WS-1024_30199_CA_LAB_20100302_Analytical Rpt

Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270989
G0210480
WSW-2
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
13:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.040
Page 1 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270989
G0210480
WSW-2
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
13:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.23
Page 2 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270989
G0210480
WSW-2
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
13:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/22/10 22:31 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13089
Dibromofluoromethane 70 - 130113
Bromofluorobenzene 70 - 13095
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 3 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270990
G0210480
WSW-4
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.040
Page 4 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270990
G0210480
WSW-4
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
Chloromethane 1.1 µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.23
Page 5 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270990
G0210480
WSW-4
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/22/10 23:05 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13092
Dibromofluoromethane 70 - 130116
Bromofluorobenzene 70 - 13096
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 6 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270991
G0210480
WSW-6
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.040
Page 7 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270991
G0210480
WSW-6
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.23
Page 8 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270991
G0210480
WSW-6
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/22/10 23:38 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13092
Dibromofluoromethane 70 - 130114
Bromofluorobenzene 70 - 13097
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 9 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270992
G0210480
WSW-7
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.040
Page 10 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270992
G0210480
WSW-7
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.23
Page 11 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270992
G0210480
WSW-7
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/23/10 0:12 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13091
Dibromofluoromethane 70 - 130115
Bromofluorobenzene 70 - 13092
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 12 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270993
G0210480
WSW-8
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
10:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
1,2-Dichloroethane 1.4 µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.040
Page 13 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270993
G0210480
WSW-8
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
10:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.23
Page 14 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270993
G0210480
WSW-8
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
10:20
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/22/10 21:57 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 130102
Dibromofluoromethane 70 - 130125
Bromofluorobenzene 70 - 130108
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 15 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270994
G0210480
WSW-10
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.040
Page 16 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270994
G0210480
WSW-10
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.23
Page 17 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270994
G0210480
WSW-10
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
15:30
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/23/10 0:45 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13092
Dibromofluoromethane 70 - 130112
Bromofluorobenzene 70 - 13096
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 18 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270995
G0210480
WSW-11
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:45
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.040
Page 19 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270995
G0210480
WSW-11
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:45
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
Chloromethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.23
Page 20 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270995
G0210480
WSW-11
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
14:45
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/23/10 1:19 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 130101
Dibromofluoromethane 70 - 130127
Bromofluorobenzene 70 - 130106
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 21 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270996
G0210480
WSW-12
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
16:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
1,1,1-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
1,1,2,2-Tetrachloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
1,1,2-Trichloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
1,1-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
1,1-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
1,1-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
1,2,3-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.23
1,2,3-Trichloropropane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.15
1,2,4-Trichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.28
1,2,4-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.14
1,2-Dibromo-3-chloropropane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.37
1,2-Dibromoethane (EDB)BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.11
1,2-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
1,2-Dichloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
1,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.080
1,3,5-Trimethylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.080
1,3-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.10
1,3-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.060
1,4-Dichlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
2,2-Dichloropropane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.22
2-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
2-Hexanone BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry5.0 0.19
4-Chlorotoluene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.13
4-Methyl-2-pentanone (MIBK)BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry5.0 0.13
Acetone BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry5.0 0.62
Benzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.040
Page 22 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270996
G0210480
WSW-12
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
16:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
Bromobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.10
Bromochloromethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.14
Bromodichloromethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.080
Bromoform BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.040
Bromomethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.27
Carbon tetrachloride BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.11
Chlorobenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
Chlorodibromomethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
Chloroethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.22
Chloroform BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
Chloromethane 1.3 µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.30
cis-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
cis-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.10
Dibromomethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.21
Dichlorodifluoromethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.30
Ethanol BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry200 42
Ethylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
Hexachlorobutadiene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.30
Isopropyl ether (IPE)BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.080
Isopropylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.10
m,p-Xylenes BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.13
Methyl ethyl ketone (MEK)BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry5.0 0.90
Methyl t-butyl ether (MTBE)BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.11
Methylene chloride BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.080
n-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry1.0 0.24
n-Propylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.090
Naphthalene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.23
Page 23 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Laboratory Report
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
03/02/10
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Moores Exxon
TA-02 30199Project Name:
Project ID:
WaterSample Matrix:
270996
G0210480
WSW-12
02/12/10
02/15/10
Client Sample ID:
Prism Sample ID:
COC Group:
Time Collected:
Time Submitted:17:20
16:00
Parameter Units ReportResult
Limit
MDL Dilution
Factor
Method Analysis
Date/Time
Analyst Batch
ID
o-Xylene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.060
p-Isopropyltoluene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.14
sec-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.12
Styrene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.050
tert-Butylbenzene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
Tetrachloroethene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.12
Toluene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.060
trans-1,2-Dichloroethene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
trans-1,3-Dichloropropene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.043
Trichloroethene BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.070
Trichlorofluoromethane BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.31
Vinyl acetate BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry2.0 0.10
Vinyl chloride BRL µg/L 1 SM6200 B 02/23/10 4:41 Q48108lwitry0.50 0.28
Surrogate % Recovery Control Limits
Toluene-d8 70 - 13096
Dibromofluoromethane 70 - 130101
Bromofluorobenzene 70 - 13093
Angela D. Overcash, V.P. Laboratory Services
Sample Comment(s):
J- Estimated value between the Reporting Limit and the MDL.
The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than
NELAC certification except for those instances indicated in the case narrative and/or test comments.
All results are reported on a wet-weight basis
BRL = Below Reporting Limit
Page 24 of 24
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Volatile Organic Compounds by GC/MS, method SM6200 B
Method Blank QC Batch
IDUnitsRL Control LimitResult
1,1,1,2-Tetrachloroethane ND Q481080.5 <0.25 µg/L
1,1,1-Trichloroethane ND Q481080.5 <0.25 µg/L
1,1,2,2-Tetrachloroethane ND Q481080.5 <0.25 µg/L
1,1,2-Trichloroethane ND Q481080.5 <0.25 µg/L
1,1-Dichloroethane ND Q481080.5 <0.25 µg/L
1,1-Dichloroethene ND Q481080.5 <0.25 µg/L
1,1-Dichloropropene ND Q481080.5 <0.25 µg/L
1,2,3-Trichlorobenzene ND Q481082<1 µg/L
1,2,3-Trichloropropane ND Q481081<0.5 µg/L
1,2,4-Trichlorobenzene ND Q481081<0.5 µg/L
1,2,4-Trimethylbenzene ND Q481080.5 <0.25 µg/L
1,2-Dibromo-3-chloropropane ND Q481082<1 µg/L
1,2-Dibromoethane (EDB) ND Q481080.5 <0.25 µg/L
1,2-Dichlorobenzene ND Q481080.5 <0.25 µg/L
1,2-Dichloroethane ND Q481080.5 <0.25 µg/L
1,2-Dichloropropane ND Q481080.5 <0.25 µg/L
1,3,5-Trimethylbenzene ND Q481080.5 <0.25 µg/L
1,3-Dichlorobenzene ND Q481080.5 <0.25 µg/L
1,3-Dichloropropane ND Q481080.5 <0.25 µg/L
1,4-Dichlorobenzene ND Q481080.5 <0.25 µg/L
2,2-Dichloropropane ND Q481082<1 µg/L
2-Chlorotoluene ND Q481080.5 <0.25 µg/L
2-Hexanone ND Q481085<2.5 µg/L
4-Chlorotoluene ND Q481080.5 <0.25 µg/L
4-Methyl-2-pentanone (MIBK) ND Q481085<2.5 µg/L
Acetone ND Q481085<2.5 µg/L
Benzene ND Q481080.5 <0.25 µg/L
Bromobenzene ND Q481080.5 <0.25 µg/L
Bromochloromethane ND Q481080.5 <0.25 µg/L
Bromodichloromethane ND Q481080.5 <0.25 µg/L
Bromoform ND Q481082<1 µg/L
Bromomethane ND Q481081<0.5 µg/L
Carbon tetrachloride ND Q481080.5 <0.25 µg/L
Chlorobenzene ND Q481080.5 <0.25 µg/L
Page 1 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Method Blank QC Batch
IDUnitsRL Control LimitResult
Chlorodibromomethane ND Q481080.5 <0.25 µg/L
Chloroethane ND Q481080.5 <0.25 µg/L
Chloroform ND Q481080.5 <0.25 µg/L
Chloromethane ND Q481080.5 <0.25 µg/L
cis-1,2-Dichloroethene ND Q481080.5 <0.25 µg/L
cis-1,3-Dichloropropene ND Q481080.5 <0.25 µg/L
Dibromomethane ND Q481080.5 <0.25 µg/L
Dichlorodifluoromethane ND Q481081<0.5 µg/L
Ethanol ND Q48108200 <100 µg/L
Ethylbenzene ND Q481080.5 <0.25 µg/L
Hexachlorobutadiene ND Q481082<1 µg/L
Isopropyl ether (IPE) ND Q481080.5 <0.25 µg/L
Isopropylbenzene ND Q481080.5 <0.25 µg/L
m,p-Xylenes ND Q481081<0.5 µg/L
Methyl ethyl ketone (MEK) ND Q481085<2.5 µg/L
Methyl t-butyl ether (MTBE) ND Q481080.5 <0.25 µg/L
Methylene chloride ND Q481082<1 µg/L
n-Butylbenzene ND Q481081<0.5 µg/L
n-Propylbenzene ND Q481080.5 <0.25 µg/L
Naphthalene ND Q481082<1 µg/L
o-Xylene ND Q481080.5 <0.25 µg/L
p-Isopropyltoluene ND Q481080.5 <0.25 µg/L
sec-Butylbenzene ND Q481080.5 <0.25 µg/L
Styrene ND Q481080.5 <0.25 µg/L
tert-Butylbenzene ND Q481080.5 <0.25 µg/L
Tetrachloroethene ND Q481080.5 <0.25 µg/L
Toluene ND Q481080.5 <0.25 µg/L
trans-1,2-Dichloroethene ND Q481080.5 <0.25 µg/L
trans-1,3-Dichloropropene ND Q481080.5 <0.25 µg/L
Trichloroethene ND Q481080.5 <0.25 µg/L
Trichlorofluoromethane ND Q481080.5 <0.25 µg/L
Vinyl acetate ND Q481082<1 µg/L
Vinyl chloride ND Q481080.5 <0.25 µg/L
Laboratory Control Sample QC Batch IDUnitsSpike Amount %
Recovery Recovery
Ranges
%Result
1,1,1,2-Tetrachloroethane 22.39 Q4810820µg/L 112 70-130
Page 2 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Laboratory Control Sample QC Batch
IDUnitsSpike Amount %
Recovery Recovery Ranges
%Result
1,1,1-Trichloroethane 20.8 Q4810820µg/L 104 70-130
1,1,2,2-Tetrachloroethane 19.14 Q4810820µg/L 96 70-130
1,1,2-Trichloroethane 22.66 Q4810820µg/L 113 70-130
1,1-Dichloroethane 20.03 Q4810820µg/L 100 70-130
1,1-Dichloroethene 20.43 Q4810820µg/L 102 70-130
1,1-Dichloropropene 19.86 Q4810820µg/L 99 70-130
1,2,3-Trichlorobenzene 19.25 Q4810820µg/L 96 70-130
1,2,3-Trichloropropane 18.91 Q4810820µg/L 95 70-130
1,2,4-Trichlorobenzene 18.77 Q4810820µg/L 94 70-130
1,2,4-Trimethylbenzene 20.63 Q4810820µg/L 103 70-130
1,2-Dibromo-3-chloropropane 15.07 Q4810820µg/L 75 70-130
1,2-Dibromoethane (EDB) 20.51 Q4810820µg/L 103 70-130
1,2-Dichlorobenzene 18.85 Q4810820µg/L 94 70-130
1,2-Dichloroethane 22.79 Q4810820µg/L 114 70-130
1,2-Dichloropropane 19.67 Q4810820µg/L 98 70-130
1,3,5-Trimethylbenzene 20.71 Q4810820µg/L 104 70-130
1,3-Dichlorobenzene 18.97 Q4810820µg/L 95 70-130
1,3-Dichloropropane 20.2 Q4810820µg/L 101 70-130
1,4-Dichlorobenzene 18.32 Q4810820µg/L 92 70-130
2,2-Dichloropropane 21.59 Q4810820µg/L 108 70-130
2-Chlorotoluene 18.37 Q4810820µg/L 92 70-130
2-Hexanone 14.76 Q4810820µg/L 74 60-140
4-Chlorotoluene 18.97 Q4810820µg/L 95 70-130
4-Methyl-2-pentanone (MIBK) 15.33 Q4810820µg/L 77 60-140
Acetone 12.44 Q4810820µg/L 62 40-160
Benzene 21.68 Q4810820µg/L 108 70-130
Bromobenzene 19.14 Q4810820µg/L 96 70-130
Bromochloromethane 21.84 Q4810820µg/L 109 70-130
Bromodichloromethane 22.06 Q4810820µg/L 110 70-130
Bromoform 23 Q4810820µg/L 115 70-130
Bromomethane 21.64 Q4810820µg/L 108 60-140
Carbon tetrachloride 23.01 Q4810820µg/L 115 70-130
Chlorobenzene 19.57 Q4810820µg/L 98 70-130
Chlorodibromomethane 21.74 Q4810820µg/L 109 70-130
Chloroethane 20.43 Q4810820µg/L 102 60-140
Chloroform 23.98 Q4810820µg/L 120 70-130
Page 3 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Laboratory Control Sample QC Batch
IDUnitsSpike Amount %
Recovery Recovery Ranges
%Result
Chloromethane 21.47 Q4810820µg/L 107 60-140
cis-1,2-Dichloroethene 20.39 Q4810820µg/L 102 70-130
cis-1,3-Dichloropropene 20.33 Q4810820µg/L 102 70-130
Dibromomethane 21.69 Q4810820µg/L 108 70-130
Dichlorodifluoromethane 26.64 Q4810820µg/L 133 60-140
Ethanol 207.62 Q48108200µg/L 104 60-140
Ethylbenzene 21.99 Q4810820µg/L 110 70-130
Hexachlorobutadiene 18.25 Q4810820µg/L 91 70-130
Isopropyl ether (IPE) 18.49 Q4810820µg/L 92 70-130
Isopropylbenzene 19.19 Q4810820µg/L 96 70-130
m,p-Xylenes 44.32 Q4810840µg/L 111 70-130
Methyl ethyl ketone (MEK) 14.58 Q4810820µg/L 73 60-140
Methyl t-butyl ether (MTBE) 19.02 Q4810820µg/L 95 70-130
Methylene chloride 20.13 Q4810820µg/L 101 70-130
n-Butylbenzene 19.68 Q4810820µg/L 98 70-130
n-Propylbenzene 19.92 Q4810820µg/L 100 70-130
Naphthalene 17.46 Q4810820µg/L 87 70-130
o-Xylene 21.28 Q4810820µg/L 106 70-130
p-Isopropyltoluene 20.01 Q4810820µg/L 100 70-130
sec-Butylbenzene 19.18 Q4810820µg/L 96 70-130
Styrene 22.8 Q4810820µg/L 114 70-130
tert-Butylbenzene 19.51 Q4810820µg/L 98 70-130
Tetrachloroethene 20.54 Q4810820µg/L 103 70-130
Toluene 22.23 Q4810820µg/L 111 70-130
trans-1,2-Dichloroethene 19.09 Q4810820µg/L 95 70-130
trans-1,3-Dichloropropene 21.18 Q4810820µg/L 106 70-130
Trichloroethene 21.25 Q4810820µg/L 106 70-130
Trichlorofluoromethane 23.86 Q4810820µg/L 119 60-140
Vinyl acetate 24.88 Q4810820µg/L 124 60-140
Vinyl chloride 21.1 Q4810820µg/L 106 60-140
Matrix Spike QC Batch IDUnitsSpike Amount %
Recovery Recovery
Ranges
%Sample ID:Result
1,1,1,2-Tetrachloroethane 208.3 Q48108200µg/L 104 70-130270993
1,1,1-Trichloroethane 218.9 Q48108200µg/L 109 70-130
1,1,2,2-Tetrachloroethane 146 Q48108200µg/L 73 70-130
1,1,2-Trichloroethane 165.3 Q48108200µg/L 83 70-130
Page 4 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Matrix Spike QC Batch
IDUnitsSpike Amount %
Recovery Recovery Ranges
%Sample ID:Result
1,1-Dichloroethane 198.2 Q48108200µg/L 99 70-130270993
1,1-Dichloroethene 216 Q48108200µg/L 108 70-130
1,1-Dichloropropene 203.9 Q48108200µg/L 102 70-130
1,2,3-Trichlorobenzene 161.8 Q48108200µg/L 81 70-130
1,2,3-Trichloropropane 147.1 Q48108200µg/L 74 70-130
1,2,4-Trichlorobenzene 162.7 Q48108200µg/L 81 70-130
1,2,4-Trimethylbenzene 224 Q48108200µg/L 112 70-130
1,2-Dibromo-3-chloropropane 112.2 Q48108200µg/L 56 70-130#
1,2-Dibromoethane (EDB) 154 Q48108200µg/L 77 70-130
1,2-Dichlorobenzene 172.7 Q48108200µg/L 86 70-130
1,2-Dichloroethane 177 Q48108200µg/L 88 70-130
1,2-Dichloropropane 169.7 Q48108200µg/L 85 70-130
1,3,5-Trimethylbenzene 234.4 Q48108200µg/L 117 70-130
1,3-Dichlorobenzene 190.1 Q48108200µg/L 95 70-130
1,3-Dichloropropane 159 Q48108200µg/L 80 70-130
1,4-Dichlorobenzene 180.6 Q48108200µg/L 90 70-130
2,2-Dichloropropane 210.5 Q48108200µg/L 105 70-130
2-Chlorotoluene 198.4 Q48108200µg/L 99 70-130
2-Hexanone 91.2 Q48108200µg/L 46 60-140#
4-Chlorotoluene 202.1 Q48108200µg/L 101 70-130
4-Methyl-2-pentanone (MIBK) 86.7 Q48108200µg/L 43 60-140#
Acetone 77.3 Q48108200µg/L 39 40-160#
Benzene 212.2 Q48108200µg/L 106 70-130
Bromobenzene 179.8 Q48108200µg/L 90 70-130
Bromochloromethane 174.3 Q48108200µg/L 87 70-130
Bromodichloromethane 182 Q48108200µg/L 91 70-130
Bromoform 173.8 Q48108200µg/L 87 70-130
Bromomethane 228.6 Q48108200µg/L 114 60-140
Carbon tetrachloride 240.8 Q48108200µg/L 120 70-130
Chlorobenzene 197.6 Q48108200µg/L 99 70-130
Chlorodibromomethane 176.3 Q48108200µg/L 88 70-130
Chloroethane 221.9 Q48108200µg/L 111 60-140
Chloroform 225.5 Q48108200µg/L 113 70-130
Chloromethane 237.1 Q48108200µg/L 119 60-140
cis-1,2-Dichloroethene 190.7 Q48108200µg/L 95 70-130
cis-1,3-Dichloropropene 153 Q48108200µg/L 77 70-130
Page 5 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Matrix Spike QC Batch
IDUnitsSpike Amount %
Recovery Recovery Ranges
%Sample ID:Result
Dibromomethane 161.1 Q48108200µg/L 81 70-130270993
Dichlorodifluoromethane 316.9 Q48108200µg/L 158 60-140#
Ethanol 1722.1 Q481082000µg/L 86 60-140
Ethylbenzene 244.6 Q48108200µg/L 122 70-130
Hexachlorobutadiene 211.5 Q48108200µg/L 106 70-130
Isopropyl ether (IPE) 152.6 Q48108200µg/L 76 70-130
Isopropylbenzene 220.5 Q48108200µg/L 110 70-130
m,p-Xylenes 493.2 Q48108400µg/L 123 70-130
Methyl ethyl ketone (MEK) 107.4 Q48108200µg/L 54 60-140#
Methyl t-butyl ether (MTBE) 129 Q48108200µg/L 65 70-130#
Methylene chloride 178 Q48108200µg/L 89 70-130
n-Butylbenzene 227.5 Q48108200µg/L 114 70-130
n-Propylbenzene 229.4 Q48108200µg/L 115 70-130
Naphthalene 128.7 Q48108200µg/L 64 70-130#
o-Xylene 221.8 Q48108200µg/L 111 70-130
p-Isopropyltoluene 230.8 Q48108200µg/L 115 70-130
sec-Butylbenzene 220.7 Q48108200µg/L 110 70-130
Styrene 222.2 Q48108200µg/L 111 70-130
tert-Butylbenzene 225.2 Q48108200µg/L 113 70-130
Tetrachloroethene 231.3 Q48108200µg/L 116 70-130
Toluene 220.1 Q48108200µg/L 110 70-130
trans-1,2-Dichloroethene 198.6 Q48108200µg/L 99 70-130
trans-1,3-Dichloropropene 151.6 Q48108200µg/L 76 70-130
Trichloroethene 216 Q48108200µg/L 108 70-130
Trichlorofluoromethane 259.6 Q48108200µg/L 130 60-140
Vinyl acetate 166 Q48108200µg/L 83 60-140
Vinyl chloride 231.4 Q48108200µg/L 116 60-140
Matrix Spike Duplicate QC Batch IDUnitsSpike Amount %
Recovery RPD RPD
Range
Recovery
Ranges
%%%Sample ID:Result
1,1,1,2-Tetrachloroethane 212.4 Q48108200µg/L 106 70-130 2 0 - 20270993
1,1,1-Trichloroethane 220.6 Q48108200µg/L 110 70-130 1 0 - 20
1,1,2,2-Tetrachloroethane 151.2 Q48108200µg/L 76 70-130 3 0 - 20
1,1,2-Trichloroethane 168.4 Q48108200µg/L 84 70-130 2 0 - 20
1,1-Dichloroethane 203.1 Q48108200µg/L 102 70-130 2 0 - 20
1,1-Dichloroethene 222.3 Q48108200µg/L 111 70-130 3 0 - 20
1,1-Dichloropropene 213.8 Q48108200µg/L 107 70-130 5 0 - 20
Page 6 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Matrix Spike Duplicate QC Batch
IDUnitsSpike Amount %
Recovery RPD RPD RangeRecovery Ranges
%%%Sample ID:Result
1,2,3-Trichlorobenzene 168.9 Q48108200µg/L 84 70-130 4 0 - 20270993
1,2,3-Trichloropropane 154.8 Q48108200µg/L 77 70-130 5 0 - 20
1,2,4-Trichlorobenzene 172.1 Q48108200µg/L 86 70-130 6 0 - 20
1,2,4-Trimethylbenzene 230.4 Q48108200µg/L 115 70-130 3 0 - 20
1,2-Dibromo-3-chloropropane 115.8 Q48108200µg/L 58 70-130#30 - 20
1,2-Dibromoethane (EDB) 160.7 Q48108200µg/L 80 70-130 4 0 - 20
1,2-Dichlorobenzene 177.7 Q48108200µg/L 89 70-130 3 0 - 20
1,2-Dichloroethane 180.7 Q48108200µg/L 90 70-130 2 0 - 20
1,2-Dichloropropane 175.4 Q48108200µg/L 88 70-130 3 0 - 20
1,3,5-Trimethylbenzene 239.4 Q48108200µg/L 120 70-130 2 0 - 20
1,3-Dichlorobenzene 195.2 Q48108200µg/L 98 70-130 3 0 - 20
1,3-Dichloropropane 162.3 Q48108200µg/L 81 70-130 2 0 - 20
1,4-Dichlorobenzene 183.5 Q48108200µg/L 92 70-130 2 0 - 20
2,2-Dichloropropane 211.4 Q48108200µg/L 106 70-130 0 0 - 20
2-Chlorotoluene 204 Q48108200µg/L 102 70-130 3 0 - 20
2-Hexanone 96.8 Q48108200µg/L 48 60-140#60 - 20
4-Chlorotoluene 207.8 Q48108200µg/L 104 70-130 3 0 - 20
4-Methyl-2-pentanone (MIBK) 93.2 Q48108200µg/L 47 60-140#70 - 20
Acetone 88.9 Q48108200µg/L 44 40-160 14 0 - 20
Benzene 217.6 Q48108200µg/L 109 70-130 3 0 - 20
Bromobenzene 184.1 Q48108200µg/L 92 70-130 2 0 - 20
Bromochloromethane 177.2 Q48108200µg/L 89 70-130 2 0 - 20
Bromodichloromethane 187.3 Q48108200µg/L 94 70-130 3 0 - 20
Bromoform 172.9 Q48108200µg/L 86 70-130 1 0 - 20
Bromomethane 228.9 Q48108200µg/L 114 60-140 0 0 - 20
Carbon tetrachloride 244.8 Q48108200µg/L 122 70-130 2 0 - 20
Chlorobenzene 200.3 Q48108200µg/L 100 70-130 1 0 - 20
Chlorodibromomethane 178.2 Q48108200µg/L 89 70-130 1 0 - 20
Chloroethane 219.2 Q48108200µg/L 110 60-140 1 0 - 20
Chloroform 229.7 Q48108200µg/L 115 70-130 2 0 - 20
Chloromethane 242.7 Q48108200µg/L 121 60-140 2 0 - 20
cis-1,2-Dichloroethene 195.5 Q48108200µg/L 98 70-130 2 0 - 20
cis-1,3-Dichloropropene 159.2 Q48108200µg/L 80 70-130 4 0 - 20
Dibromomethane 165.7 Q48108200µg/L 83 70-130 3 0 - 20
Dichlorodifluoromethane 323.6 Q48108200µg/L 162 60-140#20 - 20
Ethanol 1879.1 Q481082000µg/L 94 60-140 9 0 - 20
Page 7 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
Level II QC Report
03/02/10
G0210480
02/15/10
COC Group Number:
Date/Time Submitted:17:20
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
NC DENR State Trust Fund
Connel Ware
3718 Old Battleground Road
Greensboro, NC 27410
Attn:
Moores Exxon
TA-02 30199Project
Name:
Project ID:
Matrix Spike Duplicate QC Batch
IDUnitsSpike Amount %
Recovery RPD RPD RangeRecovery Ranges
%%%Sample ID:Result
Ethylbenzene 244.8 Q48108200µg/L 122 70-130 0 0 - 20270993
Hexachlorobutadiene 223.1 Q48108200µg/L 112 70-130 5 0 - 20
Isopropyl ether (IPE) 157.5 Q48108200µg/L 79 70-130 3 0 - 20
Isopropylbenzene 228.9 Q48108200µg/L 114 70-130 4 0 - 20
m,p-Xylenes 492 Q48108400µg/L 123 70-130 0 0 - 20
Methyl ethyl ketone (MEK) 109.4 Q48108200µg/L 55 60-140#20 - 20
Methyl t-butyl ether (MTBE) 132.9 Q48108200µg/L 66 70-130#30 - 20
Methylene chloride 184.1 Q48108200µg/L 92 70-130 3 0 - 20
n-Butylbenzene 234.1 Q48108200µg/L 117 70-130 3 0 - 20
n-Propylbenzene 235.4 Q48108200µg/L 118 70-130 3 0 - 20
Naphthalene 138.3 Q48108200µg/L 69 70-130#70 - 20
o-Xylene 224.9 Q48108200µg/L 112 70-130 1 0 - 20
p-Isopropyltoluene 235.1 Q48108200µg/L 118 70-130 2 0 - 20
sec-Butylbenzene 228.8 Q48108200µg/L 114 70-130 4 0 - 20
Styrene 226.9 Q48108200µg/L 113 70-130 2 0 - 20
tert-Butylbenzene 230.9 Q48108200µg/L 115 70-130 2 0 - 20
Tetrachloroethene 232.8 Q48108200µg/L 116 70-130 1 0 - 20
Toluene 225.3 Q48108200µg/L 113 70-130 2 0 - 20
trans-1,2-Dichloroethene 203.1 Q48108200µg/L 102 70-130 2 0 - 20
trans-1,3-Dichloropropene 158.8 Q48108200µg/L 79 70-130 5 0 - 20
Trichloroethene 221.8 Q48108200µg/L 111 70-130 3 0 - 20
Trichlorofluoromethane 254.1 Q48108200µg/L 127 60-140 2 0 - 20
Vinyl acetate 175.6 Q48108200µg/L 88 60-140 6 0 - 20
Vinyl chloride 234.7 Q48108200µg/L 117 60-140 1 0 - 20
#-See Case Narrative
Page 8 of 8449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.