FA-56_3601_CA_LTR_20230705_WSW9

220 Old Dairy Road
Wilmington, NC 28405
[phone]
www.CatlinUSA.com
Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA

ENVIRONMENTAL | CIVIL | GEOTECHNICAL

Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA | Charleston, SC

July 5, 2023
North Carolina Department of Environmental Quality Division of Waste Management UST Section Attn: Mr. Hassan Osman 1646 Mail Service Center Raleigh, NC 27699-1646 Re: Letter Report Former Kwik Shop 3625 Cumberland Road Fayetteville, Cumberland County, NC 28306 Incident Number: 3601 Risk Classification: H0215R CATLIN Project No. 220275 Dear Mr. Osman,
CATLIN Engineers and Scientists (CATLIN) is pleased to provide you with this letter report documenting field activities performed in general accordance with CATLIN proposal number 220275.5P, prepared April 18, 2023. Services were authorized by the North Carolina Environmental Quality (NCDEQ) Task Authorization (TA) #05, accepted April 19, 2023, and Contract Number N122019D. The approved scope of services for this Task Authorization included:
• Sample water supply well WSW-9;
• Analyze the groundwater sample from WSW-9 per Standard Method (SM) 6200B [plus ethylene dibromide (EDB), methyl tert-butyl ether (MTBE), and diisopropyl ether (DIPE)]; and
• Prepare a letter report documenting the findings. The Former Kwik Shop site is located at 3625 Cumberland Road, Fayetteville, Cumberland
County, NC. (See Figures in Attachment A). CATLIN conducted field activities on May 4, 2023, in accordance with the approved TA. Potential hazards were evaluated before beginning fieldwork and documented on an electronic Job Hazard Analysis (JHA) form, provided in Attachment B. Photographs of the site activities are included in Attachment C. Water Supply Well Sampling Water supply well WSW-9 was sampled in accordance with NCDEQ Guidelines and EPA
Region 4 Operating Procedures. Prior to obtaining a representative groundwater sample, the well
NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023
July 5, 2023 Page 2 of 2
was purged by running the tap (located on the front of the well house) for fifteen minutes. Information was entered into a field data sheet, a copy of which is included in
Attachment B. After the well was purged, a groundwater sample was collected from the spigot directly into laboratory-provided, pre-preserved glassware, labeled, and placed on ice in an insulated cooler.
A laboratory-provided trip blank was maintained in the cooler for the duration of the sampling event.
Samples were submitted to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC) protocol and analyzed per SM 6200B.
Groundwater Sample Results
Based on the results of the SM 6200B laboratory analysis, the sample from WSW-9 contained estimated (“J”-flag) concentrations of acetone (a known laboratory artifact) and also the target analyte 2-butanone. These detections were well below their respective 2L GWQS and no additional analytes were detected.
Trip Blank Sample Results
Based on the results of the SM 6200B laboratory analysis, no targeted analytes were detected in the trip blank sample.
The results of the WSW-9 analysis (and a summary of the water supply wells sampled under TA04 and TA05) are summarized in Table 1 (presented in Attachment D) and the laboratory analytical report and COC document are included in Attachment E.
Recommendations
CATLIN recommends conducting semi-annual groundwater sampling and consider deploying passive remediation devices in monitoring wells MW-1 and MW-2D or conducting
contaminant fate and transport modeling activities.
CATLIN Engineers and Scientists will proceed upon notification of your approval. Should you
have any questions or require additional information, please contact us at [phone].
Sincerely,
Benjamin J. Ashba, P.G.Contract Manager
Attachments: A Figures B Job Hazard Analysis and Field Data Sheet C Site Photographs
D Table E Laboratory Analytical Report and Chain of Custody Document
NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023
ATTACHMENT A
FIGURES
FIGUREPROJECTTITLE
1FORMER KWIK SHOP3625 CUMBERLAND RDFAYETTEVILLE, NC SITE VICINITY MAP
C U M B E R L A N D R DOWEN DRBOONE TRLFORMER KWIKSHOP SITE
FORMER BALL'S GROCERY SITE
APPROXIMATE FORMER BALL'S GROCERY SITE1,500 FEET RADIUS
APPROXIMATE FORMER KWIK SHOP SITE1,500 FEET RADIUS
Copyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220275JUNE 2023 AS SHOWN KMC/BJAINCIDENT NO.3601
FIGUREPROJECTTITLE
2FORMER KWIK SHOP3625 CUMBERLAND RDFAYETTEVILLE, NC
WATER SUPPLY WELL SAMPLEANALYTICAL RESULTS –MAY 4, 2023
!(P !(P
!(P
!(P
!(P !(P
!(P
!(P !(P
!(P
!(P
!(P
!(P
!(P
!(P!(P
!(P!(P
!(P !(P
!(P
!(P!(P!(P !(P
!(P !(P !(P !(P
!(P !(P
!(P!(P !(P !(P
!(P
!(P
!(P
!(P!(P
!(P
!(P
!(P
!(P!(P
!(P !(P !(P
!(P
!(P
!(P!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
!(P
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!(P
!(P!(P !(P
!(P
!(P
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!(P!(P
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!(P
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!(P
!(P
!(P
!(P!(W
!(P
!(P
!(P
!(P
!(P
!(P
!(P!(P
SITE LOCATION
C U M B E R L A N D R D
SW-47
SW-17
SW-5
SW-9
SW-45
SW-46
SW-44
SW-40
SW-43
SW-42
SW-41
SW-39SW-38
SW-37
SW-36
SW-35 SW-18
SW-34
SW-33 SW-2
SW-22
SW-4
SW-6
SW-3
SW-50
SW-20
SW-23
SW-7
SW-13SW-14
SW-10SW-11SW-12
SW-49SW-48SW-21SW-15
SW-16
SW-29
SW-30
SW-28SW-27
SW-24
SW-26
SW-25
SW-19
SW-31SW-32
WSW-21
WSW-22
WSW-23
WSW-24
WSW-23
WSW-25
WSW-26
WSW-27
WSW-17
WSW-18
WSW-19
WSW-20 WSW-12
WSW-13WSW-14
WSW-6
WSW-7 WSW-10
WSW-1
WSW-4
WSW-5
WSW-31
WSW-30
WSW-35
WSW-37
WSW-38
WSW-41
WSW-33
WSW-34
WSW-45
WSW-36 WSW-46WSW-39
WSW-47WSW-42 WSW-43
WSW-44
WSW-11 WSW-40
WSW-3
WSW-2
WSW-32WSW-9
WSW-8WSW-16WSW-29
WSW-15
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220275JUNE 2023 AS SHOWN KMC/BJAINCIDENT NO.3601
NOTES: 1. Well locations were obtained from previous reports prepared by other consultants and are approximate.2. Water supply wells historically associated with the Former Ball's Grocery Site are named "WSW-##", water supply wells originally associated with the Former Kwik Mart are named "SW-##".
LEGEND
!(W Active Non-Potable Water Supply Well
!(P
!(P
Active Potable Water Supply Well
Inactive PotableWater Supply Well
!(P Sampled PotableWater Supply Well
DateCollected(mm/dd/yy)
05/04/23 4.2 J 1.8 J
All results in micrograms per liter (µg/L).See Table 4 for all other notes and definitions.
WSW-9
SUMMARY OF WATER SUPPLY WELL LABORATORY RESULTS — STANDARD METHOD 6200BIncident Name and No.: Former Kwik Shop - 3601
4,000,0004,000GCL (µg/L)2L GWQS (µg/L) 6,000,0006,000
Well/Sample ID
Contaminant of Concern
Acetone 2-Butanone
NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023
ATTACHMENT B
JOB HAZARD ANALYSIS AND FIELD DATA SHEET
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Exposure Potential
Likely
Likely
Likely
Start Stop
13:15 14:30
14:30 14:45
14:45 15:00
15:00 18:00
Date and Time:
5/4/23 @ 14:45
NAPHTHALENE ppm
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
* Gas and/or Diesel
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
Potential Chemicals Concentration
BENZENE ppm
ETHYL BENZENE ppm
Chemical Hazards
Sunny, Breezy, low 70's
Site-Specific Job Hazard Analysis
Location Where Task/Operation Performed
Former Kwik Shop (WSW-9 2202 Dixie Tr.), Fayetteville, NC
Task/Operation
Sample One Water Supply Well
Employee Certifying this JHA
Print Name: Benjamin J. Ashba, P.G.Signature:
Operational Phase
Monitoring
Date(s) this JHA
Conducted:
5/4/23
PERSONNEL ONSITE
Name and Company (Print)Signature
Sandra Miller / CATLIN
Unlikely
Slips/Trips/Falls Unlikely
surroundings
Departed site, got ice for samples, completed COC & got PO#, and dropped samples off, got gas for van,
returned to office, demob van.
Start:End:
DAILY TASK
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
Equipment Used:PPE D/Sampling Supplies
Van #59 Mileage:
Weather:
Mob equipment and supplies, travel to WSW-9 location.
Onsite health & safety briefing; watch for spiders, snakes,and ants in the bushes near the spigot.
WSW-9 purged and sampled from spigot on well house, took pics.
Biological Hazards
Name of Biological Hazard Source
Insect bites and stings
Cold Weather Operations Unlikely
Heat (ambient)
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
WSW-9
14:30
14:45
No
14:45
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
Laboratory:Con-Test Analysis:
Purge Stop Time Screen Interval
WATER SUPPLY WELL SAMPLING FORM
Kwik Shop Cumberland Sandy Miller
220275.5 5/4/2023
NCDEQ-Osman
Water Supply Well Purging Information
Water Supply Well ID Well Depth
Purge Start Time Well Diamater
6200B
Was Well Purged Dry?Date Installled
Sample Time Well Material
Comments
Sample collected from spigot at front of house.
Geochemical Parameters
Turbidity and Additional
Sampling Notes
Water appeared to be somewhat discolored
(yellowish) despite a full
flow for 15 minutes.
Laboratory Analysis Information
NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023
ATTACHMENT C
SITE PHOTOGRAPHS
ATTACHMENT C
SITE PHOTOGRAPHS – MAY 4, 2023
NCDEQ; 3601_Kwik Shop CATLIN Engineers and Scientists
CATLIN Project No. 220275 June 2023
View of the spigot on the front of the WSW-9 residence, facing west.
Kwik Shop
WSW-9
Residence 19 19
NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023
ATTACHMENT D
TABLE
Page 1 of 1
TABLE 1
SUMMARY OF WATER SUPPLY WELL LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Former Kwik Shop - 3601
Well Owner/
User Property Address Owner Address Phone
Number
Date
Collected
(mm/dd/yy)
Gerry & Robin D.
Moore
2201 Dixie Trail
Fayetteville, NC
28306
P.O. Box 188,
Lakeview, NC
28350
(910)
424-1795 03/14/23 <2.0 <0.16 <1.7 <0.14 <0.17 BMDL
John P. & Evelene
McLamb
2210 Dixie Tr.,
Fayetteville, NC
28306
2210 Dixie Tr.,
Fayetteville, NC
28306
(910)
424-2604 03/14/23 <2.0 0.29 J <1.7 1.4 0.24 J BMDL
Clifford Yoder & Wife
2202 Dixie Trail
Fayetteville, NC
28306
3206 Rouse Dr.,
Fayetteville, NC
28306
[phone] 05/04/23 4.2 J <0.16 1.8 J <0.14 <0.17 BMDL
James C. &
Margaret P. Ross
2616 Everitte St., Fayetteville, NC
28306
2616 Everitte St., Fayetteville, NC
28306
(910)
920-2768 03/14/23 <2.0 <0.16 <1.7 0.20 J 2.8 BMDL
03/14/23 <2.0 <0.16 <0.17 0.38 <0.17 BMDL
05/04/23 <2.0 <0.16 <1.7 <0.14 <0.17 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
Bold Well/Sample IDs indicate detectable concentrations.
GCL = Gross Contaminant Level
NE = Not Established
< = Less than method detection limit
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).
NE
NE
70,000
70
20,000
20
Varies
Varies
WSW-3
WSW-7
SW-19
Trip Blank Not Applicable
GCL (µg/L)
2L GWQS (µg/L)
WSW-9
4,000,000
4,000
6,000,000
6,000
Trip Blank Not Applicable
Contaminant of
Concern
BromodichloromethaneChloroformMethyl tert-Butyl Ether (MTBE)All Other SM 6200B AnalytesWell/
Sample
ID
Acetone2-ButanoneNCDEQ; WSW Summary.xlsx; WSW Summary
CATLIN Project No. 220275
CATLIN Engineers and Scientists
July 2023

NCDEQ; Kwik Shop WSW Letter Report CATLIN Engineers and Scientists
CATLIN Project No. 220275 July 2023

ATTACHMENT E LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
May 15, 2023
Ben Ashba
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
Project Location: Fayetville, NC
Client Job Number:
Project Number: 220275.5
Laboratory Work Order Number: 23E1013
Enclosed are results of analyses for samples as received by the laboratory on May 6, 2023. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Page 1 of 21
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 6
Sample Results 7
23E1013-01 7
23E1013-02 9
Sample Preparation Information 11
QC Data 12
Volatile Organic Compounds by GC/MS 12
B339823 12
Flag/Qualifier Summary 16
Certifications 17
Chain of Custody/Sample Receipt 19
Page 2 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
5/15/2023
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
ATTN: Ben Ashba
220275.5
23E1013
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Fayetville, NC
230504.3
WSW-9 23E1013-01 Ground Water SM21-23 6200B
TB 23E1013-02 Trip Blank Water SM21-23 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:23E1013-02TB
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E1013-01WSW-9
DL
2-Butanone (MEK)1.8 5.0 g/L SM21-23 6200BJ1.7
Acetone 4.2 50 g/L SM21-23 6200BJ2.0
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 5 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 6 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/6/2023
Work Order: 23E1013Sample Description:Project Location: Fayetville, NC
Sample ID: 23E1013-01
Field Sample #: WSW-9
Sample Matrix: Ground Water
Sampled: 5/4/2023 14:45
[TOC_2]23E1013-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
4.2 50 5/12/23 0:52 EEHg/L2.0 5/10/23SM21-23 6200B1JAcetone
ND 0.50 5/12/23 0:52 EEHg/L0.18 5/10/23SM21-23 6200B1Benzene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B1Bromobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.28 5/10/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/12/23 0:52 EEHg/L0.16 5/10/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/12/23 0:52 EEHg/L0.41 5/10/23SM21-23 6200B1Bromoform
ND 2.0 5/12/23 0:52 EEHg/L1.3 5/10/23SM21-23 6200B1Bromomethane
1.8 5.0 5/12/23 0:52 EEHg/L1.7 5/10/23SM21-23 6200B1J2-Butanone (MEK)
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/12/23 0:52 EEHg/L0.13 5/10/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/12/23 0:52 EEHg/L0.16 5/10/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/12/23 0:52 EEHg/L0.12 5/10/23SM21-23 6200B1Chlorobenzene
ND 50 5/12/23 0:52 EEHg/L20 5/10/23SM21-23 6200B1Ethanol
ND 0.50 5/12/23 0:52 EEHg/L0.20 5/10/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/12/23 0:52 EEHg/L0.34 5/10/23SM21-23 6200B1Chloroethane
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B1Chloroform
ND 0.60 5/12/23 0:52 EEHg/L0.50 5/10/23SM21-23 6200B1Chloromethane
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/12/23 0:52 EEHg/L0.16 5/10/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/12/23 0:52 EEHg/L0.13 5/10/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.13 5/10/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.16 5/10/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/12/23 0:52 EEHg/L0.30 5/10/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/12/23 0:52 EEHg/L0.17 5/10/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/12/23 0:52 EEHg/L0.19 5/10/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/12/23 0:52 EEHg/L0.12 5/10/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/12/23 0:52 EEHg/L0.35 5/10/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/12/23 0:52 EEHg/L0.16 5/10/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/12/23 0:52 EEHg/L0.20 5/10/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/12/23 0:52 EEHg/L0.22 5/10/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/12/23 0:52 EEHg/L1.2 5/10/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/12/23 0:52 EEHg/L0.13 5/10/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/12/23 0:52 EEHg/L0.17 5/10/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/12/23 0:52 EEHg/L0.18 5/10/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/12/23 0:52 EEHg/L1.3 5/10/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 7 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/6/2023
Work Order: 23E1013Sample Description:Project Location: Fayetville, NC
Sample ID: 23E1013-01
Field Sample #: WSW-9
Sample Matrix: Ground Water
Sampled: 5/4/2023 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/12/23 0:52 EEHg/L0.38 5/10/23SM21-23 6200B1Naphthalene
ND 0.50 5/12/23 0:52 EEHg/L0.12 5/10/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B1Styrene
ND 0.50 5/12/23 0:52 EEHg/L0.14 5/10/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/12/23 0:52 EEHg/L0.17 5/10/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/12/23 0:52 EEHg/L0.22 5/10/23SM21-23 6200B1Toluene
ND 1.0 5/12/23 0:52 EEHg/L0.34 5/10/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.30 5/10/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/12/23 0:52 EEHg/L0.19 5/10/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/12/23 0:52 EEHg/L0.17 5/10/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/12/23 0:52 EEHg/L0.28 5/10/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/12/23 0:52 EEHg/L0.20 5/10/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/12/23 0:52 EEHg/L0.15 5/10/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/12/23 0:52 EEHg/L1.7 5/10/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/12/23 0:52 EEHg/L0.24 5/10/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/12/23 0:52 EEHg/L0.49 5/10/23SM21-23 6200B1m+p Xylene
ND 0.50 5/12/23 0:52 EEHg/L0.24 5/10/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 5/12/23 0:5270-130
Toluene-d8 100 5/12/23 0:5270-130
4-Bromofluorobenzene 85.3 5/12/23 0:5270-130
Page 8 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/6/2023
Work Order: 23E1013Sample Description:Project Location: Fayetville, NC
Sample ID: 23E1013-02
Field Sample #: TB
Sample Matrix: Trip Blank Water
Sampled: 5/4/2023 14:45
[TOC_2]23E1013-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/12/23 0:25 EEHg/L2.0 5/10/23SM21-23 6200B1Acetone
ND 0.50 5/12/23 0:25 EEHg/L0.18 5/10/23SM21-23 6200B1Benzene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B1Bromobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.28 5/10/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/12/23 0:25 EEHg/L0.16 5/10/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/12/23 0:25 EEHg/L0.41 5/10/23SM21-23 6200B1Bromoform
ND 2.0 5/12/23 0:25 EEHg/L1.3 5/10/23SM21-23 6200B1Bromomethane
ND 5.0 5/12/23 0:25 EEHg/L1.7 5/10/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/12/23 0:25 EEHg/L0.13 5/10/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/12/23 0:25 EEHg/L0.16 5/10/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/12/23 0:25 EEHg/L0.12 5/10/23SM21-23 6200B1Chlorobenzene
ND 50 5/12/23 0:25 EEHg/L20 5/10/23SM21-23 6200B1Ethanol
ND 0.50 5/12/23 0:25 EEHg/L0.20 5/10/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/12/23 0:25 EEHg/L0.34 5/10/23SM21-23 6200B1Chloroethane
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B1Chloroform
ND 0.60 5/12/23 0:25 EEHg/L0.50 5/10/23SM21-23 6200B1Chloromethane
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/12/23 0:25 EEHg/L0.16 5/10/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/12/23 0:25 EEHg/L0.13 5/10/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.13 5/10/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.16 5/10/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/12/23 0:25 EEHg/L0.30 5/10/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/12/23 0:25 EEHg/L0.17 5/10/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/12/23 0:25 EEHg/L0.19 5/10/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/12/23 0:25 EEHg/L0.12 5/10/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/12/23 0:25 EEHg/L0.35 5/10/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/12/23 0:25 EEHg/L0.16 5/10/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/12/23 0:25 EEHg/L0.20 5/10/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/12/23 0:25 EEHg/L0.22 5/10/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/12/23 0:25 EEHg/L1.2 5/10/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/12/23 0:25 EEHg/L0.13 5/10/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/12/23 0:25 EEHg/L0.17 5/10/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/12/23 0:25 EEHg/L0.18 5/10/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/12/23 0:25 EEHg/L1.3 5/10/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
Page 9 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/6/2023
Work Order: 23E1013Sample Description:Project Location: Fayetville, NC
Sample ID: 23E1013-02
Field Sample #: TB
Sample Matrix: Trip Blank Water
Sampled: 5/4/2023 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/12/23 0:25 EEHg/L0.38 5/10/23SM21-23 6200B1Naphthalene
ND 0.50 5/12/23 0:25 EEHg/L0.12 5/10/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B1Styrene
ND 0.50 5/12/23 0:25 EEHg/L0.14 5/10/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/12/23 0:25 EEHg/L0.17 5/10/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/12/23 0:25 EEHg/L0.22 5/10/23SM21-23 6200B1Toluene
ND 1.0 5/12/23 0:25 EEHg/L0.34 5/10/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.30 5/10/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/12/23 0:25 EEHg/L0.19 5/10/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/12/23 0:25 EEHg/L0.17 5/10/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/12/23 0:25 EEHg/L0.28 5/10/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/12/23 0:25 EEHg/L0.20 5/10/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/12/23 0:25 EEHg/L0.15 5/10/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/12/23 0:25 EEHg/L1.7 5/10/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/12/23 0:25 EEHg/L0.24 5/10/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/12/23 0:25 EEHg/L0.49 5/10/23SM21-23 6200B1m+p Xylene
ND 0.50 5/12/23 0:25 EEHg/L0.24 5/10/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 105 5/12/23 0:2570-130
Toluene-d8 101 5/12/23 0:2570-130
4-Bromofluorobenzene 97.4 5/12/23 0:2570-130
Page 10 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B339823 05/10/235 5.0023E1013-01 [WSW-9]
B339823 05/10/235 5.0023E1013-02 [TB]
[TOC_1]Sample Preparation Information[TOC]
Page 11 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B339823 - SW-846 5030B
[TOC_3]B339823[TOC]
Blank (B339823-BLK1) Prepared: 05/10/23 Analyzed: 05/11/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 12 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B339823 - SW-846 5030B
Blank (B339823-BLK1) Prepared: 05/10/23 Analyzed: 05/11/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10726.7
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.423.8
LCS (B339823-BS1) Prepared: 05/10/23 Analyzed: 05/11/23
Acetone g/L50 100 70-130106106
Benzene g/L0.50 10.0 70-13010110.1
Bromobenzene g/L0.50 10.0 70-13010310.3
Bromochloromethane g/L0.50 10.0 70-13010710.7
Bromodichloromethane g/L0.50 10.0 70-13010210.2
Bromoform g/L0.50 10.0 70-13096.09.60
Bromomethane g/L2.0 10.0 60-14085.88.58
2-Butanone (MEK)g/L5.0 100 70-13096.796.7
n-Butylbenzene g/L0.50 10.0 70-13092.79.27
sec-Butylbenzene g/L0.50 10.0 70-13097.39.73
tert-Butylbenzene g/L0.50 10.0 70-13099.39.93
Carbon Tetrachloride g/L0.50 10.0 70-13010210.2
Chlorobenzene g/L0.50 10.0 70-13010110.1
Ethanol g/L50 100 70-130105105
Chlorodibromomethane g/L0.50 10.0 70-13098.59.85
Chloroethane g/L0.50 10.0 60-14099.09.90
Chloroform g/L0.50 10.0 70-13010510.5
Chloromethane g/L0.60 10.0 60-14070.77.07
2-Chlorotoluene g/L0.50 10.0 70-13092.19.21
4-Chlorotoluene g/L0.50 10.0 70-13098.69.86
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010410.4
1,2-Dichlorobenzene g/L0.50 10.0 70-13010310.3
1,3-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,4-Dichlorobenzene g/L0.50 10.0 70-13099.19.91
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14075.87.58
1,1-Dichloroethane g/L0.50 10.0 70-13010510.5
1,2-Dichloroethane g/L0.50 10.0 70-13010310.3
1,1-Dichloroethylene g/L0.50 10.0 70-13094.19.41
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010710.7
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010210.2
1,2-Dichloropropane g/L0.50 10.0 70-13099.79.97
1,3-Dichloropropane g/L0.50 10.0 70-13010610.6
2,2-Dichloropropane g/L0.50 10.0 70-13084.98.49
1,1-Dichloropropene g/L0.50 10.0 70-13099.89.98
cis-1,3-Dichloropropene g/L0.50 10.0 70-13094.39.43
trans-1,3-Dichloropropene g/L0.50 10.0 70-13093.99.39
Page 13 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B339823 - SW-846 5030B
LCS (B339823-BS1) Prepared: 05/10/23 Analyzed: 05/11/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010410.4
Ethylbenzene g/L0.50 10.0 70-13010010.0
2-Hexanone (MBK)g/L5.0 100 70-130109109
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13099.39.93
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13093.09.30
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13099.99.99
Methylene Chloride g/L5.0 10.0 70-13081.98.19
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130107107
Naphthalene g/L0.50 10.0 70-13088.88.88
n-Propylbenzene g/L0.50 10.0 70-13096.89.68
Styrene g/L0.50 10.0 70-13098.39.83
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010110.1
Tetrachloroethylene g/L0.50 10.0 70-13010110.1
Toluene g/L0.50 10.0 70-13010210.2
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13097.19.71
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13094.09.40
1,1,1-Trichloroethane g/L0.50 10.0 70-13010610.6
1,1,2-Trichloroethane g/L0.50 10.0 70-13010610.6
Trichloroethylene g/L0.50 10.0 70-13010510.5
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13094.19.41
1,2,3-Trichloropropane g/L0.50 10.0 70-13010510.5
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13096.89.68
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13094.49.44
Vinyl Acetate g/L20 100 70-13074.174.1
Vinyl Chloride g/L0.50 10.0 60-14011511.5
m+p Xylene g/L1.0 20.0 70-13099.219.8
o-Xylene g/L0.50 10.0 70-13010110.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10726.8
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.925.0
LCS Dup (B339823-BSD1) Prepared: 05/10/23 Analyzed: 05/11/23
Acetone g/L50 100 2570-130109 2.40109
Benzene g/L0.50 10.0 2570-13099.3 1.809.93
Bromobenzene g/L0.50 10.0 2570-130101 1.8610.1
Bromochloromethane g/L0.50 10.0 2570-130107 0.093610.7
Bromodichloromethane g/L0.50 10.0 2570-13098.2 3.899.82
Bromoform g/L0.50 10.0 2570-13096.1 0.1049.61
Bromomethane g/L2.0 10.0 2560-140101 16.410.1
2-Butanone (MEK)g/L5.0 100 2570-130105 8.28105
n-Butylbenzene g/L0.50 10.0 2570-13099.1 6.679.91
sec-Butylbenzene g/L0.50 10.0 2570-13094.5 2.929.45
tert-Butylbenzene g/L0.50 10.0 2570-13096.0 3.389.60
Carbon Tetrachloride g/L0.50 10.0 2570-130101 0.29610.1
Chlorobenzene g/L0.50 10.0 2570-13099.1 1.909.91
Ethanol g/L50 100 2570-13095.8 9.5295.8
Chlorodibromomethane g/L0.50 10.0 2570-13097.5 1.029.75
Chloroethane g/L0.50 10.0 2560-14098.3 0.7109.83
Chloroform g/L0.50 10.0 2570-130105 0.095010.5
Chloromethane g/L0.60 10.0 2560-14083.0 16.08.30
2-Chlorotoluene g/L0.50 10.0 2570-13086.1 6.738.61
4-Chlorotoluene g/L0.50 10.0 2570-13095.3 3.409.53
Page 14 of 21
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B339823 - SW-846 5030B
LCS Dup (B339823-BSD1) Prepared: 05/10/23 Analyzed: 05/11/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130102 1.9410.2
1,2-Dichlorobenzene g/L0.50 10.0 2570-130115 10.711.5
1,3-Dichlorobenzene g/L0.50 10.0 2570-13099.7 2.779.97
1,4-Dichlorobenzene g/L0.50 10.0 2570-13098.0 1.129.80
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14078.6 3.637.86
1,1-Dichloroethane g/L0.50 10.0 2570-130104 1.1510.4
1,2-Dichloroethane g/L0.50 10.0 2570-130103 0.58310.3
1,1-Dichloroethylene g/L0.50 10.0 2570-13092.3 1.939.23
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130103 4.1810.3
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.6 5.059.66
1,2-Dichloropropane g/L0.50 10.0 2570-130100 0.79910.0
1,3-Dichloropropane g/L0.50 10.0 2570-130107 1.2210.7
2,2-Dichloropropane g/L0.50 10.0 2570-13083.4 1.788.34
1,1-Dichloropropene g/L0.50 10.0 2570-13098.4 1.419.84
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13091.8 2.699.18
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13092.8 1.189.28
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130102 1.6410.2
Ethylbenzene g/L0.50 10.0 2570-13096.4 3.779.64
2-Hexanone (MBK)g/L5.0 100 2570-130109 0.881109
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13095.2 4.229.52
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13091.1 2.069.11
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13098.7 1.219.87
Methylene Chloride g/L5.0 10.0 2570-130103 23.010.3
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130105 1.34105
Naphthalene g/L0.50 10.0 2570-13092.9 4.519.29
n-Propylbenzene g/L0.50 10.0 2570-13095.3 1.569.53
Styrene g/L0.50 10.0 2570-13095.8 2.589.58
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13099.1 1.809.91
Tetrachloroethylene g/L0.50 10.0 2570-13097.3 3.439.73
Toluene g/L0.50 10.0 2570-13099.0 2.999.90
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13099.8 2.749.98
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13091.8 2.379.18
1,1,1-Trichloroethane g/L0.50 10.0 2570-130103 2.3010.3
1,1,2-Trichloroethane g/L0.50 10.0 2570-130106 0.094110.6
Trichloroethylene g/L0.50 10.0 2570-130105 0.19010.5
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13091.9 2.379.19
1,2,3-Trichloropropane g/L0.50 10.0 2570-130106 0.57010.6
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13095.1 1.779.51
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13092.0 2.589.20
Vinyl Acetate g/L20 100 2570-13075.2 1.4675.2
Vinyl Chloride g/L0.50 10.0 2560-14094.2 20.19.42
m+p Xylene g/L1.0 20.0 2570-13096.6 2.7119.3
o-Xylene g/L0.50 10.0 2570-13098.5 2.219.85
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10826.9
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.624.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
652North Carolina Div. of Water QualityNC 12/31/2023
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