MO-4209_36384_CA_MRP_20230713

GROUNDWATER MONITORING REPORT
SCARLETT’S 66
1030 SEIGLE AVENUE
CHARLOTTE, MECKLENBURG CO., NC 28205
NCDEQ INCIDENT NO. 36384
ATC PROJECT NO. STL3638401
TASK AUTHORIZATION NO. TA-01

Prepared for:

North Carolina Department of Environmental Quality
Division of Waste Management – Underground Storage Tank Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Submittal Date:

July 13, 2023

Prepared By:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina 28273
p: [phone] / f: [phone]

Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION ............................................................................... 1
2.0 EXECUTIVE SUMMARY ............................................................................. 2
3.0 SITE DESCRIPTION ................................................................................... 2
3.1 Site Characterization .................................................................... 2
3.2 Site Background ........................................................................... 3
3.3 Site and Regional Geology .......................................................... 4
3.4 Site and Regional Hydrogeology .................................................. 5
4.0 GROUNDWATER CHARACTERIZATION .................................................. 5
4.1 Groundwater Levels ..................................................................... 5
4.2 Groundwater Quality .................................................................... 6
5.0 CONCLUSIONS ......................................................................................... 6
TABLES
Table 1 Groundwater Elevation Data
Table 2 Field Parameters
Table 3 Recent Groundwater Analytical Data
Table 4 Historical Groundwater Analytical Data

FIGURES

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Groundwater Elevation Contour Map
Figure 4 Groundwater Quality Map

APPENDICES

Appendix A Conceptual Site Model
Appendix B Field Notes and Photolog
Appendix C Laboratory Analytical Report

Groundwater Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) has performed consulting services for Scarlett’s
66, located at 1030 Seigle Avenue in Charlotte, Mecklenburg County, North Carolina. The
adjoining properties are developed as commercial properties with residential properties further
from the site. This work was performed based on the April 27, 2023 Task Authorization (TA-01)
by the Trust Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste
Management, North Carolina Department of Environmental Quality (NCDEQ). The work was
performed as part of the State Lead Contract # N70522-B between NCDEQ and ATC.

The site is vacant as of July 13, 2023, but previously operated as an auto repair shop, Automax
Lube and Tune. The new property owner has applied for and been granted eligigability into the
NCDEQ Brownfields Program, Project#26037-22-060. The site formerly operated four 4,000-
gallon gasoline USTs, one 1,000-gallon kerosene, one 550-gallon waste oil, and one 550-gallon
heating oil UST which were removed in 1994. The UST Closure Report indicated that at the
time of the UST removals, releases from the kerosene and heating oil USTs were reported to
the NCDEQ, although gasoline constituents are also detected in the groundwater.

ATC was authorized to sample groundwater monitoring wells MW-1, MW-3, MW-4, MW-5, and
AS-1 and measured the depth to groundwater in all monitoring wells. The work was conducted
on May 16, 2023. The following site conditions are noted based on the recent and historical
assessment activities and are listed in the Conceptual Site Model (Appendix A):

 Municipal water is available to the site and surrounding area. No water supply wells are
reportedly located within 1,500 feet of the source area.
 Little Sugar Creek is located approximately 480 feet northwest of the source area.
 Light non-aqueous phase liquid (LNAPL) was measured in MW-2 at a thickness of 0.06
feet on May 16, 2023.
 Concentrations of volatile organic compounds (VOCs) exceeded the 15A NCAC 02B
Surface Water Quality Standards (2B Standards) by more than ten times in wells MW-1
and MW-4 and exceeded the Gross Contamination Levels (GCLs) in well MW-1 (for
benzene only at 6,720 micrograms per liter or µg/L).
 Concentrations of VOCs exceeded the 15A NCAC 02L .0202 Groundwater Quality
Standards (2L Standards) in MW-1 and MW-4.
 The concentration of benzene was 7% less in well MW-1, and 207.5% greater in well MW-4
than reported in February 2022.
 Concentrations of VOCs are decreasing over time in MW-1 and are increasing in MW-4.
 The depth to groundwater in the shallow monitoring wells ranged from 15.62 ft-toc in MW-4
to 19.33 ft-toc in MW-5 on May 16, 2023, with groundwater flow to the northwest.

3.0 SITE DESCRIPTION
3.1 Site Characterization
The NCDEQ retained ATC to provide environmental consulting services for Scarlett’s 66,
located at 1030 Seigle Avenue in Charlotte, Mecklenburg County, North Carolina. Figure 1
depicts the site location on a topographic map. The site includes a commercial building and
former dispenser islands and former UST basins. The commercial building formerly operated as
a retail gasoline station and recently operated as an auto repair facility. Municipal water is
provided to the site and other surrounding properties. Little Sugar Creek is located approximately
480 feet northwest of the source area. Four shallow monitoring wells (MW-1 through MW-4) and
Groundwater Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

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one deep air sparge well (AS-1) are located on the site, and one shallow well (MW-5) is located
northwest of the site across Seigle Avenue (Figure 2).

3.2 Site Background
The site operated as an auto repair shop, Automax Lube and Tune, through August 31, 2021, and
is currently vacant. The site formerly operated four 4,000-gallon gasoline USTs, one 1,000-
gallon kerosene, one 550-gallon waste oil, and one 550-gallon heating oil UST which were
removed in 1994. The UST Closure Report indicated that at the time of the UST removals,
releases from the kerosene and heating oil USTs were reported to the NCDEQ. A surface
water body, identified as Little Sugar Creek (Class C), is located approximately 480 feet west of
the site.

A Phase II Limited Site Assessment (LSA) was completed by S&ME, dated August 10, 2009. The
Phase II LSA indicated that the site qualified as a high risk site due to the presence of an active
water supply well (WSW-1) approximately 500 feet southwest of the site. A Groundwater
Monitoring Report dated August 6, 2010, by S&ME indicated that water supply well (WSW-1) was
out of service. This water supply well is not included in Mecklenburg County’s Well Information
database. The report also indicated that an AFVR event was completed in April 2010.

A Groundwater Monitoring Report dated June 13, 2012, by S&ME indicated that there were no
active water supply wells within 1,000 feet of the site. The report indicated that GCLs were
exceeded for benzene on-site. A Groundwater Monitoring Report dated July 23, 2013, by Crawford
Environmental Services indicated that there was no LNAPL identified in the site monitoring well
network. The report indicated that the GCL for benzene had been exceeded.

ATC performed groundwater monitoring activities at the site on December 30, 2014, which
identified LNAPL in well MW-2 at a thickness of 0.24 feet. Monitoring wells MW-1 and MW-4 each
contained multiple constituent concentrations above the 2L Standards and ten times the 2B
Standards. No constituents were noted above 2L Standards for wells MW-3 and MW-5. The
December 2014 sampling event indicated that no compounds were noted above the GCLs in wells
that did not contain LNAPL, and groundwater appears to flow generally to the northwest.

ATC performed an AFVR event on June 19, 2015, using well MW-2 as the extraction point. Prior to
performing the AFVR event, LNAPL was measured at a thickness of 0.32 feet in well MW-2. In
compliance with the tenant’s request to cease AFVR activities, the AFVR operation was
discontinued after running for approximately 1 hour and 30 minutes. Forty-two gallons of petroleum
impacted groundwater from well MW-2 was removed during that time. A return visit was performed
on September 16, 2015, and 0.60 feet of LNAPL was measured in well MW-2. During this visit,
ATC installed an absorbent sock in the well to aid in the removal of LNAPL. ATC conducted an 8-
hour AFVR event on March 8, 2016. This event was followed by post-AFVR groundwater
monitoring activities conducted on April 13, 2016. LNAPL was still present in well MW-2, and
wells MW-1 and MW-4 contained contaminant concentrations that exceeded the 2L Standards.

During the March 2018 sampling event, free product was detected in monitoring well MW-2 at a
thickness of 0.44 feet. Monitoring wells MW-1 and MW-4 each contained multiple constituents at
concentrations above the 2L and 2B Standards. The GCL for benzene was exceeded in the
sample from well MW-1 at a concentration of 12,000 µg/L.

Based on the March 2018 sampling event, ATC recommended an AFVR event using well MW-2 to
remove free product, and using well MW-1 to remove dissolved phase petroleum.
Groundwater Monitoring Report July 13, 2023
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ATC subcontracted CCI to perform an 8-hour AFVR on August 9, 2019. On September 9, 2019,
ATC completed a groundwater sampling event. Based on the AFVR and groundwater sampling
events, ATC concluded the contaminant plume appeared to be stable, although VOC
concentrations increased slightly in monitoring well MW-1. The AFVR event appears to have been
successful in removing LNAPL from monitoring well MW-2, but not in reducing VOC concentrations
in monitoring well MW-1.

ATC performed a groundwater monitoring event on January 15, 2021. ATC gauged and
sampled groundwater monitoring wells MW-1, MW-2, MW-3, MW-4 and MW-5. Dissolved VOC
concentrations exceeded the 2B Standards by more than ten times in wells MW-1, MW-2, and
MW-4, and the benzene concentration exceeded the GCL in well MW-1 (8,800 µg/L). ATC
concluded that the VOC plume appeared to be decreasing with time and recommended the
installation of a deeper well (AS-1) to be used for air sparging during an MMPE event. Well AS-1
was installed on March 31, 2021.

ATC sampled air-sparge well AS-1 on August 2, 2021 prior to the initiation of the combined
Mobile Multi-Phase Extraction (MMPE)/Air Sparging (AS) event. The MMPE/AS event was
performed between August 2 and August 6, 2021. ATC sampled groundwater monitoring wells
MW-1, MW-2, MW-4, and AS-1 and measured the depth to groundwater in all monitoring wells
on August 20, 2021.

On October 29, 2021, ATC collected a sample from monitoring well MW-1. Benzene was
reported in excess of its GCL, and the concentration was higher than that reported in January
2021 and August 2021, but less than the concentrations detected in 2016, 2018, and 2019.

ATC performed a 96-hour Mobile Multi-Point Extraction (MMPE)/Air Sparging (AS) event between
December 13 and 17, 2021, using well MW-1 and MW-4 as the extraction wells while sparging
AS-1. Approximately 737 gallons of petroleum hydrocarbons were recovered as vapors and 3,475
gallons of petroleum impacted groundwater from well MW-1 and MW-4 were removed during this
event. A groundwater sampling event was performed post-MMPE/AS on December 27, 2021. ATC
sampled groundwater monitoring wells MW-1, MW-4, and AS-1 and measured the depth to
groundwater in all monitoring wells. LNAPL was measured in MW-2 at a thickness of 0.14 feet.
ATC concluded concentrations of VOCs generally decreased subsequent to the MMPE event and
decreased over time.

On August 3, 2022, 1030 Siegle, LLC purchase the property. On October 10, 2022, The
NCDEQ Brownfields program issued a Letter of Eligibility into the Brownfields Program
(Scarlett’s 66 Brownfields Project #26037-22-060). On January 9, 2023, 1030 Siegle LLC
submitted plans for the future development of for commercial and business use (restaurant,
office).

3.3 Site and Regional Geology
According to the Geologic Map of North Carolina, produced by the State of North Carolina in
1985, the Site lies in the Charlotte Belt of the Piedmont Physiographic Province of North
Carolina. The rock type at the site has been identified as phyllite and schist, which are
crystalline metamorphic rocks. The shallow subsurface in most areas of the Piedmont contains
residual soil overburden, including structure-free residuum, saprolite, and partially weathered
rock (PWR) that derive from in-place weathering of the crystalline bedrock. Occasional areas
containing recent deposits of alluvium in the uppermost subsurface are found near streams and
Groundwater Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

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rivers. Saprolite and PWR typically contain some relict structures from the original rock material.
Depth to rock ranges from ground surface at occasional outcrops to depths of greater than 100
feet in areas of easily weathered rock. The well construction record for AS-1 indicates silty clay
to a depth of 45 feet below ground surface (ft-bgs).

3.4 Site and Regional Hydrogeology
The shallow aquifer occurrence varies in depth from ground surface at springs, creeks,
and rivers to as deep as 50 feet or more beneath upland surfaces in some parts of the
Piedmont. Water in the alluvium or unconsolidated residual material, including saprolite
and PWR, usually behaves as an unconfined aquifer, or water table, and will yield water
with head elevation equivalent to the first elevation where water was encountered.
Permeability varies with lithology and is typically relatively low in residual soils, with
higher permeability in saprolite or PWR due to relict rock texture and variable
susceptibility to weathering exhibited by different minerals in the rock. Groundwater flow
in residual soils or alluvium is usually in rough concurrence with local topographic
conditions and is toward local drainage features. Groundwater has been encountered at
depths ranging between 13 feet and 17 feet below the top of casing in site monitoring
wells. Based on groundwater elevation data from the existing site wells, the
groundwater flow direction is to the northwest, toward Little Sugar creek located
approximately 480 feet to the northwest.

The bedrock fractures or other planar features of the Charlotte Belt Physiographic
Province generally constitute the bedrock aquifer, with the surrounding rock material
being effectively impermeable. Along with fractures, contacts between rock bodies
probably constitute zones of significant groundwater occurrence in the bedrock. The
surrounding material and overlying residuum tend to make the bedrock aquifer a semi-
confined aquifer. That is, the overlying water and soil weight normally results in
pressure that causes water in a borehole, which intersects a fracture or other feature, to
rise above the elevation of the fracture or feature.

4.0 GROUNDWATER CHARACTERIZATION
4.1 Groundwater Levels
On May 16, 2023, ATC measured the depth to groundwater in wells MW-1, MW-2, MW-3, MW-
4, MW-5, and AS-1 prior to sampling monitoring wells (Table 1). The depth to groundwater in
the shallow monitoring wells ranged from 15.62 ft-toc in MW-4 to 19.33 ft-toc in MW-5 on May
16, 2023. LNAPL was detected in MW-2 at a thickness of 0.06 feet during the May 2023
groundwater monitoring event and has decreased since the last sampling event in February
2022..

A groundwater elevation contour map is provided as Figure 3, which depicts groundwater flow
generally to the northwest. Field notes and photographs from the May 16, 2023 gauging event is
provided in Appendix B.

Groundwater Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

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4.2 Groundwater Quality
On May 16, 2023, ATC sampled groundwater monitoring wells MW-1, MW-3, MW-4, MW-5 and
AS-1. MW-2 contained LNAPL as was not sampled. During sampling activities, a three-volume
well purge was implemented prior to groundwater sample collection to ensure collection of
representative groundwater samples. The water samples were collected in laboratory-supplied,
preserved containers; entered into chain of custody control; placed on ice; and shipped to North
Carolina accredited laboratory Pace Analytical Services, LLC, in Charlotte, North Carolina. The
groundwater samples were analyzed by Standard Method 6200B for VOCs, including ethanol
and oxygenates. The laboratory report is included in Appendix C.

At the completion of sampling each well, field parameters were measured (temperature,
conductivity, oxygen-reduction potential, and dissolved oxygen) as presented in Table 2.

Recent and historical groundwater analytical results are summarized in Table 3 and Table 4,
respectively. The groundwater analytical results were compared to the 2L Standards, 2B
Standards, and GCLs. Results from the groundwater monitoring event indicated the following:

 Concentrations of VOCs exceeded the 2B Standards by more than ten times in wells MW-1
and MW-4.
 The benzene concentration in well MW-1 (6,720 µg/L) exceeded the GCL of 5,000 µg/L.
The benzene concentration in well MW-1 was 7% less than reported in February 2022.
 Benzene increased 207.5% in MW-4 since it was reported in February 2022.
 VOCs concentrations exceeded the 2L Standards in wells MW-1 and MW-4.

Figure 4 depicts dissolved phase concentrations for petroleum compounds exceeding the 2L
Standards.

As part of ATC’s quality assurance and quality control (QA/QC) measures, a data review of the
laboratory reports was conducted. During the review, it was found that the samples were
received from the laboratory in acceptable condition and properly preserved. The samples were
analyzed within correct holding times and reported within the lab report, and the chain of
custody was properly completed by all parties. The laboratory QC report shows that an internal
blank was analyzed for each method that was used for the original samples. The laboratory
fortified blank (LFB) and laboratory control sample (LCS) data results were also provided for
each analytical method. Refer to the laboratory reports in Appendix C for details regarding QA
results for the laboratory samples and any noted exceptions. VOCs were not detected in the
field blank or the laboratory method blanks. Overall, ATC concludes that the laboratory results
are usable, and any exceptions do not significantly impact the conclusions presented in this
report.
5.0 CONCLUSIONS

On behalf of the Trust Fund Branch of the UST Section, ATC has completed consulting services
for Scarlett’s 66, located at 1030 Seigle Avenue in Charlotte, Mecklenburg County, North
Carolina.

ATC sampled groundwater monitoring wells MW-1, MW-3, MW-4, MW-5, MW-6 and AS-1 and
measured the depth to groundwater in all monitoring wells on May 16, 2023. Based on the
recent and historical assessment activities, the following site conditions are noted:
Groundwater Monitoring Report July 13, 2023
Scarlett’s 66, Charlotte, NC, Incident No. 36384 ATC Project No. SLC3638405

7

 Municipal water is available to the site and surrounding area. No water supply wells are
reportedly located within 1,500 feet of the source area.
 Little Sugar Creek is located approximately 480 feet northwest of the source area.
 LNAPL was measured in MW-2 at a thickness of 0.06 feet on May 16, 2023.
 The concentrations of VOCs exceeded the 2B Standards by more than ten times in wells
MW-1 and MW-4 and exceeded the GCLs in well MW-1 (for benzene only at 6,720
micrograms per liter or µg/L).
 VOCs concentrations exceeded the 2L Standards in MW-1 and MW-4.
 Concentrations of VOCs are decreasing over time in MW-1 and are increasing in MW-4.
 The depth to groundwater in the shallow monitoring wells ranged from 15.62 ft-toc in MW-4
to 19.33 ft-toc in MW-5 on May 16, 2023, with groundwater flow to the northwest.

TABLES
TABLE 1
GROUNDWATER ELEVATION DATA
Scarlett's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, North Carolina
NCDEQ Incident #36384
Well ID Gauging Date Comments
Depth to
Groundwater
(ft-toc)
Depth To
LNAPL
(ft-toc)
LNAPL
Thickness
(ft)
TOC
Elevation
(ft)
Groundwater
Elevation
(ft)
12/30/2014 -- 16.89 ND NA 682.11
4/13/2016 -- 13.24 ND NA 685.76
3/14/2018 -- 18.94 ND NA 680.06
8/9/2019 Pre-AFVR 16.12 ND NA 682.88
8/9/2019 Post-AFVR 21.53 ND NA 677.47
9/9/2019 -- 17.04 ND NA 681.96
1/15/2021 -- 14.10 ND NA 684.90
8/2/2021 Pre-MMPE 15.39 ND NA 683.61
8/6/2021 Post-MMPE 18.38 ND NA 680.62
8/20/2021 -- 15.87 ND NA 683.13
10/29/2021 -- 17.70 ND NA 681.30
12/13/2021 Pre-MMPE 18.42 ND NA 680.58
12/17/2021 Post-MMPE 24.49 ND NA 674.51
12/27/2021 -- 18.47 ND NA 680.53
5/16/2023 -- 15.83 ND NA 683.17
12/30/2014 -- 16.95 16.71 0.24 682.95
6/19/2015 -- 16.30 15.98 0.32 683.67
9/16/2015 -- 19.25 18.65 0.60 680.96
3/8/2016 -- 12.81 ND NA 686.89
4/13/2016 -- 13.09 12.92 0.17 686.75
3/14/2018 -- 19.66 19.22 0.44 680.41
8/9/2019 Pre-AFVR 16.27 16.00 0.27 683.66
8/9/2019 Post-AFVR 11.67 ND NA 688.03
9/9/2019 -- 17.18 ND NA 682.52
1/15/2021 -- 14.07 ND NA 685.63
8/2/2021 Pre-MMPE 15.31 ND NA 684.39
8/6/2021 Post-MMPE 16.22 ND NA 683.48
8/20/2021 -- 15.73 ND NA 683.97
12/27/2021 -- 18.56 18.42 0.14 681.26
5/16/2023 -- 15.78 15.72 0.06 683.97
12/30/2014 -- 17.37 ND NA 681.51
3/14/2018 -- 13.74 ND NA 685.14
3/14/2018 -- 19.52 ND NA 679.36
8/9/2019 Pre-AFVR 16.79 ND NA 682.09
8/9/2019 Post-AFVR 16.89 ND NA 681.99
9/9/2019 -- 17.66 ND NA 681.22
1/15/2021 -- 14.50 ND NA 684.38
8/20/2021 -- 16.42 ND NA 682.46
12/27/2021 -- 19.19 ND NA 679.69
5/16/2023 -- 16.41 ND NA 682.47
12/30/2014 -- 16.68 ND NA 682.28
4/13/2016 -- 13.12 ND NA 685.84
3/14/2018 -- 19.00 ND NA 679.96
9/9/2019 -- NA
1/15/2021 -- 13.78 ND NA 685.18
8/2/2021 Pre-MMPE 15.58 ND NA 683.38
8/6/2021 Post-MMPE 17.70 ND NA 681.26
8/20/2021 -- 15.71 ND NA 683.25
12/13/2021 Pre-MMPE 18.23 ND NA 680.73
12/17/2021 Post-MMPE 24.12 ND NA 674.84
12/27/2021 -- 18.29 ND NA 680.67
5/16/2023 -- 15.62 ND NA 683.34
12/30/2014 -- 20.25 ND NA 678.71
4/13/2016 -- 17.15 ND NA 681.81
3/14/2018 -- 21.32 ND NA 677.64
9/9/2019 -- 20.68 ND NA 678.28
1/15/2021 -- 17.48 ND NA 681.48
8/20/2021 -- 19.77 ND NA 679.19
12/27/2021 -- 22.21 ND NA 676.75
5/16/2023 -- 19.33 ND NA 679.63
8/2/2021 Pre-MMPE 15.50 ND NA Unknown
8/6/2021 Post-MMPE 24.55 ND NA Unknown
8/20/2021 -- 15.60 ND NA Unknown
12/13/2021 Pre-MMPE 18.13 ND NA Unknown
12/17/2021 Post-MMPE 27.30 ND NA Unknown
12/27/2021 -- 18.23 ND NA Unknown
5/16/2023 -- 15.65 ND NA Unknown
Notes:
ft = feet LNAPL - Light Non-Aqueous Phase Liquid
ft-toc = feet below top of casing NA = Not Applicable
ND = Not Detected
When free product is present, groundwater elevation calculated by [Top of Casing Elevation - Dept to water] + [Free Product Thickness*0.85]
Depths to water measured on 8/9/19 reflect data collected before and after an AFVR event.
MW-1 699.00
MW-2 699.70
MW-3 698.88
AS-1 Unknown
Not Located
698.96
MW-5 698.96
MW-4
Well Date Temperature
(◦C)
Conductivity
(µS/cm)
pH
(su)
ORP
(mV)
DO
(mg/L)
MW-1 5/16/2023 22.20 0.549 6.2 -101 6.8
MW-3 5/16/2023 21.20 0.406 6.6 -13 6.6
MW-4 5/16/2023 21.20 0.413 6.1 -48 7.4
MW-5 5/16/2023 25.80 0.266 5.7 123 6.9
AS-1 5/16/2023 22.70 0.260 6.6 -77 3.7
Notes:
°C - Degrees Celcius
mS/cm - milliSiemens per centimeter
su - Standard Units
ORP - Oxidation Reduction Potential (mv - millivolts)
DO - Dissolved Oxygen (mg/L - milligrams per liter)
TABLE 2
FIELD PARAMETERS
Scarlett's 66
1030 Siegle Ave
Charlotte, Mecklenburg County, North Carolina
NCDEQ Incident #36384
TABLE 3
RECENT GROUNDWATER ANALYTICAL DATA
Scarlett's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, North Carolina
NCDEQ Incident #36384
Sample ID Constituent of
Concern
BenzeneTolueneEthylbenzeneXylene (Total)Methyl-tert-butyl etherNaphthalenen-PropylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenesec-Butylbenzenetert-Butylbenzene1 600 600 500 20 6 70 70 400 400 70 70
51 11 97 670 1,500 12 2,700 250 390 215 NE NE
5,000 260,000 80,000 50,000 20,000 6,000 26,100 30,500 28,500 24,100 8,800 14,750
AS-1 5/16/2023 <0.34 <0.24 <0.30 <0.71 <0.42 <0.64 <0.34 <0.33 <0.50 <0.33 <0.40 <0.32
MW-1 5/16/2023 6,720 39,500 3,820 22,080 <84.4 687 345 132 3,100 794 <80.0 <64.6
MW-3 5/16/2023 <0.34 <0.24 <0.30 <0.71 0.94 <0.64 <0.34 <0.33 <0.50 <0.33 2.9 0.65
MW-4 5/16/2023 2,390 10.4J 571 2,321 <10.6 582 243 134 2,190 492 <10.0 <8.1
MW-5 5/16/2023 <0.34 <0.24 <0.30 <0.71 <0.42 <0.64 <0.34 <0.33 <0.50 <0.33 <0.40 <0.32
FB-1 5/16/2023 <0.34 <0.24 <0.30 <0.71 <0.42 <0.64 <0.34 <0.33 <0.50 <0.33 <0.40 <0.32
Notes:
"<" = Not Detected at or above the laboratory detection limit
Concentrations are reported in micrograms per liter (µg/L)
Concentrations in BOLD print exceed the 15A 02L .0202 Groundwater Quality Standard (2L Standard).
Concentrations ITALIC print exceed 10 times the 2B Water Standards for Class C surface water bodies.
Concentration in UNDERLINED print exceed the Gross Contamination Level (GCL)
J = Estimated value below method detection limit
2B Standards
2L Standards
GCL

TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL DATA
Scarlett's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, North Carolina
NCDEQ Incident #36384
Well ID Sample Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl tert-butyl EtherNaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneIsopropyl etherp-Isopropyltoluenen-PropylbenzeneTetrachloroethyleneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneEthanolMethylene Chloridetert-Amylmethyl ether1 600 600 500 20 6 70 70 70 70 25 70 0.7 70 400 400 4000 5 128
51 11 97 670 670 12 3.9 NE NE 20,000 320 3,200 3.3 250 390 215 5000 1,000 NE
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 15,000 70,000 NE 30,000 700 25,000 28,500 25,000 4,000,000 5,000 12,800
12/30/2014 4,800 24,000 1,500 11,000 <2.2 430 35 24 <2.0 <2.0 31 140 <2.0 <2.8 2,500 740 NA BQL NA
4/13/2016 12,000 44,000 2,500 16,700 97 440 20 J 15 J <2.0 <2.0 <50 200 <50 87 2,500 610 NA BQL NA
3/14/2018 12,000 46,000 3,400 20,200 28 J 530 68 19 J <12 <12 <15 280 <16 130 3,000 800 NA BQL NA
9/9/2019 14,500 55,400 3,700 23,000 258 707J <125 <125 <125 <125 NA <125 <125 <125 2,970 <125 NA <500 NA
01/15/2021 8,840 43,200 3,250 19,100 <111 685 <88.2 <61.5 <62.5 <83.5 NR <60.2 <58.0 125 3,220 <56.8 <24700 <375 NA
08/20/2021 5,180 24,200 2,050 15,300 <106 684 <122 <100 <80.8 <77.0 NA 270 <73.0 135 2,690 686 <18000 1,290 <665
10/29/2021 9,080 38,500 3,200 18,100 <106 771 <122 <100 <80.8 <77.0 NA 307 <73.0 118J 2,760 660 <18000 <488 <665
12/27/2021 7,210 23,300 2,680 18,800 <106 840 <122 <100 <80.8 <77.0 <104 194 <73.0 <83.2 3,530 <83.0 <18000 <488 <665
5/16/2023 6,720 39,500 3,820 22,080 <84.4 687 <98.0 <80.0 <64.6 NA NA 345 <58.4 132 3,100 794 <14,400 <390 <1,850
12/30/2014
4/13/2016
3/14/2018
9/9/2019 1,060 158 604 2,800 373 1,260 856 <5.0 <5.0 18.5 NA <5.0 <5.0 197 2,450 <5.0 NA <20.0 NA
01/15/2021 542 63.5 213 879 147 242 49.3 <0.98 <1.0 10.4 NR <0.96 <0.93 45 494 <0.91 <396 <6.0 NA
08/20/2021 474 48.3 165 704 237 170 31.4 <1.6 <1.3 11.5 NA 59.9 <1.2 34.6 361 92.7 <289 18.3 40.1
10/29/2021
12/27/2021
5/16/2023
12/30/2014 <0.079 <0.090 <0.092 <0.29 <0.090 <0.12 <0.054 <0.084 <0.12 <0.12 <0.12 <0.094 0.37 J <0.11 <0.18 <0.10 NA BQL NA
4/13/2016 <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA BQL NA
3/14/2018 <0.12 <0.17 <0.13 <0.39 1.5 <0.12 <0.15 4.4 0.78 <0.15 <0.15 <0.13 <0.27 0.12 J <0.18 <0.13 NA BQL NA
09/09/2019 <0.25 <0.25 <0.25 <0.25 0.48 J <1.0 <0.25 0.44 J <0.25 <0.25 NA <0.25 <0.25 <0.25 0.49 J <0.25 NA <1.0 NA
01/15/2021 <0.24 0.63 <0.24 <0.50 <0.44 <0.66 <0.35 <0.25 <0.25 <0.33 NR <0.24 <0.23 <0.24 <0.19 <0.23 1,280 <1.5 NA
08/20/2021
10/29/2021
12/27/2021
5/16/2023 <0.34 <0.24 <0.30 <0.71 0.94 <0.64 <0.49 2.9 0.65 NA NA <0.34 <0.24 <0.33 <0.50 <0.33 <72.2 <2.0 <9.2
Standard Method 6200B
Not Sampled - LNAPL (0.17 feet)
Not Sampled - LNAPL (0.17 feet)
Not Sampled - LNAPL (0.44 feet)
GCL
Lab Anaylsis
2B Standard
2L Standard
Not Sampled
Sampling not Required
Sampling not Required
Not Sampled - LNAPL (0.14 feet)
Not Sampled - LNAPL (0.06 feet)
Sampling not Required
MW-1
MW-2
MW-3
Page 1 of 2

TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL DATA
Scarlett's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, North Carolina
NCDEQ Incident #36384
Well ID Sample Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl tert-butyl EtherNaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneIsopropyl etherp-Isopropyltoluenen-PropylbenzeneTetrachloroethyleneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneEthanolMethylene Chloridetert-Amylmethyl ether1 600 600 500 20 6 70 70 70 70 25 70 0.7 70 400 400 4000 5 128
51 11 97 670 670 12 3.9 NE NE 20,000 320 3,200 3.3 250 390 215 5000 1,000 NE
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 15,000 70,000 NE 30,000 700 25,000 28,500 25,000 4,000,000 5,000 12,800
Standard Method 6200B
GCL
Lab Anaylsis
2B Standard
2L Standard
12/30/2014 240 220 1,400 5,000 <4.5 780 <2.7 <4.2 <4.0 <4.0 60 310 <4.0 120 2,900 670 NA BQL NA
4/13/2016 260 85 540 1,820 <25 440 15 J 14 J <25 <25 <25 150 <25 76 1,500 340 NA BQL NA
3/14/2018 280 30 290 3,560 <4.5 380 24 J 24 J <4.0 <4.0 12 J 240 <14 140 2,800 540 NA BQL NA
09/09/2019
01/15/2021 76.0 <4.6 577 1,590 <8.9 393 <7.1 <4.9 <5.0 <6.7 NR <4.8 <4.6 93.2 2,230 506 <1980 <30.0 NA
08/20/2021 2,880 78.8 159 986 19.3 141 <9.8 <8.0 <6.5 <6.2 NA 52.2 <5.8 43.3 416 122 <1440 116 <53.2
10/29/2021
12/27/2021 777 98.3 246 2,040 13.2 200 <4.9 <4.0 <3.2 <3.1 <4.1 39.5 <2.9 21.7 832 236 <722 <19.5 <26.6
5/16/2023 2,390 10.4J 571 2,321 <10.6 582 <12.2 <10.0 <8.1 NA NA 243 <7.3 134 2,190 492 <1,800 <48.8 <231
12/30/2014 <0.079 <0.090 <0.092 <0.29 2.1 <0.12 <0.054 <0.084 <0.12 <0.12 <0.12 <0.094 0.52 <0.11 <0.18 <0.10 NA BQL NA
4/13/2016 <0.5 <0.5 <0.5 <1.5 0.61 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.33 J <0.5 <0.5 <0.5 NA BQL NA
3/14/2018 <0.12 <0.17 <0.13 <0.39 2.4 <0.12 <0.15 <0.13 <0.12 <0.12 <0.15 <0.13 <0.27 <0.12 <0.18 <0.13 NA BQL NA
09/09/2019 <0.25 <0.25 <0.25 <0.25 0.69 <1.0 <0.25 <0.25 <0.25 <0.25 NA <0.25 <0.25 <0.25 <0.25 <0.25 NA <1.0 NA
01/15/2021 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.35 <0.25 <0.25 <0.33 NR <0.24 <0.23 <0.24 <0.19 <0.23 <98.9 <1.5 NA
08/20/2021
10/29/2021
12/27/2021
5/16/2023 <0.34 <0.24 <0.30 <0.71 <0.42 <0.64 <0.49 <0.40 <0.32 NA NA <0.34 <0.29 <0.33 <0.50 <0.33 <0.33 <2.0 <9.2
08/02/2021 18.5 0.61 1.1 2.4 1.5 <0.64 <0.49 0.77 <0.32 0.34J NA 0.45J <0.29 0.78 <0.50 <0.33 <72.2 <2.0 <2.7
08/20/2021 <0.34 <0.48 <0.30 <0.34 1.1 <0.64 <0.49 <0.40 <0.32 1.1 NA <0.34 <0.29 <0.33 <0.50 <0.33 <72.2 <2.0 <2.7
10/29/2021
12/27/2021 <0.34 <0.48 <0.30 <0.34 0.52 <0.64 <0.49 <0.40 <0.32 <0.31 <0.41 <0.34 <0.29 <0.33 <0.50 <0.33 <72.2 <2.0 <2.7
5/16/2023 <0.34 <0.24 <0.30 <0.71 <0.42 <0.64 <0.49 <0.40 <0.32 <0.31 <0.41 <0.34 <0.29 <0.33 <0.50 <0.33 <72.2 <2.0 <9.2
Notes:NA - Not Applicable
Concentrations are reported in micrograms per liter (µg/L)NE - Not Established
"<" = Not Detected at or above the laboratory detection limit LNAPL - Light Non-Aqueous Phase Liquid
J = Estimated value below method reporting limit
Concentrations in BOLD print exceed the 15A 02L .0202 Groundwater Quality Standard (2L Standard).
Concentrations ITALIC print exceed 10 times the 2B Water Standards for Class C surface water bodies.
Concentration in UNDERLINED print exceed the Gross Contamination Level (GCL)
BQL = Below Quantitation Limit
Not Located
AS-1
Not Sampled
Sampling not Required
Sampling not Required
Sampling not Required
Sampling not Required
MW-4
MW-5
Page 2 of 2

FIGURES
SITE
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
REFERENCE: USGS 7.5-MINUTE MAP CHARLOTTE
EAST, NORTH CAROLINA. DATED 2016.
MW-3
MW-4
MW-1
MW-2
FORMER
SCARLETTE'S
66
APPROXIMATE FORMER
FUEL OIL UST & WASTE OIL UST
FORMER GASOLINE
USTs
FORMER GASOLINE
DISPENSER ISLAND
FORMER GASOLINE
DISPENSER ISLAND
FORMER
KEROSENE UST
FORMER KEROSENE
DISPENSER ISLANDSEIGLE AVEN
U
E
B
E
LM
O
N
T

A
V
E
N
U
E
MW-5
P
R
O
P
E
R
T
Y

B
O
U
N
D
A
R
Y
AS-1
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
EXPLANATION
MONITORING WELL LOCATION
AIR SPARGE WELL
SITE MAP
SCARLETTE'S 66 - NCDEQ INCIDENT #36384
1030 SEIGLE AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
2
LB NF AS SHOWN 09/01/2021 SLC3638403
MW-3
MW-4
MW-1
MW-2
FORMER
SCARLETTE'S
66
APPROXIMATE FORMER
FUEL OIL UST & WASTE OIL UST
FORMER GASOLINE
USTs
FORMER GASOLINE
DISPENSER ISLAND
FORMER GASOLINE
DISPENSER ISLAND
FORMER
KEROSENE UST
FORMER KEROSENE
DISPENSER ISLAND
SEI
GLE AVE
N
U
E
B
E
LM
O
N
T

A
V
E
N
U
E
MW-5
P
R
O
P
E
R
T
Y

B
O
U
N
D
A
R
Y
AS-1
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
EXPLANATION
GROUNDWATER ELEVATION (AT WELL)
GROUNDWATER CONTOUR LINE
GROUNDWATER FLOW DIRECTION
MONITORING WELL LOCATION
683.17
683.97
682.47
683.34
679.63
680.41
NOTES:
1.GROUNDWATER LEVELS MEASURED ON 05/16/2023
2.DASHED LINES INDICATE AREAS OF LESS CERTAINTY
NOT MEASUREDNM
NM
AIR SPARGE WELL
GROUNDWATER ELEVATION CONTOUR MAP
SCARLETTE'S 66 - NCDEQ INCIDENT #36384
1030 SEIGLE AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
3
LB VH AS SHOWN 05/24/2023 STL3638401681.0683.0
MW-3
MW-4
MW-1
MW-2
FORMER
SCARLETTE'S
66
APPROXIMATE FORMER
FUEL OIL UST & WASTE OIL UST
FORMER GASOLINE
USTs
FORMER GASOLINE
DISPENSER ISLAND
FORMER GASOLINE
DISPENSER ISLAND
FORMER
KEROSENE UST
FORMER KEROSENE
DISPENSER ISLAND
SEI
GLE AVE
N
U
E
B
E
L
M
O
N
T

A
V
E
N
U
E
MW-5
P
RO
P
E
R
T
Y

B
O
U
N
D
A
R
Y
AS-1
EXPLANATION
MONITORING WELL LOCATION
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
1.GROUNDWATER MONITORING WELLS SAMPLED
05/16/2023
2.CONCENTRATIONS EXPRESSED IN µg/L
(MICROGRAMS PER LITER)
3.ONLY CONCENTRATIONS EXCEEDING 2L
STANDARDS ARE SHOWN
AIR SPARGE WELL
GROUNDWATER QUALITY MAP
SCARLETTE'S 66 - NCDEQ INCIDENT #36384
1030 SEIGLE AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
4
LB VH AS SHOWN 05/24/2023 STL3638401
NS
NS
NS NOT SAMPLED
NS
NS

APPENDIX A
CONCEPTUAL SITE MODEL

Site Name: Scarlett's 66 Date:5/25/2023
Property Owner:Griffith Anderson Pearson Last Field Event Date:5/16/2023
Site Name:Scarlett's 66 Release Discovery Date:1994
NCDEQ UST Incident No.:36384 Source of Release:UST System
Facility ID No.:Unknown Estimated Volume of Release:Unknown
Risk Classification:Intermediate
Risk Rank:Unknown Gasoline (leaded)N
Site Address:1030 Seigle Avenue Gasoline (unleaded)Y
Site City, ST ZIP:Charlotte, North Carolina 28214 Gasoline (ethanol blend)N
Site County:Mecklenburg Diesel N
NCDEQ Regional Office:Mooresville Kerosene Y
Active UST Facility:N Heating Oil (#2)Y
USTs Present:N Heating Oil (>#2)Y
Motor Oil N
Hydraulic Oil N
Major Soil Type:Silty clay Used Oil N
Surface Cover over impacted soil:Pavement
Utilities within plume (Y/N/U):Unknown
>S-W MSCCs (Y/N/U):Unknown
>Residential MSCCs (Y/N/U):Unknown Site (Current):Commercial
>Comm/Ind MSCCs (Y/N/U):Unknown Site (Future):Commercial
North Adjacent:Residential
East Adjacent:Commercial
Litho-Tectonic Zone Charlotte Belt South Adjacent:Commercial
Geologic Formation Unknown West Adjacent:Residential
Rock Type Phylllite/schist/granite
Depth to Bedrock (ft bgs)Unknown Municipal Water (Y/N/U):Y
Active Potable Wells <1000 ft (#/U):N
Active Potable Wells <500 ft (#/U):N
Depth to water (ft-bgs)~15.5ft-bgs Impacted Wells (Y/N/U):N
Gradient (ft/ft):0.033 Any wells <250 ft (Y/N/U):N
Direction (N E S W combo):Northwest
Hydraulic Conductivity (ft/day):Unknown <500 ft (Y/N):Y
Total Porosity (%):Unknown Type of Surface Water:Creek
Effective Porosity (%):Unknown Name of Nearest Stream:Little Sugar Creek
Flow Rate (ft/year):Unknown Stream Classification:Uknown
COCs >2L (Y/N/U):Y Impacted Surface Water (Y/N/U):Unknown
COCs >2L Extent Defined (Y/N):N
COCs >GCLs (Y/N/U):Y
COCs >GCLs (Wells):MW-1 >LEL in Structures:Unknown
COCs >GCLs Extent Defined (Y/N):N Vapors in Buildings:Unknown
COCs >2B Standards by 10X (Y/N/U):Y Slab-on-grade or Crawlspace:Unknown
LNAPL (Y/N/U):Y Dissolved VOCs <5 ft of Structures:Unknown
LNAPL (Max Thickness ft):0.06 LNAPL <15 ft of Structures:Unknown
LNAPL (Wells):MW-2 Basement <30 ft of Dissolved COCs:Unknown
LNAPL Extent Defined (Y/N):N
LNAPL (<5 ft beneath buildings/U):N
Utilities within plume (Y/N/U):Unknown
Alternative Water Source:N/A
NORP:N/A
Site Remediation:N/A
Soil Excavation:N/A
AFVR:N/A
MMPE:targetting MW-1 and MW-2
SVE/AS:N/A
Other:Fate and Transport Model
Additional Support Documentation Available / Data Gaps:
Data Gap: No Risk-Based Parameter soil data to evaluate Maximum Soil
Contaminant Concentrations (MSCCs)
NCDEQ Brownfield, Site#26033-22-060
Approach (general discussion):
Surface Water
Land Use / Zoning
Concentrations of VOCs exceeded the 15A NCAC 02B Surface Water Quality
Standards by more than ten times in wells MW-1 and MW-4, and exceeded the
GCLs in well MW-1 (for benzene only at 6,720 micrograms per liter or µg/L).
Concentrations of VOCs exceeded the 15A NCAC 02L .0202 Groundwater Quality
Standards (2L Standards) in MW-1 and MW-4. Concentrations of VOCs are
decreasing over time in MW-1, and are increasing in MW-4.
CONCEPTUAL SITE MODEL
Soil Information
Possible Path(s) to Closure
Site Information Release Information
Petroleum Type Released
Geologic Information
Groundwater Information
Comments:
Receptor Information
Water Supply
Vapor
Page 1 of 1

APPENDIX B

FIELD NOTES
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: STL3638401
REVIEWED BY: NF SCALE: NTS DATE: 5/23/2023
Scarlette's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, NC 28205
NCDEQ UST Incident #36384
Photo #2: MW-2 Well Location
Photo #1: MW-1 Well Location
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: STL3638401
REVIEWED BY: NF SCALE: NTS DATE: 5/23/2023
Scarlette's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, NC 28205
NCDEQ UST Incident #36384
Photo #4: MW-3 Well Location
Photo #3: MW-2 LNAPL
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: STL3638401
REVIEWED BY: NF SCALE: NTS DATE: 5/23/2023
Scarlette's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, NC 28205
NCDEQ UST Incident #36384
Photo #6: MW-4 Well Location
Photo #5: MW-4 Well Location
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: STL3638401
REVIEWED BY: NF SCALE: NTS DATE: 5/23/2023
Scarlette's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, NC 28205
NCDEQ UST Incident #36384
Photo #8: AS-1 Well Location
Photo #7: MW-5 Well Location
ATC Associates of North Carolina, P.C.
7606 Whitehall Exec Ctr Dr, Ste 800
Charlotte, NC 28273
[phone]
PHOTOGRAPHS
ATC PROJECT NO: STL3638401
REVIEWED BY: NF SCALE: NTS DATE: 5/30/2023
Scarlette's 66
1030 Seigle Avenue
Charlotte, Mecklenburg County, NC 28205
NCDEQ UST Incident #36384
Photo #10: General Site Photo
Photo #9: General Site Photo

APPENDIX C

LABORATORY ANALYTICAL REPORT

#=CL#
May 23, 2023
LIMS USE: FR - NOELLE FRANCE
LIMS OBJECT ID: 92667617
92667617
Project:
Pace Project No.:
RE:
Noelle France
ATC Group Services LLC- South Charlotte
7606 Whitehall Exe Center Dr
Suite 800
Charlotte, NC 28273
SCARLETT'S 66
Dear Noelle France:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Lab ID Sample ID Matrix Date Collected Date Received
92667617001 MW-1 Water 05/16/23 10:45 05/16/23 13:49
92667617002 MW-3 Water 05/16/23 09:40 05/16/23 13:49
92667617003 MW-4 Water 05/16/23 10:15 05/16/23 13:49
92667617004 MW-5 Water 05/16/23 12:15 05/16/23 13:49
92667617005 AS-1 Water 05/16/23 11:45 05/16/23 13:49
92667617006 FB-01 Water 05/16/23 12:20 05/16/23 13:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667617001 MW-1 SM 6200B 69 PASI-CSAS
92667617002 MW-3 SM 6200B 69 PASI-CSAS
92667617003 MW-4 SM 6200B 69 PASI-CLMB
92667617004 MW-5 SM 6200B 69 PASI-CSAS
92667617005 AS-1 SM 6200B 69 PASI-CSAS
92667617006 FB-01 SM 6200B 69 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-1 Lab ID:92667617001 Collected:05/16/23 10:45 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <7280 ug/L 05/21/23 18:57 75-85-4200007280200
tert-Amylmethyl ether <1850 ug/L 05/21/23 18:57 994-05-820001850200
Benzene 6720 ug/L 05/21/23 18:57 71-43-210069.0 200
Bromobenzene <58.0 ug/L 05/21/23 18:57 108-86-110058.0 200
Bromochloromethane <93.6 ug/L 05/21/23 18:57 74-97-510093.6 200
Bromodichloromethane <61.4 ug/L 05/21/23 18:57 75-27-410061.4 200
Bromoform <68.2 ug/L 05/21/23 18:57 75-25-210068.2 200
Bromomethane <332 ug/L 05/21/23 18:57 74-83-91000332200
tert-Butyl Alcohol <5360 ug/L 05/21/23 18:57 75-65-0100005360200
n-Butylbenzene <98.0 ug/L 05/21/23 18:57 104-51-810098.0 200
sec-Butylbenzene <80.0 ug/L 05/21/23 18:57 135-98-810080.0 200
tert-Butylbenzene <64.6 ug/L 05/21/23 18:57 98-06-610064.6 200
tert-Butyl Formate <5880 ug/L 05/21/23 18:57 762-75-4100005880200
Carbon tetrachloride <66.6 ug/L 05/21/23 18:57 56-23-510066.6 200
Chlorobenzene <56.8 ug/L 05/21/23 18:57 108-90-710056.8 200
Chloroethane <130 ug/L 05/21/23 18:57 75-00-3 L1200130200
Chloroform <86.0 ug/L 05/21/23 18:57 67-66-310086.0 200
Chloromethane <108 ug/L 05/21/23 18:57 74-87-3200108200
2-Chlorotoluene <64.2 ug/L 05/21/23 18:57 95-49-810064.2 200
4-Chlorotoluene <64.8 ug/L 05/21/23 18:57 106-43-410064.8 200
1,2-Dibromo-3-chloropropane <68.0 ug/L 05/21/23 18:57 96-12-820068.0 200
Dibromochloromethane <71.8 ug/L 05/21/23 18:57 124-48-1 IH10071.8 200
1,2-Dibromoethane (EDB)<54.4 ug/L 05/21/23 18:57 106-93-410054.4 200
Dibromomethane <78.8 ug/L 05/21/23 18:57 74-95-310078.8 200
1,2-Dichlorobenzene <67.8 ug/L 05/21/23 18:57 95-50-110067.8 200
1,3-Dichlorobenzene <68.0 ug/L 05/21/23 18:57 541-73-110068.0 200
1,4-Dichlorobenzene <66.6 ug/L 05/21/23 18:57 106-46-710066.6 200
Dichlorodifluoromethane <69.2 ug/L 05/21/23 18:57 75-71-810069.2 200
1,1-Dichloroethane <73.4 ug/L 05/21/23 18:57 75-34-310073.4 200
1,2-Dichloroethane <64.4 ug/L 05/21/23 18:57 107-06-210064.4 200
1,1-Dichloroethene <69.6 ug/L 05/21/23 18:57 75-35-410069.6 200
cis-1,2-Dichloroethene <76.8 ug/L 05/21/23 18:57 156-59-210076.8 200
trans-1,2-Dichloroethene <79.2 ug/L 05/21/23 18:57 156-60-510079.2 200
1,2-Dichloropropane <71.0 ug/L 05/21/23 18:57 78-87-510071.0 200
1,3-Dichloropropane <56.8 ug/L 05/21/23 18:57 142-28-910056.8 200
2,2-Dichloropropane <77.6 ug/L 05/21/23 18:57 594-20-710077.6 200
1,1-Dichloropropene <85.4 ug/L 05/21/23 18:57 563-58-610085.4 200
cis-1,3-Dichloropropene <73.0 ug/L 05/21/23 18:57 10061-01-510073.0 200
trans-1,3-Dichloropropene <72.6 ug/L 05/21/23 18:57 10061-02-610072.6 200
Diisopropyl ether <61.6 ug/L 05/21/23 18:57 108-20-310061.6 200
Ethanol <14400 ug/L 05/21/23 18:57 64-17-54000014400200
Ethylbenzene 3820 ug/L 05/21/23 18:57 100-41-410060.8 200
Ethyl-tert-butyl ether <648 ug/L 05/21/23 18:57 637-92-32000648200
Hexachloro-1,3-butadiene <306 ug/L 05/21/23 18:57 87-68-3400306200
Isopropylbenzene (Cumene)132 ug/L 05/21/23 18:57 98-82-810066.6 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-1 Lab ID:92667617001 Collected:05/16/23 10:45 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <390 ug/L 05/21/23 18:57 75-09-2400390200
Methyl-tert-butyl ether <84.4 ug/L 05/21/23 18:57 1634-04-410084.4 200
Naphthalene 687 ug/L 05/21/23 18:57 91-20-3400129200
n-Propylbenzene 345 ug/L 05/21/23 18:57 103-65-110068.0 200
Styrene <58.4 ug/L 05/21/23 18:57 100-42-510058.4 200
1,1,1,2-Tetrachloroethane <62.2 ug/L 05/21/23 18:57 630-20-610062.2 200
1,1,2,2-Tetrachloroethane <45.0 ug/L 05/21/23 18:57 79-34-510045.0 200
Tetrachloroethene <58.4 ug/L 05/21/23 18:57 127-18-410058.4 200
Toluene 39500 ug/L 05/21/23 18:57 108-88-310047.8 200
1,2,3-Trichlorobenzene <161 ug/L 05/21/23 18:57 87-61-6400161200
1,2,4-Trichlorobenzene <128 ug/L 05/21/23 18:57 120-82-1400128200
1,1,1-Trichloroethane <66.4 ug/L 05/21/23 18:57 71-55-610066.4 200
1,1,2-Trichloroethane <65.0 ug/L 05/21/23 18:57 79-00-510065.0 200
Trichloroethene <76.6 ug/L 05/21/23 18:57 79-01-610076.6 200
Trichlorofluoromethane <59.6 ug/L 05/21/23 18:57 75-69-420059.6 200
1,2,3-Trichloropropane <52.2 ug/L 05/21/23 18:57 96-18-410052.2 200
1,2,4-Trimethylbenzene 3100 ug/L 05/21/23 18:57 95-63-610099.0 200
1,3,5-Trimethylbenzene 794 ug/L 05/21/23 18:57 108-67-810066.4 200
Vinyl chloride <77.2 ug/L 05/21/23 18:57 75-01-420077.2 200
m&p-Xylene 14100 ug/L 05/21/23 18:57 179601-23-1200142200
o-Xylene 7980 ug/L 05/21/23 18:57 95-47-610067.6 200
Surrogates
1,2-Dichloroethane-d4 (S)120 %05/21/23 18:57 17060-07-070-130 200
4-Bromofluorobenzene (S)96 %05/21/23 18:57 460-00-470-130 200
Toluene-d8 (S)101 %05/21/23 18:57 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-3 Lab ID:92667617002 Collected:05/16/23 09:40 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/21/23 18:04 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/21/23 18:04 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/21/23 18:04 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/21/23 18:04 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/21/23 18:04 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/21/23 18:04 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/21/23 18:04 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/21/23 18:04 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/21/23 18:04 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/21/23 18:04 104-51-80.50 0.49 1
sec-Butylbenzene 2.9 ug/L 05/21/23 18:04 135-98-80.50 0.40 1
tert-Butylbenzene 0.65 ug/L 05/21/23 18:04 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/21/23 18:04 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/21/23 18:04 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/21/23 18:04 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/21/23 18:04 75-00-3 L11.0 0.65 1
Chloroform <0.43 ug/L 05/21/23 18:04 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/21/23 18:04 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/21/23 18:04 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/21/23 18:04 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/21/23 18:04 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/21/23 18:04 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/21/23 18:04 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/21/23 18:04 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/21/23 18:04 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/21/23 18:04 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/21/23 18:04 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/21/23 18:04 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/21/23 18:04 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/21/23 18:04 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/21/23 18:04 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/21/23 18:04 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/21/23 18:04 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/21/23 18:04 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/21/23 18:04 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/21/23 18:04 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/21/23 18:04 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/21/23 18:04 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/21/23 18:04 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/21/23 18:04 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/21/23 18:04 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/21/23 18:04 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/21/23 18:04 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/21/23 18:04 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/21/23 18:04 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-3 Lab ID:92667617002 Collected:05/16/23 09:40 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/21/23 18:04 75-09-22.0 2.0 1
Methyl-tert-butyl ether 0.94 ug/L 05/21/23 18:04 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/21/23 18:04 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/21/23 18:04 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/21/23 18:04 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/21/23 18:04 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/21/23 18:04 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/21/23 18:04 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/21/23 18:04 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/21/23 18:04 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/21/23 18:04 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/21/23 18:04 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/21/23 18:04 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/21/23 18:04 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/21/23 18:04 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/21/23 18:04 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/21/23 18:04 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/21/23 18:04 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/21/23 18:04 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/21/23 18:04 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/21/23 18:04 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)124 %05/21/23 18:04 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %05/21/23 18:04 460-00-470-130 1
Toluene-d8 (S)103 %05/21/23 18:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-4 Lab ID:92667617003 Collected:05/16/23 10:15 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <910 ug/L 05/22/23 17:38 75-85-4250091025
tert-Amylmethyl ether <231 ug/L 05/22/23 17:38 994-05-825023125
Benzene 2390 ug/L 05/22/23 17:38 71-43-212.5 8.6 25
Bromobenzene <7.2 ug/L 05/22/23 17:38 108-86-112.5 7.2 25
Bromochloromethane <11.7 ug/L 05/22/23 17:38 74-97-512.5 11.7 25
Bromodichloromethane <7.7 ug/L 05/22/23 17:38 75-27-412.5 7.7 25
Bromoform <8.5 ug/L 05/22/23 17:38 75-25-212.5 8.5 25
Bromomethane <41.5 ug/L 05/22/23 17:38 74-83-912541.5 25
tert-Butyl Alcohol <670 ug/L 05/22/23 17:38 75-65-0125067025
n-Butylbenzene <12.2 ug/L 05/22/23 17:38 104-51-812.5 12.2 25
sec-Butylbenzene <10.0 ug/L 05/22/23 17:38 135-98-812.5 10.0 25
tert-Butylbenzene <8.1 ug/L 05/22/23 17:38 98-06-612.5 8.1 25
tert-Butyl Formate <735 ug/L 05/22/23 17:38 762-75-4125073525
Carbon tetrachloride <8.3 ug/L 05/22/23 17:38 56-23-512.5 8.3 25
Chlorobenzene <7.1 ug/L 05/22/23 17:38 108-90-712.5 7.1 25
Chloroethane <16.2 ug/L 05/22/23 17:38 75-00-325.0 16.2 25
Chloroform <10.8 ug/L 05/22/23 17:38 67-66-312.5 10.8 25
Chloromethane <13.5 ug/L 05/22/23 17:38 74-87-325.0 13.5 25
2-Chlorotoluene <8.0 ug/L 05/22/23 17:38 95-49-812.5 8.0 25
4-Chlorotoluene <8.1 ug/L 05/22/23 17:38 106-43-412.5 8.1 25
1,2-Dibromo-3-chloropropane <8.5 ug/L 05/22/23 17:38 96-12-825.0 8.5 25
Dibromochloromethane <9.0 ug/L 05/22/23 17:38 124-48-112.5 9.0 25
1,2-Dibromoethane (EDB)<6.8 ug/L 05/22/23 17:38 106-93-412.5 6.8 25
Dibromomethane <9.8 ug/L 05/22/23 17:38 74-95-312.5 9.8 25
1,2-Dichlorobenzene <8.5 ug/L 05/22/23 17:38 95-50-112.5 8.5 25
1,3-Dichlorobenzene <8.5 ug/L 05/22/23 17:38 541-73-112.5 8.5 25
1,4-Dichlorobenzene <8.3 ug/L 05/22/23 17:38 106-46-712.5 8.3 25
Dichlorodifluoromethane <8.6 ug/L 05/22/23 17:38 75-71-812.5 8.6 25
1,1-Dichloroethane <9.2 ug/L 05/22/23 17:38 75-34-312.5 9.2 25
1,2-Dichloroethane <8.0 ug/L 05/22/23 17:38 107-06-212.5 8.0 25
1,1-Dichloroethene <8.7 ug/L 05/22/23 17:38 75-35-412.5 8.7 25
cis-1,2-Dichloroethene <9.6 ug/L 05/22/23 17:38 156-59-212.5 9.6 25
trans-1,2-Dichloroethene <9.9 ug/L 05/22/23 17:38 156-60-512.5 9.9 25
1,2-Dichloropropane <8.9 ug/L 05/22/23 17:38 78-87-512.5 8.9 25
1,3-Dichloropropane <7.1 ug/L 05/22/23 17:38 142-28-912.5 7.1 25
2,2-Dichloropropane <9.7 ug/L 05/22/23 17:38 594-20-712.5 9.7 25
1,1-Dichloropropene <10.7 ug/L 05/22/23 17:38 563-58-612.5 10.7 25
cis-1,3-Dichloropropene <9.1 ug/L 05/22/23 17:38 10061-01-512.5 9.1 25
trans-1,3-Dichloropropene <9.1 ug/L 05/22/23 17:38 10061-02-612.5 9.1 25
Diisopropyl ether <7.7 ug/L 05/22/23 17:38 108-20-312.5 7.7 25
Ethanol <1800 ug/L 05/22/23 17:38 64-17-55000180025
Ethylbenzene 571 ug/L 05/22/23 17:38 100-41-412.5 7.6 25
Ethyl-tert-butyl ether <81.0 ug/L 05/22/23 17:38 637-92-325081.0 25
Hexachloro-1,3-butadiene <38.2 ug/L 05/22/23 17:38 87-68-350.0 38.2 25
Isopropylbenzene (Cumene)134 ug/L 05/22/23 17:38 98-82-812.5 8.3 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-4 Lab ID:92667617003 Collected:05/16/23 10:15 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <48.8 ug/L 05/22/23 17:38 75-09-250.0 48.8 25
Methyl-tert-butyl ether <10.6 ug/L 05/22/23 17:38 1634-04-412.5 10.6 25
Naphthalene 582 ug/L 05/22/23 17:38 91-20-350.0 16.1 25
n-Propylbenzene 243 ug/L 05/22/23 17:38 103-65-112.5 8.5 25
Styrene <7.3 ug/L 05/22/23 17:38 100-42-512.5 7.3 25
1,1,1,2-Tetrachloroethane <7.8 ug/L 05/22/23 17:38 630-20-612.5 7.8 25
1,1,2,2-Tetrachloroethane <5.6 ug/L 05/22/23 17:38 79-34-512.5 5.6 25
Tetrachloroethene <7.3 ug/L 05/22/23 17:38 127-18-412.5 7.3 25
Toluene 10.4J ug/L 05/22/23 17:38 108-88-312.5 6.0 25
1,2,3-Trichlorobenzene <20.2 ug/L 05/22/23 17:38 87-61-650.0 20.2 25
1,2,4-Trichlorobenzene <16.0 ug/L 05/22/23 17:38 120-82-150.0 16.0 25
1,1,1-Trichloroethane <8.3 ug/L 05/22/23 17:38 71-55-612.5 8.3 25
1,1,2-Trichloroethane <8.1 ug/L 05/22/23 17:38 79-00-512.5 8.1 25
Trichloroethene <9.6 ug/L 05/22/23 17:38 79-01-612.5 9.6 25
Trichlorofluoromethane <7.4 ug/L 05/22/23 17:38 75-69-425.0 7.4 25
1,2,3-Trichloropropane <6.5 ug/L 05/22/23 17:38 96-18-412.5 6.5 25
1,2,4-Trimethylbenzene 2190 ug/L 05/22/23 17:38 95-63-612.5 12.4 25
1,3,5-Trimethylbenzene 492 ug/L 05/22/23 17:38 108-67-812.5 8.3 25
Vinyl chloride <9.6 ug/L 05/22/23 17:38 75-01-425.0 9.6 25
m&p-Xylene 2210 ug/L 05/22/23 17:38 179601-23-125.0 17.7 25
o-Xylene 111 ug/L 05/22/23 17:38 95-47-612.5 8.4 25
Surrogates
1,2-Dichloroethane-d4 (S)91 %05/22/23 17:38 17060-07-070-130 25
4-Bromofluorobenzene (S)100 %05/22/23 17:38 460-00-470-130 25
Toluene-d8 (S)102 %05/22/23 17:38 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-5 Lab ID:92667617004 Collected:05/16/23 12:15 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/21/23 14:48 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/21/23 14:48 994-05-8 M110.0 9.2 1
Benzene <0.34 ug/L 05/21/23 14:48 71-43-2 M10.50 0.34 1
Bromobenzene <0.29 ug/L 05/21/23 14:48 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/21/23 14:48 74-97-5 M10.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/21/23 14:48 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/21/23 14:48 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/21/23 14:48 74-83-9 M15.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/21/23 14:48 75-65-0 M150.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/21/23 14:48 104-51-8 M10.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/21/23 14:48 135-98-8 M10.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/21/23 14:48 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/21/23 14:48 762-75-4 M150.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/21/23 14:48 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/21/23 14:48 108-90-7 M10.50 0.28 1
Chloroethane <0.65 ug/L 05/21/23 14:48 75-00-3 L1,M01.0 0.65 1
Chloroform <0.43 ug/L 05/21/23 14:48 67-66-3 M10.50 0.43 1
Chloromethane <0.54 ug/L 05/21/23 14:48 74-87-3 M11.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/21/23 14:48 95-49-8 M10.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/21/23 14:48 106-43-4 M10.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/21/23 14:48 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/21/23 14:48 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/21/23 14:48 106-93-4 M10.50 0.27 1
Dibromomethane <0.39 ug/L 05/21/23 14:48 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/21/23 14:48 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/21/23 14:48 541-73-1 M10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/21/23 14:48 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/21/23 14:48 75-71-8 IH,M10.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/21/23 14:48 75-34-3 M10.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/21/23 14:48 107-06-2 M10.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/21/23 14:48 75-35-4 M10.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/21/23 14:48 156-59-2 M10.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/21/23 14:48 156-60-5 M10.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/21/23 14:48 78-87-5 M10.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/21/23 14:48 142-28-9 M10.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/21/23 14:48 594-20-7 M10.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/21/23 14:48 563-58-6 M10.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/21/23 14:48 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/21/23 14:48 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/21/23 14:48 108-20-3 M10.50 0.31 1
Ethanol <72.2 ug/L 05/21/23 14:48 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/21/23 14:48 100-41-4 M10.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/21/23 14:48 637-92-3 M110.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/21/23 14:48 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/21/23 14:48 98-82-8 M10.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:MW-5 Lab ID:92667617004 Collected:05/16/23 12:15 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/21/23 14:48 75-09-2 M12.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/21/23 14:48 1634-04-4 M10.50 0.42 1
Naphthalene <0.64 ug/L 05/21/23 14:48 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/21/23 14:48 103-65-1 M10.50 0.34 1
Styrene <0.29 ug/L 05/21/23 14:48 100-42-5 M10.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/21/23 14:48 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/21/23 14:48 79-34-5 M10.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/21/23 14:48 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/21/23 14:48 108-88-3 M10.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/21/23 14:48 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/21/23 14:48 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/21/23 14:48 71-55-6 M10.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/21/23 14:48 79-00-5 M10.50 0.32 1
Trichloroethene <0.38 ug/L 05/21/23 14:48 79-01-6 M10.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/21/23 14:48 75-69-4 M11.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/21/23 14:48 96-18-4 M10.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/21/23 14:48 95-63-6 M10.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/21/23 14:48 108-67-8 M10.50 0.33 1
Vinyl chloride <0.39 ug/L 05/21/23 14:48 75-01-4 M11.0 0.39 1
m&p-Xylene <0.71 ug/L 05/21/23 14:48 179601-23-1 M11.0 0.71 1
o-Xylene <0.34 ug/L 05/21/23 14:48 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %05/21/23 14:48 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %05/21/23 14:48 460-00-470-130 1
Toluene-d8 (S)102 %05/21/23 14:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:AS-1 Lab ID:92667617005 Collected:05/16/23 11:45 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/21/23 15:06 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/21/23 15:06 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/21/23 15:06 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/21/23 15:06 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/21/23 15:06 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/21/23 15:06 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/21/23 15:06 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/21/23 15:06 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/21/23 15:06 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/21/23 15:06 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/21/23 15:06 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/21/23 15:06 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/21/23 15:06 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/21/23 15:06 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/21/23 15:06 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/21/23 15:06 75-00-3 L11.0 0.65 1
Chloroform <0.43 ug/L 05/21/23 15:06 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/21/23 15:06 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/21/23 15:06 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/21/23 15:06 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/21/23 15:06 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/21/23 15:06 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/21/23 15:06 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/21/23 15:06 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/21/23 15:06 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/21/23 15:06 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/21/23 15:06 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/21/23 15:06 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/21/23 15:06 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/21/23 15:06 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/21/23 15:06 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/21/23 15:06 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/21/23 15:06 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/21/23 15:06 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/21/23 15:06 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/21/23 15:06 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/21/23 15:06 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/21/23 15:06 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/21/23 15:06 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/21/23 15:06 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/21/23 15:06 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/21/23 15:06 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/21/23 15:06 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/21/23 15:06 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/21/23 15:06 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:AS-1 Lab ID:92667617005 Collected:05/16/23 11:45 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/21/23 15:06 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/21/23 15:06 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/21/23 15:06 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/21/23 15:06 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/21/23 15:06 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/21/23 15:06 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/21/23 15:06 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/21/23 15:06 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/21/23 15:06 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/21/23 15:06 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/21/23 15:06 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/21/23 15:06 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/21/23 15:06 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/21/23 15:06 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/21/23 15:06 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/21/23 15:06 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/21/23 15:06 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/21/23 15:06 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/21/23 15:06 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/21/23 15:06 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/21/23 15:06 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)124 %05/21/23 15:06 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %05/21/23 15:06 460-00-470-130 1
Toluene-d8 (S)104 %05/21/23 15:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:FB-01 Lab ID:92667617006 Collected:05/16/23 12:20 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol <36.4 ug/L 05/21/23 14:13 75-85-410036.4 1
tert-Amylmethyl ether <9.2 ug/L 05/21/23 14:13 994-05-810.0 9.2 1
Benzene <0.34 ug/L 05/21/23 14:13 71-43-20.50 0.34 1
Bromobenzene <0.29 ug/L 05/21/23 14:13 108-86-10.50 0.29 1
Bromochloromethane <0.47 ug/L 05/21/23 14:13 74-97-50.50 0.47 1
Bromodichloromethane <0.31 ug/L 05/21/23 14:13 75-27-40.50 0.31 1
Bromoform <0.34 ug/L 05/21/23 14:13 75-25-20.50 0.34 1
Bromomethane <1.7 ug/L 05/21/23 14:13 74-83-95.0 1.7 1
tert-Butyl Alcohol <26.8 ug/L 05/21/23 14:13 75-65-050.0 26.8 1
n-Butylbenzene <0.49 ug/L 05/21/23 14:13 104-51-80.50 0.49 1
sec-Butylbenzene <0.40 ug/L 05/21/23 14:13 135-98-80.50 0.40 1
tert-Butylbenzene <0.32 ug/L 05/21/23 14:13 98-06-60.50 0.32 1
tert-Butyl Formate <29.4 ug/L 05/21/23 14:13 762-75-450.0 29.4 1
Carbon tetrachloride <0.33 ug/L 05/21/23 14:13 56-23-50.50 0.33 1
Chlorobenzene <0.28 ug/L 05/21/23 14:13 108-90-70.50 0.28 1
Chloroethane <0.65 ug/L 05/21/23 14:13 75-00-3 L11.0 0.65 1
Chloroform <0.43 ug/L 05/21/23 14:13 67-66-30.50 0.43 1
Chloromethane <0.54 ug/L 05/21/23 14:13 74-87-31.0 0.54 1
2-Chlorotoluene <0.32 ug/L 05/21/23 14:13 95-49-80.50 0.32 1
4-Chlorotoluene <0.32 ug/L 05/21/23 14:13 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane <0.34 ug/L 05/21/23 14:13 96-12-81.0 0.34 1
Dibromochloromethane <0.36 ug/L 05/21/23 14:13 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)<0.27 ug/L 05/21/23 14:13 106-93-40.50 0.27 1
Dibromomethane <0.39 ug/L 05/21/23 14:13 74-95-30.50 0.39 1
1,2-Dichlorobenzene <0.34 ug/L 05/21/23 14:13 95-50-10.50 0.34 1
1,3-Dichlorobenzene <0.34 ug/L 05/21/23 14:13 541-73-10.50 0.34 1
1,4-Dichlorobenzene <0.33 ug/L 05/21/23 14:13 106-46-70.50 0.33 1
Dichlorodifluoromethane <0.35 ug/L 05/21/23 14:13 75-71-8 IH0.50 0.35 1
1,1-Dichloroethane <0.37 ug/L 05/21/23 14:13 75-34-30.50 0.37 1
1,2-Dichloroethane <0.32 ug/L 05/21/23 14:13 107-06-20.50 0.32 1
1,1-Dichloroethene <0.35 ug/L 05/21/23 14:13 75-35-40.50 0.35 1
cis-1,2-Dichloroethene <0.38 ug/L 05/21/23 14:13 156-59-20.50 0.38 1
trans-1,2-Dichloroethene <0.40 ug/L 05/21/23 14:13 156-60-50.50 0.40 1
1,2-Dichloropropane <0.36 ug/L 05/21/23 14:13 78-87-50.50 0.36 1
1,3-Dichloropropane <0.28 ug/L 05/21/23 14:13 142-28-90.50 0.28 1
2,2-Dichloropropane <0.39 ug/L 05/21/23 14:13 594-20-70.50 0.39 1
1,1-Dichloropropene <0.43 ug/L 05/21/23 14:13 563-58-60.50 0.43 1
cis-1,3-Dichloropropene <0.36 ug/L 05/21/23 14:13 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.36 ug/L 05/21/23 14:13 10061-02-60.50 0.36 1
Diisopropyl ether <0.31 ug/L 05/21/23 14:13 108-20-30.50 0.31 1
Ethanol <72.2 ug/L 05/21/23 14:13 64-17-520072.2 1
Ethylbenzene <0.30 ug/L 05/21/23 14:13 100-41-40.50 0.30 1
Ethyl-tert-butyl ether <3.2 ug/L 05/21/23 14:13 637-92-310.0 3.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 05/21/23 14:13 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)<0.33 ug/L 05/21/23 14:13 98-82-80.50 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Sample:FB-01 Lab ID:92667617006 Collected:05/16/23 12:20 Received:05/16/23 13:49 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methylene Chloride <2.0 ug/L 05/21/23 14:13 75-09-22.0 2.0 1
Methyl-tert-butyl ether <0.42 ug/L 05/21/23 14:13 1634-04-40.50 0.42 1
Naphthalene <0.64 ug/L 05/21/23 14:13 91-20-32.0 0.64 1
n-Propylbenzene <0.34 ug/L 05/21/23 14:13 103-65-10.50 0.34 1
Styrene <0.29 ug/L 05/21/23 14:13 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane <0.31 ug/L 05/21/23 14:13 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane <0.22 ug/L 05/21/23 14:13 79-34-50.50 0.22 1
Tetrachloroethene <0.29 ug/L 05/21/23 14:13 127-18-40.50 0.29 1
Toluene <0.24 ug/L 05/21/23 14:13 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene <0.81 ug/L 05/21/23 14:13 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene <0.64 ug/L 05/21/23 14:13 120-82-12.0 0.64 1
1,1,1-Trichloroethane <0.33 ug/L 05/21/23 14:13 71-55-60.50 0.33 1
1,1,2-Trichloroethane <0.32 ug/L 05/21/23 14:13 79-00-50.50 0.32 1
Trichloroethene <0.38 ug/L 05/21/23 14:13 79-01-60.50 0.38 1
Trichlorofluoromethane <0.30 ug/L 05/21/23 14:13 75-69-41.0 0.30 1
1,2,3-Trichloropropane <0.26 ug/L 05/21/23 14:13 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/21/23 14:13 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene <0.33 ug/L 05/21/23 14:13 108-67-80.50 0.33 1
Vinyl chloride <0.39 ug/L 05/21/23 14:13 75-01-41.0 0.39 1
m&p-Xylene <0.71 ug/L 05/21/23 14:13 179601-23-11.0 0.71 1
o-Xylene <0.34 ug/L 05/21/23 14:13 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)123 %05/21/23 14:13 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %05/21/23 14:13 460-00-470-130 1
Toluene-d8 (S)102 %05/21/23 14:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775917
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667617001, 92667617002, 92667617004, 92667617005, 92667617006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026083
Associated Lab Samples:92667617001, 92667617002, 92667617004, 92667617005, 92667617006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 05/21/23 13:550.31
1,1,1-Trichloroethane ug/L <0.33 0.50 05/21/23 13:550.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 05/21/23 13:550.22
1,1,2-Trichloroethane ug/L <0.32 0.50 05/21/23 13:550.32
1,1-Dichloroethane ug/L <0.37 0.50 05/21/23 13:550.37
1,1-Dichloroethene ug/L <0.35 0.50 05/21/23 13:550.35
1,1-Dichloropropene ug/L <0.43 0.50 05/21/23 13:550.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 05/21/23 13:550.81
1,2,3-Trichloropropane ug/L <0.26 0.50 05/21/23 13:550.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 05/21/23 13:550.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/21/23 13:550.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 05/21/23 13:550.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 05/21/23 13:550.27
1,2-Dichlorobenzene ug/L <0.34 0.50 05/21/23 13:550.34
1,2-Dichloroethane ug/L <0.32 0.50 05/21/23 13:550.32
1,2-Dichloropropane ug/L <0.36 0.50 05/21/23 13:550.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 05/21/23 13:550.33
1,3-Dichlorobenzene ug/L <0.34 0.50 05/21/23 13:550.34
1,3-Dichloropropane ug/L <0.28 0.50 05/21/23 13:550.28
1,4-Dichlorobenzene ug/L <0.33 0.50 05/21/23 13:550.33
2,2-Dichloropropane ug/L <0.39 0.50 05/21/23 13:550.39
2-Chlorotoluene ug/L <0.32 0.50 05/21/23 13:550.32
4-Chlorotoluene ug/L <0.32 0.50 05/21/23 13:550.32
Benzene ug/L <0.34 0.50 05/21/23 13:550.34
Bromobenzene ug/L <0.29 0.50 05/21/23 13:550.29
Bromochloromethane ug/L <0.47 0.50 05/21/23 13:550.47
Bromodichloromethane ug/L <0.31 0.50 05/21/23 13:550.31
Bromoform ug/L <0.34 0.50 05/21/23 13:550.34
Bromomethane ug/L <1.7 5.0 05/21/23 13:551.7
Carbon tetrachloride ug/L <0.33 0.50 05/21/23 13:550.33
Chlorobenzene ug/L <0.28 0.50 05/21/23 13:550.28
Chloroethane ug/L <0.65 1.0 05/21/23 13:550.65
Chloroform ug/L <0.43 0.50 05/21/23 13:550.43
Chloromethane ug/L <0.54 1.0 05/21/23 13:550.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 05/21/23 13:550.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 05/21/23 13:550.36
Dibromochloromethane ug/L <0.36 0.50 05/21/23 13:550.36
Dibromomethane ug/L <0.39 0.50 05/21/23 13:550.39
Dichlorodifluoromethane ug/L <0.35 0.50 IH05/21/23 13:550.35
Diisopropyl ether ug/L <0.31 0.50 05/21/23 13:550.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026083
Associated Lab Samples:92667617001, 92667617002, 92667617004, 92667617005, 92667617006
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 05/21/23 13:5572.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 05/21/23 13:553.2
Ethylbenzene ug/L <0.30 0.50 05/21/23 13:550.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 05/21/23 13:551.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 05/21/23 13:550.33
m&p-Xylene ug/L <0.71 1.0 05/21/23 13:550.71
Methyl-tert-butyl ether ug/L <0.42 0.50 05/21/23 13:550.42
Methylene Chloride ug/L <2.0 2.0 05/21/23 13:552.0
n-Butylbenzene ug/L <0.49 0.50 05/21/23 13:550.49
n-Propylbenzene ug/L <0.34 0.50 05/21/23 13:550.34
Naphthalene ug/L <0.64 2.0 05/21/23 13:550.64
o-Xylene ug/L <0.34 0.50 05/21/23 13:550.34
sec-Butylbenzene ug/L <0.40 0.50 05/21/23 13:550.40
Styrene ug/L <0.29 0.50 05/21/23 13:550.29
tert-Amyl Alcohol ug/L <36.4 100 05/21/23 13:5536.4
tert-Amylmethyl ether ug/L <9.2 10.0 05/21/23 13:559.2
tert-Butyl Alcohol ug/L <26.8 50.0 05/21/23 13:5526.8
tert-Butyl Formate ug/L <29.4 50.0 05/21/23 13:5529.4
tert-Butylbenzene ug/L <0.32 0.50 05/21/23 13:550.32
Tetrachloroethene ug/L <0.29 0.50 05/21/23 13:550.29
Toluene ug/L <0.24 0.50 05/21/23 13:550.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 05/21/23 13:550.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 05/21/23 13:550.36
Trichloroethene ug/L <0.38 0.50 05/21/23 13:550.38
Trichlorofluoromethane ug/L <0.30 1.0 05/21/23 13:550.30
Vinyl chloride ug/L <0.39 1.0 05/21/23 13:550.39
1,2-Dichloroethane-d4 (S)%123 70-130 05/21/23 13:55
4-Bromofluorobenzene (S)%97 70-130 05/21/23 13:55
Toluene-d8 (S)%103 70-130 05/21/23 13:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026084LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.920 105 60-140
1,1,1-Trichloroethane ug/L 23.020 115 60-140
1,1,2,2-Tetrachloroethane ug/L 22.820 114 60-140
1,1,2-Trichloroethane ug/L 21.420 107 60-140
1,1-Dichloroethane ug/L 25.520 127 60-140
1,1-Dichloroethene ug/L 25.120 126 60-140
1,1-Dichloropropene ug/L 26.320 131 60-140
1,2,3-Trichlorobenzene ug/L 18.420 92 60-140
1,2,3-Trichloropropane ug/L 21.820 109 60-140
1,2,4-Trichlorobenzene ug/L 19.020 95 60-140
1,2,4-Trimethylbenzene ug/L 22.120 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026084LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 17.320 86 60-140
1,2-Dibromoethane (EDB)ug/L 21.720 109 60-140
1,2-Dichlorobenzene ug/L 21.120 106 60-140
1,2-Dichloroethane ug/L 23.720 119 60-140
1,2-Dichloropropane ug/L 23.820 119 60-140
1,3,5-Trimethylbenzene ug/L 22.820 114 60-140
1,3-Dichlorobenzene ug/L 21.620 108 60-140
1,3-Dichloropropane ug/L 22.320 112 60-140
1,4-Dichlorobenzene ug/L 20.920 105 60-140
2,2-Dichloropropane ug/L 24.520 122 60-140
2-Chlorotoluene ug/L 23.120 115 60-140
4-Chlorotoluene ug/L 23.020 115 60-140
Benzene ug/L 22.720 113 60-140
Bromobenzene ug/L 21.020 105 60-140
Bromochloromethane ug/L 22.520 112 60-140
Bromodichloromethane ug/L 20.420 102 60-140
Bromoform ug/L 16.220 81 60-140
Bromomethane ug/L 24.920 124 60-140
Carbon tetrachloride ug/L 19.820 99 60-140
Chlorobenzene ug/L 21.820 109 60-140
Chloroethane ug/L 35.6 L12017860-140
Chloroform ug/L 24.820 124 60-140
Chloromethane ug/L 23.120 116 60-140
cis-1,2-Dichloroethene ug/L 24.420 122 60-140
cis-1,3-Dichloropropene ug/L 21.320 106 60-140
Dibromochloromethane ug/L 19.320 96 60-140
Dibromomethane ug/L 19.420 97 60-140
Dichlorodifluoromethane ug/L 26.2 IH2013160-140
Diisopropyl ether ug/L 22.820 114 60-140
Ethanol ug/L 764800 96 60-140
Ethyl-tert-butyl ether ug/L 44.340 111 60-140
Ethylbenzene ug/L 21.820 109 60-140
Hexachloro-1,3-butadiene ug/L 19.820 99 60-140
Isopropylbenzene (Cumene)ug/L 21.420 107 60-140
m&p-Xylene ug/L 43.040 108 60-140
Methyl-tert-butyl ether ug/L 21.120 105 60-140
Methylene Chloride ug/L 22.820 114 60-140
n-Butylbenzene ug/L 24.120 121 60-140
n-Propylbenzene ug/L 23.220 116 60-140
Naphthalene ug/L 21.120 106 60-140
o-Xylene ug/L 21.020 105 60-140
sec-Butylbenzene ug/L 22.620 113 60-140
Styrene ug/L 21.620 108 60-140
tert-Amyl Alcohol ug/L 328400 82 60-140
tert-Amylmethyl ether ug/L 41.240 103 60-140
tert-Butyl Alcohol ug/L 176200 88 60-140
tert-Butyl Formate ug/L 136160 85 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026084LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 17.920 89 60-140
Tetrachloroethene ug/L 19.020 95 60-140
Toluene ug/L 20.820 104 60-140
trans-1,2-Dichloroethene ug/L 25.620 128 60-140
trans-1,3-Dichloropropene ug/L 20.220 101 60-140
Trichloroethene ug/L 21.420 107 60-140
Trichlorofluoromethane ug/L 23.420 117 60-140
Vinyl chloride ug/L 19.520 97 60-140
1,2-Dichloroethane-d4 (S)%115 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667617004
4026086
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 140 60-140124 12 3020<0.31 28.0 24.9
1,1,1-Trichloroethane ug/L M12016360-140142 13 3020<0.33 32.6 28.5
1,1,2,2-Tetrachloroethane ug/L M12015060-140135 11 3020<0.22 30.1 27.0
1,1,2-Trichloroethane ug/L M12014460-140127 12 3020<0.32 28.8 25.4
1,1-Dichloroethane ug/L M12017960-140155 14 3020<0.37 35.8 31.0
1,1-Dichloroethene ug/L M12018160-140158 13 3020<0.35 36.1 31.6
1,1-Dichloropropene ug/L M12018860-140167 12 3020<0.43 37.6 33.4
1,2,3-Trichlorobenzene ug/L 20 114 60-140107 6 3020<0.81 22.8 21.5
1,2,3-Trichloropropane ug/L M12014360-140130 10 3020<0.26 28.6 25.9
1,2,4-Trichlorobenzene ug/L 20 119 60-140111 7 3020<0.64 23.9 22.2
1,2,4-Trimethylbenzene ug/L M12014560-140133 8 3020<0.50 28.9 26.7
1,2-Dibromo-3-
chloropropane ug/L 20 113 60-140106 7 3020<0.34 22.7 21.1
1,2-Dibromoethane (EDB)ug/L M12014560-140131 11 3020<0.27 29.0 26.1
1,2-Dichlorobenzene ug/L 20 137 60-140126 8 3020<0.34 27.3 25.2
1,2-Dichloroethane ug/L M12016560-140144 14 3020<0.32 33.0 28.7
1,2-Dichloropropane ug/L M12016360-140143 14 3020<0.36 32.7 28.5
1,3,5-Trimethylbenzene ug/L M12014860-140134 10 3020<0.33 29.6 26.8
1,3-Dichlorobenzene ug/L M12014160-140130 8 3020<0.34 28.2 25.9
1,3-Dichloropropane ug/L M12015060-140134 11 3020<0.28 30.1 26.9
1,4-Dichlorobenzene ug/L 20 135 60-140123 9 3020<0.33 26.9 24.5
2,2-Dichloropropane ug/L M12017560-140151 15 3020<0.39 35.1 30.3
2-Chlorotoluene ug/L M12015260-140141 7 3020<0.32 30.4 28.3
4-Chlorotoluene ug/L M12015360-140140 9 3020<0.32 30.6 28.0
Benzene ug/L M12015660-140137 13 3020<0.34 31.2 27.4
Bromobenzene ug/L 20 137 60-140126 8 3020<0.29 27.4 25.2
Bromochloromethane ug/L M12015460-140132 15 3020<0.47 30.8 26.4
Bromodichloromethane ug/L 20 139 60-140120 15 3020<0.31 27.8 24.0
Bromoform ug/L 20 107 60-14096 11 3020<0.34 21.5 19.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667617004
4026086
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M12016460-140145 13 3020<1.7 32.9 29.0
Carbon tetrachloride ug/L 20 138 60-140121 13 3020<0.33 27.6 24.2
Chlorobenzene ug/L M12014460-140132 9 3020<0.28 28.9 26.4
Chloroethane ug/L M02026160-140231 12 3020<0.65 52.1 46.3
Chloroform ug/L M12016460-140143 14 3020<0.43 32.9 28.5
Chloromethane ug/L M12019560-140177 10 3020<0.54 39.0 35.4
cis-1,2-Dichloroethene ug/L M12017160-140150 13 3020<0.38 34.1 30.0
cis-1,3-Dichloropropene ug/L 20 139 60-140123 13 3020<0.36 27.9 24.5
Dibromochloromethane ug/L 20 131 60-140115 13 3020<0.36 26.3 23.0
Dibromomethane ug/L 20 132 60-140114 15 3020<0.39 26.4 22.7
Dichlorodifluoromethane ug/L IH,M12026660-140238 11 3020<0.35 53.2 47.7
Diisopropyl ether ug/L M12015860-140138 13 3020<0.31 31.6 27.7
Ethanol ug/L 800 137 60-140126 8 30800<72.2 1100 1010
Ethyl-tert-butyl ether ug/L M14015660-140137 13 3040<3.2 62.3 54.8
Ethylbenzene ug/L M12014860-140134 10 3020<0.30 29.5 26.8
Hexachloro-1,3-butadiene ug/L 20 126 60-140116 9 3020<1.5 25.3 23.2
Isopropylbenzene
(Cumene)ug/L M12014460-140129 11 3020<0.33 28.8 25.8
m&p-Xylene ug/L M14014660-140130 11 3040<0.71 58.4 52.0
Methyl-tert-butyl ether ug/L M12014360-140128 11 3020<0.42 29.1 26.0
Methylene Chloride ug/L M12015160-140135 12 3020<2.0 30.3 27.0
n-Butylbenzene ug/L M12015760-140142 10 3020<0.49 31.5 28.5
n-Propylbenzene ug/L M12015660-140142 10 3020<0.34 31.2 28.3
Naphthalene ug/L 20 134 60-140126 6 3020<0.64 26.9 25.3
o-Xylene ug/L 20 140 60-140127 9 3020<0.34 28.0 25.5
sec-Butylbenzene ug/L M12014960-140135 10 3020<0.40 29.9 27.1
Styrene ug/L M12014460-140130 11 3020<0.29 28.9 25.9
tert-Amyl Alcohol ug/L 400 111 60-140101 9 30400<36.4 442 406
tert-Amylmethyl ether ug/L M14014160-140124 13 3040<9.2 56.5 49.7
tert-Butyl Alcohol ug/L M120016260-140156 3 30200<26.8 323 313
tert-Butyl Formate ug/L M11604160-14021 30160<29.4 65.1 33.6J
tert-Butylbenzene ug/L 20 122 60-140111 9 3020<0.32 24.4 22.3
Tetrachloroethene ug/L 20 131 60-140118 10 3020<0.29 26.2 23.7
Toluene ug/L M12014160-140125 12 3020<0.24 28.2 25.0
trans-1,2-Dichloroethene ug/L M12018160-140160 13 3020<0.40 36.3 32.0
trans-1,3-Dichloropropene ug/L 20 138 60-140119 15 3020<0.36 27.6 23.9
Trichloroethene ug/L M12014860-140132 12 3020<0.38 29.6 26.3
Trichlorofluoromethane ug/L M12017960-140155 14 3020<0.30 35.8 31.0
Vinyl chloride ug/L M12016460-140143 13 3020<0.39 32.8 28.7
1,2-Dichloroethane-d4 (S)%120 70-130118
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
776053
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667617003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026368
Associated Lab Samples:92667617003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.31 0.50 05/22/23 10:120.31
1,1,1-Trichloroethane ug/L <0.33 0.50 05/22/23 10:120.33
1,1,2,2-Tetrachloroethane ug/L <0.22 0.50 05/22/23 10:120.22
1,1,2-Trichloroethane ug/L <0.32 0.50 05/22/23 10:120.32
1,1-Dichloroethane ug/L <0.37 0.50 05/22/23 10:120.37
1,1-Dichloroethene ug/L <0.35 0.50 05/22/23 10:120.35
1,1-Dichloropropene ug/L <0.43 0.50 05/22/23 10:120.43
1,2,3-Trichlorobenzene ug/L <0.81 2.0 05/22/23 10:120.81
1,2,3-Trichloropropane ug/L <0.26 0.50 05/22/23 10:120.26
1,2,4-Trichlorobenzene ug/L <0.64 2.0 05/22/23 10:120.64
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/22/23 10:120.50
1,2-Dibromo-3-chloropropane ug/L <0.34 1.0 05/22/23 10:120.34
1,2-Dibromoethane (EDB)ug/L <0.27 0.50 05/22/23 10:120.27
1,2-Dichlorobenzene ug/L <0.34 0.50 05/22/23 10:120.34
1,2-Dichloroethane ug/L <0.32 0.50 05/22/23 10:120.32
1,2-Dichloropropane ug/L <0.36 0.50 05/22/23 10:120.36
1,3,5-Trimethylbenzene ug/L <0.33 0.50 05/22/23 10:120.33
1,3-Dichlorobenzene ug/L <0.34 0.50 05/22/23 10:120.34
1,3-Dichloropropane ug/L <0.28 0.50 05/22/23 10:120.28
1,4-Dichlorobenzene ug/L <0.33 0.50 05/22/23 10:120.33
2,2-Dichloropropane ug/L <0.39 0.50 05/22/23 10:120.39
2-Chlorotoluene ug/L <0.32 0.50 05/22/23 10:120.32
4-Chlorotoluene ug/L <0.32 0.50 05/22/23 10:120.32
Benzene ug/L <0.34 0.50 05/22/23 10:120.34
Bromobenzene ug/L <0.29 0.50 05/22/23 10:120.29
Bromochloromethane ug/L <0.47 0.50 05/22/23 10:120.47
Bromodichloromethane ug/L <0.31 0.50 05/22/23 10:120.31
Bromoform ug/L <0.34 0.50 05/22/23 10:120.34
Bromomethane ug/L <1.7 5.0 05/22/23 10:121.7
Carbon tetrachloride ug/L <0.33 0.50 05/22/23 10:120.33
Chlorobenzene ug/L <0.28 0.50 05/22/23 10:120.28
Chloroethane ug/L <0.65 1.0 05/22/23 10:120.65
Chloroform ug/L <0.43 0.50 05/22/23 10:120.43
Chloromethane ug/L <0.54 1.0 05/22/23 10:120.54
cis-1,2-Dichloroethene ug/L <0.38 0.50 05/22/23 10:120.38
cis-1,3-Dichloropropene ug/L <0.36 0.50 05/22/23 10:120.36
Dibromochloromethane ug/L <0.36 0.50 05/22/23 10:120.36
Dibromomethane ug/L <0.39 0.50 05/22/23 10:120.39
Dichlorodifluoromethane ug/L <0.35 0.50 05/22/23 10:120.35
Diisopropyl ether ug/L <0.31 0.50 05/22/23 10:120.31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4026368
Associated Lab Samples:92667617003
Matrix:Water
AnalyzedMDL
Ethanol ug/L <72.2 200 05/22/23 10:1272.2
Ethyl-tert-butyl ether ug/L <3.2 10.0 05/22/23 10:123.2
Ethylbenzene ug/L <0.30 0.50 05/22/23 10:120.30
Hexachloro-1,3-butadiene ug/L <1.5 2.0 05/22/23 10:121.5
Isopropylbenzene (Cumene)ug/L <0.33 0.50 05/22/23 10:120.33
m&p-Xylene ug/L <0.71 1.0 05/22/23 10:120.71
Methyl-tert-butyl ether ug/L <0.42 0.50 05/22/23 10:120.42
Methylene Chloride ug/L <2.0 2.0 05/22/23 10:122.0
n-Butylbenzene ug/L <0.49 0.50 05/22/23 10:120.49
n-Propylbenzene ug/L <0.34 0.50 05/22/23 10:120.34
Naphthalene ug/L <0.64 2.0 05/22/23 10:120.64
o-Xylene ug/L <0.34 0.50 05/22/23 10:120.34
sec-Butylbenzene ug/L <0.40 0.50 05/22/23 10:120.40
Styrene ug/L <0.29 0.50 05/22/23 10:120.29
tert-Amyl Alcohol ug/L <36.4 100 05/22/23 10:1236.4
tert-Amylmethyl ether ug/L <9.2 10.0 05/22/23 10:129.2
tert-Butyl Alcohol ug/L <26.8 50.0 05/22/23 10:1226.8
tert-Butyl Formate ug/L <29.4 50.0 05/22/23 10:1229.4
tert-Butylbenzene ug/L <0.32 0.50 05/22/23 10:120.32
Tetrachloroethene ug/L <0.29 0.50 05/22/23 10:120.29
Toluene ug/L <0.24 0.50 05/22/23 10:120.24
trans-1,2-Dichloroethene ug/L <0.40 0.50 05/22/23 10:120.40
trans-1,3-Dichloropropene ug/L <0.36 0.50 05/22/23 10:120.36
Trichloroethene ug/L <0.38 0.50 05/22/23 10:120.38
Trichlorofluoromethane ug/L <0.30 1.0 05/22/23 10:120.30
Vinyl chloride ug/L <0.39 1.0 05/22/23 10:120.39
1,2-Dichloroethane-d4 (S)%92 70-130 05/22/23 10:12
4-Bromofluorobenzene (S)%102 70-130 05/22/23 10:12
Toluene-d8 (S)%99 70-130 05/22/23 10:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026369LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.420 97 60-140
1,1,1-Trichloroethane ug/L 19.620 98 60-140
1,1,2,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,2-Trichloroethane ug/L 18.420 92 60-140
1,1-Dichloroethane ug/L 19.420 97 60-140
1,1-Dichloroethene ug/L 21.520 108 60-140
1,1-Dichloropropene ug/L 21.520 107 60-140
1,2,3-Trichlorobenzene ug/L 21.320 106 60-140
1,2,3-Trichloropropane ug/L 19.520 98 60-140
1,2,4-Trichlorobenzene ug/L 22.620 113 60-140
1,2,4-Trimethylbenzene ug/L 20.720 104 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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Huntersville, NC 28078
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026369LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 19.420 97 60-140
1,2-Dibromoethane (EDB)ug/L 19.720 98 60-140
1,2-Dichlorobenzene ug/L 21.120 105 60-140
1,2-Dichloroethane ug/L 19.020 95 60-140
1,2-Dichloropropane ug/L 20.420 102 60-140
1,3,5-Trimethylbenzene ug/L 21.020 105 60-140
1,3-Dichlorobenzene ug/L 21.220 106 60-140
1,3-Dichloropropane ug/L 20.620 103 60-140
1,4-Dichlorobenzene ug/L 20.120 100 60-140
2,2-Dichloropropane ug/L 18.920 95 60-140
2-Chlorotoluene ug/L 21.120 105 60-140
4-Chlorotoluene ug/L 20.320 102 60-140
Benzene ug/L 20.420 102 60-140
Bromobenzene ug/L 20.120 101 60-140
Bromochloromethane ug/L 20.520 102 60-140
Bromodichloromethane ug/L 17.920 89 60-140
Bromoform ug/L 19.320 97 60-140
Bromomethane ug/L 12.020 60 60-140
Carbon tetrachloride ug/L 19.920 99 60-140
Chlorobenzene ug/L 20.720 103 60-140
Chloroethane ug/L 19.020 95 60-140
Chloroform ug/L 17.720 89 60-140
Chloromethane ug/L 21.220 106 60-140
cis-1,2-Dichloroethene ug/L 19.620 98 60-140
cis-1,3-Dichloropropene ug/L 20.020 100 60-140
Dibromochloromethane ug/L 17.920 89 60-140
Dibromomethane ug/L 18.520 92 60-140
Dichlorodifluoromethane ug/L 25.020 125 60-140
Diisopropyl ether ug/L 19.220 96 60-140
Ethanol ug/L 819800 102 60-140
Ethyl-tert-butyl ether ug/L 36.540 91 60-140
Ethylbenzene ug/L 20.820 104 60-140
Hexachloro-1,3-butadiene ug/L 22.720 113 60-140
Isopropylbenzene (Cumene)ug/L 21.220 106 60-140
m&p-Xylene ug/L 42.140 105 60-140
Methyl-tert-butyl ether ug/L 17.920 89 60-140
Methylene Chloride ug/L 20.720 104 60-140
n-Butylbenzene ug/L 22.720 113 60-140
n-Propylbenzene ug/L 21.520 107 60-140
Naphthalene ug/L 21.920 110 60-140
o-Xylene ug/L 20.320 101 60-140
sec-Butylbenzene ug/L 21.520 108 60-140
Styrene ug/L 20.420 102 60-140
tert-Amyl Alcohol ug/L 364400 91 60-140
tert-Amylmethyl ether ug/L 37.740 94 60-140
tert-Butyl Alcohol ug/L 171200 86 60-140
tert-Butyl Formate ug/L 146160 91 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4026369LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 17.720 88 60-140
Tetrachloroethene ug/L 20.420 102 60-140
Toluene ug/L 19.220 96 60-140
trans-1,2-Dichloroethene ug/L 20.120 100 60-140
trans-1,3-Dichloropropene ug/L 18.720 93 60-140
Trichloroethene ug/L 20.020 100 60-140
Trichlorofluoromethane ug/L 18.820 94 60-140
Vinyl chloride ug/L 17.020 85 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432001
4026371
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 87 60-140101 16 3020ND17.3 20.2
1,1,1-Trichloroethane ug/L 20 92 60-140102 11 3020ND18.4 20.4
1,1,2,2-Tetrachloroethane ug/L 20 86 60-140100 14 3020ND17.3 19.9
1,1,2-Trichloroethane ug/L 20 84 60-14096 13 3020ND16.9 19.2
1,1-Dichloroethane ug/L 20 95 60-140108 12 3020ND19.1 21.5
1,1-Dichloroethene ug/L 20 108 60-140118 9 3020ND21.5 23.5
1,1-Dichloropropene ug/L 20 103 60-140114 10 3020ND20.6 22.8
1,2,3-Trichlorobenzene ug/L 20 91 60-140115 24 3020ND18.1 23.0
1,2,3-Trichloropropane ug/L 20 87 60-14094 8 3020ND17.4 18.9
1,2,4-Trichlorobenzene ug/L 20 91 60-140115 23 3020ND18.2 22.9
1,2,4-Trimethylbenzene ug/L 20 93 60-140109 15 3020ND18.6 21.7
1,2-Dibromo-3-
chloropropane ug/L 20 80 60-14092 14 3020ND16.1 18.5
1,2-Dibromoethane (EDB)ug/L 20 90 60-140100 11 3020ND18.0 20.1
1,2-Dichlorobenzene ug/L 20 94 60-140111 17 3020ND18.8 22.2
1,2-Dichloroethane ug/L 20 89 60-140103 14 3020ND17.9 20.6
1,2-Dichloropropane ug/L 20 93 60-140109 16 3020ND18.6 21.7
1,3,5-Trimethylbenzene ug/L 20 95 60-140111 15 3020ND19.1 22.2
1,3-Dichlorobenzene ug/L 20 95 60-140112 16 3020ND19.1 22.5
1,3-Dichloropropane ug/L 20 93 60-140104 12 3020ND18.5 20.8
1,4-Dichlorobenzene ug/L 20 90 60-140105 16 3020ND18.0 21.0
2,2-Dichloropropane ug/L 20 90 60-140100 10 3020ND18.1 20.0
2-Chlorotoluene ug/L 20 96 60-140110 13 3020ND19.3 21.9
4-Chlorotoluene ug/L 20 93 60-140106 13 3020ND18.6 21.2
Benzene ug/L 20 95 60-140107 12 3020ND19.0 21.5
Bromobenzene ug/L 20 90 60-140102 12 3020ND18.0 20.3
Bromochloromethane ug/L 20 96 60-140108 12 3020ND19.2 21.6
Bromodichloromethane ug/L 20 80 60-14090 12 3020ND16.0 18.0
Bromoform ug/L 20 85 60-14097 13 3020ND17.0 19.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4026370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667432001
4026371
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M1205160-14067 28 3020ND10.1 13.5
Carbon tetrachloride ug/L 20 88 60-140100 13 3020ND17.5 20.0
Chlorobenzene ug/L 20 96 60-140105 9 3020ND19.2 21.0
Chloroethane ug/L 20 102 60-140114 11 3020ND20.4 22.8
Chloroform ug/L 20 86 60-14095 9 3020ND17.2 18.9
Chloromethane ug/L 20 102 60-140112 10 3020ND20.4 22.5
cis-1,2-Dichloroethene ug/L 20 93 60-140106 13 3020ND18.5 21.2
cis-1,3-Dichloropropene ug/L 20 87 60-14098 12 3020ND17.4 19.6
Dibromochloromethane ug/L 20 79 60-14091 14 3020ND15.9 18.2
Dibromomethane ug/L 20 84 60-14093 10 3020ND16.9 18.6
Dichlorodifluoromethane ug/L 20 127 60-140132 4 3020ND25.3 26.5
Diisopropyl ether ug/L 20 90 60-140104 14 30201.1 19.2 22.0
Ethanol ug/L 800 102 60-140106 3 30800ND817845
Ethyl-tert-butyl ether ug/L 40 84 60-14098 15 3040ND33.7 39.3
Ethylbenzene ug/L 20 96 60-140106 9 3020ND19.3 21.2
Hexachloro-1,3-butadiene ug/L 20 109 60-140125 13 3020ND21.8 24.9
Isopropylbenzene
(Cumene)ug/L 20 99 60-140111 11 3020ND19.9 22.2
m&p-Xylene ug/L 40 98 60-140109 10 3040ND39.2 43.5
Methyl-tert-butyl ether ug/L 20 88 60-140107 11 302014.3 32.0 35.6
Methylene Chloride ug/L 20 100 60-140113 12 3020ND20.0 22.6
n-Butylbenzene ug/L 20 103 60-140122 16 3020ND20.7 24.4
n-Propylbenzene ug/L 20 98 60-140112 13 3020ND19.7 22.4
Naphthalene ug/L 20 90 60-140112 22 3020ND18.0 22.3
o-Xylene ug/L 20 96 60-140104 9 3020ND19.2 20.9
sec-Butylbenzene ug/L 20 101 60-140118 16 3020ND20.1 23.7
Styrene ug/L 20 94 60-140102 9 3020ND18.7 20.4
tert-Amyl Alcohol ug/L 400 87 60-14092 5 30400120467489
tert-Amylmethyl ether ug/L 40 86 60-14099 13 3040ND36.6 41.7
tert-Butyl Alcohol ug/L 200 112 60-140130 12 3020052.5 276 312
tert-Butyl Formate ug/L M11602760-14024 30160ND43.4J 38.5J
tert-Butylbenzene ug/L 20 83 60-14094 13 3020ND16.6 18.9
Tetrachloroethene ug/L 20 93 60-140102 10 3020ND18.5 20.4
Toluene ug/L 20 91 60-140101 11 3020ND18.2 20.3
trans-1,2-Dichloroethene ug/L 20 94 60-140110 15 3020ND18.8 22.0
trans-1,3-Dichloropropene ug/L 20 82 60-14094 14 3020ND16.3 18.8
Trichloroethene ug/L 20 99 60-140104 5 3020ND19.7 20.7
Trichlorofluoromethane ug/L 20 93 60-140103 10 3020ND18.6 20.5
Vinyl chloride ug/L 20 86 60-14094 9 3020ND17.2 18.8
1,2-Dichloroethane-d4 (S)%97 70-130101
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667617
SCARLETT'S 66
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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Huntersville, NC 28078
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667617
SCARLETT'S 66
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667617001 775917MW-1 SM 6200B
92667617002 775917MW-3 SM 6200B
92667617003 776053MW-4 SM 6200B
92667617004 775917MW-5 SM 6200B
92667617005 775917AS-1 SM 6200B
92667617006 775917FB-01 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/23/2023 11:27 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 28 of 31
Page 29 of 31
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Page 31 of 31