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HomeMy WebLinkAbout8102_Rutherford_South_MSWLF_June2023GW_FID 1817170_20230831ftv[:]Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
$_011It iBa ittL? „Ubm3. gal; Itll7 iIcsn.,.
�..�, .
Name of entity submitting data (laboratory, consultant, facility owner):
SCARLETT GEOPHYSICAL CONSULTING, PC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: E. W. SCARLETT, JR Phone: 919-452-1236
E-mail: wes-scarlett(cDnc.rr.com
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
RUTHERFORD COUNTY SR 2138 81-02 .0500 JUNE 15, 2023
SOUTH LANDFILL FOREST CITY, NC
Environmental Status: (Check all that apply)
Initial/Background Monitoring Q Detection Monitoring
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Si irfara water monitorina data
Assessment Monitoring
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Corrective Action
Notification attached?
8)( No. No groundwater or surface water standards were exceeded.
Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
To the bestTof1 11 my knowledge, the information reported and statements made on this data submittal and attacriments are true ario GOIFIFUGL.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. 1 am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
E. W. SCARLETT, JR PG 919-452-1236
❑—iii , W.— (Print) — Title (Area Code) Telephone Number
AUGUST 25, 2023
Signature Date
500 HEPOWIL TRACE, HILLSBOROUGH, NC 27278
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
Affix NC Licensed/ Professional Geologist Seal
Revised 6/2009
RESULTS OF WATER QUALITY SAMPLING
RUTHERFORD COUNTY SOUTH LANDFILL
PERMIT # 81-02
JUNE 2023
I hereby certify this 25th day of August, 2023, that this report was prepared by me or under my
direct supervision.
ARo
e
SEAL i
o a
681 s
E.W. Scarlett, Jr., P.G. OjQGO��°
+j nee• moe �e
Principal °'••asCAE�;o.0°�°
RESULTS OF WATER QUALITY SAMPLING
RUTHERFORD COUNTY SOUTH LANDFILL
RUTHERFORD COUNTY, N.C.
PERMIT # 81-02
JUNE 2023
SGC PROJECT NUMBER 0001.002
PREPARED FOR
RUTHERFORD COUNTY
AUGUST 25, 2023
SCARLETT GEOPHYSICAL CONSULTING, P.C.
500 Hepowil Trace Telephone: 919-477-9519
Hillsborough, NC 27278 Website: www.searlettgeophysics.com
RESULTS OF WATER QUALITY SAMPLING
RUTHERFORD COUNTY SOUTH LANDFILL
PERMIT # 81-02
JUNE 2023
I hereby certify this 25th day of August, 2023, that this report was prepared by me or under my
direct supervision.
E.W. Scarlett, Jr., P.G.
Principal
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY.................................................................................................1
2.0 INTRODUCTION..............................................................................................................2
3.0 SCOPE OF WORK.............................................................................................................2
4.0 METHODS EMPLOYED...................................................................................................2
4.1 Monitoring Well Sampling......................................................................................2
4.2 Stream Sampling.....................................................................................................3
5.0 RESULTS..........................................................................................................................3
5.1 Groundwater...........................................................................................................3
5.2 Surface Water.........................................................................................................5
6.0 REFERENCES................................................................................................................... 5
TABLES
Table 1 Summary of Monitoring Well Data
Table 2 Ground and Surface Water Sampling Field Data, Rutherford County South Landfill,
June 15, 2023
Table 3 Ground and Surface Water Sampling Results, RCRA Metals, Rutherford County
South Landfill, June 15, 2023
Table 4 Ground and Surface Water Sampling Results, Appendix I Volatile Organics by SW-
846 Method 8260, Rutherford County South Landfill, June 15, 2023
Table 5 Notification Table
FIGURES
Figure 1 Site Location Map
Figure 2 Site Map with Groundwater Contours
APPENDICES
Appendix A Ground and Surface Water Sampling Field Data Sheets
Appendix B Laboratory Reports
RESULTS OF WATER QUALITY SAMPLING
RUTHERFORD COUNTY SOUTH LANDFILL
PERMIT # 81-02
JUNE 15 2023
1.0 EXECUTIVE SUMMARY
Ten monitoring wells and two stream locations at the Rutherford County South Landfill were
sampled on June 15, 2023. All sampling was conducted in accordance with North Carolina Solid
Waste Management Guidelines. The samples were submitted to a North Carolina certified
laboratory and tested for the Federal Appendix I list of volatile organic constituents for detection
monitoring; 1,4-dioxane; and the eight RCRA metals.
Results from ten monitoring well sample analyses show that the concentrations of five RCRA
metals (arsenic in 8102-MW-2A and 8102-MW-5; barium in 8102-MW-8; chromium in 8102-MW-
2A, 8102-MW4A, 8102-MW-7, and 8102-MW-8; lead in 8102-MW-8; and mercury in 8102-MW-
8) exceeded the 15A NCAC 2L (2L) Standard for Class GA groundwater on the date that the
samples were collected. Barium, chromium, lead, and mercury were detected in one or more of the
monitoring well samples at concentrations that did not exceed the 2L Standards.
Results from the ten monitoring well sample analyses show that concentrations of four Appendix I
volatile organic constituents (1,1-dichloroethane in 8102-MW-1; benzene in 8102-MW-1 and
8102-MW-6; methylene chloride in 8102-MW-1; and vinyl chloride in 8102-MW-5) exceeded the
2L Standards on the date that the samples were collected. Concentrations of 1,4-dioxane exceeded
the 2L Standard in 8102-MW-2A, 8102-MW-5, and 8102-MW-6 on the date that samples were
collected. The following Appendix I volatile organic constituents (1,1-dichloroethane; 1,1-
dichloroethene; 1,2-dichloroethane; 1,4-diclorobenzene; acetone; benzene; chlorobenzene;
chloroethane; chloroform; cis-1,2-dichloroethene; total xylenes; and trichloroethene) were detected
in one or more of the monitoring well samples at concentrations that did not exceed the 2L or NC
Groundwater Protection (NCGP) Standards.
June 2023 Report August 25, 2023
Rutherford County South Landfill Page 1
No RCRA metals were detected at concentrations that exceeded the 15A NCAC 2B Standard for
Class B/C Surface Waters (213) in the surface water samples collected from the creek that flows
along the northeast boundary of the landfill property. One RCRA metal that does not have an
established 2B standard (barium) was detected in both surface water samples. No Appendix I
volatile organic constituents were detected in either surface water sample. 1,4-Dioxane was
detected in 8102-SW-2 at 3.7 ppb.
2.0 INTRODUCTION
Scarlett Geophysical Consulting, P.C. (SGC) was contracted by Rutherford County, North
Carolina, to sample the ground and surface water at ten monitoring well and two surface water
locations on or adjacent to the South Landfill property. The site location is shown on Figure 1.
3.0 SCOPE OF WORK
The scope of work for this sampling event was to sample ten monitoring wells and two stream
locations for Federal Appendix I volatile organic constituents as listed in 40 CFR, Part 258, and the
eight RCRA metals, and to prepare and submit reports to the client and NC Division of Solid
Waste Management documenting the sample collection procedures and analytical results.
4.0 METHODS EMPLOYED
4.1 Monitoring Well Sampling
Groundwater sampling took place on October 19, 2022. Water levels were measured in each well
to provide data for water volume calculations (Table 1). The wells were then purged by removing
a minimum of three well volumes or bailing the wells dry prior to obtaining water samples. The
water samples were collected using properly decontaminated bailers. Immediately upon collection,
the water samples were field tested for temperature, specific conductance, and pH. These data are
summarized in Table 2. Field data sheets are included as Appendix A. Samples were placed in
laboratory cleaned and supplied containers, packed on ice, and placed under chain -of -custody.
Samples were shipped to the laboratory under chain -of -custody upon completion of the field work.
June 2023 Sampling Report August 25, 2023
Rutherford County South Landfill Page 2
Analyses were conducted by Pace Analytical Laboratories, a North Carolina certified laboratory.
The monitoring well locations are shown on Figure 2.
4.2 Stream Sampling
Surface water sampling took place on October 19, 2022. Samples 8102-SW-1 and 8102-SW-2
were collected from a stream that flows southeastward along the northeast boundary of the South
Landfill property. This stream flows into the Second Broad River, which bounds the landfill to the
east. All stream samples were analyzed for the same parameters as the ground water samples. The
stream sample locations are shown on Figure 2.
5.0 RESULTS
The results of the laboratory analyses are summarized in Tables 3 and 4, and the complete
laboratory reports are included as Appendix B.
5.1 Groundwater
The groundwater sample analyses revealed nine constituents that had concentrations at or above
the 2L Standards in one or more of the ten wells sampled. These analytical results are listed below
and shown in the Notification Table (Table 5).
• Arsenic was detected in 8102-MW-2A at 17.2 ppb. The 2L Standard is 10.0 ppb.
• Chromium was detected in 8102-MW-2A at 13.6 ppb, 8102-MW-4A at 18.4 ppb, and 8102-
MW-7 at 13.7 ppb. The 2L Standard is 10.0 ppb.
• Mercury was detected in 8102-MW-8 at 5.8 ppb. The 2L Standard is 1.0 ppb.
• 1, 1 -Dichloro ethane was detected in 8102-MW-1 at 45.1 ppb and 8102-MW-8 at 6.9 ppb.
The 2L Standard is 6.0 ppb.
• 1,4-Dioxane was detected in 8102-MW-2A at 17.0 ppb, 8102-MW-5 at 19.0 ppb, 8102-
MW-6 at 33.4 ppb, and 8102-MW-7 at 15.6 ppb. The 2L Standard is 3.0 ppb.
June 2023 Report August 25, 2023
Rutherford County South Landfill Page 3
• Benzene was detected in 8102-MW-1 at 2.4 ppb and 8102-MW-6 at 2.0 ppb. The 2L
Standard is 1.0 ppb.
• Methylene Chloride was detected in 8102-MW-1 at 13.6 ppb. The 2L Standard is 5.0 ppb.
• Vinyl chloride was detected in 8102-MW-5 at 0.39 ppb. The 2L Standard is 0.03 ppb.
The following constituents were detected in one or more of the wells at concentrations above the
method detection limits (MDL) but below the 2L or NCGP Standards.
• Arsenic
• Barium
• Chromium
• Lead
• Mercury
• Selenium
• 1, 1 -Dichloro ethane
• 1,1-Dichloroethene
• 1,2-Dichloroethane
• 1,4-Dichlorobenzene
• Benzene
• Chlorobenzene
• Chloroethane
• Chloroform
• cis-1,2-Dichloroethene
• Total xylene
The volatile organic constituents present in the groundwater samples are likely due to past waste
disposal; however, contributions by ongoing farming activities immediately north and south of the
old property boundaries and vehicles involved in active maintenance of the landfill cover cannot be
ruled out. Groundwater flow direction data indicate that all groundwater from the disposal area is
intercepted by perennial streams to the north, south, and east. There is no evidence indicating that
volatile organic constituent concentrations resulting from waste disposal at South Landfill
currently exceed the 2L or NCGP Standards at locations beyond the property boundaries. The
June 2023 Sampling Report August 25, 2023
Rutherford County South Landfill Page 4
interval since the last waste disposal suggests that significant impacts on groundwater
contamination from the source area are unlikely to increase in the future.
The inorganic constituents present in the groundwater samples may have been influenced by past
waste disposal, but it is likely that local geology also has an impact. 8102-MW-4A, which is
upgradient from the waste disposal area (see Figure 2), shows minimal volatile organic impact, yet
historically has shown inorganic constituent concentrations similar to those in the downgradient
monitoring wells. For this and previous events, the impact of RCRA metals was significantly
greater in 8102-MW-4A than in the downgradient wells. The presence of measurable
concentrations of barium in the upgradient surface water sample for this event in addition to
cadmium, chromium, lead, mercury, silver, and selenium during prior events suggests the likely
influence of contributions from off site sources (local geological and/or cultural).
5.2 Surface Water
The surface water sample analyses did not reveal any constituents that had concentrations at or
above the 2B Standards.
The constituent (listed below) for which no 2B Standard has been established was detected at
concentrations above the MDL.
• Barium in 8102-SW-1 and 8102-SW-2
6.0 REFERENCES
Department of Environment, Health and Natural Resources, Division of Solid Waste Management,
Solid Waste Section, NC Solid Waste Program, Environmental Monitoring Constituent List
(downloaded June 1, 2012).
North Carolina Administrative Code, Title 15A, Department of Environment and Natural
Resources, Division of Water Quality, Subchapter 2L, Sections .0100, .0200, and .0300,
June 2023 Report August 25, 2023
Rutherford County South Landfill Page 5
Classifications and Water Quality Standards Applicable to the Groundwaters of North Carolina,
(April 1, 2005, Amended July 1, 2021); from the Environmental Management Commission,
Raleigh, North Carolina.
North Carolina Administrative Code Section: 15A NCAC 2B .0200, Department of Environment,
and Natural Resources, Division of Water Quality, Classifications and Water Quality Standards
Applicable to Surface Waters and Wetlands of North Carolina, Section .0200 (May 1, 2007); from
the Environmental Management Commission, Raleigh, North Carolina.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural
Resources, Division of Solid Waste Management, Subchapter 13B, Solid Waste Management,
Section .1600 (August 27, 2001).
North Carolina Solid Waste Section Memorandum Regarding New Guidelines for Electronic
Submittal of Environmental Data, October 27, 2006.
Addendum to October 27, 2006, North Carolina Solid Waste Section Memorandum Regarding New
Guidelines for Electronic Submittal of Environmental Data, February 23, 2007.
North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities,
Department of Environment, Health and Natural Resources, Division of Solid Waste Management,
Solid Waste Section, (January 2000), Download from NCSW Web Site.
North Carolina Solid Waste Section Memorandum, 1,4-Dioxane Analysis, Solid Waste Section
Limits and Laboratory Analytical Methods, May 29, 2018.
June 2023 Sampling Report August 25, 2023
Rutherford County South Landfill Page 6
TABLE 1
SUMMARY OF MONITORING WELL DATA
RUTHERFORD COUNTY SOUTH LANDFILL
RUTHERFORD COUNTY, NORTH CAROLINA
Well Number
Elevation (ft)
Top of Casing
Depth of Well (ft)
Static Water Levels
June 15, 2023
Depth (ft)2
Elevation (ft)
8102-MW-1
811.88
37.58
29.16
782.72
8102-MW-2A
790.40
45.21
31.06
759.34
8102-MW-3
783.42
19.00
15.50
767.92
8102-MW-4A
845.17
30.35
23.36
821.81
8102-MW-5
765.32
20.13
11.25
754.07
8102-MW-6
801.87
37.00
27.66
774.21
8102-MW-7
770.68
30.30
14.48
756.20
8102-MW-8
813.03
42.30
31.22
781.81
8102-MW-9D
764.28
67.70
6.06
758.22
8102-MW-9S
763.93
24.85
6.61
757.32
Notes:
Elevations determined by survey: Burnt Chimney Surveying, Forest City, NC
2 Depths measured from top of casing by Scarlett Geophysical Consulting, P.C.
RuthSouthTables-0623
TABLE 2
GROUND AND SURFACE WATER SAMPLING FIELD DATA
RUTHERFORD COUNTY SOUTH LANDFILL
JUNE 15, 2023
Field Parameter
Sample No.
8102-MW-1
8102-MW-2A
8102-MW-3
8102-MW-4A
8102-MW-5
8102-MW-6
8102-MW-7
8102-MW-8
Temperature
17.0°C
17.5°C
16.3 °C
16.5°C
16.2°C
17.9°C
17.8°C
17.5°C
Specific Conductance
55.4 pmhos/cm
192.5 pmhos/cm
82.3 pmhos/cm
41.3 pmhos/cm
448.0 pmhos/cm
865.0 pmhos/cm
42.4 pmhos/cm
38.2 pmhos/cm
pH
5.10
5.92
5.45
5.06
6.38
6.42
5.20
5.27
Field Parameter
Sample No.
8102-MW-9D
8102-MW-9S
8102-SW-1
8102SW-2
Temperature
17.2°C
15.8°C
18.4°C
18.2°C
Specific Conductance
43.5 pmhos/cm
36.8 pmhos/cm
55.4 pmhos/cm
80.2 pmhos/cm
_pH
5.78
6.48
6.78
6.73
NA - Not analyzed
Ruth SouthTables-0623
TABLE 3
GROUND AND SURFACE WATER SAMPLING RESULTS
RCRA METALS
RUTHERFORD COUNTY SOUTH LANDFILL
PERMIT # 81-02
JUNE 15, 2023
Compound
Sample No.
15A NCAC 2L
Standards for Class
GA Ground Water
15A NCAC 2B
Standards for Class
B, C Surface Waters
8102-MW-1
8102-MW-2A
8102-MW-3
8102-MW-4A
8102MW-5
8102-MW-6
8102-MW-7
8102-MW-8
8102-MW-9D
8102-MW-9S
8102-SW-1
8102-SW-2
Arsenic, Total
BQL
19.40
BQL
BQL
12 30'
BQL
BQL
BQL
BQL
BQL
BQL
BQL
10.0
50.0
Barium, Total
179.00
180.00
45.10
127.00
176.00
33.80
108.00
714.00
26.50
50.60
29.00
29.80
700.0
Cadmium, Total
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
2.0
2.0
Chromium, Total
8.60
12.90
BQL
15.10
BQL
BQL
21.60 '
12.66
BQL
BQL
BQL
BQL
10.0
50.0
Lead, Total
5.20
BQL
BQL
11.10
BQL
BQL
5.90
30.56
BQL
BQL
BQL
BQL
15.0
25.0
Mercury, Total
0.91
BQL
BQL
0.78
BQL
BQL
0.12
7.30'
BQL
BQL
BQL
BQL
1.0
0.012
Selenium, Total
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
20.0
5.0
Silver, Total
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
20.0
0.06
Notes:
• All results in parts per billion (ppb)
• BQL - Below Method Detection Limit
Shaded cells„ denote concentrations that exceed 15A NCAC 2L Standards for Class GA
Groundwater (MW data) or 15A NCAC 2B Standards for Class B surface waters (SW data)
• ' - Standard not established
• �'� - Action Level
• NS - Not Sampled (Dry Well)
RuthSouthTables-0623
TABLE 4
GROUND AND SURFACE WATER SAMPLING RESULTS
APPENDIX I VOLATILE ORGANICS BY SW-846 METHOD 8260
RUTHERFORD COUNTY SOUTH LANDFILL
PERMIT # 81-02
JUNE 15, 2023
COMPOUND
Sam le No.
15A NCAC 2L
Standards for Class
GA Ground Water
NC Groundwater
Protection
Standards
15A NCAC 2B
Standards for Class
B, C Surface Water
8102-MW-1
8102-MW-2A
8102-MW-3
8102-MW-4A
8102-MW-5
8102-MW-6
8102-MW-7
8102-MW-8
8102-MW-9D
8102-MW-9S
8102-SW-1
8102-SW-2
1,1,1,2-Tetrachloroethane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
1.0
1,1,1-Trichloroethane
BOL
BQL
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BOL
BQL
200.0
1,1,2,2-Tetrachloroethane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
1.0
1,1,2-Trichloroethane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.6
'
1,1-Dichloroethane
66.'90
BQL
BQL
BQL
1.50
0.37
BQL
3.50
BQL
BQL
BQL
BQL
6.0
1,1-Dichloroethene'
1.40
BQL
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
350.0
1,2,3-Tdchloro ro ane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.005
1,2-Dibromo-3-Chloro ro ane
BQL
BQL
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.04
1,2-Dibromoethane'
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.02
1,2-Dichlorobenzene'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
20.0
1,2-Dichloroethane'
0.32
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.4
1,2-Dichloropropane'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.6
1,4-Dichlorobenzene'
2.00
1.60
BQL
BQL
1.20
1.60
BQL
BQL
BQL
BQL
BQL
BQL
6.0
1,4-Dioxane
0.86
11.10
BQL
BQL
111.30 "
" 46.001,
BQL
BQL
BQL
BQL
BQL
3.70
3.0
2 - Butanone MEK
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
4,000.0
2-Hexanone'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
40.0
4-Methyl-2-pentanone'
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
*
560.0
Acetone
BOL
BQL
BQL
107.00
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
6,000.0
Acrylonitrile
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Benzene
2.20
0.34
BQL
BQL
0.34
1.30
BQL
BQL
BQL
BQL
BQL
BQL
1.0
Bromochloromethane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
*
0.6
Bromodichloromethane
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.6
'
Bromoform
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
4.0
Bromomethane'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
10.0
Carbon Disulfide
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
700.0
Carbon Tetrachloride
BQL
BQL
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.3
Chlorobenzene
2.30
4.70
BQL
BQL
1.20
3.20
BQL
BQL
BQL
BQL
BQL
BQL
50.0
Chloroethane
7.80
0.65
BQL
BQL
1.20
BQL
BQL
BQL
BQL
BQL
BQL
BQL
3,000.0
'
Chloroform
1.10
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
70.0
Chloromethane'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
3.0
cis-1,2-Dichloroethene
7.60
0.38
BQL
BQL
3.20
1.80
BQL
BQL
BQL
BQL
BQL
BQL
70.0
cis-1,3-Dichloro ro ene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.4
Dibromochloromethane'
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.4
0.41
Dibromomethane'
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
70.0
Ethylbenzene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
600.0
Methyl iodide
BQL
BQL
BOL
BQL
BOL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Methylene Chloride
26.80
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
5.0
Styrene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
70.0
'
Tetrachloroethene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.7
Toluene
BQL
BQL
BQL
BOL
BQL
BOL
BQL
BOL
BQL
BOL
BQL
BOL
600.0
*
11.0
Total Xylenes
4.90
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
500.0
trans-1,2-Dichloroethene
BQL
BQL
BQL
BOL
BQL
BQL
BQL
BOL
BQL
BQL
BQL
BQL
100.0
trans-1,3-Dichloro ro ene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.4
trans-1,4-Dichloro-2-butene
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Trchloroethene
0.38
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
3.0
Trichlorofluoromethane'
BOL
BQL
BQL
BQL
BQL
BQL
BOL
BQL
BOL
BQL
BQL
BQL
2,000.0
Vinyl acetate
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
*
88.0
Vinyl chloride
BQL
BQL
BQL
BQL
'0.39
BQL
BQL
BQL
BQL
BQL
BQL
BQL
0.03
Notes:
• All results in parts per billion (ppb)
• BQL - Below Method Detection Limit
• * - Standard not established
Shaded cells denote concentrations that equal or exceed 2L, Groundwater Protection,
or 2B (Class B/C) Standards
• NS - Not Sampled (Dry Well)
• 1,4-Dioxane added to constituent list Oct 2018
' Synonyms:
1,1-Dichloroethene = Vinylidene Chloride
1,2-Dibromoethane = Ethylene Dibromide
1,2-Dichloroethane = Ethylene Dichloride
1,2-Dichloropropane = Propylene Dichloride
1,4-Dichlorobenzene = p Dichlorobenzene
4-Methyl-2-Pentanone = Methyl Isobutly Keytone
Bromomethane - Methyl Bromide
Dibromochloromethane = Chlorodibromomethane
Dibromomethane = Methylene Bromide
Methylene Chloride = Dichloromethane
RuthSouthTa bles-0623
TABLE 5
NOTIFICATION TABLE
CONSTITUENTS DETECTED AT OR ABOVE GROUND AND SURFACE WATER STANDARDS
RUTHERFORD COUNTY SOUTH LANDFILL (PERMIT # 81-02)
JUNE 15, 2023
COMPOUND
Sample Location
15A NCAC 2L
Standards for Class
GA Ground Water
NC Groundwater
Protection
Standards
15A NCAC 2B
Standards for Class
B, C Surface Water
8102-MW-1
8102-MW-2A
8102-MW-3
8102-MW-4A
8102-MW-5
8102-MW-6
8102-MW-7
8102-MW-8
8102-MW-9D
8102-MW-9S
8102-SW-1
8102-SW-2
Arsenic, Total
19.4
12.3
10.0
50.0
Barium
714.0
700.0
"
Chromium, Total
12.8„
35.7,
21.6
12.6
10.0
50.0
Lead
39.5
15.0
"
Mercury
7.3
1.0
0.012
1, 1 -Dichloroethane
65.9
11
6.0
1,4-Dioxane
11.1
11.3
46.0
3.0
Benzene
2.2
1.3
1.0
Meth ene Chloride
26.8'
5.0
Vinyl Chloride
0.39
0.03
Notes:
• All results in parts per billion (ppb)
• * - Standard not established
-Shaded cells denote concentrations that equal or exceed 2L, Groundwater Protection, or 2B (Class B/C) Standards
Ell - Action Level
RuthSouthTa bles-0623
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SCALE IN FEET
SOUTH SANITARY LANDFILL
RUTHERFORD COUNTY, NORTH CAROLINA
SCARLETT GEOPHYSICAL CONSULTING, P.C.
SITE LOCATION MAP
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SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-1
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
1100 to 1117
Sample Date:
June 15, 2023
Sample Time:
1125
Sampled by:
K. Vanhoy
Weather:
Sunny, 77°F
29.16 ft.
3 7.5 8 ft.
8.42 ft.
Teflon bailer
Teflon bailer
1.37 gal.
4.1 gal.
YES: _ NO: X
17.0°C
55.4 µmhos/cm
5.10
Cloudy, aW, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location:
Rutherford County South
Purge Date:
June 15, 2023
Source/Well:
8102-MW-2A
Purge Time:
1223 to 1241
Locked:
Yes X No _
Sample Date:
June 15, 2023
PVC X
Steel _ Stainless Steel _
Sample Time:
1250
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Sampled by: K. Vanhoy
Weather: Sunny, 80°F
31.06 ft.
45.21 ft.
14.15 ft.
Teflon bailer
Teflon bailer
1.22 gal.
6.9 gal.
YES _ NO X
17.5°C
192.5 µmhos/cm
5.92
Cloud gray, septic odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-3
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
I ) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
1408 to 1411
Sample Date:
June 15, 2023
Sample Time:
1420
Sampled by:
E. W. Scarlett
Weather:
Sunny, 85°F
15.50 ft.
19.00 ft.
3.50 ft.
Teflon bailer
Teflon bailer
0.57 gal.
1.7 gal.
YES NO X
16.3°C
82.3 µmhos/cm
5.45
Clear, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-4A
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
1340 to 1410
Sample Date:
June 15, 2023
Sample Time:
1400
Sampled by:
E. W. Scarlett
Weather:
Sunny, 82°F
23.36 ft.
3 0.3 5 ft.
6.99 ft.
Teflon bailer
Teflon bailer
1.14 gal.
3.4 gal.
YES NO X
16.5°C
41.3 µmhos/cm
5.06
Cloudy, tan, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-5
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
0928 to 0936
Sample Date:
June 15, 2023
Sample Time:
0945
Sampled by:
K. Vanhoy
Weather:
Sunny, 70°F
11.25 ft.
20.13 ft.
8.88 ft.
Teflon bailer
Teflon bailer
1.45 gal.
4.4 gal.
YES _ NO X
16.2°C
448.0 µmhos/cm
6.38
Cloudy, reddish -tan, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-6
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Note: Only two VOAs for 8260. One arrived broken.
Purge Date:
June 15, 2023
Purge Time:
1312 to 1325
Sample Date:
June 15, 2023
Sample Time:
1335
Sampled by:
K. Vanhoy
Weather:
Sunny, 83°F
27.66 ft.
37.00 ft.
9.34 ft.
Teflon bailer
Teflon bailer
1.52 gal.
4.6 gal.
YES NO X
17.9°C
865.0 µmhos/cm
6.42
Cloudy, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-7
Locked: Yes No X
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
1230 to 1249
Sample Date:
June 15, 2023
Sample Time:
1250
Sampled by:
E. W. Scarlett
Weather:
Sunny, 77°F
14.48 ft.
3 0.3 0 ft.
15.82 ft.
Teflon bailer
Teflon bailer
2.58 gal.
7.7 gal.
YES _ NO X
17.8°C
42.4 µmhos/cm
5.20
Cloudy, tan, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-8
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
1100 to 1120
Sample Date:
June 15, 2023
Sample Time:
1125
Sampled by:
E, W. Scarlett
Weather:
Sunny, 77°F
31.22 ft.
42.30 ft.
11.08 ft.
Teflon bailer
Teflon bailer
1.81 gal.
5.4 gal.
YES _ NO X
17.5°C
38.2 µmhos/cm
5.27
Muddy, brown, septic odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-9D
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
0924 to 0954
Sample Date:
June 15, 2023
Sample Time:
0954
Sampled by:
E. W. Scarlett
Weather:
Sunny, 70°F
6.06 ft.
67.70 ft.
61.64 ft.
Pump
Teflon bailer
10.05 gal.
30+ gal.
YES _ NO X
17.2 °C
43.5 µmhos/cm
5.78
Clear. No odor.
SCARLETT GEOPHYSICAL CONSULTING, P. C.
GROUNDWATER SAMPLING FIELD DATA
Location: Rutherford County South
Source/Well: 8102-MW-9S
Locked: Yes X No
PVC X Steel Stainless Steel
Measuring point description:
Top of PVC Casing
Water Level and Well Data
1) Depth to water from measuring point
2) Depth to well bottom from measuring point
3) Height of water column (h)
Well Purging and Sample Collection
1) Purge Method
2) Sample Method
3) Volume of water in well
1" well .... (v = 0.041 x h)
X 2" well .... (v = 0.163 x h)
4" well .... (v = 0.651 x h)
6" well .... (v = 1.5 x h)
4) Volume of water removed prior to sampling
5) Was well purged DRY?
Field Analysis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
Purge Date:
June 15, 2023
Purge Time:
0940 to 0955
Sample Date:
June 15, 2023
Sample Time:
1000
Sampled by:
E. W. Scarlett
Weather:
Sunny, 70°F
6.61 ft.
24.85 ft.
18.44 ft.
Teflon bailer
Teflon bailer
2.97 gal.
8.9 gal.
YES _ NO X
15.8°C
36.8 µmhos/cm
6.48
Cloudy, tan, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
SURFACE WATER SAMPLING FIELD DATA
Location: Rutherford County South Sample Date: June 15, 2023
Source/Well: 8102-SW-1 Sample Time: 1035
Sampled by: K. Vanhoy Weather: Sunny, 70°F
Field Analvsis
1) Temperature 18.4°C
2) Specific Conductance 55.4 µmhos/cm
3) pH 6.78
4) Physical Appearance and Odor Clear, no odor
SCARLETT GEOPHYSICAL CONSULTING, P. C.
SURFACE WATER SAMPLING FIELD DATA
Location: Rutherford County South Sample Date: June 15, 2023
Source/Well: 8102-SW-2 Sample Time: 1010
Sampled by: K. Vanhoy Weather: Sunny, 70°F
Field Analvsis
1) Temperature
2) Specific Conductance
3) pH
4) Physical Appearance and Odor
18.2°C
80.2 µmhos/cm
6.73
Slightly, no odor
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DC#_T€tle: ENV-FRM-HUN1-0083 02_Sampie Condition Upon Receipt
ace,
Id1G SfIYC?l
Effective Date: 11/14/2022 8:18.30 AM
Laboratory refelving samples:
Asheville I Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[:] Atlanta❑ Kernersville❑
Client Name:
Upon Receipt C—�
Project ff:
Tr t� e�
Courier: LJFedEx uUPs L_.tUsP5 Uclient
❑ Commercial IKace ❑Other!-__
Custody Seal Present? Oyes )gNo Seals Intact? ❑Yes �No IQ R
Date/initials Person Examining Contents:_
Packing Material: ❑ Bubble Wrap Bubble Bags ElNone ❑ Other Biological Tissue Frozen?
Thermometer: V []Yeses []No ❑ N/A
❑ IR Gun ID. IQia Type of Ice: �Qel
1 Correction Factor:
Cooler Temp: - �' S Add/5ubtract ('C) C)
Cooler Temp Corrected ('C): �.
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United Slates: CA, NY, or SC
fcherk mansi? ❑Yes ❑No
❑ Blue ❑ None
Temp should be above freezing to 6'C
❑ Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (Internationally,
includine Hawaii and Puerto Ricol? ❑Yes ❑ No
Comments/Discrepancy:
Chain of Custody Present?
Me,
❑ No
:J N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
No
❑ WA
3.
Rush Turn Around Time Requested?
❑ Yes
o
❑NIA
4.
Sufficient Volume?
Yes
❑No
❑NIA
S.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑No
❑No
❑NIA
❑N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7
Dissolved analysis. Samples Field Filtered?
❑Yes
tft
❑N/A
a.
Sample Labels Match COC?
-includes Date/Ttme/ID/Analysis Matrix:
®Yes
T
❑No
❑H/A
9
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
#fW
o
❑ N/A
❑N/A
11,
COMMENTS/SAMPLE DISCREPANCY f` Field Data Required? UYes U No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: _. . _..._.. _.. _ ...._ Date/Time:
Project Manager SCURF Review: Date:
Project Manager S R F Review: Date:
DC# Title: ENV-FRM-HUN1-0083 02- Sample Condition Upon Receipt
l41 SIG;SlrFiff
Effective Date- 11/14/2022 8:18:30 AM
*Check mark top half of box If pH and/or dechlorination is verified and project N
within the acceptance range for preservation samples.
Exceptions; VOA, Collfornt, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
;* Bottom half of box Is to list number of bottles
' * "`Check jJ1 unpreserved Nitrates for chlorine
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pH adjustment
Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot A
i
Note. Whenever there " sad1 screpancyaffectingNarth Carolina compliancesamples, a copy oft his form wiU be sent to the North Carolira DENRCerbrcat!Dn Office (i e.
Out of hold, incorrect preservative, out of temp, incorrect Containers.
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
June 30, 2023
Wes Scarlett
Scarlett Geophysical
500 Heporwil Trace
Hillsborough, NC 27278
RE: Project: Rutherford South
Pace Project No.: 92673197
Dear Wes Scarlett:
Enclosed are the analytical results for sample(s) received by the laboratory on June 19, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
stephanie.knott@pacelabs.com
704-977-0981
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 55
lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Rutherford South
92673197
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92673197001
MW-1
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197002
MW-2A
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197003
MW-3
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
SAS
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197004
MW-4A
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197005
MW-5
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197006
MW-6
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197007
MW-7
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197008
MW-8
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197009
MW-9S
EPA 6010D
DBB1
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197010
MW-91)
EPA 6010D
DBB1
7
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
SAMPLE ANALYTE COUNT
Project:
Rutherford South
Pace Project No.:
92673197
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197011
SW-1
EPA 6010D
D661
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
92673197012
SW-2
EPA 6010D
D661
7
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 8260D
CL
52
PASI-C
EPA 8260D Mod.
TEG
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MWA
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197001 Collected: 06/15/23 11:25 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:43
7440-38-2
Barium
179
ug/L
3.5
1
06/21/2310:50
06/22/2314:43
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/21/2310:50
06/22/2314:43
7440-43-9
Chromium
8.6
ug/L
3.7
1
06/21/2310:50
06/22/2314:43
7440-47-3
Lead
5.2
ug/L
4.5
1
06/21/2310:50
06/22/2314:43
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:43
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/21/2310:50
06/22/2314:43
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
0.91
ug/L
0.12
1
06/26/2313:03
06/27/2312:52
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/23/23 21:05
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 21:05
107-13-1
Benzene
2.2
ug/L
0.34
1
06/23/23 21:05
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 21:05
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 21:05
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 21:05
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 21:05
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 21:05
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 21:05
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 21:05
56-23-5
Chlorobenzene
2.3
ug/L
0.28
1
06/23/23 21:05
108-90-7
Chloroethane
7.8
ug/L
0.65
1
06/23/23 21:05
75-00-3
Chloroform
1.1
ug/L
0.43
1
06/23/23 21:05
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 21:05
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 21:05
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 21:05
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 21:05
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 21:05
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 21:05
95-50-1
1,4-Dichlorobenzene
2.0
ug/L
0.33
1
06/23/23 21:05
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 21:05
110-57-6
1,1-Dichloroethane
65.9
ug/L
0.37
1
06/23/23 21:05
75-34-3
1,2-Dichloroethane
0.32
ug/L
0.32
1
06/23/23 21:05
107-06-2
1,1-Dichloroethene
1.4
ug/L
0.35
1
06/23/23 21:05
75-35-4
cis-1,2-Dichloroethene
7.6
ug/L
0.38
1
06/23/23 21:05
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 21:05
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 21:05
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 21:05
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 21:05
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 21:05
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 21:05
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v3
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-1 Lab ID: 92673197001 Collected: 06/15/23 11:25 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
lodomethane
<9.7
ug/L
9.7
1
06/23/23 21:05
74-88-4
Methylene Chloride
26.8
ug/L
2.0
1
06/23/23 21:05
75-09-2
4-Methyl-2-pentanone (MIBK)
<2.7
ug/L
2.7
1
06/23/23 21:05
108-10-1
Styrene
<0.29
ug/L
0.29
1
06/23/23 21:05
100-42-5
1,1,1,2-Tetrachloroethane
<0.31
ug/L
0.31
1
06/23/23 21:05
630-20-6
1,1,2,2-Tetrachloroethane
<0.22
ug/L
0.22
1
06/23/23 21:05
79-34-5
Tetrachloroethene
<0.29
ug/L
0.29
1
06/23/23 21:05
127-18-4
Toluene
<0.24
ug/L
0.24
1
06/23/23 21:05
108-88-3
1,1,1-Trichloroethane
<0.33
ug/L
0.33
1
06/23/23 21:05
71-55-6
1,1,2-Trichloroethane
<0.32
ug/L
0.32
1
06/23/23 21:05
79-00-5
Trichloroethene
0.38
ug/L
0.38
1
06/23/23 21:05
79-01-6
Trichlorofluoromethane
<0.30
ug/L
0.30
1
06/23/23 21:05
75-69-4
1,2,3-Trichloropropane
<0.26
ug/L
0.26
1
06/23/23 21:05
96-18-4
Vinyl acetate
<1.3
ug/L
1.3
1
06/23/23 21:05
108-05-4
Vinyl chloride
<0.39
ug/L
0.39
1
06/23/23 21:05
75-01-4
Xylene (Total)
4.9
ug/L
0.34
1
06/23/23 21:05
1330-20-7
m&p-Xylene
<0.71
ug/L
0.71
1
06/23/23 21:05
179601-23-1
o-Xylene
4.9
ug/L
0.34
1
06/23/23 21:05
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/23/23 21:05
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
06/23/23 21:05
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
06/23/23 21:05
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
0.86
ug/L
0.86
1
06/21/23 23:03
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
120
%
67-130
1
06/21/23 23:03
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
06/21/23 23:03
2037-26-5
Date: 06/30/2023 04:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-2A
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197002 Collected: 06/15/23 12:50 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
19.4
ug/L
4.7
1
06/21/2310:50
06/22/2314:46
7440-38-2
Barium
180
ug/L
3.5
1
06/21/2310:50
06/22/2314:46
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/21/2310:50
06/22/2314:46
7440-43-9
Chromium
12.8
ug/L
3.7
1
06/21/2310:50
06/22/2314:46
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/21/2310:50
06/22/2314:46
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:46
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/21/2310:50
06/22/2314:46
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2312:54
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/23/23 21:23
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 21:23
107-13-1
Benzene
0.34
ug/L
0.34
1
06/23/23 21:23
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 21:23
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 21:23
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 21:23
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 21:23
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 21:23
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 21:23
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 21:23
56-23-5
Chlorobenzene
4.7
ug/L
0.28
1
06/23/23 21:23
108-90-7
Chloroethane
0.65
ug/L
0.65
1
06/23/23 21:23
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/23/23 21:23
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 21:23
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 21:23
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 21:23
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 21:23
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 21:23
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 21:23
95-50-1
1,4-Dichlorobenzene
1.6
ug/L
0.33
1
06/23/23 21:23
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 21:23
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/23/23 21:23
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/23/23 21:23
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/23/23 21:23
75-35-4
cis-1,2-Dichloroethene
0.38
ug/L
0.38
1
06/23/23 21:23
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 21:23
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 21:23
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 21:23
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 21:23
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 21:23
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 21:23
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-2A Lab ID: 92673197002 Collected: 06/15/23 12:50 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
lodomethane
<9.7
ug/L
9.7
1
06/23/23 21:23
74-88-4
Methylene Chloride
<2.0
ug/L
2.0
1
06/23/23 21:23
75-09-2
4-Methyl-2-pentanone (MIBK)
<2.7
ug/L
2.7
1
06/23/23 21:23
108-10-1
Styrene
<0.29
ug/L
0.29
1
06/23/23 21:23
100-42-5
1,1,1,2-Tetrachloroethane
<0.31
ug/L
0.31
1
06/23/23 21:23
630-20-6
1,1,2,2-Tetrachloroethane
<0.22
ug/L
0.22
1
06/23/23 21:23
79-34-5
Tetrachloroethene
<0.29
ug/L
0.29
1
06/23/23 21:23
127-18-4
Toluene
<0.24
ug/L
0.24
1
06/23/23 21:23
108-88-3
1,1,1-Trichloroethane
<0.33
ug/L
0.33
1
06/23/23 21:23
71-55-6
1,1,2-Trichloroethane
<0.32
ug/L
0.32
1
06/23/23 21:23
79-00-5
Trichloroethene
<0.38
ug/L
0.38
1
06/23/23 21:23
79-01-6
Trichlorofluoromethane
<0.30
ug/L
0.30
1
06/23/23 21:23
75-69-4
1,2,3-Trichloropropane
<0.26
ug/L
0.26
1
06/23/23 21:23
96-18-4
Vinyl acetate
<1.3
ug/L
1.3
1
06/23/23 21:23
108-05-4
Vinyl chloride
<0.39
ug/L
0.39
1
06/23/23 21:23
75-01-4
Xylene (Total)
<0.34
ug/L
0.34
1
06/23/23 21:23
1330-20-7
m&p-Xylene
<0.71
ug/L
0.71
1
06/23/23 21:23
179601-23-1
o-Xylene
<0.34
ug/L
0.34
1
06/23/23 21:23
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/23/23 21:23
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
06/23/23 21:23
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
06/23/23 21:23
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
11.1
ug/L
0.86
1
06/21/23 23:24
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
120
%
67-130
1
06/21/23 23:24
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
06/21/23 23:24
2037-26-5
Date: 06/30/2023 04:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-3
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197003 Collected: 06/15/23 14:20 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:49
7440-38-2
Barium
45.1
ug/L
3.5
1
06/21/2310:50
06/22/2314:49
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/21/2310:50
06/22/2314:49
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/21/2310:50
06/22/2314:49
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/21/2310:50
06/22/2314:49
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:49
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/21/2310:50
06/22/2314:49
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:01
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/27/23 13:21
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/27/23 13:21
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/27/23 13:21
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/27/23 13:21
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/27/23 13:21
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/27/23 13:21
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/27/23 13:21
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/27/23 13:21
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/27/23 13:21
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/27/23 13:21
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/27/23 13:21
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/27/23 13:21
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/27/23 13:21
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/27/23 13:21
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/27/23 13:21
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/27/23 13:21
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/27/23 13:21
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/27/23 13:21
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/27/23 13:21
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/27/23 13:21
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/27/23 13:21
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/27/23 13:21
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/27/23 13:21
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/27/23 13:21
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/27/23 13:21
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/27/23 13:21
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/27/23 13:21
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/27/23 13:21
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/27/23 13:21
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/27/23 13:21
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/27/23 13:21
591-78-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-3 Lab ID: 92673197003 Collected: 06/15/23 14:20 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
98
%
103
%
101
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
123
%
107
%
9.7
1
06/27/23 13:21
74-88-4
2.0
1
06/27/23 13:21
75-09-2
2.7
1
06/27/23 13:21
108-10-1
0.29
1
06/27/23 13:21
100-42-5
0.31
1
06/27/23 13:21
630-20-6
0.22
1
06/27/23 13:21
79-34-5
0.29
1
06/27/23 13:21
127-18-4
0.24
1
06/27/23 13:21
108-88-3
0.33
1
06/27/23 13:21
71-55-6
0.32
1
06/27/23 13:21
79-00-5
0.38
1
06/27/23 13:21
79-01-6
0.30
1
06/27/23 13:21
75-69-4
0.26
1
06/27/23 13:21
96-18-4
1.3
1
06/27/23 13:21
108-05-4
0.39
1
06/27/23 13:21
75-01-4
0.34
1
06/27/23 13:21
1330-20-7
0.71
1
06/27/23 13:21
179601-23-1
0.34
1
06/27/23 13:21
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/27/23 13:21 460-00-4
06/27/23 13:21 17060-07-0
06/27/23 13:21 2037-26-5
[eI:If��ilf��c3��c3C�.'><if��c?�;SQiI
06/21 /23 23:45 17060-07-0
06/21 /23 23:45 2037-26-5
Page 10 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-4A
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197004 Collected: 06/15/23 14:00 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:52
7440-38-2
Barium
127
ug/L
3.5
1
06/21/2310:50
06/22/2314:52
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/21/2310:50
06/22/2314:52
7440-43-9
Chromium
35.7
ug/L
3.7
1
06/21/2310:50
06/22/2314:52
7440-47-3
Lead
11.1
ug/L
4.5
1
06/21/2310:50
06/22/2314:52
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:52
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/21/2310:50
06/22/2314:52
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
0.78
ug/L
0.12
1
06/26/2313:03
06/27/2313:03
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
107
ug/L
5.1
1
06/23/23 22:54
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 22:54
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/23/23 22:54
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 22:54
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 22:54
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 22:54
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 22:54
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 22:54
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 22:54
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 22:54
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/23/23 22:54
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/23/23 22:54
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/23/23 22:54
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 22:54
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 22:54
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 22:54
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 22:54
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 22:54
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 22:54
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/23/23 22:54
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 22:54
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/23/23 22:54
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/23/23 22:54
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/23/23 22:54
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/23/23 22:54
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 22:54
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 22:54
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 22:54
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 22:54
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 22:54
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 22:54
591-78-6
REPORT OF LABORATORY ANALYSIS
M1
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-4A Lab ID: 92673197004 Collected: 06/15/23 14:00 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
97
%
101
%
101
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
123
%
106
%
9.7
1
06/23/23 22:54
74-88-4
2.0
1
06/23/23 22:54
75-09-2
2.7
1
06/23/23 22:54
108-10-1
0.29
1
06/23/23 22:54
100-42-5
0.31
1
06/23/23 22:54
630-20-6
0.22
1
06/23/23 22:54
79-34-5
0.29
1
06/23/23 22:54
127-18-4
0.24
1
06/23/23 22:54
108-88-3
0.33
1
06/23/23 22:54
71-55-6
0.32
1
06/23/23 22:54
79-00-5
0.38
1
06/23/23 22:54
79-01-6
0.30
1
06/23/23 22:54
75-69-4
0.26
1
06/23/23 22:54
96-18-4
1.3
1
06/23/23 22:54
108-05-4
0.39
1
06/23/23 22:54
75-01-4
0.34
1
06/23/23 22:54
1330-20-7
0.71
1
06/23/23 22:54
179601-23-1
0.34
1
06/23/23 22:54
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/23/23 22:54 460-00-4
06/23/23 22:54 17060-07-0
06/23/23 22:54 2037-26-5
[eI:If��af��cIeIei[eI'1<if��c?�;SQiI
06/22/23 00:06 17060-07-0
06/22/23 00:06 2037-26-5
Page 12 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-5
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197005 Collected: 06/15/23 09:45 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
12.3
ug/L
4.7
1
06/21/2310:50
06/22/2314:55
7440-38-2
Barium
176
ug/L
3.5
1
06/21/2310:50
06/22/2314:55
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/21/2310:50
06/22/2314:55
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/21/2310:50
06/22/2314:55
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/21/2310:50
06/22/2314:55
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/21/2310:50
06/22/2314:55
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/21/2310:50
06/22/2314:55
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:05
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/23/23 23:13
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 23:13
107-13-1
Benzene
0.34
ug/L
0.34
1
06/23/23 23:13
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 23:13
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 23:13
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 23:13
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 23:13
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 23:13
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 23:13
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 23:13
56-23-5
Chlorobenzene
1.2
ug/L
0.28
1
06/23/23 23:13
108-90-7
Chloroethane
1.2
ug/L
0.65
1
06/23/23 23:13
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/23/23 23:13
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 23:13
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 23:13
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 23:13
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 23:13
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 23:13
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 23:13
95-50-1
1,4-Dichlorobenzene
1.2
ug/L
0.33
1
06/23/23 23:13
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 23:13
110-57-6
1,1-Dichloroethane
1.5
ug/L
0.37
1
06/23/23 23:13
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/23/23 23:13
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/23/23 23:13
75-35-4
cis-1,2-Dichloroethene
3.2
ug/L
0.38
1
06/23/23 23:13
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 23:13
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 23:13
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:13
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:13
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 23:13
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 23:13
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v3
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-5 Lab ID: 92673197005 Collected: 06/15/23 09:45 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
97
%
98
%
101
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
11.3
ug/L
119
%
104
%
9.7
1
06/23/23 23:13
74-88-4
2.0
1
06/23/23 23:13
75-09-2
2.7
1
06/23/23 23:13
108-10-1
0.29
1
06/23/23 23:13
100-42-5
0.31
1
06/23/23 23:13
630-20-6
0.22
1
06/23/23 23:13
79-34-5
0.29
1
06/23/23 23:13
127-18-4
0.24
1
06/23/23 23:13
108-88-3
0.33
1
06/23/23 23:13
71-55-6
0.32
1
06/23/23 23:13
79-00-5
0.38
1
06/23/23 23:13
79-01-6
0.30
1
06/23/23 23:13
75-69-4
0.26
1
06/23/23 23:13
96-18-4
1.3
1
06/23/23 23:13
108-05-4
0.39
1
06/23/23 23:13
75-01-4
0.34
1
06/23/23 23:13
1330-20-7
0.71
1
06/23/23 23:13
179601-23-1
0.34
1
06/23/23 23:13
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/23/23 23:13 460-00-4
06/23/23 23:13 17060-07-0
06/23/23 23:13 2037-26-5
IeIe7 Y831111111i f �XS*1 N
06/22/23 00:28 17060-07-0
06/22/23 00:28 2037-26-5
Page 14 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-6
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197006 Collected: 06/15/23 13:35 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:40
7440-38-2
Barium
33.8
ug/L
3.5
1
06/26/2310:22
06/27/2314:40
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2314:40
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/26/2310:22
06/27/2314:40
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/26/2310:22
06/27/2314:40
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:40
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2314:40
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:07
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/24/23 01:20
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/24/23 01:20
107-13-1
Benzene
1.3
ug/L
0.34
1
06/24/23 01:20
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/24/23 01:20
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/24/23 01:20
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/24/23 01:20
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/24/23 01:20
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/24/23 01:20
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/24/23 01:20
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/24/23 01:20
56-23-5
Chlorobenzene
3.2
ug/L
0.28
1
06/24/23 01:20
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/24/23 01:20
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/24/23 01:20
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/24/23 01:20
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/24/23 01:20
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/24/23 01:20
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/24/23 01:20
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/24/23 01:20
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/24/23 01:20
95-50-1
1,4-Dichlorobenzene
1.6
ug/L
0.33
1
06/24/23 01:20
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/24/23 01:20
110-57-6
1,1-Dichloroethane
0.37
ug/L
0.37
1
06/24/23 01:20
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/24/23 01:20
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/24/23 01:20
75-35-4
cis-1,2-Dichloroethene
1.8
ug/L
0.38
1
06/24/23 01:20
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/24/23 01:20
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/24/23 01:20
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 01:20
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 01:20
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/24/23 01:20
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/24/23 01:20
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-6 Lab ID: 92673197006 Collected: 06/15/23 13:35 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
97
%
98
%
103
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
46.0
ug/L
121
%
104
%
9.7
1
06/24/23 01:20
74-88-4
2.0
1
06/24/23 01:20
75-09-2
2.7
1
06/24/23 01:20
108-10-1
0.29
1
06/24/23 01:20
100-42-5
0.31
1
06/24/23 01:20
630-20-6
0.22
1
06/24/23 01:20
79-34-5
0.29
1
06/24/23 01:20
127-18-4
0.24
1
06/24/23 01:20
108-88-3
0.33
1
06/24/23 01:20
71-55-6
0.32
1
06/24/23 01:20
79-00-5
0.38
1
06/24/23 01:20
79-01-6
0.30
1
06/24/23 01:20
75-69-4
0.26
1
06/24/23 01:20
96-18-4
1.3
1
06/24/23 01:20
108-05-4
0.39
1
06/24/23 01:20
75-01-4
0.34
1
06/24/23 01:20
1330-20-7
0.71
1
06/24/23 01:20
179601-23-1
0.34
1
06/24/23 01:20
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/24/23 01:20 460-00-4
06/24/23 01:20 17060-07-0
06/24/23 01:20 2037-26-5
[eI:If��af��cIeIe101E, PaS4 N
06/22/23 00:49 17060-07-0
06/22/23 00:49 2037-26-5
Page 16 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-7
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197007 Collected: 06/15/23 12:50 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:52
7440-38-2
Barium
108
ug/L
3.5
1
06/26/2310:22
06/27/2314:52
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2314:52
7440-43-9
Chromium
21.6
ug/L
3.7
1
06/26/2310:22
06/27/2314:52
7440-47-3
Lead
5.9
ug/L
4.5
1
06/26/2310:22
06/27/2314:52
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:52
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2314:52
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:10
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/23/23 23:31
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 23:31
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/23/23 23:31
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 23:31
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 23:31
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 23:31
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 23:31
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 23:31
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 23:31
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 23:31
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/23/23 23:31
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/23/23 23:31
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/23/23 23:31
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 23:31
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 23:31
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 23:31
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 23:31
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 23:31
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 23:31
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/23/23 23:31
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 23:31
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/23/23 23:31
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/23/23 23:31
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/23/23 23:31
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/23/23 23:31
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 23:31
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 23:31
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:31
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:31
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 23:31
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 23:31
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-7 Lab ID: 92673197007 Collected: 06/15/23 12:50 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
98
%
97
%
102
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
122
%
105
%
9.7
1
06/23/23 23:31
74-88-4
2.0
1
06/23/23 23:31
75-09-2
2.7
1
06/23/23 23:31
108-10-1
0.29
1
06/23/23 23:31
100-42-5
0.31
1
06/23/23 23:31
630-20-6
0.22
1
06/23/23 23:31
79-34-5
0.29
1
06/23/23 23:31
127-18-4
0.24
1
06/23/23 23:31
108-88-3
0.33
1
06/23/23 23:31
71-55-6
0.32
1
06/23/23 23:31
79-00-5
0.38
1
06/23/23 23:31
79-01-6
0.30
1
06/23/23 23:31
75-69-4
0.26
1
06/23/23 23:31
96-18-4
1.3
1
06/23/23 23:31
108-05-4
0.39
1
06/23/23 23:31
75-01-4
0.34
1
06/23/23 23:31
1330-20-7
0.71
1
06/23/23 23:31
179601-23-1
0.34
1
06/23/23 23:31
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/23/23 23:31 460-00-4
06/23/23 23:31 17060-07-0
06/23/23 23:31 2037-26-5
[eZ:If��af��c 111HElm PaS4 N
06/22/23 01:10 17060-07-0
06/22/23 01:10 2037-26-5
Page 18 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-8 Lab ID: 92673197008 Collected: 06/15/23 11:25 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<9.4
ug/L
9.4
2
06/26/2310:22
06/28/2313:12
7440-38-2
Barium
714
ug/L
7.0
2
06/26/2310:22
06/28/2313:12
7440-39-3
Cadmium
<0.80
ug/L
0.80
2
06/26/2310:22
06/28/2313:12
7440-43-9
Chromium
12.6
ug/L
7.3
2
06/26/2310:22
06/28/2313:12
7440-47-3
Lead
39.5
ug/L
9.1
2
06/26/2310:22
06/28/2313:12
7439-92-1
Selenium
<9.4
ug/L
9.4
2
06/26/2310:22
06/28/2313:12
7782-49-2
Silver
<5.0
ug/L
5.0
2
06/26/2310:22
06/28/2313:12
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
7.3
ug/L
0.61
5
06/26/2313:03
06/27/2313:48
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/23/23 23:49
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/23/23 23:49
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/23/23 23:49
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/23/23 23:49
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/23/23 23:49
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/23/23 23:49
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/23/23 23:49
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/23/23 23:49
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/23/23 23:49
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/23/23 23:49
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/23/23 23:49
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/23/23 23:49
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/23/23 23:49
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/23/23 23:49
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/23/23 23:49
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/23/23 23:49
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/23/23 23:49
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/23/23 23:49
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/23/23 23:49
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/23/23 23:49
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/23/23 23:49
110-57-6
1,1-Dichloroethane
3.5
ug/L
0.37
1
06/23/23 23:49
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/23/23 23:49
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/23/23 23:49
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/23/23 23:49
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/23/23 23:49
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/23/23 23:49
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:49
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/23/23 23:49
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/23/23 23:49
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/23/23 23:49
591-78-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
D3
D3
D3
D3
v2
v2
Page 19 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-8 Lab ID: 92673197008 Collected: 06/15/23 11:25 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
98
%
97
%
102
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
120
%
105
%
9.7
1
06/23/23 23:49
74-88-4
2.0
1
06/23/23 23:49
75-09-2
2.7
1
06/23/23 23:49
108-10-1
0.29
1
06/23/23 23:49
100-42-5
0.31
1
06/23/23 23:49
630-20-6
0.22
1
06/23/23 23:49
79-34-5
0.29
1
06/23/23 23:49
127-18-4
0.24
1
06/23/23 23:49
108-88-3
0.33
1
06/23/23 23:49
71-55-6
0.32
1
06/23/23 23:49
79-00-5
0.38
1
06/23/23 23:49
79-01-6
0.30
1
06/23/23 23:49
75-69-4
0.26
1
06/23/23 23:49
96-18-4
1.3
1
06/23/23 23:49
108-05-4
0.39
1
06/23/23 23:49
75-01-4
0.34
1
06/23/23 23:49
1330-20-7
0.71
1
06/23/23 23:49
179601-23-1
0.34
1
06/23/23 23:49
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/23/23 23:49 460-00-4
06/23/23 23:49 17060-07-0
06/23/23 23:49 2037-26-5
[eZ:If��af��cIeyiEc1itiPaS4 N
06/22/23 01:31 17060-07-0
06/22/23 01:31 2037-26-5
Page 20 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-9S
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197009 Collected: 06/15/23 10:00 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:58
7440-38-2
Barium
50.6
ug/L
3.5
1
06/26/2310:22
06/27/2314:58
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2314:58
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/26/2310:22
06/27/2314:58
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/26/2310:22
06/27/2314:58
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2314:58
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2314:58
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:14
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/24/23 00:07
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/24/23 00:07
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/24/23 00:07
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/24/23 00:07
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/24/23 00:07
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/24/23 00:07
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/24/23 00:07
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/24/23 00:07
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/24/23 00:07
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/24/23 00:07
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/24/23 00:07
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/24/23 00:07
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/24/23 00:07
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/24/23 00:07
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/24/23 00:07
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/24/23 00:07
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/24/23 00:07
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/24/23 00:07
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/24/23 00:07
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/24/23 00:07
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/24/23 00:07
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/24/23 00:07
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/24/23 00:07
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/24/23 00:07
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/24/23 00:07
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/24/23 00:07
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/24/23 00:07
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:07
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:07
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/24/23 00:07
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/24/23 00:07
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-9S Lab ID: 92673197009 Collected: 06/15/23 10:00 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
99
%
101
%
103
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
122
%
105
%
9.7
1
06/24/23 00:07
74-88-4
2.0
1
06/24/23 00:07
75-09-2
2.7
1
06/24/23 00:07
108-10-1
0.29
1
06/24/23 00:07
100-42-5
0.31
1
06/24/23 00:07
630-20-6
0.22
1
06/24/23 00:07
79-34-5
0.29
1
06/24/23 00:07
127-18-4
0.24
1
06/24/23 00:07
108-88-3
0.33
1
06/24/23 00:07
71-55-6
0.32
1
06/24/23 00:07
79-00-5
0.38
1
06/24/23 00:07
79-01-6
0.30
1
06/24/23 00:07
75-69-4
0.26
1
06/24/23 00:07
96-18-4
1.3
1
06/24/23 00:07
108-05-4
0.39
1
06/24/23 00:07
75-01-4
0.34
1
06/24/23 00:07
1330-20-7
0.71
1
06/24/23 00:07
179601-23-1
0.34
1
06/24/23 00:07
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/24/23 00:07 460-00-4
06/24/23 00:07 17060-07-0
06/24/23 00:07 2037-26-5
[eZ:If��af��c 1111117cltiPaS4 N
06/22/23 01:53 17060-07-0
06/22/23 01:53 2037-26-5
Page 22 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-91)
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197010 Collected: 06/15/23 09:54 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:01
7440-38-2
Barium
26.5
ug/L
3.5
1
06/26/2310:22
06/27/2315:01
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2315:01
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/26/2310:22
06/27/2315:01
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/26/2310:22
06/27/2315:01
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:01
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2315:01
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:16
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/24/23 00:25
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/24/23 00:25
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/24/23 00:25
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/24/23 00:25
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/24/23 00:25
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/24/23 00:25
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/24/23 00:25
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/24/23 00:25
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/24/23 00:25
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/24/23 00:25
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/24/23 00:25
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/24/23 00:25
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/24/23 00:25
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/24/23 00:25
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/24/23 00:25
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/24/23 00:25
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/24/23 00:25
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/24/23 00:25
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/24/23 00:25
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/24/23 00:25
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/24/23 00:25
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/24/23 00:25
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/24/23 00:25
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/24/23 00:25
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/24/23 00:25
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/24/23 00:25
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/24/23 00:25
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:25
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:25
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/24/23 00:25
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/24/23 00:25
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: MW-9D Lab ID: 92673197010 Collected: 06/15/23 09:54 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
98
%
101
%
103
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
126
%
106
%
9.7
1
06/24/23 00:25
74-88-4
2.0
1
06/24/23 00:25
75-09-2
2.7
1
06/24/23 00:25
108-10-1
0.29
1
06/24/23 00:25
100-42-5
0.31
1
06/24/23 00:25
630-20-6
0.22
1
06/24/23 00:25
79-34-5
0.29
1
06/24/23 00:25
127-18-4
0.24
1
06/24/23 00:25
108-88-3
0.33
1
06/24/23 00:25
71-55-6
0.32
1
06/24/23 00:25
79-00-5
0.38
1
06/24/23 00:25
79-01-6
0.30
1
06/24/23 00:25
75-69-4
0.26
1
06/24/23 00:25
96-18-4
1.3
1
06/24/23 00:25
108-05-4
0.39
1
06/24/23 00:25
75-01-4
0.34
1
06/24/23 00:25
1330-20-7
0.71
1
06/24/23 00:25
179601-23-1
0.34
1
06/24/23 00:25
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/24/23 00:25 460-00-4
06/24/23 00:25 17060-07-0
06/24/23 00:25 2037-26-5
[eI:If��af��c [11)"aC!<iPaS4 N
06/22/23 02:14 17060-07-0
06/22/23 02:14 2037-26-5
Page 24 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: SW-1
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197011 Collected: 06/15/23 10:35 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:10
7440-38-2
Barium
29.0
ug/L
3.5
1
06/26/2310:22
06/27/2315:10
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2315:10
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/26/2310:22
06/27/2315:10
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/26/2310:22
06/27/2315:10
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:10
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2315:10
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:19
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/24/23 00:44
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/24/23 00:44
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/24/23 00:44
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/24/23 00:44
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/24/23 00:44
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/24/23 00:44
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/24/23 00:44
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/24/23 00:44
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/24/23 00:44
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/24/23 00:44
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/24/23 00:44
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/24/23 00:44
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/24/23 00:44
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/24/23 00:44
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/24/23 00:44
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/24/23 00:44
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/24/23 00:44
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/24/23 00:44
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/24/23 00:44
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/24/23 00:44
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/24/23 00:44
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/24/23 00:44
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/24/23 00:44
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/24/23 00:44
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/24/23 00:44
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/24/23 00:44
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/24/23 00:44
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:44
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 00:44
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/24/23 00:44
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/24/23 00:44
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: SW-1 Lab ID: 92673197011 Collected: 06/15/23 10:35 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
97
%
101
%
103
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
<0.86
ug/L
120
%
104
%
9.7
1
06/24/23 00:44
74-88-4
2.0
1
06/24/23 00:44
75-09-2
2.7
1
06/24/23 00:44
108-10-1
0.29
1
06/24/23 00:44
100-42-5
0.31
1
06/24/23 00:44
630-20-6
0.22
1
06/24/23 00:44
79-34-5
0.29
1
06/24/23 00:44
127-18-4
0.24
1
06/24/23 00:44
108-88-3
0.33
1
06/24/23 00:44
71-55-6
0.32
1
06/24/23 00:44
79-00-5
0.38
1
06/24/23 00:44
79-01-6
0.30
1
06/24/23 00:44
75-69-4
0.26
1
06/24/23 00:44
96-18-4
1.3
1
06/24/23 00:44
108-05-4
0.39
1
06/24/23 00:44
75-01-4
0.34
1
06/24/23 00:44
1330-20-7
0.71
1
06/24/23 00:44
179601-23-1
0.34
1
06/24/23 00:44
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/24/23 00:44 460-00-4
06/24/23 00:44 17060-07-0
06/24/23 00:44 2037-26-5
[eI:If��af��c [it5CK3<iPaS4 N
06/22/23 04:43 17060-07-0
06/22/23 04:43 2037-26-5
Page 26 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
Project: Rutherford South
Pace Project No.: 92673197
Sample: SW-2
Parameters
ANALYTICAL RESULTS
Lab ID: 92673197012 Collected: 06/15/23 10:10 Received: 06/19/23 14:00 Matrix: Water
Results Units PQL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Arsenic
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:12
7440-38-2
Barium
29.8
ug/L
3.5
1
06/26/2310:22
06/27/2315:12
7440-39-3
Cadmium
<0.40
ug/L
0.40
1
06/26/2310:22
06/27/2315:12
7440-43-9
Chromium
<3.7
ug/L
3.7
1
06/26/2310:22
06/27/2315:12
7440-47-3
Lead
<4.5
ug/L
4.5
1
06/26/2310:22
06/27/2315:12
7439-92-1
Selenium
<4.7
ug/L
4.7
1
06/26/2310:22
06/27/2315:12
7782-49-2
Silver
<2.5
ug/L
2.5
1
06/26/2310:22
06/27/2315:12
7440-22-4
7470 Mercury
Analytical Method:
EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical
Services -Asheville
Mercury
<0.12
ug/L
0.12
1
06/26/2313:03
06/27/2313:21
7439-97-6
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
<5.1
ug/L
5.1
1
06/24/23 01:02
67-64-1
Acrylonitrile
<1.8
ug/L
1.8
1
06/24/23 01:02
107-13-1
Benzene
<0.34
ug/L
0.34
1
06/24/23 01:02
71-43-2
Bromochloromethane
<0.47
ug/L
0.47
1
06/24/23 01:02
74-97-5
Bromodichloromethane
<0.31
ug/L
0.31
1
06/24/23 01:02
75-27-4
Bromoform
<0.34
ug/L
0.34
1
06/24/23 01:02
75-25-2
Bromomethane
<1.7
ug/L
1.7
1
06/24/23 01:02
74-83-9
2-Butanone (MEK)
<4.0
ug/L
4.0
1
06/24/23 01:02
78-93-3
Carbon disulfide
<0.36
ug/L
0.36
1
06/24/23 01:02
75-15-0
Carbon tetrachloride
<0.33
ug/L
0.33
1
06/24/23 01:02
56-23-5
Chlorobenzene
<0.28
ug/L
0.28
1
06/24/23 01:02
108-90-7
Chloroethane
<0.65
ug/L
0.65
1
06/24/23 01:02
75-00-3
Chloroform
<0.43
ug/L
0.43
1
06/24/23 01:02
67-66-3
Chloromethane
<0.54
ug/L
0.54
1
06/24/23 01:02
74-87-3
1,2-Dibromo-3-chloropropane
<0.34
ug/L
0.34
1
06/24/23 01:02
96-12-8
Dibromochloromethane
<0.36
ug/L
0.36
1
06/24/23 01:02
124-48-1
1,2-Dibromoethane (EDB)
<0.27
ug/L
0.27
1
06/24/23 01:02
106-93-4
Dibromomethane
<0.39
ug/L
0.39
1
06/24/23 01:02
74-95-3
1,2-Dichlorobenzene
<0.34
ug/L
0.34
1
06/24/23 01:02
95-50-1
1,4-Dichlorobenzene
<0.33
ug/L
0.33
1
06/24/23 01:02
106-46-7
trans-1,4-Dichloro-2-butene
<0.56
ug/L
0.56
1
06/24/23 01:02
110-57-6
1,1-Dichloroethane
<0.37
ug/L
0.37
1
06/24/23 01:02
75-34-3
1,2-Dichloroethane
<0.32
ug/L
0.32
1
06/24/23 01:02
107-06-2
1,1-Dichloroethene
<0.35
ug/L
0.35
1
06/24/23 01:02
75-35-4
cis-1,2-Dichloroethene
<0.38
ug/L
0.38
1
06/24/23 01:02
156-59-2
trans-1,2-Dichloroethene
<0.40
ug/L
0.40
1
06/24/23 01:02
156-60-5
1,2-Dichloropropane
<0.36
ug/L
0.36
1
06/24/23 01:02
78-87-5
cis-1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 01:02
10061-01-5
trans- 1,3-Dichloropropene
<0.36
ug/L
0.36
1
06/24/23 01:02
10061-02-6
Ethylbenzene
<0.30
ug/L
0.30
1
06/24/23 01:02
100-41-4
2-Hexanone
<0.48
ug/L
0.48
1
06/24/23 01:02
591-78-6
REPORT OF LABORATORY ANALYSIS
v2
v2
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
ANALYTICAL RESULTS
Project: Rutherford South
Pace Project No.: 92673197
Sample: SW-2 Lab ID: 92673197012 Collected: 06/15/23 10:10 Received: 06/19/23 14:00 Matrix: Water
Parameters Results Units PQL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/30/2023 04:44 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
<9.7
ug/L
<2.0
ug/L
<2.7
ug/L
<0.29
ug/L
<0.31
ug/L
<0.22
ug/L
<0.29
ug/L
<0.24
ug/L
<0.33
ug/L
<0.32
ug/L
<0.38
ug/L
<0.30
ug/L
<0.26
ug/L
<1.3
ug/L
<0.39
ug/L
<0.34
ug/L
<0.71
ug/L
<0.34
ug/L
98
%
100
%
102
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
3.7
ug/L
120
%
105
%
9.7
1
06/24/23 01:02
74-88-4
2.0
1
06/24/23 01:02
75-09-2
2.7
1
06/24/23 01:02
108-10-1
0.29
1
06/24/23 01:02
100-42-5
0.31
1
06/24/23 01:02
630-20-6
0.22
1
06/24/23 01:02
79-34-5
0.29
1
06/24/23 01:02
127-18-4
0.24
1
06/24/23 01:02
108-88-3
0.33
1
06/24/23 01:02
71-55-6
0.32
1
06/24/23 01:02
79-00-5
0.38
1
06/24/23 01:02
79-01-6
0.30
1
06/24/23 01:02
75-69-4
0.26
1
06/24/23 01:02
96-18-4
1.3
1
06/24/23 01:02
108-05-4
0.39
1
06/24/23 01:02
75-01-4
0.34
1
06/24/23 01:02
1330-20-7
0.71
1
06/24/23 01:02
179601-23-1
0.34
1
06/24/23 01:02
95-47-6
70-130 1
70-130 1
70-130 1
[e1E:I:i
67-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/24/23 01:02 460-00-4
06/24/23 01:02 17060-07-0
06/24/23 01:02 2037-26-5
[eI:If��af��c 111MIZI=PaS4 N
06/22/23 05:04 17060-07-0
06/22/23 05:04 2037-26-5
Page 28 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 783001 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92673197001, 92673197002, 92673197003, 92673197004, 92673197005, 92673197006, 92673197007,
92673197008,92673197009,92673197010,92673197011,92673197012
METHOD BLANK: 4061266 Matrix: Water
Associated Lab Samples: 92673197001, 92673197002, 92673197003, 92673197004, 92673197005, 92673197006, 92673197007,
92673197008,92673197009,92673197010,92673197011,92673197012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L <0.12 0.12 06/27/2312:34
LABORATORY CONTROL SAMPLE: 4061267
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.7 108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4061268 4061269
MS MSD
92672242001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.4 2.6 94 102 75-125 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 781913 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92673197001, 92673197002, 92673197003, 92673197004, 92673197005
METHOD BLANK: 4056224
Matrix:
Water
Associated Lab Samples:
92673197001, 92673197002, 92673197003, 92673197004, 92673197005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
<4.7
4.7
06/22/2313:53
Barium
ug/L
<3.5
3.5
06/22/2313:53
Cadmium
ug/L
<0.40
0.40
06/22/2313:53
Chromium
ug/L
<3.7
3.7
06/22/2313:53
Lead
ug/L
<4.5
4.5
06/22/2313:53
Selenium
ug/L
<4.7
4.7
06/22/2313:53
Silver
ug/L
<2.5
2.5
06/22/2313:53
LABORATORY CONTROL SAMPLE:
4056225
Parameter
Units
Arsenic
ug/L
Barium
ug/L
Cadmium
ug/L
Chromium
ug/L
Lead
ug/L
Selenium
ug/L
Silver
ug/L
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
500
526
105
80-120
500
529
106
80-120
500
528
106
80-120
500
532
106
80-120
500
526
105
80-120
500
523
105
80-120
250
262
105
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4056226
MS
92673295001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
4056227
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
ug/L
ND
500
500
571
589
113
117
75-125
3
Barium
ug/L
204
500
500
779
806
115
121
75-125
3
Cadmium
ug/L
0.014
500
500
437
447
85
87
75-125
2
mg/L
Chromium
ug/L
ND
500
500
509
524
102
105
75-125
3
Lead
ug/L
0.012
500
500
479
493
93
96
75-125
3
mg/L
Selenium
ug/L
535
500
500
1140
1190
120
130
75-125
4
Silver
ug/L
ND
250
250
348
364
139
145
75-125
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 782949 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92673197006,92673197007,92673197008,92673197009,92673197010,92673197011,92673197012
METHOD BLANK: 4061015
Matrix:
Water
Associated Lab Samples:
92673197006,92673197007,92673197008,92673197009,92673197010,92673197011,92673197012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
<4.7
4.7
06/27/2314:35
Barium
ug/L
<3.5
3.5
06/27/2314:35
Cadmium
ug/L
<0.40
0.40
06/27/2314:35
Chromium
ug/L
<3.7
3.7
06/27/2314:35
Lead
ug/L
<4.5
4.5
06/27/2314:35
Selenium
ug/L
<4.7
4.7
06/27/2314:35
Silver
ug/L
<2.5
2.5
06/27/2314:35
LABORATORY CONTROL SAMPLE: 4061016
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
500
481
96
80-120
Barium
ug/L
500
494
99
80-120
Cadmium
ug/L
500
487
97
80-120
Chromium
ug/L
500
489
98
80-120
Lead
ug/L
500
491
98
80-120
Selenium
ug/L
500
478
96
80-120
Silver
ug/L
250
241
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4061017
4061018
MS
MSD
92673197006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
ug/L
<4.7
500
500
518
505
103
101
75-125
3
Barium
ug/L
33.8
500
500
541
531
101
99
75-125
2
Cadmium
ug/L
<0.40
500
500
497
486
99
97
75-125
2
Chromium
ug/L
<3.7
500
500
511
498
102
99
75-125
2
Lead
ug/L
<4.5
500
500
501
491
100
98
75-125
2
Selenium
ug/L
<4.7
500
500
532
520
106
104
75-125
2
Silver
ug/L
<2.5
250
250
255
251
102
100
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 782397 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92673197001, 92673197002
METHOD BLANK: 4058511
Associated Lab Samples: 92673197001, 92673197002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
<0.31
0.31
06/23/23 16:13
1,1,1-Trichloroethane
ug/L
<0.33
0.33
06/23/23 16:13
1,1,2,2-Tetrachloroethane
ug/L
<0.22
0.22
06/23/23 16:13
1,1,2-Trichloroethane
ug/L
<0.32
0.32
06/23/23 16:13
1,1-Dichloroethane
ug/L
<0.37
0.37
06/23/23 16:13
1,1-Dichloroethene
ug/L
<0.35
0.35
06/23/23 16:13
1,2,3-Trichloropropane
ug/L
<0.26
0.26
06/23/23 16:13
1,2-Dibromo-3-chloropropane
ug/L
<0.34
0.34
06/23/23 16:13
1,2-Dibromoethane (EDB)
ug/L
<0.27
0.27
06/23/23 16:13
1,2-Dichlorobenzene
ug/L
<0.34
0.34
06/23/23 16:13
1,2-Dichloroethane
ug/L
<0.32
0.32
06/23/23 16:13
1,2-Dichloropropane
ug/L
<0.36
0.36
06/23/23 16:13
1,4-Dichlorobenzene
ug/L
<0.33
0.33
06/23/23 16:13
2-Butanone (MEK)
ug/L
<4.0
4.0
06/23/23 16:13
2-Hexanone
ug/L
<0.48
0.48
06/23/23 16:13
4-Methyl-2-pentanone (MIBK)
ug/L
<2.7
2.7
06/23/23 16:13
Acetone
ug/L
<5.1
5.1
06/23/23 16:13
Acrylonitrile
ug/L
<1.8
1.8
06/23/23 16:13
Benzene
ug/L
<0.34
0.34
06/23/23 16:13
Bromochloromethane
ug/L
<0.47
0.47
06/23/23 16:13
Bromodichloromethane
ug/L
<0.31
0.31
06/23/23 16:13
Bromoform
ug/L
<0.34
0.34
06/23/23 16:13
Bromomethane
ug/L
<1.7
1.7
06/23/23 16:13
Carbon disulfide
ug/L
<0.36
0.36
06/23/23 16:13
Carbon tetrachloride
ug/L
<0.33
0.33
06/23/23 16:13
Chlorobenzene
ug/L
<0.28
0.28
06/23/23 16:13
Chloroethane
ug/L
<0.65
0.65
06/23/23 16:13
Chloroform
ug/L
<0.43
0.43
06/23/23 16:13
Chloromethane
ug/L
<0.54
0.54
06/23/23 16:13
cis-1,2-Dichloroethene
ug/L
<0.38
0.38
06/23/23 16:13
cis-1,3-Dichloropropene
ug/L
<0.36
0.36
06/23/23 16:13
Dibromochloromethane
ug/L
<0.36
0.36
06/23/23 16:13
Dibromomethane
ug/L
<0.39
0.39
06/23/23 16:13
Ethylbenzene
ug/L
<0.30
0.30
06/23/23 16:13
lodomethane
ug/L
<9.7
9.7
06/23/23 16:13
m&p-Xylene
ug/L
<0.71
0.71
06/23/23 16:13
Methylene Chloride
ug/L
<2.0
2.0
06/23/23 16:13
o-Xylene
ug/L
<0.34
0.34
06/23/23 16:13
Styrene
ug/L
<0.29
0.29
06/23/23 16:13
Tetrachloroethene
ug/L
<0.29
0.29
06/23/23 16:13
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
METHOD BLANK: 4058511
Associated Lab Samples: 92673197001, 92673197002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
<0.24
0.24
06/23/23 16:13
trans-1,2-Dichloroethene
ug/L
<0.40
0.40
06/23/23 16:13
trans- 1,3-Dichloropropene
ug/L
<0.36
0.36
06/23/23 16:13
trans-1,4-Dichloro-2-butene
ug/L
<0.56
0.56
06/23/23 16:13
Trichloroethene
ug/L
<0.38
0.38
06/23/23 16:13
Trichlorofluoromethane
ug/L
<0.30
0.30
06/23/23 16:13
Vinyl acetate
ug/L
<1.3
1.3
06/23/23 16:13
Vinyl chloride
ug/L
<0.39
0.39
06/23/23 16:13
Xylene (Total)
ug/L
<0.34
0.34
06/23/23 16:13
1,2-Dichloroethane-d4 (S)
%
101
70-130
06/23/23 16:13
4-Bromofluorobenzene (S)
%
98
70-130
06/23/23 16:13
Toluene-d8 (S)
%
101
70-130
06/23/23 16:13
LABORATORY CONTROL SAMPLE:
Parameter
4058512
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
20
19.7
98
70-130
1,1,1-Trichloroethane
ug/L
20
19.6
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
21.2
106
70-130
1,1,2-Trichloroethane
ug/L
20
20.2
101
70-130
1,1-Dichloroethane
ug/L
20
19.8
99
70-130
1,1-Dichloroethene
ug/L
20
20.1
101
70-130
1,2,3-Trichloropropane
ug/L
20
20.3
102
70-130
1,2-Dibromo-3-chloropropane
ug/L
20
18.7
94
70-131
1,2-Dibromoethane (EDB)
ug/L
20
20.1
101
70-130
1,2-Dichlorobenzene
ug/L
20
19.6
98
70-130
1,2-Dichloroethane
ug/L
20
19.6
98
70-130
1,2-Dichloropropane
ug/L
20
19.9
99
70-130
1,4-Dichlorobenzene
ug/L
20
19.7
99
70-130
2-Butanone (MEK)
ug/L
40
41.0
102
70-134
2-Hexanone
ug/L
40
42.6
107
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
40
40.9
102
70-130
Acetone
ug/L
40
40.8
102
70-133
Acrylonitrile
ug/L
100
107
107
70-130
Benzene
ug/L
20
20.0
100
70-130
Bromochloromethane
ug/L
20
20.0
100
70-130
Bromodichloromethane
ug/L
20
18.3
92
70-130
Bromoform
ug/L
20
18.1
90
70-130
Bromomethane
ug/L
20
15.2
76
45-151 v3
Carbon disulfide
ug/L
20
19.6
98
70-130
Carbon tetrachloride
ug/L
20
18.2
91
70-130
Chlorobenzene
ug/L
20
19.7
99
70-130
Chloroethane
ug/L
20
14.7
73
39-152 v3
Chloroform
ug/L
20
18.5
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
LABORATORY CONTROL SAMPLE:
Parameter
4058512
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
20
17.4
87
58-130
cis-1,2-Dichloroethene
ug/L
20
19.7
98
70-130
cis-1,3-Dichloropropene
ug/L
20
19.2
96
70-130
Dibromochloromethane
ug/L
20
18.6
93
70-130
Dibromomethane
ug/L
20
19.1
95
70-130
Ethylbenzene
ug/L
20
19.5
98
70-130
lodomethane
ug/L
40
35.0
87
53-141
m&p-Xylene
ug/L
40
39.4
98
70-130
Methylene Chloride
ug/L
20
20.2
101
66-130
o-Xylene
ug/L
20
19.4
97
70-130
Styrene
ug/L
20
19.8
99
70-130
Tetrachloroethene
ug/L
20
19.1
95
70-130
Toluene
ug/L
20
19.2
96
70-130
trans-1,2-Dichloroethene
ug/L
20
19.8
99
70-130
trans- 1,3-Dichloropropene
ug/L
20
18.6
93
70-130
trans-1,4-Dichloro-2-butene
ug/L
20
21.2
106
57-185
Trichloroethene
ug/L
20
19.1
96
70-130
Trichlorofluoromethane
ug/L
20
19.1
95
62-130
Vinyl acetate
ug/L
40
40.9
102
70-144
Vinyl chloride
ug/L
20
17.3
86
62-130
Xylene (Total)
ug/L
60
58.8
98
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
4058518
Units
92673056001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
22.9
115
70-141
1,1,1-Trichloroethane
ug/L
ND
20
23.4
117
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
21.3
107
69-142
1,1,2-Trichloroethane
ug/L
ND
20
21.7
108
70-138
1,1-Dichloroethane
ug/L
ND
20
24.7
123
70-150
1,1-Dichloroethene
ug/L
ND
20
27.7
139
70-156
1,2,3-Trichloropropane
ug/L
ND
20
21.4
107
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.2
106
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
22.5
113
70-138
1,2-Dichlorobenzene
ug/L
ND
20
21.1
106
70-141
1,2-Dichloroethane
ug/L
ND
20
23.5
117
69-143
1,2-Dichloropropane
ug/L
ND
20
23.5
118
68-156
1,4-Dichlorobenzene
ug/L
ND
20
21.2
106
70-142
2-Butanone (MEK)
ug/L
ND
40
42.7
107
60-157
2-Hexanone
ug/L
ND
40
43.5
109
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
43.3
108
70-141
Acetone
ug/L
ND
40
42.9
107
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
MATRIX SPIKE SAMPLE:
Parameter
4058518
Units
92673056001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
114
114
69-147
Benzene
ug/L
ND
20
23.3
116
70-142
Bromochloromethane
ug/L
ND
20
25.1
126
70-146
Bromodichloromethane
ug/L
ND
20
21.3
106
70-139
Bromoform
ug/L
ND
20
22.0
110
64-140
Bromomethane
ug/L
ND
20
16.3
81
28-192 v3
Carbon disulfide
ug/L
ND
20
27.1
135
70-151
Carbon tetrachloride
ug/L
ND
20
23.5
117
70-148
Chlorobenzene
ug/L
0.75J
20
22.9
111
70-141
Chloroethane
ug/L
ND
20
32.8
164
58-191
Chloroform
ug/L
ND
20
22.8
114
70-148
Chloromethane
ug/L
ND
20
27.2
136
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
24.1
121
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
23.0
115
70-139
Dibromochloromethane
ug/L
ND
20
22.6
113
70-144
Dibromomethane
ug/L
ND
20
21.8
109
70-139
Ethylbenzene
ug/L
ND
20
21.8
109
70-143
lodomethane
ug/L
ND
40
52.1
130
35-171
m&p-Xylene
ug/L
ND
40
42.9
107
70-144
Methylene Chloride
ug/L
ND
20
24.2
121
62-149
o-Xylene
ug/L
ND
20
21.4
107
70-145
Styrene
ug/L
ND
20
21.9
109
70-143
Tetrachloroethene
ug/L
ND
20
21.8
109
70-145
Toluene
ug/L
ND
20
22.1
110
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
25.8
129
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
22.6
113
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
22.7
113
51-159 v1
Trichloroethene
ug/L
ND
20
23.1
115
62-146
Trichlorofluoromethane
ug/L
ND
20
25.7
128
63-153
Vinyl acetate
ug/L
ND
40
47.4
118
61-162
Vinyl chloride
ug/L
ND
20
22.2
111
61-163
Xylene (Total)
ug/L
ND
60
64.3
107
70-143
1,2-Dichloroethane-d4 (S)
%
108
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 4058519
Parameter
Units
92673056003
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
<0.31
1,1,1-Trichloroethane
ug/L
ND
<0.33
1,1,2,2-Tetrachloroethane
ug/L
ND
<0.22
1,1,2-Trichloroethane
ug/L
ND
<0.32
1,1-Dichloroethane
ug/L
ND
<0.37
1,1-Dichloroethene
ug/L
ND
<0.35
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
SAMPLE DUPLICATE: 4058519
Parameter
Units
92673056003
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
<0.26
1,2-Dibromo-3-chloropropane
ug/L
ND
<0.34
1,2-Dibromoethane (EDB)
ug/L
ND
<0.27
1,2-Dichlorobenzene
ug/L
ND
<0.34
1,2-Dichloroethane
ug/L
ND
<0.32
1,2-Dichloropropane
ug/L
ND
<0.36
1,4-Dichlorobenzene
ug/L
ND
<0.33
2-Butanone (MEK)
ug/L
ND
<4.0
2-Hexanone
ug/L
ND
<0.48
4-Methyl-2-pentanone (MIBK)
ug/L
ND
<2.7
Acetone
ug/L
ND
<5.1
Acrylonitrile
ug/L
ND
<1.8
Benzene
ug/L
ND
<0.34
Bromochloromethane
ug/L
ND
<0.47
Bromodichloromethane
ug/L
ND
<0.31
Bromoform
ug/L
ND
<0.34
Bromomethane
ug/L
ND
<1.7
Carbon disulfide
ug/L
ND
<0.36
Carbon tetrachloride
ug/L
ND
<0.33
Chlorobenzene
ug/L
ND
<0.28
Chloroethane
ug/L
ND
<0.65
Chloroform
ug/L
ND
<0.43
Chloromethane
ug/L
ND
<0.54
cis-1,2-Dichloroethene
ug/L
ND
<0.38
cis-1,3-Dichloropropene
ug/L
ND
<0.36
Dibromochloromethane
ug/L
ND
<0.36
Dibromomethane
ug/L
ND
<0.39
Ethylbenzene
ug/L
ND
<0.30
lodomethane
ug/L
ND
<9.7
m&p-Xylene
ug/L
ND
<0.71
Methylene Chloride
ug/L
ND
<2.0
o-Xylene
ug/L
ND
<0.34
Styrene
ug/L
ND
<0.29
Tetrachloroethene
ug/L
ND
<0.29
Toluene
ug/L
ND
<0.24
trans-1,2-Dichloroethene
ug/L
ND
<0.40
trans- 1,3-Dichloropropene
ug/L
ND
<0.36
trans-1,4-Dichloro-2-butene
ug/L
ND
<0.56
Trichloroethene
ug/L
ND
<0.38
Trichlorofluoromethane
ug/L
ND
<0.30
Vinyl acetate
ug/L
ND
<1.3
Vinyl chloride
ug/L
ND
<0.39
Xylene (Total)
ug/L
ND
<0.34
1,2-Dichloroethane-d4 (S)
%
97
112
4-Bromofluorobenzene (S)
%
97
101
Toluene-d8 (S)
%
102
102
RPD Qualifiers
v2
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 782401 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92673197004, 92673197005, 92673197006, 92673197007, 92673197008, 92673197009, 92673197010,
92673197011,92673197012
METHOD BLANK: 4058548
Matrix: Water
Associated Lab Samples: 92673197004, 92673197005, 92673197006, 92673197007, 92673197008, 92673197009, 92673197010,
92673197011,92673197012
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
<0.31
0.31
06/23/23 15:55
1,1,1-Trichloroethane
ug/L
<0.33
0.33
06/23/23 15:55
1,1,2,2-Tetrachloroethane
ug/L
<0.22
0.22
06/23/23 15:55
1,1,2-Trichloroethane
ug/L
<0.32
0.32
06/23/23 15:55
1,1-Dichloroethane
ug/L
<0.37
0.37
06/23/23 15:55
1,1-Dichloroethene
ug/L
<0.35
0.35
06/23/23 15:55
1,2,3-Trichloropropane
ug/L
<0.26
0.26
06/23/23 15:55
1,2-Dibromo-3-chloropropane
ug/L
<0.34
0.34
06/23/23 15:55
1,2-Dibromoethane (EDB)
ug/L
<0.27
0.27
06/23/23 15:55
1,2-Dichlorobenzene
ug/L
<0.34
0.34
06/23/23 15:55
1,2-Dichloroethane
ug/L
<0.32
0.32
06/23/23 15:55
1,2-Dichloropropane
ug/L
<0.36
0.36
06/23/23 15:55
1,4-Dichlorobenzene
ug/L
<0.33
0.33
06/23/23 15:55
2-Butanone (MEK)
ug/L
<4.0
4.0
06/23/23 15:55
2-Hexanone
ug/L
<0.48
0.48
06/23/23 15:55
4-Methyl-2-pentanone (MIBK)
ug/L
<2.7
2.7
06/23/23 15:55
Acetone
ug/L
<5.1
5.1
06/23/23 15:55
Acrylonitrile
ug/L
<1.8
1.8
06/23/23 15:55
Benzene
ug/L
<0.34
0.34
06/23/23 15:55
Bromochloromethane
ug/L
<0.47
0.47
06/23/23 15:55
Bromodichloromethane
ug/L
<0.31
0.31
06/23/23 15:55
Bromoform
ug/L
<0.34
0.34
06/23/23 15:55
Bromomethane
ug/L
<1.7
1.7
06/23/23 15:55
Carbon disulfide
ug/L
<0.36
0.36
06/23/23 15:55
Carbon tetrachloride
ug/L
<0.33
0.33
06/23/23 15:55
Chlorobenzene
ug/L
<0.28
0.28
06/23/23 15:55
Chloroethane
ug/L
<0.65
0.65
06/23/23 15:55
Chloroform
ug/L
<0.43
0.43
06/23/23 15:55
Chloromethane
ug/L
<0.54
0.54
06/23/23 15:55
cis-1,2-Dichloroethene
ug/L
<0.38
0.38
06/23/23 15:55
cis-1,3-Dichloropropene
ug/L
<0.36
0.36
06/23/23 15:55
Dibromochloromethane
ug/L
<0.36
0.36
06/23/23 15:55
Dibromomethane
ug/L
<0.39
0.39
06/23/23 15:55
Ethylbenzene
ug/L
<0.30
0.30
06/23/23 15:55
lodomethane
ug/L
<9.7
9.7
06/23/23 15:55
m&p-Xylene
ug/L
<0.71
0.71
06/23/23 15:55
Methylene Chloride
ug/L
<2.0
2.0
06/23/23 15:55
o-Xylene
ug/L
<0.34
0.34
06/23/23 15:55
Styrene
ug/L
<0.29
0.29
06/23/23 15:55
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
METHOD BLANK: 4058548 Matrix: Water
Associated Lab Samples: 92673197004, 92673197005, 92673197006, 92673197007, 92673197008, 92673197009, 92673197010,
92673197011,92673197012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Tetrachloroethene
ug/L
<0.29
0.29
06/23/23 15:55
Toluene
ug/L
<0.24
0.24
06/23/23 15:55
trans-1,2-Dichloroethene
ug/L
<0.40
0.40
06/23/23 15:55
trans- 1,3-Dichloropropene
ug/L
<0.36
0.36
06/23/23 15:55
trans-1,4-Dichloro-2-butene
ug/L
<0.56
0.56
06/23/23 15:55
Trichloroethene
ug/L
<0.38
0.38
06/23/23 15:55
Trichlorofluoromethane
ug/L
<0.30
0.30
06/23/23 15:55
Vinyl acetate
ug/L
<1.3
1.3
06/23/23 15:55
Vinyl chloride
ug/L
<0.39
0.39
06/23/23 15:55
Xylene (Total)
ug/L
<0.34
0.34
06/23/23 15:55
1,2-Dichloroethane-d4 (S)
%
96
70-130
06/23/23 15:55
4-Bromofluorobenzene (S)
%
98
70-130
06/23/23 15:55
Toluene-d8 (S)
%
103
70-130
06/23/23 15:55
LABORATORY CONTROL SAMPLE:
Parameter
4058549
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
20
19.9
99
70-130
1,1,1-Trichloroethane
ug/L
20
19.8
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
21.0
105
70-130
1,1,2-Trichloroethane
ug/L
20
20.5
102
70-130
1,1-Dichloroethane
ug/L
20
18.8
94
70-130
1,1-Dichloroethene
ug/L
20
20.2
101
70-130
1,2,3-Trichloropropane
ug/L
20
20.5
103
70-130
1,2-Dibromo-3-chloropropane
ug/L
20
19.4
97
70-131
1,2-Dibromoethane (EDB)
ug/L
20
20.2
101
70-130
1,2-Dichlorobenzene
ug/L
20
19.9
100
70-130
1,2-Dichloroethane
ug/L
20
19.6
98
70-130
1,2-Dichloropropane
ug/L
20
19.9
100
70-130
1,4-Dichlorobenzene
ug/L
20
19.7
98
70-130
2-Butanone (MEK)
ug/L
40
39.2
98
70-134
2-Hexanone
ug/L
40
41.2
103
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
40
40.5
101
70-130
Acetone
ug/L
40
38.9
97
70-133
Acrylonitrile
ug/L
100
103
103
70-130
Benzene
ug/L
20
19.9
100
70-130
Bromochloromethane
ug/L
20
18.8
94
70-130
Bromodichloromethane
ug/L
20
18.7
93
70-130
Bromoform
ug/L
20
18.3
92
70-130
Bromomethane
ug/L
20
16.1
80
45-151 v3
Carbon disulfide
ug/L
20
19.8
99
70-130
Carbon tetrachloride
ug/L
20
19.4
97
70-130
Chlorobenzene
ug/L
20
19.8
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
LABORATORY CONTROL SAMPLE:
Parameter
4058549
Units
Spike LCS
Conc. Result
Chloroethane
ug/L
20
Chloroform
ug/L
20
Chloromethane
ug/L
20
cis-1,2-Dichloroethene
ug/L
20
cis-1,3-Dichloropropene
ug/L
20
Dibromochloromethane
ug/L
20
Dibromomethane
ug/L
20
Ethylbenzene
ug/L
20
lodomethane
ug/L
40
m&p-Xylene
ug/L
40
Methylene Chloride
ug/L
20
o-Xylene
ug/L
20
Styrene
ug/L
20
Tetrachloroethene
ug/L
20
Toluene
ug/L
20
trans-1,2-Dichloroethene
ug/L
20
trans- 1,3-Dichloropropene
ug/L
20
trans-1,4-Dichloro-2-butene
ug/L
20
Trichloroethene
ug/L
20
Trichlorofluoromethane
ug/L
20
Vinyl acetate
ug/L
40
Vinyl chloride
ug/L
20
Xylene (Total)
ug/L
60
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
15.5
78
39-152 v3
20.0
100
70-130
17.9
90
58-130
19.9
100
70-130
19.1
96
70-130
19.0
95
70-130
19.4
97
70-130
19.6
98
70-130
35.8
89
53-141
39.3
98
70-130
20.5
102
66-130
19.9
99
70-130
19.8
99
70-130
19.3
96
70-130
19.5
97
70-130
19.6
98
70-130
18.9
94
70-130
20.7
103
57-185
19.4
97
70-130
19.3
97
62-130
41.1
103
70-144
17.3
87
62-130
59.2
99
70-130
100
70-130
101
70-130
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
4058555
Units
92673197004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
<0.31
20
21.5
108
70-141
1,1,1-Trichloroethane
ug/L
<0.33
20
23.2
116
70-150
1,1,2,2-Tetrachloroethane
ug/L
<0.22
20
20.6
103
69-142
1,1,2-Trichloroethane
ug/L
<0.32
20
21.3
106
70-138
1,1-Dichloroethane
ug/L
<0.37
20
24.3
121
70-150
1,1-Dichloroethene
ug/L
<0.35
20
27.1
136
70-156
1,2,3-Trichloropropane
ug/L
<0.26
20
20.8
104
70-140
1,2-Dibromo-3-chloropropane
ug/L
<0.34
20
20.2
101
68-146
1,2-Dibromoethane (EDB)
ug/L
<0.27
20
21.5
107
70-138
1,2-Dichlorobenzene
ug/L
<0.34
20
20.1
100
70-141
1,2-Dichloroethane
ug/L
<0.32
20
23.4
117
69-143
1,2-Dichloropropane
ug/L
<0.36
20
22.8
114
68-156
1,4-Dichlorobenzene
ug/L
<0.33
20
19.9
99
70-142
2-Butanone (MEK)
ug/L
<4.0
40
42.7
107
60-157
2-Hexanone
ug/L
<0.48
40
41.6
104
68-146
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
MATRIX SPIKE SAMPLE:
Parameter
4058555
Units
92673197004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
4-Methyl-2-pentanone (MIBK)
ug/L
<2.7
40
41.2
103
70-141
Acetone
ug/L
107
40
82.6
-62
58-157 M1
Acrylonitrile
ug/L
<1.8
100
114
114
69-147
Benzene
ug/L
<0.34
20
22.6
113
70-142
Bromochloromethane
ug/L
<0.47
20
24.4
122
70-146
Bromodichloromethane
ug/L
<0.31
20
21.0
105
70-139
Bromoform
ug/L
<0.34
20
21.0
105
64-140
Bromomethane
ug/L
<1.7
20
16.1
80
28-192 v3
Carbon disulfide
ug/L
<0.36
20
25.6
128
70-151
Carbon tetrachloride
ug/L
<0.33
20
22.5
113
70-148
Chlorobenzene
ug/L
<0.28
20
20.7
104
70-141
Chloroethane
ug/L
<0.65
20
26.0
130
58-191
Chloroform
ug/L
<0.43
20
23.1
116
70-148
Chloromethane
ug/L
<0.54
20
26.0
130
43-162
cis-1,2-Dichloroethene
ug/L
<0.38
20
23.8
119
68-151
cis-1,3-Dichloropropene
ug/L
<0.36
20
22.4
112
70-139
Dibromochloromethane
ug/L
<0.36
20
21.6
108
70-144
Dibromomethane
ug/L
<0.39
20
21.5
108
70-139
Ethylbenzene
ug/L
<0.30
20
20.5
103
70-143
lodomethane
ug/L
<9.7
40
50.5
126
35-171
m&p-Xylene
ug/L
<0.71
40
40.7
102
70-144
Methylene Chloride
ug/L
<2.0
20
23.4
117
62-149
o-Xylene
ug/L
<0.34
20
20.2
101
70-145
Styrene
ug/L
<0.29
20
20.5
102
70-143
Tetrachloroethene
ug/L
<0.29
20
19.9
100
70-145
Toluene
ug/L
<0.24
20
21.0
105
70-142
trans-1,2-Dichloroethene
ug/L
<0.40
20
25.4
127
70-151
trans- 1,3-Dichloropropene
ug/L
<0.36
20
22.0
110
70-139
trans-1,4-Dichloro-2-butene
ug/L
<0.56
20
21.1
105
51-159 v1
Trichloroethene
ug/L
<0.38
20
22.5
112
62-146
Trichlorofluoromethane
ug/L
<0.30
20
24.0
120
63-153
Vinyl acetate
ug/L
<1.3
40
45.5
114
61-162
Vinyl chloride
ug/L
<0.39
20
21.8
109
61-163
Xylene (Total)
ug/L
<0.34
60
60.9
102
70-143
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
SAMPLE DUPLICATE: 4058556
92673197005
Dup
Parameter
Units
Result
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
<0.31
<0.31
1,1,1-Trichloroethane
ug/L
<0.33
<0.33
1,1,2,2-Tetrachloroethane
ug/L
<0.22
<0.22
1,1,2-Trichloroethane
ug/L
<0.32
<0.32
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
SAMPLE DUPLICATE: 4058556
Parameter
Units
92673197005
Result
Dup
Result
1,1-Dichloroethane
ug/L
1.5
1.8
1,1-Dichloroethene
ug/L
<0.35
<0.35
1,2,3-Trichloropropane
ug/L
<0.26
<0.26
1,2-Dibromo-3-chloropropane
ug/L
<0.34
<0.34
1,2-Dibromoethane (EDB)
ug/L
<0.27
<0.27
1,2-Dichlorobenzene
ug/L
<0.34
<0.34
1,2-Dichloroethane
ug/L
<0.32
<0.32
1,2-Dichloropropane
ug/L
<0.36
<0.36
1,4-Dichlorobenzene
ug/L
1.2
1.1
2-Butanone (MEK)
ug/L
<4.0
<4.0
2-Hexanone
ug/L
<0.48
<0.48
4-Methyl-2-pentanone (MIBK)
ug/L
<2.7
<2.7
Acetone
ug/L
<5.1
<5.1
Acrylonitrile
ug/L
<1.8
<1.8
Benzene
ug/L
0.34
0.34
Bromochloromethane
ug/L
<0.47
<0.47
Bromodichloromethane
ug/L
<0.31
<0.31
Bromoform
ug/L
<0.34
<0.34
Bromomethane
ug/L
<1.7
<1.7
Carbon disulfide
ug/L
<0.36
0.36
Carbon tetrachloride
ug/L
<0.33
<0.33
Chlorobenzene
ug/L
1.2
1.2
Chloroethane
ug/L
1.2
1.2
Chloroform
ug/L
<0.43
<0.43
Chloromethane
ug/L
<0.54
<0.54
cis-1,2-Dichloroethene
ug/L
3.2
3.5
cis-1,3-Dichloropropene
ug/L
<0.36
<0.36
Dibromochloromethane
ug/L
<0.36
<0.36
Dibromomethane
ug/L
<0.39
<0.39
Ethylbenzene
ug/L
<0.30
<0.30
lodomethane
ug/L
<9.7
<9.7
m&p-Xylene
ug/L
<0.71
<0.71
Methylene Chloride
ug/L
<2.0
<2.0
o-Xylene
ug/L
<0.34
<0.34
Styrene
ug/L
<0.29
<0.29
Tetrachloroethene
ug/L
<0.29
<0.29
Toluene
ug/L
<0.24
<0.24
trans-1,2-Dichloroethene
ug/L
<0.40
<0.40
trans- 1,3-Dichloropropene
ug/L
<0.36
<0.36
trans-1,4-Dichloro-2-butene
ug/L
<0.56
<0.56
Trichloroethene
ug/L
<0.38
<0.38
Trichlorofluoromethane
ug/L
<0.30
<0.30
Vinyl acetate
ug/L
<1.3
<1.3
Vinyl chloride
ug/L
0.39
0.39
Xylene (Total)
ug/L
<0.34
<0.34
1,2-Dichloroethane-d4 (S)
%
98
114
4-Bromofluorobenzene (S)
%
97
103
RPD Qualifiers
W61
8
7
1
HE
v2
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 55
leAnalyiical
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
SAMPLE DUPLICATE: 4058556
92673197005 Dup
Parameter Units Result Result RPD Qualifiers
Toluene-d8(S) % 101 103
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 783090 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92673197003
METHOD BLANK: 4061703
Associated Lab Samples: 92673197003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
<0.31
0.31
06/27/23 11:17
1,1,1-Trichloroethane
ug/L
<0.33
0.33
06/27/23 11:17
1,1,2,2-Tetrachloroethane
ug/L
<0.22
0.22
06/27/23 11:17
1,1,2-Trichloroethane
ug/L
<0.32
0.32
06/27/23 11:17
1,1-Dichloroethane
ug/L
<0.37
0.37
06/27/23 11:17
1,1-Dichloroethene
ug/L
<0.35
0.35
06/27/23 11:17
1,2,3-Trichloropropane
ug/L
<0.26
0.26
06/27/23 11:17
1,2-Dibromo-3-chloropropane
ug/L
<0.34
0.34
06/27/23 11:17
1,2-Dibromoethane (EDB)
ug/L
<0.27
0.27
06/27/23 11:17
1,2-Dichlorobenzene
ug/L
<0.34
0.34
06/27/23 11:17
1,2-Dichloroethane
ug/L
<0.32
0.32
06/27/23 11:17
1,2-Dichloropropane
ug/L
<0.36
0.36
06/27/23 11:17
1,4-Dichlorobenzene
ug/L
<0.33
0.33
06/27/23 11:17
2-Butanone (MEK)
ug/L
<4.0
4.0
06/27/23 11:17
2-Hexanone
ug/L
<0.48
0.48
06/27/23 11:17
4-Methyl-2-pentanone (MIBK)
ug/L
<2.7
2.7
06/27/23 11:17
Acetone
ug/L
<5.1
5.1
06/27/23 11:17
Acrylonitrile
ug/L
<1.8
1.8
06/27/23 11:17
Benzene
ug/L
<0.34
0.34
06/27/23 11:17
Bromochloromethane
ug/L
<0.47
0.47
06/27/23 11:17
Bromodichloromethane
ug/L
<0.31
0.31
06/27/23 11:17
Bromoform
ug/L
<0.34
0.34
06/27/23 11:17
Bromomethane
ug/L
<1.7
1.7
06/27/23 11:17
Carbon disulfide
ug/L
<0.36
0.36
06/27/23 11:17
Carbon tetrachloride
ug/L
<0.33
0.33
06/27/23 11:17
Chlorobenzene
ug/L
<0.28
0.28
06/27/23 11:17
Chloroethane
ug/L
<0.65
0.65
06/27/23 11:17
Chloroform
ug/L
<0.43
0.43
06/27/23 11:17
Chloromethane
ug/L
<0.54
0.54
06/27/23 11:17
cis-1,2-Dichloroethene
ug/L
<0.38
0.38
06/27/23 11:17
cis-1,3-Dichloropropene
ug/L
<0.36
0.36
06/27/23 11:17
Dibromochloromethane
ug/L
<0.36
0.36
06/27/23 11:17
Dibromomethane
ug/L
<0.39
0.39
06/27/23 11:17
Ethylbenzene
ug/L
<0.30
0.30
06/27/23 11:17
lodomethane
ug/L
<9.7
9.7
06/27/23 11:17
m&p-Xylene
ug/L
<0.71
0.71
06/27/23 11:17
Methylene Chloride
ug/L
<2.0
2.0
06/27/23 11:17
o-Xylene
ug/L
<0.34
0.34
06/27/23 11:17
Styrene
ug/L
<0.29
0.29
06/27/23 11:17
Tetrachloroethene
ug/L
<0.29
0.29
06/27/23 11:17
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
METHOD BLANK: 4061703
Associated Lab Samples: 92673197003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
<0.24
0.24
06/27/23 11:17
trans-1,2-Dichloroethene
ug/L
<0.40
0.40
06/27/23 11:17
trans- 1,3-Dichloropropene
ug/L
<0.36
0.36
06/27/23 11:17
trans-1,4-Dichloro-2-butene
ug/L
<0.56
0.56
06/27/23 11:17
Trichloroethene
ug/L
<0.38
0.38
06/27/23 11:17
Trichlorofluoromethane
ug/L
<0.30
0.30
06/27/23 11:17
Vinyl acetate
ug/L
<1.3
1.3
06/27/23 11:17
Vinyl chloride
ug/L
<0.39
0.39
06/27/23 11:17
Xylene (Total)
ug/L
<0.34
0.34
06/27/23 11:17
1,2-Dichloroethane-d4 (S)
%
102
70-130
06/27/23 11:17
4-Bromofluorobenzene (S)
%
99
70-130
06/27/23 11:17
Toluene-d8 (S)
%
102
70-130
06/27/23 11:17
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
4061704
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
20
19.1
95
70-130
1,1,1-Trichloroethane
ug/L
20
18.4
92
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
18.5
92
70-130
1,1,2-Trichloroethane
ug/L
20
17.8
89
70-130
1,1-Dichloroethane
ug/L
20
16.5
83
70-130
1,1-Dichloroethene
ug/L
20
18.2
91
70-130
1,2,3-Trichloropropane
ug/L
20
18.1
90
70-130
1,2-Dibromo-3-chloropropane
ug/L
20
16.7
83
70-131
1,2-Dibromoethane (EDB)
ug/L
20
18.8
94
70-130
1,2-Dichlorobenzene
ug/L
20
18.7
94
70-130
1,2-Dichloroethane
ug/L
20
17.5
88
70-130
1,2-Dichloropropane
ug/L
20
18.1
91
70-130
1,4-Dichlorobenzene
ug/L
20
18.7
93
70-130
2-Butanone (MEK)
ug/L
40
34.3
86
70-134
2-Hexanone
ug/L
40
37.6
94
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
40
35.3
88
70-130
Acetone
ug/L
40
34.2
86
70-133
Acrylonitrile
ug/L
100
84.1
84
70-130
Benzene
ug/L
20
17.9
90
70-130
Bromochloromethane
ug/L
20
17.0
85
70-130
Bromodichloromethane
ug/L
20
17.6
88
70-130
Bromoform
ug/L
20
16.8
84
70-130
Bromomethane
ug/L
20
18.5
93
45-151
Carbon disulfide
ug/L
20
18.1
90
70-130
Carbon tetrachloride
ug/L
20
18.5
93
70-130
Chlorobenzene
ug/L
20
18.7
94
70-130
Chloroethane
ug/L
20
21.6
108
39-152
Chloroform
ug/L
20
17.7
89
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
LABORATORY CONTROL SAMPLE:
Parameter
4061704
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
20
19.8
99
58-130
cis-1,2-Dichloroethene
ug/L
20
17.5
88
70-130
cis-1,3-Dichloropropene
ug/L
20
17.7
89
70-130
Dibromochloromethane
ug/L
20
19.2
96
70-130
Dibromomethane
ug/L
20
17.5
88
70-130
Ethylbenzene
ug/L
20
18.6
93
70-130
lodomethane
ug/L
40
31.1
78
53-141
m&p-Xylene
ug/L
40
37.2
93
70-130
Methylene Chloride
ug/L
20
18.8
94
66-130
o-Xylene
ug/L
20
18.7
93
70-130
Styrene
ug/L
20
18.8
94
70-130
Tetrachloroethene
ug/L
20
18.3
92
70-130
Toluene
ug/L
20
17.3
87
70-130
trans-1,2-Dichloroethene
ug/L
20
17.9
89
70-130
trans- 1,3-Dichloropropene
ug/L
20
17.5
87
70-130
trans-1,4-Dichloro-2-butene
ug/L
20
15.6
78
57-185
Trichloroethene
ug/L
20
17.7
89
70-130
Trichlorofluoromethane
ug/L
20
20.9
105
62-130
Vinyl acetate
ug/L
40
33.2
83
70-144
Vinyl chloride
ug/L
20
19.0
95
62-130
Xylene (Total)
ug/L
60
55.9
93
70-130
1,2-Dichloroethane-d4 (S)
%
109
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
4061706
Units
92673315002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
28.1
141
70-141
1,1,1-Trichloroethane
ug/L
ND
20
26.8
134
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
25.2
126
69-142
1,1,2-Trichloroethane
ug/L
ND
20
26.4
132
70-138
1,1-Dichloroethane
ug/L
ND
20
25.1
125
70-150
1,1-Dichloroethene
ug/L
ND
20
28.2
141
70-156
1,2,3-Trichloropropane
ug/L
ND
20
23.3
117
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
26.2
131
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
27.0
135
70-138
1,2-Dichlorobenzene
ug/L
ND
20
26.7
133
70-141
1,2-Dichloroethane
ug/L
ND
20
23.5
117
69-143
1,2-Dichloropropane
ug/L
ND
20
26.1
131
68-156
1,4-Dichlorobenzene
ug/L
ND
20
26.5
133
70-142
2-Butanone (MEK)
ug/L
ND
40
42.3
106
60-157
2-Hexanone
ug/L
ND
40
49.9
125
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
47.3
118
70-141
Acetone
ug/L
ND
40
40.5
101
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
MATRIX SPIKE SAMPLE:
Parameter
4061706
Units
92673315002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
113
113
69-147
Benzene
ug/L
ND
20
27.4
137
70-142
Bromochloromethane
ug/L
ND
20
25.7
129
70-146
Bromodichloromethane
ug/L
ND
20
25.4
127
70-139
Bromoform
ug/L
ND
20
27.6
138
64-140
Bromomethane
ug/L
ND
20
22.6
113
28-192 v3
Carbon disulfide
ug/L
ND
20
29.7
148
70-151
Carbon tetrachloride
ug/L
ND
20
29.0
145
70-148
Chlorobenzene
ug/L
ND
20
27.8
139
70-141
Chloroethane
ug/L
ND
20
26.5
132
58-191
Chloroform
ug/L
ND
20
24.2
121
70-148
Chloromethane
ug/L
ND
20
26.0
130
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
24.2
121
68-151
cis-1,3-Dichloropropene
ug/L
ND
20
25.9
129
70-139
Dibromochloromethane
ug/L
ND
20
27.3
137
70-144
Dibromomethane
ug/L
ND
20
28.6
143
70-139 M1
Ethylbenzene
ug/L
ND
20
26.8
134
70-143
lodomethane
ug/L
ND
40
49.0
122
35-171
m&p-Xylene
ug/L
ND
40
54.0
135
70-144
Methylene Chloride
ug/L
ND
20
22.4
112
62-149
o-Xylene
ug/L
ND
20
27.3
137
70-145
Styrene
ug/L
ND
20
28.0
140
70-143
Tetrachloroethene
ug/L
ND
20
28.5
143
70-145
Toluene
ug/L
ND
20
26.9
134
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
26.1
131
70-151
trans- 1,3-Dichloropropene
ug/L
ND
20
25.7
128
70-139
trans-1,4-Dichloro-2-butene
ug/L
ND
20
22.9
114
51-159
Trichloroethene
ug/L
ND
20
28.4
142
62-146
Trichlorofluoromethane
ug/L
ND
20
28.8
144
63-153
Vinyl acetate
ug/L
ND
40
46.6
117
61-162
Vinyl chloride
ug/L
ND
20
25.7
128
61-163
Xylene (Total)
ug/L
ND
60
81.3
136
70-143
1,2-Dichloroethane-d4 (S)
%
85
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 4061705
Parameter
Units
92673315001
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
<0.31
1,1,1-Trichloroethane
ug/L
ND
<0.33
1,1,2,2-Tetrachloroethane
ug/L
ND
<0.22
1,1,2-Trichloroethane
ug/L
ND
<0.32
1,1-Dichloroethane
ug/L
ND
<0.37
1,1-Dichloroethene
ug/L
ND
<0.35
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
SAMPLE DUPLICATE: 4061705
Parameter
Units
92673315001
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
<0.26
1,2-Dibromo-3-chloropropane
ug/L
ND
<0.34
1,2-Dibromoethane (EDB)
ug/L
ND
<0.27
1,2-Dichlorobenzene
ug/L
ND
<0.34
1,2-Dichloroethane
ug/L
ND
<0.32
1,2-Dichloropropane
ug/L
ND
<0.36
1,4-Dichlorobenzene
ug/L
ND
<0.33
2-Butanone (MEK)
ug/L
ND
<4.0
2-Hexanone
ug/L
ND
<0.48
4-Methyl-2-pentanone (MIBK)
ug/L
ND
<2.7
Acetone
ug/L
ND
<5.1
Acrylonitrile
ug/L
ND
<1.8
Benzene
ug/L
ND
<0.34
Bromochloromethane
ug/L
ND
<0.47
Bromodichloromethane
ug/L
ND
<0.31
Bromoform
ug/L
ND
<0.34
Bromomethane
ug/L
ND
<1.7
Carbon disulfide
ug/L
ND
<0.36
Carbon tetrachloride
ug/L
ND
<0.33
Chlorobenzene
ug/L
ND
<0.28
Chloroethane
ug/L
ND
<0.65
Chloroform
ug/L
ND
<0.43
Chloromethane
ug/L
ND
<0.54
cis-1,2-Dichloroethene
ug/L
ND
<0.38
cis-1,3-Dichloropropene
ug/L
ND
<0.36
Dibromochloromethane
ug/L
ND
<0.36
Dibromomethane
ug/L
ND
<0.39
Ethylbenzene
ug/L
ND
<0.30
lodomethane
ug/L
ND
<9.7
m&p-Xylene
ug/L
ND
<0.71
Methylene Chloride
ug/L
ND
<2.0
o-Xylene
ug/L
ND
<0.34
Styrene
ug/L
ND
<0.29
Tetrachloroethene
ug/L
ND
<0.29
Toluene
ug/L
ND
<0.24
trans-1,2-Dichloroethene
ug/L
ND
<0.40
trans- 1,3-Dichloropropene
ug/L
ND
<0.36
trans-1,4-Dichloro-2-butene
ug/L
ND
<0.56
Trichloroethene
ug/L
ND
<0.38
Trichlorofluoromethane
ug/L
ND
<0.30
Vinyl acetate
ug/L
ND
<1.3
Vinyl chloride
ug/L
ND
<0.39
Xylene (Total)
ug/L
ND
<0.34
1,2-Dichloroethane-d4 (S)
%
103
85
4-Bromofluorobenzene (S)
%
98
93
Toluene-d8 (S)
%
101
98
RPD Qualifiers
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 782001 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92673197001, 92673197002, 92673197003, 92673197004, 92673197005, 92673197006, 92673197007,
92673197008,92673197009,92673197010
METHOD BLANK: 4056696 Matrix:
Water
Associated Lab Samples:
92673197001, 92673197002, 92673197003, 92673197004, 92673197005,
92673197006, 92673197007,
92673197008,92673197009,92673197010
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L <0.86
0.86
06/21/23 15:36
1,2-Dichloroethane-d4 (S)
% 118
67-130
06/21/23 15:36
Toluene-d8 (S)
% 104
70-130
06/21/23 15:36
LABORATORY CONTROL SAMPLE: 4056697
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 21.2 106 70-130
1,2-Dichloroethane-d4 (S) % 117 67-130
Toluene-d8(S) % 104 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4056698
4056699
MS
MSD
92673197001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 0.86 20
20 21.0
20.6 100
98
55-137 2 H1
1,2-Dichloroethane-d4 (S)
%
118
119
67-130
Toluene-d8(S)
%
105
105
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA
Project: Rutherford South
Pace Project No.: 92673197
QC Batch: 782002 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92673197011, 92673197012
METHOD BLANK: 4056706
Associated Lab Samples: 92673197011, 92673197012
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit Analyzed
<0.86 0.86 06/22/23 04:00
120 67-130 06/22/23 04:00
105 70-130 06/22/23 04:00
Qualifiers
LABORATORY CONTROL SAMPLE: 4056707
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 22.3 112 70-130
1,2-Dichloroethane-d4 (S) % 120 67-130
Toluene-d8 (S) % 105 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4056708
4056709
MS
MSD
92673197011 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L <0.86 20
20 20.2
20.2 101
101
55-137 0 H1
1,2-Dichloroethane-d4 (S)
%
121
123
67-130
Toluene-d8(S)
%
107
106
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 55
Pace Analytical Services, LLC
leac,yficalAnal1377 South Park Drive
Kernersville, NC 27284
www.pacelabs.com (704)977-0981
QUALIFIERS
Project: Rutherford South
Pace Project No.: 92673197
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Rutherford South
92673197
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92673197001
MW-1
EPA 3010A
781913
EPA 6010D
782012
92673197002
MW-2A
EPA 3010A
781913
EPA 6010D
782012
92673197003
MW-3
EPA 3010A
781913
EPA 6010D
782012
92673197004
MW-4A
EPA 3010A
781913
EPA 6010D
782012
92673197005
MW-5
EPA 3010A
781913
EPA 6010D
782012
92673197006
MW-6
EPA 3010A
782949
EPA 6010D
783083
92673197007
MW-7
EPA 3010A
782949
EPA 6010D
783083
92673197008
MW-8
EPA 3010A
782949
EPA 6010D
783083
92673197009
MW-9S
EPA 3010A
782949
EPA 6010D
783083
92673197010
MW-91)
EPA 3010A
782949
EPA 6010D
783083
92673197011
SW-1
EPA 3010A
782949
EPA 6010D
783083
92673197012
SW-2
EPA 3010A
782949
EPA 6010D
783083
92673197001
MW-1
EPA 7470A
783001
EPA 7470A
783118
92673197002
MW-2A
EPA 7470A
783001
EPA 7470A
783118
92673197003
MW-3
EPA 7470A
783001
EPA 7470A
783118
92673197004
MW-4A
EPA 7470A
783001
EPA 7470A
783118
92673197005
MW-5
EPA 7470A
783001
EPA 7470A
783118
92673197006
MW-6
EPA 7470A
783001
EPA 7470A
783118
92673197007
MW-7
EPA 7470A
783001
EPA 7470A
783118
92673197008
MW-8
EPA 7470A
783001
EPA 7470A
783118
92673197009
MW-9S
EPA 7470A
783001
EPA 7470A
783118
92673197010
MW-91)
EPA 7470A
783001
EPA 7470A
783118
92673197011
SW-1
EPA 7470A
783001
EPA 7470A
783118
92673197012
SW-2
EPA 7470A
783001
EPA 7470A
783118
92673197001
MW-1
EPA 8260D
782397
92673197002
MW-2A
EPA 8260D
782397
92673197003
MW-3
EPA 8260D
783090
92673197004
MW-4A
EPA 8260D
782401
92673197005
MW-5
EPA 8260D
782401
92673197006
MW-6
EPA 8260D
782401
92673197007
MW-7
EPA 8260D
782401
92673197008
MW-8
EPA 8260D
782401
92673197009
MW-9S
EPA 8260D
782401
92673197010
MW-913
EPA 8260D
782401
92673197011
SW-1
EPA 8260D
782401
92673197012
SW-2
EPA 8260D
782401
92673197001
MW-1
EPA 8260D Mod.
782001
92673197002
MW-2A
EPA 8260D Mod.
782001
92673197003
MW-3
EPA 8260D Mod.
782001
92673197004
MW-4A
EPA 8260D Mod.
782001
92673197005
MW-5
EPA 8260D Mod.
782001
92673197006
MW-6
EPA 8260D Mod.
782001
92673197007
MW-7
EPA 8260D Mod.
782001
92673197008
MW-8
EPA 8260D Mod.
782001
92673197009
MW-9S
EPA 8260D Mod.
782001
92673197010
MW-91)
EPA 8260D Mod.
782001
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 06/30/2023 04:44 PM
without the written consent of Pace Analytical Services, LLC.
Page 51 of 55
leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
(704)977-0981
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Rutherford South
Pace Project No.: 92673197
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92673197011 SW-1 EPA 8260D Mod.
92673197012 SW-2 EPA 8260D Mod.
782002
782002
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2023 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 55
C)
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Page 53 of 55
DC#_T€tle: ENV-FRM-HUN1-0083 02_Sampie Condition Upon Receipt
ace,
Id1G SfIYC?l
Effective Date: 11/14/2022 8:18.30 AM
Laboratory refelving samples:
Asheville I Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[:] Atlanta❑ Kernersville❑
Client Name:
Upon Receipt C—�
Project ff:
Tr t� e�
Courier: LJFedEx uUPs L_.tUsP5 Uclient
❑ Commercial IKace ❑Other!-__
Custody Seal Present? Oyes )gNo Seals Intact? ❑Yes �No I R
Date/initials Person Examining Contents:_
Packing Material: ❑ Bubble Wrap Bubble Bags ElNone ❑ other Biological Tissue Frozen?
Thermometer: V []Yes []No ❑ N/A
❑ IR Gun ID. IQRCT Type of Ice: �Qet
1 Correction Factor:
Cooler Temp: - �' S Add/5ubtract ('C) C)
Cooler Temp Corrected ('C): �.
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United Slates: CA, NY, or SC
fcherk mansi? ❑Yes ❑No
❑ Blue ❑ None
Temp should be above freezing to 6'C
❑ Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (Internationally,
includine Hawaii and Puerto Ricol? ❑Yes ❑ No
Comments/Discrepancy:
Chain of Custody Present?
Me,
❑ No
:J N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
No
❑ WA
3.
Rush Turn Around Time Requested?
❑ Yes
o
❑NIA
4.
Sufficient Volume?
Yes
❑No
❑NIA
S.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑No
❑No
❑NIA
❑N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7
Dissolved analysis. Samples Field Filtered?
❑Yes
tft
❑N/A
a.
Sample Labels Match COC?
-includes Date/Ttme/ID/Analysis Matrix:
®Yes
T
❑No
❑H/A
9
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
#fW
o
❑ N/A
❑N/A
11,
COMMENTS/SAMPLE DISCREPANCY f` Field Data Required? UYes U No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: _. . _..._.. _.. _ ...._ Date/Time:
Project Manager SCURF Review: Date:
Project Manager S R F Review:
Date:
Page 54 of 55
DC# Title: ENV-FRM-HUN1-0083 02- Sample Condition Upon Receipt
l41 SIG;SlrFiff
Effective Date- 11/14/2022 8:18:30 AM
*Check mark top half of box If pH and/or dechlorination is verified and project N
within the acceptance range for preservation samples.
Exceptions; VOA, Collfornt, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
;* Bottom half of box Is to list number of bottles
' * "`Check jJ1 unpreserved Nitrates for chlorine
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pH adjustment
Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot A
i
Note. Whenever there " sad1 screpancyaffectingNarth Carolina compliancesamples, a copy oft his form wiU be sent to the North Carolira DENRCerbrcat!Dn Office (t e.
Out of hold, incorrect preservative, out of temp, Incorrect containers. Page 55 of 55