MO-7369_36031_CA_MRP_20100917

Force Environmental Service Company, LLC
147 Vera Road Suite F, Lexington, South Carolina 29072 [phone] [phone]/ax
September 17, 2010
Mr. Scott Ryals, Hydro geologist
Division of Waste Management
NCDENR
1637 Mail Service Center
Raleigh, NC 27699-1637
Re: Cornelius Road Property; NCDENR Incident #36031
Cornelius Road and Charlotte Highway, Mooresville, NC
Dear Mr. Ryals:
t;?J -ii=,
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Force Environmental Service Company, LLC (Force Environmental) is pleased to submit
the results from the latest round of groundwater monitoring performed at the referenced facility.
This site was formerly a service station, but has been cleared and is now a vacant lot. In addition
to sampling four groundwater monitoring wells and a water supply well, the out-of-service on-
site water supply was abandoned on August 24, 2010 in accordance with the Iredell County
Health Department-Environmental Health Division Private Drinking Water Well Permit dated
April 13, 2010. A copy of the permit and the abandonment report are provided in Appendix E .
. wQ!LA~1_gust 19, ... ~010, monitoring wells .MW.::1~~,J~i:Y:?, ... ~~:.J1~~,.1!n~LJ\1W-4 were
sampled along with the water supply well WSW-Apventure 117. Groundwater samples were
collected from the monitoring wells using dedicated disposable bailers and a fresh pair of
disposable nitrile gloves was worn during the collection of each san1ple. Prior to sampling the
wells, well booms in monitoring wells MW-2 and MW-3R were removed and inspected, and the
'"•~~.,,.,m=•-,-•~¼""' "•~~'••---"""'~•--•~-•h"'e=~W~•>,=~<sm=•-~•e>J static water level in the monitoring wells was gauged using an electronic water level indicator.
The monitoring wells were then purged by bailing three well volumes of water using dedicated
disposable bailers.
The temperature, pH, and specific conductivity were measured to ensure the collection of
groundwater samples representative of surficial aquifer conditions prior to sampling. Since the
well booms had not been consumed to the point of replacement, they were returned to their
respective wells after sampling was completed. Field screening data is summarized in Appendix
D. The monitoring well gauging and elevation data is summarized in Table 1.
Cornelius Road Site
Incident #36031
I Force Environmental
Service Company, LLC
Table 1: Monitoring Well and Groundwater Data
Monitoring Screen Depth Screened roe Depth to Depth to GW
interval Elevation Water Product Elevation Well# (feet bgs) (feet) (feet) (ft btoc) (feet) (feet)
MW-1 36 26 to 36 98.00 NA NA
MW-1R 45 35 to 45 99.09 36.02 NA 63.07
MW-2 45 35 to 45 99.53 36.0 NA 63.53
MW-3 45 35 to 45 100.00 Destroyed NA Destroyed
M\.'IJ-3R 45 30 to 45 99.59 36.10 NA 63.49
MW-4 64.3 55 to 65 99.84 34.7 NA 65.14
bgs = below ground surface ft btoc = feet below top of casing NA= Not applicable
a e : a er T bl 2 Wt S uppy e aa I W llD t
Distance/
Water Supply Well Owner/User Physical Address Tax Direction Well Status Comments Wells Map# from / Use
source
US 21 and On-site dug
WSW-Site Goodman, Stanley F. Cornelius Rd., 77396797 Site Abandoned well
Mooresville, NC Abandoned
2811 8/25/10
WSW-117 117 Adventure 450-ft Well is used Adventure Rallis, Betty S Lane Mooresville, 4658548141 East Active for all needs Lane. NC, 28117
Samples collected from the monitoring wells and one water supply well (WSW Adventure
117) were transferred to appropriately labeled, laboratory supplied, 40-millilter (mi) volatile
organic analysis (VOA) vials, preserved with hydrochloric acid, placed into an iced cooler and
shipped with completed Chain of Custody documentation to Shealy Environmental Services, Inc.
(Shealy/NCDENR Certification Number 329) for analysis of Standard Method 6200B
constituents. The analytical results are summarized in Table 3. The analytical data report
prepared by Shealy is included in Appendix B and the field sampling data summary sheets are
included in Appendix C.
Cornelius Road Site
Incident #36031
2 Force Environmental
Service Company, LLC
NC 2L
Coe (µg/1) Standards
(µg/1)
Date Sampled NA
Benzene 1.0
n-Butylben~ene 70
sec-Butyl benzene 70
tert-8 utyl benzene 70
1,2-Dichloroethane 0.38
niic:.nprnpyl othor 70
Ethyl benzene 550
Hexachlorobutadiene
EDB 0.0004
lsopropylbenzene 70
p-lsopropyltoluene NA
MTBE 200
Naphthalene 21
n-Propylbenzene 70
Styrene 100
Toluene 1000
1,2,4-Trimethylbenzene 350
1,3,5-Trimethylbenzene 350
Total Xylenes 530
B = Detected in the method blank
J = Estimated result< PQL and 2: MDL
Coe (µg/1)
Date Sampled
Benzene
n-Butylbenzene
sec-Butyl benzene
tert-Butylbenzene
1,2-Dichloroethane
Diisopropyl ether
Ethyl benzene
EDB
lsopropylbenzene
p-lsopropyltoluene
MTBE
Naphthalene
n-Propylbenzene
Styrene
Toluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Total Xylenes
Cornelius Road Site
Incident #3603 I
a..1r, <'"JI l't\.l .C.L.
Standards
(µg/1)
NA
1.0
70
70
70
0.38
70
550
0.0004
70
NA
200
21
70
100
1000
350
350
530
Table 3: Analytical Results
MW-1
6/29/05 2/14/07 10/12/07 5/9/08 5/20/09
0.5 Dry Dry Dry Dry
NR Dry Dry Dry ~
Dry
NR Dry Dry Dry Dry
NR Dry Dry Dry Dry
ND Dry Dry Dry Dry
NR nn, Dry nn, Dry -·, -·,
NR Dry Dry Dry Dry
ND Dry Dry Dry Dry
NR Dry Dry Dry Dry
NR Dry Dry Dry Dry
1.8 Dry Dry Dry Dry
ND Dry Dry Dry Dry
NR Dry Dry Dry Dry
NR Dry Dry Dry Dry
0.36 Dry Dry Dry Dry
NR Dry Dry Dry Dry
NR Dry Dry Dry Dry
ND Dry Dry Dry Dry
MW-2
6/29/05 2/14/07 10/12/07 5/9/08 5/20/09
140 960 1030 1430 270
NR ND ND ND 6.4
NR ND ND ND <1.2
NR ND ND ND <1.4
42 220 261 543 200
NR 130 166 371 110
NR 250 292 439 110
19 110 164 278 69
NR 15 18.7 26.6 8.2
NR ND ND ND <1.3
51 360 487 1020 300
17 120 201 252 84
NR 30 34.6 60 18
NR 36 ND ND <1.3
140 2000 1960 2790 240
NR 330 443 598 180
NR ND 155 248 100
264 1810 2096 3230 950
3
MW-1R
11/5/09 2/12/10 8/19/10
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
<0.50 0.17BJ
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <0.50 <0.50
Dry <1.0 <0.50
-
11/5/09 2/12/10 8/19/10
294 91 79
<1.2 <0.50 <0.50
<1.2 <0.50 0.42 J
<1.2 <0.50 <0.50
201 <0.50 37
103 29 21
90.6 33 28
76.1 12 19
7.7 2.6 2.3
NS <0.50 0.38 J
305 64 70
79.4 19 39
12.4 4.7 4.0
9.3 <0.50 <0.50
297 5.0 110
155 53 50
73.1 30 21
814 261 235
"
Force Environmental
Service Company, LLC
NC 2L
Coe (µg/1) Standards
(µg/1)
Date Sampled NA
Benzene 1.0
n-Butylbenzene 70
sec-Butyl benzene 70
tert-Butylbenzene 70
1,2-Dichloroethane 0.38
Diisopropyl ether 70
Fthylht>n71>n1> 550
EDS 0.0004
lsopropylbenzene 70
p-lsopropyltoluene NA
MTBE 200
Naphthalene 21
n-Propylbenzene 70
Styrene 100
Toluene 1000
1,2,4-Trimethylbenzene 350
1,3,5-Trimethylbenzene 350
Total Xylenes 530
J = Estimated result< PQL and::,: MDL
NC 2L
Coe (µg/1) Standards
(µg/1)
Date Sampled NA
Benzene 1.0
n-Butylbenzene 70
sec-Butyl benzene 70
tert-Butylbenzene 70
1,2-Dichloroethane 0.38
Diisopropyl ether 70
Ethyl benzene 550
EDS 0.0004
1,4-Dichlorobenzene
Tetrachloroethene
lsopropylbenzene 70
p-lsopropyltoluene NA
MTBE 200
Naphthalene 21
n-Propylbenzene 70
Styrene 100
Toluene 1000
1,2,4.:: Tri methyl benzene 350
1,3,5-Trimethylbenzene 350
Total Xylenes 530
J = Estimated result< PQL and::,: MDL
Cornelius Road Site
Incident #36031
MW-3
6/29/05 2/14/07 10/12/07
ND 190 CNL
NR ND CNL
NR ND CNL
NR ND CNL
260 220 CNL
NR 140 CNL
NR 140 CNL
180 91 CNL
NR 14 CNL
NR ND CNL
250 170 CNL
360 75 CNL
NR 33 CNL
NR ND CNL
2500 940 CNL
NR 470 CNL
NR 280 CNL
3400 1870 CNL
6/29/05 2/14/07 10/12/07
ND ND CNL
NR ND CNL
NR ND CNL
NR ND CNL
ND <0.5 CNL
NR ND CNL
NR ND CNL
ND <0.5 CNL
NR ND CNL
NR ND CNL
ND ND CNL
ND ND CNL
NR ND CNL
NR ND CNL
ND ND CNL
NR ND CNL
NR ND CNL
ND ND CNL
4
5/9/08 5/20/09
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
CNL CNL
MW-4
5/9/08 5/20/09
ND <0.2
ND <0.20
ND <0.24
ND <0.28
ND <0.65
ND <0.21
ND <0.20
ND <0.42
ND <0.24
ND <0.26
ND <0.38
ND <0.39
ND <0.30
ND <0.26
ND <0.27
·~ ND <0.20
ND <0.25
ND <0.40
MW-3R
11/16/09 2/12/10 8/19/10
<0.5 <0.50 0.31 J
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
2.2 5.1 4.4
6.9 11 14
0.88 3.2 3.5
0.5 2.9 3.0
<0.5 <0.50 0.32 J
NS 1.9 2.2
5.0 13 16
<2.0 0.87 0.59
<0.5 0.61 0.43
<0.5 <0.50 <0.50
1.6 6.1 13
<0.5 5.1 9.8
5.9 25 32
9.4 37.1 70
11/5/09 2/12/10 8/19/10
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.5 <0.50 <0.50
<0.50 0.38 J
<0.50 0.33 J
<0.5 <0.50 <0.50
NS <0.50 <0.50
<0.5 <0.50 <0.50
<2.0 <0.50 <0.50
<5.0 <0.50 <0.50
<5.0 <0.50 <0.50
<5.0 <0.50 <0.50
<5.0 <0.50 <0.50
<5.0 <0.50 <0.50
<1.5 <1.0 <0.50 =
Force Environmental
Service Company, LLC
I!
!
NC2l WSW-117 Coe (1,19/t) Standards Adventure Rd {µg/1)
Date Sampled NA 10/12/07 5/09/08 5/20/09 11/5109
Benzene 1.0 5.5 ND <0.2 <0.5
n-Butylbenzene 70 ND ND <0,20 <0.5
sec-Butylbenzene 70 ND ND <0.24 <0.5
tert-Butylbenzene 70 ND ND <0.28 <0.5
1,2-Dichloroethane 0.38 29.6 ND <0.65 <0.5
Diisopropyl ether 70 16.8 ND <0,21 <0.5
Ethylbenzene 550 ND ND <0,20 <0.5
EDB 0.0004 1.8 ND <0,019 <0.5
lsopropylbenzene 70 ND ND <0.24 <0.5
p-lsopropyltoluene NA ND ND <0.26 NS
MTBE 200 ND ND <0.38 <0.5
Naphthalene 21 15.2 ND <0.39 <2.0
n-Propylbenzene 70 ND ND <0.30 <5.0
Styrene 100 ND ND <0.26 <5.0
Toluene 1000 0.53 ND <0.27 <5.0
1,2,4-Trimethylbenzene 350 1 ND <0.20 <5.0
1,3,5-Trimethylbenzene 350 ND ND <0.25 <5.0 --
Total Xylenes 530 4.7 ND <0.40 <1.5 . ··-----·
ND = Non Detect NS = Not Sampled NA = Not Applicable
Bold type indicates a reported concentration exceeding the respective NC2L Standard.
All data are expressed in micrograms per liter (Jig/I).
NR= Not t¥7ported in historical results
WSW-
Site
2/12/10 8119/10 314/10
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0,50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<0.50 <0.50 <0.50
<1.0 <0.50 <1.0 ! ·-·-
Thank you for your assistance with this project. A site plan and WSW location map,
analytical results, and field data sheets are appended for your review. Since benzene, 1,2 DCA,
EDB and Naphthalene were detected at concentrations greater than the NC 2L-Standards in
monitoring well MW-2 and 1,2 DCA, and EDB were detected at concentrations greater than the
NC 2L-Standards in monitoring well MW-3R, a Task Authorization (TA) Proposal to conduct a
semi-annual groundwater monitoring event is also enclosed. If you have questions regarding this
report or need additional infonnation, please do not hesitate to contact om office toll free at
[phone].
Sincerely,
FQR
1
r ~a;NMENTAL SERVICE CO.flif PANY, LLC
'\ Jr ~ um
f'i<eene Flee LG
Proj~ct olog~·
,,,/ "'\.fl-ti ,,/" ~-J
Greg Force '
Project Manager
Cornelius Road Site
Incident #36031
5 Force Environmental
Service Company, LLC
APPENDIX A
MAPS
~ 0 ;3-
" a::
Cl) ::, 'al E §,
.; a a Ol ~ JJ
.M. 0
N
ct Q ~~Wmt'i>'.'.,~&':W~S 2QQft
2 3, REFERENCE: Bose Ian for this drawin
0
hnabel
LEGEND
MONITORING WELL LOCATIONS
© Schnabel Engineering 2008 All Rights Reserved
C. 0 ::;
.3
vi
3: ~
" 0::
(I) .:!
oi E 0 :;, ,-.. 0 0 N
0
-::::. ,-..
-::::. N
WSW-124
CORNELIUS RD WSW-114
CORNELIUS RD
WSW-123
CORNELIUS
RD WSW-117
CORNELIUS
RD WSW-113
CORNELIUS
RD
WSW-108
CORNELIUS RD
SITE
WSW-2148
CHARLOTTE HWY
,f" .:i;-1:1 & ~ ~"'<' CT 2147
CHARLOTTE HWY
2161
CHARLOTTE HWY
WSW-2173
CHARLOTTE HWY
UNDER HIS
WINGS DAYCARE
2179
CHARLOTTE HWY
WSW-2186
CHARLOTTE HWY
hnabel
2187
CHARLOTTE HWY
ACTIVE
BP STATION
FORMER BROWN'S ,
STORE SERVICE
. STATION
"WSW-ADVENTURE
N
© Schnabel Engineering 2007 All Rights Reserved
APPENDIXB
LABORTARY DATA SHEETS
SHEALYENVIRONMENTAL SERVICES,JNC.
Report of Analysis
NCDENR-DWM-UST Section
1637 Mail Service Ctr.
Raleigh, NC 27699
Attention: Linda Blalock
Project Name: Cornelius Road Incident 36031
Lot Number:LH20021
Date Completed:08/26/2010
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 1 of 21
Level 1 Report v2.1
SC DHEC No: 32010
SHEALY ENVIRONMENTAL SERVICES, INC.
NELAC No: E87653
Case Narrative
NCDENR-DWM-UST Section
Lot Number: LH20021
NC DEHNR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
GC/MSVOC
The LCS/LCSD associated with batch 40921 recovered Dichlorodifluoro methane above QC limits. No corrective action was required as all
associated samples were Non-Detect for this compound.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 2 of 21
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Number
001
002
003
004
005
(5 samples)
Sample ID
MW-1R
MW-2
MW-3R
MW-4
WSW-ADVENTURE 117
Shealy Environmental Services, Inc.
Sample Summary
NCDENR-DWM-UST Section
Lot Number: LH20021
Matrix
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Date Sampled
08/19/2010 1445
08/19/2010 1500
08/19/2010 1430
08/19/2010 1400
08/19/2010 1415
Date Received
08/20/2010
08/20/2010
08/20/2010
08/20/2010
08/20/2010
Page: 3 of 21
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
NCDENR-DWM-UST Section
Lot Number: LH20021
Sample Sample ID Matrix Parameter Method Result Q
001 MW-1R Aqueous Hexachlorobutadiene SM 6200B 0.17 BJ
002 MW-2 Aqueous Benzene SM 6200B 79
002 MW-2 Aqueous sec-Butyl benzene SM 6200B 0.42 J
002 MW-2 Aqueous 1,2-Dibromoethane (EDB) SM 6200B 19
002 MW-2 Aqueous 1,2-Dichloroethane SM 6200B 37
002 M\AJ-2 ,~,queous Diisopropy! ether (!PE) SM 6200B 21
002 MW-2 Aqueous Ethyl benzene SM 6200B 28
002 MW-2 Aqueous lsopropylbenzene (Cumene) SM 6200B 2.3
002 MW-2 Aqueous p-lsopropyltoluene (p-Cymene) SM 6200B 0.38 J
002 MW-2 Aqueous Methyl tertiary butyl ether (MTBE) SM 6200B 70
002 MW-2 Aqueous Naphthalene SM 6200B 39
002 MW-2 Aqueous n-Propylbenzene SM 6200B 4.0
002 MW-2 Aqueous Toluene SM 6200B 110
002 MW-2 Aqueous 1,3,5-Trimethylbenzene (Mesitylene) SM 6200B 21
002 MW-2 Aqueous 1,2,4-Trimethylbenzene SM 6200B 50
002 MW-2 Aqueous m+p -Xylenes SM 6200B 150
002 MW-2 Aqueous o -Xylenes SM 6200B 85
003 MW-3R Aqueous Benzene SM 6200B 0.31 J
003 MW-3R Aqueous 1,2-Dibromoethane (EDB) SM 6200B 3.0
003 MW-3R Aqueous 1,2-Dichloroethane SM 6200B 4.4
003 MW-3R Aqueous Diisopropyl ether (!PE) SM 6200B 14
003 MW-3R Aqueous Ethyl benzene SM 6200B 3.5
003 MW-3R Aqueous lsopropylbenzene (Cumene) SM 6200B 0.32 J
003 MW-3R Aqueous p-lsopropyltoluene (p-Cymene) SM 6200B 2.2
003 MW-3R Aqueous Methyl tertiary butyl ether (MTBE) SM 6200B 16
003 MW-3R Aqueous Naphthalene SM 6200B 0.59
003 MW-3R Aqueous n-Propylbenzene SM 6200B 0.43 J
003 MW-3R Aqueous Toluene SM 6200B 13
003 MW-3R Aqueous 1,3,5-Trimethylbenzene (Mesitylene) SM 6200B 32
003 MW-3R Aqueous 1,2,4-Trimethylbenzene SM 6200B 9.8
003 MW-3R Aqueous m+p -Xylenes SM 6200B 20
003 MW-3R Aqueous o -Xylenes SM 6200B 50
004 MW-4 Aqueous 1,4-Dichlorobenzene SM 6200B 0.38 J
004 MW-4 Aqueous Tetrachloroethene SM 6200B 0.33 J
(34 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Units Page
ug/L 5
ug/L. 7
ug/L 7
ug/L 7
ug/L 7
ug/L 7
ug/L 7
ug/L 7
ug/L 7
ug/L 8
ug/L 8
ug/L 8
ug/L 8
ug/L 8
ug/L 8
ug/L 8
ug/L 8
ug/L 9
ug/L 9
ug/L 9
ug/L 9
ug/L 9
ug/L 9
ug/L 9
ug/L 10
ug/L 10
ug/L 10
ug/L. 10
ug/L 10
ug/L 10
ug/L 10
ug/L 10
ug/L 11
ug/L 12
Page: 4 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-001
Description: MW-1 R Matrix: Aqueous
Date Sampled :08/19/201 O 1445
Date Received: 08/20/2010
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0209 DLB
GAS Analytical
Parameter Number Method
Benzene 71-43-2 SM 6200B
Bromobenzene 108-86-1 SM 6200B
Bromochloromethane 74-97-5 SM 6200B
Bromodichloromethane 75-27-4 SM 6200B
Bromoform 75-25-2 SM 6200B
Bromomethane (Methyl bromide) 74-83-9 SM 6200B
n-Butylbenzene 104-51-8 SM 6200B
sec-Butylbenzene 135-98-8 SM 6200B
tert-Butylbenzene 98-06-6 SM 6200B
Carbon tetrachloride 56-23-5 SM 6200B
Chlorobenzene 108-90-7 SM 6200B
Chloroethane 75-00-3 SM 6200B
Chloroform 67-66-3 SM 6200B
Chloromethane (Methyl chloride) 74-87-3 SM 6200B
2-Chlorotoluene 95-49-8 SM 6200B
4-Chlorotoluene 106-43-4 SM 6200B
Dibromochloromethane 124-48-1 SM 6200B
1,2-Dibromoethane (EDB) 106-93-4 SM 6200B
Dibromomethane (Methylene bromide) 74-95-3 SM 6200B
1,2-Dichlorobenzene 95-50-1 SM 6200B
1,3-Dichlorobenzene 541-73-1 SM 6200B
1,4-Dichlorobenzene 106-46-7 SM 6200B
Dichlorodifluoromethane 75-71-8 SM 6200B
1, 1-Dichloroethane 75-34-3 SM 6200B
1,2-Dichloroethane 107-06-2 SM 6200B
1, 1-Dichloroethene 75-35-4 SM 6200B
cis-1 ,2-Dichloroethene 156-59-2 SM 6200B
trans-1,2-Dichloroethene 156-60-5 SM 6200B
1,2-Dichloropropane 78-87-5 SM 6200B
1,3-Dichloropropane 142-28-9 SM 6200B
2,2-Dichloropropane 594-20-7 SM 6200B
1, 1-Dichloropropene 563-58-6 SM 6200B
cis-1,3-Dichloropropene 10061-01-5 SM 6200B
trans-1,3-Dichloropropene 10061-02-6 SM 6200B
Diisopropyl ether (IPE) 108-20-3 SM 6200B
Ethanol 64-17-5 SM 6200B
Ethylbenzene 100-41-4 SM 6200B
Hexachlorobutadiene 87-68-3 SM 62008
lsopropylbenzene (Cumene) 98-82-8 SM 6200B
p-lsopropyltoluene (p-Cymene) 99-87-6 SM 6200B
POL= Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and.':: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.027 ug/L
ND 0.50 0.027 ug/L
ND 0.50 0.055 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.010 ug/L
ND 0.50 0.20 ug/L
ND 0.50 0.017 ug/L
ND 0.50 0.010 ug/L
ND 0.50 0.037 ug/L
ND 0.50 0.085 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.059 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.061 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.071 ug/L
ND 0.50 0.054 ug/L
ND 0.50 0.023 ug/L
ND 0.50 0.094 ug/l.
ND 0.50 0.087 ug/l.
ND 0.50 0.079 ug/L
ND 0.50 0.081 ug/l.
ND 0.50 0.019 ug/l.
ND 0.50 0.060 ug/L
ND 0.50 0.074 ug/L
ND 0.50 0.090 ug/L
ND 0.50 0.18 ug/l.
ND 0.50 0.052 ug/l.
ND 100 33 ug/L
ND 0.50 0.17 ug/L
0.17 BJ 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.018 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The RPO between two GC columns exceeds 40%
Run
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 5 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section
Description: MW-1R
Date Sampled:08/19/201 O 1445
Date Received: 08/20/201 O
Laboratory ID: LH20021-001
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0209 DLB
CAS Analytical
Parameter Number Method
Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B
Methylene chloride 75-09-2 SM 6200B
Naphthalene 91-20-3 SM 6200B
n-Propylbenzene 103-65-1 SM 6200B
Styrene ·100-42-5 Sivi 62008
1, 1, 1,2-Tetrachloroethane 630-20-6 SM 6200B
1, 1,2,2-Tetrachloroethane 79-34-5 SM 6200B
Tetrachloroethene 127-18-4 SM 6200B
Toluene 108-88-3 SM 6200B
1, 1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B
1,2, 3-Trichlorobenzene 87-61-6 SM 6200B
1,2,4-Trichlorobenzene 120-82-1 SM 6200B
1, 1, 1-Trichloroethane 71-55-6 SM 6200B
1, 1,2-Trichloroethane 79-00-5 SM 6200B
Trichloroethene 79-01-6 SM 6200B
Trichlorofluoromethane 75-69-4 SM 6200B
1,2,3-Trichloropropane 96-18-4 SM 6200B
1,3,5-Trimethylbenzene (Mesitylene) 108-67-8 SM 6200B
1,2,4-T rimethylbenzene 95-63-6 SM 6200B
Vinyl chloride 75-01-4 SM 6200B
m+p -Xylenes 179601-23-1 SM 6200B
o -Xylenes 95-47-6 SM 6200B
Run 1 Acceptance Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 52-138
Bromofluorobenzene 111 70-147
Toluene-dB 99 76-125
POL= Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result < POL and .': MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.015 ug/L
ND 0.50 0.057 ug/L
ND 0.50 0.013 ug/L
ND 0.50 0.014 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.30 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.031 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.051 ug/L
ND 0.50 0.33 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.065 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Run
l
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 6 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-002
Description: MW-2 Matrix: Aqueous
Date Sampled:08/19/2010 1500
Date Received: 08/20/201 O
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0502 DLB
CAS Analytical
Parameter Number Method
Benzene 71-43-2 SM 6200B
Bromobenzene 108-86-1 SM 6200B
Bromochloromethane 74-97-5 SM 6200B
Bromodichloromethane 75-27-4 SM 6200B
Bromoform 75-25-2 SM 6200B
Bromomethane (Methyl bromide) 74-83-9 SM 6200B
n-Butylbenzene 104-51-8 SM 6200B
sec-Buty !benzene 135-98-8 SM 62008
tert-Butylbenzene 98-06-6 SM 6200B
Carbon tetrachloride 56-23-5 SM 6200B
Chlorobenzene 108-90-7 SM 6200B
Chloroethane 75-00-3 SM 6200B
Chloroform 67-66-3 SM 6200B
Chloromethane (Methyl chloride) 74-87-3 SM 6200B
2-Chlorotoluene 95-49-8 SM 6200B
4-Chlorotoluene 106-43-4 SM 6200B
Dibromochloromethane 124-48-1 SM 6200B
1,2-Dibromoethane (EDB) 106-93-4 SM 62008
Dibromomethane (Methylene bromide) 74-95-3 SM 6200B
1,2-Dichlorobenzene 95-50-1 SM 6200B
1 ,3-Dichlorobenzene 541-73-1 SM 6200B
1,4-Dichlorobenzene 106-46-7 SM 6200B
Dichlorodifluoromethane 75-71-8 SM 6200B
1, 1-Dichloroethane 75-34-3 SM 6200B
1,2-Dichloroethane 107-06-2 SM 62008
1, 1-Dichloroethene 75-35-4 SM 6200B
cis-1,2-Dichloroethene 156-59-2 SM 6200B
trans-1,2-Dichloroethene 156-60-5 SM 6200B
1,2-Dichloropropane 78-87-5 SM 6200B
1,3-Dichloropropane 142-28-9 SM 6200B
2,2-Dichloropropane 594-20-7 SM 6200B
1, 1-Dichloropropene 563-58-6 SM 6200B
cis-1,3-Dichloropropene 10061-01-5 SM 6200B
trans-1,3-Dichloropropene 10061-02-6 SM 6200B
Diisopropyl ether (IPE) 108-20-3 SM 6200B
Ethanol 64-17-5 SM 6200B
Ethyl benzene 100-41-4 SM 62008
Hexachlorobutadiene 87-68-3 SM 6200B
lsopropylbenzene (Cumene) 98-82-8 SM 6200B
p-lsopropyltoluene (p-Cymene) 99-87-6 SM 6200B
POL= Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and.?: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
79 0.50 0.027 ug/L
ND 0.50 0.027 ug/L
ND 0.50 0.055 ug/L
ND 0.50 0.17 ug/L
ND 0.50 O.OiO ug/L
ND 0.50 0.20 ug/L
ND 0.50 0.017 ug/L
0.42 J 0.50 0.010 ug/L
ND 0.50 0.037 ug/L
ND 0.50 0.085 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.059 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/1..
19 0.50 0.061 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.071 ug/L
ND 0.50 0.054 ug/L
37 0.50 0.023 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.087 ug/L
ND 0.50 0.079 ug/L
ND 0.50 0.081 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.060 ug/L.
ND 0.50 0.074 ug/L
ND 0.50 0.090 ug/L
ND 0.50 0.18 ug/L
21 0.50 0.052 ug/L
ND 100 33 ug/L
28 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
2.3 0.50 0.029 ug/L
0.38 J 0.50 0.018 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The RPO between two GC columns exceeds 40%
Run
1
1
1
1
1
1
1
1
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 7 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section
Description: MW-2
Date Sampled:08/19/201 O 1500
Date Received:08/20/2010
Laboratory ID: LH20021-002
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0502 DLB
CAS Analytical
Parameter Number Method
Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B
Methylene chloride 75-09-2 SM 6200B
Naphthalene 91-20-3 SM 6200B
n-Propylbenzene 103-65-1 SM 6200B
Styrene 100-42-5 SM 6200B
1, 1, 1,2-Tetrachloroethane 630-20-6 SM 6200B
1, 1,2,2-Tetrachloroethane 79-34-5 SM 6200B
Tetrachloroethene 127-18-4 SM 62008
Toluene 108-88-3 SM 6200B
1, 1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B
1,2,3-Trichlorobenzene 87-61-6 SM 62008
1,2,4-Trichlorobenzene 120-82-1 SM 62008
1, 1, 1-Trichloroethane 71-55-6 SM 62008
1, 1,2-Trichloroethane 79-00-5 SM 6200B
Trichloroethene 79-01-6 SM 62008
Trichlorofluoromethane 75-69-4 SM 62008
1,2,3-Trichloropropane 96-18-4 SM 6200B
1,3,5-Trimethylbenzene (Mesitylene) 108-67-8 SM 6200B
1,2,4-Trimethylbenzene 95-63-6 SM 6200B
Vinyl chloride 75-01-4 SM 6200B
m+p -Xylenes 179601-23-1 SM 6200B
o -Xylenes 95-47-6 SM 6200B
Run 1 Acceotance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 52-138
8romofluorobenzene 119 70-147
Toluene-dB 107 76-125
POL = Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and.:.: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
70 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
39 0.50 0.17 ug/L
4.0 0.50 0.024 ug/L
ND 0.50 0.015 ugil
ND 0.50 0.057 ug/L
ND 0.50 0.013 ug/L
ND 0.50 0.014 ug/L
110 0.50 0.17 ug/L
ND 0.50 0.30 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.031 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.051 ug/L
ND 0.50 0.33 ug/L
21 0.50 0.17 ug/L
50 0.50 0.17 ug/L
ND 0.50 0.065 ug/L
150 0.50 0.17 ug/L
85 0.50 0.17 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The RPO between two GC columns exceeds 40%
Run
1
1
1
1
1
1
1
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 8 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-003
Description: MW-3R Matrix: Aqueous
Date Sampled:08/19/2010 1430
Date Received: 08/20/201 O
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0230 DL8
GAS Analytical
Parameter Number Method
Benzene 71-43-2 SM 62008
Bromobenzene 108-86-1 SM 62008
8romochloromethane 74-97-5 SM 62008
8romodichloromethane 75-27-4 SM 62008
Bromoform 75-25-2 SM 62008
8romomethane (Methyl bromide) 74-83-9 SM 62008
n-8utylbenzene 104-51-8 SM 62008
sec-8utylbenzene 135-98-8 SM 6200B
tert-8utylbenzene 98-06-6 SM 62008
Carbon tetrachloride 56-23-5 SM 62008
Chlorobenzene 108-90-7 SM 62008
Chloroethane 75-00-3 SM 62008
Chloroform 67-66-3 SM 62008
Chloromethane (Methyl chloride) 74-87-3 SM 62008
2-Chlorotoluene 95-49-8 SM 62008
4-Chlorotoluene 106-43-4 SM 62008
Dibromochloromethane 124-48-1 SM 62008
1,2-Dibromoethane (EDS) 106-93-4 SM 62008
Dibromomethane (Methylene bromide) 74-95-3 SM 62008
1,2-Dichlorobenzene 95-50-1 SM 62008
1,3-Dichlorobenzene 541-73-1 SM 62008
1,4-Dichlorobenzene 106-46-7 SM 62008
Dichlorodifluoromethane 75-71-8 SM 62008
1, 1-Dichloroethane 75-34-3 SM 62008
1,2-Dichloroethane 107-06-2 SM 62008
1, 1-Dichloroethene 75-35-4 SM 62008
cis-1,2-Dichloroethene 156-59-2 SM 62008
trans-1,2-Dichloroethene 156-60-5 SM 62008
1,2-Dichloropropane 78-87-5 SM 62008
1,3-Dichloropropane 142-28-9 SM 62008
2,2-Dichloropropane 594-20-7 SM 62008
1, 1-Dichloropropene 563-58-6 SM 62008
cis-1,3-Dichloropropene 10061-01-5 SM 62008
trans-1,3-Dichloropropene 10061-02-6 SM 62008
Diisopropyl ether (IPE) 108-20-3 SM 62008
Ethanol 64-17-5 SM 62008
Ethylbenzene 100-41-4 SM 62008
Hexachlorobutadiene 87-68-3 SM 62008
lsopropylbenzene (Cumene) 98-82-8 SM 62008
p-lsopropyltoluene (p-Cymene) 99-87-6 SM 62008
POL= Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and!: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
0.31 J 0.50 0.027 ug/L
ND 0.50 0.027 ug/L
ND 0.50 0.055 ug/L
ND 0.50 0.17 ug/L
ND 0.50 O.OiO ugil
ND 0.50 0.20 ug/L
ND 0.50 0.017 ug/L
ND 0.50 0.010 ug/L
ND 0.50 0.037 ug/L
ND 0.50 0.085 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.059 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
3.0 0.50 0.061 ug/L.
ND 0.50 0.094 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.071 ug/L
ND 0.50 0.054 ug/L
4.4 0.50 0.023 ug/L.
ND 0.50 0.094 ug/L
ND 0.50 0.087 ug/L
ND 0.50 0.079 ug/L
ND 0.50 0.081 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.060 ug/L
ND 0.50 0.074 ug/L
ND 0.50 0.090 ug/L
ND 0.50 0.18 ug/L
14 0.50 0.052 ug/L
ND 100 33 ug/L
3.5 0.50 0.17 ug/L
ND 0.50 0,17 ug/L
0.32 J 0.50 0.029 ug/L
2.2 0.50 0.018 ug/L
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Run
1
1
1
1
1
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 9 of 21
· Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-003
Description: MW-3R Matrix: Aqueous
Date Sampled:08/19/2010 1430
Date Received: 08/20/201 O
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0230 DLB
CAS Analytical
Parameter Number Method
Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 62008
Methylene chloride 75-09-2 SM 6200B
Naphthalene 91-20-3 SM 6200B
n-Propylbenzene 103-65-1 SM 62008
Styrene 100-42-5 SM 6200B
1, 1, 1,2-Tetrachloroethane 630-20-6 SM 6200B
1, 1,2,2-Tetrachloroethane 79-34-5 SM 6200B
Tetrachloroethene 127-18-4 SM 6200B
Toluene 108-88-3 SM 62008
1, 1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B
1,2,3-Trichlorobenzene 87-61-6 SM 6200B
1,2,4-Trichlorobenzene 120-82-1 SM 6200B
1, 1, 1-Trichloroethane 71-55-6 SM 6200B
1, 1,2-Trichloroethane 79-00-5 SM 6200B
Trichloroethene 79-01-6 SM 6200B
Trichlorofluoromethane 75-69-4 SM 6200B
1,2, 3-Trichloropropane 96-18-4 SM 6200B
1,3,5-Trimethylbenzene (Mesitylene) 108-67-8 SM 62008
1,2,4-Trimethylbenzene 95-63-6 SM 62008
Vinyl chloride 75-01-4 SM 6200B
m+p -Xylenes 179601-23-1 SM 62008
o -Xylenes 95-47-6 SM 62008
Run 1 Acceptance Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 96 52-138
Bromofluorobenzene 114 70-147
Toluene-dB 103 76-125
PQL = Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< PQL and.:: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
16 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
0.59 0.50 0.17 ug/L
0.43 J 0.50 0.024 ug/L
i'>JD 0.50 0.015 ug/L
ND 0.50 0.057 ug/L
ND 0.50 0.013 ug/L
ND 0.50 0.014 ug/L
13 0.50 0.17 ug/L
ND 0.50 0.30 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.031 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.051 ug/L
ND 0.50 0.33 ug/L
32 0.50 0.17 ug/L
9.8 0.50 0.17 ug/L
ND 0.50 0.065 ug/L
20 0.50 0.17 ug/L
50 0.50 0.17 ug/L
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Run
1
1
1
1
1
1
1
1
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a '"W" N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 10 of 21
Level 1 R1eport v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-004
Description: MW-4 Matrix: Aqueous
Date Sampled:08/19/2010 1400
Date Received: 08/20/2010
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0252 DLB
GAS Analytical
Parameter Number Method
Benzene 71-43-2 SM 6200B
Bromobenzene 108-86-1 SM 6200B
Bromochloromethane 74-97-5 SM 6200B
Bromodichloromethane 75-27-4 SM 6200B
Bromoform 75-25-2 SM 6200B
Bromomethane (Methyl bromide) 74-83-9 SM 6200B
n-Butylbenzene 104-51-8 SM 6200B
sec-Butylbenzene 135-98-8 SM 6200B
tert-Butylbenzene 98-06-6 SM 6200B
Carbon tetrachloride 56-23-5 SM 6200B
Chlorobenzene 108-90-7 SM 6200B
Chloroethane 75-00-3 SM 6200B
Chloroform 67-66-3 SM 6200B
Chloromethane (Methyl chloride) 74-87-3 SM 6200B
2-Chlorotoluene 95-49-8 SM 6200B
4-Chlorotoluene 106-43-4 SM 6200B
Dibromochloromethane 124-48-1 SM 6200B
1,2-Dibromoethane (EDB) 106-93-4 SM 6200B
Dibromomethane (Methylene bromide) 74-95-3 SM 6200B
1,2-Dichl~robenzene 95-50-1 SM 6200B
1,3-Dichlorobenzene 541-73-1 SM 6200B
1,4-Dichlorobenzene 106-46-7 SM 62008
Dichlorodifluoromethane 75-71-8 SM 6200B
1, 1-Dichloroethane 75-34-3 SM 6200B
1,2-Dichloroethane 107-06-2 SM 6200B
1, 1-Dichloroethene 75-35-4 SM 6200B
cis-1 ,2-Dichloroethene 156-59-2 SM 6200B
trans-1,2-Dichloroethene 156-60-5 SM 6200B
1,2-Dichloropropane 78-87-5 SM 6200B
1,3-Dichloropropane 142-28-9 SM 6200B
2,2-Dichloropropane 594-20-7 SM 6200B
1, 1-Dichloropropene 563-58-6 SM 6200B
cis-1,3-Dichloropropene 10061-01-5 SM 6200B
trans-1,3-Dichloropropene 10061-02-6 SM 6200B
Diisopropyl ether (IPE) 108-20-3 SM 6200B
Ethanol 64-17-5 SM 6200B
Ethylbenzene 100-41-4 SM 6200B
Hexachlorobutadiene 87-68-3 SM 6200B
lsopropylbenzene (Cumene) 98-82-8 SM 6200B
p-lsopropyltoluene (p-Cymene) 99-87-6 SM 6200B
PQL = Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< PQL and:': MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.027 ug/L
ND 0.50 0.027 ug/L
ND 0.50 0.055 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.010 ug/L
ND 0.50 0.20 ug/L
ND 0.50 0.017 ug/L
ND 0,50 0.010 ug/L
ND 0.50 0.037 ug/L
ND 0.50 0.085 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.059 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.061 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L
0.38 J 0.50 0.17 ug/L
ND 0.50 0.071 ug/L
ND 0.50 0.054 ug/L.
ND 0.50 0.023 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.087 ug/L
ND 0.50 0.079 ug/L.
ND 0.50 0.081 ug/L
ND 0.50 0.019 ug/L.
ND 0.50 0.060 ug/L
ND 0.50 0.074 ug/L
ND 0.50 0.090 ug/L
ND 0.50 0.18 ug/L
ND 0.50 0.052 ug/L
ND 100 33 ug/L.
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L.
ND 0.50 0.029 ug/L
ND 0.50 0.018 ug/L
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Run
1
1
W11ere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 11 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-004
Description: MW-4 Matrix: Aqueous
Date Sampled:08/19/2010 1400
Date Received:08/20/2010
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0252 DLB
CAS Analytical
Parameter Number Method
Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B
Methylene chloride 75-09-2 SM 6200B
Naphthalene 91-20-3 SM 6200B
n-Propylbenzene 103-65-1 SM 6200B
Styrene 100-42-5 SM 6200B
1, 1, 1,2-Tetrachloroethane 630-20-6 SM 6200B
1, 1,2,2-Tetrachloroethane 79-34-5 SM 6200B
Tetrachloroethene 127-18-4 SM 6200B
Toluene 108-88-3 SM 6200B
1, 1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B
1,2,3-Trichlorobenzene 87-61-6 SM 6200B
1,2, 4-Trichlorobenzene 120-82-1 SM 6200B
1, 1, 1-Trichloroethane 71-55-6 SM 6200B
1, 1,2-Trichloroethane 79-00-5 SM 6200B
Trichloroethene 79-01-6 SM 6200B
Trichlorofluoromethane 75-69-4 SM 6200B
1,2,3-Trichloropropane 96-18-4 SM 6200B
1,3,5-Trimethylbenzene (Mesitylene) 108-67-8 SM 6200B
1,2,4-Trimethylbenzene 95-63-6 SM 6200B
Vinyl chloride 75-01-4 SM 6200B
m+p -Xylenes 179601-23-1 SM 6200B
o -Xylenes 95-47-6 SM 6200B
Run 1 .drropt::1nr..A-
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 52-138
Bromofluorobenzene 115 70-147
Toluene-dB 103 76-125
POL = Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and.". MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.015 ug/L
ND 0.50 0.057 ug/L
ND 0.50 0.013 ug/L
0.33 J 0.50 0.014 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.30 ug/L.
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L.
ND 0.50 0.031 ug/L
ND 0.50 0.024 ug/L.
ND 0.50 0.051 ug/L
ND 0.50 0.33 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.065 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L
E ;:: Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Run
1
1
1
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 12 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section Laboratory ID: LH20021-005
Description: WSW-ADVENTURE 117 Matrix: Aqueous
Date Sampled:08/19/2010 1415
Date Received: 08/20/201 O
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0314 DLB
CAS Analytical
Parameter Number Method
Benzene 71-43-2 SM 6200B
Bromobenzene 108-86-1 SM 6200B
Bromochloromethane 74-97-5 SM 6200B
Bromodichloromethane 75-27-4 SM 6200B
Bromoform 75-25-2 Siv1 6200B
Bromomethane (Methyl bromide) 74-83-9 SM 6200B
n-Butylbenzene 104-51-8 SM 6200B
sec-Butylbenzene 135-98-8 SM 6200B
tert-Butylbenzene 98-06-6 SM 6200B
Carbon tetrachloride 56-23-5 SM 6200B
Chlorobenzene 108-90-7 SM 6200B
Chloroethane 75-00-3 SM 6200B
Chloroform 67-66-3 SM 6200B
Chloromethane (Methyl chloride) 74-87-3 SM 6200B
2-Chlorotoluene 95-49-8 SM 6200B
4-Chlorotoluene 106-43-4 SM 6200B
Dibromochloromethane 124-48-1 SM 6200B
1,2-Dibromoethane (EDB) 106-93-4 SM 6200B
Dibromomethane (Methylene bromide) 74-95-3 SM 6200B
1,2-Dichlorobenzene 95-50-1 SM 6200B
1,3-Dichlorobenzene 541-73-1 SM 6200B
1,4-Dichlorobenzene 106-46-7 SM 6200B
Dichlorodifluoromethane 75-71-8 SM 6200B
1, 1-Dichloroethane 75-34-3 SM 62008
1,2-Dichloroethane 107-06-2 SM 6200B
1, 1-Dichloroethene 75-35-4 SM 6200B
cis-1,2-Dichloroethene 156-59-2 SM 6200B
trans-1,2-Dichloroethene 156-60-5 SM 6200B
1,2-Dichloropropane 78-87-5 SM 6200B
1,3-Dichloropropane 142-28-9 SM 6200B
2,2-Dichloropropane 594-20-7 SM 6200B
1, 1-Dichloropropene 563-58-6 SM 6200B
cis-1,3-Dichloropropene 10061-01-5 SM 6200B
trans-1,3-Dichloropropene 10061-02-6 SM 6200B
Diisopropyl ether (IPE) 108-20-3 SM 6200B
Ethanol 64-17-5 SM 6200B
Ethylbenzene 100-41-4 SM 6200B
Hexachlorobutadiene 87-68-3 SM 6200B
lsopropylbenzene (Cumene) 98-82-8 SM 6200B
p-lsopropyltoluene (p-Cymene) 99-87-6 SM 6200B
POL= Practical quantitation limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result< POL and;: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.027 ug/L
ND 0.50 0.027 ug/L
ND 0.50 0.055 ug/L
ND 0.50 0.17 ug/L
~~D 0.50 0.010 ug/L
ND 0.50 0.20 ug/L
ND 0.50 0.017 ug/L
ND 0.50 0.010 ug/L
ND 0.50 0.037 ug/L
ND 0.50 0.085 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L.
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.059 ug/L.
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L.
ND 0.50 0.061 ug/L
ND 0.50 0.094 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.071 ug/L
ND 0.50 0.054 ug/L
ND 0.50 0.023 ug/L
ND 0.50 0.094 ug/L.
ND 0.50 0.087 ug/L
ND 0.50 0.079 ug/L
ND 0.50 0.081 ug/L
ND 0.50 0.019 ug/L
ND 0.50 0.060 ug/L
ND 0.50 0.074 ug/L.
ND 0.50 0.090 ug/L
ND 0.50 0.18 ug/L
ND 0.50 0.052 ug/L
ND 100 33 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.018 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The R PD between two GC columns exceeds 40%
Run
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 13 of 21
Level 1 Report v2.1
Client: NCDENR-DWM-UST Section
Description: WSW-ADVENTURE 117
Date Sampled:08/19/2010 1415
Date Received: 08/20/201 O
Laboratory ID: LH20021-005
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
1 6200B SM 6200B 1 08/26/2010 0314 DLB
CAS Analytical
Parameter Number Method
Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B
Methylene chloride 75-09-2 SM 6200B
Naphthalene 91-20-3 SM 6200B
n-Propylbenzene 103-65-1 SM 6200B
Styrene 100-42-5 SM 6200B
1, 1, 1,2-Tetrachloroethane 630-20-6 SM 6200B
1, 1,2,2-Tetrachloroethane 79-34-5 SM 6200B
Tetrachloroethene 127-18-4 SM 6200B
Toluene 108-88-3 SM 6200B
1, 1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B
1,2,3-T richlorobenzene 87-61-6 SM 6200B
1,2,4-Trichlorobenzene 120-82-1 SM 6200B
1, 1, 1-Trichloroethane 71-55-6 SM 6200B
1, 1,2-Trichloroethane 79-00-5 SM 6200B
Trichloroethene 79-01-6 SM 6200B
Trichlorofluoromethane 75-69-4 SM 6200B
1,2,3-Trichloropropane 96-18-4 SM 6200B
1,3,5-Trimethylbenzene (Mesitylene) 108-67-8 SM 6200B
1,2,4-Trimethylbenzene 95-63-6 SM 6200B
Vinyl chloride 75-01-4 SM 6200B
m+p -Xylenes 179601-23-1 SM 6200B
o -Xylenes 95-47-6 SM 6200B
Run 1 Acceptance Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 52-138
Bromofluorobenzene 115 70-147
Toluene-dB 102 76-125
POL = Practical quantitalion limit B = Detected in the method blank
ND= Not detected at or above the MDL J = Estimated result < POL and;: MDL
Prep Date Batch
40921
Result Q PQL MDL Units
ND 0.50 0.019 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.024 ug/L
i'-JD 0.50 0.015 ug/L
ND 0.50 0.057 ug/L
ND 0 50 0.013 ug/L
ND 0.50 0.014 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.30 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.029 ug/L
ND 0.50 0.031 ug/L
ND 0.50 0.024 ug/L
ND 0.50 0.051 ug/L
ND 0.50 0.33 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.065 ug/L
ND 0.50 0.17 ug/L
ND 0.50 0.17 ug/L
E = Ouantitation of compound exceeded the calibration range
P = The RPO between two GC columns exceeds 40%
Run
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 14 of 21
Level 1 Report v2.1
QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page: 15 of 21
Level 1 Report v2.1
Sample ID: LQ40921-001
Batch: 40921
Analytical Method: SM 6200B
Parameter
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
tert-Butylbenzene
sec-Butyl benzene
n-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
4-Chlorotoluene
2-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane (Methylene bromide)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1 , 1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1, 1-Dichloroethene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1, 1-Dichloropropene
Diisopropyl ether (IPE)
Ethanol
Ethyl benzene
Hexachlorobutadiene
lsopropylbenzene (Cumene)
p-lsopropyltoluene (p-Cymene)
Methyl tertiary butyl ether (MTBE)
Methylene chloride
Naphthalene
n-Propylbenzene
PQL = Practical quantitation limit
ND= Not detected at or above the MDL
Volatile Organic Compounds by GC/MS -MB
Matrix: Aqueous
Prep Method: 6200B
Result Q Dil PQL MDL
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.19
ND
ND
ND
ND
ND
ND
J
P = The RPD between two GC columns exceeds 40%
J = Estimated result< PQL and ::_MDL
0.50 0.027
0.50 0.027
0.50 0.055
0.50 0.17
0.50 0.010
0.50 0.20
0.50 0.037
0.50 0.010
0.50 0.017
0.50 0.085
0.50 0.17
0.50 0.17
0.50 0.17
0.50 0.17
0.50 0.019
0.50 0.059
0.50 0.17
0.50 0.061
0.50 0.094
0.50 0.17
0.50 0.17
0.50 0.17
0.50 0.071
0.50 0.023
0.50 0.054
0.50 0.079
0.50 0.087
0.50 0.094
0.50 0.060
0.50 0.019
0.50 0.081
0.50 0.18
0.50 0.090
0.50 0.074
0.50 0.052
100 33
0.50 0.17
0.50 0.17
0.50 0.029
0.50 0.018
0.50 0.019
0.50 0.17
0.50 0.17
0.50 0.024
N -Recovery is out of criteria
+ -RPO is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W''
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analysis Date
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133'
08/26/2010 0133
08/26/2010 0133
Page: 16 of 21
Level 1 Report v2.1
Sample ID: LQ40921-001
Batch: 40921
Analytical Method: SM 6200B
Parameter
Styrene
1, 1,2,2-Tetrachloroethane
1, 1, 1,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
1, 1,2-Trichloroethane
1, 1, 1-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene (Mesitylene)
Vinyl chloride
o -Xylenes
m+p -Xylenes
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
PQL = Practical quantitation limit
ND= Not detected at or above the MDL
Volatile Organic Compounds by GC/MS -MB
Matrix: Aqueous
Prep Method: 6200B
Result Q Dil PQL MDL
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Q % Rec Acceptance
Limit
116 70-147
100 52-138
103 76-125
P = The RPD between two GC columns exceeds 40%
J = Estimated result< PQL and c. MDL
0.50 0.015
0.50 0.013
0.50 0.057
0.50 0.014
0.50 0.17
0.50 0.30
0.50 0.17
0.50 0.17
0.50 0.031
0.50 0.029
0.50 0.024
0.50 0.051
0.50 0.33
0.50 0.17
0.50 0.17
0.50 0.065
0.50 0.17
0.50 0.17
N -Recovery is out of criteria
+ ~ RPO is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Analysis Date
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
08/26/2010 0133
Page: 17 of 21
Level 1 Report v2.1
Sample ID: LQ40921-002
Batch: 40921
Analytical Method: SM 6200B
Parameter
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
4-Chlorotoluene
2-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane (Methylene bromide)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1, 1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1, 1-Dichloroethene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1, 1-Dichloropropene
Diisopropyl ether (IPE)
Ethanol
Ethyl benzene
Hexachlorobutadiene
lsopropylbenzene (Cumene)
p-lsopropyltoluene (p-Cymene)
Methyl tertiary butyl ether (MTBE)
Methylene chloride
Naphthalene
n-Propylbenzene
POL= Practical quantitation limit
ND~ Not detected at or above the MDL
Volatile Organic Compounds by GC/MS -LCS
Matrix: Aqueous
Prep Method: 6200B
Spike
Amount Result % Rec
(ug/L) (ug/L) Q Oil % Rec Limit
50 53 106 70-130
50 61 123 70-130
50 56 112 70-130
50 60 120 70-130
50 60 120 70-130
50 47 95 60-140
50 61 122 70-130
50 60 120 70-130
50 58 116 70-130
50 58 116 70-130
50 56 113 70-130
50 48 96 42-163
50 51 102 70-130
50 60 121 20-158
50 56 112 70-130
50 57 114 70-130
50 58 116 70-130
50 63 126 70-130
50 59 119 70-130
50 56 112 70-130
50 59 118 70-130
50 58 115 70-130
50 90 N 180 60-140
50 52 105 70-130
50 49 97 70-130
50 51 102 70-130
50 53 105 70-130
50 52 104 70-130
50 57 114 70-130
50 59 118 70-130
50 51 102 70-130
50 56 111 70-130
50 58 115 70-130
50 52 103 70-130
50 56 111 70-130
5000 6500 129 40-130
50 59 117 70-130
50 56 112 70-130
50 61 122 70-130
50 61 123 70-130
50 60 120 70-130
50 48 97 70-130
50 66 131 50-140
50 58 117 70-130
P = The RPO between two GC columns exceeds 40%
J = Estimated result < POL and ':.MDL
N -Recovery is out of criteria
+ -RPO is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] ·1 www.shealylab.com
Analysis Date
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
08/25/2010 2156
Page: 18 of 21
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS -LCS
Sample ID: LO40921-002 Matrix: Aqueous
Batch: 40921 Prep Method: 6200B
Analytical Method: SM 6200B
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit
Styrene 50 55 110 70-130
1, 1,2,2-Tetrachloroethane 50 57 114 70-130
1, 1, 1,2-Tetrachloroethane 50 63 126 70-130
Tetrachloroethene 50 62 124 70-130
Toluene 50 57 114 70-130
1, 1,2-Trich!oro-1,2;2-Trifluoroethane 50 59 118 70-130
1 ,2 ,4-Trichlorobenzene 50 63 126 70-130
1,2,3-Trichlorobenzene 50 62 125 70-130
1, 1,2-Trichloroethane 50 59 118 70-130
1, 1, 1-Trichloroethane 50 55 109 70-130
Trichloroethene 50 59 117 70-130
Trichlorofluoromethane 50 58 115 60-140
1,2,3-Trichloropropane 50 63 126 70-130
1,2,4-Trimethylbenzene 50 59 118 70-130
1,3,5-Trimethylbenzene (Mesitylene) 50 55 109 70-130
Vinyl chloride 50 51 101 60-140
o -Xylenes 50 61 122 70-130
m+p -Xylenes 50 61 122 70-130
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 115 70-147
1,2-Dichloroethane-M 95 52-138
Toluene-dB 101 76-125
PQL = Practical quantitation limit
ND= Not detected at or above the MDL
P = The RPO between two GC columns exceeds 40%
J = Estimated result< PQL and:':-MDL
N M Recovery is out of criteria
+ RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Analysis Date
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Level 1 Report v2.1
Sample ID: LQ40921-003
Batch: 40921
Analytical Method: SM 6200B
Parameter
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane (Methyl bromide)
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane (Methyl chloride)
4-Chlorotoluene
2-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane (Methylene bromide)
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dichlorodifluoromethane
1,2-Dichloroethane
1, 1-Dichloroethane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1, 1-Dichloroethene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1, 1-Dichloropropene
Diisopropyl ether {IPE)
Ethanol
Ethylbenzene
Hexachlorobutadiene
lsopropylbenzene (Cumene)
p-lsopropyltoluene (p-Cymene)
Methyl tertiary butyl ether (MTBE)
Methylene chloride
Naphthalene
n-Propylbenzene
POL= Practical quantitation limit
ND= Not detected at or above the MDL
Volatile Organic Compounds by GC/MS -LCSD
Matrix: Aqueous
Prep Method: 6200B
Spike
Amount Result % Rec
{ug/L) (ug/L) 0 Dil % Rec % RPD Limit
50 52 103 2.2 70-130
50 60 119 2.9 70-130
50 57 113 1.5 70-130
50 61 122 1.7 70-130
50 60 119 0.74 70-130
50 51 102 7.2 60-140
50 56 112 8.7 70-130
50 54 109 9.7 70-130
50 51 102 12 70-130
50 54 107 8.1 70-130
50 53 107 5.2 70-130
50 48 95 1.2 42-163
50 51 103 1.1 70-130
50 59 118 2.7 20-158
50 53 106 5.3 70-130
50 53 107 6.2 70-130
50 59 117 0.99 70-130
50 62 124 1.3 70-130
50 60 119 0.45 70-130
50 53 105 6.1 70-130
50 56 112 4.9 70-130
50 55 110 4.6 70-130
50 81 N 162 11 60-140
50 53 105 0.62 70-130
50 49 98 0.79 70-130
50 51 102 0.60 70-130
50 53 105 0.20 70-130
50 49 98 5.5 70-130
50 52 104 9.5 70-130
50 59 117 0.56 70-130
50 52 103 1.0 70-130
50 55 110 1.4 70-130
50 57 114 0.65 70-130
50 47 95 8.8 70-130
50 57 114 2.8 70-130
5000 4600 + 92 34 40-130
50 55 109 7.2 70-130
50 48 96 15 70-130
50 57 114 7.1 70-130
50 56 112 9.4 70-130
50 63 126 4.4 70-130
50 50 101 4.1 70-130
50 60 120 8.6 50-140
50 54 107 8.2 70-130
P = The RPD between two GC columns exceeds 40%
J = Estimated result< POL and "._MDL
N -Recovery is out of criteria
+ -RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPD
Limit
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Analysis Date
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Level 1 Report v2.1
Sample ID: LQ40921-003
Batch: 40921
Analytical Method: SM 6200B
Parameter
Styrene
1, 1,2,2-Tetrachloroethane
1, 1, 1,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1,2-Trichloro-1,2,2-Trifluoroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
1, 1,2-Trichloroethane
1, 1, 1-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2, 3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene (Mesitylene)
Vinyl chloride
o -Xylenes
m+p -Xylenes
Surrogate
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-dB
PQL = Practical quanlitation limit
ND = Not detected at or above the MDL
Volatile Organic Compounds by GC/MS -LCSD
Matrix: Aqueous
Prep Method: 6200B
Spike
Amount Result % Rec
(ug/L) (ug/L) Q Oil % Rec % RPO Limit
50 52 104 5.3 70-130
50 58 115 0.92 70-130
50 62 124 2.1 70-130
50 56 112 10 70-130
50 55 111 2.7 70-130
50 53 106 10 70-130
50 58 116 8.3 70-130
50 56 112 11 70-130
50 58 117 1.5 70-130
50 52 104 4.9 70-130
50 56 112 4.6 70-130
50 52 104 9.9 60-140
50 63 127 0.76 70-130
50 55 111 6.3 70-130
50 51 103 6.6 70-130
50 46 91 10 60-140
50 57 114 6.7 70-130
50 57 114 6.8 70-130
Q % Rec Acceptance
Limit
116 70-147
97 52-138
103 76-125
P = The RPD between two GC columns exceeds 40%
J = Estimated result< PQL and c_MDL
N • Recovery is out of criteria
+ -RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
% RPO
Limit
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Analysis Date
08/26/2010 0011
08/26/2010 0011
08/26/2010 0011
08/26/2010 0011
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08/26/2010 0011
08/26/20'100011
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Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
APPENDIXC
FIELD DATA SHEETS
WSW-
Well Number MW-1R MW-2 MW-3R MW-4 Adventure
117
Total Well Depth (feet btoc) 45 45 45 65 (Unknown)
Depth to Product (feet btoc) None None None None None
Measured Measured Measured Measured Measured
Depth to Water (feet btoc) 36.02 36.00 36.10 34.70 (Unknown)
\tv'eH Volume (gallons) 1.46 1.46 1.45 A OA NA '+.OV
Purge Date 8/19/10 8/19/10 8/19/10 8/19/10 8/19/10
Purge Method Disposable Disposable Disposable Disposable Ran spigot
Bailer Bailer Bailer Bailer for ~10 mins
Gallons Purged 4.5 4.0 4.35 14.50 ~50
Date Sampled 8/19/10 8/19/10 8/19/10 8/19/10 8/19/10
Sampling Method Disposable Disposable Disposable Disposable spigot Bailer Bailer Bailer Bailer
Time of Sample 14:45 15:00 14:30 14:00 14:15
Comments none none none none none
APPENDIXD
FIELD MEASUREMENTS
Site: Cornelius Road
Incident#: 36031
Volume
pH
Specific Conductivity
Temperature
Volume
pH
Specific Conductivity
Temperature
Volume
pH
Specific Conductivity
Temperature
Field Screening Summary Data
August 19, 2010 Sampling Event
Cornelius Road Site
Mooresville, North Carolina
MW-lR
Initial First
5.76 5.91
74 79
23.2 22.4
MW-2
Initial First
5.28 5.25
107 123
20.1 19.7
MW-3R
Initial First
5.72 5.71
110 95
24.2 22.6
Second
5.57
81
20.7
Second
5.22
141
19.6
Second
5.71
61
21.5
*Well was going dry and was sampled after the third volume was removed.
MW-4
Volume Initial First Second
pH 6.55 6.75 6.81
Specific Conductivity 256 244 281
Temperature 23.1 23.8 23.6
.. ·
Third
5.63
80
19.7
Third
5.32
142
19.8
Third
5.95
49
21.4
Third
5.95
151
24.4 -
APPENDIXE
WSW ABANDONMENT RECORD
WELL ABANDONMENT RECORD
North Carolina Department ofEnviromnent and Natural Resources-Division ofWater Quality
WELL CONTRACTOR CERTIFICATION# .5 '.{ 1 >
L WELL CONTRACTOR:
.]JM A, r~~ft5'J
W ~,?':tractor (TndividuaJ}_ Name .
':::::j( t,.,~J ~.A'--1 b"t.."ln.o~<AL
Weil Contractor Company Name
STREET ADDRESS 2b:i bl!.Ot.\:)G:j l""' ,
LQe1;1 ml'sctl.s2 9:. 2Ciq. <c:>~
City lll' Town · · State Zip Code
~ '-t.3 )-q (:)9 )'I>~\)
Area code • Phone number
2. WELL INFORMATION:
SITE WELL ID I# (ifapplicable),~W~S-W~-~1 _______ _
STATE WELL PERMIT# (ifapplicable}_~~~/~A.--'-----
COUNTY WELL PERMIT# (ifapplicable) __ l'\_(_A ____ _
DWQ or OTHER PERMIT# (if applicable), __ N_~/,(t..c,..;:.. ____ _
WELL USE (Check applicable use): 0 Monitoring Ill Residential
0 Mnnlclpalll'nblk D Iwlnstrial/Commercial O Agric&Ituntl
D Recovery D Injection D Irrigation
00ther(listuse) ____________ _
3. WELL LOCATION:
C0UNTY.Jre9eB. ~QUADRANGLENAME ____ _
NEAREST TOWN: .s;M,:,:Q,oO,..,_r,.,es""vuilwle,,___ _______ _
275 Cornelius Road. PIN #4658543024
(Srn>et/RQad Name, Ntnllbcr, Com,wuity, Subdivi,ioo, Lot No .. Part:cl, Zip Code)
TOPOGRAPHIC I LAND SETI!NG:
□Slope □Valley '?(Flat 0Ridge00ther ______ _
(Check appropriate setting)
LATITUDE 3t;" ~ \; b0 May be in d,,grees,
winutcs. sceoooa, or in a
LONGITUDE g_o....!.. (53,'Z.,{pp d<:<:imalrormat
Lalitude'longitude soura,: 0 GPS bd_ Topograpllic map
{LOC41ion of well mwt be shown on a USGS topo map and
allaChed to this form if not ustngGPS.)
4a. FACILITY-The natne of the business whore tho well is hcat,:d Complelc 4a and4b.
(If a resideiltial ...,n, slap 4a; comp1etr: 4b, well owner infonnation only.)
FACllJTY ID #(if applicable) __________ _
NAME oF FACILITY Cornelius Road Site
sTREET ADDRESS Cornelius Rd and Charlotte Hwy
Mooresville NC 2a115;:0000
City or Town State Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME Stanley F. GOQC;lman
STREET ADDRESS 27§ Cornelius Road. Mooresville
5. WELL DETAILS:
a. Total Depth: 45 ft. Diameter: 32 in.
b. War.er Level {Below Measuring Point): NIA ft.
Measuring point is NIA ft. above land surface.
6. CASING: Le.ngth Diameter
a. Casing Depth (ifknown): NIA ft. _MA_in.
b. Casing Removed: ~ ft. ---in. 3 3<-7. DISINFECTION: -"ry1 fl_.£
(Amount of 65%-75% calcium hypochlorite used)
8. SEALING MATERIAL:
Nta!C•.......t Sand Cement
Cement lb. Cement lb.
Water gal. Wan:r gal.
~
Bentonite lb.
Type: 0 Slurry □Pellets
Watt:r gal.
~
Type material CoMf~CT~ CLJ:;..'1
Amount l4YW
9. EXPLAIN METIIOD OF EMPLACEMENT OF MA TERJAL:
~ El Lt~ f"l'lPM ~ Dl:.t"fU. -ro l' gw f;SE 1.,ol JJ , ~ o ~A.gfAt:E:
~I~ c::..tllM f~C:tGO r::.~ C.p..tt~ #
&,11 (JH,IC(2t-:It: Ge,.f .AND QA~~L~
S'\.-\f...fAUe
10. WELL DIAGRAM: Draw a delailed sketch of the well on tl:te baclc of this
fomi showing total depth. depth and dimnere,.-of screens (if any) ICll1aining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials used. . 5 ·cx5 .k'(r"~W M--1\ f
11. DA TE WELL ABANDONED 8-blt_\-to
I 00 IIBREBY CERTIFY TiiAT THIS WEU WAS ABANDONED IN ACCORDANCE wrm !SA NCAC 2C, WELL CONSTRUCTION STANDARDS, AND 1RAT A COPY OF
THIS RECORD HAS BEEN PROVIDED 1'0 TIIE WElL OWNER.
@o,~+ 8-~4-lt,
DATE
SIGNATURE OF PRIVATE WELL OWNER ABANDONING Til1l. WEI.IL DATE
(The privale weK ~ 1m1St be llll individual who ~cbaoclc.a bis/luresidenlial well
inaccoalanccwilh 1SANCAC2C .0113.)
Todd Allred
PRINTED NAME OF PERSON ABANDONING TW: WElL
Submit a copy to the owuer and tbe ongiu.l to the Division of Water Quality within 30 days.
Attn: Information Mllugement, 1617 Mall Service Center -R,ileigh, NC 27699-1617, Phone No. [phone] ert 568.
FormGW-30
Rev. 5/06