Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
3901_Granville_Oxford_MSWLF_Unit2_March23GW_FID1812294_20230728
hart '-4 hickman SMARTER ENVIRONMENTAL SOLUTIONS Via E-Mail sbray@garTett-moore.com July 25, 2023 Garrett & Moore, Inc. 1029 West South Street Raleigh, NC 27603 Attn: Mr. Stefan Bray, PE Re: Water Quality Monitoring Report — March 2023 Granville County Oxford Unit 2 Landfill Oxford, Granville County, NC Facility Permit No. 3 901 -MSWLF-2012 H&H Job No. GMI-005 Dear Stefan: Hart & Hickman, PC (H&H) is submitting the attached Water Quality Monitoring Report — March 2023 documenting sample results for the Oxford Unit 2 Landfill for the first semi-annual sampling event of 2023. H&H appreciates the opportunity to work with you on this project. If you have any questions or require additional information, please do not hesitate to contact us at 704-586- 0007. Very truly yours, Hart & Hickman, PC Jason Soban, PG Project Manager Jeffrey 011ison Project Environmental Scientist 2923 South Tryon Street, Suite 100 Charlotte, NC 28203 704.S86.0007 main 3921 Sunset Ridge Rd, Suite 307 Raleigh, NC 27607 www.harthickman.com 919.847.4241 main I ENR USE ONLY: ❑Paper Report [:]Electronic Data - Email CD (data loaded: Yes / No )_ Doc/Event #: NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Garrett & Moore, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Stefan Bray Phone: 919-792-1903 E-mail: sbray@garrett-moore.com INC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address Facility Permit # (.0500 or .1600) October 20-24. 2006) Granville County 15854 Landfill Road 3901- Oxford Landfill Unit 2 Oxford. NC 27565 MSWLF-2012 1600 March 29-30, 2023 i Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring OX Assessment Monitoring Corrective Action T e of data submitted: (Check all that apply) X Groundwater monitoring data from monitoring wells ❑ Methane gas monitoring data Groundwater monitoring data from private water supply wells ❑ Corrective action data (specify) Leachate monitoring data X Surface water monitoring data ❑ Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Jason Soban, PG Consultant for Facility (704) 887-4622 Facility Representative Name (Print) Title (Are Ile ?1 2sI z3 Signature iF Date 2923 S Tryon Street, Suite 100, Charlotte, NC 28203 Facility Representative Address C-1269 (Engineering) 245 (Geology) NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Code) Telephone Number Affix NC LicenVAPM%I11p1*+Geologist Seal .L "s SEAL 2318 We OL '�'grrrrr urrr<+H++ Water Quality Monitoring Report March 2023 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 July 25, 2023 GARRETT &MOOREEP22 Engineering for the Power and Waste Industries hart � hickman SMARTER ENVIRONMENTAL SOLUTIONS 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd , Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919,847.4241 main Water Quality Monitoring Report — March 2023 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 Table of Contents Section Paj4e 1.0 Introduction.................................................................................................................I 1.1 Site Information........................................................................................................1 1.2 Regulatory Status......................................................................................................2 1.3 Groundwater Monitoring Program...........................................................................2 1.4 Surface Water Monitoring Program.........................................................................2 2.0 Water Quality Monitoring Activities........................................................................3 2.1 Water Level Measurements......................................................................................3 2.2 Groundwater Sampling Methods..............................................................................3 2.3 Surface Water Sampling Methods............................................................................4 2.4 Sample Equipment Management..............................................................................4 2.5 Sample Handling and Laboratory Analyses .............................................................4 3.0 Water Quality Monitoring Results............................................................................6 3.1 Groundwater Flow and Hydraulic Gradient .............................................................6 3.2 Groundwater Analytical Results...............................................................................7 3.3 Surface Water Analytical Results.............................................................................8 3.4 Quality Assurance/Quality Control Results..............................................................9 4.0 Conclusions ................................................................................................................10 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 hart h i c km a n First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Much 2023.docx P. SMARTER ENVIRONMENTAL SOLUTIONS List of Tables Table 1 Summary of Well Construction Details Table 2 Summary of Groundwater Elevations Table 3 Summary of Field Parameters Table 4 Summary of Groundwater Flow Velocity Table 5 Summary of Groundwater and Surface Water Constituent Detections List of Figures Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Groundwater Potentiometric Map (March 2023) List of Appendices Appendix A Groundwater and Surface Water Sampling Records Appendix B Laboratory Analytical Reports Appendix C Summary of Historical Groundwater Elevations Appendix D Summary of Historical Constituents in Groundwater Appendix E Summary of Historical Constituents in Surface Water ii https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 ■ First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_Much 2023.docx hart : h i C km a n SMARTER ENVIRONMENTAL SOLUTIONS Water Quality Monitoring Report — March 2023 Granville County Oxford Unit 2 Landfill Oxford, North Carolina Permit No. 3901-MSWLF-2012 H&H Job No. GMI-005 1.0 Introduction This Water Quality Monitoring Report (Report) has been prepared by Hart & Hickman, PC (H&H) to document the methods and results of semi-annual groundwater and surface water monitoring activities conducted at the Granville County Oxford Unit 2 Landfill located at 6584 Landfill Road, Oxford, Granville County, North Carolina. A site location map is included as Figure 1. Water quality monitoring at the site was performed in general accordance with the Water Quality Monitoring Plan (WQMP; March 2019) which was approved by the North Carolina Department of Environmental Quality (DEQ) Solid Waste Section (SWS). 1.1 Site Information The Granville County Oxford Landfill consists of two separate waste disposal units (Unit 1 and Unit 2). The facility is owned and operated by Granville County under Permit Numbers 3901- CDLF-1997 (Unit 1) and 3901-MSWLF-2012 (Unit 2) issued by DEQ SWS. The permitted facility consists of approximately 283 acres, of which approximately 29 acres constitutes the Unit 1 waste unit and 37.3 acres constitutes the Unit 2 waste unit. A site layout map that depicts the facility features is included as Figure 2. The Oxford Unit 1 Landfill is a former unlined municipal solid waste (MSW) landfill originally permitted for disposal of domestic, institutional, industrial, agricultural, and demolition wastes. The Oxford Unit 1 Landfill was closed in 1997. Between 1997 and 2017, the facility disposed of construction and demolition (C&D) waste on top of the closed MSW landfill in accordance with the Transition Plan dated 1994. The subject Oxford Unit 2 Landfill is a Subtitle-D MSW landfill which was permitted to operate in February 2013 and began receiving waste in May 2013. This report covers water quality monitoring conducted at the Oxford Unit 2 Landfill. A separate Water Quality Monitoring Report will be submitted for the Oxford Unit 1 Landfill. 1 https://harthick.shmepoint.com/sites/MmtuFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx Ad hart hickman SMARTER ENVIRONMENTAL SOLUTION5 1.2 Regulatory Status The Granville County Oxford Unit 2 Landfill is currently in a Detection Monitoring Program. Water quality monitoring is completed following the North Carolina Administrative Code Title 15A-Environmental Quality Chapter 13 Sub -Chapter B Solid Waste Management Rule (NCSWMR) § 1633. Statistical analyses of the laboratory data when required is prepared following the required compliance demonstration of the NCSWMR Rule .1632(g), (h), and (i). 1.3 Groundwater Monitoring Program The groundwater monitoring program at the Oxford Unit 2 Landfill consists of the following six monitoring wells: MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Monitoring well MW- 7 is located south and upgradient of the landfill and serves as a background location. Compliance monitoring well MW-8 serves to monitor groundwater conditions downgradient of the leachate tank area which is located south to southwest and upgradient of the landfill. Compliance monitoring wells MW-9, MW-10, MW-11, and NES-2S are located along the northern downgradient side of the landfill. Groundwater samples are collected semi-annually for analysis of North Carolina Solid Waste Management Rules Appendix I list of constituents (hereafter referred to as Appendix I constituents) plus 1,4-dioxane. The monitoring well locations and other site features are identified on Figure 2. A summary of well construction details is provided in Table 1. 1.4 Surface Water Monitoring Program The surface water monitoring program at the Oxford Unit 2 Landfill consists of collecting samples from two locations which are located upstream (SW-3) and downstream (SW-4) of the waste unit. The sampling points are situated along an unnamed tributary to Little Grassy Creek which runs along the eastern and northern side of the landfill. Little Grassy Creek is classified as a Class C (Aquatic Life and Secondary Recreation) stream. The locations of the surface water monitoring points are identified on Figure 2. Surface water samples are collected semi-annually and analyzed for Appendix I constituents plus 1,4-dioxane. 2 14 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx SMARTER ENVIRONMENTAL SOLUTIONS 2.0 Water Quality Monitoring Activities 2.1 Water Level Measurements On March 29 and 30, 2023, H&H measured depth -to -water and total depths in monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Depth -to -water measurements were collected from the top -of -casing utilizing a decontaminated electronic water level indicator. Depth -to -water measurements were made after the wells were opened for a sufficient period of time to allow water levels to equilibrate with atmospheric pressure. Water level measurements and calculated groundwater elevations are presented in Table 2. 2.2 Groundwater Sampling Methods On March 29 and 30, 2023, H&H collected groundwater samples from site monitoring wells MW- 7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Monitoring well MW-7 serves as the upgradient background well for the facility, and monitoring wells MW-8, MW-9, MW-10, MW-11, and NES- 2S serve as compliance monitoring wells. The groundwater samples were collected and handled in general accordance with the sampling protocols included in the WQMP and DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling document. Monitoring wells were purged utilizing a peristaltic pump under low flow (<200 milliliters/minute) conditions. Water levels were recorded during the purging process to ensure the pump rate did not cause significant drawdown of the water column, and samples were collected following stabilization of field parameters over three consecutive readings. Field measurements of pH, temperature, specific conductance, oxygen reduction potential (ORP), and dissolved oxygen (DO) were measured using a YSI Pro Plus water quality meter. Turbidity was measured using a Hach 2100Q turbidity meter. A summary of the final field parameters recorded prior to sample collection are presented in Table 3. Copies of groundwater sampling forms containing pertinent information recorded in the field during purging and sampling at each monitoring well are provided in Appendix A. 3 https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS The results of the field -measured water quality parameters indicate that the values measured in groundwater collected from site monitoring wells were within applicable stabilization criteria. Groundwater at the site is slightly acidic to slightly basic based on the pH values measured in the field (5.67 to 7.95 Standard Units). Specific conductance values in site groundwater ranged from 184.2 (MW-11) to 375.3 (MW-9) microsiemens per centimeter (µS/cm). Turbidity values ranged from <0.01 (NES-2S) to 9.63 (MW-10) nephelometric turbidity units (NTUs). 2.3 Surface Water Sampling Methods On March 30, 2023, H&H collected surface water samples from sample locations SW-3 and SW- 4 (Figure 2). Surface water samples were collected in general accordance with the WQMP as well as the DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling document with the exception of collecting the samples from upstream to downstream. Based on the minimal disturbance to the stream when collecting the samples, and reported similar analytical results in comparison to prior sampling events, the sample order for the current sampling event is not considered to affect the usability of the reported results. Field parameters were measured during sample collection and copies of surface water sampling forms are provided in Appendix A. A summary of field parameters recorded prior to sample collection is provided in Table 3. 2.4 Sample Equipment Management All reusable sampling equipment (e.g., water level indicator) was properly decontaminated between sampling locations with a non -phosphate soap and water wash, followed by multiple rinses with distilled water. New disposable nitrile or latex gloves were worn during all sampling activities. Disposable sampling equipment/material was discarded after each use. 2.5 Sample Handling and Laboratory Analyses Upon sample collection, samples for laboratory analysis were placed directly into dedicated laboratory -supplied sample bottles, labeled, and placed into ice -filled coolers. A chain -of -custody record was completed and included sample description, analyses required, matrix, sample 4 14 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx SMARTER ENVIRONMENTAL SOLUTIONS container information, and date and time of sample collection. The samples were transported on ice, under standard protocol, to Pace Analytical Services, LLC (Pace) a North Carolina -certified laboratory. The laboratory analytical reports and chain -of -custody records for the March 2023 sampling event are included in Appendix B. A summary of samples collected during the subject reporting period is provided below. The groundwater samples from monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S were analyzed for Appendix I constituents plus 1,4-dioxane. The surface water samples from SW-1 and SW- 2 were analyzed for Appendix I constituents plus 1,4-dioxane. s https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 3.0 Water Quality Monitoring Results Groundwater and surface water monitoring activities were conducted at the site on March 29 and 30, 2023. Groundwater and surface water samples were collected and analyzed in accordance with the DEQ approved WQMP. The monitoring results are discussed in the following sections. 3.1 Groundwater Flow and Hydraulic Gradient A summary of monitoring well gauging and water level elevation data is provided in Table 2. Historical groundwater elevation data is provided in Appendix C. Groundwater flow direction, average hydraulic gradient, and average interstitial flow velocity were derived from water -level measurements recorded during the March 2023 sampling event. A potentiometric map generated from the March 2023 gauging event is provided as Figure 3. The March 2023 water levels are within the range of historical seasonal fluctuations observed at the site. Consistent with historical trends, the overall direction of shallow groundwater flow at the site is generally north to northeast towards an unnamed tributary to Little Grassy Creek. The hydraulic gradient in the vicinity of each well was derived by dividing the elevation difference between water table elevations measured at the monitoring wells and proximal potentiometric contour lines, by the perpendicular horizontal distance between the wells and potentiometric contours (Figure 3 and Table 4). The potentiometric contours indicate an average hydraulic gradient of approximately 0.012 ft/ft. Results of in -situ slug testing reported by others (LaBella Associates, 2021) indicate an average hydraulic conductivity value in the bedrock aquifer of approximately 4.43 feet/day. Using the horizontal hydraulic gradient measurements, the individual estimate of hydraulic conductivity, and an assumed effective porosity of 0.15 (LaBella Associates, 2021), the range of average interstitial groundwater flow velocities for the shallow bedrock aquifer was calculated using the following equation: VX = (K/ne) x dh/dl. 0 https://harthick.sharepoint.con/site"asterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Where: VX = average interstitial groundwater flow velocity; K = hydraulic conductivity; ne = effective porosity; and, dh/d1= horizontal hydraulic gradient Average linear flow velocities are estimated to range between approximately 64.48 to 403.93 feet/year (approximately 0.177 to 1.107 feet/day) with a geometric mean of approximately 127.8 feet/year (0.35 feet/day). These values are consistent with prior monitoring events. Table 4 summarizes the data used to calculate the average interstitial groundwater flow velocity in the vicinity of each monitoring well. 3.2 Groundwater Analytical Results Semi-annual groundwater sampling consisted of collecting samples from six site monitoring wells. A summary of groundwater constituent detections from the March 2023 sampling event is provided in Table 5. Historical analytical results are presented in Appendix D. A summary of the groundwater results is provided below. VOCs The analytical results indicate that no VOCs were detected at concentrations above laboratory method detection limits (MDLs) in groundwater samples collected during the March 2023 sampling event. Metals The analytical results indicate barium, cobalt, copper, chromium, nickel, and zinc were detected above the laboratory MDL in one or more wells during the March 2023 sampling event. Cobalt was detected in monitoring well NES-2S (1.28 J) at an estimated concentration above its North Carolina 2L Groundwater Standard (2L Standard; 1.0 µg/L), and the concentration is consistent with historical detections at this location. No other metal constituents were detected above 2L 7 14 hart hickman https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx SMARTER ENVIRONMENTAL SOLUTIONS Standards during the March 2023 sampling event, and the observed detections are generally consistent with historical data at the site. 3.3 Surface Water Analytical Results Semi-annual surface water sampling consisted of collecting samples from two locations, one upstream (SW-3) and one downstream (SW-4) location. A summary of surface water constituent detections from the March 2023 sampling event is provided in Table 5. Historical analytical results are presented in Appendix E. A summary of the surface water results is provided below. VOCs The analytical results indicate methylene chloride was detected in SW-3 (4.2 J µg/L) at an estimated concentration above the laboratory MDL. Methylene chloride was detected in the laboratory method blank sample at a similar concentration (3.8 J µg/L), and the detection in SW- 3 was flagged as a common laboratory contaminant. Therefore, the detection in SW-3 may be attributed to laboratory -introduced contamination and not representative of site conditions. No other VOCs were detected above MDLs during the March 2023 sampling event. Metals The analytical results indicate arsenic, barium, chromium, copper, nickel, vanadium, and zinc were detected above the laboratory MDL in one or both of the surface water samples collected during the March 2023 sampling event. The detected concentrations of arsenic, chromium, nickel, and zinc do not exceed the 2B Standards and are generally consistent with historical data. Copper (4.07 J µg/L) was detected at a concentration above its 213 Standard (2.91 µg/L) in the sample collected from upstream location SW-3, and concentrations are similar to historical detections at this location. Barium does not have a 2B Standard and the detected concentrations were compared to its North Carolina In -Stream Target Value for Surface Water (ISTV), and there were no exceedances. There are no screening criteria established for comparison of vanadium results. No other constituents were detected above MDLs during the March 2023 sampling event. https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 3.4 Quality Assurance/Quality Control Results Quality assurance procedures and protocols for sampling activities were conducted in general accordance with the DEQ approved WQMP. Quality assurance samples included the collection of trip blanks and a field blank sample. Samples were received by the lab in good condition and met holding times and preservation requirements. Based upon a review of the data packages, no significant quality assurance/quality control (QA/QC) issues were identified for the laboratory analyses. In summary, the QA/QC results indicate that the data collected during the semi-annual monitoring event is suitable for its intended purpose. Trip Blanks Laboratory -filled trip blanks accompanied the sampling team during sampling and the transport of VOC samples to the laboratory. The trip blank samples serve as a QC check on potential external contamination and/or cross -contamination between VOC water samples during shipping and storage. The trip blank sample was analyzed for Appendix I VOCs and 1,4-dioxane. The results indicate no constituents were detected above laboratory MDLs. Field Blanks A field blank sample was collected in the field by exposing laboratory -supplied deionized water to the sampling environment. The field blank is used to evaluate the potential for contamination of a sample by site contaminants from a source not associated with the samples collected. The field blank sample was analyzed for Appendix I constituents plus 1,4-dioxane. The results indicate no constituents were detected above laboratory MDLs. 0 https://harthick.sharepoint.com/sites/MasterFiles-I/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS 4.0 Conclusions The analytical results for groundwater and surface water samples collected during the March 2023 event indicate cobalt in groundwater at compliance monitoring well NES-2S and copper in surface water at the upstream location SW-3 were the only constituents detected above their applicable groundwater and surface water standards. The detected concentrations of cobalt and copper were similar to historical concentrations detected at the site. Cobalt and copper will continue to be monitored for evidence of increasing or sustained concentrations in exceedance of groundwater and/or surface water standards. Based on the water quality monitoring results, the Granville County Oxford Unit 2 Landfill will remain in the Detection Monitoring Program. The next semi- annual sampling event will be conducted in September 2023. 10 https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/GMI.005 Granville County Oxford Unit 2_WQMR_March 2023.docx 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Table 1 Summary of Well Construction Details Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Ground TOC Top of Top Bottom Bottom Auger Total Depth Total Depth Screened Well ID Date Installed Northing Easting Elevation Elevation Screen Screen Screen Screen Refusal Comments (ft BGS) (ft BTOC) Lithology (ft AMSL) (ft AMSL) (ft BGS) (Ft BTOC) (Ft BGS) (Ft BTOC) (ft BGS) Background Well Units MW-7 7/28/2008 953292.1160 2112043.44800 531.24 534.24 34.50 37.50 19.50 22.50 34.50 37.50 34.50 Saprolite 1 & 2 MW-8 7/18/2012 953360.2000 2111527.6910 500.57 503.31 25.00 20.00 10.00 12.74 20.00 22.74 1.00 Bedrock Unit 2 Compliance MW-9 10/6/2008 954799.7410 2112842.3890 485.05 487.51 40.00 43.00 20.00 22.46 40.00 42.46 1.50 Bedrock Unit 2 Compliance MW-10 10/2/2008 955136.0000 2112571.1750 481.81 484.92 30.00 32.90 15.00 18.11 30.00 33.11 6.00 Bedrock Unit 2 Compliance MW-11 10/5/2008 954795.8510 2111957.0410 476.43 478.72 20.00 22.90 5.00 7.30 20.00 22.30 6.00 Bedrock Unit 2 Compliance MW-12 8/1/2008 954077.4350 2112567.4920 519.29 521.30 50.00 52.30 40.00 42.00 50.00 52.00 31.00 Bedrock Not Sampled Unit 2 Compliance & NES-2S 5/1/2004 955091.2902 2111945.3411 474.53 477.20 21.50 24.17 11.00 13.67 21.00 23.67 9.00 Saprolite 1 Unit 1 Performance Notes: Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. ft = feet; AMSL = above mean sea level; AGS = above ground surface TOC = top of casing; BTOC = below top of casing; * = estimated value https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 1 (Page 1 of 1) Hart & Hickman, PC Table 2 Summary of Groundwater Elevations Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Well ID Total Depth (ft BTOC) TOC Elevation (ft AMSL) March 29-30, 2023 Depth To Groundwater (ft BTOC) Groundwater Elevation (ft AMSL) MW-7 37.50 534.24 23.53 510.71 MW-8 22.74 503.31 3.32 499.99 MW-9 42.46 487.51 8.20 479.31 MW-10 33.11 484.92 8.23 476.69 MW-11 22.30 478.72 4.74 473.98 NES-2S 23.67 477.20 4.82 472.38 Notes: Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. TOC = top of casing; ft BTOC = feet below top of casing ft AMSL= feet above mean sea level Table 2 (Page 1 of 11) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Hart & Hickman, PC Table 3 Summary of Field Parameters Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Sample ID Sample Date Field Parameter Results Units Groundwater MW-7 3/29/2023 Conductivity 362.0 PS/CM Dissolved Oxygen 3.21 mg/I Oxidation Reduction Potential 91.8 mV pH 5.95 S.U. Temperature 15.83 °C Turbidity 2.19 NTU MW-8 3/30/2023 Conductivity 249.1 PS/CM Dissolved Oxygen 0.26 mg/I Oxidation Reduction Potential 93.6 mV pH 7.95 S.U. Temperature 14.0 oC Turbidity 0.59 NTU MW-9 3/30/2023 Conductivity 375.3 PS/CM Dissolved Oxygen 2.34 mg/I Oxidation Reduction Potential 117.9 mV pH 7.11 S.U. Temperature 18.9 oC Turbidity 1.81 NTU MW-10 3/30/2023 Conductivity 256.6 PS/CM Dissolved Oxygen 0.46 mg/I Oxidation Reduction Potential 103.6 mV pH 6.58 S.U. Temperature 15.6 oC Turbidity 9.63 NTU MW-11 3/30/2023 Conductivity 184.2 PS/CM Dissolved Oxygen 0.28 mg/I Oxidation Reduction Potential 112.9 mV pH 5.67 S.U. Temperature 15.3 °C Turbidity 7.97 NTU NES-2S 3/29/2023 Conductivity 279.8 PS/CM Dissolved Oxygen 0.34 mg/I Oxidation Reduction Potential 99.1 mV pH 6.36 S.U. Temperature 15.1 oC Turbidity <0.01 NTU Table 3 (Page 1 of 2) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 3 Summary of Field Parameters Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Sample ID Sample Date Field Parameter Results Units Surface Water SW-3 3/30/2023 Conductivity 50 PS/cm Dissolved Oxygen NA mg/I Oxidation Reduction Potential 112.5 mV pH 6.27 S.U. Temperature 15.1 °C Turbidity 186.6 NTU SW-4 3/30/2023 Conductivity 81 PS/cm Dissolved Oxygen NA mg/I Oxidation Reduction Potential 23.8 mV pH 7.35 S.U. Temperature 14.73 oC Turbidity 57.98 NTU Notes: S.U. = standard units; °C = degrees Celsius; pS/cm = microsiemens per centimeter NTU = nephelometric turbidity unit; mg/L = milligrams per liter; mV = millivolts ORP = oxidation reduction potential; NA = not analyzed Table 3 (Page 2 of 2) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Tables 1-5.xlsx Table 4 Summary of Groundwater Flow Velocity Granville County Oxford Unit 2 Landfill Oxford, North Carolina H&H Job No. GMI-005 Well ID Hydraulic Conductivity ��� (ft/day) Groundwater Elevation (ft AMSL) Reference Elevation (ft AMSL) Delta Elevation (ft) Map Length (ft) Hydraulic Gradient (ft/ft) Effective Porosity(') Groundwater Flow Velocity (ft/day) Groundwater Flow Velocity (ft/year) MW-7 4.43 510.71 505.00 5.71 152.38 0.037 0.15 1.107 403.93 MW-8 4.43 499.99 495.00 4.99 350.59 0.0142 0.15 0.420 153.43 MW-9 4.43 479.31 480.00 0.69 110.42 0.006 0.15 0.185 67.36 MW-10 4.43 476.69 475.00 1.69 111.95 0.015 0.15 0.446 162.73 MW-11 4.43 473.98 475.00 1.02 110.55 0.009 0.15 0.272 99.46 NES-2S 4.43 472.38 475.00 2.62 438.04 0.006 0.15 0.177 64.48 Minimum -- -- -- -- 0.006 -- 0.177 64.48 Maximum -- -- -- -- 0.037 -- 1.107 403.93 Geometric Mean -- -- -- -- 0.012 -- 0.350 127.80 Notes: 1) Hydraulic conductivity and porosity values from Labella Associates Water Quality Monitoring Report - February 2021 Event. Hydraulic conductivity is based on the geometric mean of bedrock wells at the facility in 2019 and the effective porosity value for fractured bedrock was estimated at 15%. ft = feet; ft/day = feet per day; ft/year = feet per year AMSL = feet above mean sea level; -- = not applicable Vx = (K/ne) x dh/dl Vx = groundwater flow velocity K = hydraulic conductivity ne = effective porosity dh/dl = hydraulic gradient Table 4 (Page 1 of 1) Hart & Hickman, PC Table 5 Summary of Groundwater and Surface Water Constituent Detections Granville County Oxford Unit 2 Landfill Butner, North Carolina H&H Job No. GMI-005 Well ID Sample Date Parameter Result (N9/L) Standard (Ng/L) Source Groundwater MW-7 03/29/23 Barium 3.92 J 700 NC 2L MW-8 03/30/23 Barium 43.7 700 NC 2L Copper 22.3 1,000 NC 2L Nickel 3.28 J 100 NC 2L MW-9 03/30/23 Barium 81.4 700 NC 2L Nickel 1.71 J 100 NC 2L MW-10 03/30/23 Barium 54.0 700 NC 2L Chromium 2.01 J 10 NC 2L Zinc 9.33 J 1,000 NC 2L MW-11 03/30/23 Barium 31.8 700 NC 2L Nickel 3.78 J 100 NC 2L Zinc 9.03 J 1,000 NC 2L NES-2S 03/29/23 Barium 38.3 700 NC 2L Cobalt 1.28 J 1 NC 2L Surface Water SW-3 03/30/23 Barium 32.4 21,000 ISTV (3) Chromium 2.91 J 16 NC 2B Copper 4.07 J 2.91 NC 2B I' Methylene Chloride 4.2 J 11,000 ISTV (3) Nickel 3.36 J 118.65 NC 2B I' Vanadium 12.9 J NE NE Zinc 8.27 J 29.63 NC 2B I' Hardness 16,400 NE NE SW-4 03/30/23 Arsenic 9.99 J 340 NC 2B Barium 27.9 21,000 ISTV (3) Chromium 1.68 J 16 NC 2B Nickel 3.00 J 118.65 NC 2B I'I Zinc 7.11 J 29.63 NC 2B I'I Hardness 21,200 NE NE Notes: NC 2L Standards are the Title 15A NCAC 02L .0202 Groundwater Standards dated April 1, 2022. 15A NCAC 2B Water Quality Standards (213 Standards) for Surface Water (Class C) dated July 26, 2021. Bold concentrations exceed the NC 2L Standard for groundwater or NC 2B Standard for surface water. 1. 2B Standards for hardness -dependent metals are calculated using a mean value of 19.736 mg/L obtained from averaging hardness results reported for surface water locations SW-3 and SW-4 from September 2019 to March 2023. 2. No 2B Standard established, value shown is EPA Nationally Recommended Water Quality Criteria (NRWQC) for Aquatic Life & Human Health. 3. No 2B Standard established, value shown is North Carolina In -Stream Target Value for Surface Water (ISTV). J = Estimated value above laboratory method detection limit and below laboratory method quantitation limit; ND = Non -Detect; NE = Not Established; -- = Not Applicable; Table 5 (Page 1 of 1) Hart & Hickman, PC APPROXIMATE LIMITS OF WASTE UNIT 1 l 4 "Y j 4 ^^^^ERTY BOUNDARY APPROXIMATE SrERr (4_ LIMITS OF WASTE UNIT 2 i USGS The National Map: National Boundaries Dataset, 3DEP Elevation Program, Geographic Names Information System, National Hydrography Dataset, National Land Cover Database, National Structures Dataset, and National Transportation Dataset; USGS Global Ecosystems; U.S. Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S. Department of State Humanitarian Information Unit; and NOAA National Centers for Environmental Information, U.S. Coastal Relief Model. Data refreshed August, 2021. TITLE o 2,000 4,000 SITE LOCATION MAP NPROJECT SCALE IN FEET OXFORD LANDFILL GRANVILLE COUNTY U.S.G.S. QUADRANGLE MAP OXFORD, NORTH CAROLINA 2923 South Tryon Street - Suite 100 BEREA, NORTH CAROLINA2019 hart hickman Charlotte, North Carolina28203 704-586-0007 (p) 704-586-0373 (t) OXFORD, NORTH CAROLINA 2019 SMARTER E NVrFro 7jMENT LL soLUVONs License # C-1269 / # C-245 Geology 3 QUADRANGLE DATE: 11-21-22 REVISION NO: 0 7.5 MINUTE SERIES (TOPOGRAPHIC) JOB NO: GMI-004 FIGURE NO: 1 T. 4661, GO 150' 7n 490 506 7 'o _ _ •r �/ // y � I I , _ • ��-•��-,� �90 �`.,.-� /��'�' J r /// /ram/1 // 1 r /- � ,� do 46 ib 16 ! ram... -� � I � 1 ��� •. I :�26 I \ ,� 1 \ � 1 j - \ '�.... Ig r li l I it \ ter/ � / // � r \ \ �'\ � ��✓ (/� � I 1 v\ ^\ 1 530 Appendix A Groundwater and Surface Water Sampling Records 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS hart hickman Job No:y /-l1-- � ccp� -�- ' C�� SMARTER ENVIRONMENTAL SOLUTIONS S. Cond. +/- 5% ORP +/- 20 mV ,{ Turb. +/- 10% (<10 NTLls for metals) Well ID: LOW -FLOW GROUNDWATER Water Level: slight or stable r SAMPLING RECORD drawdown during purging Well Location: (�7LTc�r l NC Facility Name: Date: 1 A'Q ,3 Top of Casing Elevation (ft msl): Casing Material: Pyc Volume of Water Per Well Volume: gallons 1-2 Total Well Depth (ftTOC): 33- s Depth to Water (ftTOC): Well Diameter: Sampling Personnel: L C. r��w ..H _ Screen Interval (ftTOC): / 1 • S' Type of Pump: e2�,S `�/ Tubing Material: �� _ Pump/Tubing set at: 3 a ft Weather Conditions: G r r l I U� NOTES: kn, H,1 3 7' S/ r- s. Kvd. 1,6z5- -/Gs a Stabilization Criteria Primary: Secondary: pH +1- 0.1 unit DO +1- 0.2 mg/L GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate (malt] L.1(AS/cm Lau-1 (mV) MUD I'1 ply 'Z'3.(v; 7 To' 7b q7. �. [. a. 1LlS-Y 23,E -z250 3. Z-cr s r g C, I , /Ifsq 25 C,7 54e�— rSr 5. IT Y51- Y7 I S"'o' 2 3 ('3 'gib /TLc (i 3. fc 31 3 r /5".<33 57 1:F '7 2. 2 I t Other Sample Parameters: du Sampled at: ��V� Parameters taken with: L S-S Hc—e,�, (W� Sample Delivered to: ��� �5 v� 1`0 _. by at Field Filtration: O Yes G No If yes, which sample parameters were field filtered: ample Parameter Containers (Types, Number of Containers, Preservatives): ') o^t t i -?X- �16n I G/t 1 - 1 rox. 123�1^ L 1144 G 4 C 4'1kr.1". r 5� "S:\BBB Master Templates\Fors - 2022 Forms\Low Flow Groundwater Sampling Form.pdf' L a- ��yy;; ��75� �'� J (75W n'L J Stabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017. Last Updated. 2/1412022 \"' C /S,, Z Vsp; d,m- �Y d• r- 1 hart _ hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Job No: GM 11. D0 S Well ID: 1_` —o Well Location: ck 6 V-j / N G Facility Name: () 1 r,, L_Cmj ,l U1nxt Date: u�ci j Top of Casing Elevation (ft msl):_ 503 .3l Casing Material: P V Volume of Water Per Well Volume: Total Well Depth (ftTOC): AA -13 . N Depth to Water MTOCY . � �. Well Diameter: A Sampling Personnel: h - w n Ayi- Screen Interval (ftTOC): Type of Pump: Pe. Y") 11) Tubing Material: s Ur1O Weather Conditions: �y , ,or NOTES:_ gallons Pump/Tubing set at: _ ft GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate lrr— ll (°C] S/cm) (SU) (MV) (NTU) f'l- 40 3-34 :nL :A 61,t r 51 , r� l Ic73,l Other Sample Parameters: Sampled at: Parameters taken with: �I S� ✓� jD 1 ut5 , IIR�'4� c\-e e(li jAT "- Sample Delivered to: i by L my1 at Field Filtration: O Yes @ No If yes, which sample parameters were field filtered: ll __ Sample Parameter Containers (Types, Number of Containers, Preservatives): V0 I �` -[-�� i l i, UK "S:\BBB Master Templates\Fors - 2022 Forms\Low Flow Groundwater Sampling Form.pdf' Last Updated: 2/14/2022 Stabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017. hart = hickman L . SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Facility Name: Job No: VMk, 0u Well ID: MW —9 Well Location: 0 _[ N L Date: 313 0 I A Top of Casing Elevation (ft msl): tiY�-7, 57 Casing Material: %. Volume of Water Per Well Volume: O Total Well Depth (ftTOC): L �, r G f'i Depth to Water (ftTOC): Well Diameter: L Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Turb. +/- 10% (<10 NTUs for metals) Water Level: slight or stable drawdown during purging aft Sampling Personnel: _ Ulf ri tA` A � Screen Interval (ftTOC). Z_ O - L+(D Type of Pump: J Tubing Material: LD-P r-, _ Pump/Tubing set at: 30 ft Weather Conditions: ., ' !'� W V� C- NOTES: gallons GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate (mall] am(AS/cm) Lul Lmvj NTU � - 10 1 7U 7_ �1 Other Sample Param Sampled at: I q - 33 Parameters taken with: �S Vti-j �lrl�, hM)o ta��Y Sample Delivered to: _ �(A U by at Field Filtration: O Yes Q No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives):y J "S:\BBB Master Templateffonns - 2022 Forms\Low Flow Groundwater Sampling Form pdr' Stabilization criteria guidelines from the EPA SESD Operating Last Updated: 2/1412022 Procedure for Groundwater Sampling, dated April 26. 2017. hart - hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Job No: b m ( • WIG Well ID: (0Ly to Well Location: D d VC, , Facility Name: Q x, C—D rA WU a Date: f , G j d 3 Top of Casing Elevation (ft msl): LA'6LLG'a Casing Material', �' C� Volume of water Per Well Volume: gallons Total Well Depth (ftTOC):a 3 k Depth to Water (ftTOC): Sampling Personnel:._ ��}} A , �N' i Al A � , Screen Intery Type of Pump: Pan J Tubing Material: p Weather Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Turb. +/- 10% (<10 NTUs for metals) Water Level: slight or stable drawdown during purging NOTES: Well Diameter: a" A (ftTOC): I - Pump/Tubing set at: /A' ft GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate m 11 u(PS/cm) aw �mV1 NTU (P,. 1 0,0 C) z7� ,l' I1 s S 13C� , Q, ..� � s 2 .,3 . ''� c I 1 . ,�Ic Other Sample Parameters:. Sampled at: I a' S�) Parameters taken with: Ct 9ry 0-i.11C L 'r-1A0,1?d 1YrJVkI- Sample Delivered to: f t (0 by W N ��% at Field Filtration: Q Yes G) No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): 'B:\BBB Master Templates\Fonns - 2022 Forms\Low Flow Groundwater Sampling Form pdf' Stabilization criteria guidelines from the EPA SESD Operating Last Updated: 2/14/2022 Procedure for Groundwater Sampling, dated April 26, 2017. hart = hickman SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Stabilization Criteria Primary: Secondary: pH +/- 0.1 unit DO +/- 0.2 mg/L S. Cond. +/- 5% ORP +/- 20 mV Turb. +/- 10% (<10 NTUs for metals) Water Level: slight or stable drawdown during purging Facility Names C s f--[) y-A L 7 Uir�t {- `� Job No: L. O((3(2 _ Well ID: LN - l l Well Location: , o X(:r) t A, N G Date: 3 I-3D l a -3 Top of Casing Elevation (ft msl): I-E7Y5 Casing Material: 2uG Volume of Water Per Well Volume: gallons Total Well Depth (ftTOC): ' Depth to Water (ftTOC): t'[_•j 4 Well Diameter: ' Sampling Personnel: Screen Interval (UOC): 5 Q, O Type of Pump: P-Z Tubing Material. LD P l=- Pump/Tubing set at: ^' I ft Weather Conditions: ` o, r NOTES: GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO Temp. S. Cond. pH ORP Turbidity Time Level Pumped Rate m 11 u Slcm LSi_uj L] LULU-1 ?r: 00''' -4� J c U J? l I +_ a `7 Other Sample Parameters: -f-r— -- Sampled at: 11- 4 O _. Parameters taken with: 'i S tPku5 T.A C \ d i rvu, P- r Sample Delivered to: P(kU. by CC CA 6 eY at Field Filtration: O Yes Q No If yes, which sample parameters were field filtered: Sample Parameter Containers (Types, Number of Containers, Preservatives): (W f at'S I V d LS I I "J sSC "S:\BBB Master Templates\Fors - 2022 Forms\Low Flow Groundwater Sampling Form pdf' Stabilization criteria guidelines from the EPA SESD Operating Last Updated: 2/14/2022 Procedure for Groundwater Sampling, dated April 26, 2017- hart t� hickman W SMARTER ENVIRONMENTAL SOLUTIONS LOW -FLOW GROUNDWATER SAMPLING RECORD Job No:`S- Well ID:� —2 Well Location: A�) C Facility Name: 0) xTQs l L t 1,-,.1- 1 'L Date: 3 Top of Casing Elevation (ft msl):- Casing Material: . f VC Volume of Water Per Well Volume: gallons Total Well Depth MTOC): `L I -s Depth to Water (ftTOC): G/• gZ Well Diameter: 2 Sampling Personnel: C' Cane Screen Interval (ftTOC): //. !T- - 2 r Type of Pump: r ; j k:(- Tubing Material' LDPE Pump/Tubing set at: �t ft Weather Conditions: � ,xm ', Q,), )Lt4 `" 1 U NOTES: GROUNDWATER SAMPLING PARAMETERS Water Volume Pumping DO 'temp. S. Cond. pH ORP Turbidity Time {rLevel Pumped Rate .e• n fs"U {mall] �[ Slcm { S' i� p�.+..S t �i � 'yrJCi �Z_ �7� LUG �� , v L � 1 Liz/. r}Z 1 Qr'7 • NTU 4 c). '<C \�, c •�.S U L G' - � .i i�'l.'L 4 _I s1 _ ��5o ISa G•3S �'S. L _ �_�fr� -2 ��_ G�' ❑ cc:._c i- ') I LI C� J(J C� • J Pf Other Sample Parameters: Sampled at: t,°-t—S-L Parameters taken with:_ Sample Delivered to: D by at Field Filtration: o Yes No If yes, which sample parameters were field filtered: Semple Parameter Containers (Types, Number of Containers, Preservatives): J k Ut;cv r ZSbnL�k► ci.tiaifi,n eritAria nuidslines from the EPA SESD Operating 'S:\BBB Master Templates\Fonns - 2022 Forms\Low Flow Groundwater Samp ing t-orm.por- Procedure for Groundwater Sampling, dated April 26, 2017. Last Updated: 2114/2022 Surface Water Sampling Form hart = hickman GENERAL INFORMATION SMARTER ENVIRONMENTAL SOLUTIONS 1 Job No.: - liVt� Location No.:. frCJ W' �3 Date: { Site Name: Location: �� C�Inf�n 1.�- �j �� Sample Type (,j�"j,) Grab (❑) Composite (❑) Other Sampling Equipment ([:]) Dedicated (❑) Decontaminated (❑) Bailer (❑) Pump Material (❑) PVC (❑) Stainless Steel (❑) Teflon (❑) Other Decontamination Method: LOCATION INFORMATION Coordinates Sample Location Dimentions Width Depth to Stream Bed PURGING INFORMATION Time pH (SU) Temp. C S. Cond. umhos/cm Redox Turbidity TU Weather Conditions Sample Condition: (❑) Clear (©) Cloudy (❑) Other: Field Filtration: (❑) Yes (Ej) No 3 x W ml � oA NtL- q�,b0) P3 uN N) � Gm Containers (T ?. 1 Odor: f1LVN-e_ _ Sample Collector: /Vw Date Time Time: r File: SW Sampling Log, SW Form Date: 2/20/2018 hart hickman Surface Water Sampling Form _��� SMARTER ENVIRONMENTAL SOLLMONS GENERAL INFORMATI N. , Job No.: L') 1M/� CS 6 S Location No.: C Date: 1-3 6 1-n Site Name:m VC ��11�� Location: 0 ov N L" Sample Type Q7) Grab (❑) Composite (❑) Other Sampling Equipment (❑) Dedicated (❑) Decontaminated (❑) Bailer (❑) Pump � Material (❑) PVC (❑) Stainless Steel (❑) Teflon (❑) Other N N Decontamination Method: - - Coordinates: Sample Location Dimentions Wirth LOCATION INFORMATION Depth to Stream Bed PURGING INFORMATION Time pH (SU) Temp. (°C) S. Cond. (umhos/cm) Redox Turbidity (NTU) Weather Conditions Sample Condition: (❑) Clear (19) Cloudy Field Filtration: (❑) Yes (M) No Containers (Types, Numbprs, P-.eservptives):( Comments: Sample Collector: File: SW Sampling Log, SW Form Date: 2/20/2018 Q -- (❑) Other: Date: Time: �� v Appendix B Laboratory Analytical Reports 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 12, 2023 Jeffrey 011ison Hart & Hickman 3921 Sunset Ridge Rd. Ste. 301 Raleigh, NC 27607 RE: Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Dear Jeffrey 011ison: Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor M Cannon taylor.cannon@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 49 laneAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Lab ID Sample ID Matrix Date Collected Date Received 92659945001 MW-8 Water 03/30/2310:05 03/31/2310:30 92659945002 MW-9 Water 03/30/2314:33 03/31/2310:30 92659945003 MW-10 Water 03/30/2312:58 03/31/2310:30 92659945004 MW-11 Water 03/30/2311:40 03/31/2310:30 92659945006 TRIP BLANK UNIT 2 Water 03/30/23 00:00 03/31/23 10:30 92659945007 NES-2S Water 03/29/2312:32 03/31/2310:30 92659945008 MW-7 Water 03/29/2315:09 03/31/2310:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659945 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92659945001 MW-8 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945002 MW-9 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945003 MW-10 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945004 MW-11 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945006 TRIP BLANK UNIT 2 EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945007 NES-2S EPA 601OD ABL 14 PAN EPA 6020E SJM 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C 92659945008 MW-7 EPA 601OD ABL 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-8 Lab ID: 92659945001 Collected: 03/30/23 10:05 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 11:42 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 11:42 7440-38-2 Barium 43.7 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 11:42 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 11:42 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 11:42 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 11:42 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 11:42 7440-48-4 Copper 22.3 ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 11:42 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 11:42 7439-92-1 Nickel 3.28J ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 11:42 7440-02-0 B,J Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 11:42 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 11:42 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 11:42 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 11:42 7440-66-6 Metals (ICPMS) 6020B Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 04/12/2023 08:14 AM Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 15:11 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 04/06/23 04:39 67-64-1 ND ug/L 10.0 1.8 1 04/06/23 04:39 107-13-1 ND ug/L 1.0 0.34 1 04/06/23 04:39 71-43-2 ND ug/L 1.0 0.47 1 04/06/23 04:39 74-97-5 ND ug/L 1.0 0.31 1 04/06/23 04:39 75-27-4 ND ug/L 1.0 0.34 1 04/06/23 04:39 75-25-2 ND ug/L 2.0 1.7 1 04/06/23 04:39 74-83-9 v2 ND ug/L 5.0 4.0 1 04/06/23 04:39 78-93-3 ND ug/L 2.0 0.36 1 04/06/23 04:39 75-15-0 ND ug/L 1.0 0.33 1 04/06/23 04:39 56-23-5 ND ug/L 1.0 0.28 1 04/06/23 04:39 108-90-7 ND ug/L 1.0 0.65 1 04/06/23 04:39 75-00-3 ND ug/L 1.0 0.43 1 04/06/23 04:39 67-66-3 ND ug/L 1.0 0.54 1 04/06/23 04:39 74-87-3 ND ug/L 2.0 0.34 1 04/06/23 04:39 96-12-8 ND ug/L 1.0 0.36 1 04/06/23 04:39 124-48-1 ND ug/L 1.0 0.27 1 04/06/23 04:39 106-93-4 ND ug/L 1.0 0.39 1 04/06/23 04:39 74-95-3 ND ug/L 1.0 0.34 1 04/06/23 04:39 95-50-1 ND ug/L 1.0 0.33 1 04/06/23 04:39 106-46-7 ND ug/L 1.0 0.56 1 04/06/23 04:39 110-57-6 ND ug/L 1.0 0.37 1 04/06/23 04:39 75-34-3 ND ug/L 1.0 0.32 1 04/06/23 04:39 107-06-2 ND ug/L 1.0 0.35 1 04/06/23 04:39 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-8 Lab ID: 92659945001 Collected: 03/30/23 10:05 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 99 % 70-130 104 % 70-130 104 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 106 % 67-130 94 % 70-130 0.38 1 04/06/23 04:39 156-59-2 0.40 1 04/06/23 04:39 156-60-5 0.36 1 04/06/23 04:39 78-87-5 0.36 1 04/06/23 04:39 10061-01-5 0.36 1 04/06/23 04:39 10061-02-6 0.30 1 04/06/23 04:39 100-41-4 0.48 1 04/06/23 04:39 591-78-6 9.7 1 04/06/23 04:39 74-88-4 v2 2.0 1 04/06/23 04:39 75-09-2 L1,v1 2.7 1 04/06/23 04:39 108-10-1 0.29 1 04/06/23 04:39 100-42-5 0.31 1 04/06/23 04:39 630-20-6 0.22 1 04/06/23 04:39 79-34-5 0.29 1 04/06/23 04:39 127-18-4 0.24 1 04/06/23 04:39 108-88-3 0.33 1 04/06/23 04:39 71-55-6 0.32 1 04/06/23 04:39 79-00-5 0.38 1 04/06/23 04:39 79-01-6 0.30 1 04/06/23 04:39 75-69-4 0.26 1 04/06/23 04:39 96-18-4 1.3 1 04/06/23 04:39 108-05-4 0.39 1 04/06/23 04:39 75-01-4 0.34 1 04/06/23 04:39 1330-20-7 1 04/06/23 04:39 460-00-4 1 04/06/23 04:39 17060-07-0 1 04/06/23 04:39 2037-26-5 0.86 1 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/07/23 01:24 123-91-1 H 1, H5 04/07/23 01:24 17060-07-0 04/07/23 01:24 2037-26-5 Page 6 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-9 Lab ID: 92659945002 Collected: 03/30/23 14:33 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 12:12 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 12:12 7440-38-2 Barium 81.4 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 12:12 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 12:12 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 12:12 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 12:12 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 12:12 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 12:12 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 12:12 7439-92-1 Nickel 1.71J ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 12:12 7440-02-0 B,J Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 12:12 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 12:12 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 12:12 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 12:12 7440-66-6 Metals (ICPMS) 6020B Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 04/12/2023 08:14 AM Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 15:14 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 04/06/23 04:58 67-64-1 ND ug/L 10.0 1.8 1 04/06/23 04:58 107-13-1 ND ug/L 1.0 0.34 1 04/06/23 04:58 71-43-2 ND ug/L 1.0 0.47 1 04/06/23 04:58 74-97-5 ND ug/L 1.0 0.31 1 04/06/23 04:58 75-27-4 ND ug/L 1.0 0.34 1 04/06/23 04:58 75-25-2 ND ug/L 2.0 1.7 1 04/06/23 04:58 74-83-9 v2 ND ug/L 5.0 4.0 1 04/06/23 04:58 78-93-3 ND ug/L 2.0 0.36 1 04/06/23 04:58 75-15-0 ND ug/L 1.0 0.33 1 04/06/23 04:58 56-23-5 ND ug/L 1.0 0.28 1 04/06/23 04:58 108-90-7 ND ug/L 1.0 0.65 1 04/06/23 04:58 75-00-3 ND ug/L 1.0 0.43 1 04/06/23 04:58 67-66-3 ND ug/L 1.0 0.54 1 04/06/23 04:58 74-87-3 ND ug/L 2.0 0.34 1 04/06/23 04:58 96-12-8 ND ug/L 1.0 0.36 1 04/06/23 04:58 124-48-1 ND ug/L 1.0 0.27 1 04/06/23 04:58 106-93-4 ND ug/L 1.0 0.39 1 04/06/23 04:58 74-95-3 ND ug/L 1.0 0.34 1 04/06/23 04:58 95-50-1 ND ug/L 1.0 0.33 1 04/06/23 04:58 106-46-7 ND ug/L 1.0 0.56 1 04/06/23 04:58 110-57-6 ND ug/L 1.0 0.37 1 04/06/23 04:58 75-34-3 ND ug/L 1.0 0.32 1 04/06/23 04:58 107-06-2 ND ug/L 1.0 0.35 1 04/06/23 04:58 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-9 Lab ID: 92659945002 Collected: 03/30/23 14:33 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 99 % 70-130 104 % 70-130 102 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 95 % 67-130 100 % 70-130 0.38 1 04/06/23 04:58 156-59-2 0.40 1 04/06/23 04:58 156-60-5 0.36 1 04/06/23 04:58 78-87-5 0.36 1 04/06/23 04:58 10061-01-5 0.36 1 04/06/23 04:58 10061-02-6 0.30 1 04/06/23 04:58 100-41-4 0.48 1 04/06/23 04:58 591-78-6 9.7 1 04/06/23 04:58 74-88-4 v2 2.0 1 04/06/23 04:58 75-09-2 L1,v1 2.7 1 04/06/23 04:58 108-10-1 0.29 1 04/06/23 04:58 100-42-5 0.31 1 04/06/23 04:58 630-20-6 0.22 1 04/06/23 04:58 79-34-5 0.29 1 04/06/23 04:58 127-18-4 0.24 1 04/06/23 04:58 108-88-3 0.33 1 04/06/23 04:58 71-55-6 0.32 1 04/06/23 04:58 79-00-5 0.38 1 04/06/23 04:58 79-01-6 0.30 1 04/06/23 04:58 75-69-4 0.26 1 04/06/23 04:58 96-18-4 1.3 1 04/06/23 04:58 108-05-4 0.39 1 04/06/23 04:58 75-01-4 0.34 1 04/06/23 04:58 1330-20-7 1 04/06/23 04:58 460-00-4 1 04/06/23 04:58 17060-07-0 1 04/06/23 04:58 2037-26-5 0.86 1 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/07/23 01:43 123-91-1 H1,H5 04/07/23 01:43 17060-07-0 04/07/23 01:43 2037-26-5 Page 8 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-10 Lab ID: 92659945003 Collected: 03/30/23 12:58 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 12:16 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 12:16 7440-38-2 Barium 54.0 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 12:16 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 12:16 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 12:16 7440-43-9 Chromium 2.01J ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 12:16 7440-47-3 J Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 12:16 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 12:16 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 12:16 7439-92-1 Nickel ND ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 12:16 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 12:16 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 12:16 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 12:16 7440-62-2 Zinc 9.33J ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 12:16 7440-66-6 J Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 15:17 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/07/23 04:29 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 04/07/23 04:29 107-13-1 Benzene ND ug/L 1.0 0.34 1 04/07/23 04:29 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/07/23 04:29 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/07/23 04:29 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/07/23 04:29 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/07/23 04:29 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/07/23 04:29 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/07/23 04:29 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/07/23 04:29 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/07/23 04:29 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/07/23 04:29 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/07/23 04:29 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/07/23 04:29 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/07/23 04:29 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/07/23 04:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/07/23 04:29 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/07/23 04:29 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/07/23 04:29 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/07/23 04:29 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/07/23 04:29 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/07/23 04:29 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/07/23 04:29 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/07/23 04:29 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-10 Lab ID: 92659945003 Collected: 03/30/23 12:58 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 96 % 70-130 102 % 70-130 100 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 102 % 67-130 122 % 70-130 0.38 1 04/07/23 04:29 156-59-2 0.40 1 04/07/23 04:29 156-60-5 0.36 1 04/07/23 04:29 78-87-5 0.36 1 04/07/23 04:29 10061-01-5 0.36 1 04/07/23 04:29 10061-02-6 0.30 1 04/07/23 04:29 100-41-4 0.48 1 04/07/23 04:29 591-78-6 9.7 1 04/07/23 04:29 74-88-4 2.0 1 04/07/23 04:29 75-09-2 L1,v1 2.7 1 04/07/23 04:29 108-10-1 0.29 1 04/07/23 04:29 100-42-5 0.31 1 04/07/23 04:29 630-20-6 0.22 1 04/07/23 04:29 79-34-5 0.29 1 04/07/23 04:29 127-18-4 0.24 1 04/07/23 04:29 108-88-3 0.33 1 04/07/23 04:29 71-55-6 0.32 1 04/07/23 04:29 79-00-5 0.38 1 04/07/23 04:29 79-01-6 0.30 1 04/07/23 04:29 75-69-4 0.26 1 04/07/23 04:29 96-18-4 1.3 1 04/07/23 04:29 108-05-4 0.39 1 04/07/23 04:29 75-01-4 v2 0.34 1 04/07/23 04:29 1330-20-7 1 04/07/23 04:29 460-00-4 1 04/07/23 04:29 17060-07-0 1 04/07/23 04:29 2037-26-5 0.86 1 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/07/23 02:02 123-91-1 H 1, H5 04/07/23 02:02 17060-07-0 04/07/23 02:02 2037-26-5 Page 10 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-11 Lab ID: 92659945004 Collected: 03/30/23 11:40 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 12:19 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 12:19 7440-38-2 Barium 31.8 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 12:19 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 12:19 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 12:19 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 12:19 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 12:19 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 12:19 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 12:19 7439-92-1 Nickel 3.78J ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 12:19 7440-02-0 B,J Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 12:19 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 12:19 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 12:19 7440-62-2 Zinc 9.03J ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 12:19 7440-66-6 J Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 15:21 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/07/23 04:48 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 04/07/23 04:48 107-13-1 Benzene ND ug/L 1.0 0.34 1 04/07/23 04:48 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/07/23 04:48 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/07/23 04:48 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/07/23 04:48 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/07/23 04:48 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/07/23 04:48 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/07/23 04:48 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/07/23 04:48 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/07/23 04:48 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/07/23 04:48 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/07/23 04:48 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/07/23 04:48 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/07/23 04:48 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/07/23 04:48 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/07/23 04:48 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/07/23 04:48 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/07/23 04:48 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/07/23 04:48 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/07/23 04:48 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/07/23 04:48 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/07/23 04:48 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/07/23 04:48 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-11 Lab ID: 92659945004 Collected: 03/30/23 11:40 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 97 % 70-130 104 % 70-130 103 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 99 % 67-130 121 % 70-130 0.38 1 04/07/23 04:48 156-59-2 0.40 1 04/07/23 04:48 156-60-5 0.36 1 04/07/23 04:48 78-87-5 0.36 1 04/07/23 04:48 10061-01-5 0.36 1 04/07/23 04:48 10061-02-6 0.30 1 04/07/23 04:48 100-41-4 0.48 1 04/07/23 04:48 591-78-6 9.7 1 04/07/23 04:48 74-88-4 IL 2.0 1 04/07/23 04:48 75-09-2 L1,v1 2.7 1 04/07/23 04:48 108-10-1 0.29 1 04/07/23 04:48 100-42-5 0.31 1 04/07/23 04:48 630-20-6 0.22 1 04/07/23 04:48 79-34-5 0.29 1 04/07/23 04:48 127-18-4 0.24 1 04/07/23 04:48 108-88-3 0.33 1 04/07/23 04:48 71-55-6 0.32 1 04/07/23 04:48 79-00-5 0.38 1 04/07/23 04:48 79-01-6 0.30 1 04/07/23 04:48 75-69-4 0.26 1 04/07/23 04:48 96-18-4 1.3 1 04/07/23 04:48 108-05-4 0.39 1 04/07/23 04:48 75-01-4 v2 0.34 1 04/07/23 04:48 1330-20-7 1 04/07/23 04:48 460-00-4 1 04/07/23 04:48 17060-07-0 1 04/07/23 04:48 2037-26-5 0.86 1 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/07/23 02:21 123-91-1 H 1, H5 04/07/23 02:21 17060-07-0 04/07/23 02:21 2037-26-5 Page 12 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: TRIP BLANK UNIT 2 Lab ID: 92659945006 Collected: 03/30/23 00:00 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 04/07/23 03:15 67-64-1 ND ug/L 10.0 1.8 1 04/07/23 03:15 107-13-1 ND ug/L 1.0 0.34 1 04/07/23 03:15 71-43-2 ND ug/L 1.0 0.47 1 04/07/23 03:15 74-97-5 ND ug/L 1.0 0.31 1 04/07/23 03:15 75-27-4 ND ug/L 1.0 0.34 1 04/07/23 03:15 75-25-2 ND ug/L 2.0 1.7 1 04/07/23 03:15 74-83-9 ND ug/L 5.0 4.0 1 04/07/23 03:15 78-93-3 ND ug/L 2.0 0.36 1 04/07/23 03:15 75-15-0 ND ug/L 1.0 0.33 1 04/07/23 03:15 56-23-5 ND ug/L 1.0 0.28 1 04/07/23 03:15 108-90-7 ND ug/L 1.0 0.65 1 04/07/23 03:15 75-00-3 ND ug/L 1.0 0.43 1 04/07/23 03:15 67-66-3 ND ug/L 1.0 0.54 1 04/07/23 03:15 74-87-3 ND ug/L 2.0 0.34 1 04/07/23 03:15 96-12-8 ND ug/L 1.0 0.36 1 04/07/23 03:15 124-48-1 ND ug/L 1.0 0.27 1 04/07/23 03:15 106-93-4 ND ug/L 1.0 0.39 1 04/07/23 03:15 74-95-3 ND ug/L 1.0 0.34 1 04/07/23 03:15 95-50-1 ND ug/L 1.0 0.33 1 04/07/23 03:15 106-46-7 ND ug/L 1.0 0.56 1 04/07/23 03:15 110-57-6 ND ug/L 1.0 0.37 1 04/07/23 03:15 75-34-3 ND ug/L 1.0 0.32 1 04/07/23 03:15 107-06-2 ND ug/L 1.0 0.35 1 04/07/23 03:15 75-35-4 ND ug/L 1.0 0.38 1 04/07/23 03:15 156-59-2 ND ug/L 1.0 0.40 1 04/07/23 03:15 156-60-5 ND ug/L 1.0 0.36 1 04/07/23 03:15 78-87-5 ND ug/L 1.0 0.36 1 04/07/23 03:15 10061-01-5 ND ug/L 1.0 0.36 1 04/07/23 03:15 10061-02-6 ND ug/L 1.0 0.30 1 04/07/23 03:15 100-41-4 ND ug/L 5.0 0.48 1 04/07/23 03:15 591-78-6 ND ug/L 20.0 9.7 1 04/07/23 03:15 74-88-4 ND ug/L 5.0 2.0 1 04/07/23 03:15 75-09-2 ND ug/L 5.0 2.7 1 04/07/23 03:15 108-10-1 ND ug/L 1.0 0.29 1 04/07/23 03:15 100-42-5 ND ug/L 1.0 0.31 1 04/07/23 03:15 630-20-6 ND ug/L 1.0 0.22 1 04/07/23 03:15 79-34-5 ND ug/L 1.0 0.29 1 04/07/23 03:15 127-18-4 ND ug/L 1.0 0.24 1 04/07/23 03:15 108-88-3 ND ug/L 1.0 0.33 1 04/07/23 03:15 71-55-6 ND ug/L 1.0 0.32 1 04/07/23 03:15 79-00-5 ND ug/L 1.0 0.38 1 04/07/23 03:15 79-01-6 ND ug/L 1.0 0.30 1 04/07/23 03:15 75-69-4 ND ug/L 1.0 0.26 1 04/07/23 03:15 96-18-4 ND ug/L 2.0 1.3 1 04/07/23 03:15 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1,v1 Page 13 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: TRIP BLANK UNIT 2 Parameters Lab ID: 92659945006 Collected: Report Results Units Limit 03/30/23 00:00 MDL DF Received: 03/31/23 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Vinyl chloride ND ug/L 1.0 0.39 1 04/07/23 03:15 75-01-4 v2 Xylene (Total) ND ug/L 1.0 0.34 1 04/07/23 03:15 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 1 04/07/23 03:15 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 04/07/23 03:15 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 04/07/23 03:15 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 04/05/23 18:27 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 78 % 67-130 1 04/05/23 18:27 17060-07-0 Toluene-d8 (S) 87 % 70-130 1 04/05/23 18:27 2037-26-5 Date: 04/12/2023 08:14 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: NES-2S Lab ID: 92659945007 Collected: 03/29/23 12:32 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/07/2310:27 04/07/2318:39 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/07/2310:27 04/07/2318:39 7440-38-2 Barium 38.3 ug/L 5.00 0.736 1 04/07/2310:27 04/07/2318:39 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/07/2310:27 04/07/2318:39 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/07/2310:27 04/07/2318:39 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/07/2310:27 04/07/2318:39 7440-47-3 Cobalt 1.28J ug/L 10.0 0.840 1 04/07/2310:27 04/07/2318:39 7440-48-4 J Copper ND ug/L 10.0 3.68 1 04/07/2310:27 04/07/2318:39 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/07/2310:27 04/07/2318:39 7439-92-1 Nickel ND ug/L 10.0 1.61 1 04/07/2310:27 04/07/2318:39 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/07/2310:27 04/07/2318:39 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/07/2310:27 04/07/2318:39 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/07/2310:27 04/07/2318:39 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/07/2310:27 04/07/2318:39 7440-66-6 Metals (ICPMS) 6020B Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 04/12/2023 08:14 AM Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet ND ug/L 2.00 0.121 1 04/09/2310:28 04/10/2311:44 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 04/05/2318:20 67-64-1 ND ug/L 10.0 1.8 1 04/05/2318:20 107-13-1 ND ug/L 1.0 0.34 1 04/05/2318:20 71-43-2 ND ug/L 1.0 0.47 1 04/05/2318:20 74-97-5 ND ug/L 1.0 0.31 1 04/05/2318:20 75-27-4 ND ug/L 1.0 0.34 1 04/05/2318:20 75-25-2 ND ug/L 2.0 1.7 1 04/05/2318:20 74-83-9 ND ug/L 5.0 4.0 1 04/05/2318:20 78-93-3 ND ug/L 2.0 0.36 1 04/05/2318:20 75-15-0 ND ug/L 1.0 0.33 1 04/05/2318:20 56-23-5 ND ug/L 1.0 0.28 1 04/05/2318:20 108-90-7 ND ug/L 1.0 0.65 1 04/05/2318:20 75-00-3 ND ug/L 1.0 0.43 1 04/05/2318:20 67-66-3 ND ug/L 1.0 0.54 1 04/05/2318:20 74-87-3 ND ug/L 2.0 0.34 1 04/05/2318:20 96-12-8 ND ug/L 1.0 0.36 1 04/05/2318:20 124-48-1 ND ug/L 1.0 0.27 1 04/05/2318:20 106-93-4 ND ug/L 1.0 0.39 1 04/05/2318:20 74-95-3 ND ug/L 1.0 0.34 1 04/05/2318:20 95-50-1 ND ug/L 1.0 0.33 1 04/05/2318:20 106-46-7 ND ug/L 1.0 0.56 1 04/05/2318:20 110-57-6 ND ug/L 1.0 0.37 1 04/05/2318:20 75-34-3 ND ug/L 1.0 0.32 1 04/05/2318:20 107-06-2 ND ug/L 1.0 0.35 1 04/05/2318:20 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v1 Page 15 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: NES-2S Lab ID: 92659945007 Collected: 03/29/23 12:32 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 102 % 70-130 99 % 70-130 101 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 81 % 67-130 87 % 70-130 0.38 1 04/05/23 18:20 156-59-2 0.40 1 04/05/23 18:20 156-60-5 0.36 1 04/05/23 18:20 78-87-5 0.36 1 04/05/23 18:20 10061-01-5 0.36 1 04/05/23 18:20 10061-02-6 0.30 1 04/05/23 18:20 100-41-4 0.48 1 04/05/23 18:20 591-78-6 9.7 1 04/05/23 18:20 74-88-4 2.0 1 04/05/23 18:20 75-09-2 L1,v1 2.7 1 04/05/23 18:20 108-10-1 0.29 1 04/05/23 18:20 100-42-5 0.31 1 04/05/23 18:20 630-20-6 0.22 1 04/05/23 18:20 79-34-5 0.29 1 04/05/23 18:20 127-18-4 0.24 1 04/05/23 18:20 108-88-3 0.33 1 04/05/23 18:20 71-55-6 0.32 1 04/05/23 18:20 79-00-5 0.38 1 04/05/23 18:20 79-01-6 0.30 1 04/05/23 18:20 75-69-4 0.26 1 04/05/23 18:20 96-18-4 1.3 1 04/05/23 18:20 108-05-4 0.39 1 04/05/23 18:20 75-01-4 v2 0.34 1 04/05/23 18:20 1330-20-7 1 04/05/23 18:20 460-00-4 1 04/05/23 18:20 17060-07-0 1 04/05/23 18:20 2037-26-5 0.86 1 8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/05/23 18:46 123-91-1 H 1 04/05/23 18:46 17060-07-0 04/05/23 18:46 2037-26-5 Page 16 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-7 Lab ID: 92659945008 Collected: 03/29/23 15:09 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/06/2311:02 04/06/2318:35 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/06/2311:02 04/06/2318:35 7440-38-2 Barium 3.92J ug/L 5.00 0.736 1 04/06/2311:02 04/06/2318:35 7440-39-3 B,J Beryllium ND ug/L 2.00 0.330 1 04/06/2311:02 04/06/2318:35 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/06/2311:02 04/06/2318:35 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/06/2311:02 04/06/2318:35 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/06/2311:02 04/06/2318:35 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/06/2311:02 04/06/2318:35 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/06/2311:02 04/06/2318:35 7439-92-1 Nickel ND ug/L 10.0 1.61 1 04/06/2311:02 04/06/2318:35 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/06/2311:02 04/06/2318:35 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/06/2311:02 04/06/2318:35 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/06/2311:02 04/06/2318:35 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/06/2311:02 04/06/2318:35 7440-66-6 Metals (ICPMS) 6020B Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 04/12/2023 08:14 AM Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet ND ug/L 2.00 0.121 1 04/06/23 08:30 04/07/23 12:25 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 04/05/2318:38 67-64-1 ND ug/L 10.0 1.8 1 04/05/2318:38 107-13-1 ND ug/L 1.0 0.34 1 04/05/2318:38 71-43-2 ND ug/L 1.0 0.47 1 04/05/2318:38 74-97-5 ND ug/L 1.0 0.31 1 04/05/2318:38 75-27-4 ND ug/L 1.0 0.34 1 04/05/2318:38 75-25-2 ND ug/L 2.0 1.7 1 04/05/2318:38 74-83-9 ND ug/L 5.0 4.0 1 04/05/2318:38 78-93-3 ND ug/L 2.0 0.36 1 04/05/2318:38 75-15-0 ND ug/L 1.0 0.33 1 04/05/2318:38 56-23-5 ND ug/L 1.0 0.28 1 04/05/2318:38 108-90-7 ND ug/L 1.0 0.65 1 04/05/2318:38 75-00-3 ND ug/L 1.0 0.43 1 04/05/2318:38 67-66-3 ND ug/L 1.0 0.54 1 04/05/2318:38 74-87-3 ND ug/L 2.0 0.34 1 04/05/2318:38 96-12-8 ND ug/L 1.0 0.36 1 04/05/2318:38 124-48-1 ND ug/L 1.0 0.27 1 04/05/2318:38 106-93-4 ND ug/L 1.0 0.39 1 04/05/2318:38 74-95-3 ND ug/L 1.0 0.34 1 04/05/2318:38 95-50-1 ND ug/L 1.0 0.33 1 04/05/2318:38 106-46-7 ND ug/L 1.0 0.56 1 04/05/2318:38 110-57-6 ND ug/L 1.0 0.37 1 04/05/2318:38 75-34-3 ND ug/L 1.0 0.32 1 04/05/2318:38 107-06-2 ND ug/L 1.0 0.35 1 04/05/2318:38 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v1 Page 17 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 Sample: MW-7 Lab ID: 92659945008 Collected: 03/29/23 15:09 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/12/2023 08:14 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.38 1 04/05/2318:38 156-59-2 ND ug/L 1.0 0.40 1 04/05/2318:38 156-60-5 ND ug/L 1.0 0.36 1 04/05/2318:38 78-87-5 ND ug/L 1.0 0.36 1 04/05/23 18:38 10061-01-5 ND ug/L 1.0 0.36 1 04/05/2318:38 10061-02-6 ND ug/L 1.0 0.30 1 04/05/2318:38 100-41-4 ND ug/L 5.0 0.48 1 04/05/2318:38 591-78-6 ND ug/L 20.0 9.7 1 04/05/2318:38 74-88-4 ND ug/L 5.0 2.0 1 04/05/2318:38 75-09-2 L1,v1 ND ug/L 5.0 2.7 1 04/05/2318:38 108-10-1 ND ug/L 1.0 0.29 1 04/05/2318:38 100-42-5 ND ug/L 1.0 0.31 1 04/05/2318:38 630-20-6 ND ug/L 1.0 0.22 1 04/05/2318:38 79-34-5 ND ug/L 1.0 0.29 1 04/05/2318:38 127-18-4 ND ug/L 1.0 0.24 1 04/05/2318:38 108-88-3 ND ug/L 1.0 0.33 1 04/05/2318:38 71-55-6 ND ug/L 1.0 0.32 1 04/05/2318:38 79-00-5 ND ug/L 1.0 0.38 1 04/05/2318:38 79-01-6 ND ug/L 1.0 0.30 1 04/05/2318:38 75-69-4 ND ug/L 1.0 0.26 1 04/05/2318:38 96-18-4 ND ug/L 2.0 1.3 1 04/05/2318:38 108-05-4 ND ug/L 1.0 0.39 1 04/05/2318:38 75-01-4 v2 ND ug/L 1.0 0.34 1 04/05/2318:38 1330-20-7 98 % 70-130 1 04/05/2318:38 460-00-4 101 % 70-130 1 04/05/2318:38 17060-07-0 101 % 70-130 1 04/05/2318:38 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 04/05/2319:05 123-91-1 79 % 67-130 1 04/05/2319:05 17060-07-0 87 % 70-130 1 04/05/2319:05 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2035939 Analysis Method: EPA 6010D QC Batch Method: 3015 Analysis Description: Metals (ICP) 6010D Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 METHOD BLANK: R3909657-1 Matrix: Water Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 Blank Reporting Parameter Units Result Limit Antimony ug/L ND 10.0 Arsenic ug/L ND 10.0 Barium ug/L ND 5.00 Beryllium ug/L ND 2.00 Cadmium ug/L ND 2.00 Chromium ug/L ND 10.0 Cobalt ug/L ND 10.0 Copper ug/L ND 10.0 Lead ug/L ND 6.00 Nickel ug/L 2.32J 10.0 Selenium ug/L ND 10.0 Silver ug/L ND 5.00 Vanadium ug/L ND 20.0 Zinc ug/L ND 50.0 MDL Analyzed 4.30 04/05/2311:37 4.40 04/05/2311:37 0.736 04/05/2311:37 0.330 04/05/2311:37 0.479 04/05/2311:37 1.40 04/05/2311:37 0.840 04/05/2311:37 3.68 04/05/2311:37 2.99 04/05/2311:37 1.61 04/05/23 11:37 7.35 04/05/2311:37 1.54 04/05/2311:37 4.99 04/05/2311:37 6.52 04/05/2311:37 LABORATORY CONTROL SAMPLE: Parameter R3909657-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 1000 966 96.6 80.0-120 Arsenic ug/L 1000 905 90.5 80.0-120 Barium ug/L 1000 978 97.8 80.0-120 Beryllium ug/L 1000 950 95.0 80.0-120 Cadmium ug/L 1000 949 94.9 80.0-120 Chromium ug/L 1000 947 94.7 80.0-120 Cobalt ug/L 1000 949 94.9 80.0-120 Copper ug/L 1000 957 95.7 80.0-120 Lead ug/L 1000 944 94.4 80.0-120 Nickel ug/L 1000 943 94.3 80.0-120 Selenium ug/L 1000 929 92.9 80.0-120 Silver ug/L 200 175 87.7 80.0-120 Vanadium ug/L 1000 971 97.1 80.0-120 Zinc ug/L 1000 933 93.3 80.0-120 Qualifiers J Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659945 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909657-4 R3909657-5 MS MSD 92659945001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 1000 1000 967 982 96.7 98.2 75.0-125 1.62 20 Arsenic ug/L ND 1000 1000 940 925 94.0 92.5 75.0-125 1.68 20 Barium ug/L 43.7 1000 1000 1040 1030 99.7 99.0 75.0-125 0.718 20 Beryllium ug/L ND 1000 1000 965 957 96.5 95.7 75.0-125 0.867 20 Cadmium ug/L ND 1000 1000 975 965 97.5 96.5 75.0-125 1.04 20 Chromium ug/L ND 1000 1000 959 958 95.9 95.8 75.0-125 0.147 20 Cobalt ug/L ND 1000 1000 966 957 96.6 95.7 75.0-125 0.933 20 Copper ug/L 22.3 1000 1000 999 986 97.7 96.4 75.0-125 1.26 20 Lead ug/L ND 1000 1000 960 953 96.0 95.3 75.0-125 0.733 20 Nickel ug/L 3.28 1000 1000 957 950 95.4 94.7 75.0-125 0.753 20 Selenium ug/L ND 1000 1000 956 951 95.6 95.1 75.0-125 0.509 20 Silver ug/L ND 200 200 179 179 89.6 89.5 75.0-125 0.089 20 Vanadium ug/L ND 1000 1000 977 968 97.7 96.8 75.0-125 0.914 20 Zinc ug/L ND 1000 1000 948 938 94.8 93.8 75.0-125 1.04 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2036804 Analysis Method: EPA 6010D QC Batch Method: 3015 Analysis Description: Metals (ICP) 6010D Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945008 METHOD BLANK: R3910433-5 Associated Lab Samples: 92659945008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 10.0 4.30 04/06/23 21:36 Arsenic ug/L ND 10.0 4.40 04/06/23 21:36 Barium ug/L 2.27J 5.00 0.736 04/06/23 21:36 J Beryllium ug/L ND 2.00 0.330 04/06/23 21:36 Cadmium ug/L 0.653J 2.00 0.479 04/06/23 21:36 J Chromium ug/L ND 10.0 1.40 04/06/23 21:36 Cobalt ug/L 0.943J 10.0 0.840 04/06/23 21:36 J Copper ug/L ND 10.0 3.68 04/06/23 21:36 Lead ug/L ND 6.00 2.99 04/06/23 21:36 Nickel ug/L ND 10.0 1.61 04/06/23 21:36 Selenium ug/L ND 10.0 7.35 04/06/23 21:36 Silver ug/L ND 5.00 1.54 04/06/23 21:36 Vanadium ug/L ND 20.0 4.99 04/06/23 21:36 Zinc ug/L ND 50.0 6.52 04/06/23 21:36 LABORATORY CONTROL SAMPLE: Parameter R3910433-1 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 1000 966 96.6 80.0-120 Arsenic ug/L 1000 940 94.0 80.0-120 Barium ug/L 1000 1030 103 80.0-120 Beryllium ug/L 1000 975 97.5 80.0-120 Cadmium ug/L 1000 977 97.7 80.0-120 Chromium ug/L 1000 947 94.7 80.0-120 Cobalt ug/L 1000 988 98.8 80.0-120 Copper ug/L 1000 952 95.2 80.0-120 Lead ug/L 1000 988 98.8 80.0-120 Nickel ug/L 1000 970 97.0 80.0-120 Selenium ug/L 1000 958 95.8 80.0-120 Silver ug/L 200 189 94.5 80.0-120 Vanadium ug/L 1000 990 99.0 80.0-120 Zinc ug/L 1000 984 98.4 80.0-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659945 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3910433-3 R3910433-4 MS MSD L1602313-03 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 1000 1000 960 942 96.0 94.2 75.0-125 1.88 20 Arsenic ug/L ND 1000 1000 933 920 93.3 92.0 75.0-125 1.47 20 Barium ug/L 87.4 1000 1000 1110 1100 103 101 75.0-125 1.19 20 Beryllium ug/L ND 1000 1000 990 980 99.0 98.0 75.0-125 0.960 20 Cadmium ug/L ND 1000 1000 962 951 96.2 95.1 75.0-125 1.09 20 Chromium ug/L 2.11 1000 1000 928 912 92.6 91.0 75.0-125 1.74 20 Cobalt ug/L ND 1000 1000 958 950 95.8 95.0 75.0-125 0.816 20 Copper ug/L ND 1000 1000 930 921 93.0 92.1 75.0-125 0.974 20 Lead ug/L ND 1000 1000 959 951 95.9 95.1 75.0-125 0.874 20 Nickel ug/L 2.28 1000 1000 937 932 93.5 92.9 75.0-125 0.574 20 Selenium ug/L ND 1000 1000 954 944 95.4 94.4 75.0-125 0.975 20 Silver ug/L ND 200 200 187 184 93.6 92.2 75.0-125 1.54 20 Vanadium ug/L ND 1000 1000 976 966 97.6 96.6 75.0-125 1.04 20 Zinc ug/L ND 1000 1000 963 953 96.3 95.3 75.0-125 1.01 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2037648 Analysis Method: EPA 6010D QC Batch Method: 3015 Analysis Description: Metals (ICP) 6010D Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945007 METHOD BLANK: R3911145-1 Associated Lab Samples: 92659945007 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 10.0 4.30 04/07/2318:24 Arsenic ug/L ND 10.0 4.40 04/07/2318:24 Barium ug/L 0.864J 5.00 0.736 04/07/2318:24 J Beryllium ug/L ND 2.00 0.330 04/07/2318:24 Cadmium ug/L ND 2.00 0.479 04/07/2318:24 Chromium ug/L ND 10.0 1.40 04/07/2318:24 Cobalt ug/L ND 10.0 0.840 04/07/2318:24 Copper ug/L ND 10.0 3.68 04/07/2318:24 Lead ug/L ND 6.00 2.99 04/07/2318:24 Nickel ug/L ND 10.0 1.61 04/07/2318:24 Selenium ug/L ND 10.0 7.35 04/07/2318:24 Silver ug/L ND 5.00 1.54 04/07/2318:24 Vanadium ug/L ND 20.0 4.99 04/07/2318:24 Zinc ug/L ND 50.0 6.52 04/07/2318:24 LABORATORY CONTROL SAMPLE: Parameter R3911145-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 1000 963 96.3 80.0-120 Arsenic ug/L 1000 942 94.2 80.0-120 Barium ug/L 1000 1020 102 80.0-120 Beryllium ug/L 1000 959 95.9 80.0-120 Cadmium ug/L 1000 980 98.0 80.0-120 Chromium ug/L 1000 947 94.7 80.0-120 Cobalt ug/L 1000 991 99.1 80.0-120 Copper ug/L 1000 970 97.0 80.0-120 Lead ug/L 1000 981 98.1 80.0-120 Nickel ug/L 1000 971 97.1 80.0-120 Selenium ug/L 1000 966 96.6 80.0-120 Silver ug/L 200 188 94.0 80.0-120 Vanadium ug/L 1000 983 98.3 80.0-120 Zinc ug/L 1000 984 98.4 80.0-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659945 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3911145-4 R3911145-5 MS MSD L1602548-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 1000 1000 983 991 98.3 99.1 75.0-125 0.830 20 Arsenic ug/L 101 1000 1000 1050 1050 94.9 94.8 75.0-125 0.106 20 Barium ug/L 18.2 1000 1000 1050 1050 103 104 75.0-125 0.016 20 Beryllium ug/L ND 1000 1000 975 979 97.5 97.9 75.0-125 0.449 20 Cadmium ug/L ND 1000 1000 996 995 99.6 99.5 75.0-125 0.096 20 Chromium ug/L 46.8 1000 1000 974 978 92.7 93.1 75.0-125 0.448 20 Cobalt ug/L ND 1000 1000 988 987 98.8 98.7 75.0-125 0.103 20 Copper ug/L ND 1000 1000 973 973 97.3 97.3 75.0-125 0.045 20 Lead ug/L ND 1000 1000 974 975 97.4 97.5 75.0-125 0.179 20 Nickel ug/L ND 1000 1000 963 962 96.3 96.2 75.0-125 0.068 20 Selenium ug/L ND 1000 1000 961 966 96.1 96.6 75.0-125 0.533 20 Silver ug/L ND 200 200 190 191 95.1 95.7 75.0-125 0.625 20 Vanadium ug/L ND 1000 1000 1000 1010 100 101 75.0-125 0.341 20 Zinc ug/L ND 1000 1000 953 954 95.3 95.4 75.0-125 0.104 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2035938 Analysis Method: EPA 6020B QC Batch Method: 3015 Analysis Description: Metals (ICPMS) 6020B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 METHOD BLANK: R3909560-1 Matrix: Water Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L 0.172J 2.00 0.121 04/05/2312:01 J LABORATORY CONTROL SAMPLE: R3909560-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 50.0 48.4 96.7 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909560-4 R3909560-5 MS MSD L1601349-02 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 50.0 50.0 48.2 50.0 96.5 100 75.0-125 3.58 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2036805 Analysis Method: EPA 6020B QC Batch Method: 3015 Analysis Description: Metals (ICPMS) 6020B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945008 METHOD BLANK: R3910616-1 Associated Lab Samples: 92659945008 Parameter Units Thallium ug/L LABORATORY CONTROL SAMPLE: R3910616-2 Parameter Units Thallium ug/L Matrix: Water Blank Reporting Result Limit ND 2.00 Spike LCS Conc. Result 50.0 48.6 MDL Analyzed Qualifiers 0.121 04/07/23 12:05 LCS % Rec % Rec Limits Qualifiers 97.3 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3910616-4 R3910616-5 MS MSD L1602134-04 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.218 50.0 50.0 50.8 52.6 101 105 75.0-125 3.58 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 2037656 Analysis Method: EPA 6020B QC Batch Method: 3015 Analysis Description: Metals (ICPMS) 6020B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659945007 METHOD BLANK: R3911419-1 Associated Lab Samples: 92659945007 Parameter Units Thallium ug/L LABORATORY CONTROL SAMPLE: R3911419-2 Parameter Units Thallium ug/L Matrix: Water Blank Reporting Result Limit 0.160J 2.00 Spike LCS Conc. Result 50.0 47.5 MDL Analyzed Qualifiers 0.121 04/10/2311:24 J LCS % Rec % Rec Limits Qualifiers 94.9 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3911419-4 R3911419-5 MS MSD L1602631-04 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.164 50.0 50.0 47.7 47.5 95.1 94.7 75.0-125 0.462 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 765935 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659945001, 92659945002 METHOD BLANK: 3976859 Associated Lab Samples: 92659945001, 92659945002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/06/23 01:55 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/06/23 01:55 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/06/23 01:55 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/06/23 01:55 1,1-Dichloroethane ug/L ND 1.0 0.37 04/06/23 01:55 1,1-Dichloroethene ug/L ND 1.0 0.35 04/06/23 01:55 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/06/23 01:55 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/06/23 01:55 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/06/23 01:55 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/06/23 01:55 1,2-Dichloroethane ug/L ND 1.0 0.32 04/06/23 01:55 1,2-Dichloropropane ug/L ND 1.0 0.36 04/06/23 01:55 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/06/23 01:55 2-Butanone (MEK) ug/L ND 5.0 4.0 04/06/23 01:55 2-Hexanone ug/L ND 5.0 0.48 04/06/23 01:55 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/06/23 01:55 Acetone ug/L ND 25.0 5.1 04/06/23 01:55 Acrylonitrile ug/L ND 10.0 1.8 04/06/23 01:55 Benzene ug/L ND 1.0 0.34 04/06/23 01:55 Bromochloromethane ug/L ND 1.0 0.47 04/06/23 01:55 Bromodichloromethane ug/L ND 1.0 0.31 04/06/23 01:55 Bromoform ug/L ND 1.0 0.34 04/06/23 01:55 Bromomethane ug/L ND 2.0 1.7 04/06/23 01:55 v2 Carbon disulfide ug/L ND 2.0 0.36 04/06/23 01:55 Carbon tetrachloride ug/L ND 1.0 0.33 04/06/23 01:55 Chlorobenzene ug/L ND 1.0 0.28 04/06/23 01:55 Chloroethane ug/L ND 1.0 0.65 04/06/23 01:55 Chloroform ug/L ND 1.0 0.43 04/06/23 01:55 Chloromethane ug/L ND 1.0 0.54 04/06/23 01:55 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/06/23 01:55 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/06/23 01:55 Dibromochloromethane ug/L ND 1.0 0.36 04/06/23 01:55 Dibromomethane ug/L ND 1.0 0.39 04/06/23 01:55 Ethylbenzene ug/L ND 1.0 0.30 04/06/23 01:55 lodomethane ug/L ND 20.0 9.7 04/06/23 01:55 v2 Methylene Chloride ug/L ND 5.0 2.0 04/06/23 01:55 v1 Styrene ug/L ND 1.0 0.29 04/06/23 01:55 Tetrachloroethene ug/L ND 1.0 0.29 04/06/23 01:55 Toluene ug/L ND 1.0 0.24 04/06/23 01:55 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/06/23 01:55 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 METHOD BLANK: 3976859 Associated Lab Samples: 92659945001, 92659945002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 04/06/23 01:55 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 04/06/23 01:55 Trichloroethene ug/L ND 1.0 0.38 04/06/23 01:55 Trichlorofluoromethane ug/L ND 1.0 0.30 04/06/23 01:55 Vinyl acetate ug/L ND 2.0 1.3 04/06/23 01:55 Vinyl chloride ug/L ND 1.0 0.39 04/06/23 01:55 Xylene (Total) ug/L ND 1.0 0.34 04/06/23 01:55 1,2-Dichloroethane-d4 (S) % 99 70-130 04/06/23 01:55 4-Bromofluorobenzene (S) % 99 70-130 04/06/23 01:55 Toluene-d8(S) % 102 70-130 04/06/23 01:55 LABORATORY CONTROL SAMPLE: Parameter 3976860 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 19.7 98 70-130 1,1,1-Trichloroethane ug/L 20 19.9 99 70-130 1,1,2,2-Tetrachloroethane ug/L 20 22.2 111 70-130 1,1,2-Trichloroethane ug/L 20 21.9 109 70-130 1,1-Dichloroethane ug/L 20 20.3 101 70-130 1,1-Dichloroethene ug/L 20 19.3 96 70-130 1,2,3-Trichloropropane ug/L 20 20.9 104 70-130 1,2-Dibromo-3-chloropropane ug/L 20 20.7 104 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.6 103 70-130 1,2-Dichlorobenzene ug/L 20 21.5 107 70-130 1,2-Dichloroethane ug/L 20 20.9 104 70-130 1,2-Dichloropropane ug/L 20 20.4 102 70-130 1,4-Dichlorobenzene ug/L 20 20.5 102 70-130 2-Butanone (MEK) ug/L 40 45.3 113 70-134 2-Hexanone ug/L 40 45.8 114 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 45.8 115 70-130 Acetone ug/L 40 43.4 109 70-133 Acrylonitrile ug/L 100 110 110 70-130 Benzene ug/L 20 20.1 100 70-130 Bromochloromethane ug/L 20 19.1 95 70-130 Bromodichloromethane ug/L 20 20.2 101 70-130 Bromoform ug/L 20 19.4 97 70-130 Bromomethane ug/L 20 15.0 75 45-151 v3 Carbon disulfide ug/L 20 17.6 88 70-130 Carbon tetrachloride ug/L 20 18.5 92 70-130 Chlorobenzene ug/L 20 20.4 102 70-130 Chloroethane ug/L 20 20.8 104 39-152 Chloroform ug/L 20 20.4 102 70-130 Chloromethane ug/L 20 19.8 99 58-130 cis-1,2-Dichloroethene ug/L 20 20.4 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 LABORATORY CONTROL SAMPLE: 3976860 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 20 19.8 99 70-130 Dibromochloromethane ug/L 20 19.8 99 70-130 Dibromomethane ug/L 20 18.8 94 70-130 Ethylbenzene ug/L 20 20.2 101 70-130 lodomethane ug/L 40 34.9 87 53-141 v3 Methylene Chloride ug/L 20 45.2 226 66-130 L1,v1 Styrene ug/L 20 20.7 103 70-130 Tetrachloroethene ug/L 20 18.7 93 70-130 Toluene ug/L 20 19.9 99 70-130 trans-1,2-Dichloroethene ug/L 20 19.5 97 70-130 trans- 1,3-Dichloropropene ug/L 20 19.7 99 70-130 trans-1,4-Dichloro-2-butene ug/L 20 24.0 120 57-185 Trichloroethene ug/L 20 19.3 96 70-130 Trichlorofluoromethane ug/L 20 18.8 94 62-130 Vinyl acetate ug/L 40 41.6 104 70-144 Vinyl chloride ug/L 20 16.0 80 62-130 Xylene (Total) ug/L 60 60.0 100 70-130 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 3976862 Units 92659774024 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.3 107 70-141 1,1,1-Trichloroethane ug/L ND 20 21.7 109 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 23.1 116 69-142 1,1,2-Trichloroethane ug/L ND 20 22.5 113 70-138 1,1-Dichloroethane ug/L 4.6 20 26.5 110 70-150 1,1-Dichloroethene ug/L ND 20 21.2 106 70-156 1,2,3-Trichloropropane ug/L ND 20 22.3 112 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 21.4 107 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 22.1 110 70-138 1,2-Dichlorobenzene ug/L ND 20 22.7 113 70-141 1,2-Dichloroethane ug/L ND 20 22.8 114 69-143 1,2-Dichloropropene ug/L ND 20 21.7 108 68-156 1,4-Dichlorobenzene ug/L ND 20 22.1 111 70-142 2-Butanone (MEK) ug/L ND 40 47.7 119 60-157 2-Hexanone ug/L ND 40 46.4 116 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 46.4 116 70-141 Acetone ug/L ND 40 41.3 103 58-157 Acrylonitrile ug/L ND 100 110 110 69-147 Benzene ug/L ND 20 21.5 106 70-142 Bromochloromethane ug/L ND 20 20.5 102 70-146 Bromodichloromethane ug/L ND 20 20.8 104 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 MATRIX SPIKE SAMPLE: Parameter 3976862 Units 92659774024 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromoform ug/L ND 20 19.5 98 64-140 Bromomethane ug/L ND 20 16.9 85 28-192 v3 Carbon disulfide ug/L ND 20 19.2 96 70-151 Carbon tetrachloride ug/L ND 20 20.0 100 70-148 Chlorobenzene ug/L ND 20 22.2 110 70-141 Chloroethane ug/L ND 20 22.8 114 58-191 Chloroform ug/L ND 20 20.0 100 70-148 Chloromethane ug/L ND 20 20.6 103 43-162 cis-1,2-Dichloroethene ug/L 1.1 20 22.7 108 68-151 cis-1,3-Dichloropropene ug/L ND 20 20.9 104 70-139 Dibromochloromethane ug/L ND 20 20.8 104 70-144 Dibromomethane ug/L ND 20 19.5 98 70-139 Ethylbenzene ug/L ND 20 22.1 110 70-143 lodomethane ug/L ND 40 36.9 92 35-171 v3 Methylene Chloride ug/L ND 20 19.0 95 62-149 v1 Styrene ug/L ND 20 22.1 110 70-143 Tetrachloroethene ug/L ND 20 19.7 99 70-145 Toluene ug/L ND 20 21.4 107 70-142 trans-1,2-Dichloroethene ug/L ND 20 21.5 107 70-151 trans- 1,3-Dichloropropene ug/L ND 20 20.7 104 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 23.2 116 51-159 Trichloroethene ug/L ND 20 21.1 102 62-146 Trichlorofluoromethane ug/L ND 20 21.0 105 63-153 Vinyl acetate ug/L ND 40 42.5 106 61-162 Vinyl chloride ug/L ND 20 17.7 88 61-163 Xylene (Total) ug/L ND 60 64.7 108 70-143 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 3976861 Parameter Units 92659774020 Result Dup Result RPD Max RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 SAMPLE DUPLICATE: 3976861 Parameter Units 92659774020 Result Dup Result RPD Max RPD 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 v2 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 v2 Methylene Chloride ug/L ND ND 30 v1 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 Xylene (Total) ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 104 102 4-Bromofluorobenzene (S) % 100 100 Toluene-d8 (S) % 103 102 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 766172 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659945007, 92659945008 METHOD BLANK: 3978025 Associated Lab Samples: 92659945007, 92659945008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/05/23 13:10 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/05/23 13:10 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/05/23 13:10 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/05/23 13:10 1,1-Dichloroethane ug/L ND 1.0 0.37 04/05/23 13:10 1,1-Dichloroethene ug/L ND 1.0 0.35 04/05/23 13:10 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/05/23 13:10 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/05/23 13:10 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/05/23 13:10 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/05/23 13:10 1,2-Dichloroethane ug/L ND 1.0 0.32 04/05/23 13:10 1,2-Dichloropropane ug/L ND 1.0 0.36 04/05/23 13:10 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/05/23 13:10 2-Butanone (MEK) ug/L ND 5.0 4.0 04/05/23 13:10 2-Hexanone ug/L ND 5.0 0.48 04/05/23 13:10 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/05/23 13:10 Acetone ug/L ND 25.0 5.1 04/05/23 13:10 Acrylonitrile ug/L ND 10.0 1.8 04/05/23 13:10 Benzene ug/L ND 1.0 0.34 04/05/23 13:10 Bromochloromethane ug/L ND 1.0 0.47 04/05/23 13:10 Bromodichloromethane ug/L ND 1.0 0.31 04/05/23 13:10 Bromoform ug/L ND 1.0 0.34 04/05/23 13:10 Bromomethane ug/L ND 2.0 1.7 04/05/23 13:10 v2 Carbon disulfide ug/L ND 2.0 0.36 04/05/23 13:10 Carbon tetrachloride ug/L ND 1.0 0.33 04/05/23 13:10 Chlorobenzene ug/L ND 1.0 0.28 04/05/23 13:10 Chloroethane ug/L ND 1.0 0.65 04/05/23 13:10 Chloroform ug/L ND 1.0 0.43 04/05/23 13:10 Chloromethane ug/L ND 1.0 0.54 04/05/23 13:10 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/05/23 13:10 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/05/23 13:10 Dibromochloromethane ug/L ND 1.0 0.36 04/05/23 13:10 Dibromomethane ug/L ND 1.0 0.39 04/05/23 13:10 Ethylbenzene ug/L ND 1.0 0.30 04/05/23 13:10 lodomethane ug/L ND 20.0 9.7 04/05/23 13:10 Methylene Chloride ug/L ND 5.0 2.0 04/05/23 13:10 v1 Styrene ug/L ND 1.0 0.29 04/05/23 13:10 Tetrachloroethene ug/L ND 1.0 0.29 04/05/23 13:10 Toluene ug/L ND 1.0 0.24 04/05/23 13:10 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/05/23 13:10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 METHOD BLANK: 3978025 Associated Lab Samples: 92659945007, 92659945008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 04/05/23 13:10 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 04/05/23 13:10 v1 Trichloroethene ug/L ND 1.0 0.38 04/05/23 13:10 Trichlorofluoromethane ug/L ND 1.0 0.30 04/05/23 13:10 Vinyl acetate ug/L ND 2.0 1.3 04/05/23 13:10 Vinyl chloride ug/L ND 1.0 0.39 04/05/23 13:10 v2 Xylene (Total) ug/L ND 1.0 0.34 04/05/23 13:10 1,2-Dichloroethane-d4 (S) % 102 70-130 04/05/23 13:10 4-Bromofluorobenzene (S) % 99 70-130 04/05/23 13:10 Toluene-d8 (S) % 103 70-130 04/05/23 13:10 LABORATORY CONTROL SAMPLE: Parameter 3978026 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 19.3 97 70-130 1,1,1-Trichloroethane ug/L 20 19.1 96 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.2 106 70-130 1,1,2-Trichloroethane ug/L 20 20.4 102 70-130 1,1-Dichloroethane ug/L 20 18.8 94 70-130 1,1-Dichloroethene ug/L 20 18.9 94 70-130 1,2,3-Trichloropropane ug/L 20 20.0 100 70-130 1,2-Dibromo-3-chloropropane ug/L 20 19.5 98 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.0 100 70-130 1,2-Dichlorobenzene ug/L 20 20.9 105 70-130 1,2-Dichloroethane ug/L 20 20.6 103 70-130 1,2-Dichloropropane ug/L 20 20.0 100 70-130 1,4-Dichlorobenzene ug/L 20 20.5 103 70-130 2-Butanone (MEK) ug/L 40 40.1 100 70-134 2-Hexanone ug/L 40 41.1 103 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 41.9 105 70-130 Acetone ug/L 40 37.6 94 70-133 Acrylonitrile ug/L 100 97.5 97 70-130 Benzene ug/L 20 18.9 95 70-130 Bromochloromethane ug/L 20 18.1 91 70-130 Bromodichloromethane ug/L 20 19.7 98 70-130 Bromoform ug/L 20 18.2 91 70-130 Bromomethane ug/L 20 14.2 71 45-151 v3 Carbon disulfide ug/L 20 17.1 85 70-130 Carbon tetrachloride ug/L 20 17.7 88 70-130 Chlorobenzene ug/L 20 19.6 98 70-130 Chloroethane ug/L 20 20.1 101 39-152 Chloroform ug/L 20 19.7 98 70-130 Chloromethane ug/L 20 19.8 99 58-130 cis-1,2-Dichloroethene ug/L 20 18.9 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 LABORATORY CONTROL SAMPLE: 3978026 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 20 19.3 97 70-130 Dibromochloromethane ug/L 20 19.3 96 70-130 Dibromomethane ug/L 20 17.8 89 70-130 Ethylbenzene ug/L 20 19.8 99 70-130 lodomethane ug/L 40 33.8 85 53-141 Methylene Chloride ug/L 20 46.8 234 66-130 L1,v1 Styrene ug/L 20 20.0 100 70-130 Tetrachloroethene ug/L 20 18.3 92 70-130 Toluene ug/L 20 19.0 95 70-130 trans-1,2-Dichloroethene ug/L 20 18.9 95 70-130 trans- 1,3-Dichloropropene ug/L 20 19.2 96 70-130 trans-1,4-Dichloro-2-butene ug/L 20 24.3 122 57-185 v1 Trichloroethene ug/L 20 18.5 93 70-130 Trichlorofluoromethane ug/L 20 18.0 90 62-130 Vinyl acetate ug/L 40 40.0 100 70-144 Vinyl chloride ug/L 20 15.9 79 62-130 v3 Xylene (Total) ug/L 60 57.4 96 70-130 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 3978028 Units 92659923020 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 23.2 116 70-141 1,1,1-Trichloroethane ug/L ND 20 23.1 116 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 25.5 127 69-142 1,1,2-Trichloroethane ug/L ND 20 23.6 118 70-138 1,1-Dichloroethane ug/L ND 20 23.0 115 70-150 1,1-Dichloroethene ug/L ND 20 22.7 113 70-156 1,2,3-Trichloropropane ug/L ND 20 24.5 123 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 23.4 117 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 24.3 121 70-138 1,2-Dichlorobenzene ug/L ND 20 24.3 121 70-141 1,2-Dichloroethane ug/L ND 20 23.8 119 69-143 1,2-Dichloropropane ug/L ND 20 23.0 115 68-156 1,4-Dichlorobenzene ug/L ND 20 23.8 119 70-142 2-Butanone (MEK) ug/L ND 40 50.1 125 60-157 2-Hexanone ug/L ND 40 51.6 129 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 50.5 126 70-141 Acetone ug/L ND 40 45.1 113 58-157 Acrylonitrile ug/L ND 100 113 113 69-147 Benzene ug/L ND 20 22.7 113 70-142 Bromochloromethane ug/L ND 20 21.3 107 70-146 Bromodichloromethane ug/L ND 20 22.6 113 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 MATRIX SPIKE SAMPLE: Parameter 3978028 Units 92659923020 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromoform ug/L ND 20 22.2 111 64-140 Bromomethane ug/L ND 20 19.3 96 28-192 v3 Carbon disulfide ug/L ND 20 19.8 99 70-151 Carbon tetrachloride ug/L ND 20 21.9 109 70-148 Chlorobenzene ug/L ND 20 23.5 118 70-141 Chloroethane ug/L ND 20 23.0 115 58-191 Chloroform ug/L ND 20 22.3 111 70-148 Chloromethane ug/L ND 20 21.8 109 43-162 cis-1,2-Dichloroethene ug/L ND 20 22.7 113 68-151 cis-1,3-Dichloropropene ug/L ND 20 22.3 111 70-139 Dibromochloromethane ug/L ND 20 22.7 114 70-144 Dibromomethane ug/L ND 20 21.8 109 70-139 Ethylbenzene ug/L ND 20 27.5 123 70-143 lodomethane ug/L ND 40 39.7 99 35-171 v3 Methylene Chloride ug/L ND 20 20.8 104 62-149 v1 Styrene ug/L ND 20 23.6 118 70-143 Tetrachloroethene ug/L ND 20 21.5 107 70-145 Toluene ug/L 6.1 20 28.3 111 70-142 trans-1,2-Dichloroethene ug/L ND 20 23.1 116 70-151 trans- 1,3-Dichloropropene ug/L ND 20 22.7 113 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 27.4 137 51-159 Trichloroethene ug/L ND 20 22.0 110 62-146 Trichlorofluoromethane ug/L ND 20 21.7 109 63-153 Vinyl acetate ug/L ND 40 45.1 113 61-162 Vinyl chloride ug/L ND 20 18.5 92 61-163 Xylene (Total) ug/L 18.7 60 90.4 119 70-143 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 3978027 Parameter Units 92659923019 Result Dup Result RPD Max RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 SAMPLE DUPLICATE: 3978027 Parameter Units 92659923019 Result Dup Result Max RPD RPD 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND 0.42J 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 v2 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Ethylbenzene ug/L ND 4.1 5 30 lodomethane ug/L ND ND 30 v2 Methylene Chloride ug/L ND ND 30 v1 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L 10.1 10.0 1 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 Xylene (Total) ug/L 24.3 25.4 4 30 1,2-Dichloroethane-d4 (S) % 104 101 4-Bromofluorobenzene (S) % 99 100 Toluene-d8 (S) % 102 103 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 766317 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659945003, 92659945004, 92659945006 METHOD BLANK: 3978969 Matrix: Associated Lab Samples: 92659945003, 92659945004, 92659945006 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/07/23 02:20 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/07/23 02:20 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/07/23 02:20 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/07/23 02:20 1,1-Dichloroethane ug/L ND 1.0 0.37 04/07/23 02:20 1,1-Dichloroethene ug/L ND 1.0 0.35 04/07/23 02:20 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/07/23 02:20 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/07/23 02:20 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/07/23 02:20 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/07/23 02:20 1,2-Dichloroethane ug/L ND 1.0 0.32 04/07/23 02:20 1,2-Dichloropropane ug/L ND 1.0 0.36 04/07/23 02:20 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/07/23 02:20 2-Butanone (MEK) ug/L ND 5.0 4.0 04/07/23 02:20 2-Hexanone ug/L ND 5.0 0.48 04/07/23 02:20 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/07/23 02:20 Acetone ug/L ND 25.0 5.1 04/07/23 02:20 Acrylonitrile ug/L ND 10.0 1.8 04/07/23 02:20 Benzene ug/L ND 1.0 0.34 04/07/23 02:20 Bromochloromethane ug/L ND 1.0 0.47 04/07/23 02:20 Bromodichloromethane ug/L ND 1.0 0.31 04/07/23 02:20 Bromoform ug/L ND 1.0 0.34 04/07/23 02:20 Bromomethane ug/L ND 2.0 1.7 04/07/23 02:20 Carbon disulfide ug/L ND 2.0 0.36 04/07/23 02:20 Carbon tetrachloride ug/L ND 1.0 0.33 04/07/23 02:20 Chlorobenzene ug/L ND 1.0 0.28 04/07/23 02:20 Chloroethane ug/L ND 1.0 0.65 04/07/23 02:20 Chloroform ug/L ND 1.0 0.43 04/07/23 02:20 Chloromethane ug/L ND 1.0 0.54 04/07/23 02:20 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/07/23 02:20 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/07/23 02:20 Dibromochloromethane ug/L ND 1.0 0.36 04/07/23 02:20 Dibromomethane ug/L ND 1.0 0.39 04/07/23 02:20 Ethylbenzene ug/L ND 1.0 0.30 04/07/23 02:20 lodomethane ug/L ND 20.0 9.7 04/07/23 02:20 Methylene Chloride ug/L ND 5.0 2.0 04/07/23 02:20 v1 Styrene ug/L ND 1.0 0.29 04/07/23 02:20 Tetrachloroethene ug/L ND 1.0 0.29 04/07/23 02:20 Toluene ug/L ND 1.0 0.24 04/07/23 02:20 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/07/23 02:20 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 METHOD BLANK: 3978969 Matrix: Associated Lab Samples: 92659945003, 92659945004, 92659945006 Blank Parameter Units Result Water Reporting Limit MDL Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 04/07/23 02:20 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 04/07/23 02:20 Trichloroethene ug/L ND 1.0 0.38 04/07/23 02:20 Trichlorofluoromethane ug/L ND 1.0 0.30 04/07/23 02:20 Vinyl acetate ug/L ND 2.0 1.3 04/07/23 02:20 Vinyl chloride ug/L ND 1.0 0.39 04/07/23 02:20 Xylene (Total) ug/L ND 1.0 0.34 04/07/23 02:20 1,2-Dichloroethane-d4 (S) % 102 70-130 04/07/23 02:20 4-Bromofluorobenzene (S) % 95 70-130 04/07/23 02:20 Toluene-d8 (S) % 102 70-130 04/07/23 02:20 LABORATORY CONTROL SAMPLE: Parameter 3978970 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 20 19.8 99 70-130 1,1,1-Trichloroethane ug/L 20 20.2 101 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.8 109 70-130 1,1,2-Trichloroethane ug/L 20 21.2 106 70-130 1,1-Dichloroethane ug/L 20 19.5 98 70-130 1,1-Dichloroethene ug/L 20 19.5 97 70-130 1,2,3-Trichloropropane ug/L 20 20.6 103 70-130 1,2-Dibromo-3-chloropropane ug/L 20 20.0 100 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.1 100 70-130 1,2-Dichlorobenzene ug/L 20 20.9 105 70-130 1,2-Dichloroethane ug/L 20 21.4 107 70-130 1,2-Dichloropropane ug/L 20 20.5 103 70-130 1,4-Dichlorobenzene ug/L 20 19.6 98 70-130 2-Butanone (MEK) ug/L 40 43.2 108 70-134 2-Hexanone ug/L 40 42.6 107 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 43.1 108 70-130 Acetone ug/L 40 42.2 106 70-133 Acrylonitrile ug/L 100 106 106 70-130 Benzene ug/L 20 19.6 98 70-130 Bromochloromethane ug/L 20 19.9 99 70-130 Bromodichloromethane ug/L 20 19.9 100 70-130 Bromoform ug/L 20 18.7 94 70-130 Bromomethane ug/L 20 16.0 80 45-151 Carbon disulfide ug/L 20 16.4 82 70-130 Carbon tetrachloride ug/L 20 18.1 90 70-130 Chlorobenzene ug/L 20 19.7 99 70-130 Chloroethane ug/L 20 20.4 102 39-152 Chloroform ug/L 20 20.9 104 70-130 Chloromethane ug/L 20 20.1 100 58-130 cis-1,2-Dichloroethene ug/L 20 20.1 100 70-130 Qualifiers v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 LABORATORY CONTROL SAMPLE: 3978970 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 20 18.9 95 70-130 Dibromochloromethane ug/L 20 19.4 97 70-130 Dibromomethane ug/L 20 19.0 95 70-130 Ethylbenzene ug/L 20 19.7 98 70-130 lodomethane ug/L 40 33.6 84 53-141 Methylene Chloride ug/L 20 30.2 151 66-130 L1,v1 Styrene ug/L 20 19.3 96 70-130 Tetrachloroethene ug/L 20 18.4 92 70-130 Toluene ug/L 20 19.9 100 70-130 trans-1,2-Dichloroethene ug/L 20 19.1 95 70-130 trans- 1,3-Dichloropropene ug/L 20 19.7 99 70-130 trans-1,4-Dichloro-2-butene ug/L 20 22.9 114 57-185 Trichloroethene ug/L 20 18.5 93 70-130 Trichlorofluoromethane ug/L 20 18.5 92 62-130 Vinyl acetate ug/L 40 41.6 104 70-144 Vinyl chloride ug/L 20 15.8 79 62-130 v3 Xylene (Total) ug/L 60 57.9 97 70-130 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 3978972 Units 92659774022 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 22.0 110 70-141 1,1,1-Trichloroethane ug/L ND 20 21.5 108 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 23.2 116 69-142 1,1,2-Trichloroethane ug/L ND 20 22.0 110 70-138 1,1-Dichloroethane ug/L ND 20 21.7 109 70-150 1,1-Dichloroethene ug/L ND 20 22.2 111 70-156 1,2,3-Trichloropropane ug/L ND 20 22.4 112 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 23.2 116 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 22.6 113 70-138 1,2-Dichlorobenzene ug/L ND 20 23.0 115 70-141 1,2-Dichloroethane ug/L ND 20 21.8 109 69-143 1,2-Dichloropropene ug/L ND 20 22.4 112 68-156 1,4-Dichlorobenzene ug/L ND 20 22.8 114 70-142 2-Butanone (MEK) ug/L ND 40 44.8 112 60-157 2-Hexanone ug/L ND 40 49.4 123 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 46.3 116 70-141 Acetone ug/L ND 40 42.6 106 58-157 Acrylonitrile ug/L ND 100 107 107 69-147 Benzene ug/L ND 20 21.2 106 70-142 Bromochloromethane ug/L ND 20 21.9 110 70-146 Bromodichloromethane ug/L ND 20 21.1 105 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 MATRIX SPIKE SAMPLE: 3978972 92659774022 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromoform ug/L ND 20 21.2 106 64-140 Bromomethane ug/L ND 20 14.7 73 28-192 v3 Carbon disulfide ug/L ND 20 20.2 101 70-151 Carbon tetrachloride ug/L ND 20 21.3 106 70-148 Chlorobenzene ug/L ND 20 22.3 111 70-141 Chloroethane ug/L ND 20 22.0 110 58-191 Chloroform ug/L ND 20 21.2 106 70-148 Chloromethane ug/L ND 20 16.2 81 43-162 cis-1,2-Dichloroethene ug/L ND 20 21.7 108 68-151 cis-1,3-Dichloropropene ug/L ND 20 21.3 106 70-139 Dibromochloromethane ug/L ND 20 21.7 109 70-144 Dibromomethane ug/L ND 20 20.6 103 70-139 Ethylbenzene ug/L ND 20 22.0 110 70-143 lodomethane ug/L ND 40 28.8 72 35-171 IL,v3 Methylene Chloride ug/L ND 20 27.2 136 62-149 v1 Styrene ug/L ND 20 22.9 115 70-143 Tetrachloroethene ug/L ND 20 21.5 107 70-145 Toluene ug/L ND 20 21.6 108 70-142 trans-1,2-Dichloroethene ug/L ND 20 22.0 110 70-151 trans- 1,3-Dichloropropene ug/L ND 20 21.6 108 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 21.2 106 51-159 Trichloroethene ug/L ND 20 21.3 106 62-146 Trichlorofluoromethane ug/L ND 20 19.5 98 63-153 Vinyl acetate ug/L ND 40 44.9 112 61-162 Vinyl chloride ug/L ND 20 15.2 76 61-163 Xylene (Total) ug/L ND 60 67.1 112 70-143 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 3978971 92659945004 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 SAMPLE DUPLICATE: 3978971 Parameter Units 92659945004 Result 1,4-Dichlorobenzene ug/L ND 2-Butanone (MEK) ug/L ND 2-Hexanone ug/L ND 4-Methyl-2-pentanone (MIBK) ug/L ND Acetone ug/L ND Acrylonitrile ug/L ND Benzene ug/L ND Bromochloromethane ug/L ND Bromodichloromethane ug/L ND Bromoform ug/L ND Bromomethane ug/L ND Carbon disulfide ug/L ND Carbon tetrachloride ug/L ND Chlorobenzene ug/L ND Chloroethane ug/L ND Chloroform ug/L ND Chloromethane ug/L ND cis-1,2-Dichloroethene ug/L ND cis-1,3-Dichloropropene ug/L ND Dibromochloromethane ug/L ND Dibromomethane ug/L ND Ethylbenzene ug/L ND lodomethane ug/L ND Methylene Chloride ug/L ND Styrene ug/L ND Tetrachloroethene ug/L ND Toluene ug/L ND trans-1,2-Dichloroethene ug/L ND trans- 1,3-Dichloropropene ug/L ND trans-1,4-Dichloro-2-butene ug/L ND Trichloroethene ug/L ND Trichlorofluoromethane ug/L ND Vinyl acetate ug/L ND Vinyl chloride ug/L ND Xylene (Total) ug/L ND 1,2-Dichloroethane-d4 (S) % 104 4-Bromofluorobenzene (S) % 97 Toluene-d8 (S) % 103 Dup Result RPD Max RPD Qualifiers ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 v2 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 I L, v2 ND 30 v1 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 107 98 101 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 766177 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659945006, 92659945007, 92659945008 METHOD BLANK: 3978071 Matrix: Water Associated Lab Samples: 92659945006, 92659945007, 92659945008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 04/05/23 17:11 1,2-Dichloroethane-d4 (S) % 83 67-130 04/05/23 17:11 Toluene-d8 (S) % 87 70-130 04/05/23 17:11 LABORATORY CONTROL SAMPLE: 3978072 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 18.3 92 70-130 1,2-Dichloroethane-d4 (S) % 84 67-130 Toluene-d8 (S) % 88 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3978073 3978074 MS MSD 92659945007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 17.8 18.0 88 89 55-137 1 30 H1 1,2-Dichloroethane-d4 (S) % 79 83 67-130 30 Toluene-d8 (S) % 89 88 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 49 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 QC Batch: 766432 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 METHOD BLANK: 3979517 Matrix: Water Associated Lab Samples: 92659945001, 92659945002, 92659945003, 92659945004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 04/06/23 18:46 1,2-Dichloroethane-d4 (S) % 103 67-130 04/06/23 18:46 Toluene-d8 (S) % 101 70-130 04/06/23 18:46 LABORATORY CONTROL SAMPLE: 3979518 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 19.6 98 70-130 1,2-Dichloroethane-d4 (S) % 103 67-130 Toluene-d8 (S) % 102 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979519 3979520 MS MSD 92659681001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 4.6 20 20 21.1 20.8 82 81 55-137 2 30 H1 1,2-Dichloroethane-d4 (S) % 103 103 67-130 30 Toluene-d8(S) % 121 120 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659945 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. WORKORDER QUALIFIERS WO: 92659945 [1] ANALYTE QUALIFIERS Analyte was detected in the associated method blank. H1 Analysis conducted outside the EPA method holding time. H5 Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 08:14 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 49 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659945 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92659945001 MW-8 3015 2035939 EPA6010D 2035939 92659945002 MW-9 3015 2035939 EPA6010D 2035939 92659945003 MW-10 3015 2035939 EPA6010D 2035939 92659945004 MW-11 3015 2035939 EPA6010D 2035939 92659945007 NES-2S 3015 2037648 EPA6010D 2037648 92659945008 MW-7 3015 2036804 EPA6010D 2036804 92659945001 MW-8 3015 2035938 EPA 6020B 2035938 92659945002 MW-9 3015 2035938 EPA 6020B 2035938 92659945003 MW-10 3015 2035938 EPA 6020B 2035938 92659945004 MW-11 3015 2035938 EPA 6020B 2035938 92659945007 NES-2S 3015 2037656 EPA 6020B 2037656 92659945008 MW-7 3015 2036805 EPA 6020B 2036805 92659945001 MW-8 EPA 8260D 765935 92659945002 MW-9 EPA 8260D 765935 92659945003 MW-10 EPA 8260D 766317 92659945004 MW-11 EPA 8260D 766317 92659945006 TRIP BLANK UNIT 2 EPA 8260D 766317 92659945007 NES-2S EPA 8260D 766172 92659945008 MW-7 EPA 8260D 766172 92659945001 MW-8 EPA 8260D Mod. 766432 92659945002 MW-9 EPA 8260D Mod. 766432 92659945003 MW-10 EPA 8260D Mod. 766432 92659945004 MW-11 EPA 8260D Mod. 766432 92659945006 TRIP BLANK UNIT 2 EPA 8260D Mod. 766177 92659945007 NES-2S EPA 8260D Mod. 766177 92659945008 MW-7 EPA 8260D Mod. 766177 Date: 04/12/2023 08:14 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 49 � OC# Title: ENV=FRM- HUNT, 0083 v02_Sample Condition ' (( upon Receipt i sutra:sraet &fft}ctive Date: 33/]q/2022 &;18 3p AM LaboratorY receiving samples: Asheville ldeni] eenwoadEl Huntersvllle ❑ Raleigft[ Mechanicsville client Name: ❑. Atlanta[] l(erttersvilie14 j , Prglet ri, 'O# : 9265 G� �rart .Fed �x 9945 0 Cammerclai UPS USPS Pace 0Otf�er,— �flent Custody goal Present? IO92659945 ❑Yes �fa Seals Intact? �— ❑Yes WfVn - Packing MatBrlal! ©ate/initrson ! l+eminln d:BUbble Wrap ials PeH contertls;�' TherrnarrtPfQt Bubble aqs ❑None Q Other 1R CUNJI), ❑ Yegagte$} Tls90e Fretet't7 f�LIL `QNo ,�N/A COtrectlen Factor; Type of 1te: E lWet .O Blue l Dn'e CacslerT m Add/subtract (.'0 Cooler Tertlp Corrected .: Temp shodd he above freezjng to 6'C i �)05amplesoutatie USDA Regulated Sall (.E .N/A, water sam�te) !mc0eria;•Sptnpiesorrkercoall. qld sansplas erfginate_!n a quarantine zone s+ilthin the, EPrlited•$fates: t has tiegun process: (eheck maps} QYes • ONO A, NY, ar sc Old Samples ariglnatefrornafare ign.source # ++ n•. �; ,. • intfuding`Haurall and Puerto Rlca)?!0yes �litierna. Tonally, Chaim afCi�stod Piesent7.' = • ' ;' r Quo dyes ONo Cntn3deI ts/i1FsL�epa'Aa{._ ` Samples Arrived:.[Klthfh Flold,Tirrte7 �1r/q Z. Short Hold Time l yes No N/A Rnafysis (<72'hr,}T ,y� ❑O2: - RuSh Turn Around Tfrne'RcgUestedT CfYe3 A'o OWA 3, - Sufficient Voiurrie? Cl yes uo O,V/A q. correct Containers Ustd-7 Yes O t"O O N/A 5, -Pace Container- Used2 Rf Yas ❑ No ❑A'/A Containers tnlact? Yes []hp 6, ❑NIA Di'ssaivedaiafysis,'Sam fes: P Fiend Mtered7 Yes ONa Dti/A 7 Sample Labels Match GOG7. 17Yes l;TNo, WA e Q fQs l� N'o ❑ NIA 4 nea052"016 VOA Vials Trip HrtkiaPreSent? ONIMENTS/SAMPLE Y7 I Yes ®No 01i/A Fyes Cj Ko O N/A I.Yes 0 No O N/A � 0 �0 .s e,Y;,,� , FieldData J!"'red? .OAS ONo V'r Lot I of sloflt conta..— Date/Time; Pr61ect Manager SCLIRF Review.. prn}ect ManagerSRF Review; Date; Date: Fray in- ,;Qp'id Page 47 of • ac�� u�rrusraxts DO Title: ENV-FRM•HUNI-0083 02 Sample Condition Upon Receipt r Efteativa Date:11J14/Z{122 81$:30 14M ---, WO# : 92659945 *Check rnark:top Ralf of. box if pH and/or dechlorination Is verified and Project q PM: TMC Due Date: 04/07/23 vsrithlnthe acceptance range for preseruationsamples. CLIENT: 92—Harb Ral FS a:01uns: VOA, Collform, TOCi Oil and Grease, DRO/8015 lWa er):DoC, LLHg "Bottum half of box is -to fist number of battles I_ i **+Check a u.nprese►vsd Alltrates for chlorine — µ 217 Z Vry• Z 'nl 4 Z N i T al 2. _ C�y?3 Cr r j fgry��I a -` d-.- --•' ��, se �s`C• 4 Vvy e.. Z u a x S = a 2 fl c - •� A to ,'�1' �+' S - L �j. b C 2• 2:,. T= U �' CI G7 U ra �r R Y . �ro a. ¢ � �E E JE E a� � --- - n -4 -° -J a � 4 d � d > � � a a Ui ui N �. a ..� 5{ :.M•I' ., rl ri .r4 _ N Q An 0 N ry Co.,. E E ,iyyn I. Y , - i. go rA it'v. .�.. „f�i � Q:� .01 ' ,� [J• (,�� a x 3 ®aSO«T®w -I-F- - .: pH Adjustment .dog for Preserued-Samples Sample.1D Type;pf Preservative pH upon receipt Date preservation adjusted Time_proservolla t Amount of PreservatiVe adjusted added Note: Wheneverthefaisadis0epancyaffecting NasthCarallnacompllahcesamples, acolriofthis formwillbesenttotheNorthCarallnaDENR.Certifir Out othgld, incorrect preservative, Out Oftemp, inCorfect:craritalners, Lot k ion Wice fiuntfr•nv lnl A09 ld P ena ? r%f ? Page 48 of 49 ITEMS n f I C o n 3 7 7 p r p rn [ 7 v � S S � \ S C r 0 `-' � � fn7 V• .- Qom' � -cfi` � , •a�1h � re I s S d E = x w 3 ;F 'Q.4£ f raaralxce_ a SAl.,PZE TrE (G-GPCp C=CCU,•?i v3 u► w g �5� ❑ O r m Ln •v L V `, 7i b a z c AMPLF,TEM-AT CCLEC,O`, i7 Q OF C6NTAI'i_RS 7�4 Unpreservaa 5 h2SO4 OA-X HNa3 t ! s r nagH c q � Na25203 C It Gz � c� D n Anlyisa 7t,; Y1N v rr7 4121VOCbya2ao a fp a' i,4dicrone by828D, 1I.q N q Tr: ,dank H ( a z re 1,4tllo%ena7,;p9ank c d crip n 0 W n L c 7FplP Ij C o- I d Receiyed cn IF (YltJj P?4Mdua' Chto4ne "� Ica . (YIN) us o.,y ianled • ro. VN YINJ Page 49 of lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 12, 2023 Jeffrey 011ison Hart & Hickman 3921 Sunset Ridge Rd. Ste. 301 Raleigh, NC 27607 RE: Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Dear Jeffrey 011ison: Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor M Cannon taylor.cannon@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 28 laneAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Lab ID Sample ID Matrix Date Collected Date Received 92659940001 92659940002 SW-3 SW-4 Water Water 03/30/2313:23 03/30/2313:40 03/31/2310:30 03/31/2310:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92659940001 SW-3 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C SM2340-97 ZSA 1 PAN 92659940002 SW-4 EPA 601OD ZSA 14 PAN EPA 6020E JPD 1 PAN EPA 8260D CL 50 PASI-C EPA 8260D Mod. TEG 3 PASI-C SM2340-97 ZSA 1 PAN PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Sample: SW-3 Lab ID: 92659940001 Collected: 03/30/23 13:23 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 11:53 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 11:53 7440-38-2 Barium 32.4 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 11:53 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 11:53 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 11:53 7440-43-9 Chromium 2.91J ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 11:53 7440-47-3 J Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 11:53 7440-48-4 Copper 4.07J ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 11:53 7440-50-8 J Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 11:53 7439-92-1 Nickel 3.36J ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 11:53 7440-02-0 B,J Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 11:53 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 11:53 7440-22-4 Vanadium 12.9J ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 11:53 7440-62-2 J Zinc 8.27J ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 11:53 7440-66-6 J Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 14:57 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/06/23 10:27 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 04/06/23 10:27 107-13-1 Benzene ND ug/L 1.0 0.34 1 04/06/23 10:27 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/06/23 10:27 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/06/23 10:27 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/06/23 10:27 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/06/23 10:27 74-83-9 v2 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/06/23 10:27 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/06/23 10:27 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/06/23 10:27 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/06/23 10:27 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/06/23 10:27 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/06/23 10:27 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/06/23 10:27 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/06/23 10:27 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/06/23 10:27 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/06/23 10:27 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/06/23 10:27 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/06/23 10:27 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/06/23 10:27 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/06/23 10:27 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/06/23 10:27 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/06/23 10:27 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/06/23 10:27 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Sample: SW-3 Lab ID: 92659940001 Collected: 03/30/23 13:23 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Calculated Results Hardness, Total(SM 2340B) Date: 04/12/2023 07:28 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 4.2J ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 96 % 70-130 115 % 70-130 100 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.38 1 04/06/23 10:27 156-59-2 0.40 1 04/06/23 10:27 156-60-5 0.36 1 04/06/23 10:27 78-87-5 0.36 1 04/06/23 10:27 10061-01-5 0.36 1 04/06/23 10:27 10061-02-6 0.30 1 04/06/23 10:27 100-41-4 0.48 1 04/06/23 10:27 591-78-6 9.7 1 04/06/23 10:27 74-88-4 IL,v2 2.0 1 04/06/23 10:27 75-09-2 B,C9, L1,v1 2.7 1 04/06/23 10:27 108-10-1 0.29 1 04/06/23 10:27 100-42-5 0.31 1 04/06/23 10:27 630-20-6 0.22 1 04/06/23 10:27 79-34-5 0.29 1 04/06/23 10:27 127-18-4 0.24 1 04/06/23 10:27 108-88-3 0.33 1 04/06/23 10:27 71-55-6 0.32 1 04/06/23 10:27 79-00-5 0.38 1 04/06/23 10:27 79-01-6 0.30 1 04/06/23 10:27 75-69-4 0.26 1 04/06/23 10:27 96-18-4 1.3 1 04/06/23 10:27 108-05-4 0.39 1 04/06/23 10:27 75-01-4 0.34 1 04/06/23 10:27 1330-20-7 1 04/06/23 10:27 460-00-4 1 04/06/23 10:27 17060-07-0 1 04/06/23 10:27 2037-26-5 0.86 1 91 % 67-130 1 99 % 70-130 1 Analytical Method: SM2340-97 Preparation Method: SM2340B Pace National - Mt. Juliet 04/07/23 00:27 123-91-1 H 1, H 5 04/07/23 00:27 17060-07-0 04/07/23 00:27 2037-26-5 16400 ug/L 2500 198 1 04/05/23 11:53 04/05/23 11:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Sample: SW-4 Lab ID: 92659940002 Collected: 03/30/23 13:40 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/05/23 07:27 04/05/23 11:55 7440-36-0 Arsenic 9.991 ug/L 10.0 4.40 1 04/05/23 07:27 04/05/23 11:55 7440-38-2 J Barium 27.9 ug/L 5.00 0.736 1 04/05/23 07:27 04/05/23 11:55 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/05/23 07:27 04/05/23 11:55 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/05/23 07:27 04/05/23 11:55 7440-43-9 Chromium 1.68J ug/L 10.0 1.40 1 04/05/23 07:27 04/05/23 11:55 7440-47-3 J Cobalt ND ug/L 10.0 0.840 1 04/05/23 07:27 04/05/23 11:55 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/05/23 07:27 04/05/23 11:55 7440-50-8 Lead ND ug/L 6.00 2.99 1 04/05/23 07:27 04/05/23 11:55 7439-92-1 Nickel 3.00J ug/L 10.0 1.61 1 04/05/23 07:27 04/05/23 11:55 7440-02-0 B,J Selenium ND ug/L 10.0 7.35 1 04/05/23 07:27 04/05/23 11:55 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/05/23 07:27 04/05/23 11:55 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/05/23 07:27 04/05/23 11:55 7440-62-2 Zinc 7.11J ug/L 50.0 6.52 1 04/05/23 07:27 04/05/23 11:55 7440-66-6 J Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 08:22 04/05/23 15:01 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/07/23 03:34 67-64-1 Acrylonitrile ND ug/L 10.0 1.8 1 04/07/23 03:34 107-13-1 Benzene ND ug/L 1.0 0.34 1 04/07/23 03:34 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/07/23 03:34 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/07/23 03:34 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/07/23 03:34 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/07/23 03:34 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/07/23 03:34 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/07/23 03:34 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/07/23 03:34 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/07/23 03:34 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/07/23 03:34 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/07/23 03:34 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/07/23 03:34 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/07/23 03:34 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/07/23 03:34 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/07/23 03:34 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/07/23 03:34 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/07/23 03:34 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/07/23 03:34 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/07/23 03:34 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/07/23 03:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/07/23 03:34 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/07/23 03:34 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 Sample: SW-4 Lab ID: 92659940002 Collected: 03/30/23 13:40 Received: 03/31/23 10:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Calculated Results Hardness, Total(SM 234013) Date: 04/12/2023 07:28 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 95 % 70-130 106 % 70-130 102 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 106 % 67-130 92 % 70-130 0.38 1 04/07/23 03:34 156-59-2 0.40 1 04/07/23 03:34 156-60-5 0.36 1 04/07/23 03:34 78-87-5 0.36 1 04/07/23 03:34 10061-01-5 0.36 1 04/07/23 03:34 10061-02-6 0.30 1 04/07/23 03:34 100-41-4 0.48 1 04/07/23 03:34 591-78-6 9.7 1 04/07/23 03:34 74-88-4 2.0 1 04/07/23 03:34 75-09-2 L1,v1 2.7 1 04/07/23 03:34 108-10-1 0.29 1 04/07/23 03:34 100-42-5 0.31 1 04/07/23 03:34 630-20-6 0.22 1 04/07/23 03:34 79-34-5 0.29 1 04/07/23 03:34 127-18-4 0.24 1 04/07/23 03:34 108-88-3 0.33 1 04/07/23 03:34 71-55-6 0.32 1 04/07/23 03:34 79-00-5 0.38 1 04/07/23 03:34 79-01-6 0.30 1 04/07/23 03:34 75-69-4 0.26 1 04/07/23 03:34 96-18-4 1.3 1 04/07/23 03:34 108-05-4 0.39 1 04/07/23 03:34 75-01-4 v2 0.34 1 04/07/23 03:34 1330-20-7 1 04/07/23 03:34 460-00-4 1 04/07/23 03:34 17060-07-0 1 04/07/23 03:34 2037-26-5 0.86 1 8 04/07/23 00:46 123-91-1 H 1, H5 04/07/23 00:46 17060-07-0 04/07/23 00:46 2037-26-5 Analytical Method: SM2340-97 Preparation Method: SM2340B Pace National - Mt. Juliet 21200 ug/L 2500 198 1 04/05/23 11:55 04/05/23 11:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 QC Batch: 2035939 Analysis Method: EPA 6010D QC Batch Method: 3015 Analysis Description: Metals (ICP) 6010D Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659940001, 92659940002 METHOD BLANK: R3909657-1 Associated Lab Samples: 92659940001, 92659940002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 10.0 4.30 04/05/2311:37 Arsenic ug/L ND 10.0 4.40 04/05/2311:37 Barium ug/L ND 5.00 0.736 04/05/2311:37 Beryllium ug/L ND 2.00 0.330 04/05/2311:37 Cadmium ug/L ND 2.00 0.479 04/05/2311:37 Chromium ug/L ND 10.0 1.40 04/05/2311:37 Cobalt ug/L ND 10.0 0.840 04/05/2311:37 Copper ug/L ND 10.0 3.68 04/05/2311:37 Lead ug/L ND 6.00 2.99 04/05/2311:37 Nickel ug/L 2.32J 10.0 1.61 04/05/2311:37 J Selenium ug/L ND 10.0 7.35 04/05/2311:37 Silver ug/L ND 5.00 1.54 04/05/2311:37 Vanadium ug/L ND 20.0 4.99 04/05/2311:37 Zinc ug/L ND 50.0 6.52 04/05/2311:37 LABORATORY CONTROL SAMPLE: Parameter R3909657-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 1000 966 96.6 80.0-120 Arsenic ug/L 1000 905 90.5 80.0-120 Barium ug/L 1000 978 97.8 80.0-120 Beryllium ug/L 1000 950 95.0 80.0-120 Cadmium ug/L 1000 949 94.9 80.0-120 Chromium ug/L 1000 947 94.7 80.0-120 Cobalt ug/L 1000 949 94.9 80.0-120 Copper ug/L 1000 957 95.7 80.0-120 Lead ug/L 1000 944 94.4 80.0-120 Nickel ug/L 1000 943 94.3 80.0-120 Selenium ug/L 1000 929 92.9 80.0-120 Silver ug/L 200 175 87.7 80.0-120 Vanadium ug/L 1000 971 97.1 80.0-120 Zinc ug/L 1000 933 93.3 80.0-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659940 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909657-4 R3909657-5 MS MSD L1601527-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 1000 1000 967 982 96.7 98.2 75.0-125 1.62 20 Arsenic ug/L ND 1000 1000 940 925 94.0 92.5 75.0-125 1.68 20 Barium ug/L 43.7 1000 1000 1040 1030 99.7 99.0 75.0-125 0.718 20 Beryllium ug/L ND 1000 1000 965 957 96.5 95.7 75.0-125 0.867 20 Cadmium ug/L ND 1000 1000 975 965 97.5 96.5 75.0-125 1.04 20 Chromium ug/L ND 1000 1000 959 958 95.9 95.8 75.0-125 0.147 20 Cobalt ug/L ND 1000 1000 966 957 96.6 95.7 75.0-125 0.933 20 Copper ug/L 22.3 1000 1000 999 986 97.7 96.4 75.0-125 1.26 20 Lead ug/L ND 1000 1000 960 953 96.0 95.3 75.0-125 0.733 20 Nickel ug/L 3.28 1000 1000 957 950 95.4 94.7 75.0-125 0.753 20 Selenium ug/L ND 1000 1000 956 951 95.6 95.1 75.0-125 0.509 20 Silver ug/L ND 200 200 179 179 89.6 89.5 75.0-125 0.089 20 Vanadium ug/L ND 1000 1000 977 968 97.7 96.8 75.0-125 0.914 20 Zinc ug/L ND 1000 1000 948 938 94.8 93.8 75.0-125 1.04 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 QC Batch: 2035938 Analysis Method: EPA 6020B QC Batch Method: 3015 Analysis Description: Metals (ICPMS) 6020B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659940001, 92659940002 METHOD BLANK: R3909560-1 Matrix: Water Associated Lab Samples: 92659940001, 92659940002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L 0.172J 2.00 0.121 04/05/2312:01 J LABORATORY CONTROL SAMPLE: R3909560-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 50.0 48.4 96.7 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909560-4 R3909560-5 MS MSD L1601349-02 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 50.0 50.0 48.2 50.0 96.5 100 75.0-125 3.58 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 QC Batch: 765918 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659940001 METHOD BLANK: 3976746 Associated Lab Samples: 92659940001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/06/23 00:45 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/06/23 00:45 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/06/23 00:45 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/06/23 00:45 1,1-Dichloroethane ug/L ND 1.0 0.37 04/06/23 00:45 1,1-Dichloroethene ug/L ND 1.0 0.35 04/06/23 00:45 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/06/23 00:45 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/06/23 00:45 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/06/23 00:45 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/06/23 00:45 1,2-Dichloroethane ug/L ND 1.0 0.32 04/06/23 00:45 1,2-Dichloropropane ug/L ND 1.0 0.36 04/06/23 00:45 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/06/23 00:45 2-Butanone (MEK) ug/L ND 5.0 4.0 04/06/23 00:45 2-Hexanone ug/L ND 5.0 0.48 04/06/23 00:45 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/06/23 00:45 Acetone ug/L ND 25.0 5.1 04/06/23 00:45 Acrylonitrile ug/L ND 10.0 1.8 04/06/23 00:45 Benzene ug/L ND 1.0 0.34 04/06/23 00:45 Bromochloromethane ug/L ND 1.0 0.47 04/06/23 00:45 Bromodichloromethane ug/L ND 1.0 0.31 04/06/23 00:45 Bromoform ug/L ND 1.0 0.34 04/06/23 00:45 Bromomethane ug/L ND 2.0 1.7 04/06/23 00:45 v2 Carbon disulfide ug/L ND 2.0 0.36 04/06/23 00:45 Carbon tetrachloride ug/L ND 1.0 0.33 04/06/23 00:45 Chlorobenzene ug/L ND 1.0 0.28 04/06/23 00:45 Chloroethane ug/L ND 1.0 0.65 04/06/23 00:45 Chloroform ug/L ND 1.0 0.43 04/06/23 00:45 Chloromethane ug/L ND 1.0 0.54 04/06/23 00:45 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/06/23 00:45 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/06/23 00:45 Dibromochloromethane ug/L ND 1.0 0.36 04/06/23 00:45 Dibromomethane ug/L ND 1.0 0.39 04/06/23 00:45 Ethylbenzene ug/L ND 1.0 0.30 04/06/23 00:45 lodomethane ug/L ND 20.0 9.7 04/06/23 00:45 IL,v2 Methylene Chloride ug/L 3.8J 5.0 2.0 04/06/23 00:45 v1 Styrene ug/L ND 1.0 0.29 04/06/23 00:45 Tetrachloroethene ug/L ND 1.0 0.29 04/06/23 00:45 Toluene ug/L ND 1.0 0.24 04/06/23 00:45 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/06/23 00:45 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 METHOD BLANK: 3976746 Associated Lab Samples: 92659940001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 04/06/23 00:45 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 04/06/23 00:45 Trichloroethene ug/L ND 1.0 0.38 04/06/23 00:45 Trichlorofluoromethane ug/L ND 1.0 0.30 04/06/23 00:45 Vinyl acetate ug/L ND 2.0 1.3 04/06/23 00:45 Vinyl chloride ug/L ND 1.0 0.39 04/06/23 00:45 Xylene (Total) ug/L ND 1.0 0.34 04/06/23 00:45 1,2-Dichloroethane-d4 (S) % 104 70-130 04/06/23 00:45 4-Bromofluorobenzene (S) % 99 70-130 04/06/23 00:45 Toluene-d8 (S) % 101 70-130 04/06/23 00:45 LABORATORY CONTROL SAMPLE: Parameter 3976747 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 21.4 107 70-130 1,1,1-Trichloroethane ug/L 20 19.2 96 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.8 109 70-130 1,1,2-Trichloroethane ug/L 20 21.5 108 70-130 1,1-Dichloroethane ug/L 20 18.9 95 70-130 1,1-Dichloroethene ug/L 20 20.5 103 70-130 1,2,3-Trichloropropane ug/L 20 20.5 103 70-130 1,2-Dibromo-3-chloropropane ug/L 20 21.9 110 70-131 1,2-Dibromoethane (EDB) ug/L 20 21.3 107 70-130 1,2-Dichlorobenzene ug/L 20 21.3 106 70-130 1,2-Dichloroethane ug/L 20 20.0 100 70-130 1,2-Dichloropropane ug/L 20 20.1 101 70-130 1,4-Dichlorobenzene ug/L 20 21.0 105 70-130 2-Butanone (MEK) ug/L 40 38.1 95 70-134 2-Hexanone ug/L 40 43.0 108 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 41.3 103 70-130 Acetone ug/L 40 38.6 96 70-133 Acrylonitrile ug/L 100 97.1 97 70-130 Benzene ug/L 20 18.9 94 70-130 Bromochloromethane ug/L 20 20.2 101 70-130 Bromodichloromethane ug/L 20 19.8 99 70-130 Bromoform ug/L 20 21.1 106 70-130 Bromomethane ug/L 20 15.5 78 45-151 v3 Carbon disulfide ug/L 20 19.2 96 70-130 Carbon tetrachloride ug/L 20 18.7 93 70-130 Chlorobenzene ug/L 20 20.3 101 70-130 Chloroethane ug/L 20 21.1 106 39-152 Chloroform ug/L 20 19.4 97 70-130 Chloromethane ug/L 20 19.3 97 58-130 cis-1,2-Dichloroethene ug/L 20 19.3 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 LABORATORY CONTROL SAMPLE: 3976747 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 20 19.6 98 70-130 Dibromochloromethane ug/L 20 21.0 105 70-130 Dibromomethane ug/L 20 20.0 100 70-130 Ethylbenzene ug/L 20 19.9 99 70-130 lodomethane ug/L 40 31.8 79 53-141 IL,v3 Methylene Chloride ug/L 20 45.8 229 66-130 L1,v1 Styrene ug/L 20 21.1 105 70-130 Tetrachloroethene ug/L 20 20.2 101 70-130 Toluene ug/L 20 19.4 97 70-130 trans-1,2-Dichloroethene ug/L 20 19.2 96 70-130 trans- 1,3-Dichloropropene ug/L 20 19.8 99 70-130 trans-1,4-Dichloro-2-butene ug/L 20 20.8 104 57-185 Trichloroethene ug/L 20 19.4 97 70-130 Trichlorofluoromethane ug/L 20 18.6 93 62-130 Vinyl acetate ug/L 40 37.7 94 70-144 Vinyl chloride ug/L 20 16.0 80 62-130 Xylene (Total) ug/L 60 59.9 100 70-130 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: Parameter 3976749 Units 92659774035 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.3 106 70-141 1,1,1-Trichloroethane ug/L ND 20 21.9 109 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 24.2 121 69-142 1,1,2-Trichloroethane ug/L ND 20 23.0 115 70-138 1,1-Dichloroethane ug/L ND 20 20.7 103 70-150 1,1-Dichloroethene ug/L ND 20 20.7 104 70-156 1,2,3-Trichloropropane ug/L ND 20 22.6 113 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 21.8 109 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 21.8 109 70-138 1,2-Dichlorobenzene ug/L ND 20 22.7 114 70-141 1,2-Dichloroethane ug/L ND 20 23.1 115 69-143 1,2-Dichloropropene ug/L ND 20 22.1 111 68-156 1,4-Dichlorobenzene ug/L ND 20 21.5 108 70-142 2-Butanone (MEK) ug/L ND 40 51.0 127 60-157 2-Hexanone ug/L ND 40 48.6 121 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 49.4 123 70-141 Acetone ug/L ND 40 46.0 115 58-157 Acrylonitrile ug/L ND 100 116 116 69-147 Benzene ug/L ND 20 21.3 107 70-142 Bromochloromethane ug/L ND 20 20.6 103 70-146 Bromodichloromethane ug/L ND 20 21.6 108 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 MATRIX SPIKE SAMPLE: Parameter 3976749 Units 92659774035 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromoform ug/L ND 20 19.8 99 64-140 Bromomethane ug/L ND 20 17.5 87 28-192 v3 Carbon disulfide ug/L ND 20 19.3 97 70-151 Carbon tetrachloride ug/L ND 20 20.4 102 70-148 Chlorobenzene ug/L ND 20 21.4 107 70-141 Chloroethane ug/L ND 20 22.2 111 58-191 Chloroform ug/L ND 20 22.1 110 70-148 Chloromethane ug/L ND 20 20.8 104 43-162 cis-1,2-Dichloroethene ug/L ND 20 21.9 110 68-151 cis-1,3-Dichloropropene ug/L ND 20 20.8 104 70-139 Dibromochloromethane ug/L ND 20 20.2 101 70-144 Dibromomethane ug/L ND 20 20.1 101 70-139 Ethylbenzene ug/L ND 20 22.0 110 70-143 lodomethane ug/L ND 40 36.6 91 35-171 v3 Methylene Chloride ug/L ND 20 20.3 83 62-149 v1 Styrene ug/L ND 20 22.0 110 70-143 Tetrachloroethene ug/L ND 20 19.2 96 70-145 Toluene ug/L ND 20 21.7 108 70-142 trans-1,2-Dichloroethene ug/L ND 20 21.0 105 70-151 trans- 1,3-Dichloropropene ug/L ND 20 21.5 107 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 25.7 129 51-159 Trichloroethene ug/L ND 20 20.7 103 62-146 Trichlorofluoromethane ug/L ND 20 20.9 104 63-153 Vinyl acetate ug/L ND 40 44.7 112 61-162 Vinyl chloride ug/L ND 20 17.5 88 61-163 Xylene (Total) ug/L ND 60 64.4 107 70-143 1,2-Dichloroethane-d4 (S) % 111 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8(S) % 101 70-130 SAMPLE DUPLICATE: 3976748 Parameter Units 92659774029 Result Dup Result RPD Max RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 SAMPLE DUPLICATE: 3976748 Parameter Units 92659774029 Result Dup Result RPD Max RPD 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 v2 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 v2 Methylene Chloride ug/L ND ND 30 v1 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 Xylene (Total) ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 108 100 4-Bromofluorobenzene (S) % 96 101 Toluene-d8 (S) % 99 102 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 QC Batch: 766317 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659940002 METHOD BLANK: 3978969 Associated Lab Samples: 92659940002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/07/23 02:20 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/07/23 02:20 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/07/23 02:20 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/07/23 02:20 1,1-Dichloroethane ug/L ND 1.0 0.37 04/07/23 02:20 1,1-Dichloroethene ug/L ND 1.0 0.35 04/07/23 02:20 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/07/23 02:20 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/07/23 02:20 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/07/23 02:20 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/07/23 02:20 1,2-Dichloroethane ug/L ND 1.0 0.32 04/07/23 02:20 1,2-Dichloropropane ug/L ND 1.0 0.36 04/07/23 02:20 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/07/23 02:20 2-Butanone (MEK) ug/L ND 5.0 4.0 04/07/23 02:20 2-Hexanone ug/L ND 5.0 0.48 04/07/23 02:20 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/07/23 02:20 Acetone ug/L ND 25.0 5.1 04/07/23 02:20 Acrylonitrile ug/L ND 10.0 1.8 04/07/23 02:20 Benzene ug/L ND 1.0 0.34 04/07/23 02:20 Bromochloromethane ug/L ND 1.0 0.47 04/07/23 02:20 Bromodichloromethane ug/L ND 1.0 0.31 04/07/23 02:20 Bromoform ug/L ND 1.0 0.34 04/07/23 02:20 Bromomethane ug/L ND 2.0 1.7 04/07/23 02:20 Carbon disulfide ug/L ND 2.0 0.36 04/07/23 02:20 Carbon tetrachloride ug/L ND 1.0 0.33 04/07/23 02:20 Chlorobenzene ug/L ND 1.0 0.28 04/07/23 02:20 Chloroethane ug/L ND 1.0 0.65 04/07/23 02:20 Chloroform ug/L ND 1.0 0.43 04/07/23 02:20 Chloromethane ug/L ND 1.0 0.54 04/07/23 02:20 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/07/23 02:20 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/07/23 02:20 Dibromochloromethane ug/L ND 1.0 0.36 04/07/23 02:20 Dibromomethane ug/L ND 1.0 0.39 04/07/23 02:20 Ethylbenzene ug/L ND 1.0 0.30 04/07/23 02:20 lodomethane ug/L ND 20.0 9.7 04/07/23 02:20 Methylene Chloride ug/L ND 5.0 2.0 04/07/23 02:20 v1 Styrene ug/L ND 1.0 0.29 04/07/23 02:20 Tetrachloroethene ug/L ND 1.0 0.29 04/07/23 02:20 Toluene ug/L ND 1.0 0.24 04/07/23 02:20 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/07/23 02:20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 METHOD BLANK: 3978969 Associated Lab Samples: 92659940002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL trans- 1,3-Dichloropropene ug/L ND 1.0 trans-1,4-Dichloro-2-butene ug/L ND 1.0 Trichloroethene ug/L ND 1.0 Trichlorofluoromethane ug/L ND 1.0 Vinyl acetate ug/L ND 2.0 Vinyl chloride ug/L ND 1.0 Xylene (Total) ug/L ND 1.0 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8(S) % 102 70-130 Analyzed 0.36 04/07/23 02:20 0.56 04/07/23 02:20 0.38 04/07/23 02:20 0.30 04/07/23 02:20 1.3 04/07/23 02:20 0.39 04/07/23 02:20 0.34 04/07/23 02:20 04/07/23 02:20 04/07/23 02:20 04/07/23 02:20 LABORATORY CONTROL SAMPLE: Parameter 3978970 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 20 19.8 99 70-130 1,1,1-Trichloroethane ug/L 20 20.2 101 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.8 109 70-130 1,1,2-Trichloroethane ug/L 20 21.2 106 70-130 1,1-Dichloroethane ug/L 20 19.5 98 70-130 1,1-Dichloroethene ug/L 20 19.5 97 70-130 1,2,3-Trichloropropane ug/L 20 20.6 103 70-130 1,2-Dibromo-3-chloropropane ug/L 20 20.0 100 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.1 100 70-130 1,2-Dichlorobenzene ug/L 20 20.9 105 70-130 1,2-Dichloroethane ug/L 20 21.4 107 70-130 1,2-Dichloropropane ug/L 20 20.5 103 70-130 1,4-Dichlorobenzene ug/L 20 19.6 98 70-130 2-Butanone (MEK) ug/L 40 43.2 108 70-134 2-Hexanone ug/L 40 42.6 107 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 43.1 108 70-130 Acetone ug/L 40 42.2 106 70-133 Acrylonitrile ug/L 100 106 106 70-130 Benzene ug/L 20 19.6 98 70-130 Bromochloromethane ug/L 20 19.9 99 70-130 Bromodichloromethane ug/L 20 19.9 100 70-130 Bromoform ug/L 20 18.7 94 70-130 Bromomethane ug/L 20 16.0 80 45-151 Carbon disulfide ug/L 20 16.4 82 70-130 Carbon tetrachloride ug/L 20 18.1 90 70-130 Chlorobenzene ug/L 20 19.7 99 70-130 Chloroethane ug/L 20 20.4 102 39-152 Chloroform ug/L 20 20.9 104 70-130 Chloromethane ug/L 20 20.1 100 58-130 cis-1,2-Dichloroethene ug/L 20 20.1 100 70-130 Qualifiers v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 LABORATORY CONTROL SAMPLE: 3978970 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 20 18.9 95 70-130 Dibromochloromethane ug/L 20 19.4 97 70-130 Dibromomethane ug/L 20 19.0 95 70-130 Ethylbenzene ug/L 20 19.7 98 70-130 lodomethane ug/L 40 33.6 84 53-141 Methylene Chloride ug/L 20 30.2 151 66-130 L1,v1 Styrene ug/L 20 19.3 96 70-130 Tetrachloroethene ug/L 20 18.4 92 70-130 Toluene ug/L 20 19.9 100 70-130 trans-1,2-Dichloroethene ug/L 20 19.1 95 70-130 trans- 1,3-Dichloropropene ug/L 20 19.7 99 70-130 trans-1,4-Dichloro-2-butene ug/L 20 22.9 114 57-185 Trichloroethene ug/L 20 18.5 93 70-130 Trichlorofluoromethane ug/L 20 18.5 92 62-130 Vinyl acetate ug/L 40 41.6 104 70-144 Vinyl chloride ug/L 20 15.8 79 62-130 v3 Xylene (Total) ug/L 60 57.9 97 70-130 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 3978972 Units 92659774022 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 22.0 110 70-141 1,1,1-Trichloroethane ug/L ND 20 21.5 108 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 23.2 116 69-142 1,1,2-Trichloroethane ug/L ND 20 22.0 110 70-138 1,1-Dichloroethane ug/L ND 20 21.7 109 70-150 1,1-Dichloroethene ug/L ND 20 22.2 111 70-156 1,2,3-Trichloropropane ug/L ND 20 22.4 112 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 23.2 116 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 22.6 113 70-138 1,2-Dichlorobenzene ug/L ND 20 23.0 115 70-141 1,2-Dichloroethane ug/L ND 20 21.8 109 69-143 1,2-Dichloropropene ug/L ND 20 22.4 112 68-156 1,4-Dichlorobenzene ug/L ND 20 22.8 114 70-142 2-Butanone (MEK) ug/L ND 40 44.8 112 60-157 2-Hexanone ug/L ND 40 49.4 123 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 46.3 116 70-141 Acetone ug/L ND 40 42.6 106 58-157 Acrylonitrile ug/L ND 100 107 107 69-147 Benzene ug/L ND 20 21.2 106 70-142 Bromochloromethane ug/L ND 20 21.9 110 70-146 Bromodichloromethane ug/L ND 20 21.1 105 70-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 MATRIX SPIKE SAMPLE: 3978972 92659774022 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromoform ug/L ND 20 21.2 106 64-140 Bromomethane ug/L ND 20 14.7 73 28-192 v3 Carbon disulfide ug/L ND 20 20.2 101 70-151 Carbon tetrachloride ug/L ND 20 21.3 106 70-148 Chlorobenzene ug/L ND 20 22.3 111 70-141 Chloroethane ug/L ND 20 22.0 110 58-191 Chloroform ug/L ND 20 21.2 106 70-148 Chloromethane ug/L ND 20 16.2 81 43-162 cis-1,2-Dichloroethene ug/L ND 20 21.7 108 68-151 cis-1,3-Dichloropropene ug/L ND 20 21.3 106 70-139 Dibromochloromethane ug/L ND 20 21.7 109 70-144 Dibromomethane ug/L ND 20 20.6 103 70-139 Ethylbenzene ug/L ND 20 22.0 110 70-143 lodomethane ug/L ND 40 28.8 72 35-171 IL,v3 Methylene Chloride ug/L ND 20 27.2 136 62-149 v1 Styrene ug/L ND 20 22.9 115 70-143 Tetrachloroethene ug/L ND 20 21.5 107 70-145 Toluene ug/L ND 20 21.6 108 70-142 trans-1,2-Dichloroethene ug/L ND 20 22.0 110 70-151 trans- 1,3-Dichloropropene ug/L ND 20 21.6 108 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 21.2 106 51-159 Trichloroethene ug/L ND 20 21.3 106 62-146 Trichlorofluoromethane ug/L ND 20 19.5 98 63-153 Vinyl acetate ug/L ND 40 44.9 112 61-162 Vinyl chloride ug/L ND 20 15.2 76 61-163 Xylene (Total) ug/L ND 60 67.1 112 70-143 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 3978971 92659945004 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 SAMPLE DUPLICATE: 3978971 Parameter Units 92659945004 Result 1,4-Dichlorobenzene ug/L ND 2-Butanone (MEK) ug/L ND 2-Hexanone ug/L ND 4-Methyl-2-pentanone (MIBK) ug/L ND Acetone ug/L ND Acrylonitrile ug/L ND Benzene ug/L ND Bromochloromethane ug/L ND Bromodichloromethane ug/L ND Bromoform ug/L ND Bromomethane ug/L ND Carbon disulfide ug/L ND Carbon tetrachloride ug/L ND Chlorobenzene ug/L ND Chloroethane ug/L ND Chloroform ug/L ND Chloromethane ug/L ND cis-1,2-Dichloroethene ug/L ND cis-1,3-Dichloropropene ug/L ND Dibromochloromethane ug/L ND Dibromomethane ug/L ND Ethylbenzene ug/L ND lodomethane ug/L ND Methylene Chloride ug/L ND Styrene ug/L ND Tetrachloroethene ug/L ND Toluene ug/L ND trans-1,2-Dichloroethene ug/L ND trans- 1,3-Dichloropropene ug/L ND trans-1,4-Dichloro-2-butene ug/L ND Trichloroethene ug/L ND Trichlorofluoromethane ug/L ND Vinyl acetate ug/L ND Vinyl chloride ug/L ND Xylene (Total) ug/L ND 1,2-Dichloroethane-d4 (S) % 104 4-Bromofluorobenzene (S) % 97 Toluene-d8 (S) % 103 Dup Result RPD Max RPD Qualifiers ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 v2 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 I L, v2 ND 30 v1 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 ND 30 107 98 101 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 28 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 QC Batch: 766432 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659940001, 92659940002 METHOD BLANK: 3979517 Matrix: Water Associated Lab Samples: 92659940001, 92659940002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 04/06/23 18:46 1,2-Dichloroethane-d4 (S) % 103 67-130 04/06/23 18:46 Toluene-d8 (S) % 101 70-130 04/06/23 18:46 LABORATORY CONTROL SAMPLE: 3979518 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 19.6 98 70-130 1,2-Dichloroethane-d4 (S) % 103 67-130 Toluene-d8 (S) % 102 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979519 3979520 MS MSD 92659681001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 4.6 20 20 21.1 20.8 82 81 55-137 2 30 H1 1,2-Dichloroethane-d4 (S) % 103 103 67-130 30 Toluene-d8(S) % 121 120 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. WORKORDER QUALIFIERS WO: 92659940 [1] ANALYTE QUALIFIERS Analyte was detected in the associated method blank. C9 Common Laboratory Contaminant. H1 Analysis conducted outside the EPA method holding time H5 Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GM1.005-OXFORD LANDFILL UNIT 2 Pace Project No.: 92659940 ANALYTE QUALIFIERS v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/12/2023 07:28 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GM1.005-OXFORD LANDFILL UNIT 2 92659940 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92659940001 SW-3 3015 2035939 EPA 6010D 2035939 92659940002 SW-4 3015 2035939 EPA 6010D 2035939 92659940001 SW-3 3015 2035938 EPA 6020B 2035938 92659940002 SW-4 3015 2035938 EPA 6020B 2035938 92659940001 SW-3 EPA 8260D 765918 92659940002 SW-4 EPA 8260D 766317 92659940001 SW-3 EPA 8260D Mod. 766432 92659940002 SW-4 EPA 8260D Mod. 766432 92659940001 SW-3 SM2340B 2035939 SM2340-97 2035939 92659940002 SW-4 SM2340B 2035939 SM2340-97 2035939 Date: 04/12/2023 07:28 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 28 siau jinuda J! Id s JO Q 1401 firur-1 -sbifn iblailitham RIffn WON :m0iogs A 6�6 A439119W 1340M A3NVd3N3310 31dWVS1&LN3WV403 VM VM ONO .04-Cf-- SU-0 LitiagaiA -gepS ApOjS(!:).4Uej8 d131 Lluasojil XveII3.d lij, --701— V/N 61 oy Ej 5aAa-- NW9;54-) WIA VOA MI 029TSPL'aH Cna aldLues 8 VN0-- plall sajow.gs.�AMJeLr. Pawns IQ14 V/M 0 V/N E) MO: 0v_Cr IOAQ( S13;kq 4PAM 519UPPIU03 prwo:) 1:1 ONO- VIA 19 "WnIDA JUB13U . IfIS, V/N ❑ ON Op RA VIN ON SAhn- P143H 1104S ..z V/N ON 4,lW[L;p I OF S a;4 tuts .1 WN rN 0 URI' FNE ",n4 pue (jemeH a4!pnpul 'Alleuallidie'lul unpeg seq sspr6id OJ lJoW3iiJ.1 uo sold tU9s'e44a;i.J!; dw al j a Ino $a JdWOS q.9 91,guipaij aAcqu aq pinoqs dwoi guON(:j onla [3 -35 An 'AN UNIPA -6VO2 -DUM103ifib R U1 PIRLfIgNia Sajdwgs PIC3 ...910wes Jm;" �.'YiN ROSY44ulnUs vasn Oupi Ja 1,>ejzqnS/ppv WWOJL J81003 . lam M :a,!1*16 ild4 ,ze-Rayb. :avurmin 4wia4i w i In S dejM,8jqqr' 0 Aut-am . t I T — r--S-ffkfBl U 03 YU 111 [WWI WwBd SPhOOMO ONt4 52.ka APM111 slvaS ON SBA leas Apajmj ObsesgEs pspjaupwto SdSb Sd rl F1 XX 3 P4 R I jsjjna3 u L7LAV � -7.1 H PAY ji vt� C]Ujj!ASJ9U19M 10 ULijjV' C]8jjjAS31UE43GW nqojaft❑ 0111AS10JUn}1 C] Poomumq) Ouiqpj; tlWOW wv, -091:9 ZZOOOT/T I 811fd -R-Mi . Q . . jdjaaajj uodn uompuoo9jdWUS-ZOA S9OO-1NnH-1NHd-ANR :01111 #00 :)acie 26-of.98 'vauleaunIoaiimu)'dwa}IaIra 'anl; AJOSaid ->laajjo}u{'Flogjo3np 'a•y) a}[gp uoge3U.tjja::aNja E�IIa:e3uUahs a+tl ai luaS,aq III M'w]n4stU1 to hdo3 e'saldtuesaAueiidW4] 2Id ;a]ON 11101 Popp. an)IQivasaad 0IP"QWV pa35nlpe 0011MOSOA.0tULL patsnjpe U01jeniasaid o;eo 1dle+3ai uadn Hd ax1junaasaid jo adhi p)-a)dtuey sajduiES-panJasaJd 10) 201 1VOWISMOV Hd I zi of s s - z s 4 E C Gi Ip :C SS{{yy Ll D. Gi O p W ••, 1 � v � •K ci X • V fl w •ta. < {[,1 p.. C _ G+ LO W. w 'i= 3e �b r �. p � Tf• i r•. _ pp m Q� `po I moo r ' (�' • p C O ID�r O L4 p.. .b p N.;r{. ! H L/? ,. 'iQ to N r w v v C << y r r—. r r r r a y- r r -• ' ' v ' �� r'1 e"i' C aZi, S r W v. 'rci: r� •Yl, . FL Z ryy :.� rl 7 1545 pj 99 - F au�ao�y� aa) sa�rraal� Parwesaadun � ��a43�� � sapoq jo:agwnu 1sil 03.9 Knq 1011,e4 w01309 £Z/LO/00 : 9120 ann OWl : Wd sajdua s Uopm-tasaid ao}; a3ue,t e1ue4dO2)0 941 u1411M 0ir6659Z 6 ' #Ors # oaf OJd PUB palgllan.sl° Uopoulaolyaap jo/pue tad j! xoq ;9 04 dol4jew X3343 . ;8 ZZ4Z%bTj11 :e1$p ent�aejy� Idlaaell uodn UO!jjpUoa ajdu.lfg-ZOA £8O0=6NnH-WHJ-ANR :0R1 . #00 c z E s a Pelul (NIA) E3 ._ MOOS Kpolsro WA) ' } Sal o;aAla�az� } (NA) s-amj IEnp�Suz a i can a ul dW�l L 01 l �G ruejg di I euexul❑ Y' l E x' w 9BBupjeH+slelu;N I ddy �- � '� o � i�lS 09iB Fq euexalp p'l � u 89TA Fq 3oA I ddv a. cc Y , .5 �7 " HOeti € tOSLH V �y' Pevac-dun ,e = a E .� 61i3N1YiN0? �a a u to _ d ci � a a � � a: SpFL�377��,1Yd1Y3131dfYY5 W ....,_� �-- � a qa� W It U) sn F c7� l R e r~n N O f j1 E � � �'•f n tdil?i? 9�k1F]=J) 3dA13ldSYYS .Q .,,�' _ UP] n Sep- p.:eA aas) 346a Xrb1Vl'l 0 �+ '�' a o m �, i4-• � H Z iti ij tt 33 i rA ��35(cSlo3aor O i x L '� g r C g jj m � h q c3 L" Z Li q 0 W ILI • :N M v 'ao a o'� a Page 28 of 28 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 20, 2023 Jeffrey 011ison Hart & Hickman 3921 Sunset Ridge Rd. Ste. 301 Raleigh, NC 27607 RE: Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Dear Jeffrey 011ison: Enclosed are the analytical results for sample(s) received by the laboratory on March 30, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Gulf Coast • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, �+ Taylor M Cannon taylor.cannon@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 76 laneAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Gulf Coast 7979 Innovation Park Drive, Baton Rouge, LA 70820 Arkansas Certification #: 88-0655 DoD ELAP Certification M 6429-01 Florida Certification #: E87854 Illinois Certification #: 004585 Kansas Certification #: E-10354 Louisiana/LELAP Certification #: 01955 North Carolina Certification M 618 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21LA 2926.01 A2LA-ISO 17025 Certification #: 1461.01 A2LA-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 North Dakota Certification #: R-195 Oklahoma Certification #: 2019-101 South Carolina Certification #: 73006001 Texas Certification #: T104704178-19-11 USDA Soil Permit # P330-19-00209 Virginia Certification #: 460215 Washington Certification #: C929 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Lab ID Sample ID Matrix Date Collected Date Received 92659639001 MW-5R Water 03/29/2314:05 03/30/23 10:00 92659639002 MW-7 Water 03/29/2315:09 03/30/23 10:00 92659639003 FIELD BLANK UNIT 1 Water 03/29/23 16:45 03/30/23 10:00 92659639004 MW-3RR Water 03/29/2316:30 03/30/23 10:00 92659639005 TRIP BLANK Water 03/29/23 00:00 03/30/23 10:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: GM1.004 OXFORD LANDFILL UNIT 1 92659639 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92659639001 MW-5R EPA8151A NWH 5 PAN EPA 8081 B SEM 21 PASI-C EPA 8082A SEM 8 PASI-C RSK-175 LMB 1 GCLA EPA 601 OD SPL 17 PAN EPA 6020E JPD 1 PAN EPA 7470A SRT 1 PAN EPA 8270E PKS 111 PASI-C EPA 8260D Mod. TEG 3 PASI-C EPA 8260D CL 68 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 RVS 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92659639002 MW-7 EPA8151A NWH 5 PAN EPA 8081 B SEM 21 PASI-C EPA 8082A SEM 8 PASI-C RSK-175 LMB 1 GCLA EPA 601 OD SPL 17 PAN EPA 6020E JPD 1 PAN EPA 7470A SRT 1 PAN EPA 8270E PKS 111 PASI-C EPA 8260D Mod. TEG 3 PASI-C EPA 8260D CL 68 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 RVS 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92659639003 FIELD BLANK UNIT 1 EPA8151A NWH 5 PAN EPA 8081 B SEM 21 PASI-C EPA 8082A SEM 8 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Lab ID Sample ID Method Analysts Analytes Reported Laboratory RSK-175 LMB 1 GCLA EPA 601 OD SPL 17 PAN EPA 6020E JPD 1 PAN EPA 7470A SRT 1 PAN EPA 8270E PKS 111 PASI-C EPA 8260D Mod. TEG 3 PASI-C EPA 8260D CL 68 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 RVS 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A SM 4500-CN-E-2016 ANM 1 PASI-A 92659639004 MW-3RR EPA 601 OD SPL 16 PAN EPA 6020E JPD 1 PAN EPA 7470A AKB 1 PAN EPA 8260D CL 51 PASI-C EPA 8260D Mod. TEG 3 PASI-C SM 2320B-2011 SMS 1 PASI-A SM 2540C-2015 RVS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 ANM 1 PASI-A 92659639005 TRIP BLANK EPA 8260D Mod. TEG 3 PASI-C EPA 8260D CL 67 PASI-C GCLA = Pace Analytical Gulf Coast PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 04/04/23 14:45 04/06/23 12:00 94-75-7 R1 Dinoseb ND ug/L 2.00 0.250 1 04/04/23 14:45 04/06/23 12:00 88-85-7 2,4,5-T ND ug/L 2.00 0.258 1 04/04/23 14:45 04/06/23 12:00 93-76-5 R1 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 04/04/23 14:45 04/06/23 12:00 93-72-1 R1 Surrogates 2,4-DCAA (S) 80.2 % 14.0-158 1 04/04/23 14:45 04/06/23 12:00 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:05 309-00-2 alpha-BHC ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:05 319-84-6 beta-BHC ND ug/L 0.042 0.041 1 04/05/23 11:13 04/06/23 15:05 319-85-7 delta-BHC ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:05 319-86-8 gamma-BHC (Lindane) ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:05 58-89-9 Chlordane (Technical) ND ug/L 0.42 0.13 1 04/05/23 11:13 04/06/23 15:05 57-74-9 4,4'-DDD ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:05 72-54-8 4,4'-DDE ND ug/L 0.042 0.020 1 04/05/23 11:13 04/06/23 15:05 72-55-9 4,4'-DDT ND ug/L 0.042 0.022 1 04/05/23 11:13 04/06/23 15:05 50-29-3 Dieldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:05 60-57-1 Endosulfan I ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:05 959-98-8 Endosulfan II ND ug/L 0.042 0.013 1 04/05/23 11:13 04/06/23 15:05 33213-65-9 Endosulfan sulfate ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:05 1031-07-8 Endrin ND ug/L 0.042 0.015 1 04/05/23 11:13 04/06/23 15:05 72-20-8 Endrin aldehyde ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:05 7421-93-4 Heptachlor ND ug/L 0.042 0.016 1 04/05/23 11:13 04/06/23 15:05 76-44-8 Heptachlor epoxide ND ug/L 0.042 0.024 1 04/05/23 11:13 04/06/23 15:05 1024-57-3 Methoxychlor ND ug/L 0.12 0.035 1 04/05/23 11:13 04/06/23 15:05 72-43-5 Toxaphene ND ug/L 0.42 0.18 1 04/05/23 11:13 04/06/23 15:05 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 116 % 10-182 1 04/05/23 11:13 04/06/23 15:05 877-09-8 Decachlorobiphenyl (S) 131 % 10-200 1 04/05/23 11:13 04/06/23 15:05 2051-24-3 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) ND ug/L 0.42 0.18 1 04/14/23 11:02 04/17/23 14:45 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.42 0.19 1 04/14/23 11:02 04/17/23 14:45 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.42 0.19 1 04/14/23 11:02 04/17/23 14:45 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.21 1 04/14/23 11:02 04/17/23 14:45 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.24 1 04/14/23 11:02 04/17/23 14:45 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.18 1 04/14/23 11:02 04/17/23 14:45 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.13 1 04/14/23 11:02 04/17/23 14:45 11096-82-5 Surrogates Decachlorobiphenyl (S) 115 % 10-193 1 04/14/23 11:02 04/17/23 14:45 2051-24-3 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane 31 ug/L 5.0 2.0 1 04/10/23 09:29 74-82-8 Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/03/23 09:02 04/03/23 19:40 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/03/23 09:02 04/03/23 19:40 7440-38-2 Barium 44.6 ug/L 5.00 0.736 1 04/03/23 09:02 04/03/23 19:40 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/03/23 09:02 04/03/23 19:40 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/03/23 09:02 04/03/23 19:40 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/03/23 09:02 04/03/23 19:40 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/03/23 09:02 04/03/23 19:40 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/03/23 09:02 04/03/23 19:40 7440-50-8 Iron 292 ug/L 100 18.0 1 04/03/23 09:02 04/03/23 19:40 7439-89-6 Lead ND ug/L 6.00 2.99 1 04/03/23 09:02 04/03/23 19:40 7439-92-1 Manganese 102 ug/L 10.0 0.934 1 04/03/23 09:02 04/03/23 19:40 7439-96-5 Nickel 2.16J ug/L 10.0 1.61 1 04/03/23 09:02 04/03/23 19:40 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/03/23 09:02 04/03/23 19:40 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/03/23 09:02 04/03/23 19:40 7440-22-4 Tin ND ug/L 50.0 4.87 1 04/03/23 09:02 04/03/23 19:40 7440-31-5 Vanadium ND ug/L 20.0 4.99 1 04/03/23 09:02 04/03/23 19:40 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/03/23 09:02 04/03/23 19:40 7440-66-6 Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 01:56 04/05/23 10:45 7440-28-0 Mercury 7470A Analytical Method: EPA 7470A Preparation Method: 7470A Pace National - Mt. Juliet Mercury ND ug/L 0.200 0.100 1 04/04/23 08:56 04/04/23 19:30 7439-97-6 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 8.3 1.7 1 04/04/2318:28 04/06/2319:44 83-32-9 Acenaphthylene ND ug/L 8.3 1.6 1 04/04/2318:28 04/06/2319:44 208-96-8 Acetophenone ND ug/L 8.3 1.2 1 04/04/2318:28 04/06/2319:44 98-86-2 2-Acetylaminofluorene ND ug/L 8.3 3.4 1 04/04/2318:28 04/06/2319:44 53-96-3 4-Aminobiphenyl ND ug/L 8.3 4.0 1 04/04/2318:28 04/06/2319:44 92-67-1 Anthracene ND ug/L 8.3 1.9 1 04/04/2318:28 04/06/2319:44 120-12-7 Benzo(a)anthracene ND ug/L 8.3 2.2 1 04/04/2318:28 04/06/2319:44 56-55-3 Benzo(a)pyrene ND ug/L 8.3 2.3 1 04/04/2318:28 04/06/2319:44 50-32-8 Benzo(b)fluoranthene ND ug/L 8.3 2.2 1 04/04/2318:28 04/06/2319:44 205-99-2 Benzo(g,h,i)perylene ND ug/L 8.3 2.4 1 04/04/2318:28 04/06/2319:44 191-24-2 Benzo(k)fluoranthene ND ug/L 8.3 2.3 1 04/04/2318:28 04/06/2319:44 207-08-9 Benzyl alcohol ND ug/L 16.7 2.4 1 04/04/23 18:28 04/06/23 19:44 100-51-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. J Page 8 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 4-Bromophenylphenyl ether ND ug/L 8.3 1.5 1 04/04/23 18:28 04/06/23 19:44 101-55-3 Butylbenzylphthalate ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 19:44 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 19:44 59-50-7 4-Chloroaniline ND ug/L 16.7 3.0 1 04/04/23 18:28 04/06/23 19:44 106-47-8 Chlorobenzilate ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 19:44 510-15-6 bis(2-Chloroethoxy)methane ND ug/L 8.3 1.5 1 04/04/23 18:28 04/06/23 19:44 111-91-1 bis(2-Chloroethyl) ether ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 111-44-4 2-Chloronaphthalene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 19:44 91-58-7 2-Chlorophenol ND ug/L 8.3 1.0 1 04/04/23 18:28 04/06/23 19:44 95-57-8 4-Chlorophenylphenyl ether ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 19:44 7005-72-3 Chrysene ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 19:44 218-01-9 Diallate ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 19:44 2303-16-4 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 19:44 53-70-3 Dibenzofuran ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 132-64-9 3,3'-Dichlorobenzidine ND ug/L 16.7 6.8 1 04/04/23 18:28 04/06/23 19:44 91-94-1 2,4-Dichlorophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 19:44 120-83-2 2,6-Dichlorophenol ND ug/L 8.3 3.5 1 04/04/23 18:28 04/06/23 19:44 87-65-0 Diethylphthalate ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 19:44 84-66-2 Dimethoate ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 19:44 60-51-5 P-Dimethylaminoazobenzene ND ug/L 4.2 2.0 1 04/04/23 18:28 04/06/23 19:44 60-11-7 IL 7,12-Dimethylbenz(a)anthracene ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 19:44 57-97-6 3,3'-Dimethylbenzidine ND ug/L 41.7 25.9 1 04/04/23 18:28 04/06/23 19:44 119-93-7 IH 2,4-Dimethylphenol ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 19:44 105-67-9 L1 Dimethylphthalate ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 131-11-3 Di-n-butylphthalate ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 16.7 6.5 1 04/04/23 18:28 04/06/23 19:44 534-52-1 v1 1,3-Dinitrobenzene ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 19:44 99-65-0 2,4-Dinitrophenol ND ug/L 41.7 21.7 1 04/04/23 18:28 04/06/23 19:44 51-28-5 2,4-Dinitrotoluene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 19:44 121-14-2 2,6-Dinitrotoluene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 19:44 606-20-2 Di-n-octylphthalate ND ug/L 8.3 3.3 1 04/04/23 18:28 04/06/23 19:44 117-84-0 Diphenylamine ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 19:44 122-39-4 Disulfoton ND ug/L 8.3 3.9 1 04/04/23 18:28 04/06/23 19:44 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 04/04/23 18:28 04/06/23 19:44 117-81-7 Ethyl methanesulfonate ND ug/L 16.7 2.5 1 04/04/23 18:28 04/06/23 19:44 62-50-0 Famphur ND ug/L 8.3 5.1 1 04/04/23 18:28 04/06/23 19:44 52-85-7 Fluoranthene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 206-44-0 Fluorene ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 19:44 86-73-7 Hexachlorobenzene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 118-74-1 Hexachlorocyclopentadiene ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 19:44 77-47-4 Hexachloroethane ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 19:44 67-72-1 Hexachloropropene ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 19:44 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 04/04/23 18:28 04/06/23 19:44 193-39-5 Isodrin ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 19:44 465-73-6 Isophorone ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 19:44 78-59-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Isosafrole ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 19:44 120-58-1 Kepone ND ug/L 16.7 11.8 1 04/04/23 18:28 04/06/23 19:44 143-50-0 Methapyrilene ND ug/L 41.7 14.2 1 04/04/23 18:28 04/06/23 19:44 91-80-5 IH,v1 3-Methylcholanthrene ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 19:44 56-49-5 Methyl methanesulfonate ND ug/L 4.2 2.6 1 04/04/23 18:28 04/06/23 19:44 66-27-3 2-Methylnaphthalene ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 91-57-6 Methyl parathion ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 19:44 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 8.3 1.0 1 04/04/23 18:28 04/06/23 19:44 15831-10-4 1-Naphthalenamine ND ug/L 8.3 5.0 1 04/04/23 18:28 04/06/23 19:44 134-32-7 2-Naphthalenamine ND ug/L 8.3 4.5 1 04/04/23 18:28 04/06/23 19:44 91-59-8 1,4-Naphthoquinone ND ug/L 4.2 3.7 1 04/04/23 18:28 04/06/23 19:44 130-15-4 2-Nitroaniline ND ug/L 16.7 2.5 1 04/04/23 18:28 04/06/23 19:44 88-74-4 3-Nitroaniline ND ug/L 16.7 3.1 1 04/04/23 18:28 04/06/23 19:44 99-09-2 4-Nitroaniline ND ug/L 16.7 4.2 1 04/04/23 18:28 04/06/23 19:44 100-01-6 Nitrobenzene ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 98-95-3 2-Nitrophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 19:44 88-75-5 4-Nitrophenol ND ug/L 41.7 5.5 1 04/04/23 18:28 04/06/23 19:44 100-02-7 5-Nitro-o-toluidine ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 19:44 99-55-8 N-Nitrosodiethylamine ND ug/L 8.3 1.9 1 04/04/23 18:28 04/06/23 19:44 55-18-5 N-Nitrosodimethylamine ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 19:44 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 8.3 1.1 1 04/04/23 18:28 04/06/23 19:44 621-64-7 N-Nitrosodiphenylamine ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 19:44 86-30-6 N-Nitrosomethylethylamine ND ug/L 8.3 6.2 1 04/04/23 18:28 04/06/23 19:44 10595-95-6 N-Nitrosopiperidine ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 19:44 100-75-4 N-Nitrosopyrrolidine ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 19:44 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 19:44 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 8.3 0.96 1 04/04/23 18:28 04/06/23 19:44 108-60-1 Parathion (Ethyl parathion) ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 19:44 56-38-2 Pentachlorobenzene ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 19:44 608-93-5 Pentachloronitrobenzene ND ug/L 8.3 2.7 1 04/04/23 18:28 04/06/23 19:44 82-68-8 Pentachlorophenol ND ug/L 16.7 3.1 1 04/04/23 18:28 04/06/23 19:44 87-86-5 Phenacetin ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 19:44 62-44-2 Phenanthrene ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 19:44 85-01-8 Phenol ND ug/L 8.3 1.1 1 04/04/23 18:28 04/06/23 19:44 108-95-2 p-Phenylenediamine ND ug/L 8.3 8.3 1 04/04/23 18:28 04/06/23 19:44 106-50-3 Phorate ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 19:44 298-02-2 Pronamide ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 19:44 23950-58-5 Pyrene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 19:44 129-00-0 Safrole ND ug/L 8.3 1.9 1 04/04/23 18:28 04/06/23 19:44 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 8.3 3.7 1 04/04/23 18:28 04/06/23 19:44 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 19:44 58-90-2 Thionazin ND ug/L 8.3 2.4 1 04/04/23 18:28 04/06/23 19:44 297-97-2 O-Toluidine ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 19:44 95-53-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2,4,5-Trichlorophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 19:44 95-95-4 2,4,6-Trichlorophenol ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 19:44 88-06-2 1,3,5-Trinitrobenzene ND ug/L 8.3 4.6 1 04/04/23 18:28 04/06/23 19:44 99-35-4 v1 Surrogates Nitrobenzene-d5 (S) 69 % 10-138 1 04/04/23 18:28 04/06/23 19:44 4165-60-0 2-Fluorobiphenyl (S) 59 % 10-130 1 04/04/23 18:28 04/06/23 19:44 321-60-8 Terphenyl-d14 (S) 104 % 19-191 1 04/04/23 18:28 04/06/23 19:44 1718-51-0 Phenol-d6 (S) 39 % 10-130 1 04/04/23 18:28 04/06/23 19:44 13127-88-3 2-Fluorophenol (S) 49 % 10-130 1 04/04/23 18:28 04/06/23 19:44 367-12-4 2,4,6-Tribromophenol (S) 103 % 10-164 1 04/04/23 18:28 04/06/23 19:44 118-79-6 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 58.6 ug/L 2.0 0.86 1 04/05/23 01:42 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 80 % 67-130 1 04/05/23 01:42 17060-07-0 Toluene-d8 (S) 88 % 70-130 1 04/05/23 01:42 2037-26-5 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/01/23 07:04 67-64-1 Acetonitrile ND ug/L 50.0 24.8 1 04/01/23 07:04 75-05-8 Acrolein ND ug/L 10.0 8.5 1 04/01/23 07:04 107-02-8 Acrylonitrile ND ug/L 10.0 1.8 1 04/01/23 07:04 107-13-1 Allyl chloride ND ug/L 2.0 0.50 1 04/01/23 07:04 107-05-1 Benzene ND ug/L 1.0 0.34 1 04/01/23 07:04 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/01/23 07:04 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/01/23 07:04 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/01/23 07:04 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/01/23 07:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/01/23 07:04 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/01/23 07:04 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/01/23 07:04 56-23-5 Chlorobenzene 1.4 ug/L 1.0 0.28 1 04/01/23 07:04 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/01/23 07:04 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/01/23 07:04 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/01/23 07:04 74-87-3 Chloroprene ND ug/L 5.0 1.6 1 04/01/23 07:04 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/01/23 07:04 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/01/23 07:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/01/23 07:04 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/01/23 07:04 74-95-3 1,2-Dichlorobenzene 1.3 ug/L 1.0 0.34 1 04/01/23 07:04 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 04/01/23 07:04 541-73-1 1,4-Dichlorobenzene 0.94J ug/L 1.0 0.33 1 04/01/23 07:04 106-46-7 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/01/23 07:04 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 04/01/23 07:04 75-71-8 1,1-Dichloroethane 1.4 ug/L 1.0 0.37 1 04/01/23 07:04 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/01/23 07:04 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/01/23 07:04 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 04/01/23 07:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 04/01/23 07:04 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 04/01/23 07:04 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 04/01/23 07:04 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 04/01/23 07:04 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 04/01/23 07:04 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 07:04 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 07:04 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 04/01/23 07:04 100-41-4 Ethyl methacrylate ND ug/L 1.0 0.28 1 04/01/23 07:04 97-63-2 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 04/01/23 07:04 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 04/01/23 07:04 591-78-6 lodomethane ND ug/L 20.0 9.7 1 04/01/23 07:04 74-88-4 Isobutanol ND ug/L 100 52.3 1 04/01/23 07:04 78-83-1 Methacrylonitrile ND ug/L 10.0 4.2 1 04/01/23 07:04 126-98-7 Methylene Chloride ND ug/L 5.0 2.0 1 04/01/23 07:04 75-09-2 Methyl methacrylate ND ug/L 2.0 0.32 1 04/01/23 07:04 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 04/01/23 07:04 108-10-1 Naphthalene ND ug/L 1.0 0.64 1 04/01/23 07:04 91-20-3 Propionitrile ND ug/L 20.0 3.6 1 04/01/23 07:04 107-12-0 Styrene ND ug/L 1.0 0.29 1 04/01/23 07:04 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 04/01/23 07:04 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 04/01/23 07:04 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 04/01/23 07:04 127-18-4 Tetrahydrofuran ND ug/L 10.0 3.5 1 04/01/23 07:04 109-99-9 Toluene ND ug/L 1.0 0.24 1 04/01/23 07:04 108-88-3 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 04/01/23 07:04 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 04/01/23 07:04 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 04/01/23 07:04 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 04/01/23 07:04 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 04/01/23 07:04 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 04/01/23 07:04 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 04/01/23 07:04 108-05-4 Vinyl chloride 0.81J ug/L 1.0 0.39 1 04/01/23 07:04 75-01-4 v2 Xylene (Total) ND ug/L 1.0 0.34 1 04/01/23 07:04 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 04/01/23 07:04 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 04/01/23 07:04 17060-07-0 Toluene-d8 (S) 94 % 70-130 1 04/01/23 07:04 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-5R Lab ID: 92659639001 Collected: 03/29/23 14:05 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 186000 ug/L 5000 5000 1 04/06/23 19:17 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 307 mg/L 25.0 25.0 1 03/31/23 19:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 04/04/23 02:45 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 8200 ug/L 1000 500 1 04/01/23 01:19 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 17.6J ug/L 40.0 10.0 1 03/31/23 03:25 14797-55-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 50000 ug/L 2000 1000 2 04/05/23 20:40 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 04/03/23 18:41 04/03/23 22:04 57-12-5 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 04/04/23 14:45 04/06/23 12:11 94-75-7 R1 Dinoseb ND ug/L 2.00 0.250 1 04/04/23 14:45 04/06/23 12:11 88-85-7 2,4,5-T ND ug/L 2.00 0.258 1 04/04/23 14:45 04/06/23 12:11 93-76-5 R1 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 04/04/23 14:45 04/06/23 12:11 93-72-1 R1 Surrogates 2,4-DCAA (S) 71.8 % 14.0-158 1 04/04/23 14:45 04/06/23 12:11 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:17 309-00-2 alpha-BHC ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:17 319-84-6 beta-BHC ND ug/L 0.042 0.041 1 04/05/23 11:13 04/06/23 15:17 319-85-7 delta-BHC ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:17 319-86-8 gamma-BHC (Lindane) ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:17 58-89-9 Chlordane (Technical) ND ug/L 0.42 0.13 1 04/05/23 11:13 04/06/23 15:17 57-74-9 4,4'-DDD ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:17 72-54-8 4,4'-DDE ND ug/L 0.042 0.020 1 04/05/23 11:13 04/06/23 15:17 72-55-9 4,4'-DDT ND ug/L 0.042 0.022 1 04/05/23 11:13 04/06/23 15:17 50-29-3 Dieldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:17 60-57-1 Endosulfan I ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:17 959-98-8 Endosulfan II ND ug/L 0.042 0.013 1 04/05/23 11:13 04/06/23 15:17 33213-65-9 Endosulfan sulfate ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:17 1031-07-8 Endrin ND ug/L 0.042 0.015 1 04/05/23 11:13 04/06/23 15:17 72-20-8 Endrin aldehyde ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:17 7421-93-4 Heptachlor ND ug/L 0.042 0.016 1 04/05/23 11:13 04/06/23 15:17 76-44-8 Heptachlor epoxide ND ug/L 0.042 0.024 1 04/05/23 11:13 04/06/23 15:17 1024-57-3 Methoxychlor ND ug/L 0.12 0.035 1 04/05/23 11:13 04/06/23 15:17 72-43-5 Toxaphene ND ug/L 0.42 0.18 1 04/05/23 11:13 04/06/23 15:17 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 96 % 10-182 1 04/05/23 11:13 04/06/23 15:17 877-09-8 Decachlorobiphenyl (S) 116 % 10-200 1 04/05/23 11:13 04/06/23 15:17 2051-24-3 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) ND ug/L 0.42 0.18 1 04/14/23 11:02 04/17/23 14:58 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.42 0.19 1 04/14/23 11:02 04/17/23 14:58 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.42 0.19 1 04/14/23 11:02 04/17/23 14:58 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.21 1 04/14/23 11:02 04/17/23 14:58 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.24 1 04/14/23 11:02 04/17/23 14:58 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.18 1 04/14/23 11:02 04/17/23 14:58 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.13 1 04/14/23 11:02 04/17/23 14:58 11096-82-5 Surrogates Decachlorobiphenyl (S) 149 % 10-193 1 04/14/23 11:02 04/17/23 14:58 2051-24-3 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane ND ug/L 5.0 2.0 1 04/10/23 09:45 74-82-8 Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/03/23 09:02 04/03/23 19:43 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/03/23 09:02 04/03/23 19:43 7440-38-2 Barium 3.74J ug/L 5.00 0.736 1 04/03/23 09:02 04/03/23 19:43 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/03/23 09:02 04/03/23 19:43 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/03/23 09:02 04/03/23 19:43 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/03/23 09:02 04/03/23 19:43 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/03/23 09:02 04/03/23 19:43 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/03/23 09:02 04/03/23 19:43 7440-50-8 Iron ND ug/L 100 18.0 1 04/03/23 09:02 04/03/23 19:43 7439-89-6 Lead ND ug/L 6.00 2.99 1 04/03/23 09:02 04/03/23 19:43 7439-92-1 Manganese ND ug/L 10.0 0.934 1 04/03/23 09:02 04/03/23 19:43 7439-96-5 Nickel 1.92J ug/L 10.0 1.61 1 04/03/23 09:02 04/03/23 19:43 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/03/23 09:02 04/03/23 19:43 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/03/23 09:02 04/03/23 19:43 7440-22-4 Tin ND ug/L 50.0 4.87 1 04/03/23 09:02 04/03/23 19:43 7440-31-5 Vanadium ND ug/L 20.0 4.99 1 04/03/23 09:02 04/03/23 19:43 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/03/23 09:02 04/03/23 19:43 7440-66-6 Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 01:56 04/05/23 10:49 7440-28-0 Mercury 7470A Mercury 8270E APP9 RV Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol Date: 04/20/2023 03:37 PM Analytical Method: EPA 7470A Preparation Method: 7470A Pace National - Mt. Juliet ND ug/L 0.200 0.100 1 04/04/23 08:56 04/04/23 19:32 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 20:09 83-32-9 ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 208-96-8 ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 20:09 98-86-2 ND ug/L 8.3 3.4 1 04/04/23 18:28 04/06/23 20:09 53-96-3 ND ug/L 8.3 4.0 1 04/04/23 18:28 04/06/23 20:09 92-67-1 ND ug/L 8.3 1.9 1 04/04/23 18:28 04/06/23 20:09 120-12-7 ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 20:09 56-55-3 ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 20:09 50-32-8 ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 20:09 205-99-2 ND ug/L 8.3 2.4 1 04/04/23 18:28 04/06/23 20:09 191-24-2 ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 20:09 207-08-9 ND ug/L 16.7 2.4 1 04/04/23 18:28 04/06/23 20:09 100-51-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. J J Page 15 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 4-Bromophenylphenyl ether ND ug/L 8.3 1.5 1 04/04/23 18:28 04/06/23 20:09 101-55-3 Butylbenzylphthalate ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 20:09 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 20:09 59-50-7 4-Chloroaniline ND ug/L 16.7 3.0 1 04/04/23 18:28 04/06/23 20:09 106-47-8 Chlorobenzilate ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 20:09 510-15-6 bis(2-Chloroethoxy)methane ND ug/L 8.3 1.5 1 04/04/23 18:28 04/06/23 20:09 111-91-1 bis(2-Chloroethyl) ether ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 111-44-4 2-Chloronaphthalene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 20:09 91-58-7 2-Chlorophenol ND ug/L 8.3 1.0 1 04/04/23 18:28 04/06/23 20:09 95-57-8 4-Chlorophenylphenyl ether ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 20:09 7005-72-3 Chrysene ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 20:09 218-01-9 Diallate ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 20:09 2303-16-4 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 20:09 53-70-3 Dibenzofuran ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 132-64-9 3,3'-Dichlorobenzidine ND ug/L 16.7 6.8 1 04/04/23 18:28 04/06/23 20:09 91-94-1 2,4-Dichlorophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 20:09 120-83-2 2,6-Dichlorophenol ND ug/L 8.3 3.5 1 04/04/23 18:28 04/06/23 20:09 87-65-0 Diethylphthalate ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 20:09 84-66-2 Dimethoate ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 20:09 60-51-5 P-Dimethylaminoazobenzene ND ug/L 4.2 2.0 1 04/04/23 18:28 04/06/23 20:09 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 20:09 57-97-6 3,3'-Dimethylbenzidine ND ug/L 41.7 25.9 1 04/04/23 18:28 04/06/23 20:09 119-93-7 2,4-Dimethylphenol ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 20:09 105-67-9 Dimethylphthalate ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 131-11-3 Di-n-butylphthalate ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 16.7 6.5 1 04/04/23 18:28 04/06/23 20:09 534-52-1 1,3-Dinitrobenzene ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 20:09 99-65-0 2,4-Dinitrophenol ND ug/L 41.7 21.7 1 04/04/23 18:28 04/06/23 20:09 51-28-5 2,4-Dinitrotoluene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 20:09 121-14-2 2,6-Dinitrotoluene ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 20:09 606-20-2 Di-n-octylphthalate ND ug/L 8.3 3.3 1 04/04/23 18:28 04/06/23 20:09 117-84-0 Diphenylamine ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 20:09 122-39-4 Disulfoton ND ug/L 8.3 3.9 1 04/04/23 18:28 04/06/23 20:09 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 04/04/23 18:28 04/06/23 20:09 117-81-7 Ethyl methanesulfonate ND ug/L 16.7 2.5 1 04/04/23 18:28 04/06/23 20:09 62-50-0 Famphur ND ug/L 8.3 5.1 1 04/04/23 18:28 04/06/23 20:09 52-85-7 Fluoranthene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 206-44-0 Fluorene ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 20:09 86-73-7 Hexachlorobenzene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 118-74-1 Hexachlorocyclopentadiene ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 20:09 77-47-4 Hexachloroethane ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 20:09 67-72-1 Hexachloropropene ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 20:09 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 04/04/23 18:28 04/06/23 20:09 193-39-5 Isodrin ND ug/L 8.3 2.3 1 04/04/23 18:28 04/06/23 20:09 465-73-6 Isophorone ND ug/L 8.3 1.4 1 04/04/23 18:28 04/06/23 20:09 78-59-1 REPORT OF LABORATORY ANALYSIS IL IH L1 v1 This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Isosafrole ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 20:09 120-58-1 Kepone ND ug/L 16.7 11.8 1 04/04/23 18:28 04/06/23 20:09 143-50-0 Methapyrilene ND ug/L 41.7 14.2 1 04/04/23 18:28 04/06/23 20:09 91-80-5 IH,v1 3-Methylcholanthrene ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 20:09 56-49-5 Methyl methanesulfonate ND ug/L 4.2 2.6 1 04/04/23 18:28 04/06/23 20:09 66-27-3 2-Methylnaphthalene ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 91-57-6 Methyl parathion ND ug/L 8.3 3.1 1 04/04/23 18:28 04/06/23 20:09 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 8.3 1.0 1 04/04/23 18:28 04/06/23 20:09 15831-10-4 1-Naphthalenamine ND ug/L 8.3 5.0 1 04/04/23 18:28 04/06/23 20:09 134-32-7 2-Naphthalenamine ND ug/L 8.3 4.5 1 04/04/23 18:28 04/06/23 20:09 91-59-8 1,4-Naphthoquinone ND ug/L 4.2 3.7 1 04/04/23 18:28 04/06/23 20:09 130-15-4 2-Nitroaniline ND ug/L 16.7 2.5 1 04/04/23 18:28 04/06/23 20:09 88-74-4 3-Nitroaniline ND ug/L 16.7 3.1 1 04/04/23 18:28 04/06/23 20:09 99-09-2 4-Nitroaniline ND ug/L 16.7 4.2 1 04/04/23 18:28 04/06/23 20:09 100-01-6 Nitrobenzene ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 98-95-3 2-Nitrophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 20:09 88-75-5 4-Nitrophenol ND ug/L 41.7 5.5 1 04/04/23 18:28 04/06/23 20:09 100-02-7 5-Nitro-o-toluidine ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 20:09 99-55-8 N-Nitrosodiethylamine ND ug/L 8.3 1.9 1 04/04/23 18:28 04/06/23 20:09 55-18-5 N-Nitrosodimethylamine ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 8.3 1.6 1 04/04/23 18:28 04/06/23 20:09 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 8.3 1.1 1 04/04/23 18:28 04/06/23 20:09 621-64-7 N-Nitrosodiphenylamine ND ug/L 8.3 2.5 1 04/04/23 18:28 04/06/23 20:09 86-30-6 N-Nitrosomethylethylamine ND ug/L 8.3 6.2 1 04/04/23 18:28 04/06/23 20:09 10595-95-6 N-Nitrosopiperidine ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 20:09 100-75-4 N-Nitrosopyrrolidine ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 20:09 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 8.3 2.1 1 04/04/23 18:28 04/06/23 20:09 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 8.3 0.96 1 04/04/23 18:28 04/06/23 20:09 108-60-1 Parathion (Ethyl parathion) ND ug/L 8.3 3.2 1 04/04/23 18:28 04/06/23 20:09 56-38-2 Pentachlorobenzene ND ug/L 8.3 2.8 1 04/04/23 18:28 04/06/23 20:09 608-93-5 Pentachloronitrobenzene ND ug/L 8.3 2.7 1 04/04/23 18:28 04/06/23 20:09 82-68-8 Pentachlorophenol ND ug/L 16.7 3.1 1 04/04/23 18:28 04/06/23 20:09 87-86-5 Phenacetin ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 20:09 62-44-2 Phenanthrene ND ug/L 8.3 1.7 1 04/04/23 18:28 04/06/23 20:09 85-01-8 Phenol ND ug/L 8.3 1.1 1 04/04/23 18:28 04/06/23 20:09 108-95-2 p-Phenylenediamine ND ug/L 8.3 8.3 1 04/04/23 18:28 04/06/23 20:09 106-50-3 Phorate ND ug/L 8.3 3.0 1 04/04/23 18:28 04/06/23 20:09 298-02-2 Pronamide ND ug/L 8.3 2.6 1 04/04/23 18:28 04/06/23 20:09 23950-58-5 Pyrene ND ug/L 8.3 1.8 1 04/04/23 18:28 04/06/23 20:09 129-00-0 Safrole ND ug/L 8.3 1.9 1 04/04/23 18:28 04/06/23 20:09 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 8.3 3.7 1 04/04/23 18:28 04/06/23 20:09 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 20:09 58-90-2 Thionazin ND ug/L 8.3 2.4 1 04/04/23 18:28 04/06/23 20:09 297-97-2 O-Toluidine ND ug/L 8.3 2.2 1 04/04/23 18:28 04/06/23 20:09 95-53-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2,4,5-Trichlorophenol ND ug/L 8.3 1.2 1 04/04/23 18:28 04/06/23 20:09 95-95-4 2,4,6-Trichlorophenol ND ug/L 8.3 1.3 1 04/04/23 18:28 04/06/23 20:09 88-06-2 1,3,5-Trinitrobenzene ND ug/L 8.3 4.6 1 04/04/23 18:28 04/06/23 20:09 99-35-4 v1 Surrogates Nitrobenzene-d5 (S) 52 % 10-138 1 04/04/23 18:28 04/06/23 20:09 4165-60-0 2-Fluorobiphenyl (S) 46 % 10-130 1 04/04/23 18:28 04/06/23 20:09 321-60-8 Terphenyl-d14 (S) 68 % 19-191 1 04/04/23 18:28 04/06/23 20:09 1718-51-0 Phenol-d6 (S) 32 % 10-130 1 04/04/23 18:28 04/06/23 20:09 13127-88-3 2-Fluorophenol (S) 40 % 10-130 1 04/04/23 18:28 04/06/23 20:09 367-12-4 2,4,6-Tribromophenol (S) 58 % 10-164 1 04/04/23 18:28 04/06/23 20:09 118-79-6 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 04/05/23 01:04 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 80 % 67-130 1 04/05/23 01:04 17060-07-0 Toluene-d8 (S) 89 % 70-130 1 04/05/23 01:04 2037-26-5 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/01/23 07:22 67-64-1 Acetonitrile ND ug/L 50.0 24.8 1 04/01/23 07:22 75-05-8 Acrolein ND ug/L 10.0 8.5 1 04/01/23 07:22 107-02-8 Acrylonitrile ND ug/L 10.0 1.8 1 04/01/23 07:22 107-13-1 Allyl chloride ND ug/L 2.0 0.50 1 04/01/23 07:22 107-05-1 Benzene ND ug/L 1.0 0.34 1 04/01/23 07:22 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/01/23 07:22 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/01/23 07:22 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/01/23 07:22 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/01/23 07:22 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/01/23 07:22 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/01/23 07:22 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/01/23 07:22 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/01/23 07:22 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/01/23 07:22 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/01/23 07:22 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/01/23 07:22 74-87-3 Chloroprene ND ug/L 5.0 1.6 1 04/01/23 07:22 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/01/23 07:22 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/01/23 07:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/01/23 07:22 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/01/23 07:22 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/01/23 07:22 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 04/01/23 07:22 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/01/23 07:22 106-46-7 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Lab ID: 92659639002 Collected: 03/29/23 15:09 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/01/23 07:22 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 04/01/23 07:22 75-71-8 M1 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/01/23 07:22 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/01/23 07:22 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/01/23 07:22 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 04/01/23 07:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 04/01/23 07:22 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 04/01/23 07:22 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 04/01/23 07:22 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 04/01/23 07:22 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 04/01/23 07:22 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 07:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 07:22 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 04/01/23 07:22 100-41-4 Ethyl methacrylate ND ug/L 1.0 0.28 1 04/01/23 07:22 97-63-2 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 04/01/23 07:22 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 04/01/23 07:22 591-78-6 lodomethane ND ug/L 20.0 9.7 1 04/01/23 07:22 74-88-4 Isobutanol ND ug/L 100 52.3 1 04/01/23 07:22 78-83-1 Methacrylonitrile ND ug/L 10.0 4.2 1 04/01/23 07:22 126-98-7 Methylene Chloride ND ug/L 5.0 2.0 1 04/01/23 07:22 75-09-2 Methyl methacrylate ND ug/L 2.0 0.32 1 04/01/23 07:22 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 04/01/23 07:22 108-10-1 Naphthalene ND ug/L 1.0 0.64 1 04/01/23 07:22 91-20-3 Propionitrile ND ug/L 20.0 3.6 1 04/01/23 07:22 107-12-0 Styrene ND ug/L 1.0 0.29 1 04/01/23 07:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 04/01/23 07:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 04/01/23 07:22 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 04/01/23 07:22 127-18-4 Tetrahydrofuran ND ug/L 10.0 3.5 1 04/01/23 07:22 109-99-9 Toluene ND ug/L 1.0 0.24 1 04/01/23 07:22 108-88-3 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 04/01/23 07:22 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 04/01/23 07:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 04/01/23 07:22 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 04/01/23 07:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 04/01/23 07:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 04/01/23 07:22 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 04/01/23 07:22 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 04/01/23 07:22 75-01-4 M1,v2 Xylene (Total) ND ug/L 1.0 0.34 1 04/01/23 07:22 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 04/01/23 07:22 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 04/01/23 07:22 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 04/01/23 07:22 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-7 Parameters Lab ID: 92659639002 Collected: Report Results Units Limit 03/29/23 15:09 MDL DF Received: 03/30/23 10:00 Matrix: Water Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 151000 ug/L 5000 5000 1 04/06/23 19:30 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 252 mg/L 25.0 25.0 1 03/31/23 19:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 04/04/23 02:46 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 47700 ug/L 1000 500 1 04/01/23 02:10 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 305 ug/L 40.0 10.0 1 03/31/23 03:33 14797-55-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 9360 ug/L 1000 500 1 04/05/2319:15 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 40.0 30.0 5 04/03/23 18:41 04/03/23 22:16 57-12-5 D3 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 04/04/23 14:45 04/06/23 12:55 94-75-7 R1 Dinoseb ND ug/L 2.00 0.250 1 04/04/23 14:45 04/06/23 12:55 88-85-7 2,4,5-T ND ug/L 2.00 0.258 1 04/04/23 14:45 04/06/23 12:55 93-76-5 R1 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 04/04/23 14:45 04/06/23 12:55 93-72-1 R1 Surrogates 2,4-DCAA (S) 66.2 % 14.0-158 1 04/04/23 14:45 04/06/23 12:55 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:30 309-00-2 alpha-BHC ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:30 319-84-6 beta-BHC ND ug/L 0.042 0.041 1 04/05/23 11:13 04/06/23 15:30 319-85-7 delta-BHC ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:30 319-86-8 gamma-BHC (Lindane) ND ug/L 0.042 0.010 1 04/05/23 11:13 04/06/23 15:30 58-89-9 Chlordane (Technical) ND ug/L 0.42 0.13 1 04/05/23 11:13 04/06/23 15:30 57-74-9 4,4'-DDD ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:30 72-54-8 4,4'-DDE ND ug/L 0.042 0.020 1 04/05/23 11:13 04/06/23 15:30 72-55-9 4,4'-DDT ND ug/L 0.042 0.022 1 04/05/23 11:13 04/06/23 15:30 50-29-3 Dieldrin ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:30 60-57-1 Endosulfan I ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:30 959-98-8 Endosulfan II ND ug/L 0.042 0.013 1 04/05/23 11:13 04/06/23 15:30 33213-65-9 Endosulfan sulfate ND ug/L 0.042 0.012 1 04/05/23 11:13 04/06/23 15:30 1031-07-8 Endrin ND ug/L 0.042 0.015 1 04/05/23 11:13 04/06/23 15:30 72-20-8 Endrin aldehyde ND ug/L 0.042 0.014 1 04/05/23 11:13 04/06/23 15:30 7421-93-4 Heptachlor ND ug/L 0.042 0.016 1 04/05/23 11:13 04/06/23 15:30 76-44-8 Heptachlor epoxide ND ug/L 0.042 0.024 1 04/05/23 11:13 04/06/23 15:30 1024-57-3 Methoxychlor ND ug/L 0.12 0.035 1 04/05/23 11:13 04/06/23 15:30 72-43-5 Toxaphene ND ug/L 0.42 0.18 1 04/05/23 11:13 04/06/23 15:30 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 70 % 10-182 1 04/05/23 11:13 04/06/23 15:30 877-09-8 Decachlorobiphenyl (S) 93 % 10-200 1 04/05/23 11:13 04/06/23 15:30 2051-24-3 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) ND ug/L 0.45 0.19 1 04/11/23 14:07 04/12/23 19:27 12674-11-2 R1 PCB-1221 (Aroclor 1221) ND ug/L 0.45 0.21 1 04/11/23 14:07 04/12/23 19:27 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.45 0.21 1 04/11/23 14:07 04/12/23 19:27 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.23 1 04/11/23 14:07 04/12/23 19:27 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.26 1 04/11/23 14:07 04/12/23 19:27 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.19 1 04/11/23 14:07 04/12/23 19:27 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.14 1 04/11/23 14:07 04/12/23 19:27 11096-82-5 M1,R1 Surrogates Decachlorobiphenyl (S) 120 % 10-193 1 04/11/23 14:07 04/12/23 19:27 2051-24-3 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Biodegradation Indicator Gases Analytical Method: RSK-175 Pace Analytical Gulf Coast Methane ND ug/L 5.0 2.0 1 04/10/2310:01 74-82-8 Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/03/23 09:02 04/03/23 19:46 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/03/23 09:02 04/03/23 19:46 7440-38-2 Barium ND ug/L 5.00 0.736 1 04/03/23 09:02 04/03/23 19:46 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/03/23 09:02 04/03/23 19:46 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/03/23 09:02 04/03/23 19:46 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/03/23 09:02 04/03/23 19:46 7440-47-3 Cobalt ND ug/L 10.0 0.840 1 04/03/23 09:02 04/03/23 19:46 7440-48-4 Copper ND ug/L 10.0 3.68 1 04/03/23 09:02 04/03/23 19:46 7440-50-8 Iron ND ug/L 100 18.0 1 04/03/23 09:02 04/03/23 19:46 7439-89-6 Lead ND ug/L 6.00 2.99 1 04/03/23 09:02 04/03/23 19:46 7439-92-1 Manganese ND ug/L 10.0 0.934 1 04/03/23 09:02 04/03/23 19:46 7439-96-5 Nickel ND ug/L 10.0 1.61 1 04/03/23 09:02 04/03/23 19:46 7440-02-0 Selenium ND ug/L 10.0 7.35 1 04/03/23 09:02 04/03/23 19:46 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/03/23 09:02 04/03/23 19:46 7440-22-4 Tin ND ug/L 50.0 4.87 1 04/03/23 09:02 04/03/23 19:46 7440-31-5 Vanadium ND ug/L 20.0 4.99 1 04/03/23 09:02 04/03/23 19:46 7440-62-2 Zinc ND ug/L 50.0 6.52 1 04/03/23 09:02 04/03/23 19:46 7440-66-6 Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 01:56 04/05/23 10:52 7440-28-0 Mercury 7470A Mercury 8270E APP9 RV Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol Date: 04/20/2023 03:37 PM Analytical Method: EPA 7470A Preparation Method: 7470A Pace National - Mt. Juliet ND ug/L 0.200 0.100 1 04/04/23 08:56 04/04/23 19:34 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 83-32-9 ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 208-96-8 ND ug/L 8.7 1.3 1 04/04/23 18:28 04/06/23 20:35 98-86-2 ND ug/L 8.7 3.5 1 04/04/23 18:28 04/06/23 20:35 53-96-3 ND ug/L 8.7 4.1 1 04/04/23 18:28 04/06/23 20:35 92-67-1 ND ug/L 8.7 2.0 1 04/04/23 18:28 04/06/23 20:35 120-12-7 ND ug/L 8.7 2.3 1 04/04/23 18:28 04/06/23 20:35 56-55-3 ND ug/L 8.7 2.4 1 04/04/23 18:28 04/06/23 20:35 50-32-8 ND ug/L 8.7 2.3 1 04/04/23 18:28 04/06/23 20:35 205-99-2 ND ug/L 8.7 2.5 1 04/04/23 18:28 04/06/23 20:35 191-24-2 ND ug/L 8.7 2.4 1 04/04/23 18:28 04/06/23 20:35 207-08-9 ND ug/L 17.4 2.5 1 04/04/23 18:28 04/06/23 20:35 100-51-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 4-Bromophenylphenyl ether ND ug/L 8.7 1.5 1 04/04/23 18:28 04/06/23 20:35 101-55-3 Butylbenzylphthalate ND ug/L 8.7 2.7 1 04/04/23 18:28 04/06/23 20:35 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 8.7 2.9 1 04/04/23 18:28 04/06/23 20:35 59-50-7 4-Chloroaniline ND ug/L 17.4 3.2 1 04/04/23 18:28 04/06/23 20:35 106-47-8 Chlorobenzilate ND ug/L 8.7 3.3 1 04/04/23 18:28 04/06/23 20:35 510-15-6 bis(2-Chloroethoxy)methane ND ug/L 8.7 1.6 1 04/04/23 18:28 04/06/23 20:35 111-91-1 bis(2-Chloroethyl) ether ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 111-44-4 2-Chloronaphthalene ND ug/L 8.7 1.5 1 04/04/23 18:28 04/06/23 20:35 91-58-7 2-Chlorophenol ND ug/L 8.7 1.0 1 04/04/23 18:28 04/06/23 20:35 95-57-8 4-Chlorophenylphenyl ether ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 7005-72-3 Chrysene ND ug/L 8.7 2.4 1 04/04/23 18:28 04/06/23 20:35 218-01-9 Diallate ND ug/L 8.7 3.0 1 04/04/23 18:28 04/06/23 20:35 2303-16-4 Dibenz(a,h)anthracene ND ug/L 8.7 2.6 1 04/04/23 18:28 04/06/23 20:35 53-70-3 Dibenzofuran ND ug/L 8.7 1.8 1 04/04/23 18:28 04/06/23 20:35 132-64-9 3,3'-Dichlorobenzidine ND ug/L 17.4 7.1 1 04/04/23 18:28 04/06/23 20:35 91-94-1 2,4-Dichlorophenol ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 120-83-2 2,6-Dichlorophenol ND ug/L 8.7 3.7 1 04/04/23 18:28 04/06/23 20:35 87-65-0 Diethylphthalate ND ug/L 8.7 1.8 1 04/04/23 18:28 04/06/23 20:35 84-66-2 Dimethoate ND ug/L 8.7 3.2 1 04/04/23 18:28 04/06/23 20:35 60-51-5 P-Dimethylaminoazobenzene ND ug/L 4.3 2.1 1 04/04/23 18:28 04/06/23 20:35 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 8.7 2.6 1 04/04/23 18:28 04/06/23 20:35 57-97-6 3,3'-Dimethylbenzidine ND ug/L 43.5 27.0 1 04/04/23 18:28 04/06/23 20:35 119-93-7 2,4-Dimethylphenol ND ug/L 8.7 1.5 1 04/04/23 18:28 04/06/23 20:35 105-67-9 Dimethylphthalate ND ug/L 8.7 1.9 1 04/04/23 18:28 04/06/23 20:35 131-11-3 Di-n-butylphthalate ND ug/L 8.7 1.9 1 04/04/23 18:28 04/06/23 20:35 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 17.4 6.8 1 04/04/23 18:28 04/06/23 20:35 534-52-1 1,3-Dinitrobenzene ND ug/L 8.7 3.3 1 04/04/23 18:28 04/06/23 20:35 99-65-0 2,4-Dinitrophenol ND ug/L 43.5 22.6 1 04/04/23 18:28 04/06/23 20:35 51-28-5 2,4-Dinitrotoluene ND ug/L 8.7 1.4 1 04/04/23 18:28 04/06/23 20:35 121-14-2 2,6-Dinitrotoluene ND ug/L 8.7 1.5 1 04/04/23 18:28 04/06/23 20:35 606-20-2 Di-n-octylphthalate ND ug/L 8.7 3.4 1 04/04/23 18:28 04/06/23 20:35 117-84-0 Diphenylamine ND ug/L 8.7 2.6 1 04/04/23 18:28 04/06/23 20:35 122-39-4 Disulfoton ND ug/L 8.7 4.0 1 04/04/23 18:28 04/06/23 20:35 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 5.2 3.2 1 04/04/23 18:28 04/06/23 20:35 117-81-7 Ethyl methanesulfonate ND ug/L 17.4 2.6 1 04/04/23 18:28 04/06/23 20:35 62-50-0 Famphur ND ug/L 8.7 5.3 1 04/04/23 18:28 04/06/23 20:35 52-85-7 Fluoranthene ND ug/L 8.7 1.9 1 04/04/23 18:28 04/06/23 20:35 206-44-0 Fluorene ND ug/L 8.7 1.8 1 04/04/23 18:28 04/06/23 20:35 86-73-7 Hexachlorobenzene ND ug/L 8.7 1.9 1 04/04/23 18:28 04/06/23 20:35 118-74-1 Hexachlorocyclopentadiene ND ug/L 8.7 1.4 1 04/04/23 18:28 04/06/23 20:35 77-47-4 Hexachloroethane ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 67-72-1 Hexachloropropene ND ug/L 8.7 2.3 1 04/04/23 18:28 04/06/23 20:35 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.7 2.5 1 04/04/23 18:28 04/06/23 20:35 193-39-5 Isodrin ND ug/L 8.7 2.4 1 04/04/23 18:28 04/06/23 20:35 465-73-6 Isophorone ND ug/L 8.7 1.4 1 04/04/23 18:28 04/06/23 20:35 78-59-1 REPORT OF LABORATORY ANALYSIS IL IH L1 v1 This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Isosafrole ND ug/L 8.7 2.2 1 04/04/23 18:28 04/06/23 20:35 120-58-1 Kepone ND ug/L 17.4 12.3 1 04/04/23 18:28 04/06/23 20:35 143-50-0 Methapyrilene ND ug/L 43.5 14.8 1 04/04/23 18:28 04/06/23 20:35 91-80-5 IH,v1 3-Methylcholanthrene ND ug/L 8.7 3.3 1 04/04/23 18:28 04/06/23 20:35 56-49-5 Methyl methanesulfonate ND ug/L 4.3 2.7 1 04/04/23 18:28 04/06/23 20:35 66-27-3 2-Methylnaphthalene ND ug/L 8.7 1.6 1 04/04/23 18:28 04/06/23 20:35 91-57-6 Methyl parathion ND ug/L 8.7 3.2 1 04/04/23 18:28 04/06/23 20:35 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 8.7 1.6 1 04/04/23 18:28 04/06/23 20:35 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 8.7 1.1 1 04/04/23 18:28 04/06/23 20:35 15831-10-4 1-Naphthalenamine ND ug/L 8.7 5.2 1 04/04/23 18:28 04/06/23 20:35 134-32-7 2-Naphthalenamine ND ug/L 8.7 4.7 1 04/04/23 18:28 04/06/23 20:35 91-59-8 1,4-Naphthoquinone ND ug/L 4.3 3.8 1 04/04/23 18:28 04/06/23 20:35 130-15-4 2-Nitroaniline ND ug/L 17.4 2.6 1 04/04/23 18:28 04/06/23 20:35 88-74-4 3-Nitroaniline ND ug/L 17.4 3.3 1 04/04/23 18:28 04/06/23 20:35 99-09-2 4-Nitroaniline ND ug/L 17.4 4.4 1 04/04/23 18:28 04/06/23 20:35 100-01-6 Nitrobenzene ND ug/L 8.7 1.6 1 04/04/23 18:28 04/06/23 20:35 98-95-3 2-Nitrophenol ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 88-75-5 4-Nitrophenol ND ug/L 43.5 5.7 1 04/04/23 18:28 04/06/23 20:35 100-02-7 5-Nitro-o-toluidine ND ug/L 8.7 3.3 1 04/04/23 18:28 04/06/23 20:35 99-55-8 N-Nitrosodiethylamine ND ug/L 8.7 2.0 1 04/04/23 18:28 04/06/23 20:35 55-18-5 N-Nitrosodimethylamine ND ug/L 8.7 1.6 1 04/04/23 18:28 04/06/23 20:35 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 621-64-7 N-Nitrosodiphenylamine ND ug/L 8.7 2.6 1 04/04/23 18:28 04/06/23 20:35 86-30-6 N-Nitrosomethylethylamine ND ug/L 8.7 6.5 1 04/04/23 18:28 04/06/23 20:35 10595-95-6 N-Nitrosopiperidine ND ug/L 8.7 2.2 1 04/04/23 18:28 04/06/23 20:35 100-75-4 N-Nitrosopyrrolidine ND ug/L 8.7 2.7 1 04/04/23 18:28 04/06/23 20:35 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 8.7 2.2 1 04/04/23 18:28 04/06/23 20:35 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 8.7 1.0 1 04/04/23 18:28 04/06/23 20:35 108-60-1 Parathion (Ethyl parathion) ND ug/L 8.7 3.4 1 04/04/23 18:28 04/06/23 20:35 56-38-2 Pentachlorobenzene ND ug/L 8.7 3.0 1 04/04/23 18:28 04/06/23 20:35 608-93-5 Pentachloronitrobenzene ND ug/L 8.7 2.8 1 04/04/23 18:28 04/06/23 20:35 82-68-8 Pentachlorophenol ND ug/L 17.4 3.3 1 04/04/23 18:28 04/06/23 20:35 87-86-5 Phenacetin ND ug/L 8.7 3.1 1 04/04/23 18:28 04/06/23 20:35 62-44-2 Phenanthrene ND ug/L 8.7 1.7 1 04/04/23 18:28 04/06/23 20:35 85-01-8 Phenol ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 108-95-2 p-Phenylenediamine ND ug/L 8.7 8.7 1 04/04/23 18:28 04/06/23 20:35 106-50-3 Phorate ND ug/L 8.7 3.1 1 04/04/23 18:28 04/06/23 20:35 298-02-2 Pronamide ND ug/L 8.7 2.7 1 04/04/23 18:28 04/06/23 20:35 23950-58-5 Pyrene ND ug/L 8.7 1.9 1 04/04/23 18:28 04/06/23 20:35 129-00-0 Safrole ND ug/L 8.7 2.0 1 04/04/23 18:28 04/06/23 20:35 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 8.7 3.9 1 04/04/23 18:28 04/06/23 20:35 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 8.7 1.3 1 04/04/23 18:28 04/06/23 20:35 58-90-2 Thionazin ND ug/L 8.7 2.5 1 04/04/23 18:28 04/06/23 20:35 297-97-2 O-Toluidine ND ug/L 8.7 2.3 1 04/04/23 18:28 04/06/23 20:35 95-53-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2,4,5-Trichlorophenol ND ug/L 8.7 1.2 1 04/04/23 18:28 04/06/23 20:35 95-95-4 2,4,6-Trichlorophenol ND ug/L 8.7 1.3 1 04/04/23 18:28 04/06/23 20:35 88-06-2 1,3,5-Trinitrobenzene ND ug/L 8.7 4.8 1 04/04/23 18:28 04/06/23 20:35 99-35-4 v1 Surrogates Nitrobenzene-d5 (S) 105 % 10-138 1 04/04/23 18:28 04/06/23 20:35 4165-60-0 2-Fluorobiphenyl (S) 90 % 10-130 1 04/04/23 18:28 04/06/23 20:35 321-60-8 Terphenyl-d14 (S) 105 % 19-191 1 04/04/23 18:28 04/06/23 20:35 1718-51-0 Phenol-d6 (S) 50 % 10-130 1 04/04/23 18:28 04/06/23 20:35 13127-88-3 2-Fluorophenol (S) 69 % 10-130 1 04/04/23 18:28 04/06/23 20:35 367-12-4 2,4,6-Tribromophenol (S) 115 % 10-164 1 04/04/23 18:28 04/06/23 20:35 118-79-6 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 04/04/23 22:13 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 80 % 67-130 1 04/04/23 22:13 17060-07-0 Toluene-d8 (S) 88 % 70-130 1 04/04/23 22:13 2037-26-5 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 5.1 1 04/01/23 06:27 67-64-1 Acetonitrile ND ug/L 50.0 24.8 1 04/01/23 06:27 75-05-8 Acrolein ND ug/L 10.0 8.5 1 04/01/23 06:27 107-02-8 Acrylonitrile ND ug/L 10.0 1.8 1 04/01/23 06:27 107-13-1 Allyl chloride ND ug/L 2.0 0.50 1 04/01/23 06:27 107-05-1 Benzene ND ug/L 1.0 0.34 1 04/01/23 06:27 71-43-2 Bromochloromethane ND ug/L 1.0 0.47 1 04/01/23 06:27 74-97-5 Bromodichloromethane ND ug/L 1.0 0.31 1 04/01/23 06:27 75-27-4 Bromoform ND ug/L 1.0 0.34 1 04/01/23 06:27 75-25-2 Bromomethane ND ug/L 2.0 1.7 1 04/01/23 06:27 74-83-9 2-Butanone (MEK) ND ug/L 5.0 4.0 1 04/01/23 06:27 78-93-3 Carbon disulfide ND ug/L 2.0 0.36 1 04/01/23 06:27 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.33 1 04/01/23 06:27 56-23-5 Chlorobenzene ND ug/L 1.0 0.28 1 04/01/23 06:27 108-90-7 Chloroethane ND ug/L 1.0 0.65 1 04/01/23 06:27 75-00-3 Chloroform ND ug/L 1.0 0.43 1 04/01/23 06:27 67-66-3 Chloromethane ND ug/L 1.0 0.54 1 04/01/23 06:27 74-87-3 Chloroprene ND ug/L 5.0 1.6 1 04/01/23 06:27 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 2.0 0.34 1 04/01/23 06:27 96-12-8 Dibromochloromethane ND ug/L 1.0 0.36 1 04/01/23 06:27 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/01/23 06:27 106-93-4 Dibromomethane ND ug/L 1.0 0.39 1 04/01/23 06:27 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.34 1 04/01/23 06:27 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.34 1 04/01/23 06:27 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 04/01/23 06:27 106-46-7 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level - Acrolein Analytical Method: EPA 8260D Pace Analytical Services - Charlotte trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.56 1 04/01/23 06:27 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 0.35 1 04/01/23 06:27 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.37 1 04/01/23 06:27 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.32 1 04/01/23 06:27 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.35 1 04/01/23 06:27 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.38 1 04/01/23 06:27 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.40 1 04/01/23 06:27 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.36 1 04/01/23 06:27 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 04/01/23 06:27 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.39 1 04/01/23 06:27 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.43 1 04/01/23 06:27 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 06:27 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.36 1 04/01/23 06:27 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 04/01/23 06:27 100-41-4 Ethyl methacrylate ND ug/L 1.0 0.28 1 04/01/23 06:27 97-63-2 Hexachloro-1,3-butadiene ND ug/L 2.0 1.5 1 04/01/23 06:27 87-68-3 2-Hexanone ND ug/L 5.0 0.48 1 04/01/23 06:27 591-78-6 lodomethane ND ug/L 20.0 9.7 1 04/01/23 06:27 74-88-4 Isobutanol ND ug/L 100 52.3 1 04/01/23 06:27 78-83-1 Methacrylonitrile ND ug/L 10.0 4.2 1 04/01/23 06:27 126-98-7 Methylene Chloride ND ug/L 5.0 2.0 1 04/01/23 06:27 75-09-2 Methyl methacrylate ND ug/L 2.0 0.32 1 04/01/23 06:27 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 2.7 1 04/01/23 06:27 108-10-1 Naphthalene ND ug/L 1.0 0.64 1 04/01/23 06:27 91-20-3 Propionitrile ND ug/L 20.0 3.6 1 04/01/23 06:27 107-12-0 Styrene ND ug/L 1.0 0.29 1 04/01/23 06:27 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.31 1 04/01/23 06:27 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.22 1 04/01/23 06:27 79-34-5 Tetrachloroethene ND ug/L 1.0 0.29 1 04/01/23 06:27 127-18-4 Tetrahydrofuran ND ug/L 10.0 3.5 1 04/01/23 06:27 109-99-9 Toluene ND ug/L 1.0 0.24 1 04/01/23 06:27 108-88-3 1,2,4-Trichlorobenzene ND ug/L 1.0 0.64 1 04/01/23 06:27 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.33 1 04/01/23 06:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.32 1 04/01/23 06:27 79-00-5 Trichloroethene ND ug/L 1.0 0.38 1 04/01/23 06:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.30 1 04/01/23 06:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 04/01/23 06:27 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 04/01/23 06:27 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 04/01/23 06:27 75-01-4 v2 Xylene (Total) ND ug/L 1.0 0.34 1 04/01/23 06:27 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 04/01/23 06:27 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 04/01/23 06:27 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 04/01/23 06:27 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: FIELD BLANK UNIT 1 Lab ID: 92659639003 Collected: 03/29/23 16:45 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 ND ug/L 5000 5000 1 04/06/23 19:52 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND mg/L 25.0 25.0 1 03/31/23 19:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 22.0 1 04/04/23 02:46 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 04/01/23 03:02 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate ND ug/L 40.0 10.0 1 03/31/23 03:41 14797-55-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 04/05/2319:16 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 04/03/23 18:41 04/03/23 22:09 57-12-5 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-3RR Lab ID: 92659639004 Collected: 03/29/23 16:30 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Metals (ICP) 6010D Analytical Method: EPA 601 OD Preparation Method: 3015 Pace National - Mt. Juliet Antimony ND ug/L 10.0 4.30 1 04/03/23 09:02 04/03/23 19:48 7440-36-0 Arsenic ND ug/L 10.0 4.40 1 04/03/23 09:02 04/03/23 19:48 7440-38-2 Barium 54.5 ug/L 5.00 0.736 1 04/03/23 09:02 04/03/23 19:48 7440-39-3 Beryllium ND ug/L 2.00 0.330 1 04/03/23 09:02 04/03/23 19:48 7440-41-7 Cadmium ND ug/L 2.00 0.479 1 04/03/23 09:02 04/03/23 19:48 7440-43-9 Chromium ND ug/L 10.0 1.40 1 04/03/23 09:02 04/03/23 19:48 7440-47-3 Cobalt 3.64J ug/L 10.0 0.840 1 04/03/23 09:02 04/03/23 19:48 7440-48-4 J Copper 20.2 ug/L 10.0 3.68 1 04/03/23 09:02 04/03/23 19:48 7440-50-8 Iron 2940 ug/L 100 18.0 1 04/03/23 09:02 04/03/23 19:48 7439-89-6 Lead ND ug/L 6.00 2.99 1 04/03/23 09:02 04/03/23 19:48 7439-92-1 Manganese 2890 ug/L 10.0 0.934 1 04/03/23 09:02 04/03/23 19:48 7439-96-5 Nickel 3.25.1 ug/L 10.0 1.61 1 04/03/23 09:02 04/03/23 19:48 7440-02-0 J Selenium ND ug/L 10.0 7.35 1 04/03/23 09:02 04/03/23 19:48 7782-49-2 Silver ND ug/L 5.00 1.54 1 04/03/23 09:02 04/03/23 19:48 7440-22-4 Vanadium ND ug/L 20.0 4.99 1 04/03/23 09:02 04/03/23 19:48 7440-62-2 Zinc 8.44.1 ug/L 50.0 6.52 1 04/03/23 09:02 04/03/23 19:48 7440-66-6 J Metals (ICPMS) 6020B Analytical Method: EPA 6020E Preparation Method: 3015 Pace National - Mt. Juliet Thallium ND ug/L 2.00 0.121 1 04/05/23 01:56 04/05/23 10:55 7440-28-0 Mercury 7470A Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane Date: 04/20/2023 03:37 PM Analytical Method: EPA 7470A Preparation Method: 7470A Pace National - Mt. Juliet ND ug/L 0.200 0.100 1 04/05/23 10:35 04/05/23 21:54 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 04/07/23 02:32 67-64-1 1.8 1 04/07/23 02:32 107-13-1 0.34 1 04/07/23 02:32 71-43-2 0.47 1 04/07/23 02:32 74-97-5 0.31 1 04/07/23 02:32 75-27-4 0.34 1 04/07/23 02:32 75-25-2 1.7 1 04/07/23 02:32 74-83-9 4.0 1 04/07/23 02:32 78-93-3 0.36 1 04/07/23 02:32 75-15-0 0.33 1 04/07/23 02:32 56-23-5 0.28 1 04/07/23 02:32 108-90-7 0.65 1 04/07/23 02:32 75-00-3 0.43 1 04/07/23 02:32 67-66-3 0.54 1 04/07/23 02:32 74-87-3 0.34 1 04/07/23 02:32 96-12-8 0.36 1 04/07/23 02:32 124-48-1 0.27 1 04/07/23 02:32 106-93-4 0.39 1 04/07/23 02:32 74-95-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-3RR Lab ID: 92659639004 Collected: 03/29/23 16:30 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 04/20/2023 03:37 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.34 1 04/07/23 02:32 95-50-1 ND ug/L 1.0 0.33 1 04/07/23 02:32 106-46-7 ND ug/L 1.0 0.56 1 04/07/23 02:32 110-57-6 ND ug/L 1.0 0.37 1 04/07/23 02:32 75-34-3 ND ug/L 1.0 0.32 1 04/07/23 02:32 107-06-2 ND ug/L 1.0 0.35 1 04/07/23 02:32 75-35-4 ND ug/L 1.0 0.38 1 04/07/23 02:32 156-59-2 ND ug/L 1.0 0.40 1 04/07/23 02:32 156-60-5 ND ug/L 1.0 0.36 1 04/07/23 02:32 78-87-5 ND ug/L 1.0 0.36 1 04/07/23 02:32 10061-01-5 ND ug/L 1.0 0.36 1 04/07/23 02:32 10061-02-6 ND ug/L 1.0 0.30 1 04/07/23 02:32 100-41-4 ND ug/L 5.0 0.48 1 04/07/23 02:32 591-78-6 ND ug/L 20.0 9.7 1 04/07/23 02:32 74-88-4 ND ug/L 5.0 2.0 1 04/07/23 02:32 75-09-2 ND ug/L 5.0 2.7 1 04/07/23 02:32 108-10-1 ND ug/L 1.0 0.29 1 04/07/23 02:32 100-42-5 ND ug/L 1.0 0.31 1 04/07/23 02:32 630-20-6 ND ug/L 1.0 0.22 1 04/07/23 02:32 79-34-5 ND ug/L 1.0 0.29 1 04/07/23 02:32 127-18-4 ND ug/L 1.0 0.24 1 04/07/23 02:32 108-88-3 ND ug/L 1.0 0.81 1 04/07/23 02:32 87-61-6 ND ug/L 1.0 0.33 1 04/07/23 02:32 71-55-6 ND ug/L 1.0 0.32 1 04/07/23 02:32 79-00-5 ND ug/L 1.0 0.38 1 04/07/23 02:32 79-01-6 ND ug/L 1.0 0.30 1 04/07/23 02:32 75-69-4 ND ug/L 1.0 0.26 1 04/07/23 02:32 96-18-4 ND ug/L 2.0 1.3 1 04/07/23 02:32 108-05-4 ND ug/L 1.0 0.39 1 04/07/23 02:32 75-01-4 ND ug/L 1.0 0.34 1 04/07/23 02:32 1330-20-7 98 % 70-130 1 04/07/23 02:32 460-00-4 98 % 70-130 1 04/07/23 02:32 17060-07-0 97 % 70-130 1 04/07/23 02:32 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 20.2 ug/L 2.0 0.86 1 04/05/23 02:01 123-91-1 82 % 67-130 1 04/05/23 02:01 17060-07-0 88 % 70-130 1 04/05/23 02:01 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 163000 ug/L 5000 5000 1 04/06/2319:56 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: MW-3RR Parameters Lab ID: 92659639004 Collected: Report Results Units Limit 03/29/23 16:30 MDL DF Received: 03/30/23 10:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 192 mg/L 25.0 25.0 1 03/31/23 19:58 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 2870 ug/L 1000 500 1 04/01/23 03:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 21600 ug/L 1000 500 1 04/05/2319:17 16887-00-6 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: TRIP BLANK Parameters 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV Low Level -Acrolein Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Date: 04/20/2023 03:37 PM ANALYTICAL RESULTS Lab ID: 92659639005 Collected: 03/29/23 00:00 Received: 03/30/23 10:00 Matrix: Water Report Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 04/04/23 22:32 123-91-1 83 % 67-130 89 % 70-130 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 10.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 1 04/04/23 22:32 17060-07-0 1 04/04/23 22:32 2037-26-5 5.1 1 04/01/23 06:46 67-64-1 24.8 1 04/01/23 06:46 75-05-8 8.5 1 04/01/23 06:46 107-02-8 1.8 1 04/01/23 06:46 107-13-1 0.50 1 04/01/23 06:46 107-05-1 0.34 1 04/01/23 06:46 71-43-2 0.47 1 04/01/23 06:46 74-97-5 0.31 1 04/01/23 06:46 75-27-4 0.34 1 04/01/23 06:46 75-25-2 1.7 1 04/01/23 06:46 74-83-9 4.0 1 04/01/23 06:46 78-93-3 0.36 1 04/01/23 06:46 75-15-0 0.33 1 04/01/23 06:46 56-23-5 0.28 1 04/01/23 06:46 108-90-7 0.65 1 04/01/23 06:46 75-00-3 0.43 1 04/01/23 06:46 67-66-3 0.54 1 04/01/23 06:46 74-87-3 1.6 1 04/01/23 06:46 126-99-8 0.34 1 04/01/23 06:46 96-12-8 0.36 1 04/01/23 06:46 124-48-1 0.27 1 04/01/23 06:46 106-93-4 0.39 1 04/01/23 06:46 74-95-3 0.34 1 04/01/23 06:46 95-50-1 0.34 1 04/01/23 06:46 541-73-1 0.33 1 04/01/23 06:46 106-46-7 0.56 1 04/01/23 06:46 110-57-6 0.35 1 04/01/23 06:46 75-71-8 0.37 1 04/01/23 06:46 75-34-3 0.32 1 04/01/23 06:46 107-06-2 0.35 1 04/01/23 06:46 75-35-4 0.38 1 04/01/23 06:46 156-59-2 0.40 1 04/01/23 06:46 156-60-5 0.36 1 04/01/23 06:46 78-87-5 0.28 1 04/01/23 06:46 142-28-9 0.39 1 04/01/23 06:46 594-20-7 0.43 1 04/01/23 06:46 563-58-6 0.36 1 04/01/23 06:46 10061-01-5 0.36 1 04/01/23 06:46 10061-02-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 Sample: TRIP BLANK Lab ID: 92659639005 Collected: 03/29/23 00:00 Received: 03/30/23 10:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level -Acrolein Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pentanone (MIBK) Naphthalene Propionitrile Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 04/20/2023 03:37 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.30 1 04/01/23 06:46 100-41-4 ND ug/L 1.0 0.28 1 04/01/23 06:46 97-63-2 ND ug/L 2.0 1.5 1 04/01/23 06:46 87-68-3 ND ug/L 5.0 0.48 1 04/01/23 06:46 591-78-6 ND ug/L 20.0 9.7 1 04/01/23 06:46 74-88-4 ND ug/L 100 52.3 1 04/01/23 06:46 78-83-1 ND ug/L 10.0 4.2 1 04/01/23 06:46 126-98-7 ND ug/L 5.0 2.0 1 04/01/23 06:46 75-09-2 ND ug/L 2.0 0.32 1 04/01/23 06:46 80-62-6 ND ug/L 5.0 2.7 1 04/01/23 06:46 108-10-1 ND ug/L 1.0 0.64 1 04/01/23 06:46 91-20-3 ND ug/L 20.0 3.6 1 04/01/23 06:46 107-12-0 ND ug/L 1.0 0.29 1 04/01/23 06:46 100-42-5 ND ug/L 1.0 0.31 1 04/01/23 06:46 630-20-6 ND ug/L 1.0 0.22 1 04/01/23 06:46 79-34-5 ND ug/L 1.0 0.29 1 04/01/23 06:46 127-18-4 ND ug/L 1.0 0.24 1 04/01/23 06:46 108-88-3 ND ug/L 1.0 0.64 1 04/01/23 06:46 120-82-1 ND ug/L 1.0 0.33 1 04/01/23 06:46 71-55-6 ND ug/L 1.0 0.32 1 04/01/23 06:46 79-00-5 ND ug/L 1.0 0.38 1 04/01/23 06:46 79-01-6 ND ug/L 1.0 0.30 1 04/01/23 06:46 75-69-4 ND ug/L 1.0 0.26 1 04/01/23 06:46 96-18-4 ND ug/L 2.0 1.3 1 04/01/23 06:46 108-05-4 ND ug/L 1.0 0.39 1 04/01/23 06:46 75-01-4 ND ug/L 1.0 0.34 1 04/01/23 06:46 1330-20-7 100 % 70-130 1 04/01/23 06:46 460-00-4 100 % 70-130 1 04/01/23 06:46 17060-07-0 93 % 70-130 1 04/01/23 06:46 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 32 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 2034529 Analysis Method: EPA 8151A QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151A Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: R3910270-1 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 0.547 04/06/23 00:08 Dinoseb ug/L ND 2.00 0.250 04/06/23 00:08 2,4,5-T ug/L ND 2.00 0.258 04/06/23 00:08 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 04/06/23 00:08 2,4-DCAA (S) % 59 14.0-158 04/06/23 00:08 LABORATORY CONTROL SAMPLE & LCSD: R3910270-2 R3910270-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 2.84 3.51 56.8 70.2 50.0-120 21.1 20 P9,R1 Dinoseb ug/L 5.00 3.39 4.01 67.8 80.2 36.0-134 16.8 20 2,4,5-T ug/L 5.00 3.22 3.98 64.4 79.6 54.0-120 21.1 20 R1 2,4,5-TP (Silvex) ug/L 5.00 2.65 3.41 53.0 68.2 50.0-125 25.1 20 P9,R1 2,4-DCAA (S) % 66.4 83.4 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 763417 Analysis Method: RSK-175 QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases Laboratory: Pace Analytical Gulf Coast Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 2470311 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Methane ug/L ND 5.0 2.0 04/10/23 07:24 LABORATORY CONTROL SAMPLE & LCSD: 2470312 2470313 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Methane ug/L 380 280 370 73 98 70-130 29 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 2034556 Analysis Method: EPA 6010D QC Batch Method: 3015 Analysis Description: Metals (ICP) 6010D Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: R3908792-1 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 10.0 4.30 04/03/2318:54 Arsenic ug/L ND 10.0 4.40 04/03/2318:54 Barium ug/L ND 5.00 0.736 04/03/2318:54 Beryllium ug/L ND 2.00 0.330 04/03/2318:54 Cadmium ug/L ND 2.00 0.479 04/03/2318:54 Chromium ug/L ND 10.0 1.40 04/03/2318:54 Cobalt ug/L ND 10.0 0.840 04/03/2318:54 Copper ug/L ND 10.0 3.68 04/03/2318:54 Iron ug/L ND 100 18.0 04/03/2318:54 Lead ug/L ND 6.00 2.99 04/03/2318:54 Manganese ug/L ND 10.0 0.934 04/03/2318:54 Nickel ug/L ND 10.0 1.61 04/03/2318:54 Selenium ug/L ND 10.0 7.35 04/03/2318:54 Silver ug/L ND 5.00 1.54 04/03/2318:54 Tin ug/L ND 50.0 4.87 04/03/2318:54 Vanadium ug/L ND 20.0 4.99 04/03/2318:54 Zinc ug/L ND 50.0 6.52 04/03/2318:54 LABORATORY CONTROL SAMPLE: R3908792-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 1000 966 96.6 80.0-120 Arsenic ug/L 1000 968 96.8 80.0-120 Barium ug/L 1000 1020 102 80.0-120 Beryllium ug/L 1000 949 94.9 80.0-120 Cadmium ug/L 1000 974 97.4 80.0-120 Chromium ug/L 1000 943 94.3 80.0-120 Cobalt ug/L 1000 978 97.8 80.0-120 Copper ug/L 1000 974 97.4 80.0-120 Iron ug/L 10000 9550 95.5 80.0-120 Lead ug/L 1000 968 96.8 80.0-120 Manganese ug/L 1000 901 90.1 80.0-120 Nickel ug/L 1000 953 95.3 80.0-120 Selenium ug/L 1000 1020 102 80.0-120 Silver ug/L 200 186 92.9 80.0-120 Tin ug/L 1000 984 98.4 80.0-120 Vanadium ug/L 1000 979 97.9 80.0-120 Zinc ug/L 1000 962 96.2 80.0-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: GM1.004 OXFORD LANDFILL UNIT 1 92659639 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3908792-4 R3908792-5 MS MSD L1600694-05 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 1000 1000 961 959 96.1 95.9 75.0-125 0.155 20 Arsenic ug/L ND 1000 1000 962 962 96.2 96.2 75.0-125 0.016 20 Barium ug/L 29.5 1000 1000 1040 1030 101 100 75.0-125 0.147 20 Beryllium ug/L ND 1000 1000 941 946 94.1 94.6 75.0-125 0.571 20 Cadmium ug/L ND 1000 1000 965 963 96.5 96.3 75.0-125 0.263 20 Chromium ug/L ND 1000 1000 931 928 93.1 92.8 75.0-125 0.348 20 Cobalt ug/L ND 1000 1000 957 955 95.7 95.5 75.0-125 0.243 20 Copper ug/L ND 1000 1000 965 963 96.5 96.3 75.0-125 0.178 20 Iron ug/L 34.9 10000 10000 9440 9470 94.0 94.4 75.0-125 0.375 20 Lead ug/L ND 1000 1000 954 950 95.4 95.0 75.0-125 0.398 20 Manganese ug/L 1.23 1000 1000 888 886 88.6 88.5 75.0-125 0.166 20 Nickel ug/L ND 1000 1000 933 928 93.3 92.8 75.0-125 0.536 20 Selenium ug/L ND 1000 1000 1010 1010 101 101 75.0-125 0.408 20 Silver ug/L ND 200 200 185 185 92.5 92.4 75.0-125 0.063 20 Tin ug/L ND 1000 1000 975 971 97.5 97.1 75.0-125 0.413 20 Vanadium ug/L ND 1000 1000 970 964 97.0 96.4 75.0-125 0.554 20 Zinc ug/L ND 1000 1000 945 946 94.5 94.6 75.0-125 0.105 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 2034561 Analysis Method: EPA 6020B QC Batch Method: 3015 Analysis Description: Metals (ICPMS) 6020B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: R3909569-1 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 2.00 0.121 04/05/2310:26 LABORATORY CONTROL SAMPLE: R3909569-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 50.0 50.0 100 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909569-4 R3909569-5 MS MSD L1600881-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 4.02 50.0 50.0 54.3 53.6 101 99.1 75.0-125 1.46 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 2034660 Analysis Method: EPA 7470A QC Batch Method: 7470A Analysis Description: Mercury 7470A Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: R3909264-1 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.200 0.100 04/04/2318:46 LABORATORY CONTROL SAMPLE: R3909264-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 3.00 2.84 94.6 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909264-3 R3909264-4 MS MSD L1600626-07 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 3.00 3.00 2.91 2.86 96.8 95.3 75.0-125 1.58 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 2035866 Analysis Method: EPA 7470A QC Batch Method: 7470A Analysis Description: Mercury 7470A Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92659639004 METHOD BLANK: R3909862-1 Associated Lab Samples: 92659639004 Parameter Units Mercury ug/L LABORATORY CONTROL SAMPLE: R3909862-2 Parameter Units Mercury ug/L Matrix: Water Blank Reporting Result Limit ND 0.200 Spike LCS Conc. Result 3.00 3.24 MDL Analyzed Qualifiers 0.100 04/05/23 21:32 LCS % Rec % Rec Limits Qualifiers 108 80.0-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3909862-3 R3909862-4 MS MSD L1601546-04 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 3.00 3.00 3.26 3.30 109 110 75.0-125 1.22 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765937 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639004 METHOD BLANK: 3976888 Associated Lab Samples: 92659639004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 04/07/23 00:43 1,1,1-Trichloroethane ug/L ND 1.0 0.33 04/07/23 00:43 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 04/07/23 00:43 1,1,2-Trichloroethane ug/L ND 1.0 0.32 04/07/23 00:43 1,1-Dichloroethane ug/L ND 1.0 0.37 04/07/23 00:43 1,1-Dichloroethene ug/L ND 1.0 0.35 04/07/23 00:43 1,2,3-Trichlorobenzene ug/L ND 1.0 0.81 04/07/23 00:43 1,2,3-Trichloropropane ug/L ND 1.0 0.26 04/07/23 00:43 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 04/07/23 00:43 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 04/07/23 00:43 1,2-Dichlorobenzene ug/L ND 1.0 0.34 04/07/23 00:43 1,2-Dichloroethane ug/L ND 1.0 0.32 04/07/23 00:43 1,2-Dichloropropane ug/L ND 1.0 0.36 04/07/23 00:43 1,4-Dichlorobenzene ug/L ND 1.0 0.33 04/07/23 00:43 2-Butanone (MEK) ug/L ND 5.0 4.0 04/07/23 00:43 2-Hexanone ug/L ND 5.0 0.48 04/07/23 00:43 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 04/07/23 00:43 Acetone ug/L ND 25.0 5.1 04/07/23 00:43 Acrylonitrile ug/L ND 10.0 1.8 04/07/23 00:43 Benzene ug/L ND 1.0 0.34 04/07/23 00:43 Bromochloromethane ug/L ND 1.0 0.47 04/07/23 00:43 Bromodichloromethane ug/L ND 1.0 0.31 04/07/23 00:43 Bromoform ug/L ND 1.0 0.34 04/07/23 00:43 Bromomethane ug/L ND 2.0 1.7 04/07/23 00:43 Carbon disulfide ug/L ND 2.0 0.36 04/07/23 00:43 Carbon tetrachloride ug/L ND 1.0 0.33 04/07/23 00:43 Chlorobenzene ug/L ND 1.0 0.28 04/07/23 00:43 Chloroethane ug/L ND 1.0 0.65 04/07/23 00:43 Chloroform ug/L ND 1.0 0.43 04/07/23 00:43 Chloromethane ug/L ND 1.0 0.54 04/07/23 00:43 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 04/07/23 00:43 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 04/07/23 00:43 Dibromochloromethane ug/L ND 1.0 0.36 04/07/23 00:43 Dibromomethane ug/L ND 1.0 0.39 04/07/23 00:43 Ethylbenzene ug/L ND 1.0 0.30 04/07/23 00:43 lodomethane ug/L ND 20.0 9.7 04/07/23 00:43 Methylene Chloride ug/L ND 5.0 2.0 04/07/23 00:43 Styrene ug/L ND 1.0 0.29 04/07/23 00:43 Tetrachloroethene ug/L ND 1.0 0.29 04/07/23 00:43 Toluene ug/L ND 1.0 0.24 04/07/23 00:43 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 METHOD BLANK: 3976888 Associated Lab Samples: 92659639004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.40 04/07/23 00:43 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 04/07/23 00:43 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 04/07/23 00:43 Trichloroethene ug/L ND 1.0 0.38 04/07/23 00:43 Trichlorofluoromethane ug/L ND 1.0 0.30 04/07/23 00:43 Vinyl acetate ug/L ND 2.0 1.3 04/07/23 00:43 Vinyl chloride ug/L ND 1.0 0.39 04/07/23 00:43 Xylene (Total) ug/L ND 1.0 0.34 04/07/23 00:43 1,2-Dichloroethane-d4 (S) % 98 70-130 04/07/23 00:43 4-Bromofluorobenzene (S) % 100 70-130 04/07/23 00:43 Toluene-d8 (S) % 97 70-130 04/07/23 00:43 LABORATORY CONTROL SAMPLE: 3976889 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 21.2 106 70-130 1,1,1-Trichloroethane ug/L 20 19.0 95 70-130 1,1,2,2-Tetrachloroethane ug/L 20 21.2 106 70-130 1,1,2-Trichloroethane ug/L 20 20.5 102 70-130 1,1-Dichloroethane ug/L 20 18.4 92 70-130 1,1-Dichloroethene ug/L 20 18.2 91 70-130 1,2,3-Trichlorobenzene ug/L 20 22.1 111 70-130 1,2,3-Trichloropropane ug/L 20 20.5 102 70-130 1,2-Dibromo-3-chloropropane ug/L 20 20.8 104 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.7 104 70-130 1,2-Dichlorobenzene ug/L 20 21.3 107 70-130 1,2-Dichloroethane ug/L 20 19.5 97 70-130 1,2-Dichloropropane ug/L 20 19.9 100 70-130 1,4-Dichlorobenzene ug/L 20 21.4 107 70-130 2-Butanone (MEK) ug/L 40 37.1 93 70-134 2-Hexanone ug/L 40 40.2 100 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 39.2 98 70-130 Acetone ug/L 40 31.1 78 70-133 Acrylonitrile ug/L 100 90.6 91 70-130 Benzene ug/L 20 19.5 98 70-130 Bromochloromethane ug/L 20 19.1 96 70-130 Bromodichloromethane ug/L 20 19.7 98 70-130 Bromoform ug/L 20 20.5 103 70-130 Bromomethane ug/L 20 15.2 76 45-151 Carbon disulfide ug/L 20 16.8 84 70-130 Carbon tetrachloride ug/L 20 19.7 99 70-130 Chlorobenzene ug/L 20 20.9 105 70-130 Chloroethane ug/L 20 17.9 90 39-152 Chloroform ug/L 20 19.2 96 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 76 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: Parameter 3976889 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Chloromethane ug/L 20 17.0 85 58-130 cis-1,2-Dichloroethene ug/L 20 18.6 93 70-130 cis-1,3-Dichloropropene ug/L 20 19.8 99 70-130 Dibromochloromethane ug/L 20 20.6 103 70-130 Dibromomethane ug/L 20 20.6 103 70-130 Ethylbenzene ug/L 20 20.4 102 70-130 lodomethane ug/L 40 36.3 91 53-141 Methylene Chloride ug/L 20 15.6 78 66-130 Styrene ug/L 20 21.0 105 70-130 Tetrachloroethene ug/L 20 20.1 100 70-130 Toluene ug/L 20 19.6 98 70-130 trans-1,2-Dichloroethene ug/L 20 18.4 92 70-130 trans- 1,3-Dichloropropene ug/L 20 19.8 99 70-130 trans-1,4-Dichloro-2-butene ug/L 20 22.5 113 57-185 Trichloroethene ug/L 20 20.2 101 70-130 Trichlorofluoromethane ug/L 20 18.2 91 62-130 Vinyl acetate ug/L 40 38.7 97 70-144 Vinyl chloride ug/L 20 14.9 74 62-130 Xylene (Total) ug/L 60 61.3 102 70-130 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: Parameter 3976891 Units 92659923009 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 25.7 129 70-141 1,1,1-Trichloroethane ug/L ND 20 20.6 103 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 24.5 122 69-142 1,1,2-Trichloroethane ug/L ND 20 22.3 111 70-138 1,1-Dichloroethane ug/L ND 20 18.7 94 70-150 1,1-Dichloroethene ug/L ND 20 21.5 107 70-156 1,2,3-Trichlorobenzene ug/L ND 20 27.8 139 70-148 1,2,3-Trichloropropane ug/L ND 20 23.9 120 70-140 1,2-Dibromo-3-chloropropane ug/L ND 20 25.2 126 68-146 1,2-Dibromoethane (EDB) ug/L ND 20 25.2 126 70-138 1,2-Dichlorobenzene ug/L ND 20 26.2 131 70-141 1,2-Dichloroethane ug/L ND 20 21.3 106 69-143 1,2-Dichloropropene ug/L ND 20 22.2 111 68-156 1,4-Dichlorobenzene ug/L ND 20 25.7 128 70-142 2-Butanone (MEK) ug/L ND 40 42.4 106 60-157 2-Hexanone ug/L ND 40 48.5 121 68-146 4-Methyl-2-pentanone (MIBK) ug/L ND 40 43.7 109 70-141 Acetone ug/L ND 40 37.5 94 58-157 Acrylonitrile ug/L ND 100 104 104 69-147 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 MATRIX SPIKE SAMPLE: Parameter 3976891 Units 92659923009 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Benzene ug/L ND 20 22.3 112 70-142 Bromochloromethane ug/L ND 20 21.7 108 70-146 Bromodichloromethane ug/L ND 20 22.0 110 70-139 Bromoform ug/L ND 20 26.4 132 64-140 Bromomethane ug/L ND 20 19.0 95 28-192 Carbon disulfide ug/L ND 20 20.4 102 70-151 Carbon tetrachloride ug/L ND 20 22.5 112 70-148 Chlorobenzene ug/L ND 20 24.9 124 70-141 Chloroethane ug/L ND 20 24.2 121 58-191 Chloroform ug/L ND 20 20.5 103 70-148 Chloromethane ug/L ND 20 22.8 114 43-162 cis-1,2-Dichloroethene ug/L ND 20 20.5 102 68-151 cis-1,3-Dichloropropene ug/L ND 20 22.7 113 70-139 Dibromochloromethane ug/L ND 20 25.7 128 70-144 Dibromomethane ug/L ND 20 22.9 114 70-139 Ethylbenzene ug/L ND 20 23.9 119 70-143 lodomethane ug/L ND 40 45.1 113 35-171 Methylene Chloride ug/L ND 20 8.9 45 62-149 IK,M1,v3 Styrene ug/L ND 20 24.6 123 70-143 Tetrachloroethene ug/L ND 20 23.5 117 70-145 Toluene ug/L ND 20 21.5 107 70-142 trans-1,2-Dichloroethene ug/L ND 20 20.7 103 70-151 trans- 1,3-Dichloropropene ug/L ND 20 22.6 113 70-139 trans-1,4-Dichloro-2-butene ug/L ND 20 25.1 125 51-159 Trichloroethene ug/L ND 20 22.3 112 62-146 Trichlorofluoromethane ug/L ND 20 23.0 115 63-153 Vinyl acetate ug/L ND 40 39.9 100 61-162 Vinyl chloride ug/L ND 20 18.4 92 61-163 Xylene (Total) ug/L ND 60 72.3 121 70-143 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 96 70-130 Toluene-d8 (S) % 97 70-130 SAMPLE DUPLICATE: 3976890 92659670001 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichlorobenzene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 SAMPLE DUPLICATE: 3976890 Parameter Units 92659670001 Result Dup Result RPD Max RPD 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 v2 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 v2 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 Xylene (Total) ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 99 102 4-Bromofluorobenzene (S) % 98 99 Toluene-d8 (S) % 97 96 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765904 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004, 92659639005 METHOD BLANK: 3976660 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004, 92659639005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 04/04/23 20:00 1,2-Dichloroethane-d4 (S) % 80 67-130 04/04/23 20:00 Toluene-d8 (S) % 87 70-130 04/04/23 20:00 LABORATORY CONTROL SAMPLE: 3976661 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 20.6 103 70-130 1,2-Dichloroethane-d4 (S) % 80 67-130 Toluene-d8 (S) % 88 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3976662 3976663 MS MSD 92659666001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 18.6 18.5 92 92 55-137 0 30 H1 1,2-Dichloroethane-d4 (S) % 84 85 67-130 30 Toluene-d8 (S) % 109 80 70-130 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765322 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639005 METHOD BLANK: 3973928 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639005 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 03/31/23 22:54 1,1,1-Trichloroethane ug/L ND 1.0 0.33 03/31/23 22:54 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 03/31/23 22:54 1,1,2-Trichloroethane ug/L ND 1.0 0.32 03/31/23 22:54 1,1-Dichloroethane ug/L ND 1.0 0.37 03/31/23 22:54 1,1-Dichloroethene ug/L ND 1.0 0.35 03/31/23 22:54 1,1-Dichloropropene ug/L ND 1.0 0.43 03/31/23 22:54 1,2,3-Trichloropropane ug/L ND 1.0 0.26 03/31/23 22:54 1,2,4-Trichlorobenzene ug/L ND 1.0 0.64 03/31/23 22:54 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 03/31/23 22:54 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 03/31/23 22:54 1,2-Dichlorobenzene ug/L ND 1.0 0.34 03/31/23 22:54 1,2-Dichloroethane ug/L ND 1.0 0.32 03/31/23 22:54 1,2-Dichloropropane ug/L ND 1.0 0.36 03/31/23 22:54 1,3-Dichlorobenzene ug/L ND 1.0 0.34 03/31/23 22:54 1,3-Dichloropropane ug/L ND 1.0 0.28 03/31/23 22:54 1,4-Dichlorobenzene ug/L ND 1.0 0.33 03/31/23 22:54 2,2-Dichloropropane ug/L ND 1.0 0.39 03/31/23 22:54 2-Butanone (MEK) ug/L ND 5.0 4.0 03/31/23 22:54 2-Hexanone ug/L ND 5.0 0.48 03/31/23 22:54 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 03/31/23 22:54 Acetone ug/L ND 25.0 5.1 03/31/23 22:54 Acetonitrile ug/L ND 50.0 24.8 03/31/23 22:54 Acrolein ug/L ND 10.0 8.5 03/31/23 22:54 Acrylonitrile ug/L ND 10.0 1.8 03/31/23 22:54 Allyl chloride ug/L ND 2.0 0.50 03/31/23 22:54 Benzene ug/L ND 1.0 0.34 03/31/23 22:54 Bromochloromethane ug/L ND 1.0 0.47 03/31/23 22:54 Bromodichloromethane ug/L ND 1.0 0.31 03/31/23 22:54 Bromoform ug/L ND 1.0 0.34 03/31/23 22:54 Bromomethane ug/L ND 2.0 1.7 03/31/23 22:54 Carbon disulfide ug/L ND 2.0 0.36 03/31/23 22:54 Carbon tetrachloride ug/L ND 1.0 0.33 03/31/23 22:54 Chlorobenzene ug/L ND 1.0 0.28 03/31/23 22:54 Chloroethane ug/L ND 1.0 0.65 03/31/23 22:54 Chloroform ug/L ND 1.0 0.43 03/31/23 22:54 Chloromethane ug/L ND 1.0 0.54 03/31/23 22:54 Chloroprene ug/L ND 5.0 1.6 03/31/23 22:54 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 03/31/23 22:54 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 03/31/23 22:54 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 METHOD BLANK: 3973928 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639005 Blank Reporting Parameter Units Result Limit MDL Analyzed Dibromochloromethane ug/L ND 1.0 0.36 03/31/23 22:54 Dibromomethane ug/L ND 1.0 0.39 03/31/23 22:54 Dichlorodifluoromethane ug/L ND 1.0 0.35 03/31/23 22:54 Ethyl methacrylate ug/L ND 1.0 0.28 03/31/23 22:54 Ethylbenzene ug/L ND 1.0 0.30 03/31/23 22:54 Hexachloro-1,3-butadiene ug/L ND 2.0 1.5 03/31/23 22:54 lodomethane ug/L ND 20.0 9.7 03/31/23 22:54 Isobutanol ug/L ND 100 52.3 03/31/23 22:54 Methacrylonitrile ug/L ND 10.0 4.2 03/31/23 22:54 Methyl methacrylate ug/L ND 2.0 0.32 03/31/23 22:54 Methylene Chloride ug/L ND 5.0 2.0 03/31/23 22:54 Naphthalene ug/L ND 1.0 0.64 03/31/23 22:54 Propionitrile ug/L ND 20.0 3.6 03/31/23 22:54 Styrene ug/L ND 1.0 0.29 03/31/23 22:54 Tetrachloroethene ug/L ND 1.0 0.29 03/31/23 22:54 Tetrahydrofuran ug/L ND 10.0 3.5 03/31/23 22:54 Toluene ug/L ND 1.0 0.24 03/31/23 22:54 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 03/31/23 22:54 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 03/31/23 22:54 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 03/31/23 22:54 Trichloroethene ug/L ND 1.0 0.38 03/31/23 22:54 Trichlorofluoromethane ug/L ND 1.0 0.30 03/31/23 22:54 Vinyl acetate ug/L ND 2.0 1.3 03/31/23 22:54 Vinyl chloride ug/L ND 1.0 0.39 03/31/23 22:54 Xylene (Total) ug/L ND 1.0 0.34 03/31/23 22:54 1,2-Dichloroethane-d4 (S) % 98 70-130 03/31/23 22:54 4-Bromofluorobenzene (S) % 98 70-130 03/31/23 22:54 Toluene-d8 (S) % 100 70-130 03/31/23 22:54 LABORATORY CONTROL SAMPLE: Parameter 3973929 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 20 20.1 100 70-130 1,1,1-Trichloroethane ug/L 20 19.2 96 70-130 1,1,2,2-Tetrachloroethane ug/L 20 20.0 100 70-130 1,1,2-Trichloroethane ug/L 20 20.0 100 70-130 1,1-Dichloroethane ug/L 20 18.3 91 70-130 1,1-Dichloroethene ug/L 20 17.4 87 70-130 1,1-Dichloropropene ug/L 20 19.7 99 70-130 1,2,3-Trichloropropane ug/L 20 19.2 96 70-130 1,2,4-Trichlorobenzene ug/L 20 20.2 101 70-130 1,2-Dibromo-3-chloropropane ug/L 20 20.5 102 70-131 1,2-Dibromoethane (EDB) ug/L 20 20.3 102 70-130 1,2-Dichlorobenzene ug/L 20 19.7 98 70-130 Qualifiers v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: Parameter 3973929 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dichloroethane ug/L 20 19.0 95 70-130 1,2-Dichloropropane ug/L 20 19.4 97 70-130 1,3-Dichlorobenzene ug/L 20 19.6 98 70-130 1,3-Dichloropropane ug/L 20 19.0 95 70-130 1,4-Dichlorobenzene ug/L 20 19.4 97 70-130 2,2-Dichloropropane ug/L 20 17.5 88 68-135 2-Butanone (MEK) ug/L 40 34.3 86 70-134 2-Hexanone ug/L 40 37.7 94 70-131 4-Methyl-2-pentanone (MIBK) ug/L 40 37.3 93 70-130 Acetone ug/L 40 34.7 87 70-133 Acetonitrile ug/L 200 169 85 70-130 Acrolein ug/L 100 88.1 88 52-170 Acrylonitrile ug/L 100 89.1 89 70-130 Allyl chloride ug/L 20 17.4 87 70-130 Benzene ug/L 20 18.6 93 70-130 Bromochloromethane ug/L 20 20.1 101 70-130 Bromodichloromethane ug/L 20 19.0 95 70-130 Bromoform ug/L 20 19.0 95 70-130 Bromomethane ug/L 20 16.1 80 45-151 Carbon disulfide ug/L 20 16.2 81 70-130 Carbon tetrachloride ug/L 20 19.0 95 70-130 Chlorobenzene ug/L 20 19.3 97 70-130 Chloroethane ug/L 20 17.4 87 39-152 Chloroform ug/L 20 19.4 97 70-130 Chloromethane ug/L 20 17.5 87 58-130 Chloroprene ug/L 20 17.8 89 70-130 cis-1,2-Dichloroethene ug/L 20 18.2 91 70-130 cis-1,3-Dichloropropene ug/L 20 19.3 97 70-130 Dibromochloromethane ug/L 20 19.4 97 70-130 Dibromomethane ug/L 20 20.1 100 70-130 Dichlorodifluoromethane ug/L 20 19.7 98 54-133 Ethyl methacrylate ug/L 20 18.5 92 70-130 Ethylbenzene ug/L 20 18.9 94 70-130 Hexachloro-1,3-butadiene ug/L 20 19.8 99 70-135 lodomethane ug/L 40 35.4 88 53-141 Isobutanol ug/L 400 346 86 70-136 Methacrylonitrile ug/L 200 171 85 70-130 Methyl methacrylate ug/L 20 18.4 92 70-130 Methylene Chloride ug/L 20 16.6 83 66-130 Naphthalene ug/L 20 21.7 109 70-130 Propionitrile ug/L 200 181 91 70-130 Styrene ug/L 20 19.9 100 70-130 Tetrachloroethene ug/L 20 20.0 100 70-130 Tetrahydrofuran ug/L 200 173 86 70-130 Toluene ug/L 20 19.2 96 70-130 trans-1,2-Dichloroethene ug/L 20 18.5 93 70-130 trans- 1,3-Dichloropropene ug/L 20 19.5 97 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: Parameter 3973929 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers trans-1,4-Dichloro-2-butene ug/L 20 21.6 108 57-185 Trichloroethene ug/L 20 19.3 97 70-130 Trichlorofluoromethane ug/L 20 17.0 85 62-130 Vinyl acetate ug/L 40 34.4 86 70-144 Vinyl chloride ug/L 20 14.3 72 62-130 v3 Xylene (Total) ug/L 60 58.5 98 70-130 1,2-Dichloroethane-d4 (S) % 93 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3973930 MS 92659639002 Spike Parameter Units Result Conc. MSD Spike Conc. 3973931 MS Result MSD MS Result % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.7 21.8 113 109 70-141 4 30 H1 1,1,1-Trichloroethane ug/L ND 20 20 22.3 21.6 111 108 70-150 3 30 H1 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.1 22.3 105 111 69-142 6 30 H1 1,1,2-Trichloroethane ug/L ND 20 20 22.8 22.1 114 110 70-138 3 30 H1 1,1-Dichloroethane ug/L ND 20 20 22.0 20.9 110 105 70-150 5 30 H1 1,1-Dichloroethene ug/L ND 20 20 18.6 17.4 93 87 70-156 6 30 H1 1,1-Dichloropropene ug/L ND 20 20 23.4 22.7 117 113 70-150 3 30 H1 1,2,3-Trichloropropane ug/L ND 20 20 20.8 21.2 104 106 70-140 2 30 H1 1,2,4-Trichlorobenzene ug/L ND 20 20 23.3 22.7 117 114 70-146 3 30 H1 1,2-Dibromo-3- ug/L ND 20 20 23.1 21.5 116 108 68-146 7 30 H1 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.5 21.5 112 108 70-138 4 30 H1 1,2-Dichlorobenzene ug/L ND 20 20 22.5 20.9 113 104 70-141 8 30 H1 1,2-Dichloroethane ug/L ND 20 20 22.2 21.2 111 106 69-143 5 30 H1 1,2-Dichloropropane ug/L ND 20 20 22.8 21.5 114 108 68-156 6 30 H1 1,3-Dichlorobenzene ug/L ND 20 20 22.3 21.7 111 109 70-143 3 30 H1 1,3-Dichloropropane ug/L ND 20 20 21.9 20.9 109 104 70-138 5 30 H1 1,4-Dichlorobenzene ug/L ND 20 20 22.6 21.9 113 110 70-142 3 30 H1 2,2-Dichloropropane ug/L ND 20 20 22.6 22.7 113 114 52-170 1 30 H1 2-Butanone (MEK) ug/L ND 40 40 43.2 42.2 108 106 60-157 2 30 H1 2-Hexanone ug/L ND 40 40 46.4 45.5 116 114 68-146 2 30 H1 4-Methyl-2-pentanone ug/L ND 40 40 46.4 44.1 116 110 70-141 5 30 H1 (MIBK) Acetone ug/L ND 40 40 34.8 34.6 87 86 58-157 1 30 H1 Acetonitrile ug/L ND 200 200 199 197 100 99 66-153 1 30 H1,v3 Acrolein ug/L ND 100 100 89.7 87.5 90 87 10-200 3 30 H1,v3 Acrylonitrile ug/L ND 100 100 107 103 107 103 69-147 4 30 H1 Allyl chloride ug/L ND 20 20 18.9 18.3 95 92 65-153 3 30 H1 Benzene ug/L ND 20 20 21.5 20.5 107 102 70-142 5 30 H1 Bromochloromethane ug/L ND 20 20 22.7 22.1 113 111 70-146 2 30 H1 Bromodichloromethane ug/L ND 20 20 22.0 20.9 110 105 70-139 5 30 H1 Bromoform ug/L ND 20 20 21.4 21.6 107 108 64-140 1 30 H1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3973930 3973931 MS MSD 92659639002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromomethane ug/L ND 20 20 13.6 13.4 68 67 28-192 1 30 H1 Carbon disulfide ug/L ND 20 20 16.4 15.6 82 78 70-151 5 30 H1 Carbon tetrachloride ug/L ND 20 20 21.8 20.5 109 103 70-148 6 30 H1 Chlorobenzene ug/L ND 20 20 22.2 21.5 111 107 70-141 3 30 H1 Chloroethane ug/L ND 20 20 15.9 15.8 79 79 58-191 1 30 H1 Chloroform ug/L ND 20 20 22.9 21.5 114 107 70-148 6 30 H1 Chloromethane ug/L ND 20 20 11.0 10.7 55 53 43-162 3 30 H1 Chloroprene ug/L ND 20 20 21.8 21.0 109 105 69-158 4 30 H1 cis-1,2-Dichloroethene ug/L ND 20 20 22.0 21.1 110 105 68-151 4 30 H1 cis-1,3-Dichloropropene ug/L ND 20 20 22.9 21.7 114 109 70-139 5 30 H1 Dibromochloromethane ug/L ND 20 20 22.3 21.6 112 108 70-144 4 30 H1 Dibromomethane ug/L ND 20 20 21.9 21.0 109 105 70-139 4 30 H1 Dichlorodifluoromethane ug/L ND 20 20 7.6 7.3 38 37 39-171 4 30 H1,M1, v3 Ethyl methacrylate ug/L ND 20 20 23.0 21.7 115 109 70-140 6 30 H1 Ethylbenzene ug/L ND 20 20 22.3 21.5 112 108 70-143 4 30 H1 Hexachloro-1,3-butadiene ug/L ND 20 20 24.2 23.4 121 117 64-163 3 30 H1 lodomethane ug/L ND 40 40 29.8 30.4 75 76 35-171 2 30 H1,v3 Isobutanol ug/L ND 400 400 459 441 115 110 49-152 4 30 H1 Methacrylonitrile ug/L ND 200 200 212 205 106 103 66-145 3 30 H1 Methyl methacrylate ug/L ND 20 20 21.6 19.4 108 97 70-135 11 30 H1 Methylene Chloride ug/L ND 20 20 21.9 21.5 110 107 62-149 2 30 H1,v1 Naphthalene ug/L ND 20 20 25.1 24.4 125 122 67-147 3 30 H1 Propionitrile ug/L ND 200 200 216 210 108 105 69-143 3 30 H1 Styrene ug/L ND 20 20 21.9 22.3 110 111 70-143 2 30 H1 Tetrachloroethene ug/L ND 20 20 21.7 20.8 109 104 70-145 4 30 H1 Tetrahydrofuran ug/L ND 200 200 205 199 103 100 69-144 3 30 H1 Toluene ug/L ND 20 20 21.5 21.2 108 106 70-142 1 30 H1 trans-1,2-Dichloroethene ug/L ND 20 20 20.8 20.3 104 102 70-151 2 30 H1 trans-1,3-Dichloropropene ug/L ND 20 20 22.7 21.7 113 109 70-139 4 30 H1 trans-1,4-Dichloro-2-butene ug/L ND 20 20 22.0 23.7 110 118 51-159 7 30 H1 Trichloroethene ug/L ND 20 20 21.3 21.0 107 105 62-146 2 30 H1 Trichlorofluoromethane ug/L ND 20 20 16.8 15.9 84 80 63-153 5 30 H1,v3 Vinyl acetate ug/L ND 40 40 42.9 41.3 107 103 61-162 4 30 H1 Vinyl chloride ug/L ND 20 20 11.0 10.5 55 52 61-163 5 30 H1,M1, v3 Xylene (Total) ug/L ND 60 60 66.7 65.3 111 109 70-143 2 30 1,2-Dichloroethane-d4 (S) % 100 99 70-130 4-Bromofluorobenzene (S) % 94 102 70-130 Toluene-d8 (S) % 101 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 766042 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 3977305 Matrix: Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 0.017 04/06/23 16:21 4,4'-DDE ug/L ND 0.050 0.024 04/06/23 16:21 4,4'-DDT ug/L ND 0.050 0.026 04/06/23 16:21 Aldrin ug/L ND 0.050 0.014 04/06/23 16:21 alpha-BHC ug/L ND 0.050 0.012 04/06/23 16:21 beta-BHC ug/L ND 0.050 0.049 04/06/23 16:21 Chlordane (Technical) ug/L ND 0.50 0.16 04/06/23 16:21 delta-BHC ug/L ND 0.050 0.014 04/06/23 16:21 Dieldrin ug/L ND 0.050 0.015 04/06/23 16:21 Endosulfan I ug/L ND 0.050 0.017 04/06/23 16:21 Endosulfan II ug/L ND 0.050 0.016 04/06/23 16:21 Endosulfan sulfate ug/L ND 0.050 0.015 04/06/23 16:21 Endrin ug/L ND 0.050 0.018 04/06/23 16:21 Endrin aldehyde ug/L ND 0.050 0.016 04/06/23 16:21 gamma-BHC (Lindane) ug/L ND 0.050 0.012 04/06/23 16:21 Heptachlor ug/L ND 0.050 0.020 04/06/23 16:21 Heptachlor epoxide ug/L ND 0.050 0.028 04/06/23 16:21 Methoxychlor ug/L ND 0.15 0.042 04/06/23 16:21 Toxaphene ug/L ND 0.50 0.22 04/06/23 16:21 Decachlorobiphenyl (S) % 97 10-200 04/06/23 16:21 Tetrachloro-m-xylene (S) % 87 10-182 04/06/23 16:21 LABORATORY CONTROL SAMPLE: 3977306 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.34 137 50-178 4,4'-DDE ug/L 0.25 0.34 134 43-164 4,4'-DDT ug/L 0.25 0.34 137 23-198 Aldrin ug/L 0.25 0.25 102 13-137 alpha-BHC ug/L 0.25 0.26 105 32-161 beta-BHC ug/L 0.25 0.28 111 54-180 delta-BHC ug/L 0.25 0.26 104 42-169 Dieldrin ug/L 0.25 0.31 126 42-173 Endosulfan I ug/L 0.25 0.29 115 44-168 Endosulfan II ug/L 0.25 0.27 109 45-176 Endosulfan sulfate ug/L 0.25 0.29 116 48-178 Endrin ug/L 0.25 0.34 135 46-178 Endrin aldehyde ug/L 0.25 0.36 142 35-168 gamma-BHC (Lindane) ug/L 0.25 0.27 107 38-162 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: 3977306 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Heptachlor ug/L 0.25 0.29 116 25-153 Heptachlor epoxide ug/L 0.25 0.27 110 43-170 Methoxychlor ug/L 0.75 0.84 112 37-187 Decachlorobiphenyl (S) % 125 10-200 Tetrachloro-m-xylene (S) % 104 10-182 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3977307 3977308 MS MSD 92659774007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.42 0.42 0.43 0.37 103 89 13-200 15 30 4,4'-DDE ug/L ND 0.42 0.42 0.42 0.36 102 86 10-182 17 30 4,4'-DDT ug/L ND 0.42 0.42 0.46 0.39 109 93 10-200 17 30 Aldrin ug/L ND 0.42 0.42 0.30 0.24 71 57 10-161 23 30 alpha-BHC ug/L ND 0.42 0.42 0.34 0.29 82 69 10-186 16 30 beta-BHC ug/L ND 0.42 0.42 0.35 0.31 83 75 10-200 11 30 delta-BHC ug/L ND 0.42 0.42 0.29 0.26 71 62 11-199 14 30 Dieldrin ug/L ND 0.42 0.42 0.37 0.34 88 81 10-185 8 30 Endosulfan I ug/L ND 0.42 0.42 0.35 0.32 83 76 10-191 10 30 Endosulfan II ug/L ND 0.42 0.42 0.35 0.31 84 74 10-200 14 30 Endosulfan sulfate ug/L ND 0.42 0.42 0.42 0.36 100 88 17-199 13 30 Endrin ug/L ND 0.42 0.42 0.43 0.37 103 88 11-193 15 30 Endrin aldehyde ug/L ND 0.42 0.42 0.53 0.40 128 96 10-198 29 30 gamma-BHC (Lindane) ug/L ND 0.42 0.42 0.33 0.29 79 68 10-190 14 30 Heptachlor ug/L ND 0.42 0.42 0.36 0.29 85 70 13-166 20 30 Heptachlor epoxide ug/L ND 0.42 0.42 0.33 0.30 80 71 10-200 12 30 Methoxychlor ug/L ND 1.2 1.2 1.2 1.0 97 81 10-200 17 30 Decachlorobiphenyl (S) % 90 73 10-200 Tetrachloro-m-xylene (S) % 86 69 10-182 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 767213 Analysis Method: EPA 8082A QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639003 METHOD BLANK: 3983526 Matrix: Water Associated Lab Samples: 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.21 04/12/23 20:18 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.23 04/12/23 20:18 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.23 04/12/23 20:18 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.25 04/12/23 20:18 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.29 04/12/23 20:18 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.21 04/12/23 20:18 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.16 04/12/23 20:18 Decachlorobiphenyl (S) % 124 10-193 04/12/23 20:18 LABORATORY CONTROL SAMPLE: 3983527 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 4.8 95 34-137 PCB-1260 (Aroclor 1260) ug/L 5 5.0 99 39-145 Decachlorobiphenyl (S) % 82 10-193 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3983528 3983529 MS MSD 92659639003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 9.1 9.1 10.3 6.3 113 69 10-153 48 30 R1 PCB-1260 (Aroclor 1260) ug/L ND 9.1 9.1 9.3 42.6 103 469 10-156 128 30 M1,R1 Decachlorobiphenyl (S) % 107 99 10-193 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 768105 Analysis Method: EPA 8082A QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639001, 92659639002 METHOD BLANK: 3987883 Matrix: Water Associated Lab Samples: 92659639001, 92659639002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.21 04/17/23 09:16 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.23 04/17/23 09:16 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.23 04/17/23 09:16 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.25 04/17/23 09:16 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.29 04/17/23 09:16 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.21 04/17/23 09:16 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.16 04/17/23 09:16 Decachlorobiphenyl (S) % 113 10-193 04/17/23 09:16 LABORATORY CONTROL SAMPLE: 3987884 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 4.6 91 34-137 PCB-1260 (Aroclor 1260) ug/L 5 4.5 90 39-145 Decachlorobiphenyl (S) % 122 10-193 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3987885 3987886 MS MSD 92660170001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 8.3 8.3 8.7 8.4 104 101 10-153 3 30 PCB-1260 (Aroclor 1260) ug/L ND 8.3 8.3 7.6 7.7 91 92 10-156 1 30 Decachlorobiphenyl (S) % 106 86 10-193 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765677 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water APP9 RV MSSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 3975539 Matrix: Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 4.5 04/06/23 10:15 1,3,5-Trinitrobenzene ug/L ND 10.0 5.5 04/06/23 10:15 1,3-Dinitrobenzene ug/L ND 10.0 3.8 04/06/23 10:15 1,4-Naphthoquinone ug/L ND 5.0 4.4 04/06/23 10:15 1-Naphthalenamine ug/L ND 10.0 6.0 04/06/23 10:15 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 1.2 04/06/23 10:15 2,3,4,6-Tetrachlorophenol ug/L ND 10.0 1.5 04/06/23 10:15 2,4,5-Trichlorophenol ug/L ND 10.0 1.4 04/06/23 10:15 2,4,6-Trichlorophenol ug/L ND 10.0 1.6 04/06/23 10:15 2,4-Dichlorophenol ug/L ND 10.0 1.4 04/06/23 10:15 2,4-Dimethylphenol ug/L ND 10.0 1.7 04/06/23 10:15 2,4-Dinitrophenol ug/L ND 50.0 26.0 04/06/23 10:15 2,4-Dinitrotoluene ug/L ND 10.0 1.6 04/06/23 10:15 2,6-Dichlorophenol ug/L ND 10.0 4.2 04/06/23 10:15 2,6-Dinitrotoluene ug/L ND 10.0 1.7 04/06/23 10:15 2-Acetylaminofluorene ug/L ND 10.0 4.1 04/06/23 10:15 2-Chloronaphthalene ug/L ND 10.0 1.7 04/06/23 10:15 2-Chlorophenol ug/L ND 10.0 1.2 04/06/23 10:15 2-Methylnaphthalene ug/L ND 10.0 1.9 04/06/23 10:15 2-Methylphenol(o-Cresol) ug/L ND 10.0 1.9 04/06/23 10:15 2-Naphthalenamine ug/L ND 10.0 5.4 04/06/23 10:15 2-Nitroaniline ug/L ND 20.0 3.0 04/06/23 10:15 2-Nitrophenol ug/L ND 10.0 1.4 04/06/23 10:15 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 1.2 04/06/23 10:15 3,3'-Dichlorobenzidine ug/L ND 20.0 8.1 04/06/23 10:15 3,3'-Dimethylbenzidine ug/L ND 50.0 31.1 04/06/23 10:15 3-Methylcholanthrene ug/L ND 10.0 3.7 04/06/23 10:15 3-Nitroaniline ug/L ND 20.0 3.8 04/06/23 10:15 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 7.8 04/06/23 10:15 4-Aminobiphenyl ug/L ND 10.0 4.7 04/06/23 10:15 4-Bromophenylphenyl ether ug/L ND 10.0 1.8 04/06/23 10:15 4-ChIoro-3-methyl phenol ug/L ND 10.0 3.3 04/06/23 10:15 4-Chloroaniline ug/L ND 20.0 3.6 04/06/23 10:15 4-Chlorophenylphenyl ether ug/L ND 10.0 2.0 04/06/23 10:15 4-Nitroaniline ug/L ND 20.0 5.1 04/06/23 10:15 4-Nitrophenol ug/L ND 50.0 6.6 04/06/23 10:15 5-Nitro-o-toluidine ug/L ND 10.0 3.8 04/06/23 10:15 7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 3.0 04/06/23 10:15 Acenaphthene ug/L ND 10.0 2.0 04/06/23 10:15 Acenaphthylene ug/L ND 10.0 2.0 04/06/23 10:15 v1 IH v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 METHOD BLANK: 3975539 Matrix: Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Acetophenone ug/L ND 10.0 1.5 04/06/23 10:15 Anthracene ug/L ND 10.0 2.3 04/06/23 10:15 Benzo(a)anthracene ug/L ND 10.0 2.7 04/06/23 10:15 Benzo(a)pyrene ug/L ND 10.0 2.8 04/06/23 10:15 Benzo(b)fluoranthene ug/L ND 10.0 2.6 04/06/23 10:15 Benzo(g,h,i)perylene ug/L ND 10.0 2.8 04/06/23 10:15 Benzo(k)fluoranthene ug/L ND 10.0 2.7 04/06/23 10:15 Benzyl alcohol ug/L ND 20.0 2.9 04/06/23 10:15 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.8 04/06/23 10:15 bis(2-Chloroethyl) ether ug/L ND 10.0 1.9 04/06/23 10:15 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 3.7 04/06/23 10:15 Butylbenzylphthalate ug/L ND 10.0 3.1 04/06/23 10:15 Chlorobenzilate ug/L ND 10.0 3.8 04/06/23 10:15 Chrysene ug/L ND 10.0 2.8 04/06/23 10:15 Di-n-butylphthalate ug/L ND 10.0 2.2 04/06/23 10:15 Di-n-octylphthalate ug/L ND 10.0 3.9 04/06/23 10:15 Diallate ug/L ND 10.0 3.4 04/06/23 10:15 Dibenz(a,h)anthracene ug/L ND 10.0 3.0 04/06/23 10:15 Dibenzofuran ug/L ND 10.0 2.1 04/06/23 10:15 Diethylphthalate ug/L ND 10.0 2.0 04/06/23 10:15 Dimethoate ug/L ND 10.0 3.7 04/06/23 10:15 Dimethylphthalate ug/L ND 10.0 2.1 04/06/23 10:15 Diphenylamine ug/L ND 10.0 3.0 04/06/23 10:15 Disulfoton ug/L ND 10.0 4.6 04/06/23 10:15 Ethyl methanesulfonate ug/L ND 20.0 3.0 04/06/23 10:15 Famphur ug/L ND 10.0 6.1 04/06/23 10:15 Fluoranthene ug/L ND 10.0 2.2 04/06/23 10:15 Fluorene ug/L ND 10.0 2.1 04/06/23 10:15 Hexachlorobenzene ug/L ND 10.0 2.2 04/06/23 10:15 Hexachlorocyclopentadiene ug/L ND 10.0 1.6 04/06/23 10:15 Hexachloroethane ug/L ND 10.0 1.4 04/06/23 10:15 Hexachloropropene ug/L ND 10.0 2.7 04/06/23 10:15 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.9 04/06/23 10:15 Isodrin ug/L ND 10.0 2.8 04/06/23 10:15 Isophorone ug/L ND 10.0 1.7 04/06/23 10:15 Isosafrole ug/L ND 10.0 2.5 04/06/23 10:15 Kepone ug/L ND 20.0 14.1 04/06/23 10:15 Methapyrilene ug/L ND 50.0 17.0 04/06/23 10:15 Methyl methanesulfonate ug/L ND 5.0 3.1 04/06/23 10:15 Methyl parathion ug/L ND 10.0 3.7 04/06/23 10:15 N-Nitroso-di-n-butylamine ug/L ND 10.0 2.0 04/06/23 10:15 N-Nitroso-di-n-propylamine ug/L ND 10.0 1.3 04/06/23 10:15 N-Nitrosodiethylamine ug/L ND 10.0 2.3 04/06/23 10:15 N-Nitrosodimethylamine ug/L ND 10.0 1.9 04/06/23 10:15 N-Nitrosodiphenylamine ug/L ND 10.0 3.0 04/06/23 10:15 Qualifiers IH,v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 76 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 METHOD BLANK: 3975539 Matrix: Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Qualifiers N-Nitrosomethylethylamine ug/L ND 10.0 7.5 04/06/23 10:15 N-Nitrosopiperidine ug/L ND 10.0 2.5 04/06/23 10:15 N-Nitrosopyrrolidine ug/L ND 10.0 3.1 04/06/23 10:15 Nitrobenzene ug/L ND 10.0 1.9 04/06/23 10:15 O,O,O-Triethylphosphorothioate ug/L ND 10.0 2.6 04/06/23 10:15 O-Toluidine ug/L ND 10.0 2.6 04/06/23 10:15 P-Dimethylaminoazobenzene ug/L ND 5.0 2.4 04/06/23 10:15 IL p-Phenylenediamine ug/L ND 10.0 10.0 04/06/23 10:15 Parathion (Ethyl parathion) ug/L ND 10.0 3.9 04/06/23 10:15 Pentachlorobenzene ug/L ND 10.0 3.4 04/06/23 10:15 Pentachloronitrobenzene ug/L ND 10.0 3.3 04/06/23 10:15 Pentachlorophenol ug/L ND 20.0 3.8 04/06/23 10:15 Phenacetin ug/L ND 10.0 3.6 04/06/23 10:15 Phenanthrene ug/L ND 10.0 2.0 04/06/23 10:15 Phenol ug/L ND 10.0 1.4 04/06/23 10:15 Phorate ug/L ND 10.0 3.6 04/06/23 10:15 Pronamide ug/L ND 10.0 3.1 04/06/23 10:15 Pyrene ug/L ND 10.0 2.2 04/06/23 10:15 Safrole ug/L ND 10.0 2.3 04/06/23 10:15 Thionazin ug/L ND 10.0 2.9 04/06/23 10:15 2,4,6-Tribromophenol (S) % 109 10-164 04/06/23 10:15 2-Fluorobiphenyl (S) % 94 10-130 04/06/23 10:15 2-Fluorophenol (S) % 73 10-130 04/06/23 10:15 Nitrobenzene-d5 (S) % 95 10-138 04/06/23 10:15 Phenol-d6 (S) % 60 10-130 04/06/23 10:15 Terphenyl-d14 (S) % 103 19-191 04/06/23 10:15 LABORATORY CONTROL SAMPLE: Parameter 3975540 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L 50 37.4 75 10-130 1,3,5-Trinitrobenzene ug/L 50 36.6 73 55-200 v1 1,3-Dinitrobenzene ug/L 50 46.9 94 48-176 1,4-Naphthoquinone ug/L 50 35.5 71 18-130 1-Naphthalenamine ug/L 50 44.9 90 29-149 2,2'-Oxybis(1-chloropropane) ug/L 50 45.5 91 21-135 2,3,4,6-Tetrachlorophenol ug/L 50 56.6 113 39-157 2,4,5-Trichlorophenol ug/L 50 54.0 108 38-147 2,4,6-Trichlorophenol ug/L 50 54.4 109 34-142 2,4-Dichlorophenol ug/L 50 52.9 106 36-136 2,4-Dimethylphenol ug/L 50 82.1 164 38-134 L1 2,4-Dinitrophenol ug/L 250 188 75 10-169 2,4-Dinitrotoluene ug/L 50 54.8 110 44-154 2,6-Dichlorophenol ug/L 50 44.3 89 37-145 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: Parameter 3975540 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,6-Dinitrotoluene ug/L 50 56.6 113 44-156 2-Acetylaminofluorene ug/L 50 48.7 97 25-175 2-Chloronaphthalene ug/L 50 49.8 100 25-130 2-Chlorophenol ug/L 50 49.2 98 29-130 2-Methylnaphthalene ug/L 50 48.1 96 23-130 2-Methylphenol(o-Cresol) ug/L 50 50.1 100 31-130 2-Naphthalenamine ug/L 50 42.9 86 34-147 2-Nitroaniline ug/L 100 103 103 39-145 2-Nitrophenol ug/L 50 54.2 108 29-142 3&4-Methyl phenol (m&p Cresol) ug/L 50 47.7 95 30-130 3,3'-Dichlorobenzidine ug/L 100 116 116 44-158 3,3'-Dimethylbenzidine ug/L 100 183 183 38-2001H 3-Methylcholanthrene ug/L 50 46.1 92 46-153 3-Nitroaniline ug/L 100 111 111 45-152 4,6-Dinitro-2-methyl phenol ug/L 100 114 114 39-158 v1 4-Aminobiphenyl ug/L 50 45.1 90 30-144 4-Bromophenylphenyl ether ug/L 50 51.8 104 47-147 4-Chloro-3-methylphenol ug/L 100 104 104 40-138 4-Chloroaniline ug/L 100 99.9 100 35-130 4-Chlorophenylphenyl ether ug/L 50 50.0 100 36-139 4-Nitroaniline ug/L 100 107 107 46-157 4-Nitrophenol ug/L 250 177 71 17-130 5-Nitro-o-toluidine ug/L 50 49.7 99 50-182 7,12-Dimethylbenz(a)anthracene ug/L 50 51.1 102 46-157 Acenaphthene ug/L 50 50.3 101 34-135 Acenaphthylene ug/L 50 51.5 103 35-137 Acetophenone ug/L 50 49.6 99 30-137 Anthracene ug/L 50 48.0 96 47-146 Benzo(a)anthracene ug/L 50 53.8 108 48-160 Benzo(a)pyrene ug/L 50 53.0 106 47-165 Benzo(b)fluoranthene ug/L 50 57.6 115 49-171 Benzo(g,h,i)perylene ug/L 50 51.5 103 46-166 Benzo(k)fluoranthene ug/L 50 53.3 107 55-162 Benzyl alcohol ug/L 100 95.0 95 29-132 bis(2-Chloroethoxy)methane ug/L 50 49.3 99 33-136 bis(2-Chloroethyl) ether ug/L 50 48.9 98 30-142 bis(2-Ethylhexyl)phthalate ug/L 50 58.5 117 46-173 Butylbenzylphthalate ug/L 50 61.6 123 53-169 Chlorobenzilate ug/L 50 48.9 98 43-155 Chrysene ug/L 50 52.8 106 54-152 Di-n-butylphthalate ug/L 50 52.8 106 49-161 Di-n-octylphthalate ug/L 50 60.5 121 50-166 Diallate ug/L 50 39.2 78 47-136 Dibenz(a,h)anthracene ug/L 50 53.3 107 46-166 Dibenzofuran ug/L 50 49.8 100 37-136 Diethylphthalate ug/L 50 52.2 104 45-149 Dimethoate ug/L 50 44.7 89 49-145 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 76 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: Parameter 3975540 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Dimethylphthalate ug/L 50 51.8 104 43-145 Diphenylamine ug/L 50 51.3 103 49-142 Disulfoton ug/L 50 38.6 77 42-130 Ethyl methanesulfonate ug/L 50 40.1 80 26-135 Famphur ug/L 100 61.6 62 10-130 Fluoranthene ug/L 50 51.6 103 50-153 Fluorene ug/L 50 51.3 103 42-142 Hexachlorobenzene ug/L 50 50.7 101 44-138 Hexachlorocyclopentadiene ug/L 50 51.0 102 10-130 Hexachloroethane ug/L 50 33.8 68 10-130 Hexachloropropene ug/L 50 32.3 65 10-130 Indeno(1,2,3-cd)pyrene ug/L 50 53.1 106 46-166 Isodrin ug/L 50 38.9 78 48-141 Isophorone ug/L 50 53.1 106 36-135 Isosafrole ug/L 50 42.4 85 33-135 Kepone ug/L 100 46.1 46 10-130 Methapyrilene ug/L 50 55.9 112 10-1851H,v1 Methyl methanesulfonate ug/L 50 38.8 78 21-130 Methyl parathion ug/L 50 46.2 92 57-173 N-Nitroso-di-n-butylamine ug/L 50 36.0 72 28-130 N-Nitroso-di-n-propylamine ug/L 50 54.0 108 33-140 N-Nitrosodiethylamine ug/L 50 45.4 91 27-141 N-Nitrosodimethylamine ug/L 50 44.6 89 24-130 N-Nitrosodiphenylamine ug/L 50 51.3 103 46-144 N-Nitrosomethylethylamine ug/L 50 41.2 82 22-141 N-Nitrosopiperidine ug/L 50 45.5 91 36-141 N-Nitrosopyrrolidine ug/L 50 45.3 91 31-145 Nitrobenzene ug/L 50 50.5 101 33-133 O,O,O-Triethylphosphorothioate ug/L 50 40.1 80 30-152 O-Toluidine ug/L 50 43.5 87 30-131 P-Dimethylaminoazobenzene ug/L 50 23.0 46 23-130IL p-Phenylenediamine ug/L ND Parathion (Ethyl parathion) ug/L 50 48.0 96 52-169 Pentachlorobenzene ug/L 50 39.6 79 31-136 Pentachloronitrobenzene ug/L 50 54.2 108 59-177 Pentachlorophenol ug/L 100 110 110 21-163 Phenacetin ug/L 50 47.5 95 52-159 Phenanthrene ug/L 50 50.9 102 47-146 Phenol ug/L 50 33.2 66 19-130 Phorate ug/L 50 42.6 85 35-184 Pronamide ug/L 50 47.6 95 53-155 Pyrene ug/L 50 55.8 112 53-155 Safrole ug/L 50 42.3 85 31-130 Thionazin ug/L 50 41.8 84 46-148 2,4,6-Tribromophenol (S) % 121 10-164 2-Fluorobiphenyl (S) % 98 10-130 2-Fluorophenol (S) % 76 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 LABORATORY CONTROL SAMPLE: 3975540 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrobenzene-d5 (S) % 104 10-138 Phenol-d6 (S) % 64 10-130 Terphenyl-d14 (S) % 114 19-191 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975541 3975542 MS MSD 92659539007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,2,4,5-Tetrachlorobenzene ug/L ND 83.3 83.3 78.2 73.8 94 89 12-130 6 30 1,3,5-Trinitrobenzene ug/L ND 83.3 83.3 83.7 83.2 100 100 34-200 0 30 v1 1,3-Dinitrobenzene ug/L ND 83.3 83.3 103 97.6 123 117 34-183 5 30 1,4-Naphthoquinone ug/L ND 83.3 83.3 81.3 73.0 98 88 14-136 11 30 1-Naphthalenamine ug/L ND 83.3 83.3 86.6 82.4 104 99 10-173 5 30 2,2'-Oxybis(1- ug/L ND 83.3 83.3 68.2 64.8 82 78 11-143 5 30 chloropropane) 2,3,4,6-Tetrachlorophenol ug/L ND 83.3 83.3 90.2 90.1 108 108 10-180 0 30 2,4,5-Trichlorophenol ug/L ND 83.3 83.3 88.3 89.4 106 107 10-170 1 30 2,4,6-Trichlorophenol ug/L ND 83.3 83.3 84.9 86.4 102 104 10-166 2 30 2,4-Dichlorophenol ug/L ND 83.3 83.3 82.8 81.4 99 98 10-153 2 30 2,4-Dimethylphenol ug/L ND 83.3 83.3 129 124 154 149 20-147 3 30 MO 2,4-Dinitrophenol ug/L ND 417 417 403 423 97 101 10-172 5 30 2,4-Dinitrotoluene ug/L ND 83.3 83.3 87.9 86.3 105 104 30-164 2 30 2,6-Dichlorophenol ug/L ND 83.3 83.3 92.9 86.2 112 103 10-161 8 30 2,6-Dinitrotoluene ug/L ND 83.3 83.3 90.9 88.6 109 106 31-163 3 30 2-Acetylam inofl uorene ug/L ND 83.3 83.3 87.2 96.6 105 116 20-166 10 30 2-Chloronaphthalene ug/L ND 83.3 83.3 75.5 76.2 91 91 15-134 1 30 2-Chlorophenol ug/L ND 83.3 83.3 73.3 72.7 88 87 10-139 1 30 2-Methyl naphthalene ug/L ND 83.3 83.3 74.6 71.9 90 86 12-130 4 30 2-Methyl phenol(o-Cresol) ug/L ND 83.3 83.3 74.4 74.4 89 89 19-132 0 30 2-Naphthalenamine ug/L ND 83.3 83.3 89.3 86.4 107 104 10-164 3 30 2-Nitroaniline ug/L ND 167 167 163 160 98 96 23-154 1 30 2-Nitrophenol ug/L ND 83.3 83.3 84.0 83.4 101 100 10-159 1 30 3&4-Methylphenol(m&p ug/L ND 83.3 83.3 71.4 70.1 86 84 13-136 2 30 Cresol) 3,3'-Dichlorobenzidine ug/L ND 167 167 175 174 105 104 10-178 1 30 3,3'-Dimethylbenzidine ug/L ND 167 167 294 290 176 174 10-200 1 30 IH 3-Methylcholanthrene ug/L ND 83.3 83.3 96.8 93.2 116 112 36-158 4 30 3-Nitroaniline ug/L ND 167 167 179 173 107 104 20-166 3 30 4,6-Dinitro-2-methylphenol ug/L ND 167 167 179 186 108 112 10-187 4 30 v1 4-Aminobiphenyl ug/L ND 83.3 83.3 64.6 71.6 78 86 10-181 10 30 4-Bromophenylphenyl ether ug/L ND 83.3 83.3 78.2 81.9 94 98 31-157 5 30 4-Chloro-3-methylphenol ug/L ND 167 167 166 162 99 97 27-146 2 30 4-Chloroaniline ug/L ND 167 167 149 146 89 87 13-143 2 30 4-Chlorophenylphenyl ether ug/L ND 83.3 83.3 76.6 78.0 92 94 23-149 2 30 4-Nitroaniline ug/L ND 167 167 173 163 104 98 24-171 6 30 4-Nitrophenol ug/L ND 417 417 302 296 72 71 10-130 2 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975541 MS 92659539007 Spike Parameter Units Result Conc. MSD Spike Conc. 3975542 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 5-Nitro-o-toluidine ug/L ND 83.3 83.3 111 100 133 120 33-192 10 30 7,12- ug/L ND 83.3 83.3 108 105 129 127 36-161 2 30 Dimethylbenz(a)anthracene Acenaphthene ug/L ND 83.3 83.3 78.0 78.1 94 94 21-147 0 30 Acenaphthylene ug/L ND 83.3 83.3 78.1 78.7 94 94 19-150 1 30 Acetophenone ug/L ND 83.3 83.3 74.7 73.5 90 88 22-145 2 30 Anthracene ug/L ND 83.3 83.3 73.4 75.2 88 90 36-152 2 30 Benzo(a)anth race ne ug/L ND 83.3 83.3 81.4 82.9 98 100 42-163 2 30 Benzo(a)pyrene ug/L ND 83.3 83.3 81.0 81.6 97 98 40-169 1 30 Benzo(b)fluoranthene ug/L ND 83.3 83.3 89.0 90.8 107 109 40-177 2 30 Benzo(g,h,i)perylene ug/L ND 83.3 83.3 80.2 77.5 96 93 38-174 3 30 Benzo(k)fluoranthene ug/L ND 83.3 83.3 81.4 83.7 98 100 41-171 3 30 Benzyl alcohol ug/L ND 167 167 143 142 86 85 18-141 1 30 bis(2- ug/L ND 83.3 83.3 76.7 73.8 92 89 19-146 4 30 Chloroethoxy)methane bis(2-Chloroethyl) ether ug/L ND 83.3 83.3 73.4 71.2 88 85 19-151 3 30 bis(2- Ethyl hexyl)phthalate ug/L ND 83.3 83.3 87.3 91.1 105 109 42-168 4 30 Butylbenzylphthalate ug/L ND 83.3 83.3 92.6 97.4 111 117 42-177 5 30 Chlorobenzilate ug/L ND 83.3 83.3 117 102 141 122 36-158 14 30 Chrysene ug/L ND 83.3 83.3 79.3 80.9 95 97 43-159 2 30 Di-n-butylphthalate ug/L ND 83.3 83.3 81.8 82.3 98 99 42-160 1 30 Di-n-octylphthalate ug/L ND 83.3 83.3 92.8 92.8 111 111 42-171 0 30 Diallate ug/L ND 83.3 83.3 79.5 80.0 95 96 38-139 1 30 Dibenz(a,h)anthracene ug/L ND 83.3 83.3 82.6 80.3 99 96 40-171 3 30 Dibenzofuran ug/L ND 83.3 83.3 76.4 77.1 92 92 23-147 1 30 Diethylphthalate ug/L ND 83.3 83.3 83.7 81.0 100 97 33-157 3 30 Dimethoate ug/L ND 83.3 83.3 95.8 91.0 115 109 41-146 5 30 Dimethylphthalate ug/L ND 83.3 83.3 81.7 80.9 98 97 27-154 1 30 Diphenylamine ug/L ND 83.3 83.3 77.4 80.6 93 97 38-146 4 30 Disulfoton ug/L ND 83.3 83.3 80.1 78.9 96 95 39-130 1 30 Ethyl methanesulfonate ug/L ND 83.3 83.3 84.9 79.9 102 96 25-136 6 30 Famphur ug/L ND 167 167 85.1 85.1 51 51 10-130 0 30 Fluoranthene ug/L ND 83.3 83.3 79.3 78.6 95 94 42-157 1 30 Fluorene ug/L ND 83.3 83.3 80.4 80.6 96 97 25-155 0 30 Hexachlorobenzene ug/L ND 83.3 83.3 77.6 80.5 93 97 32-145 4 30 Hexachlorocyclopentadiene ug/L ND 83.3 83.3 77.5 76.9 93 92 10-130 1 30 Hexachloroethane ug/L ND 83.3 83.3 45.1 44.9 54 54 10-130 0 30 Hexachloropropene ug/L ND 83.3 83.3 73.4 64.3 88 77 10-130 13 30 Indeno(1,2,3-cd)pyrene ug/L ND 83.3 83.3 82.2 80.4 99 97 39-174 2 30 Isodrin ug/L ND 83.3 83.3 83.1 80.6 100 97 34-148 3 30 Isophorone ug/L ND 83.3 83.3 81.4 78.9 98 95 19-146 3 30 Isosafrole ug/L ND 83.3 83.3 90.6 85.6 109 103 25-139 6 30 Kepone ug/L ND 167 167 103 92.5 62 55 10-130 11 30 Methapyrilene ug/L ND 83.3 83.3 ND 36.1J 18 43 10-200 30 IH,v1 Methyl methanesulfonate ug/L ND 83.3 83.3 80.5 76.0 97 91 22-130 6 30 Methyl parathion ug/L ND 83.3 83.3 102 98.7 122 118 48-174 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975541 3975542 MS MSD 92659539007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual N-Nitroso-di-n-butylamine ug/L ND 83.3 83.3 75.3 71.7 90 86 19-130 5 30 N-Nitroso-di-n-propylamine ug/L ND 83.3 83.3 81.1 79.1 97 95 20-150 2 30 N-Nitrosodiethylamine ug/L ND 83.3 83.3 94.9 86.8 114 104 27-140 9 30 N-Nitrosodimethylamine ug/L ND 83.3 83.3 65.9 65.4 79 79 13-130 1 30 N-Nitrosodiphenylamine ug/L ND 83.3 83.3 77.4 80.6 93 97 33-149 4 30 N-Nitrosomethylethylamine ug/L ND 83.3 83.3 83.8 73.8 101 89 22-144 13 30 N-Nitrosopiperidine ug/L ND 83.3 83.3 97.8 90.3 117 108 31-144 8 30 N-Nitrosopyrrolidine ug/L ND 83.3 83.3 92.4 88.2 111 106 27-146 5 30 Nitrobenzene ug/L ND 83.3 83.3 76.3 74.5 92 89 19-145 2 30 0,0,0- ug/L ND 83.3 83.3 86.4 80.2 104 96 25-138 7 30 Triethylphosphorothioate O-Toluidine ug/L ND 83.3 83.3 84.2 80.8 101 97 24-133 4 30 P- ug/L ND 83.3 83.3 47.2 48.8 57 59 17-130 3 30 IL Dimethylaminoazobenzene p-Phenylenediamine ug/L ND ND ND 30 Parathion (Ethyl parathion) ug/L ND 83.3 83.3 104 99.3 125 119 46-168 5 30 Pentachlorobenzene ug/L ND 83.3 83.3 84.0 79.7 101 96 28-140 5 30 Pentachloronitrobenzene ug/L ND 83.3 83.3 111 108 133 130 46-177 2 30 Pentachlorophenol ug/L ND 167 167 181 182 108 109 10-188 1 30 Phenacetin ug/L ND 83.3 83.3 102 97.1 123 116 41-167 5 30 Phenanthrene ug/L ND 83.3 83.3 76.6 78.4 92 94 38-150 2 30 Phenol ug/L ND 83.3 83.3 48.3 49.7 58 60 10-130 3 30 Phorate ug/L ND 83.3 83.3 87.3 87.2 105 105 36-176 0 30 Pronamide ug/L ND 83.3 83.3 101 98.2 121 118 43-159 3 30 Pyrene ug/L ND 83.3 83.3 83.3 88.8 100 107 42-163 6 30 Safrole ug/L ND 83.3 83.3 86.4 79.6 104 96 26-134 8 30 Thionazin ug/L ND 83.3 83.3 94.6 87.7 113 105 37-152 8 30 2,4,6-Tribromophenol (S) % 102 107 10-164 2-Fluorobiphenyl (S) % 84 83 10-130 2-Fluorophenol (S) % 63 62 10-130 Nitrobenzene-d5 (S) % 89 86 10-138 Phenol-d6 (S) % 52 53 10-130 Terphenyl-d14 (S) % 94 100 19-191 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 766385 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: 3979186 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 04/06/23 17:11 LABORATORY CONTROL SAMPLE: 3979187 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51400 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979189 3979190 MS MSD 92659639004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 163000 50000 50000 218000 222000 110 117 80-120 2 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3979191 3979192 MS MSD 92659666001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 96700 50000 50000 154000 155000 114 116 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 76 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765313 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: 3973916 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit Total Dissolved Solids mg/L ND 25.0 LABORATORY CONTROL SAMPLE: 3973917 Spike LCS Parameter Units Conc. Result Total Dissolved Solids mg/L 251 264 SAMPLE DUPLICATE: 3973918 92659509001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 189 184 MDL Analyzed Qualifiers 25.0 03/31 /23 19:53 LCS % Rec % Rec Limits Qualifiers 105 90-110 Max RPD RPD Qualifiers 3 25 SAMPLE DUPLICATE: 3973919 92659750001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids mg/L 61.0 66.0 8 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765654 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 3975496 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 22.0 04/04/23 02:39 LABORATORY CONTROL SAMPLE: 3975497 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 508 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975498 3975499 MS MSD 92659613002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 491 491 97 97 80-120 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975500 3975501 MS MSD 92659613003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 486 511 97 102 80-120 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765128 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: 3972863 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 03/31/23 21:12 LABORATORY CONTROL SAMPLE: 3972864 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 52400 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972865 3972866 MS MSD 92659779003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 1.0 mg/L 50000 50000 53100 53400 104 105 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972867 3972868 MS MSD 92659639002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 47700 50000 50000 99900 95300 104 95 90-110 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765066 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 3972661 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Nitrogen, Nitrate ug/L ND 40.0 10.0 03/31/23 03:17 LABORATORY CONTROL SAMPLE: 3972662 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate ug/L 1500 1440 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972663 3972664 MS MSD 92659588003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, Nitrate ug/L 2.5 mg/L 1500 1500 3920 3970 96 100 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972665 3972666 MS MSD 92659588009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, Nitrate ug/L 4.8 mg/L 1500 1500 6220 6840 93 135 90-110 10 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 766156 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 METHOD BLANK: 3977938 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003, 92659639004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 04/05/2318:48 LABORATORY CONTROL SAMPLE: 3977939 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 21000 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3977940 3977941 MS MSD 92659399002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 48.7 mg/L 10000 10000 57400 58000 87 93 90-110 1 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3977942 3977943 MS MSD 92659463001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 78.8 mg/L 10000 10000 86800 86800 80 80 90-110 0 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 76 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 QC Batch: 765550 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92659639001, 92659639002, 92659639003 METHOD BLANK: 3975100 Matrix: Water Associated Lab Samples: 92659639001, 92659639002, 92659639003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 04/03/23 21:49 LABORATORY CONTROL SAMPLE: 3975101 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 103 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975102 3975103 MS MSD 92659555001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 97.8 102 98 102 80-120 4 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3975104 3975105 MS MSD 92659555002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 89.7 87.6 89 87 80-120 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. WORKORDER QUALIFIERS WO: 92659639 [1] ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. H1 Analysis conducted outside the EPA method holding time. IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 70 of 76 Pace Analytical Services, LLC ceAnalytrcal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: GM1.004 OXFORD LANDFILL UNIT 1 Pace Project No.: 92659639 ANALYTE QUALIFIERS P9 RPD between the primary and confirmatory analysis exceeded 40%. R1 RPD value was outside control limits. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GM1.004 OXFORD 92659639 LANDFILL UNIT 1 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92659639001 MW-5R 8151A 2034529 EPA 8151A 2034529 92659639002 MW-7 8151A 2034529 EPA 8151A 2034529 92659639003 FIELD BLANK UNIT 1 8151A 2034529 EPA 8151A 2034529 92659639001 MW-5R EPA 3510C 766042 EPA 8081 B 766417 92659639002 MW-7 EPA 3510C 766042 EPA 8081 B 766417 92659639003 FIELD BLANK UNIT 1 EPA 3510C 766042 EPA 8081 B 766417 92659639001 MW-5R EPA 3510C 768105 EPA 8082A 768338 92659639002 MW-7 EPA 3510C 768105 EPA 8082A 768338 92659639003 FIELD BLANK UNIT 1 EPA 3510C 767213 EPA 8082A 767466 92659639001 MW-5R RSK-175 763417 92659639002 MW-7 RSK-175 763417 92659639003 FIELD BLANK UNIT 1 RSK-175 763417 92659639001 MW-5R 3015 2034556 EPA6010D 2034556 92659639002 MW-7 3015 2034556 EPA6010D 2034556 92659639003 FIELD BLANK UNIT 1 3015 2034556 EPA6010D 2034556 92659639004 MW-3RR 3015 2034556 EPA6010D 2034556 92659639001 MW-5R 3015 2034561 EPA6020B 2034561 92659639002 MW-7 3015 2034561 EPA6020B 2034561 92659639003 FIELD BLANK UNIT 1 3015 2034561 EPA6020B 2034561 92659639004 MW-3RR 3015 2034561 EPA 6020B 2034561 92659639001 MW-5R 7470A 2034660 EPA 7470A 2034660 92659639002 MW-7 7470A 2034660 EPA 7470A 2034660 92659639003 FIELD BLANK UNIT 1 7470A 2034660 EPA 7470A 2034660 92659639004 MW-3RR 7470A 2035866 EPA 7470A 2035866 92659639001 MW-5R EPA 3510C 765677 EPA 8270E 766258 92659639002 MW-7 EPA 3510C 765677 EPA 8270E 766258 92659639003 FIELD BLANK UNIT 1 EPA 3510C 765677 EPA 8270E 766258 92659639004 MW-3RR EPA 8260D 765937 92659639001 MW-5R EPA 8260D Mod. 765904 92659639002 MW-7 EPA 8260D Mod. 765904 92659639003 FIELD BLANK UNIT 1 EPA 8260D Mod. 765904 92659639004 MW-3RR EPA 8260D Mod. 765904 92659639005 TRIP BLANK EPA 8260D Mod. 765904 92659639001 MW-5R EPA 8260D 765322 92659639002 MW-7 EPA 8260D 765322 92659639003 FIELD BLANK UNIT 1 EPA 8260D 765322 92659639005 TRIP BLANK EPA 8260D 765322 92659639001 MW-5R SM 2320B-2011 766385 92659639002 MW-7 SM 2320B-2011 766385 92659639003 FIELD BLANK UNIT 1 SM 2320E-2011 766385 92659639004 MW-3RR SM 2320B-2011 766385 92659639001 MW-5R SM 2540C-2015 765313 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/20/2023 03:37 PM without the written consent of Pace Analytical Services, LLC. Page 72 of 76 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GM1.004 OXFORD 92659639 LANDFILL UNIT 1 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92659639002 MW-7 SM 2540C-2015 765313 92659639003 FIELD BLANK UNIT 1 SM 2540C-2015 765313 92659639004 MW-3RR SM 2540C-2015 765313 92659639001 MW-5R SM 4500-S2D-2011 765654 92659639002 MW-7 SM 4500-S2D-2011 765654 92659639003 FIELD BLANK UNIT 1 SM 4500-S2D-2011 765654 92659639001 MW-5R EPA 300.0 Rev 2.1 1993 765128 92659639002 MW-7 EPA 300.0 Rev 2.1 1993 765128 92659639003 FIELD BLANK UNIT 1 EPA 300.0 Rev 2.1 1993 765128 92659639004 MW-3RR EPA 300.0 Rev 2.1 1993 765128 92659639001 MW-5R EPA 353.2 Rev 2.0 1993 765066 92659639002 MW-7 EPA 353.2 Rev 2.0 1993 765066 92659639003 FIELD BLANK UNIT 1 EPA 353.2 Rev 2.0 1993 765066 92659639001 MW-5R SM 4500-CI-E-2011 766156 92659639002 MW-7 SM 4500-CI-E-2011 766156 92659639003 FIELD BLANK UNIT 1 SM 4500-CI-E-2011 766156 92659639004 MW-3RR SM 4500-CI-E-2011 766156 92659639001 MW-5R SM 4500-CN-E-2016 765550 SM 4500-CN-E-2016 765649 92659639002 MW-7 SM 4500-CN-E-2016 765550 SM 4500-CN-E-2016 765649 92659639003 FIELD BLANK UNIT 1 SM 4500-CN-E-2016 765550 SM 4500-CN-E-2016 765649 Date: 04/20/2023 03:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 73 of 76 DC#Title: ENV-=FRM. HUNT- '083.vO; ample Canditlah U06 Floc#Ipt Eiiectiv`e 4411p. 3 ,X4j ► 18: ti,'. M ta-bomtory r!?cocing�siimpl6m, silQvtge xdt-n-cl Gre :pr�taI) 'f-uift9: sville [] [tateigh0 M ltg icsvitleQ. tl�ntal Ker+tie sville ] Cfient Name..: ....:.. ....... _ _. ,_:..: �-�,iother:_0. IWI4II# �I II9I�2� I 6I !�5� �9�� 639lbSPe$u.'r El Cmmertia: EWdCe. 92659639 tvii ly Self Present? r ❑Na Seals Intact7" 'EWS .Yes [,�.Nsi .. • date/IniEiai; PBksoA OPM46000O'ent',_e� , .C}f� . PakittgfatRteClal; $lyla'Wpbble:.tgs ❑N.orte :(]than ajofoglcalTfcsuEFroal�n? Theji*om OYas..dtJb WoferTsrrn� .. . �G r'� �i4ddj5uhiiett (°�} CaoterTerriR-CW'+®.d ('Cr. ''?.� t�i.� .�•�a.... ., USDA ttegi�f�atedr�5oi . � ::.. �W(Ar water sample j.: � � . Dld samples:arigindte:its a_quarantlnsa.. zonewIthlo theitinfiid;Siates: CA, 1A ©r sc ]Blue �Npr<e . Trwl Ihms l:bd4tw6fr6daif'g.tn6WG : Samplesbut;pf.Cemp;c.:kerlm..5arnplevor%lea coQjIr .prdress has bd9un ❑itl asimnla e'rYrieFnaier,i�re,n� � ir,:dliin eei',i.:rs l�..s.,ti„ ��i,... �Yi.. check rnapLA LJ Yes ' 1 i�a - ..�:. _ . -.. - ncl iig a ass Pueittj Rind ? :YES: Aid. fAdi�� .. �l ,_.... ,yaw - G iaits.isf.CuStrrciypttserit?; , Yes bi 3FijA 7 Samples'Arrlv�it:witfil Nold;Tlrne Yes C]Ni+. O.NIA - Sfsort ©66 Ci *AL . I, Rusts °ittWAsOund View a uestO? C1 Ygs M1 () DrWA. Stfl#isientVot3is>?ie7 '' .i�iY�s 1r11�d �.7.NI� 5�.. � � , . earrec>t t o�tai'ners:tl3aett.?.eg p eve: O NIA 6: :.. Pace..ContalwtIAW. Yqa LINO- ©:NIA CiNIA 7.. . l►istol�teri analysts. 5arintilet Field TOte€ed t.. O y$k tj No �►. V. 8:... , $wnpts i a>zeis MatSh;CO, �- Na i sctl�des;Qate :.r ll ltnal sis Matrix: .. ........:::. :.... tiea8 aee I0 MOA Vlal s (t 5.6mm)? O Ye3 . .° ©AtjA. Trtit7ftfslc Rresen#7 es I t{oe QW- A. lA. Tri - i iikCsis2od"5gaitPreseist7Coos ;QNA: 0WA. CDlhlttViMlkfSAMPLE DISCREPANCY -Nelo pata Required? .UYes Li NA Rer-son wntacted„. Date/Time: P[ojsaci M�.rtagpr 5:�i1RFtt®view: Dat"e: . POJ* M8** —sRf RevieW.:: Date; Page 74 of 76 HUMA 83 v02L-S roit C nd t a . U o R pt DOAL-TTRIW-.EN-FRK. 0,0 6 11 h h deal Off rzfr4O.i1v-p.,.1D te: 21A404 AM Ache& mark torrMf:id-bok W-i-PHAnd/or, 4%4110010016rk -k:vff.f"1OacfL"d prqje"WO#:92659639 W.1olin twarcoptikoe tfta:for preseNcit1q. Mojik�. PM: THC Due Date. 04/13/23 W*OOW-yqA. Cpllforo,:%q pdGr pQGrease R51 CLIENT: 92—Hart—Ral .p ***Check- I LWpre:W*0j.1UA ri m X 136 Y. s m M. V4 0 1w mm: m ry ' X 4E, .SE 1 S :.F- S E-' E �C- qq lop ij: 'D ARl' E E Aj g, 'm.. E CCL*' NN i. � r . -'N XJ .�N! 1: L 2. 4 3 �aiii����i�i�i■�■ii� a� ��ii���aii�iiiiiiiia��i�� p"HAO mples svmm r1i. it) 'Typit %if Prosarv'11OW PH !loan rocalp.1 - va jsres ryatton adjtlscs Wn.11 Prese NWOK :adjusted Amau,nt of Pr,6SOfVA1jVe added " tot# ., f: . q GeWntlatne KOFTITEW011na ULUK.Larulication Vince pic, but atba!Oincoffec !es, f6t1VL-jb1jtQfti hers. Page 75 of 76 {NIA} M f t�g►ul 1• a �� salettrag j leloaO 5nn Z e. {N%J ,.... ^ ' tN1A? aul�o 14O l IeeN ,� } 0tryJw-; L AA M2 c E CL" car ��a w 0 .. g W19 dllteuexolp y'4 {�•i © $ 4UNIS i! dlil U E Wiwi+Blalevi Jill ddy ;C i e 3 ` 4WS asEa Aq euexolP V,' lu cr c ' AHL+D9i6 AQ 08h IM ddtl _ � a L4 J2 c _ + 2 C IoueyiaW 1! if JtT c COMM OU g HOeN O Q 'y I m i R EpNM a opatiasaidull t. Up YI 5 a s S113NIVINOO d0 p LL 9 ' N'L173110aIVdPI3131dViVS p� qq W Z F 3 m c c3 N lu LU n �, w id��evu�n] 3dAia7dwv9 �� ' ipalgss�cs�enees) 3d07XIULtlW IL p 9t " a gosda}a"aok 5I jLd2 SI A W . � CL Jog ►�R t `j 4C roNz FIR U?o o � � � � � ,�'" � • � � � � 7r of 76 a Q # IIV311Lu ANSI 9� a a �� Appendix C Summary of Historical Groundwater Elevations 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix C Summary of Historical Groundwater Elevations Granville County Oxford Unit 2 Landfill Oxford North Carolina H&H Job No. GMI-005 Date Groundwater Elevations (ft AMSL) Background Downgradient MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S 06/13/12 513.48 503.31 479.70 477.42 473.20 468.81 08/22/12 509.73 500.82 477.97 475.31 471.50 469.36 09/25/12 508.45 499.85 478.10 475.06 471.86 469.30 10/17/12 507.95 499.90 478.00 474.23 471.04 467.98 08/06/13 514.33 499.92 478.81 475.32 472.80 469.29 02/25/14 511.75 499.91 480.34 476.26 473.47 470.28 08/12/14 511.98 500.16 479.91 476.54 473.42 470.29 03/12/15 516.39 499.99 479.73 476.47 473.66 470.63 08/18/15 512.39 499.86 478.41 474.92 472.17 469.25 02/16/16 515.79 499.90 481.44 476.37 474.12 471.15 08/10/16 514.29 499.82 478.86 475.51 472.91 470.40 02/14/17 510.89 496.36 479.36 475.97 472.77 468.85 08/23/17 508.84 499.61 477.86 474.74 472.02 469.80 02/07/18 505.74 499.86 479.88 476.25 473.54 471.40 08/14/18 510.22 499.95 478.22 475.31 473.57* 470.81 02/05/19 515.74 500.01 480.72 476.63 474.03 472.18 08/07/19 512.11 500.15 478.86 475.75 473.09 472.31 09/04/19 NM NM NM 475.09 NM NM 02/12/20 511.37 499.99 481.41 477.10 475.06 472.76 03/19/20 512.89 NM NM 476.33 473.90 471.82 04/23/20 NM NM NM NM NM 472.06 08/26/20 512.24 499.98 479.78 476.64 473.97 453.00 09/29/20 NM N M NM 476.76 NM N M 02/10/21 517.28 499.88 481.52 476.92 474.32 472.06 08/18/21 511.96 500.19 478.96 475.95 473.13 471.20 02/15/22 507.49 500.10 479.40 476.18 473.22 471.26 10/05/22 507.52 500.22 478.06 476.57 473.52 472.23 03/30/23 510.71* 499.99 479.31 476.69 473.98 472.38* Notes: Groundwater elevations from June 2012 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Groundwater elevations from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. ft AMSL = ft above mean sea level; NM = not measured; * = measurement collected on 03/29/23 Appendix C (Page 1 of 1) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables.xlsx Appendix D Summary of Historical Constituents in Groundwater 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Inorganics Antimony 02/15/22 3 --- ND ND ND ND --- 10/05/22 3 ND ND 0.28 J ND ND ND NC2L = 1 pg/L 03/30/23 4.30 ND ND ND ND ND ND Arsenic 03/12/15 2.5 4.2 J ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND NC2L = 10 pg/L 02/18/16 2.5 ND ND 2.7 ND 3.9 J ND 08/11/16 2.5 ND ND ND 3.1 J 3.2 J ND 02/14/17 5 ND ND ND ND ND ND 08/23/17 5 ND ND ND ND ND ND 02/06/18 --- ND ND ND ND ND ND 08/16/18 5 ND ND ND ND NA ND 02/05/19 5 ND ND ND ND ND ND 08/08/19 5 ND ND ND ND ND ND 02/14/20 4.7 ND ND ND ND ND --- 03/19/20 4.7 ND NS NS NS NS ND 08/26/20 4.7 ND ND ND ND ND J 5.2 J 02/10/21 4.7 4.7 J 5.5 J ND ND --- ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 4.7 5.9 J 4.9 J 5.4 J ND ND NA 10/05/22 4.7 ND 1.4 0.37 J 0.33 J 0.19 J ND 03/30/23 4.40 ND ND ND ND ND ND Barium 06/13/12 --- 9.2 J 36.8 J 59.2 J 48.2 J 30.6 J 31.4 J 08/22/12 --- ND 37.3 J 60.9 J 58.9 J 85 J 28.2 J NC2L = 700 fag/L 09/25/12 --- 10.3 J 40.8 J 64.2 J 72.7 J 43.8 J 30.5 J 10/17/12 --- 24.2 J 57.3 J 65.1 J 48.7 J 110 28 J 08/06/13 --- ND 37.1 J 66.5 J 36.8 J 28.5 J 24.8 J 02/25/14 --- ND 43.6 J 65 J 41.1 J 20.3 J 58.6 J 08/13/14 5 6.2 J 52.7 J 72.7 J 40.7 J 19.7 J 21.7 J 03/12/15 2.5 9.8 J 47.9 J 76.3 J 49.1 J 19.1 J 35.5 J 08/18/15 --- 11 J 45.6 J 72.1 J 43.5 J 20.5 J 31.3 J 02/18/16 2.5 14.8 J 59.5 J 76.1 J 54.2 J 31.8 J 28.6 J 08/11/16 2.5 6.2 J 42.9 J 81 J 61.2 J 49.9 J 31.1 J 02/14/17 2.5 11.8 J 41.9 J 89 J 46.2 J 40.8 J 27.6 J 08/23/17 2.5 25.2 J 42.6 J 126 40.8 J 51.4 J 33.8 J 02/06/18 --- 19.3 J 62.6 J 90.7 J 47.1 J 33.9 J 25.4 J 08/16/18 2.5 3.8 J 40.3 J 68.9 J 47.5 J NA 25.8 J 02/05/19 2.5 4 J 39.8 78 59.4 27.7 19.6 08/08/19 2.5 4.5 J 40.2 71.4 60.5 30.1 ND 02/14/20 1 11 39.3 85 47.2 45 --- 03/19/20 1 NS NS NS NS NS 31.8 08/26/20 3.5 8.8 37.9 73.7 49.3 35.6 32.4 02/10/21 3.5 ND 40.1 76.3 60.6 31.2 ND 08/17/21 --- --- 37.0 76.2 50.2 27.0 --- 02/15/22 3.5 3.8 J 37.5 76.5 37.5 29.0 NA 10/05/22 3.5 4.3 J 38.3 78.4 51.2 28.6 33.7 03/30/23 0.736 3.92 J,B 43.7 81.4 54.0 31.8 38.3 Cadmium 08/23/17 0.5 ND ND ND 0.56 J ND ND 02/06/18 --- ND ND ND ND 0.59 J ND NC2L = 2 pg/L 08/16/18 0.5 ND ND ND ND NA ND 02/05/19 0.5 ND ND ND ND ND ND 08/08/19 0.5 ND ND ND ND ND ND 02/14/20 0.4 ND ND ND ND 0.45 J --- 03/19/20 0.4 NS NS NS NS NS ND 08/26/20 0.4 ND ND ND ND ND ND 02/10/21 0.4 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.4 ND ND ND ND ND NA 10/05/22 0.4 ND ND 0.15 J ND ND ND 03/30/23 0.479 ND ND ND ND ND ND Appendix D (Page 1 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Chromium 06/13/12 --- ND ND ND 10.9 ND ND 08/22/12 --- ND ND ND 10.4 18.3 ND NC21- = 10 pg/L 09/25/12 --- ND ND ND 10.3 ND ND 10/17/12 --- ND ND ND 15.8 20.9 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 --- ND ND ND 5.1 J ND ND 03/12/15 2.5 ND 3 J ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 2.5 ND ND ND ND ND 3 J 08/11/16 2.5 2.8 J ND ND 4.3 J 6.3 J ND 02/14/17 2.5 ND ND ND ND 4.4 J ND 08/23/17 2.5 ND ND ND ND 4.5 J ND 02/06/18 --- 4.4 J ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NA ND 02/05/19 2.5 ND ND ND ND ND ND 08/08/19 2.5 ND ND ND 1 J ND ND 02/14/20 1 3 J ND 1.6 J 2.6 J 8.8 --- 03/19/20 1 NS NS NS NS NS ND 08/26/20 3.7 ND ND ND ND ND ND 02/10/21 3.7 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.7 ND ND ND ND ND NA 10/05/22 3.7 ND ND ND 0.54 J 0.54 J ND 03/30/23 1.40 ND ND ND 2.01 J ND ND Cobalt 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND ND ND ND ND ND NC21- = 1 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- 10.3 ND ND ND 12.4 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5 ND ND ND ND ND ND 03/12/15 2.5 ND ND ND ND ND 3.6 J 08/18/15 --- ND ND ND ND ND ND 02/18/16 2.5 ND ND ND ND ND ND 08/11/16 2.5 ND ND ND ND ND ND 02/14/17 2.5 ND ND ND ND ND 3.2 J 08/23/17 2.5 ND ND ND ND ND ND 02/06/18 --- 3.4 J ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NA ND 02/05/19 2.5 ND ND ND ND ND ND 08/08/19 2.5 ND ND ND ND 1.2 J ND 02/14/20 1.1 2.7 J ND ND ND 3.9 J --- 03/19/20 1.1 NS NS NS NS NS 4.1 J 08/26/20 3.6 ND ND ND ND ND ND 02/10/21 3.6 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.6 ND ND ND ND ND NA 10/05/22 3.6 ND ND 0.052 J 0.73 J 1 ND 03/30/23 0.840 ND ND ND ND ND 1.28 J Copper 06/13/12 --- ND ND ND 46 ND ND 08/22/12 --- ND ND ND 56.2 19.8 ND NC21- = 1,000 pg/L 09/25/12 --- 7.4 J ND ND 63.6 5.7 J ND 10/17/12 --- 19.9 7.6 J ND 35.5 23.1 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND 7.9 J ND ND 08/13/14 5 ND 11.6 ND 13.4 ND ND 03/12/15 2.5 ND 47 ND 6 J ND 3.3 J 08/18/15 --- 2.8 J 26.6 ND 12.3 ND 4.3 J 02/18/16 2.5 ND 7.8 J ND ND ND ND 08/11/16 2.5 ND 30.7 ND 14.6 4.5 J 2.7 J 02/14/17 2.5 ND 16.6 3.2 J 9.9 J 4.9 J 3.9 J 08/23/17 2.5 8.8 J 6.4 J ND 6.4 J 4.5 J ND 02/06/18 --- 18.6 133 3.7 J 5.4 J ND ND 08/16/18 2.5 ND 24.7 ND 3.6 J NA ND 02/05/19 2.5 ND 11 ND 3 J ND ND 08/08/19 2.5 2.5 J 8.3 ND 6.9 ND ND 02/14/20 2.1 5.5 11.8 ND 4.6 J 17.6 --- 03/19/20 2.1 NS NS NS NS NS ND 08/26/20 4.3 ND 10.9 ND 5.6 ND ND 02/10/21 4.3 ND 7.8 ND 4.5 J ND ND 08/17/21 --- --- 4.6 J ND 8.7 ND --- 02/15/22 4.3 ND 4.5 J ND ND ND NA 10/05/22 1.1 ND 12.3 1.2 J ND ND ND 03/30/23 3.68 ND 22.3 ND ND ND ND Appendix D (Page 2 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Iron 02/06/18 --- 9990 1500 1190 1670 1630 353 08/16/18 25 340 --- --- --- NA --- NC2L = 300 pg/L 02/05/19 25 183 --- --- --- --- --- 08/08/19 25 176 --- --- --- --- --- 02/14/20 19.5 3750 --- --- --- --- --- Resample 03/19/20 0.9 1310 NS NS NS ND NS 08/26/20 41.5 1570 --- --- --- --- 1030 02/10/21 41.5 --- --- --- --- -- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA 03/30/23 --- NA NA NA NA NA NA Lead 02/14/17 2.5 ND ND ND ND 2.9 J ND 08/23/17 2.5 ND ND ND ND ND ND NC21- = 15 pg/L 02/06/18 2.5 ND ND ND ND ND ND 08/16/18 2.5 ND ND ND ND NA ND 02/14/20 1.6 ND 1.8 J 1.9 J ND 4.2 J --- 03/19/20 1.6 NS NS NS NS NS ND 02/10/21 1.6 ND ND ND ND ND --- 08/17/21 --- --- ND ND ND ND --- 02/15/22 4.5 ND ND ND ND ND --- 10/05/22 4.5 ND ND ND 0.12 J 0.14 J ND 03/30/23 2.99 ND ND ND ND ND ND Manganese 02/06/18 --- 241 394 53 25.8 J 410 411 08/16/18 2.5 6.7 J --- --- --- NA --- NC21- = 50 pg/L 02/05/19 2.5 5.5 --- --- --- --- --- 08/08/19 2.5 6 --- --- --- --- --- 02/14/20 0.9 85.8 --- --- --- --- --- Resample 03/19/20 0.9 26.4 NS NS NS ND NS 08/26/20 3.4 35.2 --- --- --- --- 431 02/10/21 3.4 --- --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA 03/30/23 --- NA NA NA NA NA NA Nickel 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND ND ND ND 6.1 J ND NC21- = 100 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND 6.9 J 8.9 J ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5 ND ND ND ND ND ND 03/12/15 2.5 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND 2.7 J ND 02/18/16 2.5 ND ND ND ND 2.9 J ND 08/11/16 2.5 ND ND ND ND 6.2 J ND 02/14/17 2.5 ND ND ND ND 5.2 J ND 08/23/17 2.5 5.2 J ND ND 2.8 J 5.8 J ND 02/06/18 --- 5.9 J ND ND ND 3.4 J ND 08/16/18 2.5 ND ND ND ND NA ND 02/05/19 2.5 ND ND ND ND 2.7 J ND 08/08/19 2.5 0.93 J ND ND 1.6 J 3.2 J ND 02/14/20 0.9 2.5 J ND ND 1.3 J 16 --- 03/19/20 0.9 NS NS NS NS NS 1.5 J 08/26/20 3.5 ND ND ND ND 4 J ND 02/10/21 3.5 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.5 --- ND ND ND ND NA 10/05/22 3.5 ND ND ND 0.58 J 2.6 ND 03/30/23 1.61 ND 3.28 J 1.71 J, B ND 3.78 J, B ND Selenium 02/15/22 4.7 --- ND ND ND ND --- 10/05/22 4.7 ND ND 0.27 J ND ND ND NC21- = 20 pg/L 03/30/23 7.35 ND ND ND ND ND ND Appendix D (Page 3 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Thallium 06/13/12 --- ND ND ND ND ND ND 08/22/12 --- ND 6.8 6.8 ND ND ND NC21- = 2 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND ND ND ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 5.4 ND ND ND ND ND ND 03/12/15 5 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 5 ND ND ND ND ND ND 08/11/16 5 ND ND ND ND ND ND 02/14/17 0.02 0.039 J 0.059 J ND ND ND ND 08/23/17 0.02 0.04 J 0.044 J ND ND 0.021 J ND 02/06/18 --- ND 0.034 J ND ND ND ND 08/16/18 0.02 ND ND ND ND NA ND 02/05/19 0.06 ND ND ND ND ND ND 08/08/19 0.06 ND ND ND ND ND ND 02/14/20 0.06 ND ND ND ND ND --- 03/19/20 0.06 NS NS NS NS NS ND 08/26/20 0.05 ND ND ND ND ND ND 02/10/21 0.05 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.05 ND ND ND ND ND NA 10/05/22 0.05 ND ND ND ND ND ND 03/30/23 0.121 ND ND ND ND ND ND Total Dissolved Solids, Dissolved 08/26/20 25000 262000 --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- NC 2L = 500,000 pg/L 02/10/21 25000 274000 --- --- --- --- --- 08/17/21 --- --- NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA 03/30/23 --- NA NA NA NA NA NA Vanadium 06/13/12 --- 5.2 J ND ND 27.8 17.3 J 11 J 08/22/12 --- ND ND ND 30.2 69.5 9 J NC21- = 7 pg/L 09/25/12 --- 8.3 J ND ND 33.4 16.5 J 8.2 J 10/17/12 --- 29.7 ND ND 19.5 J 63.8 J 6.2 J 08/06/13 --- ND ND ND ND 9.2 J ND 02/25/14 --- ND ND ND 10.2 J ND ND 08/13/14 5 ND ND ND 11.8 J ND ND 03/12/15 2.5 ND 4.4 J 7.3 J 5 J ND 6.7 J 08/18/15 --- 6.1 J ND ND 6.5 J 3.6 J 9.1 J 02/18/16 2.5 ND 2.9 J ND ND ND ND 08/11/16 2.5 ND ND 5.8 J 10 J 14.3 J 6.6 J 02/14/17 2.5 ND ND 5.2 J 4 J 9.1 J 5.4 J 08/23/17 2.5 18.6 J ND 2.6 J 4.6 J 11.9 J 6.4 J 02/06/18 --- 23.5 J 3.4 J 4.4 J 4.7 J 3.3 J ND 08/16/18 2.5 ND ND ND 2.9 J NA 2.5 J 02/05/19 2.5 ND ND ND 2.9 J ND ND 08/08/19 2.5 2.2 J ND ND 5.3 1.8 ND Resample 09/04/19 1.3 NS NS NS ND NS NS 02/14/20 1.3 9.2 ND 3.4 J 5.5 13.3 --- 03/19/20 1.3 7.9 J NS NS 3.2 J ND 5.6 Resample 04/23/20 1.3 NS NS NS NS NS 3 J 08/26/20 3.9 4.4 J ND ND 5.5 ND ND 09/29/20 3.9 --- --- --- ND --- --- 02/10/21 3.9 ND ND ND 4.4 J ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 3.9 ND ND ND ND ND NA 10/05/22 3.9 ND ND 3.1 1.7 1.1 ND 03/30/23 4.99 ND ND ND ND ND ND Zinc 06/13/12 --- ND ND ND 10.5 ND ND 08/22/12 --- ND ND 32 31 21.9 10.6 NC21-= 1,000 pg/L 09/25/12 --- 11.7 ND ND 14.8 ND ND 10/17/12 --- 32.5 ND ND 10.5 29 ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 10 ND ND ND ND ND ND 03/12/15 5 9.8 B 10.9 B 10.7 B 8.7 B 7.8 B 9.9 B 08/18/15 --- 8.9 B ND ND ND ND 5.2 B 02/18/16 5 ND 13.1 ND ND ND 8.6 J 08/11/16 5 7.2 J 5.4 J ND 19.5 11.7 8.7 J 02/14/17 5 7 J 6 J 5.4 J 5.3 J 8.3 J 6 J 08/23/17 5 18 ND 6.3 J 5.1 J 15.5 6.9 J 02/06/18 --- ND ND ND ND ND ND 08/16/18 5 ND ND ND ND NA ND 02/05/19 5 ND ND ND ND ND ND 08/08/19 5 ND ND ND ND ND ND 02/14/20 3.9 9.6 J ND ND ND 20.2 --- 03/19/20 3.9 NS NS NS NS NS ND 08/26/20 9.5 ND ND ND ND ND ND 02/10/21 9.5 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 9.5 ND ND ND ND ND NA 10/05/22 9.5 ND ND ND ND ND ND 03/30/23 6.52 ND ND ND 9.33 J 9.03 J ND Appendix D (Page 4 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Organics 1,4-Dioxane 08/16/18 1.9 ND ND ND ND NA ND 02/05/19 1.9 ND ND ND ND ND ND NC21- = 3 pg/L 08/08/19 1.9 ND ND ND ND ND ND 02/14/20 1.2 ND ND ND ND ND ND 08/26/20 1.2 ND ND ND ND ND ND 02/10/21 1.2 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.86 ND ND ND ND ND --- 10/05/22 0.86 1.7 J ND ND ND ND ND 03/30/23 0.86 ND ND ND ND ND ND 2-Butanone (MEK) 02/15/22 4 --- ND ND ND ND --- 10/05/22 4 5.1 11.4 7.7 ND ND ND NC21- = 4,000 pg/L 03/30/23 4.0 ND ND ND ND ND ND 2-Hexanone 02/15/22 0.48 --- ND ND ND ND --- 10/05/22 0.48 ND ND 0.71 J ND ND ND NC21- = 40 pg/L 03/30/23 0.48 ND ND ND ND ND ND Chloromethane 02/15/22 0.54 --- ND ND ND ND --- 10/05/22 0.86 ND ND ND ND ND ND NC21- = 3 pg/L 03/30/23 0.54 ND ND ND ND ND ND cis- 1,2-Dichloroethene 08/18/15 5 0.71 J 0.36 J ND ND ND ND 02/18/16 5 ND ND ND ND ND ND NC21- = 70 pg/L 08/11/16 5 ND ND ND ND ND ND 02/14/17 0.19 ND ND ND ND ND ND 08/23/17 0.19 ND ND ND ND ND ND 02/06/18 0.19 ND ND ND ND ND ND 08/16/18 0.19 ND ND ND ND NA ND 02/05/19 0.29 ND ND ND ND ND ND 08/08/19 0.29 ND ND ND ND ND ND 02/14/20 0.29 ND ND ND ND ND ND 08/26/20 0.29 ND ND ND ND ND ND 02/10/21 0.29 --- ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.38 ND ND ND ND ND --- 10/05/22 0.38 ND ND ND ND ND ND 03/30/23 0.38 ND ND ND ND ND ND Methylene Chloride 02/14/17 0.97 ND ND ND ND ND ND 08/23/17 0.97 ND ND ND ND ND ND NC21-= 5 pg/L 02/06/18 --- 0 ND ND ND ND ND 08/16/18 0.97 ND 0 ND ND ND ND 02/05/19 3.7 ND ND 0 ND ND ND 08/08/19 3.7 ND ND ND ND ND ND 02/14/20 3.7 ND ND ND ND ND ND 08/26/20 3.7 ND ND ND ND ND ND 02/10/21 3.7 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 2 ND ND ND ND ND --- 10/05/22 2 ND ND ND ND ND ND 03/30/23 2.0 ND ND ND ND ND ND Sulfate 08/26/20 500 53300 --- --- --- --- -- 02/10/21 500 65000 --- --- --- --- 24900 NC21- = 250,000 pg/L 08/17/21 --- NA NA NA NA NA --- 02/15/22 --- NA NA NA NA NA NA 10/05/22 --- NA NA NA NA NA NA 03/30/23 -- NA NA NA NA NA NA Appendix D (Page 5 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix D Summary of Historical Constituents in Groundwater Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL MW-7 MW-8 MW-9 MW-10 MW-11 NES-2S Trichlorofluoromethane 06/13/12 --- ND ND ND ND 0.78 B 0.85 B 08/22/12 --- ND ND ND ND ND ND NC2L = 2,000 pg/L 09/25/12 --- ND ND ND ND ND ND 10/17/12 --- ND ND ND ND ND ND 08/06/13 --- ND ND ND ND ND ND 02/25/14 --- ND ND ND ND ND ND 08/13/14 --- ND ND ND ND ND ND 03/12/15 0.2 ND ND ND ND ND ND 08/18/15 --- ND ND ND ND ND ND 02/18/16 0.2 ND ND ND ND ND ND 08/11/16 0.2 ND ND ND ND ND ND 02/14/17 0.2 ND ND ND ND ND ND 08/23/17 0.2 ND ND ND ND ND ND 02/06/18 --- ND ND ND ND ND ND 08/16/18 0.2 ND ND ND ND NA ND 02/05/19 0.31 ND ND ND ND ND ND 08/08/19 0.31 ND ND ND ND ND ND 02/14/20 0.31 ND ND ND ND ND ND 08/26/20 0.31 ND ND ND ND ND ND 02/10/21 0.31 ND ND ND ND ND ND 08/17/21 --- --- ND ND ND ND --- 02/15/22 0.3 ND ND ND ND ND --- 10/05/22 0.3 ND ND ND ND ND ND 03/30/23 0.30 ND ND ND ND ND ND Notes. Analytical results from September June 2012 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. The March 19, 2020 sampling event was a resampling event for MW-7, MW-10, and MW-11; however, it was the initial 2020 semiannual sampling event for NES-2S. NC 2L Standards are the Title 15A NCAC 02L.0202 Groundwater Standards dated April 1, 2022. Bold concentrations exceed the NC2L Standard for groundwater. Detections of cis-1,2-dichloroethylene in MW-7 and MW-8 in August 2015 are suspect. Results for the Unit 1 MW-7 sample, collected in concurrence with the Unit 2 sample, was reported as non -detect for cis- 1,2-dichloroethylene. NES-2S 8/17/21 sample data shown in table collected on 08/18/21. NES-2S and MW-7 10/05/2022 sample data show in in table collected on 09/29/22. NES-2S and MW-7 03/30/2023 sample data show in in table collected on 03/29/23. All concentrations are in micrograms per liter (pg/L). J = Estimated value above laboratory method detection limit and below laboratory method quantitation limit; MDL = laboratory method detection limit ND = not detected; NA = not analyzed/not available; NS = not sampled; NE = not established; --- = data not available/not reported; B = blank -qualified data, result is expected to be biased high based on concentrations in the blank; Appendix D (Page 6 of 6) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix E Summary of Historical Constituents in Surface Water 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Inorganics Arsenic 03/12/15 2.5 ND ND 08/19/15 2.5 ND ND NC2B = 340 pg/L 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 02/14/17 5 ND ND 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND 6.1 J 08/08/19 4.7 ND ND 02/14/20 4.7 ND ND 08/26/20 4.7 ND 7.2 J 02/10/21 4.7 4.7 J Dry 08/17/21 --- ND ND 02/15/22 4.7 ND ND 10/05/22 0.087 0.28 J 1.2 03/30/23 4.40 ND 9.99 J Barium 08/13/14 5 22.1 J 33.9 J 03/12/15 2.5 22.5 J 24.6 J ISTV 3 = 21,000 pg/L 08/19/15 2.5 23.9 J 32.7 J 02/18/16 2.5 22 J 26.3 J 08/11/16 2.5 23.4 J 26.5 J 02/14/17 2.5 18.6 J 21.4 J 08/23/17 2.5 32.3 J 33.3 J 02/06/18 2.5 23.7 J 32.3 J 08/16/18 2.5 24.2 J 38.2 J 02/05/19 2.5 22.9 23.1 08/08/19 1 23.3 44.5 02/14/20 1 26.5 29.3 08/26/20 3.5 21.2 47.5 02/10/21 3.5 18.8 DRY 08/17/21 --- 19.9 28.5 02/15/22 3.5 16.6 29.7 10/05/22 0.21 19.5 40.8 03/30/23 0.736 32.4 27.9 Beryllium 08/11/16 0.5 ND ND 02/14/17 0.5 ND ND NC2B = 65 pg/L 08/23/17 0.5 ND ND 02/06/18 0.5 ND ND 08/16/18 0.5 ND ND 02/05/19 0.5 ND ND 08/08/19 0.2 ND ND 02/14/20 0.2 ND ND 08/26/20 0.7 ND ND 02/10/21 0.7 ND DRY 08/17/21 --- ND ND 02/15/22 0.7 ND ND 10/05/22 0.05 ND 0.1 03/30/23 0.330 ND ND Chromium 08/13/14 5 ND ND 03/12/15 2.5 ND 2.6 J NC2B = 16 pg/L 08/19/15 2.5 ND ND 02/18/16 2.5 ND ND 08/11/16 2.5 5.2 J ND 9/13/16(4) 2.5 NS NS 02/14/17 2.5 3 J ND 08/23/17 2.5 ND ND 02/06/18 2.5 ND 2.7 J 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1 ND 2.2 J 02/14/20 1 2.6 J 3.1 J 08/26/20 3.7 ND 9.8 02/10/21 3.7 ND DRY 08/17/21 --- ND ND 02/15/22 3.7 ND ND 10/05/22 0.5 0.91 J 5 03/30/23 1.40 2.91 J 1.68 J Cobalt 08/11/16 2.5 ND ND 02/14/17 2.5 ND ND ISTV (3) = 16 pg/L 08/23/17 2.5 ND ND 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1.1 ND 2.9 J 02/14/20 1.1 ND ND 08/26/20 3.6 ND ND 02/10/21 3.6 ND DRY 08/17/21 --- ND ND 02/15/22 3.6 ND ND 10/05/22 0.05 0.27 J 2.1 03/30/23 0.840 ND ND Appendix E (Page 1 of 3) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Copper 08/13/14 5 ND ND 03/12/15 2.5 ND ND NC213 ' = 2.91 µg/L 08/19/15 2.5 ND ND 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 9/13/16(4) 2.5 NS NS 02/14/17 2.5 ND ND 08/23/17 2.5 ND ND 02/06/18 2.5 2.7 J 3.6 J 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 2.1 2.7 J 2.7 J 02/14/20 2.1 2.8 J 2.9 J 08/26/20 4.3 ND 8.1 02/10/21 4.3 ND DRY 08/17/21 --- ND ND 02/15/22 4.3 ND ND 10/05/22 1.1 ND 5.1 03/30/23 3.68 4.07 J ND Hardness, Total (SM 23408) 02/05/19 662 13,800 17,400 08/08/19 131 17,400 28,200 NC213 = NE 02/14/20 131 10,800 12,300 08/26/20 131 14,900 34,900 02/10/21 131 --- DRY 08/17/21 --- 16,500 28,900 02/15/22 --- NA NA 10/05/22 541 13,400 30,200 03/30/23 198 16,400 21,200 Iron 02/06/18 25 1,520 2,920 08/16/18 25 --- --- NRWQC (2) = 1,000 µg/L 02/05/19 25 --- --- 02/14/20 19.5 --- --- 02/10/21 41.5 --- DRY 08/17/21 --- NA NA 02/15/22 --- NA NA 10/05/22 --- NA NA 03/30/23 --- NA NA Lead 02/18/16 2.5 ND ND 08/11/16 2.5 ND ND 9/13/16(4) 2.5 NS NS NC213 ' = 10.63 µg/L 02/14/17 2.5 ND ND 08/23/17 2.5 ND ND 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 1.6 ND 1.6 J 02/14/20 1.6 ND ND 08/26/20 4.5 ND ND 02/10/21 4.5 ND DRY 08/17/21 --- ND ND 02/15/22 4.5 ND ND 10/05/22 0.077 0.42 J 1.6 03/30/23 2.99 ND ND Manganese 02/06/18 2.5 11.6 J 25.8 J 08/16/18 2.5 --- --- NRWQC 12) = 100 µg/L 02/05/19 2.5 --- --- 02/14/20 0.9 --- --- 02/10/21 3.4 --- DRY 08/17/21 --- NA NA 02/15/22 --- NA NA 10/05/22 --- NA NA 03/30/23 --- NA NA Nickel 08/13/14 5 ND ND 03/12/15 2.5 ND ND NC213 ' = 118.65 µg/L 08/19/15 2.5 ND ND 02/18/16 2.5 ND ND 08/11/16 2.5 2.8 J ND 02/14/17 2.5 ND ND 08/23/17 2.5 ND ND 02/06/18 2.5 ND ND 08/16/18 2.5 ND ND 02/05/19 2.5 ND ND 08/08/19 0.9 ND 1.9 J 02/14/20 0.9 1.2 J 1.3 J 08/26/20 3.5 ND 4.3 J 02/10/21 3.5 ND DRY 08/17/21 --- ND ND 02/15/22 3.5 ND ND 10/05/22 0.42 ND 2.5 03/30/23 1.61 3.36 J,B 3.00 J,B Selenium 08/11/16 5 ND ND 02/14/17 5 ND ND NC213 = 5 µg/L 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND ND 08/08/19 4.7 ND ND 02/14/20 4.7 ND ND 08/26/20 4.7 ND ND 02/10/21 4.7 ND DRY 08/17/21 --- ND ND 02/15/22 4.7 ND ND 10/05/22 0.072 ND 0.26 J 03/30/23 1 7.35 1 ND I ND Appendix E (Page 2 of 3) Hart & Hickman, PC https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Appendix E Summary of Historical Constituents in Surface Water Granville County Oxford Unit 2 Landfill Granville County, North Carolina H&H Job No. GMI-005 Analyte Sample Date MDL SW-3 SW-4 Vanadium 08/13/14 5 ND 9.3 J 03/12/15 2.5 3.1 J 6.3 J NC2B = NE 08/19/15 2.5 2.7 J 4.3 J 02/18/16 2.5 ND ND 08/11/16 2.5 ND 2.7 J 02/14/17 2.5 ND ND 08/23/17 2.5 4.6 J ND 02/06/18 2.5 4.3 J 8.2 J 08/16/18 2.5 3.7 J ND 02/05/19 2.5 ND ND 08/08/19 1.3 3.3 J 7.9 02/14/20 1.3 3.8 J 6.1 08/26/20 3.9 ND 24.3 02/10/21 3.9 ND DRY 08/17/21 --- ND ND 02/15/22 3.9 ND ND 10/05/22 0.25 2.1 14.2 03/30/23 4.99 12.9 J ND Zinc 08/13/14 5 ND ND 03/12/15 5 8.5 B 10.8 B NC2B 1 = 29.63 µg/L 08/19/15 5 ND ND 02/18/16 5 ND ND 08/11/16 5 13 5.6 J 9/13/16(4) 5 --- --- 02/14/17 5 7 J ND 08/23/17 5 ND ND 02/06/18 5 ND ND 08/16/18 5 ND ND 02/05/19 5 ND ND 08/08/19 3.9 ND 7.2 J 02/14/20 3.9 4 J 4.7 J 08/26/20 9.5 ND 11.3 02/10/21 9.5 ND DRY 08/17/21 --- ND ND 02/15/22 9.5 ND ND 10/05/22 2.7 ND 9.8 J 03/30/23 6.52 8.27 J 7.11 J Organics 1,4-Dioxane 08/16/18 1.9 ND ND 02/05/19 1.9 ND ND ISTV (31= 80 pg/L 08/08/19 1.2 ND ND 02/14/20 1.2 ND ND 08/26/20 1.2 ND ND 02/10/21 1.2 ND DRY 08/17/21 --- ND ND 02/15/22 0.86 ND ND 10/05/22 0.86 ND ND 03/30/23 0.86 ND ND 2-Hexanone 08/11/16 0.46 ND ND 02/14/17 0.46 ND ND NC213 = NE 08/23/17 0.46 ND ND 02/06/18 0.46 ND ND 08/16/18 0.46 ND ND 02/05/19 0.57 ND ND 08/08/19 0.57 ND ND 02/14/20 0.57 ND ND 08/26/20 0.57 ND ND 02/10/21 0.57 ND DRY 08/17/21 --- --- --- 02/15/22 0.48 ND ND 10/05/22 0.48 ND ND 03/30/23 0.48 ND ND Methylene Chloride 08/26/20 3.7 --- 8.2 02/10/21 3.7 ND DRY ISTV (3) = 11,000 pg/L 08/17/21 --- ND ND 02/15/22 2.0 ND ND 10/05/22 2.0 ND ND 03/30/23 2.0 4.2 J,B,C9,L1,v1 ND Toluene 08/26/20 0.24 ND 0.33 J 02/10/21 0.24 ND DRY NC213 = 11 pg/L 08/17/21 --- ND ND 02/15/22 0.48 ND ND 10/05/22 0.48 ND ND 03/30/23 1 0.24 1 ND ND Notes: Analytical results from November 1996 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event. Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event. NC 2L Standards are the Title 15A NCAC 02L .0202 Groundwater Standards dated April 1, 2022. 15A NCAC 213 Water Quality Standards (2B Standards) for Surface Water (Class C) dated July 26, 2021. Bold concentrations exceed the NC 2L Standard for groundwater or NC 213 Standard for surface water. 1. 213 Standards for hardness -dependent metals are calculated using a mean value of 19.736 mg/L obtained from averaging hardness results reported for surface water locations SW-3 and SW-4 from September 2019 to March 2023. 2. No 26 Standard established, value shown is EPA Nationally Recommended Water Quality Criteria (NRWQC) for Aquatic Life & Human Health. 3. No 2B Standard established, value shown is North Carolina In -Stream Target Value for Surface Water (ISTV). 4. The 9/13/16 sampling event was a resampling event. All concentrations are in micrograms per liter (pg/L). J = estimated concentration above the laboratory method detection limit and below the laboratory method reporting limit; B = analyte was detected in the associated method blank; C9 = common laboratory contaminant; MDL = laboratory method detection limit; ND = Not detected; NE = Not established; --- = Not Sampled/ Data not available DRY = surface water sample location was dry Appendix E (Page 3 of 3) https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2023 First Half GWM/Tables/Oxford Unit 2 Historic Tables JAO Hart & Hickman, PC