WS-6093_22446_CA_LAB_20130208

#=CL#
February 08, 2013
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 92146489
92146489
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR - UST Section
1637 Mail Service Center
Raleigh, NC 276991637
Moody's Grocery #22446
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on January 31, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin for
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Lab ID Sample ID Matrix Date Collected Date Received
92146489001 WSW-1 Water 01/28/13 16:00 01/31/13 12:10
92146489002 WSW-3 Water 01/28/13 16:30 01/31/13 12:10
92146489003 WSW-4 Water 01/28/13 17:10 01/31/13 12:10
92146489004 WSW-5 Water 01/28/13 17:40 01/31/13 12:10
92146489005 WSW-6 Water 01/28/13 16:50 01/31/13 12:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92146489001 WSW-1 SM 6200B 64 PASI-CMCK
92146489002 WSW-3 SM 6200B 64 PASI-CMCK
92146489003 WSW-4 SM 6200B 64 PASI-CMCK
92146489004 WSW-5 SM 6200B 64 PASI-CMCK
92146489005 WSW-6 SM 6200B 64 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=HO#
HITS ONLY
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92146489004 WSW-5
1,2-Dichloroethane 0.32J ug/L 02/07/13 01:020.50SM 6200B
92146489005 WSW-6
1,2-Dichloroethane 1.4 ug/L 02/07/13 01:170.50SM 6200B
Diisopropyl ether 7.2 ug/L 02/07/13 01:170.50SM 6200B
Ethylbenzene 0.60 ug/L 02/07/13 01:170.50SM 6200B
Isopropylbenzene (Cumene)0.79 ug/L 02/07/13 01:170.50SM 6200B
n-Propylbenzene 0.54 ug/L 02/07/13 01:170.50SM 6200B
1,2,4-Trimethylbenzene 1.2 ug/L 02/07/13 01:170.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-1 Lab ID:92146489001 Collected:01/28/13 16:00 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 02/07/13 00:14 71-43-20.50 0.25
Bromobenzene ND ug/L 1 02/07/13 00:14 108-86-10.50 0.25
Bromochloromethane ND ug/L 1 02/07/13 00:14 74-97-50.50 0.25
Bromodichloromethane ND ug/L 1 02/07/13 00:14 75-27-40.50 0.25
Bromoform ND ug/L 1 02/07/13 00:14 75-25-20.50 0.25
Bromomethane ND ug/L 1 02/07/13 00:14 74-83-95.0 0.50
n-Butylbenzene ND ug/L 1 02/07/13 00:14 104-51-80.50 0.25
sec-Butylbenzene ND ug/L 1 02/07/13 00:14 135-98-80.50 0.25
tert-Butylbenzene ND ug/L 1 02/07/13 00:14 98-06-60.50 0.25
Carbon tetrachloride ND ug/L 1 02/07/13 00:14 56-23-50.50 0.25
Chlorobenzene ND ug/L 1 02/07/13 00:14 108-90-70.50 0.25
Chloroethane ND ug/L 1 02/07/13 00:14 75-00-31.0 0.50
Chloroform ND ug/L 1 02/07/13 00:14 67-66-30.50 0.25
Chloromethane ND ug/L 1 02/07/13 00:14 74-87-31.0 0.50
2-Chlorotoluene ND ug/L 1 02/07/13 00:14 95-49-80.50 0.25
4-Chlorotoluene ND ug/L 1 02/07/13 00:14 106-43-40.50 0.25
1,2-Dibromo-3-chloropropane ND ug/L 1 02/07/13 00:14 96-12-81.0 0.50
Dibromochloromethane ND ug/L 1 02/07/13 00:14 124-48-10.50 0.25
1,2-Dibromoethane (EDB)ND ug/L 1 02/07/13 00:14 106-93-40.50 0.25
Dibromomethane ND ug/L 1 02/07/13 00:14 74-95-30.50 0.25
1,2-Dichlorobenzene ND ug/L 1 02/07/13 00:14 95-50-10.50 0.25
1,3-Dichlorobenzene ND ug/L 1 02/07/13 00:14 541-73-10.50 0.25
1,4-Dichlorobenzene ND ug/L 1 02/07/13 00:14 106-46-70.50 0.25
Dichlorodifluoromethane ND ug/L 1 02/07/13 00:14 75-71-80.50 0.25
1,1-Dichloroethane ND ug/L 1 02/07/13 00:14 75-34-30.50 0.25
1,2-Dichloroethane ND ug/L 1 02/07/13 00:14 107-06-20.50 0.25
1,1-Dichloroethene ND ug/L 1 02/07/13 00:14 75-35-40.50 0.25
cis-1,2-Dichloroethene ND ug/L 1 02/07/13 00:14 156-59-20.50 0.25
trans-1,2-Dichloroethene ND ug/L 1 02/07/13 00:14 156-60-50.50 0.25
1,2-Dichloropropane ND ug/L 1 02/07/13 00:14 78-87-50.50 0.25
1,3-Dichloropropane ND ug/L 1 02/07/13 00:14 142-28-90.50 0.25
2,2-Dichloropropane ND ug/L 1 02/07/13 00:14 594-20-70.50 0.25
1,1-Dichloropropene ND ug/L 1 02/07/13 00:14 563-58-60.50 0.25
cis-1,3-Dichloropropene ND ug/L 1 02/07/13 00:14 10061-01-50.50 0.25
trans-1,3-Dichloropropene ND ug/L 1 02/07/13 00:14 10061-02-60.50 0.25
Diisopropyl ether ND ug/L 1 02/07/13 00:14 108-20-30.50 0.25
Ethylbenzene ND ug/L 1 02/07/13 00:14 100-41-40.50 0.25
Hexachloro-1,3-butadiene ND ug/L 1 02/07/13 00:14 87-68-32.0 1.0
Isopropylbenzene (Cumene)ND ug/L 1 02/07/13 00:14 98-82-80.50 0.25
Methylene Chloride ND ug/L 1 02/07/13 00:14 75-09-22.0 1.0
Methyl-tert-butyl ether ND ug/L 1 02/07/13 00:14 1634-04-40.50 0.25
Naphthalene ND ug/L 1 02/07/13 00:14 91-20-32.0 1.0
n-Propylbenzene ND ug/L 1 02/07/13 00:14 103-65-10.50 0.25
Styrene ND ug/L 1 02/07/13 00:14 100-42-50.50 0.25
1,1,1,2-Tetrachloroethane ND ug/L 1 02/07/13 00:14 630-20-60.50 0.25
1,1,2,2-Tetrachloroethane ND ug/L 1 02/07/13 00:14 79-34-50.50 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 6 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-1 Lab ID:92146489001 Collected:01/28/13 16:00 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 02/07/13 00:14 127-18-40.50 0.25
Toluene ND ug/L 1 02/07/13 00:14 108-88-30.50 0.25
1,2,3-Trichlorobenzene ND ug/L 1 02/07/13 00:14 87-61-62.0 1.0
1,2,4-Trichlorobenzene ND ug/L 1 02/07/13 00:14 120-82-12.0 1.0
1,1,1-Trichloroethane ND ug/L 1 02/07/13 00:14 71-55-60.50 0.25
1,1,2-Trichloroethane ND ug/L 1 02/07/13 00:14 79-00-50.50 0.25
Trichloroethene ND ug/L 1 02/07/13 00:14 79-01-60.50 0.25
Trichlorofluoromethane ND ug/L 1 02/07/13 00:14 75-69-41.0 0.50
1,2,3-Trichloropropane ND ug/L 1 02/07/13 00:14 96-18-40.50 0.25
1,2,4-Trimethylbenzene ND ug/L 1 02/07/13 00:14 95-63-60.50 0.25
1,3,5-Trimethylbenzene ND ug/L 1 02/07/13 00:14 108-67-80.50 0.25
Vinyl chloride ND ug/L 1 02/07/13 00:14 75-01-41.0 0.25
m&p-Xylene ND ug/L 1 02/07/13 00:14 179601-23-11.0 0.50
o-Xylene ND ug/L 1 02/07/13 00:14 95-47-60.50 0.25
Surrogates
1,2-Dichloroethane-d4 (S)106 %1 02/07/13 00:14 17060-07-070-130
Dibromofluoromethane (S)100 %1 02/07/13 00:14 1868-53-770-130
4-Bromofluorobenzene (S)97 %1 02/07/13 00:14 460-00-470-130
Toluene-d8 (S)99 %1 02/07/13 00:14 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 7 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-3 Lab ID:92146489002 Collected:01/28/13 16:30 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 02/07/13 00:30 71-43-20.50 0.25
Bromobenzene ND ug/L 1 02/07/13 00:30 108-86-10.50 0.25
Bromochloromethane ND ug/L 1 02/07/13 00:30 74-97-50.50 0.25
Bromodichloromethane ND ug/L 1 02/07/13 00:30 75-27-40.50 0.25
Bromoform ND ug/L 1 02/07/13 00:30 75-25-20.50 0.25
Bromomethane ND ug/L 1 02/07/13 00:30 74-83-95.0 0.50
n-Butylbenzene ND ug/L 1 02/07/13 00:30 104-51-80.50 0.25
sec-Butylbenzene ND ug/L 1 02/07/13 00:30 135-98-80.50 0.25
tert-Butylbenzene ND ug/L 1 02/07/13 00:30 98-06-60.50 0.25
Carbon tetrachloride ND ug/L 1 02/07/13 00:30 56-23-50.50 0.25
Chlorobenzene ND ug/L 1 02/07/13 00:30 108-90-70.50 0.25
Chloroethane ND ug/L 1 02/07/13 00:30 75-00-31.0 0.50
Chloroform ND ug/L 1 02/07/13 00:30 67-66-30.50 0.25
Chloromethane ND ug/L 1 02/07/13 00:30 74-87-31.0 0.50
2-Chlorotoluene ND ug/L 1 02/07/13 00:30 95-49-80.50 0.25
4-Chlorotoluene ND ug/L 1 02/07/13 00:30 106-43-40.50 0.25
1,2-Dibromo-3-chloropropane ND ug/L 1 02/07/13 00:30 96-12-81.0 0.50
Dibromochloromethane ND ug/L 1 02/07/13 00:30 124-48-10.50 0.25
1,2-Dibromoethane (EDB)ND ug/L 1 02/07/13 00:30 106-93-40.50 0.25
Dibromomethane ND ug/L 1 02/07/13 00:30 74-95-30.50 0.25
1,2-Dichlorobenzene ND ug/L 1 02/07/13 00:30 95-50-10.50 0.25
1,3-Dichlorobenzene ND ug/L 1 02/07/13 00:30 541-73-10.50 0.25
1,4-Dichlorobenzene ND ug/L 1 02/07/13 00:30 106-46-70.50 0.25
Dichlorodifluoromethane ND ug/L 1 02/07/13 00:30 75-71-80.50 0.25
1,1-Dichloroethane ND ug/L 1 02/07/13 00:30 75-34-30.50 0.25
1,2-Dichloroethane ND ug/L 1 02/07/13 00:30 107-06-20.50 0.25
1,1-Dichloroethene ND ug/L 1 02/07/13 00:30 75-35-40.50 0.25
cis-1,2-Dichloroethene ND ug/L 1 02/07/13 00:30 156-59-20.50 0.25
trans-1,2-Dichloroethene ND ug/L 1 02/07/13 00:30 156-60-50.50 0.25
1,2-Dichloropropane ND ug/L 1 02/07/13 00:30 78-87-50.50 0.25
1,3-Dichloropropane ND ug/L 1 02/07/13 00:30 142-28-90.50 0.25
2,2-Dichloropropane ND ug/L 1 02/07/13 00:30 594-20-70.50 0.25
1,1-Dichloropropene ND ug/L 1 02/07/13 00:30 563-58-60.50 0.25
cis-1,3-Dichloropropene ND ug/L 1 02/07/13 00:30 10061-01-50.50 0.25
trans-1,3-Dichloropropene ND ug/L 1 02/07/13 00:30 10061-02-60.50 0.25
Diisopropyl ether ND ug/L 1 02/07/13 00:30 108-20-30.50 0.25
Ethylbenzene ND ug/L 1 02/07/13 00:30 100-41-40.50 0.25
Hexachloro-1,3-butadiene ND ug/L 1 02/07/13 00:30 87-68-32.0 1.0
Isopropylbenzene (Cumene)ND ug/L 1 02/07/13 00:30 98-82-80.50 0.25
Methylene Chloride ND ug/L 1 02/07/13 00:30 75-09-22.0 1.0
Methyl-tert-butyl ether ND ug/L 1 02/07/13 00:30 1634-04-40.50 0.25
Naphthalene ND ug/L 1 02/07/13 00:30 91-20-32.0 1.0
n-Propylbenzene ND ug/L 1 02/07/13 00:30 103-65-10.50 0.25
Styrene ND ug/L 1 02/07/13 00:30 100-42-50.50 0.25
1,1,1,2-Tetrachloroethane ND ug/L 1 02/07/13 00:30 630-20-60.50 0.25
1,1,2,2-Tetrachloroethane ND ug/L 1 02/07/13 00:30 79-34-50.50 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 8 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-3 Lab ID:92146489002 Collected:01/28/13 16:30 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 02/07/13 00:30 127-18-40.50 0.25
Toluene ND ug/L 1 02/07/13 00:30 108-88-30.50 0.25
1,2,3-Trichlorobenzene ND ug/L 1 02/07/13 00:30 87-61-62.0 1.0
1,2,4-Trichlorobenzene ND ug/L 1 02/07/13 00:30 120-82-12.0 1.0
1,1,1-Trichloroethane ND ug/L 1 02/07/13 00:30 71-55-60.50 0.25
1,1,2-Trichloroethane ND ug/L 1 02/07/13 00:30 79-00-50.50 0.25
Trichloroethene ND ug/L 1 02/07/13 00:30 79-01-60.50 0.25
Trichlorofluoromethane ND ug/L 1 02/07/13 00:30 75-69-41.0 0.50
1,2,3-Trichloropropane ND ug/L 1 02/07/13 00:30 96-18-40.50 0.25
1,2,4-Trimethylbenzene ND ug/L 1 02/07/13 00:30 95-63-60.50 0.25
1,3,5-Trimethylbenzene ND ug/L 1 02/07/13 00:30 108-67-80.50 0.25
Vinyl chloride ND ug/L 1 02/07/13 00:30 75-01-41.0 0.25
m&p-Xylene ND ug/L 1 02/07/13 00:30 179601-23-11.0 0.50
o-Xylene ND ug/L 1 02/07/13 00:30 95-47-60.50 0.25
Surrogates
1,2-Dichloroethane-d4 (S)103 %1 02/07/13 00:30 17060-07-070-130
Dibromofluoromethane (S)103 %1 02/07/13 00:30 1868-53-770-130
4-Bromofluorobenzene (S)94 %1 02/07/13 00:30 460-00-470-130
Toluene-d8 (S)98 %1 02/07/13 00:30 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 9 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-4 Lab ID:92146489003 Collected:01/28/13 17:10 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 02/07/13 00:46 71-43-20.50 0.25
Bromobenzene ND ug/L 1 02/07/13 00:46 108-86-10.50 0.25
Bromochloromethane ND ug/L 1 02/07/13 00:46 74-97-50.50 0.25
Bromodichloromethane ND ug/L 1 02/07/13 00:46 75-27-40.50 0.25
Bromoform ND ug/L 1 02/07/13 00:46 75-25-20.50 0.25
Bromomethane ND ug/L 1 02/07/13 00:46 74-83-95.0 0.50
n-Butylbenzene ND ug/L 1 02/07/13 00:46 104-51-80.50 0.25
sec-Butylbenzene ND ug/L 1 02/07/13 00:46 135-98-80.50 0.25
tert-Butylbenzene ND ug/L 1 02/07/13 00:46 98-06-60.50 0.25
Carbon tetrachloride ND ug/L 1 02/07/13 00:46 56-23-50.50 0.25
Chlorobenzene ND ug/L 1 02/07/13 00:46 108-90-70.50 0.25
Chloroethane ND ug/L 1 02/07/13 00:46 75-00-31.0 0.50
Chloroform ND ug/L 1 02/07/13 00:46 67-66-30.50 0.25
Chloromethane ND ug/L 1 02/07/13 00:46 74-87-31.0 0.50
2-Chlorotoluene ND ug/L 1 02/07/13 00:46 95-49-80.50 0.25
4-Chlorotoluene ND ug/L 1 02/07/13 00:46 106-43-40.50 0.25
1,2-Dibromo-3-chloropropane ND ug/L 1 02/07/13 00:46 96-12-81.0 0.50
Dibromochloromethane ND ug/L 1 02/07/13 00:46 124-48-10.50 0.25
1,2-Dibromoethane (EDB)ND ug/L 1 02/07/13 00:46 106-93-40.50 0.25
Dibromomethane ND ug/L 1 02/07/13 00:46 74-95-30.50 0.25
1,2-Dichlorobenzene ND ug/L 1 02/07/13 00:46 95-50-10.50 0.25
1,3-Dichlorobenzene ND ug/L 1 02/07/13 00:46 541-73-10.50 0.25
1,4-Dichlorobenzene ND ug/L 1 02/07/13 00:46 106-46-70.50 0.25
Dichlorodifluoromethane ND ug/L 1 02/07/13 00:46 75-71-80.50 0.25
1,1-Dichloroethane ND ug/L 1 02/07/13 00:46 75-34-30.50 0.25
1,2-Dichloroethane ND ug/L 1 02/07/13 00:46 107-06-20.50 0.25
1,1-Dichloroethene ND ug/L 1 02/07/13 00:46 75-35-40.50 0.25
cis-1,2-Dichloroethene ND ug/L 1 02/07/13 00:46 156-59-20.50 0.25
trans-1,2-Dichloroethene ND ug/L 1 02/07/13 00:46 156-60-50.50 0.25
1,2-Dichloropropane ND ug/L 1 02/07/13 00:46 78-87-50.50 0.25
1,3-Dichloropropane ND ug/L 1 02/07/13 00:46 142-28-90.50 0.25
2,2-Dichloropropane ND ug/L 1 02/07/13 00:46 594-20-70.50 0.25
1,1-Dichloropropene ND ug/L 1 02/07/13 00:46 563-58-60.50 0.25
cis-1,3-Dichloropropene ND ug/L 1 02/07/13 00:46 10061-01-50.50 0.25
trans-1,3-Dichloropropene ND ug/L 1 02/07/13 00:46 10061-02-60.50 0.25
Diisopropyl ether ND ug/L 1 02/07/13 00:46 108-20-30.50 0.25
Ethylbenzene ND ug/L 1 02/07/13 00:46 100-41-40.50 0.25
Hexachloro-1,3-butadiene ND ug/L 1 02/07/13 00:46 87-68-32.0 1.0
Isopropylbenzene (Cumene)ND ug/L 1 02/07/13 00:46 98-82-80.50 0.25
Methylene Chloride ND ug/L 1 02/07/13 00:46 75-09-22.0 1.0
Methyl-tert-butyl ether ND ug/L 1 02/07/13 00:46 1634-04-40.50 0.25
Naphthalene ND ug/L 1 02/07/13 00:46 91-20-32.0 1.0
n-Propylbenzene ND ug/L 1 02/07/13 00:46 103-65-10.50 0.25
Styrene ND ug/L 1 02/07/13 00:46 100-42-50.50 0.25
1,1,1,2-Tetrachloroethane ND ug/L 1 02/07/13 00:46 630-20-60.50 0.25
1,1,2,2-Tetrachloroethane ND ug/L 1 02/07/13 00:46 79-34-50.50 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 10 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-4 Lab ID:92146489003 Collected:01/28/13 17:10 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 02/07/13 00:46 127-18-40.50 0.25
Toluene ND ug/L 1 02/07/13 00:46 108-88-30.50 0.25
1,2,3-Trichlorobenzene ND ug/L 1 02/07/13 00:46 87-61-62.0 1.0
1,2,4-Trichlorobenzene ND ug/L 1 02/07/13 00:46 120-82-12.0 1.0
1,1,1-Trichloroethane ND ug/L 1 02/07/13 00:46 71-55-60.50 0.25
1,1,2-Trichloroethane ND ug/L 1 02/07/13 00:46 79-00-50.50 0.25
Trichloroethene ND ug/L 1 02/07/13 00:46 79-01-60.50 0.25
Trichlorofluoromethane ND ug/L 1 02/07/13 00:46 75-69-41.0 0.50
1,2,3-Trichloropropane ND ug/L 1 02/07/13 00:46 96-18-40.50 0.25
1,2,4-Trimethylbenzene ND ug/L 1 02/07/13 00:46 95-63-60.50 0.25
1,3,5-Trimethylbenzene ND ug/L 1 02/07/13 00:46 108-67-80.50 0.25
Vinyl chloride ND ug/L 1 02/07/13 00:46 75-01-41.0 0.25
m&p-Xylene ND ug/L 1 02/07/13 00:46 179601-23-11.0 0.50
o-Xylene ND ug/L 1 02/07/13 00:46 95-47-60.50 0.25
Surrogates
1,2-Dichloroethane-d4 (S)110 %1 02/07/13 00:46 17060-07-070-130
Dibromofluoromethane (S)110 %1 02/07/13 00:46 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 02/07/13 00:46 460-00-470-130
Toluene-d8 (S)98 %1 02/07/13 00:46 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 11 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-5 Lab ID:92146489004 Collected:01/28/13 17:40 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 02/07/13 01:02 71-43-20.50 0.25
Bromobenzene ND ug/L 1 02/07/13 01:02 108-86-10.50 0.25
Bromochloromethane ND ug/L 1 02/07/13 01:02 74-97-50.50 0.25
Bromodichloromethane ND ug/L 1 02/07/13 01:02 75-27-40.50 0.25
Bromoform ND ug/L 1 02/07/13 01:02 75-25-20.50 0.25
Bromomethane ND ug/L 1 02/07/13 01:02 74-83-95.0 0.50
n-Butylbenzene ND ug/L 1 02/07/13 01:02 104-51-80.50 0.25
sec-Butylbenzene ND ug/L 1 02/07/13 01:02 135-98-80.50 0.25
tert-Butylbenzene ND ug/L 1 02/07/13 01:02 98-06-60.50 0.25
Carbon tetrachloride ND ug/L 1 02/07/13 01:02 56-23-50.50 0.25
Chlorobenzene ND ug/L 1 02/07/13 01:02 108-90-70.50 0.25
Chloroethane ND ug/L 1 02/07/13 01:02 75-00-31.0 0.50
Chloroform ND ug/L 1 02/07/13 01:02 67-66-30.50 0.25
Chloromethane ND ug/L 1 02/07/13 01:02 74-87-31.0 0.50
2-Chlorotoluene ND ug/L 1 02/07/13 01:02 95-49-80.50 0.25
4-Chlorotoluene ND ug/L 1 02/07/13 01:02 106-43-40.50 0.25
1,2-Dibromo-3-chloropropane ND ug/L 1 02/07/13 01:02 96-12-81.0 0.50
Dibromochloromethane ND ug/L 1 02/07/13 01:02 124-48-10.50 0.25
1,2-Dibromoethane (EDB)ND ug/L 1 02/07/13 01:02 106-93-40.50 0.25
Dibromomethane ND ug/L 1 02/07/13 01:02 74-95-30.50 0.25
1,2-Dichlorobenzene ND ug/L 1 02/07/13 01:02 95-50-10.50 0.25
1,3-Dichlorobenzene ND ug/L 1 02/07/13 01:02 541-73-10.50 0.25
1,4-Dichlorobenzene ND ug/L 1 02/07/13 01:02 106-46-70.50 0.25
Dichlorodifluoromethane ND ug/L 1 02/07/13 01:02 75-71-80.50 0.25
1,1-Dichloroethane ND ug/L 1 02/07/13 01:02 75-34-30.50 0.25
1,2-Dichloroethane 0.32J ug/L 1 02/07/13 01:02 107-06-20.50 0.25
1,1-Dichloroethene ND ug/L 1 02/07/13 01:02 75-35-40.50 0.25
cis-1,2-Dichloroethene ND ug/L 1 02/07/13 01:02 156-59-20.50 0.25
trans-1,2-Dichloroethene ND ug/L 1 02/07/13 01:02 156-60-50.50 0.25
1,2-Dichloropropane ND ug/L 1 02/07/13 01:02 78-87-50.50 0.25
1,3-Dichloropropane ND ug/L 1 02/07/13 01:02 142-28-90.50 0.25
2,2-Dichloropropane ND ug/L 1 02/07/13 01:02 594-20-70.50 0.25
1,1-Dichloropropene ND ug/L 1 02/07/13 01:02 563-58-60.50 0.25
cis-1,3-Dichloropropene ND ug/L 1 02/07/13 01:02 10061-01-50.50 0.25
trans-1,3-Dichloropropene ND ug/L 1 02/07/13 01:02 10061-02-60.50 0.25
Diisopropyl ether ND ug/L 1 02/07/13 01:02 108-20-30.50 0.25
Ethylbenzene ND ug/L 1 02/07/13 01:02 100-41-40.50 0.25
Hexachloro-1,3-butadiene ND ug/L 1 02/07/13 01:02 87-68-32.0 1.0
Isopropylbenzene (Cumene)ND ug/L 1 02/07/13 01:02 98-82-80.50 0.25
Methylene Chloride ND ug/L 1 02/07/13 01:02 75-09-22.0 1.0
Methyl-tert-butyl ether ND ug/L 1 02/07/13 01:02 1634-04-40.50 0.25
Naphthalene ND ug/L 1 02/07/13 01:02 91-20-32.0 1.0
n-Propylbenzene ND ug/L 1 02/07/13 01:02 103-65-10.50 0.25
Styrene ND ug/L 1 02/07/13 01:02 100-42-50.50 0.25
1,1,1,2-Tetrachloroethane ND ug/L 1 02/07/13 01:02 630-20-60.50 0.25
1,1,2,2-Tetrachloroethane ND ug/L 1 02/07/13 01:02 79-34-50.50 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 12 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-5 Lab ID:92146489004 Collected:01/28/13 17:40 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 02/07/13 01:02 127-18-40.50 0.25
Toluene ND ug/L 1 02/07/13 01:02 108-88-30.50 0.25
1,2,3-Trichlorobenzene ND ug/L 1 02/07/13 01:02 87-61-62.0 1.0
1,2,4-Trichlorobenzene ND ug/L 1 02/07/13 01:02 120-82-12.0 1.0
1,1,1-Trichloroethane ND ug/L 1 02/07/13 01:02 71-55-60.50 0.25
1,1,2-Trichloroethane ND ug/L 1 02/07/13 01:02 79-00-50.50 0.25
Trichloroethene ND ug/L 1 02/07/13 01:02 79-01-60.50 0.25
Trichlorofluoromethane ND ug/L 1 02/07/13 01:02 75-69-41.0 0.50
1,2,3-Trichloropropane ND ug/L 1 02/07/13 01:02 96-18-40.50 0.25
1,2,4-Trimethylbenzene ND ug/L 1 02/07/13 01:02 95-63-60.50 0.25
1,3,5-Trimethylbenzene ND ug/L 1 02/07/13 01:02 108-67-80.50 0.25
Vinyl chloride ND ug/L 1 02/07/13 01:02 75-01-41.0 0.25
m&p-Xylene ND ug/L 1 02/07/13 01:02 179601-23-11.0 0.50
o-Xylene ND ug/L 1 02/07/13 01:02 95-47-60.50 0.25
Surrogates
1,2-Dichloroethane-d4 (S)106 %1 02/07/13 01:02 17060-07-070-130
Dibromofluoromethane (S)97 %1 02/07/13 01:02 1868-53-770-130
4-Bromofluorobenzene (S)93 %1 02/07/13 01:02 460-00-470-130
Toluene-d8 (S)98 %1 02/07/13 01:02 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 13 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-6 Lab ID:92146489005 Collected:01/28/13 16:50 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 02/07/13 01:17 71-43-20.50 0.25
Bromobenzene ND ug/L 1 02/07/13 01:17 108-86-10.50 0.25
Bromochloromethane ND ug/L 1 02/07/13 01:17 74-97-50.50 0.25
Bromodichloromethane ND ug/L 1 02/07/13 01:17 75-27-40.50 0.25
Bromoform ND ug/L 1 02/07/13 01:17 75-25-20.50 0.25
Bromomethane ND ug/L 1 02/07/13 01:17 74-83-95.0 0.50
n-Butylbenzene ND ug/L 1 02/07/13 01:17 104-51-80.50 0.25
sec-Butylbenzene ND ug/L 1 02/07/13 01:17 135-98-80.50 0.25
tert-Butylbenzene ND ug/L 1 02/07/13 01:17 98-06-60.50 0.25
Carbon tetrachloride ND ug/L 1 02/07/13 01:17 56-23-50.50 0.25
Chlorobenzene ND ug/L 1 02/07/13 01:17 108-90-70.50 0.25
Chloroethane ND ug/L 1 02/07/13 01:17 75-00-31.0 0.50
Chloroform ND ug/L 1 02/07/13 01:17 67-66-30.50 0.25
Chloromethane ND ug/L 1 02/07/13 01:17 74-87-31.0 0.50
2-Chlorotoluene ND ug/L 1 02/07/13 01:17 95-49-80.50 0.25
4-Chlorotoluene ND ug/L 1 02/07/13 01:17 106-43-40.50 0.25
1,2-Dibromo-3-chloropropane ND ug/L 1 02/07/13 01:17 96-12-81.0 0.50
Dibromochloromethane ND ug/L 1 02/07/13 01:17 124-48-10.50 0.25
1,2-Dibromoethane (EDB)ND ug/L 1 02/07/13 01:17 106-93-40.50 0.25
Dibromomethane ND ug/L 1 02/07/13 01:17 74-95-30.50 0.25
1,2-Dichlorobenzene ND ug/L 1 02/07/13 01:17 95-50-10.50 0.25
1,3-Dichlorobenzene ND ug/L 1 02/07/13 01:17 541-73-10.50 0.25
1,4-Dichlorobenzene ND ug/L 1 02/07/13 01:17 106-46-70.50 0.25
Dichlorodifluoromethane ND ug/L 1 02/07/13 01:17 75-71-80.50 0.25
1,1-Dichloroethane ND ug/L 1 02/07/13 01:17 75-34-30.50 0.25
1,2-Dichloroethane 1.4 ug/L 1 02/07/13 01:17 107-06-20.50 0.25
1,1-Dichloroethene ND ug/L 1 02/07/13 01:17 75-35-40.50 0.25
cis-1,2-Dichloroethene ND ug/L 1 02/07/13 01:17 156-59-20.50 0.25
trans-1,2-Dichloroethene ND ug/L 1 02/07/13 01:17 156-60-50.50 0.25
1,2-Dichloropropane ND ug/L 1 02/07/13 01:17 78-87-50.50 0.25
1,3-Dichloropropane ND ug/L 1 02/07/13 01:17 142-28-90.50 0.25
2,2-Dichloropropane ND ug/L 1 02/07/13 01:17 594-20-70.50 0.25
1,1-Dichloropropene ND ug/L 1 02/07/13 01:17 563-58-60.50 0.25
cis-1,3-Dichloropropene ND ug/L 1 02/07/13 01:17 10061-01-50.50 0.25
trans-1,3-Dichloropropene ND ug/L 1 02/07/13 01:17 10061-02-60.50 0.25
Diisopropyl ether 7.2 ug/L 1 02/07/13 01:17 108-20-30.50 0.25
Ethylbenzene 0.60 ug/L 1 02/07/13 01:17 100-41-40.50 0.25
Hexachloro-1,3-butadiene ND ug/L 1 02/07/13 01:17 87-68-32.0 1.0
Isopropylbenzene (Cumene)0.79 ug/L 1 02/07/13 01:17 98-82-80.50 0.25
Methylene Chloride ND ug/L 1 02/07/13 01:17 75-09-22.0 1.0
Methyl-tert-butyl ether ND ug/L 1 02/07/13 01:17 1634-04-40.50 0.25
Naphthalene ND ug/L 1 02/07/13 01:17 91-20-32.0 1.0
n-Propylbenzene 0.54 ug/L 1 02/07/13 01:17 103-65-10.50 0.25
Styrene ND ug/L 1 02/07/13 01:17 100-42-50.50 0.25
1,1,1,2-Tetrachloroethane ND ug/L 1 02/07/13 01:17 630-20-60.50 0.25
1,1,2,2-Tetrachloroethane ND ug/L 1 02/07/13 01:17 79-34-50.50 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 14 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Sample:WSW-6 Lab ID:92146489005 Collected:01/28/13 16:50 Received:01/31/13 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Tetrachloroethene ND ug/L 1 02/07/13 01:17 127-18-40.50 0.25
Toluene ND ug/L 1 02/07/13 01:17 108-88-30.50 0.25
1,2,3-Trichlorobenzene ND ug/L 1 02/07/13 01:17 87-61-62.0 1.0
1,2,4-Trichlorobenzene ND ug/L 1 02/07/13 01:17 120-82-12.0 1.0
1,1,1-Trichloroethane ND ug/L 1 02/07/13 01:17 71-55-60.50 0.25
1,1,2-Trichloroethane ND ug/L 1 02/07/13 01:17 79-00-50.50 0.25
Trichloroethene ND ug/L 1 02/07/13 01:17 79-01-60.50 0.25
Trichlorofluoromethane ND ug/L 1 02/07/13 01:17 75-69-41.0 0.50
1,2,3-Trichloropropane ND ug/L 1 02/07/13 01:17 96-18-40.50 0.25
1,2,4-Trimethylbenzene 1.2 ug/L 1 02/07/13 01:17 95-63-60.50 0.25
1,3,5-Trimethylbenzene ND ug/L 1 02/07/13 01:17 108-67-80.50 0.25
Vinyl chloride ND ug/L 1 02/07/13 01:17 75-01-41.0 0.25
m&p-Xylene ND ug/L 1 02/07/13 01:17 179601-23-11.0 0.50
o-Xylene ND ug/L 1 02/07/13 01:17 95-47-60.50 0.25
Surrogates
1,2-Dichloroethane-d4 (S)109 %1 02/07/13 01:17 17060-07-070-130
Dibromofluoromethane (S)107 %1 02/07/13 01:17 1868-53-770-130
4-Bromofluorobenzene (S)94 %1 02/07/13 01:17 460-00-470-130
Toluene-d8 (S)99 %1 02/07/13 01:17 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 15 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/21917
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92146489001, 92146489002, 92146489003, 92146489004, 92146489005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:917359
Associated Lab Samples:92146489001, 92146489002, 92146489003, 92146489004, 92146489005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/06/13 23:58
1,1,1-Trichloroethane ug/L ND 0.50 02/06/13 23:58
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/06/13 23:58
1,1,2-Trichloroethane ug/L ND 0.50 02/06/13 23:58
1,1-Dichloroethane ug/L ND 0.50 02/06/13 23:58
1,1-Dichloroethene ug/L ND 0.50 02/06/13 23:58
1,1-Dichloropropene ug/L ND 0.50 02/06/13 23:58
1,2,3-Trichlorobenzene ug/L ND 2.0 02/06/13 23:58
1,2,3-Trichloropropane ug/L ND 0.50 02/06/13 23:58
1,2,4-Trichlorobenzene ug/L ND 2.0 02/06/13 23:58
1,2,4-Trimethylbenzene ug/L ND 0.50 02/06/13 23:58
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/06/13 23:58
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/06/13 23:58
1,2-Dichlorobenzene ug/L ND 0.50 02/06/13 23:58
1,2-Dichloroethane ug/L ND 0.50 02/06/13 23:58
1,2-Dichloropropane ug/L ND 0.50 02/06/13 23:58
1,3,5-Trimethylbenzene ug/L ND 0.50 02/06/13 23:58
1,3-Dichlorobenzene ug/L ND 0.50 02/06/13 23:58
1,3-Dichloropropane ug/L ND 0.50 02/06/13 23:58
1,4-Dichlorobenzene ug/L ND 0.50 02/06/13 23:58
2,2-Dichloropropane ug/L ND 0.50 02/06/13 23:58
2-Chlorotoluene ug/L ND 0.50 02/06/13 23:58
4-Chlorotoluene ug/L ND 0.50 02/06/13 23:58
Benzene ug/L ND 0.50 02/06/13 23:58
Bromobenzene ug/L ND 0.50 02/06/13 23:58
Bromochloromethane ug/L ND 0.50 02/06/13 23:58
Bromodichloromethane ug/L ND 0.50 02/06/13 23:58
Bromoform ug/L ND 0.50 02/06/13 23:58
Bromomethane ug/L ND 5.0 02/06/13 23:58
Carbon tetrachloride ug/L ND 0.50 02/06/13 23:58
Chlorobenzene ug/L ND 0.50 02/06/13 23:58
Chloroethane ug/L ND 1.0 02/06/13 23:58
Chloroform ug/L ND 0.50 02/06/13 23:58
Chloromethane ug/L ND 1.0 02/06/13 23:58
cis-1,2-Dichloroethene ug/L ND 0.50 02/06/13 23:58
cis-1,3-Dichloropropene ug/L ND 0.50 02/06/13 23:58
Dibromochloromethane ug/L ND 0.50 02/06/13 23:58
Dibromomethane ug/L ND 0.50 02/06/13 23:58
Dichlorodifluoromethane ug/L ND 0.50 02/06/13 23:58
Diisopropyl ether ug/L ND 0.50 02/06/13 23:58
Ethylbenzene ug/L ND 0.50 02/06/13 23:58
Hexachloro-1,3-butadiene ug/L ND 2.0 02/06/13 23:58
Isopropylbenzene (Cumene)ug/L ND 0.50 02/06/13 23:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 16 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:917359
Associated Lab Samples:92146489001, 92146489002, 92146489003, 92146489004, 92146489005
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 02/06/13 23:58
Methyl-tert-butyl ether ug/L ND 0.50 02/06/13 23:58
Methylene Chloride ug/L ND 2.0 02/06/13 23:58
n-Butylbenzene ug/L ND 0.50 02/06/13 23:58
n-Propylbenzene ug/L ND 0.50 02/06/13 23:58
Naphthalene ug/L ND 2.0 02/06/13 23:58
o-Xylene ug/L ND 0.50 02/06/13 23:58
sec-Butylbenzene ug/L ND 0.50 02/06/13 23:58
Styrene ug/L ND 0.50 02/06/13 23:58
tert-Butylbenzene ug/L ND 0.50 02/06/13 23:58
Tetrachloroethene ug/L ND 0.50 02/06/13 23:58
Toluene ug/L ND 0.50 02/06/13 23:58
trans-1,2-Dichloroethene ug/L ND 0.50 02/06/13 23:58
trans-1,3-Dichloropropene ug/L ND 0.50 02/06/13 23:58
Trichloroethene ug/L ND 0.50 02/06/13 23:58
Trichlorofluoromethane ug/L ND 1.0 02/06/13 23:58
Vinyl chloride ug/L ND 1.0 02/06/13 23:58
1,2-Dichloroethane-d4 (S)%102 70-130 02/06/13 23:58
4-Bromofluorobenzene (S)%96 70-130 02/06/13 23:58
Dibromofluoromethane (S)%101 70-130 02/06/13 23:58
Toluene-d8 (S)%98 70-130 02/06/13 23:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
917360LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.850 94 60-140
1,1,1-Trichloroethane ug/L 45.250 90 60-140
1,1,2,2-Tetrachloroethane ug/L 46.750 93 60-140
1,1,2-Trichloroethane ug/L 53.350 107 60-140
1,1-Dichloroethane ug/L 48.250 96 60-140
1,1-Dichloroethene ug/L 44.150 88 60-140
1,1-Dichloropropene ug/L 48.950 98 60-140
1,2,3-Trichlorobenzene ug/L 52.350 105 60-140
1,2,3-Trichloropropane ug/L 48.150 96 60-140
1,2,4-Trichlorobenzene ug/L 51.450 103 60-140
1,2,4-Trimethylbenzene ug/L 48.250 96 60-140
1,2-Dibromo-3-chloropropane ug/L 54.650 109 60-140
1,2-Dibromoethane (EDB)ug/L 49.450 99 60-140
1,2-Dichlorobenzene ug/L 49.250 98 60-140
1,2-Dichloroethane ug/L 45.450 91 60-140
1,2-Dichloropropane ug/L 49.250 98 60-140
1,3,5-Trimethylbenzene ug/L 50.250 100 60-140
1,3-Dichlorobenzene ug/L 48.350 97 60-140
1,3-Dichloropropane ug/L 50.350 101 60-140
1,4-Dichlorobenzene ug/L 47.750 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 17 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
917360LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 40.550 81 60-140
2-Chlorotoluene ug/L 47.150 94 60-140
4-Chlorotoluene ug/L 49.850 100 60-140
Benzene ug/L 51.250 102 60-140
Bromobenzene ug/L 50.650 101 60-140
Bromochloromethane ug/L 38.450 77 60-140
Bromodichloromethane ug/L 50.150 100 60-140
Bromoform ug/L 50.150 100 60-140
Bromomethane ug/L 46.350 93 60-140
Carbon tetrachloride ug/L 48.350 97 60-140
Chlorobenzene ug/L 48.350 97 60-140
Chloroethane ug/L 42.250 84 60-140
Chloroform ug/L 43.250 86 60-140
Chloromethane ug/L 31.950 64 60-140
cis-1,2-Dichloroethene ug/L 46.650 93 60-140
cis-1,3-Dichloropropene ug/L 48.050 96 60-140
Dibromochloromethane ug/L 50.250 100 60-140
Dibromomethane ug/L 47.350 95 60-140
Dichlorodifluoromethane ug/L 38.350 77 60-140
Diisopropyl ether ug/L 46.850 94 60-140
Ethylbenzene ug/L 48.350 97 60-140
Hexachloro-1,3-butadiene ug/L 54.350 109 60-140
Isopropylbenzene (Cumene)ug/L 47.250 94 60-140
m&p-Xylene ug/L 96.7100 97 60-140
Methyl-tert-butyl ether ug/L 45.950 92 60-140
Methylene Chloride ug/L 49.750 99 60-140
n-Butylbenzene ug/L 50.750 101 60-140
n-Propylbenzene ug/L 52.450 105 60-140
Naphthalene ug/L 50.550 101 60-140
o-Xylene ug/L 46.350 93 60-140
sec-Butylbenzene ug/L 53.850 108 60-140
Styrene ug/L 48.250 96 60-140
tert-Butylbenzene ug/L 51.350 103 60-140
Tetrachloroethene ug/L 48.650 97 60-140
Toluene ug/L 48.050 96 60-140
trans-1,2-Dichloroethene ug/L 48.850 98 60-140
trans-1,3-Dichloropropene ug/L 48.050 96 60-140
Trichloroethene ug/L 50.350 101 60-140
Trichlorofluoromethane ug/L 47.550 95 60-140
Vinyl chloride ug/L 44.950 90 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%96 70-130
Dibromofluoromethane (S)%95 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 18 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
917361MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92146489002
917362
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 106 60-140107 1 3020ND21.2 21.4
1,1,1-Trichloroethane ug/L 20 108 60-140106 2 3020ND21.6 21.1
1,1,2,2-Tetrachloroethane ug/L 20 102 60-140101 1 3020ND20.4 20.3
1,1,2-Trichloroethane ug/L 20 113 60-140115 2 3020ND22.6 23.0
1,1-Dichloroethane ug/L 20 113 60-140111 1 3020ND22.5 22.2
1,1-Dichloroethene ug/L 20 105 60-140105 0 3020ND21.0 21.0
1,1-Dichloropropene ug/L 20 113 60-140109 4 3020ND22.6 21.7
1,2,3-Trichlorobenzene ug/L 20 106 60-140112 6 3020ND21.1 22.4
1,2,3-Trichloropropane ug/L 20 100 60-140104 5 3020ND19.9 20.9
1,2,4-Trichlorobenzene ug/L 20 105 60-140110 5 3020ND20.9 22.0
1,2,4-Trimethylbenzene ug/L 20 105 60-140106 1 3020ND21.0 21.2
1,2-Dibromo-3-chloropropane ug/L 20 114 60-140116 2 3020ND22.9 23.2
1,2-Dibromoethane (EDB)ug/L 20 106 60-140106 0 3020ND21.1 21.2
1,2-Dichlorobenzene ug/L 20 105 60-140107 2 3020ND20.9 21.4
1,2-Dichloroethane ug/L 20 105 60-140104 2 3020ND21.0 20.7
1,2-Dichloropropane ug/L 20 113 60-140107 5 3020ND22.5 21.5
1,3,5-Trimethylbenzene ug/L 20 108 60-140109 1 3020ND21.6 21.8
1,3-Dichlorobenzene ug/L 20 104 60-140104 1 3020ND20.8 20.7
1,3-Dichloropropane ug/L 20 109 60-140112 2 3020ND21.8 22.3
1,4-Dichlorobenzene ug/L 20 104 60-140105 1 3020ND20.7 21.0
2,2-Dichloropropane ug/L 20 87 60-14085 3 3020ND17.4 17.0
2-Chlorotoluene ug/L 20 104 60-140105 0 3020ND20.8 20.9
4-Chlorotoluene ug/L 20 109 60-140110 1 3020ND21.8 21.9
Benzene ug/L 20 115 60-140115 0 3020ND22.9 22.9
Bromobenzene ug/L 20 111 60-140112 1 3020ND22.1 22.4
Bromochloromethane ug/L 20 94 60-14092 2 3020ND18.8 18.5
Bromodichloromethane ug/L 20 109 60-140108 1 3020ND21.8 21.5
Bromoform ug/L 20 106 60-140107 1 3020ND21.3 21.4
Bromomethane ug/L 20 83 60-14093 12 3020ND16.6 18.7
Carbon tetrachloride ug/L 20 112 60-140112 0 3020ND22.5 22.4
Chlorobenzene ug/L 20 109 60-140110 1 3020ND21.8 22.0
Chloroethane ug/L 20 125 60-140124 1 3020ND25.1 24.8
Chloroform ug/L 20 111 60-140101 10 3020ND22.2 20.2
Chloromethane ug/L 20 97 60-14097 0 3020ND19.4 19.4
cis-1,2-Dichloroethene ug/L 20 109 60-140104 5 3020ND21.9 20.9
cis-1,3-Dichloropropene ug/L 20 102 60-140104 3 3020ND20.3 20.9
Dibromochloromethane ug/L 20 110 60-140110 0 3020ND22.0 22.1
Dibromomethane ug/L 20 102 60-140105 2 3020ND20.5 20.9
Dichlorodifluoromethane ug/L 20 87 60-14086 2 3020ND17.4 17.1
Diisopropyl ether ug/L 20 106 60-140106 0 3020ND21.3 21.3
Ethylbenzene ug/L 20 109 60-140111 2 3020ND21.7 22.1
Hexachloro-1,3-butadiene ug/L 20 103 60-140109 5 3020ND21.0 22.1
Isopropylbenzene (Cumene)ug/L 20 106 60-140106 0 3020ND21.2 21.2
m&p-Xylene ug/L 40 112 60-140112 0 3040ND45.0 44.9
Methyl-tert-butyl ether ug/L 20 108 60-140100 8 3020ND21.5 19.9
Methylene Chloride ug/L 20 113 60-140114 1 3020ND23.1 23.3
n-Butylbenzene ug/L 20 104 60-140107 3 3020ND20.8 21.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 19 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
917361MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92146489002
917362
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 114 60-140116 2 3020ND22.7 23.2
Naphthalene ug/L 20 104 60-140107 3 3020ND20.8 21.5
o-Xylene ug/L 20 103 60-140105 3 3020ND20.5 21.1
sec-Butylbenzene ug/L 20 115 60-140118 2 3020ND23.1 23.6
Styrene ug/L 20 103 60-140106 2 3020ND20.7 21.1
tert-Butylbenzene ug/L 20 114 60-140113 1 3020ND22.8 22.6
Tetrachloroethene ug/L 20 110 60-140109 0 3020ND21.9 21.9
Toluene ug/L 20 107 60-140108 1 3020ND21.4 21.5
trans-1,2-Dichloroethene ug/L 20 112 60-140114 1 3020ND22.5 22.8
trans-1,3-Dichloropropene ug/L 20 103 60-140104 1 3020ND20.6 20.7
Trichloroethene ug/L 20 113 60-140109 4 3020ND22.6 21.7
Trichlorofluoromethane ug/L 20 105 60-140106 1 3020ND21.0 21.3
Vinyl chloride ug/L 20 101 60-140101 1 3020ND20.2 20.3
1,2-Dichloroethane-d4 (S)%94 70-130101
4-Bromofluorobenzene (S)%96 70-13095
Dibromofluoromethane (S)%96 70-130100
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 20 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 21 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92146489
Moody's Grocery #22446
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92146489001 MSV/21917WSW-1 SM 6200B
92146489002 MSV/21917WSW-3 SM 6200B
92146489003 MSV/21917WSW-4 SM 6200B
92146489004 MSV/21917WSW-5 SM 6200B
92146489005 MSV/21917WSW-6 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/08/2013 03:16 PM Page 22 of 22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]