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NCD980602163_19981026_Warren County PCB Landfill_SERB C_Well Log Sheets-OCR
. , WELL LOG SHEET Facility: Warren Countv PCB Landfill Location: Warrenton Purge/Sample Team: grvlebi,Jgvi'::lt(["""" -Well #: _/_~------. tD-hJ ' . \ Comments (well construction, etc): Y\'\W-l L . · lkpt\. 3g, ~ dtf>tL· tc €,\,0 ".)), ef'l · . I\::-\0 .... , . ,.EJceC ~:> · 7.11 ·y.. D,~ = 3, 57-.v ~t, . Purge Information Conversion Factors:. For 2" well 3 volumes (gallons) ·do.5 x height of water column (feet) · For 4" well 3 volumes (gallons) = 2.0 x height of water column (feet) -. For .hailers: 4 bails· = 1 gallon . 1 Well Volume (gal): /. 2J ti.J, 3 Well Volumes (gal): .3,.fr ~d Purge Equipment: .);)t.1/1;11) J -J+-='-"-'-+-'J ~---Date Purged: · / ~ /,£)..,fr /q<( r r , · Purge Time Start: /(Jt/J1+1-v1 Purge Time End: l 13tfu,\ ; Did well purge dry? . Y @,-Actual.purge volume: . '7 ;ta,e, . V "' .. ' .... --Volume_l Volume__£ . Volume _a_ Volume-5.Y,3,., Volume.±_ Volume _k Temp ("C) •/ Jo I~ r,L, ~v I 1o0c.. ~\,~ t< I. l j 3 ~:J"c-pH • ·:5,4~ S.11 5,q3 5. 14? f5,41 S. c: . I icr-1 "~ I J~\ ,,~ ·\ :>5{) A, S i 9-.iv rJ? JI 5J.vS r I D. 0. ,.,_ ~ I . Turbidity · ~q I n-\i~ · ¾S'n·hh 3:'.3 l ntvs ~5J nhA j (o~ fltlfS ct-,,;_~1 -~, }'Tl\)~ -ia,.u.r.~ 7'.L..4-t• --' I u rb?ct-t+Yj I ,53, nfvs . 1Ll{nfl.Js 31{nw,,. Mtmtis .J&tJl'iN~ ;i35h-hh 141 nh> ll£4nrv~ ~ Sample Information Sample Date: / v /JIJ { Cf8 Sample Time: / /3t --'--'---'----Sample Equipment: -P1,.._J...__1~...,,v,""f?-----Water Condition (turbidity, odor, etc.): llt'¼f. -:;; JJJ30G f H--;; 5 ,4:7 l\;ud, fJ : bi. d4, to ~23 n 1'JS-_ D~.d . ~ ) I 9,u..,\ l Samples Collected J,/-f · · -~ VOCs (2 40 ml vials) / SVOCs/PCBs (1 2L Amber bottle) Metals (1 IL HDPE bottle) Dioxin (1 IL bottle) Pest./Herb. (1 2L amber bottle) Temp(° C): _2~, 3 pH: 6',4] SC(umhos): / /.5~ DO(ppm): __ Turb(NTUs): XJ ~ Comments: --------------------------------------______________________________________________________________ pcbwells.frm WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Well#: I/\ .. ,_ ;\ Purge/Sample Team: --------------------------'-----Comments (well construction, etc): :,,.,u.1 ~ -~ ;:,. ,·:.. -~.-:---::.. :.._ 1 [!._:; -.. _ _ L. . -. t Purge Information -=(-!. Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet) For bailers: 4 bails = 1 gallon 1 Well Volume (gal): b. 'to 3 Well Volumes (gal): a,o Purge Equipment: cf,...,. ...... ~~-> Date Purged: · / IJ-2 t,-1 ~ Purge Time Start: /CJ: I> /2:'i,(..) Purge Time End: :f-'J( u o ,i/c... Did well purge dry? Y @_, Actual purge volume: lo. S' 1"" ( Volume C Volume I Volume ;,,-Volume J Volume Volume -----Temp (°C) .. , . -~ ...... t-\ . !. ~-1'.5.'7 {'. L,, :~f. '.) {.U ,,,_., L . -,_ -pH ·~·~~--(~ ,_--: b (_., , :~ ~.; S. C. l3oi1 v~ / ;17 /"d i1--i3 f" i 1 .,,. . ' D. 0. -Turbidity 3~S-4 3.:rv r;_ ,''}, I 0/1·-{ Sample Date: Sample Information Io~ 2,-'i ~ Sample Time: /l-·5c!J Sample Equipment: &"rv J ~> f!-, :£ Water Condition (turbidity, odor, etc.) :_:.....,N....::a_-1'---'--l.=:....:....,,.=k---'-';J,:c_____ _ _;_~-=-=--"-J._.,_,,,,.. ____________ _ Samples Collected (✓): __ -VOCs (2 40 ml vials) _J SVoc€)1 2L Amber bottle) Metals (1 IL HDPE bottle) Temp(° C): __ _ pH: SC(umhos): Comments: ---Dioxin (1 IL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ _ Turb(NTUs): ------------------------------------------_____________________________________________________________ pcbwells.frm WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Purge/Sample Team: tr~1JJ:GC Well#: I (d.1£j'J Comments (well construction, etc): ~ill diftiu 51 , q 2 ( 4-11 y\ll\l) d1{ci't" lD ~o -4 z . D~ 1 '-Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet) , For bailers: 4 bails = 1 ~allon Gvt ir'llt · 1 Well Volume (gal): lv -~::f9.t-( 3 Well Volumes (gal): I "f i 1 o Purge Equipment: Oiw~ . , ( { ;1,;20 5 Zi) Date Purged: / 61 J{;/ff Purge Time Start: ol {Wu Purge Time End: f'»1 Did well purge dry? Y ,'t)-Actual purge volume: J. IJ, S-0 J61 . Volume _Q_ VolumeJ/42., Volume _42/ Volume.a ~ Volume...:'.) Volume -Temp (°C) ~/.0 0(,, lq, lf0c /C1.1i)0 ,:2 I. D ;)0 J7,tcL pH s.1+ 5 ,9) '5/73 lt, Dl 5.q~ S. C. /3~ µ_S 1315..u5 J 210 .oS 12 Vlt ,tlS I 255'} ;i'~ D. 0. Turbidity • q(o mus 0, lo 3nh,i~ 5.l/t nit>~ 0, &'& n-fv O ,37ntus Sample Information Sample Date: /D~e/qf ' J . Sample Time: 5'2-<J . l,;r:JM Sample Equipment: ~ ~ Water Condition (turbidity, odor, etc.): -------------------------Samples Collected (✓): VOCs (2 40 ml vials) ✓ SVOCs/PCBs (1 2L Amber bottle) Metals (1 IL HDPE bottle) Dioxin (1 IL bottle) Pest./Herb. (1 2L amber bottle) Temp(°C): n,ltG pH: s i q) SC(umhos): IJ81,4t..~ DO(ppm): --Turb(NTUs): 6, 3/n-b.,'S Comments: --------------------------------------_____________________________________________________________ pcbwells.frm WELL LOG ·SHEET Facility: Warren County PCB Landfill Location: Warrenton Purge/Sample Team: ------------------'~/ 1, I 1 Well#: . • , cv 1--Comments (well construction, etc): 4 { :: G. T.=.id ]\,,.•rl, _:,,: 2... L J\ ., +,,.I~._ k--2.. -.:.'1 )f1 ,j, --' ..... -i "C~ i....,>-~.-r~ Purge Information Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet) For hailers: 4 bails = 1 gallon 1 Well Volume (gal): 7,04 3 Well Volumes (gal): .,;t 1. l. ~ Purge Equipment: ~I?,;) 6 f Date Purged:· I/J-U-"i 7 Did well purge dry? Y Volume 0 N / -Temp (°C) I/ i~ ,1 pH ·6,"7 S. c: /b'6D D. 0. Turbidity tJ ,t f Sample Date: /o-J....(;-'t 'r> Purge Time Start: _j_s-.-o D Purge Time End: ______ _ Actual purge volume: _____ _ Volume_! Volume '2-Volume 3 Volume Volume -/q ( 1 /1,S-l'f,S° i,oo ~S.Cftf HY-~~ /02.'( I 16 I /!l> C>,i2-3,oL J.')._~ Sample Information Sample Time: _J 1 !/C Sample Equipment: ?r-~", -Water Condition (turbidity, odor, etc.): th I, +..J .f.-r V--1 3 _.....:...._....-',j£ ____________________ _ Samples Collected (✓): __ -VOCs (2 40 ml vials) ✓ ~ 2L Amber bottle) Metals (1 lL HDPE bottle) Temp(°C): __ _ pH: SC(umhos): ---Dioxin (1 IL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ Turb(NTUs): ---Comments: G-4.e,r~~ c.:,.,__-t.,vp✓~L, s..l,~',"'1 £.,,.. fv(.,l /,~.,_ JLC,~,«, ____________________________________________________________ pcbwells.frm ; ' , t ' ' t f ~ WELLLOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Well#: ·17 Purge/Sample Team: . f {utlA{ /l{a,...-V --------Comments (well construction, etc): 1'1"'-i)_~,..~ Yt rt, D-r-' .::: iLI. f · Conversion Factors: For 2" well: 3 volumes (gallons) ·= 0.5 x height of water column (feet) ·· . Purge Information For 4" well: . 3 volumes (gallons) = 2.0 x height of water ~olu~ (feet)· . . .. , . For _bailers: 4 bails = 1 gallon t; r-~ i'Dttf 1 Well Volume (gal): t 1 3 Well Volumes (gal): J'. { 6-f'L Purge Equipment: ~ f'J>A-,_~ Date Purged: · /o/ 2 7 /1~ r 1 Purge Time Start: _JO,· O <t Purge Time End: ______ _ Did well purge dry? Y N Actual purge volume: ------Volume F,,. "L .. -Volume CJ Volume _j_ Volume ..:k:_ Volume..3._ Volume , --Temp (°C) ,.,. /"a.~ "'2,.0. t/ 1-0. 1 1,,c.7 pH :_ \S-.3Cf ,_i-, l,J ..r. L1 s. '-7 -r i S. C. I 10 f / q \ ,'\.--'10.l./ t7.9 -.-i I ;· ! I Ii D. 0. •-I ' -..::,,,-, I I Turbidity 3 /, C/ L/, I\.{ (, .oL LL. Y {1.r-Sample Date: IO /i 1 / 1 ( Sample Information Sample Time: ID :Sb Sample Equiprrient: 6 flA"-,JllfiJJ p1,1 ,,..f> ' Water Condition (turbidity, odor, etc.): ------------------------,--Samples Collected (✓): VOCs (2 40 ml vials) ,( SVOCs~ (1 2L Amber bottle) Metals (1 IL HDPE bottle) Temp(°C): __ _ pH: SC(umhos): __ _ Comments: Dioxin (1 IL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ _ Turb(NTUs): -----------------------------------------__________________________________________________________ pchwells.frm WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Purge/Sample Team: fji~ /<f1tmcc: Well#: Y\~~.,, <;'° (dfzf) Comments (well construction, etc): -~ d1t4i'--Ul !139\ 11-lpt:{&-b:, t;bQ -3(,,-,4-1< Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) Purge Information For 4" well: 3 volumes (gallons)= 2.0 x height of water column (feet) For hailers: 4 bails = 1 gallon 1 Well Volume (gal): 4, j~. 3 Well Volumes (gal): / ~, S'cttJ Purge Equipment: r'·f '{)Jrn.{2 J f J Date Purged: lo /;;21/1¥ Purge Time Start: / 0 '&l'J Purge Time End: i f4<Jf'hn I 7 Did well purge dry? Y @ Actual purge volume: / J... . 1 S' /t'-f-. Volume _L Volume oL Temp (0C) i q, L-/cJ u Ii..</ pH u,Z'l-(p , Ii S. C. ID z;i },L~ { I o I ,u5 D.O. Turbidity 0 l17.H1{( Orli1 r1tJs Volume3 Volume I q '('0 {_;. OU IO 1lr µ<;. 0, ~1whl'> Sample Information 114 6 .A1V\ Volume Volume ---Sample Date: Jo/:27/c;'( I J Sample Time: • Sample Equipment: -+-p.;:c..v-'--'Y½f""'.f-L-----Water Condition (turbidity, odof,-:.etc.): ------------------------Samples Collected (✓): VOCs (2 40 ml vials) / SVOCs/PCBs (1 2L Amber bottle) Metals (1 lL HDPE bottle) Temp(°C): (q. [ pH: (o.aJ SC(umhos): __ Comments: Dioxin (1 lL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ Turb(NTU s): ----------------------______________________________________________________ pcbwells.frm WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Purge/Sample Team: fZei5--e_ / S'/;;.n (e y Well#: /'17 tJ -/ / r I ------------'----'------Co mm en ts (well construction, etc): fJ Y--/ f A f c..1 /4J fr z---J (p • 17 1 Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) Purge Information For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet) For bailers: 4 bails = 1 gallon 1 Well Volume (gal):___ 3 Well Volumes (gal): ____ Purge Equipment: jJ_c,1·/ er' Date Purged:· J J/ -:Z 7 ;··'1 r Purge Time Start: "1_,' /D I I Purge Time End:____,_?--'·:_, 3,e__u_ .... __ _ Did well purge dry? Y @ , Actual purge volume: t, f:tJi.. .· --I h;:J ~l G. u Volume · Volume Volume Volume Volume Volume -----, Temp (·C) ,., pH S. c: D.O. Turbidity Sample Information Sample Date: / tJ) · ?-'7. / I Y Sample Time: /:.JO t r1 I . 7 Sample Equipment: j]_ 4, / e..r Water Condition (turbidity, odor, etc.): i'.Lvs,,__ ...,.,,. f-':i. v,.J -~;[ b, J i~& ,~\d Samples Collected (✓): · VOCs (2 40 ml vials) V svocs@c1 2L Amber bottle) Metals (1 lL HDPE bottle) Temp(°C): ___ pH: ___ SC(umhos): __ _ Comments: ~ /""-// U--Tt.,,, r ~ 1 d l Dioxin (1 lL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ Turb(NTUs): ---__________________________________________________________ pcbwells.frm ~ -1 -I- WELL LOG SHEET Facility: Warren County PCB Landfill Location: Warrenton Purge/Sample Team: P~ ,e, / J)✓ a 11 h ~ ' :, / ·. / Comments (well construction, etc): De.pl/ /2 t,., ~r -:-~d. t / ,✓ /JR,t-.!f ~-) ,~. ue. // -,' -Well#: h tJ -1 /) / // -~ 7.,.,,u ,-✓ ~/ ✓-Purge Information Conversion Factors: For 2" well: 3 volumes (gallons) = 0.5 x height of water column (feet) For 4" well: 3 volumes (gallons) = 2.0 x height of water column (feet) For .bailers: 4 bails = 1 gallon 3 Well Volumes (gal): ___ _ 1 Well Volume (gal): __ _ Purge Equipment: /3 c.. //-!: ,.,-.. Date Purged: · Io/) 7 / lY Purge Time Start: o/ .' 3-S-<::?'/'"'1 Purge Time End: 9 ,' t/S-c;-/Y1 Did well purge dry? Y @ i A~tual purge volume: /' C .S-,~ Clo 5-e_ ~ At /2e,,:i /CA_ Volume Volume Volume Volume Volume Volume ------Temp (0C) ,,,. pH S. c: D. 0. Turbidity Sample Information Sample Date: ! 0 / 1-, /f"t I Sample Time: /,' '-fD Sample Equipment: _/;zg""--l--_/JZ.-c. ___ _ Water Condition (turbidity, odor, etc.): ~~/4 ~/:;d · .. --"~-=-=,.,==------=~-=--------------P ,_._._1r w rd;;:. L k1 d Samples Collected (✓): __ · VOCs (2 40 ml vials) ✓ SVOcs@(l 2L Amber bottle) Metals (1 IL HDPE bottle) Temp(°C): __ _ pH: SC(umhos): ---Dioxin (1 lL bottle) Pest./Herb. (1 2L amber bottle) DO(ppm): __ Turb(NTUs): ---Comments: _____________________________________ _ _______________________________________________________________ 1pcbwells.frm NC Ocp,11~cnl of l::nvircnmcnl, Hullh, & N,wrsl Resources Solid W,,~ M1r..1gcmcnl Divi,ion SAJYIPLE AL'\' AL YSIS REQUEST SL.Ate uboraLOry of Public Hu.Ith P.O. Box '.:8047, 306 N. Wilmington St. Raleii;h, North Cuolim 27611-8047 SitcNi..lrnbcr _______________ SamplcID,Nurnbcr/Namc Olu5sl .. ······ Na1I1eofSit.c (j} ARR'f N Guf\r(Y PcE LN DFL Collected By· l+ L.. IDll ---,----SiteLoC2.tion W 1\/l.,P,EIJ ~NTY Date Collected Ito-)..(;~ '1. '6 Time .. · ll:.30 Azency: Hazardous Waste Solid Waste __ Superfund-TCLP Compounds / \J 1-11. o ~lJAJiE, }11111&--/1'\ --. Sample Type Environment.al Concentrate _i Ground Water (1) ._ Solid (5) Surface Water (2) __L'Liquid (6) Soil (3) _ Sludge (7) Other ( 4) _ Other (8) Organic Chemistry Comments Yh.w -l 'L T....i cb:'...\ s...__,..,..,,,~lt Iuorganic Chemistry Inorganic faJ~~VEQesults(~g/1) arseruc b . . . (Y ' ') ~ -JQl°V"I . anum N 1_1 V ,.,_, -'-,i_. -'-'-'·-'-''-l-"_,-.,,-,.-'-------cadmium cbffiJPERFU N.0..SE CTION lead mercur; selenium silver Parameter ?&T:GC/MS Acid:B/N Ext. Results (m~il) j Par2.;-neter Results(mg/l)(mg/kg) 1 · Organic Compounds antimony _______ be!lUue . Resu!ls(mg/1) 2,4-D _:__ ·2,4,5-TP(Silvex) chlordane heptachlor hexachlorobeo.z.ene ______ _ hexachlorobut.adieqe ______ _ endrin li.ndane arseruc barium beryllium c:ad mi u cc chloride chrorniu:n cobalt c~pper fluoride carbo!l tet[?.ci:uo,-icc chlord.zne chlorobeuz.ene chloroform o-crcsol m-cresol p-creso). cresol 1, 4-d:cl-Jorobenzene rnethoxychlor ;ron J ,2-,jid1.loroethane _______ _ __ toxaphene _L Pc~ i-.1 lead manganese mercury nickel nitrate sele!lium silver sulfates thallium vanadiuc.· Zli1C 1, J-dichlo_rocthylene _______ _ _<O,0Do/f1'/'t\.. \ ___ _ FOR LAB USE ONLY L':!tc Rccciv~C/-Cjf3 pd · .· ~c,dt/, Da:~ Extractpiffe~ pH condu~tivir; ______ _ 2, 4-dichloroethyleue beptachlor hex.acWo ro ben.zcne bex.ac hloro b'...!t.adi~~e -~. hex.acb.loroetbar:e methyl ethyl k~:o:ie n.i t roben..z.ene pentacblo:-ophcncl pyridine tetrachloroethylen:: __ trid1.!c:octhylc:nc 2, 4 ,5-lrichlorophcr.ol ---------------------------Date ~lvz.ed Jo-.3"-9?"VP TDS 2,4,6-trichlorophen,11 _____ . flash point vinyl chloride cndrin . .{l . .. I ·--I r ch.i Date R0;~-~~_U~J f_-i/ . = ~---__ -. ----------··--\ = :clh:,~yc:hlr,r · · · 9835 ~4 I __________ · _ toxaphene L1bNurnber ______ ~--____ ---l-?.,4-D • "2 •; 5-TP Sil·1,·r\ ul!~ 3$cf,J';?n_£-t;-y .-C/ F~--=~----· __ ~-=--·: __ ~~-~--• ~-----~ --~ ~---~=:=~~~-~-. NC Dqanmcnl of Environment, Hulth, &. Nu1Jr1l Re.source& Solid W=<!.c Muugcrncnl Divi&ion SAJvIPLE AJ.'\l"ALYSIS REQUEST Swc ubomory of Public Hu.Ith . P.O. Box: :28047, 306 N: Wilm..ington St. R,lcii;h, North C,rolina 27611-8047 Site Number ______________ SamplclD,Numbcr/Namc () J...O SS i_·· ti a.me of Site UJ AB,R'~N Gul\JN PcJ3 LN DFL CDllcctcdBy·: \-½L ID# ,· --:--:-----:---_;_;__ SiteLocation W Ptlli/J fo.jNTY Date Collected . !o-2.o Tim~. · . (i,.'i ·:3, 6 Agency: Hazardous W a.stc Solid Waste __ Superfund-TCLP Ce-mpounds 7 0 I~\/. 0 ~lJA,;tE, fl1111~,1'i -Sample Type Inorganic Compound:: Resulls(mg/1) Environmental Concentrate Comm en ls arseruc -barium -~ Ground Water (1) -. Solid (5) mw 3A cadmium -chromium -_ Surface Water (2) L Liquid (6) lead -_ mercury . ; _ Soil (3) _ Sludge (7) selenium silver -Other (4) _ Other (8) ---Organ.ic Chemistry Inorgan.i,: .Chemistry -Parameter Resul ls (mg/I) Parameter Restilts(mg/l)(mg/kg) · Organ::: Compounds Resulls(mg/1) P&T:GC/MS _ ""'7timony benzene ----Acid:B/N Ext. arseruc carbon tetrachloride ---2,4-D barium chlordane ---_·_ ·2,4,5-TP(Silvex) _ beryllium -ch.faro benzene chlordane cadmium chloroform ----_ heptachlor chloride o-cresol -· -hexachlorobenzeoe chromium m-cresol . -----hexachlorobutadieQe cobalt p~resol --endrin _ c?pper cresol --lindane fluoride 1,4-dichloroben.zeoe --_ methoxychlor lfOn 1,2--dichloroethane --_ toxaphene lead _ 1,1-dichlo_roethylene ✓PC~'..s -< o. ~ o o I .f?l2./"'I\.. _ manganese _ 2,4-dichloroethylene --_ mercury _ bept.achlor -nickel hexachl o ro benzene ----nitrate bexachlorobutadiene --selenium ... hexachJoroclhane --· •· ·• silver _ methyl ethyl ketone -FOR LAB USE ONLY : sulfates nitroben:u:ne --thallium . _ pent.achlorophcnol -Dato Rocc;vod · LO-.J9i/!_8Z2d vanadium p•1:idine --, z.inc -telrachloroethylene . tf'eBtf !'Jlfj -Date .Extracted h. -~ ~9g"y"f} _, pH _. _ tri::hJoroethylcne <; _. . pes~/1;$"nr) . _ conduc_tivity _· _ ·2,4,5-trichlorophcnol · Date j1J1alyzed Lo·..,. 0-LJr-vp TDS _ 2,4,6-trichlorophenol . ·.· ~-. -Reported .By _ flash point _· vinyl chloride _ endrin -Dale R~p-~~~ -lind.ane -'98351!5 --_ mcthoxyr.blor .. ub Number -_ toxaphenc 2,4-D --OHS 319 i (Rcvi,.cd 12/9]) -_ 2,4,5-TP (Silvcx) I I I I I ------ NC Dcp,r1mcnt of Environment, Hullh, & Nawr•l R"-<ourccs Solid W,,tc M1r ... gcmen1 Divi,ion SAlvrPLE A.t"'lALYSIS REQUEST Sutc uboratory of Public Health P.O. Box 28047, 306 N. Wilmini;ton St. Raleii;h, North C,rolin, 27611-804, Site Number---------------'---Sample ID, Numbcr/N amc __ ._D-:-1....-'o=-._,,5"'----'5,__'3=---.:..._:_:_.:.c..:_~..:..:_---NameofSit.c L0ARRi£N Cut\JN PCT3 LNOFL CollcctcdBy·:· l-ID# ---:---:----SiteLo~tion W ttlliJ.J {c,.j/\/J'i Dat.cColl~tcd lo-l. G Tii:ne I~~ --•' Agency: Hazardous W a.st.c Solid Waste __ · Superfund· TCLP Compounds / \J l'v. o \'="lJA~Th f)lNv/1\ --Sample Type Inorganic Compounds Results(mg/1) Environment.al Concentrate Comments arseruc -barium -V Ground Water (1) _ Solid (5) (Y)W I cadmium -chromium -V Liquid (6) _ Surface Water (2) lead -_ mercury ' Soil (3) _ Sludge (7) selenium -silver -Other (4) _ Other (8) ---Organic Chemistry Inorganic Chenuc;try -Parameter Results (mg/1) Parameter Re:sul ls (mg/1) (mg/kg) · Organic Compounds Results(mg/i) P&T:GC/MS _ antimony benzene ,--l-f.·~id:B/N Ext. arseruc carbo:i tetrachloride --I 2,4-D I barium chlordane 1--·-I _·_ ·2,4,5-TP(Sdvex) I _ beryllium chJorobeo.zeoe --1 chlordane · cadmium chloroform I ---.. -_ hept.act.lor i chloride o-cresol ! --hexachlorobec.zene chromium m-cresol . ---·---hexachlorobut.adiene cobalt p-cresol ---endrin · _ copper cresol --Ii.ndan~ fluoride 1,4-dichloi-obeuz.eoe --I methoxychlcir iron -1,2-dichloroethane I= toxaphene -lead _ l, 1-dichloroethylene ~ PCB '..s -<o,ooo/f'ftt1 _ manganese _ 2,4-dichloroethyleoe . , _ hept.achlor -_ mercury I nickel hcxacWo ro benzene 1= --nitrate hexachlorobut.adiene --selenium ... hexacWoroethane L_ --· silver _ methyl ethyl ketone --·----·---·--FOR LAB USE ONLY sulfates n.itrobeuieue --thallium . _ pent.achlorophenol _L'.:Ie Received · /0-;l'i-98 7J.j_ -vanadium _ pyridine . . {f'Cf3 5-(/ilsrT~ .· -2U1C _ tetracWoroethylene Dat~ Extracted /I ...:-3~ -_, pH _. _ tri::hJoroethylene . . f'e8 f (M · . _ condu<::tivity _· _ ·2,4,5-trichlorophenol · Daie.Analyzed / /-"-J -rr.yp TDS _ 2,4,6-trichlorophenol • •. -~ ;. ,1 ..• -Reported .By _ flash point _· vinyl cliloride -endrin -lindanc -Date R~p-;rt:~ -__ methnxy,.hlor toxaohenc: Lab Number 9835l;t6 DH:; 3191 (\l.c-,i,cd l'2/93) ~---·----___ J~ ;:;,}," cs;1~aJ __ _ I I NC Dcp,nmcnl of Environment, Hullh, J.: N,wnl Re.sources -Solid Wa,tc Muu~cmcnl Divi,ion SA.lvIPLE ANALYSIS REQUEST Sulc Libom~ry of Public H~ilh P.O. Box 28047, 306 N. Wilmington St. Ralcii;h, North Cuolina 27611-8047 Site Number -----------------'---Sample ID, N umbcr/N a.me C> )....o S S-~ . NameofSitc ltJARRi::NGvNT'{ PcB LNDFL CollcctcdBy· . \A:'L.. ID# --~-'--SiteLocation W 1/U.e/J ~1,ffi Date Collected tD -l.-<;. -:-1 "'l Time . . \'l :;:.-6 Agency: Hazardous Waste Solid Waste __ · Superfund-TCLP Compounds. / \J tv. o ilJA.iilS t11r-1t---,,-; -Sample Type Environmental ✓ Ground Water (1) Surface Water (2) Soil (3) Other (4) Concentrate Solid (5) ✓ Liquid (6) Sludge (7) Other (8) Organic Chemi.5try Comments r,1_ w 1-Inorga!lic .Chemistry Inorganic Compounds arseruc · barium cadmium chromium lead mercury selenium silver Results(mg/1) Parameter P&T:GC/MS Results (mg/I) I Parameter Results(mg/l)(mg/kg) 1 · Organic Compounds antimony _______ benzene Resul ts(mg/1) .c ... c:d: P./N Ext. 2,4-D _·_ ·2,4,5-TP(Silvex) chlordane heptachlor hexachlorobeuzene _____ _ hexachlorobutadiene end~ -~------!ind.an~ . methoxych16r toxaphenc ✓ pc~ i.j <o, oool ff'P'l. FOR LAB USE ONLY Date Received ,c, oL , --, u -',: :..:.i-11 • -,. Date Ex.tract Dat~-'Analyzed 77:9~'hnfp • • ••.P•.•;•:~\~'•: • • Reported .By Date R~p·~-rt~ S83547 Lab Number OHS J 191 (P.cvis,:d J::i.i93) I L__ arseruc barium beryllium cadmium chloride chromium co ball c~pper fluoride iron lead manganese ---------=-mercury nickel_ nitrate selen.ium silver sulfates thallium vanadium ZlllC pH conduC:tivity _______ _ TDS flash point -'--------carbon tetrachloride chJordane chJorobeuzenc chJoroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenz.ene -------1,2-<lichloroethane 1,1-dichlo_roethyleoe ______ _ 2, 4-dichloroethylene hept.achlor hexachlorobenz.c:::ie hexachlorobutadiene ... hcxachloroethane methyl ethyl ketone nitrobcnzenc pent.acWorophenol pyridine tetrachJoroethylene _ trichloroethylene _· _ ·2,4,5-trich.Iorophcnol -2,4,6-trichlorophenol vinyl chloride endrin lind.ane methoxyr:hJor ---------------------------------------1 ~:t:c(S;i"c,) NC Dcp1r1mcnl of Environment, Hc.,_\lh, & N,wr1\ Resources Solid W,,~ Muu~cmcnt Division SAJYIPLE ANALYSIS REQUEST St.He L..bor•tory of Public Health P.O. Box 28047, 306 N. Wilmington S1. R•lci~h. North Cuoli.ru 27611-8047 Site Number _______________ Sample ID, Number/N amc --'----:=-o....::..J....v_·_:.')_:5'=-cS"=---,-.-..:.._:___~.::..:::.~--....:..--NameofSite WAR,R·~/\( Cr.11\JN PcE LNDFL Colkctc<lBy· \-h_ ID#. ---,----Site Location W 1(U,,£.IJ lc,J/\JT'i DatcCollectcd 10~~1-q f Ti~c ·/o::so Agency: Hazardous Wa9tc / \J 1·11. o ~lJAi1iE, Solid Waste __ . Superfund· TCLP Compounds fl'\Nv,1\ -. Sample Type Environmental Concentrate _J{ Ground Water (1) _ Solid (5) _ Surface Water (2) v' Liquid (6) Soil (3) _ Sludge (7) _ Other (4) _ Other (8) Organic Chemistry Parameter P&T:GC/MS Acid:B/N Ext. __ 2,4-D _._ ·2,4,5-TP(Silvex) 1-chlordane hept.achlor hexachlorobenzene Results (mg/I) -------hexachlorobut.adiene ______ _ endrin -... lindane _ rnethox.ychlor _ toxaphene ✓ Pc~ '.s . <: a .. "ao '-f¥!-.nt FOR LAB USE ONLY Date Received · /O-;Lq -9 fl>. tJ.j . . . rv'--U .-~ . . . ~AA~ ~ Date :Extracted /CJ-:; 9 · · .. ·.·. PctJ4'M;r-oY) ·D~t(Analyzed 1/~-c<fWP : · ·:• t·:r ·::.'·:.. • Reported By .. Date R~i;~rtcd · --Lb Number 983548 OHS 319\ (Rc-,i,d 12,9:i) Comments Mw J Inorganic Chemistry Parameter Resul ts(mg/1) (r:1g/kg) antimony arseruc. barium beryllium cadmium chloride chromium cobalt copper fluorioe iron lead manganese _______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium ZlllC pH conductivity _______ _ TDS f1ash point ______ _ Inorganic Compounds arseruc --barium -cadmium --chromium -lead· -__ mercury selenium silver -----· Grganic-CompoW1ds benzene carbon tetrachloride chlord?.ne chlorobenzene chloroform o-r,resol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-<lichloroethane Results(mg/1) . Results(mg/1) 1, 1-dichlornethylene ______ _ 2, 4-dichloroethylene ______ _ bept.achlor hexacWorobenzene hexachloro but.adiene ~. hex3:chloroethane _ methyl ethyl ketone nitroben.z.ene _ pentachlorophenol _ pyridi.ne _ telrachloroethylene _. _ ·trichloroethylcae _· _ ·2,4,5-trichlorophcnol ------------------------_· 2,4,6-tricWorophenol ______ _ _ vinyl chloride endrin lind.ane methoxychlor toxaphen~ 2,4-D 2,4,5-TP (Silvc.x) ' I I I --·---·---·--·····-· NC Dc:p,nmcnl of Environment, Hu-Ith, &. N,wral Rc•ourccs Solid W ,<Le Marugcmcnt Division SMIPLE ANALYSIS REQUEST S1..ate ubor1tory of Public Hc:.ailh P.O. Box 28047, 306 N. Wilmington St. Raleigh, North C,rolina 27611-8047 SitcNumbcr _____________ SarriplcID,Numbcr/Namc Dl-<> S-5 G _: . · ·--... ~a;ncofSite LtJ AIUE;N Cu,v N PcB LN DFL CollectulBy· . ID# . <'::· ... ·.:. SiteLoc.ation W lt/U,E.IJ 0xiNJY DatcCollcctcd !C)•l.. 7-:< i Time__Jj_: 4-D Agency: Hazardous W.a.stc Solid Waste __ · Superfund-TCLP Compounds. / Otv. o ~lJA.rt6 Yl"\r.1&--,,.; --Sample Type Environment.a! __ t/bround Water (1) Surface Water (2) Soil (3) Other ( 4) Concentrate _ Solid (5) ✓ Liquid (6) Sludge (7) Other (8) Organic Chemistry Paranieter P&T:GC/MS Acid:B/N Ext. 2,4-D _._ ·2,4,5-TP(Silvex) chlordane heptachlor hexachlorobenzene Results (mg/I) ------hexachlorobutadien,e:.. _____ _ endrin linciane meth~xychlor toxaphene ✓ Pc~ '.J FOR LAB USE ONLY -.Date Received -10-;)_CJ-C/t!, ·7).:J . . . Pees-r M::50'~ · Dale Extracted / . , . .,. r,, . . .·. (/UJ-; -n • · Date Analyzed /J--'-'----rA v-,-· • '-~. #, :'. :. • •• Reported .By Date R~po·rt~ ---------~ Lab Number S83549 OHS 3191 0~c•,iscd l"2/9]) Comments !!]W S -Inorganic .Chemistry Inorganic Compounds arseruc barium cadmium chromium leaJi mercury selenium silver Results(mg/1) Parameter ResuJts(mg/I)(mg/k.f;:: I· Organ:(;-Compounds Results(mg/1) antimony arseruc barium beryllium cadmium chloride chromium co ball · copper fluoride iron lead manganese _______ _ mercury nickel. nitrate selenium silver su! fates thallium vanadium Zil1C pH conduC:ti vity _______ _ TDS flash point bcazene carbon tetrachloride chlordane cliJorobenzene chioroform o-c:esol m-cresol p-cresol cresol 1, 4-dichlorobenzene 1,2-dichloroethane 1,1-dichlo_roethylcne ______ _ 2, 4-dichloroethylene ______ _ heptachlor hexachloroben.zcnc bexachlorobutadiene _.:::..... hex3:cb.!oroetbane methyl ethyl ketone nit ro ben.z.ene pentachloropbenol pyridine telrachloroethyleae _ tricWoroethylcnc _· _· ·2,4,5-trichlorophenol -----------~---2,4,6-trichlorophcnol ______ _ ·1--vinyl chloride endrin li.nd.ane ---1-melhoxychJor toxaphenc 2,4-D 2, 4, 5-TP (Si !v.:x) NC DC)'.l•rtrncnt of Environment, Hc.ilth, &. N1rur1l Rcrnurccs Solid \1/,tt.c M11ugement Divi,ion SAJvfPLE ANALYSIS REQUEST SL.ale L,.bomory of Public He.aith P.O. Bo:x: 28047, 306 N. Wilmington St. Ralcii;h, North C,rolina 27611-8047 Site Ni.u:cbcr --------------'--Sample ID, Numbcr/N amc ---~O'----==u"'-0--'-'IT"--"''---·-7~-~-:.:._,.___;_;_.:..;..:__:__ f'l~cofSi~ LO AR,R,·i:;N Cv/1.JN PcB LN ~FL Collected By· lk ID#_.---:---,--.--SiteLocation W PtllilJ Cc,.,;l'liTY Date Collected / t:> -'LJ-~ ~ Time_. ·_t~ i.3 o Agency: Hazardous Waste Solid Waste __ · Superfund· TCLP Compounds ✓ 0 l~\/. 0 ~lJA~Th i'l1r.&-,1i -Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments arseruc -· barium ~ Ground Water (1) -_ Solid (5) f'0W l I cadmium -V Liquid (6) chromium -_ Surface Water (2) T "c~:J 5,.,...._,p/.,.., lead -_ mercury : Soil (3) _ Sludge (7) selenium silver -_ Other (4) _ Other (8) ---Organic Chemistry Inorganic .Chemistry -Parameter Results (mg/I) Parameter ResuJts(mg/1) (mg/kg) · Organic Compou.nd.s . Results(mg/1) P&T:GC/MS _ antimony ben;:"!ne --Acid:B/N Ext. arseruc carbon tetrnchloride ---2,4-D barium chlordane --_._ ·2,4,5-TP(Silvex) _ beryllium chJorobenzene ---· chlordane cadmium chloroform ----_ hept.achlor chloride o-cresol ---------hexachlorobenzene chromium m-cresol ----hexachlorobut.adiene cobalt __ p-cresol ---endrin .. _ c~pper cresol -··•' . --lindane fluori•de _ 1,4-dichlorobenzene -_ methox.ychlor iron -1,2-dichlorcc.:hane -_ toxaphene lead _ 1, 1 ~dichlorncthylene ✓ PC\r> '..s <:o, '1QP 7 ~M -_ manganese __ . _ 2,4-dichloroethylene ,, _ mercury __ hept.acWor -nickel hexachl o ro benzene ---nitrate hexachlorobutadiene -·--selenium ... hcxacWoroethane --· silver _ methyl ethyl ketone --FOR LAB USE ONLY sulfates rutroben.une .. --thallium . _ penlachlorophenol · /0-;;29-9'6 72.::l -. Date Re'..'.::ived vanadium _ pyridine --.·. . . . PeB:f{At~ ZlilC _ tetrachloroethylene Datc,:Extracted Jq-:kJ-:-9_ P -_, pH _.· _ trichloroethylcne . ·> PtUJs-{)lfsr:rtJ . conductivity _· _ ·2,4,5-tnchlorophcnol . Daid'/\nalyw:l / 1--t/-7f"VE!_ -TDS _ 2,4,6-trichlorophenol .. ·---:·.-. .-.. ··: -_ flash point _· vinyl chloride Reported .By cndrin I --Date R~i;~~~ -lindane --mcthoxvchlor 983550 ----·-------·-· --· 1 = toxaph;n~ · ··· Lab Number -j _ 2,4-D ·---· DW 319 -I _ 2,4,5-T)l (Silv..::,:) ·------,J I (Rc•,iscd l?.,9]) -----_____ I---------------------·--·------------•···-------···. I I I I NC Oqi.nmcnt of Environment, Hullh, &. N,OJr•I Rc.J;ourccs S0\id ',l,',<tc Muugcmcnl Divi,ion SA1\t1PLE ANALYSIS REQUEST Sute ubomory of Public He&\lh . P.O. Box: 28047, 306 N. Wilmington St. R•lci~h. North C,rolina 27611-8047 Sir..cNi.!mber ---------------'--Sample ID Number/Na.me 0-) ... <Y:S '5"3 -. ~ . . ......... . !'1a,meofSit.e (fl ARR~N Gul\JN PcB LN DFL .Col!cctwBy· ld:1..-. ID#_.----:-----Site Location W 1/U.£/J GJr.JTY Date Collected Io· J..., '1 -1 t. Time.· · -~3-/<-to :\gcucy: Hazardous Wa.st.e 7 \J,'v. o~lJA.fi1:i Solid Waste __ Superfund TCLP Compounds -----Y))N&-f1'i Sample Type Environ.mental Concentrate jL Ground Water (1) _ Solid (5) _ Surface Water (2) V Liquid (6) _ Soil (3) _ Sludge (7) Other (4) Other (8) Organic Chemistry Parameter. P&T:GC/MS Acid:B/N Ext. _ 2,4-D _·_ ·2,4,5-TP(Silvex) · chlordane _ heptachlor hexachlorobenzene Results (mg/1) ------hexachlorobutadielle endrin -. lindane _ rnethoxychlor toxaphene . ✓ Pc~ '.s ------~o.oot:JltpntJ FOR LAB USE ONLY D,to Rec,; vcd • / ,0 -,;i ffj,__ 8: TbJ . . . . R!-8 :s-~ S'tJ:;? Daie .. Extractw //-~ -=V f' . . .. i pe,Br-CM__~ol[) -Datd'A.nalyw:l J/..g.-,rvp · · .. :~::·?!'··. . -· .. Report~ .By . ..~.' Date R~p;rt6_d _________ · Lab Number S83S51 ::;;.,:; } 19\ (Rcvi,c<l 11/93) ~Qrnments "(Y\t,,J iA 'T..,r6,J .s-~ '<-Inorganic Chemistry Parameter Results(mg/1) (mg/kg) Inorganic Compounds Results(mg/1) arseruc --barium --cadmium --chromium --lead --__ mercury selenium silver ------------------------· Organic-Com~ounds benzene carbon tetrachloride -chlord.?..ne -c!-Jorobenzene -chloroform Resul ts(mg/1) antimony arsenic barium beryllium cadmium chloride chromium cobalt c~pper fluoride iron ---I = o-cresol rn-cresol ------------lead manganese mercury nickel nitrate · selenium silver sulfates thallium vanadium zinc -pH _ conduc_tivity_ TDS --_ flash point --·--·· --------j _ p-cresol --I cresol -_ 1,4-dichlorobenzene _ 1,2-dichloroethane _ 1, 1-dichlo_roethylenc _ 2,4-dichloroelhylene _ heptachlor hexachloroben.zene -bexachlorobut.adiene -... hexa_chloroethane -_ methyl ethyl ketone nitroben:z.ene -_ pentachlorophenol _ pyridine tetnichloroethylcne -. _ trichloroethylcne _· _ ·2,4,5-trichlorophcnol _ 2,4,6-trichlorophenol _ vinyl chJoride endri.n -lind.ane -me\ hoxvc:h 1 nr · j --toxaph;ne--. -'2,4-D -_ 2,4,5-TP (Silv.:x) . ----I I I i I I I 1 NC Dcp,nmcnl of Environment, Hulth, &. N,rur•l Ruourcc, Solid W,,u, Muui:ement Divi,ion SA1v1PLE ANALYSIS REQUEST St.Ate Ltboratory of Public Hc.aith P.O. Box 28047, 306 N. Wilmington St. . . Ralei~h. Nonh C,rolim 27611-3047 Site Number--------------'--SaniplcID,NumbcriNamc O 2, D 5-S c.\ .· . ··-· _ ~~cofSitc ltJ AR,RE;N Cv/1.JN Pc£ LN DFL Collected By·: \f)_ ID#. ·. . . --~-.:__ SitcLocation LtJ f!WIJ ~r..J.ii DatcCollcctcd lD-.l..b -~, ~ Time ... to)io_·_. --Agency: Hazardous W astc / \),-v _o\'.="lJAliE Solid Waste __ Superfund· TCLP Compounds Yll 1116--,"i -Sample Type Environmental Concentrate _ Ground Water (1) _ Solid (5) ✓ Surface Water (2) / Liquid (6) _ Soil (3) _ Sludge (7) _ Other (4) _ Other (8) Organic Chemistry Parameter P&T:GC/MS· Acid:B/N Ext. _ 2,4-D Results (mg/!) _._ ·2,4,5-TP(Silvex) chlordane -_ hept.E.chlor --hexachlorobenz.ene hexachlorobuta.dieQe cndrin lindan~ _ methoxychlor toxaphene -✓ _pc,~ '-l _<o,aoo/ff,K, FOR LAB USE ONLY .Date Received · 10 -;l.-9-9? 7JJ . . . . . f)e,B;.(MJ?JY') Dat.o.Extmtcd %-.;2..-~ • . . pe.e s-(, .:S-0?, . · Date'Analyzed -3-. . -·---.·-=-::~-.... . . Reported .By Date R~p~rt~ ---.~"17r"fr-'"1F"T.,---~ · 983552 Lab Number DHS] 191 (Rcvi,cd 12/93) Comments ~Lt.) -V1 DS Inorganic .Chemistry Parameter Results (mg/I) (mg/kg) antimony arseruc barium berylEum cadmium chloiide chromium cobalt c~pper fluoride iron lead manganese _______ _ mercury nickel nitrate selenium silver sulfates thallium vanadium ZJJ1C _, pH conduC:tivity _______ _ TDS flash point _______ _ ----------------Inorganic Compounds arseruc --barium --cadmium --chromium --lead· --__ mercury selenium silver --------· Organic-Compounds benzene carban tetrachloride ·chJ0rdane chlorobeuz.ene chloroform o-cresol m-cresol p-creso! cresol Results(mg/1) .. Resu'.ts(mg/1) -------·-----1, 4-dichlorobcn.z.ene ______ _ 1,2--<lichloroethanc l, 1-dichlornethylene ______ _ 2,4-dichloroethylene ---'------hepta.chlor. hexachl o ro ben.zcne hexachlorobutadiene ______ _ ~. hexa_chloroethane _ methyl ethyl ketone n.itrobe112.ene _ pentachlorophenol _ pyridine _ tetrachloroethylene _ trichloroethylcnc -----------_· _ ·2,4,5-trichlorophcnol ______ _ _ 2,4,6-trichlorophenol ______ _ _ vinyl chloride endrin lind.ane mr.thoxychJM 1-toxaphcoc .. ---2,4-D ---2,4,S-TP cs·1 1 vi.:x) ---·------------------ I NC Dcp,rtmcnt of Environment, Hullh, & N,rural Resources Solid w~,u, Muugement Division SAJvIPLE Al"IA.L YSIS REQUEST Sute uboratory of Public HC4llh P.O. Box 28047, 306 N. Wilmington St. Ralei~h. North C,ro!ina 27611-8047 Si(.cNumber ________________ SampleID,Number/Na.me l)"l.,c S ~O ...... . fia;neofSite lvAR,Ri:;N Cvt\J!'{ PCB LNDFL CollcctedB_y-_: ___ 1.-t~·'-----..,,.--~-ID#. -'-----::__ SiteLoc.1tion W ttW/J ~f\JTY Date Collected LO-)..'-~ ~ Tin:ie . . · L D ;_ ~ 6 Agency: Hazardous Waste Solid Waste __ Superfund / \J ,-11. o ~lJA.,15 Yl'\r.1~,"i -Sample Type Environmental _ Ground Water (1) V Surface Water (2) Concentrate Solid (5) ✓ Liquid (6) Comments _S,, vJ -V 1U .5 Soil (3) Other (4) Sludge (7) . __________ _ Other (8) . _ TCLP Compounds_ -Inorganic Compounds arseruc barium cadmium chromium lead· mercury selenium silver Results(mg/1) I Organic Chemistry I fa·ameter Results (mg/t) Inorganic Chemistry . P&T:GC/MS i I I Acid:B/N Ext. 2,4-D _._ ·2,4,5-TP(Silvex) chlordane bepLachlor hexachloroben.z.ene ______ _ hexachlorobuLadiene::.__ _____ _ endrui' · Ii.nciai-i'e methox.ychlor ___ toxaphene ✓PC~<.s <o, ()0071?. L---~--~--~ FOR LAB USE ONLY , Date Received · /, -9 -9 8' 7'J.J. l)-ai~ .Extr~cted ~p · : __ ·. _ ·. f't ~r_. Ci ·. D;t?Ana1;zed / -??VP ·: ~:~~?\1-~·:; \. ' . . Re~o~·;t/By _ ~--,-------, · .. _. -'~··):{. Dite R~p-~frt-~ -.,.....,._ 9 ...... _ g....,,3~5,....~...,.,3---~-lab Number · DHS J 191 (Rc'✓iscd 12/9]) Parameter Rest.ilts(mg/1) (mg/kg) antimony arseruc barium beryllium cadmium chloride chromium cobalt c~pper fluori•de iron. lead manganese _______ _ mercury nickel. nitrate selenium silver sulfates thallium vanadium nnc pH conductivity _______ _ TDS flash point --------· Organic Compound:s benzene carbon tetrachloride chlordane chlcrob~n.z.eoe chloroform o-cresol m-cresol p-creso[ creso] 1, 4-d ichl o ro beo.z.ene 1,2-<lichloroethane ·n.csul ts(m g/1) -----------1,1-dichlo_roethylenc ______ _ 2,4-dichloroethyleoe ______ _ l.icpt.achlor hcxachl o ro benzene hexachlorobuladieoe _::.._. hexachloroelhane methyl ethyl ketor.e n.itrobeo.z.ene pent.achlorophenol pyridine tetrachloroethylene tri::Woroethylcoc · 2, 4 ,5-trichlorophcnol 2, 4, 6-trichloi-ophenol vinyl chloride cndrin lind..a.ne ---------------------mcthnx.ycblo~ · I .-loxaph;n~ ____ ---------~~J = ;:::~Tl' (Silm) ----·--·-------------------- NC DC?•r1mcnl of Environment, HulL'i, & NAOJr1I Riosourcc& S0lid Wo,cco M1n.igcmcnl Division SMfPLE ANALYSIS REQUEST Swc uboratory of Public Hc..o.ith P.O. Box 28047, 306 N. Wilmington St. R•lcigh, Nonh Cuolin1 276 I 1-8047 Site Number _______________ Sample ID, N umbcr/N a.me --·~(~2~::l_o~S:~t.~I -"'-:--,.-..--'----....:.-....:.::..:..;.::._,.._:.___.:_ Name of Site LO AR.R:i:uv Cv/1.JN PcE LN DFL CoHectcdBy·:_ ·. ID#. ---,---..:_;_;_ SiteLoc.ation W ltfU.e/J 0:,.i(liJ'{ Date Collected io-1.J .. -~ "-Time .. t I~ o:6 .. Agency: Hazardous Waste Solid Waste __ · Superfund· TCLP Compounds / \Jtv. o ~lJA,,i!S )'ll,.v-A -Sample Type Inorganic Compounds Results(mg/1) En vi r.onmen ta! Concentrate Comments arseil.lC -barium -_ Ground Water (1) _ Solid (5) Sw R.ct)s cadmium -chromium ..,/ Surfacr: Water (2) -✓ Liquid (6) lead -_ mercury . ' _ Soil (3) _ Sludge (7) selen.ium silver -Other (4) _ Otber_(8) ---Organic Chemistry Inorganic Chemistry -t'arameter Results (mg/I) Parameter ResuJts(mg/1) (mg/kg) · Organic Compounds Resu! ts (:-,1g/l) .F&T:GC/MS _ antimony benzene -----· --Acid:B/N Ext. arseruc carbon tetrachlorici~ ---2,4-D barium chJord..?..ne --_·_ ·2,4,5-TP(Silvex) _ beryllium chJorobeuzene -chlordme cadmium ·chloroform -------___ hept:, .. ~Wor chloride o-cresol --hexachlorobeD..Z.Cne chrom.iurn m-cresol ' ------hexachJorobutadieqe cobalt _ p-cresol ---cndrin . , _ c~pper cresol --lindai1e fluoride 1,4-dichlorobeo.z.ene --, __ rneth-J~.ychlor iron _ 1,2-<lichJoroethane -toxanl::ene lead _ 1, 1-dichlornethylene ✓Pc·~,.$ -_<0-.(700~ _ manganese _ 2,4-dichloroetbylene -_ mercury _ hcptachJor nickel hexachlorobenzene ----nitrate hexacWorobutadiene --selenium ... hexachloroethane ---· I silver _ methyl ethyl ketone -FOR LAB USE ONLY : sulfates nitrobe112.Cne --Date Received · JO c:i-9-q &-;fJ.:J_ . thallium . _ pentachlorophenol ---vanadiurn _ pyridine . . . . . ~(;qJ?'"A . -zinc _ tetrachJorodhyleue Date .. Extracted //-,2--~ -_. pH _, _ trichloroethylcne .. . ft?;e scAIIJV 'i!J _ conduC:tivity _· _· ·2,4,5-trichJorophenol . Date'Analyze<l L/_;S-93'YP TDS -_ 2,4,6-trichlorophenol . ·-:-:··_··._ ... '.-· -_ fla.sh point _-vinyl chloride Ref)Orted .By -_ endrin lindane Date R~p6rt~ --_ melhoxyr:hln(' -·--.. S83SS4 -·_ toxapheoc Lab Number 2,4-D ------------;:;;5 ) I 9 I (?c-,i~d P/9J\ 1-__ 2,4,'.i-TP (Silvu) ·--------~-----, -----· -----~---------------·-I I I ! I NC Dcp1nmcnl of Environment, Hc...t.lL~, &. Nuur•I Resources Solid \l:'a,Lc M1ru~cmcnl Divi,ion SA.iYIPLE ANALYSIS REQUEST St.ate l..,bor.tory of Public Hu.Ith p. O. Box '.'.804 7, 306 N. Wilmington St. Ralcii,;h, North C,roli.n1 27611-8047 Site Number--------------''-----Sa.a.iplcID, Numbcr/N a.me ---~-0--'-1-.:>'--_.s_,_1-_~-'--:__~~~-_:_~ NarneofSit.e Lil ARR'f N Gul\J!'{ PCf3 LN DFL Collected By-1-( '2.__ ID# . ----..:__ SiteLoc.ation W 1W/J ~r,i'T'i Date Collected IC>-'2.. 6-__Ci '6 Time . J lf :\j.0 · ,· Agency: Hall!dous Wa.9tc Solid Wasu erfund TCLP Compounds ✓ l) ,-.,, . 0 ~lJA.1il5 }')']N&--,1\ -Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate ---------nts arseruc -barium _ Ground Water (1) -. Solid (5) .sw -~c.us cadmium -chromium __1('Surface Water(?.) ✓ Liquid (6) -lead· _ mercury ' Soil (3) _ Sludge (7) _ selenium silver __ Other (4) Other (8) ---Organic Chemistry Inorganic Chemistry --Parame:,,r Results (mg/I) Parameter Results(mg/1) (mg/kg) · Organic Compounds . Result.s(mg/1) P&T::";C/\1S _ antimony .benzene --Acid:3/N Ext. arseruc c.:ubon tetrachlmic!e ---, 2,4-D barium chJord.2.ne ! • ·2,4,5-TP(Silvex) --_ beryllium chJoroben.zene -chlordane cadmium chJoroform ---_ bepL,chlor chloride o-cresol --hexachlorobenzene chromium m-cresol . -------hexachloro butadieo,e cobalt p-cresol --endrio . ,, _ c~pper cresol Iincian'e --fluoride 1,4-dichloi·obenzene --_ rncthcixychlor iron 1,2-dichloroelhane --_ toxaphene lead _ 1, 1-dichlo_roethyleoe -L re~ '.J -_<tJ•O<>o/~ , _ manganese _ 2,4-dichloroethylene ,, _ mercury _ bept.achlor ---nickel hexachl o ro benzene ---nitrate bexachlorobut.adieoe --selenium ... hexa_chloroetbane -· -_·. silver _ methyl ethyl ketone -FOR LAB USE ONLY : sulfates nitrobe!llene -· -thallium . _ pent.achlorophenol · ~Date Received~,.. ;l'.z~y: -/J._1 -·" vanadium _ pyridine . . . . Pi c1_~ zinc _ tetrachloroethylene . Date.Extracted 11-~~rrvP -_, pH _. _ trichloroethylenc· .. ' : ~5-014S"OY2 _ conductivity _· _· ·2,4,5-trichlorophenol · _Date'Analyzed 1/-:'Z,t:-"7h/p TDS _ 2,4,6-trichlorophcnol .-.. ~-_,\-.=.:·.-. . . -.•·· _ flash point _· vinyl chloride Reported .By endrin I --Date R~p~-~ed lind.ane ---_ mr..thoxyc::Wor -----Lab Number SS3SSS -_ toxapheoc 2,4-D -----------o;s:; :!i'.ll (?cvi,d 1?.,93) --_ 2,4,5-TP (Sil~c:z) ----~-------------I I I I I ! i I I ! I NC Dcp,r.mcnt of Environment, Hu.Ith, &. N,uir•I Resource& S0lid \1/o,tc M,r ... gcmcnl Divi&ion SAlvIPLE A.J.'l"AL YSIS REQUEST St..tc ubomory of Public He.Ith . P.O. Box 28047, 306 N. Wilmington St. Raleigh, North Carolin, 276 l 1-8047 · SitcNi.lrnbcr SamplcID,Nurnbcr/Namc 62.o:51. 3· ...... . NarncofSitc UJARR~N CvNN PCT3 LNDFL Collccte<lBy· l-t,_ ~ ID# -:-~~--SiteLocation W 1&8.EIJ WNJY DatcCollccted /b-j..b~'c ~ Tiibe. ·. · Jq/'i() Agency: Hazardous Waste Solid Waste / 0/11. of"l.JA.iiE, Y>),,c,.-~ -· Superfund· Sample Type Environmental Concentrate Comments Ground Water (1) _ Solid (5) I"' r-: (...,1.,..) <-✓·-( Surface Water (2) ✓ Liquid (6) k ~,__t".J·-e-f-e~J M!) _ Soil (3) _ Sludge (7) f\_t'~.,. s·1->'t~ * ..L Other (4) _ Other (8) Organic Chemis·"ry Inorganic Chemistry TCLP Compounds. Inorganic Compounds arseruc barium cadmium chromium lead mercury selenium silver Results(mg/1) Pa:-;uneter P&T:GC/l'v~S Acid:B/N Ext. Roults (mg/1) I Parame~er Reswts(mgll)(mg/kg) 1 · Organic.CompoW1ds 2nt1mony _______ benzene . Results(mg/1) 2,4-D _·_ ·2,4,5-TP(Silvex) chlordane lieptachJor hexachloroben.zene _____ _ hexachlorobutadie:Qe:.. ___ _ endrin lindane arser""c barium beryllium cadmium chloride chromium cobalt c~pper fl uori<le rneiliorychl6r ________ iron toxaohene ______ lead ✓ Pc'ir> i.j(Lo1g O, ()()1)4/P" + manganese----------~--· --I mercury * I E!-~ V,< ddJ>JPru cu, (!,Ir a ti? . C ft-nickel ~~[~ /C& I q~;,,t;keLLI. _· -nitrate '6-CJms, . selenium FOR LAB USE ONLY .Date Rccciv~ · /<' -:;1.CJ-9¥' -nr.J .. (?~ Daic .Extracted / /-3. -,-.,.. , , pc/3 s { M ;;-cry-' DattAnaiyw:l ~ :S--9ITP · .. ····•·_, .. _-'.•. Reported .By · Date R~p·~:~~ _________ _ Lab Number SS3SS6 silver sulfates thallium vanadiuL" ZJJ1C pH conduc.tivity _______ _ TDS flash point _______ _ carbon t~tracWoride chlordane chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichlorobenzene 1,2-dichloroethane 1,1-dichloroethylene ______ _ 2,4-dichloroethylene __ . -·----bcptachlor bexachlorobenzene bexachlorobutadiene ____ _ ~-. hex~cWoroctbane methyl ethyl ketone nilroberu.ene pent.achloropbenol pyridine tetrachlo.roethylene trichJoroethylcne 2,4,5-trichJorophenol ______ _ 2,4,6-tricWorophenol ______ _ vi.iyl chloride endrin lindane metho-x:yc:h I or toxapheoe 2,4-D 2, 4 ,5-TP (Si lv¢x.) OHS ]191 (Rovi,d 12,'JJ) -----------·-----------·--------l----·-··---.. --------------- NC Dcp1nmcnl of Environment, Hullh, &. Nu11r,I Re.sources Solid \¥a,~ Muu~cmcn_l Divi,ion SMvrPLE ANALYSIS REQUE.ST Sutc ubor•tory of Public Hc.ailh P.O. Bo:,:: 28047, 306 N. Wilminf:"lon St. R•lcii:h, North C,rotin, 27611-8047 . . SitcNumbcr ____________ ----''---SarriplclD,Numbcr/Namc . OJ-c'.lSE':, t.f .--··-·•·· NameofSite L0Ai\R'£N Cu,,rH PCI3 LNbFL ColkctedBy· -I ~ · ID# .. ·. --:----:-:--..:.__ SiteLocation W ltRJ,£/J GxlrJJY Date Collected io-µ.,-•I'< Tirrie _--. , s-: iS · .-Agency: Hazardous W a.st.c Solid Waste __ · Superfuod-TCLP Compounds 7 0 1'11. o ~l.JA1111S )')lNv,,.; -Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments arsell.lc -barium _ Ground Water (1) __ Solid (5) _ 0f.L.vr:?:r.J·, --cadmium chromium __:(Liquid (6) Le.-..J-~k .~.,.~~ -lead· _ Surface Water (2) _ mercury .. 1?~'2-r--_ Soil (3) _ Sludge (7) -f-i\-fev _ selenium silver V()the~ (4) -_ Other (8) ---Organic Chemistry Inorganic Chemistry -Parameter P •~ults (mg/I) Parameter ResuJts(mg/1) (mg/kg) · Organic-Compounds . Results(mg/1) P&T:GC/MS _ antimony be!l.Zene --·--Acid:B/N Ext. arseruc carbon tetrachloride ---2,4-D ~arium chlordane . --_·_ ·2,4,5-TP(Silvex) _ beryllium chlorobeo.z.ene -chlordane cadmium chloroform --------_ hept.acWor chloride o-cresol --hexachlorobenz.ene chromium m-cresol . ----hexachlorobut.adieo,e cobalt _ p-cresol -endrin ·-cresol -.. _ c~pper -_ lindane fluoride 1,4-dichloroben.z.ene --_ methcixychlor -iron . _ 1,2-dichloroethane _ toxaphene lead _ 1, 1-dichJo_roethylene ✓ re~ '.J -. -C::::o, aaow.-11... _ manganese _ 2,4-dichloroethylene -_ mercury _ bept.achlor -nickel hexacWo ro beo.z.cne ---nitrate hexachlorobutadieoe --selenium .... hexa_cWoroethane ' ---silver _ methyl ethyl ketone -FOR LAB USE ONLY sulfates nitrobeo.zeae --thallium . _ pent.acWorophenol ---Date Received Jo -:i 9 -<J 8 nJ vanadium _ pyridine -. · .pce;c~ ZillC _ tetrachloroethyieae -_, pH _. _ tricWoroethylcae Date£~.tracted / /=i-Z'. _ conduc_tivity _· -_-·2,4,5-trichlorophcO:ol • -.: . PCE if-M so _ · Da_ttJ\naJyzed //~S~ '7YJ/P TDS _ 2,4,6-trichlorophenol : .. :""?~•\;?: . . . . . . . . -_-vinyl chloride _ flash point Reported .By --endrin . ;' : .. ·-~ :· .. lindane Date R~p.~rt~ ----·-_ methox.yd:tlor 983557 .... -toxaoheoe lab Number -DHS ]191 (Revised 12,93) --------_________ L ___ _ I I i ' NC 0cp,r1mcnt of Environment, Hc..t\Lh, & N<wr•I Rcrnurccs Solid \l:',sce M1rugcment Division SAlvfPLE ANALYSIS REQUEST Sr..otc wboratory of Public Hc.ailh P.O. Box '.:8047, 306 N. Wilmington St. Ralcii:h, North Cuolim 27611-8047 Site Number---------'-------'----Sample ID, Nurnbcr/N a.inc __ . ....::C>:::;.._1-D:--""S_b=) ____ .:..__:__: _ _:.:.:_.:..:..:..:. __ _ Name of Site LO AR,R·~N CuNN PcE LN DFL Collected By· I-+)-ID# . --~-.:.__ SitcLocation W 1(U.E.IJ [c,.jfliT'f Date Collected \ o-J...b-i ~ Time~~ ~~u .. Agency: Hazardous ·waste Solid Waste __ · Superfund-TCLP Compounds 7 ol~V. 0 ~l.JA..,15 Y>livv~ -Sample Type Inorganic Compounds R~ults(mg/1) Environmental Concentrate Comments arscruc -R.;$<--l_ barium f~¾ -_ Ground Water (1) _ Solid (5) cadmium -chromium F .~\J -_ Surface Water (2) / Liquid (6) Pu~p ~~~ lead· -_ mercury ' _ Soil (3) _ Sludge (7) \-,;:;~ ..... -t-L r>,.,?-11 L~ selcniurn -silver ✓ Othe; (4) -_ Other_(8) --· -Organic Chemistry Inl)rganic .Chemistry -Parameter Results (mg/1) Pararr:.2ter Resw ts(mg/1) (mg/kg) · Organic-Compounds . Results(mg/1) P&T:GC/MS _ antimony benzene ---Acid:B/N Ext. arseruc carbon telr.achkrice ---_ 2,4-D barium chJord.?.ne -_._ ·2,4,5-TP(Silvex) _ beryllium chJorobenzene -chlordane cadmium chJoro fo!!Il ----__ heptachlor c}·Joi:ide o-cresol --hexachloroberu.ene chromium m-cresol --·---hcxachlorobutadieqe cobalt p-cresol --endrin-. ' _ c~pper cresol li.ndan·e . -fluoride 1,4-dichlorobenzene = rnetho'x.ychlor --iron 1,2--dichlorodhanc --_ toxaphene le:id _ 1,1-dichlo_roethylene _:L Pc~ '..s -< cJ • lf!J ~ o I a::;w1, __ manganese _ 2,4-dichloroethylene , _ hcpt.achJor -_ mercury nickel hexachlorobcc.zcne ---nitrate hex.achJoro butadiec.e ------selenium .,_ hexachloroethane --· silver _ recthyl ethyl ketone -----··· FOR LAB USE ONLY : sulfates n.ilrobe0.2.ene --thallium __ pcntachlorophcnol Date Received • /0 -,)..CJ -9 S, ;l),:J -vanadium ._ _ pyridine . tlce1f.~ . -ZillC _ tetrachloroethylene Dace .Extracted i °-2J ~ -_, pH _. _ tricWoroethylcoe f'~/41~,. ~ _ conduC:tivity _· _ ·2,4,5-trichlorophcnol Dat~).nalyz.e<l /f-:S--_Vf' · .. TDS ·_ 2,4,6-trichloroph<":nol ·. ·-:·•,'?/t!:·~. -.. , . .-. --_ flash point _-vinyl chloride .. Reported .By cndrin ' ---.. ::-:.; .. -linchne Date R~p-~rt6<l ---mi:thoxvchlor ~-983-558 ----·----·· ----✓ • -_ toxaphcoc:: Lab Number 2,4-D ----DHS 3191 (Roi5td J?.,'9]) ------------· _ 2/,,5-TP (Si!·-,o:) ·------I i I i ! ~------·--------------------------------. NC Dcpuimcnt of Environment, Hu.Ith,&. N.nir•·I Rcsourcu Solid. W,<t.c. Muugcmcnt Division SAlvIPLE A.1'-l"A.LYSIS REQUEST State Gboratory of Public Hcai(h P.O. Box 28047, 306 N. Wilm..ing.on St. R•lci~h. North C,rotina 276 l 1-8047 SitcNurnbcr _____________ ___c __ SamplclD,Nurnbcr/Namc OJ-<> S-6 b .... Name of Site UJ ARR~N Gur\JN PcE LN DFL Collected By· \-4 '1-. ID# --~--SiteLoc.ation W ttlli/J fo.j,,.rry DateCollected tD-l-b~'l"l: Time .. l·D:·~·. Agcocy: Hazardous W B..'.lle / \J,~v. o~lJAliE Solid Waste __ Superfund· TCLP Compounds ~Nvr'\ -Sample Type Environment.al Concentrate _ Grouod Water (1) ✓ Solid (5) _ Surface Water (2) -. Liquid (6) _ Soil (3) _ Sludge (7) _£. Othe; (4) _ Other (8) Organic Chemistry Parameter Results (mg/I) P&T:GC/MS -Acid:B/N Ext. l -2 4-D 1-I I _...:_ ·2,4,5-TP(Silvex) chlordane I-i bept.acWor I = hexachloroben.zeoe _ bexachlorobut.adie~e endrin !--/ifndane _ methoxychlor toxaphene ✓_pc~ i..s . ~"·'C)ff"l FOR LAB USE ONLY ·.Date Received · / 6)-;J_CJ--9 &' 7l j · .. ··. . . /J<0f(-ftl7& ;"< Date.Extracted //-9-'P ·· · . . •· P:-B~(Mrortt} · '· Date~Analyzed //f..;.lo-9"iTYP •... ,·--!•:.·.:..:!• .·•:·.·: Rcpo_rtcd .By DatcJZ~p:~~~ _________ _ Lb Number 983559 DlcS ]191 ('ioi~d 1"2i9J) 1 t Comments ~E, p I ,-.C::/\.l<f" u,os !!lorganic Chemistry Par;; r71eter . J.:t.Swt.s(mg/l)(mg/kg) _ antimony arseruc -barium -_ beryllium cadmium -chloride -chromium -cobalt -_ c~pper fluoride -,ron -lead -_ manganese _ mercury nickel -nitrate -selenium -silver -sulfates -thallium -. vanadium -ZJJ1C --pH _ conduc_tivity TDS -_ flash point Inorganic Compounds arseruc -barium -cadmium -chromium -lead· -__ mercury selenium silver ------Organic.Compounds benzene ·-carbon tetrachloride -chlord2.Ilc -cWorobenzeoe -chloroform -o-cresol -m-cresoi -_ p-cresol cresol -_ l,4-dich1orobe111..eoe _ 1,2-<lichloroethanc _ l, 1-dichJornethyleoe _ 2,4-dichloroethyleoe _ hept.achlor bcxachloroben.zcoe -hexachlorobuladieoe -.... hcxa_cWorocthaoe -_ methyl ethyl ketone nitrobe112.eoe pcnt.achlorophcnol ;'lyridine tetrachloroetby lcne tricWorocthykac Results(mg/1) Results(mg/1) ---··-·-·-· _ ·2,4,5-trichJorophenol ______ _ 2,4,6-trichlorophenol ______ _ vinyl chJ~ridc I ~;:;:e methoxvr.hlor ------1-·,· .. --------·----· ________ ... _1-=---~~:J;:'(SdmJ ____ _ I I I i NC Oqi,nmcnl of Environment, Hc.,llh, &. N,CJral Riosourccs Solid Wa<!.c M1r..1gcmcnt Division SAlYIPLE A.l'l"ALYSIS REQUEST Sl.llc L...bor,tory of Ptiblic Health P.O. Box 28047, 306 N. Wilming.on St. Ralci~h. North C1rolina 27611-8047 SitcNumbcr ___________ --''---SamplclD,Numbcr/Namc Dws -61 : •;:±::::.:< Name of Site (J) AR,R~N Cut.JN PcI3 LN DFL Collected By·: L. ID# :;;_;/;~?)(' .· ::--:.-:' ·•::'. -· .. _.-· Site Location W ltlli/J Gxir-.JJY DateCollected lo-)..._ ... --4 (l Tim~> --(;·,~:-.3~ Agency: __ Hazardous ·Waste __ Solid Waste __ Superfund TCLP Compounds ✓ \J ,-v. o l='l.JA,1il:, >1lr.1t--,,.; -Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments _ arseruc . barium _ Ground Water (1) V Solid (5) 660 -u·,u ·.::, _ cadmium chromium _ Surface Water (2) _ Liquid (6) _____________ __ lead· _ me~ury · _ Soil (3) _ Sludge (7) ____________ selenium silver _/'.)the; (4) _ Other (8) ___________ = I -l Organic Chemistry Inorganic Chemistry _ I Parameter Results (mg/I) Parameter Ri__;t.iHs(mgii)(mg/kg) · Organic-Compound:; . Re:sults(mg/1) I _ P&T:GC/MS ______ _ antimony _______ __ benzene I Acid:B/N Ext. _____ arseruc ________ carbon tetr-.;cWoride I -2,4-D ---barium _______ = chJord.?.ne _._ ·2,4,5-TP(Silvex) ______ _ beryllium _______ __ chJorobenzene _ chlordane _______ __ cadmium _______ _ chloroform _____ _ _ hept.acWor ______ _ chloride _______ _ o-cresol _ hexachlorobeo.z.ene ______ _ chromium _______ __ m-cresol • _ hexachlorobut.adieJ'.\e _ cobalt _______ _ p-cresol _ cndrin .. ______ _ C?pper ----'-----_ cresol _ li.ndane --~---_ fluoride _______ _ 1,4-dichloi-obeo.z.ene ______ _ _ methoxychJor ______ _ iron _______ __ 1,2-<lichloroethane _ toxaphene ______ lead _______ 1, 1 ~dichloroethylene ______ _ _:L Pc~ i .s _ < Q, IO~ = manganese -------= 2,4-dichlo.roetl:iylene -------_______ _______ __ mercury _______ __ bept.achJor nickel hexachlorobeo.zene ---------------------------' _ _______ _______ __ nitrate _______ _ hexachlorobutadiene _______ 1 _ _ selenium _______ _::_ _ hexacWoroethane _______ I ---------,--------------1 _ silver _______ __ methyl ethyl ketone FOR LAB USE ONLY _ sulfates _______ __ nitroben.z.ene _ thallium . _______ __ pent.achloropbenol · _Date Received · /t) -;;l Cf -q'ij-7l~ _· vanadium _______ __ pyridine . pe2½-ifi1701°-) _ Zl!lC -------_ letrachloroethylene Date fa.lracted / /--9,-1£'Yp _' pH _______ _. _ tricWoroethyieoe p<:.B"is(M3'DY".J°. . . conductivity_______ · ·2,4,5-trichJorophcnol .-~D_aie),nalyzed //-/0-93VP .. '. = TDS.. ------= 2,4,6-trichlorophenol ______ _ • ·' ···,'":',:,°'-·. ·· · · flash point _______ -· vinyl chloride Reported.~y ~---,--------= · _______ = enc:rin ··-1 _ ·,,. ____ _______ lindane Date R~p-grt~ ,----------~ --____ _______ --rnethnxvcbJor ______ , Lab Number. 983560 --====== =========== I _ ~~:t"' . _··· ~------1 OHS )191 (Hcvi1d 12i9J) ------____ I -2,4,5-J }-l (Sdvu:) -----------·-! NC Dqanrncnl of Environment, Hc..t.lth, &. N,tural R<.<ourcc& Solid W,i'.c M1rugcrncn1 Division SAIYIPLE ANALYSIS REQUEST Sute Liboratory of Public He.alth P.O. Box 28047, 306 N. Wilmington St. Raleii;h, North C,roli.na 27611-8047 SitcNurnbcr ______________ '--_ SarnplcID,Numbcr/Na.mc 62..:>S•i:::<g. , -··-·•: ... ~apicofSite LO AR.Rf N Cul'IJ!'{ P03 LN DFL .Collected By· /D-;U,.-4 8 _.., ·,;,ID# .. ::; /:·:_:: ·. DateCoUectcd l±i j · 'i'~~e. ·,,;·';•~c:. Site Location W I\P.J,,eJJ ~f'liT'i Agency: Hazardous Waste Solid Waste __ Superfund-TCLJ) Compounds. 7 0 ,-., . o ~lJA,1i5 it\Nv~ -Sample Type Environment.al Concentrate Ground Water (1) ✓ Solid (5) Surface Water (2) _ Liquid (6) Soil (3) _ Sludge (7) V Othe; (4) _ Other (8) Organic Chemistry Comments S&P -:8-l.., ~ s Inorganic Chemist:..--y Inorganic Compounds arseruc I --barium cadmium chromium lead· mercury selen.ium silver Results(mg/1) Parameter P&T:GC/MS Acid:B/N Ext. Results (mg/!) I Parameter RestiJts(mg/))(mg/kg) i · Organic-Compounds Resul ts(mg/!) 2,4-D _·_ ·2,4,5-TP(Silvex) chlordane hept.achlor hexachloroben.zeoe _____ _ hexachlorobut.adieqe=-------endrin li.ndane rnetho.xychlor __ toxaphene ✓Pc~,_., -~ FOR LAB USE ONLY . Date Received · /t) -.;,.q-9y tJJ . •. . . PCB;-(/!/ Y'O',{P Date .Extracted ·· //-'7 . -:-.· .· · .. :: <p<!E"!s-r_MyCJTO_) · Dat(/Analyzed //-/Oi':JYW · •. "'::.,:_s!:_·~·-,>'·: . . .. Repcrtcd .By DateR~p;rt~. _ ~83561 Lab Number DIis } I 'i I (Revised 12/93) antimony _______ I . benzene arseruc barium beryllium cadm.iurn chloride chromium cobalt copper fluoride iron lead manganese _______ _ mercury nickel_ n.itrale selenium silver sulfates thallium vanadium ZlIJC , pH conduc_tivity _______ _ TDS flash point --------carbon tetrachlorice chlordane . chlorobenzene chloroform o-cresol m-cresol p-cresol cresol 1,4-dichloroben.zene ______ _ 1,2-dichloroethane 1,1-dichlo_roethylene ______ _ 2,4-dichloroethylene --'------heptachlor hexachl o ro benzene hexachlorobutadiene ..... hexachloroethane -· .. methyl ethyl ketone nitrobeo.iene pentachlorophenol pyridine tetrachlo roe thy I eoc trichloroethylene -------_· _ ·2,4,5-trichloropheool _______ _ _ 2,4,6-trichlorophenol ______ _ vinyl chloride endri.n lincl.ane methoxycbJor toxapheoc 2,4-D 2,4,5-TP (Silv.::x) ------··---------~--------------------~--~ - l NC Ocp,nmen( of Environment, Hc.,!Lh, &-N,wral Resources Solid Uf,<'..c M111.1gement Division SAivf:PLE ANALYSIS REQUEST Swe Ltboratery of Public Hc:..a!Lh P.O. Box :?.8047, 306 N. Wilmington St. Raleii;h, Nonh C,rolina 27611-8047 Site Number--------------'---SamplcID,Numbcr/Name O 1....D ~-6:\ _ Name of Site (j} AR,R·ff\{ Cvl'IJN PO~ LN DFL Collected By-:· · l:f:'2-. ID# __ ~--SiteLoc.ation W 1/UEIJ Co..;/\JJY DatcCol!ccted k>-)..,.,c,-~ CZ Time_. · I q;· do Agency: Hazardous W astc Solid W a.ste __ Superfund-TCLP Compounds. / \J ; '11 . o ~ lJ A ,ii75 Y>1 N t;--f'i -Sample Type Environmental Concentrate Ground Water (1) . ~ Solid (5) Surface Water (2) Soil (3) ./ Othe~ (4) l Liquid (6) Sludge (7) _ Other_(8) Organic Chemistry Parameter .P&T:GC/MS Acid:B/N Ext. 2,4-D • ·2,4,5-TP(Silvex) chiordane hcpl.acb.Jor Results (mg/I) hexachlorobenzene _____ _ hexachlorobut.adieQe ::__ ____ _ endri.n lindane methoxychlor _ toxaphene _.L re~ ;J -~ FOR LAB USE ONLY Date Received_· JC) -o19_.; 7)Q . PZe!s--(;yf~ DateExtracted F/-/~€ ---. pc.s's { "'1 ~8"1. -· Date'Analyzed //-/0-93'Vr' • : •. ~-j·,.--,• .. Reported By .. Date R~p-~rtcd __________ _ Lab Number ·c,,1r,,-r0 Juuuio""' r,;,~ 3191 (Roi,d l?./9]) Comments 5e-o -f'..< LJ .. L'S -Inorganic Cb:~mistry Parameter ResuJ ts (mg/I) (mg/kg) antimony arsen.:c barium beryilium cadmium chloride chromium cobalt C?pper fluoride iron lead manganese _______ _ mercury nickel_ nitrate selenium silver sulfates thallium vanadium Zll1C , pH condu<::tivity _______ _ TDS flash point --------Inorganic Compounds arseruc barium cadmium chromium lead· mercury selenium silver j _ Organic-Compounds benzene carbc;:: tetrachloride chlorJane chJoroben.zene chloroform o-crt:sol m-cr:::sol p-cresol cresol 1,4-dichloroben.z.ene 1,:?.-dichloroethane Resul ts(mg/1) . Results(mg/1) -------1,1-dichlo_roethylene ______ _ 2,4-dichloroethylene bep~chlor bexachloroben.zene hexachlorobutadiene .... hexachloroethane methyl ethyl ketone nitroben:z..ene pent.achlorophenol pyridine tetrachloroethylene trichJoroethylcne --------------·2,4,5-trichlorophcnol ______ _ ·1-= 2,4 ,6-trichJorophenol vinyl chloride endrin lind.ane mr.thoxychlor loxaphenc 2,4-D 2,4,5-TP (Silvu.) -------·-· --· .. ___ _ NCDEHNR Organics Lab: / Division of Waste Management D Superfund Section Inorganics Lab: __ _ 0 Hazardous Waste Section D Solid Waste Section CHAIN OF CUSTODY RECORD Project Name: wA~R.BN fovN-ry Pcs UWtJfcU... Sampled By: \.+PrR&t L-11v,v Site ID# (NCD#) ______ _ Sampler ID __________ _ Location: w.A/l~gN C:,✓,vr'/ Telephone:~ T~ ~ :i.-g-o 1 Address: ___________ _ Date Sampled: 10-.l.G;,-'"t'i to-1-1-q;;:: Time Sampled: _________ _ Sample Types: Soil v .Water / Waste ---Other Remarks: lJ A-1"5,:t.. 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