.0-120 11/25/2022 11:39 WG1962878 (S) Nitrobenzene-d5 50.5 10.0-122 11/25/2022 11:39 WG1962878 (S) 2-Fluorobiphenyl 48.9 15.0-120 11/25/2022 11:39 WG1962878 (S) 2,4,6-Tribromophenol 72.7 10.0-127 11/25/2022 11:39 WG1962878 (S) p-Terphenyl-d14 56.8 10.0-120 11/25/2022 11:39 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 15 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 15 of 70 SAMPLE RESULTS - 04 L1558771 CS-4 Collected date/time: 11/14/22 14:45 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 79.3 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0668 0.0227 0.0504 1 11/21/2022 15:03 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 7.87 0.126 1.26 5 12/01/2022 18:50 WG1962098 Barium 32.4 0.192 3.15 5 12/01/2022 18:50 WG1962098 Cadmium U 0.108 1.26 5 12/01/2022 18:50 WG1962098 Chromium 28.4 0.373 6.30 5 12/01/2022 18:50 WG1962098 Lead 14.8 0.125 2.52 5 12/01/2022 18:50 WG1962098 Selenium 0.817 J 0.227 3.15 5 12/01/2022 18:50 WG1962098 Silver U 0.109 0.630 5 12/01/2022 18:50 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0562 0.0770 1 11/19/2022 13:15 WG1962462 Acrylonitrile U 0.00556 0.0192 1 11/19/2022 13:15 WG1962462 Benzene U 0.000719 0.00154 1 11/19/2022 13:15 WG1962462 Bromobenzene U 0.00139 0.0192 1 11/19/2022 13:15 WG1962462 Bromodichloromethane U 0.00112 0.00385 1 11/19/2022 13:15 WG1962462 Bromoform U 0.00180 0.0385 1 11/19/2022 13:15 WG1962462 Bromomethane U C3 0.00303 0.0192 1 11/19/2022 13:15 WG1962462 n-Butylbenzene U 0.00808 0.0192 1 11/19/2022 13:15 WG1962462 sec-Butylbenzene U 0.00443 0.0192 1 11/19/2022 13:15 WG1962462 tert-Butylbenzene U 0.00300 0.00770 1 11/19/2022 13:15 WG1962462 Carbon tetrachloride U 0.00138 0.00770 1 11/19/2022 13:15 WG1962462 Chlorobenzene U 0.000323 0.00385 1 11/19/2022 13:15 WG1962462 Chlorodibromomethane U 0.000942 0.00385 1 11/19/2022 13:15 WG1962462 Chloroethane U C3 J4 0.00262 0.00770 1 11/19/2022 13:15 WG1962462 Chloroform 0.00416 0.00159 0.00385 1 11/19/2022 13:15 WG1962462 Chloromethane U C3 0.00670 0.0192 1 11/19/2022 13:15 WG1962462 2-Chlorotoluene U 0.00133 0.00385 1 11/19/2022 13:15 WG1962462 4-Chlorotoluene U 0.000693 0.00770 1 11/19/2022 13:15 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00600 0.0385 1 11/19/2022 13:15 WG1962462 1,2-Dibromoethane U 0.000997 0.00385 1 11/19/2022 13:15 WG1962462 Dibromomethane U 0.00115 0.00770 1 11/19/2022 13:15 WG1962462 1,2-Dichlorobenzene U 0.000654 0.00770 1 11/19/2022 13:15 WG1962462 1,3-Dichlorobenzene U 0.000924 0.00770 1 11/19/2022 13:15 WG1962462 1,4-Dichlorobenzene U 0.00108 0.00770 1 11/19/2022 13:15 WG1962462 Dichlorodifluoromethane U C3 0.00248 0.00385 1 11/19/2022 13:15 WG1962462 1,1-Dichloroethane U 0.000756 0.00385 1 11/19/2022 13:15 WG1962462 1,2-Dichloroethane U 0.000999 0.00385 1 11/19/2022 13:15 WG1962462 1,1-Dichloroethene U 0.000933 0.00385 1 11/19/2022 13:15 WG1962462 cis-1,2-Dichloroethene U 0.00113 0.00385 1 11/19/2022 13:15 WG1962462 trans-1,2-Dichloroethene U 0.00160 0.00770 1 11/19/2022 13:15 WG1962462 1,2-Dichloropropane U 0.00219 0.00770 1 11/19/2022 13:15 WG1962462 1,1-Dichloropropene U 0.00125 0.00385 1 11/19/2022 13:15 WG1962462 1,3-Dichloropropane U 0.000771 0.00770 1 11/19/2022 13:15 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 16 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 16 of 70 SAMPLE RESULTS - 04 L1558771 CS-4 Collected date/time: 11/14/22 14:45 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00117 0.00385 1 11/19/2022 13:15 WG1962462 trans-1,3-Dichloropropene U 0.00175 0.00770 1 11/19/2022 13:15 WG1962462 2,2-Dichloropropane U C3 0.00212 0.00385 1 11/19/2022 13:15 WG1962462 Di-isopropyl ether U 0.000631 0.00154 1 11/19/2022 13:15 WG1962462 Ethylbenzene U 0.00113 0.00385 1 11/19/2022 13:15 WG1962462 Hexachloro-1,3-butadiene U 0.00924 0.0385 1 11/19/2022 13:15 WG1962462 Isopropylbenzene U 0.000654 0.00385 1 11/19/2022 13:15 WG1962462 p-Isopropyltoluene U 0.00393 0.00770 1 11/19/2022 13:15 WG1962462 2-Butanone (MEK)U 0.0977 0.154 1 11/19/2022 13:15 WG1962462 Methylene Chloride U 0.0102 0.0385 1 11/19/2022 13:15 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00351 0.0385 1 11/19/2022 13:15 WG1962462 Methyl tert-butyl ether U 0.000539 0.00154 1 11/19/2022 13:15 WG1962462 Naphthalene U 0.00751 0.0192 1 11/19/2022 13:15 WG1962462 n-Propylbenzene U 0.00146 0.00770 1 11/19/2022 13:15 WG1962462 Styrene U 0.000352 0.0192 1 11/19/2022 13:15 WG1962462 1,1,1,2-Tetrachloroethane U 0.00146 0.00385 1 11/19/2022 13:15 WG1962462 1,1,2,2-Tetrachloroethane U 0.00107 0.00385 1 11/19/2022 13:15 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00116 0.00385 1 11/19/2022 13:15 WG1962462 Tetrachloroethene U 0.00138 0.00385 1 11/19/2022 13:15 WG1962462 Toluene U 0.00200 0.00770 1 11/19/2022 13:15 WG1962462 1,2,3-Trichlorobenzene U 0.0113 0.0192 1 11/19/2022 13:15 WG1962462 1,2,4-Trichlorobenzene U J4 0.00677 0.0192 1 11/19/2022 13:15 WG1962462 1,1,1-Trichloroethane U 0.00142 0.00385 1 11/19/2022 13:15 WG1962462 1,1,2-Trichloroethane U 0.000919 0.00385 1 11/19/2022 13:15 WG1962462 Trichloroethene U 0.000899 0.00154 1 11/19/2022 13:15 WG1962462 Trichlorofluoromethane U C3 0.00127 0.00385 1 11/19/2022 13:15 WG1962462 1,2,3-Trichloropropane U 0.00249 0.0192 1 11/19/2022 13:15 WG1962462 1,2,4-Trimethylbenzene U 0.00243 0.00770 1 11/19/2022 13:15 WG1962462 1,2,3-Trimethylbenzene U 0.00243 0.00770 1 11/19/2022 13:15 WG1962462 1,3,5-Trimethylbenzene U 0.00308 0.00770 1 11/19/2022 13:15 WG1962462 Vinyl chloride U C3 J4 0.00179 0.00385 1 11/19/2022 13:15 WG1962462 Xylenes, Total 0.00369 J 0.00135 0.0100 1 11/19/2022 13:15 WG1962462 (S) Toluene-d8 105 75.0-131 11/19/2022 13:15 WG1962462 (S) 4-Bromofluorobenzene 97.3 67.0-138 11/19/2022 13:15 WG1962462 (S) 1,2-Dichloroethane-d4 83.4 70.0-130 11/19/2022 13:15 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00679 0.0420 1 11/25/2022 11:19 WG1962878 Acenaphthylene U 0.00591 0.0420 1 11/25/2022 11:19 WG1962878 Anthracene U 0.00748 0.0420 1 11/25/2022 11:19 WG1962878 Benzidine U 0.0789 2.11 1 11/25/2022 11:19 WG1962878 Benzo(a)anthracene U 0.00740 0.0420 1 11/25/2022 11:19 WG1962878 Benzo(b)fluoranthene U 0.00783 0.0420 1 11/25/2022 11:19 WG1962878 Benzo(k)fluoranthene U 0.00746 0.0420 1 11/25/2022 11:19 WG1962878 Benzo(g,h,i)perylene U 0.00768 0.0420 1 11/25/2022 11:19 WG1962878 Benzo(a)pyrene U 0.00780 0.0420 1 11/25/2022 11:19 WG1962878 Bis(2-chlorethoxy)methane U 0.0126 0.420 1 11/25/2022 11:19 WG1962878 Bis(2-chloroethyl)ether U 0.0139 0.420 1 11/25/2022 11:19 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0182 0.420 1 11/25/2022 11:19 WG1962878 4-Bromophenyl-phenylether U 0.0147 0.420 1 11/25/2022 11:19 WG1962878 2-Chloronaphthalene U 0.00737 0.0420 1 11/25/2022 11:19 WG1962878 4-Chlorophenyl-phenylether U 0.0146 0.420 1 11/25/2022 11:19 WG1962878 Chrysene U 0.00835 0.0420 1 11/25/2022 11:19 WG1962878 Dibenz(a,h)anthracene U 0.0116 0.0420 1 11/25/2022 11:19 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 17 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 17 of 70 SAMPLE RESULTS - 04 L1558771 CS-4 Collected date/time: 11/14/22 14:45 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0124 0.420 1 11/25/2022 11:19 WG1962878 1,3-Dichlorobenzene U 0.0127 0.420 1 11/25/2022 11:19 WG1962878 1,4-Dichlorobenzene U 0.0125 0.420 1 11/25/2022 11:19 WG1962878 3,3-Dichlorobenzidine U 0.0155 0.420 1 11/25/2022 11:19 WG1962878 2,4-Dinitrotoluene U 0.0120 0.420 1 11/25/2022 11:19 WG1962878 2,6-Dinitrotoluene U 0.0137 0.420 1 11/25/2022 11:19 WG1962878 Fluoranthene U 0.00758 0.0420 1 11/25/2022 11:19 WG1962878 Fluorene U 0.00683 0.0420 1 11/25/2022 11:19 WG1962878 Hexachlorobenzene U 0.0149 0.420 1 11/25/2022 11:19 WG1962878 Hexachloro-1,3-butadiene U 0.0141 0.420 1 11/25/2022 11:19 WG1962878 Hexachlorocyclopentadiene U 0.0221 0.420 1 11/25/2022 11:19 WG1962878 Hexachloroethane U 0.0165 0.420 1 11/25/2022 11:19 WG1962878 Indeno(1,2,3-cd)pyrene U 0.0119 0.0420 1 11/25/2022 11:19 WG1962878 Isophorone U 0.0129 0.420 1 11/25/2022 11:19 WG1962878 Naphthalene U 0.0105 0.0420 1 11/25/2022 11:19 WG1962878 Nitrobenzene U 0.0146 0.420 1 11/25/2022 11:19 WG1962878 n-Nitrosodimethylamine U 0.0623 0.420 1 11/25/2022 11:19 WG1962878 n-Nitrosodiphenylamine U 0.0318 0.420 1 11/25/2022 11:19 WG1962878 n-Nitrosodi-n-propylamine U 0.0140 0.420 1 11/25/2022 11:19 WG1962878 Phenanthrene U 0.00833 0.0420 1 11/25/2022 11:19 WG1962878 Benzylbutyl phthalate U 0.0131 0.420 1 11/25/2022 11:19 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0532 0.420 1 11/25/2022 11:19 WG1962878 Di-n-butyl phthalate U 0.0144 0.420 1 11/25/2022 11:19 WG1962878 Diethyl phthalate U 0.0139 0.420 1 11/25/2022 11:19 WG1962878 Dimethyl phthalate U 0.0890 0.420 1 11/25/2022 11:19 WG1962878 Di-n-octyl phthalate U 0.0284 0.420 1 11/25/2022 11:19 WG1962878 Pyrene U 0.00817 0.0420 1 11/25/2022 11:19 WG1962878 1,2,4-Trichlorobenzene U 0.0131 0.420 1 11/25/2022 11:19 WG1962878 4-Chloro-3-methylphenol U 0.0136 0.420 1 11/25/2022 11:19 WG1962878 2-Chlorophenol U 0.0139 0.420 1 11/25/2022 11:19 WG1962878 2,4-Dichlorophenol U 0.0122 0.420 1 11/25/2022 11:19 WG1962878 2,4-Dimethylphenol U 0.0110 0.420 1 11/25/2022 11:19 WG1962878 4,6-Dinitro-2-methylphenol U 0.0952 0.420 1 11/25/2022 11:19 WG1962878 2,4-Dinitrophenol U 0.0982 0.420 1 11/25/2022 11:19 WG1962878 2-Nitrophenol U 0.0150 0.420 1 11/25/2022 11:19 WG1962878 4-Nitrophenol U 0.0131 0.420 1 11/25/2022 11:19 WG1962878 Pentachlorophenol U 0.0113 0.420 1 11/25/2022 11:19 WG1962878 Phenol U 0.0169 0.420 1 11/25/2022 11:19 WG1962878 2,4,6-Trichlorophenol U 0.0135 0.420 1 11/25/2022 11:19 WG1962878 (S) 2-Fluorophenol 64.0 12.0-120 11/25/2022 11:19 WG1962878 (S) Phenol-d5 59.1 10.0-120 11/25/2022 11:19 WG1962878 (S) Nitrobenzene-d5 57.0 10.0-122 11/25/2022 11:19 WG1962878 (S) 2-Fluorobiphenyl 54.9 15.0-120 11/25/2022 11:19 WG1962878 (S) 2,4,6-Tribromophenol 83.4 10.0-127 11/25/2022 11:19 WG1962878 (S) p-Terphenyl-d14 63.7 10.0-120 11/25/2022 11:19 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 18 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 18 of 70 SAMPLE RESULTS - 05 L1558771 CS-4-A Collected date/time: 11/14/22 14:45 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 66.2 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury U 0.0272 0.0604 1 11/21/2022 15:05 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.25 J 0.151 1.51 5 11/28/2022 17:31 WG1963015 Barium 21.0 0.230 3.78 5 11/28/2022 17:31 WG1963015 Cadmium U 0.129 1.51 5 11/28/2022 17:31 WG1963015 Chromium 1.84 J 0.447 7.56 5 11/28/2022 17:31 WG1963015 Lead 22.9 0.150 3.02 5 11/28/2022 17:31 WG1963015 Selenium 0.330 B J 0.272 3.78 5 11/28/2022 17:31 WG1963015 Silver U 0.131 0.756 5 11/28/2022 17:31 WG1963015 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0740 0.101 1 11/19/2022 13:34 WG1962462 Acrylonitrile U 0.00732 0.0253 1 11/19/2022 13:34 WG1962462 Benzene U 0.000946 0.00203 1 11/19/2022 13:34 WG1962462 Bromobenzene U 0.00182 0.0253 1 11/19/2022 13:34 WG1962462 Bromodichloromethane U 0.00147 0.00507 1 11/19/2022 13:34 WG1962462 Bromoform U 0.00237 0.0507 1 11/19/2022 13:34 WG1962462 Bromomethane U C3 0.00399 0.0253 1 11/19/2022 13:34 WG1962462 n-Butylbenzene U 0.0106 0.0253 1 11/19/2022 13:34 WG1962462 sec-Butylbenzene U 0.00584 0.0253 1 11/19/2022 13:34 WG1962462 tert-Butylbenzene U 0.00395 0.0101 1 11/19/2022 13:34 WG1962462 Carbon tetrachloride U 0.00182 0.0101 1 11/19/2022 13:34 WG1962462 Chlorobenzene U 0.000426 0.00507 1 11/19/2022 13:34 WG1962462 Chlorodibromomethane U 0.00124 0.00507 1 11/19/2022 13:34 WG1962462 Chloroethane U C3 J4 0.00344 0.0101 1 11/19/2022 13:34 WG1962462 Chloroform 0.00496 J 0.00209 0.00507 1 11/19/2022 13:34 WG1962462 Chloromethane U C3 0.00881 0.0253 1 11/19/2022 13:34 WG1962462 2-Chlorotoluene U 0.00175 0.00507 1 11/19/2022 13:34 WG1962462 4-Chlorotoluene U 0.000912 0.0101 1 11/19/2022 13:34 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00790 0.0507 1 11/19/2022 13:34 WG1962462 1,2-Dibromoethane U 0.00131 0.00507 1 11/19/2022 13:34 WG1962462 Dibromomethane U 0.00152 0.0101 1 11/19/2022 13:34 WG1962462 1,2-Dichlorobenzene U 0.000861 0.0101 1 11/19/2022 13:34 WG1962462 1,3-Dichlorobenzene U 0.00122 0.0101 1 11/19/2022 13:34 WG1962462 1,4-Dichlorobenzene U 0.00142 0.0101 1 11/19/2022 13:34 WG1962462 Dichlorodifluoromethane U C3 0.00326 0.00507 1 11/19/2022 13:34 WG1962462 1,1-Dichloroethane U 0.000995 0.00507 1 11/19/2022 13:34 WG1962462 1,2-Dichloroethane U 0.00132 0.00507 1 11/19/2022 13:34 WG1962462 1,1-Dichloroethene U 0.00123 0.00507 1 11/19/2022 13:34 WG1962462 cis-1,2-Dichloroethene U 0.00149 0.00507 1 11/19/2022 13:34 WG1962462 trans-1,2-Dichloroethene U 0.00211 0.0101 1 11/19/2022 13:34 WG1962462 1,2-Dichloropropane U 0.00288 0.0101 1 11/19/2022 13:34 WG1962462 1,1-Dichloropropene U 0.00164 0.00507 1 11/19/2022 13:34 WG1962462 1,3-Dichloropropane U 0.00102 0.0101 1 11/19/2022 13:34 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 19 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 19 of 70 SAMPLE RESULTS - 05 L1558771 CS-4-A Collected date/time: 11/14/22 14:45 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00153 0.00507 1 11/19/2022 13:34 WG1962462 trans-1,3-Dichloropropene U 0.00231 0.0101 1 11/19/2022 13:34 WG1962462 2,2-Dichloropropane U C3 0.00280 0.00507 1 11/19/2022 13:34 WG1962462 Di-isopropyl ether U 0.000831 0.00203 1 11/19/2022 13:34 WG1962462 Ethylbenzene U 0.00149 0.00507 1 11/19/2022 13:34 WG1962462 Hexachloro-1,3-butadiene U 0.0122 0.0507 1 11/19/2022 13:34 WG1962462 Isopropylbenzene U 0.000861 0.00507 1 11/19/2022 13:34 WG1962462 p-Isopropyltoluene U 0.00517 0.0101 1 11/19/2022 13:34 WG1962462 2-Butanone (MEK)U 0.129 0.203 1 11/19/2022 13:34 WG1962462 Methylene Chloride U 0.0135 0.0507 1 11/19/2022 13:34 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00462 0.0507 1 11/19/2022 13:34 WG1962462 Methyl tert-butyl ether U 0.000709 0.00203 1 11/19/2022 13:34 WG1962462 Naphthalene U 0.00989 0.0253 1 11/19/2022 13:34 WG1962462 n-Propylbenzene U 0.00193 0.0101 1 11/19/2022 13:34 WG1962462 Styrene U 0.000464 0.0253 1 11/19/2022 13:34 WG1962462 1,1,1,2-Tetrachloroethane U 0.00192 0.00507 1 11/19/2022 13:34 WG1962462 1,1,2,2-Tetrachloroethane U 0.00141 0.00507 1 11/19/2022 13:34 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00153 0.00507 1 11/19/2022 13:34 WG1962462 Tetrachloroethene U 0.00182 0.00507 1 11/19/2022 13:34 WG1962462 Toluene 0.00306 J 0.00263 0.0101 1 11/19/2022 13:34 WG1962462 1,2,3-Trichlorobenzene U 0.0149 0.0253 1 11/19/2022 13:34 WG1962462 1,2,4-Trichlorobenzene U J4 0.00892 0.0253 1 11/19/2022 13:34 WG1962462 1,1,1-Trichloroethane U 0.00187 0.00507 1 11/19/2022 13:34 WG1962462 1,1,2-Trichloroethane U 0.00121 0.00507 1 11/19/2022 13:34 WG1962462 Trichloroethene U 0.00118 0.00203 1 11/19/2022 13:34 WG1962462 Trichlorofluoromethane U C3 0.00168 0.00507 1 11/19/2022 13:34 WG1962462 1,2,3-Trichloropropane U 0.00328 0.0253 1 11/19/2022 13:34 WG1962462 1,2,4-Trimethylbenzene U 0.00320 0.0101 1 11/19/2022 13:34 WG1962462 1,2,3-Trimethylbenzene U 0.00320 0.0101 1 11/19/2022 13:34 WG1962462 1,3,5-Trimethylbenzene U 0.00405 0.0101 1 11/19/2022 13:34 WG1962462 Vinyl chloride U C3 J4 0.00235 0.00507 1 11/19/2022 13:34 WG1962462 Xylenes, Total U 0.00178 0.0132 1 11/19/2022 13:34 WG1962462 (S) Toluene-d8 105 75.0-131 11/19/2022 13:34 WG1962462 (S) 4-Bromofluorobenzene 99.9 67.0-138 11/19/2022 13:34 WG1962462 (S) 1,2-Dichloroethane-d4 84.7 70.0-130 11/19/2022 13:34 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00814 0.0503 1 11/25/2022 10:19 WG1962878 Acenaphthylene U 0.00709 0.0503 1 11/25/2022 10:19 WG1962878 Anthracene U 0.00896 0.0503 1 11/25/2022 10:19 WG1962878 Benzidine U 0.0946 2.52 1 11/25/2022 10:19 WG1962878 Benzo(a)anthracene U 0.00887 0.0503 1 11/25/2022 10:19 WG1962878 Benzo(b)fluoranthene U 0.00938 0.0503 1 11/25/2022 10:19 WG1962878 Benzo(k)fluoranthene U 0.00895 0.0503 1 11/25/2022 10:19 WG1962878 Benzo(g,h,i)perylene U 0.00920 0.0503 1 11/25/2022 10:19 WG1962878 Benzo(a)pyrene U 0.00935 0.0503 1 11/25/2022 10:19 WG1962878 Bis(2-chlorethoxy)methane U 0.0151 0.503 1 11/25/2022 10:19 WG1962878 Bis(2-chloroethyl)ether U 0.0166 0.503 1 11/25/2022 10:19 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0218 0.503 1 11/25/2022 10:19 WG1962878 4-Bromophenyl-phenylether U 0.0177 0.503 1 11/25/2022 10:19 WG1962878 2-Chloronaphthalene U 0.00884 0.0503 1 11/25/2022 10:19 WG1962878 4-Chlorophenyl-phenylether U 0.0175 0.503 1 11/25/2022 10:19 WG1962878 Chrysene U 0.0100 0.0503 1 11/25/2022 10:19 WG1962878 Dibenz(a,h)anthracene U 0.0139 0.0503 1 11/25/2022 10:19 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 20 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 20 of 70 SAMPLE RESULTS - 05 L1558771 CS-4-A Collected date/time: 11/14/22 14:45 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0149 0.503 1 11/25/2022 10:19 WG1962878 1,3-Dichlorobenzene U 0.0153 0.503 1 11/25/2022 10:19 WG1962878 1,4-Dichlorobenzene U 0.0150 0.503 1 11/25/2022 10:19 WG1962878 3,3-Dichlorobenzidine U 0.0186 0.503 1 11/25/2022 10:19 WG1962878 2,4-Dinitrotoluene U 0.0144 0.503 1 11/25/2022 10:19 WG1962878 2,6-Dinitrotoluene U 0.0165 0.503 1 11/25/2022 10:19 WG1962878 Fluoranthene U 0.00908 0.0503 1 11/25/2022 10:19 WG1962878 Fluorene U 0.00819 0.0503 1 11/25/2022 10:19 WG1962878 Hexachlorobenzene U 0.0178 0.503 1 11/25/2022 10:19 WG1962878 Hexachloro-1,3-butadiene U 0.0169 0.503 1 11/25/2022 10:19 WG1962878 Hexachlorocyclopentadiene U 0.0264 0.503 1 11/25/2022 10:19 WG1962878 Hexachloroethane U 0.0198 0.503 1 11/25/2022 10:19 WG1962878 Indeno(1,2,3-cd)pyrene U 0.0142 0.0503 1 11/25/2022 10:19 WG1962878 Isophorone U 0.0154 0.503 1 11/25/2022 10:19 WG1962878 Naphthalene U 0.0126 0.0503 1 11/25/2022 10:19 WG1962878 Nitrobenzene U 0.0175 0.503 1 11/25/2022 10:19 WG1962878 n-Nitrosodimethylamine U 0.0746 0.503 1 11/25/2022 10:19 WG1962878 n-Nitrosodiphenylamine U 0.0381 0.503 1 11/25/2022 10:19 WG1962878 n-Nitrosodi-n-propylamine U 0.0168 0.503 1 11/25/2022 10:19 WG1962878 Phenanthrene U 0.00999 0.0503 1 11/25/2022 10:19 WG1962878 Benzylbutyl phthalate U 0.0157 0.503 1 11/25/2022 10:19 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0638 0.503 1 11/25/2022 10:19 WG1962878 Di-n-butyl phthalate U 0.0172 0.503 1 11/25/2022 10:19 WG1962878 Diethyl phthalate U 0.0166 0.503 1 11/25/2022 10:19 WG1962878 Dimethyl phthalate U 0.107 0.503 1 11/25/2022 10:19 WG1962878 Di-n-octyl phthalate U 0.0340 0.503 1 11/25/2022 10:19 WG1962878 Pyrene U 0.00979 0.0503 1 11/25/2022 10:19 WG1962878 1,2,4-Trichlorobenzene U 0.0157 0.503 1 11/25/2022 10:19 WG1962878 4-Chloro-3-methylphenol U 0.0163 0.503 1 11/25/2022 10:19 WG1962878 2-Chlorophenol U 0.0166 0.503 1 11/25/2022 10:19 WG1962878 2,4-Dichlorophenol U 0.0147 0.503 1 11/25/2022 10:19 WG1962878 2,4-Dimethylphenol U 0.0131 0.503 1 11/25/2022 10:19 WG1962878 4,6-Dinitro-2-methylphenol U 0.114 0.503 1 11/25/2022 10:19 WG1962878 2,4-Dinitrophenol U 0.118 0.503 1 11/25/2022 10:19 WG1962878 2-Nitrophenol U 0.0180 0.503 1 11/25/2022 10:19 WG1962878 4-Nitrophenol U 0.0157 0.503 1 11/25/2022 10:19 WG1962878 Pentachlorophenol U 0.0135 0.503 1 11/25/2022 10:19 WG1962878 Phenol U 0.0202 0.503 1 11/25/2022 10:19 WG1962878 2,4,6-Trichlorophenol U 0.0162 0.503 1 11/25/2022 10:19 WG1962878 (S) 2-Fluorophenol 56.8 12.0-120 11/25/2022 10:19 WG1962878 (S) Phenol-d5 51.7 10.0-120 11/25/2022 10:19 WG1962878 (S) Nitrobenzene-d5 51.5 10.0-122 11/25/2022 10:19 WG1962878 (S) 2-Fluorobiphenyl 51.2 15.0-120 11/25/2022 10:19 WG1962878 (S) 2,4,6-Tribromophenol 70.2 10.0-127 11/25/2022 10:19 WG1962878 (S) p-Terphenyl-d14 55.1 10.0-120 11/25/2022 10:19 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 21 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 21 of 70 SAMPLE RESULTS - 06 L1558771 CS-5 Collected date/time: 11/14/22 13:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 74.9 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0731 0.0240 0.0534 1 11/21/2022 15:07 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.60 0.134 1.34 5 12/01/2022 18:53 WG1962098 Barium 39.5 0.203 3.34 5 12/01/2022 18:53 WG1962098 Cadmium 0.506 J 0.114 1.34 5 12/01/2022 18:53 WG1962098 Chromium 30.9 0.395 6.68 5 12/01/2022 18:53 WG1962098 Lead 61.1 0.132 2.67 5 12/01/2022 18:53 WG1962098 Selenium 0.785 J 0.240 3.34 5 12/01/2022 18:53 WG1962098 Silver U 0.116 0.668 5 12/01/2022 18:53 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0645 0.0882 1.07 11/19/2022 13:54 WG1962462 Acrylonitrile U 0.00637 0.0221 1.07 11/19/2022 13:54 WG1962462 Benzene U 0.000825 0.00176 1.07 11/19/2022 13:54 WG1962462 Bromobenzene U 0.00159 0.0221 1.07 11/19/2022 13:54 WG1962462 Bromodichloromethane U 0.00128 0.00442 1.07 11/19/2022 13:54 WG1962462 Bromoform U 0.00206 0.0442 1.07 11/19/2022 13:54 WG1962462 Bromomethane U C3 0.00348 0.0221 1.07 11/19/2022 13:54 WG1962462 n-Butylbenzene U 0.00927 0.0221 1.07 11/19/2022 13:54 WG1962462 sec-Butylbenzene U 0.00508 0.0221 1.07 11/19/2022 13:54 WG1962462 tert-Butylbenzene U 0.00345 0.00882 1.07 11/19/2022 13:54 WG1962462 Carbon tetrachloride U 0.00159 0.00882 1.07 11/19/2022 13:54 WG1962462 Chlorobenzene U 0.000371 0.00442 1.07 11/19/2022 13:54 WG1962462 Chlorodibromomethane U 0.00108 0.00442 1.07 11/19/2022 13:54 WG1962462 Chloroethane U C3 J4 0.00300 0.00882 1.07 11/19/2022 13:54 WG1962462 Chloroform 0.00459 0.00181 0.00442 1.07 11/19/2022 13:54 WG1962462 Chloromethane U C3 0.00767 0.0221 1.07 11/19/2022 13:54 WG1962462 2-Chlorotoluene U 0.00153 0.00442 1.07 11/19/2022 13:54 WG1962462 4-Chlorotoluene U 0.000793 0.00882 1.07 11/19/2022 13:54 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00688 0.0442 1.07 11/19/2022 13:54 WG1962462 1,2-Dibromoethane U 0.00114 0.00442 1.07 11/19/2022 13:54 WG1962462 Dibromomethane U 0.00132 0.00882 1.07 11/19/2022 13:54 WG1962462 1,2-Dichlorobenzene U 0.000750 0.00882 1.07 11/19/2022 13:54 WG1962462 1,3-Dichlorobenzene U 0.00106 0.00882 1.07 11/19/2022 13:54 WG1962462 1,4-Dichlorobenzene U 0.00124 0.00882 1.07 11/19/2022 13:54 WG1962462 Dichlorodifluoromethane U C3 0.00284 0.00442 1.07 11/19/2022 13:54 WG1962462 1,1-Dichloroethane U 0.000866 0.00442 1.07 11/19/2022 13:54 WG1962462 1,2-Dichloroethane U 0.00114 0.00442 1.07 11/19/2022 13:54 WG1962462 1,1-Dichloroethene U 0.00107 0.00442 1.07 11/19/2022 13:54 WG1962462 cis-1,2-Dichloroethene U 0.00129 0.00442 1.07 11/19/2022 13:54 WG1962462 trans-1,2-Dichloroethene U 0.00183 0.00882 1.07 11/19/2022 13:54 WG1962462 1,2-Dichloropropane U 0.00251 0.00882 1.07 11/19/2022 13:54 WG1962462 1,1-Dichloropropene U 0.00143 0.00442 1.07 11/19/2022 13:54 WG1962462 1,3-Dichloropropane U 0.000884 0.00882 1.07 11/19/2022 13:54 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 22 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 22 of 70 SAMPLE RESULTS - 06 L1558771 CS-5 Collected date/time: 11/14/22 13:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00134 0.00442 1.07 11/19/2022 13:54 WG1962462 trans-1,3-Dichloropropene U 0.00201 0.00882 1.07 11/19/2022 13:54 WG1962462 2,2-Dichloropropane U C3 0.00244 0.00442 1.07 11/19/2022 13:54 WG1962462 Di-isopropyl ether U 0.000724 0.00176 1.07 11/19/2022 13:54 WG1962462 Ethylbenzene U 0.00130 0.00442 1.07 11/19/2022 13:54 WG1962462 Hexachloro-1,3-butadiene U 0.0106 0.0442 1.07 11/19/2022 13:54 WG1962462 Isopropylbenzene 0.000838 J 0.000750 0.00442 1.07 11/19/2022 13:54 WG1962462 p-Isopropyltoluene U 0.00450 0.00882 1.07 11/19/2022 13:54 WG1962462 2-Butanone (MEK)U 0.112 0.176 1.07 11/19/2022 13:54 WG1962462 Methylene Chloride U 0.0117 0.0442 1.07 11/19/2022 13:54 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00402 0.0442 1.07 11/19/2022 13:54 WG1962462 Methyl tert-butyl ether U 0.000617 0.00176 1.07 11/19/2022 13:54 WG1962462 Naphthalene U 0.00861 0.0221 1.07 11/19/2022 13:54 WG1962462 n-Propylbenzene U 0.00168 0.00882 1.07 11/19/2022 13:54 WG1962462 Styrene U 0.000404 0.0221 1.07 11/19/2022 13:54 WG1962462 1,1,1,2-Tetrachloroethane U 0.00167 0.00442 1.07 11/19/2022 13:54 WG1962462 1,1,2,2-Tetrachloroethane U 0.00123 0.00442 1.07 11/19/2022 13:54 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00133 0.00442 1.07 11/19/2022 13:54 WG1962462 Tetrachloroethene U 0.00158 0.00442 1.07 11/19/2022 13:54 WG1962462 Toluene 0.00261 J 0.00229 0.00882 1.07 11/19/2022 13:54 WG1962462 1,2,3-Trichlorobenzene U 0.0129 0.0221 1.07 11/19/2022 13:54 WG1962462 1,2,4-Trichlorobenzene U J4 0.00777 0.0221 1.07 11/19/2022 13:54 WG1962462 1,1,1-Trichloroethane U 0.00163 0.00442 1.07 11/19/2022 13:54 WG1962462 1,1,2-Trichloroethane U 0.00105 0.00442 1.07 11/19/2022 13:54 WG1962462 Trichloroethene U 0.00103 0.00176 1.07 11/19/2022 13:54 WG1962462 Trichlorofluoromethane U C3 0.00146 0.00442 1.07 11/19/2022 13:54 WG1962462 1,2,3-Trichloropropane U 0.00285 0.0221 1.07 11/19/2022 13:54 WG1962462 1,2,4-Trimethylbenzene U 0.00279 0.00882 1.07 11/19/2022 13:54 WG1962462 1,2,3-Trimethylbenzene U 0.00279 0.00882 1.07 11/19/2022 13:54 WG1962462 1,3,5-Trimethylbenzene U 0.00353 0.00882 1.07 11/19/2022 13:54 WG1962462 Vinyl chloride U C3 J4 0.00205 0.00442 1.07 11/19/2022 13:54 WG1962462 Xylenes, Total 0.00238 J 0.00155 0.0115 1.07 11/19/2022 13:54 WG1962462 (S) Toluene-d8 105 75.0-131 11/19/2022 13:54 WG1962462 (S) 4-Bromofluorobenzene 101 67.0-138 11/19/2022 13:54 WG1962462 (S) 1,2-Dichloroethane-d4 83.2 70.0-130 11/19/2022 13:54 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.103 0.0144 0.0890 2 11/25/2022 14:01 WG1962878 Acenaphthylene 2.07 0.0125 0.0890 2 11/25/2022 14:01 WG1962878 Anthracene 0.629 0.0159 0.0890 2 11/25/2022 14:01 WG1962878 Benzidine U 0.167 4.46 2 11/25/2022 14:01 WG1962878 Benzo(a)anthracene 1.75 0.0156 0.0890 2 11/25/2022 14:01 WG1962878 Benzo(b)fluoranthene 6.95 0.0830 0.445 10 11/26/2022 17:06 WG1962878 Benzo(k)fluoranthene 1.46 0.0158 0.0890 2 11/25/2022 14:01 WG1962878 Benzo(g,h,i)perylene 1.84 0.0163 0.0890 2 11/25/2022 14:01 WG1962878 Benzo(a)pyrene 5.12 0.0827 0.445 10 11/26/2022 17:06 WG1962878 Bis(2-chlorethoxy)methane U 0.0267 0.890 2 11/25/2022 14:01 WG1962878 Bis(2-chloroethyl)ether U 0.0294 0.890 2 11/25/2022 14:01 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0385 0.890 2 11/25/2022 14:01 WG1962878 4-Bromophenyl-phenylether U 0.0313 0.890 2 11/25/2022 14:01 WG1962878 2-Chloronaphthalene U 0.0156 0.0890 2 11/25/2022 14:01 WG1962878 4-Chlorophenyl-phenylether U 0.0310 0.890 2 11/25/2022 14:01 WG1962878 Chrysene 2.04 0.0176 0.0890 2 11/25/2022 14:01 WG1962878 Dibenz(a,h)anthracene 0.604 0.0247 0.0890 2 11/25/2022 14:01 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 23 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 23 of 70 SAMPLE RESULTS - 06 L1558771 CS-5 Collected date/time: 11/14/22 13:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0263 0.890 2 11/25/2022 14:01 WG1962878 1,3-Dichlorobenzene U 0.0270 0.890 2 11/25/2022 14:01 WG1962878 1,4-Dichlorobenzene U 0.0265 0.890 2 11/25/2022 14:01 WG1962878 3,3-Dichlorobenzidine U 0.0329 0.890 2 11/25/2022 14:01 WG1962878 2,4-Dinitrotoluene U 0.0255 0.890 2 11/25/2022 14:01 WG1962878 2,6-Dinitrotoluene U 0.0291 0.890 2 11/25/2022 14:01 WG1962878 Fluoranthene 2.16 0.0160 0.0890 2 11/25/2022 14:01 WG1962878 Fluorene 0.152 0.0144 0.0890 2 11/25/2022 14:01 WG1962878 Hexachlorobenzene U 0.0315 0.890 2 11/25/2022 14:01 WG1962878 Hexachloro-1,3-butadiene U 0.0299 0.890 2 11/25/2022 14:01 WG1962878 Hexachlorocyclopentadiene U 0.0468 0.890 2 11/25/2022 14:01 WG1962878 Hexachloroethane U 0.0350 0.890 2 11/25/2022 14:01 WG1962878 Indeno(1,2,3-cd)pyrene 2.36 0.0251 0.0890 2 11/25/2022 14:01 WG1962878 Isophorone U 0.0273 0.890 2 11/25/2022 14:01 WG1962878 Naphthalene 0.220 0.0223 0.0890 2 11/25/2022 14:01 WG1962878 Nitrobenzene U 0.0310 0.890 2 11/25/2022 14:01 WG1962878 n-Nitrosodimethylamine U 0.132 0.890 2 11/25/2022 14:01 WG1962878 n-Nitrosodiphenylamine U 0.0673 0.890 2 11/25/2022 14:01 WG1962878 n-Nitrosodi-n-propylamine U 0.0297 0.890 2 11/25/2022 14:01 WG1962878 Phenanthrene 0.757 0.0176 0.0890 2 11/25/2022 14:01 WG1962878 Benzylbutyl phthalate U 0.0278 0.890 2 11/25/2022 14:01 WG1962878 Bis(2-ethylhexyl)phthalate U 0.113 0.890 2 11/25/2022 14:01 WG1962878 Di-n-butyl phthalate U 0.0305 0.890 2 11/25/2022 14:01 WG1962878 Diethyl phthalate U 0.0294 0.890 2 11/25/2022 14:01 WG1962878 Dimethyl phthalate U 0.188 0.890 2 11/25/2022 14:01 WG1962878 Di-n-octyl phthalate U 0.0601 0.890 2 11/25/2022 14:01 WG1962878 Pyrene 2.63 0.0174 0.0890 2 11/25/2022 14:01 WG1962878 1,2,4-Trichlorobenzene U 0.0278 0.890 2 11/25/2022 14:01 WG1962878 4-Chloro-3-methylphenol U 0.0289 0.890 2 11/25/2022 14:01 WG1962878 2-Chlorophenol U 0.0294 0.890 2 11/25/2022 14:01 WG1962878 2,4-Dichlorophenol U 0.0259 0.890 2 11/25/2022 14:01 WG1962878 2,4-Dimethylphenol U 0.0232 0.890 2 11/25/2022 14:01 WG1962878 4,6-Dinitro-2-methylphenol U 0.202 0.890 2 11/25/2022 14:01 WG1962878 2,4-Dinitrophenol U 0.208 0.890 2 11/25/2022 14:01 WG1962878 2-Nitrophenol U 0.0318 0.890 2 11/25/2022 14:01 WG1962878 4-Nitrophenol U 0.0278 0.890 2 11/25/2022 14:01 WG1962878 Pentachlorophenol U 0.0239 0.890 2 11/25/2022 14:01 WG1962878 Phenol U 0.0358 0.890 2 11/25/2022 14:01 WG1962878 2,4,6-Trichlorophenol U 0.0286 0.890 2 11/25/2022 14:01 WG1962878 (S) 2-Fluorophenol 70.0 12.0-120 11/25/2022 14:01 WG1962878 (S) 2-Fluorophenol 62.3 12.0-120 11/26/2022 17:06 WG1962878 (S) Phenol-d5 60.2 10.0-120 11/26/2022 17:06 WG1962878 (S) Phenol-d5 67.7 10.0-120 11/25/2022 14:01 WG1962878 (S) Nitrobenzene-d5 64.2 10.0-122 11/25/2022 14:01 WG1962878 (S) Nitrobenzene-d5 59.7 10.0-122 11/26/2022 17:06 WG1962878 (S) 2-Fluorobiphenyl 74.8 15.0-120 11/26/2022 17:06 WG1962878 (S) 2-Fluorobiphenyl 64.2 15.0-120 11/25/2022 14:01 WG1962878 (S) 2,4,6-Tribromophenol 74.2 10.0-127 11/26/2022 17:06 WG1962878 (S) 2,4,6-Tribromophenol 91.7 10.0-127 11/25/2022 14:01 WG1962878 (S) p-Terphenyl-d14 87.3 10.0-120 11/26/2022 17:06 WG1962878 (S) p-Terphenyl-d14 73.9 10.0-120 11/25/2022 14:01 WG1962878 Sample Narrative: L1558771-06 WG1962878: Dilution due to matrix impact during extract concentration procedure 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 24 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 24 of 70 SAMPLE RESULTS - 07 L1558771 CS-5 (DUP) Collected date/time: 11/14/22 13:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 83.6 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0502 0.0215 0.0478 1 11/21/2022 15:09 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.90 0.120 1.20 5 12/01/2022 18:56 WG1962098 Barium 44.0 0.182 2.99 5 12/01/2022 18:56 WG1962098 Cadmium 0.380 J 0.102 1.20 5 12/01/2022 18:56 WG1962098 Chromium 31.5 0.354 5.98 5 12/01/2022 18:56 WG1962098 Lead 67.3 0.118 2.39 5 12/01/2022 18:56 WG1962098 Selenium 0.704 J 0.215 2.99 5 12/01/2022 18:56 WG1962098 Silver U 0.103 0.598 5 12/01/2022 18:56 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0509 0.0697 1 11/19/2022 14:12 WG1962462 Acrylonitrile U 0.00504 0.0174 1 11/19/2022 14:12 WG1962462 Benzene U 0.000651 0.00139 1 11/19/2022 14:12 WG1962462 Bromobenzene U 0.00126 0.0174 1 11/19/2022 14:12 WG1962462 Bromodichloromethane U 0.00101 0.00349 1 11/19/2022 14:12 WG1962462 Bromoform U 0.00163 0.0349 1 11/19/2022 14:12 WG1962462 Bromomethane U C3 0.00275 0.0174 1 11/19/2022 14:12 WG1962462 n-Butylbenzene U 0.00732 0.0174 1 11/19/2022 14:12 WG1962462 sec-Butylbenzene U 0.00402 0.0174 1 11/19/2022 14:12 WG1962462 tert-Butylbenzene U 0.00272 0.00697 1 11/19/2022 14:12 WG1962462 Carbon tetrachloride U 0.00125 0.00697 1 11/19/2022 14:12 WG1962462 Chlorobenzene U 0.000293 0.00349 1 11/19/2022 14:12 WG1962462 Chlorodibromomethane U 0.000854 0.00349 1 11/19/2022 14:12 WG1962462 Chloroethane U C3 J4 0.00237 0.00697 1 11/19/2022 14:12 WG1962462 Chloroform 0.00321 J 0.00144 0.00349 1 11/19/2022 14:12 WG1962462 Chloromethane U C3 0.00607 0.0174 1 11/19/2022 14:12 WG1962462 2-Chlorotoluene U 0.00121 0.00349 1 11/19/2022 14:12 WG1962462 4-Chlorotoluene U 0.000628 0.00697 1 11/19/2022 14:12 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00544 0.0349 1 11/19/2022 14:12 WG1962462 1,2-Dibromoethane U 0.000904 0.00349 1 11/19/2022 14:12 WG1962462 Dibromomethane U 0.00105 0.00697 1 11/19/2022 14:12 WG1962462 1,2-Dichlorobenzene U 0.000593 0.00697 1 11/19/2022 14:12 WG1962462 1,3-Dichlorobenzene U 0.000837 0.00697 1 11/19/2022 14:12 WG1962462 1,4-Dichlorobenzene U 0.000976 0.00697 1 11/19/2022 14:12 WG1962462 Dichlorodifluoromethane U C3 0.00225 0.00349 1 11/19/2022 14:12 WG1962462 1,1-Dichloroethane U 0.000685 0.00349 1 11/19/2022 14:12 WG1962462 1,2-Dichloroethane U 0.000905 0.00349 1 11/19/2022 14:12 WG1962462 1,1-Dichloroethene U 0.000845 0.00349 1 11/19/2022 14:12 WG1962462 cis-1,2-Dichloroethene U 0.00102 0.00349 1 11/19/2022 14:12 WG1962462 trans-1,2-Dichloroethene U 0.00145 0.00697 1 11/19/2022 14:12 WG1962462 1,2-Dichloropropane U 0.00198 0.00697 1 11/19/2022 14:12 WG1962462 1,1-Dichloropropene U 0.00113 0.00349 1 11/19/2022 14:12 WG1962462 1,3-Dichloropropane U 0.000699 0.00697 1 11/19/2022 14:12 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 25 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 25 of 70 SAMPLE RESULTS - 07 L1558771 CS-5 (DUP) Collected date/time: 11/14/22 13:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00106 0.00349 1 11/19/2022 14:12 WG1962462 trans-1,3-Dichloropropene U 0.00159 0.00697 1 11/19/2022 14:12 WG1962462 2,2-Dichloropropane U C3 0.00192 0.00349 1 11/19/2022 14:12 WG1962462 Di-isopropyl ether U 0.000572 0.00139 1 11/19/2022 14:12 WG1962462 Ethylbenzene U 0.00103 0.00349 1 11/19/2022 14:12 WG1962462 Hexachloro-1,3-butadiene U 0.00837 0.0349 1 11/19/2022 14:12 WG1962462 Isopropylbenzene U 0.000593 0.00349 1 11/19/2022 14:12 WG1962462 p-Isopropyltoluene U 0.00356 0.00697 1 11/19/2022 14:12 WG1962462 2-Butanone (MEK)U 0.0886 0.139 1 11/19/2022 14:12 WG1962462 Methylene Chloride U 0.00926 0.0349 1 11/19/2022 14:12 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00318 0.0349 1 11/19/2022 14:12 WG1962462 Methyl tert-butyl ether U 0.000488 0.00139 1 11/19/2022 14:12 WG1962462 Naphthalene U 0.00681 0.0174 1 11/19/2022 14:12 WG1962462 n-Propylbenzene U 0.00133 0.00697 1 11/19/2022 14:12 WG1962462 Styrene U 0.000319 0.0174 1 11/19/2022 14:12 WG1962462 1,1,1,2-Tetrachloroethane U 0.00132 0.00349 1 11/19/2022 14:12 WG1962462 1,1,2,2-Tetrachloroethane U 0.000969 0.00349 1 11/19/2022 14:12 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00105 0.00349 1 11/19/2022 14:12 WG1962462 Tetrachloroethene U 0.00125 0.00349 1 11/19/2022 14:12 WG1962462 Toluene 0.00232 J 0.00181 0.00697 1 11/19/2022 14:12 WG1962462 1,2,3-Trichlorobenzene U 0.0102 0.0174 1 11/19/2022 14:12 WG1962462 1,2,4-Trichlorobenzene U J4 0.00614 0.0174 1 11/19/2022 14:12 WG1962462 1,1,1-Trichloroethane U 0.00129 0.00349 1 11/19/2022 14:12 WG1962462 1,1,2-Trichloroethane U 0.000833 0.00349 1 11/19/2022 14:12 WG1962462 Trichloroethene U 0.000815 0.00139 1 11/19/2022 14:12 WG1962462 Trichlorofluoromethane U C3 0.00115 0.00349 1 11/19/2022 14:12 WG1962462 1,2,3-Trichloropropane U 0.00226 0.0174 1 11/19/2022 14:12 WG1962462 1,2,4-Trimethylbenzene U 0.00220 0.00697 1 11/19/2022 14:12 WG1962462 1,2,3-Trimethylbenzene U 0.00220 0.00697 1 11/19/2022 14:12 WG1962462 1,3,5-Trimethylbenzene U 0.00279 0.00697 1 11/19/2022 14:12 WG1962462 Vinyl chloride U C3 J4 0.00162 0.00349 1 11/19/2022 14:12 WG1962462 Xylenes, Total 0.00487 J 0.00123 0.00907 1 11/19/2022 14:12 WG1962462 (S) Toluene-d8 107 75.0-131 11/19/2022 14:12 WG1962462 (S) 4-Bromofluorobenzene 99.0 67.0-138 11/19/2022 14:12 WG1962462 (S) 1,2-Dichloroethane-d4 81.4 70.0-130 11/19/2022 14:12 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.0512 J 0.0129 0.0797 2 11/25/2022 14:21 WG1962878 Acenaphthylene 0.0677 J 0.0112 0.0797 2 11/25/2022 14:21 WG1962878 Anthracene 0.105 0.0142 0.0797 2 11/25/2022 14:21 WG1962878 Benzidine U 0.150 4.00 2 11/25/2022 14:21 WG1962878 Benzo(a)anthracene 0.280 0.0140 0.0797 2 11/25/2022 14:21 WG1962878 Benzo(b)fluoranthene 0.390 0.0148 0.0797 2 11/25/2022 14:21 WG1962878 Benzo(k)fluoranthene 0.127 0.0141 0.0797 2 11/25/2022 14:21 WG1962878 Benzo(g,h,i)perylene 0.101 0.0146 0.0797 2 11/25/2022 14:21 WG1962878 Benzo(a)pyrene 0.286 0.0148 0.0797 2 11/25/2022 14:21 WG1962878 Bis(2-chlorethoxy)methane U 0.0239 0.797 2 11/25/2022 14:21 WG1962878 Bis(2-chloroethyl)ether U 0.0263 0.797 2 11/25/2022 14:21 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0345 0.797 2 11/25/2022 14:21 WG1962878 4-Bromophenyl-phenylether U 0.0280 0.797 2 11/25/2022 14:21 WG1962878 2-Chloronaphthalene U 0.0140 0.0797 2 11/25/2022 14:21 WG1962878 4-Chlorophenyl-phenylether U 0.0278 0.797 2 11/25/2022 14:21 WG1962878 Chrysene 0.291 0.0158 0.0797 2 11/25/2022 14:21 WG1962878 Dibenz(a,h)anthracene 0.0315 J 0.0221 0.0797 2 11/25/2022 14:21 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 26 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 26 of 70 SAMPLE RESULTS - 07 L1558771 CS-5 (DUP) Collected date/time: 11/14/22 13:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0236 0.797 2 11/25/2022 14:21 WG1962878 1,3-Dichlorobenzene U 0.0242 0.797 2 11/25/2022 14:21 WG1962878 1,4-Dichlorobenzene U 0.0237 0.797 2 11/25/2022 14:21 WG1962878 3,3-Dichlorobenzidine U 0.0294 0.797 2 11/25/2022 14:21 WG1962878 2,4-Dinitrotoluene U 0.0228 0.797 2 11/25/2022 14:21 WG1962878 2,6-Dinitrotoluene U 0.0261 0.797 2 11/25/2022 14:21 WG1962878 Fluoranthene 0.581 0.0144 0.0797 2 11/25/2022 14:21 WG1962878 Fluorene 0.0434 J 0.0129 0.0797 2 11/25/2022 14:21 WG1962878 Hexachlorobenzene U 0.0282 0.797 2 11/25/2022 14:21 WG1962878 Hexachloro-1,3-butadiene U 0.0268 0.797 2 11/25/2022 14:21 WG1962878 Hexachlorocyclopentadiene U 0.0419 0.797 2 11/25/2022 14:21 WG1962878 Hexachloroethane U 0.0313 0.797 2 11/25/2022 14:21 WG1962878 Indeno(1,2,3-cd)pyrene 0.122 0.0225 0.0797 2 11/25/2022 14:21 WG1962878 Isophorone U 0.0244 0.797 2 11/25/2022 14:21 WG1962878 Naphthalene 0.0230 J 0.0200 0.0797 2 11/25/2022 14:21 WG1962878 Nitrobenzene U 0.0278 0.797 2 11/25/2022 14:21 WG1962878 n-Nitrosodimethylamine U 0.118 0.797 2 11/25/2022 14:21 WG1962878 n-Nitrosodiphenylamine U 0.0603 0.797 2 11/25/2022 14:21 WG1962878 n-Nitrosodi-n-propylamine U 0.0266 0.797 2 11/25/2022 14:21 WG1962878 Phenanthrene 0.416 0.0158 0.0797 2 11/25/2022 14:21 WG1962878 Benzylbutyl phthalate U 0.0249 0.797 2 11/25/2022 14:21 WG1962878 Bis(2-ethylhexyl)phthalate U 0.101 0.797 2 11/25/2022 14:21 WG1962878 Di-n-butyl phthalate U 0.0273 0.797 2 11/25/2022 14:21 WG1962878 Diethyl phthalate U 0.0263 0.797 2 11/25/2022 14:21 WG1962878 Dimethyl phthalate U 0.169 0.797 2 11/25/2022 14:21 WG1962878 Di-n-octyl phthalate U 0.0538 0.797 2 11/25/2022 14:21 WG1962878 Pyrene 0.484 0.0156 0.0797 2 11/25/2022 14:21 WG1962878 1,2,4-Trichlorobenzene U 0.0249 0.797 2 11/25/2022 14:21 WG1962878 4-Chloro-3-methylphenol U 0.0258 0.797 2 11/25/2022 14:21 WG1962878 2-Chlorophenol U 0.0263 0.797 2 11/25/2022 14:21 WG1962878 2,4-Dichlorophenol U 0.0232 0.797 2 11/25/2022 14:21 WG1962878 2,4-Dimethylphenol U 0.0208 0.797 2 11/25/2022 14:21 WG1962878 4,6-Dinitro-2-methylphenol U 0.181 0.797 2 11/25/2022 14:21 WG1962878 2,4-Dinitrophenol U 0.187 0.797 2 11/25/2022 14:21 WG1962878 2-Nitrophenol U 0.0285 0.797 2 11/25/2022 14:21 WG1962878 4-Nitrophenol U 0.0249 0.797 2 11/25/2022 14:21 WG1962878 Pentachlorophenol U 0.0214 0.797 2 11/25/2022 14:21 WG1962878 Phenol U 0.0321 0.797 2 11/25/2022 14:21 WG1962878 2,4,6-Trichlorophenol U 0.0256 0.797 2 11/25/2022 14:21 WG1962878 (S) 2-Fluorophenol 68.3 12.0-120 11/25/2022 14:21 WG1962878 (S) Phenol-d5 63.9 10.0-120 11/25/2022 14:21 WG1962878 (S) Nitrobenzene-d5 61.9 10.0-122 11/25/2022 14:21 WG1962878 (S) 2-Fluorobiphenyl 60.7 15.0-120 11/25/2022 14:21 WG1962878 (S) 2,4,6-Tribromophenol 90.4 10.0-127 11/25/2022 14:21 WG1962878 (S) p-Terphenyl-d14 69.2 10.0-120 11/25/2022 14:21 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 27 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 27 of 70 SAMPLE RESULTS - 08 L1558771 CS-6 Collected date/time: 11/14/22 13:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 80.3 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0638 0.0224 0.0498 1 11/21/2022 15:15 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 7.69 0.125 1.25 5 12/01/2022 19:09 WG1962098 Barium 33.2 0.189 3.11 5 12/01/2022 19:09 WG1962098 Cadmium U 0.106 1.25 5 12/01/2022 19:09 WG1962098 Chromium 26.6 0.369 6.23 5 12/01/2022 19:09 WG1962098 Lead 46.8 0.123 2.49 5 12/01/2022 19:09 WG1962098 Selenium 0.827 J 0.224 3.11 5 12/01/2022 19:09 WG1962098 Silver U 0.108 0.623 5 12/01/2022 19:09 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0559 0.0766 1 11/19/2022 14:32 WG1962462 Acrylonitrile U 0.00553 0.0192 1 11/19/2022 14:32 WG1962462 Benzene U 0.000716 0.00153 1 11/19/2022 14:32 WG1962462 Bromobenzene U 0.00138 0.0192 1 11/19/2022 14:32 WG1962462 Bromodichloromethane U 0.00111 0.00383 1 11/19/2022 14:32 WG1962462 Bromoform U 0.00179 0.0383 1 11/19/2022 14:32 WG1962462 Bromomethane U C3 0.00302 0.0192 1 11/19/2022 14:32 WG1962462 n-Butylbenzene U 0.00804 0.0192 1 11/19/2022 14:32 WG1962462 sec-Butylbenzene U 0.00441 0.0192 1 11/19/2022 14:32 WG1962462 tert-Butylbenzene U 0.00299 0.00766 1 11/19/2022 14:32 WG1962462 Carbon tetrachloride U 0.00138 0.00766 1 11/19/2022 14:32 WG1962462 Chlorobenzene U 0.000322 0.00383 1 11/19/2022 14:32 WG1962462 Chlorodibromomethane U 0.000938 0.00383 1 11/19/2022 14:32 WG1962462 Chloroethane U C3 J4 0.00260 0.00766 1 11/19/2022 14:32 WG1962462 Chloroform 0.00332 J 0.00158 0.00383 1 11/19/2022 14:32 WG1962462 Chloromethane U C3 0.00667 0.0192 1 11/19/2022 14:32 WG1962462 2-Chlorotoluene U 0.00133 0.00383 1 11/19/2022 14:32 WG1962462 4-Chlorotoluene U 0.000689 0.00766 1 11/19/2022 14:32 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00598 0.0383 1 11/19/2022 14:32 WG1962462 1,2-Dibromoethane U 0.000993 0.00383 1 11/19/2022 14:32 WG1962462 Dibromomethane U 0.00115 0.00766 1 11/19/2022 14:32 WG1962462 1,2-Dichlorobenzene U 0.000651 0.00766 1 11/19/2022 14:32 WG1962462 1,3-Dichlorobenzene U 0.000919 0.00766 1 11/19/2022 14:32 WG1962462 1,4-Dichlorobenzene U 0.00107 0.00766 1 11/19/2022 14:32 WG1962462 Dichlorodifluoromethane U C3 0.00247 0.00383 1 11/19/2022 14:32 WG1962462 1,1-Dichloroethane U 0.000752 0.00383 1 11/19/2022 14:32 WG1962462 1,2-Dichloroethane U 0.000994 0.00383 1 11/19/2022 14:32 WG1962462 1,1-Dichloroethene U 0.000929 0.00383 1 11/19/2022 14:32 WG1962462 cis-1,2-Dichloroethene U 0.00112 0.00383 1 11/19/2022 14:32 WG1962462 trans-1,2-Dichloroethene U 0.00159 0.00766 1 11/19/2022 14:32 WG1962462 1,2-Dichloropropane U 0.00218 0.00766 1 11/19/2022 14:32 WG1962462 1,1-Dichloropropene U 0.00124 0.00383 1 11/19/2022 14:32 WG1962462 1,3-Dichloropropane U 0.000768 0.00766 1 11/19/2022 14:32 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 28 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 28 of 70 SAMPLE RESULTS - 08 L1558771 CS-6 Collected date/time: 11/14/22 13:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00116 0.00383 1 11/19/2022 14:32 WG1962462 trans-1,3-Dichloropropene U 0.00175 0.00766 1 11/19/2022 14:32 WG1962462 2,2-Dichloropropane U C3 0.00211 0.00383 1 11/19/2022 14:32 WG1962462 Di-isopropyl ether U 0.000628 0.00153 1 11/19/2022 14:32 WG1962462 Ethylbenzene U 0.00113 0.00383 1 11/19/2022 14:32 WG1962462 Hexachloro-1,3-butadiene U 0.00919 0.0383 1 11/19/2022 14:32 WG1962462 Isopropylbenzene U 0.000651 0.00383 1 11/19/2022 14:32 WG1962462 p-Isopropyltoluene U 0.00391 0.00766 1 11/19/2022 14:32 WG1962462 2-Butanone (MEK)U 0.0973 0.153 1 11/19/2022 14:32 WG1962462 Methylene Chloride U 0.0102 0.0383 1 11/19/2022 14:32 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00349 0.0383 1 11/19/2022 14:32 WG1962462 Methyl tert-butyl ether U 0.000536 0.00153 1 11/19/2022 14:32 WG1962462 Naphthalene 0.00834 J 0.00748 0.0192 1 11/19/2022 14:32 WG1962462 n-Propylbenzene U 0.00146 0.00766 1 11/19/2022 14:32 WG1962462 Styrene U 0.000351 0.0192 1 11/19/2022 14:32 WG1962462 1,1,1,2-Tetrachloroethane U 0.00145 0.00383 1 11/19/2022 14:32 WG1962462 1,1,2,2-Tetrachloroethane U 0.00106 0.00383 1 11/19/2022 14:32 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00116 0.00383 1 11/19/2022 14:32 WG1962462 Tetrachloroethene U 0.00137 0.00383 1 11/19/2022 14:32 WG1962462 Toluene 0.00277 J 0.00199 0.00766 1 11/19/2022 14:32 WG1962462 1,2,3-Trichlorobenzene U 0.0112 0.0192 1 11/19/2022 14:32 WG1962462 1,2,4-Trichlorobenzene U J4 0.00674 0.0192 1 11/19/2022 14:32 WG1962462 1,1,1-Trichloroethane U 0.00141 0.00383 1 11/19/2022 14:32 WG1962462 1,1,2-Trichloroethane U 0.000915 0.00383 1 11/19/2022 14:32 WG1962462 Trichloroethene U 0.000895 0.00153 1 11/19/2022 14:32 WG1962462 Trichlorofluoromethane U C3 0.00127 0.00383 1 11/19/2022 14:32 WG1962462 1,2,3-Trichloropropane U 0.00248 0.0192 1 11/19/2022 14:32 WG1962462 1,2,4-Trimethylbenzene U 0.00242 0.00766 1 11/19/2022 14:32 WG1962462 1,2,3-Trimethylbenzene U 0.00242 0.00766 1 11/19/2022 14:32 WG1962462 1,3,5-Trimethylbenzene U 0.00306 0.00766 1 11/19/2022 14:32 WG1962462 Vinyl chloride U C3 J4 0.00178 0.00383 1 11/19/2022 14:32 WG1962462 Xylenes, Total 0.00218 J 0.00135 0.00996 1 11/19/2022 14:32 WG1962462 (S) Toluene-d8 103 75.0-131 11/19/2022 14:32 WG1962462 (S) 4-Bromofluorobenzene 101 67.0-138 11/19/2022 14:32 WG1962462 (S) 1,2-Dichloroethane-d4 82.1 70.0-130 11/19/2022 14:32 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.0644 J 0.0135 0.0830 2 11/25/2022 12:40 WG1962878 Acenaphthylene 0.496 0.0117 0.0830 2 11/25/2022 12:40 WG1962878 Anthracene 0.340 0.0148 0.0830 2 11/25/2022 12:40 WG1962878 Benzidine U J6 0.156 4.16 2 11/25/2022 12:40 WG1962878 Benzo(a)anthracene 1.09 J6 0.0146 0.0830 2 11/25/2022 12:40 WG1962878 Benzo(b)fluoranthene 1.73 J6 0.0154 0.0830 2 11/25/2022 12:40 WG1962878 Benzo(k)fluoranthene 0.494 0.0147 0.0830 2 11/25/2022 12:40 WG1962878 Benzo(g,h,i)perylene 0.831 J3 J6 0.0152 0.0830 2 11/25/2022 12:40 WG1962878 Benzo(a)pyrene 1.53 J6 0.0154 0.0830 2 11/25/2022 12:40 WG1962878 Bis(2-chlorethoxy)methane U 0.0249 0.830 2 11/25/2022 12:40 WG1962878 Bis(2-chloroethyl)ether U 0.0274 0.830 2 11/25/2022 12:40 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0359 0.830 2 11/25/2022 12:40 WG1962878 4-Bromophenyl-phenylether U 0.0291 0.830 2 11/25/2022 12:40 WG1962878 2-Chloronaphthalene U 0.0146 0.0830 2 11/25/2022 12:40 WG1962878 4-Chlorophenyl-phenylether U 0.0289 0.830 2 11/25/2022 12:40 WG1962878 Chrysene 1.32 J6 0.0164 0.0830 2 11/25/2022 12:40 WG1962878 Dibenz(a,h)anthracene 0.243 0.0230 0.0830 2 11/25/2022 12:40 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 29 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 29 of 70 SAMPLE RESULTS - 08 L1558771 CS-6 Collected date/time: 11/14/22 13:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0245 0.830 2 11/25/2022 12:40 WG1962878 1,3-Dichlorobenzene U 0.0252 0.830 2 11/25/2022 12:40 WG1962878 1,4-Dichlorobenzene U 0.0247 0.830 2 11/25/2022 12:40 WG1962878 3,3-Dichlorobenzidine U J3 0.0306 0.830 2 11/25/2022 12:40 WG1962878 2,4-Dinitrotoluene U 0.0238 0.830 2 11/25/2022 12:40 WG1962878 2,6-Dinitrotoluene U 0.0272 0.830 2 11/25/2022 12:40 WG1962878 Fluoranthene 1.47 J6 0.0149 0.0830 2 11/25/2022 12:40 WG1962878 Fluorene 0.189 0.0135 0.0830 2 11/25/2022 12:40 WG1962878 Hexachlorobenzene U 0.0294 0.830 2 11/25/2022 12:40 WG1962878 Hexachloro-1,3-butadiene U 0.0279 0.830 2 11/25/2022 12:40 WG1962878 Hexachlorocyclopentadiene U J6 0.0436 0.830 2 11/25/2022 12:40 WG1962878 Hexachloroethane U 0.0326 0.830 2 11/25/2022 12:40 WG1962878 Indeno(1,2,3-cd)pyrene 0.882 J6 0.0234 0.0830 2 11/25/2022 12:40 WG1962878 Isophorone U 0.0254 0.830 2 11/25/2022 12:40 WG1962878 Naphthalene 0.167 0.0208 0.0830 2 11/25/2022 12:40 WG1962878 Nitrobenzene U 0.0289 0.830 2 11/25/2022 12:40 WG1962878 n-Nitrosodimethylamine U 0.123 0.830 2 11/25/2022 12:40 WG1962878 n-Nitrosodiphenylamine U 0.0628 0.830 2 11/25/2022 12:40 WG1962878 n-Nitrosodi-n-propylamine U 0.0277 0.830 2 11/25/2022 12:40 WG1962878 Phenanthrene 1.54 J6 0.0164 0.0830 2 11/25/2022 12:40 WG1962878 Benzylbutyl phthalate U 0.0259 0.830 2 11/25/2022 12:40 WG1962878 Bis(2-ethylhexyl)phthalate U 0.105 0.830 2 11/25/2022 12:40 WG1962878 Di-n-butyl phthalate U 0.0284 0.830 2 11/25/2022 12:40 WG1962878 Diethyl phthalate U 0.0274 0.830 2 11/25/2022 12:40 WG1962878 Dimethyl phthalate U 0.176 0.830 2 11/25/2022 12:40 WG1962878 Di-n-octyl phthalate U 0.0561 0.830 2 11/25/2022 12:40 WG1962878 Pyrene 1.94 J6 0.0162 0.0830 2 11/25/2022 12:40 WG1962878 1,2,4-Trichlorobenzene U 0.0259 0.830 2 11/25/2022 12:40 WG1962878 4-Chloro-3-methylphenol U 0.0269 0.830 2 11/25/2022 12:40 WG1962878 2-Chlorophenol U 0.0274 0.830 2 11/25/2022 12:40 WG1962878 2,4-Dichlorophenol U 0.0242 0.830 2 11/25/2022 12:40 WG1962878 2,4-Dimethylphenol U 0.0217 0.830 2 11/25/2022 12:40 WG1962878 4,6-Dinitro-2-methylphenol U 0.188 0.830 2 11/25/2022 12:40 WG1962878 2,4-Dinitrophenol U 0.194 0.830 2 11/25/2022 12:40 WG1962878 2-Nitrophenol U 0.0296 0.830 2 11/25/2022 12:40 WG1962878 4-Nitrophenol U 0.0259 0.830 2 11/25/2022 12:40 WG1962878 Pentachlorophenol U 0.0223 0.830 2 11/25/2022 12:40 WG1962878 Phenol U 0.0334 0.830 2 11/25/2022 12:40 WG1962878 2,4,6-Trichlorophenol U 0.0267 0.830 2 11/25/2022 12:40 WG1962878 (S) 2-Fluorophenol 76.5 12.0-120 11/25/2022 12:40 WG1962878 (S) Phenol-d5 72.4 10.0-120 11/25/2022 12:40 WG1962878 (S) Nitrobenzene-d5 68.8 10.0-122 11/25/2022 12:40 WG1962878 (S) 2-Fluorobiphenyl 67.0 15.0-120 11/25/2022 12:40 WG1962878 (S) 2,4,6-Tribromophenol 100 10.0-127 11/25/2022 12:40 WG1962878 (S) p-Terphenyl-d14 76.1 10.0-120 11/25/2022 12:40 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 30 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 30 of 70 SAMPLE RESULTS - 09 L1558771 CS-6-A Collected date/time: 11/14/22 13:15 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 84.0 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0669 0.0214 0.0476 1 11/21/2022 15:17 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 10.7 0.119 1.19 5 12/01/2022 19:12 WG1962098 Barium 46.8 0.181 2.98 5 12/01/2022 19:12 WG1962098 Cadmium U 0.102 1.19 5 12/01/2022 19:12 WG1962098 Chromium 37.0 0.352 5.95 5 12/01/2022 19:12 WG1962098 Lead 46.9 0.118 2.38 5 12/01/2022 19:12 WG1962098 Selenium 0.882 J 0.214 2.98 5 12/01/2022 19:12 WG1962098 Silver U 0.103 0.595 5 12/01/2022 19:12 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.154 0.0515 0.0705 1 11/19/2022 14:51 WG1962462 Acrylonitrile U 0.00509 0.0176 1 11/19/2022 14:51 WG1962462 Benzene U 0.000659 0.00141 1 11/19/2022 14:51 WG1962462 Bromobenzene U 0.00127 0.0176 1 11/19/2022 14:51 WG1962462 Bromodichloromethane U 0.00102 0.00353 1 11/19/2022 14:51 WG1962462 Bromoform U 0.00165 0.0353 1 11/19/2022 14:51 WG1962462 Bromomethane U C3 0.00278 0.0176 1 11/19/2022 14:51 WG1962462 n-Butylbenzene U 0.00741 0.0176 1 11/19/2022 14:51 WG1962462 sec-Butylbenzene U 0.00406 0.0176 1 11/19/2022 14:51 WG1962462 tert-Butylbenzene U 0.00275 0.00705 1 11/19/2022 14:51 WG1962462 Carbon tetrachloride U 0.00127 0.00705 1 11/19/2022 14:51 WG1962462 Chlorobenzene U 0.000296 0.00353 1 11/19/2022 14:51 WG1962462 Chlorodibromomethane U 0.000863 0.00353 1 11/19/2022 14:51 WG1962462 Chloroethane U C3 J4 0.00240 0.00705 1 11/19/2022 14:51 WG1962462 Chloroform 0.00346 J 0.00145 0.00353 1 11/19/2022 14:51 WG1962462 Chloromethane U C3 0.00614 0.0176 1 11/19/2022 14:51 WG1962462 2-Chlorotoluene U 0.00122 0.00353 1 11/19/2022 14:51 WG1962462 4-Chlorotoluene U 0.000635 0.00705 1 11/19/2022 14:51 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00550 0.0353 1 11/19/2022 14:51 WG1962462 1,2-Dibromoethane U 0.000914 0.00353 1 11/19/2022 14:51 WG1962462 Dibromomethane U 0.00106 0.00705 1 11/19/2022 14:51 WG1962462 1,2-Dichlorobenzene U 0.000600 0.00705 1 11/19/2022 14:51 WG1962462 1,3-Dichlorobenzene U 0.000846 0.00705 1 11/19/2022 14:51 WG1962462 1,4-Dichlorobenzene U 0.000988 0.00705 1 11/19/2022 14:51 WG1962462 Dichlorodifluoromethane U C3 0.00227 0.00353 1 11/19/2022 14:51 WG1962462 1,1-Dichloroethane U 0.000693 0.00353 1 11/19/2022 14:51 WG1962462 1,2-Dichloroethane U 0.000916 0.00353 1 11/19/2022 14:51 WG1962462 1,1-Dichloroethene U 0.000855 0.00353 1 11/19/2022 14:51 WG1962462 cis-1,2-Dichloroethene U 0.00104 0.00353 1 11/19/2022 14:51 WG1962462 trans-1,2-Dichloroethene U 0.00147 0.00705 1 11/19/2022 14:51 WG1962462 1,2-Dichloropropane U 0.00200 0.00705 1 11/19/2022 14:51 WG1962462 1,1-Dichloropropene U 0.00114 0.00353 1 11/19/2022 14:51 WG1962462 1,3-Dichloropropane U 0.000707 0.00705 1 11/19/2022 14:51 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 31 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 31 of 70 SAMPLE RESULTS - 09 L1558771 CS-6-A Collected date/time: 11/14/22 13:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00107 0.00353 1 11/19/2022 14:51 WG1962462 trans-1,3-Dichloropropene U 0.00161 0.00705 1 11/19/2022 14:51 WG1962462 2,2-Dichloropropane U C3 0.00195 0.00353 1 11/19/2022 14:51 WG1962462 Di-isopropyl ether U 0.000578 0.00141 1 11/19/2022 14:51 WG1962462 Ethylbenzene 0.00133 J 0.00104 0.00353 1 11/19/2022 14:51 WG1962462 Hexachloro-1,3-butadiene U 0.00846 0.0353 1 11/19/2022 14:51 WG1962462 Isopropylbenzene U 0.000600 0.00353 1 11/19/2022 14:51 WG1962462 p-Isopropyltoluene U 0.00360 0.00705 1 11/19/2022 14:51 WG1962462 2-Butanone (MEK)U 0.0896 0.141 1 11/19/2022 14:51 WG1962462 Methylene Chloride U 0.00937 0.0353 1 11/19/2022 14:51 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00322 0.0353 1 11/19/2022 14:51 WG1962462 Methyl tert-butyl ether U 0.000494 0.00141 1 11/19/2022 14:51 WG1962462 Naphthalene U 0.00688 0.0176 1 11/19/2022 14:51 WG1962462 n-Propylbenzene U 0.00134 0.00705 1 11/19/2022 14:51 WG1962462 Styrene U 0.000323 0.0176 1 11/19/2022 14:51 WG1962462 1,1,1,2-Tetrachloroethane U 0.00134 0.00353 1 11/19/2022 14:51 WG1962462 1,1,2,2-Tetrachloroethane U 0.000980 0.00353 1 11/19/2022 14:51 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00106 0.00353 1 11/19/2022 14:51 WG1962462 Tetrachloroethene U 0.00126 0.00353 1 11/19/2022 14:51 WG1962462 Toluene 0.00219 J 0.00183 0.00705 1 11/19/2022 14:51 WG1962462 1,2,3-Trichlorobenzene U 0.0103 0.0176 1 11/19/2022 14:51 WG1962462 1,2,4-Trichlorobenzene U J4 0.00621 0.0176 1 11/19/2022 14:51 WG1962462 1,1,1-Trichloroethane U 0.00130 0.00353 1 11/19/2022 14:51 WG1962462 1,1,2-Trichloroethane U 0.000842 0.00353 1 11/19/2022 14:51 WG1962462 Trichloroethene U 0.000824 0.00141 1 11/19/2022 14:51 WG1962462 Trichlorofluoromethane U C3 0.00117 0.00353 1 11/19/2022 14:51 WG1962462 1,2,3-Trichloropropane U 0.00229 0.0176 1 11/19/2022 14:51 WG1962462 1,2,4-Trimethylbenzene U 0.00223 0.00705 1 11/19/2022 14:51 WG1962462 1,2,3-Trimethylbenzene U 0.00223 0.00705 1 11/19/2022 14:51 WG1962462 1,3,5-Trimethylbenzene U 0.00282 0.00705 1 11/19/2022 14:51 WG1962462 Vinyl chloride U C3 J4 0.00164 0.00353 1 11/19/2022 14:51 WG1962462 Xylenes, Total 0.00161 J 0.00124 0.00917 1 11/19/2022 14:51 WG1962462 (S) Toluene-d8 106 75.0-131 11/19/2022 14:51 WG1962462 (S) 4-Bromofluorobenzene 99.6 67.0-138 11/19/2022 14:51 WG1962462 (S) 1,2-Dichloroethane-d4 81.4 70.0-130 11/19/2022 14:51 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene 0.0200 J 0.0129 0.0793 2 11/25/2022 13:41 WG1962878 Acenaphthylene 0.252 0.0112 0.0793 2 11/25/2022 13:41 WG1962878 Anthracene 0.135 0.0142 0.0793 2 11/25/2022 13:41 WG1962878 Benzidine U 0.149 3.98 2 11/25/2022 13:41 WG1962878 Benzo(a)anthracene 0.519 0.0139 0.0793 2 11/25/2022 13:41 WG1962878 Benzo(b)fluoranthene 0.789 0.0148 0.0793 2 11/25/2022 13:41 WG1962878 Benzo(k)fluoranthene 0.274 0.0140 0.0793 2 11/25/2022 13:41 WG1962878 Benzo(g,h,i)perylene 0.313 0.0145 0.0793 2 11/25/2022 13:41 WG1962878 Benzo(a)pyrene 0.711 0.0148 0.0793 2 11/25/2022 13:41 WG1962878 Bis(2-chlorethoxy)methane U 0.0238 0.793 2 11/25/2022 13:41 WG1962878 Bis(2-chloroethyl)ether U 0.0262 0.793 2 11/25/2022 13:41 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0343 0.793 2 11/25/2022 13:41 WG1962878 4-Bromophenyl-phenylether U 0.0279 0.793 2 11/25/2022 13:41 WG1962878 2-Chloronaphthalene U 0.0139 0.0793 2 11/25/2022 13:41 WG1962878 4-Chlorophenyl-phenylether U 0.0276 0.793 2 11/25/2022 13:41 WG1962878 Chrysene 0.645 0.0157 0.0793 2 11/25/2022 13:41 WG1962878 Dibenz(a,h)anthracene 0.0937 0.0220 0.0793 2 11/25/2022 13:41 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 32 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 32 of 70 SAMPLE RESULTS - 09 L1558771 CS-6-A Collected date/time: 11/14/22 13:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0235 0.793 2 11/25/2022 13:41 WG1962878 1,3-Dichlorobenzene U 0.0240 0.793 2 11/25/2022 13:41 WG1962878 1,4-Dichlorobenzene U 0.0236 0.793 2 11/25/2022 13:41 WG1962878 3,3-Dichlorobenzidine U 0.0293 0.793 2 11/25/2022 13:41 WG1962878 2,4-Dinitrotoluene U 0.0227 0.793 2 11/25/2022 13:41 WG1962878 2,6-Dinitrotoluene U 0.0260 0.793 2 11/25/2022 13:41 WG1962878 Fluoranthene 0.771 0.0143 0.0793 2 11/25/2022 13:41 WG1962878 Fluorene 0.0612 J 0.0129 0.0793 2 11/25/2022 13:41 WG1962878 Hexachlorobenzene U 0.0281 0.793 2 11/25/2022 13:41 WG1962878 Hexachloro-1,3-butadiene U 0.0267 0.793 2 11/25/2022 13:41 WG1962878 Hexachlorocyclopentadiene U 0.0417 0.793 2 11/25/2022 13:41 WG1962878 Hexachloroethane U 0.0312 0.793 2 11/25/2022 13:41 WG1962878 Indeno(1,2,3-cd)pyrene 0.346 0.0224 0.0793 2 11/25/2022 13:41 WG1962878 Isophorone U 0.0243 0.793 2 11/25/2022 13:41 WG1962878 Naphthalene 0.0361 J 0.0199 0.0793 2 11/25/2022 13:41 WG1962878 Nitrobenzene U 0.0276 0.793 2 11/25/2022 13:41 WG1962878 n-Nitrosodimethylamine U 0.118 0.793 2 11/25/2022 13:41 WG1962878 n-Nitrosodiphenylamine U 0.0600 0.793 2 11/25/2022 13:41 WG1962878 n-Nitrosodi-n-propylamine U 0.0264 0.793 2 11/25/2022 13:41 WG1962878 Phenanthrene 0.606 0.0157 0.0793 2 11/25/2022 13:41 WG1962878 Benzylbutyl phthalate U 0.0248 0.793 2 11/25/2022 13:41 WG1962878 Bis(2-ethylhexyl)phthalate U 0.100 0.793 2 11/25/2022 13:41 WG1962878 Di-n-butyl phthalate U 0.0271 0.793 2 11/25/2022 13:41 WG1962878 Diethyl phthalate U 0.0262 0.793 2 11/25/2022 13:41 WG1962878 Dimethyl phthalate U 0.168 0.793 2 11/25/2022 13:41 WG1962878 Di-n-octyl phthalate U 0.0536 0.793 2 11/25/2022 13:41 WG1962878 Pyrene 0.981 0.0155 0.0793 2 11/25/2022 13:41 WG1962878 1,2,4-Trichlorobenzene U 0.0248 0.793 2 11/25/2022 13:41 WG1962878 4-Chloro-3-methylphenol U 0.0257 0.793 2 11/25/2022 13:41 WG1962878 2-Chlorophenol U 0.0262 0.793 2 11/25/2022 13:41 WG1962878 2,4-Dichlorophenol U 0.0231 0.793 2 11/25/2022 13:41 WG1962878 2,4-Dimethylphenol U 0.0207 0.793 2 11/25/2022 13:41 WG1962878 4,6-Dinitro-2-methylphenol U 0.180 0.793 2 11/25/2022 13:41 WG1962878 2,4-Dinitrophenol U 0.186 0.793 2 11/25/2022 13:41 WG1962878 2-Nitrophenol U 0.0283 0.793 2 11/25/2022 13:41 WG1962878 4-Nitrophenol U 0.0248 0.793 2 11/25/2022 13:41 WG1962878 Pentachlorophenol U 0.0213 0.793 2 11/25/2022 13:41 WG1962878 Phenol U 0.0319 0.793 2 11/25/2022 13:41 WG1962878 2,4,6-Trichlorophenol U 0.0255 0.793 2 11/25/2022 13:41 WG1962878 (S) 2-Fluorophenol 71.7 12.0-120 11/25/2022 13:41 WG1962878 (S) Phenol-d5 66.6 10.0-120 11/25/2022 13:41 WG1962878 (S) Nitrobenzene-d5 64.9 10.0-122 11/25/2022 13:41 WG1962878 (S) 2-Fluorobiphenyl 63.0 15.0-120 11/25/2022 13:41 WG1962878 (S) 2,4,6-Tribromophenol 94.8 10.0-127 11/25/2022 13:41 WG1962878 (S) p-Terphenyl-d14 73.7 10.0-120 11/25/2022 13:41 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 33 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 33 of 70 SAMPLE RESULTS - 10 L1558771 CS-7 Collected date/time: 11/14/22 12:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 81.9 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0390 J 0.0220 0.0488 1 11/21/2022 15:19 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 4.51 0.122 1.22 5 12/01/2022 19:15 WG1962098 Barium 39.6 0.186 3.05 5 12/01/2022 19:15 WG1962098 Cadmium 0.709 J 0.104 1.22 5 12/01/2022 19:15 WG1962098 Chromium 15.2 0.361 6.11 5 12/01/2022 19:15 WG1962098 Lead 52.8 0.121 2.44 5 12/01/2022 19:15 WG1962098 Selenium 0.607 J 0.220 3.05 5 12/01/2022 19:15 WG1962098 Silver U 0.106 0.611 5 12/01/2022 19:15 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0533 0.0730 1 11/19/2022 15:10 WG1962462 Acrylonitrile U 0.00527 0.0182 1 11/19/2022 15:10 WG1962462 Benzene U 0.000682 0.00146 1 11/19/2022 15:10 WG1962462 Bromobenzene U 0.00131 0.0182 1 11/19/2022 15:10 WG1962462 Bromodichloromethane U 0.00106 0.00365 1 11/19/2022 15:10 WG1962462 Bromoform U 0.00171 0.0365 1 11/19/2022 15:10 WG1962462 Bromomethane U C3 0.00288 0.0182 1 11/19/2022 15:10 WG1962462 n-Butylbenzene U 0.00766 0.0182 1 11/19/2022 15:10 WG1962462 sec-Butylbenzene U 0.00420 0.0182 1 11/19/2022 15:10 WG1962462 tert-Butylbenzene U 0.00285 0.00730 1 11/19/2022 15:10 WG1962462 Carbon tetrachloride U 0.00131 0.00730 1 11/19/2022 15:10 WG1962462 Chlorobenzene U 0.000307 0.00365 1 11/19/2022 15:10 WG1962462 Chlorodibromomethane U 0.000894 0.00365 1 11/19/2022 15:10 WG1962462 Chloroethane U C3 J4 0.00248 0.00730 1 11/19/2022 15:10 WG1962462 Chloroform 0.00387 0.00150 0.00365 1 11/19/2022 15:10 WG1962462 Chloromethane U C3 0.00635 0.0182 1 11/19/2022 15:10 WG1962462 2-Chlorotoluene U 0.00126 0.00365 1 11/19/2022 15:10 WG1962462 4-Chlorotoluene U 0.000657 0.00730 1 11/19/2022 15:10 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00569 0.0365 1 11/19/2022 15:10 WG1962462 1,2-Dibromoethane U 0.000946 0.00365 1 11/19/2022 15:10 WG1962462 Dibromomethane U 0.00109 0.00730 1 11/19/2022 15:10 WG1962462 1,2-Dichlorobenzene U 0.000620 0.00730 1 11/19/2022 15:10 WG1962462 1,3-Dichlorobenzene U 0.000876 0.00730 1 11/19/2022 15:10 WG1962462 1,4-Dichlorobenzene U 0.00102 0.00730 1 11/19/2022 15:10 WG1962462 Dichlorodifluoromethane U C3 0.00235 0.00365 1 11/19/2022 15:10 WG1962462 1,1-Dichloroethane U 0.000717 0.00365 1 11/19/2022 15:10 WG1962462 1,2-Dichloroethane U 0.000948 0.00365 1 11/19/2022 15:10 WG1962462 1,1-Dichloroethene U 0.000885 0.00365 1 11/19/2022 15:10 WG1962462 cis-1,2-Dichloroethene U 0.00107 0.00365 1 11/19/2022 15:10 WG1962462 trans-1,2-Dichloroethene U 0.00152 0.00730 1 11/19/2022 15:10 WG1962462 1,2-Dichloropropane U 0.00207 0.00730 1 11/19/2022 15:10 WG1962462 1,1-Dichloropropene U 0.00118 0.00365 1 11/19/2022 15:10 WG1962462 1,3-Dichloropropane U 0.000731 0.00730 1 11/19/2022 15:10 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 34 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 34 of 70 SAMPLE RESULTS - 10 L1558771 CS-7 Collected date/time: 11/14/22 12:30 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00111 0.00365 1 11/19/2022 15:10 WG1962462 trans-1,3-Dichloropropene U 0.00166 0.00730 1 11/19/2022 15:10 WG1962462 2,2-Dichloropropane U C3 0.00201 0.00365 1 11/19/2022 15:10 WG1962462 Di-isopropyl ether U 0.000599 0.00146 1 11/19/2022 15:10 WG1962462 Ethylbenzene U 0.00108 0.00365 1 11/19/2022 15:10 WG1962462 Hexachloro-1,3-butadiene U 0.00876 0.0365 1 11/19/2022 15:10 WG1962462 Isopropylbenzene U 0.000620 0.00365 1 11/19/2022 15:10 WG1962462 p-Isopropyltoluene U 0.00372 0.00730 1 11/19/2022 15:10 WG1962462 2-Butanone (MEK)U 0.0927 0.146 1 11/19/2022 15:10 WG1962462 Methylene Chloride U 0.00969 0.0365 1 11/19/2022 15:10 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00333 0.0365 1 11/19/2022 15:10 WG1962462 Methyl tert-butyl ether U 0.000511 0.00146 1 11/19/2022 15:10 WG1962462 Naphthalene U 0.00712 0.0182 1 11/19/2022 15:10 WG1962462 n-Propylbenzene U 0.00139 0.00730 1 11/19/2022 15:10 WG1962462 Styrene U 0.000334 0.0182 1 11/19/2022 15:10 WG1962462 1,1,1,2-Tetrachloroethane U 0.00138 0.00365 1 11/19/2022 15:10 WG1962462 1,1,2,2-Tetrachloroethane U 0.00101 0.00365 1 11/19/2022 15:10 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00110 0.00365 1 11/19/2022 15:10 WG1962462 Tetrachloroethene U 0.00131 0.00365 1 11/19/2022 15:10 WG1962462 Toluene 0.00274 J 0.00190 0.00730 1 11/19/2022 15:10 WG1962462 1,2,3-Trichlorobenzene U 0.0107 0.0182 1 11/19/2022 15:10 WG1962462 1,2,4-Trichlorobenzene U J4 0.00642 0.0182 1 11/19/2022 15:10 WG1962462 1,1,1-Trichloroethane U 0.00135 0.00365 1 11/19/2022 15:10 WG1962462 1,1,2-Trichloroethane U 0.000872 0.00365 1 11/19/2022 15:10 WG1962462 Trichloroethene U 0.000853 0.00146 1 11/19/2022 15:10 WG1962462 Trichlorofluoromethane U C3 0.00121 0.00365 1 11/19/2022 15:10 WG1962462 1,2,3-Trichloropropane U 0.00237 0.0182 1 11/19/2022 15:10 WG1962462 1,2,4-Trimethylbenzene U 0.00231 0.00730 1 11/19/2022 15:10 WG1962462 1,2,3-Trimethylbenzene U 0.00231 0.00730 1 11/19/2022 15:10 WG1962462 1,3,5-Trimethylbenzene U 0.00292 0.00730 1 11/19/2022 15:10 WG1962462 Vinyl chloride U C3 J4 0.00169 0.00365 1 11/19/2022 15:10 WG1962462 Xylenes, Total 0.00206 J 0.00128 0.00949 1 11/19/2022 15:10 WG1962462 (S) Toluene-d8 105 75.0-131 11/19/2022 15:10 WG1962462 (S) 4-Bromofluorobenzene 98.5 67.0-138 11/19/2022 15:10 WG1962462 (S) 1,2-Dichloroethane-d4 83.8 70.0-130 11/19/2022 15:10 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00658 0.0407 1 11/25/2022 10:59 WG1962878 Acenaphthylene 0.00917 J 0.00573 0.0407 1 11/25/2022 10:59 WG1962878 Anthracene U 0.00724 0.0407 1 11/25/2022 10:59 WG1962878 Benzidine U 0.0764 2.04 1 11/25/2022 10:59 WG1962878 Benzo(a)anthracene 0.0354 J 0.00717 0.0407 1 11/25/2022 10:59 WG1962878 Benzo(b)fluoranthene 0.0580 0.00758 0.0407 1 11/25/2022 10:59 WG1962878 Benzo(k)fluoranthene 0.0186 J 0.00723 0.0407 1 11/25/2022 10:59 WG1962878 Benzo(g,h,i)perylene 0.0297 J 0.00744 0.0407 1 11/25/2022 10:59 WG1962878 Benzo(a)pyrene 0.0408 0.00756 0.0407 1 11/25/2022 10:59 WG1962878 Bis(2-chlorethoxy)methane U 0.0122 0.407 1 11/25/2022 10:59 WG1962878 Bis(2-chloroethyl)ether U 0.0134 0.407 1 11/25/2022 10:59 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0176 0.407 1 11/25/2022 10:59 WG1962878 4-Bromophenyl-phenylether U 0.0143 0.407 1 11/25/2022 10:59 WG1962878 2-Chloronaphthalene U 0.00714 0.0407 1 11/25/2022 10:59 WG1962878 4-Chlorophenyl-phenylether U 0.0142 0.407 1 11/25/2022 10:59 WG1962878 Chrysene 0.0446 0.00808 0.0407 1 11/25/2022 10:59 WG1962878 Dibenz(a,h)anthracene U 0.0113 0.0407 1 11/25/2022 10:59 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 35 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 35 of 70 SAMPLE RESULTS - 10 L1558771 CS-7 Collected date/time: 11/14/22 12:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0121 0.407 1 11/25/2022 10:59 WG1962878 1,3-Dichlorobenzene U 0.0123 0.407 1 11/25/2022 10:59 WG1962878 1,4-Dichlorobenzene U 0.0121 0.407 1 11/25/2022 10:59 WG1962878 3,3-Dichlorobenzidine U 0.0150 0.407 1 11/25/2022 10:59 WG1962878 2,4-Dinitrotoluene U 0.0117 0.407 1 11/25/2022 10:59 WG1962878 2,6-Dinitrotoluene U 0.0133 0.407 1 11/25/2022 10:59 WG1962878 Fluoranthene 0.0708 0.00734 0.0407 1 11/25/2022 10:59 WG1962878 Fluorene U 0.00662 0.0407 1 11/25/2022 10:59 WG1962878 Hexachlorobenzene U 0.0144 0.407 1 11/25/2022 10:59 WG1962878 Hexachloro-1,3-butadiene U 0.0137 0.407 1 11/25/2022 10:59 WG1962878 Hexachlorocyclopentadiene U 0.0214 0.407 1 11/25/2022 10:59 WG1962878 Hexachloroethane U 0.0160 0.407 1 11/25/2022 10:59 WG1962878 Indeno(1,2,3-cd)pyrene 0.0286 J 0.0115 0.0407 1 11/25/2022 10:59 WG1962878 Isophorone U 0.0125 0.407 1 11/25/2022 10:59 WG1962878 Naphthalene U 0.0102 0.0407 1 11/25/2022 10:59 WG1962878 Nitrobenzene U 0.0142 0.407 1 11/25/2022 10:59 WG1962878 n-Nitrosodimethylamine U 0.0603 0.407 1 11/25/2022 10:59 WG1962878 n-Nitrosodiphenylamine U 0.0308 0.407 1 11/25/2022 10:59 WG1962878 n-Nitrosodi-n-propylamine U 0.0136 0.407 1 11/25/2022 10:59 WG1962878 Phenanthrene 0.0379 J 0.00807 0.0407 1 11/25/2022 10:59 WG1962878 Benzylbutyl phthalate U 0.0127 0.407 1 11/25/2022 10:59 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0515 0.407 1 11/25/2022 10:59 WG1962878 Di-n-butyl phthalate U 0.0139 0.407 1 11/25/2022 10:59 WG1962878 Diethyl phthalate U 0.0134 0.407 1 11/25/2022 10:59 WG1962878 Dimethyl phthalate U 0.0862 0.407 1 11/25/2022 10:59 WG1962878 Di-n-octyl phthalate U 0.0275 0.407 1 11/25/2022 10:59 WG1962878 Pyrene 0.0624 0.00791 0.0407 1 11/25/2022 10:59 WG1962878 1,2,4-Trichlorobenzene U 0.0127 0.407 1 11/25/2022 10:59 WG1962878 4-Chloro-3-methylphenol U 0.0132 0.407 1 11/25/2022 10:59 WG1962878 2-Chlorophenol U 0.0134 0.407 1 11/25/2022 10:59 WG1962878 2,4-Dichlorophenol U 0.0118 0.407 1 11/25/2022 10:59 WG1962878 2,4-Dimethylphenol U 0.0106 0.407 1 11/25/2022 10:59 WG1962878 4,6-Dinitro-2-methylphenol U 0.0922 0.407 1 11/25/2022 10:59 WG1962878 2,4-Dinitrophenol U 0.0951 0.407 1 11/25/2022 10:59 WG1962878 2-Nitrophenol U 0.0145 0.407 1 11/25/2022 10:59 WG1962878 4-Nitrophenol U 0.0127 0.407 1 11/25/2022 10:59 WG1962878 Pentachlorophenol U 0.0109 0.407 1 11/25/2022 10:59 WG1962878 Phenol U 0.0164 0.407 1 11/25/2022 10:59 WG1962878 2,4,6-Trichlorophenol U 0.0131 0.407 1 11/25/2022 10:59 WG1962878 (S) 2-Fluorophenol 63.9 12.0-120 11/25/2022 10:59 WG1962878 (S) Phenol-d5 60.5 10.0-120 11/25/2022 10:59 WG1962878 (S) Nitrobenzene-d5 59.3 10.0-122 11/25/2022 10:59 WG1962878 (S) 2-Fluorobiphenyl 57.1 15.0-120 11/25/2022 10:59 WG1962878 (S) 2,4,6-Tribromophenol 80.4 10.0-127 11/25/2022 10:59 WG1962878 (S) p-Terphenyl-d14 64.8 10.0-120 11/25/2022 10:59 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 36 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 36 of 70 SAMPLE RESULTS - 11 L1558771 CS-8 Collected date/time: 11/14/22 13:35 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 84.8 1 11/18/2022 12:52 WG1961476 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0458 J 0.0212 0.0472 1 11/21/2022 15:21 WG1961812 Metals (ICPMS) by Method 6020B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 5.57 0.118 1.18 5 12/01/2022 19:19 WG1962098 Barium 37.8 0.179 2.95 5 12/01/2022 19:19 WG1962098 Cadmium U 0.101 1.18 5 12/01/2022 19:19 WG1962098 Chromium 13.1 0.349 5.90 5 12/01/2022 19:19 WG1962098 Lead 15.8 0.117 2.36 5 12/01/2022 19:19 WG1962098 Selenium 0.876 J 0.212 2.95 5 12/01/2022 19:19 WG1962098 Silver U 0.102 0.590 5 12/01/2022 19:19 WG1962098 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0496 0.0679 1 11/19/2022 15:29 WG1962462 Acrylonitrile U 0.00490 0.0170 1 11/19/2022 15:29 WG1962462 Benzene U 0.000634 0.00136 1 11/19/2022 15:29 WG1962462 Bromobenzene U 0.00122 0.0170 1 11/19/2022 15:29 WG1962462 Bromodichloromethane U 0.000985 0.00340 1 11/19/2022 15:29 WG1962462 Bromoform U 0.00159 0.0340 1 11/19/2022 15:29 WG1962462 Bromomethane U C3 0.00268 0.0170 1 11/19/2022 15:29 WG1962462 n-Butylbenzene U 0.00713 0.0170 1 11/19/2022 15:29 WG1962462 sec-Butylbenzene U 0.00391 0.0170 1 11/19/2022 15:29 WG1962462 tert-Butylbenzene U 0.00265 0.00679 1 11/19/2022 15:29 WG1962462 Carbon tetrachloride U 0.00122 0.00679 1 11/19/2022 15:29 WG1962462 Chlorobenzene U 0.000285 0.00340 1 11/19/2022 15:29 WG1962462 Chlorodibromomethane U 0.000832 0.00340 1 11/19/2022 15:29 WG1962462 Chloroethane U C3 J4 0.00231 0.00679 1 11/19/2022 15:29 WG1962462 Chloroform 0.00435 0.00140 0.00340 1 11/19/2022 15:29 WG1962462 Chloromethane U C3 0.00591 0.0170 1 11/19/2022 15:29 WG1962462 2-Chlorotoluene U 0.00118 0.00340 1 11/19/2022 15:29 WG1962462 4-Chlorotoluene U 0.000611 0.00679 1 11/19/2022 15:29 WG1962462 1,2-Dibromo-3-Chloropropane U 0.00530 0.0340 1 11/19/2022 15:29 WG1962462 1,2-Dibromoethane U 0.000880 0.00340 1 11/19/2022 15:29 WG1962462 Dibromomethane U 0.00102 0.00679 1 11/19/2022 15:29 WG1962462 1,2-Dichlorobenzene U 0.000577 0.00679 1 11/19/2022 15:29 WG1962462 1,3-Dichlorobenzene U 0.000815 0.00679 1 11/19/2022 15:29 WG1962462 1,4-Dichlorobenzene U 0.000951 0.00679 1 11/19/2022 15:29 WG1962462 Dichlorodifluoromethane U C3 0.00219 0.00340 1 11/19/2022 15:29 WG1962462 1,1-Dichloroethane U 0.000667 0.00340 1 11/19/2022 15:29 WG1962462 1,2-Dichloroethane U 0.000882 0.00340 1 11/19/2022 15:29 WG1962462 1,1-Dichloroethene U 0.000823 0.00340 1 11/19/2022 15:29 WG1962462 cis-1,2-Dichloroethene U 0.000997 0.00340 1 11/19/2022 15:29 WG1962462 trans-1,2-Dichloroethene U 0.00141 0.00679 1 11/19/2022 15:29 WG1962462 1,2-Dichloropropane U 0.00193 0.00679 1 11/19/2022 15:29 WG1962462 1,1-Dichloropropene U 0.00110 0.00340 1 11/19/2022 15:29 WG1962462 1,3-Dichloropropane U 0.000681 0.00679 1 11/19/2022 15:29 WG1962462 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 37 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 37 of 70 SAMPLE RESULTS - 11 L1558771 CS-8 Collected date/time: 11/14/22 13:35 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.00103 0.00340 1 11/19/2022 15:29 WG1962462 trans-1,3-Dichloropropene U 0.00155 0.00679 1 11/19/2022 15:29 WG1962462 2,2-Dichloropropane U C3 0.00187 0.00340 1 11/19/2022 15:29 WG1962462 Di-isopropyl ether U 0.000557 0.00136 1 11/19/2022 15:29 WG1962462 Ethylbenzene U 0.00100 0.00340 1 11/19/2022 15:29 WG1962462 Hexachloro-1,3-butadiene U 0.00815 0.0340 1 11/19/2022 15:29 WG1962462 Isopropylbenzene 0.000679 J 0.000577 0.00340 1 11/19/2022 15:29 WG1962462 p-Isopropyltoluene U 0.00346 0.00679 1 11/19/2022 15:29 WG1962462 2-Butanone (MEK)U 0.0863 0.136 1 11/19/2022 15:29 WG1962462 Methylene Chloride U 0.00902 0.0340 1 11/19/2022 15:29 WG1962462 4-Methyl-2-pentanone (MIBK)U 0.00310 0.0340 1 11/19/2022 15:29 WG1962462 Methyl tert-butyl ether U 0.000476 0.00136 1 11/19/2022 15:29 WG1962462 Naphthalene U 0.00663 0.0170 1 11/19/2022 15:29 WG1962462 n-Propylbenzene U 0.00129 0.00679 1 11/19/2022 15:29 WG1962462 Styrene 0.000781 B J 0.000311 0.0170 1 11/19/2022 15:29 WG1962462 1,1,1,2-Tetrachloroethane U 0.00129 0.00340 1 11/19/2022 15:29 WG1962462 1,1,2,2-Tetrachloroethane U 0.000944 0.00340 1 11/19/2022 15:29 WG1962462 1,1,2-Trichlorotrifluoroethane U 0.00102 0.00340 1 11/19/2022 15:29 WG1962462 Tetrachloroethene U 0.00122 0.00340 1 11/19/2022 15:29 WG1962462 Toluene U 0.00177 0.00679 1 11/19/2022 15:29 WG1962462 1,2,3-Trichlorobenzene U 0.00996 0.0170 1 11/19/2022 15:29 WG1962462 1,2,4-Trichlorobenzene U J4 0.00598 0.0170 1 11/19/2022 15:29 WG1962462 1,1,1-Trichloroethane U 0.00125 0.00340 1 11/19/2022 15:29 WG1962462 1,1,2-Trichloroethane U 0.000811 0.00340 1 11/19/2022 15:29 WG1962462 Trichloroethene U 0.000793 0.00136 1 11/19/2022 15:29 WG1962462 Trichlorofluoromethane U C3 0.00112 0.00340 1 11/19/2022 15:29 WG1962462 1,2,3-Trichloropropane U 0.00220 0.0170 1 11/19/2022 15:29 WG1962462 1,2,4-Trimethylbenzene U 0.00215 0.00679 1 11/19/2022 15:29 WG1962462 1,2,3-Trimethylbenzene U 0.00215 0.00679 1 11/19/2022 15:29 WG1962462 1,3,5-Trimethylbenzene U 0.00272 0.00679 1 11/19/2022 15:29 WG1962462 Vinyl chloride U C3 J4 0.00158 0.00340 1 11/19/2022 15:29 WG1962462 Xylenes, Total U 0.00120 0.00883 1 11/19/2022 15:29 WG1962462 (S) Toluene-d8 107 75.0-131 11/19/2022 15:29 WG1962462 (S) 4-Bromofluorobenzene 101 67.0-138 11/19/2022 15:29 WG1962462 (S) 1,2-Dichloroethane-d4 79.6 70.0-130 11/19/2022 15:29 WG1962462 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00636 0.0393 1 11/25/2022 09:58 WG1962878 Acenaphthylene 0.0114 J 0.00553 0.0393 1 11/25/2022 09:58 WG1962878 Anthracene U 0.00699 0.0393 1 11/25/2022 09:58 WG1962878 Benzidine U 0.0738 1.97 1 11/25/2022 09:58 WG1962878 Benzo(a)anthracene 0.0202 J 0.00692 0.0393 1 11/25/2022 09:58 WG1962878 Benzo(b)fluoranthene 0.0493 0.00732 0.0393 1 11/25/2022 09:58 WG1962878 Benzo(k)fluoranthene 0.0143 J 0.00698 0.0393 1 11/25/2022 09:58 WG1962878 Benzo(g,h,i)perylene 0.0269 J 0.00718 0.0393 1 11/25/2022 09:58 WG1962878 Benzo(a)pyrene 0.0304 J 0.00730 0.0393 1 11/25/2022 09:58 WG1962878 Bis(2-chlorethoxy)methane U 0.0118 0.393 1 11/25/2022 09:58 WG1962878 Bis(2-chloroethyl)ether U 0.0130 0.393 1 11/25/2022 09:58 WG1962878 2,2-Oxybis(1-Chloropropane)U 0.0170 0.393 1 11/25/2022 09:58 WG1962878 4-Bromophenyl-phenylether U 0.0138 0.393 1 11/25/2022 09:58 WG1962878 2-Chloronaphthalene U 0.00690 0.0393 1 11/25/2022 09:58 WG1962878 4-Chlorophenyl-phenylether U 0.0137 0.393 1 11/25/2022 09:58 WG1962878 Chrysene 0.0269 J 0.00781 0.0393 1 11/25/2022 09:58 WG1962878 Dibenz(a,h)anthracene U 0.0109 0.0393 1 11/25/2022 09:58 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 38 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 38 of 70 SAMPLE RESULTS - 11 L1558771 CS-8 Collected date/time: 11/14/22 13:35 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 1,2-Dichlorobenzene U 0.0116 0.393 1 11/25/2022 09:58 WG1962878 1,3-Dichlorobenzene U 0.0119 0.393 1 11/25/2022 09:58 WG1962878 1,4-Dichlorobenzene U 0.0117 0.393 1 11/25/2022 09:58 WG1962878 3,3-Dichlorobenzidine U 0.0145 0.393 1 11/25/2022 09:58 WG1962878 2,4-Dinitrotoluene U 0.0113 0.393 1 11/25/2022 09:58 WG1962878 2,6-Dinitrotoluene U 0.0129 0.393 1 11/25/2022 09:58 WG1962878 Fluoranthene 0.0525 0.00709 0.0393 1 11/25/2022 09:58 WG1962878 Fluorene U 0.00639 0.0393 1 11/25/2022 09:58 WG1962878 Hexachlorobenzene U 0.0139 0.393 1 11/25/2022 09:58 WG1962878 Hexachloro-1,3-butadiene U 0.0132 0.393 1 11/25/2022 09:58 WG1962878 Hexachlorocyclopentadiene U 0.0206 0.393 1 11/25/2022 09:58 WG1962878 Hexachloroethane U 0.0155 0.393 1 11/25/2022 09:58 WG1962878 Indeno(1,2,3-cd)pyrene 0.0278 J 0.0111 0.0393 1 11/25/2022 09:58 WG1962878 Isophorone U 0.0120 0.393 1 11/25/2022 09:58 WG1962878 Naphthalene U 0.00986 0.0393 1 11/25/2022 09:58 WG1962878 Nitrobenzene U 0.0137 0.393 1 11/25/2022 09:58 WG1962878 n-Nitrosodimethylamine U 0.0583 0.393 1 11/25/2022 09:58 WG1962878 n-Nitrosodiphenylamine U 0.0297 0.393 1 11/25/2022 09:58 WG1962878 n-Nitrosodi-n-propylamine U 0.0131 0.393 1 11/25/2022 09:58 WG1962878 Phenanthrene 0.0213 J 0.00780 0.0393 1 11/25/2022 09:58 WG1962878 Benzylbutyl phthalate U 0.0123 0.393 1 11/25/2022 09:58 WG1962878 Bis(2-ethylhexyl)phthalate U 0.0498 0.393 1 11/25/2022 09:58 WG1962878 Di-n-butyl phthalate U 0.0134 0.393 1 11/25/2022 09:58 WG1962878 Diethyl phthalate U 0.0130 0.393 1 11/25/2022 09:58 WG1962878 Dimethyl phthalate U 0.0833 0.393 1 11/25/2022 09:58 WG1962878 Di-n-octyl phthalate U 0.0265 0.393 1 11/25/2022 09:58 WG1962878 Pyrene 0.0479 0.00764 0.0393 1 11/25/2022 09:58 WG1962878 1,2,4-Trichlorobenzene U 0.0123 0.393 1 11/25/2022 09:58 WG1962878 4-Chloro-3-methylphenol U 0.0127 0.393 1 11/25/2022 09:58 WG1962878 2-Chlorophenol U 0.0130 0.393 1 11/25/2022 09:58 WG1962878 2,4-Dichlorophenol U 0.0114 0.393 1 11/25/2022 09:58 WG1962878 2,4-Dimethylphenol U 0.0103 0.393 1 11/25/2022 09:58 WG1962878 4,6-Dinitro-2-methylphenol U 0.0890 0.393 1 11/25/2022 09:58 WG1962878 2,4-Dinitrophenol U 0.0919 0.393 1 11/25/2022 09:58 WG1962878 2-Nitrophenol U 0.0140 0.393 1 11/25/2022 09:58 WG1962878 4-Nitrophenol U 0.0123 0.393 1 11/25/2022 09:58 WG1962878 Pentachlorophenol U 0.0106 0.393 1 11/25/2022 09:58 WG1962878 Phenol U 0.0158 0.393 1 11/25/2022 09:58 WG1962878 2,4,6-Trichlorophenol U 0.0126 0.393 1 11/25/2022 09:58 WG1962878 (S) 2-Fluorophenol 60.4 12.0-120 11/25/2022 09:58 WG1962878 (S) Phenol-d5 56.3 10.0-120 11/25/2022 09:58 WG1962878 (S) Nitrobenzene-d5 55.3 10.0-122 11/25/2022 09:58 WG1962878 (S) 2-Fluorobiphenyl 54.1 15.0-120 11/25/2022 09:58 WG1962878 (S) 2,4,6-Tribromophenol 85.7 10.0-127 11/25/2022 09:58 WG1962878 (S) p-Terphenyl-d14 61.9 10.0-120 11/25/2022 09:58 WG1962878 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 39 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 39 of 70 QUALITY CONTROL SUMMARYWG1961475 Total Solids by Method 2540 G-2011 L1558771-01,02,03 Method Blank (MB) (MB) R3862976-1 11/18/22 10:32 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00200 L1558766-01 Original Sample (OS) • Duplicate (DUP) (OS) L1558766-01 11/18/22 10:32 • (DUP) R3862976-3 11/18/22 10:32 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 86.4 86.2 1 0.225 10 Laboratory Control Sample (LCS) (LCS) R3862976-2 11/18/22 10:32 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85.0-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 40 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 40 of 70 QUALITY CONTROL SUMMARYWG1961476 Total Solids by Method 2540 G-2011 L1558771-04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3862989-1 11/18/22 12:52 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0.00500 L1558660-12 Original Sample (OS) • Duplicate (DUP) (OS) L1558660-12 11/18/22 12:52 • (DUP) R3862989-3 11/18/22 12:52 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 99.7 99.7 1 0.00782 10 Laboratory Control Sample (LCS) (LCS) R3862989-2 11/18/22 12:52 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 99.9 85.0-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 41 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 41 of 70 QUALITY CONTROL SUMMARYWG1961812 Mercury by Method 7471B L1558771-01,02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3863564-1 11/21/22 14:23 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Mercury U 0.0180 0.0400 Laboratory Control Sample (LCS) (LCS) R3863564-2 11/21/22 14:25 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Mercury 0.500 0.485 96.9 80.0-120 L1558738-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558738-07 11/21/22 14:27 • (MS) R3863564-3 11/21/22 14:29 • (MSD) R3863564-4 11/21/22 14:31 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Mercury 0.619 U 0.654 0.622 106 100 1 75.0-125 5.10 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 42 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 42 of 70 QUALITY CONTROL SUMMARYWG1961902 Metals (ICPMS) by Method 6020B L1558771-01,02,03 Method Blank (MB) (MB) R3865068-1 11/25/22 13:10 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.100 1.00 Barium U 0.152 2.50 Cadmium U 0.0855 1.00 Chromium U 0.297 5.00 Lead U 0.0990 2.00 Selenium U 0.180 2.50 Silver U 0.0865 0.500 Laboratory Control Sample (LCS) (LCS) R3865068-2 11/25/22 13:13 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Arsenic 100 106 106 80.0-120 Barium 100 102 102 80.0-120 Cadmium 100 107 107 80.0-120 Chromium 100 107 107 80.0-120 Lead 100 106 106 80.0-120 Selenium 100 113 113 80.0-120 Silver 20.0 20.9 104 80.0-120 L1558817-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558817-12 11/25/22 13:17 • (MS) R3865068-5 11/25/22 13:27 • (MSD) R3865068-6 11/25/22 13:30 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 123 3.37 119 109 93.4 85.3 5 75.0-125 8.84 20 Barium 123 215 350 335 109 97.4 5 75.0-125 4.29 20 Cadmium 123 U 130 120 106 97.5 5 75.0-125 8.09 20 Chromium 123 71.4 186 184 92.6 91.3 5 75.0-125 0.873 20 Lead 123 11.9 135 129 100 95.0 5 75.0-125 4.60 20 Selenium 123 0.670 129 117 104 94.5 5 75.0-125 9.32 20 Silver 24.7 U 25.2 22.8 102 92.3 5 75.0-125 10.2 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 43 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 43 of 70 QUALITY CONTROL SUMMARYWG1962098 Metals (ICPMS) by Method 6020B L1558771-04,06,07,08,09,10,11 Method Blank (MB) (MB) R3867273-1 12/01/22 17:46 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.100 1.00 Barium 0.252 J 0.152 2.50 Cadmium U 0.0855 1.00 Chromium U 0.297 5.00 Lead U 0.0990 2.00 Selenium U 0.180 2.50 Silver U 0.0865 0.500 Laboratory Control Sample (LCS) (LCS) R3867273-2 12/01/22 17:49 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Arsenic 100 91.6 91.6 80.0-120 Barium 100 90.6 90.6 80.0-120 Cadmium 100 94.6 94.6 80.0-120 Chromium 100 92.1 92.1 80.0-120 Lead 100 88.4 88.4 80.0-120 Selenium 100 97.4 97.4 80.0-120 Silver 20.0 17.5 87.7 80.0-120 L1558563-37 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558563-37 12/01/22 17:52 • (MS) R3867273-5 12/01/22 18:02 • (MSD) R3867273-6 12/01/22 18:06 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 125 7.54 126 133 95.0 101 5 75.0-125 5.66 20 Barium 125 225 350 502 100 223 5 75.0-125 J3 J5 35.8 20 Cadmium 125 0.108 129 136 103 109 5 75.0-125 5.08 20 Chromium 125 25.2 148 158 98.5 106 5 75.0-125 6.47 20 Lead 125 14.4 128 136 91.3 97.1 5 75.0-125 5.57 20 Silver 25.0 U 24.5 24.7 98.4 99.2 5 75.0-125 0.819 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 44 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 44 of 70 QUALITY CONTROL SUMMARYWG1963015 Metals (ICPMS) by Method 6020B L1558771-05 Method Blank (MB) (MB) R3865785-1 11/28/22 17:25 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.100 1.00 Barium U 0.152 2.50 Cadmium U 0.0855 1.00 Chromium U 0.297 5.00 Lead U 0.0990 2.00 Selenium 0.235 J 0.180 2.50 Silver U 0.0865 0.500 Laboratory Control Sample (LCS) (LCS) R3865785-2 11/28/22 17:28 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Arsenic 100 92.9 92.9 80.0-120 Barium 100 89.9 89.9 80.0-120 Cadmium 100 93.1 93.1 80.0-120 Chromium 100 93.8 93.8 80.0-120 Lead 100 88.7 88.7 80.0-120 Selenium 100 99.4 99.4 80.0-120 Silver 20.0 17.9 89.7 80.0-120 L1558771-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558771-05 11/28/22 17:31 • (MS) R3865785-5 11/28/22 17:41 • (MSD) R3865785-6 11/28/22 17:45 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 151 1.25 143 133 93.9 87.1 5 75.0-125 7.53 20 Barium 151 21.0 160 151 92.1 86.3 5 75.0-125 E 5.62 20 Cadmium 151 U 145 134 95.8 88.8 5 75.0-125 7.61 20 Chromium 151 1.84 142 131 92.9 85.7 5 75.0-125 7.93 20 Lead 151 22.9 162 156 91.7 87.8 5 75.0-125 3.71 20 Selenium 151 0.330 155 146 102 96.4 5 75.0-125 5.71 20 Silver 30.2 U 28.0 25.6 92.5 84.8 5 75.0-125 8.68 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 45 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 45 of 70 QUALITY CONTROL SUMMARYWG1962259 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-01 Method Blank (MB) (MB) R3864420-3 11/19/22 02:14 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0365 0.0500 Acrylonitrile U 0.00361 0.0125 Benzene U 0.000467 0.00100 Bromobenzene U 0.000900 0.0125 Bromodichloromethane U 0.000725 0.00250 Bromoform U 0.00117 0.0250 Bromomethane U 0.00197 0.0125 n-Butylbenzene U 0.00525 0.0125 sec-Butylbenzene U 0.00288 0.0125 tert-Butylbenzene U 0.00195 0.00500 Carbon tetrachloride U 0.000898 0.00500 Chlorobenzene U 0.000210 0.00250 Chlorodibromomethane U 0.000612 0.00250 Chloroethane U 0.00170 0.00500 Chloroform U 0.00103 0.00250 Chloromethane U 0.00435 0.0125 2-Chlorotoluene U 0.000865 0.00250 4-Chlorotoluene U 0.000450 0.00500 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1,2-Dibromoethane U 0.000648 0.00250 Dibromomethane U 0.000750 0.00500 1,2-Dichlorobenzene U 0.000425 0.00500 1,3-Dichlorobenzene U 0.000600 0.00500 1,4-Dichlorobenzene 0.000750 J 0.000700 0.00500 Dichlorodifluoromethane U 0.00161 0.00250 1,1-Dichloroethane U 0.000491 0.00250 1,2-Dichloroethane U 0.000649 0.00250 1,1-Dichloroethene U 0.000606 0.00250 cis-1,2-Dichloroethene U 0.000734 0.00250 trans-1,2-Dichloroethene U 0.00104 0.00500 1,2-Dichloropropane U 0.00142 0.00500 1,1-Dichloropropene U 0.000809 0.00250 1,3-Dichloropropane U 0.000501 0.00500 cis-1,3-Dichloropropene U 0.000757 0.00250 trans-1,3-Dichloropropene U 0.00114 0.00500 2,2-Dichloropropane U 0.00138 0.00250 Di-isopropyl ether U 0.000410 0.00100 Ethylbenzene U 0.000737 0.00250 Hexachloro-1,3-butadiene U 0.00600 0.0250 Isopropylbenzene 0.000425 J 0.000425 0.00250 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 46 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 46 of 70 QUALITY CONTROL SUMMARYWG1962259 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-01 Method Blank (MB) (MB) R3864420-3 11/19/22 02:14 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.00255 0.00500 2-Butanone (MEK)U 0.0635 0.100 Methylene Chloride U 0.00664 0.0250 4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250 Methyl tert-butyl ether U 0.000350 0.00100 Naphthalene U 0.00488 0.0125 n-Propylbenzene 0.00170 J 0.000950 0.00500 Styrene 0.00270 J 0.000229 0.0125 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 Tetrachloroethene U 0.000896 0.00250 Toluene U 0.00130 0.00500 1,2,3-Trichlorobenzene U 0.00733 0.0125 1,2,4-Trichlorobenzene U 0.00440 0.0125 1,1,1-Trichloroethane U 0.000923 0.00250 1,1,2-Trichloroethane U 0.000597 0.00250 Trichloroethene U 0.000584 0.00100 Trichlorofluoromethane U 0.000827 0.00250 1,2,3-Trichloropropane U 0.00162 0.0125 1,2,4-Trimethylbenzene U 0.00158 0.00500 1,2,3-Trimethylbenzene U 0.00158 0.00500 1,3,5-Trimethylbenzene U 0.00200 0.00500 Vinyl chloride U 0.00116 0.00250 Xylenes, Total U 0.000880 0.00650 (S) Toluene-d8 113 75.0-131 (S) 4-Bromofluorobenzene 97.1 67.0-138 (S) 1,2-Dichloroethane-d4 91.6 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864420-1 11/19/22 00:57 • (LCSD) R3864420-2 11/19/22 01:16 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acetone 0.625 0.536 0.646 85.8 103 10.0-160 18.6 31 Acrylonitrile 0.625 0.705 0.737 113 118 45.0-153 4.44 22 Benzene 0.125 0.137 0.152 110 122 70.0-123 10.4 20 Bromobenzene 0.125 0.142 0.150 114 120 73.0-121 5.48 20 Bromodichloromethane 0.125 0.144 0.153 115 122 73.0-121 J4 6.06 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 47 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 47 of 70 QUALITY CONTROL SUMMARYWG1962259 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864420-1 11/19/22 00:57 • (LCSD) R3864420-2 11/19/22 01:16 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Bromoform 0.125 0.126 0.137 101 110 64.0-132 8.37 20 Bromomethane 0.125 0.109 0.128 87.2 102 56.0-147 16.0 20 n-Butylbenzene 0.125 0.150 0.149 120 119 68.0-135 0.669 20 sec-Butylbenzene 0.125 0.157 0.167 126 134 74.0-130 J4 6.17 20 tert-Butylbenzene 0.125 0.148 0.155 118 124 75.0-127 4.62 20 Carbon tetrachloride 0.125 0.134 0.146 107 117 66.0-128 8.57 20 Chlorobenzene 0.125 0.130 0.141 104 113 76.0-128 8.12 20 Chlorodibromomethane 0.125 0.139 0.152 111 122 74.0-127 8.93 20 Chloroethane 0.125 0.113 0.129 90.4 103 61.0-134 13.2 20 Chloroform 0.125 0.137 0.148 110 118 72.0-123 7.72 20 Chloromethane 0.125 0.108 0.131 86.4 105 51.0-138 19.2 20 2-Chlorotoluene 0.125 0.151 0.134 121 107 75.0-124 11.9 20 4-Chlorotoluene 0.125 0.159 0.167 127 134 75.0-124 J4 J4 4.91 20 1,2-Dibromo-3-Chloropropane 0.125 0.120 0.127 96.0 102 59.0-130 5.67 20 1,2-Dibromoethane 0.125 0.131 0.146 105 117 74.0-128 10.8 20 Dibromomethane 0.125 0.141 0.167 113 134 75.0-122 J4 16.9 20 1,2-Dichlorobenzene 0.125 0.133 0.138 106 110 76.0-124 3.69 20 1,3-Dichlorobenzene 0.125 0.136 0.143 109 114 76.0-125 5.02 20 1,4-Dichlorobenzene 0.125 0.134 0.142 107 114 77.0-121 5.80 20 Dichlorodifluoromethane 0.125 0.135 0.138 108 110 43.0-156 2.20 20 1,1-Dichloroethane 0.125 0.139 0.151 111 121 70.0-127 8.28 20 1,2-Dichloroethane 0.125 0.126 0.138 101 110 65.0-131 9.09 20 1,1-Dichloroethene 0.125 0.133 0.140 106 112 65.0-131 5.13 20 cis-1,2-Dichloroethene 0.125 0.138 0.154 110 123 73.0-125 11.0 20 trans-1,2-Dichloroethene 0.125 0.125 0.151 100 121 71.0-125 18.8 20 1,2-Dichloropropane 0.125 0.135 0.145 108 116 74.0-125 7.14 20 1,1-Dichloropropene 0.125 0.132 0.152 106 122 73.0-125 14.1 20 1,3-Dichloropropane 0.125 0.129 0.143 103 114 80.0-125 10.3 20 cis-1,3-Dichloropropene 0.125 0.138 0.153 110 122 76.0-127 10.3 20 trans-1,3-Dichloropropene 0.125 0.136 0.148 109 118 73.0-127 8.45 20 2,2-Dichloropropane 0.125 0.132 0.147 106 118 59.0-135 10.8 20 Di-isopropyl ether 0.125 0.143 0.152 114 122 60.0-136 6.10 20 Ethylbenzene 0.125 0.131 0.144 105 115 74.0-126 9.45 20 Hexachloro-1,3-butadiene 0.125 0.100 0.116 80.0 92.8 57.0-150 14.8 20 Isopropylbenzene 0.125 0.148 0.161 118 129 72.0-127 J4 8.41 20 p-Isopropyltoluene 0.125 0.148 0.155 118 124 72.0-133 4.62 20 2-Butanone (MEK)0.625 0.687 0.681 110 109 30.0-160 0.877 24 Methylene Chloride 0.125 0.130 0.150 104 120 68.0-123 14.3 20 4-Methyl-2-pentanone (MIBK)0.625 0.746 0.802 119 128 56.0-143 7.24 20 Methyl tert-butyl ether 0.125 0.148 0.161 118 129 66.0-132 8.41 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 48 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 48 of 70 QUALITY CONTROL SUMMARYWG1962259 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3864420-1 11/19/22 00:57 • (LCSD) R3864420-2 11/19/22 01:16 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Naphthalene 0.125 0.142 0.149 114 119 59.0-130 4.81 20 n-Propylbenzene 0.125 0.167 0.171 134 137 74.0-126 J4 J4 2.37 20 Styrene 0.125 0.137 0.147 110 118 72.0-127 7.04 20 1,1,1,2-Tetrachloroethane 0.125 0.136 0.149 109 119 74.0-129 9.12 20 1,1,2,2-Tetrachloroethane 0.125 0.134 0.148 107 118 68.0-128 9.93 20 1,1,2-Trichlorotrifluoroethane 0.125 0.135 0.159 108 127 61.0-139 16.3 20 Tetrachloroethene 0.125 0.133 0.149 106 119 70.0-136 11.3 20 Toluene 0.125 0.133 0.147 106 118 75.0-121 10.0 20 1,2,3-Trichlorobenzene 0.125 0.138 0.152 110 122 59.0-139 9.66 20 1,2,4-Trichlorobenzene 0.125 0.120 0.127 96.0 102 62.0-137 5.67 20 1,1,1-Trichloroethane 0.125 0.141 0.163 113 130 69.0-126 J4 14.5 20 1,1,2-Trichloroethane 0.125 0.138 0.147 110 118 78.0-123 6.32 20 Trichloroethene 0.125 0.131 0.142 105 114 76.0-126 8.06 20 Trichlorofluoromethane 0.125 0.143 0.163 114 130 61.0-142 13.1 20 1,2,3-Trichloropropane 0.125 0.133 0.147 106 118 67.0-129 10.0 20 1,2,4-Trimethylbenzene 0.125 0.146 0.153 117 122 70.0-126 4.68 20 1,2,3-Trimethylbenzene 0.125 0.145 0.151 116 121 74.0-124 4.05 20 1,3,5-Trimethylbenzene 0.125 0.152 0.160 122 128 73.0-127 J4 5.13 20 Vinyl chloride 0.125 0.124 0.139 99.2 111 63.0-134 11.4 20 Xylenes, Total 0.375 0.410 0.446 109 119 72.0-127 8.41 20 (S) Toluene-d8 103 103 75.0-131 (S) 4-Bromofluorobenzene 102 102 67.0-138 (S) 1,2-Dichloroethane-d4 97.5 98.4 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 49 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 49 of 70 QUALITY CONTROL SUMMARYWG1962462 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3865698-2 11/19/22 11:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0365 0.0500 Acrylonitrile U 0.00361 0.0125 Benzene U 0.000467 0.00100 Bromobenzene U 0.000900 0.0125 Bromodichloromethane U 0.000725 0.00250 Bromoform U 0.00117 0.0250 Bromomethane U 0.00197 0.0125 n-Butylbenzene U 0.00525 0.0125 sec-Butylbenzene U 0.00288 0.0125 tert-Butylbenzene U 0.00195 0.00500 Carbon tetrachloride U 0.000898 0.00500 Chlorobenzene U 0.000210 0.00250 Chlorodibromomethane U 0.000612 0.00250 Chloroethane U 0.00170 0.00500 Chloroform U 0.00103 0.00250 Chloromethane U 0.00435 0.0125 2-Chlorotoluene U 0.000865 0.00250 4-Chlorotoluene U 0.000450 0.00500 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1,2-Dibromoethane U 0.000648 0.00250 Dibromomethane U 0.000750 0.00500 1,2-Dichlorobenzene U 0.000425 0.00500 1,3-Dichlorobenzene U 0.000600 0.00500 1,4-Dichlorobenzene U 0.000700 0.00500 Dichlorodifluoromethane U 0.00161 0.00250 1,1-Dichloroethane U 0.000491 0.00250 1,2-Dichloroethane U 0.000649 0.00250 1,1-Dichloroethene U 0.000606 0.00250 cis-1,2-Dichloroethene U 0.000734 0.00250 trans-1,2-Dichloroethene U 0.00104 0.00500 1,2-Dichloropropane U 0.00142 0.00500 1,1-Dichloropropene U 0.000809 0.00250 1,3-Dichloropropane U 0.000501 0.00500 cis-1,3-Dichloropropene U 0.000757 0.00250 trans-1,3-Dichloropropene U 0.00114 0.00500 2,2-Dichloropropane U 0.00138 0.00250 Di-isopropyl ether U 0.000410 0.00100 Ethylbenzene U 0.000737 0.00250 Hexachloro-1,3-butadiene U 0.00600 0.0250 Isopropylbenzene U 0.000425 0.00250 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 50 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 50 of 70 QUALITY CONTROL SUMMARYWG1962462 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3865698-2 11/19/22 11:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.00255 0.00500 2-Butanone (MEK)U 0.0635 0.100 Methylene Chloride U 0.00664 0.0250 4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250 Methyl tert-butyl ether U 0.000350 0.00100 Naphthalene U 0.00488 0.0125 n-Propylbenzene U 0.000950 0.00500 Styrene 0.00193 J 0.000229 0.0125 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 Tetrachloroethene U 0.000896 0.00250 Toluene U 0.00130 0.00500 1,2,3-Trichlorobenzene U 0.00733 0.0125 1,2,4-Trichlorobenzene U 0.00440 0.0125 1,1,1-Trichloroethane U 0.000923 0.00250 1,1,2-Trichloroethane U 0.000597 0.00250 Trichloroethene U 0.000584 0.00100 Trichlorofluoromethane U 0.000827 0.00250 1,2,3-Trichloropropane U 0.00162 0.0125 1,2,4-Trimethylbenzene U 0.00158 0.00500 1,2,3-Trimethylbenzene U 0.00158 0.00500 1,3,5-Trimethylbenzene U 0.00200 0.00500 Vinyl chloride U 0.00116 0.00250 Xylenes, Total U 0.000880 0.00650 (S) Toluene-d8 103 75.0-131 (S) 4-Bromofluorobenzene 98.8 67.0-138 (S) 1,2-Dichloroethane-d4 82.8 70.0-130 Laboratory Control Sample (LCS) (LCS) R3865698-1 11/19/22 10:03 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Acetone 0.625 0.316 50.6 10.0-160 Acrylonitrile 0.625 0.574 91.8 45.0-153 Benzene 0.125 0.129 103 70.0-123 Bromobenzene 0.125 0.125 100 73.0-121 Bromodichloromethane 0.125 0.123 98.4 73.0-121 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 51 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 51 of 70 QUALITY CONTROL SUMMARYWG1962462 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) (LCS) R3865698-1 11/19/22 10:03 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Bromoform 0.125 0.127 102 64.0-132 Bromomethane 0.125 0.0771 61.7 56.0-147 n-Butylbenzene 0.125 0.119 95.2 68.0-135 sec-Butylbenzene 0.125 0.116 92.8 74.0-130 tert-Butylbenzene 0.125 0.118 94.4 75.0-127 Carbon tetrachloride 0.125 0.117 93.6 66.0-128 Chlorobenzene 0.125 0.132 106 76.0-128 Chlorodibromomethane 0.125 0.123 98.4 74.0-127 Chloroethane 0.125 0.0761 60.9 61.0-134 J4 Chloroform 0.125 0.115 92.0 72.0-123 Chloromethane 0.125 0.0719 57.5 51.0-138 2-Chlorotoluene 0.125 0.121 96.8 75.0-124 4-Chlorotoluene 0.125 0.122 97.6 75.0-124 1,2-Dibromo-3-Chloropropane 0.125 0.118 94.4 59.0-130 1,2-Dibromoethane 0.125 0.132 106 74.0-128 Dibromomethane 0.125 0.121 96.8 75.0-122 1,2-Dichlorobenzene 0.125 0.132 106 76.0-124 1,3-Dichlorobenzene 0.125 0.129 103 76.0-125 1,4-Dichlorobenzene 0.125 0.126 101 77.0-121 Dichlorodifluoromethane 0.125 0.101 80.8 43.0-156 1,1-Dichloroethane 0.125 0.115 92.0 70.0-127 1,2-Dichloroethane 0.125 0.110 88.0 65.0-131 1,1-Dichloroethene 0.125 0.116 92.8 65.0-131 cis-1,2-Dichloroethene 0.125 0.121 96.8 73.0-125 trans-1,2-Dichloroethene 0.125 0.124 99.2 71.0-125 1,2-Dichloropropane 0.125 0.124 99.2 74.0-125 1,1-Dichloropropene 0.125 0.126 101 73.0-125 1,3-Dichloropropane 0.125 0.132 106 80.0-125 cis-1,3-Dichloropropene 0.125 0.126 101 76.0-127 trans-1,3-Dichloropropene 0.125 0.123 98.4 73.0-127 2,2-Dichloropropane 0.125 0.102 81.6 59.0-135 Di-isopropyl ether 0.125 0.119 95.2 60.0-136 Ethylbenzene 0.125 0.129 103 74.0-126 Hexachloro-1,3-butadiene 0.125 0.140 112 57.0-150 Isopropylbenzene 0.125 0.127 102 72.0-127 p-Isopropyltoluene 0.125 0.123 98.4 72.0-133 2-Butanone (MEK)0.625 0.596 95.4 30.0-160 Methylene Chloride 0.125 0.129 103 68.0-123 4-Methyl-2-pentanone (MIBK)0.625 0.585 93.6 56.0-143 Methyl tert-butyl ether 0.125 0.106 84.8 66.0-132 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 52 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 52 of 70 QUALITY CONTROL SUMMARYWG1962462 Volatile Organic Compounds (GC/MS) by Method 8260D L1558771-02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) (LCS) R3865698-1 11/19/22 10:03 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Naphthalene 0.125 0.149 119 59.0-130 n-Propylbenzene 0.125 0.119 95.2 74.0-126 Styrene 0.125 0.125 100 72.0-127 1,1,1,2-Tetrachloroethane 0.125 0.128 102 74.0-129 1,1,2,2-Tetrachloroethane 0.125 0.115 92.0 68.0-128 1,1,2-Trichlorotrifluoroethane 0.125 0.121 96.8 61.0-139 Tetrachloroethene 0.125 0.137 110 70.0-136 Toluene 0.125 0.132 106 75.0-121 1,2,3-Trichlorobenzene 0.125 0.172 138 59.0-139 1,2,4-Trichlorobenzene 0.125 0.178 142 62.0-137 J4 1,1,1-Trichloroethane 0.125 0.115 92.0 69.0-126 1,1,2-Trichloroethane 0.125 0.124 99.2 78.0-123 Trichloroethene 0.125 0.133 106 76.0-126 Trichlorofluoromethane 0.125 0.0975 78.0 61.0-142 1,2,3-Trichloropropane 0.125 0.113 90.4 67.0-129 1,2,4-Trimethylbenzene 0.125 0.122 97.6 70.0-126 1,2,3-Trimethylbenzene 0.125 0.114 91.2 74.0-124 1,3,5-Trimethylbenzene 0.125 0.116 92.8 73.0-127 Vinyl chloride 0.125 0.0695 55.6 63.0-134 J4 Xylenes, Total 0.375 0.399 106 72.0-127 (S) Toluene-d8 101 75.0-131 (S) 4-Bromofluorobenzene 100 67.0-138 (S) 1,2-Dichloroethane-d4 84.8 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 53 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 53 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 Method Blank (MB) (MB) R3863963-2 11/22/22 10:54 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acenaphthene U 0.00539 0.0333 Acenaphthylene U 0.00469 0.0333 Anthracene U 0.00593 0.0333 Benzidine U 0.0626 1.67 Benzo(a)anthracene U 0.00587 0.0333 Benzo(b)fluoranthene U 0.00621 0.0333 Benzo(k)fluoranthene U 0.00592 0.0333 Benzo(g,h,i)perylene U 0.00609 0.0333 Benzo(a)pyrene U 0.00619 0.0333 Bis(2-chlorethoxy)methane U 0.0100 0.333 Bis(2-chloroethyl)ether U 0.0110 0.333 2,2-Oxybis(1-Chloropropane)U 0.0144 0.333 4-Bromophenyl-phenylether U 0.0117 0.333 2-Chloronaphthalene U 0.00585 0.0333 4-Chlorophenyl-phenylether U 0.0116 0.333 Chrysene U 0.00662 0.0333 Dibenz(a,h)anthracene U 0.00923 0.0333 1,2-Dichlorobenzene U 0.00987 0.333 1,3-Dichlorobenzene U 0.0101 0.333 1,4-Dichlorobenzene U 0.00991 0.333 3,3-Dichlorobenzidine U 0.0123 0.333 2,4-Dinitrotoluene U 0.00955 0.333 2,6-Dinitrotoluene U 0.0109 0.333 Fluoranthene U 0.00601 0.0333 Fluorene U 0.00542 0.0333 Hexachlorobenzene U 0.0118 0.333 Hexachloro-1,3-butadiene U 0.0112 0.333 Hexachlorocyclopentadiene U 0.0175 0.333 Hexachloroethane U 0.0131 0.333 Indeno(1,2,3-cd)pyrene U 0.00941 0.0333 Isophorone U 0.0102 0.333 Naphthalene U 0.00836 0.0333 Nitrobenzene U 0.0116 0.333 n-Nitrosodimethylamine U 0.0494 0.333 n-Nitrosodiphenylamine U 0.0252 0.333 n-Nitrosodi-n-propylamine U 0.0111 0.333 Phenanthrene U 0.00661 0.0333 Benzylbutyl phthalate U 0.0104 0.333 Bis(2-ethylhexyl)phthalate U 0.0422 0.333 Di-n-butyl phthalate U 0.0114 0.333 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 54 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 54 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 Method Blank (MB) (MB) R3863963-2 11/22/22 10:54 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Diethyl phthalate U 0.0110 0.333 Dimethyl phthalate U 0.0706 0.333 Di-n-octyl phthalate U 0.0225 0.333 Pyrene U 0.00648 0.0333 1,2,4-Trichlorobenzene U 0.0104 0.333 4-Chloro-3-methylphenol U 0.0108 0.333 2-Chlorophenol U 0.0110 0.333 2,4-Dichlorophenol U 0.00970 0.333 2,4-Dimethylphenol U 0.00870 0.333 4,6-Dinitro-2-methylphenol U 0.0755 0.333 2,4-Dinitrophenol U 0.0779 0.333 2-Nitrophenol U 0.0119 0.333 4-Nitrophenol U 0.0104 0.333 Pentachlorophenol U 0.00896 0.333 Phenol U 0.0134 0.333 2,4,6-Trichlorophenol U 0.0107 0.333 (S) 2-Fluorophenol 76.6 12.0-120 (S) Phenol-d5 70.3 10.0-120 (S) Nitrobenzene-d5 65.2 10.0-122 (S) 2-Fluorobiphenyl 74.2 15.0-120 (S) 2,4,6-Tribromophenol 72.1 10.0-127 (S) p-Terphenyl-d14 87.1 10.0-120 Laboratory Control Sample (LCS) (LCS) R3863963-1 11/22/22 10:30 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Acenaphthene 0.666 0.441 66.2 38.0-120 Acenaphthylene 0.666 0.494 74.2 40.0-120 Anthracene 0.666 0.448 67.3 42.0-120 Benzidine 1.33 0.146 11.0 10.0-120 Benzo(a)anthracene 0.666 0.514 77.2 44.0-120 Benzo(b)fluoranthene 0.666 0.486 73.0 43.0-120 Benzo(k)fluoranthene 0.666 0.477 71.6 44.0-120 Benzo(g,h,i)perylene 0.666 0.447 67.1 43.0-120 Benzo(a)pyrene 0.666 0.543 81.5 45.0-120 Bis(2-chlorethoxy)methane 0.666 0.353 53.0 20.0-120 Bis(2-chloroethyl)ether 0.666 0.346 52.0 16.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 55 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 55 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 Laboratory Control Sample (LCS) (LCS) R3863963-1 11/22/22 10:30 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2,2-Oxybis(1-Chloropropane)0.666 0.427 64.1 23.0-120 4-Bromophenyl-phenylether 0.666 0.533 80.0 40.0-120 2-Chloronaphthalene 0.666 0.453 68.0 35.0-120 4-Chlorophenyl-phenylether 0.666 0.490 73.6 40.0-120 Chrysene 0.666 0.481 72.2 43.0-120 Dibenz(a,h)anthracene 0.666 0.462 69.4 44.0-120 1,2-Dichlorobenzene 0.666 0.423 63.5 32.0-120 1,3-Dichlorobenzene 0.666 0.400 60.1 30.0-120 1,4-Dichlorobenzene 0.666 0.410 61.6 31.0-120 3,3-Dichlorobenzidine 1.33 0.769 57.8 28.0-120 2,4-Dinitrotoluene 0.666 0.539 80.9 45.0-120 2,6-Dinitrotoluene 0.666 0.519 77.9 42.0-120 Fluoranthene 0.666 0.498 74.8 44.0-120 Fluorene 0.666 0.459 68.9 41.0-120 Hexachlorobenzene 0.666 0.478 71.8 39.0-120 Hexachloro-1,3-butadiene 0.666 0.408 61.3 15.0-120 Hexachlorocyclopentadiene 0.666 0.421 63.2 15.0-120 Hexachloroethane 0.666 0.394 59.2 17.0-120 Indeno(1,2,3-cd)pyrene 0.666 0.449 67.4 45.0-120 Isophorone 0.666 0.341 51.2 23.0-120 Naphthalene 0.666 0.360 54.1 18.0-120 Nitrobenzene 0.666 0.324 48.6 17.0-120 n-Nitrosodimethylamine 0.666 0.303 45.5 10.0-125 n-Nitrosodiphenylamine 0.666 0.379 56.9 40.0-120 n-Nitrosodi-n-propylamine 0.666 0.398 59.8 26.0-120 Phenanthrene 0.666 0.454 68.2 42.0-120 Benzylbutyl phthalate 0.666 0.463 69.5 40.0-120 Bis(2-ethylhexyl)phthalate 0.666 0.464 69.7 41.0-120 Di-n-butyl phthalate 0.666 0.426 64.0 43.0-120 Diethyl phthalate 0.666 0.501 75.2 43.0-120 Dimethyl phthalate 0.666 0.481 72.2 43.0-120 Di-n-octyl phthalate 0.666 0.484 72.7 40.0-120 Pyrene 0.666 0.458 68.8 41.0-120 1,2,4-Trichlorobenzene 0.666 0.395 59.3 17.0-120 4-Chloro-3-methylphenol 0.666 0.379 56.9 28.0-120 2-Chlorophenol 0.666 0.435 65.3 28.0-120 2,4-Dichlorophenol 0.666 0.410 61.6 25.0-120 2,4-Dimethylphenol 0.666 0.352 52.9 15.0-120 4,6-Dinitro-2-methylphenol 0.666 0.457 68.6 16.0-120 2,4-Dinitrophenol 0.666 0.342 51.4 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 56 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 56 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 Laboratory Control Sample (LCS) (LCS) R3863963-1 11/22/22 10:30 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2-Nitrophenol 0.666 0.401 60.2 20.0-120 4-Nitrophenol 0.666 0.501 75.2 27.0-120 Pentachlorophenol 0.666 0.456 68.5 29.0-120 Phenol 0.666 0.405 60.8 28.0-120 2,4,6-Trichlorophenol 0.666 0.477 71.6 37.0-120 (S) 2-Fluorophenol 69.8 12.0-120 (S) Phenol-d5 64.9 10.0-120 (S) Nitrobenzene-d5 50.8 10.0-122 (S) 2-Fluorobiphenyl 68.2 15.0-120 (S) 2,4,6-Tribromophenol 83.0 10.0-127 (S) p-Terphenyl-d14 73.3 10.0-120 L1557921-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557921-01 11/22/22 16:05 • (MS) R3863963-3 11/22/22 16:29 • (MSD) R3863963-4 11/22/22 16:53 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.834 U 0.548 0.580 65.8 70.4 1 18.0-120 5.60 32 Acenaphthylene 0.834 U 0.609 0.652 73.0 79.1 1 25.0-120 6.81 32 Anthracene 0.834 U 0.567 0.594 68.0 72.1 1 22.0-120 4.57 29 Benzidine 1.67 U U U 2.46 3.68 1 10.0-120 J6 J6 38.1 40 Benzo(a)anthracene 0.834 U 0.652 0.672 78.2 81.6 1 25.0-120 3.05 29 Benzo(b)fluoranthene 0.834 U 0.658 0.673 78.9 81.7 1 19.0-122 2.28 31 Benzo(k)fluoranthene 0.834 U 0.605 0.652 72.6 79.1 1 23.0-120 7.44 30 Benzo(g,h,i)perylene 0.834 U 0.357 0.308 42.9 37.4 1 10.0-120 14.8 33 Benzo(a)pyrene 0.834 U 0.697 0.722 83.6 87.7 1 24.0-120 3.56 30 Bis(2-chlorethoxy)methane 0.834 U 0.427 0.452 51.2 54.9 1 10.0-120 5.75 34 Bis(2-chloroethyl)ether 0.834 U 0.433 0.451 52.0 54.8 1 10.0-120 4.00 40 2,2-Oxybis(1-Chloropropane)0.834 U 0.515 0.551 61.8 66.9 1 10.0-120 6.64 40 4-Bromophenyl-phenylether 0.834 U 0.668 0.692 80.2 84.0 1 27.0-120 3.53 30 2-Chloronaphthalene 0.834 U 0.554 0.589 66.5 71.5 1 20.0-120 5.97 32 4-Chlorophenyl-phenylether 0.834 U 0.610 0.645 73.2 78.4 1 24.0-120 5.63 29 Chrysene 0.834 U 0.616 0.629 73.9 76.4 1 21.0-120 2.03 29 Dibenz(a,h)anthracene 0.834 U 0.450 0.402 53.9 48.8 1 10.0-120 11.3 32 1,2-Dichlorobenzene 0.834 U 0.513 0.532 61.5 64.6 1 10.0-120 3.63 38 1,3-Dichlorobenzene 0.834 U 0.479 0.505 57.4 61.3 1 10.0-120 5.39 40 1,4-Dichlorobenzene 0.834 U 0.491 0.519 58.9 63.0 1 10.0-120 5.50 39 3,3-Dichlorobenzidine 1.67 U 0.594 0.727 35.6 44.3 1 10.0-120 20.3 34 2,4-Dinitrotoluene 0.834 U 0.676 0.729 81.1 88.5 1 30.0-120 7.55 31 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 57 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 57 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 L1557921-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557921-01 11/22/22 16:05 • (MS) R3863963-3 11/22/22 16:29 • (MSD) R3863963-4 11/22/22 16:53 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% 2,6-Dinitrotoluene 0.834 U 0.628 0.671 75.3 81.4 1 25.0-120 6.61 31 Fluoranthene 0.834 U 0.637 0.664 76.4 80.7 1 18.0-126 4.27 32 Fluorene 0.834 U 0.572 0.602 68.6 73.2 1 25.0-120 5.16 30 Hexachlorobenzene 0.834 U 0.602 0.631 72.3 76.7 1 27.0-120 4.71 28 Hexachloro-1,3-butadiene 0.834 U 0.490 0.519 58.8 63.0 1 10.0-120 5.76 38 Hexachlorocyclopentadiene 0.834 U 0.0500 0.0544 6.00 6.61 1 10.0-120 J6 J6 8.46 40 Hexachloroethane 0.834 U 0.314 0.320 37.7 38.8 1 10.0-120 1.59 40 Indeno(1,2,3-cd)pyrene 0.834 U 0.426 0.380 51.1 46.2 1 10.0-120 11.3 32 Isophorone 0.834 U 0.410 0.437 49.2 53.1 1 13.0-120 6.26 34 Naphthalene 0.834 U 0.436 0.464 52.3 56.3 1 10.0-120 6.18 35 Nitrobenzene 0.834 U 0.392 0.419 47.0 50.9 1 10.0-120 6.85 36 n-Nitrosodimethylamine 0.834 U 0.349 0.354 41.8 42.9 1 10.0-127 1.44 40 n-Nitrosodiphenylamine 0.834 U 0.434 0.477 52.1 58.0 1 17.0-120 9.42 29 n-Nitrosodi-n-propylamine 0.834 U 0.496 0.524 59.5 63.7 1 10.0-120 5.45 37 Phenanthrene 0.834 U 0.565 0.602 67.7 73.2 1 17.0-120 6.49 31 Benzylbutyl phthalate 0.834 U 0.618 0.642 74.1 77.9 1 23.0-120 3.81 30 Bis(2-ethylhexyl)phthalate 0.834 U 0.624 0.642 74.8 77.9 1 17.0-126 2.79 30 Di-n-butyl phthalate 0.834 U 0.553 0.572 66.4 69.5 1 30.0-120 3.37 29 Diethyl phthalate 0.834 U 0.626 0.662 75.2 80.4 1 26.0-120 5.49 28 Dimethyl phthalate 0.834 U 0.582 0.629 69.8 76.4 1 25.0-120 7.72 29 Di-n-octyl phthalate 0.834 U 0.700 0.700 83.9 85.0 1 21.0-123 0.000 29 Pyrene 0.834 U 0.573 0.594 68.8 72.1 1 16.0-121 3.46 32 1,2,4-Trichlorobenzene 0.834 U 0.477 0.498 57.3 60.4 1 12.0-120 4.15 37 4-Chloro-3-methylphenol 0.834 U 0.474 0.508 56.8 61.7 1 15.0-120 6.95 30 2-Chlorophenol 0.834 U 0.529 0.566 63.5 68.7 1 15.0-120 6.69 37 2,4-Dichlorophenol 0.834 U 0.496 0.533 59.5 64.7 1 20.0-120 7.12 31 2,4-Dimethylphenol 0.834 U 0.307 0.392 36.8 47.5 1 10.0-120 24.2 33 4,6-Dinitro-2-methylphenol 0.834 U 0.456 0.493 54.7 59.8 1 10.0-120 7.72 39 2,4-Dinitrophenol 0.834 U 0.389 0.436 46.7 52.9 1 10.0-121 11.3 40 2-Nitrophenol 0.834 U 0.508 0.532 60.9 64.6 1 12.0-120 4.62 39 4-Nitrophenol 0.834 U 0.687 0.735 82.4 89.3 1 10.0-137 6.75 32 Pentachlorophenol 0.834 U 0.661 0.693 79.2 84.2 1 10.0-160 4.85 31 Phenol 0.834 U 0.498 0.532 59.7 64.6 1 12.0-120 6.63 38 2,4,6-Trichlorophenol 0.834 U 0.570 0.642 68.3 77.9 1 19.0-120 11.9 32 (S) 2-Fluorophenol 71.8 75.0 12.0-120 (S) Phenol-d5 67.1 68.7 10.0-120 (S) Nitrobenzene-d5 51.2 52.1 10.0-122 (S) 2-Fluorobiphenyl 69.4 72.7 15.0-120 (S) 2,4,6-Tribromophenol 87.6 89.6 10.0-127 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 58 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 58 of 70 QUALITY CONTROL SUMMARYWG1962624 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-01 L1557921-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1557921-01 11/22/22 16:05 • (MS) R3863963-3 11/22/22 16:29 • (MSD) R3863963-4 11/22/22 16:53 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% (S) p-Terphenyl-d14 78.5 77.6 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 59 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 59 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3865164-2 11/25/22 07:17 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acenaphthene U 0.00539 0.0333 Acenaphthylene U 0.00469 0.0333 Anthracene U 0.00593 0.0333 Benzidine U 0.0626 1.67 Benzo(a)anthracene U 0.00587 0.0333 Benzo(b)fluoranthene U 0.00621 0.0333 Benzo(k)fluoranthene U 0.00592 0.0333 Benzo(g,h,i)perylene U 0.00609 0.0333 Benzo(a)pyrene U 0.00619 0.0333 Bis(2-chlorethoxy)methane U 0.0100 0.333 Bis(2-chloroethyl)ether U 0.0110 0.333 2,2-Oxybis(1-Chloropropane)U 0.0144 0.333 4-Bromophenyl-phenylether U 0.0117 0.333 2-Chloronaphthalene U 0.00585 0.0333 4-Chlorophenyl-phenylether U 0.0116 0.333 Chrysene U 0.00662 0.0333 Dibenz(a,h)anthracene U 0.00923 0.0333 1,2-Dichlorobenzene U 0.00987 0.333 1,3-Dichlorobenzene U 0.0101 0.333 1,4-Dichlorobenzene U 0.00991 0.333 3,3-Dichlorobenzidine U 0.0123 0.333 2,4-Dinitrotoluene U 0.00955 0.333 2,6-Dinitrotoluene U 0.0109 0.333 Fluoranthene U 0.00601 0.0333 Fluorene U 0.00542 0.0333 Hexachlorobenzene U 0.0118 0.333 Hexachloro-1,3-butadiene U 0.0112 0.333 Hexachlorocyclopentadiene U 0.0175 0.333 Hexachloroethane U 0.0131 0.333 Indeno(1,2,3-cd)pyrene U 0.00941 0.0333 Isophorone U 0.0102 0.333 Naphthalene U 0.00836 0.0333 Nitrobenzene U 0.0116 0.333 n-Nitrosodimethylamine U 0.0494 0.333 n-Nitrosodiphenylamine U 0.0252 0.333 n-Nitrosodi-n-propylamine U 0.0111 0.333 Phenanthrene U 0.00661 0.0333 Benzylbutyl phthalate U 0.0104 0.333 Bis(2-ethylhexyl)phthalate U 0.0422 0.333 Di-n-butyl phthalate U 0.0114 0.333 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 60 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 60 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 Method Blank (MB) (MB) R3865164-2 11/25/22 07:17 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Diethyl phthalate U 0.0110 0.333 Dimethyl phthalate U 0.0706 0.333 Di-n-octyl phthalate U 0.0225 0.333 Pyrene U 0.00648 0.0333 1,2,4-Trichlorobenzene U 0.0104 0.333 4-Chloro-3-methylphenol U 0.0108 0.333 2-Chlorophenol U 0.0110 0.333 2,4-Dichlorophenol U 0.00970 0.333 2,4-Dimethylphenol U 0.00870 0.333 4,6-Dinitro-2-methylphenol U 0.0755 0.333 2,4-Dinitrophenol U 0.0779 0.333 2-Nitrophenol U 0.0119 0.333 4-Nitrophenol U 0.0104 0.333 Pentachlorophenol U 0.00896 0.333 Phenol U 0.0134 0.333 2,4,6-Trichlorophenol U 0.0107 0.333 (S) 2-Fluorophenol 77.6 12.0-120 (S) Phenol-d5 73.1 10.0-120 (S) Nitrobenzene-d5 67.0 10.0-122 (S) 2-Fluorobiphenyl 67.3 15.0-120 (S) 2,4,6-Tribromophenol 83.8 10.0-127 (S) p-Terphenyl-d14 79.3 10.0-120 Laboratory Control Sample (LCS) (LCS) R3865164-1 11/25/22 06:57 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Acenaphthene 0.666 0.524 78.7 38.0-120 Acenaphthylene 0.666 0.537 80.6 40.0-120 Anthracene 0.666 0.528 79.3 42.0-120 Benzidine 1.33 0.286 21.5 10.0-120 Benzo(a)anthracene 0.666 0.565 84.8 44.0-120 Benzo(b)fluoranthene 0.666 0.543 81.5 43.0-120 Benzo(k)fluoranthene 0.666 0.539 80.9 44.0-120 Benzo(g,h,i)perylene 0.666 0.546 82.0 43.0-120 Benzo(a)pyrene 0.666 0.592 88.9 45.0-120 Bis(2-chlorethoxy)methane 0.666 0.387 58.1 20.0-120 Bis(2-chloroethyl)ether 0.666 0.556 83.5 16.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 61 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 61 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) (LCS) R3865164-1 11/25/22 06:57 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2,2-Oxybis(1-Chloropropane)0.666 0.496 74.5 23.0-120 4-Bromophenyl-phenylether 0.666 0.582 87.4 40.0-120 2-Chloronaphthalene 0.666 0.501 75.2 35.0-120 4-Chlorophenyl-phenylether 0.666 0.529 79.4 40.0-120 Chrysene 0.666 0.558 83.8 43.0-120 Dibenz(a,h)anthracene 0.666 0.543 81.5 44.0-120 1,2-Dichlorobenzene 0.666 0.473 71.0 32.0-120 1,3-Dichlorobenzene 0.666 0.456 68.5 30.0-120 1,4-Dichlorobenzene 0.666 0.470 70.6 31.0-120 3,3-Dichlorobenzidine 1.33 0.940 70.7 28.0-120 2,4-Dinitrotoluene 0.666 0.656 98.5 45.0-120 2,6-Dinitrotoluene 0.666 0.606 91.0 42.0-120 Fluoranthene 0.666 0.567 85.1 44.0-120 Fluorene 0.666 0.521 78.2 41.0-120 Hexachlorobenzene 0.666 0.554 83.2 39.0-120 Hexachloro-1,3-butadiene 0.666 0.407 61.1 15.0-120 Hexachlorocyclopentadiene 0.666 0.397 59.6 15.0-120 Hexachloroethane 0.666 0.443 66.5 17.0-120 Indeno(1,2,3-cd)pyrene 0.666 0.513 77.0 45.0-120 Isophorone 0.666 0.376 56.5 23.0-120 Naphthalene 0.666 0.381 57.2 18.0-120 Nitrobenzene 0.666 0.412 61.9 17.0-120 n-Nitrosodimethylamine 0.666 0.554 83.2 10.0-125 n-Nitrosodiphenylamine 0.666 0.465 69.8 40.0-120 n-Nitrosodi-n-propylamine 0.666 0.486 73.0 26.0-120 Phenanthrene 0.666 0.552 82.9 42.0-120 Benzylbutyl phthalate 0.666 0.584 87.7 40.0-120 Bis(2-ethylhexyl)phthalate 0.666 0.559 83.9 41.0-120 Di-n-butyl phthalate 0.666 0.555 83.3 43.0-120 Diethyl phthalate 0.666 0.528 79.3 43.0-120 Dimethyl phthalate 0.666 0.548 82.3 43.0-120 Di-n-octyl phthalate 0.666 0.569 85.4 40.0-120 Pyrene 0.666 0.549 82.4 41.0-120 1,2,4-Trichlorobenzene 0.666 0.383 57.5 17.0-120 4-Chloro-3-methylphenol 0.666 0.446 67.0 28.0-120 2-Chlorophenol 0.666 0.507 76.1 28.0-120 2,4-Dichlorophenol 0.666 0.422 63.4 25.0-120 2,4-Dimethylphenol 0.666 0.404 60.7 15.0-120 4,6-Dinitro-2-methylphenol 0.666 0.717 108 16.0-120 2,4-Dinitrophenol 0.666 0.641 96.2 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 62 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 62 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 Laboratory Control Sample (LCS) (LCS) R3865164-1 11/25/22 06:57 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% 2-Nitrophenol 0.666 0.478 71.8 20.0-120 4-Nitrophenol 0.666 0.633 95.0 27.0-120 Pentachlorophenol 0.666 0.569 85.4 29.0-120 Phenol 0.666 0.532 79.9 28.0-120 2,4,6-Trichlorophenol 0.666 0.500 75.1 37.0-120 (S) 2-Fluorophenol 78.8 12.0-120 (S) Phenol-d5 74.3 10.0-120 (S) Nitrobenzene-d5 59.5 10.0-122 (S) 2-Fluorobiphenyl 67.9 15.0-120 (S) 2,4,6-Tribromophenol 94.0 10.0-127 (S) p-Terphenyl-d14 79.9 10.0-120 L1558771-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558771-08 11/25/22 12:40 • (MS) R3865164-3 11/25/22 13:00 • (MSD) R3865164-4 11/25/22 13:20 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.815 0.0644 0.675 0.613 75.0 67.5 2 18.0-120 9.67 32 Acenaphthylene 0.815 0.496 0.877 0.772 46.8 34.0 2 25.0-120 12.7 32 Anthracene 0.815 0.340 0.756 0.694 51.1 43.6 2 22.0-120 8.59 29 Benzidine 1.63 U U U 0.000 0.000 2 10.0-120 J6 J6 0.000 40 Benzo(a)anthracene 0.815 1.09 1.12 0.977 3.36 0.000 2 25.0-120 J6 J6 13.7 29 Benzo(b)fluoranthene 0.815 1.73 1.36 1.16 0.000 0.000 2 19.0-122 J6 J6 15.3 31 Benzo(k)fluoranthene 0.815 0.494 0.903 0.750 50.2 31.4 2 23.0-120 18.5 30 Benzo(g,h,i)perylene 0.815 0.831 0.922 0.659 11.2 0.000 2 10.0-120 J3 J6 33.3 33 Benzo(a)pyrene 0.815 1.53 1.38 1.13 0.000 0.000 2 24.0-120 J6 J6 20.0 30 Bis(2-chlorethoxy)methane 0.815 U 0.527 0.447 64.7 55.1 2 10.0-120 16.4 34 Bis(2-chloroethyl)ether 0.815 U 0.620 0.483 76.1 59.5 2 10.0-120 24.8 40 2,2-Oxybis(1-Chloropropane)0.815 U 0.617 0.517 75.7 63.7 2 10.0-120 17.6 40 4-Bromophenyl-phenylether 0.815 U 0.721 0.668 88.5 82.2 2 27.0-120 7.71 30 2-Chloronaphthalene 0.815 U 0.639 0.569 78.4 70.1 2 20.0-120 11.5 32 4-Chlorophenyl-phenylether 0.815 U 0.674 0.622 82.7 76.5 2 24.0-120 8.08 29 Chrysene 0.815 1.32 1.21 1.00 0.000 0.000 2 21.0-120 J6 J6 18.6 29 Dibenz(a,h)anthracene 0.815 0.243 0.685 0.551 54.3 37.9 2 10.0-120 21.8 32 1,2-Dichlorobenzene 0.815 U 0.615 0.471 75.5 58.0 2 10.0-120 26.6 38 1,3-Dichlorobenzene 0.815 U 0.588 0.443 72.2 54.6 2 10.0-120 28.0 40 1,4-Dichlorobenzene 0.815 U 0.599 0.451 73.5 55.5 2 10.0-120 28.2 39 3,3-Dichlorobenzidine 1.63 U 0.845 0.430 51.8 26.5 2 10.0-120 J3 65.1 34 2,4-Dinitrotoluene 0.815 U 0.908 0.858 111 106 2 30.0-120 5.64 31 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 63 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 63 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 L1558771-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558771-08 11/25/22 12:40 • (MS) R3865164-3 11/25/22 13:00 • (MSD) R3865164-4 11/25/22 13:20 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% 2,6-Dinitrotoluene 0.815 U 0.737 0.704 90.5 86.7 2 25.0-120 4.67 31 Fluoranthene 0.815 1.47 1.27 1.11 0.000 0.000 2 18.0-126 J6 J6 13.4 32 Fluorene 0.815 0.189 0.727 0.653 66.1 57.1 2 25.0-120 10.8 30 Hexachlorobenzene 0.815 U 0.698 0.629 85.6 77.5 2 27.0-120 10.3 28 Hexachloro-1,3-butadiene 0.815 U 0.609 0.511 74.8 62.9 2 10.0-120 17.6 38 Hexachlorocyclopentadiene 0.815 U 0.0539 0.0475 6.62 5.84 2 10.0-120 J6 J6 12.8 40 Hexachloroethane 0.815 U 0.420 0.344 51.5 42.3 2 10.0-120 19.9 40 Indeno(1,2,3-cd)pyrene 0.815 0.882 0.969 0.730 10.7 0.000 2 10.0-120 J6 28.2 32 Isophorone 0.815 U 0.497 0.433 61.0 53.4 2 13.0-120 13.7 34 Naphthalene 0.815 0.167 0.587 0.483 51.5 39.0 2 10.0-120 19.3 35 Nitrobenzene 0.815 U 0.559 0.455 68.7 56.0 2 10.0-120 20.6 36 n-Nitrosodimethylamine 0.815 U 0.497 0.344 61.0 42.3 2 10.0-127 36.4 40 n-Nitrosodiphenylamine 0.815 U 0.548 0.518 67.3 63.8 2 17.0-120 5.61 29 n-Nitrosodi-n-propylamine 0.815 U 0.594 0.496 72.9 61.0 2 10.0-120 18.1 37 Phenanthrene 0.815 1.54 1.12 0.991 0.000 0.000 2 17.0-120 J6 J6 11.9 31 Benzylbutyl phthalate 0.815 U 0.681 0.630 83.6 77.6 2 23.0-120 7.79 30 Bis(2-ethylhexyl)phthalate 0.815 U 0.646 0.594 79.4 73.2 2 17.0-126 8.43 30 Di-n-butyl phthalate 0.815 U 0.655 0.605 80.4 74.5 2 30.0-120 7.91 29 Diethyl phthalate 0.815 U 0.673 0.615 82.6 75.8 2 26.0-120 8.90 28 Dimethyl phthalate 0.815 U 0.686 0.624 84.3 76.8 2 25.0-120 9.51 29 Di-n-octyl phthalate 0.815 U 0.690 0.632 84.7 77.8 2 21.0-123 8.86 29 Pyrene 0.815 1.94 1.43 1.23 0.000 0.000 2 16.0-121 J6 J6 15.0 32 1,2,4-Trichlorobenzene 0.815 U 0.572 0.480 70.2 59.0 2 12.0-120 17.5 37 4-Chloro-3-methylphenol 0.815 U 0.633 0.583 77.7 71.8 2 15.0-120 8.20 30 2-Chlorophenol 0.815 U 0.630 0.544 77.4 67.0 2 15.0-120 14.6 37 2,4-Dichlorophenol 0.815 U 0.599 0.558 73.5 68.7 2 20.0-120 7.10 31 2,4-Dimethylphenol 0.815 U 0.564 0.517 69.3 63.7 2 10.0-120 8.76 33 4,6-Dinitro-2-methylphenol 0.815 U 0.810 0.788 99.4 97.1 2 10.0-120 2.65 39 2,4-Dinitrophenol 0.815 U 0.818 0.803 100 98.9 2 10.0-121 1.84 40 2-Nitrophenol 0.815 U 0.701 0.580 86.1 71.5 2 12.0-120 18.9 39 4-Nitrophenol 0.815 U 0.845 0.811 104 99.8 2 10.0-137 4.06 32 Pentachlorophenol 0.815 U 0.818 0.756 100 93.1 2 10.0-160 7.91 31 Phenol 0.815 U 0.638 0.553 78.3 68.1 2 12.0-120 14.2 38 2,4,6-Trichlorophenol 0.815 U 0.650 0.614 79.8 75.6 2 19.0-120 5.71 32 (S) 2-Fluorophenol 79.4 66.4 12.0-120 (S) Phenol-d5 71.9 66.1 10.0-120 (S) Nitrobenzene-d5 66.1 54.0 10.0-122 (S) 2-Fluorobiphenyl 70.0 63.2 15.0-120 (S) 2,4,6-Tribromophenol 103 99.1 10.0-127 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 64 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 64 of 70 QUALITY CONTROL SUMMARYWG1962878 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1558771-02,03,04,05,06,07,08,09,10,11 L1558771-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1558771-08 11/25/22 12:40 • (MS) R3865164-3 11/25/22 13:00 • (MSD) R3865164-4 11/25/22 13:20 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% (S) p-Terphenyl-d14 78.3 73.3 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 65 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 65 of 70 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions (dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. MDL (dry)Method Detection Limit. RDL Reported Detection Limit. RDL (dry)Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptable. C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Data is likely to show a low bias concerning the result. E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 66 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 66 of 70 GLOSSARY OF TERMS Qualifier Description J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 67 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 67 of 70 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:30 68 of 70 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.EAS-225234 L1558771 12/01/22 22:44 68 of 70 ANALYTICAL REPORT December 27, 2022 EAS Professionals, Inc. Sample Delivery Group:L1568172 Samples Received:12/15/2022 Project Number:22-5234 Description:450 Polo Road Report To:Ashley Brown 9 Pilgrim Road Greenville, SC 29607 Entire Report Reviewed By: December 27, 2022 [Preliminary Report] Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 1 of 63 December 27, 2022 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 1 of 63 TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 5 Sr: Sample Results 6 MW-1 L1568172-01 6 MW-5 L1568172-02 9 MW-4 L1568172-03 12 MW-3 L1568172-04 15 MW-3 DUPE L1568172-05 18 MW-2 L1568172-06 21 MW-6 L1568172-07 24 TRIPBLANK L1568172-08 27 Qc: Quality Control Summary 29 Mercury by Method 7470A 29 Metals (ICPMS) by Method 6020B 31 Volatile Organic Compounds (GC/MS) by Method 8260D 35 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 44 Gl: Glossary of Terms 61 Al: Accreditations & Locations 62 Sc: Sample Chain of Custody 63 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 2 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 2 of 63 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-1 L1568172-01 GW Tim Green 12/12/22 14:30 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975421 1 12/18/22 14:18 12/19/22 16:37 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977117 1 12/20/22 21:41 12/21/22 03:21 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977117 1 12/20/22 21:41 12/21/22 22:13 LD Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978139 1 12/22/22 06:52 12/22/22 06:52 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1974730 1 12/16/22 04:26 12/18/22 16:04 AO Mt. Juliet, TN Collected by Collected date/time Received date/time MW-5 L1568172-02 GW Tim Green 12/13/22 07:15 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975421 1 12/18/22 14:18 12/19/22 16:43 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:16 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 5 12/22/22 11:58 12/26/22 11:54 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978139 1 12/22/22 07:13 12/22/22 07:13 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975396 1 12/18/22 06:20 12/19/22 19:39 AMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW-4 L1568172-03 GW Tim Green 12/13/22 09:10 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975421 1 12/18/22 14:18 12/19/22 16:45 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:19 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 5 12/22/22 11:58 12/26/22 11:57 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 04:40 12/22/22 04:40 ADM Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975396 1 12/18/22 06:20 12/19/22 20:01 AMG Mt. Juliet, TN Collected by Collected date/time Received date/time MW-3 L1568172-04 GW Tim Green 12/13/22 11:05 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975421 1 12/18/22 14:18 12/19/22 16:47 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:23 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 5 12/22/22 11:58 12/26/22 12:00 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 05:02 12/22/22 05:02 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978665 100 12/22/22 21:37 12/22/22 21:37 JAH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975661 1 12/17/22 04:55 12/18/22 18:24 JNJ Mt. Juliet, TN Collected by Collected date/time Received date/time MW-3 DUPE L1568172-05 GW Tim Green 12/13/22 11:05 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975422 1 12/18/22 19:44 12/19/22 18:36 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:33 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/26/22 12:04 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 05:24 12/22/22 05:24 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978665 100 12/22/22 21:57 12/22/22 21:57 JAH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975661 1 12/17/22 04:55 12/18/22 18:45 AGW Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 3 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 3 of 63 SAMPLE SUMMARY Collected by Collected date/time Received date/time MW-2 L1568172-06 GW Tim Green 12/13/22 12:00 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975422 1 12/18/22 19:44 12/19/22 18:38 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:36 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/26/22 12:07 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 05:46 12/22/22 05:46 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978665 1 12/22/22 19:14 12/22/22 19:14 JAH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975661 1 12/17/22 04:55 12/18/22 19:06 AGW Mt. Juliet, TN Collected by Collected date/time Received date/time MW-6 L1568172-07 GW Tim Green 12/13/22 13:10 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Mercury by Method 7470A WG1975422 1 12/18/22 19:44 12/19/22 18:40 AKB Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 1 12/22/22 11:58 12/23/22 12:39 SJM Mt. Juliet, TN Metals (ICPMS) by Method 6020B WG1977121 5 12/22/22 11:58 12/26/22 12:10 SJM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 06:08 12/22/22 06:08 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1978665 1 12/22/22 19:34 12/22/22 19:34 JAH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1975661 1 12/17/22 04:55 12/18/22 19:27 AGW Mt. Juliet, TN Collected by Collected date/time Received date/time TRIPBLANK L1568172-08 GW Tim Green 12/13/22 00:00 12/15/22 09:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260D WG1978145 1 12/22/22 01:45 12/22/22 01:45 ADM Mt. Juliet, TN 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 4 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 4 of 63 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Heather J Wagner Project Manager Project Narrative Method 8270: WG1975661, WG1974730, WG1975396 Benzidine is reporting with critically low recovery in the laboratory control samples. Benzidine is a method defined poor performer. Results are estimated. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 5 of 63 Heather J Wagner Project Manager ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 5 of 63 SAMPLE RESULTS - 01 L1568172 MW-1 Collected date/time: 12/12/22 14:30 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury U 0.100 0.200 1 12/19/2022 16:37 WG1975421 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 0.656 B J 0.180 2.00 1 12/21/2022 03:21 WG1977117 Barium 94.7 0.381 2.00 1 12/21/2022 03:21 WG1977117 Cadmium U 0.150 1.00 1 12/21/2022 03:21 WG1977117 Chromium U 1.24 2.00 1 12/21/2022 22:13 WG1977117 Lead 2.58 0.849 2.00 1 12/21/2022 03:21 WG1977117 Selenium 1.74 B J 0.300 2.00 1 12/21/2022 22:13 WG1977117 Silver U 0.0700 2.00 1 12/21/2022 03:21 WG1977117 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 12/22/2022 06:52 WG1978139 Acrolein U C3 2.54 50.0 1 12/22/2022 06:52 WG1978139 Acrylonitrile U 0.671 10.0 1 12/22/2022 06:52 WG1978139 Benzene U 0.0941 1.00 1 12/22/2022 06:52 WG1978139 Bromobenzene U 0.118 1.00 1 12/22/2022 06:52 WG1978139 Bromodichloromethane U 0.136 1.00 1 12/22/2022 06:52 WG1978139 Bromoform U 0.129 1.00 1 12/22/2022 06:52 WG1978139 Bromomethane U 0.605 5.00 1 12/22/2022 06:52 WG1978139 n-Butylbenzene U 0.157 1.00 1 12/22/2022 06:52 WG1978139 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 06:52 WG1978139 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 06:52 WG1978139 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 06:52 WG1978139 Chlorobenzene U 0.116 1.00 1 12/22/2022 06:52 WG1978139 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 06:52 WG1978139 Chloroethane U 0.192 5.00 1 12/22/2022 06:52 WG1978139 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 06:52 WG1978139 Chloroform U 0.111 5.00 1 12/22/2022 06:52 WG1978139 Chloromethane U 0.960 2.50 1 12/22/2022 06:52 WG1978139 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 06:52 WG1978139 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 06:52 WG1978139 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 06:52 WG1978139 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 06:52 WG1978139 Dibromomethane U 0.122 1.00 1 12/22/2022 06:52 WG1978139 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 06:52 WG1978139 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 06:52 WG1978139 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 06:52 WG1978139 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 06:52 WG1978139 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 06:52 WG1978139 1,2-Dichloroethane U 0.0819 1.00 1 12/22/2022 06:52 WG1978139 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 06:52 WG1978139 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 06:52 WG1978139 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 06:52 WG1978139 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 06:52 WG1978139 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 06:52 WG1978139 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 06:52 WG1978139 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 06:52 WG1978139 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 06:52 WG1978139 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 06:52 WG1978139 Di-isopropyl ether U 0.105 1.00 1 12/22/2022 06:52 WG1978139 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 6 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 6 of 63 SAMPLE RESULTS - 01 L1568172 MW-1 Collected date/time: 12/12/22 14:30 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene U 0.137 1.00 1 12/22/2022 06:52 WG1978139 Hexachloro-1,3-butadiene U C3 0.337 1.00 1 12/22/2022 06:52 WG1978139 Isopropylbenzene U 0.105 1.00 1 12/22/2022 06:52 WG1978139 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 06:52 WG1978139 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 06:52 WG1978139 Methylene Chloride U 0.430 5.00 1 12/22/2022 06:52 WG1978139 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 06:52 WG1978139 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 06:52 WG1978139 Naphthalene U C3 1.00 5.00 1 12/22/2022 06:52 WG1978139 n-Propylbenzene U 0.0993 1.00 1 12/22/2022 06:52 WG1978139 Styrene U 0.118 1.00 1 12/22/2022 06:52 WG1978139 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 06:52 WG1978139 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 06:52 WG1978139 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 06:52 WG1978139 Tetrachloroethene U 0.300 1.00 1 12/22/2022 06:52 WG1978139 Toluene U 0.278 1.00 1 12/22/2022 06:52 WG1978139 1,2,3-Trichlorobenzene U 0.230 1.00 1 12/22/2022 06:52 WG1978139 1,2,4-Trichlorobenzene U C3 0.481 1.00 1 12/22/2022 06:52 WG1978139 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 06:52 WG1978139 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 06:52 WG1978139 Trichloroethene U 0.190 1.00 1 12/22/2022 06:52 WG1978139 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 06:52 WG1978139 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 06:52 WG1978139 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 06:52 WG1978139 1,2,3-Trimethylbenzene U 0.104 1.00 1 12/22/2022 06:52 WG1978139 1,3,5-Trimethylbenzene U 0.104 1.00 1 12/22/2022 06:52 WG1978139 Vinyl chloride U 0.234 1.00 1 12/22/2022 06:52 WG1978139 Xylenes, Total U 0.174 3.00 1 12/22/2022 06:52 WG1978139 (S) Toluene-d8 108 80.0-120 12/22/2022 06:52 WG1978139 (S) 4-Bromofluorobenzene 92.4 77.0-126 12/22/2022 06:52 WG1978139 (S) 1,2-Dichloroethane-d4 93.8 70.0-130 12/22/2022 06:52 WG1978139 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/18/2022 16:04 WG1974730 Acenaphthylene U 0.0921 1.00 1 12/18/2022 16:04 WG1974730 Anthracene U 0.0804 1.00 1 12/18/2022 16:04 WG1974730 Benzidine U J4 3.74 10.0 1 12/18/2022 16:04 WG1974730 Benzo(a)anthracene U 0.199 1.00 1 12/18/2022 16:04 WG1974730 Benzo(b)fluoranthene U 0.130 1.00 1 12/18/2022 16:04 WG1974730 Benzo(k)fluoranthene U 0.120 1.00 1 12/18/2022 16:04 WG1974730 Benzo(g,h,i)perylene U 0.121 1.00 1 12/18/2022 16:04 WG1974730 Benzo(a)pyrene U 0.0381 1.00 1 12/18/2022 16:04 WG1974730 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/18/2022 16:04 WG1974730 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/18/2022 16:04 WG1974730 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/18/2022 16:04 WG1974730 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/18/2022 16:04 WG1974730 2-Chloronaphthalene U 0.0648 1.00 1 12/18/2022 16:04 WG1974730 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/18/2022 16:04 WG1974730 Chrysene U 0.130 1.00 1 12/18/2022 16:04 WG1974730 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/18/2022 16:04 WG1974730 1,2-Dichlorobenzene U 0.0713 10.0 1 12/18/2022 16:04 WG1974730 1,3-Dichlorobenzene U 0.132 10.0 1 12/18/2022 16:04 WG1974730 1,4-Dichlorobenzene U 0.0942 10.0 1 12/18/2022 16:04 WG1974730 3,3-Dichlorobenzidine U 0.212 10.0 1 12/18/2022 16:04 WG1974730 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 7 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 7 of 63 SAMPLE RESULTS - 01 L1568172 MW-1 Collected date/time: 12/12/22 14:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 2,4-Dinitrotoluene U 0.0983 10.0 1 12/18/2022 16:04 WG1974730 2,6-Dinitrotoluene U 0.250 10.0 1 12/18/2022 16:04 WG1974730 Fluoranthene U 0.102 1.00 1 12/18/2022 16:04 WG1974730 Fluorene U 0.0844 1.00 1 12/18/2022 16:04 WG1974730 Hexachlorobenzene U 0.0755 1.00 1 12/18/2022 16:04 WG1974730 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/18/2022 16:04 WG1974730 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/18/2022 16:04 WG1974730 Hexachloroethane U 0.127 10.0 1 12/18/2022 16:04 WG1974730 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/18/2022 16:04 WG1974730 Isophorone U 0.143 10.0 1 12/18/2022 16:04 WG1974730 Naphthalene 0.373 J 0.159 1.00 1 12/18/2022 16:04 WG1974730 Nitrobenzene U 0.297 10.0 1 12/18/2022 16:04 WG1974730 n-Nitrosodimethylamine U 0.998 10.0 1 12/18/2022 16:04 WG1974730 n-Nitrosodiphenylamine U 2.37 10.0 1 12/18/2022 16:04 WG1974730 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/18/2022 16:04 WG1974730 Phenanthrene U 0.112 1.00 1 12/18/2022 16:04 WG1974730 Benzylbutyl phthalate U 0.765 3.00 1 12/18/2022 16:04 WG1974730 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/18/2022 16:04 WG1974730 Di-n-butyl phthalate U 0.453 3.00 1 12/18/2022 16:04 WG1974730 Diethyl phthalate U 0.287 3.00 1 12/18/2022 16:04 WG1974730 Dimethyl phthalate U 0.260 3.00 1 12/18/2022 16:04 WG1974730 Di-n-octyl phthalate U 0.932 3.00 1 12/18/2022 16:04 WG1974730 Pyrene U 0.107 1.00 1 12/18/2022 16:04 WG1974730 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/18/2022 16:04 WG1974730 4-Chloro-3-methylphenol U 0.131 10.0 1 12/18/2022 16:04 WG1974730 2-Chlorophenol U 0.133 10.0 1 12/18/2022 16:04 WG1974730 2,4-Dichlorophenol U 0.102 10.0 1 12/18/2022 16:04 WG1974730 2,4-Dimethylphenol U 0.0636 10.0 1 12/18/2022 16:04 WG1974730 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/18/2022 16:04 WG1974730 2,4-Dinitrophenol U 5.93 10.0 1 12/18/2022 16:04 WG1974730 2-Nitrophenol U 0.117 10.0 1 12/18/2022 16:04 WG1974730 4-Nitrophenol U J4 0.143 10.0 1 12/18/2022 16:04 WG1974730 Pentachlorophenol U 0.313 10.0 1 12/18/2022 16:04 WG1974730 Phenol U 4.33 10.0 1 12/18/2022 16:04 WG1974730 2,4,6-Trichlorophenol U 0.100 10.0 1 12/18/2022 16:04 WG1974730 (S) 2-Fluorophenol 19.2 10.0-120 12/18/2022 16:04 WG1974730 (S) Phenol-d5 14.8 10.0-120 12/18/2022 16:04 WG1974730 (S) Nitrobenzene-d5 64.2 10.0-127 12/18/2022 16:04 WG1974730 (S) 2-Fluorobiphenyl 50.8 10.0-130 12/18/2022 16:04 WG1974730 (S) 2,4,6-Tribromophenol 22.1 10.0-155 12/18/2022 16:04 WG1974730 (S) p-Terphenyl-d14 37.6 10.0-128 12/18/2022 16:04 WG1974730 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 8 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 8 of 63 SAMPLE RESULTS - 02 L1568172 MW-5 Collected date/time: 12/13/22 07:15 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury U 0.100 0.200 1 12/19/2022 16:43 WG1975421 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 12.1 0.900 10.0 5 12/26/2022 11:54 WG1977121 Barium 746 1.90 10.0 5 12/26/2022 11:54 WG1977121 Cadmium 0.272 J 0.150 1.00 1 12/23/2022 12:16 WG1977121 Chromium 7.57 J 6.20 10.0 5 12/26/2022 11:54 WG1977121 Lead 65.3 0.849 2.00 1 12/23/2022 12:16 WG1977121 Selenium 7.71 0.300 2.00 1 12/23/2022 12:16 WG1977121 Silver U 0.0700 2.00 1 12/23/2022 12:16 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U 11.3 50.0 1 12/22/2022 07:13 WG1978139 Acrolein U C3 2.54 50.0 1 12/22/2022 07:13 WG1978139 Acrylonitrile U 0.671 10.0 1 12/22/2022 07:13 WG1978139 Benzene U 0.0941 1.00 1 12/22/2022 07:13 WG1978139 Bromobenzene U 0.118 1.00 1 12/22/2022 07:13 WG1978139 Bromodichloromethane U 0.136 1.00 1 12/22/2022 07:13 WG1978139 Bromoform U 0.129 1.00 1 12/22/2022 07:13 WG1978139 Bromomethane U 0.605 5.00 1 12/22/2022 07:13 WG1978139 n-Butylbenzene U 0.157 1.00 1 12/22/2022 07:13 WG1978139 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 07:13 WG1978139 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 07:13 WG1978139 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 07:13 WG1978139 Chlorobenzene U 0.116 1.00 1 12/22/2022 07:13 WG1978139 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 07:13 WG1978139 Chloroethane U 0.192 5.00 1 12/22/2022 07:13 WG1978139 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 07:13 WG1978139 Chloroform U 0.111 5.00 1 12/22/2022 07:13 WG1978139 Chloromethane U 0.960 2.50 1 12/22/2022 07:13 WG1978139 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 07:13 WG1978139 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 07:13 WG1978139 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 07:13 WG1978139 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 07:13 WG1978139 Dibromomethane U 0.122 1.00 1 12/22/2022 07:13 WG1978139 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 07:13 WG1978139 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 07:13 WG1978139 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 07:13 WG1978139 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 07:13 WG1978139 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 07:13 WG1978139 1,2-Dichloroethane U 0.0819 1.00 1 12/22/2022 07:13 WG1978139 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 07:13 WG1978139 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 07:13 WG1978139 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 07:13 WG1978139 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 07:13 WG1978139 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 07:13 WG1978139 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 07:13 WG1978139 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 07:13 WG1978139 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 07:13 WG1978139 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 07:13 WG1978139 Di-isopropyl ether U 0.105 1.00 1 12/22/2022 07:13 WG1978139 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 9 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 9 of 63 SAMPLE RESULTS - 02 L1568172 MW-5 Collected date/time: 12/13/22 07:15 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene U 0.137 1.00 1 12/22/2022 07:13 WG1978139 Hexachloro-1,3-butadiene U C3 0.337 1.00 1 12/22/2022 07:13 WG1978139 Isopropylbenzene U 0.105 1.00 1 12/22/2022 07:13 WG1978139 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 07:13 WG1978139 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 07:13 WG1978139 Methylene Chloride U 0.430 5.00 1 12/22/2022 07:13 WG1978139 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 07:13 WG1978139 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 07:13 WG1978139 Naphthalene U C3 1.00 5.00 1 12/22/2022 07:13 WG1978139 n-Propylbenzene U 0.0993 1.00 1 12/22/2022 07:13 WG1978139 Styrene U 0.118 1.00 1 12/22/2022 07:13 WG1978139 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 07:13 WG1978139 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 07:13 WG1978139 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 07:13 WG1978139 Tetrachloroethene U 0.300 1.00 1 12/22/2022 07:13 WG1978139 Toluene U 0.278 1.00 1 12/22/2022 07:13 WG1978139 1,2,3-Trichlorobenzene U 0.230 1.00 1 12/22/2022 07:13 WG1978139 1,2,4-Trichlorobenzene U C3 0.481 1.00 1 12/22/2022 07:13 WG1978139 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 07:13 WG1978139 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 07:13 WG1978139 Trichloroethene U 0.190 1.00 1 12/22/2022 07:13 WG1978139 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 07:13 WG1978139 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 07:13 WG1978139 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 07:13 WG1978139 1,2,3-Trimethylbenzene U 0.104 1.00 1 12/22/2022 07:13 WG1978139 1,3,5-Trimethylbenzene U 0.104 1.00 1 12/22/2022 07:13 WG1978139 Vinyl chloride U 0.234 1.00 1 12/22/2022 07:13 WG1978139 Xylenes, Total U 0.174 3.00 1 12/22/2022 07:13 WG1978139 (S) Toluene-d8 106 80.0-120 12/22/2022 07:13 WG1978139 (S) 4-Bromofluorobenzene 92.8 77.0-126 12/22/2022 07:13 WG1978139 (S) 1,2-Dichloroethane-d4 90.8 70.0-130 12/22/2022 07:13 WG1978139 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/19/2022 19:39 WG1975396 Acenaphthylene U 0.0921 1.00 1 12/19/2022 19:39 WG1975396 Anthracene U 0.0804 1.00 1 12/19/2022 19:39 WG1975396 Benzidine U J4 3.74 10.0 1 12/19/2022 19:39 WG1975396 Benzo(a)anthracene U 0.199 1.00 1 12/19/2022 19:39 WG1975396 Benzo(b)fluoranthene U 0.130 1.00 1 12/19/2022 19:39 WG1975396 Benzo(k)fluoranthene U 0.120 1.00 1 12/19/2022 19:39 WG1975396 Benzo(g,h,i)perylene U 0.121 1.00 1 12/19/2022 19:39 WG1975396 Benzo(a)pyrene U 0.0381 1.00 1 12/19/2022 19:39 WG1975396 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/19/2022 19:39 WG1975396 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/19/2022 19:39 WG1975396 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/19/2022 19:39 WG1975396 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/19/2022 19:39 WG1975396 2-Chloronaphthalene U 0.0648 1.00 1 12/19/2022 19:39 WG1975396 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/19/2022 19:39 WG1975396 Chrysene U 0.130 1.00 1 12/19/2022 19:39 WG1975396 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/19/2022 19:39 WG1975396 1,2-Dichlorobenzene U 0.0713 10.0 1 12/19/2022 19:39 WG1975396 1,3-Dichlorobenzene U 0.132 10.0 1 12/19/2022 19:39 WG1975396 1,4-Dichlorobenzene U 0.0942 10.0 1 12/19/2022 19:39 WG1975396 3,3-Dichlorobenzidine U 0.212 10.0 1 12/19/2022 19:39 WG1975396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 10 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 10 of 63 SAMPLE RESULTS - 02 L1568172 MW-5 Collected date/time: 12/13/22 07:15 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 2,4-Dinitrotoluene U 0.0983 10.0 1 12/19/2022 19:39 WG1975396 2,6-Dinitrotoluene U 0.250 10.0 1 12/19/2022 19:39 WG1975396 Fluoranthene U 0.102 1.00 1 12/19/2022 19:39 WG1975396 Fluorene U 0.0844 1.00 1 12/19/2022 19:39 WG1975396 Hexachlorobenzene U 0.0755 1.00 1 12/19/2022 19:39 WG1975396 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/19/2022 19:39 WG1975396 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/19/2022 19:39 WG1975396 Hexachloroethane U 0.127 10.0 1 12/19/2022 19:39 WG1975396 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/19/2022 19:39 WG1975396 Isophorone U 0.143 10.0 1 12/19/2022 19:39 WG1975396 Naphthalene U 0.159 1.00 1 12/19/2022 19:39 WG1975396 Nitrobenzene U 0.297 10.0 1 12/19/2022 19:39 WG1975396 n-Nitrosodimethylamine U 0.998 10.0 1 12/19/2022 19:39 WG1975396 n-Nitrosodiphenylamine U J4 2.37 10.0 1 12/19/2022 19:39 WG1975396 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/19/2022 19:39 WG1975396 Phenanthrene U 0.112 1.00 1 12/19/2022 19:39 WG1975396 Benzylbutyl phthalate U 0.765 3.00 1 12/19/2022 19:39 WG1975396 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/19/2022 19:39 WG1975396 Di-n-butyl phthalate U 0.453 3.00 1 12/19/2022 19:39 WG1975396 Diethyl phthalate U 0.287 3.00 1 12/19/2022 19:39 WG1975396 Dimethyl phthalate U 0.260 3.00 1 12/19/2022 19:39 WG1975396 Di-n-octyl phthalate U 0.932 3.00 1 12/19/2022 19:39 WG1975396 Pyrene U 0.107 1.00 1 12/19/2022 19:39 WG1975396 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/19/2022 19:39 WG1975396 4-Chloro-3-methylphenol U 0.131 10.0 1 12/19/2022 19:39 WG1975396 2-Chlorophenol U 0.133 10.0 1 12/19/2022 19:39 WG1975396 2,4-Dichlorophenol U 0.102 10.0 1 12/19/2022 19:39 WG1975396 2,4-Dimethylphenol U 0.0636 10.0 1 12/19/2022 19:39 WG1975396 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/19/2022 19:39 WG1975396 2,4-Dinitrophenol U 5.93 10.0 1 12/19/2022 19:39 WG1975396 2-Nitrophenol U 0.117 10.0 1 12/19/2022 19:39 WG1975396 4-Nitrophenol U 0.143 10.0 1 12/19/2022 19:39 WG1975396 Pentachlorophenol U 0.313 10.0 1 12/19/2022 19:39 WG1975396 Phenol U 4.33 10.0 1 12/19/2022 19:39 WG1975396 2,4,6-Trichlorophenol U 0.100 10.0 1 12/19/2022 19:39 WG1975396 (S) 2-Fluorophenol 17.0 10.0-120 12/19/2022 19:39 WG1975396 (S) Phenol-d5 12.1 10.0-120 12/19/2022 19:39 WG1975396 (S) Nitrobenzene-d5 48.6 10.0-127 12/19/2022 19:39 WG1975396 (S) 2-Fluorobiphenyl 44.8 10.0-130 12/19/2022 19:39 WG1975396 (S) 2,4,6-Tribromophenol 54.6 10.0-155 12/19/2022 19:39 WG1975396 (S) p-Terphenyl-d14 60.1 10.0-128 12/19/2022 19:39 WG1975396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 11 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 11 of 63 SAMPLE RESULTS - 03 L1568172 MW-4 Collected date/time: 12/13/22 09:10 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury U 0.100 0.200 1 12/19/2022 16:45 WG1975421 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 14.1 0.900 10.0 5 12/26/2022 11:57 WG1977121 Barium 854 1.90 10.0 5 12/26/2022 11:57 WG1977121 Cadmium 0.427 J 0.150 1.00 1 12/23/2022 12:19 WG1977121 Chromium 18.8 6.20 10.0 5 12/26/2022 11:57 WG1977121 Lead 91.8 0.849 2.00 1 12/23/2022 12:19 WG1977121 Selenium 7.71 0.300 2.00 1 12/23/2022 12:19 WG1977121 Silver 0.116 J 0.0700 2.00 1 12/23/2022 12:19 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U J3 11.3 50.0 1 12/22/2022 04:40 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 04:40 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 04:40 WG1978145 Benzene U 0.0941 1.00 1 12/22/2022 04:40 WG1978145 Bromobenzene U 0.118 1.00 1 12/22/2022 04:40 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 04:40 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 04:40 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 04:40 WG1978145 n-Butylbenzene U 0.157 1.00 1 12/22/2022 04:40 WG1978145 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 04:40 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 04:40 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 04:40 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 04:40 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 04:40 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 04:40 WG1978145 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 04:40 WG1978145 Chloroform U 0.111 5.00 1 12/22/2022 04:40 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 04:40 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 04:40 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 04:40 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 04:40 WG1978145 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 04:40 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 04:40 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 04:40 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 04:40 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 04:40 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 04:40 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 04:40 WG1978145 1,2-Dichloroethane U 0.0819 1.00 1 12/22/2022 04:40 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 04:40 WG1978145 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 04:40 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 04:40 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 04:40 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 04:40 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 04:40 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 04:40 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 04:40 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 04:40 WG1978145 Di-isopropyl ether U 0.105 1.00 1 12/22/2022 04:40 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 12 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 12 of 63 SAMPLE RESULTS - 03 L1568172 MW-4 Collected date/time: 12/13/22 09:10 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene U 0.137 1.00 1 12/22/2022 04:40 WG1978145 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 04:40 WG1978145 Isopropylbenzene U 0.105 1.00 1 12/22/2022 04:40 WG1978145 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 04:40 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 04:40 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 04:40 WG1978145 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 04:40 WG1978145 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 04:40 WG1978145 Naphthalene U J3 1.00 5.00 1 12/22/2022 04:40 WG1978145 n-Propylbenzene U 0.0993 1.00 1 12/22/2022 04:40 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 04:40 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 04:40 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 04:40 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 04:40 WG1978145 Tetrachloroethene U 0.300 1.00 1 12/22/2022 04:40 WG1978145 Toluene U 0.278 1.00 1 12/22/2022 04:40 WG1978145 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 04:40 WG1978145 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 04:40 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 04:40 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 04:40 WG1978145 Trichloroethene U 0.190 1.00 1 12/22/2022 04:40 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 04:40 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 04:40 WG1978145 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 04:40 WG1978145 1,2,3-Trimethylbenzene U 0.104 1.00 1 12/22/2022 04:40 WG1978145 1,3,5-Trimethylbenzene U 0.104 1.00 1 12/22/2022 04:40 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 04:40 WG1978145 Xylenes, Total U 0.174 3.00 1 12/22/2022 04:40 WG1978145 (S) Toluene-d8 99.6 80.0-120 12/22/2022 04:40 WG1978145 (S) 4-Bromofluorobenzene 94.6 77.0-126 12/22/2022 04:40 WG1978145 (S) 1,2-Dichloroethane-d4 113 70.0-130 12/22/2022 04:40 WG1978145 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/19/2022 20:01 WG1975396 Acenaphthylene U 0.0921 1.00 1 12/19/2022 20:01 WG1975396 Anthracene U 0.0804 1.00 1 12/19/2022 20:01 WG1975396 Benzidine U J4 3.74 10.0 1 12/19/2022 20:01 WG1975396 Benzo(a)anthracene U 0.199 1.00 1 12/19/2022 20:01 WG1975396 Benzo(b)fluoranthene U 0.130 1.00 1 12/19/2022 20:01 WG1975396 Benzo(k)fluoranthene U 0.120 1.00 1 12/19/2022 20:01 WG1975396 Benzo(g,h,i)perylene U 0.121 1.00 1 12/19/2022 20:01 WG1975396 Benzo(a)pyrene U 0.0381 1.00 1 12/19/2022 20:01 WG1975396 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/19/2022 20:01 WG1975396 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/19/2022 20:01 WG1975396 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/19/2022 20:01 WG1975396 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/19/2022 20:01 WG1975396 2-Chloronaphthalene U 0.0648 1.00 1 12/19/2022 20:01 WG1975396 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/19/2022 20:01 WG1975396 Chrysene U 0.130 1.00 1 12/19/2022 20:01 WG1975396 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/19/2022 20:01 WG1975396 1,2-Dichlorobenzene U 0.0713 10.0 1 12/19/2022 20:01 WG1975396 1,3-Dichlorobenzene U 0.132 10.0 1 12/19/2022 20:01 WG1975396 1,4-Dichlorobenzene U 0.0942 10.0 1 12/19/2022 20:01 WG1975396 3,3-Dichlorobenzidine U 0.212 10.0 1 12/19/2022 20:01 WG1975396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 13 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 13 of 63 SAMPLE RESULTS - 03 L1568172 MW-4 Collected date/time: 12/13/22 09:10 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 2,4-Dinitrotoluene U 0.0983 10.0 1 12/19/2022 20:01 WG1975396 2,6-Dinitrotoluene U 0.250 10.0 1 12/19/2022 20:01 WG1975396 Fluoranthene U 0.102 1.00 1 12/19/2022 20:01 WG1975396 Fluorene U 0.0844 1.00 1 12/19/2022 20:01 WG1975396 Hexachlorobenzene U 0.0755 1.00 1 12/19/2022 20:01 WG1975396 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/19/2022 20:01 WG1975396 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/19/2022 20:01 WG1975396 Hexachloroethane U 0.127 10.0 1 12/19/2022 20:01 WG1975396 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/19/2022 20:01 WG1975396 Isophorone U 0.143 10.0 1 12/19/2022 20:01 WG1975396 Naphthalene U 0.159 1.00 1 12/19/2022 20:01 WG1975396 Nitrobenzene U 0.297 10.0 1 12/19/2022 20:01 WG1975396 n-Nitrosodimethylamine U 0.998 10.0 1 12/19/2022 20:01 WG1975396 n-Nitrosodiphenylamine U J4 2.37 10.0 1 12/19/2022 20:01 WG1975396 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/19/2022 20:01 WG1975396 Phenanthrene U 0.112 1.00 1 12/19/2022 20:01 WG1975396 Benzylbutyl phthalate U 0.765 3.00 1 12/19/2022 20:01 WG1975396 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/19/2022 20:01 WG1975396 Di-n-butyl phthalate U 0.453 3.00 1 12/19/2022 20:01 WG1975396 Diethyl phthalate U 0.287 3.00 1 12/19/2022 20:01 WG1975396 Dimethyl phthalate U 0.260 3.00 1 12/19/2022 20:01 WG1975396 Di-n-octyl phthalate U 0.932 3.00 1 12/19/2022 20:01 WG1975396 Pyrene U 0.107 1.00 1 12/19/2022 20:01 WG1975396 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/19/2022 20:01 WG1975396 4-Chloro-3-methylphenol U 0.131 10.0 1 12/19/2022 20:01 WG1975396 2-Chlorophenol U 0.133 10.0 1 12/19/2022 20:01 WG1975396 2,4-Dichlorophenol U 0.102 10.0 1 12/19/2022 20:01 WG1975396 2,4-Dimethylphenol U 0.0636 10.0 1 12/19/2022 20:01 WG1975396 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/19/2022 20:01 WG1975396 2,4-Dinitrophenol U 5.93 10.0 1 12/19/2022 20:01 WG1975396 2-Nitrophenol U 0.117 10.0 1 12/19/2022 20:01 WG1975396 4-Nitrophenol U 0.143 10.0 1 12/19/2022 20:01 WG1975396 Pentachlorophenol U 0.313 10.0 1 12/19/2022 20:01 WG1975396 Phenol U 4.33 10.0 1 12/19/2022 20:01 WG1975396 2,4,6-Trichlorophenol U 0.100 10.0 1 12/19/2022 20:01 WG1975396 (S) 2-Fluorophenol 14.5 10.0-120 12/19/2022 20:01 WG1975396 (S) Phenol-d5 10.6 10.0-120 12/19/2022 20:01 WG1975396 (S) Nitrobenzene-d5 43.4 10.0-127 12/19/2022 20:01 WG1975396 (S) 2-Fluorobiphenyl 36.0 10.0-130 12/19/2022 20:01 WG1975396 (S) 2,4,6-Tribromophenol 29.1 10.0-155 12/19/2022 20:01 WG1975396 (S) p-Terphenyl-d14 41.4 10.0-128 12/19/2022 20:01 WG1975396 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 14 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 14 of 63 SAMPLE RESULTS - 04 L1568172 MW-3 Collected date/time: 12/13/22 11:05 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury 1.67 0.100 0.200 1 12/19/2022 16:47 WG1975421 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 22.8 0.180 2.00 1 12/23/2022 12:23 WG1977121 Barium 420 1.90 10.0 5 12/26/2022 12:00 WG1977121 Cadmium 0.271 J 0.150 1.00 1 12/23/2022 12:23 WG1977121 Chromium 19.3 6.20 10.0 5 12/26/2022 12:00 WG1977121 Lead 239 0.849 2.00 1 12/23/2022 12:23 WG1977121 Selenium 3.32 0.300 2.00 1 12/23/2022 12:23 WG1977121 Silver 0.109 J 0.0700 2.00 1 12/23/2022 12:23 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone 15.8 J J3 11.3 50.0 1 12/22/2022 05:02 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 05:02 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 05:02 WG1978145 Benzene 772 9.41 100 100 12/22/2022 21:37 WG1978665 Bromobenzene U 0.118 1.00 1 12/22/2022 05:02 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 05:02 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 05:02 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 05:02 WG1978145 n-Butylbenzene 2.48 0.157 1.00 1 12/22/2022 05:02 WG1978145 sec-Butylbenzene 2.31 0.125 1.00 1 12/22/2022 05:02 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 05:02 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 05:02 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 05:02 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 05:02 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 05:02 WG1978145 2-Chloroethyl vinyl ether 0.667 J 0.575 50.0 1 12/22/2022 05:02 WG1978145 Chloroform U 0.111 5.00 1 12/22/2022 05:02 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 05:02 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 05:02 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 05:02 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 05:02 WG1978145 1,2-Dibromoethane 29.4 0.126 1.00 1 12/22/2022 05:02 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 05:02 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 05:02 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 05:02 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 05:02 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 05:02 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 05:02 WG1978145 1,2-Dichloroethane 97.1 0.0819 1.00 1 12/22/2022 05:02 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 05:02 WG1978145 cis-1,2-Dichloroethene 0.186 J 0.126 1.00 1 12/22/2022 05:02 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 05:02 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 05:02 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 05:02 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 05:02 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 05:02 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 05:02 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 05:02 WG1978145 Di-isopropyl ether 15.5 0.105 1.00 1 12/22/2022 05:02 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 15 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 15 of 63 SAMPLE RESULTS - 04 L1568172 MW-3 Collected date/time: 12/13/22 11:05 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene 304 13.7 100 100 12/22/2022 21:37 WG1978665 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 05:02 WG1978145 Isopropylbenzene 15.7 0.105 1.00 1 12/22/2022 05:02 WG1978145 p-Isopropyltoluene 1.15 0.120 1.00 1 12/22/2022 05:02 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 05:02 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 05:02 WG1978145 4-Methyl-2-pentanone (MIBK)8.15 J 0.478 10.0 1 12/22/2022 05:02 WG1978145 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 05:02 WG1978145 Naphthalene 40.7 J3 1.00 5.00 1 12/22/2022 05:02 WG1978145 n-Propylbenzene 34.5 0.0993 1.00 1 12/22/2022 05:02 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 05:02 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 05:02 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 05:02 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 05:02 WG1978145 Tetrachloroethene 20.6 0.300 1.00 1 12/22/2022 05:02 WG1978145 Toluene 2330 27.8 100 100 12/22/2022 21:37 WG1978665 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 05:02 WG1978145 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 05:02 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 05:02 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 05:02 WG1978145 Trichloroethene U 0.190 1.00 1 12/22/2022 05:02 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 05:02 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 05:02 WG1978145 1,2,4-Trimethylbenzene 224 32.2 100 100 12/22/2022 21:37 WG1978665 1,2,3-Trimethylbenzene 91.9 0.104 1.00 1 12/22/2022 05:02 WG1978145 1,3,5-Trimethylbenzene 74.3 0.104 1.00 1 12/22/2022 05:02 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 05:02 WG1978145 Xylenes, Total 1110 17.4 300 100 12/22/2022 21:37 WG1978665 (S) Toluene-d8 93.4 80.0-120 12/22/2022 05:02 WG1978145 (S) Toluene-d8 95.3 80.0-120 12/22/2022 21:37 WG1978665 (S) 4-Bromofluorobenzene 83.3 77.0-126 12/22/2022 05:02 WG1978145 (S) 4-Bromofluorobenzene 92.3 77.0-126 12/22/2022 21:37 WG1978665 (S) 1,2-Dichloroethane-d4 97.9 70.0-130 12/22/2022 05:02 WG1978145 (S) 1,2-Dichloroethane-d4 79.2 70.0-130 12/22/2022 21:37 WG1978665 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/18/2022 18:24 WG1975661 Acenaphthylene U 0.0921 1.00 1 12/18/2022 18:24 WG1975661 Anthracene U 0.0804 1.00 1 12/18/2022 18:24 WG1975661 Benzidine U J4 3.74 10.0 1 12/18/2022 18:24 WG1975661 Benzo(a)anthracene U 0.199 1.00 1 12/18/2022 18:24 WG1975661 Benzo(b)fluoranthene U 0.130 1.00 1 12/18/2022 18:24 WG1975661 Benzo(k)fluoranthene U 0.120 1.00 1 12/18/2022 18:24 WG1975661 Benzo(g,h,i)perylene U 0.121 1.00 1 12/18/2022 18:24 WG1975661 Benzo(a)pyrene U 0.0381 1.00 1 12/18/2022 18:24 WG1975661 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/18/2022 18:24 WG1975661 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/18/2022 18:24 WG1975661 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/18/2022 18:24 WG1975661 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/18/2022 18:24 WG1975661 2-Chloronaphthalene U 0.0648 1.00 1 12/18/2022 18:24 WG1975661 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/18/2022 18:24 WG1975661 Chrysene U 0.130 1.00 1 12/18/2022 18:24 WG1975661 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/18/2022 18:24 WG1975661 1,2-Dichlorobenzene U 0.0713 10.0 1 12/18/2022 18:24 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 16 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 16 of 63 SAMPLE RESULTS - 04 L1568172 MW-3 Collected date/time: 12/13/22 11:05 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,3-Dichlorobenzene U 0.132 10.0 1 12/18/2022 18:24 WG1975661 1,4-Dichlorobenzene U 0.0942 10.0 1 12/18/2022 18:24 WG1975661 3,3-Dichlorobenzidine U 0.212 10.0 1 12/18/2022 18:24 WG1975661 2,4-Dinitrotoluene U 0.0983 10.0 1 12/18/2022 18:24 WG1975661 2,6-Dinitrotoluene U 0.250 10.0 1 12/18/2022 18:24 WG1975661 Fluoranthene U 0.102 1.00 1 12/18/2022 18:24 WG1975661 Fluorene U 0.0844 1.00 1 12/18/2022 18:24 WG1975661 Hexachlorobenzene U 0.0755 1.00 1 12/18/2022 18:24 WG1975661 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/18/2022 18:24 WG1975661 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/18/2022 18:24 WG1975661 Hexachloroethane U 0.127 10.0 1 12/18/2022 18:24 WG1975661 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/18/2022 18:24 WG1975661 Isophorone U 0.143 10.0 1 12/18/2022 18:24 WG1975661 Naphthalene 11.9 0.159 1.00 1 12/18/2022 18:24 WG1975661 Nitrobenzene U 0.297 10.0 1 12/18/2022 18:24 WG1975661 n-Nitrosodimethylamine U 0.998 10.0 1 12/18/2022 18:24 WG1975661 n-Nitrosodiphenylamine U 2.37 10.0 1 12/18/2022 18:24 WG1975661 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/18/2022 18:24 WG1975661 Phenanthrene 0.117 J 0.112 1.00 1 12/18/2022 18:24 WG1975661 Benzylbutyl phthalate U 0.765 3.00 1 12/18/2022 18:24 WG1975661 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/18/2022 18:24 WG1975661 Di-n-butyl phthalate U 0.453 3.00 1 12/18/2022 18:24 WG1975661 Diethyl phthalate U 0.287 3.00 1 12/18/2022 18:24 WG1975661 Dimethyl phthalate U 0.260 3.00 1 12/18/2022 18:24 WG1975661 Di-n-octyl phthalate U 0.932 3.00 1 12/18/2022 18:24 WG1975661 Pyrene U 0.107 1.00 1 12/18/2022 18:24 WG1975661 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/18/2022 18:24 WG1975661 4-Chloro-3-methylphenol U 0.131 10.0 1 12/18/2022 18:24 WG1975661 2-Chlorophenol U 0.133 10.0 1 12/18/2022 18:24 WG1975661 2,4-Dichlorophenol U 0.102 10.0 1 12/18/2022 18:24 WG1975661 2,4-Dimethylphenol 0.881 J 0.0636 10.0 1 12/18/2022 18:24 WG1975661 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/18/2022 18:24 WG1975661 2,4-Dinitrophenol U 5.93 10.0 1 12/18/2022 18:24 WG1975661 2-Nitrophenol U 0.117 10.0 1 12/18/2022 18:24 WG1975661 4-Nitrophenol U 0.143 10.0 1 12/18/2022 18:24 WG1975661 Pentachlorophenol U 0.313 10.0 1 12/18/2022 18:24 WG1975661 Phenol U 4.33 10.0 1 12/18/2022 18:24 WG1975661 2,4,6-Trichlorophenol U 0.100 10.0 1 12/18/2022 18:24 WG1975661 (S) 2-Fluorophenol 21.0 10.0-120 12/18/2022 18:24 WG1975661 (S) Phenol-d5 15.6 10.0-120 12/18/2022 18:24 WG1975661 (S) Nitrobenzene-d5 65.8 10.0-127 12/18/2022 18:24 WG1975661 (S) 2-Fluorobiphenyl 64.9 10.0-130 12/18/2022 18:24 WG1975661 (S) 2,4,6-Tribromophenol 62.6 10.0-155 12/18/2022 18:24 WG1975661 (S) p-Terphenyl-d14 73.1 10.0-128 12/18/2022 18:24 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 17 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 17 of 63 SAMPLE RESULTS - 05 L1568172 MW-3 DUPE Collected date/time: 12/13/22 11:05 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury 0.860 0.100 0.200 1 12/19/2022 18:36 WG1975422 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 13.7 0.180 2.00 1 12/23/2022 12:33 WG1977121 Barium 201 0.381 2.00 1 12/23/2022 12:33 WG1977121 Cadmium 0.211 J 0.150 1.00 1 12/23/2022 12:33 WG1977121 Chromium 12.6 1.24 2.00 1 12/26/2022 12:04 WG1977121 Lead 119 0.849 2.00 1 12/23/2022 12:33 WG1977121 Selenium 1.66 J 0.300 2.00 1 12/23/2022 12:33 WG1977121 Silver 0.0957 J 0.0700 2.00 1 12/23/2022 12:33 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U J3 11.3 50.0 1 12/22/2022 05:24 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 05:24 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 05:24 WG1978145 Benzene 1300 9.41 100 100 12/22/2022 21:57 WG1978665 Bromobenzene U 0.118 1.00 1 12/22/2022 05:24 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 05:24 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 05:24 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 05:24 WG1978145 n-Butylbenzene 2.26 0.157 1.00 1 12/22/2022 05:24 WG1978145 sec-Butylbenzene 2.07 0.125 1.00 1 12/22/2022 05:24 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 05:24 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 05:24 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 05:24 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 05:24 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 05:24 WG1978145 2-Chloroethyl vinyl ether 0.894 J 0.575 50.0 1 12/22/2022 05:24 WG1978145 Chloroform U 0.111 5.00 1 12/22/2022 05:24 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 05:24 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 05:24 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 05:24 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 05:24 WG1978145 1,2-Dibromoethane 28.4 0.126 1.00 1 12/22/2022 05:24 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 05:24 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 05:24 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 05:24 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 05:24 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 05:24 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 05:24 WG1978145 1,2-Dichloroethane 88.4 0.0819 1.00 1 12/22/2022 05:24 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 05:24 WG1978145 cis-1,2-Dichloroethene 0.240 J 0.126 1.00 1 12/22/2022 05:24 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 05:24 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 05:24 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 05:24 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 05:24 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 05:24 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 05:24 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 05:24 WG1978145 Di-isopropyl ether 14.4 0.105 1.00 1 12/22/2022 05:24 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 18 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 18 of 63 SAMPLE RESULTS - 05 L1568172 MW-3 DUPE Collected date/time: 12/13/22 11:05 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene 297 13.7 100 100 12/22/2022 21:57 WG1978665 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 05:24 WG1978145 Isopropylbenzene 14.4 0.105 1.00 1 12/22/2022 05:24 WG1978145 p-Isopropyltoluene 0.995 J 0.120 1.00 1 12/22/2022 05:24 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 05:24 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 05:24 WG1978145 4-Methyl-2-pentanone (MIBK)7.68 J 0.478 10.0 1 12/22/2022 05:24 WG1978145 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 05:24 WG1978145 Naphthalene 39.8 J3 1.00 5.00 1 12/22/2022 05:24 WG1978145 n-Propylbenzene 30.4 0.0993 1.00 1 12/22/2022 05:24 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 05:24 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 05:24 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 05:24 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 05:24 WG1978145 Tetrachloroethene 21.8 0.300 1.00 1 12/22/2022 05:24 WG1978145 Toluene 2160 27.8 100 100 12/22/2022 21:57 WG1978665 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 05:24 WG1978145 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 05:24 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 05:24 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 05:24 WG1978145 Trichloroethene U 0.190 1.00 1 12/22/2022 05:24 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 05:24 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 05:24 WG1978145 1,2,4-Trimethylbenzene 215 32.2 100 100 12/22/2022 21:57 WG1978665 1,2,3-Trimethylbenzene 81.6 0.104 1.00 1 12/22/2022 05:24 WG1978145 1,3,5-Trimethylbenzene 65.2 0.104 1.00 1 12/22/2022 05:24 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 05:24 WG1978145 Xylenes, Total 1040 17.4 300 100 12/22/2022 21:57 WG1978665 (S) Toluene-d8 95.8 80.0-120 12/22/2022 05:24 WG1978145 (S) Toluene-d8 94.9 80.0-120 12/22/2022 21:57 WG1978665 (S) 4-Bromofluorobenzene 87.4 77.0-126 12/22/2022 05:24 WG1978145 (S) 4-Bromofluorobenzene 93.0 77.0-126 12/22/2022 21:57 WG1978665 (S) 1,2-Dichloroethane-d4 91.8 70.0-130 12/22/2022 05:24 WG1978145 (S) 1,2-Dichloroethane-d4 103 70.0-130 12/22/2022 21:57 WG1978665 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/18/2022 18:45 WG1975661 Acenaphthylene U 0.0921 1.00 1 12/18/2022 18:45 WG1975661 Anthracene U 0.0804 1.00 1 12/18/2022 18:45 WG1975661 Benzidine U J4 3.74 10.0 1 12/18/2022 18:45 WG1975661 Benzo(a)anthracene U 0.199 1.00 1 12/18/2022 18:45 WG1975661 Benzo(b)fluoranthene U 0.130 1.00 1 12/18/2022 18:45 WG1975661 Benzo(k)fluoranthene U 0.120 1.00 1 12/18/2022 18:45 WG1975661 Benzo(g,h,i)perylene U 0.121 1.00 1 12/18/2022 18:45 WG1975661 Benzo(a)pyrene U 0.0381 1.00 1 12/18/2022 18:45 WG1975661 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/18/2022 18:45 WG1975661 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/18/2022 18:45 WG1975661 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/18/2022 18:45 WG1975661 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/18/2022 18:45 WG1975661 2-Chloronaphthalene U 0.0648 1.00 1 12/18/2022 18:45 WG1975661 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/18/2022 18:45 WG1975661 Chrysene U 0.130 1.00 1 12/18/2022 18:45 WG1975661 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/18/2022 18:45 WG1975661 1,2-Dichlorobenzene U 0.0713 10.0 1 12/18/2022 18:45 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 19 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 19 of 63 SAMPLE RESULTS - 05 L1568172 MW-3 DUPE Collected date/time: 12/13/22 11:05 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,3-Dichlorobenzene U 0.132 10.0 1 12/18/2022 18:45 WG1975661 1,4-Dichlorobenzene U 0.0942 10.0 1 12/18/2022 18:45 WG1975661 3,3-Dichlorobenzidine U 0.212 10.0 1 12/18/2022 18:45 WG1975661 2,4-Dinitrotoluene U 0.0983 10.0 1 12/18/2022 18:45 WG1975661 2,6-Dinitrotoluene U 0.250 10.0 1 12/18/2022 18:45 WG1975661 Fluoranthene U 0.102 1.00 1 12/18/2022 18:45 WG1975661 Fluorene U 0.0844 1.00 1 12/18/2022 18:45 WG1975661 Hexachlorobenzene U 0.0755 1.00 1 12/18/2022 18:45 WG1975661 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/18/2022 18:45 WG1975661 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/18/2022 18:45 WG1975661 Hexachloroethane U 0.127 10.0 1 12/18/2022 18:45 WG1975661 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/18/2022 18:45 WG1975661 Isophorone U 0.143 10.0 1 12/18/2022 18:45 WG1975661 Naphthalene 15.5 0.159 1.00 1 12/18/2022 18:45 WG1975661 Nitrobenzene U 0.297 10.0 1 12/18/2022 18:45 WG1975661 n-Nitrosodimethylamine U 0.998 10.0 1 12/18/2022 18:45 WG1975661 n-Nitrosodiphenylamine U 2.37 10.0 1 12/18/2022 18:45 WG1975661 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/18/2022 18:45 WG1975661 Phenanthrene U 0.112 1.00 1 12/18/2022 18:45 WG1975661 Benzylbutyl phthalate U 0.765 3.00 1 12/18/2022 18:45 WG1975661 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/18/2022 18:45 WG1975661 Di-n-butyl phthalate U 0.453 3.00 1 12/18/2022 18:45 WG1975661 Diethyl phthalate U 0.287 3.00 1 12/18/2022 18:45 WG1975661 Dimethyl phthalate U 0.260 3.00 1 12/18/2022 18:45 WG1975661 Di-n-octyl phthalate U 0.932 3.00 1 12/18/2022 18:45 WG1975661 Pyrene U 0.107 1.00 1 12/18/2022 18:45 WG1975661 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/18/2022 18:45 WG1975661 4-Chloro-3-methylphenol U 0.131 10.0 1 12/18/2022 18:45 WG1975661 2-Chlorophenol U 0.133 10.0 1 12/18/2022 18:45 WG1975661 2,4-Dichlorophenol U 0.102 10.0 1 12/18/2022 18:45 WG1975661 2,4-Dimethylphenol U 0.0636 10.0 1 12/18/2022 18:45 WG1975661 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/18/2022 18:45 WG1975661 2,4-Dinitrophenol U 5.93 10.0 1 12/18/2022 18:45 WG1975661 2-Nitrophenol U 0.117 10.0 1 12/18/2022 18:45 WG1975661 4-Nitrophenol U 0.143 10.0 1 12/18/2022 18:45 WG1975661 Pentachlorophenol U 0.313 10.0 1 12/18/2022 18:45 WG1975661 Phenol U 4.33 10.0 1 12/18/2022 18:45 WG1975661 2,4,6-Trichlorophenol U 0.100 10.0 1 12/18/2022 18:45 WG1975661 (S) 2-Fluorophenol 24.9 10.0-120 12/18/2022 18:45 WG1975661 (S) Phenol-d5 16.3 10.0-120 12/18/2022 18:45 WG1975661 (S) Nitrobenzene-d5 52.3 10.0-127 12/18/2022 18:45 WG1975661 (S) 2-Fluorobiphenyl 65.1 10.0-130 12/18/2022 18:45 WG1975661 (S) 2,4,6-Tribromophenol 62.6 10.0-155 12/18/2022 18:45 WG1975661 (S) p-Terphenyl-d14 72.4 10.0-128 12/18/2022 18:45 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 20 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 20 of 63 SAMPLE RESULTS - 06 L1568172 MW-2 Collected date/time: 12/13/22 12:00 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury 1.29 0.100 0.200 1 12/19/2022 18:38 WG1975422 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 2.11 0.180 2.00 1 12/23/2022 12:36 WG1977121 Barium 127 0.381 2.00 1 12/23/2022 12:36 WG1977121 Cadmium U 0.150 1.00 1 12/23/2022 12:36 WG1977121 Chromium 13.4 1.24 2.00 1 12/26/2022 12:07 WG1977121 Lead 38.8 0.849 2.00 1 12/23/2022 12:36 WG1977121 Selenium U 0.300 2.00 1 12/23/2022 12:36 WG1977121 Silver U 0.0700 2.00 1 12/23/2022 12:36 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U J3 11.3 50.0 1 12/22/2022 05:46 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 05:46 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 05:46 WG1978145 Benzene 0.205 J 0.0941 1.00 1 12/22/2022 19:14 WG1978665 Bromobenzene U 0.118 1.00 1 12/22/2022 05:46 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 05:46 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 05:46 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 05:46 WG1978145 n-Butylbenzene U 0.157 1.00 1 12/22/2022 05:46 WG1978145 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 05:46 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 05:46 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 05:46 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 05:46 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 05:46 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 05:46 WG1978145 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 05:46 WG1978145 Chloroform 0.825 J 0.111 5.00 1 12/22/2022 05:46 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 05:46 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 05:46 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 05:46 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 05:46 WG1978145 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 05:46 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 05:46 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 05:46 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 05:46 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 05:46 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 05:46 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 05:46 WG1978145 1,2-Dichloroethane 0.210 J 0.0819 1.00 1 12/22/2022 05:46 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 05:46 WG1978145 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 05:46 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 05:46 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 05:46 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 05:46 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 05:46 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 05:46 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 05:46 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 05:46 WG1978145 Di-isopropyl ether 0.125 J 0.105 1.00 1 12/22/2022 05:46 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 21 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 21 of 63 SAMPLE RESULTS - 06 L1568172 MW-2 Collected date/time: 12/13/22 12:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene 0.187 J 0.137 1.00 1 12/22/2022 19:14 WG1978665 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 05:46 WG1978145 Isopropylbenzene U 0.105 1.00 1 12/22/2022 05:46 WG1978145 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 05:46 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 05:46 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 05:46 WG1978145 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 05:46 WG1978145 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 05:46 WG1978145 Naphthalene U J3 1.00 5.00 1 12/22/2022 05:46 WG1978145 n-Propylbenzene 0.133 J 0.0993 1.00 1 12/22/2022 05:46 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 05:46 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 05:46 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 05:46 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 05:46 WG1978145 Tetrachloroethene 0.409 J 0.300 1.00 1 12/22/2022 05:46 WG1978145 Toluene 0.852 J 0.278 1.00 1 12/22/2022 19:14 WG1978665 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 05:46 WG1978145 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 05:46 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 05:46 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 05:46 WG1978145 Trichloroethene 0.241 J 0.190 1.00 1 12/22/2022 05:46 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 05:46 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 05:46 WG1978145 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 19:14 WG1978665 1,2,3-Trimethylbenzene 0.285 J 0.104 1.00 1 12/22/2022 05:46 WG1978145 1,3,5-Trimethylbenzene 0.251 J 0.104 1.00 1 12/22/2022 05:46 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 05:46 WG1978145 Xylenes, Total 0.661 J 0.174 3.00 1 12/22/2022 19:14 WG1978665 (S) Toluene-d8 98.4 80.0-120 12/22/2022 05:46 WG1978145 (S) Toluene-d8 99.5 80.0-120 12/22/2022 19:14 WG1978665 (S) 4-Bromofluorobenzene 97.7 77.0-126 12/22/2022 05:46 WG1978145 (S) 4-Bromofluorobenzene 95.1 77.0-126 12/22/2022 19:14 WG1978665 (S) 1,2-Dichloroethane-d4 101 70.0-130 12/22/2022 05:46 WG1978145 (S) 1,2-Dichloroethane-d4 102 70.0-130 12/22/2022 19:14 WG1978665 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/18/2022 19:06 WG1975661 Acenaphthylene U 0.0921 1.00 1 12/18/2022 19:06 WG1975661 Anthracene U 0.0804 1.00 1 12/18/2022 19:06 WG1975661 Benzidine U J4 3.74 10.0 1 12/18/2022 19:06 WG1975661 Benzo(a)anthracene U 0.199 1.00 1 12/18/2022 19:06 WG1975661 Benzo(b)fluoranthene U 0.130 1.00 1 12/18/2022 19:06 WG1975661 Benzo(k)fluoranthene U 0.120 1.00 1 12/18/2022 19:06 WG1975661 Benzo(g,h,i)perylene U 0.121 1.00 1 12/18/2022 19:06 WG1975661 Benzo(a)pyrene U 0.0381 1.00 1 12/18/2022 19:06 WG1975661 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/18/2022 19:06 WG1975661 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/18/2022 19:06 WG1975661 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/18/2022 19:06 WG1975661 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/18/2022 19:06 WG1975661 2-Chloronaphthalene U 0.0648 1.00 1 12/18/2022 19:06 WG1975661 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/18/2022 19:06 WG1975661 Chrysene U 0.130 1.00 1 12/18/2022 19:06 WG1975661 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/18/2022 19:06 WG1975661 1,2-Dichlorobenzene U 0.0713 10.0 1 12/18/2022 19:06 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 22 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 22 of 63 SAMPLE RESULTS - 06 L1568172 MW-2 Collected date/time: 12/13/22 12:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,3-Dichlorobenzene U 0.132 10.0 1 12/18/2022 19:06 WG1975661 1,4-Dichlorobenzene U 0.0942 10.0 1 12/18/2022 19:06 WG1975661 3,3-Dichlorobenzidine U 0.212 10.0 1 12/18/2022 19:06 WG1975661 2,4-Dinitrotoluene U 0.0983 10.0 1 12/18/2022 19:06 WG1975661 2,6-Dinitrotoluene U 0.250 10.0 1 12/18/2022 19:06 WG1975661 Fluoranthene U 0.102 1.00 1 12/18/2022 19:06 WG1975661 Fluorene U 0.0844 1.00 1 12/18/2022 19:06 WG1975661 Hexachlorobenzene U 0.0755 1.00 1 12/18/2022 19:06 WG1975661 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/18/2022 19:06 WG1975661 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/18/2022 19:06 WG1975661 Hexachloroethane U 0.127 10.0 1 12/18/2022 19:06 WG1975661 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/18/2022 19:06 WG1975661 Isophorone U 0.143 10.0 1 12/18/2022 19:06 WG1975661 Naphthalene U 0.159 1.00 1 12/18/2022 19:06 WG1975661 Nitrobenzene U 0.297 10.0 1 12/18/2022 19:06 WG1975661 n-Nitrosodimethylamine U 0.998 10.0 1 12/18/2022 19:06 WG1975661 n-Nitrosodiphenylamine U 2.37 10.0 1 12/18/2022 19:06 WG1975661 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/18/2022 19:06 WG1975661 Phenanthrene U 0.112 1.00 1 12/18/2022 19:06 WG1975661 Benzylbutyl phthalate U 0.765 3.00 1 12/18/2022 19:06 WG1975661 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/18/2022 19:06 WG1975661 Di-n-butyl phthalate U 0.453 3.00 1 12/18/2022 19:06 WG1975661 Diethyl phthalate U 0.287 3.00 1 12/18/2022 19:06 WG1975661 Dimethyl phthalate U 0.260 3.00 1 12/18/2022 19:06 WG1975661 Di-n-octyl phthalate U 0.932 3.00 1 12/18/2022 19:06 WG1975661 Pyrene U 0.107 1.00 1 12/18/2022 19:06 WG1975661 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/18/2022 19:06 WG1975661 4-Chloro-3-methylphenol U 0.131 10.0 1 12/18/2022 19:06 WG1975661 2-Chlorophenol U 0.133 10.0 1 12/18/2022 19:06 WG1975661 2,4-Dichlorophenol U 0.102 10.0 1 12/18/2022 19:06 WG1975661 2,4-Dimethylphenol U 0.0636 10.0 1 12/18/2022 19:06 WG1975661 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/18/2022 19:06 WG1975661 2,4-Dinitrophenol U 5.93 10.0 1 12/18/2022 19:06 WG1975661 2-Nitrophenol U 0.117 10.0 1 12/18/2022 19:06 WG1975661 4-Nitrophenol U 0.143 10.0 1 12/18/2022 19:06 WG1975661 Pentachlorophenol U 0.313 10.0 1 12/18/2022 19:06 WG1975661 Phenol U 4.33 10.0 1 12/18/2022 19:06 WG1975661 2,4,6-Trichlorophenol U 0.100 10.0 1 12/18/2022 19:06 WG1975661 (S) 2-Fluorophenol 28.1 10.0-120 12/18/2022 19:06 WG1975661 (S) Phenol-d5 19.2 10.0-120 12/18/2022 19:06 WG1975661 (S) Nitrobenzene-d5 65.6 10.0-127 12/18/2022 19:06 WG1975661 (S) 2-Fluorobiphenyl 69.6 10.0-130 12/18/2022 19:06 WG1975661 (S) 2,4,6-Tribromophenol 57.7 10.0-155 12/18/2022 19:06 WG1975661 (S) p-Terphenyl-d14 73.3 10.0-128 12/18/2022 19:06 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 23 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 23 of 63 SAMPLE RESULTS - 07 L1568172 MW-6 Collected date/time: 12/13/22 13:10 Mercury by Method 7470A Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Mercury U 0.100 0.200 1 12/19/2022 18:40 WG1975422 Metals (ICPMS) by Method 6020B Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Arsenic 8.99 J 0.900 10.0 5 12/26/2022 12:10 WG1977121 Barium 224 1.90 10.0 5 12/26/2022 12:10 WG1977121 Cadmium 0.265 J 0.150 1.00 1 12/23/2022 12:39 WG1977121 Chromium 8.55 J 6.20 10.0 5 12/26/2022 12:10 WG1977121 Lead 40.5 0.849 2.00 1 12/23/2022 12:39 WG1977121 Selenium 5.22 0.300 2.00 1 12/23/2022 12:39 WG1977121 Silver U 0.0700 2.00 1 12/23/2022 12:39 WG1977121 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U J3 11.3 50.0 1 12/22/2022 06:08 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 06:08 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 06:08 WG1978145 Benzene 0.145 J 0.0941 1.00 1 12/22/2022 19:34 WG1978665 Bromobenzene U 0.118 1.00 1 12/22/2022 06:08 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 06:08 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 06:08 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 06:08 WG1978145 n-Butylbenzene U 0.157 1.00 1 12/22/2022 06:08 WG1978145 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 06:08 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 06:08 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 06:08 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 06:08 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 06:08 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 06:08 WG1978145 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 06:08 WG1978145 Chloroform 0.283 J 0.111 5.00 1 12/22/2022 06:08 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 06:08 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 06:08 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 06:08 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 06:08 WG1978145 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 06:08 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 06:08 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 06:08 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 06:08 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 06:08 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 06:08 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 06:08 WG1978145 1,2-Dichloroethane 0.143 J 0.0819 1.00 1 12/22/2022 06:08 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 06:08 WG1978145 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 06:08 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 06:08 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 06:08 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 06:08 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 06:08 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 06:08 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 06:08 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 06:08 WG1978145 Di-isopropyl ether 0.688 J 0.105 1.00 1 12/22/2022 06:08 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 24 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 24 of 63 SAMPLE RESULTS - 07 L1568172 MW-6 Collected date/time: 12/13/22 13:10 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Ethylbenzene U 0.137 1.00 1 12/22/2022 19:34 WG1978665 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 06:08 WG1978145 Isopropylbenzene U 0.105 1.00 1 12/22/2022 06:08 WG1978145 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 06:08 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 06:08 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 06:08 WG1978145 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 06:08 WG1978145 Methyl tert-butyl ether 0.238 J 0.101 1.00 1 12/22/2022 06:08 WG1978145 Naphthalene U J3 1.00 5.00 1 12/22/2022 06:08 WG1978145 n-Propylbenzene U 0.0993 1.00 1 12/22/2022 06:08 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 06:08 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 06:08 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 06:08 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 06:08 WG1978145 Tetrachloroethene 25.8 0.300 1.00 1 12/22/2022 06:08 WG1978145 Toluene 0.526 J 0.278 1.00 1 12/22/2022 19:34 WG1978665 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 06:08 WG1978145 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 06:08 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 06:08 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 06:08 WG1978145 Trichloroethene U 0.190 1.00 1 12/22/2022 06:08 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 06:08 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 06:08 WG1978145 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 06:08 WG1978145 1,2,3-Trimethylbenzene U 0.104 1.00 1 12/22/2022 06:08 WG1978145 1,3,5-Trimethylbenzene U 0.104 1.00 1 12/22/2022 06:08 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 06:08 WG1978145 Xylenes, Total 0.373 J 0.174 3.00 1 12/22/2022 19:34 WG1978665 (S) Toluene-d8 95.9 80.0-120 12/22/2022 06:08 WG1978145 (S) Toluene-d8 97.4 80.0-120 12/22/2022 19:34 WG1978665 (S) 4-Bromofluorobenzene 93.3 77.0-126 12/22/2022 06:08 WG1978145 (S) 4-Bromofluorobenzene 90.4 77.0-126 12/22/2022 19:34 WG1978665 (S) 1,2-Dichloroethane-d4 99.8 70.0-130 12/22/2022 06:08 WG1978145 (S) 1,2-Dichloroethane-d4 99.6 70.0-130 12/22/2022 19:34 WG1978665 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acenaphthene U 0.0886 1.00 1 12/18/2022 19:27 WG1975661 Acenaphthylene U 0.0921 1.00 1 12/18/2022 19:27 WG1975661 Anthracene U 0.0804 1.00 1 12/18/2022 19:27 WG1975661 Benzidine U J4 3.74 10.0 1 12/18/2022 19:27 WG1975661 Benzo(a)anthracene U 0.199 1.00 1 12/18/2022 19:27 WG1975661 Benzo(b)fluoranthene U 0.130 1.00 1 12/18/2022 19:27 WG1975661 Benzo(k)fluoranthene U 0.120 1.00 1 12/18/2022 19:27 WG1975661 Benzo(g,h,i)perylene U 0.121 1.00 1 12/18/2022 19:27 WG1975661 Benzo(a)pyrene U 0.0381 1.00 1 12/18/2022 19:27 WG1975661 Bis(2-chlorethoxy)methane U 0.116 10.0 1 12/18/2022 19:27 WG1975661 Bis(2-chloroethyl)ether U 0.137 10.0 1 12/18/2022 19:27 WG1975661 2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 12/18/2022 19:27 WG1975661 4-Bromophenyl-phenylether U 0.0877 10.0 1 12/18/2022 19:27 WG1975661 2-Chloronaphthalene U 0.0648 1.00 1 12/18/2022 19:27 WG1975661 4-Chlorophenyl-phenylether U 0.0926 10.0 1 12/18/2022 19:27 WG1975661 Chrysene U 0.130 1.00 1 12/18/2022 19:27 WG1975661 Dibenz(a,h)anthracene U 0.0644 1.00 1 12/18/2022 19:27 WG1975661 1,2-Dichlorobenzene U 0.0713 10.0 1 12/18/2022 19:27 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 25 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 25 of 63 SAMPLE RESULTS - 07 L1568172 MW-6 Collected date/time: 12/13/22 13:10 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,3-Dichlorobenzene U 0.132 10.0 1 12/18/2022 19:27 WG1975661 1,4-Dichlorobenzene U 0.0942 10.0 1 12/18/2022 19:27 WG1975661 3,3-Dichlorobenzidine U 0.212 10.0 1 12/18/2022 19:27 WG1975661 2,4-Dinitrotoluene U 0.0983 10.0 1 12/18/2022 19:27 WG1975661 2,6-Dinitrotoluene U 0.250 10.0 1 12/18/2022 19:27 WG1975661 Fluoranthene U 0.102 1.00 1 12/18/2022 19:27 WG1975661 Fluorene U 0.0844 1.00 1 12/18/2022 19:27 WG1975661 Hexachlorobenzene U 0.0755 1.00 1 12/18/2022 19:27 WG1975661 Hexachloro-1,3-butadiene U 0.0968 10.0 1 12/18/2022 19:27 WG1975661 Hexachlorocyclopentadiene U 0.0598 10.0 1 12/18/2022 19:27 WG1975661 Hexachloroethane U 0.127 10.0 1 12/18/2022 19:27 WG1975661 Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 12/18/2022 19:27 WG1975661 Isophorone U 0.143 10.0 1 12/18/2022 19:27 WG1975661 Naphthalene U 0.159 1.00 1 12/18/2022 19:27 WG1975661 Nitrobenzene U 0.297 10.0 1 12/18/2022 19:27 WG1975661 n-Nitrosodimethylamine U 0.998 10.0 1 12/18/2022 19:27 WG1975661 n-Nitrosodiphenylamine U 2.37 10.0 1 12/18/2022 19:27 WG1975661 n-Nitrosodi-n-propylamine U 0.261 10.0 1 12/18/2022 19:27 WG1975661 Phenanthrene U 0.112 1.00 1 12/18/2022 19:27 WG1975661 Benzylbutyl phthalate U 0.765 3.00 1 12/18/2022 19:27 WG1975661 Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 12/18/2022 19:27 WG1975661 Di-n-butyl phthalate U 0.453 3.00 1 12/18/2022 19:27 WG1975661 Diethyl phthalate U 0.287 3.00 1 12/18/2022 19:27 WG1975661 Dimethyl phthalate U 0.260 3.00 1 12/18/2022 19:27 WG1975661 Di-n-octyl phthalate U 0.932 3.00 1 12/18/2022 19:27 WG1975661 Pyrene U 0.107 1.00 1 12/18/2022 19:27 WG1975661 1,2,4-Trichlorobenzene U 0.0698 10.0 1 12/18/2022 19:27 WG1975661 4-Chloro-3-methylphenol U 0.131 10.0 1 12/18/2022 19:27 WG1975661 2-Chlorophenol U 0.133 10.0 1 12/18/2022 19:27 WG1975661 2,4-Dichlorophenol U 0.102 10.0 1 12/18/2022 19:27 WG1975661 2,4-Dimethylphenol U 0.0636 10.0 1 12/18/2022 19:27 WG1975661 4,6-Dinitro-2-methylphenol U 1.12 10.0 1 12/18/2022 19:27 WG1975661 2,4-Dinitrophenol U 5.93 10.0 1 12/18/2022 19:27 WG1975661 2-Nitrophenol U 0.117 10.0 1 12/18/2022 19:27 WG1975661 4-Nitrophenol U 0.143 10.0 1 12/18/2022 19:27 WG1975661 Pentachlorophenol U 0.313 10.0 1 12/18/2022 19:27 WG1975661 Phenol U 4.33 10.0 1 12/18/2022 19:27 WG1975661 2,4,6-Trichlorophenol U 0.100 10.0 1 12/18/2022 19:27 WG1975661 (S) 2-Fluorophenol 24.7 10.0-120 12/18/2022 19:27 WG1975661 (S) Phenol-d5 16.4 10.0-120 12/18/2022 19:27 WG1975661 (S) Nitrobenzene-d5 61.6 10.0-127 12/18/2022 19:27 WG1975661 (S) 2-Fluorobiphenyl 67.4 10.0-130 12/18/2022 19:27 WG1975661 (S) 2,4,6-Tribromophenol 49.0 10.0-155 12/18/2022 19:27 WG1975661 (S) p-Terphenyl-d14 74.4 10.0-128 12/18/2022 19:27 WG1975661 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 26 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 26 of 63 SAMPLE RESULTS - 08 L1568172 TRIPBLANK Collected date/time: 12/13/22 00:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time Acetone U J3 11.3 50.0 1 12/22/2022 01:45 WG1978145 Acrolein U 2.54 50.0 1 12/22/2022 01:45 WG1978145 Acrylonitrile U 0.671 10.0 1 12/22/2022 01:45 WG1978145 Benzene U 0.0941 1.00 1 12/22/2022 01:45 WG1978145 Bromobenzene U 0.118 1.00 1 12/22/2022 01:45 WG1978145 Bromodichloromethane U 0.136 1.00 1 12/22/2022 01:45 WG1978145 Bromoform U 0.129 1.00 1 12/22/2022 01:45 WG1978145 Bromomethane U 0.605 5.00 1 12/22/2022 01:45 WG1978145 n-Butylbenzene U 0.157 1.00 1 12/22/2022 01:45 WG1978145 sec-Butylbenzene U 0.125 1.00 1 12/22/2022 01:45 WG1978145 tert-Butylbenzene U 0.127 1.00 1 12/22/2022 01:45 WG1978145 Carbon tetrachloride U 0.128 1.00 1 12/22/2022 01:45 WG1978145 Chlorobenzene U 0.116 1.00 1 12/22/2022 01:45 WG1978145 Chlorodibromomethane U 0.140 1.00 1 12/22/2022 01:45 WG1978145 Chloroethane U 0.192 5.00 1 12/22/2022 01:45 WG1978145 2-Chloroethyl vinyl ether U 0.575 50.0 1 12/22/2022 01:45 WG1978145 Chloroform U 0.111 5.00 1 12/22/2022 01:45 WG1978145 Chloromethane U 0.960 2.50 1 12/22/2022 01:45 WG1978145 2-Chlorotoluene U 0.106 1.00 1 12/22/2022 01:45 WG1978145 4-Chlorotoluene U 0.114 1.00 1 12/22/2022 01:45 WG1978145 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 12/22/2022 01:45 WG1978145 1,2-Dibromoethane U 0.126 1.00 1 12/22/2022 01:45 WG1978145 Dibromomethane U 0.122 1.00 1 12/22/2022 01:45 WG1978145 1,2-Dichlorobenzene U 0.107 1.00 1 12/22/2022 01:45 WG1978145 1,3-Dichlorobenzene U 0.110 1.00 1 12/22/2022 01:45 WG1978145 1,4-Dichlorobenzene U 0.120 1.00 1 12/22/2022 01:45 WG1978145 Dichlorodifluoromethane U 0.374 5.00 1 12/22/2022 01:45 WG1978145 1,1-Dichloroethane U 0.100 1.00 1 12/22/2022 01:45 WG1978145 1,2-Dichloroethane U 0.0819 1.00 1 12/22/2022 01:45 WG1978145 1,1-Dichloroethene U 0.188 1.00 1 12/22/2022 01:45 WG1978145 cis-1,2-Dichloroethene U 0.126 1.00 1 12/22/2022 01:45 WG1978145 trans-1,2-Dichloroethene U 0.149 1.00 1 12/22/2022 01:45 WG1978145 1,2-Dichloropropane U 0.149 1.00 1 12/22/2022 01:45 WG1978145 1,1-Dichloropropene U 0.142 1.00 1 12/22/2022 01:45 WG1978145 1,3-Dichloropropane U 0.110 1.00 1 12/22/2022 01:45 WG1978145 cis-1,3-Dichloropropene U 0.111 1.00 1 12/22/2022 01:45 WG1978145 trans-1,3-Dichloropropene U 0.118 1.00 1 12/22/2022 01:45 WG1978145 2,2-Dichloropropane U 0.161 1.00 1 12/22/2022 01:45 WG1978145 Di-isopropyl ether U 0.105 1.00 1 12/22/2022 01:45 WG1978145 Ethylbenzene U 0.137 1.00 1 12/22/2022 01:45 WG1978145 Hexachloro-1,3-butadiene U J3 0.337 1.00 1 12/22/2022 01:45 WG1978145 Isopropylbenzene U 0.105 1.00 1 12/22/2022 01:45 WG1978145 p-Isopropyltoluene U 0.120 1.00 1 12/22/2022 01:45 WG1978145 2-Butanone (MEK)U 1.19 10.0 1 12/22/2022 01:45 WG1978145 Methylene Chloride U 0.430 5.00 1 12/22/2022 01:45 WG1978145 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 12/22/2022 01:45 WG1978145 Methyl tert-butyl ether U 0.101 1.00 1 12/22/2022 01:45 WG1978145 Naphthalene U J3 1.00 5.00 1 12/22/2022 01:45 WG1978145 n-Propylbenzene U 0.0993 1.00 1 12/22/2022 01:45 WG1978145 Styrene U 0.118 1.00 1 12/22/2022 01:45 WG1978145 1,1,1,2-Tetrachloroethane U 0.147 1.00 1 12/22/2022 01:45 WG1978145 1,1,2,2-Tetrachloroethane U 0.133 1.00 1 12/22/2022 01:45 WG1978145 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 12/22/2022 01:45 WG1978145 Tetrachloroethene U 0.300 1.00 1 12/22/2022 01:45 WG1978145 Toluene U 0.278 1.00 1 12/22/2022 01:45 WG1978145 1,2,3-Trichlorobenzene U J3 0.230 1.00 1 12/22/2022 01:45 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 27 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 27 of 63 SAMPLE RESULTS - 08 L1568172 TRIPBLANK Collected date/time: 12/13/22 00:00 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/l ug/l ug/l date / time 1,2,4-Trichlorobenzene U J3 0.481 1.00 1 12/22/2022 01:45 WG1978145 1,1,1-Trichloroethane U 0.149 1.00 1 12/22/2022 01:45 WG1978145 1,1,2-Trichloroethane U 0.158 1.00 1 12/22/2022 01:45 WG1978145 Trichloroethene U 0.190 1.00 1 12/22/2022 01:45 WG1978145 Trichlorofluoromethane U 0.160 5.00 1 12/22/2022 01:45 WG1978145 1,2,3-Trichloropropane U 0.237 2.50 1 12/22/2022 01:45 WG1978145 1,2,4-Trimethylbenzene U 0.322 1.00 1 12/22/2022 01:45 WG1978145 1,2,3-Trimethylbenzene U 0.104 1.00 1 12/22/2022 01:45 WG1978145 1,3,5-Trimethylbenzene U 0.104 1.00 1 12/22/2022 01:45 WG1978145 Vinyl chloride U 0.234 1.00 1 12/22/2022 01:45 WG1978145 Xylenes, Total U 0.174 3.00 1 12/22/2022 01:45 WG1978145 (S) Toluene-d8 96.7 80.0-120 12/22/2022 01:45 WG1978145 (S) 4-Bromofluorobenzene 100 77.0-126 12/22/2022 01:45 WG1978145 (S) 1,2-Dichloroethane-d4 105 70.0-130 12/22/2022 01:45 WG1978145 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 28 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 28 of 63 QUALITY CONTROL SUMMARYWG1975421 Mercury by Method 7470A L1568172-01,02,03,04 Method Blank (MB) (MB) R3873622-1 12/19/22 15:54 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Mercury U 0.100 0.200 Laboratory Control Sample (LCS) (LCS) R3873622-2 12/19/22 15:56 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Mercury 3.00 3.00 99.9 80.0-120 L1567163-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567163-07 12/19/22 15:58 • (MS) R3873622-3 12/19/22 16:00 • (MSD) R3873622-4 12/19/22 16:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Mercury 3.00 U 3.08 2.84 103 94.8 1 75.0-125 7.94 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 29 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 29 of 63 QUALITY CONTROL SUMMARYWG1975422 Mercury by Method 7470A L1568172-05,06,07 Method Blank (MB) (MB) R3873601-1 12/19/22 18:20 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Mercury U 0.100 0.200 Laboratory Control Sample (LCS) (LCS) R3873601-2 12/19/22 18:22 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Mercury 3.00 2.79 93.0 80.0-120 L1568174-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1568174-01 12/19/22 18:24 • (MS) R3873601-3 12/19/22 18:32 • (MSD) R3873601-4 12/19/22 18:34 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Mercury 3.00 U 2.82 2.34 93.9 78.0 1 75.0-125 18.5 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 30 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 30 of 63 QUALITY CONTROL SUMMARYWG1977117 Metals (ICPMS) by Method 6020B L1568172-01 Method Blank (MB) (MB) R3874393-1 12/21/22 01:49 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Arsenic 0.184 J 0.180 2.00 Barium 0.807 J 0.381 2.00 Cadmium U 0.150 1.00 Lead U 0.849 2.00 Selenium 2.35 0.300 2.00 Silver U 0.0700 2.00 Method Blank (MB) (MB) R3874631-1 12/21/22 21:50 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Chromium U 1.24 2.00 Laboratory Control Sample (LCS) (LCS) R3874393-2 12/21/22 01:52 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Arsenic 50.0 49.4 98.8 80.0-120 Barium 50.0 52.3 105 80.0-120 Cadmium 50.0 47.7 95.3 80.0-120 Lead 50.0 47.9 95.8 80.0-120 Selenium 50.0 50.9 102 80.0-120 Silver 50.0 50.9 102 80.0-120 Laboratory Control Sample (LCS) (LCS) R3874631-2 12/21/22 21:54 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Chromium 50.0 50.9 102 80.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 31 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 31 of 63 QUALITY CONTROL SUMMARYWG1977117 Metals (ICPMS) by Method 6020B L1568172-01 L1567347-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567347-04 12/21/22 01:55 • (MS) R3874393-4 12/21/22 02:02 • (MSD) R3874393-5 12/21/22 02:05 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Arsenic 50.0 U 47.9 47.2 95.8 94.3 1 75.0-125 1.55 20 Barium 50.0 41.3 88.8 92.3 95.0 102 1 75.0-125 3.83 20 Cadmium 50.0 U 47.6 48.8 95.2 97.5 1 75.0-125 2.43 20 Lead 50.0 U 48.3 47.3 96.5 94.6 1 75.0-125 2.05 20 Selenium 50.0 U 49.6 50.3 99.1 101 1 75.0-125 1.50 20 Silver 50.0 U 50.2 51.0 100 102 1 75.0-125 1.56 20 L1567347-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567347-04 12/21/22 21:57 • (MS) R3874631-4 12/21/22 22:04 • (MSD) R3874631-5 12/21/22 22:07 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Chromium 50.0 5.90 54.2 54.0 96.5 96.2 1 75.0-125 0.300 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 32 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 32 of 63 QUALITY CONTROL SUMMARYWG1977121 Metals (ICPMS) by Method 6020B L1568172-02,03,04,05,06,07 Method Blank (MB) (MB) R3875235-1 12/23/22 11:53 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Arsenic U 0.180 2.00 Barium U 0.381 2.00 Cadmium U 0.150 1.00 Lead U 0.849 2.00 Selenium U 0.300 2.00 Silver U 0.0700 2.00 Method Blank (MB) (MB) R3875446-1 12/26/22 12:57 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Chromium U 1.24 2.00 Laboratory Control Sample (LCS) (LCS) R3875235-2 12/23/22 11:56 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Arsenic 50.0 53.2 106 80.0-120 Barium 50.0 48.2 96.5 80.0-120 Cadmium 50.0 49.3 98.6 80.0-120 Lead 50.0 48.9 97.8 80.0-120 Selenium 50.0 48.8 97.6 80.0-120 Silver 50.0 47.8 95.5 80.0-120 Laboratory Control Sample (LCS) (LCS) R3875446-2 12/26/22 13:00 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Chromium 50.0 52.1 104 80.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 33 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 33 of 63 QUALITY CONTROL SUMMARYWG1977121 Metals (ICPMS) by Method 6020B L1568172-02,03,04,05,06,07 L1567844-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567844-01 12/23/22 12:00 • (MS) R3875235-4 12/23/22 12:06 • (MSD) R3875235-5 12/23/22 12:09 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Arsenic 50.0 U 53.0 51.5 106 103 1 75.0-125 2.94 20 Barium 50.0 46.9 98.1 96.5 102 99.3 1 75.0-125 1.60 20 Cadmium 50.0 U 49.6 50.8 99.1 102 1 75.0-125 2.58 20 Lead 50.0 U 50.5 50.6 101 101 1 75.0-125 0.258 20 Selenium 50.0 U 52.7 52.8 105 106 1 75.0-125 0.0902 20 Silver 50.0 0.0731 48.8 48.2 97.4 96.2 1 75.0-125 1.21 20 L1567844-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567844-01 12/26/22 13:04 • (MS) R3875446-4 12/26/22 13:10 • (MSD) R3875446-5 12/26/22 13:14 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Chromium 50.0 4.60 55.7 55.2 102 101 1 75.0-125 0.890 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 34 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 34 of 63 QUALITY CONTROL SUMMARYWG1978139 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-01,02 Method Blank (MB) (MB) R3874904-2 12/22/22 00:14 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acetone U 11.3 50.0 Acrolein U 2.54 50.0 Acrylonitrile U 0.671 10.0 Benzene U 0.0941 1.00 Bromobenzene U 0.118 1.00 Bromodichloromethane U 0.136 1.00 Bromoform U 0.129 1.00 Bromomethane U 0.605 5.00 n-Butylbenzene U 0.157 1.00 sec-Butylbenzene U 0.125 1.00 tert-Butylbenzene U 0.127 1.00 Carbon tetrachloride U 0.128 1.00 Chlorobenzene U 0.116 1.00 Chlorodibromomethane U 0.140 1.00 Chloroethane U 0.192 5.00 2-Chloroethyl vinyl ether U 0.575 50.0 Chloroform U 0.111 5.00 Chloromethane U 0.960 2.50 2-Chlorotoluene U 0.106 1.00 4-Chlorotoluene U 0.114 1.00 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1,2-Dibromoethane U 0.126 1.00 Dibromomethane U 0.122 1.00 1,2-Dichlorobenzene U 0.107 1.00 1,3-Dichlorobenzene U 0.110 1.00 1,4-Dichlorobenzene U 0.120 1.00 Dichlorodifluoromethane U 0.374 5.00 1,1-Dichloroethane U 0.100 1.00 1,2-Dichloroethane U 0.0819 1.00 1,1-Dichloroethene U 0.188 1.00 cis-1,2-Dichloroethene U 0.126 1.00 trans-1,2-Dichloroethene U 0.149 1.00 1,2-Dichloropropane U 0.149 1.00 1,1-Dichloropropene U 0.142 1.00 1,3-Dichloropropane U 0.110 1.00 cis-1,3-Dichloropropene U 0.111 1.00 trans-1,3-Dichloropropene U 0.118 1.00 2,2-Dichloropropane U 0.161 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 35 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 35 of 63 QUALITY CONTROL SUMMARYWG1978139 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-01,02 Method Blank (MB) (MB) R3874904-2 12/22/22 00:14 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Hexachloro-1,3-butadiene U 0.337 1.00 Isopropylbenzene U 0.105 1.00 p-Isopropyltoluene U 0.120 1.00 2-Butanone (MEK)U 1.19 10.0 Methylene Chloride U 0.430 5.00 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 n-Propylbenzene U 0.0993 1.00 Styrene U 0.118 1.00 1,1,1,2-Tetrachloroethane U 0.147 1.00 1,1,2,2-Tetrachloroethane U 0.133 1.00 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 Tetrachloroethene U 0.300 1.00 Toluene U 0.278 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 1,2,4-Trichlorobenzene U 0.481 1.00 1,1,1-Trichloroethane U 0.149 1.00 1,1,2-Trichloroethane U 0.158 1.00 Trichloroethene U 0.190 1.00 Trichlorofluoromethane U 0.160 5.00 1,2,3-Trichloropropane U 0.237 2.50 1,2,4-Trimethylbenzene U 0.322 1.00 1,2,3-Trimethylbenzene U 0.104 1.00 1,3,5-Trimethylbenzene U 0.104 1.00 Vinyl chloride U 0.234 1.00 Xylenes, Total U 0.174 3.00 (S) Toluene-d8 102 80.0-120 (S) 4-Bromofluorobenzene 94.3 77.0-126 (S) 1,2-Dichloroethane-d4 92.2 70.0-130 Laboratory Control Sample (LCS) (LCS) R3874904-1 12/21/22 23:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acetone 25.0 24.2 96.8 19.0-160 Acrolein 25.0 12.9 51.6 10.0-160 Acrylonitrile 25.0 25.4 102 55.0-149 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 36 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 36 of 63 QUALITY CONTROL SUMMARYWG1978139 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-01,02 Laboratory Control Sample (LCS) (LCS) R3874904-1 12/21/22 23:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Benzene 5.00 4.21 84.2 70.0-123 Bromobenzene 5.00 4.51 90.2 73.0-121 Bromodichloromethane 5.00 4.38 87.6 75.0-120 Bromoform 5.00 4.35 87.0 68.0-132 Bromomethane 5.00 5.57 111 10.0-160 n-Butylbenzene 5.00 4.03 80.6 73.0-125 sec-Butylbenzene 5.00 4.32 86.4 75.0-125 tert-Butylbenzene 5.00 4.16 83.2 76.0-124 Carbon tetrachloride 5.00 4.36 87.2 68.0-126 Chlorobenzene 5.00 4.61 92.2 80.0-121 Chlorodibromomethane 5.00 4.38 87.6 77.0-125 Chloroethane 5.00 5.97 119 47.0-150 2-Chloroethyl vinyl ether 25.0 22.4 89.6 51.0-160 Chloroform 5.00 4.50 90.0 73.0-120 Chloromethane 5.00 4.51 90.2 41.0-142 2-Chlorotoluene 5.00 4.47 89.4 76.0-123 4-Chlorotoluene 5.00 4.42 88.4 75.0-122 1,2-Dibromo-3-Chloropropane 5.00 4.07 81.4 58.0-134 1,2-Dibromoethane 5.00 4.39 87.8 80.0-122 Dibromomethane 5.00 4.60 92.0 80.0-120 1,2-Dichlorobenzene 5.00 4.73 94.6 79.0-121 1,3-Dichlorobenzene 5.00 4.51 90.2 79.0-120 1,4-Dichlorobenzene 5.00 4.44 88.8 79.0-120 Dichlorodifluoromethane 5.00 5.51 110 51.0-149 1,1-Dichloroethane 5.00 4.46 89.2 70.0-126 1,2-Dichloroethane 5.00 4.50 90.0 70.0-128 1,1-Dichloroethene 5.00 4.37 87.4 71.0-124 cis-1,2-Dichloroethene 5.00 4.29 85.8 73.0-120 trans-1,2-Dichloroethene 5.00 4.46 89.2 73.0-120 1,2-Dichloropropane 5.00 4.43 88.6 77.0-125 1,1-Dichloropropene 5.00 4.58 91.6 74.0-126 1,3-Dichloropropane 5.00 4.87 97.4 80.0-120 cis-1,3-Dichloropropene 5.00 4.14 82.8 80.0-123 trans-1,3-Dichloropropene 5.00 4.31 86.2 78.0-124 2,2-Dichloropropane 5.00 4.28 85.6 58.0-130 Di-isopropyl ether 5.00 4.47 89.4 58.0-138 Ethylbenzene 5.00 4.30 86.0 79.0-123 Hexachloro-1,3-butadiene 5.00 3.97 79.4 54.0-138 Isopropylbenzene 5.00 4.33 86.6 76.0-127 p-Isopropyltoluene 5.00 4.23 84.6 76.0-125 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 37 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 37 of 63 QUALITY CONTROL SUMMARYWG1978139 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-01,02 Laboratory Control Sample (LCS) (LCS) R3874904-1 12/21/22 23:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2-Butanone (MEK)25.0 23.4 93.6 44.0-160 Methylene Chloride 5.00 4.63 92.6 67.0-120 4-Methyl-2-pentanone (MIBK)25.0 24.0 96.0 68.0-142 Methyl tert-butyl ether 5.00 4.35 87.0 68.0-125 Naphthalene 5.00 4.22 84.4 54.0-135 n-Propylbenzene 5.00 4.35 87.0 77.0-124 Styrene 5.00 3.95 79.0 73.0-130 1,1,1,2-Tetrachloroethane 5.00 4.49 89.8 75.0-125 1,1,2,2-Tetrachloroethane 5.00 4.83 96.6 65.0-130 1,1,2-Trichlorotrifluoroethane 5.00 5.36 107 69.0-132 Tetrachloroethene 5.00 4.47 89.4 72.0-132 Toluene 5.00 4.66 93.2 79.0-120 1,2,3-Trichlorobenzene 5.00 4.38 87.6 50.0-138 1,2,4-Trichlorobenzene 5.00 4.43 88.6 57.0-137 1,1,1-Trichloroethane 5.00 4.29 85.8 73.0-124 1,1,2-Trichloroethane 5.00 4.74 94.8 80.0-120 Trichloroethene 5.00 4.54 90.8 78.0-124 Trichlorofluoromethane 5.00 5.41 108 59.0-147 1,2,3-Trichloropropane 5.00 4.47 89.4 73.0-130 1,2,4-Trimethylbenzene 5.00 4.17 83.4 76.0-121 1,2,3-Trimethylbenzene 5.00 3.95 79.0 77.0-120 1,3,5-Trimethylbenzene 5.00 4.38 87.6 76.0-122 Vinyl chloride 5.00 5.50 110 67.0-131 Xylenes, Total 15.0 13.1 87.3 79.0-123 (S) Toluene-d8 101 80.0-120 (S) 4-Bromofluorobenzene 91.1 77.0-126 (S) 1,2-Dichloroethane-d4 95.8 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 38 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 38 of 63 QUALITY CONTROL SUMMARYWG1978145 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-03,04,05,06,07,08 Method Blank (MB) (MB) R3874762-3 12/22/22 00:17 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acetone U 11.3 50.0 Acrolein U 2.54 50.0 Acrylonitrile U 0.671 10.0 Benzene U 0.0941 1.00 Bromobenzene U 0.118 1.00 Bromodichloromethane U 0.136 1.00 Bromoform U 0.129 1.00 Bromomethane U 0.605 5.00 n-Butylbenzene U 0.157 1.00 sec-Butylbenzene U 0.125 1.00 tert-Butylbenzene U 0.127 1.00 Carbon tetrachloride U 0.128 1.00 Chlorobenzene U 0.116 1.00 Chlorodibromomethane U 0.140 1.00 Chloroethane U 0.192 5.00 2-Chloroethyl vinyl ether U 0.575 50.0 Chloroform U 0.111 5.00 Chloromethane U 0.960 2.50 2-Chlorotoluene U 0.106 1.00 4-Chlorotoluene U 0.114 1.00 1,2-Dibromo-3-Chloropropane U 0.276 5.00 1,2-Dibromoethane U 0.126 1.00 Dibromomethane U 0.122 1.00 1,2-Dichlorobenzene U 0.107 1.00 1,3-Dichlorobenzene U 0.110 1.00 1,4-Dichlorobenzene U 0.120 1.00 Dichlorodifluoromethane U 0.374 5.00 1,1-Dichloroethane U 0.100 1.00 1,2-Dichloroethane U 0.0819 1.00 1,1-Dichloroethene U 0.188 1.00 cis-1,2-Dichloroethene U 0.126 1.00 trans-1,2-Dichloroethene U 0.149 1.00 1,2-Dichloropropane U 0.149 1.00 1,1-Dichloropropene U 0.142 1.00 1,3-Dichloropropane U 0.110 1.00 cis-1,3-Dichloropropene U 0.111 1.00 trans-1,3-Dichloropropene U 0.118 1.00 2,2-Dichloropropane U 0.161 1.00 Di-isopropyl ether U 0.105 1.00 Ethylbenzene U 0.137 1.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 39 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 39 of 63 QUALITY CONTROL SUMMARYWG1978145 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-03,04,05,06,07,08 Method Blank (MB) (MB) R3874762-3 12/22/22 00:17 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Hexachloro-1,3-butadiene U 0.337 1.00 Isopropylbenzene U 0.105 1.00 p-Isopropyltoluene U 0.120 1.00 2-Butanone (MEK)U 1.19 10.0 Methylene Chloride U 0.430 5.00 4-Methyl-2-pentanone (MIBK)U 0.478 10.0 Methyl tert-butyl ether U 0.101 1.00 Naphthalene U 1.00 5.00 n-Propylbenzene U 0.0993 1.00 Styrene U 0.118 1.00 1,1,1,2-Tetrachloroethane U 0.147 1.00 1,1,2,2-Tetrachloroethane U 0.133 1.00 1,1,2-Trichlorotrifluoroethane U 0.180 1.00 Tetrachloroethene U 0.300 1.00 Toluene U 0.278 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 1,2,4-Trichlorobenzene U 0.481 1.00 1,1,1-Trichloroethane U 0.149 1.00 1,1,2-Trichloroethane U 0.158 1.00 Trichloroethene U 0.190 1.00 Trichlorofluoromethane U 0.160 5.00 1,2,3-Trichloropropane U 0.237 2.50 1,2,4-Trimethylbenzene U 0.322 1.00 1,2,3-Trimethylbenzene U 0.104 1.00 1,3,5-Trimethylbenzene U 0.104 1.00 Vinyl chloride U 0.234 1.00 Xylenes, Total U 0.174 3.00 (S) Toluene-d8 98.9 80.0-120 (S) 4-Bromofluorobenzene 95.2 77.0-126 (S) 1,2-Dichloroethane-d4 101 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3874762-1 12/21/22 23:11 • (LCSD) R3874762-2 12/21/22 23:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Acetone 25.0 39.7 28.3 159 113 19.0-160 J3 33.5 27 Acrolein 25.0 28.4 26.0 114 104 10.0-160 8.82 26 Acrylonitrile 25.0 28.7 26.0 115 104 55.0-149 9.87 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 40 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 40 of 63 QUALITY CONTROL SUMMARYWG1978145 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-03,04,05,06,07,08 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3874762-1 12/21/22 23:11 • (LCSD) R3874762-2 12/21/22 23:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% Benzene 5.00 4.41 4.30 88.2 86.0 70.0-123 2.53 20 Bromobenzene 5.00 4.69 4.40 93.8 88.0 73.0-121 6.38 20 Bromodichloromethane 5.00 4.41 4.22 88.2 84.4 75.0-120 4.40 20 Bromoform 5.00 4.94 4.65 98.8 93.0 68.0-132 6.05 20 Bromomethane 5.00 6.56 6.34 131 127 10.0-160 3.41 25 n-Butylbenzene 5.00 5.37 4.58 107 91.6 73.0-125 15.9 20 sec-Butylbenzene 5.00 5.04 4.39 101 87.8 75.0-125 13.8 20 tert-Butylbenzene 5.00 4.85 4.45 97.0 89.0 76.0-124 8.60 20 Carbon tetrachloride 5.00 5.24 4.98 105 99.6 68.0-126 5.09 20 Chlorobenzene 5.00 4.57 4.62 91.4 92.4 80.0-121 1.09 20 Chlorodibromomethane 5.00 5.08 5.05 102 101 77.0-125 0.592 20 Chloroethane 5.00 6.58 6.59 132 132 47.0-150 0.152 20 2-Chloroethyl vinyl ether 25.0 21.6 20.7 86.4 82.8 51.0-160 4.26 20 Chloroform 5.00 4.69 4.67 93.8 93.4 73.0-120 0.427 20 Chloromethane 5.00 4.92 4.44 98.4 88.8 41.0-142 10.3 20 2-Chlorotoluene 5.00 5.12 4.63 102 92.6 76.0-123 10.1 20 4-Chlorotoluene 5.00 4.83 4.31 96.6 86.2 75.0-122 11.4 20 1,2-Dibromo-3-Chloropropane 5.00 5.28 4.61 106 92.2 58.0-134 13.5 20 1,2-Dibromoethane 5.00 4.54 4.74 90.8 94.8 80.0-122 4.31 20 Dibromomethane 5.00 4.75 4.85 95.0 97.0 80.0-120 2.08 20 1,2-Dichlorobenzene 5.00 5.32 4.80 106 96.0 79.0-121 10.3 20 1,3-Dichlorobenzene 5.00 4.86 4.47 97.2 89.4 79.0-120 8.36 20 1,4-Dichlorobenzene 5.00 4.89 4.28 97.8 85.6 79.0-120 13.3 20 Dichlorodifluoromethane 5.00 4.95 5.33 99.0 107 51.0-149 7.39 20 1,1-Dichloroethane 5.00 4.61 4.46 92.2 89.2 70.0-126 3.31 20 1,2-Dichloroethane 5.00 4.69 4.70 93.8 94.0 70.0-128 0.213 20 1,1-Dichloroethene 5.00 5.42 4.98 108 99.6 71.0-124 8.46 20 cis-1,2-Dichloroethene 5.00 4.67 4.15 93.4 83.0 73.0-120 11.8 20 trans-1,2-Dichloroethene 5.00 4.61 4.64 92.2 92.8 73.0-120 0.649 20 1,2-Dichloropropane 5.00 4.44 4.31 88.8 86.2 77.0-125 2.97 20 1,1-Dichloropropene 5.00 4.57 4.88 91.4 97.6 74.0-126 6.56 20 1,3-Dichloropropane 5.00 4.54 4.63 90.8 92.6 80.0-120 1.96 20 cis-1,3-Dichloropropene 5.00 4.39 4.17 87.8 83.4 80.0-123 5.14 20 trans-1,3-Dichloropropene 5.00 4.37 4.38 87.4 87.6 78.0-124 0.229 20 2,2-Dichloropropane 5.00 5.17 4.36 103 87.2 58.0-130 17.0 20 Di-isopropyl ether 5.00 4.47 4.25 89.4 85.0 58.0-138 5.05 20 Ethylbenzene 5.00 4.77 4.78 95.4 95.6 79.0-123 0.209 20 Hexachloro-1,3-butadiene 5.00 4.90 3.75 98.0 75.0 54.0-138 J3 26.6 20 Isopropylbenzene 5.00 5.07 4.79 101 95.8 76.0-127 5.68 20 p-Isopropyltoluene 5.00 5.22 4.44 104 88.8 76.0-125 16.1 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 41 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 41 of 63 QUALITY CONTROL SUMMARYWG1978145 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-03,04,05,06,07,08 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3874762-1 12/21/22 23:11 • (LCSD) R3874762-2 12/21/22 23:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l %%%%% 2-Butanone (MEK)25.0 26.8 24.8 107 99.2 44.0-160 7.75 20 Methylene Chloride 5.00 4.90 4.96 98.0 99.2 67.0-120 1.22 20 4-Methyl-2-pentanone (MIBK)25.0 25.5 25.2 102 101 68.0-142 1.18 20 Methyl tert-butyl ether 5.00 4.89 4.62 97.8 92.4 68.0-125 5.68 20 Naphthalene 5.00 5.52 4.49 110 89.8 54.0-135 J3 20.6 20 n-Propylbenzene 5.00 5.09 4.62 102 92.4 77.0-124 9.68 20 Styrene 5.00 4.90 4.81 98.0 96.2 73.0-130 1.85 20 1,1,1,2-Tetrachloroethane 5.00 5.03 4.92 101 98.4 75.0-125 2.21 20 1,1,2,2-Tetrachloroethane 5.00 4.62 4.27 92.4 85.4 65.0-130 7.87 20 1,1,2-Trichlorotrifluoroethane 5.00 4.76 5.08 95.2 102 69.0-132 6.50 20 Tetrachloroethene 5.00 4.48 4.44 89.6 88.8 72.0-132 0.897 20 Toluene 5.00 4.53 4.56 90.6 91.2 79.0-120 0.660 20 1,2,3-Trichlorobenzene 5.00 5.42 4.19 108 83.8 50.0-138 J3 25.6 20 1,2,4-Trichlorobenzene 5.00 5.47 4.32 109 86.4 57.0-137 J3 23.5 20 1,1,1-Trichloroethane 5.00 5.30 4.79 106 95.8 73.0-124 10.1 20 1,1,2-Trichloroethane 5.00 4.58 4.76 91.6 95.2 80.0-120 3.85 20 Trichloroethene 5.00 4.67 4.75 93.4 95.0 78.0-124 1.70 20 Trichlorofluoromethane 5.00 6.91 6.97 138 139 59.0-147 0.865 20 1,2,3-Trichloropropane 5.00 5.00 4.88 100 97.6 73.0-130 2.43 20 1,2,4-Trimethylbenzene 5.00 4.94 4.44 98.8 88.8 76.0-121 10.7 20 1,2,3-Trimethylbenzene 5.00 5.01 4.36 100 87.2 77.0-120 13.9 20 1,3,5-Trimethylbenzene 5.00 5.09 4.55 102 91.0 76.0-122 11.2 20 Vinyl chloride 5.00 5.50 5.69 110 114 67.0-131 3.40 20 Xylenes, Total 15.0 14.3 14.3 95.3 95.3 79.0-123 0.000 20 (S) Toluene-d8 99.2 101 80.0-120 (S) 4-Bromofluorobenzene 99.1 100 77.0-126 (S) 1,2-Dichloroethane-d4 103 108 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 42 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 42 of 63 QUALITY CONTROL SUMMARYWG1978665 Volatile Organic Compounds (GC/MS) by Method 8260D L1568172-04,05,06,07 Method Blank (MB) (MB) R3875578-2 12/22/22 11:23 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Benzene U 0.0941 1.00 Ethylbenzene U 0.137 1.00 Toluene U 0.278 1.00 1,2,4-Trimethylbenzene U 0.322 1.00 Xylenes, Total U 0.174 3.00 (S) Toluene-d8 97.5 80.0-120 (S) 4-Bromofluorobenzene 89.6 77.0-126 (S) 1,2-Dichloroethane-d4 122 70.0-130 Laboratory Control Sample (LCS) (LCS) R3875578-1 12/22/22 10:42 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Benzene 5.00 5.22 104 70.0-123 Ethylbenzene 5.00 5.13 103 79.0-123 Toluene 5.00 5.45 109 79.0-120 1,2,4-Trimethylbenzene 5.00 5.53 111 76.0-121 Xylenes, Total 15.0 15.1 101 79.0-123 (S) Toluene-d8 96.8 80.0-120 (S) 4-Bromofluorobenzene 89.8 77.0-126 (S) 1,2-Dichloroethane-d4 104 70.0-130 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 43 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 43 of 63 QUALITY CONTROL SUMMARYWG1974730 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-01 Method Blank (MB) (MB) R3873855-2 12/18/22 12:36 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acenaphthene U 0.0886 1.00 Acenaphthylene U 0.0921 1.00 Anthracene U 0.0804 1.00 Benzidine U 3.74 10.0 Benzo(a)anthracene U 0.199 1.00 Benzo(b)fluoranthene U 0.130 1.00 Benzo(k)fluoranthene U 0.120 1.00 Benzo(g,h,i)perylene U 0.121 1.00 Benzo(a)pyrene U 0.0381 1.00 Bis(2-chlorethoxy)methane U 0.116 10.0 Bis(2-chloroethyl)ether U 0.137 10.0 2,2-oxybis(1-chloropropane)U 0.210 10.0 4-Bromophenyl-phenylether U 0.0877 10.0 2-Chloronaphthalene U 0.0648 1.00 4-Chlorophenyl-phenylether U 0.0926 10.0 Chrysene U 0.130 1.00 Dibenz(a,h)anthracene U 0.0644 1.00 1,2-Dichlorobenzene U 0.0713 10.0 1,3-Dichlorobenzene U 0.132 10.0 1,4-Dichlorobenzene U 0.0942 10.0 3,3-Dichlorobenzidine U 0.212 10.0 2,4-Dinitrotoluene U 0.0983 10.0 2,6-Dinitrotoluene U 0.250 10.0 Fluoranthene U 0.102 1.00 Fluorene U 0.0844 1.00 Hexachlorobenzene U 0.0755 1.00 Hexachloro-1,3-butadiene U 0.0968 10.0 Hexachlorocyclopentadiene U 0.0598 10.0 Hexachloroethane U 0.127 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.143 10.0 Naphthalene U 0.159 1.00 Nitrobenzene U 0.297 10.0 n-Nitrosodimethylamine U 0.998 10.0 n-Nitrosodiphenylamine U 2.37 10.0 n-Nitrosodi-n-propylamine U 0.261 10.0 Phenanthrene U 0.112 1.00 Benzylbutyl phthalate U 0.765 3.00 Bis(2-ethylhexyl)phthalate U 0.895 3.00 Di-n-butyl phthalate U 0.453 3.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 44 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 44 of 63 QUALITY CONTROL SUMMARYWG1974730 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-01 Method Blank (MB) (MB) R3873855-2 12/18/22 12:36 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Diethyl phthalate U 0.287 3.00 Dimethyl phthalate U 0.260 3.00 Di-n-octyl phthalate U 0.932 3.00 Pyrene U 0.107 1.00 1,2,4-Trichlorobenzene U 0.0698 10.0 4-Chloro-3-methylphenol U 0.131 10.0 2-Chlorophenol U 0.133 10.0 2,4-Dichlorophenol U 0.102 10.0 2,4-Dimethylphenol U 0.0636 10.0 4,6-Dinitro-2-methylphenol U 1.12 10.0 2,4-Dinitrophenol U 5.93 10.0 2-Nitrophenol U 0.117 10.0 4-Nitrophenol U 0.143 10.0 Pentachlorophenol U 0.313 10.0 Phenol U 4.33 10.0 2,4,6-Trichlorophenol U 0.100 10.0 (S) 2-Fluorophenol 27.6 10.0-120 (S) Phenol-d5 16.8 10.0-120 (S) Nitrobenzene-d5 61.8 10.0-127 (S) 2-Fluorobiphenyl 52.6 10.0-130 (S) 2,4,6-Tribromophenol 43.0 10.0-155 (S) p-Terphenyl-d14 57.2 10.0-128 Laboratory Control Sample (LCS) (LCS) R3873855-1 12/18/22 12:15 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acenaphthene 50.0 31.3 62.6 41.0-120 Acenaphthylene 50.0 32.0 64.0 43.0-120 Anthracene 50.0 30.9 61.8 45.0-120 Benzidine 100 0.629 0.629 10.0-120 J4 Benzo(a)anthracene 50.0 36.1 72.2 47.0-120 Benzo(b)fluoranthene 50.0 34.7 69.4 46.0-120 Benzo(k)fluoranthene 50.0 33.4 66.8 46.0-120 Benzo(g,h,i)perylene 50.0 35.2 70.4 48.0-121 Benzo(a)pyrene 50.0 37.0 74.0 47.0-120 Bis(2-chlorethoxy)methane 50.0 29.9 59.8 33.0-120 Bis(2-chloroethyl)ether 50.0 29.5 59.0 23.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 45 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 45 of 63 QUALITY CONTROL SUMMARYWG1974730 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-01 Laboratory Control Sample (LCS) (LCS) R3873855-1 12/18/22 12:15 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2,2-oxybis(1-chloropropane)50.0 24.4 48.8 28.0-120 4-Bromophenyl-phenylether 50.0 29.4 58.8 45.0-120 2-Chloronaphthalene 50.0 29.7 59.4 37.0-120 4-Chlorophenyl-phenylether 50.0 29.9 59.8 44.0-120 Chrysene 50.0 35.6 71.2 48.0-120 Dibenz(a,h)anthracene 50.0 34.3 68.6 47.0-120 1,2-Dichlorobenzene 50.0 24.7 49.4 20.0-120 1,3-Dichlorobenzene 50.0 24.3 48.6 17.0-120 1,4-Dichlorobenzene 50.0 24.5 49.0 18.0-120 3,3-Dichlorobenzidine 100 54.5 54.5 44.0-120 2,4-Dinitrotoluene 50.0 35.3 70.6 49.0-124 2,6-Dinitrotoluene 50.0 32.2 64.4 46.0-120 Fluoranthene 50.0 38.3 76.6 51.0-120 Fluorene 50.0 32.2 64.4 47.0-120 Hexachlorobenzene 50.0 25.3 50.6 44.0-120 Hexachloro-1,3-butadiene 50.0 25.0 50.0 19.0-120 Hexachlorocyclopentadiene 50.0 14.1 28.2 15.0-120 Hexachloroethane 50.0 28.0 56.0 15.0-120 Indeno(1,2,3-cd)pyrene 50.0 32.4 64.8 49.0-122 Isophorone 50.0 30.8 61.6 36.0-120 Naphthalene 50.0 25.4 50.8 27.0-120 Nitrobenzene 50.0 31.7 63.4 27.0-120 n-Nitrosodimethylamine 50.0 28.2 56.4 10.0-120 n-Nitrosodiphenylamine 50.0 25.9 51.8 47.0-120 n-Nitrosodi-n-propylamine 50.0 33.2 66.4 31.0-120 Phenanthrene 50.0 33.3 66.6 46.0-120 Benzylbutyl phthalate 50.0 46.7 93.4 43.0-121 Bis(2-ethylhexyl)phthalate 50.0 44.8 89.6 43.0-122 Di-n-butyl phthalate 50.0 41.3 82.6 49.0-121 Diethyl phthalate 50.0 34.5 69.0 48.0-122 Dimethyl phthalate 50.0 31.3 62.6 48.0-120 Di-n-octyl phthalate 50.0 44.3 88.6 42.0-125 Pyrene 50.0 36.4 72.8 47.0-120 1,2,4-Trichlorobenzene 50.0 23.1 46.2 24.0-120 4-Chloro-3-methylphenol 50.0 24.5 49.0 40.0-120 2-Chlorophenol 50.0 19.9 39.8 25.0-120 2,4-Dichlorophenol 50.0 22.3 44.6 36.0-120 2,4-Dimethylphenol 50.0 21.0 42.0 33.0-120 4,6-Dinitro-2-methylphenol 50.0 35.0 70.0 38.0-138 2,4-Dinitrophenol 50.0 28.2 56.4 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 46 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 46 of 63 QUALITY CONTROL SUMMARYWG1974730 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-01 Laboratory Control Sample (LCS) (LCS) R3873855-1 12/18/22 12:15 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2-Nitrophenol 50.0 25.9 51.8 31.0-120 4-Nitrophenol 50.0 85.2 170 10.0-120 J4 Pentachlorophenol 50.0 22.0 44.0 23.0-120 Phenol 50.0 9.75 19.5 10.0-120 2,4,6-Trichlorophenol 50.0 28.0 56.0 42.0-120 (S) 2-Fluorophenol 27.8 10.0-120 (S) Phenol-d5 16.5 10.0-120 (S) Nitrobenzene-d5 62.0 10.0-127 (S) 2-Fluorobiphenyl 55.8 10.0-130 (S) 2,4,6-Tribromophenol 52.0 10.0-155 (S) p-Terphenyl-d14 64.5 10.0-128 L1567902-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567902-01 12/18/22 13:17 • (MS) R3873855-3 12/18/22 13:38 • (MSD) R3873855-4 12/18/22 13:59 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Acenaphthene 50.0 U 34.5 31.3 69.0 62.6 1 28.0-120 9.73 25 Acenaphthylene 50.0 U 36.5 32.4 73.0 64.8 1 31.0-121 11.9 25 Anthracene 50.0 U 33.2 29.5 66.4 59.0 1 36.0-120 11.8 23 Benzidine 100 U U U 0.000 0.000 1 10.0-120 J6 J6 0.000 37 Benzo(a)anthracene 50.0 U 36.8 33.7 73.6 67.4 1 39.0-120 8.79 23 Benzo(b)fluoranthene 50.0 U 36.5 34.5 73.0 69.0 1 37.0-120 5.63 23 Benzo(k)fluoranthene 50.0 U 34.5 32.5 69.0 65.0 1 37.0-120 5.97 26 Benzo(g,h,i)perylene 50.0 U 34.7 32.6 69.4 65.2 1 37.0-123 6.24 25 Benzo(a)pyrene 50.0 U 39.0 37.0 78.0 74.0 1 37.0-120 5.26 24 Bis(2-chlorethoxy)methane 50.0 U 32.5 29.0 65.0 58.0 1 17.0-120 11.4 31 Bis(2-chloroethyl)ether 50.0 U 37.1 29.9 74.2 59.8 1 14.0-120 21.5 33 2,2-oxybis(1-chloropropane)50.0 U 28.9 23.8 57.8 47.6 1 18.0-120 19.4 34 4-Bromophenyl-phenylether 50.0 U 31.2 29.0 62.4 58.0 1 37.0-120 7.31 24 2-Chloronaphthalene 50.0 U 32.4 28.9 64.8 57.8 1 29.0-120 11.4 28 4-Chlorophenyl-phenylether 50.0 U 32.2 28.3 64.4 56.6 1 36.0-120 12.9 23 Chrysene 50.0 U 36.1 33.5 72.2 67.0 1 38.0-120 7.47 23 Dibenz(a,h)anthracene 50.0 U 34.7 33.2 69.4 66.4 1 36.0-121 4.42 24 1,2-Dichlorobenzene 50.0 U 29.1 24.1 58.2 48.2 1 18.0-120 18.8 40 1,3-Dichlorobenzene 50.0 U 28.5 23.8 57.0 47.6 1 15.0-120 18.0 40 1,4-Dichlorobenzene 50.0 U 29.8 23.9 59.6 47.8 1 17.0-120 22.0 40 3,3-Dichlorobenzidine 100 U 42.3 44.0 42.3 44.0 1 10.0-134 3.94 30 2,4-Dinitrotoluene 50.0 U 39.0 34.0 78.0 68.0 1 39.0-125 13.7 25 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 47 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 47 of 63 QUALITY CONTROL SUMMARYWG1974730 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-01 L1567902-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567902-01 12/18/22 13:17 • (MS) R3873855-3 12/18/22 13:38 • (MSD) R3873855-4 12/18/22 13:59 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% 2,6-Dinitrotoluene 50.0 U 35.6 32.4 71.2 64.8 1 36.0-120 9.41 27 Fluoranthene 50.0 U 38.9 36.3 77.8 72.6 1 41.0-121 6.91 22 Fluorene 50.0 U 34.7 30.5 69.4 61.0 1 37.0-120 12.9 24 Hexachlorobenzene 50.0 U 27.7 24.9 55.4 49.8 1 35.0-122 10.6 24 Hexachloro-1,3-butadiene 50.0 U 27.5 24.8 55.0 49.6 1 12.0-120 10.3 34 Hexachlorocyclopentadiene 50.0 U 16.4 16.1 32.8 32.2 1 10.0-120 1.85 33 Hexachloroethane 50.0 U 31.7 26.6 63.4 53.2 1 10.0-120 17.5 40 Indeno(1,2,3-cd)pyrene 50.0 U 32.1 30.7 64.2 61.4 1 38.0-125 4.46 24 Isophorone 50.0 U 33.9 29.7 67.8 59.4 1 21.0-120 13.2 27 Naphthalene 50.0 0.843 28.1 24.8 54.5 47.9 1 10.0-120 12.5 31 Nitrobenzene 50.0 U 35.7 30.9 71.4 61.8 1 12.0-120 14.4 30 n-Nitrosodimethylamine 50.0 U 34.2 31.4 68.4 62.8 1 10.0-120 8.54 40 n-Nitrosodiphenylamine 50.0 U 28.3 25.8 56.6 51.6 1 37.0-120 9.24 24 n-Nitrosodi-n-propylamine 50.0 U 38.2 33.0 76.4 66.0 1 16.0-120 14.6 30 Phenanthrene 50.0 U 36.9 33.2 73.8 66.4 1 33.0-120 10.6 22 Benzylbutyl phthalate 50.0 U 47.7 43.4 95.4 86.8 1 34.0-126 9.44 24 Bis(2-ethylhexyl)phthalate 50.0 U 45.3 42.0 90.6 84.0 1 33.0-126 7.56 25 Di-n-butyl phthalate 50.0 8.71 52.0 47.6 86.6 77.8 1 35.0-128 8.84 23 Diethyl phthalate 50.0 0.795 40.5 35.4 79.4 69.2 1 39.0-125 13.4 24 Dimethyl phthalate 50.0 U 35.8 31.3 71.6 62.6 1 37.0-120 13.4 24 Di-n-octyl phthalate 50.0 U 45.1 42.2 90.2 84.4 1 25.0-135 6.64 26 Pyrene 50.0 U 37.3 34.4 74.6 68.8 1 39.0-120 8.09 22 1,2,4-Trichlorobenzene 50.0 U 25.8 22.1 51.6 44.2 1 15.0-120 15.4 31 4-Chloro-3-methylphenol 50.0 U 28.6 25.2 57.2 50.4 1 26.0-120 12.6 27 2-Chlorophenol 50.0 U 25.8 20.5 51.6 41.0 1 18.0-120 22.9 34 2,4-Dichlorophenol 50.0 U 26.2 22.3 52.4 44.6 1 19.0-120 16.1 27 2,4-Dimethylphenol 50.0 U 21.3 20.0 42.6 40.0 1 15.0-120 6.30 28 4,6-Dinitro-2-methylphenol 50.0 U 37.9 33.8 75.8 67.6 1 10.0-144 11.4 39 2,4-Dinitrophenol 50.0 U 36.9 32.6 73.8 65.2 1 10.0-120 12.4 40 2-Nitrophenol 50.0 U 28.1 26.2 56.2 52.4 1 20.0-120 7.00 30 4-Nitrophenol 50.0 U 96.5 87.5 193 175 1 10.0-120 J5 J5 9.78 40 Pentachlorophenol 50.0 U 26.8 26.0 53.6 52.0 1 10.0-128 3.03 37 Phenol 50.0 U 12.2 10.6 24.4 21.2 1 10.0-120 14.0 40 2,4,6-Trichlorophenol 50.0 U 31.4 28.5 62.8 57.0 1 26.0-120 9.68 31 (S) 2-Fluorophenol 31.4 27.4 10.0-120 (S) Phenol-d5 22.1 17.1 10.0-120 (S) Nitrobenzene-d5 67.3 61.8 10.0-127 (S) 2-Fluorobiphenyl 60.2 57.2 10.0-130 (S) 2,4,6-Tribromophenol 59.5 51.0 10.0-155 (S) p-Terphenyl-d14 57.6 56.3 10.0-128 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 48 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 48 of 63 QUALITY CONTROL SUMMARYWG1975396 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-02,03 Method Blank (MB) (MB) R3873728-2 12/19/22 14:40 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acenaphthene U 0.0886 1.00 Acenaphthylene U 0.0921 1.00 Anthracene U 0.0804 1.00 Benzidine U 3.74 10.0 Benzo(a)anthracene U 0.199 1.00 Benzo(b)fluoranthene U 0.130 1.00 Benzo(k)fluoranthene U 0.120 1.00 Benzo(g,h,i)perylene U 0.121 1.00 Benzo(a)pyrene U 0.0381 1.00 Bis(2-chlorethoxy)methane U 0.116 10.0 Bis(2-chloroethyl)ether U 0.137 10.0 2,2-oxybis(1-chloropropane)U 0.210 10.0 4-Bromophenyl-phenylether U 0.0877 10.0 2-Chloronaphthalene U 0.0648 1.00 4-Chlorophenyl-phenylether U 0.0926 10.0 Chrysene U 0.130 1.00 Dibenz(a,h)anthracene U 0.0644 1.00 1,2-Dichlorobenzene U 0.0713 10.0 1,3-Dichlorobenzene U 0.132 10.0 1,4-Dichlorobenzene U 0.0942 10.0 3,3-Dichlorobenzidine U 0.212 10.0 2,4-Dinitrotoluene U 0.0983 10.0 2,6-Dinitrotoluene U 0.250 10.0 Fluoranthene U 0.102 1.00 Fluorene U 0.0844 1.00 Hexachlorobenzene U 0.0755 1.00 Hexachloro-1,3-butadiene U 0.0968 10.0 Hexachlorocyclopentadiene U 0.0598 10.0 Hexachloroethane U 0.127 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.143 10.0 Naphthalene U 0.159 1.00 Nitrobenzene U 0.297 10.0 n-Nitrosodimethylamine U 0.998 10.0 n-Nitrosodiphenylamine U 2.37 10.0 n-Nitrosodi-n-propylamine U 0.261 10.0 Phenanthrene U 0.112 1.00 Benzylbutyl phthalate U 0.765 3.00 Bis(2-ethylhexyl)phthalate U 0.895 3.00 Di-n-butyl phthalate U 0.453 3.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 49 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 49 of 63 QUALITY CONTROL SUMMARYWG1975396 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-02,03 Method Blank (MB) (MB) R3873728-2 12/19/22 14:40 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Diethyl phthalate U 0.287 3.00 Dimethyl phthalate U 0.260 3.00 Di-n-octyl phthalate U 0.932 3.00 Pyrene U 0.107 1.00 1,2,4-Trichlorobenzene U 0.0698 10.0 4-Chloro-3-methylphenol U 0.131 10.0 2-Chlorophenol U 0.133 10.0 2,4-Dichlorophenol U 0.102 10.0 2,4-Dimethylphenol U 0.0636 10.0 4,6-Dinitro-2-methylphenol U 1.12 10.0 2,4-Dinitrophenol U 5.93 10.0 2-Nitrophenol U 0.117 10.0 4-Nitrophenol U 0.143 10.0 Pentachlorophenol U 0.313 10.0 Phenol U 4.33 10.0 2,4,6-Trichlorophenol U 0.100 10.0 (S) 2-Fluorophenol 19.4 10.0-120 (S) Phenol-d5 14.5 10.0-120 (S) Nitrobenzene-d5 56.3 10.0-127 (S) 2-Fluorobiphenyl 54.0 10.0-130 (S) 2,4,6-Tribromophenol 45.4 10.0-155 (S) p-Terphenyl-d14 71.8 10.0-128 Laboratory Control Sample (LCS) (LCS) R3873728-1 12/19/22 14:18 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acenaphthene 50.0 26.4 52.8 41.0-120 Acenaphthylene 50.0 28.6 57.2 43.0-120 Anthracene 50.0 28.0 56.0 45.0-120 Benzidine 100 4.48 4.48 10.0-120 J4 Benzo(a)anthracene 50.0 34.0 68.0 47.0-120 Benzo(b)fluoranthene 50.0 33.2 66.4 46.0-120 Benzo(k)fluoranthene 50.0 33.7 67.4 46.0-120 Benzo(g,h,i)perylene 50.0 29.6 59.2 48.0-121 Benzo(a)pyrene 50.0 36.2 72.4 47.0-120 Bis(2-chlorethoxy)methane 50.0 29.1 58.2 33.0-120 Bis(2-chloroethyl)ether 50.0 23.8 47.6 23.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 50 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 50 of 63 QUALITY CONTROL SUMMARYWG1975396 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-02,03 Laboratory Control Sample (LCS) (LCS) R3873728-1 12/19/22 14:18 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2,2-oxybis(1-chloropropane)50.0 20.9 41.8 28.0-120 4-Bromophenyl-phenylether 50.0 30.0 60.0 45.0-120 2-Chloronaphthalene 50.0 26.0 52.0 37.0-120 4-Chlorophenyl-phenylether 50.0 31.3 62.6 44.0-120 Chrysene 50.0 34.1 68.2 48.0-120 Dibenz(a,h)anthracene 50.0 31.0 62.0 47.0-120 1,2-Dichlorobenzene 50.0 21.2 42.4 20.0-120 1,3-Dichlorobenzene 50.0 20.3 40.6 17.0-120 1,4-Dichlorobenzene 50.0 20.7 41.4 18.0-120 3,3-Dichlorobenzidine 100 46.6 46.6 44.0-120 2,4-Dinitrotoluene 50.0 35.3 70.6 49.0-124 2,6-Dinitrotoluene 50.0 32.4 64.8 46.0-120 Fluoranthene 50.0 33.2 66.4 51.0-120 Fluorene 50.0 29.0 58.0 47.0-120 Hexachlorobenzene 50.0 27.7 55.4 44.0-120 Hexachloro-1,3-butadiene 50.0 28.9 57.8 19.0-120 Hexachlorocyclopentadiene 50.0 18.3 36.6 15.0-120 Hexachloroethane 50.0 22.5 45.0 15.0-120 Indeno(1,2,3-cd)pyrene 50.0 29.0 58.0 49.0-122 Isophorone 50.0 30.6 61.2 36.0-120 Naphthalene 50.0 21.3 42.6 27.0-120 Nitrobenzene 50.0 28.5 57.0 27.0-120 n-Nitrosodimethylamine 50.0 15.9 31.8 10.0-120 n-Nitrosodiphenylamine 50.0 23.4 46.8 47.0-120 J4 n-Nitrosodi-n-propylamine 50.0 28.6 57.2 31.0-120 Phenanthrene 50.0 28.5 57.0 46.0-120 Benzylbutyl phthalate 50.0 37.8 75.6 43.0-121 Bis(2-ethylhexyl)phthalate 50.0 37.4 74.8 43.0-122 Di-n-butyl phthalate 50.0 36.7 73.4 49.0-121 Diethyl phthalate 50.0 35.3 70.6 48.0-122 Dimethyl phthalate 50.0 32.8 65.6 48.0-120 Di-n-octyl phthalate 50.0 37.2 74.4 42.0-125 Pyrene 50.0 35.4 70.8 47.0-120 1,2,4-Trichlorobenzene 50.0 28.0 56.0 24.0-120 4-Chloro-3-methylphenol 50.0 29.1 58.2 40.0-120 2-Chlorophenol 50.0 18.1 36.2 25.0-120 2,4-Dichlorophenol 50.0 28.8 57.6 36.0-120 2,4-Dimethylphenol 50.0 17.1 34.2 33.0-120 4,6-Dinitro-2-methylphenol 50.0 34.0 68.0 38.0-138 2,4-Dinitrophenol 50.0 28.1 56.2 10.0-120 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 51 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 51 of 63 QUALITY CONTROL SUMMARYWG1975396 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-02,03 Laboratory Control Sample (LCS) (LCS) R3873728-1 12/19/22 14:18 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2-Nitrophenol 50.0 26.7 53.4 31.0-120 4-Nitrophenol 50.0 12.0 24.0 10.0-120 Pentachlorophenol 50.0 23.2 46.4 23.0-120 Phenol 50.0 10.1 20.2 10.0-120 2,4,6-Trichlorophenol 50.0 29.1 58.2 42.0-120 (S) 2-Fluorophenol 26.2 10.0-120 (S) Phenol-d5 19.1 10.0-120 (S) Nitrobenzene-d5 59.4 10.0-127 (S) 2-Fluorobiphenyl 56.0 10.0-130 (S) 2,4,6-Tribromophenol 65.5 10.0-155 (S) p-Terphenyl-d14 71.4 10.0-128 L1567889-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567889-01 12/20/22 15:08 • (MS) R3874009-1 12/20/22 15:29 • (MSD) R3874009-2 12/20/22 15:50 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Acenaphthene 50.0 U 28.2 30.6 56.4 61.2 1 28.0-120 8.16 25 Acenaphthylene 50.0 U 29.5 32.2 59.0 64.4 1 31.0-121 8.75 25 Anthracene 50.0 U 30.6 30.0 61.2 60.0 1 36.0-120 1.98 23 Benzidine 100 U 7.41 U 7.41 0.000 1 10.0-120 J6 J3 J6 200 37 Benzo(a)anthracene 50.0 U 33.5 32.5 67.0 65.0 1 39.0-120 3.03 23 Benzo(b)fluoranthene 50.0 U 36.3 34.3 72.6 68.6 1 37.0-120 5.67 23 Benzo(k)fluoranthene 50.0 U 36.5 34.5 73.0 69.0 1 37.0-120 5.63 26 Benzo(g,h,i)perylene 50.0 U 27.5 26.6 55.0 53.2 1 37.0-123 3.33 25 Benzo(a)pyrene 50.0 U 33.3 31.8 66.6 63.6 1 37.0-120 4.61 24 Bis(2-chlorethoxy)methane 50.0 U 22.3 24.9 44.6 49.8 1 17.0-120 11.0 31 Bis(2-chloroethyl)ether 50.0 U 22.7 24.1 45.4 48.2 1 14.0-120 5.98 33 2,2-oxybis(1-chloropropane)50.0 U 21.7 23.1 43.4 46.2 1 18.0-120 6.25 34 4-Bromophenyl-phenylether 50.0 U 33.2 33.8 66.4 67.6 1 37.0-120 1.79 24 2-Chloronaphthalene 50.0 U 24.9 27.9 49.8 55.8 1 29.0-120 11.4 28 4-Chlorophenyl-phenylether 50.0 U 29.4 30.6 58.8 61.2 1 36.0-120 4.00 23 Chrysene 50.0 U 33.4 32.8 66.8 65.6 1 38.0-120 1.81 23 Dibenz(a,h)anthracene 50.0 U 25.7 25.2 51.4 50.4 1 36.0-121 1.96 24 1,2-Dichlorobenzene 50.0 U 21.0 21.8 42.0 43.6 1 18.0-120 3.74 40 1,3-Dichlorobenzene 50.0 U 20.6 20.9 41.2 41.8 1 15.0-120 1.45 40 1,4-Dichlorobenzene 50.0 U 20.7 21.1 41.4 42.2 1 17.0-120 1.91 40 3,3-Dichlorobenzidine 100 U 10.4 6.52 10.4 6.52 1 10.0-134 J3 J6 45.9 30 2,4-Dinitrotoluene 50.0 U 35.5 37.2 71.0 74.4 1 39.0-125 4.68 25 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 52 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 52 of 63 QUALITY CONTROL SUMMARYWG1975396 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-02,03 L1567889-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1567889-01 12/20/22 15:08 • (MS) R3874009-1 12/20/22 15:29 • (MSD) R3874009-2 12/20/22 15:50 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% 2,6-Dinitrotoluene 50.0 U 33.0 36.1 66.0 72.2 1 36.0-120 8.97 27 Fluoranthene 50.0 U 33.0 32.3 66.0 64.6 1 41.0-121 2.14 22 Fluorene 50.0 U 30.3 32.1 60.6 64.2 1 37.0-120 5.77 24 Hexachlorobenzene 50.0 U 28.7 28.5 57.4 57.0 1 35.0-122 0.699 24 Hexachloro-1,3-butadiene 50.0 U 19.3 19.3 38.6 38.6 1 12.0-120 0.000 34 Hexachlorocyclopentadiene 50.0 U 12.2 13.8 24.4 27.6 1 10.0-120 12.3 33 Hexachloroethane 50.0 U 19.9 19.9 39.8 39.8 1 10.0-120 0.000 40 Indeno(1,2,3-cd)pyrene 50.0 U 24.3 23.0 48.6 46.0 1 38.0-125 5.50 24 Isophorone 50.0 U 22.8 25.5 45.6 51.0 1 21.0-120 11.2 27 Naphthalene 50.0 U 20.6 21.8 41.2 43.6 1 10.0-120 5.66 31 Nitrobenzene 50.0 U 25.8 26.5 51.6 53.0 1 12.0-120 2.68 30 n-Nitrosodimethylamine 50.0 U 12.1 13.2 24.2 26.4 1 10.0-120 8.70 40 n-Nitrosodiphenylamine 50.0 U 29.8 30.4 59.6 60.8 1 37.0-120 1.99 24 n-Nitrosodi-n-propylamine 50.0 U 23.3 26.7 46.6 53.4 1 16.0-120 13.6 30 Phenanthrene 50.0 U 32.2 32.3 64.4 64.6 1 33.0-120 0.310 22 Benzylbutyl phthalate 50.0 U 43.5 42.2 87.0 84.4 1 34.0-126 3.03 24 Bis(2-ethylhexyl)phthalate 50.0 U 41.3 39.5 82.6 79.0 1 33.0-126 4.46 25 Di-n-butyl phthalate 50.0 U 39.2 38.9 78.4 77.8 1 35.0-128 0.768 23 Diethyl phthalate 50.0 U 35.5 36.5 71.0 73.0 1 39.0-125 2.78 24 Dimethyl phthalate 50.0 U 33.3 35.1 66.6 70.2 1 37.0-120 5.26 24 Di-n-octyl phthalate 50.0 U 40.9 38.6 81.8 77.2 1 25.0-135 5.79 26 Pyrene 50.0 U 39.5 38.5 79.0 77.0 1 39.0-120 2.56 22 1,2,4-Trichlorobenzene 50.0 U 19.8 20.4 39.6 40.8 1 15.0-120 2.99 31 4-Chloro-3-methylphenol 50.0 U 22.9 21.6 45.8 43.2 1 26.0-120 5.84 27 2-Chlorophenol 50.0 U 17.5 15.5 35.0 31.0 1 18.0-120 12.1 34 2,4-Dichlorophenol 50.0 U 18.9 18.2 37.8 36.4 1 19.0-120 3.77 27 2,4-Dimethylphenol 50.0 U 11.0 16.8 22.0 33.6 1 15.0-120 J3 41.7 28 4,6-Dinitro-2-methylphenol 50.0 U 37.5 35.5 75.0 71.0 1 10.0-144 5.48 39 2,4-Dinitrophenol 50.0 U 34.4 33.1 68.8 66.2 1 10.0-120 3.85 40 2-Nitrophenol 50.0 U 22.6 22.1 45.2 44.2 1 20.0-120 2.24 30 4-Nitrophenol 50.0 U 12.8 12.4 25.6 24.8 1 10.0-120 3.17 40 Pentachlorophenol 50.0 U 24.8 22.9 49.6 45.8 1 10.0-128 7.97 37 Phenol 50.0 U 8.34 8.76 16.7 17.5 1 10.0-120 4.91 40 2,4,6-Trichlorophenol 50.0 U 24.6 24.7 49.2 49.4 1 26.0-120 0.406 31 (S) 2-Fluorophenol 24.2 22.2 10.0-120 (S) Phenol-d5 16.9 17.0 10.0-120 (S) Nitrobenzene-d5 42.3 44.8 10.0-127 (S) 2-Fluorobiphenyl 52.9 58.6 10.0-130 (S) 2,4,6-Tribromophenol 55.5 53.5 10.0-155 (S) p-Terphenyl-d14 80.7 77.2 10.0-128 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 53 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 53 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 Method Blank (MB) (MB) R3873595-2 12/18/22 15:37 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acenaphthene U 0.0886 1.00 Acenaphthylene U 0.0921 1.00 Anthracene U 0.0804 1.00 Benzidine U 3.74 10.0 Benzo(a)anthracene U 0.199 1.00 Benzo(b)fluoranthene U 0.130 1.00 Benzo(k)fluoranthene U 0.120 1.00 Benzo(g,h,i)perylene U 0.121 1.00 Benzo(a)pyrene U 0.0381 1.00 Bis(2-chlorethoxy)methane U 0.116 10.0 Bis(2-chloroethyl)ether U 0.137 10.0 2,2-oxybis(1-chloropropane)U 0.210 10.0 4-Bromophenyl-phenylether U 0.0877 10.0 2-Chloronaphthalene U 0.0648 1.00 4-Chlorophenyl-phenylether U 0.0926 10.0 Chrysene U 0.130 1.00 Dibenz(a,h)anthracene U 0.0644 1.00 1,2-Dichlorobenzene U 0.0713 10.0 1,3-Dichlorobenzene U 0.132 10.0 1,4-Dichlorobenzene U 0.0942 10.0 3,3-Dichlorobenzidine U 0.212 10.0 2,4-Dinitrotoluene U 0.0983 10.0 2,6-Dinitrotoluene U 0.250 10.0 Fluoranthene U 0.102 1.00 Fluorene U 0.0844 1.00 Hexachlorobenzene U 0.0755 1.00 Hexachloro-1,3-butadiene U 0.0968 10.0 Hexachlorocyclopentadiene U 0.0598 10.0 Hexachloroethane U 0.127 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.143 10.0 Naphthalene U 0.159 1.00 Nitrobenzene U 0.297 10.0 n-Nitrosodimethylamine U 0.998 10.0 n-Nitrosodiphenylamine U 2.37 10.0 n-Nitrosodi-n-propylamine U 0.261 10.0 Phenanthrene U 0.112 1.00 Benzylbutyl phthalate U 0.765 3.00 Bis(2-ethylhexyl)phthalate U 0.895 3.00 Di-n-butyl phthalate U 0.453 3.00 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 54 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 54 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 Method Blank (MB) (MB) R3873595-2 12/18/22 15:37 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Diethyl phthalate U 0.287 3.00 Dimethyl phthalate U 0.260 3.00 Di-n-octyl phthalate U 0.932 3.00 Pyrene U 0.107 1.00 1,2,4-Trichlorobenzene U 0.0698 10.0 4-Chloro-3-methylphenol U 0.131 10.0 2-Chlorophenol U 0.133 10.0 2,4-Dichlorophenol U 0.102 10.0 2,4-Dimethylphenol U 0.0636 10.0 4,6-Dinitro-2-methylphenol U 1.12 10.0 2,4-Dinitrophenol U 5.93 10.0 2-Nitrophenol U 0.117 10.0 4-Nitrophenol U 0.143 10.0 Pentachlorophenol U 0.313 10.0 Phenol U 4.33 10.0 2,4,6-Trichlorophenol U 0.100 10.0 (S) 2-Fluorophenol 34.7 10.0-120 (S) Phenol-d5 20.7 10.0-120 (S) Nitrobenzene-d5 63.6 10.0-127 (S) 2-Fluorobiphenyl 71.2 10.0-130 (S) 2,4,6-Tribromophenol 75.0 10.0-155 (S) p-Terphenyl-d14 86.5 10.0-128 Method Blank (MB) (MB) R3874301-1 12/20/22 16:06 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l Acenaphthene U 0.0886 1.00 Acenaphthylene U 0.0921 1.00 Anthracene U 0.0804 1.00 Benzidine U 3.74 10.0 Benzo(a)anthracene U 0.199 1.00 Benzo(b)fluoranthene U 0.130 1.00 Benzo(k)fluoranthene U 0.120 1.00 Benzo(g,h,i)perylene U 0.121 1.00 Benzo(a)pyrene U 0.0381 1.00 Bis(2-chlorethoxy)methane U 0.116 10.0 Bis(2-chloroethyl)ether U 0.137 10.0 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 55 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 55 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 Method Blank (MB) (MB) R3874301-1 12/20/22 16:06 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l 2,2-oxybis(1-chloropropane)U 0.210 10.0 4-Bromophenyl-phenylether U 0.0877 10.0 2-Chloronaphthalene U 0.0648 1.00 4-Chlorophenyl-phenylether U 0.0926 10.0 Chrysene U 0.130 1.00 Dibenz(a,h)anthracene U 0.0644 1.00 1,2-Dichlorobenzene U 0.0713 10.0 1,3-Dichlorobenzene U 0.132 10.0 1,4-Dichlorobenzene U 0.0942 10.0 3,3-Dichlorobenzidine U 0.212 10.0 2,4-Dinitrotoluene U 0.0983 10.0 2,6-Dinitrotoluene U 0.250 10.0 Fluoranthene U 0.102 1.00 Fluorene U 0.0844 1.00 Hexachlorobenzene U 0.0755 1.00 Hexachloro-1,3-butadiene U 0.0968 10.0 Hexachlorocyclopentadiene U 0.0598 10.0 Hexachloroethane U 0.127 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.143 10.0 Naphthalene U 0.159 1.00 Nitrobenzene U 0.297 10.0 n-Nitrosodimethylamine U 0.998 10.0 n-Nitrosodiphenylamine U 2.37 10.0 n-Nitrosodi-n-propylamine U 0.261 10.0 Phenanthrene U 0.112 1.00 Benzylbutyl phthalate U 0.765 3.00 Bis(2-ethylhexyl)phthalate U 0.895 3.00 Di-n-butyl phthalate U 0.453 3.00 Diethyl phthalate U 0.287 3.00 Dimethyl phthalate U 0.260 3.00 Di-n-octyl phthalate U 0.932 3.00 Pyrene U 0.107 1.00 1,2,4-Trichlorobenzene U 0.0698 10.0 4-Chloro-3-methylphenol U 0.131 10.0 2-Chlorophenol U 0.133 10.0 2,4-Dichlorophenol U 0.102 10.0 2,4-Dimethylphenol U 0.0636 10.0 4,6-Dinitro-2-methylphenol U 1.12 10.0 2,4-Dinitrophenol U 5.93 10.0 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 56 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 56 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 Method Blank (MB) (MB) R3874301-1 12/20/22 16:06 MB Result MB Qualifier MB MDL MB RDL Analyte ug/l ug/l ug/l 2-Nitrophenol U 0.117 10.0 4-Nitrophenol U 0.143 10.0 Pentachlorophenol U 0.313 10.0 Phenol U 4.33 10.0 2,4,6-Trichlorophenol U 0.100 10.0 (S) 2-Fluorophenol 26.3 10.0-120 (S) Phenol-d5 17.5 10.0-120 (S) Nitrobenzene-d5 50.9 10.0-127 (S) 2-Fluorobiphenyl 74.5 10.0-130 (S) 2,4,6-Tribromophenol 94.0 10.0-155 (S) p-Terphenyl-d14 84.9 10.0-128 Laboratory Control Sample (LCS) (LCS) R3873595-1 12/18/22 15:16 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% Acenaphthene 50.0 47.4 94.8 41.0-120 Acenaphthylene 50.0 50.4 101 43.0-120 Anthracene 50.0 46.3 92.6 45.0-120 Benzidine 100 0.117 0.117 10.0-120 J4 Benzo(a)anthracene 50.0 48.6 97.2 47.0-120 Benzo(b)fluoranthene 50.0 50.1 100 46.0-120 Benzo(k)fluoranthene 50.0 48.6 97.2 46.0-120 Benzo(g,h,i)perylene 50.0 48.5 97.0 48.0-121 Benzo(a)pyrene 50.0 49.7 99.4 47.0-120 Bis(2-chlorethoxy)methane 50.0 38.1 76.2 33.0-120 Bis(2-chloroethyl)ether 50.0 39.6 79.2 23.0-120 2,2-oxybis(1-chloropropane)50.0 38.5 77.0 28.0-120 4-Bromophenyl-phenylether 50.0 50.8 102 45.0-120 2-Chloronaphthalene 50.0 45.7 91.4 37.0-120 4-Chlorophenyl-phenylether 50.0 45.4 90.8 44.0-120 Chrysene 50.0 48.3 96.6 48.0-120 Dibenz(a,h)anthracene 50.0 48.2 96.4 47.0-120 1,2-Dichlorobenzene 50.0 38.5 77.0 20.0-120 1,3-Dichlorobenzene 50.0 38.0 76.0 17.0-120 1,4-Dichlorobenzene 50.0 38.2 76.4 18.0-120 3,3-Dichlorobenzidine 100 70.2 70.2 44.0-120 2,4-Dinitrotoluene 50.0 51.1 102 49.0-124 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 57 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 57 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 Laboratory Control Sample (LCS) (LCS) R3873595-1 12/18/22 15:16 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte ug/l ug/l %% 2,6-Dinitrotoluene 50.0 49.5 99.0 46.0-120 Fluoranthene 50.0 48.0 96.0 51.0-120 Fluorene 50.0 47.2 94.4 47.0-120 Hexachlorobenzene 50.0 45.0 90.0 44.0-120 Hexachloro-1,3-butadiene 50.0 34.2 68.4 19.0-120 Hexachlorocyclopentadiene 50.0 32.7 65.4 15.0-120 Hexachloroethane 50.0 38.0 76.0 15.0-120 Indeno(1,2,3-cd)pyrene 50.0 44.4 88.8 49.0-122 Isophorone 50.0 38.1 76.2 36.0-120 Naphthalene 50.0 36.2 72.4 27.0-120 Nitrobenzene 50.0 37.2 74.4 27.0-120 n-Nitrosodimethylamine 50.0 15.7 31.4 10.0-120 n-Nitrosodiphenylamine 50.0 41.6 83.2 47.0-120 n-Nitrosodi-n-propylamine 50.0 41.4 82.8 31.0-120 Phenanthrene 50.0 47.7 95.4 46.0-120 Benzylbutyl phthalate 50.0 56.4 113 43.0-121 Bis(2-ethylhexyl)phthalate 50.0 54.9 110 43.0-122 Di-n-butyl phthalate 50.0 53.6 107 49.0-121 Diethyl phthalate 50.0 49.9 99.8 48.0-122 Dimethyl phthalate 50.0 49.3 98.6 48.0-120 Di-n-octyl phthalate 50.0 54.8 110 42.0-125 Pyrene 50.0 52.6 105 47.0-120 1,2,4-Trichlorobenzene 50.0 35.8 71.6 24.0-120 4-Chloro-3-methylphenol 50.0 39.3 78.6 40.0-120 2-Chlorophenol 50.0 34.6 69.2 25.0-120 2,4-Dichlorophenol 50.0 38.3 76.6 36.0-120 2,4-Dimethylphenol 50.0 31.3 62.6 33.0-120 4,6-Dinitro-2-methylphenol 50.0 63.2 126 38.0-138 2,4-Dinitrophenol 50.0 56.0 112 10.0-120 2-Nitrophenol 50.0 43.5 87.0 31.0-120 4-Nitrophenol 50.0 15.5 31.0 10.0-120 Pentachlorophenol 50.0 40.3 80.6 23.0-120 Phenol 50.0 12.6 25.2 10.0-120 2,4,6-Trichlorophenol 50.0 48.6 97.2 42.0-120 (S) 2-Fluorophenol 39.7 10.0-120 (S) Phenol-d5 24.0 10.0-120 (S) Nitrobenzene-d5 67.8 10.0-127 (S) 2-Fluorobiphenyl 89.3 10.0-130 (S) 2,4,6-Tribromophenol 103 10.0-155 (S) p-Terphenyl-d14 99.0 10.0-128 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 58 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 58 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 L1568465-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1568465-01 12/19/22 00:20 • (MS) R3873595-3 12/19/22 00:41 • (MSD) R3873595-4 12/19/22 01:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Acenaphthene 50.0 U 39.2 37.9 78.4 75.8 1 28.0-120 3.37 25 Acenaphthylene 50.0 U 41.5 40.6 83.0 81.2 1 31.0-121 2.19 25 Anthracene 50.0 U 37.0 36.3 74.0 72.6 1 36.0-120 1.91 23 Benzidine 100 U U U 0.000 0.000 1 10.0-120 J6 J6 0.000 37 Benzo(a)anthracene 50.0 U 38.4 38.4 76.8 76.8 1 39.0-120 0.000 23 Benzo(b)fluoranthene 50.0 U 40.1 40.1 80.2 80.2 1 37.0-120 0.000 23 Benzo(k)fluoranthene 50.0 U 38.8 38.8 77.6 77.6 1 37.0-120 0.000 26 Benzo(g,h,i)perylene 50.0 U 34.1 34.4 68.2 68.8 1 37.0-123 0.876 25 Benzo(a)pyrene 50.0 U 39.2 39.6 78.4 79.2 1 37.0-120 1.02 24 Bis(2-chlorethoxy)methane 50.0 U 31.8 30.9 63.6 61.8 1 17.0-120 2.87 31 Bis(2-chloroethyl)ether 50.0 U 32.7 29.8 65.4 59.6 1 14.0-120 9.28 33 2,2-oxybis(1-chloropropane)50.0 U 33.5 31.2 67.0 62.4 1 18.0-120 7.11 34 4-Bromophenyl-phenylether 50.0 U 40.5 40.1 81.0 80.2 1 37.0-120 0.993 24 2-Chloronaphthalene 50.0 U 37.5 36.5 75.0 73.0 1 29.0-120 2.70 28 4-Chlorophenyl-phenylether 50.0 U 37.1 36.9 74.2 73.8 1 36.0-120 0.541 23 Chrysene 50.0 U 37.8 38.2 75.6 76.4 1 38.0-120 1.05 23 Dibenz(a,h)anthracene 50.0 U 35.7 36.7 71.4 73.4 1 36.0-121 2.76 24 1,2-Dichlorobenzene 50.0 U 33.0 31.1 66.0 62.2 1 18.0-120 5.93 40 1,3-Dichlorobenzene 50.0 U 32.7 30.6 65.4 61.2 1 15.0-120 6.64 40 1,4-Dichlorobenzene 50.0 U 32.6 31.1 65.2 62.2 1 17.0-120 4.71 40 3,3-Dichlorobenzidine 100 U 29.8 27.8 29.8 27.8 1 10.0-134 6.94 30 2,4-Dinitrotoluene 50.0 U 41.9 43.3 83.8 86.6 1 39.0-125 3.29 25 2,6-Dinitrotoluene 50.0 U 39.8 40.2 79.6 80.4 1 36.0-120 1.00 27 Fluoranthene 50.0 U 38.4 38.7 76.8 77.4 1 41.0-121 0.778 22 Fluorene 50.0 U 38.5 38.7 77.0 77.4 1 37.0-120 0.518 24 Hexachlorobenzene 50.0 U 35.8 35.1 71.6 70.2 1 35.0-122 1.97 24 Hexachloro-1,3-butadiene 50.0 U 30.4 29.3 60.8 58.6 1 12.0-120 3.69 34 Hexachlorocyclopentadiene 50.0 U 27.3 27.2 54.6 54.4 1 10.0-120 0.367 33 Hexachloroethane 50.0 U 31.8 30.9 63.6 61.8 1 10.0-120 2.87 40 Indeno(1,2,3-cd)pyrene 50.0 U 32.6 33.1 65.2 66.2 1 38.0-125 1.52 24 Isophorone 50.0 U 31.7 30.6 63.4 61.2 1 21.0-120 3.53 27 Naphthalene 50.0 U 31.0 29.6 62.0 59.2 1 10.0-120 4.62 31 Nitrobenzene 50.0 U 32.3 30.5 64.6 61.0 1 12.0-120 5.73 30 n-Nitrosodimethylamine 50.0 U 13.5 13.2 27.0 26.4 1 10.0-120 2.25 40 n-Nitrosodiphenylamine 50.0 U 34.5 34.3 69.0 68.6 1 37.0-120 0.581 24 n-Nitrosodi-n-propylamine 50.0 U 35.5 33.5 71.0 67.0 1 16.0-120 5.80 30 Phenanthrene 50.0 U 37.6 37.6 75.2 75.2 1 33.0-120 0.000 22 Benzylbutyl phthalate 50.0 U 45.7 46.2 91.4 92.4 1 34.0-126 1.09 24 Bis(2-ethylhexyl)phthalate 50.0 U 44.5 44.6 89.0 89.2 1 33.0-126 0.224 25 Di-n-butyl phthalate 50.0 U 43.8 43.7 87.6 87.4 1 35.0-128 0.229 23 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 59 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 59 of 63 QUALITY CONTROL SUMMARYWG1975661 Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1568172-04,05,06,07 L1568465-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1568465-01 12/19/22 00:20 • (MS) R3873595-3 12/19/22 00:41 • (MSD) R3873595-4 12/19/22 01:02 Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/l ug/l ug/l ug/l %%%%% Diethyl phthalate 50.0 U 40.3 40.7 80.6 81.4 1 39.0-125 0.988 24 Dimethyl phthalate 50.0 U 40.1 40.1 80.2 80.2 1 37.0-120 0.000 24 Di-n-octyl phthalate 50.0 U 45.2 45.4 90.4 90.8 1 25.0-135 0.442 26 Pyrene 50.0 U 42.2 41.7 84.4 83.4 1 39.0-120 1.19 22 1,2,4-Trichlorobenzene 50.0 U 30.3 29.3 60.6 58.6 1 15.0-120 3.36 31 4-Chloro-3-methylphenol 50.0 U 31.9 30.6 63.8 61.2 1 26.0-120 4.16 27 2-Chlorophenol 50.0 U 29.1 25.7 58.2 51.4 1 18.0-120 12.4 34 2,4-Dichlorophenol 50.0 U 31.0 28.4 62.0 56.8 1 19.0-120 8.75 27 2,4-Dimethylphenol 50.0 U 29.0 27.0 58.0 54.0 1 15.0-120 7.14 28 4,6-Dinitro-2-methylphenol 50.0 U 48.4 47.2 96.8 94.4 1 10.0-144 2.51 39 2,4-Dinitrophenol 50.0 U 47.5 46.9 95.0 93.8 1 10.0-120 1.27 40 2-Nitrophenol 50.0 U 35.4 32.2 70.8 64.4 1 20.0-120 9.47 30 4-Nitrophenol 50.0 U 13.9 13.5 27.8 27.0 1 10.0-120 2.92 40 Pentachlorophenol 50.0 U 38.5 36.7 77.0 73.4 1 10.0-128 4.79 37 Phenol 50.0 U 11.4 10.5 22.8 21.0 1 10.0-120 8.22 40 2,4,6-Trichlorophenol 50.0 U 38.7 36.5 77.4 73.0 1 26.0-120 5.85 31 (S) 2-Fluorophenol 32.7 30.2 10.0-120 (S) Phenol-d5 21.3 20.3 10.0-120 (S) Nitrobenzene-d5 60.5 56.5 10.0-127 (S) 2-Fluorobiphenyl 74.1 72.3 10.0-130 (S) 2,4,6-Tribromophenol 80.5 76.5 10.0-155 (S) p-Terphenyl-d14 81.4 82.3 10.0-128 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 60 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 60 of 63 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. RDL Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry)Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptable. J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 61 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 61 of 63 Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey–NELAP TN002 California 2932 New Mexico ¹TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina ¹DW21704 Georgia NELAP North Carolina ³41 Georgia ¹923 North Dakota R-140 Idaho TN00003 Ohio–VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LAO00356 Kentucky ¹ ⁶KY90010 South Carolina 84004002 Kentucky ²16 South Dakota n/a Louisiana AI30792 Tennessee ¹ ⁴2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas ⁵LAB0152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA – ISO 17025 ⁵1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA–Crypto TN00003 ACCREDITATIONS & LOCATIONS ¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable * Not all certifications held by the laboratory are applicable to the results reported in the attached report. * Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 11:25 62 of 63 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: EAS Professionals, Inc.22-5234 L1568172 12/27/22 12:35 62 of 63 27 February 2023 Enclosed is the analytical report for the above referenced project. The data herein applies to samples as received by H&P Mobile Geochemistry, Inc. on 28-Dec-22 which were analyzed in accordance with the attached Chain of Custody record(s). The results for all sample analyses and required QA/QC analyses are presented in the following sections and summarized in the documents: •Sample Summary •Case Narrative (if applicable) •Sample Results •Quality Control Summary •Notes and Definitions / Appendix •Chain of Custody •Sampling Logs (if applicable) Unless otherwise noted, I certify that all analyses were performed and reviewed in compliance with our Quality Systems Manual and Standard Operating Procedures. This report shall not be reproduced, except in full, without the written approval of H&P Mobile Geochemistry, Inc. We at H&P Mobile Geochemistry, Inc. sincerely appreciate the opportunity to provide analytical services to you on this project. If you have any questions or concerns regarding this analytical report, please contact me at your convenience at 760-804-9678. Sincerely, Client Project: 450 Polo Rd Property H&P Project: MC122822-10 Rev3 North Charleston, SC 29406 2145 N. Center St. Suite B-205 EAS Professionals Derek Ross Laboratory Director Lisa Eminhizer Dear Derek Ross: Quality. Accuracy. Experience.2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CA P 1.800.834.9888 / 760.804.9678 F 760.804.9159 W handpmg.com MobileGeochemistry Inc. H&P Mobile Geochemistry, Inc. is certified under the California ELAP and the National Environmental Laboratory Accreditation Conference (NELAC) for the fields of proficiency and analytes listed on those certificates. H&P is approved as an Environmental Testing Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs for the fields of proficiency and analytes included in the certification process and to the extent offered by the accreditation agency. Unless otherwise noted, accreditation certificate numbers, expiration of certificates, and scope of accreditation can be found at: www.handpmg.com/about/certifications. Fields of services and analytes contained in this report that are not listed on the certificates should be considered uncertified or unavailable for certification. Page 1 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Sample ID Laboratory ID Matrix Date Sampled ANALYTICAL REPORT FOR SAMPLES Date Received S6-5 E301006-01 Vapor 21-Dec-22 28-Dec-22 S6-6 E301006-02 Vapor 21-Dec-22 28-Dec-22 S6-4 E301006-03 Vapor 21-Dec-22 28-Dec-22 S6-3 E301006-04 Vapor 21-Dec-22 28-Dec-22 S6-2 E301006-05 Vapor 21-Dec-22 28-Dec-22 S6-9 E301006-06 Vapor 21-Dec-22 28-Dec-22 S6-1 E301006-07 Vapor 21-Dec-22 28-Dec-22 S6-7 E301006-09 Vapor 21-Dec-22 28-Dec-22 S6-Duplicate E301006-10 Vapor 21-Dec-22 28-Dec-22 S6-8 E301006-11 Vapor 21-Dec-22 28-Dec-22 February 27, 2023 This final has been revised to correct results. Page 2 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-5 (E301006-01) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.11.5 """""Dichlorodifluoromethane (F12)J"4.00.41.6 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """"""Trichlorofluoromethane (F11)2.3ND0.2 """"""Acetone 4.8ND0.5 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.6 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """"""Chloroform 1.0ND0.2 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.2 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.31.9 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 Page 3 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-5 (E301006-01) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.27.8 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.337 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.3 """""m,p-Xylene J"1.80.21.3 """"""Styrene 1.7ND0.2 """""o-Xylene J"1.80.20.7 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """""4-Ethyltoluene J"2.00.20.3 """""1,3,5-Trimethylbenzene J"2.00.20.3 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene J"2.00.21.2 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.4 Page 4 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-5 (E301006-01) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"99.9 %76-134Surrogate: 1,2-Dichloroethane-d4 """"98.4 %78-125Surrogate: Toluene-d8 """"102 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-6 (E301006-02) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.11.7 """"""Dichlorodifluoromethane (F12)4.0ND0.4 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """"""Trichlorofluoromethane (F11)2.3ND0.2 """"""Acetone 4.8ND0.5 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.7 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """"""Chloroform 1.0ND0.2 Page 5 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-6 (E301006-02) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.3 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.32.0 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.214 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.34.5 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.4 """""m,p-Xylene J"1.80.21.2 """"""Styrene 1.7ND0.2 """""o-Xylene J"1.80.20.7 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 Page 6 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-6 (E301006-02) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """"""4-Ethyltoluene 2.0ND0.2 """""1,3,5-Trimethylbenzene J"2.00.20.2 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene J"2.00.21.0 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.4 """"""1,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"101 %76-134Surrogate: 1,2-Dichloroethane-d4 """"97.6 %78-125Surrogate: Toluene-d8 """"101 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-4 (E301006-03) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31610 16-Jan-23 16-Jan-23ug/m3 1Propene JEPA TO-151.40.10.9 """""Dichlorodifluoromethane (F12)J"4.00.41.3 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """""Trichlorofluoromethane (F11)J"2.30.21.4 """""Acetone "4.80.513 """"""Isopropyl alcohol 5.0ND0.5 Page 7 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-4 (E301006-03) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1516-Jan-23 16-Jan-23ug/m3 EA3161011,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.11.1 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform "1.00.21.7 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.3 """""Carbon tetrachloride "1.30.31.7 """""Cyclohexane J"2.80.32.0 """""2,2,4-Trimethylpentane J"1.90.20.4 """""n-Heptane J"1.70.21.0 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.221 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.354 Page 8 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-4 (E301006-03) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1516-Jan-23 16-Jan-23ug/m3 EA3161011,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.21.1 """""m,p-Xylene "1.80.26.3 """"""Styrene 1.7ND0.2 """""o-Xylene "1.80.22.9 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """""n-Propylbenzene J"2.00.20.4 """""4-Ethyltoluene J"2.00.21.0 """""1,3,5-Trimethylbenzene J"2.00.21.0 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.23.9 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.8 """"""1,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.20.5 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"102 %76-134Surrogate: 1,2-Dichloroethane-d4 """"100 %78-125Surrogate: Toluene-d8 """"103 %77-127Surrogate: 4-Bromofluorobenzene Page 9 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-3 (E301006-04) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31610 16-Jan-23 16-Jan-23ug/m3 1Propene EPA TO-151.40.11.6 """""Dichlorodifluoromethane (F12)J"4.00.41.3 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """"""Trichlorofluoromethane (F11)2.3ND0.2 """""Acetone "4.80.514 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.4 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """""2-Butanone (MEK)J"2.40.31.7 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform "1.00.21.5 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.5 """""Carbon tetrachloride J"1.30.31.0 """"""Cyclohexane 2.8ND0.3 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 Page 10 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-3 (E301006-04) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1516-Jan-23 16-Jan-23ug/m3 EA3161011,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.24.4 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.3410 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.7 """""m,p-Xylene "1.80.25.0 """"""Styrene 1.7ND0.2 """""o-Xylene "1.80.22.8 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """""Isopropylbenzene (Cumene)J"2.00.20.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """""4-Ethyltoluene J"2.00.21.2 """""1,3,5-Trimethylbenzene J"2.00.21.3 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.24.9 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.7 Page 11 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-3 (E301006-04) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1516-Jan-23 16-Jan-23ug/m3 EA3161011,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.20.7 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"100 %76-134Surrogate: 1,2-Dichloroethane-d4 """"98.5 %78-125Surrogate: Toluene-d8 """"109 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-2 (E301006-05) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.14.0 """""Dichlorodifluoromethane (F12)J"4.00.41.4 """""Chloromethane "0.80.10.9 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """"""Trichlorofluoromethane (F11)2.3ND0.2 """""Acetone "4.80.531 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.4 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """"""Chloroform 1.0ND0.2 Page 12 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-2 (E301006-05) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.1 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.32.2 """""2,2,4-Trimethylpentane "1.90.22.5 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.23.1 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene J"2.80.32.4 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene "1.80.22.0 """""m,p-Xylene "1.80.29.8 """""Styrene J"1.70.20.7 """""o-Xylene "1.80.24.6 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """""Isopropylbenzene (Cumene)J"2.00.20.8 """"""Bromobenzene 2.6ND0.3 Page 13 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-2 (E301006-05) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """""n-Propylbenzene J"2.00.21.6 """""4-Ethyltoluene "2.00.23.9 """""1,3,5-Trimethylbenzene "2.00.25.4 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.218 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """""sec-Butylbenzene J"2.20.21.6 """""p-Isopropyltoluene "2.20.24.0 """"""1,2-Dichlorobenzene 2.4ND0.2 """""n-Butylbenzene "2.20.27.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.20.7 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"101 %76-134Surrogate: 1,2-Dichloroethane-d4 """"101 %78-125Surrogate: Toluene-d8 """"97.4 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-9 (E301006-06) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA313021Propene1.4ND0.1 """""Dichlorodifluoromethane (F12)J"4.00.41.7 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """""Trichlorofluoromethane (F11)J"2.30.22.0 """""Acetone "4.80.57.0 """"""Isopropyl alcohol 5.0ND0.5 Page 14 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-9 (E301006-06) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,1-Dichloroethene 1.6ND0.2 """""1,1,2-Trichlorotrifluoroethane (F113)J"3.10.30.5 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide "1.30.13.6 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform "1.00.22.5 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.2 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.31.2 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.23.5 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.3250 Page 15 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-9 (E301006-06) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.7 """""m,p-Xylene J"1.80.21.5 """"""Styrene 1.7ND0.2 """""o-Xylene "1.80.25.2 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """"""4-Ethyltoluene 2.0ND0.2 """"""1,3,5-Trimethylbenzene 2.0ND0.2 """"""tert-Butylbenzene 2.2ND0.2 """"""1,2,4-Trimethylbenzene 2.0ND0.2 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene "2.20.212 """"""1,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.20.6 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"99.0 %76-134Surrogate: 1,2-Dichloroethane-d4 """"101 %78-125Surrogate: Toluene-d8 """"99.8 %77-127Surrogate: 4-Bromofluorobenzene Page 16 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-1 (E301006-07) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.11.5 """""Dichlorodifluoromethane (F12)J"4.00.41.5 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """""Trichlorofluoromethane (F11)J"2.30.21.1 """""Acetone J"4.80.52.3 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.3 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """"""Chloroform 1.0ND0.2 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.2 """"""Carbon tetrachloride 1.3ND0.3 """"""Cyclohexane 2.8ND0.3 """"""2,2,4-Trimethylpentane 1.9ND0.2 """""n-Heptane J"1.70.21.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 Page 17 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-1 (E301006-07) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.210 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """"""Tetrachloroethene 2.8ND0.3 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene "1.80.22.1 """""m,p-Xylene "1.80.210 """"""Styrene 1.7ND0.2 """"""o-Xylene 1.8ND0.2 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """""Isopropylbenzene (Cumene)J"2.00.20.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """""n-Propylbenzene "2.00.22.0 """""4-Ethyltoluene J"2.00.21.0 """""1,3,5-Trimethylbenzene J"2.00.21.4 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.25.3 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.21.2 Page 18 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-1 (E301006-07) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichlorobenzene 2.4ND0.2 """""n-Butylbenzene J"2.20.21.4 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.21.0 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"97.3 %76-134Surrogate: 1,2-Dichloroethane-d4 """"101 %78-125Surrogate: Toluene-d8 """"89.1 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-7 (E301006-09) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.12.0 """""Dichlorodifluoromethane (F12)J"4.00.41.6 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """""Trichlorofluoromethane (F11)J"2.30.21.1 """""Acetone J"4.80.54.5 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.3 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """"""Chloroform 1.0ND0.2 Page 19 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-7 (E301006-09) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.4 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.30.9 """"""2,2,4-Trimethylpentane 1.9ND0.2 """""n-Heptane J"1.70.20.7 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.29.0 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene J"2.80.30.8 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.9 """""m,p-Xylene "1.80.23.0 """"""Styrene 1.7ND0.2 """""o-Xylene "1.80.24.0 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 Page 20 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-7 (E301006-09) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130212-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """""4-Ethyltoluene J"2.00.20.5 """""1,3,5-Trimethylbenzene J"2.00.20.5 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.22.1 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.4 """"""1,2-Dichlorobenzene 2.4ND0.2 """""n-Butylbenzene J"2.20.20.5 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"98.7 %76-134Surrogate: 1,2-Dichloroethane-d4 """"99.5 %78-125Surrogate: Toluene-d8 """"102 %77-127Surrogate: 4-Bromofluorobenzene J- ReportS6-Duplicate (E301006-10) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA313021Propene1.4ND0.1 """""Dichlorodifluoromethane (F12)J"4.00.41.4 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """""Trichlorofluoromethane (F11)J"2.30.21.1 """""Acetone J"4.80.51.8 """"""Isopropyl alcohol 5.0ND0.5 Page 21 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-Duplicate (E301006-10) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.2 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform J"1.00.20.9 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.3 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.31.4 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """""Trichloroethene J"2.20.31.7 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.25.9 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.34.7 Page 22 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-Duplicate (E301006-10) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.20.4 """""m,p-Xylene J"1.80.21.7 """"""Styrene 1.7ND0.2 """""o-Xylene J"1.80.20.8 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """""4-Ethyltoluene J"2.00.20.3 """""1,3,5-Trimethylbenzene J"2.00.20.4 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene J"2.00.21.4 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene J"2.20.20.3 """"""1,2-Dichlorobenzene 2.4ND0.2 """""n-Butylbenzene J"2.20.20.3 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"95.8 %76-134Surrogate: 1,2-Dichloroethane-d4 """"97.7 %78-125Surrogate: Toluene-d8 """"104 %77-127Surrogate: 4-Bromofluorobenzene Page 23 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-8 (E301006-11) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EA31302 13-Jan-23 13-Jan-23ug/m3 1Propene EPA TO-151.40.11.9 """""Dichlorodifluoromethane (F12)J"4.00.41.6 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """"""Ethanol 7.6ND1.2 """"""Trichlorofluoromethane (F11)2.3ND0.2 """"""Acetone 4.8ND0.5 """"""Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide J"1.30.10.5 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """"""n-Hexane 1.4ND0.2 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform J"1.00.20.6 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene J"0.60.10.3 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane J"2.80.32.7 """"""2,2,4-Trimethylpentane 1.9ND0.2 """"""n-Heptane 1.7ND0.2 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 Page 24 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-8 (E301006-11) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """""Toluene "3.10.212 """"""1,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene J"2.80.30.5 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene J"1.80.21.4 """""m,p-Xylene "1.80.26.8 """"""Styrene 1.7ND0.2 """""o-Xylene "1.80.23.5 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """""n-Propylbenzene J"2.00.20.2 """""4-Ethyltoluene J"2.00.20.6 """""1,3,5-Trimethylbenzene J"2.00.20.9 """"""tert-Butylbenzene 2.2ND0.2 """""1,2,4-Trimethylbenzene "2.00.24.4 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """""p-Isopropyltoluene "2.20.26.8 Page 25 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportS6-8 (E301006-11) Vapor Sampled: 21-Dec-22 Received: 28-Dec-22 EPA TO-1513-Jan-23 13-Jan-23ug/m3 EA3130211,2-Dichlorobenzene 2.4ND0.2 """""n-Butylbenzene J"2.20.20.7 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """""Naphthalene J"2.10.20.6 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"98.9 %76-134Surrogate: 1,2-Dichloroethane-d4 """"89.7 %78-125Surrogate: Toluene-d8 """"101 %77-127Surrogate: 4-Bromofluorobenzene Page 26 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31302 - TO-15 Blank (EA31302-BLK1)Prepared & Analyzed: 13-Jan-23 Propene ug/m31.4ND Dichlorodifluoromethane (F12)"4.0ND Chloromethane "0.8ND Dichlorotetrafluoroethane (F114)"2.8ND Vinyl chloride "0.5ND 1,3-Butadiene "0.9ND Bromomethane "1.6ND Chloroethane "1.1ND Ethanol "7.6ND Trichlorofluoromethane (F11)"2.3ND Acetone "4.8ND Isopropyl alcohol "5.0ND 1,1-Dichloroethene "1.6ND 1,1,2-Trichlorotrifluoroethane (F113)"3.1ND Methylene chloride (Dichloromethane)"1.4ND Carbon disulfide "1.3ND trans-1,2-Dichloroethene "1.6ND Vinyl acetate "2.9ND 1,1-Dichloroethane "1.6ND 2-Butanone (MEK)"2.4ND n-Hexane "1.4ND cis-1,2-Dichloroethene "1.6ND Ethyl acetate "2.9ND Chloroform "1.0ND 2,2-Dichloropropane "1.9ND Tetrahydrofuran "2.4ND 1,1,1-Trichloroethane "2.2ND 1,2-Dichloroethane (EDC)"1.6ND 1,1-Dichloropropene "1.8ND Benzene "0.6ND Carbon tetrachloride "1.3ND Cyclohexane "2.8ND 2,2,4-Trimethylpentane "1.9ND n-Heptane "1.7ND Page 27 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31302 - TO-15 Blank (EA31302-BLK1)Prepared & Analyzed: 13-Jan-23 Trichloroethene ug/m32.2ND Dibromomethane "2.9ND 1,2-Dichloropropane "1.9ND 1,4-Dioxane "2.9ND Bromodichloromethane "2.7ND cis-1,3-Dichloropropene "1.8ND 4-Methyl-2-pentanone (MIBK)"3.3ND trans-1,3-Dichloropropene "1.8ND 1,3-Dichloropropane "1.9ND Toluene "3.1ND 1,1,2-Trichloroethane "2.2ND 2-Hexanone (MBK)"3.3ND Dibromochloromethane "3.5ND Tetrachloroethene "2.8ND 1,2-Dibromoethane (EDB)"3.1ND 1,1,1,2-Tetrachloroethane "2.8ND Chlorobenzene "1.9ND Ethylbenzene "1.8ND m,p-Xylene "1.8ND Styrene "1.7ND o-Xylene "1.8ND Bromoform "4.2ND 1,1,2,2-Tetrachloroethane "2.8ND 1,2,3-Trichloropropane "2.4ND Isopropylbenzene (Cumene)"2.0ND Bromobenzene "2.6ND 2-Chlorotoluene "2.1ND 4-Chlorotoluene "2.1ND n-Propylbenzene "2.0ND 4-Ethyltoluene "2.0ND 1,3,5-Trimethylbenzene "2.0ND tert-Butylbenzene "2.2ND 1,2,4-Trimethylbenzene "2.0ND 1,3-Dichlorobenzene "2.4ND Page 28 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31302 - TO-15 Blank (EA31302-BLK1)Prepared & Analyzed: 13-Jan-23 Benzyl chloride ug/m32.1ND 1,4-Dichlorobenzene "2.4ND sec-Butylbenzene "2.2ND p-Isopropyltoluene "2.2ND 1,2-Dichlorobenzene "2.4ND n-Butylbenzene "2.2ND 1,2-Dibromo-3-chloropropane "9.8ND Naphthalene "2.1ND 1,2,4-Trichlorobenzene "7.5ND 1,2,3-Trichlorobenzene "6.0ND Hexachlorobutadiene "11ND "214 76-134Surrogate: 1,2-Dichloroethane-d4 95.1203 "208 78-125Surrogate: Toluene-d8 98.3204 "363 77-127Surrogate: 4-Bromofluorobenzene 99.0359 LCS (EA31302-BS1)Prepared & Analyzed: 13-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 59-12896.74.098 Vinyl chloride "52.0 64-12792.10.548 Chloroethane "53.6 63-12790.41.148 Trichlorofluoromethane (F11)"113 62-1261182.3130 1,1-Dichloroethene "80.8 61-13392.51.675 1,1,2-Trichlorotrifluoroethane (F113)"155 66-12692.43.1140 Methylene chloride (Dichloromethane)"70.8 62-11591.81.465 trans-1,2-Dichloroethene "80.8 67-12498.21.679 1,1-Dichloroethane "82.4 68-12694.71.678 cis-1,2-Dichloroethene "80.0 70-1211011.681 Chloroform "99.2 68-12392.21.091 1,1,1-Trichloroethane "111 68-12594.62.2110 1,2-Dichloroethane (EDC)"82.4 65-12895.21.678 Benzene "64.8 69-11999.20.664 Carbon tetrachloride "128 68-13293.11.3120 Trichloroethene "110 71-1231002.2110 Toluene "76.8 66-11991.73.170 Page 29 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31302 - TO-15 LCS (EA31302-BS1)Prepared & Analyzed: 13-Jan-23 1,1,2-Trichloroethane ug/m3 111 73-11997.62.2110 Tetrachloroethene "138 66-1241022.8140 1,1,1,2-Tetrachloroethane "140 67-1291012.8140 Ethylbenzene "88.4 70-1241131.8100 m,p-Xylene "88.4 61-1341281.8110 o-Xylene "88.4 67-1251141.8100 1,1,2,2-Tetrachloroethane "140 65-12796.42.8130 "214 76-134Surrogate: 1,2-Dichloroethane-d4 98.4210 "208 78-125Surrogate: Toluene-d8 99.3206 "363 77-127Surrogate: 4-Bromofluorobenzene 100364 LCS Dup (EA31302-BSD1)Prepared & Analyzed: 13-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 2559-12896.5 0.2584.097 Vinyl chloride "52.0 2564-12794.6 2.670.549 Chloroethane "53.6 2563-12790.7 0.2761.149 Trichlorofluoromethane (F11)"113 2562-126118 0.002.3130 1,1-Dichloroethene "80.8 2561-13394.9 2.501.677 1,1,2-Trichlorotrifluoroethane (F113)"155 2566-12693.2 0.8573.1140 Methylene chloride (Dichloromethane)"70.8 2562-11593.2 1.511.466 trans-1,2-Dichloroethene "80.8 2567-12499.8 1.661.681 1,1-Dichloroethane "82.4 2568-12697.7 3.161.681 cis-1,2-Dichloroethene "80.0 2570-121102 1.241.682 Chloroform "99.2 2568-12393.0 0.8601.092 1,1,1-Trichloroethane "111 2568-12593.8 0.8432.2100 1,2-Dichloroethane (EDC)"82.4 2565-12894.6 0.6831.678 Benzene "64.8 2569-119101 1.550.665 Carbon tetrachloride "128 2568-13294.2 1.231.3120 Trichloroethene "110 2571-123101 0.3962.2110 Toluene "76.8 2566-11995.8 4.453.174 1,1,2-Trichloroethane "111 2573-11996.4 1.182.2110 Tetrachloroethene "138 2566-124100 1.532.8140 1,1,1,2-Tetrachloroethane "140 2567-129104 2.192.8140 Ethylbenzene "88.4 2570-124116 3.171.8100 Page 30 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31302 - TO-15 LCS Dup (EA31302-BSD1)Prepared & Analyzed: 13-Jan-23 m,p-Xylene ug/m3 88.4 2561-134129 1.201.8110 o-Xylene "88.4 2567-125117 2.891.8100 1,1,2,2-Tetrachloroethane "140 2565-127101 4.392.8140 "214 76-134Surrogate: 1,2-Dichloroethane-d4 100214 "208 78-125Surrogate: Toluene-d8 100208 "363 77-127Surrogate: 4-Bromofluorobenzene 100364 Batch EA31610 - TO-15 Blank (EA31610-BLK1)Prepared & Analyzed: 16-Jan-23 Propene ug/m31.4ND Dichlorodifluoromethane (F12)"4.0ND Chloromethane "0.8ND Dichlorotetrafluoroethane (F114)"2.8ND Vinyl chloride "0.5ND 1,3-Butadiene "0.9ND Bromomethane "1.6ND Chloroethane "1.1ND Ethanol "7.6ND Trichlorofluoromethane (F11)"2.3ND Acetone "4.8ND Isopropyl alcohol "5.0ND 1,1-Dichloroethene "1.6ND 1,1,2-Trichlorotrifluoroethane (F113)"3.1ND Methylene chloride (Dichloromethane)"1.4ND Carbon disulfide "1.3ND trans-1,2-Dichloroethene "1.6ND Vinyl acetate "2.9ND 1,1-Dichloroethane "1.6ND 2-Butanone (MEK)"2.4ND n-Hexane "1.4ND cis-1,2-Dichloroethene "1.6ND Ethyl acetate "2.9ND Page 31 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31610 - TO-15 Blank (EA31610-BLK1)Prepared & Analyzed: 16-Jan-23 Chloroform ug/m31.0ND 2,2-Dichloropropane "1.9ND Tetrahydrofuran "2.4ND 1,1,1-Trichloroethane "2.2ND 1,2-Dichloroethane (EDC)"1.6ND 1,1-Dichloropropene "1.8ND Benzene "0.6ND Carbon tetrachloride "1.3ND Cyclohexane "2.8ND 2,2,4-Trimethylpentane "1.9ND n-Heptane "1.7ND Trichloroethene "2.2ND Dibromomethane "2.9ND 1,2-Dichloropropane "1.9ND 1,4-Dioxane "2.9ND Bromodichloromethane "2.7ND cis-1,3-Dichloropropene "1.8ND 4-Methyl-2-pentanone (MIBK)"3.3ND trans-1,3-Dichloropropene "1.8ND 1,3-Dichloropropane "1.9ND Toluene "3.1ND 1,1,2-Trichloroethane "2.2ND 2-Hexanone (MBK)"3.3ND Dibromochloromethane "3.5ND Tetrachloroethene "2.8ND 1,2-Dibromoethane (EDB)"3.1ND 1,1,1,2-Tetrachloroethane "2.8ND Chlorobenzene "1.9ND Ethylbenzene "1.8ND m,p-Xylene "1.8ND Styrene "1.7ND o-Xylene "1.8ND Bromoform "4.2ND 1,1,2,2-Tetrachloroethane "2.8ND Page 32 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31610 - TO-15 Blank (EA31610-BLK1)Prepared & Analyzed: 16-Jan-23 1,2,3-Trichloropropane ug/m32.4ND Isopropylbenzene (Cumene)"2.0ND Bromobenzene "2.6ND 2-Chlorotoluene "2.1ND 4-Chlorotoluene "2.1ND n-Propylbenzene "2.0ND 4-Ethyltoluene "2.0ND 1,3,5-Trimethylbenzene "2.0ND tert-Butylbenzene "2.2ND 1,2,4-Trimethylbenzene "2.0ND 1,3-Dichlorobenzene "2.4ND Benzyl chloride "2.1ND 1,4-Dichlorobenzene "2.4ND sec-Butylbenzene "2.2ND p-Isopropyltoluene "2.2ND 1,2-Dichlorobenzene "2.4ND n-Butylbenzene "2.2ND 1,2-Dibromo-3-chloropropane "9.8ND Naphthalene "2.1ND 1,2,4-Trichlorobenzene "7.5ND 1,2,3-Trichlorobenzene "6.0ND Hexachlorobutadiene "11ND "214 76-134Surrogate: 1,2-Dichloroethane-d4 96.6206 "208 78-125Surrogate: Toluene-d8 99.2206 "363 77-127Surrogate: 4-Bromofluorobenzene 97.7355 LCS (EA31610-BS1)Prepared & Analyzed: 16-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 59-1281004.0100 Vinyl chloride "52.0 64-12795.10.549 Chloroethane "53.6 63-12793.41.150 Trichlorofluoromethane (F11)"113 62-12690.92.3100 1,1-Dichloroethene "80.8 61-13396.11.678 1,1,2-Trichlorotrifluoroethane (F113)"155 66-12696.63.1150 Page 33 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31610 - TO-15 LCS (EA31610-BS1)Prepared & Analyzed: 16-Jan-23 Methylene chloride (Dichloromethane)ug/m3 70.8 62-11596.71.468 trans-1,2-Dichloroethene "80.8 67-12497.51.679 1,1-Dichloroethane "82.4 68-12696.41.679 cis-1,2-Dichloroethene "80.0 70-1211011.680 Chloroform "99.2 68-12395.71.095 1,1,1-Trichloroethane "111 68-12597.52.2110 1,2-Dichloroethane (EDC)"82.4 65-12897.01.680 Benzene "64.8 69-1191010.666 Carbon tetrachloride "128 68-13297.81.3130 Trichloroethene "110 71-1231022.2110 Toluene "76.8 66-1191033.179 1,1,2-Trichloroethane "111 73-11999.12.2110 Tetrachloroethene "138 66-1241042.8140 1,1,1,2-Tetrachloroethane "140 67-1291082.8150 Ethylbenzene "88.4 70-1241171.8100 m,p-Xylene "88.4 61-1341331.8120 o-Xylene "88.4 67-1251201.8110 1,1,2,2-Tetrachloroethane "140 65-1271022.8140 "214 76-134Surrogate: 1,2-Dichloroethane-d4 100214 "208 78-125Surrogate: Toluene-d8 99.5207 "363 77-127Surrogate: 4-Bromofluorobenzene 102369 LCS Dup (EA31610-BSD1)Prepared & Analyzed: 16-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 2559-12898.3 1.964.099 Vinyl chloride "52.0 2564-12795.8 0.7310.550 Chloroethane "53.6 2563-12791.4 2.161.149 Trichlorofluoromethane (F11)"113 2562-12693.4 2.652.3110 1,1-Dichloroethene "80.8 2561-13386.6 10.41.670 1,1,2-Trichlorotrifluoroethane (F113)"155 2566-12696.0 0.6193.1150 Methylene chloride (Dichloromethane)"70.8 2562-11590.0 7.101.464 trans-1,2-Dichloroethene "80.8 2567-12496.1 1.491.678 1,1-Dichloroethane "82.4 2568-12696.5 0.1031.680 cis-1,2-Dichloroethene "80.0 2570-12198.0 2.581.678 Page 34 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA31610 - TO-15 LCS Dup (EA31610-BSD1)Prepared & Analyzed: 16-Jan-23 Chloroform ug/m3 99.2 2568-12395.4 0.3121.095 1,1,1-Trichloroethane "111 2568-12596.6 0.8692.2110 1,2-Dichloroethane (EDC)"82.4 2565-12897.2 0.2051.680 Benzene "64.8 2569-11999.0 2.150.664 Carbon tetrachloride "128 2568-13296.7 1.181.3120 Trichloroethene "110 2571-123101 0.7352.2110 Toluene "76.8 2566-11992.1 11.23.171 1,1,2-Trichloroethane "111 2573-11994.7 4.562.2110 Tetrachloroethene "138 2566-124101 3.262.8140 1,1,1,2-Tetrachloroethane "140 2567-129105 3.512.8150 Ethylbenzene "88.4 2570-124113 3.841.8100 m,p-Xylene "88.4 2561-134128 3.741.8110 o-Xylene "88.4 2567-125117 2.561.8100 1,1,2,2-Tetrachloroethane "140 2565-127102 0.1472.8140 "214 76-134Surrogate: 1,2-Dichloroethane-d4 104222 "208 78-125Surrogate: Toluene-d8 99.0206 "363 77-127Surrogate: 4-Bromofluorobenzene 101367 Page 35 of 36 Project: Project Number: Project Manager: Reported: EAS Professionals 2145 N. Center St. Suite B-205 MC122822-10 Rev3 450 Polo Rd Property Derek RossNorth Charleston, SC 29406 27-Feb-23 10:35 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Notes and Definitions J- Report This sample is reported to the MDL or LOD determined for this method. All confirmed hits above the listed MDL or LOD value and below the RL/LOQ, will be flagged with a "J" result. If an MDL or LOD is not listed, the analyte is ND at the RL. J Detected but below the RL/LOQ; therefore, result is an estimated concentration. Percent Recovery Relative Percent DifferenceRPD %REC Method Detection LimitMDL Analyte NOT DETECTED at or above the reporting limitND Leak Check CompoundLCC Appendix H&P Mobile Geochemistry, Inc. is approved as an Environmental Testing Laboratory and Mobile Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs through PJLA, accreditation number 69070 for EPA Method TO-15, EPA Method 8260B and H&P 8260SV. H&P is approved by the State of California as an Environmental Laboratory and Mobile Laboratory in conformance with the Environmental Laboratory Accreditation Program (ELAP) for the category of Volatile and Semi-Volatile Organic Chemistry of Hazardous Waste, certification numbers 2740, 2741, 2743 & 2745. H&P is approved by the State of Louisiana Department of Environmental Quality under the National Environmental Laboratory Accreditation Conference (NELAC) certification number 04138. The complete list of stationary and mobile laboratory certifications along with the fields of testing (FOTs) and analyte lists are available at www.handpmg.com/about/certifications. All soil results are reported in wet weight. Page 36 of 36 Soil IDDate SampledCanister ID #Laboratory OutBeginningFinalLaboratory-ReceivedSG-1 12/21/22 819 -29.61 -27 0 +0.26 SG-2 12/21/22 563 -29.50 -26.5 0 +1.08 SG-3 12/21/22 826 -29.57 -25 0 +0.84 SG-4 12/21/22 805 -29.61 -23 0 -0.01 SG-5 12/21/22 816 -29.62 -25 0 +1.25 SG-6 12/21/22 814 -29.62 -27.5 -2.5 +1.45 SG-7 12/21/22 180 -29.60 -26 0 +1.03 SG-8 12/21/22 412 -29.59 -27.5 0 +1.01 SG-9 12/21/22 428 -29.60 -24.5 0 +0.91 SG-10 1/27/23 665 -29.58 -27.5 0 +0.22 SG-Duplicate 12/21/22 000 (812) -29.60 -26 0 +1.00 Duplicate-2 1/27/22 393 -29.58 -27.5 0 +0.20 Units in inches of mercury (in. Hg) Table 2 Summa Canister Vacuum Pressure Readings (in. Hg) 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 1 Westley Godfrey From:lisa.eminhizer handpmg.com <lisa.eminhizer@handpmg.com> Sent:Monday, February 27, 2023 3:03 PM To:Derek Ross; Westley Godfrey; J. Ashley Brown Cc:kristin.beckley handpmg.com Subject:MC122822-10 (220784) Revised 3 Final Report, EDD - Polo Road Property Attachments:MC122822-10 REV3 FINAl.pdf; MC122822-10 REV3 FINAL EXCEL 27 Feb 23 1035.xls Hi Westley, AƩached is the revised (3rd) final report and Excel EDD for MC122822-10 for the Polo Road Property. Please note that a Propene result iniƟally reported for S6-9 in the final report dated January 17, 2023, was a false posiƟve and should have been removed at that Ɵme. My apologies for the confusion and please let me know if there is anything else I can help with. Thank you, Lisa Eminhizer Laboratory Director H&P Mobile Geochemistry, Inc. 2470 Impala Drive, Carlsbad, CA O: 760.804.9678 Lisa.Eminhizer@handpmg.com W handpmg.com DOD ELAP, NELAC & CA ELAP Accredited for Analysis NEFAP Certified for Active Soil Vapor & Air Sampling NOTE: This message, including any attachments, contains information that is confidential and may be protected by law from disclosure. Any review, use, distribution or disclosure by anyone other than the intended recipient is strictly prohibited. If you are not the intended recipient, please notify the sender immediately and delete this message from your system. Thank you. 27 February 2023 Enclosed is the analytical report for the above referenced project. The data herein applies to samples as received by H&P Mobile Geochemistry, Inc. on 30-Jan-23 which were analyzed in accordance with the attached Chain of Custody record(s). The results for all sample analyses and required QA/QC analyses are presented in the following sections and summarized in the documents: •Sample Summary •Case Narrative (if applicable) •Sample Results •Quality Control Summary •Notes and Definitions / Appendix •Chain of Custody •Sampling Logs (if applicable) Unless otherwise noted, I certify that all analyses were performed and reviewed in compliance with our Quality Systems Manual and Standard Operating Procedures. This report shall not be reproduced, except in full, without the written approval of H&P Mobile Geochemistry, Inc. We at H&P Mobile Geochemistry, Inc. sincerely appreciate the opportunity to provide analytical services to you on this project. If you have any questions or concerns regarding this analytical report, please contact me at your convenience at 760-804-9678. Sincerely, Client Project: 450 Polo Rd Property H&P Project: MC013023-10 Rev3 Arden, NC 28704 8 Glenn Willow Dr, Unit 18 EAS Professionals, Inc. Derek Ross Laboratory Director Lisa Eminhizer Dear Derek Ross: Quality. Accuracy. Experience.2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CA P 1.800.834.9888 / 760.804.9678 F 760.804.9159 W handpmg.com MobileGeochemistry Inc. H&P Mobile Geochemistry, Inc. is certified under the California ELAP and the National Environmental Laboratory Accreditation Conference (NELAC) for the fields of proficiency and analytes listed on those certificates. H&P is approved as an Environmental Testing Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs for the fields of proficiency and analytes included in the certification process and to the extent offered by the accreditation agency. Unless otherwise noted, accreditation certificate numbers, expiration of certificates, and scope of accreditation can be found at: www.handpmg.com/about/certifications. Fields of services and analytes contained in this report that are not listed on the certificates should be considered uncertified or unavailable for certification. Page 1 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Sample ID Laboratory ID Matrix Date Sampled ANALYTICAL REPORT FOR SAMPLES Date Received SG-10 E301055-01 Vapor 27-Jan-23 30-Jan-23 Duplicate - 2 E301055-02 Vapor 27-Jan-23 30-Jan-23 The percent recovery for 1,1,2-Trichlorotrifluoroethane fell below the method criteria in the continuing calibration verification (CCV). Any results for this analyte may be biased low. The percent recovery for Ethanol fell above the method criteria in the CCV. Any results for this analyte may be biased high. February 27, 2023 This final has been revised to correct several sample results. Page 2 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportSG-10 (E301055-01) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA330121Propene1.4ND0.1 """""Dichlorodifluoromethane (F12)"4.00.425 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""1,3-Butadiene 0.9ND0.1 """"""Bromomethane 1.6ND0.2 """"""Chloroethane 1.1ND0.2 """""Ethanol "7.61.2190 """""Trichlorofluoromethane (F11)"2.30.213 """"10Acetone "484.8350 """""1Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide "1.30.16.6 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """""n-Hexane "1.40.2230 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform "1.00.24.1 """"""2,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene "0.60.1100 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane "2.80.353 """""2,2,4-Trimethylpentane "1.90.2230 """""n-Heptane "1.70.270 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 Page 3 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportSG-10 (E301055-01) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA3301211,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """"10Toluene "311.5940 """""11,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.3560 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene "1.80.289 """""m,p-Xylene "1.80.2390 """"10Styrene "171.71300 """"1o-Xylene "1.80.2230 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 """"""2-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """"""4-Ethyltoluene 2.0ND0.2 """"""1,3,5-Trimethylbenzene 2.0ND0.2 """"""tert-Butylbenzene 2.2ND0.2 """"""1,2,4-Trimethylbenzene 2.0ND0.2 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """"""p-Isopropyltoluene 2.2ND0.2 Page 4 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportSG-10 (E301055-01) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA3301211,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"91.2 %76-134Surrogate: 1,2-Dichloroethane-d4 """"115 %78-125Surrogate: Toluene-d8 """"95.3 %77-127Surrogate: 4-Bromofluorobenzene J- ReportDuplicate - 2 (E301055-02) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA330121Propene1.4ND0.1 """""Dichlorodifluoromethane (F12)"4.00.428 """"""Chloromethane 0.8ND0.1 """"""Dichlorotetrafluoroethane (F114)2.8ND0.3 """"""Vinyl chloride 0.5ND0.1 """"""Bromomethane 1.6ND0.2 """"""1,3-Butadiene 0.9ND0.1 """"""Chloroethane 1.1ND0.2 """"10Ethanol "7612240 """"1Trichlorofluoromethane (F11)"2.30.28.9 """"10Acetone "484.8380 """""1Isopropyl alcohol 5.0ND0.5 """"""1,1-Dichloroethene 1.6ND0.2 """"""1,1,2-Trichlorotrifluoroethane (F113)3.1ND0.3 """"""Methylene chloride (Dichloromethane)1.4ND0.1 """""Carbon disulfide "1.30.16.7 """"""trans-1,2-Dichloroethene 1.6ND0.2 """"""Vinyl acetate 2.9ND0.1 """"""1,1-Dichloroethane 1.6ND0.2 """"""2-Butanone (MEK)2.4ND0.3 """""n-Hexane "1.40.2260 """"""cis-1,2-Dichloroethene 1.6ND0.2 """"""Ethyl acetate 2.9ND0.3 """""Chloroform "1.00.24.7 Page 5 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportDuplicate - 2 (E301055-02) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA3301212,2-Dichloropropane 1.9ND0.2 """"""Tetrahydrofuran 2.4ND0.2 """"""1,1,1-Trichloroethane 2.2ND0.2 """"""1,2-Dichloroethane (EDC)1.6ND0.2 """"""1,1-Dichloropropene 1.8ND0.2 """""Benzene "0.60.1120 """"""Carbon tetrachloride 1.3ND0.3 """""Cyclohexane "2.80.369 """""2,2,4-Trimethylpentane "1.90.2250 """""n-Heptane "1.70.283 """"""Trichloroethene 2.2ND0.3 """"""Dibromomethane 2.9ND0.3 """"""1,2-Dichloropropane 1.9ND0.2 """"""1,4-Dioxane 2.9ND0.3 """"""Bromodichloromethane 2.7ND0.3 """"""cis-1,3-Dichloropropene 1.8ND0.2 """"""4-Methyl-2-pentanone (MIBK)3.3ND0.3 """"""trans-1,3-Dichloropropene 1.8ND0.2 """"""1,3-Dichloropropane 1.9ND0.2 """"10Toluene "311.51100 """""11,1,2-Trichloroethane 2.2ND0.2 """"""2-Hexanone (MBK)3.3ND0.3 """"""Dibromochloromethane 3.5ND0.3 """""Tetrachloroethene "2.80.3590 """"""1,2-Dibromoethane (EDB)3.1ND0.3 """"""1,1,1,2-Tetrachloroethane 2.8ND0.3 """"""Chlorobenzene 1.9ND0.4 """""Ethylbenzene "1.80.2150 """""m,p-Xylene "1.80.2760 """"10Styrene "171.71400 """"1o-Xylene "1.80.2300 """"""Bromoform 4.2ND0.4 """"""1,1,2,2-Tetrachloroethane 2.8ND0.3 """"""1,2,3-Trichloropropane 2.4ND0.2 """"""Isopropylbenzene (Cumene)2.0ND0.2 """"""Bromobenzene 2.6ND0.3 Page 6 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Volatile Organic Compounds by EPA TO-15 H&P Mobile Geochemistry, Inc. Result Analyte Limit Reporting Units Dilution Batch Prepared Analyzed Method Notes FactorMDL J- ReportDuplicate - 2 (E301055-02) Vapor Sampled: 27-Jan-23 Received: 30-Jan-23 EPA TO-1530-Jan-23 30-Jan-23ug/m3 EA3301212-Chlorotoluene 2.1ND0.2 """"""4-Chlorotoluene 2.1ND0.2 """"""n-Propylbenzene 2.0ND0.2 """"""4-Ethyltoluene 2.0ND0.2 """"""1,3,5-Trimethylbenzene 2.0ND0.2 """"""tert-Butylbenzene 2.2ND0.2 """"""1,2,4-Trimethylbenzene 2.0ND0.2 """"""1,3-Dichlorobenzene 2.4ND0.2 """"""Benzyl chloride 2.1ND0.2 """"""1,4-Dichlorobenzene 2.4ND0.2 """"""sec-Butylbenzene 2.2ND0.2 """"""p-Isopropyltoluene 2.2ND0.2 """"""1,2-Dichlorobenzene 2.4ND0.2 """"""n-Butylbenzene 2.2ND0.2 """"""1,2-Dibromo-3-chloropropane 9.8ND0.4 """"""Naphthalene 2.1ND0.2 """"""1,2,4-Trichlorobenzene 7.5ND0.3 """"""1,2,3-Trichlorobenzene 6.0ND0.6 """"""Hexachlorobutadiene 11ND0.9 """"88.5 %76-134Surrogate: 1,2-Dichloroethane-d4 """"124 %78-125Surrogate: Toluene-d8 """"86.4 %77-127Surrogate: 4-Bromofluorobenzene Page 7 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA33012 - TO-15 Blank (EA33012-BLK1)Prepared & Analyzed: 30-Jan-23 Propene ug/m31.4ND Dichlorodifluoromethane (F12)"4.0ND Chloromethane "0.8ND Dichlorotetrafluoroethane (F114)"2.8ND Vinyl chloride "0.5ND Bromomethane "1.6ND 1,3-Butadiene "0.9ND Chloroethane "1.1ND Ethanol "7.6ND Trichlorofluoromethane (F11)"2.3ND Acetone "4.8ND Isopropyl alcohol "5.0ND 1,1-Dichloroethene "1.6ND 1,1,2-Trichlorotrifluoroethane (F113)"3.1ND Methylene chloride (Dichloromethane)"1.4ND Carbon disulfide "1.3ND trans-1,2-Dichloroethene "1.6ND Vinyl acetate "2.9ND 1,1-Dichloroethane "1.6ND 2-Butanone (MEK)"2.4ND n-Hexane "1.4ND cis-1,2-Dichloroethene "1.6ND Ethyl acetate "2.9ND Chloroform "1.0ND 2,2-Dichloropropane "1.9ND Tetrahydrofuran "2.4ND 1,1,1-Trichloroethane "2.2ND 1,2-Dichloroethane (EDC)"1.6ND 1,1-Dichloropropene "1.8ND Benzene "0.6ND Carbon tetrachloride "1.3ND Cyclohexane "2.8ND 2,2,4-Trimethylpentane "1.9ND n-Heptane "1.7ND Page 8 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA33012 - TO-15 Blank (EA33012-BLK1)Prepared & Analyzed: 30-Jan-23 Trichloroethene ug/m32.2ND Dibromomethane "2.9ND 1,2-Dichloropropane "1.9ND 1,4-Dioxane "2.9ND Bromodichloromethane "2.7ND cis-1,3-Dichloropropene "1.8ND 4-Methyl-2-pentanone (MIBK)"3.3ND trans-1,3-Dichloropropene "1.8ND 1,3-Dichloropropane "1.9ND Toluene "3.1ND 1,1,2-Trichloroethane "2.2ND 2-Hexanone (MBK)"3.3ND Dibromochloromethane "3.5ND Tetrachloroethene "2.8ND 1,2-Dibromoethane (EDB)"3.1ND 1,1,1,2-Tetrachloroethane "2.8ND Chlorobenzene "1.9ND Ethylbenzene "1.8ND m,p-Xylene "1.8ND Styrene "1.7ND o-Xylene "1.8ND Bromoform "4.2ND 1,1,2,2-Tetrachloroethane "2.8ND 1,2,3-Trichloropropane "2.4ND Isopropylbenzene (Cumene)"2.0ND Bromobenzene "2.6ND 2-Chlorotoluene "2.1ND 4-Chlorotoluene "2.1ND n-Propylbenzene "2.0ND 4-Ethyltoluene "2.0ND 1,3,5-Trimethylbenzene "2.0ND tert-Butylbenzene "2.2ND 1,2,4-Trimethylbenzene "2.0ND 1,3-Dichlorobenzene "2.4ND Page 9 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA33012 - TO-15 Blank (EA33012-BLK1)Prepared & Analyzed: 30-Jan-23 Benzyl chloride ug/m32.1ND 1,4-Dichlorobenzene "2.4ND sec-Butylbenzene "2.2ND p-Isopropyltoluene "2.2ND 1,2-Dichlorobenzene "2.4ND n-Butylbenzene "2.2ND 1,2-Dibromo-3-chloropropane "9.8ND Naphthalene "2.1ND 1,2,4-Trichlorobenzene "7.5ND 1,2,3-Trichlorobenzene "6.0ND Hexachlorobutadiene "11ND "214 76-134Surrogate: 1,2-Dichloroethane-d4 94.0201 "208 78-125Surrogate: Toluene-d8 124257 "363 77-127Surrogate: 4-Bromofluorobenzene 89.5325 LCS (EA33012-BS1)Prepared & Analyzed: 30-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 59-1281044.0100 Vinyl chloride "52.0 64-1271000.552 Chloroethane "53.6 63-12798.81.153 Trichlorofluoromethane (F11)"113 62-12697.32.3110 1,1-Dichloroethene "80.8 61-13396.51.678 1,1,2-Trichlorotrifluoroethane (F113)"155 QL-1L66-12665.93.1100 Methylene chloride (Dichloromethane)"70.8 62-1151021.472 trans-1,2-Dichloroethene "80.8 67-12493.71.676 1,1-Dichloroethane "82.4 68-12696.11.679 cis-1,2-Dichloroethene "80.0 70-12195.51.676 Chloroform "99.2 68-12397.31.096 1,1,1-Trichloroethane "111 68-12592.32.2100 1,2-Dichloroethane (EDC)"82.4 65-12892.11.676 Benzene "64.8 69-11998.40.664 Carbon tetrachloride "128 68-13289.91.3120 Trichloroethene "110 71-12395.42.2100 Toluene "76.8 66-11993.33.172 Page 10 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA33012 - TO-15 LCS (EA33012-BS1)Prepared & Analyzed: 30-Jan-23 1,1,2-Trichloroethane ug/m3 111 73-11989.02.299 Tetrachloroethene "138 66-12488.52.8120 1,1,1,2-Tetrachloroethane "140 67-12985.22.8120 Ethylbenzene "88.4 70-1241021.890 m,p-Xylene "88.4 61-1341031.891 o-Xylene "88.4 67-1251041.892 1,1,2,2-Tetrachloroethane "140 65-12799.02.8140 "214 76-134Surrogate: 1,2-Dichloroethane-d4 98.4210 "208 78-125Surrogate: Toluene-d8 114236 "363 77-127Surrogate: 4-Bromofluorobenzene 96.9352 LCS Dup (EA33012-BSD1)Prepared & Analyzed: 30-Jan-23 Dichlorodifluoromethane (F12)ug/m3 101 2559-12895.1 8.624.096 Vinyl chloride "52.0 2564-12792.7 7.760.548 Chloroethane "53.6 2563-12792.9 6.141.150 Trichlorofluoromethane (F11)"113 2562-12688.8 9.052.3100 1,1-Dichloroethene "80.8 2561-13393.4 3.301.675 1,1,2-Trichlorotrifluoroethane (F113)"155 25 QL-1L66-12664.0 2.993.199 Methylene chloride (Dichloromethane)"70.8 2562-11596.4 5.821.468 trans-1,2-Dichloroethene "80.8 2567-12490.6 3.351.673 1,1-Dichloroethane "82.4 2568-12691.4 5.001.675 cis-1,2-Dichloroethene "80.0 2570-12193.3 2.241.675 Chloroform "99.2 2568-12391.5 6.111.091 1,1,1-Trichloroethane "111 2568-12589.0 3.612.299 1,2-Dichloroethane (EDC)"82.4 2565-12889.1 3.241.673 Benzene "64.8 2569-11994.8 3.770.661 Carbon tetrachloride "128 2568-13287.2 2.991.3110 Trichloroethene "110 2571-12398.2 2.832.2110 Toluene "76.8 2566-11995.2 2.063.173 1,1,2-Trichloroethane "111 2573-11989.1 0.1112.299 Tetrachloroethene "138 2566-12489.3 0.9542.8120 1,1,1,2-Tetrachloroethane "140 2567-12988.7 4.122.8120 Ethylbenzene "88.4 2570-124102 0.4381.890 Page 11 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by EPA TO-15 - Quality Control H&P Mobile Geochemistry, Inc. Batch EA33012 - TO-15 LCS Dup (EA33012-BSD1)Prepared & Analyzed: 30-Jan-23 m,p-Xylene ug/m3 88.4 2561-134103 0.3851.891 o-Xylene "88.4 2567-125103 0.6741.891 1,1,2,2-Tetrachloroethane "140 2565-12799.6 0.6512.8140 "214 76-134Surrogate: 1,2-Dichloroethane-d4 95.2203 "208 78-125Surrogate: Toluene-d8 113235 "363 77-127Surrogate: 4-Bromofluorobenzene 98.0356 Page 12 of 13 Project: Project Number: Project Manager: Reported: EAS Professionals, Inc. 8 Glenn Willow Dr, Unit 18 MC013023-10 Rev3 450 Polo Rd Property Derek RossArden, NC 28704 27-Feb-23 11:22 H&P Mobile Geochemistry Inc. 2470 Impala Drive Carlsbad, CA 92010 760-804-9678 Phone 760-804-9159 Fax Notes and Definitions QL-1L The LCS and/or LCSD recoveries fell below the established control specifications for this analyte. Any result for this compound is qualified and should be considered biased low. J- Report This sample is reported to the MDL or LOD determined for this method. All confirmed hits above the listed MDL or LOD value and below the RL/LOQ, will be flagged with a "J" result. If an MDL or LOD is not listed, the analyte is ND at the RL. Percent Recovery Relative Percent DifferenceRPD %REC Method Detection LimitMDL Analyte NOT DETECTED at or above the reporting limitND Leak Check CompoundLCC Appendix H&P Mobile Geochemistry, Inc. is approved as an Environmental Testing Laboratory and Mobile Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs through PJLA, accreditation number 69070 for EPA Method TO-15, EPA Method 8260B and H&P 8260SV. H&P is approved by the State of California as an Environmental Laboratory and Mobile Laboratory in conformance with the Environmental Laboratory Accreditation Program (ELAP) for the category of Volatile and Semi-Volatile Organic Chemistry of Hazardous Waste, certification numbers 2740, 2741, 2743 & 2745. H&P is approved by the State of Louisiana Department of Environmental Quality under the National Environmental Laboratory Accreditation Conference (NELAC) certification number 04138. The complete list of stationary and mobile laboratory certifications along with the fields of testing (FOTs) and analyte lists are available at www.handpmg.com/about/certifications. All soil results are reported in wet weight. Page 13 of 13 Soil IDDate SampledCanister ID #Laboratory OutBeginningFinalLaboratory-ReceivedSG-1 12/21/22 819 -29.61 -27 0 +0.26 SG-2 12/21/22 563 -29.50 -26.5 0 +1.08 SG-3 12/21/22 826 -29.57 -25 0 +0.84 SG-4 12/21/22 805 -29.61 -23 0 -0.01 SG-5 12/21/22 816 -29.62 -25 0 +1.25 SG-6 12/21/22 814 -29.62 -27.5 -2.5 +1.45 SG-7 12/21/22 180 -29.60 -26 0 +1.03 SG-8 12/21/22 412 -29.59 -27.5 0 +1.01 SG-9 12/21/22 428 -29.60 -24.5 0 +0.91 SG-10 1/27/23 665 -29.58 -27.5 0 +0.22 SG-Duplicate 12/21/22 000 (812) -29.60 -26 0 +1.00 Duplicate-2 1/27/22 393 -29.58 -27.5 0 +0.20 Units in inches of mercury (in. Hg) Table 2 Summa Canister Vacuum Pressure Readings (in. Hg) 450 POLO ROAD PROPERTY, WINSTON-SALEM, NC BROWNFIELDS PROJECT NO. 25052-21-034 1 Westley Godfrey From:lisa.eminhizer handpmg.com <lisa.eminhizer@handpmg.com> Sent:Monday, February 27, 2023 3:09 PM To:Westley Godfrey; Derek Ross; abarrow@scsengineers.com Cc:louise.adams handpmg.com Subject:MC013023-10 (230031) Revised (3rd) Final Report, Excel - Polo Rd Property Attachments:MC013023-10 REV3 FINAL.pdf; MC013023-10 REV3 FINAL EXCEL 27 Feb 23 1122.xls Westley, AƩached is the 3rd revised final report and Excel EDD for the January 2023 Polo Road Property project. My apologies again for any confusion. This data has been reviewed again and any appropriate changes made, such as diluƟon factors and the removal of a false posiƟve of 1,3-Dichloropropane reported for sample SG-10. Fell free to contact us if there is anything else we can do to help. Thank you! Lisa Eminhizer Laboratory Director H&P Mobile Geochemistry, Inc. 2470 Impala Drive, Carlsbad, CA O: 760.804.9678 Lisa.Eminhizer@handpmg.com W handpmg.com DOD ELAP, NELAC & CA ELAP Accredited for Analysis NEFAP Certified for Active Soil Vapor & Air Sampling NOTE: This message, including any attachments, contains information that is confidential and may be protected by law from disclosure. Any review, use, distribution or disclosure by anyone other than the intended recipient is strictly prohibited. If you are not the intended recipient, please notify the sender immediately and delete this message from your system. Thank you.