RA-828_5656_CA_LTRRPT_20230620

1044 Washington Street
Raleigh, NC 27605
[phone]
www.CatlinUSA.com
Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA
ENVIRONMENTAL | CIVIL | GEOTECHNICAL

Wilmington, NC | Raleigh, NC | Washington, NC | Atlanta, GA | Charleston, SC
June 20, 2023
North Carolina Department of Environmental Quality Division of Waste Management UST Section Attn: Mr. Mark Petermann1646 Mail Service Center Raleigh, NC 27699-1646
Re: Letter Report Kelly’s Grocery 3474 NC 751 Apex, NC 27523 Incident Number: 5656 Risk Classification: H280D CATLIN Project No. 221050
Dear Mr. Mark Petermann,
CATLIN Engineers and Scientists (CATLIN) is pleased to provide you with this letter report documenting field activities performed in general accordance with CATLIN proposal number 221050.01P, prepared May 11, 2023. Services were authorized by the North Carolina Environmental Quality (NCDEQ) Task Authorization (TA) #01, accepted May 11, 2023, and Contract Number N70522-A. The approved scope of services for this Task Authorization included:
•Collect a groundwater sample from water supply well WSW-7 influent and effluent andanalyze the groundwater sample, one trip blank, and one field blank via Standard Method(SM) 6200B plus ethylene dibromide (EDB), methyl tert-butyl ether (MTBE), anddiisopropyl ether (DIPE); and
•Prepare a letter report documenting the findings.
The Kelly’s Grocery site is located at 3474 NC 751, Apex, Wake County, NC (See Figures in Attachment A). CATLIN conducted field activities on May 24, 2023, in accordance with the
approved TA. Field notes are documented on a Daily Activities Log, provided in Attachment B. Site photographs are presented in Attachment C. Available water supply well/property owner information is summarized in Table 1 (Attachment D).
Groundwater Sampling
The water supply well WSW-7 was sampled at the well (WSW-7I; Influent) and after the carbon filtration system (WSW-7E; Effluent). The location for WSW-7 is illustrated on the attached
Figure 2 and the well was sampled in accordance with NCDEQ Guidelines and Environmental Protection Agency (EPA) Region 4 Operating Procedures. Prior to obtaining a representative groundwater sample, the well was purged by allowing the spigot at the well (influent) to run for approximately 45 minutes and the spigot on the house (effluent) was allowed to run for 15
June 20, 2023 Page 2 of 2
NCDEQ; 5656_Kelly's Grocery.docx CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
minutes. The groundwater samples were collected from the spigot located on the water supply well (WSW-7I) and from the spigot on the southeast side of the residence (WSW-7E). The
samples were collected from the spigots directly into appropriate laboratory-provided, pre-preserved glassware, labeled, and placed on ice in an insulated cooler. A field blank was collected by pouring water from a new, sealed gallon of distilled water directly into appropriate, laboratory-
provided, pre-preserved glassware, labelled and placed on ice in an insulated cooler. A laboratory-provided trip blank accompanied the samples for the duration of the site activities. The groundwater sample, field blank, and laboratory-provided trip blank were submitted to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC) protocol and analyzed per SM 6200B (including EDB, MTBE, and DIPE). The laboratory analytical data and COC are included in Attachment E.
Groundwater Sample Results Laboratory analysis indicated an estimated (“J”-value) benzene concentration in sample WSW-7I of 0.29 micrograms per liter (µg/L), which is below the concentration of 1 µg/L established in the Title 15A of the North Carolina Administrative Code, Subchapter 2L Groundwater Quality
Standards (2L GWQS). No additional targeted analytes were detected in either sample WSW-7I or WSW-7E.
The trip blank and field blank both indicated estimated concentrations (“J”-values) of acetone (a known laboratory artifact). No additional targeted analytes were detected in either of these two samples. The current and historical laboratory analytical results are summarized in Tables 2 and 3, respectively (Attachment D). A copy of the complete laboratory report and chain of custody documentation are presented in Attachment E. CATLIN Engineers and Scientists will proceed upon notification of your approval. Should you have any questions or require additional information, please contact us at 910-726-1307.
Sincerely,
Sean J. O’Neil, P.E.
Project Manager Attachments: A Figures B Daily Activities Log C Site Photographs D Tables E Laboratory Analytical Report and Chain of Custody Document

NCDEQ; 5656_Kelly’s Grocery CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
ATTACHMENT A FIGURES
FIGUREPROJECTTITLE
1KELLY'S GROCERY3474 NC 751APEX, NC SITE VICINITY MAP
SITE LOCATIONNC 751L E W T E R S H O P R D
Copyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY5656221050JUNE 2023 AS SHOWN KMC/SJO
FIGUREPROJECTTITLE
2KELLY'S GROCERY3474 NC 751APEX, NC POTENTIAL RECEPTOR MAP
!(P!(P
!(P
SITE LOCATION
NC 751LE WTE R S H OP R D
1 ,5 0 0 FEET RADIUS
500F E E T RADIUS
!(P WSW-7
WSW-8
WSW-5 POND 1
POND 2
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
NOTE: Well locations were obtained from previous reports prepared by other consultants and are approximate.
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY5656221050JUNE 2023 AS SHOWN KMC/SJO
LEGEND
Active PotableWater Supply Well!(P
FIGUREPROJECTTITLE
3KELLY'S GROCERY3474 NC 751APEX, NC
WATER SUPPLY WELLGROUNDWATER SAMPLEANALYTICAL RESULTS –MAY 24, 2023
!(P
!(P
!(P
!>!>
!>
!>!>
!>
!>
!>
!>
!(>NC 75
1MW-5 MW-4
MW-9
MW-8D
MW-1R
MW-2
MW-3R
MW-7R
MW-7
MW-6
WSW-7
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
60 0 60 12030
Feet
³
NOTE: Well and tank locations were obtained from previous reports prepared by other consultants and are approximate.
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY5656221050JUNE 2023 AS SHOWN KMC/SJO
Monitoring Well (Deep)((>
Approximate Location of Former USTs
Parcel Boundary
Sampled PotableWater Supply Well!(P
Monitoring Well (Type II)!>
LEGEND
Abandoned Monitoring Well (Type II)!>Well/ Sample ID
DateCollected
WSW-7I 05/24/23 0.29
All results in micrograms per liter (µg/L).B o ld results are above 2L GWQS. Refer to Table 4 for all notes and results.
GCL (µg/L)2L GWQS (µg/L) 5,0001
SUMMARY OF GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200BIncident Name and No.:Kelly's Grocery - 5656
Contaminant of Concern
Benzene

NCDEQ; 5656_Kelly's Grocery.docx CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
ATTACHMENT B DAILY ACTIVITIES LOG

NCDEQ; 5656_Kelly's Grocery.docx CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
ATTACHMENT C SITE PHOTOGRAPHS
ATTACHMENT C SITE PHOTOGRAPHS
NCDEQ; 5656_Kelly’s Grocery CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023

View of WSW-7 Influent sample point.

View of WSW-7 Effluent sample point.

NCDEQ; 5656_Kelly's Grocery.docx CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
ATTACHMENT D
TABLES
Page 1 of 1
Well ID Property Address
Chatham
County
Parcel ID
Number
Owner Name
(Last, First, MI)
Owner Mailing
Address Well Use Well Depth
(ft.)
Distance/
Direction
from
Source Area
(ft.)
WSW-5 NC Highway 751,
Apex, NC 27523 17767 D & B Farms, LLC 1132 Morrisville-Carpenter
Road, Cary, NC 27519
Active
Potable Unknown 380 / NW
WSW-7 3474 NC Highway 751,
Apex, NC 27523 63033 Johnson, David J.
& Wanda K.
3474 NC Highway 751,
Apex, NC 27523
Active
Potable 173 250 / NE
WSW-8 3396 NC Highway 751,
Apex, NC 27523 17800 Yates, George F.
& Michael N.
41 Lewter Shop Road,
Apex, NC 27523
Active
Potable Unknown 290 / SE
Receptor
ID Location Contact
Distance/
Direction from
Source Area (ft.)
Pond 1 3474 NC Highway 751,
Apex, NC 27523
Johnson,
David J. &
Wanda K.
325 / NE
Pond 2 2551 Holland's Chapel
Road, Apex, NC 27523
Apex
Nurseries,
Inc.
475 / SW
Information obtained from S&ME (2020).
ft. = feet
Description
Small pond located to the northeast
Pond located to the southwest
TABLE 1
PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
Incident Name and No.: Kelly's Grocery - 5656
NCDEQ; 5656_Kelly's Grocery; T1_Receptor Info
CATLIN Project No. 221050
CATLIN Engineers and Scientists
June 2023
Page 1 of 1
Incident Name and No.: Kelly's Grocery - 5656
Well
Type
Well/
Sample ID
Date
Collected
(mm/dd/yy)
WSW-7E 05/24/23 <2.0 <0.18 BMDL
WSW-7I 05/24/23 <2.0 0.29 J BMDL
05/24/23 3.3 J <0.18 BMDL
05/24/23 3.5 J <0.18 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits)
Bold results indicate concentrations above 2L GWQS.
PWS = Private Water Supply
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than Method Detection Limit
ƚ = The Method Detection Limit is above the 2L GWQS.
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).PWSVaries
Varies
5,000
1
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
Trip Blank
Field Blank / FB
TABLE 2
BenzeneContaminant of
Concern
AcetoneAll Other SM 6200B AnalytesSUMMARY OF GROUNDWATER LABORATORY RESULTS —
STANDARD METHOD 6200B
NCDEQ; 5656_Kelly's Grocery; T2_GW Results
CATLIN Project No. 221050
CATLIN Engineers and Scientists
June 2023
Page 1 of 2
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Kelly's Grocery - 5656
Well
Type
Well/
Sample
ID
Date
Collected
(mm/dd/yy)
06/01/21 15 J <0.52 <7.5 10 3.8 0.96 J BMDL <0.60 ƚ <1.3 ƚ 63 6.4 J 26 6.8 6.9 J 150 18 BMDL 31 270 98 720 BMDL
12/02/21 7.6 J <0.26 <3.8 9.2 4.3 1.1 BMDL <0.30 ƚ <0.64 ƚ 44 <2.8 24 6.9 <3.2 93 L 13 BMDL 20 260 88 740 BMDL
07/21/22 <8.1 <0.80 <6.5 4.6 3.9 1.0 J <0.67 <0.68 ƚ <1.2 ƚ 32 <4.5 23 6.9 <5.1 100 13 BMDL 11 240 88 580 BMDL
04/12/23 <8.0 1.1 J <6.7 1.8 J 1.8 J 1.2 J <0.56 <0.64 ƚ <1.2 ƚ 20 <4.8 6.8 6.4 <5.3 98 3.4 <0.60 12 230 120 490 BMDL
06/01/21 25 J 34 <3.8 <0.28 <0.20 <0.18 BMDL <0.30 ƚ <0.64 ƚ 25 <2.8 1.4 <0.18 <3.2 13 0.96 J BMDL 200 25 10 197 BMDL
12/02/21 13 J 68 <3.8 0.98 J <0.20 <0.18 BMDL <0.30 ƚ <0.64 ƚ 27 <2.8 1.6 1.3 <3.2 13 L 1.1 BMDL 230 30 12 240 BMDL
07/21/22 20 J 340 8.0 J <0.61 <0.44 <0.52 <0.67 <0.68 ƚ 4.1 51 28 2.9 0.44 J 12 J 24 L 2.1 BMDL 590 62 29 470 BMDL
04/12/23 <20 350 49 J 3.9 J 4.0 J 2.3 J <1.4 <1.6 ƚ <3.0 ƚ 140 <12 25 4.1 J <13 150 20 2.3 J 860 440 220 1,680 BMDL
06/01/21 59 J 400 46 5.0 1.9 J <0.45 BMDL 1.9 J 13 92 32 14 4.8 16 J 130 12 BMDL 230 100 32 490 BMDL
12/02/21 79 J 720 150 8.8 4.7 J <0.90 BMDL 6.3 <3.2 ƚ 180 29 J 27 10 <16 130 L 28 BMDL 620 230 67 940 BMDL
07/21/22 64 J 1,900 120 13 5.3 <1.3 <1.7 38 40 290 120 43 13 54 270 L 42 BMDL 1,400 330 100 1,560 BMDL
04/12/23 <50 1,800 89 J 7.5 J 7.5 J <3.5 <3.5 38 <7.6 ƚ 560 <30 54 15 <33 610 54 <3.8 2,400 460 140 3,000 BMDL
06/01/21 2.5 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 3.6 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 3.0 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 2.5 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 4.8 J <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 4.8 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 0.27 J <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 3.7 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 2.8 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
40,000
40
30,500
70
11,700
25
100,000
100sec-Butylbenzenetert-Butylbenzene1,2-Dibromoethane (EDB)Toluene1,2-Dichloroethane EthylbenzeneChloroform1,3,5-TrimethylbenzeneTotal XylenesAll Other SM 6200B Analytes2-Hexanone (MBK)Isopropylbenzene (Cumene)p-Isopropyltoluene(p-Cymene)4-Methyl-2-pentanone (MIBK)Naphthalene n-Propylbenzene1,2,4-TrimethylbenzeneStyreneTABLE 3
Contaminant of
Concern
AcetoneBenzene2-Butanone (MEK)n-ButylbenzeneGCL (µg/L)
2L GWQS (µg/L) MonitoringMW-9
MW-8D
MW-7R
MW-6
MW-5
MW-4
MW-3R
MW-2
MW-1R
6,000,000
6,000
5,000
1
4,000,000
4,000
5,900
70
8,800
70
28,500
400
24,100
400
50,000
500
Varies
Varies
14,750
70
50
0.02
400
0.4
80,000
600
6,000
6
26,100
70
260,000
600
70,000
70
70,000
70
NCDEQ; 5656_Kelly's Grocery; T3_Historical GW
CATLIN Project No. 221050
CATLIN Engineers and Scientists
June 2023
Page 2 of 2
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Kelly's Grocery - 5656
Well
Type
Well/
Sample
ID
Date
Collected
(mm/dd/yy)sec-Butylbenzenetert-Butylbenzene1,2-Dibromoethane (EDB)Toluene1,2-Dichloroethane EthylbenzeneChloroform 1,3,5-TrimethylbenzeneTotal XylenesAll Other SM 6200B Analytes2-Hexanone (MBK)Isopropylbenzene (Cumene)p-Isopropyltoluene(p-Cymene)4-Methyl-2-pentanone (MIBK)Naphthalene n-Propylbenzene1,2,4-TrimethylbenzeneStyreneTABLE 3
Contaminant of
Concern
AcetoneBenzene2-Butanone (MEK)n-ButylbenzeneWSW-5 06/01/21 2.7 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 2.6 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
01/31/22 <2.0 0.83 <1.6 <0.15 <0.11 <0.13 BMDL <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
07/21/22 <2.0 4.0 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
04/12/23 <2.0 2.2 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
05/24/23 <2.0 0.29 J <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
06/01/21 2.4 J <0.13 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.270 BMDL
12/02/21 <2.4 0.94 <1.9 <0.14 <0.10 <0.090 BMDL <0.15 ƚ <0.32 <0.090 <1.4 <0.10 <0.090 <1.6 <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
01/31/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 BMDL <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
07/21/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 <0.17 ƚ <0.31 <0.21 <1.1 <0.11 <0.097 <1.3 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
05/24/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.22 <1.2 <0.15 <0.13 <1.3 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits)
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
< = Less than Method Detection Limit
ƚ = The Method Detection Limit is above the 2L GWQS.
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).
L = Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side (L-04 Flag).
WSW-7
Influent
WSW-7
EffluentPrivate Water Supply50
0.02
70,000
70
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
5,000
1
4,000,000
4,000
5,900
70
8,800
70
14,750
70
Varies
Varies
6,000
6
26,100
70
260,000
600
28,500
400
24,100
400
50,000
500
70,000
70
100,000
100
400
0.4
11,700
25
80,000
600
40,000
40
30,500
70
NCDEQ; 5656_Kelly's Grocery; T3_Historical GW
CATLIN Project No. 221050
CATLIN Engineers and Scientists
June 2023

NCDEQ; 5656_Kelly's Grocery.docx CATLIN Engineers and Scientists
CATLIN Project No. 221050 June 2023
ATTACHMENT E LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
May 30, 2023
Sean O’Neil
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
Project Location: Apex, NC
Client Job Number:
Project Number: 221050
Laboratory Work Order Number: 23E3445
Enclosed are results of analyses for samples as received by the laboratory on May 25, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 6
Sample Results 7
23E3445-01 7
23E3445-02 9
23E3445-03 11
23E3445-04 13
Sample Preparation Information 15
QC Data 16
Volatile Organic Compounds by GC/MS 16
B341609 16
Flag/Qualifier Summary 20
Certifications 21
Chain of Custody/Sample Receipt 23
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
5/30/2023
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
ATTN: Sean O’Neil
221050
23E3445
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Apex, NC
230524-3
WSW-7I 23E3445-01 Ground Water SM21-23 6200B
WSW-7E 23E3445-02 Ground Water SM21-23 6200B
FB 23E3445-03 Field Blank SM21-23 6200B
Trip Blank 23E3445-04 Trip Blank Water SM21-23 6200B
[TOC_1]Sample Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:23E3445-02WSW-7E
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E3445-01WSW-7I
DL
Benzene 0.29 0.50 g/L SM21-23 6200BJ0.18
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E3445-03FB
DL
Acetone 3.5 50 g/L SM21-23 6200BJ2.0
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23E3445-04Trip Blank
DL
Acetone 3.3 50 g/L SM21-23 6200BJ2.0
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-01
Field Sample #: WSW-7I
Sample Matrix: Ground Water
Sampled: 5/24/2023 11:46
[TOC_2]23E3445-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/29/23 15:54 EEHg/L2.0 5/29/23SM21-23 6200B1Acetone
0.29 0.50 5/29/23 15:54 EEHg/L0.18 5/29/23SM21-23 6200B1JBenzene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B1Bromobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.28 5/29/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/29/23 15:54 EEHg/L0.16 5/29/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/29/23 15:54 EEHg/L0.41 5/29/23SM21-23 6200B1Bromoform
ND 2.0 5/29/23 15:54 EEHg/L1.3 5/29/23SM21-23 6200B1Bromomethane
ND 5.0 5/29/23 15:54 EEHg/L1.7 5/29/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/29/23 15:54 EEHg/L0.13 5/29/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/29/23 15:54 EEHg/L0.16 5/29/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/29/23 15:54 EEHg/L0.12 5/29/23SM21-23 6200B1Chlorobenzene
ND 50 5/29/23 15:54 EEHg/L20 5/29/23SM21-23 6200B1Ethanol
ND 0.50 5/29/23 15:54 EEHg/L0.20 5/29/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/29/23 15:54 EEHg/L0.34 5/29/23SM21-23 6200B1Chloroethane
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B1Chloroform
ND 0.60 5/29/23 15:54 EEHg/L0.50 5/29/23SM21-23 6200B1Chloromethane
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/29/23 15:54 EEHg/L0.16 5/29/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/29/23 15:54 EEHg/L0.13 5/29/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.13 5/29/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.16 5/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/29/23 15:54 EEHg/L0.30 5/29/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/29/23 15:54 EEHg/L0.17 5/29/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/29/23 15:54 EEHg/L0.19 5/29/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/29/23 15:54 EEHg/L0.12 5/29/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/29/23 15:54 EEHg/L0.35 5/29/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/29/23 15:54 EEHg/L0.16 5/29/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/29/23 15:54 EEHg/L0.20 5/29/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/29/23 15:54 EEHg/L0.22 5/29/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/29/23 15:54 EEHg/L1.2 5/29/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/29/23 15:54 EEHg/L0.13 5/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/29/23 15:54 EEHg/L0.17 5/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/29/23 15:54 EEHg/L0.18 5/29/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/29/23 15:54 EEHg/L1.3 5/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-01
Field Sample #: WSW-7I
Sample Matrix: Ground Water
Sampled: 5/24/2023 11:46
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/29/23 15:54 EEHg/L0.38 5/29/23SM21-23 6200B1Naphthalene
ND 0.50 5/29/23 15:54 EEHg/L0.12 5/29/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B1Styrene
ND 0.50 5/29/23 15:54 EEHg/L0.14 5/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/29/23 15:54 EEHg/L0.17 5/29/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/29/23 15:54 EEHg/L0.22 5/29/23SM21-23 6200B1Toluene
ND 1.0 5/29/23 15:54 EEHg/L0.34 5/29/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.30 5/29/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/29/23 15:54 EEHg/L0.19 5/29/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/29/23 15:54 EEHg/L0.17 5/29/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/29/23 15:54 EEHg/L0.28 5/29/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/29/23 15:54 EEHg/L0.20 5/29/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/29/23 15:54 EEHg/L0.15 5/29/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/29/23 15:54 EEHg/L1.7 5/29/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/29/23 15:54 EEHg/L0.24 5/29/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/29/23 15:54 EEHg/L0.49 5/29/23SM21-23 6200B1m+p Xylene
ND 0.50 5/29/23 15:54 EEHg/L0.24 5/29/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 5/29/23 15:5470-130
Toluene-d8 102 5/29/23 15:5470-130
4-Bromofluorobenzene 95.5 5/29/23 15:5470-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-02
Field Sample #: WSW-7E
Sample Matrix: Ground Water
Sampled: 5/24/2023 12:07
[TOC_2]23E3445-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 5/29/23 16:21 EEHg/L2.0 5/29/23SM21-23 6200B1Acetone
ND 0.50 5/29/23 16:21 EEHg/L0.18 5/29/23SM21-23 6200B1Benzene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B1Bromobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.28 5/29/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/29/23 16:21 EEHg/L0.16 5/29/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/29/23 16:21 EEHg/L0.41 5/29/23SM21-23 6200B1Bromoform
ND 2.0 5/29/23 16:21 EEHg/L1.3 5/29/23SM21-23 6200B1Bromomethane
ND 5.0 5/29/23 16:21 EEHg/L1.7 5/29/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/29/23 16:21 EEHg/L0.13 5/29/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/29/23 16:21 EEHg/L0.16 5/29/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/29/23 16:21 EEHg/L0.12 5/29/23SM21-23 6200B1Chlorobenzene
ND 50 5/29/23 16:21 EEHg/L20 5/29/23SM21-23 6200B1Ethanol
ND 0.50 5/29/23 16:21 EEHg/L0.20 5/29/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/29/23 16:21 EEHg/L0.34 5/29/23SM21-23 6200B1Chloroethane
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B1Chloroform
ND 0.60 5/29/23 16:21 EEHg/L0.50 5/29/23SM21-23 6200B1Chloromethane
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/29/23 16:21 EEHg/L0.16 5/29/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/29/23 16:21 EEHg/L0.13 5/29/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.13 5/29/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.16 5/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/29/23 16:21 EEHg/L0.30 5/29/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/29/23 16:21 EEHg/L0.17 5/29/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/29/23 16:21 EEHg/L0.19 5/29/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/29/23 16:21 EEHg/L0.12 5/29/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/29/23 16:21 EEHg/L0.35 5/29/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/29/23 16:21 EEHg/L0.16 5/29/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/29/23 16:21 EEHg/L0.20 5/29/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/29/23 16:21 EEHg/L0.22 5/29/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/29/23 16:21 EEHg/L1.2 5/29/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/29/23 16:21 EEHg/L0.13 5/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/29/23 16:21 EEHg/L0.17 5/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/29/23 16:21 EEHg/L0.18 5/29/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/29/23 16:21 EEHg/L1.3 5/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-02
Field Sample #: WSW-7E
Sample Matrix: Ground Water
Sampled: 5/24/2023 12:07
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/29/23 16:21 EEHg/L0.38 5/29/23SM21-23 6200B1Naphthalene
ND 0.50 5/29/23 16:21 EEHg/L0.12 5/29/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B1Styrene
ND 0.50 5/29/23 16:21 EEHg/L0.14 5/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/29/23 16:21 EEHg/L0.17 5/29/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/29/23 16:21 EEHg/L0.22 5/29/23SM21-23 6200B1Toluene
ND 1.0 5/29/23 16:21 EEHg/L0.34 5/29/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.30 5/29/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/29/23 16:21 EEHg/L0.19 5/29/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/29/23 16:21 EEHg/L0.17 5/29/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/29/23 16:21 EEHg/L0.28 5/29/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/29/23 16:21 EEHg/L0.20 5/29/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/29/23 16:21 EEHg/L0.15 5/29/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/29/23 16:21 EEHg/L1.7 5/29/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/29/23 16:21 EEHg/L0.24 5/29/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/29/23 16:21 EEHg/L0.49 5/29/23SM21-23 6200B1m+p Xylene
ND 0.50 5/29/23 16:21 EEHg/L0.24 5/29/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 5/29/23 16:2170-130
Toluene-d8 101 5/29/23 16:2170-130
4-Bromofluorobenzene 95.8 5/29/23 16:2170-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-03
Field Sample #: FB
Sample Matrix: Field Blank
Sampled: 5/24/2023 12:24
[TOC_2]23E3445-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.5 50 5/29/23 9:32 EEHg/L2.0 5/29/23SM21-23 6200B1JAcetone
ND 0.50 5/29/23 9:32 EEHg/L0.18 5/29/23SM21-23 6200B1Benzene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B1Bromobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.28 5/29/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/29/23 9:32 EEHg/L0.16 5/29/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/29/23 9:32 EEHg/L0.41 5/29/23SM21-23 6200B1Bromoform
ND 2.0 5/29/23 9:32 EEHg/L1.3 5/29/23SM21-23 6200B1Bromomethane
ND 5.0 5/29/23 9:32 EEHg/L1.7 5/29/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/29/23 9:32 EEHg/L0.13 5/29/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/29/23 9:32 EEHg/L0.16 5/29/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/29/23 9:32 EEHg/L0.12 5/29/23SM21-23 6200B1Chlorobenzene
ND 50 5/29/23 9:32 EEHg/L20 5/29/23SM21-23 6200B1Ethanol
ND 0.50 5/29/23 9:32 EEHg/L0.20 5/29/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/29/23 9:32 EEHg/L0.34 5/29/23SM21-23 6200B1Chloroethane
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B1Chloroform
ND 0.60 5/29/23 9:32 EEHg/L0.50 5/29/23SM21-23 6200B1Chloromethane
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/29/23 9:32 EEHg/L0.16 5/29/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/29/23 9:32 EEHg/L0.13 5/29/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.13 5/29/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.16 5/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/29/23 9:32 EEHg/L0.30 5/29/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/29/23 9:32 EEHg/L0.17 5/29/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/29/23 9:32 EEHg/L0.19 5/29/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/29/23 9:32 EEHg/L0.12 5/29/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/29/23 9:32 EEHg/L0.35 5/29/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/29/23 9:32 EEHg/L0.16 5/29/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/29/23 9:32 EEHg/L0.20 5/29/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/29/23 9:32 EEHg/L0.22 5/29/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/29/23 9:32 EEHg/L1.2 5/29/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/29/23 9:32 EEHg/L0.13 5/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/29/23 9:32 EEHg/L0.17 5/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/29/23 9:32 EEHg/L0.18 5/29/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/29/23 9:32 EEHg/L1.3 5/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-03
Field Sample #: FB
Sample Matrix: Field Blank
Sampled: 5/24/2023 12:24
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/29/23 9:32 EEHg/L0.38 5/29/23SM21-23 6200B1Naphthalene
ND 0.50 5/29/23 9:32 EEHg/L0.12 5/29/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B1Styrene
ND 0.50 5/29/23 9:32 EEHg/L0.14 5/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/29/23 9:32 EEHg/L0.17 5/29/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/29/23 9:32 EEHg/L0.22 5/29/23SM21-23 6200B1Toluene
ND 1.0 5/29/23 9:32 EEHg/L0.34 5/29/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.30 5/29/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/29/23 9:32 EEHg/L0.19 5/29/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/29/23 9:32 EEHg/L0.17 5/29/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/29/23 9:32 EEHg/L0.28 5/29/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/29/23 9:32 EEHg/L0.20 5/29/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/29/23 9:32 EEHg/L0.15 5/29/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/29/23 9:32 EEHg/L1.7 5/29/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/29/23 9:32 EEHg/L0.24 5/29/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/29/23 9:32 EEHg/L0.49 5/29/23SM21-23 6200B1m+p Xylene
ND 0.50 5/29/23 9:32 EEHg/L0.24 5/29/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 5/29/23 9:3270-130
Toluene-d8 101 5/29/23 9:3270-130
4-Bromofluorobenzene 97.6 5/29/23 9:3270-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-04
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 5/24/2023 00:00
[TOC_2]23E3445-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.3 50 5/29/23 10:00 EEHg/L2.0 5/29/23SM21-23 6200B1JAcetone
ND 0.50 5/29/23 10:00 EEHg/L0.18 5/29/23SM21-23 6200B1Benzene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B1Bromobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.28 5/29/23SM21-23 6200B1Bromochloromethane
ND 0.50 5/29/23 10:00 EEHg/L0.16 5/29/23SM21-23 6200B1Bromodichloromethane
ND 0.50 5/29/23 10:00 EEHg/L0.41 5/29/23SM21-23 6200B1Bromoform
ND 2.0 5/29/23 10:00 EEHg/L1.3 5/29/23SM21-23 6200B1Bromomethane
ND 5.0 5/29/23 10:00 EEHg/L1.7 5/29/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B1n-Butylbenzene
ND 0.50 5/29/23 10:00 EEHg/L0.13 5/29/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 5/29/23 10:00 EEHg/L0.16 5/29/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 5/29/23 10:00 EEHg/L0.12 5/29/23SM21-23 6200B1Chlorobenzene
ND 50 5/29/23 10:00 EEHg/L20 5/29/23SM21-23 6200B1Ethanol
ND 0.50 5/29/23 10:00 EEHg/L0.20 5/29/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 5/29/23 10:00 EEHg/L0.34 5/29/23SM21-23 6200B1Chloroethane
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B1Chloroform
ND 0.60 5/29/23 10:00 EEHg/L0.50 5/29/23SM21-23 6200B1Chloromethane
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B12-Chlorotoluene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B14-Chlorotoluene
ND 0.50 5/29/23 10:00 EEHg/L0.16 5/29/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 5/29/23 10:00 EEHg/L0.13 5/29/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.13 5/29/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.16 5/29/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 5/29/23 10:00 EEHg/L0.30 5/29/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 5/29/23 10:00 EEHg/L0.17 5/29/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 5/29/23 10:00 EEHg/L0.19 5/29/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 5/29/23 10:00 EEHg/L0.12 5/29/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 5/29/23 10:00 EEHg/L0.35 5/29/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 5/29/23 10:00 EEHg/L0.16 5/29/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 5/29/23 10:00 EEHg/L0.20 5/29/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 5/29/23 10:00 EEHg/L0.22 5/29/23SM21-23 6200B1Ethylbenzene
ND 5.0 5/29/23 10:00 EEHg/L1.2 5/29/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 5/29/23 10:00 EEHg/L0.13 5/29/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 5/29/23 10:00 EEHg/L0.17 5/29/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 5/29/23 10:00 EEHg/L0.18 5/29/23SM21-23 6200B1Methylene Chloride
ND 5.0 5/29/23 10:00 EEHg/L1.3 5/29/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 5/25/2023
Work Order: 23E3445Sample Description:Project Location: Apex, NC
Sample ID: 23E3445-04
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 5/24/2023 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 5/29/23 10:00 EEHg/L0.38 5/29/23SM21-23 6200B1Naphthalene
ND 0.50 5/29/23 10:00 EEHg/L0.12 5/29/23SM21-23 6200B1n-Propylbenzene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B1Styrene
ND 0.50 5/29/23 10:00 EEHg/L0.14 5/29/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 5/29/23 10:00 EEHg/L0.17 5/29/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 5/29/23 10:00 EEHg/L0.22 5/29/23SM21-23 6200B1Toluene
ND 1.0 5/29/23 10:00 EEHg/L0.34 5/29/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.30 5/29/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 5/29/23 10:00 EEHg/L0.19 5/29/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 5/29/23 10:00 EEHg/L0.17 5/29/23SM21-23 6200B1Trichloroethylene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 5/29/23 10:00 EEHg/L0.28 5/29/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 5/29/23 10:00 EEHg/L0.20 5/29/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 5/29/23 10:00 EEHg/L0.15 5/29/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 5/29/23 10:00 EEHg/L1.7 5/29/23SM21-23 6200B1Vinyl Acetate
ND 0.50 5/29/23 10:00 EEHg/L0.24 5/29/23SM21-23 6200B1Vinyl Chloride
ND 1.0 5/29/23 10:00 EEHg/L0.49 5/29/23SM21-23 6200B1m+p Xylene
ND 0.50 5/29/23 10:00 EEHg/L0.24 5/29/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 5/29/23 10:0070-130
Toluene-d8 102 5/29/23 10:0070-130
4-Bromofluorobenzene 97.9 5/29/23 10:0070-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B341609 05/29/235 5.0023E3445-01 [WSW-7I]
B341609 05/29/235 5.0023E3445-02 [WSW-7E]
B341609 05/29/235 5.0023E3445-03 [FB]
B341609 05/29/235 5.0023E3445-04 [Trip Blank]
[TOC_1]Sample Preparation Information[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B341609 - SW-846 5030B
[TOC_3]B341609[TOC]
Blank (B341609-BLK1) Prepared & Analyzed: 05/29/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B341609 - SW-846 5030B
Blank (B341609-BLK1) Prepared & Analyzed: 05/29/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10626.6
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.424.4
LCS (B341609-BS1) Prepared & Analyzed: 05/29/23
Acetone g/L50 100 70-13084.484.4
Benzene g/L0.50 10.0 70-13011011.0
Bromobenzene g/L0.50 10.0 70-13010710.7
Bromochloromethane g/L0.50 10.0 70-13011711.7
Bromodichloromethane g/L0.50 10.0 70-13010610.6
Bromoform g/L0.50 10.0 70-13087.88.78
Bromomethane g/L2.0 10.0 60-14084.68.46
2-Butanone (MEK)g/L5.0 100 70-130106106
n-Butylbenzene g/L0.50 10.0 70-13010710.7
sec-Butylbenzene g/L0.50 10.0 70-13010310.3
tert-Butylbenzene g/L0.50 10.0 70-13010210.2
Carbon Tetrachloride g/L0.50 10.0 70-13010710.7
Chlorobenzene g/L0.50 10.0 70-13010010.0
Ethanol g/L50 100 70-13080.280.2
Chlorodibromomethane g/L0.50 10.0 70-13010110.1
Chloroethane g/L0.50 10.0 60-14095.39.53
Chloroform g/L0.50 10.0 70-13011211.2
Chloromethane g/L0.60 10.0 60-14083.38.33
2-Chlorotoluene g/L0.50 10.0 70-13095.69.56
4-Chlorotoluene g/L0.50 10.0 70-13010210.2
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010610.6
1,2-Dichlorobenzene g/L0.50 10.0 70-13010410.4
1,3-Dichlorobenzene g/L0.50 10.0 70-13010210.2
1,4-Dichlorobenzene g/L0.50 10.0 70-13098.69.86
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14082.88.28
1,1-Dichloroethane g/L0.50 10.0 70-13011811.8
1,2-Dichloroethane g/L0.50 10.0 70-13010310.3
1,1-Dichloroethylene g/L0.50 10.0 70-13083.38.33
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13011611.6
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13011111.1
1,2-Dichloropropane g/L0.50 10.0 70-13010910.9
1,3-Dichloropropane g/L0.50 10.0 70-13010910.9
2,2-Dichloropropane g/L0.50 10.0 70-13011511.5
1,1-Dichloropropene g/L0.50 10.0 70-13010910.9
cis-1,3-Dichloropropene g/L0.50 10.0 70-13011011.0
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010610.6
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B341609 - SW-846 5030B
LCS (B341609-BS1) Prepared & Analyzed: 05/29/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011311.3
Ethylbenzene g/L0.50 10.0 70-13010110.1
2-Hexanone (MBK)g/L5.0 100 70-130110110
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010110.1
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010010.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13010210.2
Methylene Chloride g/L5.0 10.0 70-13091.69.16
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130111111
Naphthalene g/L0.50 10.0 70-13093.79.37
n-Propylbenzene g/L0.50 10.0 70-13010210.2
Styrene g/L0.50 10.0 70-13010010.0
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010110.1
Tetrachloroethylene g/L0.50 10.0 70-13010310.3
Toluene g/L0.50 10.0 70-13010610.6
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13097.79.77
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13097.79.77
1,1,1-Trichloroethane g/L0.50 10.0 70-13011011.0
1,1,2-Trichloroethane g/L0.50 10.0 70-13010710.7
Trichloroethylene g/L0.50 10.0 70-13010410.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13078.97.89
1,2,3-Trichloropropane g/L0.50 10.0 70-13010710.7
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010210.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13097.19.71
Vinyl Acetate g/L20 100 70-130112112
Vinyl Chloride g/L0.50 10.0 60-14079.97.99
m+p Xylene g/L1.0 20.0 70-13010020.0
o-Xylene g/L0.50 10.0 70-13010210.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10626.6
g/L 25.0 70-130Surrogate: Toluene-d8 10125.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.3
LCS Dup (B341609-BSD1) Prepared & Analyzed: 05/29/23
Acetone g/L50 100 2570-13088.2 4.4788.2
Benzene g/L0.50 10.0 2570-130113 3.1411.3
Bromobenzene g/L0.50 10.0 2570-130108 1.1110.8
Bromochloromethane g/L0.50 10.0 2570-130120 2.2812.0
Bromodichloromethane g/L0.50 10.0 2570-130106 0.094110.6
Bromoform g/L0.50 10.0 2570-13089.4 1.818.94
Bromomethane g/L2.0 10.0 2560-14094.0 10.59.40
2-Butanone (MEK)g/L5.0 100 2570-130115 7.98115
n-Butylbenzene g/L0.50 10.0 2570-130107 0.37410.7
sec-Butylbenzene g/L0.50 10.0 2570-130105 1.7310.5
tert-Butylbenzene g/L0.50 10.0 2570-130104 2.2410.4
Carbon Tetrachloride g/L0.50 10.0 2570-130112 5.2911.2
Chlorobenzene g/L0.50 10.0 2570-130102 1.3910.2
Ethanol g/L50 100 2570-13087.8 9.0587.8
Chlorodibromomethane g/L0.50 10.0 2570-130103 2.3610.3
Chloroethane g/L0.50 10.0 2560-14091.6 3.969.16
Chloroform g/L0.50 10.0 2570-130114 2.0411.4
Chloromethane g/L0.60 10.0 2560-14087.2 4.578.72
2-Chlorotoluene g/L0.50 10.0 2570-13097.2 1.669.72
4-Chlorotoluene g/L0.50 10.0 2570-130105 2.5110.5
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B341609 - SW-846 5030B
LCS Dup (B341609-BSD1) Prepared & Analyzed: 05/29/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130105 0.19010.5
1,2-Dichlorobenzene g/L0.50 10.0 2570-130105 1.6310.5
1,3-Dichlorobenzene g/L0.50 10.0 2570-130104 1.9310.4
1,4-Dichlorobenzene g/L0.50 10.0 2570-130102 3.5910.2
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14084.4 1.918.44
1,1-Dichloroethane g/L0.50 10.0 2570-130121 1.9212.1
1,2-Dichloroethane g/L0.50 10.0 2570-130103 0.29210.3
1,1-Dichloroethylene g/L0.50 10.0 2570-13086.8 4.128.68
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130119 2.6411.9
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130114 2.2211.4
1,2-Dichloropropane g/L0.50 10.0 2570-130112 2.8111.2
1,3-Dichloropropane g/L0.50 10.0 2570-130109 0.18310.9
2,2-Dichloropropane g/L0.50 10.0 2570-130116 1.0411.6
1,1-Dichloropropene g/L0.50 10.0 2570-130115 5.6211.5
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130111 0.36211.1
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130109 2.6110.9
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130115 1.6611.5
Ethylbenzene g/L0.50 10.0 2570-130104 3.3110.4
2-Hexanone (MBK)g/L5.0 100 2570-130112 2.25112
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130103 2.0610.3
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130103 2.7610.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130104 1.6510.4
Methylene Chloride g/L5.0 10.0 2570-13095.0 3.649.50
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130113 1.08113
Naphthalene g/L0.50 10.0 2570-13096.6 3.059.66
n-Propylbenzene g/L0.50 10.0 2570-130104 2.2410.4
Styrene g/L0.50 10.0 2570-130103 3.2410.3
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130103 2.0610.3
Tetrachloroethylene g/L0.50 10.0 2570-130105 1.7310.5
Toluene g/L0.50 10.0 2570-130108 2.2510.8
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130101 3.3210.1
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13098.6 0.9179.86
1,1,1-Trichloroethane g/L0.50 10.0 2570-130115 4.7011.5
1,1,2-Trichloroethane g/L0.50 10.0 2570-130110 2.6711.0
Trichloroethylene g/L0.50 10.0 2570-130107 2.9510.7
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13081.2 2.878.12
1,2,3-Trichloropropane g/L0.50 10.0 2570-130112 4.3011.2
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130103 0.88010.3
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130100 3.0410.0
Vinyl Acetate g/L20 100 2570-130114 2.10114
Vinyl Chloride g/L0.50 10.0 2560-14081.4 1.868.14
m+p Xylene g/L1.0 20.0 2570-130103 3.2920.7
o-Xylene g/L0.50 10.0 2570-130105 2.3210.5
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10726.8
g/L 25.0 70-130Surrogate: Toluene-d8 10125.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.3
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
[TOC_1]Flag/Qualifier Summary[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
652North Carolina Div. of Water QualityNC 12/31/2023