AS-3057_28266_CA_MRP_20230621

Monitoring Report

Suttles Property
1100 Newfound Road
Leicester, Buncombe County, North Carolina 28748
NCDEQ Incident #28266
ATC Project #SLC2826604

Submittal Date:

June 21, 2023

Prepared By:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina 28273
p: [phone] / f: [phone]

www.atcgroupservices.com

7606WhitehallExecutiveCenterDriveSuite800Charlotte,NC28273Tel:[phone]Fax:[phone]www.atcgroupservices.comN.C.EngineeringLicenseNo.C-1598ASSOCIATESOFNORTHCAROLINA,P.C.June21,2023Mr.ThomasChapmanNorthCarolinaDepartmentofEnvironmentalQualityDivisionofWasteManagement-UndergroundStorageTankSection1646MailServiceCenterRaleigh,NorthCarolina27699Re:MonitoringReportSuttlesProperty1100NewfoundRoadLeicester,BuncombeCounty,NorthCarolina28748NCDEQIncident#28266ATCProject#SLC2826605TaskAuthorization:TA-05DearMr.Chapman:ATCAssociatesofNorthCarolina,P.C.,(ATC)undercontracttotheNorthCarolinaDepartmentofEnvironmentalQuality(NCDEQ),issubmittingtheenclosedMonitoringReportforSuttlesPropertysite.Thereportpresentsinvestigativeprocedures,fieldactivities,andlaboratoryanalyticalresultsforthegroundwatersamplingeventconductedonApril27,2023.Ifyouhaveanyquestionsorrequireadditionalinformation,pleasecontactourofficeat(704)529-3200.Sincerely,ATCAssociatesofNorthCarolina,P.C.NoelleFrance,P.G.SeniorProjectManagerSeniorProjectManager
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION ............................................................................... 1
2.0 EXECUTIVE SUMMARY ............................................................................. 2
3.0 SITE DESCRIPTION ................................................................................... 2
3.1 Site Characterization .................................................................... 2
3.2 Site Background ........................................................................... 3
3.3 Site and Regional Geology .......................................................... 4
3.3 Site and Regional Hydrogeology .................................................. 5
4.0 GROUNDWATER CHARACTERIZATION .................................................. 5
4.1 Groundwater Levels ..................................................................... 5
4.2 Groundwater Quality .................................................................... 6
4.5 Quality Assurance and Quality Control ........................................ 6
5.0 CONCLUSIONS AND RECOMMENDATIONS ........................................... 6

TABLES
Table 1 Water Supply Well Information
Table 2 Monitoring Well Construction and Water Level Elevation Data
Table 3 Water Quality Parameters
Table 4 Monitoring Well Analytical Results

FIGURES
Figure 1 Vicinity Map
Figure 2 Water Supply Well Location Map
Figure 3 Site Map
Figure 4 Groundwater Elevation Map
Figure 5 Constituents of Concern Map

APPENDICES
Appendix A Conceptual Site Model
Appendix B Field Notes
Appendix C Laboratory Analytical Report
MonitoringReportSuttlesProperty,NCDEQIncident#28266June21,2023ATCProject#SLC28266051.0SITEIDENTIFICATION1.SiteIdentificationDateofReport:June21,2023FacilityI.D.:00-0-0000003057SiteRisk:HighSiteRank:SiteName:SiteStreetAddress:1100NewfoundRoadCity/Town:LeicesterDescriptionofGeographicalDataPoint:_LocationMethod:GoogleEarthLatitude(decimaldegrees):35.604515°NLongitude(decimaldegrees):82.731620°WUSTIncidentNumber(ifknown):28266H100DLandUseCategory:Residential/CommercialSuttlesPropertyZipCode:28748FormerUSTBasinCounty:Buncombe2.InformationaboutContactsAssociatedwiththeLeakingUSTSystemPropertyOwner:ChristopherJamesSuttlesAddress:1096NewfoundRoad,Leicester,NC28748Tel.:[phone]PropertyOwner:ChristopherJamesSuttlesAddress:1096NewfoundRoad,Leicester,NC28748PropertyOwner:ChristopherJamesSuttlesAddress:PropertyOwner:ChristopherJamesSuttlesAddress:Consultant/Contractor:ATCAssociatesofNorthCarolina.P.C.Address:7606WhitehallExecutiveCenterDr.,Charlotte.NC28273Tel.:[phone]AnalyticalLaboratory:PaceAnalyticalServices.LLCAddress:9800KincevAvenue.Ste100,Huntersville.NC28078Tel:[phone]Tel.:[phone]NewfoundRoad,Leicester.NC28748Tel.:[phone]NewfoundRoad,Leicester,NC28748Tel.:[phone]StateCertificationNo.123.InformationaboutReleaseDateDiscovered:EstimatedQuantityofRelease:UnknownCauseofRelease:UnknownSourceofRelease(Dispenser/Piping/UST):LeakingUSTSystemSizesandcontentsofUSTsystem(s)fromwhichthereleaseoccurred:Two2,000-gallongasolineUSTs,two570-gallongasolineUSTs,one990-gallongasolineUST,one430-gallonkeroseneUST,andassociatedpipinganddispenserislandCriteriaUsedtoClassifyRisk:PetroleumconstituentsingroundwaterexceedgroundwaterQualitystandardsMW-1,potablewatersupplywellswithin1,000feet,nomunicipalwatertosurroundingarea,nearbysurfacewaterreceptorsOctober18,20044.InformationabouttheMonitoringReportDate(s)ofGroundwaterMonitoringEvents(s):April27.20235.CertificationI,AlQuarles,aLicensedGeologistforATCAssociatesofNorthCarolina.P.C..docertifythattheinformationcontainedinthisreportiscorrectandaccuratetothebestofmyknowledge.ATCAssociatesofNorthCarolina.P.C.islicensedtopracticeengineeringandgeologyinNorthCarolina.ThecertificationnumberofthecompanyorcorporationforengineeringisC-1598.ThecertificationnumberofthecompanyorcorporationforgeologyisC-294.1
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) submits this Monitoring Report (MRP) documenting
the monitoring well sampling of MW-1 and MW-2 on April 27, 2023 at the Suttles Property site. The
report has been completed based on a April 17, 2023, Task Authorization (TA-05) by the Trust
Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste Management,
North Carolina Department of Environmental Quality (NCDEQ). The work was performed as part of
the State Lead Contract #N122019A between the NCDEQ and ATC.

As part of TA-05, ATC obtained groundwater samples from two monitoring wells, MW-1 and MW-2.
The samples were analyzed for Volatile Organic Compounds (VOCs) by Standard Method SM
6200B and for Volatile Petroleum Hydrocarbons (VPHs) by MADEP VPH. The following site
conditions are presented, based on the recent and historical assessment activities:

 Twelve drinking water supply wells were identified within 1,000 feet of the source area
(wells WSW-2, WSW-3, and WSW-7 within 250 feet). Additional water supply wells are
presumed to exist at occupied properties since municipal water is not available to the area.
One of the water supply wells (WSW-2) is a public water supply well that serves a
community center property north of the source area;
 Surface water bodies (tributaries of Newfound Creek) are located within 500 feet of the
source area, with the nearest approximately 75 feet west of the source area;
 No SM 6200B VOCs were detected above 15A NCAC 02L .0202 groundwater quality
standards (2L Standards) or the 15A NCAC 02B surface water standards (2B Standards)
by more than ten times in the groundwater sample collected from MW-1 and MW-2;
 ATC sampled WSW-2 and WSW-3. VOCs were not detected in the water supply well
samples. Water Supply well WSW-7 could not be accessed; and
 Based on limited historical gauging data from the two monitoring wells and proximity of
nearby tributaries, groundwater elevation contours flow cannot be estimated. However,
based on the groundwater elevations, groundwater flow is projected to be to the West -
northwest toward the nearby tributary.

The current Conceptual Site Model is included in Appendix A. Low-level groundwater impacts
above 2L Standards were previously detected in the groundwater sample from monitoring well
MW-1 where three gasoline USTs were historically located. Soil impacts exceeding Soil-to-
Water MSCCs (VPH and methyl isobutyl ketone a typical laboratory contaminant) were detected
in the soil sample near monitoring well MW-2 where the former dispenser island was located.
Additionally, VOCs have not been historically detected in nearby potable water supply wells.
Based on the recent groundwater sampling results and the Site Conceptual Model, ATC
recommends issuance of a Notice of No Further Action without restrictions.

3.0 SITE DESCRIPTION
3.1 Site Characterization
ATC, under contract to the NCDEQ, provided environmental consulting services at the Suttles
Property site, which is located at 1100 Newfound Road in Leicester, Buncombe County, North
Carolina. Figure 1 depicts the site on a topographic map. The site currently operates as an auto
repair and tire facility and is improved with a 2,394 square foot commercial building, storage shed,
and a mobile-home used as a residence by parcel owner Christopher James Suttles. Based on
receptor survey information collected during December 2020 Limited Site Assessment (LSA)
activities and previous sampling conducted by NCDEQ, twelve drinking water supply wells,
including one public water supply well, were identified within 1,000 feet of the source area.
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Additional drinking water supply wells are presumed to be present, since municipal water is not
available to the site and surrounding area. Figure 2 depicts the locations of water supply wells on
an aerial overlay. Information regarding the water supply wells is provided in Table 1. A Site Map
is presented as Figure 3.

3.2 Site Background
The former UST system at the 1100 Newfound Road property consisted of five gasoline USTs
ranging in size from 570 to 2,000 gallons, one approximate 430-gallon kerosene UST, dispenser
island, and product piping lines. The USTs were removed by Solutions Industrial &
Environmental Services (Solutions) in October 2004. During removal of the USTs, several holes
were observed in one of the gasoline tanks (UST-3) and the kerosene tank (UST-6).
Additionally, petroleum fuel odors were observed within the vicinity of gasoline tanks UST-1,
UST-2, and UST-3. Soil impacts were observed beneath each UST during tank removal
activities. Approximately 400 tons of impacted material was removed from the site.

Following the removal of the USTs, Solutions collected two closure soil samples beneath the
five gasoline tanks and one closure soil sample beneath the kerosene tank. Two additional
closure soil samples were collected from beneath the former dispenser island and product lines.
Closure soil samples were submitted for laboratory analysis of Total Petroleum Hydrocarbons
(TPH) Gasoline Range Organics (GRO) and Diesel Range Organics (DRO). Fifteen
confirmation samples were collected from beneath the dispenser island, product line, UST
bases, and UST sidewalls. Confirmation soil samples were submitted for laboratory analysis of
VOCs, semi-volatile organic compounds (SVOCs), volatile petroleum hydrocarbons (VPH),
extractable petroleum hydrocarbons (EPH), and lead.

Analytical results indicated that closure soil samples collected beneath UST-1, UST-2, UST-3,
UST-4, the dispenser island, and product line exceeded the UST Action Levels for TPH-GRO
and/or TPH-DRO which was 10 milligrams per kilogram (mg/kg). The UST Action Level for TPH-
GRO has since been increased to 50 mg/kg. TPH was not detected above laboratory method
detection limits in closure samples collected beneath UST-5 and UST-6. Analytical results
indicated that confirmation soil samples collected from the sidewalls of both UST excavations
had concentrations of various VOCs, SVOCs, VPH, and EPH compounds above their
respective Soil-to-Water Maximum Soil Contaminant Concentration Levels (MSCCs). Several
VOC compounds also exceeded Residential and Industrial/Commercial MSCCs in confirmation
soil samples collected.

Following tank closure activities, Solutions submitted a Tank Closure Report to the UST Section
on November 15, 2004. Additionally, five water supply wells (WSW-1, WSW-2, WSW-3, WSW-
4, and WSW-6) were sampled in January 2005 for analysis of VOCs. No VOCs were detected
above laboratory method detection limits. Based on the findings of tank closure activities and
water supply well sampling results, the UST Section requested an LSA be conducted in
accordance with UST Section guidelines in order to receive a No Further Action (NFA)
determination.

ATC submitted a Limited Site Assessment report to NCDEQ on February 18, 2021, which
documented LSA activities conducted at the site in December 2020. Assessment activities
included conducting a receptor survey within a 1,000 foot radius of the site and the installation
and sampling of two monitoring wells (MW-1 and MW-2). Twelve drinking water supply wells
were identified within 1,000 feet of the source area, three of which are within 250 feet. One of
the water supply wells (WSW-2) is a public water supply well that serves a community center
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property north of the source area. One of the wells (WSW-11) is inactive. ATC concluded that
additional water supply wells are presumed to exist at occupied properties since municipal water
is not available to the area. Concentrations of several VOCs including benzene, naphthalene, n-
propylbenzene, aliphatic carbon chain C5-C8, and aromatic carbon chain C9-C10 were
detected above 15A NCAC 02L .0202 Groundwater Quality Standards (2L Standards) in
monitoring well MW-1. No exceedances of 15A NCAC 2B Surface Water Quality Standards (2B
Standards) by more than ten times or the Gross Contaminant Levels (GCLs) were identified.

The responsible party for the release was identified as Christopher James Suttles, who is the
son of the late Forrest and Elaine Suttles, the previous property owners and UST operators for
the historical Suttles site operations. Several attempts were made by NCDEQ (formerly
NCDENR) between 2012 and 2019 requesting an affidavit for tank ownership to enter the site
into the State Lead Cleanup Program. Christopher James Suttles took ownership of the property
following the deaths of Forrest and Elaine Suttles. The site was accepted into the State Lead
Cleanup Program on October 14, 2020 based on the circumstances surrounding the original
property owner’s deaths, regulatory status, and inability to pay for assessment and remediation
activities.

ATC conducted soil assessment activities on April 14, 2021 which included the advancement of
two soil borings adjacent to monitoring wells MW-1 (SS-MW-1) and MW-2 (SS-MW-2) and a water
supply well sampling event for three water supply wells (WSW-2, WSW-3, and WSW-7). Soil
samples selected for laboratory analysis were from depth intervals that had the highest potential
for soil impacts based on visual and olfactory observations, as well as PID screening results.
Soil samples selected for laboratory analysis were collected from the 4 to 5 ft-bgs depth interval
in both soil borings. Several VOCs were detected above laboratory method detection limits in
the soil samples collected from soil borings SS-MW-1 and SS-MW-2. The detected
concentration of the VOC methyl isobutyl ketone (0.856 mg/kg) and aliphatic carbon chain C5-
C8 (96.3 mg/kg) in soil boring SS-MW-2 exceeded the Soil-to-Water MSCCs. No
concentrations of VOCs or VPH were detected above Residential or Industrial/Commercial
MSCCs. On April 14, 2021, ATC collected samples from water supply wells WSW-2, WSW-3, and
WSW-7. Analytical laboratory results indicated that VOCs were not detected above laboratory
method detection limits.

ATC conducted slug tests and monitoring well sampling on MW-1 and MW-2 and water supply well
sampling of WSW-7 on March 11, 2022 at the Suttles Property site. The water samples were
submitted to Pace Analytical and analyzed by SM 6200B for VOCs. The laboratory analytical report
indicated no VOCs were detected above 2L standards in MW-1, MW-2, and WSW-7. Slug testing
results indicated hydraulic conductivity values of 5.0 and 5.7 feet per day (ft/d) for MW-1 and MW-
2, respectively.

On July 19, 2022, ATC obtained depths to water and ATC collected groundwater samples from
MW-1 and MW-2. No SM 6200B VOCs were detected above 2L Standards or the 2B Standards by
more than ten times in the groundwater samples collected from MW-1 and MW-2. VPHs were
detected above the 2L Standards in the groundwater sample collected from MW-1; however, the
concentrations did not exceed the 2B standards by more than ten times.

3.3 Site and Regional Geology
According to the Geologic Map of North Carolina, produced by the North Carolina Geological
Survey and dated 1985, the site lies within the Ashe Metamorphic Suite of the Blue Ridge
Physiographic Province of North Carolina. The rock type in this area has been identified as
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

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magmatic biotite gneiss. The shallow subsurface in most areas of the Blue Ridge contains
residual soil overburden, including structure-free residuum, saprolite, and partially weathered
rock (PWR) that derive from in-place weathering of the crystalline bedrock. Occasional areas
containing recent deposits of alluvium in the uppermost subsurface are found near streams and
rivers. Saprolite and PWR typically contain some relict structures from the original rock material.
Depth to rock ranges from ground surface at occasional outcrops to depths of greater than 100
feet in areas of easily weathered rock.

Boring logs from the December 2020 LSA activities conducted at the site indicate that the
subsurface generally consists of gray to brown sandy clay saprolite (with residual rock structure)
to a depth of approximately 10 feet below ground surface (ft-bgs). Bedrock and PWR were not
encountered during LSA activities.

3.3 Site and Regional Hydrogeology
The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and
rivers to as deep as 50 feet or more beneath upland surfaces in some parts of the Blue Ridge.
Water in the alluvium or unconsolidated residual material, including saprolite and PWR, usually
behaves as an unconfined aquifer, or water table, and will yield water with head elevation
equivalent to the first elevation where water was encountered. Permeability varies with lithology
and is typically relatively low in residual soils, with higher permeability in saprolite or PWR due
to relict rock texture and variable susceptibility to weathering exhibited by different minerals in
the rock. Groundwater flow in residual soils or alluvium is usually in rough concurrence with
local topographic conditions and is toward local drainage features.

The bedrock fractures or other planar features of the Blue Ridge Physiographic Province
generally constitute the bedrock aquifer, with the surrounding rock material being effectively
impermeable. Along with fractures, contacts between rock bodies probably constitute zones of
significant groundwater occurrence in the bedrock. The surrounding material and overlying
residuum tend to make the bedrock aquifer a semi-confined aquifer. That is, the overlying water
and soil weight normally results in pressure that causes water in a borehole, which intersects a
fracture or other feature, to rise above the elevation of the fracture or feature. Modern water
supply wells in the Blue Ridge are typically installed with a surface casing through the
unconsolidated material, and an open borehole into the bedrock where water-bearing fractures
are encountered. Based on the groundwater levels measured at the site from monitoring wells
MW-1 and MW-2 and the nearby tributaries, the groundwater flow direction is anticipated to be
to the west-northwest in the western portion of the site, and to the north in the central and
eastern portions of the site.

4.0 GROUNDWATER CHARACTERIZATION
4.1 Groundwater Levels
On April 27, 2023, ATC obtained depths to water and total well depths from monitoring wells
MW-1 and MW-2. The depth to groundwater ranged from 3.25 ft-toc in MW-1 to 3.11 ft-toc in
MW-2. Depth to groundwater and elevation data are summarized in Table 2. The locations of
the monitoring wells and the groundwater elevations calculated for the monitoring wells are
indicated on Figure 4. Field notes are included in Appendix B.

Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

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4.2 Groundwater Quality
On April 27, 2023, ATC collected groundwater samples from MW-1 and MW-2. A three-volume
well purge was implemented prior to groundwater sample collection to ensure a representative
sample was collected. Upon completion of purging activities, water quality field parameters were
measured and are included in Table 3. ATC sampled water supply wells WSW-2 and WSW-3
during the sampling event and attempted to sample WSW-7; however, no one was present at the
residence and the phone number for the property owner was no longer in service.

The water samples were collected in laboratory-supplied, preserved containers, entered into chain-
of-custody control, placed on ice, and delivered to Pace Analytical in Huntersville, North Carolina.
The groundwater samples were analyzed by SM 6200B and MADEP VPH. The analytical report is
included as Appendix C. The results are summarized in Table 4 and presented on Figure 5. The
groundwater analytical results were compared to the 2L Standards, 2B Standards, and GCLs. The
groundwater analytical results indicated the following:

 No SM 6200B VOCs were detected above 2L Standards or the 2B Standards by more than
ten times in the groundwater samples collected from MW-1 and MW-2; and
 VOCs were not detected in samples from WSW-2 and WSW-3.

4.5 Quality Assurance and Quality Control
As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of the
laboratory report was conducted. During the review, it was found that the samples were received
from the laboratory in acceptable condition and properly preserved. The samples were analyzed
within correct holding times and reported within the laboratory report, and the chain-of-custody was
properly completed by all parties. The laboratory QC report shows that an internal blank was
analyzed for SM 6200B. The laboratory fortified blank (LFB) and laboratory control sample (LCS)
data results were also provided for SM 6200B. A field blank (FB-1) was also analyzed during the
groundwater monitoring event and constituents were not detected in the field blank. Refer to the
laboratory report in Appendix B for details regarding QA results for the laboratory samples and
any noted exceptions. Overall, ATC concludes that the laboratory results are usable and any
exceptions do not significantly impact the conclusions presented in this report.

5.0 CONCLUSIONS AND RECOMMENDATIONS
On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Groundwater
Monitoring Report documenting monitoring well sampling activities for the Suttles Property site,
located at 1100 Newfound Road in Leicester, Buncombe County, North Carolina. The following
site conditions are presented, based on the recent and historical assessment activities:

 Twelve drinking water supply wells were identified within 1,000 feet of the source area
(wells WSW-2, WSW-3, and WSW-7 within 250 feet). Additional water supply wells are
presumed to exist at occupied properties since municipal water is not available to the area.
One of the water supply wells (WSW-2) is a public water supply well that serves a
community center property north of the source area;
 Surface water bodies (tributaries of Newfound Creek) are located within 500 feet of the
source area, with the nearest approximately 75 feet west of the source area;
 ATC sampled WSW-2 and WSW-3. VOCs were not detected in the water supply well
samples. Water Supply well WSW-7 could not be accessed;
 No SM 6200B VOCs were detected above 2L Standards or the 2B Standards by more than
ten times in the groundwater sample collected from MW-1 and MW-2; and
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 Based on limited historical gauging data from the two monitoring wells and proximity of
nearby tributaries, groundwater elevation contours flow cannot be estimated. However,
based on the groundwater elevations, groundwater flow is projected to be to the west-
northwest toward the nearby tributary.

Based on the recent groundwater sampling results and the Site Conceptual Model, ATC
recommends issuance of a Notice of No Further Action without restrictions.
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

TABLES
Well ID Parcel ID Well Owner Property Address Owner Address Phone Number
(if available)Well Use
Distance (feet)
and Direction from
Source Area
WSW-1 869905864100000 Connie Young
Sherman Young
1108 Newfound Rd
Leicester, NC 28748
185 Mount Carmel Rd
Asheville, NC 28806 Drinking 320 SW
WSW-2 869906817500000
Newfound
Community Club
Attn: Anthony Cole
3 Morgan Branch Rd
Leicester, NC 28748
1346 Newfound Rd
Leicester, NC 28748 Drinking 250 NNW
WSW-3 *869915296400000 Katherine Towles
Michael Towles
1090 Newfound Rd
Leicester, NC 28748
38 Hayes Cove Rd
Leicester, NC 28748 [phone] Drinking 260 NE
WSW-4 869905678200000 Terry Bros
Construction Co Inc
1109 Newfound Rd
Leicester, NC 28748
1109 Newfound Rd
Leicester, NC 28748 Drinking 280 W
WSW-5 *869916233500000
Leicester Volunteer
Fire Dept
Attn: Ted Godleski
1075 Newfound Rd
Leicester, NC 28748
PO Box 100
Leicester, NC 28748 [phone] Drinking
Washing Firetrucks 550 NE
WSW-6 869915174000000 Joseph H Bradburn
Sara E Bradburn
10 Hookers Gap Rd
Leicester, NC 28748
10 Hookers Gap Rd
Leicester, NC 28748 Drinking 170 S
WSW-7 869915181300000 Christopher J.
Suttles
1100 New Found Rd
Leicester, NC 28747
1100 New Found Rd
Leicester, NC 28747 [phone] Drinking 85 SE
Source Property
869915340800000 99999 Hookers Gap Rd
Leicester, NC 28748
869915134700000 18 Hookers Gap Rd
Leicester, NC 28748
Suttles Property
WATER SUPPLY WELL INFORMATION
TABLE 1
NCDEQ Incident # 28266
Leicester, Buncombe County, North Carolina
1100 Newfound Road
18 Hookers Gap Rd
Leicester, NC 28748 [phone]Freda Ann Nodine
Donnie L NodineWSW-8 *Drinking 350 SSE
Page 1 of 2
Well ID Parcel ID Well Owner Property Address Owner Address Phone Number
(if available)Well Use
Distance (feet)
and Direction from
Source Area
Suttles Property
WATER SUPPLY WELL INFORMATION
TABLE 1
NCDEQ Incident # 28266
Leicester, Buncombe County, North Carolina
1100 Newfound Road
869905618400000 1122 Hookers Gap Rd
Leicester, NC 28748
869905636200000 1124 Newfound Rd
Leicester, NC 28748
869905360600000 50 Morgan Branch Rd
Leicester, NC 28748
WSW-10 *869904884800000 Mark Douglas
Blondin
41 Hookers Gap Rd
Leicester, NC 28748
41 Hookers Gap Rd
Leicester, NC 28748 [phone] Drinking
Irrigation 620 SSW
WSW-11 *869905649700000 David Hyatt
Mary Hyatt
1120 Newfound Rd
Leicester, NC 28748
1244 Newfound Rd
Leicester, NC 28748 [phone] Inactive
since 1988 500 SW
WSW-12 *869926206400000 Carroll E Shook
Trust
1064 Newfound Rd
Leicester, NC 28748
38 Hayes Cove Rd
Leicester, NC 28748 [phone] Drinking 950 NE
Notes:
Water supply well information based on ATC's December 23, 2020 survey and from prior assessment by NCDEQ.
Additional water supply wells are presumed to be present at other occupied properties not indicated above, since municipal water is not available to the area.
* = Water Supply Well Questionnaires returned.
Susan Holt
Michael HoltWSW-9 *1124 Newfound Rd
Leicester, NC 28748 [phone] Drinking
Livestock 520 SW
Page 2 of 2
Well ID Date
Installed
Well Casing
Diameter
(in)
Screen
Interval
(ft-TOC)
TOC
Elevation
(ft)
Date
Measured
Depth to
LNAPL
(ft-TOC)
LNAPL
Thickness
(ft)
Depth to
Groundwater
(ft-TOC)
Groundwater
Elevation
(ft)
12/30/20 ----2.95 97.05
03/11/22 ----2.58 97.42
07/19/22 ----3.64 96.36
04/27/23 ----3.25 96.75
12/30/20 ----2.93 95.95
03/11/22 ----2.64 96.24
07/19/22 ----3.61 95.27
04/27/23 ----3.11 95.77
Notes:
in = inches
ft-TOC = feet below top of casing (TOC)
ft = feet
LNAPL = Light Non-Aqueous Phase Liquid
TOC = top of casing
-- = Not Applicable, no LNAPL observed in well
TABLE 2
MONITORING WELL CONSTRUCTION AND WATER LEVEL ELEVATION DATA
Leicester, Buncombe County, North Carolina
1100 Newfound Road
Suttles Property
NCDEQ Incident # 28266
MW-1 12/02/20 2 4.5-9.5 100.00
MW-2 12/02/20 2 4.5-9.5 98.88
Page 1 of 1
12/30/20 11.40 0.39 -76 4.8 6.6
3/11/22 17.31 0.40 85 1.2 5.9
7/19/22 21.21 0.51 -78 1.1 --
4/27/23 16.41 0.40 205 9.5 4.5
12/30/20 10.10 0.30 -33 0.0 6.6
03/11/22 16.10 0.33 -46 1.8 6.5
07/19/22 21.65 0.31 -58 1.2 --
4/27/23 14.12 0.30 -60 6.4 6.0
03/11/22
4/27/23 15.82 0.15 -6.0 8.6 5.7
03/11/22
4/27/23 15.28 0.16 43 13.8 6.0
03/11/22 17.95 0.22 276 7.5 5.0
04/27/23
Notes:
°C = degrees Celsius -- = Instrument Error
mS/cm = milliSiemens per centimeter
ORP = Oxidation Reduction Potential
mV = millivolts
mg/L = milligrams per liter
s.u. = standard units
NS = Not Sampled
Temperature
(°C)
WSW-2
ORP
(mV)
Leicester, Buncombe County, North Carolina
NCDEQ Incident # 28266
TABLE 3
WATER QUALITY PARAMETERS
Suttles Property
1100 Newfound Road
Well ID Date
WSW-3
WSW-7
No Access
No Access
No Access
Conductivity
(mS/cm)
Dissolved
Oxygen
(mg/L)
pH
(s.u.)
MW-1
MW-2
Page 1 of 1
6010
Well ID Date Collected
BenzeneTolueneEthylbenzeneXylenes (total)Naphthalene1,2-Dibromomethane(EDB)*Isopropylbenzenen-Butylbenzenen-Propylbenzenesec-Butylbenzenetert-ButylbenzeneMethyl-tert-butyl-ether (MTBE)Aliphatic (C5-C8)Aliphatic (C9-C12)Aromatic (C9-C10)Lead1 600 600 500 6 0.02 70 70 70 70 70 20 400 700 200 15
51 11 97 670 12 0.1 250 3.9 80 NE NE 1,500 125 180 4000 30
5,000 260,000 80,000 50,000 6,000 50 30,500 5,900 26,100 8,800 14,750 20,000 NE NE NE 15,000
12/30/20 1.3 1.1 11.1 2.6 72.8 <0.011*54.4 11.3 141 15.3 0.49 J NA 637 587 693 <4.5
03/11/22 <0.50 <0.50 0.50J <1.0 4.9 <0.50 8.9 <0.50 9.6 3.0 <0.50 NA NA NA NA NA
07/19/22 <0.34 <0.48 0.61 <0.34 5.8 <0.27 11.1 <0.49 11.2 3.8 <0.32 <0.42 290 141 222 NA
04/27/23 <0.34 <0.24 0.43J <1.05 5.7 <0.27 11.0 <0.49 19.1 2.2 <0.32 <0.42 197J 321J <167 NA
12/30/20 <0.24 <0.23 <0.24 <0.50 <0.66 <0.011*<0.24 <0.35 <0.24 <0.25 <0.25 NA <33.3 <33.3 35.5 J <4.5
03/11/22 <0.5 <.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA
07/19/22 <0.34 <0.48 <0.30 <0.34 <0.64 <0.27 <0.33 <0.49 <0.34 <0.40 <0.32 0.47J <50.0 <50.0 <50.0 NA
04/27/23 <0.34 <0.24 <0.30 <1.05 <0.64 <0.27 <0.33 <0.49 <0.34 <0.40 <0.32 0.47J N/A N/A N/A NA
WSW-2 04/27/23 <0.34 <0.24 <0.30 <1.05 <0.64 <0.27 <0.33 <0.49 <0.34 <0.40 <0.32 <0.42 N/A N/A N/A N/A
WSW-3 04/27/23 <0.34 <0.24 <0.30 <1.05 <0.64 <0.27 <0.33 <0.49 <0.34 <0.40 <0.32 <0.42 N/A N/A N/A N/A
03/11/22 <0.50 <0.50 <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA
04/27/23
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) 15A NCAC 2L .0202 Groundwater Quality Standard (2L Standard).
2) NCDEQ Division of Waste Management (DWM) Underground Storage (UST) Section Gross Contaminant Levels (GCL) for Groundwater.
3) NCDEQ 15A NCC 2B Water Quality Standards for Surface Waters (Class C), lead calculated based on assumed hardness of 50 mg/L and for acute exposure
Only constituents detected above the laboratory method detection limit are shown
All concentrations reported in micrograms per liter (µg/L)VOC = Volatile Organic Compound
Bold concentrations indicate an exceedance of the 2L Standard VPH = Volatile Petroleum Hydrocarbon
Bold underlined concentrations indicate an exceedance of the 2B Standard by more than 10 times MADEP = Massachussetts Department of Environmental Protection
Bold italicized concentrations indicate an exceedance of the GCL NE = Not Established
<# = Less than method detection limit NS = Not Sampled
J = concentration was detected between the reporting limit and method detection limit NA = Not Analyzed
WSW-7
No Access
VPH (MADEP)
2L Standard (1)
2B Standard (3)
GCL(2)
VOCs (6200B/504.1*)
MW-1
MW-2
TABLE 4
MONITORING WELL ANALYTICAL RESULTS
Suttles Property
1100 Newfound Road
Leicester, Buncombe County, North Carolina
NCDEQ Incident # 28266
Page 1 of 1
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

FIGURES

1"= 2,000'
1
Project Number:
Date:Scale:
Drawing File:
Figure:
App'd By:
Drn. By:
Ckd. By:
N
LATITUDE: N 35° 36' 16.26"
LONGITUDE: W 82° 43' 53.79"
USGS 7.5-MINUTE TOPOGRAPHIC MAP; LEICESTER, NC QUADRANGLE 2000; SCALE 1:24,000
H:\2021\OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\SUTTLES PROPERTY\SLC2826602-VIC.DWG, FIG105/14/2021
SEE LOWER LEFT
SLC2826602 DH
SS
SS
NCDEQ INCIDENT #28266
LEICESTER, NORTH CAROLINA
1100 NEWFOUND ROAD
SUTTLES PROPERTY
VICINITY MAP
WSW-10
WSW-9WSW-11WSW-1WSW-8WSW-6WSW-7WSW-2WSW-3WSW-5WSW-12500 FT.RADIUS1,000 FT.RADIUS1,500 FT.RADIUSMORGAN BRANCH ROADN
EW
F
O
UN
D
R
O
A
D
S
T
I
L
L
H
O
U
S
E

B
R
A
N
C
H

R
O
A
D
BROOKS BRANCH ROADHOOKERS GAP ROADSITELEGEND:SITE PROPERTY LINENOTE: ALL LOCATIONS ARE APPROXIMATEPARCEL LINESTREAM/SURFACE WATER BODIESWSW-11INACTIVE WATER SUPPLY WELLWell IdentificationNEWFOUNDCREEKTRIBUTARY TONEWFOUND CREEKTRIBUTARY TONEWFOUND CREEKWSW-1ACTIVE DRINKING WATER SUPPLY WELLSWell IdentificationWSW-4Figure:Drawing File:
Project Number:
Ckd. By:
Drn. By:
App'd By:
Ckd. Date:Scale:Date:H:\2021\OTHER OFFICES\NORTH CAROLINA\NCDEQ-STATE LEAD\SUTTLES PROPERTY\SLC2826602-WSW.DWG, FIG2
WATER SUPPLY WELL LOCATION MAP05/19/2021SEE LOWER LEFTSUTTLES PROPERTY
1100 NEWFOUND ROAD
LEICESTER, NORTH CAROLINA
NCDEQ INCIDENT #28266
SLC2826602AS SHOWNDH
SS2NOTES:
1.Features shown are not an authoritative location, nor are they presented
to a stated accuracy.
COORDINATE SYSTEM:
NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET
WSW-6WSW-7MORGAN BRANCH ROADNEWFOUND R
O
A
DAUTO REPAIR ANDTIRE FACILITYLEGEND:SITE PROPERTY LINENOTE: ALL LOCATIONS ARE APPROXIMATEPARCEL LINESTREAM/SURFACE WATER BODIESWSW-7ACTIVE DRINKING WATER SUPPLY WELLWell IdentificationTRIBUTARY TONEWFOUND CREEKMOB
I
L
E
-
HOM
ERESIDE
NCESHEDFORMERASTFORMERKEROSENE UST (#6)(2) FORMERGASOLINE USTS(#1 AND #2)FORMERDISPENSERISLAND(3) FORMER GASOLINE USTS(#3, #4, AND #5)MW-1MONITORING WELLWell IdentificationMW-2MW-1Figure:Drawing File:
App'd By:
Ckd. Date:Scale:Date:AS SHOWN3NOTES:
1.Features shown are not an authoritative location, nor are they presented
to a stated accuracy.
COORDINATE SYSTEM:
NAD 1983 NORTH CAROLINA STATE PLANE FIPS 3200, US SURVEY FEET

LB
Drn. By:

NCDEQ INCIDENT #28266
LEICESTER, NORTH CAROLINA
1100 NEWFOUND ROAD
SUTTLES PROPERTY
SITE MAP
KH
Ckd. By:
SLC2826604
Project Number: 08/08/2022
WSW-7
FORMERASTAUTO REPAIR ANDTIRE FACILITYFORMERKEROSENE USTFORMERGASOLINE USTFORMERDISPENSER ISLANDGASOLINEUST BASINMOT
OR
HOM
E
R
ES
IDE
N
CE
NEWF
O
U
N
D

R
O
A
DMORGAN BRANCH ROADMW-1MW-2TRIBUTARY TONEWFOUND CREEK= GROUNDWATER ELEVATION IN FEET= MONITORING WELL LOCATION96.7595.7782.87= ACTIVE WATER SUPPLY WELL LOCATION
WSW-7
FORMERASTAUTO REPAIR ANDTIRE FACILITYFORMERKEROSENE USTFORMERGASOLINE USTFORMERDISPENSER ISLANDGASOLINEUST BASINMOT
OR
HOM
E
R
ES
IDE
N
CE
NEWF
O
U
N
D

R
O
A
DMORGAN BRANCH ROADMW-1MW-2TRIBUTARY TONEWFOUND CREEK= MONITORING WELL LOCATION= ACTIVE WATER SUPPLY WELL LOCATION
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

APPENDIX A

CONCEPTUAL SITE MODEL
Site Name: Suttles Property Date:6/6/2023
Property Owner:Last Field Event Date:4/27/2023
Site Name:Suttles Property Release Discovery Date:10/18/2004
NCDEQ UST Incident No.:28266 Source of Release:UST corrosion, possible others
Facility ID No.:00-0-0000003057 Estimated Volume of Release:Unknown
Risk Classification:High
Risk Rank:100D Gasoline (leaded)
Site Address:100 Newfound Road Gasoline (unleaded)Yes
Site City, ST ZIP:Leicester Gasoline (ethanol blend)
Site County:Buncombe Diesel
NCDEQ Regional Office:Asheville Kerosene Yes
Active UST Facility:No Heating Oil (#2)
USTs Present:No Heating Oil (>#2)
Motor Oil
Hydraulic Oil
Major Soil Type:Used Oil
Surface Cover over impacted soil:
Utilities within plume (Y/N/U):
>S-W MSCCs (Y/N/U):
>Residential MSCCs (Y/N/U):Site (Current):Commercial/Residential
>Comm/Ind MSCCs (Y/N/U):Site (Future):Commercial/Residential
North Adjacent:Community Center
East Adjacent:Residential
Litho-Tectonic Zone Blue Ridge South Adjacent:Residential
Geologic Formation Ashe Metamorphic Suite West Adjacent:Residential
Rock Type Magmatic biotite gneiss
Depth to Bedrock (ft bgs)>10 Municipal Water (Y/N/U):N
Active Potable Wells <1000 ft (#/U):Y
Active Potable Wells <500 ft (#/U):Y, 8 inc. Public well ~250 ft
Depth to water (ft-bgs)~3-4 ft bgs Impacted Wells (Y/N/U):No
Gradient (ft/ft):U Any wells <250 ft (Y/N/U):Y, 3
Direction (N E S W combo):NW-WNW
Hydraulic Conductivity (ft/day):U <500 ft (Y/N):Y
Total Porosity (%):U Type of Surface Water:Stream
Effective Porosity (%):U Name of Nearest Stream:Tributary to Newfound Creek
Flow Rate (ft/year):U Stream Classification:C
COCs >2L (Y/N/U):N Impacted Surface Water (Y/N/U):Unknown, but not likely
COCs >2L Extent Defined (Y/N):N
COCs >GCLs (Y/N/U):N
COCs >GCLs (Wells):NA >LEL in Structures:U
COCs >GCLs Extent Defined (Y/N):NA Vapors in Buildings:U
COCs >2B Standards by 10X (Y/N/U):N Slab-on-grade or Crawlspace:Not likely
LNAPL (Y/N/U):N Dissolved VOCs <5 ft of Structures:N
LNAPL (Max Thickness ft):NA LNAPL <15 ft of Structures:NA
LNAPL (Wells):NA Basement <30 ft of Dissolved COCs:N
LNAPL Extent Defined (Y/N):NA
LNAPL (<5 ft beneath buildings/U):NA
Utilities within plume (Y/N/U):N
Alternative Water Source:
NORP:
Site Remediation:
Soil Excavation:
AFVR:
MMPE:
SVE/AS:
Other:
CONCEPTUAL SITE MODEL
Soil Information
Possible Path(s) to Closure
Site Information Release Information
Petroleum Type Released
Geologic Information
Groundwater Information
Comments:
Receptor Information
Water Supply
Vapor
Additional Support Documentation Available / Data Gaps:
Approach (general discussion):No 2L exceedances, clean closure
Surface Water
Land Use / Zoning
Page 1 of 1
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

APPENDIX B

FIELD NOTES
Monitoring Report June 21, 2023
Suttles Property, NCDEQ Incident #28266 ATC Project #SLC2826605

APPENDIX C

LABORATORY ANALYTICAL REPORT
#=CL#
May 04, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92664647
92664647
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
SUTTLES PROPERTY
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on April 27, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Lab ID Sample ID Matrix Date Collected Date Received
92664647001 MW1 Water 04/27/23 10:50 04/27/23 15:05
92664647002 MW2 Water 04/27/23 11:10 04/27/23 15:05
92664647003 WSW2 Water 04/27/23 11:40 04/27/23 15:05
92664647004 WSW3 Water 04/27/23 12:15 04/27/23 15:05
92664647005 FB Water 04/27/23 11:30 04/27/23 15:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92664647001 MW1 MADEP VPH 6 PANADM
EPA 8270E 21 PASI-CPKS
SM 6200B 69 PASI-CSAS
92664647002 MW2 SM 6200B 69 PASI-CSAS
92664647003 WSW2 SM 6200B 69 PASI-CSAS
92664647004 WSW3 SM 6200B 69 PASI-CSAS
92664647005 FB SM 6200B 69 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:MW1 Lab ID:92664647001 Collected:04/27/23 10:50 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)197J ug/L 05/03/23 02:01 J05/03/23 02:015001675
Aliphatic (C09-C12)321J ug/L 05/03/23 02:01 J05/03/23 02:015001675
Aromatic (C09-C10),Unadjusted <167 ug/L 05/03/23 02:01 TPHC9C10A05/03/23 02:015001675
Total VPH 518 ug/L 05/03/23 02:01 VPH05/03/23 02:015001675
Surrogates
2,5-Dibromotoluene (FID)72.8 %05/03/23 02:01 615-59-8FID05/03/23 02:0170.0-130 5
2,5-Dibromotoluene (PID)76.0 %05/03/23 02:01 615-59-8PID05/03/23 02:0170.0-130 5
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene <3.1 ug/L 05/01/23 18:55 83-32-905/01/23 15:229.6 3.1 1
Acenaphthylene <3.7 ug/L 05/01/23 18:55 208-96-805/01/23 15:229.6 3.7 1
Anthracene <3.7 ug/L 05/01/23 18:55 120-12-705/01/23 15:229.6 3.7 1
Benzo(a)anthracene <3.9 ug/L 05/01/23 18:55 56-55-305/01/23 15:229.6 3.9 1
Benzo(a)pyrene <3.5 ug/L 05/01/23 18:55 50-32-805/01/23 15:229.6 3.5 1
Benzo(b)fluoranthene <3.8 ug/L 05/01/23 18:55 205-99-205/01/23 15:229.6 3.8 1
Benzo(g,h,i)perylene <3.6 ug/L 05/01/23 18:55 191-24-205/01/23 15:229.6 3.6 1
Benzo(k)fluoranthene <3.5 ug/L 05/01/23 18:55 207-08-905/01/23 15:229.6 3.5 1
Chrysene <3.3 ug/L 05/01/23 18:55 218-01-905/01/23 15:229.6 3.3 1
Dibenz(a,h)anthracene <4.2 ug/L 05/01/23 18:55 53-70-305/01/23 15:229.6 4.2 1
Fluoranthene <3.2 ug/L 05/01/23 18:55 206-44-005/01/23 15:229.6 3.2 1
Fluorene <3.1 ug/L 05/01/23 18:55 86-73-705/01/23 15:229.6 3.1 1
Indeno(1,2,3-cd)pyrene <3.9 ug/L 05/01/23 18:55 193-39-505/01/23 15:229.6 3.9 1
1-Methylnaphthalene <3.5 ug/L 05/01/23 18:55 90-12-005/01/23 15:229.6 3.5 1
2-Methylnaphthalene <3.3 ug/L 05/01/23 18:55 91-57-605/01/23 15:229.6 3.3 1
Naphthalene 4.7J ug/L 05/01/23 18:55 91-20-305/01/23 15:229.6 3.0 1
Phenanthrene <3.3 ug/L 05/01/23 18:55 85-01-805/01/23 15:229.6 3.3 1
Pyrene <3.7 ug/L 05/01/23 18:55 129-00-005/01/23 15:229.6 3.7 1
Surrogates
Nitrobenzene-d5 (S)114 %05/01/23 18:55 4165-60-005/01/23 15:2259-144 1
2-Fluorobiphenyl (S)83 %05/01/23 18:55 321-60-805/01/23 15:2257-152 1
Terphenyl-d14 (S)84 %05/01/23 18:55 1718-51-005/01/23 15:2210-162 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/02/23 10:54 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/02/23 10:54 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/02/23 10:54 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/02/23 10:54 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/02/23 10:54 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/02/23 10:54 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/02/23 10:54 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/02/23 10:54 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/02/23 10:54 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/02/23 10:54 104-51-80.50 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:MW1 Lab ID:92664647001 Collected:04/27/23 10:50 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
sec-Butylbenzene 2.2 ug/L 05/02/23 10:54 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/02/23 10:54 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/02/23 10:54 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/02/23 10:54 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/02/23 10:54 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/02/23 10:54 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 05/02/23 10:54 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/02/23 10:54 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/02/23 10:54 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/02/23 10:54 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/02/23 10:54 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/02/23 10:54 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/02/23 10:54 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/02/23 10:54 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/02/23 10:54 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/02/23 10:54 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/02/23 10:54 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/02/23 10:54 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/02/23 10:54 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/02/23 10:54 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/02/23 10:54 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/02/23 10:54 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/02/23 10:54 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/02/23 10:54 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/02/23 10:54 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/02/23 10:54 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/02/23 10:54 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/02/23 10:54 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/02/23 10:54 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/02/23 10:54 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/02/23 10:54 64-17-520072.2 1
Ethylbenzene 0.43J ug/L 05/02/23 10:54 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/02/23 10:54 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/02/23 10:54 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)11.0 ug/L 05/02/23 10:54 98-82-80.50 0.33 1
Methylene Chloride <2.0 ug/L 05/02/23 10:54 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/02/23 10:54 1634-04-40.50 0.42 1
Naphthalene 5.7 ug/L 05/02/23 10:54 91-20-32.0 0.64 1
n-Propylbenzene 19.1 ug/L 05/02/23 10:54 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/02/23 10:54 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/02/23 10:54 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/02/23 10:54 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/02/23 10:54 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/02/23 10:54 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/02/23 10:54 87-61-62.0 0.81 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:MW1 Lab ID:92664647001 Collected:04/27/23 10:50 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,4-Trichlorobenzene <0.64 ug/L 05/02/23 10:54 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/02/23 10:54 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/02/23 10:54 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/02/23 10:54 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/02/23 10:54 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/02/23 10:54 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/02/23 10:54 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/02/23 10:54 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/02/23 10:54 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/02/23 10:54 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/02/23 10:54 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %05/02/23 10:54 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/02/23 10:54 460-00-470-130 1
Toluene-d8 (S)101 %05/02/23 10:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:MW2 Lab ID:92664647002 Collected:04/27/23 11:10 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/02/23 11:12 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/02/23 11:12 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/02/23 11:12 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/02/23 11:12 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/02/23 11:12 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/02/23 11:12 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/02/23 11:12 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/02/23 11:12 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/02/23 11:12 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/02/23 11:12 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/02/23 11:12 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/02/23 11:12 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/02/23 11:12 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/02/23 11:12 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/02/23 11:12 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/02/23 11:12 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 05/02/23 11:12 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/02/23 11:12 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/02/23 11:12 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/02/23 11:12 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/02/23 11:12 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/02/23 11:12 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/02/23 11:12 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/02/23 11:12 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/02/23 11:12 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/02/23 11:12 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/02/23 11:12 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/02/23 11:12 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/02/23 11:12 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/02/23 11:12 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/02/23 11:12 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/02/23 11:12 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/02/23 11:12 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/02/23 11:12 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/02/23 11:12 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/02/23 11:12 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/02/23 11:12 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/02/23 11:12 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/02/23 11:12 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/02/23 11:12 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/02/23 11:12 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/02/23 11:12 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/02/23 11:12 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/02/23 11:12 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/02/23 11:12 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:MW2 Lab ID:92664647002 Collected:04/27/23 11:10 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/02/23 11:12 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.47J ug/L 05/02/23 11:12 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/02/23 11:12 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/02/23 11:12 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/02/23 11:12 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/02/23 11:12 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/02/23 11:12 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/02/23 11:12 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/02/23 11:12 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/02/23 11:12 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/02/23 11:12 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/02/23 11:12 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/02/23 11:12 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/02/23 11:12 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/02/23 11:12 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/02/23 11:12 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/02/23 11:12 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/02/23 11:12 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/02/23 11:12 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/02/23 11:12 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/02/23 11:12 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %05/02/23 11:12 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %05/02/23 11:12 460-00-470-130 1
Toluene-d8 (S)101 %05/02/23 11:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:WSW2 Lab ID:92664647003 Collected:04/27/23 11:40 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/03/23 16:43 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/03/23 16:43 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/03/23 16:43 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/03/23 16:43 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/03/23 16:43 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/03/23 16:43 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/03/23 16:43 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/03/23 16:43 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/03/23 16:43 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/03/23 16:43 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/03/23 16:43 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/03/23 16:43 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/03/23 16:43 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/03/23 16:43 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/03/23 16:43 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/03/23 16:43 75-00-3 M11.0 0.65 1
Chloroform <0.43 ug/L 05/03/23 16:43 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/03/23 16:43 74-87-3 M11.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/03/23 16:43 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/03/23 16:43 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/03/23 16:43 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/03/23 16:43 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/03/23 16:43 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/03/23 16:43 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/03/23 16:43 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/03/23 16:43 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/03/23 16:43 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/03/23 16:43 75-71-8 IH,M10.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/03/23 16:43 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/03/23 16:43 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/03/23 16:43 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/03/23 16:43 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/03/23 16:43 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/03/23 16:43 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/03/23 16:43 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/03/23 16:43 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/03/23 16:43 563-58-6 M10.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/03/23 16:43 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/03/23 16:43 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/03/23 16:43 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/03/23 16:43 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/03/23 16:43 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/03/23 16:43 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/03/23 16:43 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/03/23 16:43 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:WSW2 Lab ID:92664647003 Collected:04/27/23 11:40 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/03/23 16:43 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/03/23 16:43 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/03/23 16:43 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/03/23 16:43 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/03/23 16:43 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/03/23 16:43 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/03/23 16:43 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/03/23 16:43 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/03/23 16:43 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/03/23 16:43 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/03/23 16:43 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/03/23 16:43 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/03/23 16:43 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/03/23 16:43 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/03/23 16:43 75-69-4 M11.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/03/23 16:43 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/03/23 16:43 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/03/23 16:43 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/03/23 16:43 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/03/23 16:43 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/03/23 16:43 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %05/03/23 16:43 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/03/23 16:43 460-00-470-130 1
Toluene-d8 (S)108 %05/03/23 16:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:WSW3 Lab ID:92664647004 Collected:04/27/23 12:15 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/03/23 17:01 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/03/23 17:01 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/03/23 17:01 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/03/23 17:01 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/03/23 17:01 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/03/23 17:01 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/03/23 17:01 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/03/23 17:01 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/03/23 17:01 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/03/23 17:01 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/03/23 17:01 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/03/23 17:01 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/03/23 17:01 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/03/23 17:01 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/03/23 17:01 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/03/23 17:01 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 05/03/23 17:01 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/03/23 17:01 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/03/23 17:01 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/03/23 17:01 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/03/23 17:01 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/03/23 17:01 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/03/23 17:01 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/03/23 17:01 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/03/23 17:01 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/03/23 17:01 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/03/23 17:01 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/03/23 17:01 75-71-80.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/03/23 17:01 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/03/23 17:01 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/03/23 17:01 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/03/23 17:01 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/03/23 17:01 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/03/23 17:01 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/03/23 17:01 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/03/23 17:01 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/03/23 17:01 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/03/23 17:01 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/03/23 17:01 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/03/23 17:01 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/03/23 17:01 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/03/23 17:01 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/03/23 17:01 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/03/23 17:01 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/03/23 17:01 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:WSW3 Lab ID:92664647004 Collected:04/27/23 12:15 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/03/23 17:01 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/03/23 17:01 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/03/23 17:01 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/03/23 17:01 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/03/23 17:01 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/03/23 17:01 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/03/23 17:01 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/03/23 17:01 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/03/23 17:01 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/03/23 17:01 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/03/23 17:01 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/03/23 17:01 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/03/23 17:01 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/03/23 17:01 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/03/23 17:01 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/03/23 17:01 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/03/23 17:01 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/03/23 17:01 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/03/23 17:01 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/03/23 17:01 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/03/23 17:01 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %05/03/23 17:01 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/03/23 17:01 460-00-470-130 1
Toluene-d8 (S)110 %05/03/23 17:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:FB Lab ID:92664647005 Collected:04/27/23 11:30 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/02/23 03:34 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/02/23 03:34 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/02/23 03:34 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/02/23 03:34 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/02/23 03:34 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/02/23 03:34 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/02/23 03:34 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/02/23 03:34 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/02/23 03:34 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/02/23 03:34 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/02/23 03:34 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/02/23 03:34 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/02/23 03:34 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/02/23 03:34 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/02/23 03:34 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/02/23 03:34 75-00-31.0 0.65 1
Chloroform <0.43 ug/L 05/02/23 03:34 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/02/23 03:34 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/02/23 03:34 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/02/23 03:34 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/02/23 03:34 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/02/23 03:34 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/02/23 03:34 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/02/23 03:34 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/02/23 03:34 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/02/23 03:34 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/02/23 03:34 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/02/23 03:34 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/02/23 03:34 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/02/23 03:34 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/02/23 03:34 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/02/23 03:34 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/02/23 03:34 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/02/23 03:34 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/02/23 03:34 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/02/23 03:34 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/02/23 03:34 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/02/23 03:34 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/02/23 03:34 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/02/23 03:34 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/02/23 03:34 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/02/23 03:34 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/02/23 03:34 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/02/23 03:34 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/02/23 03:34 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Sample:FB Lab ID:92664647005 Collected:04/27/23 11:30 Received:04/27/23 15:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/02/23 03:34 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/02/23 03:34 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/02/23 03:34 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/02/23 03:34 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/02/23 03:34 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/02/23 03:34 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/02/23 03:34 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/02/23 03:34 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/02/23 03:34 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/02/23 03:34 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/02/23 03:34 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/02/23 03:34 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/02/23 03:34 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/02/23 03:34 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/02/23 03:34 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/02/23 03:34 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/02/23 03:34 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/02/23 03:34 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/02/23 03:34 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/02/23 03:34 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/02/23 03:34 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %05/02/23 03:34 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/02/23 03:34 460-00-470-130 1
Toluene-d8 (S)100 %05/02/23 03:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2052754
KS LRH/MADEPV/MTDEQ
VPH/VPH
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92664647001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3920168-3
Associated Lab Samples:92664647001
Matrix:Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L <33.3 100 05/02/23 18:3333.3
Aliphatic (C09-C12)ug/L <33.3 100 05/02/23 18:3333.3
Aromatic (C09-C10),Unadjusted ug/L <33.3 100 05/02/23 18:3333.3
Total VPH ug/L <33.3 100 05/02/23 18:3333.3
2,5-Dibromotoluene (FID)%93.7 70.0-130 05/02/23 18:33
2,5-Dibromotoluene (PID)%95.3 70.0-130 05/02/23 18:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3920168-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3920168-2
Aliphatic (C05-C08)ug/L 12101200 101 70.0-1301081300 7.17 25
Aliphatic (C09-C12)ug/L 13701400 97.9 70.0-1301061490 8.39 25
Aromatic (C09-C10),Unadjusted ug/L 215200 108 70.0-130111221 2.75 25
Total VPH ug/L 28002800 100 70.0-1301083010 7.23 25
2,5-Dibromotoluene (FID)%111 70.0-130101
2,5-Dibromotoluene (PID)%107 70.0-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771413
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92664647001, 92664647002, 92664647005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4004482
Associated Lab Samples:92664647001, 92664647002, 92664647005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 05/02/23 02:410.31
1,1,1-Trichloroethane ug/L <0.33 0.50 05/02/23 02:410.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 05/02/23 02:410.22
1,1,2-Trichloroethane ug/L <0.32 0.50 05/02/23 02:410.32
1,1-Dichloroethane ug/L <0.37 0.50 05/02/23 02:410.37
1,1-Dichloroethene ug/L <0.35 0.50 05/02/23 02:410.35
1,1-Dichloropropene ug/L <0.43 0.50 05/02/23 02:410.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 05/02/23 02:410.81
1,2,3-Trichloropropane ug/L <0.26 0.50 05/02/23 02:410.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 05/02/23 02:410.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/02/23 02:410.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 05/02/23 02:410.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 05/02/23 02:410.27
1,2-Dichlorobenzene ug/L <0.34 0.50 05/02/23 02:410.34
1,2-Dichloroethane ug/L <0.32 0.50 05/02/23 02:410.32
1,2-Dichloropropane ug/L <0.36 0.50 05/02/23 02:410.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 05/02/23 02:410.33
1,3-Dichlorobenzene ug/L <0.34 0.50 05/02/23 02:410.34
1,3-Dichloropropane ug/L <0.28 0.50 05/02/23 02:410.28
1,4-Dichlorobenzene ug/L <0.33 0.50 05/02/23 02:410.33
2,2-Dichloropropane ug/L <0.39 0.50 05/02/23 02:410.39
2-Chlorotoluene ug/L <0.32 0.50 05/02/23 02:410.32
4-Chlorotoluene ug/L <0.32 0.50 05/02/23 02:410.32
Benzene ug/L <0.34 0.50 05/02/23 02:410.34
Bromobenzene ug/L <0.29 0.50 05/02/23 02:410.29
Bromochloromethane ug/L <0.47 0.50 05/02/23 02:410.47
Bromodichloromethane ug/L <0.31 0.50 05/02/23 02:410.31
Bromoform ug/L <0.34 0.50 05/02/23 02:410.34
Bromomethane ug/L <1.7 5.0 05/02/23 02:411.7
Carbon tetrachloride ug/L <0.33 0.50 05/02/23 02:410.33
Chlorobenzene ug/L <0.28 0.50 05/02/23 02:410.28
Chloroethane ug/L <0.65 1.0 05/02/23 02:410.65
Chloroform ug/L <0.43 0.50 05/02/23 02:410.43
Chloromethane ug/L <0.54 1.0 05/02/23 02:410.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 05/02/23 02:410.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 05/02/23 02:410.36
Dibromochloromethane ug/L <0.36 0.50 05/02/23 02:410.36
Dibromomethane ug/L <0.39 0.50 05/02/23 02:410.39
Dichlorodifluoromethane ug/L <0.35 0.50 IH05/02/23 02:410.35
Diisopropyl ether ug/L <0.31 0.50 05/02/23 02:410.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4004482
Associated Lab Samples:92664647001, 92664647002, 92664647005
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 05/02/23 02:4172.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 05/02/23 02:413.2
Ethylbenzene ug/L <0.30 0.50 05/02/23 02:410.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 05/02/23 02:411.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 05/02/23 02:410.33
m&p-Xylene ug/L <0.71 1.0 05/02/23 02:410.71
Methyl-tert-butyl ether ug/L <0.42 0.50 05/02/23 02:410.42
Methylene Chloride ug/L <2.0 2.0 05/02/23 02:412.0
n-Butylbenzene ug/L <0.49 0.50 05/02/23 02:410.49
n-Propylbenzene ug/L <0.34 0.50 05/02/23 02:410.34
Naphthalene ug/L <0.64 2.0 05/02/23 02:410.64
o-Xylene ug/L <0.34 0.50 05/02/23 02:410.34
sec-Butylbenzene ug/L <0.40 0.50 05/02/23 02:410.40
Styrene ug/L <0.29 0.50 05/02/23 02:410.29
tert-Amyl Alcohol ug/L <36.4 100 05/02/23 02:4136.4
tert-Amylmethyl ether ug/L <9.2 10.0 05/02/23 02:419.2
tert-Butyl Alcohol ug/L <26.8 50.0 05/02/23 02:4126.8
tert-Butyl Formate ug/L <29.4 50.0 05/02/23 02:4129.4
tert-Butylbenzene ug/L <0.32 0.50 05/02/23 02:410.32
Tetrachloroethene ug/L <0.29 0.50 05/02/23 02:410.29
Toluene ug/L <0.24 0.50 05/02/23 02:410.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 05/02/23 02:410.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 05/02/23 02:410.36
Trichloroethene ug/L <0.38 0.50 05/02/23 02:410.38
Trichlorofluoromethane ug/L <0.30 1.0 05/02/23 02:410.30
Vinyl chloride ug/L <0.39 1.0 05/02/23 02:410.39
1,2-Dichloroethane-d4 (S)%103 70-130 05/02/23 02:41
4-Bromofluorobenzene (S)%98 70-130 05/02/23 02:41
Toluene-d8 (S)%100 70-130 05/02/23 02:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004483LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.320 92 60-140
1,1,1-Trichloroethane ug/L 18.120 90 60-140
1,1,2,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,2-Trichloroethane ug/L 18.920 94 60-140
1,1-Dichloroethane ug/L 19.220 96 60-140
1,1-Dichloroethene ug/L 18.920 94 60-140
1,1-Dichloropropene ug/L 20.420 102 60-140
1,2,3-Trichlorobenzene ug/L 18.820 94 60-140
1,2,3-Trichloropropane ug/L 18.220 91 60-140
1,2,4-Trichlorobenzene ug/L 18.220 91 60-140
1,2,4-Trimethylbenzene ug/L 18.720 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004483LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 16.920 84 60-140
1,2-Dibromoethane (EDB)ug/L 19.120 95 60-140
1,2-Dichlorobenzene ug/L 18.320 92 60-140
1,2-Dichloroethane ug/L 18.920 95 60-140
1,2-Dichloropropane ug/L 19.320 96 60-140
1,3,5-Trimethylbenzene ug/L 18.620 93 60-140
1,3-Dichlorobenzene ug/L 18.520 92 60-140
1,3-Dichloropropane ug/L 18.820 94 60-140
1,4-Dichlorobenzene ug/L 17.920 89 60-140
2,2-Dichloropropane ug/L 17.520 87 60-140
2-Chlorotoluene ug/L 18.620 93 60-140
4-Chlorotoluene ug/L 18.220 91 60-140
Benzene ug/L 18.920 94 60-140
Bromobenzene ug/L 17.920 90 60-140
Bromochloromethane ug/L 18.820 94 60-140
Bromodichloromethane ug/L 17.120 85 60-140
Bromoform ug/L 16.220 81 60-140
Bromomethane ug/L 19.220 96 60-140
Carbon tetrachloride ug/L 16.420 82 60-140
Chlorobenzene ug/L 18.820 94 60-140
Chloroethane ug/L 26.920 135 60-140
Chloroform ug/L 18.220 91 60-140
Chloromethane ug/L 21.920 110 60-140
cis-1,2-Dichloroethene ug/L 18.820 94 60-140
cis-1,3-Dichloropropene ug/L 17.820 89 60-140
Dibromochloromethane ug/L 17.220 86 60-140
Dibromomethane ug/L 17.720 89 60-140
Dichlorodifluoromethane ug/L 27.7 IH2013860-140
Diisopropyl ether ug/L 18.220 91 60-140
Ethanol ug/L 721800 90 60-140
Ethyl-tert-butyl ether ug/L 36.840 92 60-140
Ethylbenzene ug/L 18.620 93 60-140
Hexachloro-1,3-butadiene ug/L 17.620 88 60-140
Isopropylbenzene (Cumene)ug/L 18.820 94 60-140
m&p-Xylene ug/L 36.640 91 60-140
Methyl-tert-butyl ether ug/L 17.820 89 60-140
Methylene Chloride ug/L 18.420 92 60-140
n-Butylbenzene ug/L 18.620 93 60-140
n-Propylbenzene ug/L 18.120 90 60-140
Naphthalene ug/L 20.020 100 60-140
o-Xylene ug/L 18.520 93 60-140
sec-Butylbenzene ug/L 17.720 89 60-140
Styrene ug/L 18.720 94 60-140
tert-Amyl Alcohol ug/L 328400 82 60-140
tert-Amylmethyl ether ug/L 37.240 93 60-140
tert-Butyl Alcohol ug/L 173200 87 60-140
tert-Butyl Formate ug/L 126160 79 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004483LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 15.120 75 60-140
Tetrachloroethene ug/L 17.220 86 60-140
Toluene ug/L 17.920 90 60-140
trans-1,2-Dichloroethene ug/L 19.420 97 60-140
trans-1,3-Dichloropropene ug/L 17.420 87 60-140
Trichloroethene ug/L 18.920 94 60-140
Trichlorofluoromethane ug/L 19.020 95 60-140
Vinyl chloride ug/L 18.220 91 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004484MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664581011
4004485
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 130 60-140137 5 3020ND25.9 27.3
1,1,1-Trichloroethane ug/L M12014760-140152 4 3020ND29.3 30.5
1,1,2,2-Tetrachloroethane ug/L 20 131 60-140136 4 3020ND26.2 27.2
1,1,2-Trichloroethane ug/L 20 131 60-140135 3 3020ND26.2 27.0
1,1-Dichloroethane ug/L M12015260-140158 4 3020ND30.3 31.7
1,1-Dichloroethene ug/L M12015560-140158 2 3020ND31.0 31.7
1,1-Dichloropropene ug/L M12016360-140167 2 3020ND32.6 33.4
1,2,3-Trichlorobenzene ug/L 20 109 60-140116 6 3020ND21.7 23.2
1,2,3-Trichloropropane ug/L 20 125 60-140132 5 3020ND25.0 26.3
1,2,4-Trichlorobenzene ug/L 20 114 60-140122 7 3020ND22.7 24.4
1,2,4-Trimethylbenzene ug/L 20 129 60-140135 5 3020ND25.7 27.0
1,2-Dibromo-3-
chloropropane ug/L 20 112 60-140118 5 3020ND22.4 23.5
1,2-Dibromoethane (EDB)ug/L 20 132 60-140140 6 3020ND26.4 27.9
1,2-Dichlorobenzene ug/L 20 123 60-140130 6 3020ND24.5 26.0
1,2-Dichloroethane ug/L M12014060-140145 3 3020ND28.0 28.9
1,2-Dichloropropane ug/L M12014360-140147 3 3020ND28.6 29.3
1,3,5-Trimethylbenzene ug/L 20 128 60-140137 7 3020ND25.6 27.4
1,3-Dichlorobenzene ug/L 20 127 60-140135 6 3020ND25.4 26.9
1,3-Dichloropropane ug/L 20 130 60-140135 4 3020ND26.0 27.1
1,4-Dichlorobenzene ug/L 20 119 60-140126 6 3020ND23.9 25.3
2,2-Dichloropropane ug/L M12015660-140162 3 3020ND31.3 32.4
2-Chlorotoluene ug/L 20 129 60-140137 6 3020ND25.9 27.4
4-Chlorotoluene ug/L 20 130 60-140140 7 3020ND25.9 28.0
Benzene ug/L M12014260-140145 2 3020ND28.4 29.0
Bromobenzene ug/L 20 125 60-140132 6 3020ND25.0 26.4
Bromochloromethane ug/L M12014160-140146 4 3020ND28.1 29.3
Bromodichloromethane ug/L 20 128 60-140131 3 3020ND25.5 26.3
Bromoform ug/L 20 110 60-140116 6 3020ND21.9 23.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004484MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664581011
4004485
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 134 60-140123 8 3020ND26.7 24.6
Carbon tetrachloride ug/L 20 131 60-140135 3 3020ND26.2 27.0
Chlorobenzene ug/L 20 133 60-140137 3 3020ND26.6 27.3
Chloroethane ug/L M12021460-140240 11 3020ND42.8 48.1
Chloroform ug/L M12014760-140149 1 3020ND29.5 29.7
Chloromethane ug/L M12014260-140137 3 3020ND28.4 27.4
cis-1,2-Dichloroethene ug/L M12014760-140153 4 3020ND29.4 30.5
cis-1,3-Dichloropropene ug/L 20 129 60-140133 3 3020ND25.8 26.6
Dibromochloromethane ug/L 20 125 60-140129 4 3020ND24.9 25.8
Dibromomethane ug/L 20 130 60-140134 3 3020ND25.9 26.7
Dichlorodifluoromethane ug/L IH,M12014360-140147 3 3020ND28.7 29.4
Diisopropyl ether ug/L 20 132 60-140138 4 3020ND26.3 27.5
Ethanol ug/L 800 122 60-140127 4 30800ND9761020
Ethyl-tert-butyl ether ug/L 40 131 60-140138 5 3040ND52.5 55.2
Ethylbenzene ug/L 20 131 60-140137 5 3020ND26.2 27.4
Hexachloro-1,3-butadiene ug/L 20 106 60-140113 6 3020ND21.2 22.6
Isopropylbenzene
(Cumene)ug/L 20 130 60-140136 4 3020ND26.0 27.2
m&p-Xylene ug/L 40 129 60-140134 4 3040ND51.5 53.7
Methyl-tert-butyl ether ug/L 20 125 60-140131 5 3020ND25.0 26.2
Methylene Chloride ug/L 20 128 60-140130 1 3020ND25.6 26.0
n-Butylbenzene ug/L 20 127 60-140136 6 3020ND25.4 27.1
n-Propylbenzene ug/L 20 128 60-140137 7 3020ND25.6 27.5
Naphthalene ug/L 20 123 60-140132 7 3020ND24.6 26.4
o-Xylene ug/L 20 130 60-140133 2 3020ND26.0 26.6
sec-Butylbenzene ug/L 20 124 60-140132 7 3020ND24.7 26.4
Styrene ug/L 20 131 60-140136 3 30200.42J 26.7 27.6
tert-Amyl Alcohol ug/L 400 109 60-140116 5 30400ND438462
tert-Amylmethyl ether ug/L 40 127 60-140132 4 3040ND50.6 52.9
tert-Butyl Alcohol ug/L M120016260-140175 8 30200ND324350
tert-Butyl Formate ug/L P51602260-14020 30160ND35.9J 32.0J
tert-Butylbenzene ug/L 20 105 60-140111 6 3020ND21.0 22.3
Tetrachloroethene ug/L 20 125 60-140129 3 3020ND25.0 25.9
Toluene ug/L 20 129 60-140133 3 3020ND25.8 26.6
trans-1,2-Dichloroethene ug/L M12015560-140161 3 3020ND31.1 32.2
trans-1,3-Dichloropropene ug/L 20 125 60-140129 3 3020ND25.1 25.8
Trichloroethene ug/L M12014360-140147 2 3020ND28.7 29.3
Trichlorofluoromethane ug/L M12015460-140158 3 3020ND30.8 31.7
Vinyl chloride ug/L 20 123 60-140127 3 3020ND24.7 25.3
1,2-Dichloroethane-d4 (S)%104 70-130104
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771417
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92664647003, 92664647004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4004494
Associated Lab Samples:92664647003, 92664647004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 05/03/23 12:310.31
1,1,1-Trichloroethane ug/L <0.33 0.50 05/03/23 12:310.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 05/03/23 12:310.22
1,1,2-Trichloroethane ug/L <0.32 0.50 05/03/23 12:310.32
1,1-Dichloroethane ug/L <0.37 0.50 05/03/23 12:310.37
1,1-Dichloroethene ug/L <0.35 0.50 05/03/23 12:310.35
1,1-Dichloropropene ug/L <0.43 0.50 05/03/23 12:310.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 05/03/23 12:310.81
1,2,3-Trichloropropane ug/L <0.26 0.50 05/03/23 12:310.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 05/03/23 12:310.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/03/23 12:310.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 05/03/23 12:310.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 05/03/23 12:310.27
1,2-Dichlorobenzene ug/L <0.34 0.50 05/03/23 12:310.34
1,2-Dichloroethane ug/L <0.32 0.50 05/03/23 12:310.32
1,2-Dichloropropane ug/L <0.36 0.50 05/03/23 12:310.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 05/03/23 12:310.33
1,3-Dichlorobenzene ug/L <0.34 0.50 05/03/23 12:310.34
1,3-Dichloropropane ug/L <0.28 0.50 05/03/23 12:310.28
1,4-Dichlorobenzene ug/L <0.33 0.50 05/03/23 12:310.33
2,2-Dichloropropane ug/L <0.39 0.50 05/03/23 12:310.39
2-Chlorotoluene ug/L <0.32 0.50 05/03/23 12:310.32
4-Chlorotoluene ug/L <0.32 0.50 05/03/23 12:310.32
Benzene ug/L <0.34 0.50 05/03/23 12:310.34
Bromobenzene ug/L <0.29 0.50 05/03/23 12:310.29
Bromochloromethane ug/L <0.47 0.50 05/03/23 12:310.47
Bromodichloromethane ug/L <0.31 0.50 05/03/23 12:310.31
Bromoform ug/L <0.34 0.50 05/03/23 12:310.34
Bromomethane ug/L <1.7 5.0 05/03/23 12:311.7
Carbon tetrachloride ug/L <0.33 0.50 05/03/23 12:310.33
Chlorobenzene ug/L <0.28 0.50 05/03/23 12:310.28
Chloroethane ug/L <0.65 1.0 05/03/23 12:310.65
Chloroform ug/L <0.43 0.50 05/03/23 12:310.43
Chloromethane ug/L <0.54 1.0 05/03/23 12:310.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 05/03/23 12:310.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 05/03/23 12:310.36
Dibromochloromethane ug/L <0.36 0.50 05/03/23 12:310.36
Dibromomethane ug/L <0.39 0.50 05/03/23 12:310.39
Dichlorodifluoromethane ug/L <0.35 0.50 05/03/23 12:310.35
Diisopropyl ether ug/L <0.31 0.50 05/03/23 12:310.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4004494
Associated Lab Samples:92664647003, 92664647004
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 05/03/23 12:3172.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 05/03/23 12:313.2
Ethylbenzene ug/L <0.30 0.50 05/03/23 12:310.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 05/03/23 12:311.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 05/03/23 12:310.33
m&p-Xylene ug/L <0.71 1.0 05/03/23 12:310.71
Methyl-tert-butyl ether ug/L <0.42 0.50 05/03/23 12:310.42
Methylene Chloride ug/L <2.0 2.0 05/03/23 12:312.0
n-Butylbenzene ug/L <0.49 0.50 05/03/23 12:310.49
n-Propylbenzene ug/L <0.34 0.50 05/03/23 12:310.34
Naphthalene ug/L <0.64 2.0 05/03/23 12:310.64
o-Xylene ug/L <0.34 0.50 05/03/23 12:310.34
sec-Butylbenzene ug/L <0.40 0.50 05/03/23 12:310.40
Styrene ug/L <0.29 0.50 05/03/23 12:310.29
tert-Amyl Alcohol ug/L <36.4 100 05/03/23 12:3136.4
tert-Amylmethyl ether ug/L <9.2 10.0 05/03/23 12:319.2
tert-Butyl Alcohol ug/L <26.8 50.0 05/03/23 12:3126.8
tert-Butyl Formate ug/L <29.4 50.0 05/03/23 12:3129.4
tert-Butylbenzene ug/L <0.32 0.50 05/03/23 12:310.32
Tetrachloroethene ug/L <0.29 0.50 05/03/23 12:310.29
Toluene ug/L <0.24 0.50 05/03/23 12:310.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 05/03/23 12:310.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 05/03/23 12:310.36
Trichloroethene ug/L <0.38 0.50 05/03/23 12:310.38
Trichlorofluoromethane ug/L <0.30 1.0 05/03/23 12:310.30
Vinyl chloride ug/L <0.39 1.0 05/03/23 12:310.39
1,2-Dichloroethane-d4 (S)%92 70-130 05/03/23 12:31
4-Bromofluorobenzene (S)%98 70-130 05/03/23 12:31
Toluene-d8 (S)%107 70-130 05/03/23 12:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004495LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 16.320 82 60-140
1,1,1-Trichloroethane ug/L 18.120 90 60-140
1,1,2,2-Tetrachloroethane ug/L 17.220 86 60-140
1,1,2-Trichloroethane ug/L 18.220 91 60-140
1,1-Dichloroethane ug/L 17.620 88 60-140
1,1-Dichloroethene ug/L 18.820 94 60-140
1,1-Dichloropropene ug/L 17.020 85 60-140
1,2,3-Trichlorobenzene ug/L 16.920 84 60-140
1,2,3-Trichloropropane ug/L 15.520 78 60-140
1,2,4-Trichlorobenzene ug/L 17.720 88 60-140
1,2,4-Trimethylbenzene ug/L 17.920 90 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004495LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 17.820 89 60-140
1,2-Dibromoethane (EDB)ug/L 17.920 90 60-140
1,2-Dichlorobenzene ug/L 17.720 88 60-140
1,2-Dichloroethane ug/L 17.720 89 60-140
1,2-Dichloropropane ug/L 17.820 89 60-140
1,3,5-Trimethylbenzene ug/L 16.920 84 60-140
1,3-Dichlorobenzene ug/L 17.720 89 60-140
1,3-Dichloropropane ug/L 15.620 78 60-140
1,4-Dichlorobenzene ug/L 16.520 83 60-140
2,2-Dichloropropane ug/L 17.420 87 60-140
2-Chlorotoluene ug/L 17.220 86 60-140
4-Chlorotoluene ug/L 17.120 85 60-140
Benzene ug/L 16.920 85 60-140
Bromobenzene ug/L 16.520 82 60-140
Bromochloromethane ug/L 18.520 92 60-140
Bromodichloromethane ug/L 18.420 92 60-140
Bromoform ug/L 16.720 84 60-140
Bromomethane ug/L 16.120 81 60-140
Carbon tetrachloride ug/L 18.220 91 60-140
Chlorobenzene ug/L 16.820 84 60-140
Chloroethane ug/L 18.320 91 60-140
Chloroform ug/L 17.120 85 60-140
Chloromethane ug/L 17.720 88 60-140
cis-1,2-Dichloroethene ug/L 18.120 91 60-140
cis-1,3-Dichloropropene ug/L 17.420 87 60-140
Dibromochloromethane ug/L 17.320 86 60-140
Dibromomethane ug/L 18.120 91 60-140
Dichlorodifluoromethane ug/L 18.820 94 60-140
Diisopropyl ether ug/L 15.420 77 60-140
Ethanol ug/L 676800 84 60-140
Ethyl-tert-butyl ether ug/L 28.840 72 60-140
Ethylbenzene ug/L 16.120 81 60-140
Hexachloro-1,3-butadiene ug/L 17.720 89 60-140
Isopropylbenzene (Cumene)ug/L 16.820 84 60-140
m&p-Xylene ug/L 32.040 80 60-140
Methyl-tert-butyl ether ug/L 13.320 67 60-140
Methylene Chloride ug/L 16.220 81 60-140
n-Butylbenzene ug/L 18.420 92 60-140
n-Propylbenzene ug/L 16.820 84 60-140
Naphthalene ug/L 18.320 92 60-140
o-Xylene ug/L 16.820 84 60-140
sec-Butylbenzene ug/L 17.620 88 60-140
Styrene ug/L 17.320 86 60-140
tert-Amyl Alcohol ug/L 330400 82 60-140
tert-Amylmethyl ether ug/L 31.140 78 60-140
tert-Butyl Alcohol ug/L 151200 75 60-140
tert-Butyl Formate ug/L 125160 78 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
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Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004495LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 14.920 75 60-140
Tetrachloroethene ug/L 17.220 86 60-140
Toluene ug/L 16.420 82 60-140
trans-1,2-Dichloroethene ug/L 18.420 92 60-140
trans-1,3-Dichloropropene ug/L 18.120 90 60-140
Trichloroethene ug/L 15.820 79 60-140
Trichlorofluoromethane ug/L 17.020 85 60-140
Vinyl chloride ug/L 14.720 73 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004496MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664647003
4004497
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 25 117 60-140119 2 3025<0.31 29.2 29.7
1,1,1-Trichloroethane ug/L 25 127 60-140128 0 3025<0.33 31.8 32.0
1,1,2,2-Tetrachloroethane ug/L 25 118 60-140122 4 3025<0.22 29.4 30.5
1,1,2-Trichloroethane ug/L 25 114 60-140118 4 3025<0.32 28.6 29.6
1,1-Dichloroethane ug/L 25 133 60-140136 3 3025<0.37 33.2 34.1
1,1-Dichloroethene ug/L 25 139 60-140139 0 3025<0.35 34.7 34.8
1,1-Dichloropropene ug/L M12514660-140144 1 3025<0.43 36.4 36.1
1,2,3-Trichlorobenzene ug/L 25 115 60-140112 3 3025<0.81 28.8 27.9
1,2,3-Trichloropropane ug/L 25 113 60-140117 4 3025<0.26 28.2 29.2
1,2,4-Trichlorobenzene ug/L 25 115 60-140117 2 3025<0.64 28.7 29.3
1,2,4-Trimethylbenzene ug/L 25 121 60-140124 3 3025<0.50 30.3 31.1
1,2-Dibromo-3-
chloropropane ug/L 25 101 60-140101 0 3025<0.34 25.3 25.3
1,2-Dibromoethane (EDB)ug/L 25 117 60-140123 5 3025<0.27 29.2 30.7
1,2-Dichlorobenzene ug/L 25 114 60-140117 3 3025<0.34 28.4 29.4
1,2-Dichloroethane ug/L 25 124 60-140128 3 3025<0.32 31.1 32.0
1,2-Dichloropropane ug/L 25 124 60-140128 3 3025<0.36 31.1 31.9
1,3,5-Trimethylbenzene ug/L 25 123 60-140126 2 3025<0.33 30.8 31.6
1,3-Dichlorobenzene ug/L 25 119 60-140122 2 3025<0.34 29.7 30.4
1,3-Dichloropropane ug/L 25 116 60-140121 4 3025<0.28 29.0 30.2
1,4-Dichlorobenzene ug/L 25 112 60-140114 2 3025<0.33 28.0 28.6
2,2-Dichloropropane ug/L 25 138 60-140140 1 3025<0.39 34.5 35.0
2-Chlorotoluene ug/L 25 122 60-140124 1 3025<0.32 30.6 30.9
4-Chlorotoluene ug/L 25 123 60-140125 2 3025<0.32 30.7 31.3
Benzene ug/L 25 122 60-140125 2 3025<0.34 30.6 31.1
Bromobenzene ug/L 25 114 60-140117 2 3025<0.29 28.4 29.1
Bromochloromethane ug/L 25 121 60-140126 4 3025<0.47 30.2 31.4
Bromodichloromethane ug/L 25 110 60-140114 4 3025<0.31 27.5 28.5
Bromoform ug/L 25 98 60-140101 3 3025<0.34 24.4 25.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
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Huntersville, NC 28078
[phone]
Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004496MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664647003
4004497
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 25 115 60-140120 4 3025<1.7 28.8 29.9
Carbon tetrachloride ug/L 25 113 60-140114 1 3025<0.33 28.3 28.5
Chlorobenzene ug/L 25 119 60-140122 3 3025<0.28 29.7 30.5
Chloroethane ug/L M12518260-140188 3 3025<0.65 45.5 46.9
Chloroform ug/L 25 124 60-140128 3 3025<0.43 31.1 32.0
Chloromethane ug/L M12514860-140148 0 3025<0.54 37.1 37.1
cis-1,2-Dichloroethene ug/L 25 126 60-140132 4 3025<0.38 31.6 33.0
cis-1,3-Dichloropropene ug/L 25 113 60-140117 3 3025<0.36 28.4 29.3
Dibromochloromethane ug/L 25 109 60-140114 5 3025<0.36 27.3 28.6
Dibromomethane ug/L 25 111 60-140113 2 3025<0.39 27.6 28.2
Dichlorodifluoromethane ug/L IH,M12522460-140223 1 3025<0.35 56.1 55.7
Diisopropyl ether ug/L 25 118 60-140121 2 3025<0.31 29.6 30.3
Ethanol ug/L 1000 112 60-140111 1 301000<72.2 1120 1110
Ethyl-tert-butyl ether ug/L 50 118 60-140122 3 3050<3.2 59.0 60.9
Ethylbenzene ug/L 25 121 60-140123 1 3025<0.30 30.2 30.7
Hexachloro-1,3-butadiene ug/L 25 130 60-140132 1 3025<1.5 32.6 32.9
Isopropylbenzene
(Cumene)ug/L 25 121 60-140123 1 3025<0.33 30.4 30.6
m&p-Xylene ug/L 50 117 60-140121 4 3050<0.71 58.5 60.7
Methyl-tert-butyl ether ug/L 25 112 60-140115 3 3025<0.42 27.9 28.8
Methylene Chloride ug/L 25 115 60-140119 3 3025<2.0 28.7 29.7
n-Butylbenzene ug/L 25 138 60-140138 0 3025<0.49 34.5 34.5
n-Propylbenzene ug/L 25 126 60-140127 1 3025<0.34 31.4 31.8
Naphthalene ug/L 25 117 60-140116 1 3025<0.64 29.1 28.9
o-Xylene ug/L 25 115 60-140119 3 3025<0.34 28.8 29.8
sec-Butylbenzene ug/L 25 128 60-140127 0 3025<0.40 31.9 31.9
Styrene ug/L 25 117 60-140121 3 3025<0.29 29.4 30.3
tert-Amyl Alcohol ug/L 500 100 60-14097 3 30500<36.4 501 487
tert-Amylmethyl ether ug/L 50 113 60-140116 3 3050<9.2 56.5 58.0
tert-Butyl Alcohol ug/L 250 110 60-140111 2 30250<26.8 274 279
tert-Butyl Formate ug/L 200 91 60-14085 6 30200<29.4 182 171
tert-Butylbenzene ug/L 25 104 60-140104 0 3025<0.32 25.9 26.0
Tetrachloroethene ug/L 25 115 60-140116 1 3025<0.29 28.8 29.1
Toluene ug/L 25 114 60-140116 1 3025<0.24 28.6 29.0
trans-1,2-Dichloroethene ug/L 25 139 60-140139 1 3025<0.40 34.7 34.9
trans-1,3-Dichloropropene ug/L 25 111 60-140115 4 3025<0.36 27.8 28.8
Trichloroethene ug/L 25 123 60-140125 2 3025<0.38 30.8 31.3
Trichlorofluoromethane ug/L M12514160-140143 2 3025<0.30 35.3 35.9
Vinyl chloride ug/L 25 128 60-140128 0 3025<0.39 32.1 32.0
1,2-Dichloroethane-d4 (S)%109 70-130109
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771480
EPA 3511
EPA 8270E
8270E PAH Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92664647001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4004626
Associated Lab Samples:92664647001
Matrix:Water
AnalyzedMDL
1-Methylnaphthalene ug/L <3.7 10.0 05/01/23 16:483.7
2-Methylnaphthalene ug/L <3.4 10.0 05/01/23 16:483.4
Acenaphthene ug/L <3.2 10.0 05/01/23 16:483.2
Acenaphthylene ug/L <3.9 10.0 05/01/23 16:483.9
Anthracene ug/L <3.9 10.0 05/01/23 16:483.9
Benzo(a)anthracene ug/L <4.0 10.0 05/01/23 16:484.0
Benzo(a)pyrene ug/L <3.6 10.0 05/01/23 16:483.6
Benzo(b)fluoranthene ug/L <3.9 10.0 05/01/23 16:483.9
Benzo(g,h,i)perylene ug/L <3.7 10.0 05/01/23 16:483.7
Benzo(k)fluoranthene ug/L <3.6 10.0 05/01/23 16:483.6
Chrysene ug/L <3.4 10.0 05/01/23 16:483.4
Dibenz(a,h)anthracene ug/L <4.3 10.0 05/01/23 16:484.3
Fluoranthene ug/L <3.4 10.0 05/01/23 16:483.4
Fluorene ug/L <3.2 10.0 05/01/23 16:483.2
Indeno(1,2,3-cd)pyrene ug/L <4.0 10.0 05/01/23 16:484.0
Naphthalene ug/L <3.2 10.0 05/01/23 16:483.2
Phenanthrene ug/L <3.4 10.0 05/01/23 16:483.4
Pyrene ug/L <3.8 10.0 05/01/23 16:483.8
2-Fluorobiphenyl (S)%83 57-152 05/01/23 16:48
Nitrobenzene-d5 (S)%109 59-144 05/01/23 16:48
Terphenyl-d14 (S)%93 10-162 05/01/23 16:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004627LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 58.662.5 94 70-130
2-Methylnaphthalene ug/L 53.762.5 86 70-130
Acenaphthene ug/L 60.762.5 97 70-130
Acenaphthylene ug/L 59.962.5 96 70-130
Anthracene ug/L 56.262.5 90 70-130
Benzo(a)anthracene ug/L 59.762.5 95 70-130
Benzo(a)pyrene ug/L 60.562.5 97 70-130
Benzo(b)fluoranthene ug/L 59.462.5 95 70-130
Benzo(g,h,i)perylene ug/L 58.862.5 94 70-130
Benzo(k)fluoranthene ug/L 59.662.5 95 70-130
Chrysene ug/L 60.562.5 97 70-130
Dibenz(a,h)anthracene ug/L 58.162.5 93 70-130
Fluoranthene ug/L 61.762.5 99 70-130
Fluorene ug/L 63.162.5 101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004627LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/L 60.762.5 97 70-130
Naphthalene ug/L 52.062.5 83 70-130
Phenanthrene ug/L 58.762.5 94 70-130
Pyrene ug/L 58.862.5 94 70-130
2-Fluorobiphenyl (S)%89 57-152
Nitrobenzene-d5 (S)%114 59-144
Terphenyl-d14 (S)%88 10-162
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004628MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664647001
4004629
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1-Methylnaphthalene ug/L 118 104 56-16992 12 30120<3.5 124 110
2-Methylnaphthalene ug/L 118 96 52-16986 10 30120<3.3 114 103
Acenaphthene ug/L 118 108 58-17296 11 30120<3.1 128 115
Acenaphthylene ug/L 118 108 59-16895 12 30120<3.7 128 113
Anthracene ug/L 118 101 39-17389 11 30120<3.7 119 107
Benzo(a)anthracene ug/L 118 105 51-16994 10 30120<3.9 124 113
Benzo(a)pyrene ug/L 118 109 52-17095 13 30120<3.5 129 113
Benzo(b)fluoranthene ug/L 118 103 48-17295 7 30120<3.8 122 114
Benzo(g,h,i)perylene ug/L 118 112 53-17297 14 30120<3.6 133 116
Benzo(k)fluoranthene ug/L 118 107 53-17896 10 30120<3.5 126 114
Chrysene ug/L 118 111 57-17298 11 30120<3.3 131 117
Dibenz(a,h)anthracene ug/L 118 111 51-17196 13 30120<4.2 132 115
Fluoranthene ug/L 118 106 49-17095 10 30120<3.2 126 114
Fluorene ug/L 118 112 57-17496 14 30120<3.1 133 115
Indeno(1,2,3-cd)pyrene ug/L 118 110 52-17098 11 30120<3.9 130 117
Naphthalene ug/L 118 93 55-17282 11 301204.7J 115 103
Phenanthrene ug/L 118 108 54-17195 12 30120<3.3 128 114
Pyrene ug/L 118 109 47-17893 15 30120<3.7 129 111
2-Fluorobiphenyl (S)%105 57-15289
Nitrobenzene-d5 (S)%129 59-144111
Terphenyl-d14 (S)%90 10-16283
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92664647001
Volatile Petroleum Hydrocarbons by Method MADEPV - Lowest possible dilution due to sample foaming.[1]
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92664647
SUTTLES PROPERTY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92664647001 2052754 2052754MW1MADEPVMADEP VPH
92664647001 771480 771600MW1EPA 3511 EPA 8270E
92664647001 771413MW1SM 6200B
92664647002 771413MW2SM 6200B
92664647003 771417WSW2SM 6200B
92664647004 771417WSW3SM 6200B
92664647005 771413FBSM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/04/2023 03:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 33
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