WS-6081_22332_CA_MRP_20180813

MONITORING REPORT
TEXACO FOOD MART #2
17OO COTTON GROVE ROAD
LEXINGTON, DAVIDSON COUNTY, NORTH CAROLINA
INCIDENT NO. 22332
SHIELD PROJECT NO. 1001289
Contact:
David Holding
[phone]
Site Risk Classification: High Risk (H155D)
Land Use Category: Residential and commercial
Release Discovered: February 8,1999
Potential Release Source(s): Unknown
Site Latitud e: 3 5" 46' 47" Norlh
Site Longitude: 80"15'35" West
Quantity Released : Unknown
Release Cause: Unknown
David A. S
Senior
Responsible Party:
Techno, LLC for Holding
Brothers, Inc
P.O.Drawer 647
Concord, NC 28026
Consultant:
Shield Engineering, Inc.
4301Taggart Creek Road
Charlotte, North Carolina 28208
Contact:
Matthew T. Smith
[phone]
Property Owner:
United Oil of the Carolinas, Inc.
P.O. Box 68
Gastonia, Norlh Carolina 28053
Contact:
David Dulmage
[phone]
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Matthew T. Smith
Project Manager
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August 13,2018
Registered NC #
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TABLE OF CONTENTS
Paqe No.
1.0 DISCUSSION OF SAMPLING RESULTS
2.0 CONCLUSIONS 5
3.0 RECOMMENDATIONS
4.0 LIMITATIONS...
6
l
Figure 1:
Figure 2:
Figure 3:
Figure 4:
Figure 5:
Figure 6:
Figure 7:
Table 1:
Table 2:
Table 3:
Table 4:
Appendix A:
Appendix B:
LIST OF FIGURES
Site Location Map
Site Map
1500' Radius Map
Groundwater Elevation Contour Map
Benzene Isoconcentration Map
1,2-Dichloroethane (DCA) Isoconcentration Map
Ethylene Dibromide (EDB) Isoconcentration Map
LIST OF TABLES
Summary of Adjacent Property and Water Supply Well Owners
Summary of Well Construction and Historical Groundwater Elevation Data
Summary of Analytical Results - Groundwater Samples
Summary of Historical Analyical Results - Groundwater Samples
APPENDICES
Advanced Environmental Services, Inc. - MMPE Reporl
Laboratory Report - Groundwater Samples
H:\Projects\2000\l 00 I 289 - TFM#2\Reports\20 1 B-07\MR July 20 I B.doc
Texaco Food Mart #2
Lexington, Davidson County, North Carolina
Incident#:22332
Monitoring Report
August 13,2018
Page I
1.0 DISCUSSION OF SAMPLING RESULTS
1.1 Site Monitoring Requirements:
Site Location Map.
Site Map:
See Figure I
See Figure 2
Site Monitoring Requirements
Based on CAP and/or NORR
Sample Point
Type
Total Quantity of Previous
Sample Points and Their
Identification
Required by NCDEQ to be
Monitored and Sampled per CAP
and/or TA
Monitoring
Wells
10
(MW-1 through MW-6, and T-1
throueh T-4)
6 (t)
(MW-l through MW-5 and T-1)
Water Supply
Wells
13 tt)
(WSW-1 through WSW-I3)
0
(I) Individual wells identified by the North Carolina Department of Envtronmental Quality (NCDEQ) for specific
sampling at this time.
(2) Number ofwells located within 1,500 feet of site.
1.2 Summary of Analytical Results and Free Product Thickness(s):
1.2.1 Date(s) of Sampling Evenl:. June 19, 2018
1.2.2 Existing Area Receptors:
A receptor survey was conducted in 2001 as presented in the CSA report datedMay 2002
and the CAP dated October 2003.
Refer to the following Tables and Figure(s) for information and locations of area receptors
identified.
R"f", to Figure(s).' Figure 3
R"f", to Tables(s): Table I
7.2.3 Groundwater Flow Direction:
The groundwater flow direction is to the east-southeast, which is a gradual shift from
prior years which showed a flow direction of north-northeast.
Current andlor Historical Groundwater Elevation Data are included in the following Table
and Figure:
a
Rqfer to Table:
Rqfer to Figure
Table 2
Figure 4
Texaco Food Mart #2
Lexington, Davidson County, North Carolina
lncident#:22332
Monitoring Report
August 13,2018
Page 2
1.2.4 Free Product/Impacted Groundwater Recovery:
Free product detected during this reporting period?: No
Free product plume size and location:Not Applicable
Proximity of plume to nearest receptors Not Applicable
Free product recovered during this period:Not Applicable
Free product recovery method:Not Applicable
Impacted groundwater recovery during this reporting period?: Yes, aweeklongMobile
Multiphase Extraction (MMPE) event was conducted between July 9 and July 13,
2018. Free product was not detected at the beginning or conclusion of the MMPE nor
has it ever been detected at the site.
Impacted groundwater recovered during this period: A total of 1,588 gallons of
dissolved phase impacted groundwater were recovered during the aforementioned
MMPE event, plus an estimated 2.38 gallons (based on mass-removal calculations) of
volatile organic compounds (VOCs) as vapor were recovered during this period. Refer
to Appendix A.
a
o
a
a
a
a
a
a
a
Impacted groundwater recovery method: One 96-hour MMPE event (July 9 through
July 13, 2018). Refer to Appendix A.
1.2.5 Groundwater Analytical Results:
Sampled Points and Analytical Methods
The following monitoring wells and other points were sampled during this reporting
period.
Sampled Points and Analytical Methods
for this Reporting Period
Based on CAP and Pre-Approval Task Authorization Sampling Requirements
Type Points Sampled during this
Reporting Period
Analytical Methods
Monitoring
Wells
(6; r'r
(MW-l through MW-5 and T-l)
r EPA Method 62008
(l) Pre-Approval Task Authorization TA-22332-1 9
Texaco Food Mart #2
Lexington, Davidson County, North Carolina
lncident#:22332
Monitoring Report
August 13,2018
Page 3
o Laboratory Used: Pace Analytical Services Inc. Huntersville, NC
o Current GroundwaterAnalyticalData:
On June 19,2018, groundwater samples were collected from monitoring wells MW-l
through MW-5 and T-1. One or more concentrations of VOCs including benzene,
ethylbenzene, toluene, total xylenss, methyl tert-butyl ether (MTBE), naphthalene,
isopropylbetuene)n-propylbenzene, 1,2-dichloroethane (1,2-DCA), 1,2-dichloropropane,
ethylene dibromide (EDB), diisopropyl ether (IPE),1,2,4-trimethylbenzene, and 1.3.5-
trimethylbenzene were detected at concentrations above the 15,A' NC AC 2L Groundwater
Standards (2L Standards) in wells including MW-l, MW-2, MW-3, MW-4, and T-1.
Concentrations of analytes including benzene,1,2-DCA, and EDB were detected above
the North Carolina Department of Environmental Quality (NCDEQ gross contaminant
levels (GCLs) in MW-2, which are the applicable standards for this site.
Refer to the following Table and Appendix for current groundwater analytical data.
Refer to Figures
R"fe, to Table:
Rqfer to Appendix.
Figures 5 through 7
Table 3
Appendix B
a Historical Groundwater Analytic al D ata:
Total dissolved phase petroleum concentrations in monitoring wells MW-1, MW-2,
MW-3, MW-4, and TW-l have decreased in comparison to the November 2017 data.
Total dissolved phase petroleum concentrations in monitoring wells MW-1, MW-2,
MW-3, and MW-5 have decreased since the early stages of the project. The plume may
be attenuating east toward downgradient MW-4 and vertically toward T-1. No dissolved
phase petroleum concentrations have been detected at or above the laboratory detection
limits in monitoring well MW-5 since the March 2009 sampling event.
Refer to the following table(s) for historical groundwater analylical daIa.
R"f", to Table(s)Table 4
a Dissolved Phase Plume Size and Location
The on-site dissolved phase plume is oval shaped and has an approximate length of 94
feet and width of 41 feet based on the benzene concentrations above 2L Standards. The
dissolvedphase plume that is above the NCDEQ GCLs, the applicable standards forthis
site, is approximately 12 feet in length by 7 feet in width (Figure 5). The plume maps for
constituents that are above the GCLs are shown on the following figures.
Refe, to Figure(s) ' Figures 5 through 7
Texaco Food Mart #2
Lexington, Davidson County, North Carolina
lncident#:22332
Monitoring Report
August 13,2018
Page 4
o
a
Proximity of Plume to Nearest Receptor(s)
Based on the receptor survey conducted in 2}}l,there were three (3) confirmed drinking
water supply wells and six (6) inactive supply wells located within 1,000 feet of the
source area. The closest drinking water supplywell (WSW-1) is located approximately
450 feet south (hydraulically upgradient) of the site. No surface water bodies were
observed in the field or on the topographic map within 500-feet of the source area.
R"fe, to Figure
R"f", to Table:
Figure 3
Table 1
Predictive Rate of Contaminant Transport:
The contaminant plume has been fairly stable or immobile over the past several years,
and in general reducing in concentration.
Ref", to Table(s): Tables 2 through 4
1.2,6 Other Field Data Collected:
o No additional field data was collected.
Texaco Food Mart #2
Lexington Davidson County, North Carolina
lncident#:22332
Monitoring Reporl
August 13,2018
Page 5
2.0 CONCLUSIONS
o Free product was not detected in site wells during this reporting period.
o Dissolved phase petroleum constitusnt compounds were detected in concentrations above
2L Standards in monitoring wells MW-1 through MW-4 and T-1.o Dissolved phase concentrations of benzene, 1,2-DCA, and EDB were above the NCDEQ
GCLs in MW-2.
r Total dissolved phase petroleum constituent compound concentrations decreased in
monitoring wells MW-l, MW-2, MW-3, MW-4, and TW-l since November 2011.
o Total dissolved phase petroleum concentrations in monitoring wells MW-l, MW-2,
MW-3 and MW-5 have decreased since the early stages of the project.
o The plume may be attenuating east toward downgradient MW-4 & vertically toward T- 1 .
o MW-5 continues to show non-detect levels of contamination.
. After the sampling event, an MMPE event was conducted recovering a total of 1,588
gallons of dissolved phase impacted groundwater and2.38 gallons of gasoline as vapor.
. In 200I, three (3) privately owned drinking water supply wells were identified within a
1,000-foot radius of the source area with the nearest confirmed drinking water supply
well approximately 450 feet hydraulically upgradient from the source area.
o Based on a conversation with the former incident manager, Michael Rogers of the
NCDEQ on November 16,2010, since WSW-1 is approximately 450 feet upgradient of
the site and the property owner would not allow Shield or NCDEQ to sample their supply
well, the Texaco Food Mart #2 site would likelybe reduced to low risk if soil excavation
was completed to remove as much soil as feasibly possible in the area of SB-8 and if
MW-2 groundwater concentrations were below GCLs.
. Soil excavation around boring SB-8 was conducted on February 28, 2012 via over
drilling with i4-inch outside diameter hollow stem augers around the SB-8 boring.
Details of the excavation were previously submitted to the NCDEQ in the Monitoring
Report dated October 23,2012.o The contaminant plume above the applicable GCLs remains only approximately 12 feet
in diameter and located near the western gasoline dispensers.. Overall, the contamination at the site has graduallybeen cleaning up by soil removal, air
sparging, MMPE events, and attenuation processes.
Texaco Food Mart #2
Lexington Davidson County, North Carolina
lncident#:22332
Monitoring Report
August 13,2018
Page 6
a
o
a
o
3.0 RECOMMENDATIONS
It has been recommended by Shield that bi-weekly air sparging be conducted to reduce
the groundwater concentrations to below GCLs, with NCDEQ agreement. This activity
has not been agreed upon recently with the NCDEQ.
Since the plume above the GCLs is only approximately 12 feet in diameter, Shield
recommends continuing semi-annual Mobile Multi-Phase Extraction (MMPE) events at
the site in order to expedite cleanup to below the GCLs.
Shieldrecommends conducting a sampling event following an MMPE event in January
2019.
Once MW-2 is below the GCLs, a "no further action" determination should be requested
from the NCDEQ.
Texaco Food Mart #2
Lexington Davidson County, North Carolina
lncident#:22332
Monitoring Reporl
August 13,2018
Page 7
4.0 LIMITATIONS
Shield has performed environmental services at the subject site on behalf of Techno LLC for Holding
Brothers, Inc. Shield has performed this scope ofwork as an independent contractorlconsultant using
reasonable care and skill in accordance and consistent with customary industry standards of
engineering, geology, and hydrogeology practices. This standard of care is the sole and exclusive
standard of care that can be applied to measure Shield's performance of the work. No other
warranty, expressed or implied is made or intended by Shield.
The report has been prepared for the exclusive use by Techno LLC for Holding Brothers, Inc. All
recommendations, findings, and conclusions, made by Shield have been made to the best of Shield's
knowledge, opinion and belief, based upon information obtained during this scope of Techno LLC
for Holding Brothers, Inc. and Shield. Conclusions are provided with the understanding that Shield
is presenting information and not rendering legal advice. If such advice is needed, legal counsel
should be consulted. It is the responsibility of Techno LLC for Holding Brothers, Inc. under advice
of its counsel to notify the appropriate federal, state, or local public agencies as required by law; or
otherwise to disclose in a timely manner, any information that may be necessary to prevent damage
to human health, safety, or the environment.
Compliance with recommendations provided as part of this report in no way assures compliance with
federal, state and/or local laws, regulations , and/or requirements. Analytical datahas been obtained
from Pace Analyical Services Inc. andAdvanced Environmental Services,Inc. This information, to
the extent that it was relied on to generate this report, is assumed to be correct and complete. The
work performed in conjunction with this report and the data developed are intended as a description
of available information at the dates and specific locations given. Shield is not responsible for
inspecting, examining, or reporting findings or recommendations with respect to any conditions that
were knowingly or unknowingly withheld, concealed, hidden, or in any way not disclosed or
observable at the time of this scope of work.
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SH|ELD # 1001289
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LEXINGTON, NORTH CAROLINA
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^={$Foffi !oorrnrr^ oorr*rr*!DISPENSER
.Soffi o
od.U
odt'
z.o
l-ou
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UFfoduz.
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GASOLINE UsT
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zo
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#€qdN(
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ELss nono CEDAR LANE ROAD O remp-r
(Ns)
LEGEND:
+ LTGHTPoLE
/ powER poLE
ELECTRICAL LINE
SANITARY SEWER LINE
PRODUCT LINE
e TEXACO FOOD MARTMONTTORTNG WELL
O TEMco FooD lvlART DEEP MoNtroRlNG WELL
WENDYS PROPERTY
MW-5
ND}
o AMOCO RUSHCO #3 MONITORING WELT
ALL DATA TAKEN FROM THE PHAsE II LIMITED SITE ASSESSMENTREPORT PREPARED BY C8M ENVIROMENTAL SERVICES, INC.DAIED 4t16tO1.
E VE VAPOR EXTRACTION WELL
E A5 AIR SPARGING WELL
(ugll) MICROGRA 45 PER LITER
(885) 1,2'DICHLOROETHANE(DCA)CONCENTRATION(ugll)
[198] 1,2-DICHLOROETHANE (DCA) CONCENTMTION NOT USED lN CONTOURING (ugll)
-
1,2-DICHLOROETHANE (DCA) ISOCONCENIRATION LINE (ug/L)
1,2-DICHLOROETHANE (DCA) ISOCONCENTRATION LINE (ugll) EXCEEDING GROSS CONTAMIMNT LEVELs (GCts)
(ND) NOT DETECT . BELOW LABOMTORY A{ETHOD DETECTION L]AIITS
(NS) NOT SAMPLED APPROXIMATE GRAPHIC SCALE
0 15 t0
AMOCO
RUSHCO #3
NOTES:1- CROUNDWATER SA}I\PLES COLLECTED ON 6/19l18.
2- ALL LOCATIONs ARE APPROXIMATE.
3, CONTOUR INTERVALs AS sHOWN.
PARKING AREA
SCALE: I in. = 30 ft.FIGURE : 6
(,
=od
€
d
a
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udf(ftr
N
=LF
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oo
ooaN
FUUoda
I
I s H I E L D 3'"xi's",efJ."?il%*-
sw.shieldcryin*drylmtNc.
ETHYLENE DIBROMIDE (EDB)
ISOCONCENTRATION MAP '
TEXACO FOOD MART #2
17OO COTTON GROVE ROAD
LEXINGTON, NORTH CAROLINA
SH|ELD f 1001289
DATE: 8/7/18 DRAWN BY : MTS
SCALE : AS SHOWN FIGURE : 7
F
=
!!o
ASPHALT
oMW-3
(ND)
AS-6x
!
:
ac
A5-5Exo ovE.6 -t-4 YE7(Ns)
REGULAR
U5T
REGULARUST
5UPREftE
UST
5UPREilE
UST
TANK PIT
TEXACO
FOOD MART
6IIo{
o
(ND)
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f'.$o)KEROSENE
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(Ns)
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,UW-g O
(Ns)
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N DISPENSER orserrsrn!
oortnrr^!
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z
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(Ns)MW-1(Ns)
^So.5t*-€qdA4(
^S"ffi
ACCEsS ROAD CEDAR LANE ROAD O ra*p-r
(Ns)
LEGEND:
+ LTGHTPOLE
6 PowER PoLE
ELECTRICAL LINE
SANITARY SEWER LINE
PRODUCT LINE
O TDGco FooDMARTMoNtToRtNG WELL
6 TEXAco FooD MART DEEP MoNlroRrNG WELL
WENOYS PROPERTY
MW-5
o AMOCO RUSHCO #3 MONITORING WELL
ALL DATA TAKEN FROM THE PHASE II LIMITED SITE ASsESSMENT
8E?q8T PREPARED BY CBM ENVIROMENTAL 5ERVICES, INC.DATED 4t't6tO1-
O VE VAPOR EXTMCTION WELL
X AS AIR SPARGINC WELL
{ug/L) MICROGRA.t5 PER LITER
(565) ETHYLENE DIBROMIDE (EDB) CONCENTMTION (UglL}
IND] ETHYLENE DIBROTiIDE (EDB) CONCEIITRATION NOT USED lN CONTOURING (ug/L)
ETHYLENE DIBROMIDE (EDB) ISOCONCENTMTION LINE lug/L)
ETHYLENE DIBROMIDE (EDB) ISOCONCENTRATION LINE (ugll) EXCEEDING GRO55 CONTA {IMNT LEVELS (GCts)
(ND) NOT DETECTED - BELOW LABORATORY METHOD DETECTION LIMITs
(NS) NOT SAMPLED
APPROXIMATE GMPHIC SCALE
0 15 30
AMOCO
RUSHCO #3
NOTES:1 GROUNDWATER SAA,IPLES COLLECTED ON 6/19/1E,2 ALL LOCATIONS ARE APPROXIMTE.] CONTOUR INTERVATS AS sHOWN.
PARKING AREA
SCALE: 1 tn- = l0 ft.
Table: 1Summary of Adjacent Property and Water Supply Well OwnersTexaco Food Mart #21700 Cotton Grove Road,Lexington, North CarolinaNCDENR Incident # 22332PublicWaterSystemhook upNoYesYesNoYesYesYesNoYesUnk.Unk.YesNoDistancefromsource areaof release(ft.)4s0'700'650'985',7s0'760''79s',1025',1 090'I 100'117 s',800'850'WellScreenIntervalfttoyft.BGS),|,|2,)?,|?????,|?WellCasingDepth(ft. BGS),)??I2,),),|?,)???TypeofWell4"???2?,|4"?,)??IWellDepth(ftBGS)185?,)?,|?,)>100?I,)?,)Well UseDrinkingNot in UseNot in UseDrinkingNot in UseNot in UseNot in UseDrinkingNot in UseNot in UseNot in UseIrrigationDrinkingPhoneNumber336-3s7-2511336-357 -5231336-3s7 -2659336-357 -2916336-249-3266336-357-248s336-357-2565NANANANANANAAddressP.O. Box 284 Lexington, NC104 Fuller Rd., Lexington, NC106 Fuller Rd., Lexington, NC115 Cedar Ln., Lexington, NC6 Mayfair Rd., Lexington, NC*Box 8 Mayfair Rd., Lexington,NCBox 100 Mayfair Rd.,Lexington, NCBox 108 Mayfair Rd.,Lexington, NCBox 107 Mayfair Rd,Lexington, NCBox 103 Mayfair Rd.,Lexington, NC1724 Southview Rd.,Lexington, NC102 Mayfair Rd., Lexington,NC104 Mayfair Rd., Lexington,NCWell Owner/ User (indicatewhich)Flowerest O. LoppPaul & Stella BakerMargaret H. FullerHoyle R. SmithEfird E. Jr. & Kay SWilson(owner)Abe CassidyMrs. Samuel C. DavisMaxine C. HouckThomas FrankJames G. HendersonRay S. & Irene MusgraveAubrey & Helen BrewerJohn T. TetterWell #WSW-Iwsw-2wsw-3wsw-4WSW-5WSW-6WSW.7wsw-8wsw-9WSW-IOWSW-I Iwsw-12wsw-13Notes: Ft BCS = feet below ground surface- Address of well. Property owner's addr-ess is 500 Maegeo Dr., LexingtonOf the property owners without PWS hook ups, only .lohn Tetter is interested in be added to the PWS. Other property owners indicated that they are not interested at allNA - Not AccessibleHlProjects\2000\1001289 - TFM#2\Repofis\ARMR Aug 2014\Water Supply Well Information Table.doc
Table 2:
Summary of Well Construction and Historical Groundrvater Elevation Data
Texaco Food Mart#2
1700 Cotton Grove Road, Lexington, North Carolina
NCDENR Incid ent # 22332
WcII ID Date
lnstalled
Top of
Casing
Elevation
(feet)
Well
Diameter
(inches)
As-built
Depth
(fect)
Screened
Interval (feet)
Field Measurements Field Calculations
Gauging Date
Total
Depth
(feet)
Depth to
Static
Water
(feet)
Depth to
Free
Product
(feet)
Diff. Betrveen
As-Built and
Measured Total
Depth (feet)
Ground-water
Elevation
(feet)
MW-t 07 / 3t t0t 100.00 2 35 20-35 t0/t 0/01 35.00 24.09 NA 0 7 5.91
r4t22/02 3s.00 22.13 NA 0 'I t.Et
tut9to't 35.01 23.69 NA -(.).0 I 76.1t
u3t04t09 34.93 19.68 NA o.ol 80.32
wt19/13 35.07 t7.55 NA -0.07 82.4s
u7nln4 35.0./I L32 NA -(.1.07 E2.66
05t20^5 15.{t7 I 8.60 NA -0.07 8l.40
03t21t16 35.07 16.48 NA -0.07 83.52
$t1{v17 3s.07 20.08 NA -0.07 t9.92
tlt16n7 35.07 22.6t NA -0.07 77 ..t9
06/l 9/18 35.07 l 8.88 NA -o.07 8t.t2
MW-2 07/3t/0t luu.l9 2 J)2U-35 r ui r u/ut J5,UU '24.22 NA U 't5. tE
04tzztuz -15_00 22.08 NA 0 17.92
tr/t9t[7 34.75 23.84 NA 0.25 16.35
03/04t09 34.65 19.62 NA 0.35 80.57
t)6tzan2 34.9 t I E.4E NA u.09 E I,7I
07n9n3 '14.94 17.53 NA 0.06 82.66
07nl/14 34.94 t7.28 NA 0.06 82.91
05/20/15 34.94 18.65 NA 0.06 81.54
u3/21fi6 34.t)4 I 6.61 NA 0.06 ti-J.5u
05n0t17 34.94 20.26 NA 0.06 79.93
tl/16t17 34.94 22.95 NA 0.06 77.24
06/19n8 34.94 19.04 NA 0.u6 E l.l5
MW-3 I o/oxiu I l0u.l9 2 :15 20-35 I 0/l 0/01 35.00 24.27 NA 0 75.92
04t22t02 35.00 2t.93 NA 0 18.26
t1n9/07 J5.UJ 24.t0 NA -0.0J '16-0r)
u3t04t09 '34.96 19..J5 NA 0_04 ti0.lJ4
07n9n3 35.08 t1.23 NA -0.08 82.96
07nln4 35.08 17.05 NA -0.08 83.1 4
u5r2wl5 J5.OE I E.4E NA -0.0E 61.71
tJ3tzl^6 15.0t{t6.ll NA -0.08 83.88
05/l 0/l 6 35.08 20.t0 NA -0.08 80.09
tln6n7 3 5.08 23.09 NA -0.08 I I .ItJ
u6/l 9/l E 35.0u I E.96 NA -0.0u 8l.21
MW-4 I 0/()t{^) I 99.40 2 35 20-35 10/10/01 35.00 24.11 NA U /6.UU
04122102 J5.OU 2t.9 t NA 0 'tE.2E
lUt9/Lt1 :t4.lJ I 2l.lJli NA 0. l9 7 5.52
03/04iltg 34.74 19.90 NA 0.26 79.50
07/20t10 34.72 18.57 NA 0.28 EU.EJ
07^9n-t '34.91J t].90 NA 0_ I0 u l .5()
ll7 t11/l4 34.90 11.60 NA 0.10 81.80
05t20/t5 34.90 I 8.66 NA 0.l0 80.74
03tzt/16 34.9tJ I6.JE NA u. l0 E3.02
0il10/L7 14.9t)7{1.02 NA 0. l0 19.38
ll/l6t17 34.90 22.86 NA 0. l0 '7 6.54
06/19n8 34.90 r8.8r NA 0. tu EU.59
MW-5 04t04/02 I (X).1 9 2 35 20-15 04tzzt0z 35.00 23.34 NA 0 76.85
t1n9/07 35.07 24.76 NA -0.07 75.63
03t04/09 J5.09 2t.n NA -0.09 19.22
07 /t9^3 :\5.12 t9.02 NA -0.12 81 .37
07nln4 35.12 I 8.78 NA -0.12 8l .61
05t20ns 35.t2 r9.90 NA -{J.12 E0.49
ti3tzUl6 J5.12 t7.19 NA -0.'t2 t{2.60
05ntvl7 35.12 21.05 NA -0.12 79.34
11n6/17 35.12 23.01 NA -0.12 77.38
06n9/18 35.12 19.09 NA -tJ.I 2 EI,JO
Sum of well conslruclion and histoical groundwater elevation
Summary of Well Construction and Historical Groundrvater Elevation Data
Texaco Food Mart #2
1700 Cotton Grove Road, Lexington, North Carolina
NCDENR Incident# 22332
Field Measurements Field Calculations
Well ID Date
Installed
Top of
Casing
Elevation
(feet)
Well
Diameter
(inches)
As-built
Depth
(feet)
Screened
Interval (feet)Gauging Date
Total
Depth
(feet)
Depth to
Static
Water
(feet)
Depth to
Free
Product
(feet)
Diff. Between
As-Built and
Measured Total
Depth (feet)
Ground-water
Elevation
(feet)
04/22t02 25.00 23.02 NA 0 77 .17
tt/19/07 25.00 NM NA 0 NM
tJ3/U4t09 NM NM NM NM NM
MW-6 04/04/02 tol.42 2 25 t5-25
IO/lU/t l 9U.UU t4.93 NA U t5.26
u4tzztuz 90.u(,'22.O6 NA U 7E.t3
tln9/(17 86.71 2t.5t)NA 3.29 78.76
03/04t09 65.82 19.52 NA 24.t8 80.83
07/19/13 66.84 1 8.14 NA 2J.T6 62.2t
07ilUt4 66.E4 I E.5ti NA 2t.16 lit.77
tJst20n5 66.84 I9.36 NA 23.16 80.99
03t21/16 66.84 17.08 NA 23.16 83.27
u5iLon7 66.E4 '20.oJ NA 23.t6 60.32
lt/t6n7 66.u4 2',.\.51 NA 23.t6 76,84
06/19n8 66.84 t9.02 NA 23.t6 8l.33
T-1 10/09tol 100.35 2 90 85.5-90
l. NM:NotMeasured
2. NA: Not Applicable
Pnga 2 of2Sum of well conslruction and historical groundwaler elevation
Table 3:Summary of Analytical Results-Groundwater SamplesTexaco Food Mart #21700 Cotton Grove Road, Lexington, North CarolinaNCDENR Incident#22332Notes:ug^ = Micrograms per liter. ND = Below Method Detstion LimitNR = Analysis not requested. Bold numbers exc€d l5A NCAC 2L.0202 sradards.I5A. NCAC 2L.0202 = NCDEQ Standad Statute for non-risked boed mqimum allowable contaiment concentration in groundwaterIlqlicized Bold n\mber exced Gross Contaminant Levels = As presented in NCDEQ "Guidelines for Assessmflt and Cotrective Action," Iot revised Decmber I201 3EPA Method 62008X50085,500rsll,642r4,6807,970NDNDNDF40025,000rq/l,t7.4613570NDND12.8NDF40028,500rolL3032,4402J00NDND'16NDF600260,000rp/1,76.323,8001,230NDND2ND7030,000tslL40. I261334NDND3.6NDz66,000te/L99.31,010724NDND44.4NDrc2020,000usll,4.23,8r0ND242ND4.3ND6a702s,000rsll,24.9ND116NDND3.6NDa60084,500rsll,tt723701,400NDND'13.7ND7070,000rplLND131NDNDND19.5ND0.6600tsll,NDNDNDNDND4.2ND0.4400rpll,IuNDNDND198NDe0.0250tplLNDi65NDNDNDNDND7070,000nell,7.8N'DND34.6NDNDND5,000tell,86.69,78023NDND580NDAnalytical Method-->r5A NCAC 2L.0202Saandard-->lsA NCAC 2L.0llsGross Contaminationlev€l-->06/t9/1806/19/t806/t9/1806/1911a06/19/1806/19/1806/1911aMW-lMW-2MW-3MW-4MW-5T-lTrip BlakH:vrcjet*@\1401289 - TFW2RepbU1lCoreun ol Cnert Gw AnatydcdPage 1 of 1
Table 4:
Summary of Historical Analytical Results-Gloundwater Samples
Texaco Food Mart #2
1700 Cotton Grove Road, Lcxington, North Carolina
NCDENR Incident #
Atralytical Method--->EPA Method 601/602
EPA
Method
504,1 or
62008
EPA
Method
625 or
6200B
MADEP
VPH
MADEP VPH &
EPH
MADEF
EPH
MADEP VPH &
EPH
F
ts]
x
F
E]
F]
.l
z
ri
!z
d
()
il
(J
U
o
il
I
a
q
()
d.o
:
il
d
Q
5
il
o
(J
l5A NCAC 2L.0202
Standard--->I 600 600 500 0.4 70 20 0.02 6 400 700 10,000 200
l5A NCAC 2L.01 15
Gross Contnmination 5,000 260,000 84,500 85,500 400 70,000 20,000 50 6,000
roll,rs/J,tsll,rslL ralL lplL nplL tplL npll,'1,
MW-l 07l3v0t ND 53 340 1,300 ND NR NR 0.96 15 ND 3,410 ND 2,780
o4l30l03 t2 340 l3 1,470 ND ND NR NR 210 NR NR NR NR
1vt9t0'1 49.5 64.7 r79 1,210 ND ND ND ND r07 ND 665 ND 825
03t04/09 53.7 28.4 165 827 ND ND ND ND 161 468 6,170 NI)2,200
07119113 69,4 87.4 t2t 761 ND ND 7.4 ND ll4 NR NR NR NR
o7/tut4 77,2 t0l t32 190 ND ND ND ilt NR NR NR NR
0sl20lts 93.2 ll3 145 816 ND 5.2 0.63 t43 NR NR NR NR
031211t6 a2.7 '12.9 ll9 658 ND 4.4 ND 99,3 NR NR NR NR
05n0/17 126 lt9 164 899 3,6 ND 3.6 ND 120 NR NR NR NR
tllt6lt'l 168 t82 195 1,03?ND ND 4 ND t38 NR NR NR NR
06lt9ll8 86.6 76.3 |7 682 ND 4.2 ND 99,3 NR NR NR NR
MW-2 0713v0t 13,000 38,000 3,600 16,000 1,200 NR NR 720 NR 81,000 28,000 NR 9,100
04130103 12,000 29,000 2,800 16,700 1,700 ND NR ND 1,400 NR NR NR NR
tt/ t9/07 14,900 34,200 3,090 18,400 1,1 50 ND 6,090 ND t,090 60,100 71,600 308 26,630
03t04109 I 1,700 27,200 2,250 r4,500 ND ND 3,600 ND 238 59,300 58,930 ND 8,340
06t28t12 8,930 17,800 t,160 10,9s0 1,090 144 1,420 635 974 NR NR NR NR
0'rlr9t13 12,600 24,300 2,200 13,380 1,330 194 7,550 773 1,260 NR NR NR NR
o7111114 10,800 21,300 1,910 11,980 1,210 142 7,040 663 1,070 NR NR NR NR
05120/15 6,41 0 12,600 989 6,460 713 90,9 4,830 451 898 NR NR NR NR
03/2u16 I I,3oo 22,700 2,170 13,200 1,090 154 6,240 677 I,t00 NR NR NR NR
05/t0lt7 13,600 29,200 2,770 16,210 1,330 l8t 6,620 706 l,180 NR NR NR NR
tu16ll'1 I I,ooo 24,t00 2,410 14,760 910 163 5,320 621 t,080 NR NR NR NR
06/19/r8 9,780 23,800 2,370 t4,680 885 l3l J,810 565 I,0r 0 NR NR NR NR
MW-3 l0i l0/01 120 4,300 l,8oo 8,600 ND NR NR 9.5 360 ND r 1,990 ND ll,7t0
04/30103 t00 3,000 r,600 8,800 ND ND NR NIJ 660 NR NR NR NR
tv19l07 ND 4,850 2,190 13,600 ND ND ND 1.2 513 NR 3460 ND 2,440
07/04109 ND 3,430 2,090 11,400 ND ND ND ND t,520 5,560 40,926 ND I l,?80
07lt9lt3 22 t,250 1,420 8,060 NT)ND '1 3 ND 744 NR NR NR NR
07ltUt4 55.t I,t00 t!300 7,270 ND ND ND ND 831 NR NR NR NR
05120/15 17.2 954 1,250 6,7t0 ND ND 9.4 ND 88t NR NR NR NR
03l2Ut6 l1 854 t,090 5,8?0 ND ND ND NT'632 NR NR NR NR
05lt0lt7 21.6 t,630 t,680 9,510 ND ND ND ND 844 NR NR NR NR
1l16lt7 35.8 1,340 1,490 8,580 ND ND ND ND 8ll NR NR NR NR
06119118 23 t,230 1,400 7,970 ND NT)ND NIJ 724 NR NR NR NR
MW-4 l0/10/01 ND ND ND ND ND ND NR ND ND NR NR NR NR
04130103 ND Nt)Nt)ND ND NI)NR NR ND NR NR NR NR
t1/t9/07 ND ND ND ND ND ND 2.3 ND ND ND ND ND ND
03104/09 ND 5.2 ND il.6 ND ND 4.3 ND 12.3 ND t86 ND ND
07120/to Nt)ND ND ND ND ND 87 ND ND ND ND ND ND
07lt9lt3 1.9 ND ND 4.6 ND ND 40 ND ND NR NR NR NR
07ltUt4 2,7 ND ND ND ND 65.9 ND ND NR NR NR NR
05l20lts 2.7 ND ND 6.7 ND ND 106 ND ND NR NR NR NR
03l2ll t6 2.8 ND ND 6.4 ND ND ll6 ND ND NR NR NR NR
051r0117 3.6 ND ND 9.3 ND ND 213 ND ND NR NR NR NR
H:Prc1actsv00011001289 - TFW2AapnsVol &oreun ol HISTORICAL GW Anawcd Page 1 of 2
Analylical ltlelhod---->EPA Method 601/602
EPA
M€thod
504.1 or
62008
EPA
Method
625 or
62008
MADEP
VPH
I,IADEP VPH &
EPH
MADET
EPH
M.\DEP VPH &
EPH
t0 F
Q
X
F
II
l'l
!
ta
a
H
z
U
O
5
il
o
o
a
il
O
O
()
O
g
il
ol
U
il
()
(,)
r5A NCAC 2L.0202
Slandard---->600 600 500 0.4 70 20 0.02 6 400 700 10,000 c+d=
200
rsA NcAc 2L.0il5
Gross Contamination
level--->
5,000 260,000 84,500 85,500 400 70,000 20,000 50 6,000
Location Date wlL us/L ur/L tslL u!/L wlL us/L tplL wlL U!/L ug/L nxlL tslL
MW-4
CONT
1!/t6/17 1.2 ND ND ND ND ND 261 ND ND NR NR NR NR
06/t9lt8 ND ND ND ND ND ND 242 ND ND NR NR NR NR
MW-5 04t30/03 ND ND ND ND ND NR NR NA ND NR NR NR NR
lt/19/07 ND ND ND ND ND ND ND ND 4l 144 ND ND ND
01t04109 ND tg ND ND ND ND ND ND 2.9 NI'ND NI)ND
01 / t9/ t3 ND ND ND ND ND ND ND ND ND NR NR NR NR
07lt I lt4 ND ND ND ND ND ND ND ND ND NR NR NR NR
05t20/15 ND ND ND ND ND ND ND ND ND NR NR NR NR
03t21716 ND ND ND ND Nt)ND ND ND ND NR NR NR NR
05l10lt'?ND ND ND ND ND ND ND ND ND NR NR NR NR
It/16il'1 ND ND ND ND Nt)ND ND ND ND NR NR NR NR
06/t9/t8 ND ND ND ND ND ND ND ND ND NR NR NR NR
T-l I 0/l 0/0 l 390 7.8 9.4 t40 44 NR NR 2.8 24 8s0 270 ND 2s0
04t30/03 l7 2.8 ND 14.',l 8.1 ND NR ND 3.r NR NR NR NR
1l/t9/0'1 43.8 ND ND ND 1.1 ND 210 ND ND ND ND ND ND
03/04t09 20.7 ND ND ND 25,7 ND ND ND t4.4 320 ND ND ND
07/19/13 135 30.6 6.2 27.t 23.9 2.4 83 ND 7-7 NR NR NR NR
07/1114 172 0.59 5.5 13.3 43.7 2.8 2.1 ND 3.9 NR NR NR NR
05t20/15 il5 0.s4 1.5 16.2 43.9 3.2 Ll ND NR NR NR NR
03/2t/t6 t8.5 ND 0.58 ND l0.l 0.78 ND ND ND NR NR NR NR
0s/t0il7 117 0.s3 15.3 29.6 2A t.'7 ND ND 6.8 NR NR NR NR
I vt6lt7 3,120 t3.l 585 1,423 321 25 _7 ND ND 253 NR NR NR NR
061191 ta s80 2 71.'7 t2'7.6 198 19.5 41 ND 44.4 NR NR NR NR
Table 4:
Sunrnrary of Ilistorical Analytical Results-Groundlvater Sanrples
Texaco Food Mart #2
1700 Cotton Grove Road, Lexington, North Carolina
NCDENR lncident # 22332
Notes:
ug/l= Micrograms per liter. ND = Below Melhod Delection Limit
NR : Analysis not requested. Bold numbers exceed I 5A NCAC 2L.0202 standards.
l5A. NCAC 2L.0202 : NCDEQ Standard Statute for non{isked based maxinrum allowable containment concentration ir groundwater
Italicized Bold nrmbers exceed Gross Contaminant Levels = As presented in NCDEQ "Guidelines for Assessment and Corrective Action," Iast revised December I , 20 I 3.
Other delected analytes can be seen in the anal)4ical data.
Page 2 ol 2HlPtoiecrs\20061 001 249 IF MnNepons\2014 o^Suln ol I'ISIORICAL GW Analytbal
ADVANCEI)
ENVIRONMENTAL SERVICBS, INC.
"Your Environrnental Solutions Partner"
MOBILE
MULTI.PHASE
EXTRACTION REPORT
Site Location:
Texaco Food Mart
1700 Cotton Grove Road
Lexington, North Carolina
Prepared for:
Shield Engineering
4301 Taggart Creek Rd.
Charf otte, Norlh Carolina 28208
PM - Mr. Matthew Smith
July 18, 2018
TABLE OF CONTE,NTS
EVENT SUMMARY
MMPE FIELD LOG
MASS-REMOVAL CALCULATION
FIELD NOTES
DISPOSAL MANIFEST
Location:
Client:
Event Dates:
MOBILE MULTI.PHASE EXTRACTION
EVENT SUMMARY
July 18, 2018
Texaco Food Mart
1700 Cotton Grove Road
Lexington, Norlh Carolina
Shield Engineering
4301Taggart Creek Rd.
Charlotte, North Caroli na 28208
July 9 - 13,2018
Advanced Job # 07 - 1839
Advanced Personnel: Lee Heilig and Gary McDaniel
MMPE System MMPE system rated2l"hg at 130 CFM
4' discharge stack - 2" diameter
6,000 - gallon tanker
Approximately 60'of 2.0" hose to 1 well
Extraction Well: MW-2
Well Initial FP/WL(ft) Final FP/WL(ft) Stinger depth(ft) Run Time
MW-2 19.7 5 33.61 2212s129134 96.0 hours
Description of Event:
The MMPE event ran from I l:00 July 9, through 11:00 July 13,2018. The MMPE system was
active for 96.0 hours. During the event vacuum at the recovery pump ranged frorn 14.0 to 18.0
inches of mercury (hg) and stabilized at approximately 16.0 inches of mercury. Airflow rates
ranged from 3,100 to 3,600 feet per minute and stabilized at 3,500 feet per minute. System
temperature ranged from 98 - 132 degrees (F) and humidity maintained 99 percent. Field gauged
volatile organic compounds (VOC's) decreased from 1,200 parts per-million (PPM) to 900
(PPM) throughout the event.
Groundwater / Product Mix Recovered:
During the event, a total of 1,588 gallons of product/water mix were l'emoved from the site and
properly disposed at a certified North Carolina disposal facility. No free product was recovered
as liquid. Total fluids recovered, was measured based on stick readings conducted during and
followingthe event. Based on 96.0 hours of operation and atotal of 1,588 gallons recovered, the
average groundwater recovery rate was calculated to be approximately 16.54 gallons per hour.
Events Results:
Based on mass-removal calculations 14.67 pounds or 2.38 gallons of VOC's were removed as
vapor. Using Dwyer Magnehelic gauges, vacuum influence (inches of water) was rneasured at
monitoring points MW-1 and MW-3. Vacuum influence was observed at monitoring point
MW-l up to 0.10 inches of water. Draw-down was observed in MW-l and MW-3 at 0.35
and 0.38 feet respectively. Following the event, no free product was identified in any well.
MMPE FIELD LOG:
CLIENT Shield Engineering
JOB NAME: Texaco Food Mart
LOGATION: Lexington, NC
MMPE EVENT DATES: July 9 -13,2018
EXTRACTION POINTS: MW-2
AES JOB NUMBER: 07 - 1839
DATE TIME FLOW (t/m)HUM.(%)TEMP. (F)vOG'sloDml VAC. lho"l GALLONS STINGER,TU'L'S EXTRACTION POINTS ahq"l
MW-2
Stinser(ft)22,25,29,34
Start { {:OO Initial WL's 19.75
oTt09na 11=15 3,300 99.O 98 1,200 { 8.O {5.O
12=15 3,1oo 99.O 102 {,ooo 17.O 14.O
13:15 3,10o 99.O 12()1,2OO 17.O 14.O
14=15 3,100 99.0 120 t,{ oo 17.O 4O qal.14.O
oTtlona 8-.20 3,500 99.O ll5 1,2OO { 6.O 226 gal 14.O
9:2O 3,2O0 99.O 110 {,oo0 l6.o ,14.o
1O=2O 3,300 99.O 112 1,200 r 6.0 14.O
16:2O 3,5OO 99.O 122 1,00o l5.o 13.0
07t11na 8:15 3,30O 99.O 114 1,2OO 17.O 651 gal 14.O
9:15 3,300 99.O 108 1,200 17.O 14.O
I O:15 3,40O 99.O tt5 I,OOO l6.0 14.O
l6:45 3,soo 99.O 131 I,OOO { 5.O 13.O
07t12na 8:3O 3,600 99.O 122 900 { 5.O 9O4 qal.12.O
9:30 3,5OO 99.O 126 800 t5.o l3.o
{ O:3O 3,50O 99.O 128 800 r5.0 12.O
l6:OO 3,500 99.0 130 I,000 1s.0 12.O
07fi3na 8:3O 3,6OO 99.0 132 I,OOO 14.O 1,297 gal.1{.5
{ OrOO 3,600 99.O t30 900 14.O 11.5
Final WL's 33.61
End 1 l:OO Total fluids;1,588 sal.
Total free product:O qal.
DATE TIME VACUUM INFLUENCE (h2O'}WELL GAUGING (ft)
MW.l MW-3 MW-{MW-3
Start { lrOO
07togt1a 14:15 o.00 o.00 19.67 19.69
07l10na 16:.20 o.oo o.00 19.88 19.99
(J7111t18 9:15 o.05 o.o0 19.99 { 9.88
07l12na 16:OO 0.r 0 o.oo 20.o2 19.96
07l13na 't O:OO o.05 o.oo 19.99 2(J.o7
End 1 {:OO
Page 1 of 1
MOBILE MULTI-PHASE EXTRACTION EVENT
CLIENT: SHIELD ENGINEERING
AVERAGE I-JEP IH IO GROUNUWAI ER: 19 - 20 ft.
DESCRIBE SOIL IN THE SATURATED ZONE:
E HYDRAULIC
EX TRAC I ION WELLS USED FOR MMPE: MW-2
SPECIFICATIONS OF THE lvll\ilPE SYSTEM (cfm @ in Ho): 130 cfm I D 21.o"Hq
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS
Date Hours Vacuum Velocitv Pipe lD Iemp Rel Humid Water Water Q"a
(inches of Hq)(fUmin)(in)('F)(%\VaDor (Wt%)Vapor (Vol%)(flow)
7tgt1A 24.OO 17.OO 31 50.00 2 110 99.0 0.058 0.085 58
7t10t18 46.00 10.00 33 /5.00 2 115 99.0 0.06E 0.09E 61
7t11t1A 72.OO 16.00 3375.00 114 99.0 0.075 o.107 60
7t12t18 96.00 15.00 3550.00 2 128 99.O 0.1 03 o.142 60
7t't3t1a
NOTES
Qstd = Flow at DSCFM
vacuum
rale at measured at the blower or
stream bulb tn
Relative = The
water
8." = water vapor 7o by volume
EQUATIONS
+
+
EMISSION CALCULATIONS
Elapsed
lime Flow PPM----,,.-,PPM.,,.,PPM"..,K PPM..*C"PMR"PMR"PMR
(hour)(DSCFM)(ppm)(#C - qas)ilb/dsct)0b/hour)(lb/hour)flb)
5824 1125 1125 1230 1 1230 btJ 3.U3U05E-05 0.13 0.1 5 3./2
4A 61 11 00 1100 1220 1 1220 609 3.79984E-05 o.14 0.16 3.86
72 60 11 00 1100 1232 I 1232 615 3.83827E-05 0.14 0.'16 J-O4
96 1 049 1 1 049 523 3.266'l EE-05 o.12 o.'t4
Total emissions in pounds 14.67
NO-iES-
as 6.2.38
a or no
=1.or or Hexane K =
AS rybasrsatSIP
mass as
1 2.O'l molecular of
mass to at
= lb/dcsf mass concentration of VOC emissions as carbon
mass remova rate as
mass removal rate of of VOC'S as
mass as
1
C.. = (PPM.)N4. / l(.
toIMPE FneEd [.,og
Client: s;a .uf-| {:,-r, *'r.1r:
$ite NanagiT-q*r- f.n.i ay,^,* b;
Hxtraction Wells: 14 t4 - A
7 €
Joh Numb€r:4 ?* !€s3
EventDates; =lq - 7fn,2att
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ivlMpH F'fleld L*g
Ctrient: s4,:,Ll Er-s.k,,,-,':'3 t
$ite Name r!6>'noco 7..-l *tn;t * A
Extraction Wells: lntP' &-
Job Nunnbgrl" a7 " rcq
Event Dates: f /q ^ I lx,2 */d
7 ty {--1
IS " /Y)ah+
5 *-*.
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94 Ll
Fage#-,fu
MATERIAL
MANIFEST
EMERGENCY PHONE NO
[phone]
POST OFFICE BOX 357
HIGH POTNT,NC 27261
TEL (33O 841-5276
FAX (336) 84r-ss09
& lndultlal Sdlc€t
Name
Street
EPA lD No.
Phone No.
Contact&*rq I7a)
\{
Manifest Document No
ofPage
GENERATOR INFORMATION
ing Address
D
ADDITIONAL lNFORMATION
a.
b.
c.
ON OF MATERIALS
USDOT Proper Shipping Name
All ltems for Hazard s Materials)HM
a.
b
c.
Hazard
Class or Dlv
UN/NA
lD No.
Packing
Group
Containers
Aty. I Type
Total
Quantltyy0IIl
Met4 - b1,7 f+1;r,JS (41 (i>ts8{
ERG No.
Unit
Wt./Vol.
q
(ihNhttA t ot('s utstil lt-t(;A iloN
Ihis rs to certify that the above-described materials are properly classified, described, packaged, marked and labeled, and are in
proper condition for transportation according to the applicable regulations of
none of the materials described abo ve are a hazardouswaste
the materials confarn /ess
as defined by
the Department of Transpoftation. lfufther certify
EPA 40 CFR Part 261 or any applicable state law,
that
and
unless specifi cally identified above,
ofPCBs as defined b EPA40 CFR Paris 279 and 7 61,
than 1,000 total and do not contain quantifiable levels
B
:' TRANSPORTER
'Zebra Environmental & lndustrial Services lnc I hereby of the abov*described
from
Address
901 East Springfield Boad
High Point, NC 27263
I hereby acknowledge receipt of above-described materials were received
ror NCO991302669 from the generator slta and were transpo,led to the facility listed below.
EPA lD No.z/ts ltEPhone [phone] lgnature Delivery Dats
Zebra Environmental & lnduslrial Services, lnc.I hereby acknowledge receipt of the materials covered by this manifest
except for any noted below.
-e*
&901 East Springfield Road
High Point, NC 27263
zha/te
naturs Receipt Date
or NCO991302669
Phone (336) 841-s276
contact David redder
/e_l'
o.
ORIGINAL -Facility Retain COPY2- Return to Generator GOPY3 -Transporter Retain COPY4 -Generator Retain
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytrcal
wwwpacElabs.com
July 03, 2018
Matt Smith
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: Texaco Food Mart #2
Pace Project No.: 92389200
Dear Matt Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on June 20,2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
lf you have any questions concerning this report, please feel free to contact me
Sincerely,
//firdt,/j,pvr*io
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: James Gamertsfelder, Shield Engineering, lnc.
Mr. Tom Witner, Shield Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Page 1 of 30
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]www.pacelabs.com
CERTIFICATIONS
Project:
Pace Project No.:
Texaco Food Maft#2
92389200
Charlotte Certif ication lDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certilication # LA1T 0028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #:5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certifi cation #: E87627
Kentucky UST Certification #: 84
VirginiaA/ELAP Certilication #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, excepi in full,
without the written consent of Pace Analytical Services, LLC.Page 2 of 30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)87s-90e2
Anffical
wvwpa^elabs.com
SAMPLE ANALYTE COUNT
Project:
Pace Project No.
Texaco Food Marl#2
92389200
Lab lD Sample lD Method Analysts
Analytes
Reported Laboratory
9238920000r
92389200002
92389200003
92389200004
92389200005
92389200006
92389200007
MW-1
MW.2
MW-3
MW.4
MW-5
T-1
Trip Blank
SM 62008
SM 62008
sM 62008
SM 6200B
SM 62008
SM 62008
SM 62008
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
CAH
CAH
CAH
CAH
CAH
CAH
CAH
oz
62
62
62
62
62
62
PASI-C
PASI-C
PASI-C
PASI-C
PASI-C
PASI-C
PASI-C
Page 3 of 30
Analytical
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-e0e2www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No
Texaco Food Mart #2
92389200
Sample: MW-1
Parameters
Lab lD: 92389200001
Results Units
Collected: 06/19/18 13:15
Report Limit DF
Received: 06120h8 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluorometha ne
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
'1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 ,1 -Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
'1, 1, 1,2-Tetrachloroethane
'|.,1,2,2-Telr achlo roelh a ne
Tetrachloroethene
Toluene
Analytical Method: SM 62008
86.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
117
ND
24.9
4.2
99.3
40.1
ND
ND
ND
ND
76.3
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1.2
1.2
1.2
1.2
1.2
12.5
1-2
1.2
1.2
1.2
1.2
2-5
1.2
2.5
1.2
1.2
2.5
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
5.0
l.z
1.2
5.0
1.2
1.2
1.2
1.2
1.2
1.2
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2-5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
z.a
2.5
2.5
2.5
2.5
2.5
2.5
06127118'18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127hB 18t49
06127118 18:49
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06127118 18:49
06127hB 18:45
06127118 18:49
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06127h8 18:49
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061271'lB 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
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06127118 18:49
OGl27l1B 18:49
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06127118 18:49
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O6127l1B 18:49
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06t27t18 18'.49
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06127118 18:49
06127118 18:49
06t27t18 18"49
06127118 18:49
71-43-2
1 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-5't-8
1 35-98-8
98-06-6
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
95-49-B
106-43-4
96-'12-8
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
7B-87-5
142-28-9
594-20-7
563-58-6
1 0061-01 -5
1 0061 -02-6
1 08-20-3
100-41-4
B7-68-3
9B-82-8
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 0B-BB-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without lhe written consent of Pace Analytlcal Services, LLC.Date: 07 10312018 05:16 PM Page 4 of 30
6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
w.pacelabs.com
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
Sample: MW-l
Parameters
Lab lD
Results
92389200001
Units
Collected: 06/19/18',l3:15
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
'1,2,3-Trichlorobenzene
'1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogales
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
303
17.4
ND
404
278
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
5.0
5.0
1.2
1.2
't.2
2.5
1.2
1.2
1.2
2.5
2-5
1.2
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
06127118 18:49
06127118 18:49
OGl27l18 18:49
06127118 18:49
06127118 18t49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
06127118 18:49
87-6't-6
120-82-1
71-55-6
79-00-5
79-01 -6
75-69-4
96-1 8-4
95-63-6
1 0B-67-B
75-01-4
179601-23-1
95-47-6
104
oo
102
70-1 30
70-1 30
70-1 30
2.5
2.5
2-5
o/o
Yo
o/o
06127118 1B:49 17060-07-0
06127118 1B:49 460-00-4
06127 I 18 1 8:49 2037 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consenl of Pace Analytical Seruices, LLCDale: 07 10312018 05:'16 PM Page 5 of 30
@
Pace Analytical Services, LLC
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Huntersville, NC 28078
(704)875-e0s2
Analfitcal
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ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
Sample: MW-2 Lab lD: 92389200002
Results Units
Collected: 06119118 13:24
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Parameters Qual
62008 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
terLButylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1 ,1 -Dichloroethane
'l ,2-Dichloroethane
1 ,1 -Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1 ,1 -Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Elhylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methyl{ert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1 ,1 ,1 ,2-Tetrachloroethane
1,1,2,2-fet achloroethane
Tetrachloroethene
Toluene
Analytical Method: SM 62008
9780
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
565
ND
ND
ND
ND
ND
ND
885
ND
ND
ND
ND
ND
ND
ND
ND
ND
131
2370
ND
ND
381 0
1010
261
ND
ND
ND
ND
23800
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
100
100
100
100
100
1000
100
100
100
100
100
200
100
200
100
100
200
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
't 00
100
'100
100
100
400
100
100
400
100
100
'100
100
100
100
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
200
OG|2ThB 17:44
06127118 17:44
O6127l'18 17:44
06127118'17:44
06127118 17:44
06127118'17:44
06127hA 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
O6127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118'17:44
06127118 17:44
06127118 17:44
06127118 17:44
OGl27l18 17:44
06127118 17:44
06127hB 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17i44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127118 17:44
06127hB 17144
OGl27l18 17:44
06127118 17i44
06127118 17:44
06t27118 17"44
06127118'17:44
O6127118 17:44
06127118 17:44
O6127118 17:44
O6127118 17:44
06!27118 17:44
06127118 17:44
71-43-2
1 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
1 04-51 -8
1 35-98-8
98-06-6
56-23-5
1 0B-90-7
75-00-3
67-66-3
74-87-3
95-49-B
1 06-43-4
96-12-8
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-B
75-34-3
107-06-2
75-35-4
I 56-59-2
1 56-60-5
78-87-5
142-28-9
594-20-7
563-58-6
1 0061-01-5
1 0061 -02-6
1 08-20-3
100-41-4
87-68-3
98.82-B
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
I 0B-BB-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDale: 0710312018 05: 1 6 PM Page 6 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-90e2
Anffical
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.
Texaco Food Marl#2
92389200
Sample: MW-2
Parameiers
Lab lD: 92389200002
Results Units
Collected: 061191'lB 13:24
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1 ,1 ,'l -Trichloroethane
1,1,2-Trichloroethane
Trichloroelhene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
Analylical Method: SM 62008
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ugiLND ug/L
2440 ug/L613 ug/L
ND ug/L
9650 ug/L
5030 ug/L
400
400
100
100
100
200
100
100
't 00
200
200
100
'17:44
17144
17:44
17:44
17:44
17:44
17:44
17:44
17:44
17:44
17i44
17:44
200
200
200
200
200
200
200
200
200
200
200
200
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
06t27t18
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-1 B-4
95-63-6
1 08-67-8
75-01-4
179601-23-1
95-47-6
103
98
101
70-1 30
70-1 30
70-1 30
200
200
200
%
o/o
%
06127 118 17:44 17060-07 -0
06127 118 17:44 460-00-4
OBl27 118 17:44 2O37 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: O71O312018 05:16 PM Page 7 of 30
o
Pace Analytical Services, LLG
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
ww.pacelabs.rcn
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Matl#2
92389200
Sample: MW-3
Parameters
Lab lD: 92389200003
Results Units
Collected: 06/'19/18 13:33
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
lert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
'1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomeihane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,'1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2=Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropa ne
2,2-Dichloropropane
1 ,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methyltert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
I ,1 ,1 ,2-Tetrachloroethane
1,1,2,2-fet achloroetha ne
Tetrachloroethene
Toluene
Analytical Method: SM 62008
23.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1400
ND
1',t6
ND
724
334
ND
ND
ND
ND
1230
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0 20
10.0 20
10.0 2010.0 20
10.0 20
100 20
10.0 20
10.0 2010.0 20
10.0 20
10.0 20
20.0 20
10.0 20
20.0 20
10.0 20
10.0 20
20.0 20
10.0 20
10.0 20
10.0 20
10.0 20
10.0 2010.0 20
10.0 20
10.0 20
10.0 20
10.0 2010.0 20
10.0 20
10.0 20
10.0 20
10.0 20
10.0 20
10.0 20
10.0 20
't 0.0 2010.0 20
40.0 2010.0 20
10.0 20
40.0 20
10.0 20
10.0 20
10.0 20
10.0 2010.0 20
10.0 20
06127118 18:01
061271'lB 18:01
06127118 18:01
06127118 18:01
06127h8 18:01
06127118'lB:01
OG|2ThB 18:01
06127118 18:01
06127118 1B:0'l
06127118 18:01
06127118 18:01
06127h8 18i01
06127118 1801
06127118 18:01
06127118 18:O1
O6127118 18:01
06127h8 18:01
06127118 18:01
06127hB 18:0'l
06127118 18:01
06127118 1801
06127118 18:01
06127118 18:01
06127hB 18:01
06127118 1B:0'l
06127118 18:01
061271'lB 18:01
06127118 1801
O6127118 18:O1
06127118 18:01
OGl27l18 18iO1
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18i01
06127118 18:01
06127l1B 18i01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
OGl27l18 18:01
06127118 18:01
71-43-2
1 0B-86-1
74-97-5
75-27-4
75-25-2
74-83-9
'104-51-8
1 35-98-B
9B-06-6
56-23-5
1 0B-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-'12-8
124-48-1
't 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
7B-87-5
142-28-9
594-20-7
563-58-6
1 0061-01 -5
1 0061 -02-6
1 0B-20-3
100-41-4
87-68-3
9B-82.8
1634-04-4
9 1 -20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 0B-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 0710312018 05:16 PM Page B of 30
Analytical^
Pace Analytical Services, LLC
9800 KinceyAve. Suite'100
Huntersville, NC 28078
(704)875-eoe2www.pa'ielabs-com
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
Sample: MW-3
Parameters
Lab lD
Results
92389200003
Units
Collected: 06/19i18 13:33 Received: 06120118 12i15 Matrix: Water
Report Limit DF Prepared Analyzed CAS No.Qual
62008 MSV
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
'1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Su/rogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
2300
570
ND
5330
2640
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
40.0
40.0
10.0
10.0
10.0
20.0
10.0
10.0
10.0
20.0
20.0
10.0
20
20
20
20
20
20
20
20
20
20
20
20
06127118 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118 1BO1
06127118 18:01
061271'lB 1B:01
QGl27l1B 18:01
06127118 18:01
06127118 18:01
06127118 18:01
06127118'lB01
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-1 B-4
95-63-6
1 08-67-8
75-01-4
179601-23-1
95-47-6
104
100
102
70-130 20
70-130 20
70-130 20
o/o
Vo
06127118 18:01 17060-07-0
06127 l'18 1B:0'1 460-00-4
06127 118 18:01 2037 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07 10312018 05:16 PM Page 9 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-e0e2
Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Marl#2
92389200
Sample: MW-4
Parameters
Lab lD
Results
92389200004
Units
Collected: 06119118 13:42
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Bulylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 ,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
I ,1 ,1 ,2-Tetrachloroethane
1,1,2,2-Tetr achloroeth a ne
Tetrachloroethene
Toluene
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
34.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
242
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1.0
't.0
1.0
'1.0
1.0
10.0
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
4.0
1n
1.0
4.0
1.0
1.0
1.0
1.0
'1.0
1.0
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
z
2
2
2
2
2
z
2
2
071O3118 03:O7
07/03/18 03:07
07103118 03:07
07i03/18 03:07
07/03/18 03:07
07103118 03:07
07/03/18 03:07
07103118 03:07
07103118 03:07
07/03/18 03:07
07/03/18 03:07
07103118 03:07
07/03/18 03:07
07103118 03:07
07/03/18 03:07
07103118 03:07
07103118 03:07
07103118 03:07
07103118 O3:O7
07l03hg O3:O7
07103118 03:07
O7l13l18 03:07
07/03/18 03:07
07lj3l18 03:07
07103118 03:07
07/03/18 03:07
07103118 03:O7
07/03/18 03:07
07103118 03:07
07103118 03:07
07/03/1 B 03:07
07/03/1 B 03:07
07103118 03:07
07/03/18 03:07
07103118 O3:07
07/03/1B 03:07
07t03118 03"07
07103118 03:07
07/03/18 03:07
07i03/18 03:07
07/03/1 B 03:07
07/03/1 8 03:07
07/03/18 03:07
07/03/18 03:07
07/03/18 03:07
07/03/18 03:07
O7l03l18 O3:O7
7',1-43-2
1 0B-86-1
74-97-5
75-27-4
75-25-2
74-83-9
1 04-51 -B
1 35-98-B
9B-06-6
56-23-5
't08-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-B
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-B
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
7B-87-5
142-28-9
594-20-7
563-58-6
1 0061 -01 -5
I 0061 -02-6
1 0B-20-3
100-41-4
B7-68-3
98-82-8
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 08-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:16 PM Page 10 of30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-s0e2
Analytical
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
Sample: MW-4
Parameters
Lab lD: 92389200004
Results Units
Collected: O6119118 13:42
Report Limit DF
Received: 06120118 12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
6200B MSV
1,2,3-Trichlorobenzene
'1,2,4-Trichlorobenzene
1 ,1 , 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimelhylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
Analytical Method: SM 62008
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.0
4.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
2.0
2.0
1.0
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
07i03/18 03:07
07103118 03:07
07103118 03:07
07103118 03:07
07/03/18 03:07
07103118 03:07
07/03/18 03:07
07103118 03:07
07103118 03:07
07/03/1 B 03:07
07/03/18 03:07
07l03h9 03t07
87-61 -6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-1 8-4
95-63-6
1 08-67-8
75-01-4
179601-23-1
95-47-6
10'l
98
101
70-1 30
70-1 30
70-1 30
Yo
Yo
o/o
07103118 03:07 17060-07-0
07 lO3l1B 03:07 460-00-4
07 l03l 18 03:07 2037 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:16 PM Page 11 of30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytieal
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.
Texaco Food Mart #2
92389200
Sample: MW-S
Parameters
Lab lD: 92389200005
Results Units
Collected: 06119118 13:52
Report Limit DF
Received: 06120118 12:15 Malrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
'1 ,'l-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 ,1-Dichloropropene
cis-'1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Elhylbenzene
Hexachloro-'1, 3-butadiene
lsopropylbenzene (Cumene)
Methyl{ert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-felr achloroeth a ne
1,1,2,2-Telr achloroethane
Tetrachloroethene
Toluene
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.50
0.50
0.50
0.50
0.50
5.0
0.50
0.50
0.50
0.50
0.50
1.0
0.50
1.0
0.50
0.50
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
2.O
0.50
0.50
2.0
0.50
0.50
0.50
0.50
0.50
0.50
06127118 16:39
06127t18 16:39
06127hB 16:39
06127118 16:39
061271'lB'16:39
06127118 16:39
06127hB 16:39
06127118 16:39
OGl27h8 16:39
06127118 16:39
06127118 16:39
O6127118 16:39
061271'lB 16:39
06127118 16:39
06127118 16:39
OGl27l18 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127hB 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
OGI27l18 16:39
06127118 16:39
OGl27l18 16:39
06127118 16.39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
O6127118 16:39
06127118 16:39
71-43-2
1 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
1 04-51 -B
1 35-98-B
98-06-6
56-23-5
1 0B-90-7
75-00-3
67-66-3
74-87-3
95-49-B
106-43-4
96-'12-8
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
142-28-9
594-20-7
563-58-6
1 0061-01 -5
1 0061 -02-6
1 08-20-3
100-41-4
87-68-3
98-82-B
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 0B-BB-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDale: 0710312018 05:1 6 PM Page 12 of 30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-e092
Analytical
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
Sample: MW-S
Parameters
Lab lD
Results
92389200005
Units
Collected: 06119118 13:52
Report Limit DF
Received: 061201'18'12:15 Matrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1 ,I , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,S-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
2,0
2.0
0.50
0.50
0.50
1.0
0.50
0.50
0.50
1.0
1.0
0.50
1
I
1
I
1
1
1
1
1
1
1
1
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
06127hB 16139
06127118 16:39
06127118 16:39
06127118 16:39
06127118 16:39
B7-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-1 B-4
95-63-6
1 0B-67-8
75-01-4
179601-23-1
95-47-6
102
98
100
70-1 30
70-1 30
70-1 30
o/o
%
06127118 16:39 17060-07-0
06127118 16:39 460-00-4
06127 118 16:39 2037 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuil,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:1 6 PM Page '13 of 30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analyttcal
www.pacelabs.ffin
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Matl#2
92389200
Sample: T-1 Lab lD: 92389200006
Results Units
Collected: 06i'19118 14:00
Report Limit DF
Received: O6l20hB 12:15 Matrix: Water
Prepared Analyzed CAS No.Parameters Qual
62008 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomelhane
n-Butylbenzene
sec-Butylbenzene
terl-Bulylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
'1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,1-Dichloroethane
1 ,2-Dichloroethane
'1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 ,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1 ,1 ,1 ,2-Tetrachloroethane
1,1,2,2-Tet achloroethane
Tetrachloroethene
Toluene
Analytical Method: SM 62008
580
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
198
ND
ND
ND
4.2
ND
ND
ND
ND
ND
19.5
73.7
ND
3.6
4.3
44.4
3.6
ND
ND
ND
ND
2.0
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
2.0
2.0
2.0
2.0
2.0
20.0
2.0
2.0
2.0
2.0
2.0
4.0
2.0
4.0
2.0
2.O
4.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
z.u
2.0
2-0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
8.0
2.0
2-0
8.0
2.0
2.0
2.0
2.0
2.0
2.0
07/03/18 03:40
07103118 03:40
07/03i18 03:40
07/03/18 03:40
07/03/18 03:40
071031'18 O3:4O
07/03/18 03:40
07103118 03:40
07/03/1 B 03:40
07/03/18 03:40
07/03i18 03:40
07lo3l18 03:40
07103118 03:40
07/03/18 03:40
07103/18 03:40
07103118 03:40
07103118 03:40
07/03/18 03:40
07/03/18 03:40
07103118 O3:4O
07/03/18 03:40
07/03/1 I 03:40
07/03/18 03:40
07103/18 03:40
07103118 03:40
07/03/18 03:40
07103118 03:40
07103118 03:40
07/03/',l8 03:40
07103118 03:40
07103/18 03:40
07103118 03:40
07/03/'18 03:40
07/03i18 03:40
07/03i18 03:40
07/03/18 03:40
07l13l18 O3:4O
07/03/18 03:40
07103118 03:40
07/03/18 03:40
07103118 03:40
07/03/18 03:40
07/03/18 03:40
07/03/'18 03:40
07/03/1 8 03:40
07/03/1 8 03:40
07103/1 B 03:40
71-43-2
1 08-86-1
74-97-5
75-27-4
75-25-2
74-83-9
1 04-51 -B
1 35-98-8
9B-06-6
56-23-5
1 08-90-7
75-00-3
67-66-3
74-87-3
95-49-B
106-43-4
96-12-B
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
7B-87-5
142-28-9
554-20-7
563-58-6
1 0061-01 -5
1 0061 -02-6
1 0B-20-3
100-41-4
B7-68-3
98-82-8
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 08-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:'1 6 PM Page 14 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No
Texaco Food Mart#2
92389200
Sample: T-1 Lab lD: 92389200006
Results Units
Collected: 06/19/18 14:00 Received: 0612011812:15 Matrix: Water
Report Limit DF Prepared Analyzed CAS No.Parameters Qual
62008 MSV
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1, 1 -Trichloroethane
1, 1,2-Trichloroelhane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
',l,3,S-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-d8 (S)
Analytical Method: SM 62008
ND ug/L
ND ug/L
ND ug/L
ND ugiL
ND ug/LND ug/L
ND ug/L
76.0 ug/L
12.8 ug/L
ND ugil34.4 ug/L
93.2 ug/L
07/03/18 03:40
07/03/18 03:40
07/03/18 03:40
07103/18 03:40
07/03/18 03:40
07103118 03:40
07103118 03:40
07l03l18 O3:4O
07/03/18 03:40
07103/18 03:40
07/03/18 03:40
07/03/18 03:40
8.0
8.0
2.0
2.0
2.0
4.0
2.0
2.0
2.0
4.0
4.0
2.0
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
B7-61-6
120-82-1
71-55-6
79-00-5
79-01 -6
75-69-4
96-18-4
95-63-6
't 08-67-B
75-0',1-4
179601-23-1
95-47-6
101
98
101
70-1 30
70-1 30
70-1 30
o/o
to
%
07103118 03:40 17060-07-0
07 103118 03:40 460-00-4
07 l03l 1B 03:4O 2037 -26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDate: 0710312018 05: 16 PM Page l5 of30
6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-eoe2
Analfiical
www.pacelabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.
Texaco Food Mart #2
92389200
Sample: Trip Blank
Parameters
Lab lD: 92389200007
Results Units
Collected: 06/19/18 00:00
Report Limit DF
Received: 06120118 12:'15 Matrix: Water
Prepared Analyzed CAS No.Qual
62008 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1 ,2-Dichlorobenzene
'1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifl uoromethane
1 ,'l -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
'l ,3-Dichloropropane
2,2-Dichloropropane
1 ,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Elhylbenzene
Hexachloro- 1,3-butadiene
lsopropylbenzene (Cumene)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
'1 ,'1 ,1 ,2-Tetrachloroethane
1,1,2,2-Tetr achloroethane
Tetrachloroethene
Toluene
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.50
0.50
0.50
0.50
0.50
5.0
0.50
0.50
0.50
0.50
0.50
1.0
0.50
1.0
0.50
0.50
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
2.O
0.50
0.50
2.0
0.50
0.50
0.50
0.50
0.50
0.50
06127118 15:02
061271'18 15:02
06127h8 15i02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:O2
06127118 15:02
06127118 15:02
061271'lB 15:02
061271'lB 15:02
061271'18 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15iO2
06127118 15:02
06127118 15:02
06127118 15:02
06127!18 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127hB 15:02
06127118 1502
OGl27l18 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:O2
06127118 15i02
06127118 15:O2
06127118 15:O2
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
OGl27l18 15:02
O6127118 15:O2
06!27118 15:02
06127118 15:O2
7',t-43-2
1 0B-86-1
74-97-5
75-27-4
75-25-2
74-83-9
1 04-51 -8
'135-98-B
98-06-6
56-23-5
1 0B-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-B
124-48-1
1 06-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
142-28-9
594-20-7
563-58-6
'10061-01-5
'10061-02-6
1 0B-20-3
100-41-4
87-68-3
9B-82-B
1634-04-4
91-20-3
1 03-65-1
100-42-5
630-20-6
79-34-5
127-18-4
1 0B-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:16 PM Page 16of30
o
Paee Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Anffical
www.pa6elabs.con
ANALYTICAL RESULTS
Project:
Pace Project No.:
Texaco Food Marl#2
92389200
Sample: Trip Blank
Parameters
Lab lD: 92389200007
Results Units
Collected: 06i'l9i1B 00:00
Report Limit DF
Received: 06120118 12:.15 Matrix: Water
Prepared Analyzed CAS No.Qual
6200B MSV
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-d8 (S)
Analytical Method: SM 62008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
2.0
2.0
0.50
0.50
0.50
1.0
0.50
0.50
0.50
1.0
1.0
0.50
06127118 15:02
06127hB 15i02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127118 15:02
06127h8 15i02
06127hB 15:02
06127118 15:02
06127118 15:02
06127118 15:02
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-1 8-4
95-63-6
1 08-67-8
75-01-4
179601-23-1
95-47-6
101
97
103
70-'130
70-1 30
70-1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
OGl27 118 15:02'17060-07 -O
06127 118 15:02 460-00-4
06127 I 18 1 5:02 2037 -26-5
o/o
To
Dale: 0710312018 05: 1 6 PM Page '17 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)87s-9092
Analytical
www.pacelabs.con
QUALITY CONTROL DATA
Project:
Pace Project No.:
Texaco Food Mart #2
92389200
QC Batch: 416880 Analysis Method: SM 62008
QC Batch Method: SM 62008 Analysis Description: 62008 MSV
Associated Lab Samples: 92389200001, 92389200002, 92389200003, 92389200005, 92389200007
METHOD BLANK: 2311586 Matrix: Water
Associated Lab samples: 92389200001, 92389200002, 92389200003, 92389200005, 92389200007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1 , 1 ,1 ,2-Tetrachloroethane
1 , 1 ,1-Trichloroethane
1,1,2,2-fet achloroethane
1, 1,2-Trichloroethane
1 ,1-Dichloroethane
1 ,1-Dichloroethene
1 ,1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
1 ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichlorometha ne
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
D ibro moch lo rometha ne
Dibromomethane
D ich lo rod ifl uoromelha ne
Diisopropyl ether
Ethylbenzene
06127118 13:14
OGl27l18 13:14
OGl27l18 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118'13:14
06127118 13:14
06127118 13:14
06127118 13:14
OGl27l18 13:14
06127hB 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118'13:14
06127118 13:'14
06127118 13:14
06127118 13:14
06127118 13:14
OGl27l18 13:14
061271'lB 13:14
06127118'13:14
06127118 13:14
06127118 13.14
OGl27l18 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118 13:14
O6127l1B 13:14
O6127118 13:14
06127118 13:14
06127hB 13:14
06127118 13:14
06127118 13:14
06t27t18 13.14
06127118 13:14
06127118 13:14
O6127118 13:14
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.50
0.50
0.50
0.50
0.50
0.50
0.50
2.0
0.50
2.0
0.50
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
5.0
0.50
0.50
1.0
0.50
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
Results presented on this page are in the units indicated by lhe "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05: 1 6 PM Page '18 of 30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)87s-e092
Analytieal
www.pacelabs.con
QUALITY CONTROL DATA
Project:
Pace Project No.
Texaco Food Marl#2
92389200
METHOD BLANK: 2311586 Matrix: Water
Associated Lab Samples: 92389200001, 92389200002, 92389200003,92389200005, 92389200007
Blank Reporting
Parameter Units Result Limit Analyzed Oualifiers
Hexachloro-'1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyltert-butyl ether
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
lrans-1,3-Dichloropropene
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
101
97
102
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
Yo
To
%
2.0
0.50
1.0
0.50
0.50
0.50
2.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.0
1.0
70-1 30
70-'130
70-1 30
06127118 13:14
06127118 13:14
06127118'13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127hB 13:14
OGl27l18 13:14
06127118 13:14
O6127l1B 13:14
06127118 13:14
OGl27l18'13:14
061271'18 13:14
06127118 13:14
06127118'13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118 13:14
06127118 13:14
LABORATORY CONTROL SAMPLE:
Parameter
2311587
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
'' ,1, 1,2-felr achloroetha ne
1 ,'l , 1-Trichloroetharie
1,1,2,2-Telrachloroethane
1, 1,2-Trichloroethane
1 ,1 -Dichloroethane
1 ,1 -Dichloroethene
1 ,1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3,5-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
47.7
46.5
47.0
47.3
47.4
50.9
46.4
44.3
47.5
46.4
45.2
48.9
47.4
46.2
43.8
47.4
46.3
46.0
46.7
95
o'l
94
95
95
102
93
89
95
93
90
98
95
92
BB
95
93
92
93
60-140
60-140
60,140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-140
60-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented io the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDale'. 0710312018 05:16 PM Page '19 of 30
6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-eoe2
Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No.
Texaco Food Mart #2
92389200
LABORATORY CONTROL SAMPLE
Parameter
2311587
Units
Spike
Conc.
LCS
Result
LCS
o/o Rec
% Rec
Limits Qualifiers
1 ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Dibromochloromelhane
Dibromomethane
Dichlorodifl uoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl{ert-butyl ether
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Yo
%
o/o
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
qn
50
50
50
50
50
45.8
52.1
45-2
46.0
46.3
46.4
47.0
49.0
54.5
34.6
49.5
45.6
45.2
45.0
52.1
48.6
49.9
51.8
47 -4
55.3
49.2
46.2
48.4
47.7
94.7
44.4
48.3
47.2
44.3
46.9
46.8
47,7
40.3
47.7
46.3
49.6
50.2
47.3
46.9
54.0
92
104
90
92
93
93
94
9B
't 09
69
99
91
90
90
104
97
100
't04
95
111
98
92
97
OA
95
B9
97
94
B9
94
94
95
81
95
93
99
100
OA
94
108
100
101
102
60-140
60-140
60-140
60-140
60-1 40
60-140
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-140
60-140
60-140
60- 140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-1 40
60-1 40
60-140
60-140
60-140
60-140
70-1 30
70-1 30
70-1 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDale 07/0312018 05:16 PM Page 20 of 30
6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]www.pacelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No.
Texaco Food Mart #2
92389200
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2311588
Parameter
92389328002
Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
2311589
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
1 ,1 ,1 ,2-Tetrachloroethane
1,1, 1 -Trichloroethane
1,1,2,z-Ielr achloroethane
1, 1,2-Trichloroethane
1 ,1 -Dichloroethane
1 ,1-Dichloroethene
1 ,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3, s-Trimelhylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
1 ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifl uoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
n-Butylbenzene
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
98
102
97
OA
'105
118
103
93
95
96
94
103
101
96
92
97
101
97
oo
97
116
98
oo
99
100
101
97
104
fJb
107
9B
109
95
118
107
100
103
9B
129
108
100
94
103
103
95
102
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
20.4
21.0
19.9
19.8
21.8
24.6
21.8
18.7
20.5
20.1
20.4
21.7
20.7
19.9
19.0
20.7
20.9
20.3
20.3
20.0
23.1
20.3
zu.6
20.6
20,7
21.1
20.5
21.1
14.1
22.2
20.0
23.1
19.4
25.O
22.1
21.2
21.3
20.5
26.5
22.5
20.7
'19.8
20.9
42.4
19.9
21.2
19.7
20.4
19.4
19.1
21.0
23.6
20.7
18.6
19.0
19.2
18.9
20.5
20.3
19.3
18.3
19.5
20.2
19.4
19.7
19.4
23.2
19.6
19.9
19.8
20.0
20.2
19.5
20.9
13.2
21.3
19.5
21,8
19.0
23.8
21.5
20.1
20.6
'19.5
25.8
21.7
20.0
18.9
20.6
41.0
'19.0
20.5
'102
105
99
oo
109
123
109
94
103
100
102
108
103
99
95
103
105
101
't01
100
116
102
103
103
104
106
102
106
71
111
100
115
o-7
124
110
106
106
102
132
113
103
99
104
106
100
106
60-140
60-140
60-140
60-140
60-'140
60-140
60-'t40
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60- 140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-'140
60- 1 40
60-140
60-140
60-140
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
4
J
2
4
4
4
5
0
I
5
B
b
2
3
4
b
J
5
J
J
0
4
J
4
4
4
5
1
7
4
J
6
2
5
6
?
4
5
2
3
5
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presenled to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consenl of Pace Analytical Services, LLCDale: 0710312018 05:16 PM Page 21 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Fo4)A75-9092
Anffical
wwwpacelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No.
Texaco Food Maft#2
92389200
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2311588
Parameter
92389328002
Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
231 1 589
Result
MSD
Result
MS
o/o Rec
MSD
% Rec
MS % Rec
Limits RPD Qual
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroelhene
Trichlorofl uoromethane
Vinyl chloride
'1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
21.6
20.7
20.8
21.O
20.4
18.1
21.2
19.9
23.2
20.8
21.1
23.9
25.8
108
104
104
105
102
90
106
100
116
104
106
119
129
101
oo
100
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Yo
Yo
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
21.1
19.3
20.2
20.4
19.8
17.7
21.1
19.3
22.4
19.8
20.2
22.8
24.9
105
97
101
102
99
88
106
97
't12
99
101
114
124
9B
100
100
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
70-130
70-1 30
3
7
J
3
3
2
n
J
J
5
5
5
3
Results presented on this page are in the unlts indicated by the "Units" column except where an alternate unit is presented to lhe right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05:16 PM Page 22 oI 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)87s-e0e2
Analytical
www.paelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No
Texaco Food Marl#2
92389200
QC Batch: 417074
QC Batch Method: SM 62008
AssociatedLabSamples: 92389200004,92389200006
Analysis Method:
Analysis Description:
SM 62008
62008 MSV
METHOD BLANK: 2312805
Associated Lab Samples
Parameler
92389200004, 92389200006
Units
Matrix: Water
Blank
Result
Reporting
Limit Analyzed Qualifiers
1 ,1 ,1 ,2-Telrachloroethane
1,1, 1 -Trichloroethane
1,1,2,2-Telrachloroethane
1, 1,2-Trichloroethane
1 ,1 -Dichloroethane
1 ,1 -Dichloroelhene
1 ,1 -Dichloropropene
1,2,3-Trichlorobenzene
'1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
'1,2-Dibromoethane (EDB)
'I ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3,S-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
1 ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifl uoromethane
Diisopropyl ether
Ethylbenzene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.50
0.50
0.50
0.50
0.50
0.50
0.50
2.0
0.50
2.0
0.50
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
5.0
0.50
0.50
1.0
0.50
'1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/1 B 00:08
07/03/18 00:08
07/03/1 8 00:08
07/03/1 B 00:08
07/03/1 I 00:08
07/03/18 00:08
07/03/18 00:08
07/03/'18 00:08
07/03ilB 00:08
07/03/18 00:08
07/03/1 8 00:08
07/03/1 8 00:08
07/03/1 B 00:08
07/03/1 B 00:08
07/03/1 8 00:08
07/03/1B 00:08
07/03/'lB 00:08
07/03/lB 00:08
07/03/18 00:08
07/03/'lB 00:08
07103/1 8 00:08
07/03/1 B 00:08
07/03/1 8 00:08
07/03/1 B 00:08
07/03/18 00:08
07/03/1 B 00:08
07/03/18 00:08
07/03/1 B 00:08
07/03/1 8 00:08
07103/1 8 00:08
07/03/1 8 00:08
07103/1 8 00:08
07/03/1 B 00:08
07/03/1 B 00:08
07/03/1 8 00:08
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/0312018 05:16 PM Page 23 of 30
Analytical'
Pace Analytical Services, LLC
9800 KinceyAve. Suite'100
Huntersville, NC 28078
[phone]www.paiielahs.com
QUALITY CONTROL DATA
Project:
Pace Prolect No
Texaco Food Mart #2
92389200
METHOD BLANK: 2312805
AssociatedLabSamples: 92389200004,92389200006
Parameter Units
Matrix: Water
Blank
Result
Reporting
Limit Analyzed Qualifiers
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofl uoromethane
Vinyl chlorlde
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-d8 (S)
07/03i 18 00:08
07/03i18 00:08
07/03/1 B 00:08
07/03/1 B 00:08
07/03/1 8 00:08
07/03/1 I 00:08
07i03/1 I 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/18 00:08
07/03/1 B 00:08
07103/1 B 00:08
07i03/1 I 00:08
07103/18 00:08
07/03/18 00:08
07/03/18 00:08
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
To
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
a7
99
101
2.O
0.50
1.0
0.50
0.50
0.50
2.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.0
1.0
70-1 30
70-1 30
70-1 30
LABORATORY CONTROL SAMPLE:
Parameter
2312806
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1 , 1 ,1 ,2-Tetrachloroethane
1 ,1 ,1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1 ,1-Dichloroethane
1 ,1 -Dichloroethene
1 ,1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3,S-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
58.5
57.8
54.9
57.7
54.7
61.9
57.5
53.6
53.0
54.6
55.3
59.8
55.9
54.9
50.9
58.3
55.4
54.2
55.6
117
116
110
115
109
124
115
107
'106
109
111
120
112
110
102
117
111
108
111
60-'140
60-1 40
60-1 40
60-1 40
60-1 40
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-1 40
60-1 40
60-1 40
60-1 40
60-140
60-140
Resulls presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale'. 0710312018 05:16 PM Page 24 of 30
o
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
www.pacelabs.con
QUALITY CONTROL DATA
Project:
Pace Project No.:
Texaco Food Mart#2
92389200
LABORATORY CONTROL SAMPLE:
Parameter
2312806
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1 ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon letrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifl uoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl{ert-butyl ether
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Slyrene
tert-Butylbenzene
Tetrachloroelhene
Toluene
trans- 1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-dB (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
o/o
o/o
To
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
54.1
60.5
54.9
54.6
57.3
54.4
60.3
62.2
50.2
59.4
62.2
54.3
5',1.7
53.0
55.0
56.6
60.4
50.7
58.3
68.6
54.2
53.8
54.8
56.3
109
54.0
56.5
55.4
55.8
56.3
56.2
56.7
48.0
50.8
55.7
57.7
oz- I
58.5
59.5
64.1
108
121
110
109
115
'109
121
124
100
119
124
109
103
106
1'10
113
121
't 01
117
137
108
108
110
113
109
108
113
111
112
1'13
112
113
96
102
111
115
124
117
119
128
95
100
100
60-140
60-140
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-140
60-140
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-1 40
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-1 40
60-1 40
60-1 40
60-140
60-140
70-130
70- t 30
70-1 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312018 05: 1 6 PM Page 25 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No
Texaco Food Mart #2
92389200
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2312807
Parameter
92389964001Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
2312808
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
o/o Rec
Limits RPD Qual
1 ,1 ,1 ,2-Tetrachloroethane
1 ,1 ,1 -Trichloroethane
1,1,2,2-Tetachloroethane
1,1,2-Trichloroethane
1 ,1-Dichloroethane
1 ,1 -Dichloroethene
1 ,1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,2-Dichloroethane
1 ,2-Dichloropropane
1,3,s-Trimethylbenzene
1 ,3-Dichlorobenzene
1 ,3-Dichloropropane
'I ,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochlorometha ne
Dibromomethane
Dichlorodifl uoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
n-Butylbenzene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.3
ND
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
24.8
25-9
22.8
24.6
24.1
27.6
25.5
21.4
24.0
22.8
23.5
22.1
23.6
22.9
23.2
24.9
24.0
22.5
24.O
22.4
24.2
23,1
23.2
24.7
23.4
26.3
24.8
19.9
18.3
26.9
23.7
25.0
22.7
24.2
24.7
24.1
21.2
24.5
31.5
23.6
23.9
23,0
24.5
47.7
24.8
23.7
24.9
25.7
23.8
24.6
24.3
28.0
26.2
23.2
23.5
23.4
24.1
23.8
24.O
23.7
22.5
25.4
24.1
23.6
24.8
23.4
24.2
23,9
23.7
24.6
23.7
tco
25.6
20.8
17.3
27.2
24,O
25.2
23-2
23.9
24.9
24.7
21.9
24.3
32.2
23.9
23.8
23.3
25.1
48.2
25.1
24.2
124
129
114
123
121
138
127
107
120
114
'118
110
118
115
116
125
120
112
't20
112
121
115
116
124
'117
132
124
100
91
134
119
't25
114
121
123
120
106
123
158
118
120
115
123
't19
118
119
125
128
119
123
't22
140
131
116
117
117
121
119
120
'1'l I
112
127
121
118
124
117
121
119
119
123
'11 8
129
128
104
B6
136
120
126
116
119
124
124
109
122
161
120
119
117
125
121
119
121
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
60-'140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-'140
60-1 40
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60- 1 40
60-140
60-140
60- ,l40
60-140
60-140
60-140
1
1
4
0
1
2
o
2
3
2
8
2
4
3
2
1
5
3
4
0
3
2
0
1
2
3
4
6
1
1
1
2
1
1
J
J
1
2M1
1
1
2
2
1
1
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consenl of Pace Analytical Services, LLC.Dale: 0710312018 05:1 6 PM Page 26 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
halytical
wwwpalelabs.com
QUALITY CONTROL DATA
Project:
Pace Project No
Texaco Food Mart #2
92389200
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2312807
Parameter
92389964001Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
2312808
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
n-Propylbenzene
Naphthalene
o-Xylene
sec-Bulylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofl uoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofl uorobenzene (S)
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ugiL
ug/L
ug/L
ug/L
ug/L
ug/L
To
To
Yo
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
24.'.|
21.5
24.0
24.2
23.9
20.7
23.0
24.4
25.8
24.5
25.4
28.3
28.2
24.3
23-7
24.7
24.9
24.1
21.1
22.2
24.6
25.9
25.2
25.2
28.7
28.5
120
107
120
121
120
104
115
122
129
123
127
142
141
oo
99
10'l
121
119
123
124
120
105
111
123
129
126
126
143
143
100
101
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
60-140
60-140
60-140
60-140
60-140
60-140
60-'140
60-140
60-140
60-140
60-140
60-140
60-140
70-130
70-130
70-1 30
'l
10
3
?
I
2
4
1
0
3
1
1M1
1M1
Results presented on lhis page are in the units indicated by the "Units" column except where an alternate unit is presenled to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 071O312018 05: 1 6 PM Page 27 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Anffical
www.pacelabs.com
QUALIFIERS
Project:
Pace Project No.
Texaco Food Matl#2
923B9200
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate o/o iF.Covet! and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U' lndicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC lnstitute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLCDale: 0710312018 05:1 6 PM Page 28 of 30
@
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-s0e2
Analytical
tuw.pao€'labs.con
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Texaco Food Mafi#2
92389200
Lab lD Sample lD QC Batch Method
Analytical
Batch
92389200001
92389200002
92389200003
92389200004
92389200005
92389200006
92389200007
MW-I
MW.2
MW-3
MW-4
MW-5
T-1
Trip Blank
SM 62008
SM 62008
SM 62008
SM 62008
SM 62008
SM 62008
SM 62008
QC Batch Analytical Method
416880
416880
416880
417074
41 6880
417074
416880
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Dale: 0710312O18 05:1 6 PM Page 29 of 30
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