WS-6081_22332_CA_MRP_20071227

MONITORING REPORT TEXACO FOODMART #2 1700 COTTON GROVE ROAD LEXINGTON, DAVIDSON COUNTY, NORTH CAROLINA INCIDENT NO. 22332 SHIELD PROJECT NO. 1001289
Responsible Party: Techno, LLC for Holding Brothers, Inc P.O. Drawer 647 Concord, NC 28026 Contact: David Holding [phone] December 2007
Consultant: Shield Engineering, Inc. 4301 Taggart Creek Road Charlotte, North Carolina 28208 Contact: David A. Stoner [phone] Property Owner: Holding Brothers, Inc. P.O. Drawer 647 Concord, North Carolina 28208 Contact: David Holding [phone]Site Risk Classification: High Risk (H155D) Land Use Category: Residential and commercial Release Discovered: February 8, 1999 Site Latitude: 35°46'41" North Site Longitude: 80°15'35" West Potential Release Source(s): Unknown
C�s.�. Colleen Clark, P.G. Project Manager Registered NC #2077 •'• ,-
Quantity Released: Unknown
TABLE OF CONTENTS
Page No.
1.0 DISCUSSION OF SAMPLING RESULTS ........................................................................ 1
2.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................. 4
3.0 LIMITATIONS ................................................................................................ · ................... 5
Figure 1:
Figure 2:
Figure 3:
Figure 4:
Figure 5:
Figure 6:
Figure 7:
Figure 8:
Figure 9:
Figure 10:
Figure 11:
Table 1:
Table 2:
Table 3:
Table 4:
Site Location Map
Site Map
1500' Radius Map
LIST OF FIGURES
Groundwater Elevation Contour Map
Benzene Isoconcentration Map
Toluene Isoconcentration Map
Ethylbenzene Isoconcentration Map
Total Xylenes Isoconcentration Map
MTBE Isoconcentration Map
1,2-Dichloroethane Isoconcentration Map
Naphthalene Isoconcentration Map
LIST OF TABLES
Summary of Adjacent Property and Water Supply Well Owners
Summary of Well Construction and Historical Groundwater Elevation Data
Summary of Analytical Results -Groundwater Samples
Summary of Historical Analytical Results -Groundwater Samples
APPENDICES
Appendix A: Well Sampling and Field Measurement Logs
Appendix B: Laboratory Report -Groundwater Samples
H:\Projects\200(NOOJ 289'December 2007 Monitoring report\ Dec 2007.doc
1Texaco Food Mart #2
Lexington, Davidson County, North Carolina
Incident#: 22332
1.1
1.0 DISCUSSION OF SAMPLING RESULTS
Site Monitoring Requirements:
Site Location Map:
Site Map:
See Figure 1
See Figure 2
Site Monitoring Requirements
Based on CAP and/or NORR·
Monitoring Report
December 21, 2007
Page I
Sample Point Total Quantity of Previous Required by NCDENR to be
Type Sample Points and Their Monitored and Sampled per CAP
Identification and/or TA (Z)
Monitoring 6 6 (1)
Wells (MW-1 through MW-5, and T-1) (MW-1 through MW-5, and T-1)
Water Supply 13 (Z) 0
Wells (WSW-1 through WSW-13)
( 1) Individual wells identified by NCDENR for specific sampling as approved on October 23, 2007.
(2) Number of wells located within 1,500 feet of site.
1.2 Summary of Analytical Results and Free Product Thickness(s):
1.2.1 Date(s) of Sampling Event:
• Monitoring wells were sampled on November 19, 2007,
1.2.2 Existing Area Receptors:
Refer to the following Tables and Figure(s) for information and locations of area receptors.
Refer to Figure(s): Figure 3
Refer to Tables(s): Table 1
1.2.3 Groundwater Flow Direction:
• Current groundwater flow direction is to the northwest and southwest.
Current and Historical Groundwater Elevation Data is included in the following Table(s),
Figure(s) and Appendix:
Refer to Table(s):
Refer to Figure(s):
Refer to Appendix:
1.2.4 Free Product:
Table 2
Figure 4
Appendix A
' Texaco Food Mart #2 Monitoring Report
December 21, 2007
Page 2
Lexington, Davidson County, North Carolina
Incident#: 22332
• Free Product Detected During this Reporting Period?: No
1.2.5 Groundwater Analytical Results:
• Sampled Points and Analytical Methods:
The following monitoring wells and other points were sampled during this reporting
period.
Sampled Points and Analytical Methods
for this Reporting Period
Based on CAP and Pre~Approval Task Authorization Sampling Requirements
Type Points Sampled during this Analytical Methods
Reportin2 Period
Monitoring (6) (I) • EPA Method 601 and 602
Wells (MW-l,MW-2,MW-3,MW-4, extended (+MTBE, IPE, Total
MW-5, and T-1) Xylenes, EDB, Naphthalene),
• MADEP Extractable
Petroleum Hydrocarbons
(EPH) and Volatile Petroleum
Hydrocarbons (VPH) and EPA
Method 625
( 1) Pre-Approval Task Authorization TA -22332-05 ( 10/23107)
• Laboratory Used: Pace Analytical Services Inc. Huntersville, NC
• Current Groundwater Analytical Data:
On November 19, 2007 groundwater samples were collected from the six monitoring
wells. One or more concentrations of benzene, ethylbenzene, toluene, total xylenes,
MTBE, naphthalene and 1, 2-Dichloroethane ( 1,2-DCA) were detected at concentrations
above the 2L Standards in four site monitoring wells (MW-1, MW-2, MW-3 and T-1).
Refer to the following Table(s) and Appendix for current groundwater analytical data.
Refer to Table(s): Table 3
Refer to Appendix: Appendix B
• Historical Groundwater Analytical Data:
Total dissolved phase petroleum constituent compounds concentrations in monitoring
wells MW-1, MW-2, MW-3 and T-1 have increased in comparison to April 2002 data.
Refer to the following table(s) for historical groundwater analytical data.
Refer to Table(s): Table 4
' Texaco Food Mart #2
Lexington, Davidson County, North Carolina
Incident#: 22332
• Dissolved Phase Plume Size and Location:
Monitoring Report
December 21, 2007
Page3
The dissolved phase ethylbenzene plume is the largest contaminant plume greater than
the 15A NCAC 2L Groundwater Standards (2L Standards). It is elliptical in size and has
an approximate length of 105 feet and width of 50 feet. The isoconcentration maps can
be seen in the following Figures.
Refer to Figure(s): Figures 5 through 11
• Proximity of Plume to Nearest Receptor(s):
There are two (2) confirmed drinking water supply wells and five (5) inactive supply
wells located within 1,000 feet of the source area. The closest drinking water supply well
is located approximately 450 feet south of the site. No surface water bodies were
observed in the field or on the topographic map within 5O0-feet of the source area.
Refer to Table: Table 1
• Predictive Rate of Contaminant Transport:
The contaminant plume has been fairly immobile over the past several years, except for a
northwest/southwest plume migration. Contaminant transport is typically in the same
direction as groundwater flow, but with a slower velocity.
Refer to the following Table(s) and Figure(s):
Refer to Table(s):
Refer to Figure(s):
1.2.6 Other Field Data Collected:
Tables 2, 3 & 4
Figures 4 through 11
• A well sampling and field measurement log is included in Appendix A.
Texaco Food Mart #2
Lexington Davidson County, North Carolina
Incident#: 22332
2.0 CONCLUSIONS AND RECOMMENDATIONS
Monitoring Report
December 21, 2007
Page4
• Free product was not detected in site wells during this reporting period. The water table
depth has decreased by as much as 2 feet.
• Dissolved phase petroleum constituent compounds were detected in concentrations above
2L Standards in monitoring wells including MW-1, MW-2, MW-3 and T-1 during this
period. Extractable and volatile petroleum hydrocarbons were detected in a
concentration above the 2L standards in monitoring well MW-1, MW-2, MW-3 and
MW-5. Dissolved phase concentrations of benzene and 1,2-DCA in MW-2 were above
the NCDENR Gross Contaminant Levels (GCL).
• Dissolved phase petroleum constituent compound concentrations have increased in
monitoring wells MW-1, MW-2, MW-3 and T-1 since the last sampling event in April
2003.
• Two (2) privately owned water supply wells were identified within a 1,000-foot radius of
the source area with one confirmed drinking water supply well within 450 feet of the
source area.
• It is recommended that the remedial system installation previously approved by the
NCDENR be postponed at this time and instead conduct a month-long mobile multi-
phase extraction (MMPE) event be conducted on wells MW-1, MW-2, MW-3 and
possibly T-1 to reduce and accelerate this site towards closure.
• It is further recommended that monitoring wells MW-1,MW-2, MW-3,MW-4, MW-5
and T-1 be re-sampled approximately one month after completion of the MMPE event,
and the results be presented in a monitoring report to the NCDENR no longer than one
month after this sampling event.
• Further recommendations will be made based on the results of these recommended
activities.
,, Texaco Food Mart #2
Lexington Davidson County, North Carolina
Incident#: 22332
3.0 LIMITATIONS
Monitoring Report
December 21, 2007
Page5
Shield has performed environmental services at the subject site on behalf of Techno LLC for Holding
Brothers, Inc. Shield has performed this scope of work as an independent contractor/consultant using
reasonable care and skill in accordance and consistent with customary industry standards of
engineering, geology, and hydro geology practices. This standard of care is the sole and exclusive
standard of care that can be applied to measure Shield's performance of the work. No other
warranty, expressed or implied is made or intended by Shield.
The report has been prepared for the exclusive use by Techno LLC for Holding Brothers, Inc. All
recommendations, findings, and conclusions, made by Shield have been made to the best of Shield's
knowledge, opinion and belief, based upon information obtained during this scope of Techno LLC
for Holding Brothers, Inc. and Shield. Conclusions are provided with the understanding that Shield
is presenting information and not rendering legal advice. If such advice is needed, legal counsel
should be consulted. It is the responsibility of Techno LLC for Holding Brothers, Inc. under advice
of its counsel to notify the appropriate federal, state, or local public agencies as required by law; or
otherwise to disclose in a timely manner, any information that may be necessary to prevent damage
to human health, safety, or the environment.
Compliance with recommendations provided as part of this report in no way assures compliance with
federal, state and/or local laws, regulations, and/or requirements. Analytical data has been obtained
from Pace Analytical Services Inc. This information, to the extent that it was relied on to generate
this report, is assumed to be correct and complete. The work performed in conjunction with this
report and the data developed are intended as a description of available information at the dates and
specific locations given. Shield is not responsible for inspecting, examining, or reporting findings or
recommendations with respect to any conditions that were knowingly or unknowingly withheld,
concealed, hidden, or in any way not disclosed or observable at the time of this scope of work.
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0 TEM?-2 " MW-1 (NS) (NS)
CEDAR LANE ROAD
I GASOLINE UST
0
ii GASOLINE UST
SI w\SOLINl:UST
0 TEMP-1
(NS)
□DISPlaNSER
0 (NS) 1-lOT SAMPLED I APPROXIMATE GRAPHIC SCALE
0 MW-2 (NS)
-SH1~~D 4~01TAGGAFITCREEKROAD CHARLOTTE, NC 28208
704-894-81113
704--394-BBSSfax ENGINEERING, INC. www.,i, .. ,.,,,, .. ,.,,.oom
TOTAL XYLENES
ISOCONCENTRATION MAP
TEXACO FOOD MART #2
1700 COTTON GROVE ROAD
LEXINGTON, NORTH CAROLINA SHIELD fl 1001289
b NOTES: 1-GROUNDWATERSAMPLESCOLLECTEDON11l19/07. 0 15 3o DATE. 12/13/07 DRAWN BY. "' 2-ALL LOCATIONS ARE APPROXIMATE. M -! j • •
g 3-CONTOUR INTERVALS AS SHOWN. SCALE: 1in. = 30 ft, SCALE : AS S HQWN Fl GU RE :
RBS
8 ~L_ __________________________________ ....a....;..;....;..__--.,;,..;,;___,;._ .......... ___ _
~ ~
a! i
~ 8
i
f u ~
~ g
i ~ g
Cl.
LEGEND:
-¢-LIGHT POLI!
r:tf POWER POLE
EI.ECTl!lc:AL LINE
--~-SANITARYSEWERUNE
----PRODUCT LINE
TEXACO FOOD MART MONITORING WELL
TEXACO FOOD MART DEEP MONITORING WELL
AMOCO RU ALL DATA REPORTP DATI:04/1
-,t VE VAPOR ElCll!ACTJON wru
-,t AS AIR SPARGJNG WEU.
(uellt MICROGRAMS PER U1cR
MTBJ: MITHYl TERT-BlffYL ETHER
(6,090) MTBJ: CONCENTRATION (ugfL)
ASPHAI.T
[210) MTBE CONCENTRATION NOT USED IN CONTOURING (ug/L)
---MTBE ISOCONCENTRATION LINE (ug/L)
MW-4®
(2.3)
(ND) NOT DITECTED -!IELDW IABORA TORY MmiOO DE'!ECTION LIMITS
(NS) NOT SAMPLED
NOTES: 1· GROUNDWATER SAMPLES COLLECTED ON 11119/07,
Z-ALl LOCATIONS ARE APPROXIMATE.
3-CONTOUR llffl:RVAL5 AS SHOWN,
TANK
~
GASOLINE/
DISPEN>al~
REGUI.AI\ UST
M&*IAR
VACANTI.PT
UST
MW-6®
(NS)
PITI ASPHALT
I SUPREME UST
sue~
KERoSrnE UST
T-40
MW-1
{ND) T-2 @
□VERHEAD E:LECTii!IC
ACCESS ROAD
WENors PROPEIUY
· MW-5
@(ND)
@
MW· I ,(ND) i!!
PA!OONG AREA
□ DISPENSER
I
LI.I ~ Cl z §
§.
"" ..,
w e, TEMP-2 5 (NS) g
u z
CEDAR LANE ROAD
DISPENSER□
DISPENSER□
TW-1 0
(NS)
e MW-1
(NS)
I GASOLINE UST
; I GASOLINE UST
81 GASDl-lNE UST
el TEMP-1
(NS)
□DISP!,NSER
□DISPl'NSER
APPROXIMATE GRAPHIC SCALE
DIESEL UST
ONC
~ ~ ·< :-..: ::..:
:--::. ?: \: ::-:
' AMOCO RUSHCO#J ' '
'
' ~
0 MW-2 (NS)
S'lllE~D 4301TAGGARTCREEKROAO
CH'l.RLOTTE, NC 28208
704-Si4-8El1i 704,:SM-e"Slllfwc
ENGINEERING, INC. www,.,.,~'"""'"'"""""'"'
MTBE ISOCONCENTRA TION MAP
TEXACO FOOD MART #2
1700 COTTON GROVE ROAD
LEXINGTON, NORTH CAROLINA SHIELD# 1001289
DATE: 12/13/07 DRAWN BY: RBS
:i:L. ______________________________________________________________ .._ ________ .._ _______ _ SCALE: 1 in. = 30 ft. SCALE: AS SHOWN FIGURE: 9
~
.II! I ~ ~ ]l
:, 00 Li: ~ il'i
~ N g
6 g
N
LEGEND:
-Q-LIGHT POLE
Jd POWER POLE
ELECTRICAi. LINE:
SANITARY SEWER LINE
----PRODUCTUNE
@ TEXACO FOOD MART MONITORING WEU.
@ TEXACO FOOD MART DEEP MONITORING WELL
AMOCO RUSHCO #l MONITORING WEU.
ASPHALT
" :hl;8tH~~e6Rftc°k1lN'N'/,~5~..[EJIJl~.5~r.mr DATED 4/16/01.
,i,. VE VAPOR ElCTl!ACTION WEU.
-,t--A5 AIR SPARGING WELL
(u;IL) MICROGRAMS PER UT£R
(1,1501 1,2·DICHLOROETHANE (DCA) CONCENrnATIDN (u81L/
MW-4@
(ND)
[1.7] 1,2-DICHLOROETIJANE (OCA) CONCENTRATION NOT USED IN CONTOURING (ug/L)
1 ,Z·DICHLOROE'THANE (DCA) ISOCONCEN'!RATION LINE (ug/L)
(ND) NOT DETECT· BELOW LABORATORY METHOD DETECTION LIMlT5
(NS) NOTSM\PLED
REGULAR
UST
REGULAR UST
VACANT LOT
u
PITI ~---~
I SUPREME UST
KER0591E UST
ASPHALT
MW-6@
(NS)
DVE"RHEAll ELECTR?C
ACCESS ROAD
WENPY'S PROPERTY
MW-5 @(ND)
PARKING AREA
□ DISPENSER
Oo1SPENSER DISPENSER□
TW-1 0
(NS)
-' TEMP-2 " MW-1 (NS) (NS)
CEDAR LANE ROAD
I GASOLINE UST
0 ii u/lSOUNE UST
81 G,\501.INE UST
0 TEMP-1
(NS)
DIESEL UST
CONC P
□DISPENSER
□DISPENSER
AMOCO
RUSHC0#3
"'MW-2
(NS)
SRIELD 4301TAGGAATCR=~OAD
CH!\RLOTTE, NC 28208
704-3B4-1913 704-394..e9BB f8lr. ENG/NEER/NG, /NC. www.,hlold"'''"',."i-"""'
1,2-DICHLOROETHANE (DCA)
ISOCONCENTRATION MAP
TEXACO FOOD MART #2
~ APPROXIMATE GRAPHIC SCALE
~~"' Nom: 1-uR□UNOWATER.>AMPLESC01.LECTEDoN11119101. 'L _j5 2o DATE: 12/14/07 DRAWN BY: RBS • Z· ALL LOCATIONS ARE APPROXIIMTE. ~ _ ~
n. 3-CONTOURINTERVAl.SASSHOWN. SCALE: 1 in,olOFt. SCALE: A5 SHOWN FIGURE; 10
170D COTTON GROVE ROAD
LEXINGTOtt !"ORTH CAROLINA SH!tw # 1001289
::i:L.------------------------------------------------------------------------------------------------------------
I:; ~
I ..
lil ...
§
1
{
G ill
0'> ~ 8 i ~ §
i
LEGEND:
N
UGHTPOLE
POWER POLE
ELECTlllCAL LINE
SANITARY SEWER LINE
e
~
~
ASPHALT ~
w
w --
----PRODUCT UNI;
TUACO FOOD MART MONITORING WELL
TEXACO FOOD MART DEEP MONITORING WEil.
¾i°~M. 'fR~NfWRt~1Wil-t.1M11ED SITT: ASSESSMENT REPORT P D BY CBM ENVJRDMENTA!. SERVICES, INC. 0ATED41
VAPOR OORACTIONWEU.
AIR SPARGING WELL
MICROGRAMS PER LITER
NAPH'!HALENE CONCENlllATION (ug/L)
MW-4@
(ND)
0
..i,. VE
..i,. AS
(us/LJ
(1,0!IO)
[NDJ NAPHTHALENE CONCENTRATION NOT USED IN CONTOURING (ug/LJ
----NAPH'TliALENE ISOCONCENTRATION LINE (uS/LJ
(ND)
(NSI
NOT DETECTED· BELOW LABORATORY MrniOD DETECTION LlMll>
NOT SAMPLED
NOTES: 1-GROUNDWATER SAMPL.fS COLLECTED ON 11/19107.
2-ALL LOCATIONS ARE APPROXIMATE.
3-CONTOUR INTERVALS AS SHOWN
VACANTI.OT
<:,~
I REGULAR UST
PIT! Rf@*l.AR
I SUPREME UST
I sut~
2 <,""' '· ' ,::: \,
Gl>.SOLINE~ -:; ' ' DISPENSER :;: TEXACO ' ~ FOOD MART >,
llV£'.Rl-lEAD E:LE::crn1c
ACCESS ROAD
WEIIDY'S PROPf!m l MW-5
@ ND)
MW-6@
(NS)
PARKING AREA
I ..... > ~ l.:;l z: ~ §,
!lE ..... !:i g
u z
□ DISPENSER
□DISPENSER
0 TEMP·Z
(NS)
CEDAR LANE ROAD
DISPENSER□
DISPENSER□
TW-10
{NS)
0 MW•1
(NS)
I GASOIJNEUST
i l uASOUNEUST
8 I GASOLINE UST
0 TEMP•1
(NS)
APPROXIMATE GRAPHJC SCALE
o 15 :l P:Siiii -I ~
OIESEL UST
AMOCO RU5HC0#3
0MW-2 (NS)
-S1l1F.~D 4301TA.GGARTCREEKROAIJ
CHAALOTTE, NC 28208
704-394-5:813 ,....=gs,r... ENG/NEER/NG, {NC. www.ohle!O•..,,,..r1ng . .,,.
DATE:
NAPHTHALENE
ISOCONCENTRATION MAP
TEXACO FOOD MART #2
1700 COTTON GROVE ROAD
LEXINGTON, NORTH CAROLINA
SHIELD fl 1001289
12/14/07 DRAWN BY: RBS
:i:1...---------------------------------------------------------------------------------------SCALE: 1 In. • 30 ft. SCALE: AS SHOWN FIGURE: 11
-------•-····--·----------------------------·--·----·--···-------· ----•,--•·---·--·-··
Table: 1
Summary of Adjacent Property and Water Supply Well Owners
WSW-I Flowerest 0. Lopp
WSW-2 Paul & Stella Baker
WSW-3 Margaret H. Fuller
WSW-4 Hoyle R. Smith
Efird E. Jr. & Kay S.
WSW-5 Wilson
(owner)
WSW-6 Abe Cassidy
WSW-7 Mrs. Samuel C. Davis
WSW-8 Maxine C. Houck
WSW-9 Thomas Frank
WSW-10 James G. Henderson
WSW-11 Ray S. & Irene Musgrave
WSW-12 Aubrey & Helen Brewer
WSW-13 John T. Tetter
Nbtes: Ft BGS = feet below ground surface
Texaco Food Mart #2
1700 Cotton Grove Road,
Lexington, North Carolina
NCDENR Incident# 22332
P.O. Box 284 Lexington, NC 336-357-Di-inking 2511
104 Fuller Rd., Lexington, NC 336-357-Not in Use 5231
l 06 Fuller Rd., Lexington, NC 336-357-Not in Use 2659
115 Cedar Ln., Lexington, NC 336-357-Drinking 2916
336-249-6 Mayfair Rd., Lexington, NC* 3266 Not in Use
Box 8 Mayfair Rd., Lexington, 336-357-Not in Use NC 2485
Box 100 Mayfair Rd., 336-357-Not in Use Lexington, NC 2565
Box l 08 Mayfair Rd., NA Drinking Lexington, NC
Box 107 Mayfair Rd, NA Not in Use Lexington, NC
Box 103 Mayfair Rd., NA Not in Use Lexington, NC
1724 Southview Rd., NA Not in Use Lexington, NC
102 Mayfair Rd., Lexington, NA Irrigation NC
104 Mayfair Rd., Lexington, NA Drinking NC
Address of well. Property owner's address is 500 Maegeo Dr .• Lexington
185 4" ?
? ? ?
? ? ?
? ? ?
? ? ?
? ? ?
? ? ?
>100 4" ?
? ? ?
? ? ?
? ? ?
? ? ?
? ? ?
?
?
?
?
?
?
?
?
?
?
?
?
?
Of the property owners without PWS hook ups, only John Tetter is interested in be added to the PWS. Other pmperty owners indicated that they are not interested at all. . NA -Not Accessible
450' No
700' Yes
650' Yes
985' No
750' Yes
760' Yes
795' Yes
1025' No
1090' Yes
1100' Unk.
1175' Unk.
800' Yes
850' No
Top of
Well ID Date Casing
Installed Elevation
(feet)
lV.lW-1. 07/31/01 100.00
Mw-2 07/31/01 100.19
lVlW-3 lU/08/01 100.19
Mw-4 10/08/01 99.40
lVIW-5 04/04/02 100.39
1VIW•6 04/04/02 lul.42
T-1 10/uy/0l IOU.55
Notes:
1. NM ;; Not Measured.
• 2. NA ;; Not Applicable.
Table 2:
Summary or Well Construction and Historical Groundwater Elevation Data
Texaco Food Mart #2
Well
Diameter
(inches)
2
2
2
2
'l,
2
2
1700 Cotton Grove Road, Lexington, North Carolina
NCDENR Incident# 22332
Field Measurements
As-built Total Depth to
Depth Screened Gauging Date Depth Static
Interval (£eet) Water -(feet) (feet) (feet)
35 20-35 Hl/.lU/U.1. 35.0u 24.U9
04/22/0Z 35.00 22.13
11/19/07 35.01 23.69
35 20-35 10/IU/Ul .1:,.00 24.22
04/22/02 35.00 22.08
11/19/07 34.75 23.84
35 20-35 IU/10/01 35.00 24.27
04/22/U2 35.00 21.93
11/19/07 35.03 24.10
35 20-35 lU/.lU/U.l 35.00 24.II
04/22/U2 35.00 21.91
11/19/07 34.81 23.88
3.5 20-35 ■Ill.I .r'J /11', 35.00 23.34
11/19/07 35.07 24.76
25 15-25 '!..a:,=: .!rL!IJi. 25.00 23.0Z
11/19/07 25.00 NM
90 85.5-90 10/lU/Ul 90.00 24.93
04/22/02 90.00 22.06
11/19/07 86.71 21.59
Sum of well construction and historical groundwater elevation
Field Calculations
Depth to DitT. Between Ground-water Free As-Built and Elevation Product Measured Total
(feet) Depth (feet) (feet)
NA 0 7.5.91
NA 0 77.87
NA -0.01 76.31
NA 0 75.78
NA 0 77.92
NA 0.25 76.35
NA 0 75.92
NA 0 78.26
NA -0.03 76.09
NA 0 76.08
NA 0 78.28
NA 0.19 75.52
NA 0 7o.8.5
NA -0.07 75.63
NA 0 77.17
NA 0 NM
NA 0 75.20
NA 0 78.13
NA 3.29 78.76
Page 1 of 1
"Cl .. .. = 'E. .. .. ... e = = N ... ... = Well ID OI N = ...
UJ = "S ,Cl ... ;:. .. IZl E-< --= OI -Q r..:i
(ug/L) (ug/L) (ug/L)
lSA NCAC 2L.0202
Standard---> 1 1,000 550
15A NCAC 2L.0115
Gross Contamination
level-> 5,000 257,500 84,500
MW-1 11/19/07 49.5 64.7 179
MW-2 11/19/07 14,900 34,200 3,090
MW-3 11/19/07 ND 4,850 2,190
MW-4 11/19/07 ND ND ND
MW-5 11/19/07 ND ND ND
T-1 11/19/07 43.8 ND ND
NOTES:
I. ug/1 = Micrograms per liter
2. Bold numbers exceed the NCAC 2L .0202 limit
Table:3
Summary of Analytical Results -Groundwater Samples
Texaco Food Mart #2
1700 Cotton Grove Road
Lexington, North Carolina
NCDENR Inciden1#:22332
EPA Method 601/602
,-. ... cc .. 0 iii" ~ -= ... .. Ca;1 -= -rri .. .. OI
.._, u u .., ,.!, -= .. .. ... --= r I = ... .. -"Cl = °' °' ~ .... ... ·e i c:, -::I -s:. 0 ,Cl lo, 0 u u >< I Cl. 0 lo, -= ._, ._, .... 0 ~ ,Cl .... "' "' -; .. .. -= ... ... .. Q. ... :a Cl. ·,e ·,e -.... 0 iS OI 0 ~ OI OI E-< "' .. z -= -= "' I C -= iS "l ... a. a. --;:. ~ ~ ., -::; -= -rilil
(ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L)
530 200 70 0.38 0.004 21 4,200 42,000
87,500 200,000 70,000 380 50 · 15,500 --
1,210 ND ND ND ND 219 665 ND
18,400 6,090 ND 1,150 ND ND 33,900 308
13,600 ND ND ND ND 1,090 3,460 ND
ND 2.3 ND ND ND ND. ND ND
ND ND ND ND ND ND ND ND
ND 210 ND 1.7 ND ND ND ND
3. ND= Not detected at or above the method detection limit specified in the laboratory report
4. NR = Not requested ..
MADEP EPH-VPH
R QC N = u u I I -W'l -c:, u u ._, ._,
"' "' ... ... ; ·= OI OI e -= 0 a. .. ~ <
(ug/L) (ug/L)
210 420
---
825 ND
17,000 60,100
2,440 NR
ND ND
ND 144
ND ND
5. Gross Contaminant Level as presented in the NCDENR "Guidelines for Assessment and Corrective Action" dated April 2001 effective July 2001 _
H:\Projects\2000\ 1001289\Tables\groundwater table_ 11_ 19_ 07\Groundwater Analytical Results-11_ 2007
EPA Method
625
R 6' --u u .. r I
°' C"I = c:, c:, ... ";i u u ._, ._, -= .., .. .... ... ... -= -,e ·:: Q. 1"I al OI -= e z ci. 0 ~ ... -(
(ug/L) (ug/L) (ug/L)
4,200 210 21
--15,500
ND ND 107
37,700 9,630 1,090
NR NR 513
ND ND ND
ND ND 41
ND ND ND
Analytical Method->
.. "' = = "" "' N = C Q .., = E-
15A NCAC 2L.0202 1 1,000 Standard->
15A NCAC 2L.0115
Gross Contamination 5,000 257,500
lou•-->
Location Date u2;/L ue'l,
MW-1 07/31/01 ND 53
04/30/03 12 340
ll/19/07 49.5 64.7
MW-2 07/31/01 13,000 38,000
04/30/03 12,000 29,000
11/19/07 14,900 34,200
MW-3 10/10/01 120 4,300
04/30/03 100 3,000
11/19/07 ND 4,850
MW-4 lO/l0/01 ND ND
04/30/03 ND ND
l l/19/07 ND ND
Hc'Projects\2000\ 1001289\Tables\Sum of HISTORICAL GW Analylica/
Table 4:
Summary of Historical Analytical Results-Groundwater Samples
Texaco Food Mart #2
1700 Cotton Grove Road
Lexington, North Carolina
NCDENR Incident# 22332
EPA EPA EPA
EPA Method 601/602 Method Method Method
504.1 JOJOC 625 .. ~ iii' .. ~ .c 0. 41 8 i:i e ., .. .. .. .. -.. C <l,I b lo :S .. C .. i C a ~ ... .. ~ ., Q -= >-. .c -a; .. Q "' .. X ~ O:I .c .c .!. ;:, .. .. :c .c >. .; .. ...:i .. Q,, u :a Q,, -= ~ ... Q Q .. -.. .. i;.i E-;:, Q,, C z. : Q .... .2:l .. -!!l .... >-. :::.: Q : ""
550 530 200 70 0.38 0.0004 15 21
84,500 87,500 200,000 70,000 380 50 15,000 15,500
Ul>'/L ue'l, ulill. ue/L ue'l, ue'L ue'L ue'L
340 1,300 NR NR ND 0.96 ND 75
13 1,470 NR ND ND NR NR 270
179 1,210 ND ND ND ND NR 107
3,600 16,000 NR NR 1,200 720 ND NR
2800 16,700 NR ND 1,700 ND NR 1,400
3,090 18,400 6,090 ND 1,150 ND NR 1090
1,800 8,600 NR NR ND 9.5 ND 360
1,600 8,800 NR ND ND ND NR 660
2,190 13,600 ND ND ND L2 NR 513
ND ND NR ND ND ND ND ND
ND ND NR ND ND NR NR ND
ND ND 2.3 ND ND ND NR ND
MADEP MADEP MADEP MADEP MADEP MADEP
VPH VPH VPH EPH EPH EPH
,-, ,...,_ ,-.., G N' ,-, !::3 0 QO ... --M .... u ' y y u u y I I ..!. .,, °' °' °' ~ s u ~ u s \:::, _, ., _, u u u -.c -.c -.c -.c '-' ...
O:I -.c -.c -= "' .. "' O:I .. .c -= -= Q,, Q,, :t i -= -= ~ ~ .e-i < :;;:
420 4,200 4,200 42,000 210 210
---------------
Ul:,fl ue'L U!"/1 ue/L ue/L ue'L
ND 2,800 2,300 670 ND 480
NR NR NR NR NR NR
ND ND ND 665 ND 825
81,000 28,000 9,100 NR NR NR
NR NR NR NR NR NR
60,100 37,700 9,630 33,900 308 17,000
ND 11,000 11,000 990 ND 710
NR NR NR NR NR NR
NR ND ND 3,460 ND 2,440
NR NR NR NR NR NR
NR NR NR NR NR NR
ND ND ND ND ND ND
Page 1 of2
Table 4:
Summa..-y of Historical Analytical Results-Groundwater Samples
Texaco Food Mart #2
1700 Cotton Grove Road
Lexington, North Carolina
NCDENR Incident# 22332
EPA EPA EPA MADEP Analytical Method-> EPA Method 601/602 Method Method Method
"' ,= ..,
"' = ..
Q:I
ISA NCAC 2L.0202 1 Standard-->
ISA NCAC 2L.0115
Gross Contamination 5,000
... ..,.->
Location Date m>/l
MW-5 04/30/03 ND
11/19/07 ND
T-1 10/10/01 390
04/30/03 17
11/19/07 43.8
Notes:
ug/1 = Micrograms per liter.
NR = Analysis not requested.
MDL= Method Detection Limit
., = ... "' ,= .. .. ,= = ...
Q .c ;:, !-.c ~
1,000 550
257,500 84,500
us>/l u!!IL
ND ND
ND ND
7.8 9.4
2.8 ND
ND ND
Bold numbers exceed 15A NCAC 2L.0202 standards.
.. ., = ~ ;a<
"ii 0 !-
530
87,500
us>/1
ND
ND
140
14.7
ND
504.1 J0J0C 625 .. GS = ., Q -= C. ., f:!, ~ ,= r.i .. ., ., ... £i ~ "t:l = "' ., ·e .!!! ::, ; Q "2 ... ... Q "t:l ..
.2 ... .. ,s ;:, .c .., ... C. -= ...;i -= ~ i5 :s C. Q .. ;:, ... "' ;z C. = .c ~ "' ~ ... ..; "' a >, ~ .c ~
200 70 0.38 0.0004 15 21
200,000 70,000 380 50 15,000 15,500
U<'ll u!!/L u!!/L UP/I u!!/L uv/l
NR NR ND NA ND ND
ND ND ND ND NR 41
NR NR 44 2.8 ND 24
NR ND 8.1 ND NR 3.1
210 ND 1.7 ND NR ND
15A. NCAC 2L.0202 = NCDENR Standard Statute for non-risked based maximum allowable containment concentration in groundwater
Gross Contaminant Levels= NCDENR Standard Statute for risked based maximum gross
H:lProjec/s12000\1001289\Tab/eslSum of HISTORICAL GW AnalyticaJ
VPH
,-.. °l' y .,..
~ ...
:Cl OS .c C. = <
420
--
u!!/L
NR
144
850
NR
ND
MADEP MADEP MADEP MADEP MADEf
VPH VPH EPH EPH EPH
,-.. ,-.. ,-.. ,-.. N' !:! s co \0 -<-;> ~ ~ ' ~ u u u I I ' ~ -°' °' "" -~ ~ ~ 2 2 u u .... :Cl :Cl :Cl u u :Cl :0 .. OS .. OS .. .c .c .c -= .c C. l Q,, ~ = C. ~ < ~ <
4,200 4,200 42,000 210 210
-------------
uv/l u!!/L ul?IL ue/L ug/L
NR NR NR NR NR
ND ND ND ND ND
270 250 ND ND ND
NR NR NR NR NR
ND ND ND ND ND
Page 2 of 2
Client
Name: Holding Brothers
MW-01 100.00 35.01 23.69 NA NA
MW-02 100.19 34.75 23.84 NA NA
MW-03 100.19 35.03 24.10 NA NA
MW-04 99.40 34.81 23.88 NA NA
MW-05 100.39 35.07 24.76 NA NA
MW-06 101.42 NM NM NA NA
T-1 100.35 86.71 21.59 NA NA
Date: 11/19/07
Sampled by: _S_P _______ _
Weather Conditions: Sunny 55
Laboratory: _P_a_c_e_L_a_b ______ _
Page 1 of 1
H:\Assessment\2000\1001289\ncwellsamplelog
Task:
11.32 1.8
10.91 1.78
10.93 1.78
10.93 1.78
10.31 1.68
NA NA
65.12 10.6
Project
Name: Texaco Food Mart #2
Chain of
Custody 6SHIELD T"'" ENGINEERING, INC.
#:
5.5
5.3 16:00
5.3 15:45
5.3
5 15:15
NA NA
31.8 15:00
Corrected depth to water = Static depth to water (C) -{Product thickness x specific gravity) Volume Coefficient
Specific Gravities
Gasoline .75
Diesel .82
1" = .04 gal/lin. Ft
2" = .16
3" = .37
4" = .65
6" = 1.47
8" = 2.60
10" =4.1
12"= 5.9
December 05, 2007
Ms. Colleen Clark
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: TEXACO FOODMART #2
Pace Project No.: 928366
Dear Ms. Clark:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on November 21, 2007.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
j~)8_
Kevin Herring 4
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Page 1 of 32
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Charlotte Certification IDs
North Carolina Drinking Water Certification Number: 37706
North Carolina Wastewater Certification Number: 12
North Carolina Field SeNices Certlflcation Number: 5342
South Carolina Certification Number: 990060001
South Carolina Bioassay Certification Number: 990060003
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Louislana/LELAP Certification Number: 03095
New Jersey Certification Number: NC011
North Carolina Drinking Water Certification Number: 37712
North Carolina Wastewater Certification Number: 40
North Carolina Bioassay Certification Number: 9
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738
Virginia Drinking Water Certification Number: 00424
Pace Analytical Services, Inc.
2225 Riverside Dr.
CERTIFICATIONS
Asheville, NC 28804
[phone]
Tennessee Certification Number: 04010
Virginia Certification Number: 00213
Florida/NELAP Certification Number: E87627
Kansas Certification Number: E-10364
Louisiana/LELAP Certification Number: 04034
Pennsylvania Certification Number: 68~03578
South Carolina Certification Number: 99030001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, N½ 28078
[phone]
South Carolina Bioassay Certification Number: 99030002
Tennessee Certification Number: 2980
Virginia Certification Number: 00072
North Carolina Wastewater Certification Number: 633
REPORT OF LABORATORY ANALYSIS Page 2 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
( 828 )254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-1
Parameters
MADEP EPH NC Water
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane {S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
601/602 Volatiles
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
·1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Diisopropyl ether
Ethyl benzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
m&p-Xylene
Date: 12/05/200711:27 AM
LablD: 928366001 Collected: 11/19/0716:30 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed GAS No.
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
665 ug/L
ND ug/L
825 ug/L
83 %
107 %
94 %
111 %
Analytical Method: EPA 601/602
49_5 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
179 ug/L
ND ug/L
ND ug/L
219 ug/L
ND ug/L
ND ug/L
64.7 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1210 ug/L
827 ug/L
116
116
116
40-140
40-140
40-140
40-140
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
20.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
20.0 10
10.0 10
20.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
10.0 10
20.0 10
20.0 10
11/27/07 00:00 11/30/0715:44
11/27107 00:00 11/30/0715:44
11/27107 00:00 11/30/0715:44
11/27/07 00:00 11/30/07 15:44 7194-86-7
11/27/0700:00 11/30/0715:44 84-15-1
11/27107 00:00 11/30/0715:44 321-60-8
11/27107 00:00 11/30/07 15:44 580-13-2
12/01/07 21:46 71-43-2
12/01/07 21:46 75-27-4
12/01/07 21 :46 75-25-2
12/01/07 21 :46 74-83-9
12/01/07 21:46 56-23-5
12/01/07 21:46 108-90-7
12/01/07 21 :46 75-00-3
12/01/07 21 :46 67-66-3
12/01/07 21:46 74-87-3
12/01/07 21 :46 124-48-1
12/01/07 21 :46 106-93-4
12/01/07 21 :46 95-50-1
12/01/07 21:46 541-73-1
12/01/07 21:46 106-46-7
12/01/07 21 :46 75-71-8
12/01/07 21:46 75-34-3
12/01/07 21:46 107-06-2
12/01/07 21 :46 75-35-4
12/01/07 21:46 156-59-2
12/01/07 21:46 156-60-5
12/01/07 21 :46 78-87-5
12/01/07 21 :46 10061-01-5
12/01/07 21:46 10061-02-6
12/01/07 21 :46 108-20-3
12/01/07 21 :46 100-41-4
12/01/07 21:46 75-09-2
12/01/07 21 :46 1634-04-4
12/01/07 21:46 91-20-3
12/01/07 21 :46 79-34-5
12/01/07 21 :46 127-18-4
12/01/07 21:46 108-88-3
12/01/07 21 :46 71-55-6
12/01/07 21 :46 79-00-5
12/01/07 21 :46 79-01-6
12/01/07 21 :46 75-69-4
12/01/07 21 :46 75-01-4
12/01/07 21 :46 1330-20-7
12/01/07 21 :46 1330-20-7
Qual
REPORT OF LABORATORY ANALYSIS Page 3 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
1W~\1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Ashevil!e, NC 28804
(828 )254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 926366
Sample: MW-1 LablD: 928366001 Collected: 11/19/07 16:30 Received: 11/21/07 06:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 601/602
a-Xylene 382 ug/L 10.0 10 12/01/07 21:46 95-47-6 1-Chloro-3-fluorobenzene ( S) 95 % 65-137 10 12/01/07 21:46 625-98-9
MADEP VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C06) ND ug/L 5000 50 11/30/07 21 :03
Aliphatic (C09-C12) ND ug/L 5000 50 11/30/07 21 :03
Aromatic (C09-C10) ND ug/L 5000 50 11/30/07 21 :03
2,5-Dibromotoluene (PID)(S) 125 % 70-130 50 11/30/07 21 :03
2,5-Dibromotoluene (FID)(S) 118 % 70-130 50 11/30/07 21 :03
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 5.9 11/21/07 00:00 11 /26/07 22:42 83-32-9
Acenaphthylene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 208-96-8 Anthracene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 120-12-7 Benzo(a)anthracene ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 56-55-3 Benzo(a)pyrene ND ug/L 5.9 11 /21 /07 00:00 11 /28/07 22:42 50-32-8
Benzo(b)fluoranthene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 191-24-2
Benzo(k)fluoranthene ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 101-55-3
Butyl benzyl phtha late ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 11.8 11/21/07 00:00 11/26/07 22:42 111-91-1
bis(2-Chloroethyl) ether ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 108-60-1
2-Chloronaphthalene ND ug/L 5.9 11/21/07 00:00 11 /28/07 22:42 91-58-7
2-Chlorophenol ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 95-57-6
4-Chlorophenylphenyl ether ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 7005-72-3
Chrysene ND ug/L 5.9 11/21/07 00:00 11 /26/07 22:42 218-01-9 D ibenz( a, h )a nthracene ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 53-70-3 3,3'-Dichlorobenzidine ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 91-94-1 2,4-Dichlorophenol ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 120-83-2 Diethylphthalate ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 84-66-2
2,4-Dimethylphenol ND ug/L 11.8 11/21/07 00:00 11/28/07 22:42 105-67-9
Dimethylphthalate ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 131-11-3
Di-n-butylphthalate ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 23.5 11/21/07 00:00 11/28/07 22:42 534-52-1 2,4-Dinitrophenol ND ug/L 58.8 11/21/07 00:00 11/28/07 22:42 51-28-5 2,4-Dinitrotoluene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 121-14-2 2,6-Dinitrotoluene ND ug/L 5.9 11/21/07 00:00 11 /26/07 22:42 606-20-2 Di-n-octylphthalate ND ug/L 5.9 11/21/07 00:00 11/26/07 22:42 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 117-61-7
Fluoranthene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 206-44-0 Fluorene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.9 11/21/0700:00 11/28/07 22:42 87-66-3 Hexachlorobenzene ND ug/L 5.9 11/21/07 00:00 11/28/07 22:42 118-74-1
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 4 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .. -·fkf t~, .. 0/ OC'•' :; .. , . Ji
Paco Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-1
Parameters
625 MSSV
Hexachlorocyclope:ntadiene
Hexachloroethane
I ndeno( 1,2,3-cd)pyrene
lsophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4--Nitrophenol
N-Nitrosodimethylamine
N-Nitroso~di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12/05/2007 11 :27 AM
Lab ID: 928366001 Collected: 11/19/07 16:30 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 11.8 11 /21 /07 00:00
ND ug/L 5.9 11/21 /07 00:00
ND ug/L 5.9 11/21/07 00:00
ND ug/L 11.8 11/21/07 00:00
107 ug/L 5.9 11/21/07 00:00
ND ug/L 5.9 11/21/07 00:00
ND ug/L 5.9 11/21/07 00:00
ND ug/L 58.8 11/21/07 00:00
ND ug/L 5.9 11/21/07 00:00
ND ug/L 5.9 1 11 /21 /07 00:00
ND ug/L 11.8 1 11 /21 /07 00:00
ND ug/L 29.4 1 11/21/07 00:00
ND ug/L 5.9 1 11/21/07 00:00
ND ug/L 5.9 1 11/21/07 00:00
ND ug/L 5.9 1 11/21/07 00:00
ND ug/L 5.9 11/21/07 00:00
ND ug/L 11.8 11/21/07 00:00
80 % 10-120 11/21/07 00:00
55 % 15-120 11/21/07 00:00
67 % 11-131 11/21/07 00:00
38 % 10-120 11/21/07 00:00
34 % 10-120 11 /21 /0700:00
102 % 10-137 11 /21 /07 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
lti;J~t;,
Analyzed CAS No.
11/28/07 22:42 77-47-4
11/28/07 22:42 67-72-1
11 /28/07 22:42 193-39-5
11 /28/07 22:42 78-59-1
11 /28/07 22:42 91-20-3
11/28/07 22:42 98-95-3
11/28/07 22:42 88-75-5
11/28/07 22:42 100-02-7
11/28/07 22:42 62-75-9
11 /28/07 22:42 621-64-7
11 /28/07 22:42 86-30-6
11/28/07 22:42 87-86-5
11/28/07 22:42 85-01-8
11/28/07 22:42 108-95-2
11/28/07 22:42 129-00-0
11/28/07 22:42 120-82-1
11/28/07 22:42 88-06-2
11/28/07 22:42 4165-60-0
11/28/07 22:42 321-60-8
11/28/07 22:42 1718-51-0
11/28/07 22:42 13127-88-3
11 /28/07 22:42 367-12-4
11/28/07 22:42 118-79-6
Qual
Page 5 of 32
;2ceAnatyticat•
( www.paoo/sbs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
I 828 )254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, 'NC 28078
(704)875-909~
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-2 LablD: 928366002 Collected: 11/19/0716:00 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) 33900 ug/L 2810 25 11/27/07 00:00 12/03/07 12:10
Aliphatic (C19-C36) 308 ug/L 112 1 11/27/07 00:00 11/30/07 16:24
Aromatic (C11-C22) 17000 ug/L 562 5 11/27/07 00:00 12/03/07 12:10
Nonatriacontane (S) 86 % 40-140 11/27 /07 00:00 11/30/0716:24 7194-86-7
o-Terphenyl (S) 0% 40-140 5 11/27/07 00:00 12/03/0712:10 84-15-1 S4
2-Fluorobiphenyl (S) 0% 40-140 5 11/27/07 00:00 12/03/0712:10 321-60-8 S4
2-Bromonaphthalene (S) 0% 40-140 5 11/27/07 00:00 12/03/07 12:10 580-13-2 S4
601/602 Volatiles Analytical Method: EPA 601/602
Benzene 14900 ug/L 500 500 12/01/07 02:13 71-43-2
Bromodichloromethane ND ug/L 500 500 12/01/07 02:13 75-27-4
Bromoform ND ug/L 500 500 12/01/07 02:13 75-25-2
Bromomethane ND ug/L 500 500 12/01/07 02:13 74-83-9
Carbon tetrachloride ND ug/L 500 500 12/01/07 02:13 56-23-5
Chlorobenzene ND ug/L 500 500 12/01/07 02:13 108-90-7
Chloroethane ND ug/L 500 500 12/01/07 02:13 75-00-3
Chloroform ND ug/L 500 500 12/01/07 02:13 67-66-3
Chloromethane ND ug/L 1000 500 12/01/07 02:13 74-87-3
Dibromochloromethane ND ug/L 500 500 12/01/07 02:13 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 500 500 12/01/07 02:13 106-93-4
1,2-Dichlorobenzene ND ug/L 500 500 12/01/07 02:13 95-50-1
1,3-Dichlorobenzene ND ug/L 500 500 12/01/07 02:13 541-73-1
1,4-Dichlorobenzene ND ug/L 500 500 12/01/07 02:13 106-46-7
Dichlorodifluoromethane ND ug/L 500 500 12/01 /07 02: 13 75-71-8
1, 1-Dichloroethane ND ug/L 500 500 12/01/0702:13 75-34-3
1,2-Dichloroethane 1150 ug/L 500 500 12/01/07 02:13 107-06-2
1, 1-Dichloroethene ND ug/L 500 500 12/01/07 02:13 75-35-4
cis-1,2-Dichloroethene ND ug/L 500 500 12/01/07 02:13 156-59-2
trans-1,2-Dichloroethene ND ug/L 500 500 12/01/07 02:13 156-60-5
1,2-Dichloropropane ND ug/L 500 500 12/01 /07 02: 13 78-87-5
cis-1,3-Dichloropropene ND ug/L 500 500 12/01/07 02:13 10061-01-5
trans-1,3-Dichloropropene ND ug/L 500 500 12/01/07 02:13 10061-02-6
Diisopropyl ether ND ug/L 500 500 12/01/07 02:13 108-20-3
Ethylbenzene 3090 ug/L 500 500 12/01/07 02:13 100-41-4
Methylene Chloride ND ug/L 1000 500 12/01/07 02:13 75-09-2
Methyl-tert-butyl ether 6090 ug/L 500 500 12/01/07 02:13 1634-04-4
Naphthalene ND ug/L 1000 500 12/01/07 02:13 91-20-3
1, 1,2,2-Tetrachloroethane ND ug/L 500 500 12/01/07 02:13 79-34-5
T etrachloroethene ND ug/L 500 500 12/01/07 02:13 127-18-4
Toluene 34200 ug/L 1000 1000 12/01/07 22:28 108-88-3
1, 1, 1-Trichloroethane ND ug/L 500 500 12/01/07 02:13 71-55-6
1, 1,2-Trichloroethane ND ug/L 500 500 12/01/07 02:13 79-00-5
Trichloroethene ND ug/L 500 500 12/01/07 02:13 79-01-6
Trichlorofluoromethane ND ug/L 500 500 12/01/07 02:13 75-69-4
Vinyl chloride ND ug/L 500 500 12/01/07 02:13 75-01-4
Xylene (Total) 18400 ug/L 1000 500 12/01/07 02:13 1330-20-7
m&p-Xylene 11700 ug/L 1000 500 12/01/07 02:13 1330-20-7
Date: 12/05/200711:27 AM REPORT OF LABORATORY ANALYSIS Page 6 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .. ~1:~-0~~ . c: 1 _ a ,;
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-2 Lab ID: 928366002 Collected: 11/19/0716:00 Received: 11 /21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 601/602
a-Xylene 6680 ug/L 500 500 12/01/07 02:13 95-47-6
1-Chloro-3-fluorobenzene (S) 100 % 65-137 500 12/01/07 02:13 625-98-9
MADEP VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08) 60100 ug/L 1000 10 11/30/07 21 :25
Aliphatic (C09-C12) 37700 ug/L 1000 10 11/30/07 21 :25
Aromatic (C09-C10) 9630 ug/L 1000 10 11/30/07 21 :25
2,5-Dibromotoluene (PID)(S) 124 % 70-130 10 11/30/07 21 :25
2,5-Dibromotoluene (FID)(S) 117 % 70-130 10 11/30/07 21 :25
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 83-32-9
Acenaphthylene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 208-96-8
Anthracene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 120-12-7
Benzo(a)anthracene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 56-55-3
Benzo(a)pyrene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 50-32-8
Benzo(b)fluoranthene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 205-99-2
Benzo(g,h,i)perylene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 191-24-2
Benzo(k)fluoranthene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 207-08-9
4-Bromophenylphenyl ether ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 101-55-3
Butylbenzylphthalate ND ug/L 55.6 10 11/21/0700:00 11/30/07 02:01 85-68-7
4-Chloro-3-methylphenol ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 111 10 11/21/07 00:00 11/30/07 02:01 111-91-1
bis(2-Chloroethyl) ether ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 108-60-1
2-Chloronaphthalene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 91-58-7
2-Chlorophenol ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 95-57-8
4-Chlorophenylphenyl ether ND ug/L 55.6 10 11 /21 /07 00:00 11/30/07 02:01 7005-72-3
Chrysene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 218-01-9
Dibenz( a,h)anthracene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 53-70-3
3,3'-Dichlorobenzidine ND ug/L 55.6 10 11 /21 /0700:00 11/30/07 02:01 91-94-1
2,4-Dichlorophenol ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 120-83-2
Diethylphthalate ND ug/L 55.6 10 11/21/0700:00 11/30/07 02:01 84-66-2
2,4-Dimethylphenol ND ug/L 111 10 11/21/07 00:00 11/30/07 02:01 105-67-9
Dimethylphthalate ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 131-11-3
Di-n-butylphthalate ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 222 10 11/21/07 00:00 11/30/07 02:01 534-52-1
2,4-0initrophenol ND ug/L 556 10 11/21/07 00:00 11/30/07 02:01 51-28-5
2,4-Dinitrotoluene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 121-14-2
2,6-Dinitrotoluene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 606-20-2
Di-n-octylphthalate ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 117-81-7
Fluoranthene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 206-44-0
Fluorene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 86-73-7
Hexachloro-1,3-butadiene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 87-68-3
Hexachlorobenzene ND ug/L 55.6 10 11/21/07 00:00 11/30/07 02:01 118-74-1
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 7 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc .. --~Jl!:~·-. 11. _ ac:1\
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, f'J,C 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-2
Parameters
625 MSSV
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorane
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12/05/200711:27 AM
Lab ID: 928366002 Collected: 11/19/07 16:00 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 111 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 111 10 11/21/07 00:00
1090 ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 556 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 111 10 11/21/07 00:00
ND ug/L 278 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 55.6 10 11/21/07 00:00
ND ug/L 111 10 11 /21 /07 00:00
0% 10-120 10 11/21/07 00:00
0% 15-120 10 11/21/07 00:00
0% 11-131 10 11/21/07 00:00
0% 10-120 10 11/21/07 00:00
0% 10-120 10 11/21/07 00:00
0% 10-137 10 11/21/07 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
lh;,ic:\
Analyzed CAS No.
11/30/07 02:01 77-47-4
11/30/07 02:01 67-72-1
11/30/07 02:01 193-39-5
11/30/07 02:01 78-59-1
11/30/07 02:01 91-20-3
11/30/07 02:01 98-95-3
11/30/07 02:01 88-75-5
11/30/07 02:01 100-02-7
11/30/07 02:01 62-75-9
11/30/07 02:01 621-64-7
11/30/07 02:01 86-30-6
11/30/07 02:01 87-86-5
11/30/07 02:01 85-01-8
11/30/07 02:01 108-95-2
11/30/07 02:01 129-00-0
11/30/07 02:01 120-82-1
11/30/07 02:01 88-06-2
11/30/07 02:01 4165-60-0
11/30/07 02:01 321-60-8
11/30/07 02:01 1718-51-0
11/30/07 02:01 13127-88-3
11/30/07 02:01 367-12-4
11/30/07 02:01 118-79-6
Qual
D3,S4
D3,S4
D3,S4
D3,S4
D3,S4
D3,S4
Page 8 of 32
Pace Analytical Services, Jnc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Jnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-3
Parameters
MADEP EPH NC Water
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatri8contane (.S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
601/602 Volatiles
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dlchloropropelie
Diisopropyl ether
Ethyl benzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethane
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
m&p-Xylene
Date: 12/05/200711:27 AM
Lab ID: 928366003 Collected: 11/19/07 15:45 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. --------------
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
3460 ug/L
ND ug/L
2440 ug/L
87 %
102 %
131 %
106 %
Analytical Method: EPA 601/602
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
2190 ug/L
ND ug/L
ND ug/L
1090 ug/L
ND ug/L
ND ug/L
4850 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
13600 ug/L
8910 ug/L
244 2
122
122
40-140
40-140
40-140
40-140
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
500 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
500 250
250 250
500 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
250 250
500 250
500 250
11/27/07 00:00 12/03/07 12:50
11/27/07 00:00 11/30/0717:04
11/27/07 00:00 11/30/0717:04
11/27/07 00:00 11/30/0717:04 7194-86-7
11/27/07 00:00 11/30/0717:04 84-15-1
11/27/07 00:00 11/30/0717:04 321-60-8
11/27/07 00:00 11/30/07 17:04 580-13-2
12101/07 23:10 71-43-2
12/01/07 23:09 75-27-4
12/01/07 23:09 75-25-2
12/01/07 23:09 74-83-9
12/01/07 23:09 56-23-5
12/01/07 23:09 108-90-7
12/01/07 23:09 75-00-3
12/01/07 23:09 67-66-3
12/01/07 23:09 74-87-3
12/01/07 23:09 124-48-1
12/01/07 23:09 106-93-4
12/01/07 23:09 95-50-1
12/01/07 23:09 541-73-1
12/01/07 23:09 106-46-7
12/01/07 23:09 75-71-8
12/01/07 23:09 75-34-3
12/01/07 23:09 107-06-2
12/01/07 23:09 75-35-4
12/01/07 23:09 156-59-2
12/01/07 23:09 156-60-5
12/01/07 23:09 78-87-5
12/01/07 23:09 10061-01-5
12/01/07 23:09 10061-02-6
12101/07 23:10 108-20-3
12/01/07 23:10 100-41-4
12/01/07 23:09 75-09-2
12/01/07 23:10 1634-04-4
12/01/07 23:10 91-20-3
12/01/07 23:09 79-34-5
12/01/07 23:09 127-18-4
12/01/07 23:10 108-88-3
12/01/07 23:09 71-55-6
12/01/07 23:09 79-00-5
12/01/07 23:09 79-01-6
12/01/07 23:09 75-69-4
12/01/07 23:09 75-01-4
12/01/07 23:10 1330-20-7
12/01/07 23:10 1330-20-7
Qual
REPORT OF LABORATORY ANALYSIS Page 9 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analyttcal Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville,.,NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-3 LablD: 928366003 Collected: 11/19/0715:45 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 601/602
o-Xylene 4670 ug/L 250 250 12/01/07 23:10 95-47-6 1-Chloro-3-fluorobenzene (S) 94 % 65-137 250 12/01/07 23:09 625-98-9
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 83-32-9 Acenaphthylene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 208-96-8 Anthracene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 120-12-7 Benzo(a)anthracene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 56-55-3 Benzo(a)pyrene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 50-32-8
Benzo(b)fluoranthene ND ug/L 5.4 11/21/07 00:00 11 /28/07 23:32 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 191-24-2
Benzo(k)fluoranthene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 101-55-3
Butylbenzylphthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 10.9 11/21/07 00:00 11/28/07 23:32 111-91-1
bis(2-Chloroethyl) ether ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 108-60-1
2-Chloronaphthalene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 91-58-7
2-Chlorophenol ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 7005-72-3
Chrysene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 218-01-9
Di benz( a, h )a nthracene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 53-70-3
3,3'-Dichlorobenzidine ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 91-94-1
2,4-Dichlorophenol ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 120-83-2
Diethylphthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 84-66-2
2,4-Dimethylphenol ND ug/L 10.9 11/21/0700:00 11 /28/07 23:32 105-67-9
Dimethylphthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 131-11-3
Di-n-butylphthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 21.7 11/21/07 00:00 11/28/07 23:32 534-52-1
2,4-Dinitrophenol ND ug/L 54.3 11/21/07 00:00 11/28/07 23:32 51-28-5
2,4-Dinitrotoluene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 121-14-2
2,6-Dinitrotoluene ND ug/L 5.4 11 /21 /07 00:00 11/28/07 23:32 606-20-2
Di-n-octylphthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 117-81-7 Fluoranthene ND ug/L 5.4 11/21/0700:00 11/28/07 23:32 206-44-0 Fluorene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 87-68-3 Hexachlorobenzene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 118-74-1
Hexachlorocyclopentadiene ND ug/L 10.9 11/21/07 00:00 11/28/07 23:32 77-47-4
Hexachloroethane ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 67-72-1
I ndeno(1,2,3-cd)pyrene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 193-39-5 lsophorone ND ug/L 10.9 11/21/07 00:00 11/28/07 23:32 78-59-1
Naphthalene 513 ug/L 27.2 5 11/21/0700:00 11/30/07 02:27 91-20-3 Nitro benzene ND ug/L 5.4 11/21/07 00:00 11/28/07 23:32 98-95-3
2-Nitrophenol ND ug/L 5.4 11/21/0700:00 11/28/07 23:32 88-75-5
4-Nitrophenol ND ug/L 54.3 11/21/07 00:00 11/28/07 23:32 100-02-7
Date: 12/05/200711:27 AM REPORT OF LABORATORY ANALYSIS Page 10 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,~ •cc0 lfie~~ ,/ .. . "
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-3
Parameters
625 MSSV
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12105/2007 11 :27 AM
Lab ID: 928366003 Collected: 11/19107 15:45 Received: 11121/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 5.4 11121/07 00:00
ND ug/L 5.4 11/21 /07 00:00
ND ug/L 10.9 11/21/07 00:00
ND ug/L 27.2 11121/07 00:00
ND ug/L 5.4 11121/07 00:00
ND ug/L 5.4 11121 /07 00:00
ND ug/L 5.4 11121/07 00:00
ND ug/L 5.4 11121/07 00:00
ND ug/L 10.9 11121/07 00:00
51 % 10-120 11121/07 00:00
93 % 15-120 11121/07 00:00
77 % 11-131 11121/07 00:00
39 % 10-120 11/21/0700:00
65 % 10-120 11121/07 00:00
98 % 10-137 5 11/21/0700:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in ful!,
without the written consent of Pace Analytical Services, Inc ..
,f:i'.:Jac-~'.''\ .,1_ne1; h
Analyzed CAS No. Qual
11/28107 23:32 62-75-9
11 /28/07 23:32 621-64-7
11/28107 23:32 86-30-6
11128/07 23:32 87-86-5
11 /28107 23:32 85-01-8
11128107 23:32 108-95-2
11 /28107 23:32 129-00-0
11128107 23:32 120-82-1
11/28/07 23:32 88-06-2
11/28/07 23:32 4165-60-0
11/28/07 23:32 321-60-8
11/28/07 23:32 1718-51-0
11/28107 23:32 13127-88-3
11/28/07 23:32 367-12-4
11130/07 02:27 118-79-6
Page 11 of32
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NB: 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-4 LablD: 928366004 Collected: 11/19/07 15:30 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) ND ug/L 119 11/27/07 00:00 11/30/0717:44
Aliphatic (C19-C36) ND ug/L 119 11/27/07 00:00 11/30/07 17:44
Aromatic (C11-C22) ND ug/L 119 11/27/07 00:00 11/30/0717:44
Nonatriacontane (S) 76 % 40-140 11/27/07 00:00 11/30/0717:44 7194-86-7
o-Terphenyl (S) 108 % 40-140 11/27/07 00:00 11/30/0717:44 84-15-1
2-Fluorobiphenyl (S) 120 % 40-140 11/27/07 00:00 11/30/0717:44 321-60-8
2-Bromonaphthalene (S) 110 % 40-140 11/27/07 00:00 11/30/0717:44 580-13-2
601/602 Volatiles Analytical Method: EPA 601/602
Benzene ND ug/L 1.0 12/01/07 03:36 71-43-2
Bromodichloromethane ND ug/L 1.0 12/01/07 03:36 75-27-4
Bromoform ND ug/L 1.0 12/01/07 03:36 75-25-2
Bromomethane ND ug/L 1.0 12/01/07 03:36 74-83-9
Carbon tetrachloride ND ug/L 1.0 12/01/07 03:36 56-23-5
Chlorobenzene ND ug/L 1.0 12/01/07 03:36 108-90-7
Chloroethane ND ug/L 1.0 12/01 /07 03:36 75-00-3
Chloroform ND ug/L 1.0 12/01/07 03:36 67-66-3
Chloromethane ND ug/L 2.0 12/01/07 03:36 74-87-3
Dlbromochloromethane ND ug/L 1.0 12/01/07 03:36 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 12/01/07 03:36 106-93-4
1,2-Dichlorobenzene ND ug/L 1.0 12/01/07 03:36 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 12/01/07 03:36 541-73.-1
1,4-Dichlorobenzene ND ug/L 1.0 12/01 /07 03:36 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 12/01/07 03:36 75-71-8
1, 1-Dichloroethane ND ug/L 1.0 12/01/07 03:36 75-34-3
1,2-Dichloroethane ND ug/L 1.0 12/01 /07 03:36 107-06-2
1, 1-Dichloroethene ND ug/L 1.0 12/01/07 03:36 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 12/01/07 03:36 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 12/01/07 03:36 156-60-5
1,2-Dichloropropane ND ug/L 1.0 12/01/07 03:36 78-87-5
cis-1,3-Dichloropropene ND ug/L 1.0 12/01/07 03:36 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 12/01/07 03:36 10061-02-6
Diisopropyl ether ND ug/L 1.0 12/01/07 03:36 108-20-3
Ethylbenzene ND ug/L 1.0 12/01/07 03:36 100-41-4
Methylene Chloride ND ug/L 2.0 12/01/07 03:36 75-09-2
Methyl-tort-butyl ether 2.3 ug/L 1.0 12/01/07 03:36 1634-04-4
Naphthalene ND ug/L 2.0 12/01/07 03:36 91-20-3
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 12/01/07 03:36 79-34-5
T etrachloroethene ND ug/L 1.0 12/01/07 03:36 127-18-4
Toluene ND ug/L 1.0 12/01/07 03:36 108-88-3
1, 1, 1-Trichloroethane ND ug/L 1.0 1 12/01/07 03:36 71-55-6
1, 1,2-Trichloroethane ND ug/L 1.0 1 12/01/07 03:36 79-00-5
Trichloroethene ND ug/L 1.0 1 . 12/01/07 03:36 79-01-6
T richlorofluoromethane ND ug/L 1.0 12/01/07 03:36 75-69-4
Vinyl chloride ND ug/L 1.0 12/01/07 03:36 75-01-4
Xylene (Total) ND ug/L 2.0 12/01/07 03:36 1330-20-7
m&p-Xylene ND ug/L 2.0 12/01/07 03:36 1330-20-7
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 12 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
&ii2~ ff \\
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytlcal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-4 LablD: 928366004 Collected: 11/19/07 15:30 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 601/602
o-Xylene ND ug/L 1.0 12/01/07 03:36 95-47-6
1-Chloro-3-fluorobenzene (S) 88 % 65-137 12/01/07 03:36 625-98-9
MADEP VPH NC Water Analytical Method: MADEP VPH
Aliphatic (COS-COB) ND ug/L 100 11/28/07 22:56
Aliphatic (C09-C12) ND ug/L 100 11/28/07 22:56
Aromatic (C09-C10) ND ug/L 100 11/28/07 22:56
2,5-Dibromotoluene (PID)(S) 88 % 70-130 11/28/07 22:56
2,5-Dibromotoluene (FID)(S) 102 % 70-130 11/28/07 22:56
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 83-32-9
Acenaphthytene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 208-96-8
Anthracene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 120-12-7
Benzo(a)anthracene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 56-55-3
Benzo(a)pyrene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 50-32-8
Benzo(b )fluoranthene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 191-24-2
Benzo(k)fluoranthene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 101-55-3
Butylbenzylphthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.3 11/21/0700:00 11/28/07 23:58 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 10.5 11/21/07 00:00 11/28/07 23:58 111-91-1
bis(2-Chloroethyl) ether ND ug/L 5.3 11I2110700·.oo 11/28/07 23:58 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 108-60-1
2-Chloronaphthalene ND ug/L 5.3 11/21/0700:00 11/28/07 23:58 91-58-7
2-Chlorophenol ND ug/L 5.3 1 11/21/07 00:00 11/28/07 23:58 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.3 1 11/21/07 00:00 11/28/07 23:58 7005-72-3
Chrysene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 218-01-9
Dibenz(a,h )anthracene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 53-70-3
3,3'-Dichlorobenzidine ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 91-94-1
2,4-Dichlorophenol ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 120-83-2
Diethylphthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 84-66-2
2,4-Dimethylphenol ND ug/L 10.5 11/21/07 00:00 11/28/07 23:58 105-67-9
Dimethylphthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 131-11-3
Di-n-butylphthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 21.1 11/21/07 00:00 11/28/07 23:58 534-52-1
2,4-Dlnitrophenol ND ug/L 52.6 11/21/07 00:00 11/28/07 23:58 51-28-5
2,4-Dinitrotoluene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 121-14-2
2, 6-Dinitrotoluene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 606-20-2
Di-n-octylphthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 117-81-7
Fluoranthene ND ug/L 5.3 11/21107 00:00 11/28/07 23:58 206-44-0
Fluorene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 86-73-7
Hexachloro-1,3-butadiene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 87-68-3
Hexachlorobenzene ND ug/L 5.3 11/21/07 00:00 11/28/07 23:58 118-74-1
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 13 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,. -~ ii . .\t
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
[phone]
Pace Analytlcal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-4
Parameters
625 MSSV
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
Naphthalene
Nitro benzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12/05/2007 11 :27 AM
Lab ID: 928366004 Collected: 11/19/0715:30 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 10.5 11/21/07 00:00
ND ug/L 5.3 11/21/07 00:00
ND ug/L 5.3 11/21 /07 00:00
ND ug/L 10.5 11/21 /07 00:00
ND ug/L 5.3 1 11/21/07 00:00
ND ug/L 5.3 1 11/21/07 00:00
ND ug/L 5.3 1 11/21/07 00:00
ND ug/L 52.6 1 11/21 /07 00:00
ND ug/L 5.3 1 11/21/07 00:00
ND ug/L 5.3 1 11/21/07 00:00
ND ug/L 10.5 11/21/07 00:00
ND ug/L 26.3 11/21/07 00:00
ND ug/L 5.3 11/21/07 00:00
ND ug/L 5.3 11/21/07 00:00
ND ug/L 5.3 11/21/07 00:00
ND ug/L 5.3 11/21/07 00:00
ND ug/L 10.5 11/21/07 00:00
24 % 10-120 11/21/07 00:00
32 % 15-120 11/21/07 00:00
34 % 11-131 11/21/07 00:00
14 % 10-120 11/21/07 00:00
10 % 10-120 11/21/07 00:00
24 % 10-137 11/21/07 00:00
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~~2:r.Jit;;~ i1ut:=1a1..\~
Analyzed CAS No. Qual
11/28/07 23:58 77-47-4
11/28/07 23:58 67-72-1
11/28/07 23:58 193-39-5
11/28/07 23:58 78-59-1
11/28/07 23:58 91-20-3
11/28/07 23:58 98-95-3
11/28/07 23:58 88-75-5
11/28/07 23:58 100-02-7
11/28/07 23:58 62-75-9
11/28/07 23:58 621-64-7
11/28/07 23:58 86-30-6
11/28/07 23:58 87-86-5
11 /28/07 23:58 85-01-8
11 /28/07 23:58 108-95-2
11/28/07 23:58 129-00-0
11/28/07 23:58 120-82-1
11/28/07 23:58 88-06-2
11/28/07 23:58 4165-60-0
11/28/07 23:58 321-60-8
11 /28/07 23:58 1718-51-0
11/28/07 23:58 13127-88-3
11/28/07 23:58 367-12-4
11/28/07 23:58 118-79-6
Page 14 of 32
~eAnalytica/0 (~-----~a9 www.pacetabs.com
I ,,
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersvHle, NC 28078
[phone]
Project: TEXACO FOOOMART #2
Pace Project No.: 928366
Sample: MW-5 LablD: 928366005 Collected: 11/19/0715:15 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) ND ug/L 118 11/27/07 00:00 11/30/07 18:24
Aliphatic (C19-C36) ND ug/L 118 11 /27 /07 00:00 11/30/07 18:24
Aromatic (C11-C22) ND ug/L 118 11/27/07 00:00 11/30/07 18:24
Nonatriacontane (S) 73 % 40-140 11/27/07 00:00 11/30/07 18:24 7194-86-7
o-Terphenyl (S) 101 % 40-140 11/27/07 00:00 11 /30/07 18:24 84-15-1
2-Fluorobiphenyl (S) 109 % 40-140 11/27/07 00:00 11/30/0718:24 321-60-8
2-Bromonaphthalene (S) 80 % 40-140 11/27/07 00:00 11/30/0718:24 580-13-2
601/602 Volatiles Analytical Method: EPA 601/602
Benzene ND ug/L 1.0 12/01/07 04:18 71-43-2
Bromodichloromethane ND ug/L 1.0 12/01/07 04:18 75-27-4
Bromoform ND ug/L 1.0 12/01/07 04:18 75-25-2
Bromomethane ND ug/L 1.0 12/01/07 04:18 74-83-9
Carbon tetrachloride ND ug/L 1.0 12/01/07 04:18 56-23-5
Chiaro benzene ND ug/L 1.0 12/01/07 04:18 108-90-7
Chloroethane ND ug/L 1.0 12/01/07 04:18 75-00-3
Chloroform ND ug/L 1.0 12/01/07 04:18 67-66-3
Chloromethane ND ug/L 2.0 12/01/07 04:18 74-87-3
Dibromochloromethane ND ug/L 1.0 12/01/07 04:18 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 12/01/07 04:18 106-93-4
1,2-Dichlorobenzene ND ug/L 1.0 12/01/07 04:18 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 12/01/07 04:18 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 12/01/07 04:18 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 12/01/07 04:18 75-71-8
1, 1-Dichloroethane ND ug/L 1.0 12/01/07 04:18 75-34-3
1,2-Dichloroethane ND ug/L 1.0 12/01/07 04:18 107-06-2
1, 1-Dichloroethene ND ug/L 1.0 12/01/07 04:18 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 12/01/07 04:18 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 12/01/07 04:18 156-60-5
1,2-Dichloropropane ND ug/L 1.0 12/01/07 04:18 78-87-5
cis-1,3-Dichloropropene ND ug/L 1.0 1 12/01/07 04:18 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 12/01/07 04:18 10061-02-6
Diisopropyl ether ND ug/L 1.0 12/01/07 04:18 108-20-3
Ethyl benzene ND ug/L 1.0 12/01/07 04:18 100-41-4
Methylene Chloride ND ug/L 2.0 12/01/07 04:18 75-09-2
Methyl-tert-butyl ether ND ug/L 1.0 12/01/07 04:18 1634-04-4
Naphthalene ND ug/L 2.0 12/01/07 04:18 91-20-3
1, 1,2,2-Tetrachloroethane ND ug/L 1.0 12/01/07 04:18 79-34-5
T etrachloroethene ND ug/L 1.0 12/01/07 04:18 127-18-4
Toluene ND ug/L 1.0 12/01/07 04:18 108-88-3
1, 1, 1-Trichloroethane ND ug/L 1.0 12/01/07 04:18 71-55-6
1, 1,2-Trichloroethane ND ug/L 1.0 12/01/07 04:18 79-00-5
Trichloroethane ND ug/L 1.0 12/01/07 04:18 79-01-6
T richlorofluoromethane ND ug/L 1.0 12/01/07 04:18 75-69-4
Vinyl chloride ND ug/L 1.0 12/01/07 04:18 75-01-4
Xylene (Total) ND ug/L 2.0 12/01/07 04:18 1330-20-7
m&p-Xylene ND ug/L 2.0 12/01/07 04:18 1330-20-7
Date: 12/05/200711:27 AM REPORT OF LABORATORY ANALYSIS Page 15 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
i/fi'J!~\\
;2ce Analytical•
, www.pacelsbs.com
(
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RES UL TS
Asheville, NC 28804
( 828 )254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, MC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-5
Parameters
601/602 Volatiles
o-Xylene
1-Chloro-3-fluorobenzene (S)
MADEP VPH NC Water
Aliphatic (COS-COB)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (PID)(S)
2,5-Dibromotoluene (FID)(S)
625 MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Date: 12/0512007 11 :27 AM
LablD: 928366005 Collected: 11/19/0715:15 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: EPA 601/602
ND ug/L
97 %
Analytical Method: MADEP VPH
144 ug/L
ND ug/L
ND ug/L
95 %
104 %
1.0
65-137
100
100
100
70-130
70-130
------------------
12/01/07 04:18 95-47-6
12101/07 04:18 625-98-9
11/28/07 23:26
11128/07 23:26
11/28/07 23:26
11/28107 23:26
11128/07 23:26
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
11.6
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
11.6
5.8
5.8
23.3
58.1
5.8
5.8
5.8
5.8
5.8
5.8
5.8
5.8
11121/07 00:00 11/29/07 00:23 83-32-9
11121/07 00:00 11/29/07 00:23 208-96-8
11/21/07 00:00 11/29/07 00:23 120-12-7
11121/07 00:00 11129/07 00:23 56-55-3
11121/07 00:00 11/29107 00:23 50-32-8
11121/07 00:00 11/29107 00:23 205-99-2
11121/07 00:00 11129/07 00:23 191-24-2
11121/07 00:00 11129/07 00:23 207-08-9
11121/07 00:00 11129/07 00:23 101-55-3
11121/07 00:00 11/29/0700:23 85-68-7
11/21/07 00:00 11129/07 00:23 59-50-7
11/21/0700:00 11/29/0700:23 111-91-1
11121/0700:00 11/29/07 00:23 111-44-4
11/21/0700:00 11/29/07 00:23 108-60-1
11/21/07 00:00 11129/07 00:23 91-58-7
11121/07 00:00 11/29/0700:23 95-57-8
11121/0700:00 11129/07 00:23 7005-72-3
11/21/07 00:00 11129/07 00:23 218-01-9
11121/07 00:00 11/29107 00:23 53-70-3
11121/07 00:00 11/29/07 00:23 91-94-1
11121/07 00:00 11129/07 00:23 120-83-2
11121/07 00:00 11/29107 00:23 84-66-2
11121/07 00:00 11/29/07 00:23 105-67-9
11121/0700:00 11/29/0700:23 131-11-3
11/21/07 00:00 11/29107 00:23 84-74-2
11/21/07 00:00 11/29/07 00:23 534-52-1
11/21/0700:00 11/29/07 00:23 51-28-5
11/21/07 00:00 11/29107 00:23 121-14-2
11121/07 00:00 11/29/07 00:23 606-20-2
11121/0700:00 11129/07 00:23 117-84-0
11121/07 00:00 11129107 00:23 117-81-7
11121/07 00:00 11/29107 00:23 206-44-0
11121/0700:00 11/29/0700:23 86-73-7
11121/07 00:00 11129/07 00:23 87-68-3
11/21/0700:00 11/29/0700:23 118-74-1
Qual
REPORT OF LABORATORY ANALYSIS Page 16 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytlcal Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytlcal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: MW-5
Parameters
625 MSSV
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-dB (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12/05/2007 11 :27 AM
Lab ID: 928366005 Collected: 11/19/0715:15 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 11.6 11/21 /07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21 /07 00:00
ND ug/L 11.6 11/21/0700:00
41.0 ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21 /07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 58.1 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 11.6 11/21/07 00:00
ND ug/L 29.1 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 5.8 11/21/07 00:00
ND ug/L 11.6 11/21/07 00:00
60 % 10-120 11 /21 /07 00:00
75 % 15-120 11/21/07 00:00
63 % 11-131 11/21/07 00:00
33 % 10-120 11/21/07 00:00
46 % 10-120 11/21/07 00:00
84 % 10-137 11/21/07 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .. .. z:Js)-111 .. lt:lcl'-.'Jt
Analyzed CAS No. Qual
11/29/07 00:23 77-47-4
11/29/07 00:23 67-72-1
11/29/07 00:23 193-39-5
11/29/07 00:23 78-59-1
11/29/07 00:23 91-20-3
11/29/07 00:23 98-95-3
11 /29/07 00:23 88-75-5
11/29/07 00:23 100-02-7
11/29/07 00:23 62-75-9
11/29/07 00:23 621-64-7
11/29/07 00:23 86-30-6
11/29/07 00:23 87-86-5
11/29/07 00:23 85-01-8
11 /29/07 00:23 108-95-2
11/29/07 00:23 129-00-0
11/29/07 00:23 120-82-1
11/29/07 00:23 88-06-2
11/29/07 00:23 4165-60-0
11/29/07 00:23 321-60-8
11/29/07 00:23 1718-51-0
11/29/07 00:23 13127-88-3
11/29/07 00:23 367-12-4
11/29/07 00:23 118-79-6
Page 17 of 32
aeAnalytica/0
1 www.pacelabs.com
I
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, f'i-JC 28078
(704)875-~092
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: T-1
Parameters
MADEP EPH NC Water
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Nonatriacontane (S)
o-Terphenyl (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
601/602 Volatiles
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chiaro methane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
Cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
m&p-Xylene
Date: 12/05/200711:27 AM
LablD: 928366006 Collected: 11/19/0715:00 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit OF Prepared Analyzed CAS No. -----------------
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
ND ug/L
ND ug/L
ND ug/L
82 %
95 %
95 %
87 %
Analytical Method: EPA 601/602
43.8 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1.7 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
210 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
112
112
112
40-140
40-140
40-140
40-140
1.0
1.0
1 .o
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
10.0 10
2.0 1
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
2.0
11/27/07 00:00 11/30/0719:04
11/27/07 00:00 11/30/07 19:04
11/27/07 00:00 11/30/0719:04
11/27/07 00:00 11/30/0719:04 7194-86-7
11/27/07 00:00 11/30/07 19:04 84-15-1
11/27/07 00:00 11/30/0719:04 321-60-8
11/27/07 00:00 11/30/0719:04 580-13-2
12/01/07 05:00 71-43-2
12/01/07 05:00 75-27-4
12/01/07 05:00 75-25-2
12/01/07 05:00 74-83-9
12/01/07 05:00 56-23-5
12/01/07 05:00 108-90-7
12/01/07 05:00 75-00-3
12/01/07 05:00 67-66-3
12/01/07 05:00 74-87-3
12/01/07 05:00 124-48-1
12/01/07 05:00 106-93-4
12/01/07 05:00 95-50-1
12/01/07 05:00 541-73-1
12/01/07 05:00 106-46-7
12/01/07 05:00 75-71-8
12/01/07 05:00 75-34-3
12/01/07 05:00 107-06-2
12/01/07 05:00 75-35-4
12/01/07 05:00 156-59-2
12/01/07 05:00 156-60-5
12/01/07 05:00 78-87-5
12/01/07 05:00 10061-01-5
12/01/07 05:00 10061-02-6
12/01/0705:00 108-20-3
12/01/07 05:00 100-41-4
12/01/07 05:00 75-09-2
12/01/07 23:51 1634-04-4
12/01/07 05:00 91-20-3
12/01/07 05:00 79-34-5
12/01/07 05:00 127-18-4
12/01/07 05:00 108-88-3
12/01/07 05:00 71-55-6
12/01/07 05:00 79-00-5
12/01/07 05:00 79-01-6
12/01/07 05:00 75-69-4
12/01/07 05:00 75-01-4
12/01/07 05:00 1330-20-7
12/01/07 05:00 1330-20-7
Qual
REPORT OF LABORATORY ANALYSIS Page 18 of32
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc ..
,~ Acco" .l}!Cf~-~·~~ finetac\~
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: T-1 LablD: 928366006 Collected: 11/19/0715:00 Received: 11/21/07 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 601/602
o-Xylene ND ug/L 1.0 12/01/07 05:00 95-47-6
1-Chloro-3-fluorobenzene (S) 85 % 65-137 12/01/07 05:00 625-98-9
MADEP VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08) ND ug/L 100 1 11/28/07 23:57
Aliphatic (C09-C12) ND ug/L 100 1 11/28/07 23:57
Aromatic (C09-C10) ND ug/L 100 11/28/0723:57
2,5-Dibromotoluene (PID)(S) 92 % 70-130 11/28/07 23:57
2,5-Dibromotoluene (FID)(S) 101 % 70-130 11 /28/07 23:57
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 6.2 11/21/0700:00 11/29/07 00:50 83-32-9
Acenaphthylene ND ug/L 6.2 11 f.21 /0700:00 11/29/07 00:50 208-96-8
Anthracene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 120-12-7
Benzo(a)anthracene ND ug/L 6.2 11/21/0700:00 11/29/07 00:50 56-55-3
Benzo(a)pyrene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 50-32-8
Benzo(b )fluoranthene ND ug/L 6.2 1 11/21/0700:00 11/29/0700:50 205-99-2
Benzo(g,h,i)perylene ND ug/L 6.2 1 11/21/0700:00 11/29/07 00:50 191-24-2
Benzo(k)fluoranthene ND ug/L 6.2 11/21/0700:00 11/29/07 00:50 207-08-9
4-Bromophenylphenyl ether ND ug/L 6.2 11/21/07 00:00 11/29/0700:50 101-55-3
Butylbenzylphthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 85-68-7
4-Chloro-3-methylphenol ND ug/L 6.2 1 11/21/07 00:00 11/29/07 00:50 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 12.5 1 11/21/07 00:00 11/29/07 00:50 111-91-1
bis(2-Chloroethyl) ether ND ug/L 6.2 1 11/21/07 00:00 11/29/07 00:50 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 6.2 1 11/21/07 00:00 11/29/07 00:50 108-60-1
2-Chloronaphthalene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 91-58-7
2-Chlorophenol ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 95-57-8
4-Chlorophenylphenyl ether ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 7005-72-3
Chrysene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 218-01-9
Dibenz( a, h}anthracene ND ug/L 6.2 11 /21/07 00:00 11/29/07 00:50 53-70-3
3,3'-Dichlorobenzidine ND ug/L 6.2 11/21/0700:00 11/29/07 00:50 91-94-1
2,4-Dichlorophenol ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 120-83-2
Diethylphthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 84-66-2
2,4-Dimethylphenol ND ug/L 12.5 11/21/07 00:00 11/29/07 00:50 105-67-9
Dimethylphthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 131-11-3
Di-n-butylphthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 25.0 11/21/07 00:00 11/29/07 00:50 534-52-1
2,4-Dinitrophenol ND ug/L 62.5 11/21/07 00:00 11/29/07 00:50 51-28-5
2,4-Dinitrotoluene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 121-14-2
2,6-0initrotoluene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 606-20-2
Di-n-octylphthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 117-81-7
Fluoranthene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 206-44-0
Fluorene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 86-73-7
Hexachloro-1, 3-butad'iene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 87-68-3
Hexachlorobenzene ND ug/L 6.2 11/21/07 00:00 11/29/07 00:50 118-74-1
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 19 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
ittJl21
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 26604
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviller NC 26076
(704)87g-9092
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Sample: T-1
Parameters
625 MSSV
Hexachlorocyclopentadiene
Hexachloroethane
I ndeno( 1,2,3-cd)pyrene
lsophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-T richlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 12/05/2007 11 :27 AM
Lab ID: 928366006 Collected: 11/19/07 15:00 Received: 11/21/07 08:00 Matrix: Water
Results Units Report Limit DF Prepared
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 12.5 11/21 /07 00:00
ND ug/L 6.2 11 /21 /07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 12.5 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 62.5 1 11/21/07 00:00
ND ug/L 6.2 1 11/21/07 00:00
ND ug/L 6.2 1 11/21/07 00:00
ND ug/L 12.5 1 11/21/07 00:00
ND ug/L 31.2 11 /21 /07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 6.2 11/21/07 00:00
ND ug/L 12.5 11/21/07 00:00
91 % 10-120 11/21/07 00:00
79 % 15-120 11/21/07 00:00
75 % 11-131 11/21/07 00:00
44 % 10-120 11/21/07 00:00
52 % 10-120 11/21/07 00:00
99 % 10-137 11 /21 /07 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
lz::i~c~~~\ .
.. l. l .. tt:::lc.ll ; ~
Analyzed GAS No. Qual
11/29/07 00:50 77-47-4
11/29/07 00:50 67-72-1
11/29/07 00:50 193-39-5
11/29/07 00:50 78-59-1
11/29/07 00:50 91-20-3
11/29/07 00:50 98-95-3
11/29/0700:50 88-75-5
11/29/07 00:50 100-02-7
11/29/07 00:50 62-75-9
11/29/07 00:50 621-64-7
11/29/07 00:50 86-30-6
11/29/07 00:50 87-86-5
11/29/07 00:50 85-01-8
11/29/07 00:50 108-95-2
11/29/07 00:50 129-00-0
11/29/07 00:50 120-82-1
11/29/07 00:50 88-06-2
11/29/07 00:50 4165-60-0
11/29/07 00:50 321-60-8
11/29/07 00:50 1718-51-0
11/29/07 00:50 13127-88-3
11/29/07 00:50 367-12-4
11/29/07 00:50 118-79-6
Page 20 of 32
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Pace Analytical Services, Inc.
2225 Riverside Dr.
QUALITY CONTROL DATA
Asheville, NC 28804
[phone]
QC Batch: OEXT/1795 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
METHOD BLANK: 44716
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
Parameter
1,2,4-Trichlorobenzene
2,4,6-T richlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,3'-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalale
8 utylbenzyl phthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a, h)anthracene
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
I ndeno(1,2,3-cd)pyrene
lsophorone
Date: 12/05/2007 11 :27 AM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank Reporting
Units Result Limit Qualifiers
ND 5.0
ND 10.0
ND 5.0
ND 10.0
ND 50.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 20.0
ND 5.0
ND 5.0
ND 5.0
ND 50.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 10.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 5.0
ND 10.0
ND 5.0
ND 5.0
ND 10.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,~ ,cco,.., b1d~~>~+~ , ac· if . .. \1
Pace AnalytJcal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
Pace Analytical Services, Inc.
2225 Riverside Dr.
QUALITY CONTROL DATA
Asheville, NC 28804
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
METHOD BLANK: 44716
Associated Lab Samples: 928366001,928366002,928366003,928366004, 928366005,928366006
Blank Reporting
Parameter Units Result Limit Qualifiers
N-Nitroso-di-n-propylamine ug/L ND 5.0
N-Nitrosodimethylamine ug/L ND 5.0
N-Nitrosodiphenylamine ug/L ND 10.0
Naphthalene ug/L ND 5.0
Nitrobenzene ug/L ND 5.0
Pentachlorophenol ug/L ND 25.0
Phenanthrene ug/L ND 5.0
Phenol ug/L ND 5.0
Pyrene ug/L ND 5.0
2,4,6-Tribromophenol (S) % 84 10-137
2-Fluorobiphenyl (S) % 62 15-120
2-Fluorophenol (S) % 33 10-120
Nitrobenzene-d5 (S) % 71 10-120
Phenol-d6 (S) % 24 10-120
Terphenyl-d14 (S) % 71 11-131
LABORATORY CONTROL SAMPLE & LCSD: 44717 44718
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Cone. Result Result % Rec % Rec Limits
1,2,4-Trichlorobenzene ug/L 50 34.3 21.9 69 44 44-142
2,4,6-Trichlorophenol ug/L 50 37.3 23.4 75 47 37-144
2,4-Dichlorophenol ug/L 50 38.9 26.2 78 52 1-191
2,4-Dlmethylphenol ug/L 50 33.2 26.5 66 53 32-119
2,4-Dinitrophenol ug/L 50 34.4J 15.4J 69 31 1-181
2,4-Dinitrotoluene ug/L 50 41.5 25.8 83 52 39-139
2,6-Dinitrotoluene ug/L 50 39.4 26.2 79 52 50-158
2-Chloronaphthalene ug/L 50 29.5 22.5 59 45 60-118
2-Chlorophenol ug/L 50 30.6 18.2 61 36 23-134
2-Nitrophenof ug/L 50 40.9 25.0 82 50 29-182
3,3'-Dichlorobenzidlne ug/L 50 39.1 22.1 78 44 1-262
4,6-Dinitro-2-methylphenol ug/L 50 42.5 26.8 85 54 1-181
4-Bromophenylphenyl ether ug/L 50 45.9 29.1 92 58 53-127
4-Chloro-3-methylphenol ug/L 50 40.6 25.8 81 52 22-147
4-Chlorophenylphenyl ether ug/L 50 42.8 28.8 86 58 25-158
4-Nitrophenol ug/L 50 17.9J 11.3J 36 23 1-132
Acenaphthene ug/L 50 40.1 25.1 80 50 47-145
Acenaphthylene ug/L 50 40.6 26.4 81 53 33-145
Anthracene ug/L 50 42.3 28.9 85 58 1-166
Benzo(a)anthracene ug/L 50 42.7 25.3 85 51 33-143
Benzo(a)pyrene ug/L 50 44.3 28.3 89 57 17-163
Benzo(b)fluoranthene ug/L 50 38.3 23.1 77 46 24-159
Benzo(g,h,i)perylene ug/L 50 44.0 27.7 88 55 1-219
Benzo(k)fluoranthene ug/L 50 36.2 23.1 72 46 11-162
bis(2-Chloroethoxy)methane ug/L 50 40.3 27.9 81 56 33-184
bis(2-Chloroethyl) ether ug/L 50 35,5 20.7 71 41 12-158
Date: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~~~~:~~ 11 __ .. ac1~
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, N'C 28078
I [phone]
Max
RPD RPD Qualifiers
44 30 1g
46 30
39 30
22 30
76 30
47 30
40 30
27 30 LO
51 30
48 30
56 30
45 30
45 30
45 30
39 30
45 30
46 30
42 30
38 30
51 30
44 30
50 30
46 30
44 30
36 30
53 30
Page 22 of 32
p~-Pace Analytical Services, Jnc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
LABORATORY CONTROL SAMPLE & LCSD: 44717 44718
Spike LCS LCSD LCS LCSD ¾Rec
Parameter Units ConC. Result Result % Rec% Rec limits
bis(2-Chloroisopropyl) ether ug/L
bis(2-Ethylhexyl)phthalate ug/L
Butylbenzylphthalate ug/L
Chrysene ug/L
Di-n-butylphthalate ug/L
Di-n-octylphthalate ug/L
Dibenz(a,h)anthracene ug/L
Diethylphthalate ug/L
Dimethylphthalate ug/L
Fluoranthene ug/L
Fluorene ug/L
Hexachloro-1,3-butadiene ug/L
Hexachlorobenzene ug/L
Hexachlorocyclopentadiene ug/L
Hexachloroethane ug/L
lndeno(1,2,3-cd)pyrene ug/L
lsophorone ug/L
N-Nitroso-di-n-propylamine ug/L
N-NitroSodimethylamine ug/L
N-Nitrosodlphenylamine ug/L
Naphthalene ug/L
Nitrobenzene ug/L
Pentachlorophenol ug/L
Phenanthrene ug/L
Phenol ug/L
Pyrene ug/L
2,4,6-Tribromophenol (5) %
2-Fluorobiphenyl (S) %
2-Fluorophenol (S) %
Nitrobenzene-d5 (5) %
Phenol-dB (S) %
Terphenyl-d14 (5) %
Date: 12/05/200711:27 AM
----50 42.4 24.8 85
50 43.6 25.4 87
50 41.5 24.8 83
50 44.5 25.9 89
50 43.0 26.2 86
50 40.3 24.5 81
50 43.6 27.7 87
50 40.6 26.1 81
50 44.6 28.5 89
50 41.5 26.9 83
50 43.2 26.0 86
50 34.0 21.7 68
50 43.3 26.2 87
50 21.1 6.8J 42
50 29.8 15.1 60
50 43.4 27.7 87
50 47.0 31.3 94
50 37.6 25.1 75
50 12.4 7.0 25
50 43.1 31.7 86
50 34.0 22.5 68
50 39.5 26.1 79
50 34.9 21.3J 70
50 43.7 27.6 87
50 16.0 9.6 32
50 42.4 25.9 85
92
81
40
82
33
84
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
. {S'.J;!;~ ff:l lt:=ICI.\... ·,\
50
51
50
52
52
49
55
52
57
54
52
43
52
14
30
55
63
50
14
63
45
52
43
55
19
52
59
53
19
52
19
53
36-166
8-158
1-152
17-168
1-118
4-146
1-227
1-114
1-112
26-137
59-121
24-116
1-152
25-150
40-113
1-171
21-196
1-230
25-150
25-150
21-133
35-180
14-176
54-120
5-112
52-115
10-137
15-120
10-120
10-120
10-120
11-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPO RPD Qualifiers
52 30
53 30
50 30
53 30
48 30
49 30
45 30
43 30
44 30
43 30
50 30 LO
44 30
49 30
103 30
66 30 LO
44 30
40 30
40 30
56 30 LO
31 30
41 30
41 30
49 30
45 30
50 30
48 30
Page 23 of 32
~eAnalyticat"
Pace Analytical Services, Inc.
2225 Riverside Dr.
( ... /' uv, www.p,"''''·"'m Asheville, NC 28804
(626 )254-7176
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
QC Batch: OEXT/1818 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
METHOD BLANK: 45879
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
Blank Reporting
Parameter Units Result Limit Qualifiers
Aliphatic (C09-C18) ug/L ND 100
Aliphatic (C19-C36) ug/L ND 100
Aromatic (C11-C22) ug/L ND 100
2-Bromonaphthalene (S) % 74 40-140
2-Fluorobiphen0 (S) % 99 40-140
Nonatriacontane (S) % 63 40-140
o-Terphenyl (S) % 93 40-140
LABORATORY CONTROL SAMPLE & LCSD: 45880 45881
Spike LCS LCSD LCS LCSD
Parameter
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
2-Bromonaphthalene (S)
2-Fluorobiphenyl (S)
Nonatrfacontane (S)
o-Terphenyl (S)
Date: 12/05/200711:27 AM
ug/L
ug/L
ug/L
%
%
%
%
Units Cone. Result Result % Rec % Rec
300 164 175 55
400 301 314 75
850 836 709 98
100
103
110
98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc ..
58
78
83
96
93
64
70
% Rec
Limits
40-140
40-140
40-140
40-140
40-140
40-140
40-140
RPD
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville.'NC 28078
Max
RPD Qualifiers
7 50
4 50
16 50
Page 24 of 32
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828 )254-7176
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
QC Batch: GCV/1407 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: MADEP VPH NC Water
Associated Lab Samples: 928366001, 928366002, 928366004, 928366005, 928366006
METHOD BLANK: 46421
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
Blank Reporting
Parameter Units Result Limit Qualifiers
Aliphatic (COS-COB) ug/L ND 100
Aliphatic (C09-C12) ug/L ND 100
Aromatic (C09-C10) ug/L ND 100
2,5-Dibromotoluene (FID)(S) % 99 70-130
2,5-Dibromotoluene (PID)(S) % 100 70-130
LABORATORY CONTROL SAMPLE & LCSD: 46422 46423
Parameter
Aliphatic (COS-COB)
Aliphatic (C09-C12)
Aromatic (C09-C10)
2,5-Dibromotoluene (FID)(S)
2,5-Dibromotoluene (PID)(S)
Date: 12/05/200711:27 AM
ug/L
ug/L
ug/L
%
%
Spike LCS LCSD LCS LCSD
Units Cone. Result Result % Rec % Rec ----
400 431 445 108 111
100 112 116 112 116
100 102 106 102 106
94 95
97 98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,,oij'".::'.t'.s~-, ,/l_lt::lc:LC\,
% Rec
Limits
70-130
30-130
70-130
70-130
70-130
RPO
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPO Qualifiers
3 25
4 25
4 25
Page 25 of 32
~eAnalytica( 1--·~aci www.pecafsbs.com
Pace Analyttcal Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone] I
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
QC Batch: GCV/1418 Analysis Method: EPA 601/602
QC Batch Method: EPA 601/602 Analysis Description: 601/602 GCV Water
Associated Lab Samples: 928366001, 928366002, 928366003, 928366004, 928366005, 928366006
METHOD BLANK: 47305
Associated Lab Samples:
Parameter
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1, 1 -Dichloroethene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene ·
1,4-0ichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dichlorodifluoromethane
Diisopropyl ether
Ethyl benzene
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
Naphthalene
a-Xylene
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethane
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
1-Chloro-3-fluorobenzene (S)
Date: 12/05/200711:27 AM
928366001, 928366002,928366003,928366004,928366005,928366006
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
Blank Reporting
Units Result Limit Qualifiers
ND 1,0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1,0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 2.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 2,0
ND 1.0
ND 2.0
ND 2.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 1.0
ND 2.0
100 65-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, rJc 28078
(704)875-~09~
Page 26 of 32
Pace Analytical Services, Inc.
2225 Riverside Dr. a{J Ana/ytica/0
, i1 www.pacelabs.com
I
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 926366
LABORATORY CONTROL SAMPLE: 47306
Spike LCS LCS
Parameter Units Cone. Result %Rec
1, 1, 1-T richloroethane
1, 1,2,2-T etrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chiaro methane
cis-1,2-Dichloroethene
· cis-1,3-Dichloropropene
Dibromochloromethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
Naphthalene
o-Xylene
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dlchloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
1-Chloro-3-fluorobenzene (S)
MATRIX SPIKE SAMPLE:
Parameter
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
Date: 12/05/2007 11 :27 AM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
47307
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
20
20
20
20
20
20
20
20
60
928179007
22.5
15.5
20.1
23.4
18.9
23.1
22.3
23.9
20.6
20.9
20.6
21.1
20.9
22.5
23.1
15.6
21.0
19.7
15.0
16.0
15.4
16.6
21.1
19.8
20.7
22.6
44.0
19.8
22.6
21.8
21.5
20.1
20.7
16.9
20.3
21.7
20.7
16.3
65.5
Spike
112
78
101
117
95
116
112
119
104
104
104
105
105
113
116
78
105
98
75
60
77
93
105
99
103
113
110
99
113
109
107
101
104
94
101
109
103
92
109
108
MS
Units Result Cone. Result
ug/L
ug/L
ug/L
ND 20 25.1
ND 20 14.8
ND 20 15.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
zt~i~ 1lae11 . :1
%Rec
Limits
41-138
6-184
39-136
47-132
28-167
50-150
1-206
51-147
44-156
7-187
42-143
39-150
42-172
13-159
1-144
43-143
36-150
46-137
49-133
1-193
38-155
22-178
24-191
46-157
89-108
32-160
82-115
86-110
25-162
50-150
91-110
26-162
46-148
38-155
22-178
35-146
21-156
28-163
50-150
65-137
MS
% Rec
125
74
76
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
%Rec
Limits
41-136
6-164
39-136
Qualifiers
Page 27 of 32
f2·~· Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave .. Suite 100
Asheville, NC 28804 Huntersville,t\jC 28078 F!
[phone] (704}875-909i
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
MATRIX SPIKE SAMPLE: 47307
928179007 Spike MS MS %Rec
Parameter Units Result Cone. Result %Rec Limits Qualifiers
1, 1-Dichloroethane ug/L ND 20 25.3 127 47-132
1, 1-Dichloroethene ug/L ND 20 21.4 107 28-167
1,2-Dibromoethane (EDS) ug/L ND 20 19.8 99 50-150
1,2-Dichlorobenzene ug/L ND 20 20.2 101 1-208
1,2-Dichloroethane ug/L ND 20 24.2 121 51-147
1,2-Dlchloropropane ug/L ND 20 19.2 96 44-156
1,3-Dichlorobenzene ug/L ND 20 19.7 98 7-187
1,4-Dichlorobenzene ug/L ND 20 19.8 99 42-143
Benzene ug/L ND 20 20.9 105 39-150
Bromodichloromethane ug/L ND 20 19.6 98 42-172
Bromoform ug/L ND 20 20.3 101 13-159
Bromomethane ug/L ND 20 20.5 102 1-144
Carbon tetrachloride ug/L ND 20 21.1 106 43-143
Chlorobenzene ug/L ND 20 17.7 88 38-150
Chloroethane ug/L ND 20 21.1 105 46-137
Chloroform ug/L ND 20 16.4 82 49-133
Chloromethane ug/L ND 20 20.8 104 1-193
cis-1,2-Dichloroethene ug/L ND 20 18.7 93 38-155
cis-1,3-Dichloropropene ug/L ND 20 13.8 69 22-178
Dibromochloromethane ug/L ND 20 16.0 80 24-191
Dichlorodifluoromethane ug/L ND 20 21.5 107 48-157
Diisopropyl ether ug/L ND 20 20.6 103 89-108
Ethyl benzene ug/L ND 20 21.3 106 32-160
m&p-Xylene ug/L ND 40 42.7 107 82-115
Methyl-tert-butyl ether ug/L ND 20 20.1 100 88-110
Methylene Chloride ug/L ND 20 23.8 119 25-162
Naphthalene ug/L ND 20 20.6 103 50-150
a-Xylene ug/L ND 20 21.0 105 91-110
T etrachloroethene ug/L ND 20 18.1 91 26-162
Toluene ug/L ND 20 20.4 102 46-148
trans-1,2-Dichloroethene ug/L ND 20 19.8 99 38-155
trans-1,3-Dichloropropene ug/L ND 20 16.5 82 22-178
Trichloroethene ug/L ND 20 21.0 105 35-146
Trichlorofluoromethane ug/L ND 20 22.1 110 21-156
Vinyl chloride ug/L ND 20 22.6 113 28-163
Xylene (Total) ug/L ND 60 63.6 106 50-150
1-Chloro-3-fluorobenzene (S) % 95 65-137
MATRIX SPIKE SAMPLE: 47308
928718002 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
1, 1, 1-Trlchloroethane ug/L ND 20 23.0 115 41-138
1, 1,2,2-Tetrachloroethane ug/L ND 20 21.1 105 8-184
1, 1,2-Trichloroethane ug/L ND 20 17.6 88 39-136
1, 1-Dichloroethane ug/L ND 20 21.6 108 47-132
1, 1-Dichloroethene ug/L ND 20 19.2 96 28-167
1,2-Dibromoelhane (EDS) ug/L ND 20 20.6 103 50-150
Dale: 12/05/2007 11 :27 AM REPORT OF LABORATORY ANALYSIS Page 28 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Jnc ..
1tftJ~~~t
/1c~J::1.~r!-:!~!!"
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
I [phone] [phone]
QUALITY CONTROL DATA
Project: TEXACO FOODMART #2
Pace Project No.: 928366
MATRIX SPIKE SAMPLE: 47308
928718002 Spike MS MS %Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
1,2-Dichlorobenzene ug/L ND 20 21.2 106 1-208
1,2-Dichloroethane ug/L ND 20 23.1 115 51-147
1,2·Dichloropropane ug/L ND 20 20.0 100 44-156
1, 3-Dichlorobenzene ug/L ND 20 20.6 103 7-187
1 ,4-Dichlorobenzene ug/L ND 20 20.7 103 42-143
Benzene ug/L ND 20 21.1 105 39-150
Bromodichloromethane ug/L ND 20 19.4 97 42-172
Bromoform ug/L ND 20 22.5 113 13-159
Bromomethane ug/L ND 20 18.6 93 1-144
Carbon tetrachloride ug/L ND 20 23.0 115 43-143
Chlorobenzene ug/L ND 20 20.2 101 38-150
Chloroethane ug/L ND 20 20.3 101 46-137
Chloroform ug/L ND 20 15.8 79 49-133
Chloromethane ug/L ND 20 18.8 94 1-193
cis-1,2-Dichloroethene ug/L ND 20 15_8 79 38-155
cis-1,3-Dichloropropene ug/L ND 20 13.9 69 22-178
Dibromochloromethane ug/L ND 20 17.4 87 24-191
Dichlorodifluoromethane ug/L ND 20 20.9 105 48-157
Diisopropyl ether ug/L ND 20 20.2 101 89-108
Ethyl benzene ug/L ND 20 21.5 108 32-160
m&p-Xylene ug/L ND 40 43.0 108 82-115
Methyl-tart-butyl ether ug/L ND 20 19_5 98 88-110
Methylene Chloride ug/L ND 20 20.8 104 25-162
Naphthalene ug/L ND 20 20.0 100 50-150
o-Xylene ug/L ND 20 20.9 104 91-110
T etrachloroethene ug/L ND 20 19.2 96 26-162
Toluene ug/L ND 20 20.6 103 46-148
trans-1,2-Dichloroethene ug/L ND 20 17.0 85 38-155
trans-1,3-Dichloropropene ug/L ND 20 18.2 91 22-178
Trichloroethene ug/L ND 20 21.6 108 35-146
T richlorofluoromethane ug/L ND 20 19.5 97 21-156
Vinyl chloride ug/L ND 20 20.6 103 28-163
Xylene (Total) ug/L ND 60 63.9 106 50-150
1-Chloro-3-fiuorobenzene (S) % 98 65-137
SAMPLE DUPLICATE: 47309
928617001 Dup
Parameter Units Result Result RPD Qualifiers
1, 1, 1-Trichloroethane ug/L ND ND 0
1, 1,2,2-Tetrachloroethane ug/L ND ND 0
1, 1,2-Trichloroethane ug/L ND ND 0
1, 1-Dichloroethane ug/L ND ND 0
1, 1-Dichloroethene ug/L ND ND 0
1,2-Dibromoethane (EDB) ug/L ND ND 0
1,2-Dichlorobenzene ug/L ND ND 0
1,2-Dichloroethane ug/L ND ND 0
1,2-Dichloropropane ug/L ND ND 0
Date: 12/05/2007 11:27 AM REPORT OF LABORATORY ANALYSIS Page 29 of 32
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,~. •-~.~o~ ,1~!~\ .,1 ..... l,a
Pace Analytical Services, Inc.
2225 Riverside Dr.
QUALITY CONTROL DATA
Asheville, NC 28804
[phone]
Project: TEXACO FOODMART #2
Pace Project No.: 928366
SAMPLE DUPLICATE: 47309
Parameter
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dichlorodlfluoromethane
Diisopropyl ether
Ethylbenzene
m&p-Xylene
Methyl-tert-butyl ether
_Methylene Chloride
Naphthalene
o-Xylene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylene (Total)
1-Chloro-3-fluorobenzene (S)
Date: 12105/2007 11 :27 AM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
928617001 Dup
Units Result Result RPD
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
8.5 9.0
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
104 100
REPORT OF LABO RA TORY ANALYSIS
Thls report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
··ne•" .,,_1'·f,t'-'.• •• ~I ""r:.~ ,, .. ...~,,
Qualifiers
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
6
0
0
0
0
0
0
0
0
0
0
0
3
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville.~C 28078
(704)87&-09092
Page 30 of 32
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: TEXACO FOODMART #2
Pace Project No.: 928366
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes ln sample preparation, dilution of
the sample aliquot, or moisture content.
ND -Not Detected at or above adjusted reporting limit.
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S -Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D)-Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPO -Relative Percent Difference
NC -Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANAL YTE QUALIFIERS
D3
LO
S4
1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
Analyte recovery in the laboratory control sample (LCS) was outside QC llmits.
Surrogate recovery not evaluated against control limits due to sample dilution.
Percent Relative Percent Difference (RPD) fall for most of the compounds in the LCS/LCSD. Data was accepted based
on acceptable recoveries of the target compounds in the LCS/LCSD and acceptable recoveries of the surrogates in the
associated samples.
Date: 12/05/200711:27 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Page 31 of 32
./ aeAnalytica/0
( .. ,/~, uvo www.pocoleb,.o,m
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, llC 28078
(704)875'"92
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: TEXACO FOODMART #2
Pace Project No.: 928366
Lab ID Sample ID
928366001 MW-1
928366002 MW-2
928366003 MW-3
928366004 MW-4
928366005 MW-5
928366006 T-1
928366001 MW-1
928366002 MW-2
928366003 MW-3
928366004 MW-4
928366005 MW-5
928366006 T-1
928366001 MW-1
928366002 MW-2
928366004 MW-4
928366005 MW-5
928366006 T-1
928366001 MW-1
928366002 MW-2
928366003 MW-3
928366004 MW-4
928366005 MW-5
928366006 T-1
Date: 12/05/2007 11 :27 AM
QC Balch Method QC Batch
EPA 625 OEXT/1795
EPA 625 OEXT/1795
EPA 625 OEXT/1795
EPA 625 OEXT/1795
EPA 625 OEXT/1795
EPA 625 OEXT/1795
MADEP EPH OEXT/1818
MADEP EPH OEXT/1818
MADEP EPH OEXT/1818
MADEP EPH OEXT/1818
MADEP EPH OEXT/1818
MADEP EPH OEXT/1818
MADEPVPH GCV/1407
MADEP VPH GCV/1407
MADEPVPH GCV/1407
MADEP VPH GCV/1407
MADEP VPH GCV/1407
EPA 601/602 GCV/1418
EPA 601/602 GCV/1418
EPA 6011602 GCV/1418
EPA 6011602 GCV/1418
EPA 6011602 GCV/1418
EPA 601/602 GCV/1418
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
jftJ~'?i
Analytical
Analytical Method Batch
EPA 625 MSSV/1273
EPA 625 MSSV/1273
EPA 625 MSSV/1273
EPA 625 MSSV/1273
EPA 625 MSSV/1273
EPA 625 MSSV/1273
MADEP EPH GCSV/1743
MADEP EPH GCSV/1743
MADEP EPH GCSV/1743
MADEP EPH GCSV/1743
MADEP EPH GCSV/1743
MADEP EPH GCSV/1743
Page 32 of 32
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