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HomeMy WebLinkAboutWS-6694_30208_CA_LAB_20210212  Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   2/16/2021 Withers & Ravenel Laura Elliot 115 Mackenan Dr. BUILDING 117 Cary, NC, 27511 Ref: Analytical Testing Lab Report Number: 21-044-0002 Client Project Description: Liberty Handy Mart 02171219.07 Dear Laura Elliot: Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/12/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Angela D Overcash Senior Project Manager Page 1 of 24 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202137735State ProgramNorth Carolina 12/31/2021402State ProgramNorth Carolina 07/31/202199012State ProgramSouth Carolina 12/31/202099012State ProgramSouth Carolina Page 1 of 1 00016/21-044-0002 Page 2 of 24 Report Number: Sample Summary Table Client Project Description: 21-044-0002 Liberty Handy Mart 02171219.07 Lab No Client Sample ID Matrix Date Collected Date Received 02/12/2021 10:15Aqueous 92662 WSW-1 02/12/2021 12:45 02/12/2021 10:30Aqueous 92663 WSW-2 02/12/2021 12:45 02/12/2021 10:20Aqueous 92664 Field Blank 02/12/2021 12:45 Page 3 of 24 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 21-044-0002 Report Limit Project:Liberty Handy Mart V 92663WSW-2 0.612 02/15/2021 17:296200B1,1-Dichloroethene µg/L 0.500 1.67 02/15/2021 17:296200BTrichloroetheneµg/L 0.500 Page 4 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-1 92662 Matrix: 2/12/2021 10:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Benzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Bromochloromethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Bromoform 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.00Bromomethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500tert-Butyl benzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Chloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Chloroform 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Chloromethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 02/15/21 17:05 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 02/15/21 17:05 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 5 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-1 92662 Matrix: 2/12/2021 10:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.00Dichlorodifluoromethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 02/15/21 17:05 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 02/15/21 17:05 6200BJLB <200 µg/L 200Ethanol 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 02/15/21 17:05 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.002-Hexanone 1 02/15/21 17:05 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 02/15/21 17:05 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 02/15/21 17:05 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 6 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-1 92662 Matrix: 2/12/2021 10:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.00Naphthalene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Styrene 1 02/15/21 17:05 6200BJLB <10.0 µg/L 10.0tert-Amyl alcohol (TAA)1 02/15/21 17:05 6200BJLB <10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 02/15/21 17:05 6200BJLB <10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 02/15/21 17:05 6200BJLB <10.0 µg/L 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/15/21 17:05 6200BJLB <10.0 µg/L 10.0tert-Butyl formate (TBF)1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Toluene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 02/15/21 17:05 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 02/15/21 17:05 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 7 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-1 92662 Matrix: 2/12/2021 10:15 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Vinyl Chloride 1 02/15/21 17:05 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500o-Xylene 1 02/15/21 17:05 6200BJLB <0.500 µg/L 0.500Xylene (Total)1 02/15/21 17:05 6200B Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%02/15/21 17:051 JLB V582 Surrogate: Dibromofluoromethane 106 Limits: 70-130%02/15/21 17:051 JLB V582 Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%02/15/21 17:051 JLB V582 Surrogate: Toluene-d8 95.2 Limits: 70-130%02/15/21 17:051 JLB V582 Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 8 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-2 92663 Matrix: 2/12/2021 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Benzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Bromochloromethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Bromoform 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.00Bromomethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500tert-Butyl benzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Chloroethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Chloroform 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Chloromethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 02/15/21 17:29 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 02/15/21 17:29 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 9 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-2 92663 Matrix: 2/12/2021 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.00Dichlorodifluoromethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 02/15/21 17:29 6200BJLB 0.612 µg/L 0.5001,1-Dichloroethene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 02/15/21 17:29 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 02/15/21 17:29 6200BJLB <200 µg/L 200Ethanol 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 02/15/21 17:29 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.002-Hexanone 1 02/15/21 17:29 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 02/15/21 17:29 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 02/15/21 17:29 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 10 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-2 92663 Matrix: 2/12/2021 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.00Naphthalene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Styrene 1 02/15/21 17:29 6200BJLB <10.0 µg/L 10.0tert-Amyl alcohol (TAA)1 02/15/21 17:29 6200BJLB <10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 02/15/21 17:29 6200BJLB <10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 02/15/21 17:29 6200BJLB <10.0 µg/L 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/15/21 17:29 6200BJLB <10.0 µg/L 10.0tert-Butyl formate (TBF)1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Toluene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 02/15/21 17:29 6200BJLB 1.67 µg/L 0.500Trichloroethene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 02/15/21 17:29 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 02/15/21 17:29 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 11 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:WSW-2 92663 Matrix: 2/12/2021 10:30 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Vinyl Chloride 1 02/15/21 17:29 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500o-Xylene 1 02/15/21 17:29 6200BJLB <0.500 µg/L 0.500Xylene (Total)1 02/15/21 17:29 6200B Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%02/15/21 17:291 JLB V582 Surrogate: Dibromofluoromethane 106 Limits: 70-130%02/15/21 17:291 JLB V582 Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%02/15/21 17:291 JLB V582 Surrogate: Toluene-d8 96.6 Limits: 70-130%02/15/21 17:291 JLB V582 Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 12 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:Field Blank 92664 Matrix: 2/12/2021 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0Acetone 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Benzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Bromobenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Bromochloromethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Bromodichloromethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Bromoform 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.00Bromomethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500n-Butylbenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500sec-Butyl benzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500tert-Butyl benzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Carbon Tetrachloride 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Chlorobenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Chlorodibromomethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Chloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Chloroform 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Chloromethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5002-Chlorotoluene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5004-Chlorotoluene 1 02/15/21 16:41 6200BJLB <2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2-Dibromoethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Dibromomethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2-Dichlorobenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,3-Dichlorobenzene 1 02/15/21 16:41 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 13 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:Field Blank 92664 Matrix: 2/12/2021 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.5001,4-Dichlorobenzene 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.00Dichlorodifluoromethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2-Dichloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1-Dichloroethene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500cis-1,2-Dichloroethene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500trans-1,2-Dichloroethene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2-Dichloropropane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,3-Dichloropropane 1 02/15/21 16:41 6200BJLB <2.00 µg/L 2.002,2-Dichloropropane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1-Dichloropropene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500cis-1,3-Dichloropropene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500trans-1,3-Dichloropropene 1 02/15/21 16:41 6200BJLB <200 µg/L 200Ethanol 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Ethylbenzene 1 02/15/21 16:41 6200BJLB <3.00 µg/L 3.00Hexachlorobutadiene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Isopropylbenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5004-Isopropyl toluene 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.002-Hexanone 1 02/15/21 16:41 6200BJLB <5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 02/15/21 16:41 6200BJLB <2.00 µg/L 2.00Methylene Chloride 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 02/15/21 16:41 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 14 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:Field Blank 92664 Matrix: 2/12/2021 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.004-Methyl-2-Pentanone 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.00Naphthalene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500n-Propylbenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Styrene 1 02/15/21 16:41 6200BJLB <10.0 µg/L 10.0tert-Amyl alcohol (TAA)1 02/15/21 16:41 6200BJLB <10.0 µg/L 10.0tert-Amyl Methyl Ether (TAME)1 02/15/21 16:41 6200BJLB <10.0 µg/L 10.0tert-Butyl Alcohol (TBA)1 02/15/21 16:41 6200BJLB <10.0 µg/L 10.0Ethyl Tertiary Butyl Ether (ETBE)1 02/15/21 16:41 6200BJLB <10.0 µg/L 10.0tert-Butyl formate (TBF)1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Tetrachloroethene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Toluene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1,1-Trichloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,1,2-Trichloroethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Trichloroethene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Trichlorofluoromethane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2,3-Trichloropropane 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 02/15/21 16:41 6200BJLB <5.00 µg/L 5.00Vinyl Acetate 1 02/15/21 16:41 6200BJLB Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 15 of 24 , REPORT OF ANALYSISReport Number : Project Information : NC 27511 21-044-0002 01221 Withers & Ravenel 115 Mackenan Dr. BUILDING 117 Laura Elliot Cary 02171219.07 Received : 02/12/2021 Liberty Handy Mart Report Date : 02/16/2021 Sample ID : Lab No : Sampled:Field Blank 92664 Matrix: 2/12/2021 10:20 Aqueous Test Results Units MQL By Analytical Method Date / Time Analyzed DF <0.500 µg/L 0.500Vinyl Chloride 1 02/15/21 16:41 6200BJLB <1.00 µg/L 1.00m,p-Xylene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500o-Xylene 1 02/15/21 16:41 6200BJLB <0.500 µg/L 0.500Xylene (Total)1 02/15/21 16:41 6200B Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%02/15/21 16:411 JLB V582 Surrogate: Dibromofluoromethane 105 Limits: 70-130%02/15/21 16:411 JLB V582 Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%02/15/21 16:411 JLB V582 Surrogate: Toluene-d8 96.0 Limits: 70-130%02/15/21 16:411 JLB V582 Qualifiers/ Definitions Limit ExceededLDilution FactorDF Method Quantitation LimitMQL Page 16 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 Associated Lab Samples: 92662, 92663, 92664 LRB-V581 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 02/15/21 12:4310.0< 10.0µg/LAcetone 02/15/21 12:430.500< 0.500µg/LBenzene 02/15/21 12:430.500< 0.500µg/LBromobenzene 02/15/21 12:430.500< 0.500µg/LBromochloromethane 02/15/21 12:430.500< 0.500µg/LBromodichloromethane 02/15/21 12:430.500< 0.500µg/LBromoform 02/15/21 12:431.00< 1.00µg/LBromomethane 02/15/21 12:430.500< 0.500µg/Ln-Butylbenzene 02/15/21 12:430.500< 0.500µg/Lsec-Butyl benzene 02/15/21 12:430.500< 0.500µg/Ltert-Butyl benzene 02/15/21 12:430.500< 0.500µg/LCarbon Tetrachloride 02/15/21 12:430.500< 0.500µg/LChlorobenzene 02/15/21 12:430.500< 0.500µg/LChlorodibromomethane 02/15/21 12:430.500< 0.500µg/LChloroethane 02/15/21 12:430.500< 0.500µg/LChloroform 02/15/21 12:430.500< 0.500µg/LChloromethane 02/15/21 12:430.500< 0.500µg/L2-Chlorotoluene 02/15/21 12:430.500< 0.500µg/L4-Chlorotoluene 02/15/21 12:432.00< 2.00µg/L1,2-Dibromo-3-Chloropropane 02/15/21 12:430.500< 0.500µg/L1,2-Dibromoethane 02/15/21 12:430.500< 0.500µg/LDibromomethane 02/15/21 12:430.500< 0.500µg/L1,2-Dichlorobenzene 02/15/21 12:430.500< 0.500µg/L1,3-Dichlorobenzene 02/15/21 12:430.500< 0.500µg/L1,4-Dichlorobenzene 02/15/21 12:431.00< 1.00µg/LDichlorodifluoromethane 02/15/21 12:430.500< 0.500µg/L1,1-Dichloroethane 02/15/21 12:430.500< 0.500µg/L1,2-Dichloroethane Page 1 of 6Date:02/16/2021 01:38 PM Page 17 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 Associated Lab Samples: 92662, 92663, 92664 LRB-V581 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 02/15/21 12:430.500< 0.500µg/L1,1-Dichloroethene 02/15/21 12:430.500< 0.500µg/Lcis-1,2-Dichloroethene 02/15/21 12:430.500< 0.500µg/Ltrans-1,2-Dichloroethene 02/15/21 12:430.500< 0.500µg/L1,2-Dichloropropane 02/15/21 12:430.500< 0.500µg/L1,3-Dichloropropane 02/15/21 12:432.00< 2.00µg/L2,2-Dichloropropane 02/15/21 12:430.500< 0.500µg/L1,1-Dichloropropene 02/15/21 12:430.500< 0.500µg/Lcis-1,3-Dichloropropene 02/15/21 12:430.500< 0.500µg/Ltrans-1,3-Dichloropropene 02/15/21 12:43200< 200µg/LEthanol 02/15/21 12:430.500< 0.500µg/LEthylbenzene 02/15/21 12:433.00< 3.00µg/LHexachlorobutadiene 02/15/21 12:430.500< 0.500µg/LDi-Isopropyl Ether (DIPE) 02/15/21 12:430.500< 0.500µg/LIsopropylbenzene 02/15/21 12:430.500< 0.500µg/L4-Isopropyl toluene 02/15/21 12:431.00< 1.00µg/L2-Hexanone 02/15/21 12:435.00< 5.00µg/LMethyl Ethyl Ketone (MEK) 02/15/21 12:432.00< 2.00µg/LMethylene Chloride 02/15/21 12:431.00< 1.00µg/LMethyl tert-butyl ether (MTBE) 02/15/21 12:431.00< 1.00µg/L4-Methyl-2-Pentanone 02/15/21 12:431.00< 1.00µg/LNaphthalene 02/15/21 12:430.500< 0.500µg/Ln-Propylbenzene 02/15/21 12:430.500< 0.500µg/LStyrene 02/15/21 12:4310.0< 10.0µg/Ltert-Amyl alcohol (TAA) 02/15/21 12:4310.0< 10.0µg/Ltert-Amyl Methyl Ether (TAME) 02/15/21 12:4310.0< 10.0µg/Ltert-Butyl Alcohol (TBA) 02/15/21 12:4310.0< 10.0µg/LEthyl Tertiary Butyl Ether (ETBE) Page 2 of 6Date:02/16/2021 01:38 PM Page 18 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 Associated Lab Samples: 92662, 92663, 92664 LRB-V581 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLBlank ResultUnits % Recovery % Rec Limits 02/15/21 12:4310.0< 10.0µg/Ltert-Butyl formate (TBF) 02/15/21 12:430.500< 0.500µg/L1,1,1,2-Tetrachloroethane 02/15/21 12:430.500< 0.500µg/L1,1,2,2-Tetrachloroethane 02/15/21 12:430.500< 0.500µg/LTetrachloroethene 02/15/21 12:430.500< 0.500µg/LToluene 02/15/21 12:430.500< 0.500µg/L1,2,3-Trichlorobenzene 02/15/21 12:430.500< 0.500µg/L1,2,4-Trichlorobenzene 02/15/21 12:430.500< 0.500µg/L1,1,1-Trichloroethane 02/15/21 12:430.500< 0.500µg/L1,1,2-Trichloroethane 02/15/21 12:430.500< 0.500µg/LTrichloroethene 02/15/21 12:430.500< 0.500µg/LTrichlorofluoromethane 02/15/21 12:430.500< 0.500µg/L1,2,3-Trichloropropane 02/15/21 12:430.500< 0.500µg/L1,2,4-Trimethylbenzene 02/15/21 12:430.500< 0.500µg/L1,3,5-Trimethylbenzene 02/15/21 12:435.00< 5.00µg/LVinyl Acetate 02/15/21 12:430.500< 0.500µg/LVinyl Chloride 02/15/21 12:431.00< 1.00µg/Lm,p-Xylene 02/15/21 12:430.500< 0.500µg/Lo-Xylene 02/15/21 12:434-Bromofluorobenzene (S)97.8 70-130 02/15/21 12:43Dibromofluoromethane (S)106 70-130 02/15/21 12:431,2-Dichloroethane - d4 (S)102 70-130 02/15/21 12:43Toluene-d8 (S)96.4 70-130 Page 3 of 6Date:02/16/2021 01:38 PM Page 19 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 LCS-V581 LCSD-V581Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 41.5 10410240.940.0µg/LAcetone 40-160 1.4 20.0 20.8 10410721.320.0µg/LBenzene 70-130 2.3 20.0 19.6 98.095.519.120.0µg/LBromobenzene 70-130 2.5 20.0 21.8 10910721.320.0µg/LBromochloromethane 70-130 2.3 20.0 22.0 11011122.220.0µg/LBromodichloromethane 70-130 0.9 20.0 22.3 11210621.220.0µg/LBromoform 70-130 5.0 20.0 19.9 99.597.519.520.0µg/LBromomethane 60-140 2.0 20.0 19.5 97.510020.020.0µg/Ln-Butylbenzene 70-130 2.5 20.0 19.7 98.510320.520.0µg/Lsec-Butyl benzene 70-130 3.9 20.0 19.5 97.510120.220.0µg/Ltert-Butyl benzene 70-130 3.5 20.0 21.9 11011222.420.0µg/LCarbon Tetrachloride 70-130 2.2 20.0 20.3 10210220.420.0µg/LChlorobenzene 70-130 0.4 20.0 20.3 10210120.220.0µg/LChlorodibromomethane 70-130 0.4 20.0 23.2 11611923.720.0µg/LChloroethane 60-140 2.1 20.0 21.5 10810921.820.0µg/LChloroform 70-130 1.3 20.0 20.2 10110521.020.0µg/LChloromethane 60-140 3.8 20.0 19.1 95.596.519.320.0µg/L2-Chlorotoluene 70-130 1.0 20.0 19.0 95.010120.120.0µg/L4-Chlorotoluene 70-130 5.6 20.0 19.6 98.099.019.820.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.0 20.0 20.2 10110320.520.0µg/L1,2-Dibromoethane 70-130 1.4 20.0 22.0 11011122.120.0µg/LDibromomethane 70-130 0.4 20.0 20.1 10110120.120.0µg/L1,2-Dichlorobenzene 70-130 0.0 20.0 19.6 98.010220.420.0µg/L1,3-Dichlorobenzene 70-130 4.0 20.0 20.1 10110520.920.0µg/L1,4-Dichlorobenzene 70-130 3.9 20.0 25.6 12813026.020.0µg/LDichlorodifluoromethane 60-140 1.5 20.0 20.6 10310721.420.0µg/L1,1-Dichloroethane 70-130 3.8 20.0 Page 4 of 6Date:02/16/2021 01:38 PM Page 20 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 LCS-V581 LCSD-V581Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 23.1 11611422.720.0µg/L1,2-Dichloroethane 70-130 1.7 20.0 20.9 10511021.920.0µg/L1,1-Dichloroethene 70-130 4.6 20.0 20.9 10510721.320.0µg/Lcis-1,2-Dichloroethene 70-130 1.8 20.0 21.2 10611021.920.0µg/Ltrans-1,2-Dichloroethene 70-130 3.2 20.0 20.3 10210521.020.0µg/L1,2-Dichloropropane 70-130 3.3 20.0 20.0 10098.019.620.0µg/L1,3-Dichloropropane 70-130 2.0 20.0 21.2 10610821.520.0µg/L2,2-Dichloropropane 70-130 1.4 20.0 21.0 10510921.820.0µg/L1,1-Dichloropropene 70-130 3.7 20.0 21.3 10710721.420.0µg/Lcis-1,3-Dichloropropene 70-130 0.4 20.0 21.7 10911122.120.0µg/Ltrans-1,3-Dichloropropene 70-130 1.8 20.0 491 98.298.2491500µg/LEthanol 60-140 0.0 20.0 19.5 97.598.519.720.0µg/LEthylbenzene 70-130 1.0 20.0 20.5 10310721.320.0µg/LHexachlorobutadiene 70-130 3.8 20.0 20.5 10310420.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.4 20.0 19.7 98.510020.020.0µg/LIsopropylbenzene 70-130 1.5 20.0 19.5 97.510220.420.0µg/L4-Isopropyl toluene 70-130 4.5 20.0 17.8 89.085.517.120.0µg/L2-Hexanone 60-140 4.0 20.0 21.8 10911022.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.9 20.0 20.4 10210320.620.0µg/LMethylene Chloride 70-130 0.9 20.0 22.1 11111122.120.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0 19.4 97.095.019.020.0µg/L4-Methyl-2-Pentanone 60-140 2.0 20.0 17.5 87.584.516.920.0µg/LNaphthalene 70-130 3.4 20.0 19.0 95.096.019.220.0µg/Ln-Propylbenzene 70-130 1.0 20.0 19.9 99.599.519.920.0µg/LStyrene 70-130 0.0 20.0 21.3 10710721.320.0µg/Ltert-Amyl alcohol (TAA)70-130 0.0 20.0 44.6 11211144.340.0µg/Ltert-Amyl Methyl Ether (TAME)70-130 0.6 20.0 Page 5 of 6Date:02/16/2021 01:38 PM Page 21 of 24 Quality Control Data 21-044-0002Report No: Project Description: Client ID:Withers & Ravenel Liberty Handy Mart QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V582QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V581 LCS-V581 LCSD-V581Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 35.5 88.787.735.140.0µg/Ltert-Butyl Alcohol (TBA)70-130 1.1 20.0 44.9 11211445.440.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.1 20.0 45.8 11511545.840.0µg/Ltert-Butyl formate (TBF)70-130 0.0 20.0 20.1 10110320.520.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.9 20.0 19.4 97.094.018.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 3.1 20.0 20.0 10010320.520.0µg/LTetrachloroethene 70-130 2.4 20.0 21.0 10510821.520.0µg/LToluene 70-130 2.3 20.0 20.5 10310220.320.0µg/L1,2,3-Trichlorobenzene 70-130 0.9 20.0 19.5 97.510120.220.0µg/L1,2,4-Trichlorobenzene 70-130 3.5 20.0 22.0 11011222.420.0µg/L1,1,1-Trichloroethane 70-130 1.8 20.0 21.3 10710821.520.0µg/L1,1,2-Trichloroethane 70-130 0.9 20.0 21.4 10711122.120.0µg/LTrichloroethene 70-130 3.2 20.0 25.3 12713126.220.0µg/LTrichlorofluoromethane 60-140 3.4 20.0 20.3 10210420.720.0µg/L1,2,3-Trichloropropane 70-130 1.9 20.0 19.8 99.010220.420.0µg/L1,2,4-Trimethylbenzene 70-130 2.9 20.0 19.2 96.099.519.920.0µg/L1,3,5-Trimethylbenzene 70-130 3.5 20.0 20.1 10199.019.820.0µg/LVinyl Acetate 60-140 1.5 20.0 21.0 10510821.620.0µg/LVinyl Chloride 60-140 2.8 20.0 41.4 10410542.140.0µg/Lm,p-Xylene 70-130 1.6 20.0 19.9 99.599.519.920.0µg/Lo-Xylene 70-130 0.0 20.0 94.493.04-Bromofluorobenzene (S)70-130 104103Dibromofluoromethane (S)70-130 1051061,2-Dichloroethane - d4 (S)70-130 97.495.6Toluene-d8 (S)70-130 Page 6 of 6Date:02/16/2021 01:38 PM Page 22 of 24 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:21-044-0002 Withers & Ravenel 01221 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT-15 4.5C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 No TB received like COC says Signature:Talon J Yelton Date & Time:02/13/2021 07:44:28 Special precautions or instructions included? Comments: Page 23 of 24 Page 24 of 24