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HomeMy WebLinkAboutNCD980602163_20021126_Warren County PCB Landfill_SERB C_PCB Landfill Site Samples-OCR~ . ~ £Jc1s1wc wrr PONo ~ \ ..... ..... ..... 9-0.61 ppm ..... BOHOM l<ULlfilll = BOTTOM H \It 1,//}'-'''"' \/J ,.,, 111,/\ -7-ND soii:•·t 14-ND 12-ND 13-ND 15-ND 0 0 ·-= ~~ 1,4AT[R1Al PRfPARATjQN = ---~ POI.£ BUILDING 5-ND 6-ND _J 8" V.,[)[ CURB ~ = --e .. ir· -fl 1076 oo· N09"10'45"W fl 2. 21 acres ◊ \_ CURB T'IP, ~ I 11\1 /!flt f,'11) fflN If.fl 1P./I \I <,IJfftl/1,I-IP. --' 3-ND 16-0.095 ppm (inside landfill) ,., ◊ -= =Af!U-◊ 7 l,t(lJNTABL[ CURB -fl 4-ND 1 -ND 2-ND Preliminary Results from 11-26-2002 WCLF Site Sampling ~ 5 ~ ~ ::; ~ ~ .. ·'•-,. .. .. :I .. ~ HAlJI. AOAO fOfl CtEAN t,1,Al£AIAL !\ \ ,;: -"' -0 ~ 0 rcn C'-i st co o r--co (./) • -1-J\ y\ ' \ MATCH LIN[ SE[ SHEET 1 "1 ~ ... ,,, Location ID SampleID I SSEDBASINl I SSEDBASINI I SSEDBASINI l SSEDBASINI I SSEDBASINI 1 SSEDBASINl 1 SSEDBASlNl 1 SSEDBASINl 1 SSEDBASINl 2 SSEDBASIN2 2 SSEDBASIN2 2 SSEDBASIN2 2 SSEDBAS1N2 2 SSEDBAS1N2 2 SSEDBASIN2 2 SSEDBAS1N2 2 SSEDBASIN2 2 SSEDBASIN2 3 SSEDBASIN3 3 SSEDBASIN3 3 SSEDBASIN3 3 SSEDBAS1N3 3 SSEDBAS1N3 3 SSEDBAS1N3 3 SSEDBAS1N3 3 SSEDBAS1N3 3 SSEDBASIN3 4 SSLOPE4 4 SSLOPE4 4 SSLOPE4 4 SSLOPE4 4 SSLOPE4 4 SSLOPE4 4 SSLOPE4 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Sedimentation Basin South Slope South Slope South Slope South Slope South Slope South Slope South Slope Page I of 24 Sample Description Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment ir1 Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Drain from fuel access road Drain from fuel access road Drain from fuel access road Drain from fuel access road Drain from fuel access road Drain from fuel access road Drain from fuel access road 12/04/2002 Location ID SampleID 4 SSLOPE4 4 SSLOPE4 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASlN7 7 NSEDBASIN7 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area South Slope South Slope North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin North Sedimentation Basin Stripped Soil Stockpile Stripped Soil Stockpile Stripped Soil Stockpile Stripped Soil Stockpile Stripped Soil Stockpile Page 2 of24 Sample Description Drain from fuel access road Drain from fuel access road Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Entrance Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Sediment in Basin Exit Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Basin Discharge at Fence Composite from North Side Composite from North Side Composite from North Side Composite from North Side Composite from North Side 12/04/2002 Location ID SampleID 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 9 STSOILSTKP9 10 STSOILSTKPl0 10 STSOILSTKP10 10 STSOILSTKP 10 IO STSOILSTKPl0 10 STSOILSTKPl0 10 STSOILSTKPl0 10 STSOILSTKPl0 10 STSOILSTKPl0 10 STSOILSTKP 10 11 DDTOPLFl 1 11 DDTOPLFl l 11 DDTOPLFl l 11 DDTOPLFl l 11 DDTOPLFl 1 11 DDTOPLFll II DDTOPLFl 1 11 DDTOPLFll 11 DDTOPLFl 1 12 SLTFNE12 12 SLTFNE12 12 SLTFNE12 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area Sample Description Stripped Soil Stockpile Composite from North Side Stripped Soil Stockpile Composite from North Side Stripped Soil Stockpile Composite from North Side Stripped Soil Stockpile Composite from North Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Striooed Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from West Side Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Stripped Soil Stockpile Composite from South and East Sides Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Drain Discharge from Top of Landfill Discharge Rip Rap Area Silt Fence Area Northeast Area that drains to silt fence area Silt Fence Area Northeast Area that drains to silt fence area Silt Fence Area Northeast Area that drains to silt fence area Page 3 of 24 12/04/2002 Location ID SamplelD 12 SLTFNEl2 12 SLTFNE12 12 SLTFNE12 12 SLTFNE12 12 SLTFNE12 12 SLTFNE12 13 LFCVR13 13 LFCVRl3 13 LFCYRl3 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVRl3 13 LFCVRl3 14 LFCVRl4 14 LFCVRl4 14 LFCYRl4 14 LFCVRl4 14 LFCVRl4 14 LFCYRl4 14 LFCVRl4 14 LFCVRl4 14 LFCYRl4 15 LFCVRl5 15 LFCYRl5 15 LFCVR15 15 LFCVRl5 15 LFCVRl5 15 LFCVRl5 15 LFCVR15 15 LFCVRl5 15 LFCVRl5 16 ADDSMPl6 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area Silt Fence Area Northeast Silt Fence Area Northeast Silt Fence Area Northeast Silt Fence Area Northeast Silt Fence Area Northeast Silt Fence Area Northeast Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Landfill Cover Additional Samples Page 4 of 24 Sample Description Area that drains to silt fence area Area that drains to silt fence area Area that drains to silt fence area Area that drains to silt fence area Area that drains to silt fence area Area that drains to silt fence area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Auger into undisturbed cover area Extended area of landfill 12/04/2002 Location ID 16 16 16 16 16 16 16 16 Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC Lab QC MS MS MS MS MS MS MS MS Q2804revl SampleID ADDSMP16 ADDSMP16 ADDSMP16 ADDSMP16 ADDSMPl6 ADDSMP16 ADDSMPl6 ADDSMP16 PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA PBLKZA PLCSZA SSEDBASlNlMS SSEDBASJNlMS SSEDBASIN 1 MS SSEDBASIN I MS SSEDBASIN I MS SSEDBASINJ MS SSEDBASIN I MS SSEDBASTN I MS Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area Additional Samples Additional Samples Additional Samples Additional Samples Additional Samples Additional Samples Additional Samples Additional Samples Page 5 of24 Sample Description Extended area of landfill Extended area of landfill Extended area of landfill Extended area of landfill Extended area of landfill Extended area of landfill Extended area of landfill Extended area of landfill 12/04/2002 Location ID MS MSD MSD MSD MSD MSD MSD MSD MSD MSD Q2804revl SamplelD SSEDBASINlMS SSEDBASIN 1 MSD SSEDBASIN 1 MSD SSEDBASINlMSD SSEDBASIN 1 MSD SSEDBASIN 1 MSD SSEDBASIN I MSD SSEDBASIN I MSD SSEDBASIN I MSD SSEDBASINlMSD Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Area Page 6 of24 Sample Description 12/04/2002 Location ID I 1 1 1 1 1 l I 1 2 2 2 2 2 2 2 2 2 3 ,., .) ,., .) ,., .) ,., .) ,., .) 3 ,., .) 3 4 4 4 4 4 4 4 Q2804revl SampleID SSEDBASINI SSEDBASINI SSEDBASlNl SSEDBASINI SSEDBASINl SSEDBASINI SSEDBASINI SSEDBASINI SSEDBASINI SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN2 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSEDBASIN3 SSLOPE4 SSLOPE4 SSLOPE4 SSLOPE4 SSLOPE4 SSLOPE4 SSLOPE4 Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" I 9 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 19 ft from stone 6-9" 11 ft from stone 6-9" 11 ft from stone 6-9" I I ft from stone 6-9" I I ft from stone 6-9" I I ft from stone 6-9" I 1 ft from stone 6-9" 11 ft from stone 6-9" Page 7 of 24 Date Collected Time Collected CAS# 11/26/2002 14:50 12674112 11/26/2002 14:50 11104282 I l/26/2002 14:50 11141165 11/26/2002 14:50 53469219 11/26/2002 14:50 12672296 l l/26/2002 14:50 11097691 11/26/2002 14:50 11096825 11/26/2002 14:50 2051243 11/26/2002 14:50 877098 11/26/2002 14:55 12674112 11/26/2002 14:55 11104282 11/26/2002 14:55 11141165 11/26/2002 14:55 53469219 11/26/2002 14:55 12672296 11/26/2002 14:55 11097691 11/26/2002 14:55 11096825 11/26/2002 14:55 2051243 11/26/2002 14:55 877098 11/26/2002 15:00 12674112 11/26/2002 15:00 11104282 11/26/2002 15:00 11141165 11/26/2002 15:00 53469219 11/26/2002 15:00 12672296 11/26/2002 15:00 11097691 11/26/2002 15:00 11096825 11/26/2002 15:00 2051243 11/26/2002 15:00 877098 11/26/2002 14:02 12674112 11/26/2002 14:02 11104282 11/26/2002 14:02 11141165 l l/26/2002 14:02 53469219 11/26/2002 14:02 12672296 11/26/2002 14:02 I 1097691 l l/26/2002 14:02 11096825 12/04/2002 Location ID SamplelD 4 SSLOPE4 4 SSLOPE4 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBAS1N5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 5 NSEDBASIN5 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 6 NSEDBASIN6 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 7 NSEDBASIN7 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 8 STSOILSTKP8 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth 11 ft from stone 6-9" 11 ft from stone 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 11 ft from comer & 36 ft from stone 6-9" 11 ft from comer & 36 ft from stone 6-9" 11 ft from corner & 36 ft from stone 6-9" 11 ft from comer & 36 ft from stone 6-9" 11 ft from corner & 36 ft from stone 6-9" 11 ft from comer & 36 ft from stone 6-9" 11 ft from corner & 36 ft from stone 6-9" 11 ft from comer & 36 ft from stone 6-9" 11 ft from corner & 36 ft from stone 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" Page 8 of 24 Date Collected Time Collected CAS# 11/26/2002 14:02 2051243 11/26/2002 14:02 877098 11/26/2002 14: 13 12674112 11/26/2002 14: 13 11104282 11/26/2002 14: 13 11141165 11/26/2002 14: 13 53469219 11/26/2002 14:13 12672296 11/26/2002 14:13 11097691 11/26/2002 14:13 11096825 11/26/2002 14:13 2051243 11/26/2002 14: 13 877098 11/26/2002 14:20 12674112 l 1/26/2002 14:20 11104282 11/26/2002 14:20 11141165 11/26/2002 14:20 53469219 11/26/2002 14:20 12672296 11/26/2002 14:20 11097691 11/26/2002 14:20 11096825 11/26/2002 14:20 2051243 11/26/2002 14:20 877098 11/26/2002 14:25 12674112 11/26/2002 14:25 11104282 11/26/2002 14:25 11141165 11/26/2002 14:25 53469219 11/26/2002 14:25 12672296 11/26/2002 14:25 11097691 11/26/2002 14:25 11096825 11/26/2002 14:25 2051243 11/26/2002 14:25 877098 11/26/2002 15:20 12674112 11/26/2002 15:20 11104282 11/26/2002 15:20 11141165 11/26/2002 15:20 53469219 11/26/2002 15:20 12672296 12/04/2002 Location ID 8 8 8 8 9 9 9 9 9 9 9 9 9 10 IO 10 10 IO 10 10 10 IO 11 11 11 11 11 11 11 11 11 12 12 12 Q2804revl SamplelD STSOILSTKP8 STSOILSTKP8 STSOILSTKP8 STSOILSTKP8 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKP9 STSOILSTKPlt1 STSOILSTKPl0 STSOILSTKPl0 STSOlLSTKPl0 STSOILSTKPI0 STSOILSTKP 10 STSOlLSTKPl0 STSOILSTKPI0 STSOlLSTKPl0 DDTOPLFI I DDTOPLFll DDTOPLFll DDTOPLFl 1 DDTOPLFI 1 DDTOPLFl 1 DDTOPLFl 1 DDTOPLFll DDTOPLFI 1 SLTFNE12 SLTFNE12 SLTFNE12 Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 10 ft from stone 6-9" 10 ft from stone 6-9" IO ft from stone 6-9" 10 ft from stone 6-9" IO ft from stone 6-9" IO ft from stone 6-9" IO ft from stone 6-9" IO ft from stone 6-9" l 0 ft from stone 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" Page 9 of24 Date Collected Time Collected CAS# 11/26/2002 15:20 11097691 11/26/2002 15:20 11096825 11/26/2002 15:20 2051243 11/26/2002 15:20 877098 11/26/2002 15:10 12674112 11/26/2002 15: 10 11104282 11/26/2002 15:10 11141165 11/26/2002 15:10 53469219 11/26/2002 15:10 12672296 11/26/2002 15:10 11097691 11/26/2002 15: 10 11096825 11/26/2002 15: 10 2051243 11/26/2002 15:10 877098 11/26/2002 10:40 12674112 11/26/2002 10:40 11104282 11/26/2002 10:40 11141165 11/26/2002 10:40 53469219 11/26/2002 10:40 12672296 11/26/2002 10:40 11097691 11/26/2002 10:40 11096825 11/26/2002 10:40 2051243 11/26/2002 10:40 877098 11/26/2002 10:55 12674112 11/26/2002 10:55 11104282 11/26/2002 10:55 11141165 11/26/2002 10:55 53469219 11/26/2002 10:55 12672296 11/26/2002 10:55 11097691 11/26/2002 10:55 11096825 11/26/2002 10:55 2051243 11/26/2002 10:55 877098 11/26/2002 11: 15 12674112 11/26/2002 I 1:15 11104282 11/26/2002 11: 15 11141165 12/04/2002 Location ID SamplelD 12 SLTFNEl2 12 SLTFNE12 12 SLTFNE12 12 SLTFNE12 12 SLTFNEl2 12 SLTFNE12 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 13 LFCVR13 14 LFCVR14 14 LFCVR14 14 LFCVR14 14 LFCVR14 14 LFCVRl4 14 LFCVR14 14 LFCVR14 14 LFCVR14 14 LFCVR14 15 LFCVR15 15 LFCVR15 15 LFCVR15 15 LFCVRl5 15 LFCVR15 15 LFCVR15 15 LFCVR15 15 LFCVR15 15 LFCVR15 16 ADDSMP16 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" 13 ft west & 18 ft east of tank center 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from 001th well 6-9" Middle & 34 ft from north well 6-9" Middle & 34 ft from north well 6-9" 46 ft east of No. 13 6-9" 46 ft east of No. 13 6-9" 46fteastofNo. 13 6-9" 46fteastofNo.13 6-9" 46 ft east of No. 13 6-9" 46fteastofNo.13 6-9" 46 ft east of No. 13 6-9" 46 ft east of No. 13 6-9" 46 ft east of No. 13 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 62 ft west of No. 13 & 63 ft from haul road 6-9" 6-9" Page 10 of24 Date Collected Time Collected CAS# 11/26/2002 11:15 53469219 11/26/2002 11: 15 12672296 11/26/2002 11: 15 11097691 11/26/2002 11 :15 11096825 11/26/2002 11: 15 2051243 11/26/2002 11: 15 877098 11/26/2002 13:35 12674112 11/26/2002 13:35 11104282 11/26/2002 13:35 11141165 11/26/2002 13:35 53469219 11/26/2002 13:35 12672296 11/26/2002 13:35 11097691 11/26/2002 13:35 11096825 11/26/2002 13:35 2051243 11/26/2002 13:35 877098 11/26/2002 13:37 12674112 11/26/2002 . 13:37 11104282 11/26/2002 13:37 11141165 11/26/2002 13:37 53469219 11/26/2002 13:37 12672296 11/26/2002 13:37 11097691 11/26/2002 13:37 11096825 11/26/2002 13:37 2051243 11/26/2002 13:37 877098 11/26/2002 13:40 12674112 11/26/2002 13:40 11104282 11/26/2002 13:40 11141165 11/26/2002 13:40 53469219 11/26/2002 13:40 12672296 11/26/2002 13:40 11097691 11/26/2002 13:40 11096825 11/26/2002 13:40 2051243 11/26/2002 13:40 877098 11/26/2002 13:50 12674112 12/04/2002 Location ID SampleID 16 ADDSMP16 16 ADDSMPl6 16 ADDSMP16 16 ADDSMP16 16 ADDSMP16 16 ADDSMP16 16 ADDSMP16 16 ADDSMP16 Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA Lab QC PBLKZA Lab QC PLCSZA MS SSEDBASIN 1 MS MS SSEDBASINlMS MS SSEDBASIN 1 MS MS SSEDBASIN 1 MS MS SSEDBASIN I MS MS SSEDBASIN 1 MS MS SSEDBASlN I MS MS SSEDBASIN 1 MS Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" 6-9" Page 11 of24 Date Collected Time Collected 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 13:50 11/26/2002 11/26/2002 11/26/2002 11/26/2002 11/26/2002 11/26/2002 11/26/2002 11/26/2002 CAS# 11104282 11141165 53469219 12672296 11097691 11096825 2051243 877098 12674112 12674112 11104282 11104282 11141165 11141165 53469219 53469219 12672296 12672296 11097691 l 1097691 11096825 11096825 2051243 2051243 877098 877098 12674112 11104282 11141165 53469219 12672296 11097691 11096825 2051243 12/04/2002 Location ID MS MSD MSD MSD MSD MSD MSD MSD MSD MSD Q2804revl SampleJD SSEDBASIN 1 MS SSEDBASTN I MSD SSEDBASINlMSD SSEDBASINlMSD SSEDBASIN 1 MSD SSEDBASIN 1 MSD SSEDBASlN 1 MSD SSEDBASlN I MSD SSEDBASIN 1 MSD SSEDBASlNlMSD Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Additional Location Info Sample Depth Page 12of24 Date Collected Time Collected CAS# 11/26/2002 877098 11/26/2002 12674112 11/26/2002 11104282 11/26/2002 11141165 11/26/2002 53469219 11/26/2002 12672296 11/26/2002 11097691 11/26/2002 11096825 11/26/2002 2051243 11/26/2002 877098 12/04/2002 Location ID SamplelD Test Component l SSEDBASlNI Aroclor-1016 1 SSEDBASTNI Aroclor-1221 1 SSEDBASJNl Aroclor-1232 1 SSEDBASTNl Aroclor-1242 1 SSEDBASINI Aroclor-1248 1 SSEDBASJNl Aroclor-1254 1 SSEDBASTNI Aroclor-1260 1 SSEDBASINl Decachlorobiphenyl 1 SSEDBASJNl Tetrachloro-m-xylene 2 SSEDBASJN2 Aroclor-1016 2 SSEDBASIN2 Aroclor-1221 2 SSEDBASIN2 Aroclor-1232 2 SSEDBASTN2 Aroclor-1242 2 SSEDBASIN2 ' Aroclor-1248 2 SSEDBASJN2 Aroclor-1254 2 SSEDBASTN2 Aroclor-1260 2 SSEDBASIN2 Decachlorobiphenyl 2 SSEDBASIN2 Tetrachloro-m-xylene ,., SSEDBASIN3 Aroclor-1016 ., ,., SSEDBASIN3 Aroclor-1221 ., 3 SSEDBASIN3 Aroclor-1232 3 SSEDBASJN3 Aroclor-1242 ,., SSEDBASIN3 Aroclor-1248 ., 3 SSEDBASIN3 Aroclor-1254 3 SSEDBASIN3 Aroclor-1260 3 SSEDBASIN3 Decachlorobiphenyl ,., SSEDBASTN3 Tetrachloro-m-xylene ., 4 SSLOPE4 Aroclor-l O 16 4 SSLOPE4 Aroclor-1221 4 SSLOPE4 Aroclor-1232 4 SSLOPE4 Aroclor-1242 4 SSLOPE4 Aroclor-1248 4 SSLOPE4 Aroclor-1254 4 SSLOPE4 Aroclor-1260 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit LT 44 44 ug/Kg LT 57 57 ug/Kg LT 44 44 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 44 44 ug/Kg 62 0 %Rec 64 0 %Rec LT 50 50 ug/Kg LT 65 65 ug/Kg LT 50 50 ug/Kg LT 35 35 ug/Kg LT 35 ' 35 ug/Kg LT 35 35 ug/Kg LT 50 50 ug/Kg 62 0 %Rec 60 0 %Rec LT 40 40 ug/Kg LT 52 52 ug/Kg LT 40 40 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 40 40 ug/Kg 73 0 %Rec 57 0 %Rec LT 40 40 ug/Kg LT 52 52 ug/Kg LT 40 40 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 40 40 ug/Kg Page 13 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method u l 3550 8082 u 1 3550 8082 u l 3550 8082 u 1 3550 8082 u I 3550 8082 u 1 3550 8082 u 1 3550 8082 1 3550 8082 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u l 3550 8082 I 3550 8082 I 3550 8082 u 1 3550 8082 u 1 3550 8082 u l 3550 8082 u l 3550 8082 u I 3550 8082 u I 3550 8082 u 1 3550 8082 I 3550 8082 l 3550 8082 u 1 3550 8082 u l 3550 8082 u 1 3550 8082 u I 3550 8082 u l 3550 8082 u 1 3550 8082 u l 3550 8082 12/04/2002 Location ID SamplelD Test Component 4 SSLOPE4 Decachlorobiphenyl 4 SSLOPE4 Tetrachloro-m-xylene 5 NSEDBASIN5 Aroclor-1016 5 NSEDBASIN5 Aroclor-1221 5 NSEDBASIN5 Aroclor-1232 5 NSEDBASIN5 Aroclor-1242 5 NSEDBASIN5 Aroclor-1248 5 NSEDBASIN5 Aroclor-1254 5 NSEDBASIN5 Aroclor-1260 5 NSEDBASIN5 Decachlorobiphenyl 5 NSEDBASIN5 Tetrachloro-m-xylene 6 NSEDBASIN6 Aroclor-1016 6 NSEDBASIN6 Aroclor-1221 6 NSEDBAS1N6 ' Aroclor-1232 6 NSEDBASIN6 Aroclor-1242 6 NSEDBASIN6 Aroclor-1248 6 NSEDBASIN6 Aroclor-1254 6 NSEDBASIN6 Aroclor-1260 6 NSEDBASIN6 Decachlorobiphenyl 6 NSEDBASIN6 Tetrachloro-m-xylene 7 NSEDBASIN7 Aroclor-1016 7 NSEDBAS1N7 Aroclor-1221 7 NSEDBAS[N7 Aroclor-1232 7 NSEDBASIN7 Aroclor-1242 7 NSEDBASIN7 Aroclor-1248 7 NSEDBASIN7 Aroclor-1254 7 NSEDBASIN7 Aroclor-1260 7 NSEDBASIN7 Decachlorobiphenyl 7 NSEDBASIN7 Tetrachloro-m-xylene 8 STSOILSTKP8 Aroclor-1016 8 STSOILSTKP8 Aroclor-1221 8 STSOILSTKP8 Aroclor-1232 8 STSOlLSTKP8 Aroclor-1242 8 STSOILSTKP8 Aroclor-1248 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit 57 0 %Rec 60 0 %Rec LT 46 46 ug/Kg LT 61 61 ug/Kg LT 46 46 ug/Kg LT 32 32 ug/Kg LT 32 32 ug/Kg LT 32 32 ug/Kg LT 46 46 ug/Kg 70 0 %Rec 62 0 %Rec LT 36 36 ug/Kg LT 47 47 ug/Kg LT 36 36 ug/Kg LT 25 25 ug/Kg LT 25 25 ug/Kg LT 25 25 ug/Kg 31 36 ug/Kg 77 0 %Rec 50 0 %Rec LT 40 40 ug/Kg LT 52 52 ug/K,g LT 40 40 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 40 40 ug/Kg 59 0 % Rec 59 0 % Rec LT 89 89 ug/Kg LT 120 120 ug/Kg LT 89 89 ug/Kg LT 62 62 ug/Kg LT 62 62 ug/Kg Page 14 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method 1 3550 8082 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u I 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 1 3550 8082 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 J I 3550 8082 1 3550 8082 1 3550 8082 u 1 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u 1 3550 8082 I 3550 8082 I 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 12/04/2002 Location ID SamplelD Test Component 8 STSOILSTKP8 Aroclor-1254 8 STSOJLSTKP8 Aroclor-1260 8 STSOJLSTKP8 Decachlorobiphenyl 8 STSOILSTKP8 Tetrachloro-m-xylene 9 STSOILSTKP9 Aroclor-1016 9 STSOJLSTKP9 Aroclor-1221 9 STSOJLSTKP9 Aroclor-1232 9 STSOJLSTKP9 Aroclor-1242 9 STSOILSTKP9 Aroclor-1248 9 STSOJLSTKP9 Aroclor-1254 9 STSOILSTKP9 Aroclor-1260 9 STSOILSTKP9 Decachlorobiphenyl 9 STSOJLSTKP9 Tetrachloro-m-xylene 10 STSOJLSTKPl0 Aroclor-1016 10 STSOILSTKP 10 Aroclor-1221 10 STSOJLSTKP 10 Aroclor-1232 10 STSOILSTKPl 0 Aroclor-1242 10 STSOJLSTKPl 0 Aroclor-1248 10 STSOJLSTKP I 0 Aroclor-1254 10 STSOILSTKP I 0 Aroclor-1260 10 STSOILSTKPl0 Decachlorobiphenyl 10 STSOILSTKP I 0 Tetrachloro-m-xylene 11 DDTOPLFI I Aroclor-1016 11 DDTOPLFl I Aroclor-1221 11 DDTOPLFI I Aroclor-1232 11 DDTOPLFl I Aroclor-1242 11 DDTOPLFI I Aroclor-1248 11 DDTOPLFI I Aroclor-1254 11 DDTOPLFl I Aroclor-1260 11 DDTOPLFI I Decachlorobiphenyl 11 DDTOPLFI I Tetrachloro-m-xylene 12 SLTFNE12 Aroclor-1016 12 SLTFNE12 Aroclor-1221 12 SLTFNEI2 Aroclor-1232 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit LT 62 62 ug/Kg 1000 89 ug/Kg 83 0 %Rec 84 0 %Rec LT 80 80 ug/Kg LT 100 100 ug/Kg LT 80 80 ug/Kg LT 56 56 ug/Kg LT 56 56 ug/Kg LT 56 56 ug/Kg 610 80 ug/Kg 75 0 %Rec 75 0 %Rec LT 2000 2000 ug/Kg LT 2600 2600 ug/Kg LT 2000 2000 ug/Kg LT 1400 1400 ug/Kg LT 1400 1400 ug/Kg LT 1400 1400 ug/Kg 19000 2000 ug/Kg I 10 0 %Rec 107 0 %Rec LT 44 44 ug/Kg LT 57 57 ug/Kg LT 44 44 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 44 44 ug/Kg 68 0 %Rec 66 0 %Rec LT 40 40 ug/Kg LT 52 52 ug/Kg LT 40 40 ug/Kg Page 15 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method u 2 3550 8082 2 3550 8082 2 3550 8082 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 u 2 3550 8082 2 3550 8082 2 3550 8082 2 3550 8082 u 50 3550 8082 u 50 3550 8082 u 50 3550 8082 u 50 3550 8082 u 50 3550 8082 u 50 3550 8082 50 3550 8082 50 3550 8082 50 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 V 1 3550 8082 u 1 3550 8082 u 1 3550 8082 V I 3550 8082 I 3550 8082 1 3550 8082 V 1 3550 8082 V I 3550 8082 u I 3550 8082 12/04/2002 Location ID SamplelD Test Component 12 SLTFNE12 Aroclor-1242 12 SLTFNEl2 Aroclor-1248 12 SLTFNEJ2 Aroclor-1254 12 SLTFNE12 Aroclor-1260 12 SLTFNE12 Decachlorobiphenyl 12 SLTFNE12 Tetrachloro-m-xylene 13 LFCVR13 Aroclor-1016 13 LFCVR13 Aroclor-1221 13 LFCVR13 Aroclor-1232 13 LFCVRl3 Aroclor-1242 13 LFCVR13 Aroclor-1248 13 LFCVR13 Aroclor-1254 13 LFCVR13 Aroclor-1260 13 LFCVR13 Decachlorobiphenyl 13 LFCVR13 Tetrachloro-m-xylene 14 LFCVR14 Aroclor-1016 14 LFCVRl4 Aroclor-1221 14 LFCVRl4 Aroclor-1232 14 LFCVRl4 Aroclor-1242 14 LFCVRl4 Aroclor-1248 14 LFCVR14 Aroclor-1254 14 LFCVRl4 Aroclor-1260 14 LFCVR14 Decachlorobiphenyl 14 LFCVR14 Tetrachloro-m-xylene 15 LFCVR15 Aroclor-1016 15 LFCVR15 Aroclor-1221 15 LFCVRl5 Aroclor-1232 15 LFCVR15 Aroclor-1242 15 LFCVRl5 Aroclor-1248 15 LFCVRl5 Aroclor-1254 15 LFCVR15 Aroclor-1260 15 LFCVR15 Decachlorobiphenyl 15 LFCVR15 Tetrachloro-m-xylene 16 ADDSMP16 Aroclor-1016 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit LT 27 27 ug/Kg LT 27 27 ug/Kg LT 27 27 ug/Kg LT 40 40 ug/Kg 68 0 %Rec 74 0 %Rec LT 42 42 ug/Kg LT 55 55 ug/Kg LT 42 42 ug/Kg LT 29 29 ug/Kg LT 29 29 ug/Kg LT 29 29 ug/Kg LT 42 42 ug/Kg 70 0 %Rec 71 0 %Rec LT 42 42 ug/Kg LT 55 55 ug/Kg LT 42 42 ug/Kg LT 29 29 ug/Kg LT 29 29 ug/Kg LT 29 29 ug/Kg LT 42 42 ug/Kg 71 0 %Rec 78 0 %Rec LT 44 44 ug/Kg LT 57 57 ug/Kg LT 44 44 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 30 30 ug/Kg LT 44 44 ug/Kg 94 0 %Rec 99 0 % Rec LT 34 34 ug/Kg Page 16 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 I 3550 8082 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 1 3550 8082 1 3550 8082 u I 3550 8082 u I 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 1 3550 8082 1 3550 8082 u 1 3550 8082 u I 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u 1 3550 8082 u I 3550 8082 1 3550 8082 1 3550 8082 u 1 3550 8082 12/04/2002 Location ID SampleID Test Component 16 ADDSMP16 Aroclor-1221 16 ADDSMP16 Aroclor-1232 16 ADDSMP16 Aroclor-1242 16 ADDSMP16 Aroclor-1248 16 ADDSMP16 Aroclor-1254 16 ADDSMP16 Aroclor-1260 16 ADDSMP16 Decachlorobiphenyl 16 ADDSMP16 Tetrachloro-m-xylene Lab QC PBLKZA Aroclor-1016 Lab QC PLCSZA Aroclor-1016 Lab QC PBLKZA Aroclor-1221 Lab QC PLCSZA Aroclor-1221 Lab QC PBLKZA Aroclor-1232 Lab QC PLCSZA Aroclor-1232 Lab QC PBLKZA Aroclor-1242 Lab QC PLCSZA Aroclor-1242 Lab QC PBLKZA Aroclor-1248 Lab QC PLCSZA Aroclor-1248 Lab QC PBLKZA Aroclor-1254 Lab QC PLCSZA Aroclor-1254 Lab QC PBLKZA Aroclor-1260 Lab QC PLCSZA Aroclor-1260 Lab QC PBLKZA Decachlorobiphenyl Lab QC PLCSZA Decachlorobiphenyl Lab QC PBLKZA Tetrachloro-m-xylene Lab QC PLCSZA Tetrachloro-m-xylene MS SSEDBASIN I MS Aroclor-1016 MS SSEDBASINlMS Aroclor-1221 MS SSEDBASIN I MS Aroclor-1232 MS SSEDBASIN I MS Aroclor-1242 MS SSEDBASINlMS Aroclor-1248 MS SSEDBASIN 1 MS Aroclor-1254 MS SSEDBASINIMS Aroclor-1260 MS SSEDBASINIMS Decachlorobiphenyl Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit LT 44 44 ug/Kg LT 34 34 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg 95 34 ug/Kg 58 0 %Rec 68 0 %Rec LT 33 ,,,, ug/Kg .,., 84 0 %Rec LT 43 43 ug/Kg LT 43 43 ug/Kg LT 33 ,,,, ug/Kg .,., LT 33 ,,,, ug/Kg .,., LT 23 23 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg LT 23 23 ug/Kg LT ,,,, 33 ug/Kg .,., 84 0 %Rec 77 0 %Rec 75 0 %Rec 93 0 %Rec 88 0 %Rec 78 0 %Rec LT 52 52 ug/Kg LT 40 40 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg 87 0 %Rec 76 0 %Rec Page 17 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method u I 3550 8082 u 1 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 I 3550 8082 I 3550 8082 1 3550 8082 u I 3550 8082 I 3550 8082 u I 3550 8082 u I 3550 8082 u 1 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 I 3550 8082 I 3550 8082 I 3550 8082 I 3550 8082 I 3550 8082 I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 u I 3550 8082 I 3550 8082 I 3550 8082 12/04/2002 Location ID SamplelD Test Component MS SSEDBASlN 1 MS Tetrachloro-m-xylene MSD SSEDBASIN I MSD Aroclor-1016 MSD SSEDBASIN 1 MSD Aroclor-1221 MSD SSEDBASIN l MSD Aroclor-1232 MSD SSEDBASINI MSD Aroclor-1242 MSD SSEDBASIN 1 MSD Aroclor-1248 MSD SSEDBASIN I MSD Aroclor-1254 MSD SSEDBASIN 1 MSD Aroclor-1260 MSD SSEDBASIN 1 MSD Decachlorobiphenyl MSD SSEDBASIN 1 MSD Tetrachloro-m-xylene Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Detection Modifier Result Limit Unit 68 0 %Rec 0 0 RPD LT 52 52 ug/Kg LT 40 40 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg LT 28 28 ug/Kg 6 0 RPD 61 0 %Rec 61 0 % Rec Page 18 of24 Lab DV Dilution Extraction Test Qual Qual Factor Method Method 1 3550 8082 1 3550 8082 u 1 3550 8082 u l 3550 8082 u I 3550 8082 u 1 3550 8082 u 1 3550 8082 1 3550 8082 1 3550 8082 1 3550 8082 12/04/2002 Location Date ID SampleID Extracted 1 SSEDBASINl 11/27/2002 1 SSEDBASINl 11/27/2002 I SSEDBASINl 11/27/2002 I SSEDBASINl 11/27/2002 1 SSEDBASINl I 1/27/2002 I SSEDBASINl 11/27/2002 1 SSEDBASINl 11/27/2002 1 SSEDBASINl 11/27/2002 I SSEDBASINl 11/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 : 1/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 I 1/27/2002 2 SSEDBASIN2 11/27/2002 2 SSEDBASIN2 11/27/2002 3 SSEDBASIN3 11/27/2002 3 SSEDBASIN3 11/27/2002 3 SSEDBASIN3 11/27/2002 3 SSEDBASIN3 11/27/2002 3 SSEDBASIN3 11/27/2002 " SSEDBASIN3 11/27/2002 .) " SSEDBASIN3 11/27/2002 .) 3 SSEDBASIN3 11/27/2002 3 SSEDBASIN3 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 1927 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 !2/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/29/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 1903 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) Page 19 of24 Laboratory Batch/ID QC Lot lnstruments Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG2l688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG2l688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG2l688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG2l688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG2l688-1 varian43.i Q2804 WG21688-I varian43.i Q2804 WG2l688-I varian43.i Q2804 WG21688-l varian43.i 12/04/2002 Location Date ID SampleID Extracted 4 SSLOPE4 11/27/2002 4 SSLOPE4 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 5 NSEDBASIN5 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 6 NSEDBASIN6 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 7 NSEDBASIN7 11/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2102 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2326 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 11/30/2002 2150 12/03/2002 Doria Rawlings (ET) 1 l/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) l l/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) Page 20 of24 Laboratory Batch/ID QC Lot Instruments Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-1 varian43.i 12/04/2002 Location Date ID SampleID Extracted 8 STSOILSTKP8 I 1/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 8 STSOILSTKP8 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 9 STSOILSTKP9 11/27/2002 IO STSOILSTKP I 0 1 i/27/2002 10 STSOILSTKP I 0 11/27/2002 10 STSOILSTKP I 0 11/27/2002 10 STSOILSTKP10 11/27/2002 10 STSOILSTKPl0 11/27/2002 10 STSOILSTKPI0 11/27/2002 10 STSOILSTKP I 0 11/27/2002 10 STSOILSTKPl0 11/27/2002 10 STSOILSTKPI0 11/27/2002 11 DDTOPLFl I 11/27/2002 11 DDTOPLFI I 11/27/2002 11 DDTOPLFl 1 11/27/2002 11 DDTOPLFl 1 11/27/2002 11 DDTOPLFl I 11/27/2002 11 DDTOPLFl I 11/27/2002 11 DDTOPLFI 1 11/27/2002 1 I DDTOPLFI 1 11/27/2002 11 DDTOPLFI I l 1/27/2002 12 SLTFNEl2 11/27/2002 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/29/2002 1301 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/30/2002 1815 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 L:'.103/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 1125 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/29/2002 2126 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) Page 21 of24 • Laboratory Batch/ID QC Lot Instruments Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i 12/04/2002 Location Date ID SampleID Extracted 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 12 SLTFNE12 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVRl3 11/27/2002 13 LFCVR13 11/27/2002 13 LFCVR13 I 1C7/2002 13 LFCVR13 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVR14 11/27/2002 14 LFCVRl4 11/27/2002 14 LFCVR14 11/27/2002 15 LFCVR15 11/27/2002 15 LFCVR15 11/27/2002 15 LFCVR15 11/27/2002 15 LFCVR15 11/27/2002 15 LFCVRl5 11/27/2002 15 LFCVRl5 11/27/2002 15 LFCVRl5 11/27/2002 15 LFCVR15 I l/27 /2002 15 LFCVR15 11/27/2002 16 ADDSMP16 11/27/2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1927 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 1950 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) l 1/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) I 1/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/30/2002 2014 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/29/2002 1349 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) Page 22 of24 • Laboratory Batch/ID QC Lot Instruments Q2804 WG2l688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q28Qi; WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG2l688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i 12/04/2002 Location Date ID SamplelD Extracted 16 ADDSMP16 11/27/2002 16 ADDSMPl6 11/27/2002 16 ADDSMP16 11/27/2002 16 ADDSMP16 11/27/2002 16 ADDSMP16 11/27/2002 16 ADDSMP16 11/27/2002 16 ADDSMP16 11/27/2002 16 ADDSMP16 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 Lab QC PBLKZA 11/27/2002 Lab QC PLCSZA 11/27/2002 MS SSEDBASTNIMS 11/27/2002 MS SSEDBASIN IMS 11/27/2002 MS SSEDBASIN I MS 11/27/2002 MS SSEDBASJN 1 MS 11/27/2002 MS SSEDBASINlMS 11/27/2002 MS SSEDBASINlMS I 1/27/2002 MS SSEDBASfN l MS 11/27/2002 MS SSEDBASINIMS I l/27 /2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) 11/30/2002 2038 12/03/2002 Doria Rawlings (ET) I 1/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12:03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 I 101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1040 12/03/2002 Doria Rawlings (ET) 11/29/2002 1101 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) I 1/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) Page 23 of24 • Laboratory Batch/ID QC Lot Instruments Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q28C4 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-I varian43.i Q2804 WG21688-l varian43.i 12/04/2002 Location Date ID SampleID Extracted MS SSEDBASIN I MS 11/27/2002 MSD SSEDBASIN 1 MSD 11/27/2002 MSD SSEDBASIN 1 MSD 11/27/2002 MSD SSEDBASINlMSD 11/27/2002 MSD SSEDBASIN 1 MSD 11/27/2002 MSD SSEDBASIN 1 MSD 11/27/2002 MSD SSEDBASIN l MSD 11/27/2002 MSD SSEDBASIN 1 MSD 11/27/2002 MSD SSEDBASIN I MSD 11/27/2002 MSD SSEDBASIN l MSD 11/27/2002 Q2804revl Warren County PCB Landfill PCB Soil Samples Collected 11/26/02 Date Time Date Analyzed Analyzed Validated Validated By 11/29/2002 1616 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) 11/29/2002 1640 12/03/2002 Doria Rawlings (ET) Page 24 of24 .. ' . Laboratory Batch/ID QC Lot Instruments Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-1 varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i Q2804 WG21688-l varian43.i 12/04/2002 --~~-COMPUCHEM -a division of Liberty Analytical Corp. CHAIN-OF-CUSTODY RE Project Name : No. 067189 ,-··-··-·:x-·---· <1ccq: _·-kcr 1Polnt-of-Contact: (D © @ ® ~ (G 501 Madison Avenue Cary, NC 27513 1-800-833-5097 Wl1ll2~'-' l\ . Jt"" (! f Cl ON ,:i M I .,. I «1:f-co::rcc-,c _ r:-w. --,,-1<--1TelephoneNo.:f"'1</ J.3c,-3,~Stp complete? Y or N (see Note 1 Sampler Name: Df:_NA/1.S 7roJ.J e-ific (PS} or Batch (8) QC ? BOX #1 1. Surface Water 2. Ground Water 8. Trip Blink I BOX #2 A. HCI + Ice C.CLP:WO T. TCLP Sample ID (9 characters maximum) 5 I~ \,(. T H 4 • .... .. 5 E. o{ 1()1 e /J r, r, (?J A 0 ( "" 5 C) " 1 1-1 s I ~ ... . IJJ I) /)_ -r /.I ~ E d I "' E "' Tl-17'µ l'J A .s I Al 7.01 8.Waste ~ > I -JI Jt,f,P l),J 'I Jlh Ii IU> I& II /2', II 1Zt, "' I/ tU, I/ JU# Box#1 .J a "' ! j IY: ~l ll'l:S5 IS: lJ{J /l,/:6 "2~ N:13 "': 2/J IJ.J:'2.~ B. HN03+1ce C. NaOH + Ice H. NaHS04 + Ice D. H2S04 + Ice I. ZnAc+NaOH + Ice E.U lox"2 Boxllll BoxM Boxlll6 I s 1 :::, -I J I u.. I 'ts 0 z ' I I I 1 I I u. Unftlered 0 0-· !g I ~ l5 o, 1(/) ~ g m ~ :::, !. "'' V' t/ "' ,/ "" ... ,_ -~,, I g i 1 1 -... e Cl ~ M.Medlum L.Low S. SW-8-46 W. CWA 600-serles O.other ____ _ Remarks / Comments (see Notes 2 & 3) ~ f; ,j T u o, ~ i s 0 ,·. , ,,,~ IJ~7t ' I e,... .... ... (!/; ~ 1 0 C ~ D I I ~ II /'lr,p /.(: II\ I ,___ ,o i) fl. ~ ll'J l 'JJ Yi '.a.. /():t/b ' '-. ..., 'C~ II /1,J, I /; ~ Clients SDKial lnstructlona: Temoerature o/, 9 °C Lab: Reclived In Good Condllon? Y or N De1ertbe Problema, If any: #1 R--Bv: (Ski) .Jl) n;-Yl fl A. -Dtl.e: //-l"H 'I 112 Retinaulshed By: (Sig) Date: #3R .. . By: (Sig) Date: Company Name: l=At.'f H -r1:cfl / V Time: 'f ,~ Company Name: Tine: . ,., Name: Time: #1 Received By: (Sig) . ...-2::: -~~,/ r/ ~ ~:.-·.,,,.,,,,,..,,---Dae: ll-~J-'1. ... #2 Received Bv: (Sia) ~ __/.£ Dat.e:/h') 7..-W9 Received Bv: (Sia) Date: Comi,anv Name: /,r:,, ..... ,,M~cl-C,. Time: "r,(A) Company Name:/': ~ J... bL~ Time: Q : ,o Company Name: Time: Note (1): lf"N'' lab will hold samples to await remainder of project-maximizing batch size ar.~ •~inimizing QC ratio; if"Y'' lab will begin processing batches now. Note (2): Samples stored 60 days after date report mailed at no extra charge. Note (3): All lab copies of data destroyed after three years. il) ~-12.. <lJ ~ ~ --~ CHAIN-OF-CUSTODY No. 067190 COMPUCHEM a division of Liberty Analytical Corp. Project Name: !Client Address: b;µrlf Zb:C /-1-I Point-of-Contact: WAe<?l:N <!o P<!.B L14Ncll=,1.t.. /o PA7Gc;oooc..l /')~Ji/I,; 1'1m e.looMII\-A, 501 Madison Avenue Cary, NC 27513 1-800-833-5097 'Carrier: 1 euulrl!Atf v..z:: '1111u-, ,S'bD,Telephone No.:,""-;J 3 v-?tJ s ~ Alrblll No.: J.J/A-l'!~~,,,_,AJ,h/l& S. (" _ ~C,~/~Samolina camolete? Yor N (see Note 1 Sampler Name : ne N 1..t/~---fl. "'l" Ol'Je,s BOX#1 1. Surface Wat.er 2. Ground Wal.er 3.Leachate e. Trip Blank I eox #2 A. HCI + 1ce F. 1ce Ontt I eox #3 F. Fltered 7. Oil B. HN03+ Ice G. Other____ U. Unfiltered Sample ID (9 characters maximum) ~ e, it ~ I) S·C! IH, ,~ ~tJ ~.c; ~ •,t. l, IAA ,~ ~, }o L ,~ F ~.-. "~ ,; ~. ~. ,49 s I. t1' ~~ r-. .,, ~~ ~ ld--c ~v ~A ,,. I ~' It> L, I; 0 l: L 11111 ,L It ~c "" j ~ ~' ,:: c.. ~! ¥ \/c le F'/A w E 0 r:.c cl ?t/ A tf --l,4 Clients SD1Clal Instructions: 8. Waste 9.0lher __ _ 8ox#1 ~ .j ~ i..; ½ i ~ ~ ~ ! ~L Ill It~ ..t,: s s I/ I~ II:/~ 11 t l~ l}:35 IJJ IU.. /3:31 1/ l'ZL 13:<ft I -ii IU~ ,,: 51:! ... I I I C. NaOH + Ice H. NaHS04 + Ice 0. H2S0. + Ice I. ZnAc+NaOH + Ice E.U Boxn Box#3 Box#& Box#I J ! t ~ I -I I I Ill 'o ~ a: u. l I I I t :; ' 0 a £' !~ ~ ~ < I u, g ::, ~ Lab: Received in Good Condition? Y or N 0..Crlbl Problems, If anf: #1 Relinquished By: (Sia) j ),. --'j!_. ~ Dat.e: / Pt 7-lr 112 ReRnqlished By: (Sial . Company Name: ,, Time: P,. Ai Company Name: #1 Received By: (Sig) g-~J~ Date:// ·t? ·•· J... #2 Received By: (Sig) ~ -~ f ~ ComDanv Name: L--~ Time: 't. · ov Comoanv Name: L.. t1 -n, r I!'/~ __ . i i I -g I m ~ 0 Cl. 'V"' it IV ... .-, I,.. .... .,, " ..... ...... Dat.e: Time: -Date: ! /;)1...-Time: ',;/0 Box #4 H. High M.Medium L.Low e :c I!: 1 --g § #3 Relnauilhed By: (Sig) ,_ Name: #3 Received By: (Sig) Comnanv Name: PS) or Batch (Bl QC ? Box #I C. CLP 3/90 S. SW-846 T. TCLP W. CWA 600-series a.Other, ____ _ Remarks / Comments (see Notes 2 & 3) Temoerature ~. 9 °C Date: nme: Date: Tme: Note ( 1 ): If "N" lab will hold samples to await remainder of project-maximizing batch size and minimizing QC ratio; if "Y" lab will begin processing batches now. Note (2): Samples stored 60 days after date report mailed at no extra charge. Note (3): All lab copies of data destroyed after three years. lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: lSOUTH SDG No.: Q2804 Sample wt/vol: % Moisture: 26 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-l Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 44 U 57 U 44 U 30 U 30 U 30 U 44 U Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET 2SEDIMENT Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Contract: 8082 SAS No.: SDG No.: Q2804 Matrix: (soil/water} SOIL Sample wt/vol: % Moisture: 35 30.0 (g/mL) G decanted: (Y/N) N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000(uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N} N pH: CAS NO. COMPOUND 12674-11-2------Aroclor-1016 Lab Sample ID: Q2804-2 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 1.0 Sulfur Cleanup: (Y/N) Y CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 11104-28-2------Aroclor-1221 _______ _ 50 U 65 U 50 U 35 U 35 U 35 U 50 U 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 FORM I PEST 1D EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET 3BASIN Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Contract: 8082 SAS No.: SDG No.: Q2804 Matrix: (soil/water) SOIL Sample wt/vol: % Moisture: 19 30.0 (g/mL) G decanted: (Y/N) N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S0O0(uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND 12674 -11-2------Aroclor-1016 11104 -28-2------Aroclor-1221 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 11096-82-5------Aroclor-1260 Lab Sample ID: Q2804-3 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Sulfur Cleanup: (Y/N) N CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 40 52 40 28 28 28 40 Q u u u u u u u FORM I PEST lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 4SOUTHSLOPE SDG No. : Q2804 Sample wt/vol: % Moisture: 19 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-4 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-~------Aroclor-1221 _______ _ 11141-16 -5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 40 U 52 U 40 U 28 U 28 U 28 U 40 U Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: SNORTH SDG No. : Q2804 Sample wt/vol: % Moisture: 30 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-5 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000 (uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N} Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: {ug/L or ug/Kg} UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 46 U 61 U 46 U 32 U 32 U 32 U 46 U Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 6SEDIMENT SDG No. : Q2804 Sample wt/vol: % Moisture: 9 30.0 (g/mL) G decanted: {Y/N) N Lab Sample ID: Q2804-6 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: {SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 36 U 47 U 36 U 25 U 25 U 25 U 31 J Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: ?BASIN SDG No.: Q2804 Sample wt/vol: % Moisture: 19 30.0 (g/rnL) G decanted: (Y/N) N Lab Sample ID: Q2804-7 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000 (uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 40 U 52 U 40 U 28 U 28 U 28 U 40 U Q 1D EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPO Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 8S TRIPPED SDG No. : Q2804 Sample wt/vol: % Moisture: 27 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-8 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 2.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 89 U 120 U 89 U 62 U 62 U 62 U 1000 Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 9STOCKPILE SDG No.: Q2804 Sample wt/vol: % Moisture: 19 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-9 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 2.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000(uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) Y CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 110 97 - 6 9-1-- - - --Aroclor-~-2 54 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 80 U 100 U 80 U 56 U 56 U 56 U 610 Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: l0DRAINDIS. SDG No. : Q2804 Sample wt/vol: % Moisture: 19 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-10 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 50.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 ________ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 2000 U 2600 U 2000 U 1400 U 1400 U 1400 U 11096-82-5------Aroclor-1260 19000 -------- FORM I PEST Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET llDRAINDISTOP Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Contract: 8082 SAS No.: SDG No.: Q2804 Matrix: (soil/water) SOIL Sample wt/vol: % Moisture: 26 30. 0 (g/mL) G decanted: (Y/N) N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL} Injection Volume: 2.0(uL) GPC Cleanup: (Y/N} N pH: CAS NO. COMPOUND Lab Sample ID: Q2804-11 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 1.0 Sulfur Cleanup: (Y/N} Y CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 12674-11-2------Aroclor-1016 _______ _ 11104-28-2------Aroclor-1221 44 U 57 U 44 U 30 U 30 U 30 U 44 U 11141-16-5------Aroclor-1232 _______ _ 53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 _______ _ 11097-69-1------Aroclor-1254 11096-82-5------Aroclor-1260 _______ _ FORM I PEST lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS "ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 12SILTFENCE SDG No.: Q2804 Sample wt/vol: % Moisture: 18 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-12 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000 {uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 40 U 52 U 40 U 27 U 27 U 27 U 40 U Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 13LANDFILL SDG No. : Q2804 Sample wt/vol: % Moisture: 23 30.0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-13 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1 ------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 42 U 55 U 42 U 29 U 29 U 29 U 42 U Q lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Matrix: (soil/water) SOIL Contract: 8082 SAS No.: 14MIDDLELAND SDG No.: Q2804 Sample wt/vol: % Moisture: 23 30. 0 (g/mL) G decanted: (Y/N) N Lab Sample ID: Q2804-14 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1 .0 Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: 5000 (uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y /N) N pH: Sulfur Cleanup: (Y/N) N CAS NO. COMPOUND 12674-11-2------Aroclor-1016 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 11104-28-2------Aroclor-1221 _______ _ 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 _______ _ 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 _______ _ 11096-82-5------Aroclor-1260 -------- FORM I PEST 42 U 55 U 42 U 29 U 29 U 29 U 42 U Q 1D EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET lSLANDFILLCOV. Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Contract: 8082 SAS No.: SDG No. : Q2804 Matrix: (soil/water) SOIL Sample wt/vol: % Moisture: 26 30.0 (g/mL) G decanted: (Y /N) N Extraction: (SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000(uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND 12674-11-2------Aroclor-1016 111C4-28-2------Aroclor-1221 11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 11096-82-5------Aroclor-1260 Lab Sample ID: Q2804-15 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/29/02 Dilution Factor: 1.0 Sulfur Cleanup: (Y/N) N CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG 44 57 44 30 30 30 44 Q u u u u u u u FORM I PEST lD EPA SAMPLE NO. GC EXTRACTABLE ORGANICS ANALYSIS ·DATA SHEET 16EXTENDED Lab Name: COMPUCHEM Lab Code: COMPU Case No.: Contract: 8082 SAS No.: SDG No.: Q2804 Matrix: (soil/water) SOIL Sample wt/vol: % Moisture: 3 30.0 (g/mL) G decanted: (Y/N) N Extraction: {SepF/Cont/Sonc) SONC Concentrated Extract Volume: S000{uL) Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND 12674-11-2------Aroclor-1016 Lab Sample ID: Q2804-16 Lab File ID: Date Received: 11/27/02 Date Extracted:11/27/02 Date Analyzed: 11/30/02 Dilution Factor: 1.0 Sulfur Cleanup: {Y/N) Y CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 11104-28-2------Aroclor-1221 _______ _ 34 U 44 U 34 U 23 U 23 U 23 U 95 11141-16-5------Aroclor-1232 _______ _ 53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 _______ _ 11097-69-1------Aroclor-1254 11096-82-5------Aroclor-1260 _______ _ FORM I PEST