FA-7735_42022_CA_MRP_20230609

ENVIRONMENTAL | CIVIL | GEOTECHNICAL
MONITORING REPORT
HALL’S STORE 9830 HIGH HOUSE ROAD SALEMBURG, SAMPSON COUNTY, NC NCDEQ INCIDENT NO. 42022 RISK CLASSIFICATION: H105R
JUNE 9, 2023
NCDEQ CONTRACT NO. N122019D TASK AUTHORIZATION NO. 03 CATLIN PROJECT NO. 220284
PREPARED FOR:
MR. HASSAN OSMAN NCDEQ, DWM, UST SECTION 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646
PREPARED BY:
CATLIN ENGINEERS AND SCIENTISTS 220 OLD DAIRY ROAD WILMINGTON, NC 28405 [phone]
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585
CORPORATE LICENSURE NO. FOR GEOLOGY SERVICES C-118
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023
TABLE OF CONTENTS
PAGE
1.0 SITE INFORMATION 1
2.0 EXECUTIVE SUMMARY 2
3.0 SCOPE OF SERVICES 3
4.0 SITE HISTORY AND CHARACTERIZATION 3
4.1 UST OWNER AND OPERATOR INFORMATION 3 4.2 UST INFORMATION 4 4.3 CONTAMINANT SOURCE INVENTORY 4 4.4 SITE CHARACTERISTICS 5 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE 5 4.6 RECEPTOR INFORMATION 5 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES 5
5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY 7
5.1 SOIL AND BEDROCK 7
5.2 HYDROGEOLOGY 7
6.0 SITE ASSESSMENT INFORMATION 8
6.1 MONITORING WELL INSTALLATION 8 6.2 MMPE EVENT 8 6.3 GAUGING DATA 9 6.4 SAMPLING DATA 10 6.5 SUMMARY OF GROUNDWATER INFORMATION 10 6.6 EVALUATION OF ASSESSMENT INFORMATION 11
7.0 CONCLUSIONS AND RECOMMENDATIONS 12
8.0 STATEMENTS AND CERTIFICATION 13
9.0 LIMITATIONS 13
10.0 REFERENCES 14
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023
TABLES
TABLE 1 SITE HISTORY – UST AND OTHER RELEASE INFORMATION
TABLE 2 PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
TABLE 3 WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
TABLE 4 SUMMARY OF GROUNDWATER LABORATORY RESULTS – STANDARD
METHOD 6200B
TABLE 5 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B
FIGURES
FIGURE 1 SITE VICINITY MAP
FIGURE 2 POTENTIAL RECEPTOR MAP
FIGURE 3 SITE MAP
FIGURE 4 GROUNDWATER ELEVATION – MAY 11, 2023
FIGURE 5 MONITORING WELL GROUNDWATER SAMPLE ANALYTICAL RESULTS – MAY 11, 2023
FIGURE 6 ESTIMATED HORIZONTAL EXTENT OF BENZENE – MAY 11, 2023
FIGURE 7 ESTIMATED HORIZONTAL EXTENT OF NAPHTHALENE – MAY 11, 2023
APPENDICES
APPENDIX A HISTORICAL DATA
APPENDIX B SITE PHOTOGRAPHS
APPENDIX C JOB HAZARD ANALYSES AND FIELD DATA SHEETS
APPENDIX D WELL LOGS AND WELL CONSTRUCTION RECORDS
APPENDIX E MMPE REPORT AND DISPOSAL DOCUMENTS
APPENDIX F LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 1 June 2023
1.0 SITE INFORMATION
Site Identification
Date: 06/09/2023 Site Risk/Priority Rank: H105R
UST Number: FA-7735 Incident Number: 42022
Site Name: Hall’s Store Facility ID: 0-009410
Site Location: 9830 High House Road
Nearest City/Town: Salemburg County: Sampson
Description of Geographical Data Point: Former UST basin
Location Method: Google Earth
Latitude (decimal degrees): 35.11383° Longitude (decimal degrees): -78.53738°
Contacts Information
UST Owner: Hall’s Store, LLC (Kyle Hall)
Address: 307 Wilton Avenue, West Jefferson, NC Phone: [phone]
UST Operator: Hall’s Store, LLC (Kyle Hall)
Address: 307 Wilton Avenue, West Jefferson, NC Phone: [phone]
Property Owner: Hall’s Store, LLC (Kyle Hall)
Address: 307 Wilton Avenue, West Jefferson, NC Phone: [phone]
Property Occupant: Hall’s Store
Address: 9830 High House Road, Salemburg, NC 28385 Phone: Not Provided
Consultant: CATLIN Engineers and Scientists
Address: 220 Old Dairy Rd., Wilmington, NC 28405 Phone: [phone]
Corporate Licensure No. For Engineering Services: C-0585
Corporate Geology License No.: C-118
Analytical Laboratory: Con-Test Analytical Laboratory State Certification: NC 652, NC-DW 25703
Address: 39 Spruce St., E. Longmeadow, MA 01028 Phone: [phone]
Release Information
Date Discovered: 05/11/2016
Estimated Quantity of Release: Unknown
Cause of Release: Leak in the UST system
Source of Release: UST system or associated fitting(s)
Sizes and contents of UST system(s) from which the release occurred:
•Two 3,000-gallon gasoline USTs
•Two 2,000-gallon gasoline USTs
•Two 500-gallon kerosene USTs
•Two 4,000-gallon USTs (unknown contents)
•One 500-gallon UST (unknown contents)
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CATLIN Project No. 220284 2 June 2023
2.0 EXECUTIVE SUMMARY
The Hall’s Store site is located at 9830 High House Road, Salemburg, Sampson
County, North Carolina. Nine underground storage tanks (USTs) were previously
operated at the site. Two 2,000-gallon and one 500-gallon USTs were removed in May 2016 and a petroleum release was discovered during tank closure activities. Two 4,000-gallon and one 500-gallon USTs were removed in 2019, and at least one additional release was confirmed.
The purpose of this report is to document the latest monitoring well installation and groundwater sampling event. On February 1, 2023, CATLIN Engineers and Scientists (CATLIN) personnel advanced three borings for construction of Type II monitoring wells (MW-5, MW-6, and MW-7) to 20 feet below land surface (BLS). The depth to water (DTW) at monitoring wells (MW-1, MW-3, and MW-4) was gauged
prior to drilling activities at an average of approximately 15 feet deep. Monitoring
well MW-2 was dry. When CATLIN returned to gauge the new wells on February 2, 2023, light non-aqueous phase liquid (LNAPL; aka free product) was measured in all three wells (ranging from 0.61 to 0.66 feet thick).
From April 10 through 14, 2023, CATLIN coordinated a mobile multi-phase
extraction (MMPE) event conducted by Eastern Environmental Management (EEM). A total of 14,382 gallons of impacted groundwater and LNAPL were recovered, as well as a calculated 6,163.82 pounds (equivalent to 986.21 gallons) of petroleum vapors.
CATLIN returned to the site on May 11, 2023 for sampling activities. Groundwater
was measured at approximately 15 feet deep across the site. LNAPL was not measured in any of the monitoring wells. Groundwater samples from six monitoring wells (MW-1, MW-3, MW-4, MW-5, MW-6, and MW-7) were collected. The samples were submitted for laboratory analysis of volatile organic compounds (VOCs) per Standard Method (SM) 6200B plus ethylene dibromide (EDB), methyl tert-butyl ether
(MTBE), and diisopropyl ether (DIPE).
Laboratory results did not indicate any dissolved petroleum constituents above their respective laboratory reporting limits in the samples from MW-3 and MW-4. Several VOCs were detected in the MW-1, MW-5, MW-6, and MW-7 samples at concentrations greater than those established in Title 15A of the North Carolina
Administrative Code, Subchapter 2L, Section .0202 Groundwater Quality Standards (2L GWQS), but below the Gross Contaminant Levels (GCL).
The contaminant concentrations reported from MW-1 during this period are generally higher than those in the previous sampling event in November 2022.
CATLIN recommends attempting to obtain access for sampling WSW-1, WSW-4
and WSW-7 and conducting another mobile multi-phase extraction (MMPE) event followed by a monitoring/sampling event.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 3 June 2023
3.0 SCOPE OF SERVICES
The scope of services for this report was performed in general accordance with
CATLIN proposal number 220284.3P, dated January 24, 2023. Services were
authorized by the North Carolina Department of Environmental Quality’s (NCDEQ’s) Task Authorization (TA) #03, accepted on January 25, 2023, and Contract Number N122019D.
The approved scope of services for this Task Authorization included to:
•Update the site-specific Health and Safety Plan (HASP) for drilling activities;
•Install three Type II monitoring wells (MW-5, MW-6, and MW-7) to 20 feet
BLS;
•Survey the top of casing (TOC) elevations of four monitoring wells (threenewly installed wells and one preexisting well);
•Gauge three monitoring wells (MW-1, MW-3, and MW-4) once prior to drilling
and once prior to sampling;
•Gauge and collect groundwater samples from four monitoring wells (MW-2,MW-5, MW-6, and MW-7);
•Analyze five water samples (four monitoring well samples and one trip blank)according to SM 6200B (including EDB, MTBE, and DIPE); and,
•Prepare and submit a monitoring report summarizing the findings.
Due to the presence of LNAPL in the newly installed monitoring wells, a Change Order was proposed and accepted on February 3, 2023. The approved scope of services for this Change Order included to:
•Coordinate and oversee a MMPE event utilizing monitoring wells MW-5,
MW-6, and MW-7 as extraction points; and
•Conduct a groundwater sampling event approximately 30 days after theMMPE event.
The scopes of services were conducted in accordance with the approved TA and associated Change Order.
4.0 SITE HISTORY AND CHARACTERIZATION
The Hall’s Store site is located at 9830 High House Road, Salemburg, Sampson County, North Carolina (Figures 1 and 2). Summarized available historical sampling and gauging data from previous consultants are provided in Appendix A. Recent site photographs are presented in Appendix B.
4.1 UST OWNER AND OPERATOR INFORMATION
Hall’s Store, LLC (Hall’s Store) owned the six registered USTs historically operated on-site. The former grocery store and petroleum service station
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CATLIN Project No. 220284 4 June 2023
operated the tanks for retail petroleum sales. Three additional unregistered USTs were discovered during a geophysical survey in 2018. There is no available owner or operator information for the three additional tanks. The
site was accepted into the North Carolina UST Section Trust Fund Branch
State Lead Program in 2018 (NCDEQ, 2018). Available information regarding UST owners/operators is presented on Table 1.
4.2 UST INFORMATION Four gasoline and two kerosene USTs were previously operated on-site by Hall’s Store. Two 3,000-gallon gasoline USTs and one 500-gallon kerosene
UST were installed in May 1976 and closed by removal in December 1993.
Two 2,000-gallon gasoline USTs were installed in September 1986 and were removed in May 2016. A 500-gallon kerosene UST (installation date unknown) was also removed in 2016. Soil staining and a strong petroleum odor was noted in the soil beneath the removed 500-gallon kerosene UST
(S&ME, 2019A).
During a 2018 geophysical survey performed by S&ME, Inc. (S&ME), two 4,000-gallon unregistered USTs were discovered approximately seven feet north of monitoring well MW-2 and were closed by removal in October 2019.
The presence of a previously discovered unregistered 500-gallon UST was
also confirmed and removed in September 2019 (S&ME, 2019B). Available UST system information is presented in Table 1 and the approximate known former UST basin locations are illustrated on Figure 3.
4.3 CONTAMINANT SOURCE INVENTORY An on-site release was discovered in May 2016 during UST removal activities. Soil sample analytical results reported total petroleum
hydrocarbons (TPH) at concentrations up to 8.1 milligrams per kilogram
(mg/kg). Petroleum-impacted groundwater was confirmed in June 2016 during sampling of monitoring well MW-1, installed near the UST basin. Several contaminants were identified above their 2L GWQS. It was concluded that groundwater impacts were likely the result of one or more
releases from the gasoline UST system (ECE, 2016). During the installation of monitoring well MW-2 in 2018, a strong petroleum odor was noted. Soil sampling revealed multiple contaminants exceeding their Soil-to-Groundwater (STGW) maximum soil contaminant concentrations
(MSCC). This led to the discovery of two additional unregistered USTs that had contributed to the release (S&ME, 2019A).
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 5 June 2023
4.4 SITE CHARACTERISTICS The property is owned by Kyle Hall and the former store structure is now
vacant. The parcel is comprised of the store building and agricultural land.
4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE
Properties in the site vicinity are mostly residences and agricultural land. A
residence, with an active potable water supply well, adjoins the property to the east. Agricultural fields are located to the west (across Dunn Road) and south (across High House Road). A parcel with a residence and active potable water supply well is also located to the south. A former
gasoline/country store, presently operating as a Church, is located across the
Dunn-High House intersection to the southwest. Wooded land adjoins the site property to the north. 4.6 RECEPTOR INFORMATION

Conducting a receptor survey was outside the scope of this monitoring event. A review of historical files available on the NCDEQ Waste Management Online Database (aka Laserfiche) indicates that the last receptor survey for the Hall’s Store site was conducted in 2018 by S&ME.

According to previous reports, municipal water is available to the site vicinity, but multiple residences continue to use their private water supply wells for drinking water and irrigation. No water supply wells were identified within 250 feet of the site. Twelve water supply wells have been identified within 1,000
feet of the source area. Ten potable water supply wells are located within
1,000 feet of the site and of those, four (WSW-4, WSW-7, WSW-8, and WSW-9) are within 500 feet of the release and two (WSW-8 and WSW-11) are inactive. Two of the wells (WSW-8A and WSW-10) are used only for irrigation, and as of 2018 one (WSW-8A) was inactive.
A drainage ditch is located approximately 200 feet north-northeast of the site. No other surface water bodies were noted. Potential receptors are illustrated on Figure 2 and receptor information from
S&ME (2019) is shown in Table 2. 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES As discussed above, the release was discovered in 2016 during UST closure
activities. During UST removal, approximately 130 tons of petroleum impacted soil were removed from the site. Composite soil samples contained TPH gasoline range organics (GRO) and diesel range organics (DRO) concentrations up to 7.8 mg/kg and 8.1 mg/kg, respectively. Multiple
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 6 June 2023
petroleum constituents were also detected in a groundwater sample at concentrations above their respective 2L GWQS (ECE, 2016).
A Limited Site Assessment (LSA) report was prepared in 2016, and in 2018
three additional monitoring wells (MW-2, MW-3, and MW-4) were installed at the site. Strong petroleum odors were noted during the installation of MW-2, and a soil sample was collected. Analytical results revealed multiple targeted analytes above their STGW MSCC. During subsequent sampling activities,
LNAPL (1.44 feet) was measured in MW-2. Groundwater samples were
collected from the remaining wells (MW-1, MW-2, and MW-4). Analytical results revealed naphthalene and 1,2,4-trimethylbenzene at concentrations above their 2L GWQS in the MW-1 sample. No VOCs were detected in the samples from MW-3 and MW-4 (S&ME, 2019A).

Due to the elevated contamination in monitoring well MW-2, a geophysical survey was conducted in December 2018. Two additional unregistered USTs were discovered, and the location of a third previously identified tank was confirmed. These tanks were removed from the site in late 2019. A total of
486.70 tons of petroleum impacted soil was excavated and removed during
tank closure activities. Risk-based soil samples were collected from the UST excavation but were reportedly lost by the courier and never analyzed. Analytical results for TPH revealed GRO and DRO concentrations up to 12,000 mg/kg and 870 mg/kg, respectively. Reports available on Laserfiche
indicate that all known USTs have now been removed from the site (S&ME,
2019B). CATLIN conducted a groundwater monitoring event in July 2021. Three monitoring wells (MW-1, MW-3, and MW-4) were sampled. LNAPL was
measured in MW-2 at 0.88 feet thick; therefore, this well was not sampled.
No analyzed compound concentrations were detected above their laboratory reporting limits in the MW-3 and MW-4 samples. Laboratory analysis indicated several targeted analytes in the MW-1 sample; however, they were all below their 2L GWQS (CATLIN, 2021).

In October 2022, CATLIN coordinated an aggressive fluid vapor recovery (AFVR) event utilizing monitoring wells MW-1 and MW-2 as extraction points. The eight-hour event removed a total of 980 gallons of impacted groundwater and 45.26 pounds of petroleum vapor (equivalent to 7.24 gallons of
petroleum) were removed from the subsurface (CATLIN, 2022).
CATLIN personnel returned to the site in November 2022 and sampled monitoring well MW-1. No LNAPL was observed in the well. Monitoring wells MW-2 and MW-3 were dry at the time of field activities. Laboratory analysis
revealed that several targeted analytes were detected at low or estimated
(“J”-value) concentrations, but all were below their respective 2L GWQS. CATLIN attempted to gain access to sample water supply wells WSW-4 and WSW-7 but received no response (CATLIN, 2022).
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 7 June 2023
Summarized historical data prepared by S&ME are presented in Appendix A. Site photographs are included in Appendix B.
5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY
5.1 SOIL AND BEDROCK As defined in the Geologic Map of North Carolina, published by the North
Carolina Department of Natural Resources and Community Development
(1985), the site lies within the Coastal Plain physiographic province. The North Carolina Coastal Plain is approximately 90 to 150 miles wide from
the Atlantic Ocean westward to its boundary with the Piedmont province.
Two natural subdivisions of the Coastal Plain were described by Stuckey (1965): the Tidewater region and the Inner Coastal Plain. The project area is located within the Inner Coastal Plain, which is an area of erosional
topography (Horton and Zullo, 1991).
The Coastal Plain comprises a wedge-shaped sequence of stratified marine and non-marine sedimentary rocks deposited on crystalline basement. The sedimentary sequences range in age from Recent to lower Cretaceous
(Narkunas, 1980).
The site is underlain by the Black Creek formation. According to the 1985 Geologic Map of North Carolina, lignitic clay, thin beds of fine-grained micaceous sand, and thick lenses of cross-bedded sand crop out around the
site area.
According to the well logs for monitoring wells MW-6 and MW-7, silty sand or fine sand underlies the site to approximately three feet BLS. Silty clay is present from three to 13 feet BLS. Fine to medium sand was observed at
further depths up to 22 feet BLS.
5.2 HYDROGEOLOGY Groundwater - The 2020 Visual Hydrogeologic Framework (VHF) – North
Carolina Hydrogeological Database identified sufficient boreholes near the
site in order to draw a cross-section. According to the VHF, the surficial aquifer may extend to 20 feet below land surface (BLS). The Black Creek confining unit (10 feet thick) and aquifer are projected from 20 to 50 feet BLS. The Upper Cape Fear confining unit (approximately 40 feet thick) underlies
the Black Creek aquifer. The Upper Cape Fear aquifer extends from
approximately 190 to 300 feet BLS. Crystalline basement is expected to be encountered at 300 feet BLS in the site vicinity.
Surface Water – A drainage ditch is located approximately 200 feet north-
northeast of the site (S&ME, 2019A). It’s identified on the United States
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CATLIN Project No. 220284 8 June 2023
Geological Survey (USGS) Topographic Map as an unnamed intermittent tributary.
6.0 SITE ASSESSMENT INFORMATION
CATLIN conducted field activities in general accordance with the approved TA and pre-prepared HASP. Upon arrival at the site, potential hazards were evaluated before beginning field work and are documented on electronic Job Hazard Analysis
(JHA) forms. The JHA forms are included in Appendix C. Photographs from the site
visits are included in Appendix B. Well locations and site features are shown on Figure 3 and well construction details are presented in Table 3. 6.1 MONITORING WELL INSTALLATION

On February 1, 2023, two borings were advanced to 20 feet BLS (MW-5 and MW-7) and one to 22 feet BLS (MW-6) for monitoring well construction by a North Carolina Certified Well Contractor, utilizing hollow stem augers and a Diedrich D-50 drill rig. Cuttings generated during drilling activities were
spread on-site. All wells were installed to 20 feet BLS.
The wells (MW-5, MW-6, and MW-7) were constructed of new, threaded PVC casing and screen. No glues or cements were used in joining PVC components. New nitrile gloves were worn while handling all well materials.
The monitoring wells were constructed with a pointed PVC sediment trap, 15
feet of 2-inch diameter, 0.010-inch slotted PVC well screen and approximately five feet of 2-inch diameter solid PVC riser to the surface. The annular space was filled with coarse sand pack to approximately two feet above the well screen in MW-5 and MW-6 and one foot above the well
screen in MW-7. Bentonite chips were added to within one foot of the ground
surface. The bentonite chips were poured from the surface while simultaneously pouring water to facilitate hydration. The wells were finished with a concrete pad and flush-mount steel wellhead and locking well cap. After installation, the monitoring wells were developed by over-pumping. The
TOC elevations were surveyed using traditional methods (Rod and Level) in
reference to a preexisting monitoring well with a known elevation (MW-2). Monitoring well construction information is summarized in Table 3 and a site map with monitoring well location is illustrated on Figure 3. Site photographs
are presented in Appendix B. The well logs and Well Construction Records were submitted to NCDEQ on February 3, 2023; copies are provided in Appendix D. 6.2 MMPE EVENT
CATLIN mobilized to the site on April 10 and 14, 2023 to supervise a MMPE event conducted by EEM. Prior to the event, CATLIN personnel gauged MW-5, MW-6, and MW-7 and the average DTW was approximately 16.4 feet
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 9 June 2023
below top of casing (BTOC). LNAPL was not measured in any of the monitoring wells. Gauging results are included in Table 3.
The MMPE event was conducted for a duration of 96 hours, ending on April
14, 2023. Monitoring wells MW-5, MW-6, and MW-7 were utilized as extraction points. A total of 14,382 gallons of impacted groundwater was removed from the subsurface. A calculated 6,163.82 pounds of petroleum vapors were emitted during this event, equivalent to approximately 986.21
gallons of petroleum. The average rate of fluid recovery was 149.81 gallons
per hour. There was no measurable thickness of LNAPL following the event. The MMPE report from EEM, including waste manifests and emissions calculations, is included in Appendix E.
6.3 GAUGING DATA Historical gauging results show DTW ranging from 8.00 feet BTOC (MW-1) to 17.18 feet BTOC (MW-1). Historical groundwater flow direction was towards
the southwest (S&ME, 2019B; CATLIN, 2022).
CATLIN conducted multiple gauging events during this monitoring period. During each event, DTW was measured using an electronic water interface probe. To prevent cross contamination, the probe and cabling were
decontaminated according to the manufacturer’s recommendations between
use in each well. Gauging data were recorded on an electronic groundwater sampling form using a tablet device. Gauging procedures were performed in general accordance with North Carolina Department of Environmental and Natural Resources (NCDENR) and NCDEQ Guidelines, and Environmental
Protection Agency (EPA) Region 4 Operating Procedures.
Prior to drilling for monitoring well installation on February 1, 2023, three monitoring wells (MW-1, MW-3, and MW-4) were gauged. The DTW was measured at 17.26 feet BTOC (MW-1), 12.80 feet BTOC (MW-3), and 15.53
feet BTOC (MW-4). LNAPL was not detected in any of the wells.
After monitoring well installation, the three new monitoring wells (MW-5, MW-6, and MW-7) were gauged on February 2, 2023. The depths to water were measured at 18.21 feet BTOC (MW-5), 17.92 feet BTOC (MW-6), and
18.42 feet BTOC (MW-7). LNAPL was measured in all the monitoring wells;
0.61 feet thick in MW-5, 0.66 feet thick in MW-6, and 0.66 feet thick in MW-7. Approximately one month following the MMPE, on May 11, 2023, CATLIN personnel gauged all on-site monitoring wells (MW-1, MW-2, MW-3, MW-4,
MW-5, MW-6, and MW-7). The DTW ranged from 13.39 feet BTOC (MW-3)
to 16.00 feet BTOC (MW-7). LNAPL was not encountered during this event. Based on groundwater elevations calculated for this gauging event, groundwater flow direction is towards the north-northeast.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 10 June 2023
Monitoring well gauging results for events conducted by CATLIN are presented in Table 3. The groundwater elevation is illustrated on Figure 4 and groundwater sampling forms are provided in Appendix C.
6.4 SAMPLING DATA Following gauging, the monitoring wells were sampled in general accordance with NCDENR and NCDEQ Guidelines, and EPA Region 4 Operating
Procedures. Prior to obtaining a representative groundwater sample, the
monitoring wells were purged by removing a minimum of three well volumes using a new, disposable bailer. Monitoring well groundwater field parameter data were measured at one-minute intervals using an In-Situ Aqua TROLL 600 Multiparameter Sonde (Aqua TROLL). Conductivity, pH, oxidation
reduction potential (ORP), dissolved oxygen, and temperature
measurements were recorded utilizing the VuSitu mobile application (version 1.17.12). Groundwater parameter data were transferred from the VuSitu mobile application to the electronic groundwater sampling forms. Copies of the groundwater sampling forms are available in Appendix C.
After a minimum of three well volumes were removed (or the well was bailed dry), a groundwater sample was collected from each well and poured into appropriate pre-preserved laboratory-provided glassware, labeled, and placed on ice in an insulated cooler. A laboratory-provided trip blank was
maintained in the cooler for the duration of the event. The groundwater samples and laboratory-provided trip blank were submitted to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC)
protocol and analyzed per SM 6200B (including EDB, MTBE, and DIPE). The laboratory analytical data and COC are included in Appendix F. 6.5 SUMMARY OF GROUNDWATER INFORMATION
Historically, samples from monitoring well MW-1 have contained the highest petroleum constituent concentrations. LNAPL has previously been detected at this site in MW-2 ranging from 0.3 feet thick (December 7, 2018) to 1.44 feet thick (December 18, 2018). During the previous sampling event conducted by CATLIN (November 2022), the sample from MW-1 did not have
any contaminants at concentrations above 2L GWQS. No petroleum constituents have been historically detected at concentrations above GCL (S&ME, 2019A; CATLIN, 2021). The latest groundwater sampling laboratory results for SM 6200B analysis
are summarized in Table 4. Historical results for events conducted by
CATLIN are in Table 5. Monitoring well sample analytical results are illustrated on Figure 5. Historical groundwater sampling results are provided in Appendix A. A copy of the complete laboratory report and COC documentation are in Appendix F.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 11 June 2023
Monitoring Wells During the May 2023 monitoring event, six monitoring well groundwater
samples (MW-1, MW-3, MW-4, MW-5, MW-6, and MW-7) were collected and
submitted for analysis via SM 6200B (including EDB, MTBE, and DIPE). Laboratory analysis did not detect any constituents above their respective reporting limits in the samples from MW-3 and MW-4. No analyte concentrations were detected above GCL in any of the monitoring well
samples. Analytical results reported the following constituents at
concentrations above their 2L GWQS in samples MW-1, MW-5, MW-6, and MW-7:
• MW-1: n-butylbenzene, sec-butylbenzene, isopropylbenzene, p-
isopropyltoluene, 1,2,4-trimethylbenzene, and 1,3,5-
trimethylbenzene;
• MW-5: benzene, n-butylbenzene, ethylbenzene, isopropylbenzene, p-isopropyltoluene, MTBE, naphthalene, n-propylbenzene, toluene,
1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes;
• MW-6: n-butylbenzene, sec-butlybenzene, ethylbenzene, isopropylbenzene, p-isopropyltoluene, naphthalene, n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and total
xylenes; and
• MW-7: benzene, n-butylbenzene, ethylbenzene, isopropylbenzene, MTBE, naphthalene, n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and total xylenes.

Trip Blank One laboratory-provided trip blank sample was submitted for analysis per SM 6200B (including EDB, MTBE, and DIPE). No targeted analytes were
detected in the sample.
6.6 EVALUATION OF ASSESSMENT INFORMATION Extent of Contamination

Several petroleum constituents were detected above their respective 2L GWQS in samples from MW-1, MW-5, MW-6, and MW-7. However, no constituents were reported above GCL. A summary of monitoring well groundwater sample analytical results are illustrated on Figure 5. The
estimated horizontal extents of benzene and naphthalene are shown on
Figures 6 and 7, respectively.
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CATLIN Project No. 220284 12 June 2023
Cleanup Levels Achieved
Soil – To date, approximately 614.18 tons of impacted soil have been
removed from the site. Soil samples obtained in 2019 revealed TPH GRO
and DRO concentrations up to 12,000 mg/kg and 870 mg/kg, respectively. Risk-based soil sample analytical results have not been obtained (S&ME, 2019B).
Groundwater – Groundwater contaminant concentrations are above 2L
GWQS but below GCL at the site.
LNAPL – Prior to the MMPE, LNAPL was measured in monitoring wells MW-5, MW-6, and MW-7 (up to 0.66 feet thick). However, LNAPL was not
encountered one month after the MMPE. LNAPL has been periodically
measured at the site since 2018.
7.0 CONCLUSIONS AND RECOMMENDATIONS
Conclusions
Groundwater monitoring findings for this period are summarized below:
•Gauging events were conducted prior to drilling, approximately 24 hours after
well installation, before and after the MMPE event, and prior to sampling.
•Three Type II monitoring wells (MW-5, MW-6, and MW-7) were installed to20 feet BLS.
•Approximately 24 hours after well installation, LNAPL was measured in
MW-5 (0.61 feet), MW-6 (0.66 feet), and MW-7 (0.66 feet).
•A MMPE was conducted utilizing monitoring wells MW-5, MW-6, and MW-7as extraction points. A total of 14,382 gallons of impacted groundwater and
LNAPL were recovered. A calculated 6,163.82 pounds of petroleum vapors
were removed, equivalent to 986.21 gallons of petroleum.
•Groundwater samples were collected from six monitoring wells (MW-1,MW-3, MW-4, MW-5, MW-6, and MW-7).
•LNAPL was not observed in any of the monitoring wells during sampling.
•No analyzed compound concentrations were detected above their respective2L GWQS in the MW-3 and MW-4 samples.
•Several petroleum constituents were above their respective 2L GWQS in thesamples from MW-1, MW-5, MW-6, and MW-7. However, none were aboveGCL.
•Contaminant concentrations in samples from MW-1 have increased since theprevious sampling event in November 2022.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 13 June 2023
Recommendations
CATLIN recommends attempting to obtain access for sampling WSW-1, WSW-4
and WSW-7 and conducting another mobile multi-phase extraction (MMPE) event
followed by a monitoring/sampling event.
8.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. June 9, 2023
Will this report be submitted after the established due date? NO
2 Was any required information from the above template missing from this report? YES
No cross sections are provided.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? NA
No CAP has been submitted for this site.
4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? NO
6 Certification:
I, Benjamin J. Ashba, a Licensed Geologist for CATLIN Engineers and Scientists, do certify that the information contained in this report is correct and accurate to the best of my
knowledge.
CATLIN Engineers and Scientists is licensed to practice geology in North Carolina. The certification number of the company or corporation is C-118.
9.0 LIMITATIONS
The groundwater samples analyzed as part of this investigation only provide isolated
data points and may not represent conditions at every location in the project area. Analyses and conclusions of this report, being based on interpolation between data points at the project area, may not be completely representative of all site conditions. Conclusions and recommendations of this investigation and report are
based on the best available data in an effort to comply with current regulatory
requirements.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 14 June 2023
10.0 REFERENCES
CATLIN Engineers and Scientists, Monitoring Report, Hall’s Store, 9830 High
House Road, Salemburg, Sampson County, North Carolina, NCDEQ Incident
No. 42022, Risk Classification: H105R, August 13, 2021.
CATLIN Engineers and Scientists, Monitoring Report, Hall’s Store, 9830 High
House Road, Salemburg, Sampson County, NC, NCDEQ Incident No. 42022, Risk Classification: H105R, December 6, 2022.
Engineering & Environmental Science Company, UST Closure Report, Hall’s Store,
9830 High House Rd., Salemburg, NC 23835, July 26, 2016.
Horton, J. Wright, Jr. and Victor A. Zullo, An Introduction to the Geology of the
Carolinas: The Geology of the Carolinas, pp 1-11.
Narkunas, J., Groundwater Evaluation in the Central Coastal Plain of North
Carolina, North Carolina Department of Natural Resources and Community
Development, 1980, pp 119.
NCDENR, UST Section, North Carolina Department of Environment and Natural Resources, Division of Waste Management, Guidelines for Sampling, December 1, 2013.
NCDEQ, Division of Water Resources, 2020 Visual Hydrogeologic Framework,
North Carolina Hydrogeological Database, ncwater.org/?page=350, accessed August 9, 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Corrective Action Guidelines, January 19,
2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Guidelines for Site Checks, Tank Closure,
and Initial Response and Abatement, January 19, 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality,
Division of Waste Management, MEMO – Recommendation for State Lead
Cleanup, May 22, 2018.
North Carolina Department of Natural Resources and Community Development,
Geological Map of North Carolina, 1985.
S&ME, Inc., Initial Monitoring Report, Hall’s Store, Incident #42022, 9830 High
House Road, Salemburg, Sampson County, NC, S&ME Project No. 4305-18-
159A, February 15, 2019(A).
S&ME, Inc., Initial Abatement Action Report, Hall’s Store, Incident #42022, 9830
High House Road, Salemburg, Sampson County, North Carolina, S&ME Project No. 4305-18-159E, December 2, 2019(B).
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Field
Equipment Cleaning and Decontamination at the FEC, Striggow, B., U.S. EPA Report No. SESDPROC-206-R3, Effective Date December 18, 2015.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 15 June 2023
U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Groundwater Level and Well Depth Measurement, Striggow, B., U.S. EPA Report No. SESDPROC-105-R3,
Effective Date November 3, 2016.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure –
Groundwater Sampling, Striggow, B., U.S. EPA Report No. SESDPROC-301-R4, Effective Date April 26, 2017.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and
Ecosystem Support Division, Athens Georgia, Operating Procedure – In Situ Water Quality Monitoring, Chief, Field Services Branch, U.S. EPA Report No. SESDPROC-111-R4, Effective Date March 14, 2018.
Winner, M.D, Jr., and Coble, R.W., Hydrogeologic Framework of the North Carolina
Coastal Plain Aquifer System: U.S. Geological Survey Open File Report 87-
690, 1989, pp 155.
NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023
TABLES
Page 1 of 1
TABLE 1
SITE HISTORY — UST AND OTHER RELEASE INFORMATION
Incident Name and No.: Hall's Store - 42022
UST ID
Number
Name of
Owner/
Operator
Last
Contents
Previous
Contents
Capacity
(gal)
Construction
Details
Tank
Dimensions
(inches)
Installation
Date
(mm/dd/yy)
Date
Removed
(mm/dd/yy)
1 Gasoline Gasoline 3,000 Steel Unknown 05/09/76 12/31/93
2 Gasoline Gasoline 3,000 Steel Unknown 05/09/76 12/31/93
3 Kerosene Kerosene 500 Steel Unknown 05/09/76 12/31/93
4 Gasoline Gasoline 2,000 Steel 60 x 144 09/15/86 05/11/16
5 Gasoline Gasoline 2,000 Steel 60 x 144 09/15/86 05/11/16
6 Kerosene Kerosene 500 Steel Unknown Unknown 05/11/16
7 Unknown Unknown Unknown Unknown 4,000 Steel 63.6 x 288 Unknown 10/01/19
8 Unknown Unknown Unknown Unknown 4,000 Steel 63.6 x 288 Unknown 10/01/19
9 Unknown Unknown Unknown Unknown 500 Steel 39.6 x 91.2 Unknown 09/30/19
Incident
Number
Material
Released
Date Release
Discovered
(year)
42022 Gasoline 2016
Information obtained from S&ME (2019).
gal = gallons
Dates of
Ownership/Operation
(mm/dd/yy)
Description of the Release
TPH discovered in soils during excavation of USTs on May 11, 2016. Petroleum impacted groundwater
discovered during sampling of monitor well MW-1 installed near UST basin on June 21, 2016.
Hall's Store,
LLC
Unknown
Unknown
09/15/86 - 05/11/16
09/15/86 - 05/11/16
05/09/76 - 12/31/93
05/09/76 - 12/31/93
05/09/76 - 12/31/93
NCDEQ; 42022_Hall's Store.xlsx; T1_Site History
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 1 of 2
TABLE 2
Incident Name and No.: Hall's Store - 42022
Well #Well Owner Owner Address Site Address Phone
Number Well Use
Well
Depth
(ft. BGS)
Type of
Well Comments
WSW-1 Hall's Store,
LLC (Kyle Hall)
307 Wilton Ave.
West Jefferson, NC
28694
9710 High House
Road Salemburg, NC
28385
919-810-
9579
Active
Potable 30 Wash
Bored
Municipal Water
Account Inactive-
House Occupied
WSW-2
Charles
Jackson
Trustee
Unrevocable
Trust
10594 Old Furnace
Rd Seaford, DE
19973
9671 High House
Road Salemburg, NC
28385
Not
Provided
Active
Potable
Not
Provided
Wash
Bored
WSW-3 Spencer
Herring
9727 High House
Road Salemburg,
NC 28385
9727 High House
Road Salemburg, NC
28385
Not
Provided
Active
Potable 35 Wash
Bored
WSW-4 Steven
Fairchild
9757 High House
Road Salemburg,
NC 28385
9757 High House
Road Salemburg, NC
28385
Not
Provided
Active
Potable 35 Wash
Bored
Municipal Water
Account Inactive-
House Occupied
WSW-5 Angus
Jackson
11210 Dunn Road
Salemburg, NC
28385
11547 Dunn Road
Salemburg, NC 28385
Not
Provided
Active
Potable
Not
Provided
Wash
Bored
WSW-6 Ernest
Williams
11547 Dunn Road
Salemburg, NC
28385
11575 Dunn Road
Salemburg, NC 28385
Not
Provided
Active
Potable
Not
Provided
Wash
Bored
WSW-7 Jessie Mack
West
3777 Huntley
School Road
Roseboro, NC
28382
Mission Bautista
Hispana De Mingo
(Church)
Maxwell Rd Autryville,
NC 28318
Not
Provided
Active
Potable
Not
Provided
Wash
Bored
WSW-8 Wyman
Honeycutt
434 Derose Drive
Fayetteville, NC
28311
(Vacant House) 74
Maxwell Road
Autryville, NC 28318
Not
Provided
Inactive
Potable 25 Wash
Bored House Vacant
700 / SSE
400 / SE
460 / W
PUBLIC AND PRIVATE WATER SUPPLY WELLS WITH OTHER RECEPTOR INFORMATION
Distance (ft.)
/ Direction
from Source
620 / E
870 / ESE
640 / SE
390 / SE
770 / SSE
NCDEQ; 42022_Hall's Store.xlsx; T2_Receptor Info
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 2 of 2
TABLE 2
Incident Name and No.: Hall's Store - 42022
Well #Well Owner Owner Address Site Address Phone
Number Well Use
Well
Depth
(ft. BGS)
Type of
Well Comments
PUBLIC AND PRIVATE WATER SUPPLY WELLS WITH OTHER RECEPTOR INFORMATION
Distance (ft.)
/ Direction
from Source
WSW-8A Wyman
Honeycutt
434 Derose Drive
Fayetteville, NC
28311
(Vacant House) 74
Maxwell Road
Autryville, NC 28318
Not
Provided
Inactive
Irrigation
Not
Provided
Not
Provided House Vacant
WSW-9 W.E.
Honeycutt
57 Maxwell Road
Autryville, NC
28318
57 Maxwell Road
Autryville, NC 28318
Not
Provided
Active
Potable 25 Wash
Bored
WSW-10 Lossie Hall
Estate
307 Wilton Ave.
West Jefferson, NC
28694
(Vacant House) 9652
High House Road
Salemburg, NC 28385
Not
Provided
Active
Irrigation
Not
Provided
Not
Provided
Municipal Water
Account Active
WSW-11 Robert Gainey
11787 Dunn Road
Autryville, NC
28318
11787 Dunn Road
Autryville, NC 28318
Not
Provided
Inactive
Potable
Not
Provided
Not
Provided
Municipal Water
Account Inactive-
House Vacant
Receptor
ID Location Phone
Number
None Northeast of Source 919-810-
9579
Information obtained from S&ME (2019).
ft. BGS = feet Below Ground Surface
850 / E
660 / W
500 / SW
200 / NNE
Distance (ft.) / Direction
from Source
630 / NNW
Identified in USGS Topographic
Map as an unnamed intermittent
tributary
Hall's Store, LLC
(Kyle Hall)Drainage ditch
Description Contact Usage
NCDEQ; 42022_Hall's Store.xlsx; T2_Receptor Info
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 1 of 2
TABLE 3
WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
Incident Name and No.: Hall's Store - 42022
Well ID
Date
Installed
(mm/dd/yy)*
Date Water
Level
Measured
(mm/dd/yy)
Well
Diameter
(inches)
Well
Casing
Depth
(ft. BLS)*
Screened
Interval
(x to y ft.
BLS)*
Bottom
of Well
(ft. BLS)*
Top of
Casing
Elevation*
(ft.)
Free-Phase
Product
Thickness**
(ft.)
Depth to
Groundwater
from Top of
Casing (ft.)
Groundwater
Elevation (ft.)Comments
07/14/21 NMT 10.83 88.42
10/14/22 NMT 17.17 82.08 Pre-AFVR
10/14/22 NMT 16.96 82.29 Post-AFVR
11/21/22 NMT 17.18 82.07
02/01/23 NMT 17.26 81.99
05/11/23 NMT 15.28 83.97
07/14/21 0.88 12.58 88.39
10/14/22 NMT 15.74 84.47 Pre-AFVR
10/14/22 Post-AFVR
11/21/22
02/01/23
05/11/23 NMT 15.86 84.35
07/14/21 NMT 6.47 90.99
11/21/22
02/01/23 NMT 12.80 84.66
05/11/23 NMT 13.39 84.07
07/14/21 NMT 10.30 88.10
02/01/23 NMT 15.53 82.87
05/11/23 NMT 14.24 84.16
02/02/23 0.61 18.21 82.18
04/10/23 NMT 16.49 83.38 Pre-MMPE
04/14/23 NMT 16.01 83.86 Post-MMPE
05/11/23 NMT 15.89 83.98
2.0 97.46
Dry
12/06/18
12/06/18 Dry
Dry16.06.0-16.0
2.0 6.0 6.0-16.0 16.0
15.05.0-15.05.0
Dry
MW-4
MW-3
99.2518.08.0-18.08.02.006/21/16MW-1
100.216.02.012/06/18MW-2
98.40
99.8720.05.0-20.05.0MW-5 02/01/23 2.0
NCDEQ; 42022_Hall's Store.xlsx; T3_Well Construction & Gauging
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 2 of 2
TABLE 3
WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
Incident Name and No.: Hall's Store - 42022
Well ID
Date
Installed
(mm/dd/yy)*
Date Water
Level
Measured
(mm/dd/yy)
Well
Diameter
(inches)
Well
Casing
Depth
(ft. BLS)*
Screened
Interval
(x to y ft.
BLS)*
Bottom
of Well
(ft. BLS)*
Top of
Casing
Elevation*
(ft.)
Free-Phase
Product
Thickness**
(ft.)
Depth to
Groundwater
from Top of
Casing (ft.)
Groundwater
Elevation (ft.)Comments
02/02/23 0.66 17.92 82.14
04/10/23 NMT 16.12 83.37 Pre-MMPE
04/14/23 NMT 15.68 83.81 Post-MMPE
05/11/23 NMT 15.51 83.98
02/02/23 0.66 18.42 82.11
04/10/23 NMT 16.63 83.33 Pre-MMPE
04/14/23 NMT 15.89 84.07 Post-MMPE
05/11/23 NMT 16.00 83.96
ft. BLS = feet Below Land Surface
AFVR = Aggressive Fluid Vapor Recovery
MMPE = Mobile Multi-Phase Extraction
NMT = No Measurable Thickness
* = Data for wells installed prior to 2023 obtained from S&ME (2019).
** = if free-phase product is present in a well, ground water elevation should be calculated by : [top of casing elevation - depth to water]+ [free product thickness x specific gravity of the fuel type]
99.96
99.49
20.0
20.0
5.0-20.0
5.0-20.0
5.0
5.0
MW-7
MW-6
2.0
2.0
02/01/23
02/01/23
NCDEQ; 42022_Hall's Store.xlsx; T3_Well Construction & Gauging
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 1 of 1
TABLE 4
SUMMARY OF GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Hall's Store - 42022
Date
Collected
(mm/dd/yy)
05/11/23 100 J <3.7 ƚ <34 600 190 14 90 120 <3.4 <7.6 ƚ 63 <4.5 3,200 640 266 BMDL
05/11/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
05/11/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
05/11/23 510 J 430 480 J 230 54 J 3,000 180 40 J 160 920 470 14,000 4,900 1,200 23,000 BMDL
05/11/23 <800 <74 ƚ <670 1,200 230 3,800 450 170 J <68 ƚ 2,500 1,400 2,600 18,000 4,900 32,900 BMDL
05/11/23 910 J 230 440 J 130 <32 2,100 140 <32 ƚ 70 J 1,000 330 11,000 3,900 910 18,900 BMDL
05/11/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits)
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
Bold results indicate concentrations greater than 2L GWQS.
GCL = Gross Contaminant Level
< = Less than Method Detection Limit
ƚ = The Method Detection Limit is above the 2L GWQS.
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).All Other SM 6200B AnalytesGCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
8,800
70 Isopropylbenzene (Cumene)p-Isopropyltoluene(p-Cymene)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
Acetonesec-Butylbenzene Well/
Sample
ID
MW-5
MW-7
24,100
400
Varies
Varies
MW-1
30,500
70
11,700
25
28,500
400
80,000
600
20,000
20
6,000
6
26,100
70
260,000
600
50,000
500
MW-3
MW-4
MW-6
Trip Blank
5,000
1 2-Butanone (MEK)Ethylbenzenen-Butylbenzene5,900
70Benzene4,000,000
4,000 Total Xylenes Toluene n-PropylbenzeneNaphthalene Methyl tert-Butyl Ether (MTBE)NCDEQ; 42022_Hall's Store.xlsx; T4_GW Results (SM 6200B)
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023
Page 1 of 1
TABLE 5
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Hall's Store - 42022
Date
Collected(mm/dd/yy)
07/14/21 16 J BMDL BMDL 24 7.9 0.31 J BMDL 15 7.0 BMDL 4.8 1.5 BMDL 360 17 25.9 BMDL
11/21/22 <10 BMDL BMDL 7.2 3.2 <0.64 BMDL 0.60 J 2.4 J BMDL <1.2 <0.43 BMDL 26 1.6 J <3.4 BMDL
05/11/23 100 J <3.7 ƚ <34 600 190 <2.8 14 90 120 <3.4 <7.6 ƚ 63 <4.5 3,200 640 266 BMDL
07/14/21 4.3 J BMDL BMDL <0.14 <0.10 <0.090 BMDL <0.10 <0.090 BMDL <0.15 <0.080 BMDL <0.10 <0.10 <0.27 BMDL
05/11/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
07/14/21 3.4 J BMDL BMDL <0.14 <0.10 <0.090 BMDL <0.10 <0.090 BMDL <0.15 <0.080 BMDL <0.10 <0.10 <0.27 BMDL
05/11/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
05/11/23 510 J 430 480 J 230 54 J <28 3,000 180 40 J 160 920 470 14,000 4,900 1,200 23,000 BMDL
05/11/23 <800 <74 ƚ <670 1,200 230 <57 3,800 450 170 J <68 ƚ 2,500 1,400 2,600 18,000 4,900 32,900 BMDL
05/11/23 910 J 230 440 J 130 <32 <35 2,100 140 <32 ƚ 70 J 1,000 330 11,000 3,900 910 18,900 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than Method Detection Limit
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).
VariesVaries14,75070 80,000600 30,50070 11,70025 20,00020 6,0006 26,10070 260,000600 28,500400 24,100400 50,0005008,80070
MW-1
MW-3
MW-4
MW-5
MW-6
MW-7
GCL (µg/L)
2L GWQS (µg/L)
6,000,0006,000 5,0001 4,000,0004,000 5,90070 All Other SM 6200B Analytestert-Butylbenzene EthylbenzeneIsopropylbenzene (Cumene)p-Isopropyltoluene(p-Cymene)Methyl tert-Butyl Ether (MTBE)Naphthalene n-PropylbenzeneToluene 1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal Xylenessec-Butylbenzene Well/
Sample
ID
Contaminant of
Concern
Acetone Benzene2-Butanone (MEK)n-ButylbenzeneNCDEQ; 42022_Hall's Store.xlsx; T5_Historical GW (SM 6200B)
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

FIGURES
FIGUREPROJECTTITLE
1HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC SITE VICINITY MAP
SITE LOCATION
HIGH HOUSE RD
DUNN RDCopyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
FIGUREPROJECTTITLE
2HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC POTENTIAL RECEPTOR MAP
!(P
!(P!(W
!(P !(P
!(P!(P
!(P
!(P
!(P
!(W!(P
SITE LOCATION
HIGH HOUSE RD
DUNN RDWSW-11
WSW-8WSW-8A WSW-9WSW-7
WSW-6WSW-5
WSW-2
WSW-10WSW-1
WSW-3
WSW-4
1 ,0 0 0 F E ET RADIUS
500FE E T RADIUS
DRAINAGE DITCH
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
LEGEND
!(P Active Potable
Water Supply Well
!(P Inactive Potable
Water Supply Well
NOTE: Well locations were obtained from previous reports prepared by other consultants and are approximate.
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
!(W Active Non-PotableWater Supply Well
!(W Inactive Non-Potable
Water Supply Well
FIGUREPROJECTTITLE
3HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC SITE MAP
!>
!>
!>
!>
!>!>
!>
H I G H H O U S E R DDUNN RDMW-4
MW-3
MW-1
MW-2
FORMER 2,000-GAL.GASOLINE USTS
FORMER500-GAL.UST
FORMER 4,000-GAL.USTS
FORMER 500-GAL.KEROSENE UST
FORMER DISPENSER ISLAND
MW-5 MW-6
MW-7
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
30 0 30 6015
Feet
³
NOTE: Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.
Parcel Boundary
LEGEND
Monitoring Well
(Type II)!>
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
Approximate Location
of Former UST System
Water Line
FIGUREPROJECTTITLE
4HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC
GROUNDWATER ELEVATION –MAY 11, 2023
!>
!>
!>
!>
!>!>
!>
<
H I G H H O U S E R DDUNN RDMW-4(84.16)
MW-3(84.07)
MW-1(83.97)
MW-2(84.35)
MW-5(83.98)MW-6(83.98)
MW-7(83.96)
84.1 0
84.0084.20
84.10
8 4.0 0
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
30 0 30 6015
Feet
³
NOTES: 1. Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.2. The groundwater elevation contour interval is 0.10 feet.
Parcel Boundary
LEGEND
Gauged Monitoring Well (Type II)!>
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
Approximate Location of Former UST System
Water Line
Groundwater Flow Direction<Groundwater Elevation (Feet)(##)
Groundwater Contour
FIGUREPROJECTTITLE
5HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC
MONITORING WELLGROUNDWATER SAMPLEANALYTICAL RESULTS –MAY 11, 2023
!>
!>
!>
!>
!>!>
!>
H I G H H O U S E R DDUNN RDMW-4
MW-3
MW-1
MW-2(DRY)
MW-5
MW-6
MW-7???ESTIMATED HORIZONTALEXTENT OF 2L GWQSEXCEEDANCES
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
40 0 40 8020
Feet
³
NOTE: Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.
Parcel Boundary
LEGEND
Monitoring Well (Type II)!>
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
Approximate Location of Former UST System
Water Line
Sampled Monitoring Well (Type II)!>
Incident Name and No.: Hall's Store - 42022
DateCollected
05/11/23 <3.7 ƚ 600 190 14 90 120 <3.4 <7.6 ƚ 63 <4.5 3,200 640 26605/11/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.7305/11/23 <0.18 <0.15 <0.13 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.7305/11/23 430 230 54 J 3,000 180 40 J 160 920 470 14,000 4,900 1,200 23,00005/11/23 <74 ƚ 1,200 230 3,800 450 170 J <68 ƚ 2,500 1,400 2,600 18,000 4,900 32,90005/11/23 230 130 <32 2,100 140 <32 ƚ 70 J 1,000 330 11,000 3,900 910 18,900
All results in micrograms per liter (µg/L).Bold results are above 2L GWQS.Refer to Table 4 for all other results and notes.
SUMMARY OF GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
1,3,5-Trimethylbenzene80,000600 30,50070 11,70025 20,00020 6,0006 26,10070 260,000600 24,100400n-Butylbenzene5,90070 1,2,4-Trimethylbenzene28,500400EthylbenzeneIsopropylbenzene (Cumene)5,0001Benzene Total Xylenes 50,0005008,80070sec-Butylbenzene p-Isopropyltoluene(p-Cymene)Methyl tert-Butyl Ether (MTBE)Naphthalene n-PropylbenzeneToluene GCL (µg/L)2L GWQS (µg/L)
Contaminant of Concern
MW-1
Well/ SampleID
MW-3MW-4
MW-7
MW-5MW-6
FIGUREPROJECTTITLE
6HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC
ESTIMATED HORIZONTALEXTENT OF BENZENE –MAY 11, 2023
!>
!>
!>
!>
!>!>
!>
H I G H H O U S E R DDUNN RDMW-4(<0.18)
MW-3(<0.18)
MW-1(<3.7 ƚ)
MW-2(DRY)
MW-5(430)MW-6(<74 ƚ)
MW-7(230)???(1)
(50)(100)
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
40 0 40 8020
Feet
³
NOTES: 1. Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.2. 2L GWQS for Benzene is 1 μg/L
Parcel Boundary
LEGEND
Monitoring Well (Type II)!>
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
Approximate Location of Former UST System
Water Line
Sampled Monitoring Well (Type II)!>
Benzene Estimated Isoconcentration
Benzene Concentration (μg/L)(##)
FIGUREPROJECTTITLE
7HALL'S STORE9830 HIGH HOUSE RDSALEMBURG, NC
ESTIMATED HORIZONTALEXTENT OF NAPHTHALENE –MAY 11, 2023
!>
!>
!>
!>
!>!>
!>
H I G H H O U S E R DDUNN RDMW-4(<0.38)
MW-3(<0.38)
MW-1(<7.6 ƚ)
MW-2(DRY)
MW-5(920)MW-6(2,500)
MW-7(1,000)???(6 )(1,000)(2,000)
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
40 0 40 8020
Feet
³
NOTES: 1. Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.2. 2L GWQS for Naphthalene is 6 μg/L
Parcel Boundary
LEGEND
Monitoring Well (Type II)!>
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY42022220284JUNE 2023 AS SHOWN KMC/BJA
Approximate Location of Former UST System
Water Line
Sampled Monitoring Well (Type II)!>
Naphthalene Estimated Isoconcentration
NaphthaleneConcentration (μg/L)(##)

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDICES

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX A HISTORICAL DATA
TABLE 3
SUMMARY OF SOIL SAMPLING RESULTS
Hall's Store (Incident No.: 42022, UST #: FA-7735)
9830 High House Road, Salemburg, Sampson County, North Carolina
S&ME Project # 4305-18-159A
UST Facility ID # 0-00-000009410
Sample ID
Sample
Date
(mm/dd/yy)
Sample
Depth
(ft BGS)C9-C18 Aliphatics
SB-1/MW-2 12/6/18 8 0.39 0.15 0.64 0.045 J 0.045 J 0.17 J 0.79 0.039 J 0.11 3.1 0.88 0.24 3.9 4.9 1.9 4.4 0.21 0.76 <15 <23 <23 <23
0.52 0.0056 4.9 4.3 1.7 0.16 0.09 0.000098 1.7 4.3 8.5 8.3 4.6 0.16 0.004 3.6 0.64 1 68 540 31 #
1,960 18 1,560 626 1,564 313 350 0.31 626 1,200 782 782 3,129 313 20 63 312 700 939 1,500 469 31,000
51,100 164 40,000 16,350 40,880 8,176 3,100 2.8 16,350 32,000 20,440 20,440 81,760 8,176 100 1,635 8,176 20,000 24,528 40,000 12,264 810,000
Notes:1. All values reported in milligrams per kilograms (mg/kg)7. ft BGS = Feet Below Ground Surface
2. Analytes that are not shown were not detected 8. # considered immobile
3. MSCC = Maximum Soil Contaminant Concentration 9. NE = Regulatory standard has not been established for the listed constituent
4. Concentrations exceeding the laboratory's reporting limit are shown in Bold fields 10. J = Estimated concentration between method detection limit and method reporting limit
5. Concentrations exceeding the MSCC are shown in Shaded andBold fields
6. MADEP VPH/EPH = Massachusettes Department of Environmental Protection -Volatile Petroleum Hydrocarbons/Extractable Petroleum Hydrocarbons C9-C22 AromaticsC19-C36 Aliphatics
Soil to Groundwater MSCC
Residential MSCC 1,3,5-TrimethylbenzeneTotal XylenesNaphthalene2-methyl-naphthalene1,2-Dibromoethane (EDB)Benzene1-methyl-naphthalene1,2,4-TrimethylbenzeneMTBEIndustrial/Commercial MSCC C5-C8 Aliphatics
Analytical Method Volatile Organic Compounds EPA Method 8260 Semi-Volatile Organic Compounds
EPA Method 8270 MADEP - VPH/EPH
Contaminant
tert-Amyl Methyl Ether (TAME)Ethylbenzenen-Butylbenzene2,4-Dimethylphenol2-MethylphenolIsopropylbenzeneNaphthalenen-PropylbenzeneTolueneAPPENDIX A
HISTORICAL DATA (S&ME, 2019)
NCDEQ; 42022_Hall's Store
CATLIN Project No. 220284 CATLIN Engineers and Scientists
June 2023
TABLE 4
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Hall's Store (Incident No.: 42022, UST #: FA-7735)
9830 High House Road, Salemburg, Sampson County, North Carolina
S&ME Project # 4305-18-159A
UST Facility ID # 0-00-000009410
Well
ID
Sample Date
(mm/dd/yy)
6/21/16 46 BDL BDL BDL 71 BDL 150 BDL 67 1,800 470 560 BDL 279 892 820 7,700
12/7/18 25 6.9 20 J 1.3 J 14 5.7 15 1.2 J 1.6 J 530 78 53 NA NA NA NA NA
MW-2 12/7/18
MW-3 12/7/18 <0.5 <0.5 <5.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 NA NA NA NA NA
MW-4 12/7/18 <0.5 <0.5 <5.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.0 NA NA NA NA NA
70 70 4,000 600 70 25 6 600 70 400 400 500 0.02 15 400 700 200
6,900 8,500 4,000,000 84,500 25,000 11,700 6,000 260,000 30,000 28,500 25,000 85,500 50 15,000 NE NE NE
Notes:1. All values reported in micrograms per liter (µg/l)8. NA = Not Analyzed
2. Analyties that are not shown were not detected 9. NE = Regulatory standard has not been established for the listed constituent
3. 2L Standard = 15A NCAC 2L .0202 Groundwater Quality Standard 10. MADEP VPH/EPH = Massachusettes Department of Environmental Protection -Volatile Petroleum Hydrocarbons/
4. GCL = Gross Contamination Level Extractable Petroleum Hydrocarbons
5. Concentrations exceeding the laboratory's reporting limit are shown in Boldfields 11. J = Estimated concentration between method detection limit and method reporting limit
6. Concentrations exceeding the 2L Standards are shown in Shaded and Boldfields 12. On June 21, 2016, MW-1 was installed and sampled by a previous consultant
7. BDL= Below method detection limits
2L Standard LeadGCL C5-C8 AliphaticsC9-C12 Aliphatics
MW-1 1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesEDBDecember 7, 2018: Free Product (0.3 feet); December 18, 2018: Free Product (1.44 feet)n-PropylbenzeneC9-C10 Aromatics
Analytical Method Volatile Organic Compounds EPA Method 6200B EPA 504.1 EPA 6020 MADEP VPH
Contaminant
n-Butylbenzenesec-Butylbenzene2-Butanone (MEK)EthylbenzeneIsopropylbenzenep-IsopropyltolueneNaphthaleneTolueneAPPENDIX A
HISTORICAL DATA (S&ME, 2019)
NCDEQ; 42022_Hall's Store
CATLIN Project No. 220284
CATLIN Engineers and Scientists
June 2023

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX B SITE PHOTOGRAPHS
APPENDIX B SITE PHOTOGRAPHS – FEBRUARY 1, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

Hall’s Store Monitoring Well Drilling Facing Southeast
APPENDIX B SITE PHOTOGRAPHS – FEBRUARY 1, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

Hall’s Store Monitoring Well Drilling
Facing Southeast
APPENDIX B SITE PHOTOGRAPHS – FEBRUARY 8, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

Hall’s Store MW-5 Finished Well
Hall’s Store MW-5 Facing North
APPENDIX B SITE PHOTOGRAPHS – FEBRUARY 8, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

Hall’s Store
MW-6
Facing Northwest
Hall’s Store MW-6 Finished Well
APPENDIX B SITE PHOTOGRAPHS – FEBRUARY 8, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

Hall’s Store MW-7 Finished Well
Hall’s Store MW-7 (Foreground)
Facing Northwest
MW-5
MW-2
MW-7
APPENDIX B SITE PHOTOGRAPHS – APRIL 14, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MMPE equipment on site.

View of MMPE equipment on site.

APPENDIX B SITE PHOTOGRAPHS – APRIL 14, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of inside of MMPE trailer on site.

View of collection hoses on MMPE trailer on site.

APPENDIX B SITE PHOTOGRAPHS – APRIL 14, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-5 hook-up, facing east.

View of MW-6 hook-up, facing northwest.

APPENDIX B SITE PHOTOGRAPHS – APRIL 14, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-7 hook-up, facing northwest.

View of site facing northwest after equipment departure.
APPENDIX B SITE PHOTOGRAPHS – MAY 11, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-1, facing west.

View of MW-2, facing north-northwest.

APPENDIX B SITE PHOTOGRAPHS – MAY 11, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-3, facing east.

View of Mw-4, facing north.

APPENDIX B SITE PHOTOGRAPHS – MAY 11, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-5, facing north.

View of MW-6, facing northwest.

APPENDIX B SITE PHOTOGRAPHS – MAY 11, 2023
NCDEQ; 42022_Hall’s Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

View of MW-7, facing north-northwest. (Well in the forefront.)

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX C

JOB HAZARD ANALYES
AND FIELD DATA SHEETS
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Drill Rig N/A
tools and materials N/A
Drill Rig N/A
Drill Rig 85 dBA
Exposure Potential
Likely
Likely
Likely
Start Stop
10:00 10:15
10:15 10:30
10:30 15:00
15:00
Date and Time:
02/01/23 @ 10:30
02/01/23 @ 10:30
02/01/23 @ 10:30
Site-Specific Job Hazard Analysis
Operational Phase Task/Operation Location Where Task/Operation Performed
Monitoring Soil Borings/Well Installations Hall's Store, Salemburg, NC
ETHYL BENZENE ppm
Date(s) this JHA
Conducted:
02/01/2023
Employee Certifying this JHA
Print Name: Benjamin J. Ashba, P.G.Signature:
Weather:Cloudy, 40s
Potential Chemicals Concentration
BENZENE ppm
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
NAPHTHALENE ppm
* Gas and/or Diesel
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
Cold Weather Operations Unlikely
Heat (ambient)Likely
Slips/Trips/Falls Likely
Insect bites and stings surroundings
Drill Rig Operations Likely
Heavy Lifting/ Moving Likely
Rolling or Pinching Objects Likely
Noise Likely
Biological Hazards
Name of Biological Hazard Source
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
DAILY TASK
Vehicle #55
Mileage:Start: End:
Travel to site
On-site Health and Safety Meeting covering proper PPE, cold weather, and road safety.
Gauged MW-1 through MW-4. Set up, drilled, deconned equipment, moved to next well for MW-5,
MW-6, and MW-7. Will need additional concrete to do well pads. Will survey wells the next morning.
Clean up site and demob
PERSONNEL ONSITE
Name and Company (Print)Signature
Logan Hamilton / CATLIN Logan Hamilton
Tommy Chalmers / CATLIN
Carter Black/CATLIN
Equipment Used:PPE D/Water Level Indicator/Sampling Supplies/Generator/Pressure Washer
Page 1 of 1
CLIENT'S CATLIN
NAME:PROJECT:
CATLIN PROJECT #:PHASE:
INSTRUMENT #:
ELEVATION (TBM):DATE:2/2/2023 ROD #:UNITS (FT./M): feet
TOP
BOTTOM4.594.134.854.375.264.904.824.584.584.13
FIELD NOTES BY:DATE:2/2/2023 INSTRUMENT BY:
NOTES REDUCED BY:DATE:ROD PERSON:
100.21
POINT ANGLE
(degrees)
DISTANCE
(feet)MID (-)(+)
REDUCED LEVEL NOTES
NCDEQ - SLP Hall's Store
220284
BENCH MARK DESC.:MW-2
HI ELEV. (feet)CHECK (T+B)/2 NOTES
1 342 46 4.36 104.57 100.21 4.36 MW-2
2 343 48 4.61 99.96 4.61 MW-7
3 316 36 5.08 99.49 5.08 MW-6
4 1 24 4.70 99.87 4.70 MW-5
100.21 4.36 MW-2
6 0 104.57
5 342 45 4.36
0.00
7 0 104.57 0.00
8 0 104.57 0.00
104.57 0.00
10 0 104.57
9 0
0.00
11 0 104.57 0.00
12 0 104.57 0.00
104.57 0.00
14 0 104.57
13 0
0.00
15 0 104.57 0.00
16 0 104.57 0.00
104.57 0.00
18 0 104.57
17 0
0.00
19 0 104.57 0.00
20 0 104.57 0.00
104.57 0.00
22 0 104.57
21 0
0.00
23 0 104.57 0.00
24 0 104.57 0.00
104.57 0.00
26 0 104.57
25 0
0.00
27 0 104.57 0.00
28 0 104.57 0.00
104.57 0.00
30 0 104.57
29 0
HI - (-) = ELEV.* A sketch must be provided with the level notes.
C.Black
T.Chalmers
0.00
(+) = MID at TBM or BM (TOP - BOTTOM) * 100 = DISTANCE
TBM + (+) = HI (TOP + BOTTOM)/2 = MID (-)
C. Black 2/3/2023
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
MMPE Equipment 85 dBA
Exposure Potential
Unlikely
Unlikely
Unlikely
Start Stop
7:30 8:45
8:45 9:00
9:00 10:45
10:45 12:15
Date and Time:
4/10/23 @ 09:00
Site-Specific Job Hazard Analysis
Operational Phase Task/Operation Location Where Task/Operation Performed
Monitoring Mobile Multi-Phase Extraction (MMPE) Start-up Hall's Store, Salemburg, NC
ETHYL BENZENE ppm
Date(s) this JHA
Conducted:
4-10-2023
Employee Certifying this JHA
Print Name: Sean O'Neil, PE Signature:
Weather:Sunny, Mid-40s
Chemical Hazards
Potential Chemicals Concentration
BENZENE ppm
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
NAPHTHALENE ppm
* Gas and/or Diesel
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
Insect bites and stings surroundings
Cold Weather Operations Likely
Heat (ambient)Unlikely
Slips/Trips/Falls Likely
Noise Likely
Biological Hazards
Name of Biological Hazard Source
On-site health and safety briefing. Watch for cars in parking lot. Wear safety vest when near road. Watch for ants
and spiders when in and around wells. Wear hearing protection and be careful around MMPE equipment and hoses.
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
DAILY TASK
Truck #55 Mileage:Start: End:
Mob and travel to site.
Opened and gauged newly installed wells MW-5, MW-6, and MW-7. Spoke with Eastern Environmental Management (EEM) personnel about setup and took notes on vacuum (25" Hg) and PID readings (over 15 K -
that's as high as the instrument reads).
Travel to Raleigh office and Demob.
PERSONNEL ONSITE
Name and Company (Print)Signature
Matthew Aupperle / CATLIN
Equipment Used:PPE D/Oil-Water Interface Probe/Sampling Supplies
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
MMPE Equipment 85 dBA
Exposure Potential
Unlikely
Unlikely
Unlikely
Start Stop
7:00 8:15
8:15 8:30
8:30 11:00
11:00 12:45
Date and Time:
4/14/23 @ 08:30Sandra Miller / CATLIN
Equipment Used:PPE D/Oil-Water Interface Probe/Sampling Supplies
Spoke with Eastern Environmental Management (EEM) personnel about event and took notes on vacuum (25"
Hg) and PID readings (over 15 K for most of the time; dipped down once and came back up). Off-loaded liquids
on Tues. and Thurs. Total liquids disposed was 14,382 gallons.
Gauged, closed, and photographed MW-5, MW-6, and MW-7.
Depart site, gas for van, return to Raleigh office, and Demob.
PERSONNEL ONSITE
Name and Company (Print)Signature
DAILY TASK
Truck #44 Mileage:Start: End:
Mob and travel to site.
On-site health and safety briefing. Watch for cars in parking lot. Wear safety vest when near road. Watch for ants
and spiders when in and around wells. Wear hearing protection and be careful around MMPE equipment and
hoses.
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
Noise Likely
Biological Hazards
Name of Biological Hazard Source
Insect bites and stings surroundings
Cold Weather Operations Likely
Heat (ambient)Unlikely
Slips/Trips/Falls Likely
NAPHTHALENE ppm
* Gas and/or Diesel
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
Chemical Hazards
Potential Chemicals Concentration
BENZENE ppm
ETHYL BENZENE ppm
Date(s) this JHA
Conducted:
4-14-2023
Employee Certifying this JHA
Print Name: Sean O'Neil, PE Signature:
Weather:Overcast, Drizzle, Mid-60's
Site-Specific Job Hazard Analysis
Operational Phase Task/Operation Location Where Task/Operation Performed
Monitoring Mobile Multi-Phase Extraction (MMPE) Shut-down Hall's Store, Salemburg, NC
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Exposure Potential
Likely
Unlikely
Unlikely
Start Stop
14:30 15:15
15:15 15:30
15:30 17:15
17:15 18:30
Date and Time:
02/08/23 @ 15:30
Equipment Used: PPE D/Concrete/Shovel
Van #59 Mileage:
Weather:
Mob and travel to site
On site safety briefing. Watch for ants and spider in and around wells. Drink plenty of water to avoid
dehydration. Watch for cars turning around and pulling into parking lot.
Located new wells. Well pads completed for new wells (MW-05, MW-06, and MW-07). Photographs taken.
Biological Hazards
Name of Biological Hazard Source
Insect bites and stings
Cold Weather Operations Unlikely
Heat (ambient) Unlikely
Slips/Trips/Falls Likely
surroundings
Start: End:
DAILY TASK
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac) surroundings
Travel back to Raleigh office and demob van.
PERSONNEL ONSITE
Name and Company (Print) Signature
Nathaniel Newman / CATLIN
Chemical Hazards
60s Sunny
Site-Specific Job Hazard Analysis
Location Where Task/Operation Performed
Hall's Store, Salemburg, NC
Task/Operation
Finish Well Pads
Employee Certifying this JHA
Print Name: Sean O'Neil, P.E. Signature:
Operational Phase
Monitoring
Date(s) this JHA
Conducted:
02/08/2023
Potential Chemicals Concentration
BENZENE ppm
ETHYL BENZENE ppm
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
NAPHTHALENE ppm
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
* Gas and/or Diesel
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Exposure Potential
Likely
Unlikely
Unlikely
Start Stop
8:00 9:30
9:30 9:45
9:45 12:45
12:45 14:15
Date and Time:
5/11/23 @ 9:45
NAPHTHALENE ppm
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
* Gas and/or Diesel
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
Concentration
BENZENE ppm
ETHYL BENZENE ppm
Chemical Hazards
80s Sunny
Site-Specific Job Hazard Analysis
Location Where Task/Operation Performed
Hall's Store, Salemburg, NC
Task/Operation
Sample Monitoring Wells
Employee Certifying this JHA
Print Name: Sean O'Neil, P.E. Signature:
Operational Phase
Monitoring
Date(s) this JHA
Conducted:
5/11/2023
Potential Chemicals
Travel to lab, filled out the Chain of Custody and drop back to the Raleigh office.
PERSONNEL ONSITE
Name and Company (Print) Signature
Nathaniel Newman / CATLIN
Likely
Slips/Trips/Falls Likely
surroundings
Start: End:
DAILY TASK
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac) surroundings
Equipment Used: PPE D/Geochemistry Sensor Unit/Waterlevel Meter/Bailers
Van #59 Mileage:
Weather:
Mob and travel to site
On site safety briefing. Watch for ants and spider in and around wells. Drink plenty of water to avoid
dehydration. Watch for cars turning around and pulling into parking lot.
Sample all on site well that do not have LNAPL present. MW-2 was found to not have enough water in the well
to sample.
Biological Hazards
Name of Biological Hazard Source
Insect bites and stings
Cold Weather Operations Unlikely
Heat (ambient)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-1 2.72
15.28 0.444
NMT 1.332
18 2.220
2
Method:Bailer Purge Start Time:10:25
Required Bails for 3 Well Volumes:6 Purge Stop Time:10:30
Required Bails for 5 Well Volumes:10 Was Well Purged Dry?No
Number of Bails Removed:6 Sample Time:10:30
Groundwater Removed (gal):1.4
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
Laboratory: Analysis:
Laboratory Analysis Information
Geochemical Parameters
Depth to Water (ft below TOC)
GROUNDWATER SAMPLING FORM
Water Column (ft below TOC)
One Well Volume (gal)
Three Well Volumes (gal)
Five Well Volumes (gal)
NCDEQ-Hassan Osman
Monitoring Well Information
Nate Newman
5/11/2023
Hall's Store
220284
HCO. not enough water for
vusitu
Turbidity and Additional
Sampling Notes
Well Diameter (inches)
Well Data
Well ID
Depth to Product (ft below TOC)
Total Well Depth (ft)
Purging Information Information
Volume of Groundwater in Well
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-2 0.14
15.86 0.023
NMT 0.069
16 0.114
2
Method:Bailer Purge Start Time:
Required Bails for 3 Well Volumes:1 Purge Stop Time:
Required Bails for 5 Well Volumes:1 Was Well Purged Dry?
Number of Bails Removed: Sample Time:
Groundwater Removed (gal):0.0
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
Laboratory: Con-Test Analysis:
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
well was nearly dry. couldnt
get a vial of water
Laboratory Analysis Information
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-3 1.61
13.39 0.263
NMT 0.788
15 1.314
2
Method:Bailer Purge Start Time:10:20
Required Bails for 3 Well Volumes:4 Purge Stop Time:10:22
Required Bails for 5 Well Volumes:6 Was Well Purged Dry?YES
Number of Bails Removed:1.25 Sample Time:10:48
Groundwater Removed (gal):0.3
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
Laboratory: Analysis:
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Turbidity and Additional
Sampling Notes
not enough water for vusitu
Laboratory Analysis Information
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-4 1.76
14.24 0.287
NMT 0.862
16 1.436
2
Method:Bailer Purge Start Time:10:17
Required Bails for 3 Well Volumes:4 Purge Stop Time:10:19
Required Bails for 5 Well Volumes:6 Was Well Purged Dry?YES
Number of Bails Removed:1 Sample Time:10:43
Groundwater Removed (gal):0.2
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
Laboratory: Analysis:
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Turbidity and Additional
Sampling Notes
not enough data for vusitu
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-5 4.11
15.89 0.671
NMT 2.012
20 3.354
2
Method:Bailer Purge Start Time:11:43
Required Bails for 3 Well Volumes:9 Purge Stop Time:11:50
Required Bails for 5 Well Volumes:14 Was Well Purged Dry?No
Number of Bails Removed:9 Sample Time:11:50
Groundwater Removed (gal):2.2
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
11:44 74.28 36.02 5.57 380.71 20.50
11:45 83.22 28.59 5.48 387.34 19.81
11:46 83.77 29.06 5.51 387.09 19.68
11:47 83.67 34.57 5.51 387.91 19.66
11:48 84.31 36.74 5.46 391.98 19.74
11:49 84.45 40.26 5.48 391.30 19.78
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
light brown moderate
turbidity high HCO
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-6 4.49
15.51 0.733
NMT 2.198
20 3.664
2
Method:Bailer Purge Start Time:11:29
Required Bails for 3 Well Volumes:10 Purge Stop Time:11:35
Required Bails for 5 Well Volumes:16 Was Well Purged Dry?No
Number of Bails Removed:10 Sample Time:11:35
Groundwater Removed (gal):2.4
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
11:30 60.88 8.54 5.83 362.81 21.01
11:31 67.00 5.34 5.62 372.85 19.85
11:32 67.82 6.07 5.60 375.35 19.69
11:33 67.80 8.03 5.53 380.54 19.60
11:34 68.54 9.29 5.45 386.61 19.55
11:35 69.62 11.32 5.48 386.06 19.60
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
moderate turbidity light
brown incredibly high HCO
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-7 4.00
16 0.653
NMT 1.958
20 3.264
2
Method:Bailer Purge Start Time:11:14
Required Bails for 3 Well Volumes:9 Purge Stop Time:11:19
Required Bails for 5 Well Volumes:14 Was Well Purged Dry?No
Number of Bails Removed:9 Sample Time:11:19
Groundwater Removed (gal):2.2
Equipment Used:
Time
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
ORP
(mV)
Temperature
(Co)
11:14 83.30 7.93 5.75 268.46 21.74
11:15 86.88 5.81 5.45 303.17 20.40
11:16 87.49 5.93 5.42 315.95 20.05
11:17 87.69 5.77 5.33 329.87 20.07
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
HCO moderate turbidity
light brown
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Hall's Store Nate Newman
220284 5/11/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX D

WELL LOGS AND
WELL CONSTRUCTION RECORDS
20.0
0.0
5.0
10.0
15.0
18.0
4
12
7
9
3
4
4
3
5
3
3
10
6
7
10
4
7
5
5
8
20.0
5.0
20.0
0.0
1.0
3.0
20.02" Sch. 40 PVC2" Slot .010Sch. 40 PVCM
M
M
W
Sat.
8.0
11.0
13.0
8.0
11.0
13.0
20.0
(CL) - Brown, Silty slightly plastic CLAY.
HCO from 5-8' BLS
(ML) - Brown, Sandy SILT. Slight HCO
(CL) - Whitish brown, Silty moderately plastic CLAY.
Slight HCO
(SW) - Lt. brown to orange, F. to Cse. SAND. Moderate
HCO
BORING TERMINATED AT ELEVATION 79.9 ft in F. to
Cse. SAND
91.9
88.9
86.9
91.9
88.9
86.9
79.9
0.1
10.3
34.6
6.5
3.2
DRILL MACHINE:Diedrich D-50 METHOD:HSA
COUNTY:SAMPSON
2138319 496653
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
SHEET
18.8
18.2
DEPTH
1
99.87
20.0
20.0
0 HOUR DTW:
24 HOUR DTW:END DATE:2/1/23
OF1
BORING LOCATION: South of former kerosene UST
BLOW COUNT
0.5ft
START DATE:2/1/23
0.5ft
WELL ID:
STATE:
MW-5NORTHING:
LOGGED BY:
DRILLER:
CREW:
0.5ft0.5ft
EASTING:
PROJECT NO.:220284
SYSTEM:NCSP NAD 83 (USft)
220284PROJECT:C. Black
D. T. Chalmers, JR
L. Hamilton
LOCATION:SALEMBURG
ENVIRONMENTAL, CIVILGEOTECHNICAL
Wilmington, Raleigh, Washington,Charleston
CATLIN BORING LOG 220284_NCDEQ SLP HALL'S STORE.GPJ CATLIN.GDT 2/3/23Portland Cement Bentonite Pellets #2 Medium Sand
0.0
WELL LOG
WELL
DETAIL
SOIL AND ROCK
DESCRIPTIONLAB.DEPTH
MOIS
0.0 LAND SURFACE
LOG ELEVATION
99.9
OVA
(ppm)
220284
02/01/23
HSA
4146A
18.21
MW-5
-78.53747
D. T. Chalmers, JR
35.11376
SAMPSON
1
X
2/3/2023
8.25
Surface Pour
CATLIN Engineers and Scientists
X
2 Slot .010
9830 HIGH HOUSE RD, SALEMBURG, 28385
Bent. Pellets3
5
Concrete
N/A
3 20 Torpedo Sand
20.0
X
1
1
0
5 20 PVC
2
Sch. 40
Surface Pour
0 Sch. 40 PVC
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.NCDEQ-HALL'S STORE
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of
this record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:SEE
ATTAC
H
E
D
00-0-00009410
N/A
22.0
0.0
5.0
10.0
15.0
20.0
5
3
4
9
8
4
2
2
2
4
5
2
2
8
5
4
2
1
5
5
20.0
5.0
20.0
0.0
1.0
3.0
22.02" Sch. 40 PVC2" Slot .010Sch. 40 PVCM
M
M
W
Sat.
3.0
13.0
3.0
13.0
22.0
(SM) - Brown, Silty SAND with tr. gravel
(CL) - Brown, Slightly plastic CLAY with tr. sand
(SW) - Lt. brown, F. to Med. SAND. Slight HCO from
15.0-17.0' BLS
Tr. gravel from 20.0-22.0' BLS
BORING TERMINATED AT ELEVATION 77.5 ft in F. to
Med. SAND
96.5
86.5
96.5
86.5
77.5
0.1
0.3
1.4
20.2
0.2
DRILL MACHINE:Diedrich D-50 METHOD:HSA
COUNTY:SAMPSON
2138324 496675
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
SHEET
18.1
17.9
DEPTH
1
99.49
22.0
20.0
0 HOUR DTW:
24 HOUR DTW:END DATE:2/1/23
OF1
BORING LOCATION:West of former 2,000-Gal. Gasoline UST
BLOW COUNT
0.5ft
START DATE:2/1/23
0.5ft
WELL ID:
STATE:
MW-6NORTHING:
LOGGED BY:
DRILLER:
CREW:
0.5ft0.5ft
EASTING:
PROJECT NO.:220284
SYSTEM:NCSP NAD 83 (USft)
220284PROJECT:C. Black
D. T. Chalmers, JR
L. Hamilton
LOCATION:SALEMBURG
ENVIRONMENTAL, CIVILGEOTECHNICAL
Wilmington, Raleigh, Washington,Charleston
CATLIN BORING LOG 220284_NCDEQ SLP HALL'S STORE.GPJ CATLIN.GDT 2/3/23Portland Cement Bentonite Pellets #2 Medium Sand
0.0
WELL LOG
WELL
DETAIL
SOIL AND ROCK
DESCRIPTIONLAB.DEPTH
MOIS
0.0 LAND SURFACE
LOG ELEVATION
99.5
OVA
(ppm)
220284
02/01/23
HSA
4146A
17.92
MW-6
-78.53745
D. T. Chalmers, JR
35.11382
SAMPSON
1
X
2/3/2023
8.25
Surface Pour
CATLIN Engineers and Scientists
X
2 Slot .010
9830 HIGH HOUSE RD, SALEMBURG, 28385
Bent. Pellets3
5
Concrete
N/A
3 22 Torpedo Sand
20.0
X
1
1
0
5 20 PVC
2
Sch. 40
Surface Pour
0 Sch. 40 PVC
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.NCDEQ-HALL'S STORE
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of
this record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:SEE
ATTAC
H
E
D
00-0-00009410
N/A
20.0
0.0
5.0
10.0
15.0
18.0
6
4
8
6
3
5
5
2
3
4
6
11
5
4
5
6
7
5
4
5
20.0
5.0
20.0
0.0
1.0
4.0
20.02" Sch. 40 PVC2" Slot .010Sch. 40 PVCM
M
M
W
Sat.
3.0
13.0
3.0
13.0
20.0
(SP) - Gray to dark gray, F. SAND
(CH) - Brown to white, Silty highly plastic CLAY. Slight
HCO from 10.0-13.0' BLS
(SW) - Orangish brown, F. to Cse. SAND with tr. silt
from 18.0-20.0' BLS.
BORING TERMINATED AT ELEVATION 80.0 ft in Med.
to Cse. SAND w/ tr. silt
97.0
87.0
97.0
87.0
80.0
NM
NM
NM
NM
NM
DRILL MACHINE:Diedrich D-50 METHOD:HSA
COUNTY:SAMPSON
2138301 496674
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
SHEET
18.6
13.4
DEPTH
1
99.96
20.0
20.0
0 HOUR DTW:
24 HOUR DTW:END DATE:2/1/23
OF1
BORING LOCATION:South of MW-2
BLOW COUNT
0.5ft
START DATE:2/1/23
0.5ft
WELL ID:
STATE:
MW-7NORTHING:
LOGGED BY:
DRILLER:
CREW:
0.5ft0.5ft
EASTING:
PROJECT NO.:220284
SYSTEM:NCSP NAD 83 (USft)
220284PROJECT:C. Black
D. T. Chalmers, JR
L. Hamilton
LOCATION:SALEMBURG
ENVIRONMENTAL, CIVILGEOTECHNICAL
Wilmington, Raleigh, Washington,Charleston
CATLIN BORING LOG 220284_NCDEQ SLP HALL'S STORE.GPJ CATLIN.GDT 2/3/23Portland Cement Bentonite Pellets #2 Medium Sand
0.0
WELL LOG
WELL
DETAIL
SOIL AND ROCK
DESCRIPTIONLAB.DEPTH
MOIS
0.0 LAND SURFACE
LOG ELEVATION
100.0
OVA
(ppm)
220284
02/01/23
HSA
4146A
13.42
MW-7
-78.53753
D. T. Chalmers, JR
35.11382
SAMPSON
1
X
2/3/2023
8.25
Surface Pour
CATLIN Engineers and Scientists
X
2 Slot .010
9830 HIGH HOUSE RD, SALEMBURG, 28385
Bent. Pellets4
5
Concrete
N/A
4 20 Torpedo Sand
20.0
X
1
1
0
5 20 PVC
2
Sch. 40
Surface Pour
0 Sch. 40 PVC
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.NCDEQ-HALL'S STORE
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of
this record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:SEE
ATTAC
H
E
D
00-0-00009410
N/A

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX E

MMPE REPORT AND
DISPOSAL DOCUMENTS

NCDEQ; 42022_Hall's Store CATLIN Engineers and Scientists
CATLIN Project No. 220284 June 2023

APPENDIX F

LABORATORY ANALYTICAL REPORT
AND CHAIN OF CUSTODY DOCUMENT

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
May 22, 2023
Ben Ashba
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
Project Location: Salemburg, NC
Client Job Number:
Project Number: 220284.3
Laboratory Work Order Number: 23E1757
Enclosed are results of analyses for samples as received by the laboratory on May 12, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
23E1757-01 8
23E1757-02 10
23E1757-03 12
23E1757-04 14
23E1757-05 16
23E1757-06 18
23E1757-07 20
Sample Preparation Information 22
QC Data 23
Volatile Organic Compounds by GC/MS 23
B340343 23
B340602 27
Flag/Qualifier Summary 31
Certifications 32
Chain of Custody/Sample Receipt 34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
5/22/2023
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
ATTN: Ben Ashba
220284.3
23E1757
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Salemburg, NC
230511-1
Trip Blank 23E1757-01 Trip Blank Water SM21-23 6200B
MW-1 23E1757-02 Ground Water SM21-23 6200B
MW-3 23E1757-03 Ground Water SM21-23 6200B
MW-4 23E1757-04 Ground Water SM21-23 6200B
MW-5 23E1757-05 Ground Water SM21-23 6200B
MW-6 23E1757-06 Ground Water SM21-23 6200B
MW-7 23E1757-07 Ground Water SM21-23 6200B
[TOC_1]Sample Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:23E1757-01Trip Blank
No Results Detected
Client ID:Lab ID:23E1757-03MW-3
No Results Detected
Client ID:Lab ID:23E1757-04MW-4
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E1757-02MW-1
DL
1,2,4-Trimethylbenzene 3200 10 g/L SM21-23 6200B4.0
1,3,5-Trimethylbenzene 640 10 g/L SM21-23 6200B3.0
Acetone 100 1000 g/L SM21-23 6200BJ40
Ethylbenzene 14 10 g/L SM21-23 6200B4.4
Isopropylbenzene (Cumene)90 10 g/L SM21-23 6200B3.0
m+p Xylene 180 20 g/L SM21-23 6200B9.8
n-Butylbenzene 600 10 g/L SM21-23 6200B3.0
n-Propylbenzene 63 10 g/L SM21-23 6200B2.5
o-Xylene 86 10 g/L SM21-23 6200B4.9
p-Isopropyltoluene (p-Cymene)120 10 g/L SM21-23 6200B2.5
sec-Butylbenzene 190 10 g/L SM21-23 6200B2.5
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E1757-05MW-5
DL
1,2,4-Trimethylbenzene 4900 100 g/L SM21-23 6200B40
1,3,5-Trimethylbenzene 1200 100 g/L SM21-23 6200B30
2-Butanone (MEK)480 1000 g/L SM21-23 6200BJ340
Acetone 510 10000 g/L SM21-23 6200BJ400
Benzene 430 100 g/L SM21-23 6200B37
Ethylbenzene 3000 100 g/L SM21-23 6200B44
Isopropylbenzene (Cumene)180 100 g/L SM21-23 6200B30
m+p Xylene 16000 200 g/L SM21-23 6200B98
Methyl tert-Butyl Ether (MTBE)160 100 g/L SM21-23 6200B34
Naphthalene 920 100 g/L SM21-23 6200B76
n-Butylbenzene 230 100 g/L SM21-23 6200B30
n-Propylbenzene 470 100 g/L SM21-23 6200B25
o-Xylene 7000 100 g/L SM21-23 6200B49
p-Isopropyltoluene (p-Cymene)40 100 g/L SM21-23 6200BJ25
sec-Butylbenzene 54 100 g/L SM21-23 6200BJ25
Toluene 14000 100 g/L SM21-23 6200B45
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E1757-06MW-6
DL
1,2,4-Trimethylbenzene 18000 200 g/L SM21-23 6200B80
1,3,5-Trimethylbenzene 4900 200 g/L SM21-23 6200B60
Ethylbenzene 3800 200 g/L SM21-23 6200B88
Isopropylbenzene (Cumene)450 200 g/L SM21-23 6200B60
m+p Xylene 23000 400 g/L SM21-23 6200B200
Naphthalene 2500 200 g/L SM21-23 6200B150
n-Butylbenzene 1200 200 g/L SM21-23 6200B60
n-Propylbenzene 1400 200 g/L SM21-23 6200B50
o-Xylene 9900 200 g/L SM21-23 6200B97
p-Isopropyltoluene (p-Cymene)170 200 g/L SM21-23 6200BJ51
sec-Butylbenzene 230 200 g/L SM21-23 6200B51
Toluene 2600 200 g/L SM21-23 6200B89
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E1757-07MW-7
DL
1,2,4-Trimethylbenzene 3900 120 g/L SM21-23 6200B50
1,3,5-Trimethylbenzene 910 120 g/L SM21-23 6200B37
2-Butanone (MEK)440 1200 g/L SM21-23 6200BJ420
Acetone 910 12000 g/L SM21-23 6200BJ500
Benzene 230 120 g/L SM21-23 6200B46
Ethylbenzene 2100 120 g/L SM21-23 6200B55
Isopropylbenzene (Cumene)140 120 g/L SM21-23 6200B38
m+p Xylene 13000 250 g/L SM21-23 6200B120
Methyl tert-Butyl Ether (MTBE)70 120 g/L SM21-23 6200BJ43
Naphthalene 1000 120 g/L SM21-23 6200B95
n-Butylbenzene 130 120 g/L SM21-23 6200B37
n-Propylbenzene 330 120 g/L SM21-23 6200B31
o-Xylene 5900 120 g/L SM21-23 6200B61
Toluene 11000 120 g/L SM21-23 6200B56
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 23E1757-02,05,06+07 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-23 6200B
Qualifications:
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
23E1757-02[MW-1], 23E1757-05[MW-5], 23E1757-06[MW-6], 23E1757-07[MW-7]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-01
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 5/11/2023 00:00
[TOC_2]23E1757-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/18/23 0:55 EEHg/L2.0 5/15/23SM21-23 6200B1Acetone
ND 0.50 5/18/23 0:55 EEHg/L0.18 5/15/23SM21-23 6200B1Benzene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B1Bromobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.28 5/15/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/18/23 0:55 EEHg/L0.16 5/15/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/18/23 0:55 EEHg/L0.41 5/15/23SM21-23 6200B1Bromoform
ND 2.0 5/18/23 0:55 EEHg/L1.3 5/15/23SM21-23 6200B1Bromomethane
ND 5.0 5/18/23 0:55 EEHg/L1.7 5/15/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/18/23 0:55 EEHg/L0.13 5/15/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/18/23 0:55 EEHg/L0.16 5/15/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/18/23 0:55 EEHg/L0.12 5/15/23SM21-23 6200B1Chlorobenzene
ND 50 5/18/23 0:55 EEHg/L20 5/15/23SM21-23 6200B1Ethanol
ND 0.50 5/18/23 0:55 EEHg/L0.20 5/15/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/18/23 0:55 EEHg/L0.34 5/15/23SM21-23 6200B1Chloroethane
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B1Chloroform
ND 0.60 5/18/23 0:55 EEHg/L0.50 5/15/23SM21-23 6200B1Chloromethane
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/18/23 0:55 EEHg/L0.16 5/15/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/18/23 0:55 EEHg/L0.13 5/15/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.13 5/15/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.16 5/15/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/18/23 0:55 EEHg/L0.30 5/15/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/18/23 0:55 EEHg/L0.17 5/15/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/18/23 0:55 EEHg/L0.19 5/15/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/18/23 0:55 EEHg/L0.12 5/15/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/18/23 0:55 EEHg/L0.35 5/15/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/18/23 0:55 EEHg/L0.16 5/15/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/18/23 0:55 EEHg/L0.20 5/15/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/18/23 0:55 EEHg/L0.22 5/15/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/18/23 0:55 EEHg/L1.2 5/15/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/18/23 0:55 EEHg/L0.13 5/15/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/18/23 0:55 EEHg/L0.17 5/15/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/18/23 0:55 EEHg/L0.18 5/15/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/18/23 0:55 EEHg/L1.3 5/15/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-01
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 5/11/2023 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/18/23 0:55 EEHg/L0.38 5/15/23SM21-23 6200B1Naphthalene
ND 0.50 5/18/23 0:55 EEHg/L0.12 5/15/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B1Styrene
ND 0.50 5/18/23 0:55 EEHg/L0.14 5/15/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/18/23 0:55 EEHg/L0.17 5/15/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/18/23 0:55 EEHg/L0.22 5/15/23SM21-23 6200B1Toluene
ND 1.0 5/18/23 0:55 EEHg/L0.34 5/15/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.30 5/15/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/18/23 0:55 EEHg/L0.19 5/15/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/18/23 0:55 EEHg/L0.17 5/15/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/18/23 0:55 EEHg/L0.28 5/15/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/18/23 0:55 EEHg/L0.20 5/15/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/18/23 0:55 EEHg/L0.15 5/15/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/18/23 0:55 EEHg/L1.7 5/15/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/18/23 0:55 EEHg/L0.24 5/15/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/18/23 0:55 EEHg/L0.49 5/15/23SM21-23 6200B1m+p Xylene
ND 0.50 5/18/23 0:55 EEHg/L0.24 5/15/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 5/18/23 0:5570-130
Toluene-d8 99.8 5/18/23 0:5570-130
4-Bromofluorobenzene 97.4 5/18/23 0:5570-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:30
[TOC_2]23E1757-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
100 1000 5/18/23 4:19 EEHg/L40 5/15/23SM21-23 6200B20JAcetone
ND 10 5/18/23 4:19 EEHg/L3.7 5/15/23SM21-23 6200B20Benzene
ND 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B20Bromobenzene
ND 10 5/18/23 4:19 EEHg/L5.7 5/15/23SM21-23 6200B20Bromochloromethane
ND 10 5/18/23 4:19 EEHg/L3.2 5/15/23SM21-23 6200B20Bromodichloromethane
ND 10 5/18/23 4:19 EEHg/L8.2 5/15/23SM21-23 6200B20Bromoform
ND 40 5/18/23 4:19 EEHg/L26 5/15/23SM21-23 6200B20Bromomethane
ND 100 5/18/23 4:19 EEHg/L34 5/15/23SM21-23 6200B202-Butanone (MEK)
600 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B20n-Butylbenzene
190 10 5/18/23 4:19 EEHg/L2.5 5/15/23SM21-23 6200B20sec-Butylbenzene
ND 10 5/18/23 4:19 EEHg/L2.8 5/15/23SM21-23 6200B20tert-Butylbenzene
ND 10 5/18/23 4:19 EEHg/L3.3 5/15/23SM21-23 6200B20Carbon Tetrachloride
ND 10 5/18/23 4:19 EEHg/L2.4 5/15/23SM21-23 6200B20Chlorobenzene
ND 1000 5/18/23 4:19 EEHg/L410 5/15/23SM21-23 6200B20Ethanol
ND 10 5/18/23 4:19 EEHg/L4.0 5/15/23SM21-23 6200B20Chlorodibromomethane
ND 10 5/18/23 4:19 EEHg/L6.8 5/15/23SM21-23 6200B20Chloroethane
ND 10 5/18/23 4:19 EEHg/L2.8 5/15/23SM21-23 6200B20Chloroform
ND 12 5/18/23 4:19 EEHg/L10 5/15/23SM21-23 6200B20Chloromethane
ND 10 5/18/23 4:19 EEHg/L3.1 5/15/23SM21-23 6200B202-Chlorotoluene
ND 10 5/18/23 4:19 EEHg/L3.1 5/15/23SM21-23 6200B204-Chlorotoluene
ND 10 5/18/23 4:19 EEHg/L3.2 5/15/23SM21-23 6200B201,2-Dibromoethane (EDB)
ND 10 5/18/23 4:19 EEHg/L2.6 5/15/23SM21-23 6200B201,2-Dichlorobenzene
ND 10 5/18/23 4:19 EEHg/L2.7 5/15/23SM21-23 6200B201,3-Dichlorobenzene
ND 10 5/18/23 4:19 EEHg/L2.6 5/15/23SM21-23 6200B201,4-Dichlorobenzene
ND 10 5/18/23 4:19 EEHg/L3.2 5/15/23SM21-23 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 5/18/23 4:19 EEHg/L2.7 5/15/23SM21-23 6200B201,1-Dichloroethane
ND 20 5/18/23 4:19 EEHg/L6.1 5/15/23SM21-23 6200B201,2-Dichloroethane
ND 10 5/18/23 4:19 EEHg/L2.8 5/15/23SM21-23 6200B201,1-Dichloroethylene
ND 10 5/18/23 4:19 EEHg/L2.8 5/15/23SM21-23 6200B20cis-1,2-Dichloroethylene
ND 10 5/18/23 4:19 EEHg/L3.4 5/15/23SM21-23 6200B20trans-1,2-Dichloroethylene
ND 10 5/18/23 4:19 EEHg/L3.9 5/15/23SM21-23 6200B201,2-Dichloropropane
ND 10 5/18/23 4:19 EEHg/L2.3 5/15/23SM21-23 6200B201,3-Dichloropropane
ND 10 5/18/23 4:19 EEHg/L7.0 5/15/23SM21-23 6200B202,2-Dichloropropane
ND 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B201,1-Dichloropropene
ND 10 5/18/23 4:19 EEHg/L3.3 5/15/23SM21-23 6200B20cis-1,3-Dichloropropene
ND 10 5/18/23 4:19 EEHg/L2.8 5/15/23SM21-23 6200B20trans-1,3-Dichloropropene
ND 10 5/18/23 4:19 EEHg/L4.0 5/15/23SM21-23 6200B20Diisopropyl Ether (DIPE)
14 10 5/18/23 4:19 EEHg/L4.4 5/15/23SM21-23 6200B20Ethylbenzene
ND 100 5/18/23 4:19 EEHg/L24 5/15/23SM21-23 6200B202-Hexanone (MBK)
90 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B20Isopropylbenzene (Cumene)
120 10 5/18/23 4:19 EEHg/L2.5 5/15/23SM21-23 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 5/18/23 4:19 EEHg/L3.4 5/15/23SM21-23 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 5/18/23 4:19 EEHg/L3.5 5/15/23SM21-23 6200B20Methylene Chloride
ND 100 5/18/23 4:19 EEHg/L26 5/15/23SM21-23 6200B204-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-02
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 10 5/18/23 4:19 EEHg/L7.6 5/15/23SM21-23 6200B20Naphthalene
63 10 5/18/23 4:19 EEHg/L2.5 5/15/23SM21-23 6200B20n-Propylbenzene
ND 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B20Styrene
ND 10 5/18/23 4:19 EEHg/L2.7 5/15/23SM21-23 6200B201,1,2,2-Tetrachloroethane
ND 10 5/18/23 4:19 EEHg/L3.4 5/15/23SM21-23 6200B20Tetrachloroethylene
ND 10 5/18/23 4:19 EEHg/L4.5 5/15/23SM21-23 6200B20Toluene
ND 20 5/18/23 4:19 EEHg/L6.8 5/15/23SM21-23 6200B201,2,3-Trichlorobenzene
ND 10 5/18/23 4:19 EEHg/L6.0 5/15/23SM21-23 6200B201,2,4-Trichlorobenzene
ND 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B201,1,1-Trichloroethane
ND 10 5/18/23 4:19 EEHg/L3.8 5/15/23SM21-23 6200B201,1,2-Trichloroethane
ND 10 5/18/23 4:19 EEHg/L3.5 5/15/23SM21-23 6200B20Trichloroethylene
ND 10 5/18/23 4:19 EEHg/L3.1 5/15/23SM21-23 6200B20Trichlorofluoromethane (Freon 11)
ND 10 5/18/23 4:19 EEHg/L5.5 5/15/23SM21-23 6200B201,2,3-Trichloropropane
3200 10 5/18/23 4:19 EEHg/L4.0 5/15/23SM21-23 6200B201,2,4-Trimethylbenzene
640 10 5/18/23 4:19 EEHg/L3.0 5/15/23SM21-23 6200B201,3,5-Trimethylbenzene
ND 400 5/18/23 4:19 EEHg/L33 5/15/23SM21-23 6200B20Vinyl Acetate
ND 10 5/18/23 4:19 EEHg/L4.7 5/15/23SM21-23 6200B20Vinyl Chloride
180 20 5/18/23 4:19 EEHg/L9.8 5/15/23SM21-23 6200B20m+p Xylene
86 10 5/18/23 4:19 EEHg/L4.9 5/15/23SM21-23 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 5/18/23 4:1970-130
Toluene-d8 101 5/18/23 4:1970-130
4-Bromofluorobenzene 108 5/18/23 4:1970-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:48
[TOC_2]23E1757-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/18/23 1:22 EEHg/L2.0 5/15/23SM21-23 6200B1Acetone
ND 0.50 5/18/23 1:22 EEHg/L0.18 5/15/23SM21-23 6200B1Benzene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B1Bromobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.28 5/15/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/18/23 1:22 EEHg/L0.16 5/15/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/18/23 1:22 EEHg/L0.41 5/15/23SM21-23 6200B1Bromoform
ND 2.0 5/18/23 1:22 EEHg/L1.3 5/15/23SM21-23 6200B1Bromomethane
ND 5.0 5/18/23 1:22 EEHg/L1.7 5/15/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/18/23 1:22 EEHg/L0.13 5/15/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/18/23 1:22 EEHg/L0.16 5/15/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/18/23 1:22 EEHg/L0.12 5/15/23SM21-23 6200B1Chlorobenzene
ND 50 5/18/23 1:22 EEHg/L20 5/15/23SM21-23 6200B1Ethanol
ND 0.50 5/18/23 1:22 EEHg/L0.20 5/15/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/18/23 1:22 EEHg/L0.34 5/15/23SM21-23 6200B1Chloroethane
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B1Chloroform
ND 0.60 5/18/23 1:22 EEHg/L0.50 5/15/23SM21-23 6200B1Chloromethane
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/18/23 1:22 EEHg/L0.16 5/15/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/18/23 1:22 EEHg/L0.13 5/15/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.13 5/15/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.16 5/15/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/18/23 1:22 EEHg/L0.30 5/15/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/18/23 1:22 EEHg/L0.17 5/15/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/18/23 1:22 EEHg/L0.19 5/15/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/18/23 1:22 EEHg/L0.12 5/15/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/18/23 1:22 EEHg/L0.35 5/15/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/18/23 1:22 EEHg/L0.16 5/15/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/18/23 1:22 EEHg/L0.20 5/15/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/18/23 1:22 EEHg/L0.22 5/15/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/18/23 1:22 EEHg/L1.2 5/15/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/18/23 1:22 EEHg/L0.13 5/15/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/18/23 1:22 EEHg/L0.17 5/15/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/18/23 1:22 EEHg/L0.18 5/15/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/18/23 1:22 EEHg/L1.3 5/15/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:48
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/18/23 1:22 EEHg/L0.38 5/15/23SM21-23 6200B1Naphthalene
ND 0.50 5/18/23 1:22 EEHg/L0.12 5/15/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B1Styrene
ND 0.50 5/18/23 1:22 EEHg/L0.14 5/15/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/18/23 1:22 EEHg/L0.17 5/15/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/18/23 1:22 EEHg/L0.22 5/15/23SM21-23 6200B1Toluene
ND 1.0 5/18/23 1:22 EEHg/L0.34 5/15/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.30 5/15/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/18/23 1:22 EEHg/L0.19 5/15/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/18/23 1:22 EEHg/L0.17 5/15/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/18/23 1:22 EEHg/L0.28 5/15/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/18/23 1:22 EEHg/L0.20 5/15/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/18/23 1:22 EEHg/L0.15 5/15/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/18/23 1:22 EEHg/L1.7 5/15/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/18/23 1:22 EEHg/L0.24 5/15/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/18/23 1:22 EEHg/L0.49 5/15/23SM21-23 6200B1m+p Xylene
ND 0.50 5/18/23 1:22 EEHg/L0.24 5/15/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 5/18/23 1:2270-130
Toluene-d8 102 5/18/23 1:2270-130
4-Bromofluorobenzene 97.8 5/18/23 1:2270-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:43
[TOC_2]23E1757-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/18/23 1:50 EEHg/L2.0 5/15/23SM21-23 6200B1Acetone
ND 0.50 5/18/23 1:50 EEHg/L0.18 5/15/23SM21-23 6200B1Benzene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B1Bromobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.28 5/15/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/18/23 1:50 EEHg/L0.16 5/15/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/18/23 1:50 EEHg/L0.41 5/15/23SM21-23 6200B1Bromoform
ND 2.0 5/18/23 1:50 EEHg/L1.3 5/15/23SM21-23 6200B1Bromomethane
ND 5.0 5/18/23 1:50 EEHg/L1.7 5/15/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/18/23 1:50 EEHg/L0.13 5/15/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/18/23 1:50 EEHg/L0.16 5/15/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/18/23 1:50 EEHg/L0.12 5/15/23SM21-23 6200B1Chlorobenzene
ND 50 5/18/23 1:50 EEHg/L20 5/15/23SM21-23 6200B1Ethanol
ND 0.50 5/18/23 1:50 EEHg/L0.20 5/15/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/18/23 1:50 EEHg/L0.34 5/15/23SM21-23 6200B1Chloroethane
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B1Chloroform
ND 0.60 5/18/23 1:50 EEHg/L0.50 5/15/23SM21-23 6200B1Chloromethane
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/18/23 1:50 EEHg/L0.16 5/15/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/18/23 1:50 EEHg/L0.13 5/15/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.13 5/15/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.16 5/15/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/18/23 1:50 EEHg/L0.30 5/15/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/18/23 1:50 EEHg/L0.17 5/15/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/18/23 1:50 EEHg/L0.19 5/15/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/18/23 1:50 EEHg/L0.12 5/15/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/18/23 1:50 EEHg/L0.35 5/15/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/18/23 1:50 EEHg/L0.16 5/15/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/18/23 1:50 EEHg/L0.20 5/15/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/18/23 1:50 EEHg/L0.22 5/15/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/18/23 1:50 EEHg/L1.2 5/15/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/18/23 1:50 EEHg/L0.13 5/15/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/18/23 1:50 EEHg/L0.17 5/15/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/18/23 1:50 EEHg/L0.18 5/15/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/18/23 1:50 EEHg/L1.3 5/15/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 5/11/2023 10:43
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/18/23 1:50 EEHg/L0.38 5/15/23SM21-23 6200B1Naphthalene
ND 0.50 5/18/23 1:50 EEHg/L0.12 5/15/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B1Styrene
ND 0.50 5/18/23 1:50 EEHg/L0.14 5/15/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/18/23 1:50 EEHg/L0.17 5/15/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/18/23 1:50 EEHg/L0.22 5/15/23SM21-23 6200B1Toluene
ND 1.0 5/18/23 1:50 EEHg/L0.34 5/15/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.30 5/15/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/18/23 1:50 EEHg/L0.19 5/15/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/18/23 1:50 EEHg/L0.17 5/15/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/18/23 1:50 EEHg/L0.28 5/15/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/18/23 1:50 EEHg/L0.20 5/15/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/18/23 1:50 EEHg/L0.15 5/15/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/18/23 1:50 EEHg/L1.7 5/15/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/18/23 1:50 EEHg/L0.24 5/15/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/18/23 1:50 EEHg/L0.49 5/15/23SM21-23 6200B1m+p Xylene
ND 0.50 5/18/23 1:50 EEHg/L0.24 5/15/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 5/18/23 1:5070-130
Toluene-d8 101 5/18/23 1:5070-130
4-Bromofluorobenzene 97.4 5/18/23 1:5070-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-05
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:50
[TOC_2]23E1757-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
510 10000 5/19/23 5:10 MFFg/L400 5/18/23SM21-23 6200B200JAcetone
430 100 5/19/23 5:10 MFFg/L37 5/18/23SM21-23 6200B200Benzene
ND 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B200Bromobenzene
ND 100 5/19/23 5:10 MFFg/L57 5/18/23SM21-23 6200B200Bromochloromethane
ND 100 5/19/23 5:10 MFFg/L32 5/18/23SM21-23 6200B200Bromodichloromethane
ND 100 5/19/23 5:10 MFFg/L82 5/18/23SM21-23 6200B200Bromoform
ND 400 5/19/23 5:10 MFFg/L260 5/18/23SM21-23 6200B200Bromomethane
480 1000 5/19/23 5:10 MFFg/L340 5/18/23SM21-23 6200B200J2-Butanone (MEK)
230 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B200n-Butylbenzene
54 100 5/19/23 5:10 MFFg/L25 5/18/23SM21-23 6200B200Jsec-Butylbenzene
ND 100 5/19/23 5:10 MFFg/L28 5/18/23SM21-23 6200B200tert-Butylbenzene
ND 100 5/19/23 5:10 MFFg/L33 5/18/23SM21-23 6200B200Carbon Tetrachloride
ND 100 5/19/23 5:10 MFFg/L24 5/18/23SM21-23 6200B200Chlorobenzene
ND 10000 5/19/23 5:10 MFFg/L4100 5/18/23SM21-23 6200B200Ethanol
ND 100 5/19/23 5:10 MFFg/L40 5/18/23SM21-23 6200B200Chlorodibromomethane
ND 100 5/19/23 5:10 MFFg/L68 5/18/23SM21-23 6200B200Chloroethane
ND 100 5/19/23 5:10 MFFg/L28 5/18/23SM21-23 6200B200Chloroform
ND 120 5/19/23 5:10 MFFg/L100 5/18/23SM21-23 6200B200Chloromethane
ND 100 5/19/23 5:10 MFFg/L31 5/18/23SM21-23 6200B2002-Chlorotoluene
ND 100 5/19/23 5:10 MFFg/L31 5/18/23SM21-23 6200B2004-Chlorotoluene
ND 100 5/19/23 5:10 MFFg/L32 5/18/23SM21-23 6200B2001,2-Dibromoethane (EDB)
ND 100 5/19/23 5:10 MFFg/L26 5/18/23SM21-23 6200B2001,2-Dichlorobenzene
ND 100 5/19/23 5:10 MFFg/L27 5/18/23SM21-23 6200B2001,3-Dichlorobenzene
ND 100 5/19/23 5:10 MFFg/L26 5/18/23SM21-23 6200B2001,4-Dichlorobenzene
ND 100 5/19/23 5:10 MFFg/L32 5/18/23SM21-23 6200B200Dichlorodifluoromethane (Freon 12)
ND 100 5/19/23 5:10 MFFg/L27 5/18/23SM21-23 6200B2001,1-Dichloroethane
ND 100 5/19/23 5:10 MFFg/L61 5/18/23SM21-23 6200B2001,2-Dichloroethane
ND 100 5/19/23 5:10 MFFg/L28 5/18/23SM21-23 6200B2001,1-Dichloroethylene
ND 100 5/19/23 5:10 MFFg/L28 5/18/23SM21-23 6200B200cis-1,2-Dichloroethylene
ND 100 5/19/23 5:10 MFFg/L34 5/18/23SM21-23 6200B200trans-1,2-Dichloroethylene
ND 100 5/19/23 5:10 MFFg/L39 5/18/23SM21-23 6200B2001,2-Dichloropropane
ND 100 5/19/23 5:10 MFFg/L23 5/18/23SM21-23 6200B2001,3-Dichloropropane
ND 100 5/19/23 5:10 MFFg/L70 5/18/23SM21-23 6200B2002,2-Dichloropropane
ND 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B2001,1-Dichloropropene
ND 100 5/19/23 5:10 MFFg/L33 5/18/23SM21-23 6200B200cis-1,3-Dichloropropene
ND 100 5/19/23 5:10 MFFg/L28 5/18/23SM21-23 6200B200trans-1,3-Dichloropropene
ND 100 5/19/23 5:10 MFFg/L40 5/18/23SM21-23 6200B200Diisopropyl Ether (DIPE)
3000 100 5/19/23 5:10 MFFg/L44 5/18/23SM21-23 6200B200Ethylbenzene
ND 1000 5/19/23 5:10 MFFg/L240 5/18/23SM21-23 6200B2002-Hexanone (MBK)
180 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B200Isopropylbenzene (Cumene)
40 100 5/19/23 5:10 MFFg/L25 5/18/23SM21-23 6200B200Jp-Isopropyltoluene (p-Cymene)
160 100 5/19/23 5:10 MFFg/L34 5/18/23SM21-23 6200B200Methyl tert-Butyl Ether (MTBE)
ND 1000 5/19/23 5:10 MFFg/L35 5/18/23SM21-23 6200B200Methylene Chloride
ND 1000 5/19/23 5:10 MFFg/L260 5/18/23SM21-23 6200B2004-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-05
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
920 100 5/19/23 5:10 MFFg/L76 5/18/23SM21-23 6200B200Naphthalene
470 100 5/19/23 5:10 MFFg/L25 5/18/23SM21-23 6200B200n-Propylbenzene
ND 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B200Styrene
ND 100 5/19/23 5:10 MFFg/L27 5/18/23SM21-23 6200B2001,1,2,2-Tetrachloroethane
ND 100 5/19/23 5:10 MFFg/L34 5/18/23SM21-23 6200B200Tetrachloroethylene
14000 100 5/19/23 5:10 MFFg/L45 5/18/23SM21-23 6200B200Toluene
ND 200 5/19/23 5:10 MFFg/L68 5/18/23SM21-23 6200B2001,2,3-Trichlorobenzene
ND 200 5/19/23 5:10 MFFg/L60 5/18/23SM21-23 6200B2001,2,4-Trichlorobenzene
ND 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B2001,1,1-Trichloroethane
ND 100 5/19/23 5:10 MFFg/L38 5/18/23SM21-23 6200B2001,1,2-Trichloroethane
ND 100 5/19/23 5:10 MFFg/L35 5/18/23SM21-23 6200B200Trichloroethylene
ND 100 5/19/23 5:10 MFFg/L31 5/18/23SM21-23 6200B200Trichlorofluoromethane (Freon 11)
ND 100 5/19/23 5:10 MFFg/L55 5/18/23SM21-23 6200B2001,2,3-Trichloropropane
4900 100 5/19/23 5:10 MFFg/L40 5/18/23SM21-23 6200B2001,2,4-Trimethylbenzene
1200 100 5/19/23 5:10 MFFg/L30 5/18/23SM21-23 6200B2001,3,5-Trimethylbenzene
ND 4000 5/19/23 5:10 MFFg/L330 5/18/23SM21-23 6200B200Vinyl Acetate
ND 100 5/19/23 5:10 MFFg/L47 5/18/23SM21-23 6200B200Vinyl Chloride
16000 200 5/19/23 5:10 MFFg/L98 5/18/23SM21-23 6200B200m+p Xylene
7000 100 5/19/23 5:10 MFFg/L49 5/18/23SM21-23 6200B200o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.8 5/19/23 5:1070-130
Toluene-d8 99.0 5/19/23 5:1070-130
4-Bromofluorobenzene 95.6 5/19/23 5:1070-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-06
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:35
[TOC_2]23E1757-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 20000 5/19/23 5:36 MFFg/L800 5/18/23SM21-23 6200B400Acetone
ND 200 5/19/23 5:36 MFFg/L74 5/18/23SM21-23 6200B400Benzene
ND 200 5/19/23 5:36 MFFg/L59 5/18/23SM21-23 6200B400Bromobenzene
ND 200 5/19/23 5:36 MFFg/L110 5/18/23SM21-23 6200B400Bromochloromethane
ND 200 5/19/23 5:36 MFFg/L63 5/18/23SM21-23 6200B400Bromodichloromethane
ND 200 5/19/23 5:36 MFFg/L160 5/18/23SM21-23 6200B400Bromoform
ND 800 5/19/23 5:36 MFFg/L530 5/18/23SM21-23 6200B400Bromomethane
ND 2000 5/19/23 5:36 MFFg/L670 5/18/23SM21-23 6200B4002-Butanone (MEK)
1200 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B400n-Butylbenzene
230 200 5/19/23 5:36 MFFg/L51 5/18/23SM21-23 6200B400sec-Butylbenzene
ND 200 5/19/23 5:36 MFFg/L57 5/18/23SM21-23 6200B400tert-Butylbenzene
ND 200 5/19/23 5:36 MFFg/L65 5/18/23SM21-23 6200B400Carbon Tetrachloride
ND 200 5/19/23 5:36 MFFg/L48 5/18/23SM21-23 6200B400Chlorobenzene
ND 20000 5/19/23 5:36 MFFg/L8100 5/18/23SM21-23 6200B400Ethanol
ND 200 5/19/23 5:36 MFFg/L80 5/18/23SM21-23 6200B400Chlorodibromomethane
ND 200 5/19/23 5:36 MFFg/L140 5/18/23SM21-23 6200B400Chloroethane
ND 200 5/19/23 5:36 MFFg/L56 5/18/23SM21-23 6200B400Chloroform
ND 240 5/19/23 5:36 MFFg/L200 5/18/23SM21-23 6200B400Chloromethane
ND 200 5/19/23 5:36 MFFg/L62 5/18/23SM21-23 6200B4002-Chlorotoluene
ND 200 5/19/23 5:36 MFFg/L62 5/18/23SM21-23 6200B4004-Chlorotoluene
ND 200 5/19/23 5:36 MFFg/L64 5/18/23SM21-23 6200B4001,2-Dibromoethane (EDB)
ND 200 5/19/23 5:36 MFFg/L52 5/18/23SM21-23 6200B4001,2-Dichlorobenzene
ND 200 5/19/23 5:36 MFFg/L55 5/18/23SM21-23 6200B4001,3-Dichlorobenzene
ND 200 5/19/23 5:36 MFFg/L51 5/18/23SM21-23 6200B4001,4-Dichlorobenzene
ND 200 5/19/23 5:36 MFFg/L64 5/18/23SM21-23 6200B400Dichlorodifluoromethane (Freon 12)
ND 200 5/19/23 5:36 MFFg/L55 5/18/23SM21-23 6200B4001,1-Dichloroethane
ND 200 5/19/23 5:36 MFFg/L120 5/18/23SM21-23 6200B4001,2-Dichloroethane
ND 200 5/19/23 5:36 MFFg/L56 5/18/23SM21-23 6200B4001,1-Dichloroethylene
ND 200 5/19/23 5:36 MFFg/L56 5/18/23SM21-23 6200B400cis-1,2-Dichloroethylene
ND 200 5/19/23 5:36 MFFg/L69 5/18/23SM21-23 6200B400trans-1,2-Dichloroethylene
ND 200 5/19/23 5:36 MFFg/L77 5/18/23SM21-23 6200B4001,2-Dichloropropane
ND 200 5/19/23 5:36 MFFg/L46 5/18/23SM21-23 6200B4001,3-Dichloropropane
ND 200 5/19/23 5:36 MFFg/L140 5/18/23SM21-23 6200B4002,2-Dichloropropane
ND 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B4001,1-Dichloropropene
ND 200 5/19/23 5:36 MFFg/L65 5/18/23SM21-23 6200B400cis-1,3-Dichloropropene
ND 200 5/19/23 5:36 MFFg/L57 5/18/23SM21-23 6200B400trans-1,3-Dichloropropene
ND 200 5/19/23 5:36 MFFg/L81 5/18/23SM21-23 6200B400Diisopropyl Ether (DIPE)
3800 200 5/19/23 5:36 MFFg/L88 5/18/23SM21-23 6200B400Ethylbenzene
ND 2000 5/19/23 5:36 MFFg/L480 5/18/23SM21-23 6200B4002-Hexanone (MBK)
450 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B400Isopropylbenzene (Cumene)
170 200 5/19/23 5:36 MFFg/L51 5/18/23SM21-23 6200B400Jp-Isopropyltoluene (p-Cymene)
ND 200 5/19/23 5:36 MFFg/L68 5/18/23SM21-23 6200B400Methyl tert-Butyl Ether (MTBE)
ND 2000 5/19/23 5:36 MFFg/L71 5/18/23SM21-23 6200B400Methylene Chloride
ND 2000 5/19/23 5:36 MFFg/L530 5/18/23SM21-23 6200B4004-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-06
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
2500 200 5/19/23 5:36 MFFg/L150 5/18/23SM21-23 6200B400Naphthalene
1400 200 5/19/23 5:36 MFFg/L50 5/18/23SM21-23 6200B400n-Propylbenzene
ND 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B400Styrene
ND 200 5/19/23 5:36 MFFg/L55 5/18/23SM21-23 6200B4001,1,2,2-Tetrachloroethane
ND 200 5/19/23 5:36 MFFg/L67 5/18/23SM21-23 6200B400Tetrachloroethylene
2600 200 5/19/23 5:36 MFFg/L89 5/18/23SM21-23 6200B400Toluene
ND 400 5/19/23 5:36 MFFg/L140 5/18/23SM21-23 6200B4001,2,3-Trichlorobenzene
ND 400 5/19/23 5:36 MFFg/L120 5/18/23SM21-23 6200B4001,2,4-Trichlorobenzene
ND 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B4001,1,1-Trichloroethane
ND 200 5/19/23 5:36 MFFg/L76 5/18/23SM21-23 6200B4001,1,2-Trichloroethane
ND 200 5/19/23 5:36 MFFg/L70 5/18/23SM21-23 6200B400Trichloroethylene
ND 200 5/19/23 5:36 MFFg/L62 5/18/23SM21-23 6200B400Trichlorofluoromethane (Freon 11)
ND 200 5/19/23 5:36 MFFg/L110 5/18/23SM21-23 6200B4001,2,3-Trichloropropane
18000 200 5/19/23 5:36 MFFg/L80 5/18/23SM21-23 6200B4001,2,4-Trimethylbenzene
4900 200 5/19/23 5:36 MFFg/L60 5/18/23SM21-23 6200B4001,3,5-Trimethylbenzene
ND 8000 5/19/23 5:36 MFFg/L670 5/18/23SM21-23 6200B400Vinyl Acetate
ND 200 5/19/23 5:36 MFFg/L95 5/18/23SM21-23 6200B400Vinyl Chloride
23000 400 5/19/23 5:36 MFFg/L200 5/18/23SM21-23 6200B400m+p Xylene
9900 200 5/19/23 5:36 MFFg/L97 5/18/23SM21-23 6200B400o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.8 5/19/23 5:3670-130
Toluene-d8 100 5/19/23 5:3670-130
4-Bromofluorobenzene 97.2 5/19/23 5:3670-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-07
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:19
[TOC_2]23E1757-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
910 12000 5/19/23 6:03 MFFg/L500 5/18/23SM21-23 6200B250JAcetone
230 120 5/19/23 6:03 MFFg/L46 5/18/23SM21-23 6200B250Benzene
ND 120 5/19/23 6:03 MFFg/L37 5/18/23SM21-23 6200B250Bromobenzene
ND 120 5/19/23 6:03 MFFg/L71 5/18/23SM21-23 6200B250Bromochloromethane
ND 120 5/19/23 6:03 MFFg/L39 5/18/23SM21-23 6200B250Bromodichloromethane
ND 120 5/19/23 6:03 MFFg/L100 5/18/23SM21-23 6200B250Bromoform
ND 500 5/19/23 6:03 MFFg/L330 5/18/23SM21-23 6200B250Bromomethane
440 1200 5/19/23 6:03 MFFg/L420 5/18/23SM21-23 6200B250J2-Butanone (MEK)
130 120 5/19/23 6:03 MFFg/L37 5/18/23SM21-23 6200B250n-Butylbenzene
ND 120 5/19/23 6:03 MFFg/L32 5/18/23SM21-23 6200B250sec-Butylbenzene
ND 120 5/19/23 6:03 MFFg/L35 5/18/23SM21-23 6200B250tert-Butylbenzene
ND 120 5/19/23 6:03 MFFg/L41 5/18/23SM21-23 6200B250Carbon Tetrachloride
ND 120 5/19/23 6:03 MFFg/L30 5/18/23SM21-23 6200B250Chlorobenzene
ND 12000 5/19/23 6:03 MFFg/L5100 5/18/23SM21-23 6200B250Ethanol
ND 120 5/19/23 6:03 MFFg/L50 5/18/23SM21-23 6200B250Chlorodibromomethane
ND 120 5/19/23 6:03 MFFg/L86 5/18/23SM21-23 6200B250Chloroethane
ND 120 5/19/23 6:03 MFFg/L35 5/18/23SM21-23 6200B250Chloroform
ND 150 5/19/23 6:03 MFFg/L130 5/18/23SM21-23 6200B250Chloromethane
ND 120 5/19/23 6:03 MFFg/L39 5/18/23SM21-23 6200B2502-Chlorotoluene
ND 120 5/19/23 6:03 MFFg/L38 5/18/23SM21-23 6200B2504-Chlorotoluene
ND 120 5/19/23 6:03 MFFg/L40 5/18/23SM21-23 6200B2501,2-Dibromoethane (EDB)
ND 120 5/19/23 6:03 MFFg/L32 5/18/23SM21-23 6200B2501,2-Dichlorobenzene
ND 120 5/19/23 6:03 MFFg/L34 5/18/23SM21-23 6200B2501,3-Dichlorobenzene
ND 120 5/19/23 6:03 MFFg/L32 5/18/23SM21-23 6200B2501,4-Dichlorobenzene
ND 120 5/19/23 6:03 MFFg/L40 5/18/23SM21-23 6200B250Dichlorodifluoromethane (Freon 12)
ND 120 5/19/23 6:03 MFFg/L34 5/18/23SM21-23 6200B2501,1-Dichloroethane
ND 120 5/19/23 6:03 MFFg/L76 5/18/23SM21-23 6200B2501,2-Dichloroethane
ND 120 5/19/23 6:03 MFFg/L35 5/18/23SM21-23 6200B2501,1-Dichloroethylene
ND 120 5/19/23 6:03 MFFg/L35 5/18/23SM21-23 6200B250cis-1,2-Dichloroethylene
ND 120 5/19/23 6:03 MFFg/L43 5/18/23SM21-23 6200B250trans-1,2-Dichloroethylene
ND 120 5/19/23 6:03 MFFg/L48 5/18/23SM21-23 6200B2501,2-Dichloropropane
ND 120 5/19/23 6:03 MFFg/L29 5/18/23SM21-23 6200B2501,3-Dichloropropane
ND 120 5/19/23 6:03 MFFg/L87 5/18/23SM21-23 6200B2502,2-Dichloropropane
ND 120 5/19/23 6:03 MFFg/L37 5/18/23SM21-23 6200B2501,1-Dichloropropene
ND 120 5/19/23 6:03 MFFg/L41 5/18/23SM21-23 6200B250cis-1,3-Dichloropropene
ND 120 5/19/23 6:03 MFFg/L35 5/18/23SM21-23 6200B250trans-1,3-Dichloropropene
ND 120 5/19/23 6:03 MFFg/L50 5/18/23SM21-23 6200B250Diisopropyl Ether (DIPE)
2100 120 5/19/23 6:03 MFFg/L55 5/18/23SM21-23 6200B250Ethylbenzene
ND 1200 5/19/23 6:03 MFFg/L300 5/18/23SM21-23 6200B2502-Hexanone (MBK)
140 120 5/19/23 6:03 MFFg/L38 5/18/23SM21-23 6200B250Isopropylbenzene (Cumene)
ND 120 5/19/23 6:03 MFFg/L32 5/18/23SM21-23 6200B250p-Isopropyltoluene (p-Cymene)
70 120 5/19/23 6:03 MFFg/L43 5/18/23SM21-23 6200B250JMethyl tert-Butyl Ether (MTBE)
ND 1200 5/19/23 6:03 MFFg/L44 5/18/23SM21-23 6200B250Methylene Chloride
ND 1200 5/19/23 6:03 MFFg/L330 5/18/23SM21-23 6200B2504-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/12/2023
Work Order: 23E1757Sample Description:Project Location: Salemburg, NC
Sample ID: 23E1757-07
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 5/11/2023 11:19
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
1000 120 5/19/23 6:03 MFFg/L95 5/18/23SM21-23 6200B250Naphthalene
330 120 5/19/23 6:03 MFFg/L31 5/18/23SM21-23 6200B250n-Propylbenzene
ND 120 5/19/23 6:03 MFFg/L38 5/18/23SM21-23 6200B250Styrene
ND 120 5/19/23 6:03 MFFg/L34 5/18/23SM21-23 6200B2501,1,2,2-Tetrachloroethane
ND 120 5/19/23 6:03 MFFg/L42 5/18/23SM21-23 6200B250Tetrachloroethylene
11000 120 5/19/23 6:03 MFFg/L56 5/18/23SM21-23 6200B250Toluene
ND 250 5/19/23 6:03 MFFg/L86 5/18/23SM21-23 6200B2501,2,3-Trichlorobenzene
ND 250 5/19/23 6:03 MFFg/L75 5/18/23SM21-23 6200B2501,2,4-Trichlorobenzene
ND 120 5/19/23 6:03 MFFg/L37 5/18/23SM21-23 6200B2501,1,1-Trichloroethane
ND 120 5/19/23 6:03 MFFg/L48 5/18/23SM21-23 6200B2501,1,2-Trichloroethane
ND 120 5/19/23 6:03 MFFg/L44 5/18/23SM21-23 6200B250Trichloroethylene
ND 120 5/19/23 6:03 MFFg/L39 5/18/23SM21-23 6200B250Trichlorofluoromethane (Freon 11)
ND 120 5/19/23 6:03 MFFg/L69 5/18/23SM21-23 6200B2501,2,3-Trichloropropane
3900 120 5/19/23 6:03 MFFg/L50 5/18/23SM21-23 6200B2501,2,4-Trimethylbenzene
910 120 5/19/23 6:03 MFFg/L37 5/18/23SM21-23 6200B2501,3,5-Trimethylbenzene
ND 5000 5/19/23 6:03 MFFg/L420 5/18/23SM21-23 6200B250Vinyl Acetate
ND 120 5/19/23 6:03 MFFg/L59 5/18/23SM21-23 6200B250Vinyl Chloride
13000 250 5/19/23 6:03 MFFg/L120 5/18/23SM21-23 6200B250m+p Xylene
5900 120 5/19/23 6:03 MFFg/L61 5/18/23SM21-23 6200B250o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.3 5/19/23 6:0370-130
Toluene-d8 101 5/19/23 6:0370-130
4-Bromofluorobenzene 96.3 5/19/23 6:0370-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B340343 05/15/235 5.0023E1757-01 [Trip Blank]
B340343 05/15/230.25 5.0023E1757-02 [MW-1]
B340343 05/15/235 5.0023E1757-03 [MW-3]
B340343 05/15/235 5.0023E1757-04 [MW-4]
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B340602 05/18/230.025 5.0023E1757-05 [MW-5]
B340602 05/18/230.0125 5.0023E1757-06 [MW-6]
B340602 05/18/230.02 5.0023E1757-07 [MW-7]
[TOC_1]Sample Preparation Information[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B340343 - SW-846 5030B
[TOC_3]B340343[TOC]
Blank (B340343-BLK1) Prepared: 05/16/23 Analyzed: 05/18/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340343 - SW-846 5030B
Blank (B340343-BLK1) Prepared: 05/16/23 Analyzed: 05/18/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.6
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.324.6
LCS (B340343-BS1) Prepared: 05/16/23 Analyzed: 05/17/23
Acetone g/L50 100 70-13084.684.6
Benzene g/L0.50 10.0 70-13010610.6
Bromobenzene g/L0.50 10.0 70-13010410.4
Bromochloromethane g/L0.50 10.0 70-13010810.8
Bromodichloromethane g/L0.50 10.0 70-13099.49.94
Bromoform g/L0.50 10.0 70-13084.28.42
Bromomethane g/L2.0 10.0 60-14010510.5
2-Butanone (MEK)g/L5.0 100 70-130105105
n-Butylbenzene g/L0.50 10.0 70-13098.69.86
sec-Butylbenzene g/L0.50 10.0 70-13010110.1
tert-Butylbenzene g/L0.50 10.0 70-13010110.1
Carbon Tetrachloride g/L0.50 10.0 70-13010210.2
Chlorobenzene g/L0.50 10.0 70-13099.99.99
Ethanol g/L50 100 70-13092.092.0
Chlorodibromomethane g/L0.50 10.0 70-13097.89.78
Chloroethane g/L0.50 10.0 60-14096.59.65
Chloroform g/L0.50 10.0 70-13010810.8
Chloromethane g/L0.60 10.0 60-14011811.8
2-Chlorotoluene g/L0.50 10.0 70-13092.59.25
4-Chlorotoluene g/L0.50 10.0 70-13099.09.90
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010510.5
1,2-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,3-Dichlorobenzene g/L0.50 10.0 70-13010410.4
1,4-Dichlorobenzene g/L0.50 10.0 70-13099.19.91
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14084.78.47
1,1-Dichloroethane g/L0.50 10.0 70-13011211.2
1,2-Dichloroethane g/L0.50 10.0 70-13010210.2
1,1-Dichloroethylene g/L0.50 10.0 70-13081.88.18
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010910.9
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010810.8
1,2-Dichloropropane g/L0.50 10.0 70-13010210.2
1,3-Dichloropropane g/L0.50 10.0 70-13010610.6
2,2-Dichloropropane g/L0.50 10.0 70-13085.68.56
1,1-Dichloropropene g/L0.50 10.0 70-13010610.6
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010110.1
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340343 - SW-846 5030B
LCS (B340343-BS1) Prepared: 05/16/23 Analyzed: 05/17/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010310.3
Ethylbenzene g/L0.50 10.0 70-13010110.1
2-Hexanone (MBK)g/L5.0 100 70-130107107
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13097.89.78
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13097.89.78
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13099.49.94
Methylene Chloride g/L5.0 10.0 70-13083.68.36
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130106106
Naphthalene g/L0.50 10.0 70-13096.89.68
n-Propylbenzene g/L0.50 10.0 70-13097.79.77
Styrene g/L0.50 10.0 70-13099.09.90
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13099.59.95
Tetrachloroethylene g/L0.50 10.0 70-13010210.2
Toluene g/L0.50 10.0 70-13010510.5
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010410.4
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13099.59.95
1,1,1-Trichloroethane g/L0.50 10.0 70-13010610.6
1,1,2-Trichloroethane g/L0.50 10.0 70-13010810.8
Trichloroethylene g/L0.50 10.0 70-13010810.8
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13076.37.63
1,2,3-Trichloropropane g/L0.50 10.0 70-13010710.7
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010210.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13096.79.67
Vinyl Acetate g/L20 100 70-13098.098.0
Vinyl Chloride g/L0.50 10.0 60-14073.77.37
m+p Xylene g/L1.0 20.0 70-13099.820.0
o-Xylene g/L0.50 10.0 70-13010310.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10325.7
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.4
LCS Dup (B340343-BSD1) Prepared: 05/16/23 Analyzed: 05/17/23
Acetone g/L50 100 2570-13088.4 4.4488.4
Benzene g/L0.50 10.0 2570-130109 2.8910.9
Bromobenzene g/L0.50 10.0 2570-130106 2.3810.6
Bromochloromethane g/L0.50 10.0 2570-130112 4.0911.2
Bromodichloromethane g/L0.50 10.0 2570-130101 1.6010.1
Bromoform g/L0.50 10.0 2570-13084.3 0.1198.43
Bromomethane g/L2.0 10.0 2560-140110 5.4011.0
2-Butanone (MEK)g/L5.0 100 2570-130103 2.26103
n-Butylbenzene g/L0.50 10.0 2570-130104 5.2310.4
sec-Butylbenzene g/L0.50 10.0 2570-130107 5.2010.7
tert-Butylbenzene g/L0.50 10.0 2570-130107 5.9510.7
Carbon Tetrachloride g/L0.50 10.0 2570-130107 4.8710.7
Chlorobenzene g/L0.50 10.0 2570-130104 4.4110.4
Ethanol g/L50 100 2570-13094.3 2.4994.3
Chlorodibromomethane g/L0.50 10.0 2570-13099.4 1.629.94
Chloroethane g/L0.50 10.0 2560-14089.8 7.198.98
Chloroform g/L0.50 10.0 2570-130109 1.6610.9
Chloromethane g/L0.60 10.0 2560-14099.3 17.09.93
2-Chlorotoluene g/L0.50 10.0 2570-13095.6 3.309.56
4-Chlorotoluene g/L0.50 10.0 2570-130104 4.5410.4
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340343 - SW-846 5030B
LCS Dup (B340343-BSD1) Prepared: 05/16/23 Analyzed: 05/17/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130105 0.19010.5
1,2-Dichlorobenzene g/L0.50 10.0 2570-130106 4.7110.6
1,3-Dichlorobenzene g/L0.50 10.0 2570-130107 2.7510.7
1,4-Dichlorobenzene g/L0.50 10.0 2570-130102 2.8810.2
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14087.5 3.258.75
1,1-Dichloroethane g/L0.50 10.0 2570-130116 3.6811.6
1,2-Dichloroethane g/L0.50 10.0 2570-130103 0.78010.3
1,1-Dichloroethylene g/L0.50 10.0 2570-13084.8 3.608.48
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130113 3.8811.3
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130112 3.0911.2
1,2-Dichloropropane g/L0.50 10.0 2570-130108 5.2510.8
1,3-Dichloropropane g/L0.50 10.0 2570-130109 2.2310.9
2,2-Dichloropropane g/L0.50 10.0 2570-13085.1 0.5868.51
1,1-Dichloropropene g/L0.50 10.0 2570-130111 4.7011.1
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130106 2.7810.6
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130101 0.29610.1
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130108 3.8910.8
Ethylbenzene g/L0.50 10.0 2570-130105 3.8910.5
2-Hexanone (MBK)g/L5.0 100 2570-130108 0.569108
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130101 3.6110.1
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130102 4.3010.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13098.6 0.8089.86
Methylene Chloride g/L5.0 10.0 2570-13082.8 0.9628.28
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130104 1.61104
Naphthalene g/L0.50 10.0 2570-13098.7 1.949.87
n-Propylbenzene g/L0.50 10.0 2570-130103 5.3810.3
Styrene g/L0.50 10.0 2570-130101 1.6010.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13098.7 0.8079.87
Tetrachloroethylene g/L0.50 10.0 2570-130108 5.2310.8
Toluene g/L0.50 10.0 2570-130109 4.3910.9
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130108 4.1510.8
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13099.7 0.2019.97
1,1,1-Trichloroethane g/L0.50 10.0 2570-130110 3.9011.0
1,1,2-Trichloroethane g/L0.50 10.0 2570-130110 1.7411.0
Trichloroethylene g/L0.50 10.0 2570-130112 4.0911.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13079.1 3.607.91
1,2,3-Trichloropropane g/L0.50 10.0 2570-130109 2.1310.9
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130107 4.6110.7
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130101 4.4510.1
Vinyl Acetate g/L20 100 2570-13087.3 11.587.3
Vinyl Chloride g/L0.50 10.0 2560-14081.2 9.688.12
m+p Xylene g/L1.0 20.0 2570-130104 4.0220.8
o-Xylene g/L0.50 10.0 2570-130106 3.1510.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10325.7
g/L 25.0 70-130Surrogate: Toluene-d8 99.224.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.2
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340602 - SW-846 5030B
[TOC_3]B340602[TOC]
Blank (B340602-BLK1) Prepared & Analyzed: 05/18/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340602 - SW-846 5030B
Blank (B340602-BLK1) Prepared & Analyzed: 05/18/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.224.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.224.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.024.0
LCS (B340602-BS1) Prepared & Analyzed: 05/18/23
Acetone g/L50 100 70-13089.289.2
Benzene g/L0.50 10.0 70-13011211.2
Bromobenzene g/L0.50 10.0 70-13010210.2
Bromochloromethane g/L0.50 10.0 70-13011511.5
Bromodichloromethane g/L0.50 10.0 70-13099.29.92
Bromoform g/L0.50 10.0 70-13079.07.90
Bromomethane g/L2.0 10.0 60-14011911.9
2-Butanone (MEK)g/L5.0 100 70-130101101
n-Butylbenzene g/L0.50 10.0 70-13010710.7
sec-Butylbenzene g/L0.50 10.0 70-13010210.2
tert-Butylbenzene g/L0.50 10.0 70-13010110.1
Carbon Tetrachloride g/L0.50 10.0 70-13010110.1
Chlorobenzene g/L0.50 10.0 70-13010510.5
Ethanol g/L50 100 70-13072.772.7
Chlorodibromomethane g/L0.50 10.0 70-13093.79.37
Chloroethane g/L0.50 10.0 60-14093.59.35
Chloroform g/L0.50 10.0 70-13010210.2
Chloromethane g/L0.60 10.0 60-14010110.1
2-Chlorotoluene g/L0.50 10.0 70-13010210.2
4-Chlorotoluene g/L0.50 10.0 70-13010310.3
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010110.1
1,2-Dichlorobenzene g/L0.50 10.0 70-13010410.4
1,3-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,4-Dichlorobenzene g/L0.50 10.0 70-13010010.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14097.69.76
1,1-Dichloroethane g/L0.50 10.0 70-13010410.4
1,2-Dichloroethane g/L0.50 10.0 70-13094.79.47
1,1-Dichloroethylene g/L0.50 10.0 70-13093.99.39
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010310.3
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13098.39.83
1,2-Dichloropropane g/L0.50 10.0 70-13010910.9
1,3-Dichloropropane g/L0.50 10.0 70-13010710.7
2,2-Dichloropropane g/L0.50 10.0 70-13085.68.56
1,1-Dichloropropene g/L0.50 10.0 70-13010410.4
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010510.5
trans-1,3-Dichloropropene g/L0.50 10.0 70-13098.09.80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340602 - SW-846 5030B
LCS (B340602-BS1) Prepared & Analyzed: 05/18/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010810.8
Ethylbenzene g/L0.50 10.0 70-13010610.6
2-Hexanone (MBK)g/L5.0 100 70-13090.890.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010310.3
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010410.4
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13097.69.76
Methylene Chloride g/L5.0 10.0 70-13099.09.90
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13089.889.8
Naphthalene g/L0.50 10.0 70-13093.29.32
n-Propylbenzene g/L0.50 10.0 70-13010410.4
Styrene g/L0.50 10.0 70-13010710.7
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13090.69.06
Tetrachloroethylene g/L0.50 10.0 70-13010010.0
Toluene g/L0.50 10.0 70-13010610.6
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010110.1
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010010.0
1,1,1-Trichloroethane g/L0.50 10.0 70-13098.89.88
1,1,2-Trichloroethane g/L0.50 10.0 70-13010410.4
Trichloroethylene g/L0.50 10.0 70-13010410.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13091.49.14
1,2,3-Trichloropropane g/L0.50 10.0 70-13012012.0
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010110.1
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010210.2
Vinyl Acetate g/L20 100 70-13079.979.9
Vinyl Chloride g/L0.50 10.0 60-14011211.2
m+p Xylene g/L1.0 20.0 70-13010420.8
o-Xylene g/L0.50 10.0 70-13010210.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.923.5
g/L 25.0 70-130Surrogate: Toluene-d8 10125.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.124.8
LCS Dup (B340602-BSD1) Prepared & Analyzed: 05/18/23
Acetone g/L50 100 2570-13091.2 2.2591.2
Benzene g/L0.50 10.0 2570-130110 2.3411.0
Bromobenzene g/L0.50 10.0 2570-130104 1.7410.4
Bromochloromethane g/L0.50 10.0 2570-130112 2.5611.2
Bromodichloromethane g/L0.50 10.0 2570-13098.4 0.8109.84
Bromoform g/L0.50 10.0 2570-13079.6 0.7577.96
Bromomethane g/L2.0 10.0 2560-140123 3.4612.3
2-Butanone (MEK)g/L5.0 100 2570-130101 0.148101
n-Butylbenzene g/L0.50 10.0 2570-130102 4.4010.2
sec-Butylbenzene g/L0.50 10.0 2570-130100 1.7810.0
tert-Butylbenzene g/L0.50 10.0 2570-13099.2 2.099.92
Carbon Tetrachloride g/L0.50 10.0 2570-13097.1 4.239.71
Chlorobenzene g/L0.50 10.0 2570-130102 2.7110.2
Ethanol g/L50 100 2570-13078.5 7.7178.5
Chlorodibromomethane g/L0.50 10.0 2570-13092.4 1.409.24
Chloroethane g/L0.50 10.0 2560-14087.8 6.298.78
Chloroform g/L0.50 10.0 2570-130102 0.58910.2
Chloromethane g/L0.60 10.0 2560-14095.9 5.189.59
2-Chlorotoluene g/L0.50 10.0 2570-130103 0.68510.3
4-Chlorotoluene g/L0.50 10.0 2570-130102 0.29310.2
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B340602 - SW-846 5030B
LCS Dup (B340602-BSD1) Prepared & Analyzed: 05/18/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 0.0010.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130101 2.4410.1
1,3-Dichlorobenzene g/L0.50 10.0 2570-130103 0.29310.3
1,4-Dichlorobenzene g/L0.50 10.0 2570-13097.0 3.159.70
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14087.7 10.78.77
1,1-Dichloroethane g/L0.50 10.0 2570-130102 2.7210.2
1,2-Dichloroethane g/L0.50 10.0 2570-13094.8 0.1069.48
1,1-Dichloroethylene g/L0.50 10.0 2570-13089.6 4.698.96
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13098.6 4.569.86
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13091.8 6.849.18
1,2-Dichloropropane g/L0.50 10.0 2570-130106 3.0610.6
1,3-Dichloropropane g/L0.50 10.0 2570-130102 4.2110.2
2,2-Dichloropropane g/L0.50 10.0 2570-13081.1 5.408.11
1,1-Dichloropropene g/L0.50 10.0 2570-130101 3.4110.1
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130101 4.4610.1
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13096.7 1.349.67
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130104 3.5910.4
Ethylbenzene g/L0.50 10.0 2570-130104 2.0910.4
2-Hexanone (MBK)g/L5.0 100 2570-13091.7 1.0191.7
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130101 1.7710.1
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130102 2.4210.2
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13096.3 1.349.63
Methylene Chloride g/L5.0 10.0 2570-13095.4 3.709.54
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13090.2 0.47890.2
Naphthalene g/L0.50 10.0 2570-13089.3 4.278.93
n-Propylbenzene g/L0.50 10.0 2570-130104 0.096310.4
Styrene g/L0.50 10.0 2570-130106 0.75010.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13091.2 0.6609.12
Tetrachloroethylene g/L0.50 10.0 2570-13099.6 0.7009.96
Toluene g/L0.50 10.0 2570-130103 2.8710.3
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13097.7 3.129.77
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130101 0.79410.1
1,1,1-Trichloroethane g/L0.50 10.0 2570-13098.8 0.009.88
1,1,2-Trichloroethane g/L0.50 10.0 2570-130102 1.3610.2
Trichloroethylene g/L0.50 10.0 2570-130102 2.3310.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13085.8 6.328.58
1,2,3-Trichloropropane g/L0.50 10.0 2570-13093.3 24.79.33
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13097.6 3.629.76
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130100 2.1710.0
Vinyl Acetate g/L20 100 2570-13072.2 10.172.2
Vinyl Chloride g/L0.50 10.0 2560-140107 5.2010.7
m+p Xylene g/L1.0 20.0 2570-130102 2.0920.4
o-Xylene g/L0.50 10.0 2570-130101 1.1810.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.623.4
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.824.7
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
652North Carolina Div. of Water QualityNC 12/31/2023