NCD980602163_19940728_Warren County PCB Landfill_SERB C_Soil Analysis I-OCR

;-,:,C. Dcpar.mcnt of Environment.
I ir.\llh, & l--'a1ural Rc.s.ourccs
Soiic Wr,stc Manai;cmcnt Di,~sion
SAMPLE A.NA.Lr::,1::, K.t:.,'2 Ut....'.:l l ::,t•tc Lat>on.tory ol rulll,c 11ca1tn
P.O. Oox 28047, 306 1'. Wilming-ton S1rcc1
Raleigh, North Carolina 2761 l
Sile Number -----------------' Field Sam pie Num bcr _ ___.:W __ J.._-__:Oc...._.:::t!J_I_-_L__:_,G; _____ _
Name o( Site WA-R.i2.t,.J Coo,-.JT'I Pe,r;, l.DFL Site Location A F"T"o 1'J NC --'-"-....:.....:~=------'--='-------------
Collected By a. t-J ll.H.O \.., ~~ ID# 3-=i-Time /120
/,. , "20SE.
Agency: Hazardous Waste X Solid Waste ___ Super fund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) HL.T€2. 6> Ysre""'-. Cadmium --Chromium --
__ Surface water (2) Liquid (6) /A..JLS 7 -,LEACHA7e:---Lead
--Mercury
Soil (3) _ Sludge (7) ~PL ✓ Z: k,)/ ,£C..O Selenium --' --Silver --_ Other (4) A Other (8) -:re.-001-L <!.H --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (ags:P" Organic Compounds Results (mg/!)
P&T:GC/MS -.::t:_ Arsen.ic ~0 .. G) benzene ----Acid:B/N Ext. L Barium c.a3 carbon tetrachloride ----'MTBE y: Cadmium .L.. O. 0Cd--chlordane ----Chloride chlorobenzene ------_2L. Chromium '-0_.::, I chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----" Lead i_ D • D O '=:J cresol ------__ Manganese 1,4-dichlorobenzene ----
--~ Mercury L...0.0005 --1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylcne --_£_ Selenium L...o. c.o5 2,4-dinitrololucnc --_LSilver L_s;i ,.05 __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hcxachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobcnz.enc ------TOC __ pcntachlorophcnol --
--__ pyridine
Microbiology ----t elr achloroeth ylcne
----trichloroethyleoc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2, 4,6-trichJorophenol ------vinyl chloride --endrin --lindane --Dale Received Reported by __ mcthoxychlor
--toxaphcne
Date Extracted Dale Reoorted 2,4-D
. 013909 JUL 29 94 --__ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --DI IS 31'JI (llcviscd 2/91)
I I
I I
0 .C. Ucpar,rncnl o: t:.nVlronmcnl,
· I Jcc,llh, & /'.'alural Resources
Solid. Waslc Managcmcnl Di,;sion
V~T.lJ. .L.,J.:..., r,,....,. ,.,,._,_,.,._ ,_,.,~ .._.........,'< ._,..._._, > ------,1 -
. '
Site Number -----------------
· P.O. 13ox ~7. 306 N. Wilmin&1on S1rccl
RAieigh, North Carolina 2761 I
Field Sample Number (,UL-~o Z. -J. E
Name of Site WA-Ri2.e.J GorvN PC-"B l.DFL Site Location A F"To ,-J NC -~_;__...:....:::...!.::::,___..:__:-==-------------
Collected By 6. f\) 1cH.o\_.6c,),..J ID# 3-=l-Dale Collected 2.'8 -:fVL Y 94 Time /+3D
L l20S.E
Agency: Hazardous Waste X Solid Waste ____ Superfu.od TCLP Compounds ---
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) Ft L. it"/:!.... ..svsrefl"J Cadmium --Chromium --__ Surface water (2) _ Liquid (6) t)V71.£t -LE:ACM ~ Lead --__ Mercury
Soil (3) Sludge (7) Selenium ----Silver --_ Other (4) _)(__ Other (8) --'
--
--
Organic Chemistry Inorganic Chemistry --
:
Parameter Results(mg/1) Parameter Resu!Ls(mg/1)(--" '-Organic Compounds Results (mg/I)
P&T:GC/MS __)(. Arsenic L..o.c.1 benzene ----
--Acid:B/N Ext. ~Barium o.o7 --carbon tetrachloride
'MTBE 1-_ Cadmium L..o. ao.a chlordane ----
Chloride chlorobenz.enc ------
--~ Chromium ..i...O.ol chloroform --
--__ Copper o-crcsol --Fluoride m-cresol ------
--Iron __ p-crcsol --
--~ Lead -'...O. oo;S crcsol --
--__ Manganese 1, 4-dichlorobenz.ene --
--)<_ Mercury L...0-0005 --1,2-dichlorocthanc
--Nitrate __ 1,1-dichloroethylcne
_£_ Selenium ..t...o.oo_j --2,4-dinitrotolucne
LSilver ....(__c.05 __ heptachlor
Radiochemistry Sulfates hcxach lorobenz.ene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) _pH hcxachlorocthanc --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnz.cne ------TOC __ pentachlorophcnol --
--__ pyridine
Microbiology --__ tctrachlorocthylcne
--__ trichlorocthylcoc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2, 4,6-trichlorophcnol
----__ vinyl chloride
endrin --lindanc --Date Received Reported by mcthoxychlor --__ toxaphcne
Dole Extracted Date Relfitj · 2,4-D --910 JUL 29 94 __ '2,4 ,5-TP (Silvcx)
Dale Analyzed Lab Number --DI IS Jl'Jl (llcviscd 2/91)
. --. . . .-. I kalth, &. /'satvnl Rc.s.o~rces
SolilWaste Management Division
.," Sile Number -----------------
P.O. !k>x zwn, 306 ~-Wlimin[;'on S1n:c1
R.alcii;h, North Carolin• 2761 l
Field Sam pie N um bcr ___ W_L_-____;~;__0___;:2~--.!:::@=--=L:_:__ __ _
Name of Site WA-1<.i2.e.J CorJT"/ PCt> l.DFL Site Location A F"To ,.J N (_ _.t......:.....:.__~~:::___...:.__:...--=::.._ __________ _
Collected By ~. fv I U --t.o l-60)-...) ID# 3-=t--Date Collected 2'8 -:TVL 'I <=f4 Time / t--10
6r s. -S.r€"Pt-l e>--.::>
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) 0, F. IAJ,+TeR., Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --
Soil (3) Sludge ('TJ Selenium ----Silver --~ Other (4) _ Other (8) --: --
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/1) Parameter Results (mg/I) (as 01,) Organic Compounds Rcsults(mg/1)
P&T:GC/MS .1__ Arsenic benz.enc --..L-.a-c1 --Acid:B/N Ext. 1-_ Barium L 0-C\ carbon tetrachloride ----"MTBE 'le Cadmium <-<!:).cog. chlordane ------
Chloride chlorobenz.ene ------
--~ Chromium J....O.al chloroform ----
--__ Copper o-crcsol --Fluoride m-crcsol ------
--Iron p-cresol ----,<_ Lead .L...O.oo=> cresol ----
--__ Manganese 1,4-dichlorobenzcoe --
---L Mercury L.. 0-GOO!:> 1,2-dich loroet hane --
--Nitrate __ 1,1-dichloroethylcne
7 Selenium "'-o. ooS 2, 4-di nit rot oluenc ---A-Silver -ZlL O ~ __ heptachlor
Radiochemistry Sulfates hex.a ch lorobcnzcne ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcx.achloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitroben7.ene ------TOC pcntachlorophenol ----
--__ pyridine
Microbiology --__ tctrachlorocthylcnc
--__ trichloroethylc nc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ \~nyl chloride
endrin --lind;ine --Date Received Reported by --methoxychlor
--toxaphenc
D.itc ExtractccJ Dale Rcpfild · 2,.:-D
3911 JUL 29 94 --__ 2,'<.S -TP (S ilvcx)
D.ilc Analyzed Lab Number --!)I IS 3l'Jl (Revised 2/'Jl)
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I
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:
'
:
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I
:
N.E:.,Dcpar:mcnt of Environment,
I lea Ith, l,.;. 1'-atural Resources
Solid Waste Manakcmcnt Division
SAMPLE ANALYSIS REQUEST State l.Abontory of Public Health
· P.O. I3ox 28047, 306 N. Wilming,on Street
RAieigh, North Carolina 27611
Site Number Field Sample Number t.L/~ -t!>C 3-8 L ----------------
Site Location A F"To ,-J N C..
Collected By a . f\) 1 l. Ho L. 6c>"'-' ID# 3-=t-Date Collected 2g -:f Vt.. Y <1-f Time~/"--'-:/-'tf_G'_' __
~ . !:>T'FPtt?-,.J~
Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---__ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Results(mg/1) (~) Organic Compounds Results(mg/1)
P&T:GC/MS -1_ Arsenic L.... Cl-o I benzene ----_ Acid:B/N Ext. _K_Barium L_ o .a I --carbon tetrachloride
"MTBE L Cadmium £0.003-chlordane ----Chloride chlorobenzene --------_£ Chromium -'-.O_c:,j chloroform --
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --X: Lead ..L....o .oo5 cresol ------
--__ Manganese --1,4-dichlorobenzene
--_:f:_ Mercury L...o.oo o.!> 1,2-dichloroethane ---Nitrate 1,1-dichloroethylene --T Selenium --
-'-=-005 2,4-dinitrotoluene --~Silver L...o. o5 __ heptachlor
Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hex.achloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
Microbiology ----tetrachloroethylcne
--__ tr ichloroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by __ methoxychlor
__ toxaphcne
Dale Extracted Dale Reported 2,4-D
013912 JUL 29 94 --2,4,5-TP (Silvex)
Dale A nalyzed Lab Number --DIIS Jl'JI (Revised 2/91 )
. .
:,._C Dcpar.mcnt or Environment.
llc~llh, l,:. Natur.l Re5.0urccs
Solid W•astc Man;igcmcnt Division
SA.MPLc ANALY~l::, K...t.,VU.t....) 1 ::>talc Lat>ontory 01 ruo1,c 11ca11n
. P.O. nox 280-:i, 306 N. Wilmin(;lon Street
Raleigh, North Carolina 2761 !
Sile Number -----------------Field Sample Numbcr __ W=-=_L_-_,(?C....,,C~'--------"4_--==!3=---L _____ _
Name of Site WA-1<.i2.€:.J CoorJn' Per:, l.DFL Site Location A F'To IV N (._ _..c....:._...:....:::....:...::::c.__...;___;---=:;__-----------
Collected By G. N 1U--tOl,6c>-...., Date Collected ~ JIJCj q4-
~-ST€Pt-l ~~
Agency: Hazardous Waste X Solid Waste ____ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· -__ Groundwater (1) _ Solid (5) [).;:: Wttrcte. Cadmium --Chromium
A 1R-Hos~ --_ Surface water (2) Liquid (6) Le.ad --Mercury --Soil (3) _ Sludge (7) Selenium ----Silver --.)s_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Result.s(mg/l~<M:P sl Organic Compounds Results(mg/1)
P&T:GC/MS _L Arsenic .L...o_o 1 benzene ----
--Acid:B/N Ext. __L Barium o.oGz. carbon tetrachloride --.MTBE l Cadmium .L..o.oo.::l. chlordane ----Chloride chlorobenzene ------_L Chromium ,,(_D-o\ chloroform ----
--__ Copper o-crcsol --Fluoride m-crcsol ------
--Iron __ p-cresol --
--JL Le.ad O.Ol..\l cresol --
--__ Manganese --1,4-dichlorobenzenc
--L Mercury -<. O· 0 oo..!5 1,2-dichloroethanc --
--Nitrate 1,1-dichloroethylcnc ----± Selenium L..D. 005 2,4-dinitrololuene --Silver ..l..Q. 0 5 heptachlor --Radiochemistry Sulfates hex.a ch lorobcnzene ----Zinc hcxachlorobutadiene ----Paramdt:r Result.s (PCi/1) pH hcx.achloroelhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzcnc ------TOC __ pcntachlorophcnol --
----pyridine
Microbiology ----l c lra chlorocth ylenc
----trichlorocthylenc
Pcirameter Results (Col/l00ml) __ 2,4,5-lrichlorophcnol ------__ 2,4,6-trichJorophcnol
------vinyl chloride
cndrin --lindanc --Date Received Reported by mcthoxychlor --
--toxaphcne
Date Extracted
Dale RcpO'fJ91J JUL f9 94 2,4-D --__ 2,4,5-TP (Si lvcx)
Date Analyzed Lab Number --1)1 IS JJ'Jl (ltcviscd 2/91)
I
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N-.C., Depar:ment o( Environment,
l.lc'alth, &: 1':atur.l Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
· P.O. Dox ~7. 306 K Wilmington Street
Raleigh, North Carolina 27611
Sile Number ----------------Field Sam pk Num ber_~W_;__L....:..._-_(!;)---=0:-...;;..l_-----=-t;,..:..__w _____ _
Name of Site WA-1<.i2.e.J GoNTY PC-1$ l.DF'-Site Location A F"To,v NC, -~..:.._..:...:::..:..c:,:_..:.._c...c....-=------------
Collected By a. {\) ,u-1.0 L. 60..._, ID# 3-=f-Date Collected Z 'cl 3 VL -f G\ 'J-Time / 135'°
T ?VA LJ< e--,e_
Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ----
Sample Type Inor-6anic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
ti ---· -2{__ Ground water (1) _ Solid (5) We i-t. l Cadmium --Chromium --Surface water (2) Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemist!)' Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results(mg/1)~) Organic Compounds Results(mg/1)
P&T:GC/MS 25.._ Arsenic ..!...0.01 benzene ----Acid:B/N Ext. L Barium o.oS carbon tetrachloride ----"MTBE ...L Cadmium .L...c, -c,c:,d-.. chlordane ----Chloride chlorobenzene --------_!::_ Chromium ~0-0 l chloroform --
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-crcsol ----
--_x_ Lead .L.....o. oos cresol --
--__ Manganese 1,4-dichlorobenzene --
--..i,_ Mercury L_o-ooQ.5 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylene --L Selenium L..0-00;$ 2,4-dinitrololuene --£Silver L..Q.O => __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hcxachlorocthane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela TDS nilrobenzenc ------TOC __ pcntachlorophenol --
--__ pyridine
Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichJorophcnol
----__ vinyl chloride
endrin --lindane --Dale Received Reported by --methoxychlor
__ toxaphene
Dale Extracted Dale Reparted 2 . 2,4-D --13914 JUL 9 9 4 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --DIIS 3J'J1 (llcviscd 2/Yl)
. .
;,,:.c., Dcpanmcnt of Environment,
ilc!alth, &: Na1ural R=urccs
Solid •Waste 1',b.nai;cmcnt Oi,ision
SAMPLE ANALYSIS REQUEST S1a1c Laboratory of Public Hcal1h
· P.O. Dox 280-l7, 306 N. Wilminpon S1rect
Raleigh, North Carolina 27611
Site Number ----------------Field Sample Number W /.. -t) lJ Z -'i, W
Name of Site WA-1<>2.€:.J Coo,,rrt PG"'B u,FL. Site Location A F'To ,v NC -~..:...._..:....=~~-=-=--=------------
Collected By a. f\) IC.H.o \.. 6,o),,.J ID# 3-=f-Date Collected Z-S :/ O L-/ q4 Time /13b
T. t,u,..L~ £R-
Agency: Hazardous Waste X Solid Waste _·_superfund TCLP Compounds -- --
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium
fl_ Ground water (1) :Hz ---_ Solid (5) We1.L Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) ..SP~, r lAJ/ J:C.o Selenium --. --Silver --_ Other (4) _ Other (8) :re-001-'iw --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (o m'I«' Organic Compounds Results(mg/1)
P&T:GC/MS )( Arsenic -"-.o-ct benzene ----Acid:B/N Ext. X Barium ~0-0\ carbon tetrachloride ----'MTBE 1-Cadmium .L...o,oa::k.. chlordane ----Chloride chlorobenzene ------..15_ Chromium L..c,. o/ chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --...JL Lead ""-0-005 cresol ----
--__ Manganese --1,4-dichlorobenzene
--~ Mercury "'-.o.ooo.5 --1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylcne --_x_ Selenium L_ D. oQ5 --2,4-dinitrotoluene
){ Silver .t_o. o=5 __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophenol --
----pyridine
Microbiology --__ tetrachloroethylene
----trichloroethylene
Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-triehlorophcnol
------vinyl chloride
endrin --lindane --Date Received Reported by methoxychlor --__ toxaphene
Date Extracted Date Reported 2,4-D
013S15 JUL 29 94 --2,4,5-TP (Sil vex)
Dale A nalyzed Lab Number ·. --I) I IS JI 'JI ( llcviscd 2/91)
, .
.r--:.c; Depar.ment o( Env;ronmcnt,
J l\:alth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o( Public Health
· P.O. Box ~7. 306 N. Wilmingion Stn:ct
luleign, North Carolina 2761 I
Sile Number -----------------Field Sam pie N umber _ ___::_tv.;c_:ct._-_~----"0-=3_-___;~=--W;;__ ____ _
Name of Sile WA-1<.i2.€:..J Gorvrt PC"P, l.DFL Site Location A F"To 1'.J NC.. -~....:..._....:....::::....:...:,:__...c......:-=:...._-----------
Collected By G;. fv 1cHote6c::)-....> Date Collected 2j' ::JV LY t::/4 Time / I,, oo
1... /2t:>SE
Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results (mg/1)
Environmental Concentrate Comments Arsenic --
"#-3 Barium ---· L Ground water (1) _ Solid (5) lUEJ.i .. Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead ----Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)(~) Organic Compounds Results(mg/1)
P&T:GC/MS X Arsenic --l..o_ o l benzene ----Acid:B/N Ext. )( Barium L.. D-o \ carbon tetrachloride ------"MTBE X Cadmium -'-o-o oa, chlordane ------Chloride chlorobenzene ------~ Chromium -L....0.0 I chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --
--l Lead Lo_oo5 cresol --
--__ Manganese --1,4-dichlorobenzene
--~Mercury L..o-oao..5 --1,2-dichloroethane
--Nitrate _· _ 1,1-dichloroethylene --X-Selenium .t.. O-oo!:i 2,4-dinitrotoluene --.15_ Silver .L.. o_ o5 --heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC pentachlorophenol ----
--__ pyridine
Microbiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-lrichlorophc:nol --
----__ 2,4,6-trichlorophenol
------vin yl chloride
endrin --lindane --D ate Received Reported by methoxychlor --
--toxaphene
Dale Extracted Date Reported 2,4-0 --
013916 JUL 2 9 9 4 2.,4,5-TP (Si lvex)
Date AnalyLed Lab Number · --DI IS 3191 (Revised 2/91 )
< ..
•1'.C-Dcpar.mcnt of Environment,
ilcaJth, &: 1'atural Resources
Solid Waste Ma'nagemcnt Di~-ision
SAMPLE ANALYSIS REQUEST State ~boratory of Public Health
· P.O. Oox 280-l7, 306 K Wilmington Street
Raleigh, North Carolina 27611
Site Number ----------------Field Sample Numbcr __ W;;....._...;..L_-_0_0_4_-_..;:~:..:::....c.W _____ _
NameofSite WA-R.i2.€....J Gor..YN PG"'& l.r,FL. SiteLocation ArTo>J NC, -L....:...~..:....=~:.__-:..=...=.-----------
Collected By ~ . fv , U-to \... 6c,I-,.) Date Collected .:2.~ :TVL''1' q4 Time M-0D
T . l,,U.14 '-K' El<..
Agency: --Hazardous Waste X Solid Wasle __ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --
WEt..L .#4
Barium ---· 2L_ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --
wl __ Mercury
Soil (3) _ Sludge (7) SPLIT e<..o Selenium --, --Silver --_ Other (4) _ Other (8) IC -D t!:> 2. -ee, \.AJ --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) :W:10~) Organic Compounds Results(mg/1)
P&T:GC/MS ~ Arsenic ~0.01 benzene ----Acid:B/N Ext. )( Barium 0 .oa carbon tetrachloride
-.MTBE ----,< Cadmium -Lo-coa.. chlordane ------Chloride chlorobenzene ------)( Chromium L. O. 0 I chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol --
--L Lead L.g., 005 cresol --
--__ Manganese 1,4-dichlorobenzene --
--~ Mercury ..:::..0-000..S --1,2-dichloroethane
--Nitrale __ 1,1-dichloroethylene --L Selenium ~o. <!:>o5 2,4-dinitrotoluene --.JL Silver L.c,:1!0'5 __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethanc --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylcne
--__ trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane --Date Received Reported by __ methoxychlor
__ loxaphene
D..itc Extracted Date Reported 2,4-0
013917 JUL 29 94 --__ 2,4,5-TP (Silvex)
D..ilc AnalyLcd Lab Number --l)IIS 3191 (Revised 2/91)
. .
1','.C., Depar.ment o( Environment,
!i<!allh, & 1'atur.l Re.sources
Solid W.aste Man~gemenc Division
SAMPLE ANALYSIS REQUEST Stale Laboratory o( Public Health
· P.O. !3ox 28047, 306 N. Wilmington Street
RAieigh, North Carolina 27611
Site Number ----------------Field Sample Number W L -/!>O 5 -Go, uJ
Name of Site WA-1<i2.t.J C1or,rN PC"B u,FL Site Location A F"To ,-.J NC _.:....;.._...;._;;:...:..;:c..._ _ ____;.-='--------------
Collected By ~. fv •LH.o\,..6c::::>..._, Date Collected Zea -:J'f)L "I q4 Time /40 o
__, R_ / . '-"""" J..k E"
Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
.:t!: 4 ---· L Ground water (1) _ Solid (5) WE.LL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results(mg/l)Wil e.) Organic Compounds Results(mg/1)
P&T:GC/MS _K_ Arsenic ...(__c,_o\ benzene ----Acid:B /N Ext. 2-Barium o.ce carbon tetrachloride ----'MTBE 'Jf Cadmium L...Q. 99.'.;l. chlordane ----Chloride chlorobenzene ------~ Chromium -'-0-0\ chloroform --, --__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-cresol ------_½,__Lead L-.o .og.S cresol --
--__ Manganese 1,4-dichlorobenzene ----_L Mercury .L..c,.ooo'.':'.l --1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylcne --_x_ Selenium L...c,.005 2,4-dinitrotoluene --LSilver ..L..o,,.o:S __ heptachlor
Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Paramelt!r Results (PCi/1) _pH hex.achloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophenol --
--__ pyridine
Microbiology ----tetrachloroethylene
----trichloroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by methoxychlor --
--toxaphene
Date Extracted Date Reported 2,4-0
013918 JUL 2 9 9 4 --2,4,5-TP (Silvcx)
Date Analyzed Lab Number --Dl!S 3191 (llcviscd 2/91)
. . . . . ..
HAZARDOUS WASTE METAL ANALYSIS
DATE: ( J \!.. /) t: 91/ I r--s AMPLE NAME: L J >--Ir Vt! '::Ls c;, e C 1J I.., J -
LABORATORY NUMBER: __.l_,.., __ 1 ..... CZ ..... f_L.....,( __ ---, __ I..__..J.......,_? .... f ..... K: __ . _
JXTRACTAB:t.E 0
REMARKS:
-
Pa1tamUV1. Rut.du I ppm l
IJ-
----->
CJ ...( 0.002-------->
Cv-<o.o/
PG
------3
N.C. Dept. of Environ~ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
-· !~
SI ....
~-
HAZARDOUS WASTE METAL ANALYSIS
DATE: I I
SAMPLE NAME:
LABORATORY NUMBER:
( J._, Y-re ½, C12
()9o y ~
{?en L/:-
1 J tr.:r
IOTJ\Js □ F.XIR t\CTABI::e-0
REMARKS:
Pa1tame.te.1t Ruui.t.6 ( ppm I
D o/ -t( -
As 4 o. 0 (
CJ. ,< 0, 002-
C v-< o.ot
Pb ,::_ ~ .o~ c;-
N.C. Dept. of Environ~ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
~
11
"' 7
,<!J. o L
<g 02
~
7 tJ.tJ!.//
HAZARDOUS WASTE METAL ANALYSIS
DATE:
LABORATORY NUMBER:
E~CIABLE 0
REMARKS:
p cvr.ame.:tVL Ruui.U I ppm I
/J
43
N.C. Dept. of Environ~ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
. . . .
HAZARDOUS WASTE METAL ANALYSIS
LABORATORY NUMBER:
E~RACTABLE □
REMARKS:
Ruul.u (ppm)
_lj_
N.C. Dept. of Environment , Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
t 'J
. . .
t f.;Jp;:ij;_;;i~i:J ~:£:;¥£;~~ ~t~~ii~J~:~?d'ii}~;i:ii~~i~1 (r•1>~ /\~f;.,1-·:,:i'-l;~_ . ., •. t.l.'..._~·!-'i, ~~)Jo,,(\~~:.-;.,..;,~-.. ~-'!.•~·~.,{..;.(f&~ .... -r.'"~ ;~~tt~~iltttlt~iff t~t~.Wtt.1liil1~
HAZARDOUS WASTE METAL ANALYSIS
I .
DATE:
SAMPLE NAME: __ lt) __ ~-·~V~r_e_':\-----aaaa.,.__.Y, __ ~P_c __ l]....._ __ (_-E: __ _
LABORATORY NUMBER:
~R"i\C !ABLE □
REMARKS:
PaJt.ametu. Rulli.u !ppm)
{L( ---
0 ,,.-<o.o I o. =>
{ C,
<o.o I
N.C. Dept. of Environ~ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
o.og 0.08
. . HAZARDOUS WASTE METAL ANALYSIS
DATE: I Je. 12 f-: ?y
l /
SAMPLE NAME: l,) >-~f/e...... Cc /)co t:__ E
LABORATORY NUMBER: /-:J Yd z Y /J 9/ I
_EXTP ~CTABLE □
REMARKS:
PaJt.ame.t.Vt Ru <.L.l,u I ppm I
j_L
o.o7 <o,o I
N.C. Dept. of Enviro11111ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
/1
o.ob
_· . . . . .
HAZARDOUS WASTE METAL ANALYSIS
DATE:
SAMPLE NAME: __ U....__ ..... 2:>:._._t_Y_e ___ ~ ___ c __ ~ .. z __ p_c ___ l3"'-~t:._-----F ___ _
LABORATORY NUMBER: /19'07 ? /.J9/8
.m □
REMARKS:
r 01
'to
' ((
, IS-
fl 'l: -J
N.C. Dept. of Environ111ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
(ppm)
l AB a@AToR.Y C HAIAJ oF c VITO DY
LF
SAMPLE LtlBaf2An,Ry div& OeR {s) ; I JCJo::J ---t
REce(V..ED !3.Y D.ATF IDIAE=. Fo R.
{Z.J;Jstjld I
9/;/9¥ 4 I .;J:o1.o /Jlfe:/4(5.
9 Q,., I u . .! c, a.,..._-.. , •• cl'.S 0 <Q_ ~
' 71/ tGe t/2-/1r g': 00,a...,...._ ut~/4/s ., L ~j
' R~o~ . \
I ·.o :Q ~~ -~ ;i
~) 2-,/1'✓ /1:0~ ~ ~ ., 7 B ='--, Nw::wO'= ~~,~ ;:::J <::l.J\._ •• --, / l 1 ·. ;30
,,
'
----··•·--······· ... . . --·. ··-·------... ____ ,. ____ _ ---·-----. ---•··•--·•·'-•-----~----------·-· ---· --· ... --.. ------... --. -. . ---7-·Io{i;JJ
l AB a C?AToR.Y CHAI.& aF c VITO DY Re:co 12 D
S-AA,<PLE L4Ba(2tfTr1RY d/UM llcR (s)
c«re ecre:i2 (o 'c esmv Zf Y :
REcetVe.D 8Y
iAu
~Ar:i!C.
I
f4/9✓ 7.35
PE AA
0072
,I
SE1
94/09/02
07:39:08
94/09/02
07:39:08
#HOR
0009
0000000
#DATA
M.King
20
1.0
0=g
1
1=uL
1. 0E-6
4,5.0 ck,,
5,Blk,,2
6,Spike,,2
7, 13909u,,2
8, 13909s,,2
9,13910u,,2
10, 13910s,, 2
1 1 , 139 11 u, , 2
12, 13911s,,2
13, 13912u,, 2
14, 13912s,, 2
15, 13913u, , 2
16, 13913s,, 2
17,13914u,,2
18, 13914s,, 2
19, 139151.1, , 2
20,13915s,,2
21 , 139 16 u, , 2
22, 13916s,, 2
23,13917u,,2
24, 13917s,, 2
25, 13918u,, 2
26,13918s,,2
HGA IDWT ASCII 5100 PC 7. 10
-------------------------------------------------------------------------------
~lement File: SE1.GEL
Date: 09/02/94
Element: Se
Time: 11 : 24
Wavelength: 196.0
Slit: 2.0 L
~ata File:
rechniq1.1e: HGA
ID/Wt File: SE1.IDW
Calib. Type: Nonlinear
Lamp Cltrrent: 0
Energy: 61
------------------------------------------------------------------------------~
3e ID: Std. Blk Seq. No.: 00060 A/S Pas.: 40
~epl icate 1
Jeak Area <A-s): 0.003
3ackground Pk Area <A-s): 0.018
3lank Corrected Pk Area (A-s): 0.003
~1.1to-zero performed.
Time: 11 :24
Peak Height (A): 0.010
Background Pk Height (A)
3e ID: Std 1 Seq. No. : 00061 A/S Pas. : 1
Replicate 1
Jeak Area (A-s): 0.048
Backgroltnd Pk Area <A-s>: 0.023
Blank Corrected Pk Area (A-s): 0.044
3tandard nllmber 1 applied. (30.0)
:orrelation coefficient: 1.00000
Ti me: 11: 27
Peak Height <A): 0.057
Backgrollnd Pk Height (A)
Slope: 0.0015
3e ID: Std 2 Seq. No.: 00062 A/S Pas.: 2
Replicate 1
:ieak Area (A-s): 0.078
Backgrollnd Pk Area <A-s): 0.027
Blank Corrected Pk Area (A-s): 0.075
:oncentration (llg/L ): 50.7
3tandard number 2 applied. C50. 0J
:orrelation coefficient: 1.00000
Ti me: 11: 29
Peak Height (A): 0.086
Backgrollnd Pk Height <A>
Slope: 0.0014
3e ID: Lab QC Check Seq. No.: 00063 A/S Pos.: 3
Replicate 1
:ieak Area <A-s>: 0.020
Background Pk Area <A-s>: 0.018
Blank Corrected Pk Area <A-s>: 0.017
:oncent ration < 1.1g /L ) : 11. 4
]C sample is within range 7.5 -12.5
Time: 11:32
Peak Height (A): 0.023
Background Pk Height <A>
3e ID: 5.0 ck Seq. No.: 00064 A/S Pas.: 4
Replicate 1
:ieak Area (A-s > : 0. 011
Backgro1.1nd Pk Area (A-s): 0.016
Blank Corrected Pk Area <A-s>: 0.007
:oncentrat ion ( ug/L > : 5. 1
Ti me: 11: 34
Peak Height (A): 0. 015
Backgro1.1nd Pk Height (A)
Date: 09/02/94
0.014
Date: 09/02/94
0.017
Date: 09/02/94
0.020
Date: 09/02/94
0.012
Date: 09/02/94
0.012
Se ID: Blk Seq. No.: 00065 A/S Pos.: 5 Date: 09/02/94
Replicate
Peak Area
1
CA-s) : 0. 004
Background Pk Area <A-s): 0.016
Blank Corrected Pk Area CA-s): 0.001
Concentration (ug/L ) : 0.4
Ti me: 11: 36
Peak Height CA): 0.009
Background Pk Height CA> 0.012
Corrected Cone Cug/L ) : 0. 9
Se ID: Spike Seq. No.: 00066 A/S Pos. : 6 Date: 09/02/94
Replicate 1
Peak Area <A-s>: 0.034
Background Pk Area CA-s) 0.022
Blank Corrected Pk Area CA-s): 0.031
Concentration Cug/L ): 21.0
Ti me: 11: 39
Peak Height (A): 0.040
Background Pk Height CA)
Corrected Cone (ug/L ) :
0.012
42. 1
Se ID: 13909u Seq. No.: 00067 A/S Pos.: 7 Date: 09/02/94
Replicate 1
Peak Area CA-s> 0.005
Background Pk Area CA-s>: 0.043
Blank Corrected Pk Area CA-s>: 0.002
Concentration Cug/L ) : 1.4
Time: 11:41
Peak Height CA): 0.010
Background Pk Height CA) 0.035
Corrected Cone (ug/L ): 2.7
Se ID: 13909s Seq. No.: 00068 A/S Pos.: 8 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.035
Background Pk Area <A-s) 0.053
Blank Corrected Pk Area <A-s): 0.032
Concentration Cug/L ) : 22.0
Time: 11:43
Peak Height (A): 0. 031
Background Pk Height CA) 0.037
Corrected Cone (ug/L ) : 43. 9
Se ID: 13910u Seq. No.: 00069 A/S Pos. : 9 Date: 09/02/94
Replicate
Peak Area
1
CA-s) 0.004
Background Pk Area CA-s) 0.028
Blank Corrected Pk Area (A-s) 0.001
Concentration Cug/L ) : 0. 4
Time: 11: 46
Peak Height CA): 0.007
Background Pk Height (A): 0.019
Corrected Cone Cug/L ) : 0. 8
Se ID: 13910s Seq. No.: 00070 A/S Pos. : 10 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.041
Background Pk Area CA-s) 0.030
Blank Corrected Pk Area CA-s): 0.038
Concentration (ug/L ): 25.8
Time: 11 :48
Peak Height CA): 0.035
Background Pk Height CA): 0.020
Corrected Cone (ug/L ) : 51. 6
Se ID: 13911 u Seq. No.: 00071 A/S Pos. : 11 Date: 09/02/94
Replicate 1
Peak Area CA-s) 0.002
Time: 11:51
Peak Height CA) 0.007
Background Pk Area <A-s): 0.019 Background Pk Height <A>: 0.014
Blank Corrected Pk Area <A-s): -0.002
Concentration (ug/L ) : -1. 1 Corrected Cone (ug/L ): -2.2
Se ID: 13911 s Seq. No.: 00072 A/S Pas. : 12 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.041
Background Pk Area <A-s): 0.022
Blank Corrected Pk Area <A-s): 0.037
Concentration (ug/L ): 25.4
Time: 11:53
Peak Height CA): 0. 043
Background Pk Height CA): 0.013
Corrected Cone (ug/L ): 50.9
Se ID: 13912u Seq. No.: 00073 A/S Pos.: 13 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.004
Background Pk Area (A-s): 0.020
Blank Corrected Pk Area <A-s): 0.000
Concentration (ug/L ) : 0.3
Ti me: 11: 55
Peak Height (A): 0.010
Background Pk Height CA): 0.011
Corrected Cone Cug/L ) : 0. o
Se ID: 13912s Seq. No.: 00074 A/S Pas. : 14 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.036
Background Pk Area <A-s): 0.023
Blank Corrected Pk Area <A-s): 0.033
Concentration (ug/L ) : 22.2
Ti me: 11: 58
Peak Height <A>: 0.042
Background Pk Height (A): 0.015
Corrected Cone (ug/L >: 44.3
Se ID: 13913u Seq. No.: 00075 A/S Pas. : 15 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.002
Background Pk Area <A-s): 0.018
Blank Corrected Pk Area <A-s): -0.001
Concentration (ug/L ): -0.9
Ti me: 12: 00
Peak Height <A>: 0.007
Background Pk Height CA): 0.013
Corrected Cone (ug/L ) : -1. 7
Se ID: 13913s Seq. No.: 00076 A/S Pas. : 16 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.035
Background Pk Area <A-s>: 0.024
Blank Corrected Pk Area CA-s): 0.031
Concentration (ug/L ): 21.3
Ti me: 12: 02
Peak Height <A> : 0. 042
Background Pk Height CA): 0.014
Corrected Cone <ug/L ): 42.7
Se ID: 13914u Seq. No.: 00077 A/S Pos. : 17 Date: 09/02/94
Replicate 1
Peak Area CA-s): 0.002
Background Pk Area <A-s): 0.016
Blank Corrected Pk Area CA-s): -0.001
Concentration Cug/L ) : -0.8
Ti me: 12: 05
Peak Height (A>: 0.011
Background Pk Height <A): 0.012
Corrected Cone Cug/L ) : -1. 7
Se ID: 13914s Seq. No.: 00078 A/S Pos. : 18 Date: 09/02/94
I
Replicate 1
Peak Area (A-s} 0.036
Background Pk Area (A-s>: 0.020
Blank Corrected Pk Area <A-s> 0.033
Concentration (ug/L ) : 22.6
Time: 12:07
Peak Height CA>: 0.046
Background Pk Height (A} 0.012
Corrected Cone (ug/L ) : 45.3
Se ID: 139151.1 Seq. No.: 00079 A/S Pos.: 19 Date: 09/02/94
Replicate 1
Peak Area <A-s>: 0.003
Background Pk Area (A-s} 0.012
Blank Corrected Pk Area (A-s>: 0.000
Concentration (ug/L ): 0. 1
Ti me: 12: 09
Peak Height (A}: 0.011
Background Pk Height <A> 0.009
Corrected Cone (ug/L ) : 0. 2
Se ID: 13915s Seq. No.: 00080 A/S Pos.: 20 Date: 09/02/94
Replicate 1
Peak Area <A-s> 0.036
Background Pk Area (A-s}: 0.020
Blank Corrected Pk Area <A-s>: 0.033
Concentraticin (ug/L >: 22.5
Time: 12: 12
Peak Height CA}: 0.043
Background Pk Height <A>
Corrected Cone (ug/L >:
0.013
45.0
Se ID: 13916u Seq. No.: 00081 A/S Pos. : 21 Date: 09/02/94
Replicate 1
Peak Area <A-s}: 0.005
Background Pk Area (A-s}
Blank Corrected Pk Area
Concentration (ug/L }:
0.015
(A-s>: 0.002
1 .. • w
Time: 12:14
Peak Height CA) : 0. 010
Background Pk Height CA) 0.009
Corrected Cone (ug/L >: 2.7
Se ID: 13916s Seq. No.: 00082 A/S Pos.: 22 Date: 09/02/94
Replicate 1
Peak Area (A-s} 0.040
Background Pk Area (A-s}: 0.020
Blank Corrected Pk Area (A-s}
Concentration (ug/L >: 25.0
0.037
Time: 12:17
Peak Height CA): 0.047
Background Pk Height CA}: 0.014
Corrected Cone (ug/L ): 49.9
Se ID: 13917u Seq. No.: 00083 A/S Pas.: 23 Date: 09/02/94
Replicate 1
Peak Area (A-s>: 0.003
Background Pk Area (A-s): 0.017
Blank Corrected Pk Area <A-s} -0.000
Concentration (ug/L }: -0. 1
Time: 12:19
Peak Height <A>: 0.008
Background Pk Height (A) 0.010
Corrected Cone (ug/L ) : -0.2
Se ID: Lab QC Check Seq. No.: 00084 A/S Pos.: 3 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.018
Time: 12:21
Peak Height <A> 0.023
•
Background Pk Area (A-s): 0.020
Blank Corrected Pk Area (A-s): 0.014
Concentration (ug/L ): 9.9
QC sample is within range 7.5 -12.5
Background Pk Height (A) 0.012
Se ID: 13917s Seq. No.: 00085 A/S Pos.: 24 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.039
Background Pk Area <A-s): 0.021
Blank Corrected Pk Area (A-s): 0.035
Concentration (ug/L ) : 24. 1
Time: 12: 24
Peak Height <A>: 0.042
Background Pk Height (A): 0.013
Corrected Cone (ug/L ) : 48.2
Se ID: 13918u Seq. No.: 00086 A/S Pos.: 25 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.006
Background Pk Area <A-s): 0.016
Blank Corrected Pk Area <A-s): 0.003
Concentration (ug/L ) : 2.0
Ti me: 12: 26
Peak Height CA): 0. 009
Background Pk Height CA): 0.010
Corrected Cone (ug/L ) : 3. g
Se ID: 13918s Seq. No.: 00087 A/S Pos.: 26 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.039
Background Pk Area (A-s): 0.022
Blank Corrected Pk Area (A-s): 0.036
Concentration <ug/L ) : 24.3
Ti me: 12: 28
Peak Height CA): 0.042
Background Pk Height CA>: 0.014
Corrected Cone (ug/L ) : 48. 6
Se ID: Lab QC Check Seq. No.: 00088 A/S Pos.: 3 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.020
Background Pk Area (A-s): 0.020
Blank Corrected Pk Area <A-s): 0.017
Concentration (ug/L ) : 11.6
QC sample is within range 7.5 -12.5
Time: 12:31
Peak Height CA): 0.025
Background Pk Height CA): 0.012
F'E AA
0072
AS1
94/07/07
23:53:33
94/07/07
23:53:33
4:i:Hm:;:
0009
0000000
#DATA
M.f<ing
20
1. 0
O=g
1
l=uL
1.0E-6
4,5.0 ck,,
5,Blk,,2
6,spike, ,2
7 , 13909u , , 2
8, 13909s, ,2
9 , 1391 Ou, , 2
10, 13910s, ,2
11 , 13911 Ll, , 2
12,13911s, ,2
13, 13912u, , 2
1 4, l 3912s, , 2
15, 13913u, , 2
1 6 , 139 13s , , 2
1 7 , 1391 4u , , 2
18, l 3914s, , 2
19, 13915u, , 2
20, 139 l 5s, , 2
21 , 13916Ll, , 2
22, l 3916s, , 2
23 , 1391 7u , , 2
24,13917s,,2
25 , 1391 Bu, , 2
26, 1391 Bs , , 2
HGA IDWT ASCII 5100 F'C 7. 10
Element File: ASl.GEL
Date: 07/08/94
Element: As
Time: 02:00
Wavelength: 193.7
Slit: 0.70 L
Data File:
Technique: HGA
ID/Wt File : CRl.IDW
Calib. Type: Nonlinear
Lamp Current: 0
Energy: 45
-------------------------------------------------------------------------------
As ID: Std Blk Seq. No.: 00030 A/S Pos.: 40 Date: 07/08/94
Replicate 1
Peak Area (A-s): -0.001
Background Pk Area (A-s): 0.014
Blank Corrected Pk Area (A-s): -0.001
Auto-zero performed.
Time: 02:00
Peak Height (A): 0.016
Background Pk Height (A): 0.019
As ID: Std 1 Seq. No.: 00031 A/S Pos.: 1 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.141
Background Pk Area (A-s): 0.035
Blank Corrected Pk Area (A-s): 0.142
Standard number 1 applied. [30.0]
Correlation coefficiant: 1.00000
Time: 02:02
Peak Height (A): 0.206
Background Pk Height (A): 0.027
Slope: 0.0047
As ID: Std 2 Seq. No.: 00032 A/S Pos.: 2 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.242
Background Pk Area (A-s): 0.047
Blank Corrected Pk Area (A-s): 0.242
Concentration (ug/L ): 51.3
Standard number 2 applied. [50.0]
Correlation coefficient: 1.00000
Time: 02:05
Peak Height (A): 0.336
Background Pk Height (A): 0.041
Slope: 0.0046
As ID: Lab QC Check Seq . No.: 00033 A/S Pos .: 3 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.099
Background Pk Area (A-s): 0.043
Blank Corrected Pk Area (A-s): 0.100
Concentration (ug/L ): 21.3
QC sample is within range 17.5 -22.5
Time: 02:07
Peak Height (A): 0.154
Background Pk Height (A): 0.025
As ID: 5.0 ck Seq. No.: 00034 A/S Pos.: 4 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.028
Background Pk Area (A-s): 0.041
Blank Corrected Pk Area (A-s): 0.029
Concentration (ug/L ): 6.3
Time: 02:10
Peak Height (A): 0.042
Background Pk Height (A): 0.029
I
As ID: Blk Seq. No.: 00035 A/S Pos.: 5 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.004
Background Pk Area (A-s): 0.042
Blank Corrected Pk Area (A-s): 0.005
Concentration (ug/L ): 1.1
Time: 02:12
Peak Height (A): 0.016
Background Pk Height (A): 0.033
Corrected Cone (ug/L ): 2.2
As ID: spike Seq. No.: 00036 A/S Pos.: 6 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.097
Background Pk Area (A-s): 0.050
Blank Corrected Pk Area (A-s): 0.097
Concentration (ug/L ): 20.8
Time: 02:15
Peak Height (A): 0.154
Background Pk Height (A): 0.030
Corrected Cone (ug/L ): 41.7
As ID: 13909u Seq. No.: 00037 A/S Pos.: 7 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.003
Background Pk Area (A-s): 0.050
Blank Corrected Pk Area (A-s): 0.004
Concentration (ug/L ): 0.9
Time: 02:17
Peak Height (A): 0.016
Background Pk Height (A): 0.033
Corrected Cone (ug/L ): 1.8
As ID: 13909s Seq. No.: 00038 A/S Pos.: 8 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.110
Background Pk Area (A-s): 0.059
Blank Corrected Pk Area (A-s): 0.111
Concentration (ug/L ): 23.6
Time: 02:20
Peak Height (A): 0.122
Background Pk Height (A): 0.034
Corrected Cone (ug/L ): 47.3
As ID: 13910u Seq. No.: 00039 A/S Pos.: 9 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.005
Background Pk Area (A-s): 0.054
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 1.2
Time: 02:22
Peak Height (A): 0.017
Background Pk Height (A): 0.032
Corrected Cone (ug/L ): 2.4
As ID: 13910s Seq. No.: 00040 A/S Pos.: 10 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.107
Background Pk Area (A-s): 0.050
Blank Corrected Pk Area (A-s): 0.107
Concentration (ug/L ): 22.9
Time: 02:25
Peak Height (A): 0.124
Background Pk Height (A): 0.029
Corrected Cone (ug/L ): 45.8
As ID: 13911u Seq. No.: 00041 A/S Pos.: 11 Date: 07/08/94
Replicate 1 Time: 02:27
Peak Area (A-s): 0.005 Peak Height (A): 0.017
Background Pk Area (A-s): 0.046
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 1.4
Background Pk Height (A): 0.028
Corrected Cone (ug/L ): 2.7
.As ID: 13911s Seq. No.: 00042 A/S Pos.: 12 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.094
Background Pk Area (A-s): 0.052
Blank Corrected Pk Area (A-s): 0.095
Concentration (ug/L ): 20.3
Time: 02:29
Peak Height (A): 0.152
Background Pk Height (A): 0.031
Corrected Cone (ug/L ): 40.6
As ID: 13912u Seq. No.: 00043 A/S Pos.: 13 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.004
Background Pk Area (A-s): 0.045
Blank Corrected Pk Area (A-s): 0.004
Concentration (ug/L ): 1.0
Time: 02:32
Peak Height (A): 0.014
Background Pk Height (A): 0.031
Corrected Cone (ug/L ): 1.9
As ID: 13912s Seq. No.: 00044 A/S Pos.: 14 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.097
Background Pk Area (A-s): 0.054
Blank Corrected Pk Area (A-s): 0.098
Concentration (ug/L ): 20.9
Time: 02:34
Peak Height (A): 0.141
Background Pk Height (A): 0.028
Corrected Cone (ug/L ): 41.8
As ID: 13913u Seq. No.: 00045 A/S Pos.: 15 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.005
Background Pk Area (A-s): 0.057
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 1.2
Time: 02:37
Peak Height (A): 0.017
Background Pk Height (A): 0.038
Corrected Cone (ug/L ): 2.4
As ID: 13913s Seq. No.: 00046 A/S Pos.: 16 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.105
Background Pk Area (A-s): 0.062
Blank Corrected Pk Area (A-s): 0.105
Concentration (ug/L ): 22.5
Time: 02:39
Peak Height (A): 0.134
Background Pk Height (A): 0.051
Corrected Cone (ug/L ): 45.0
As ID: 13914u Seq. No.: 00047 A/S Pos.: 17 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.001
Background Pk Area (A-s): 0.050
Blank Corrected Pk Area (A-s): 0.002
Concentration (ug/L ): 0.5
Time: 02:42
Peak Height (A): 0.012
Background Pk Height (A): 0.028
Corrected Cone (ug/L ): 0.9
-------------------------------------------------------------------------------
As ID: 13914s Seq. No.: 00048 A/S Pos.: 18 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.096
'Background Pk Area (A-s): 0.059
Blank Corrected Pk Area (A-s): 0.097
Concentration (ug/L ): 20.7
Time: 02:44
Peak Height (A): 0.112
Background Pk Height (A): 0.035
Corrected Cone (ug/L ): 41.5
As ID: 13915u Seq. No.: 00049 A/S Pos.: 19 Date: 07/08/94
Replicate 1
Peak Area (A-s): -0.001
Background Pk Area (A-s): 0.051
Blank Corrected Pk Area (A-s): -0.001
Concentration (ug/L ): -0.1
Time: 02:47
Peak Height (A): 0.018
Background Pk Height (A): 0.034
Corrected Cone (ug/L ): -0.3
As ID: 13915s Seq. No.: 00050 A/S Pos.: 20 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.097
Background Pk Area (A-s): 0.057
Blank Corrected Pk Area (A-s): 0.098
Concentration (ug/L ): 20 .9
Time: 02:49
Peak Height (A): 0 .113
Background Pk Height (A): 0.031
Corrected Cone (ug/L ): 41.8
As ID: 13916u Seq. No.: 00051 A/S Pos.: 21 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0 .001
Background Pk Area (A-s): 0.044
Blank Corrected Pk Area (A-s): 0.002
Concentration (ug/L ): 0.4
Time: 02:52
Peak Height (A): 0.014
Background Pk Height (A): 0.028
Corrected Cone (ug/L ): 0.8
As ID: 13916s Seq . No.: 00052 A/S Pos.: 22 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0 .099
Background Pk Area (A-s): 0.051
Blank Corrected Pk Area (A-s): 0.100
Concentration (ug/L ): 21.4
Time: 02:54
Peak Height (A): 0.110
Background Pk Height (A): 0 .031
Corrected Cone (ug/L ): 42.8
As ID: 13917u Seq. No.: 00053 A/S Pos .: 23 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.007
Background Pk Area (A-s): 0.045
Blank Corrected Pk Area (A-s): 0.008
Concentration (ug/L ): 1.7
Time: 02:56
Peak Height (A): 0.014
Background Pk Height (A): 0.027
Corrected Cone (ug/L ): 3.4
As ID: Lab QC Check Seq . No.: 00054 A/S Pos.: 3 Date: 07/08/94
Replicate 1 Time: 02:59
Peak Area (A-s): 0.097 Peak Height (A): 0.150
.................. ,.,...........,._~....--~
Background Pk Area (A-s): 0.045
Blank Corrected Pk Area (A-s): 0.098
Concentration (ug/L ): 20.9
QC sample is within range 17.5 -22.5
Background Pk Height (A): 0 .027
-------------------------------------------------------------------------------
As ID: 13917s Seq. No.: 00055 A/S Pos.: 24 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0 .098
Background Pk Area (A-s): 0.056
Blank Corrected Pk Area (A-s): 0.099
Concentration (ug/L ): 21.2
Time: 03:01
Peak Height (A): 0.110
Background Pk Height (A): 0 .031
Corrected Cone (ug/L ): 42 .3
As ID: 13918u Seq . No.: 00056 A/S Pos.: 25 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.002
Background Pk Area (A-s): 0.049
Blank Corrected Pk Area (A-s): 0.003
Concentration (ug/L ): 0.6
Time: 03:04
Peak Height (A): 0.014
Background Pk Height (A): 0.034
Corrected Cone (ug/L ): 1 .1
As ID: 13918s Seq. No.: 00057 A/S Pos.: 26 Date : 07/08/94
Replicate 1
Peak Area (A-s): 0 .097
Background Pk Area (A-s): 0.054
Blank Corrected Pk Area (A-s): 0.097
Concentration (ug/L ): 20 .8
Time: 03:06
Peak Height (A): 0 .119
Background Pk Height (A): 0.028
Corrected Cone (ug/L ): 41.7
As ID: Lab QC Check Seq. No.: 00058 A/S Pos.: 3 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0 .095
Background Pk Area (A-s): 0.046
Blank Corrected Pk Area (A-s): 0 .096
Concentration (ug/L ): 20 .5
QC sample is within range 17.5 -22.5
Time: 03:09
Peak Height (A): 0.162
Background Pk Height (A): 0.030
-t , _ _...,,., ... C toe 4tQIHct.WWfJUt,f!,t,i◄W Q?J,.i.if\-¥,,,1 ·hJ.9 (11.f(iW", w..;1.M•J-O►CiPiVU. ,J_l<;l:!ttih\.~ PNl!o/.41,1:+tri.E:: .. ,.'thlR'C~
,-
PE AA
0072
PB1
94/09/02
07 l 39: 18
94/09/02
07: 39: 18
#HDR
0009
0000000
#DATA
M.King
20
1.0
0=g
1
l=uL
1. 0E-E,
4,5.0 ck,,
HGA
5, Bl k, , 2
&,Spike,,2
7,13909u,,2
8,13909s,,2
9,13910u,,2
10, 13910s,, 2.
11, 13911u,, 2
12, 13911 s, , 2
13,139121.1,,2
14, 13912s,, 2
15,139131.1,,2
1 & , 139 13 s, , 2
17, 13914u, ,2
18, 13914s,, 2
19, 139151.1,, 2
20,13915s,,2
21, 139 H, l.l, , 2
22, 139 1 E, s, , 2
23, 139171.1,,2
24, 13917s,, 2
25,13918u,,2
2&, 13918s,,2
IDWT ASCII 5100 PC 7. 10
Element File: PB2.GEL
Date: 09/02/94
Element: Pb
Time: 09:37
Wavelength: 283.3
Slit: 0. 7 L
Data File:
Technique: HGA
ID/Wt File: CD1. IDW
Calib. Type: Nonlinear
as modifier-21-
Lamp Current: 0
Energy: 65
Remark 1: ammonium phosphate
Remark 2: 20g to 500mls (for Cd) = 41-; make 2 dilution for Pb
Pb ID: Std Blk Seq. No. : 00031 A/S Pas.: 40
Replicate 1
Peak Area (A-s): 0.000
Background Pk Area (A-s): 0.012
Blank Corrected Pk Area (A-s): 0.000
Auto-zero performed.
Time: 09:37
Peak Height (A): 0.005
Background Pk Height (A)
Pb ID: Std 1 Seq. No.: 00032 A/S Pas. : 1
Replicate 1
Peak Area (A-s): 0.075
Background Pk Area <A-s>: 0.027
Blank Corrected Pk Area (A-s>: 0.075
Standard number 1 applied. (30.0]
Correlation coefficient: 1.00000
Time: 09:40
Peak Height (A) : 0. 166
Background Pk Height <A>
Slope: 0.0025
Pb ID: Std 2 Seq. No.: 00033 A/S Pas.: 2
Replicate 1 Time: 09:42
Date: 09/02/94
0.008
Date: 09/02/94
0.037
Date: 09/02/94
Peak Area <A-s>: 0.120
Background Pk Area (A-s>: 0.039
Blank Corrected Pk Area (A-s): 0.120
Concentration (ug/L ) : 48. 1
Peak Height <A>: 0. 231
Background Pk Height <A>: 0.047
Standard number 2 applied. (50. 0]
Correlation coefficient: 1.00000 Slope: 0.0026
Pb ID: Lab QC Check Seq. No.: 00034 A/S Pas.: 3
Replicate 1
Peak Area (A-s>: 0.052
Background Pk Area <A-s>: 0.027
Blank Corrected Pk Area (A-s): 0.052
Concentration (ug/L >: 20.5
QC sample is within range 17.5 -22.5
Time: 09:45
Peak Height <A>: 0.116
Background Pk Height <A>
Pb ID: 5.0 ck Seq. No.: 00035 A/S Pas.: 4
Replicate 1
Peak Area <A-s>: 0.014
Background Pk Area <A-s): 0.026
Blank Corrected Pk Area <A-s): 0.013
Time: 09:48
Peak Height <A>: 0.028
Background Pk Height <A>
Date: 09/02/94
0.027
Date: 09/02/94
0.014
....
Concentration (ug/L ): 5.0
Pb ID: Blk Seq. No.: 00036 A/S Pos.: 5 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.001
Background Pk Area (A-s): 0.030
Blank Corrected Pk Area (A-s>: 0.000
Concentration (ug/L ): 0. 1
Time: 09:51
Peak Height CA): 0.005
Background Pk Height CA): 0.009
Corrected Cone (ug/L ): 0.2
Pb ID: Spike Seq. No.: 00037 A/S Pos. : 6 Date: 09/02/94
Replicate 1
Peak Area <A-s) 0.048
Background Pk Area <A-s): 0.038
Blank Corrected Pk Area (A-s) 0.048
Concentration (ug/L ) : 18.8
Time: 09:54
Peak Height CA): 0.094
Background Pk Height CA): 0.025
Corrected Cone (ug/L >: 37.6
Pb ID: 13909u Seq. No.: 00038 A/S Pos.: 7 Date: 09/02/94
Replicate 1 Time: 09:56
Pe a k He i g ht <A) : 0. 005
Background Pk Height <A> 0.037
Peak Area <A-s): 0.000
Background Pk Area <A-s>
Blank Corrected Pk Area
Concentration (ug/L ):
: 0.092
<A-s): -0.000
-0. 1 Corrected Cone (ug/L ): -0.2
Pb ID: 13909s Seq. No.: 00039 A/S Pas.: 8
Replicate 1
Peak Area <A-s> 0.053
Background Pk Area (A-s>: 0.106
Blank Corrected Pk Area (A-s) 0.052
Concentration (ug/L ) : 20.7
Time: 09:59
Peak Height <A>: 0. 089
Background Pk Height (A)
Corrected Cone (ug/L ) :
Pb ID: 13910u Seq. No.: 00040 A/S Pas. : 9
Replicate 1
Peak Area (A-s): 0.002
Background Pk Area (A-s>: 0.053
Blank Corrected Pk Area (A-s) 0.001
Concentration (ug/L ) : 0.5
Ti me: 10: 02
Peak Height (A): 0.004
Background Pk Height (A)
Corrected Cone (ug/L ):
Pb ID: 13910s Seq. No.: 00041 A/S Pas. : 10
Replicate 1
Peak Area (A-s) 0.051
Ti me: 10: 05
Peak Height (A): 0.073
Background Pk Height (A)
Date: 09/02/94
0.052
41. 5
Date: 09/02/94
0.022
1. 1
Date: 09/02/94
0.034 Background Pk Area (A-s): 0.061
Blank Corrected Pk Area (A-s) 0.051
Concentration (ug/L ) : 20. 1 Corrected Cone (ug/L ) : 40.2
Pb ID: 13911 u Seq. No.: 00042 A/S Pos. : 11 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.001
Background Pk Area (A-s): 0.025
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ) : 0.4
Ti me: 10: 08
Peak Height (A): 0.005
Background Pk Height CA): 0.010
Corrected Cone (ug/L >: 0.7
Pb ID: 13911 s Seq. No.: 00043 A/S Pos. : 12 Date: 09/02/94
Replicate 1
Peak Area CA-s>: 0.054
Background Pk Area (A-s): 0.037
Blank Corrected Pk Area (A-s): 0.053
Concentration (ug/L ) : 21.0
Time: 10:11
Pe a k He i g ht CA> : 0. 100
Background Pk Height CA): 0.025
Corrected Cone (ug/L ) : 42. 1
Pb ID: 13912u Seq. No.: 00044 A/S Pos. : 13 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.001
Background Pk Area <A-s): 0.028
Blank Corrected Pk Area CA-s): 0.000
Concentration (ug/L ) : 0.0
Time: 10:13
Peak Height (A) : 0. 004
Background Pk Height CA): 0.010
Corrected Cone (ug/L >: 0.0
Pb ID: 13912s Seq. No.: 00045 A/S Pos. : 14 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.052
Background Pk Area <A-s): 0.036
Blank Corrected Pk Area (A-s): 0.052
Concentration (ug/L ): 20.5
Time: 10: H,
Peak Height <A>: 0. 122
Background Pk Height CA): 0.030
Corrected Cone (ug/L > : 41. 0
Pb ID: 13913u Seq. No.: 00046 A/S Pos. : 15 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.053
Background Pk Area (A-s): 0.037
Blank Corrected Pk Area (A-s>: 0.053
Concentration (ug/L >: 20.8
Time: 10:19
Peak Height CA> : 0. 112
Background Pk Height CA): 0.029
Corrected Cone (ug/L ) : 41. 5
Pb ID: 13913s Seq. No.: 00047 A/S Pos. : 16 Date: 09/02/94
Replicate 1
Peak Area (A-s>: 0. 101
Background Pk Area (A-s>: 0.046
Blank Corrected Pk Area (A-s>: 0.101
Concentration (ug/L ): 41.5
Ti me: 10: 22
Peak Height CA): 0. 236
Background Pk Height CA>: 0.052
Corrected Cone (ug/L >: 82.9
Pb ID: 13914u Seq. No.: 00048 A/S Pas.: 17 Date: 09/02/94
Replicate
Peak Area
1
CA-s>: 0.002
Background Pk Area <A-s>: 0.034
Blank Corrected Pk Area (A-s):
Concentration (ug/L >: 0.6
0.002
Ti me: 10: 25
Peak Height CA): 0.006
Background Pk Height CA): 0.014
Corrected Cone (ug/L ) : 1. 2
Pb ID: 13914s Seq. No.: 00049 A/S Pos. : 18 Date: 09/02/94
Replicate 1
Pe~k Area <A-s): 0.052
Background Pk Area <A-s>: 0.045
Blank Corrected Pk Area <A-s): 0.051
Concentration (ug/L ): 20.3
Ti me: 10: 27
Peak Height <A>: 0. 119
Background Pk Height CA): 0.033
Corrected Cone (ug/L >: 40.5
Pb ID: 13915u Seq. No.: 00050 A/S Pos. : 19 Date: 09/02/94
Replicate 1
Peak Area CA-s>: 0.002
Background Pk Area (A-s): 0.035
Blank Corrected Pk Area CA-s>: 0.001
Concentration (ug/L ): 0.5
Ti me: 10: 30
Peak Height CA): 0.007
Background Pk Height CA): 0.012
Corrected Cone (ug/L ) : 1. 1
Pb ID: 13915s Seq. No. : 00051 A/S Pos.: 20 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.053
Background Pk Area (A-s>: 0.047
Blank Corrected Pk Area <A-s): 0.053
Concentration (ug/L ) : 20.8
Ti me: 10: 33
Peak Height CA) : 0. 140
Background Pk Height CA>: 0.038
Corrected Cone (ug/L ) : 41. 5
Pb ID : 139 16 l.l Seq. No.: 00052 A/S Pos.: 21 Date: 09/02/94
Replicate 1
Peak Area CA-s>: 0.002
Background Pk Area (A-s): 0.031
Blank Corrected Pk Area CA-s): 0.001
Concentration (ug/L ) : 0.5
Ti me: 10: 36
Peak Height CA): 0.007
Background Pk Height CA): 0.011
Corrected Cone (ug/L ) : 1. 0
Pb ID: 13916s Seq. No.: 00053 A/S Pas.: 22 Date: 09/02/94
Replicate 1
Peak Area CA-s>: 0.052
Background Pk Area <A-s>: 0.043
Blank Corrected Pk Area (A-s): 0.052
Concentration (ug/L ) : 20.5
Ti me: 10: 39
Peak Height CA): 0. 130
Background Pk Height (A): 0.034
Corrected Cone (ug/L ) : 41. 1
Pb ID: 13917u Seq. No.: 00054 A/S Pas.: 23 Date: 09/02/94
Replicate 1
Peak Area (A-s): 0.002
Background Pk Area (A-s): 0.033
Blank Corrected Pk Area <A-s): 0.002
Concentration (ug/L ): 0.7
Time: 10:41
Peak Height CA>: 0.006
Background Pk Height <A> : 0. 011
Corrected Cone (ug/L > : 1. 3
Pb ID: Lab QC Check Seq. No.: 00055 A/S Pos.: 3 Date: 09/02/94
Replicate
Peak Area
1
CA-s> 0.054
Ti me: 10: 44
Peak Height CA) 0. 144
Background Pk Area (A-s): 0.045
Blank Corrected Pk Area (A-s): 0.053
Concentration (ug/L ) : 21.0
QC,sample is within range 17.5 -22.5
Background Pk Height <A> 0.035
Pb ID: 13917s Seq. No.: 00056 A/S Pos.: 24 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.050
Background Pk Area <A-s): 0.044
Blank Corrected Pk Area (A-s): 0.050
Concentration (ug/L ) : 19.6
Time: 10:47
Peak Height (A): 0. 119
Background Pk Height (A): 0.033
Corrected Cone <ug/L ) : 39.2
Pb ID: 13918u Seq. No.: 00057 A/S Pas.: 25 Date: 09/02/94
Replicate 1
Peak Area <A-s>: 0.002
Background Pk Area (A-s): 0.034
Blank Corrected Pk Area <A-s): 0.001
Concentration (ug/L ): 0.5
Ti me: 10: 50
Peak Height <A>: 0.007
Background Pk Height (A): 0.011
Corrected Cone (ug/L ) : 1. 0
Pb ID: 13918s Seq. No.: 00058 A/S Pos. : 2tS Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.054
Background Pk Area <A-s>: 0.044
Blank Corrected Pk Area <A-s): 0.053
Concentration (ug/L ) : 21.0
Ti me: 10: 53
Peak Height <A>: 0. 129
Background Pk Height CA): 0.034
Corrected Cone (ug/L ): 41.9
Pb ID: Lab QC Check Seq. No.: 00059 A/S Pos.: 3 Date: 09/02/94
Replicate 1
Peak Area <A-s): 0.055
Background Pk Area (A-s): 0.045
Blank Corrected Pk Area (A-s): 0.054
Concentration (ug/L ): 21.4
QC sample is within range 17.5 -22.5
Ti me: 10: 56
Peak Height (A) : 0. 139
Background Pk Height (A): 0.035
'
I
F'E AA
0072
•
CRl
94/07/07
23:53:42
94/07/07
23:53:42
1*HDR
0009
0000000
#DATA
M.king
20
1. 0
O=g
1
l=uL
1.0E-6
4.5.0 ck,,
5,Blk,.2
6,spike •• 2
7 • 1390'=tu • • 2
8 • l 3909s • • 2
9. 1391 Ou• • 2
1 0, 1391 Os • • 2
11 • 139 ·; 1 I _I_ • • 2
l 2 • 139 l 1 s • , 2
13 • 13912u • • 2
14 • l 3912s • • 2
15 • 13913u • • 2
16 • 139 l 3s • , 2
1 7 • 13914u • , 2
18 , 13914s • , 2
1 9 • 13915u , , 2
20, 139 l 5s , , 2
21,13916u,,2
22 • 13916s • , 2
23 • 1391 7u, , 2
24,13917s,,2
25, 1391 Bu , , 2
26, 13918s , , 2
HGA IDWT ASCII 5100 F'C 7. 10
--.&,1-""t&O:.; .. _, ,_, _. --•-~•-• •-•---•-•--•-~ ., ·---•~••w•--•--••"''" • •• _.._••••--•• ••-~ ••--•-•• .. ·••---._ ... o.,.v,.. -•--'-• •-••• .-••• ., _ _,~,. -••·"" o,. •
f
Element File: CR3.GEL
Date: 07/08/94
Element: Cr
Time: 00:26
Wavelength: 357.9
Slit: 0.7 L
Data File:
Technique: HGA
ID/Wt File: CRl.IDW
Calib. Type: Nonlinear
Lamp Current: 24
Energy: 65
Remark 1: Ca(NO3)2 as modifier
Cr ID: Std Blk Seq. No . : 00001 A/S Pos.: 40 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.030
Background Pk Area (A-s): 0.005
Blank Corrected Pk Area (A-s): 0.030
Auto-zero performed.
Time: 00:26
Peak Height (A): 0.018
Background Pk Height (A): 0.015
Cr ID: Std 1 Seq. No.: 00002 A/S Pos.: 1 Date : 07/08/94
Replicate 1
Peak Area (A-s): 0.254
Background Pk Area (A-s): 0.010
Blank Corrected Pk Area (A-s): 0.223
Standard number 1 applied. [10.0]
Correlation coefficient: 1.00000
Time: 00:29
Peak Height (A): 0 .133
Background Pk Height (A): 0.012
Slope: 0 .0223
Cr ID: Std 2 Seq. No .: 00003 A/S Pos.: 2 Date : 07/08/94
Replicate 1
Peak Area (A-s): 0.694
Background Pk Area (A-s): 0.024
Blank Corrected Pk Area (A-s): 0.664
Concentration (ug/L ): 29.7
Standard number 2 applied. [30.0]
Correlation coefficient: 1.00000
Time: 00:32
Peak Height (A): 0.345
Background Pk Height (A): 0.016
Slope: 0.0224
Cr ID: Lab QC Check Seq. No. : 00004 A/S Pos.: 3 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.500
Background Pk Area (A-s): 0.017
Blank Corrected Pk Area (A-s): 0 .469
Concentration (ug/L ): 21.1
QC sample is within range 17.5 -22.5
Time: 00:35
Peak Height (A): 0.248
Background Pk Height (A): 0.011
Cr ID: 5.0 ck Seq. No. : 00005 A/S Pos.: 4 Date : 07/08/94
Replicate 1
Peak Area (A-s): 0.149
Background Pk Area (A-s): 0.000
Blank Corrected Pk Area (A-s): 0 .118
Concentration (ug/L ): 5 .3
Time: 00:38
Peak Height (A): 0 .070
Background Pk Height (A): 0.007
Cr ID: Blk Seq. No.: 00006 A/S Pos.: 5 Date: 07/08/94
Replicate 1
~eak Area (A-s): 0.024
Background Pk Area (A-s): -0.001
Blank Corrected Pk Area (A-s): -0.006
Concentration (ug/L ): -0.3
Time: 00:40
Peak Height (A): 0.013
Background Pk Height (A): 0.007
Corrected Cone (ug/L ): -0.5
Cr ID: spike Seq. No.: 00007 A/S Pos.: 6 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.509
Background Pk Area (A-s): 0.015
Blank Corrected Pk Area (A-s): 0.479
Concentration (ug/L ): 21.6
Time: 00:43
Peak Height (A): 0.251
Background Pk Height (A): 0.011
Corrected Cone (ug/L ): 43.1
Cr ID: 13909u Seq. No.: 00008 A/S Pos.: 7 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.040
Background Pk Area (A-s): 0.003
Blank Corrected Pk Area (A-s): 0.010
Concentration (ug/L ): 0.4
Time: 00:46
Peak Height (A): 0.022
Background Pk Height (A): 0.005
Corrected Cone (ug/L ): 0.8
Cr ID: 13909s Seq. No.: 00009 A/S Pos.: 8 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.532
Background Pk Area (A-s): 0.021
Blank Corrected Pk Area (A-s): 0.501
Concentration (ug/L ): 22.6
Time: 00:49
Peak Height (A): 0.252
Background Pk Height (A): 0.012
Corrected Cone (ug/L ): 45.2
Cr ID: 13910u Seq. No.: 00010 A/S Pos.: 9 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.036
Background Pk Area (A-s): 0.001
Blank Corrected Pk Area (A-s): 0.005
Concentration (ug/L ): 0.2
Time: 00:52
Peak Height (A): 0.018
Background Pk Height (A): 0.005
Corrected Cone (ug/L ): 0.5
Cr ID: 13910s Seq. No.: 00011 A/S Pos.: 10 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.516
Background Pk Area (A-s): 0.018
Blank Corrected Pk Area (A-s): 0.486
Concentration (ug/L ): 21.9
Time: 00:54
Peak Height (A): 0.242
Background Pk Height (A): 0.011
Corrected Cone (ug/L ): 43.7
Cr ID: 13911u Seq. No.: 00012 A/S Pos.: 11 Date: 07/08/94
Replicate 1 Time: 00:57
Peak Area (A-s): 0.028 Peak Height (A): 0.013
•-Background Pk Area (A-s): -0.002 Background Pk Height (A): 0.006
Blank Corrected Pk Area (A-s): -0.002
Concentration (ug/L ): -0.1 Corrected Cone (ug/L ): -0.2
Cr ID: 13911s Seq. No.: 00013 A/S Pos.: 12 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.518
Background Pk Area (A-s): 0.017
Blank Corrected Pk Area (A-s): 0.488
Concentration (ug/L ): 22.0
Time: 01:00
Peak Height (A): 0.258
Background Pk Height (A): 0.012
Corrected Cone (ug/L ): 43.9
Cr ID: 13912u Seq. No.: 00014 A/S Pos.: 13 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.027
Background Pk Area (A-s): -0.002
Blank Corrected Pk Area (A-s): -0.003
Concentration (ug/L ): -0.1
Time: 01:03
Peak Height (A): 0.014
Background Pk Height (A): 0.005
Corrected Cone (ug/L ): -0.3
Cr ID: 13912s Seq. No. : 00015 A/S Pos.: 14 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.518
Background Pk Area (A-s): 0.014
Blank Corrected Pk Area (A-s): 0.487
Concentration (ug/L ): 21.9
Time: 01:06
Peak Height (A): 0.253
Background Pk Height (A): 0.010
Corrected Cone (ug/L ): 43.9
Cr ID: 13913u Seq. No.: 00016 A/S Pos.: 15 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.141
Background Pk Area (A-s): 0.001
Blank Corrected Pk Area (A-s): 0.111
Concentration (ug/L ): 4.9
Time: 01:08
Peak Height (A): 0.066
Background Pk Height (A): 0.005
Corrected Cone ( ug/L ) : 9 . 9 < .1 • 0 f
Cr ID: 13913s Seq. No.: 00017 A/S Pos.: 16 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.627
Background Pk Area (A-s): 0.020
Blank Corrected Pk Area (A-s): 0.596
Concentration (ug/L ): 26.9
Time: 01:11
Peak Height (A): 0.303
Background Pk Height (A): 0.013
Corrected Cone (ug/L ): 53.8
Cr ID: 13914u Seq. No. : 00018 A/S Pos.: 17 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.043
Background Pk Area (A-s): 0.001
Blank Corrected Pk Area (A-s): 0.013
Concentration (ug/L ): 0.6
Time: 01: 14
Peak Height (A): 0.018
Background Pk Height (A): 0.006
Corrected Cone (ug/L ): 1.1
Cr ID: 13914s Seq. No.: 00019 A/S Pos.: 18 Date : 07/08/94
Replicate 1
•Peak Area (A-s): 0.536
Background Pk Area (A-s): 0 .023
Blank Corrected Pk Area (A-s): 0.505
Concentration (ug/-L ): 22 .8
Time: 01: 17
Peak Height (A): 0.261
Background Pk Height (A): 0.013
Corrected Cone (ug/L ): 45.5
Cr ID: 13915u Seq. No.: 00020 A/S Pos .: 19 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.036
Background Pk Area (A-s): -0.003
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 0.2
Time: 01:20
Peak Height (A): 0.016
Background Pk Height (A): 0.007
Corrected Cone (ug/L ): 0.5
Cr ID: 13915s Seq. No.: 00021 A/S Pos.: 20 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.522
Background Pk Area (A-s): 0.016
Blank Corrected Pk Area (A-s): 0 .492
Concentration (ug/L ): 22.2
Time: 01:22
Peak Height (A): 0.254
Background Pk Height (A): 0.012
Corrected Cone (ug/L ): 44.3
Cr ID: 13916u Seq. No.: 00022 A/S Pos.: 21 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.051
Background Pk Area (A-s): 0.000
Blank Corrected Pk Area (A-s): 0 .021
Concentration (ug/L ): 0.9
Time: 01:25
Peak Height (A): 0 .023
Background Pk Height (A): 0.004
Corrected Cone (ug/L ): 1 .9
Cr ID : 13916s Seq. No. : 00023 A/S Pos.: 22 Date : 07/08/94
Replicate 1
Peak Area (A-s): 0.549
Background Pk Area (A-s): 0 .016
Blank Corrected Pk Area (A-s): 0.518
Concentration (ug/L ): 23.4
Time: 01:28
Peak Height (A): 0 .268
Background Pk Height (A): 0 .012
Corrected Cone (ug/L ): 46 .7
Cr ID: 13917u Seq. No.: 00024 A/S Pos.: 23 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0 .037
Background Pk Area (A-s): -0.002
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ): 0.3
Time : 01:31
Peak Height (A): 0 .019
Background Pk Height (A): 0 .004
Corrected Cone (ug/L ): 0.5
Cr ID: Lab QC Check Seq. No.: 00025 A/S Pos.: 3 Date : 07/08/94
Replicate 1 Time: 01:34
Peak Area (A-s): 0.502 Peak Height (A): 0.244
·-
Background Pk Area (A-s): 0.015
Blank Corrected Pk Area (A-s): 0.471
Concentration (ug/L ): 21.2
QC sample is within range 17.5 -22.5
Background Pk Height (A): 0.011
-------------------------------------------------------------------------------
Cr ID: 13917s Seq. No. : 00026 A/S Pos.: 24 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.536
Background Pk Area (A-s): 0.019
Blank Corrected Pk Area (A-s): 0.506
Concentration (ug/L ): 22.8
Time: 01: 37
Peak Height (A): 0.256
Background Pk Height (A): 0.011
Corrected Cone (ug/L ): 45.6
Cr ID: 13918u Seq. No. : 00027 A/S Pos.: 25 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.044
Background Pk Area (A-s): -0.002
Blank Corrected Pk Area (A-s): 0.013
Concentration (ug/L ): 0.6
Time: 01:39
Peak Height (A): 0.018
Background Pk Height (A): 0.004
Corrected Cone (ug/L ): 1.2
--------------------------------------------------------------------~~----------
Cr ID: 13918s Seq. No.: 00028 A/S Pos.: 26 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.538
Background Pk Area (A-s): 0.019
Blank Corrected Pk Area (A-s): 0.508
Concentration (ug/L ): 22.9
Time: 01:42
Peak Height (A): 0.266
Background Pk Height (A): 0.013
Corrected Cone (ug/L ): 45.8
Cr ID: Lab QC Check Seq. No. : 00029 A/S Pos.: 3 Date: 07/08/94
Replicate 1
Peak Area (A-s): 0.526
Background Pk Area (A-s): 0.015
Blank Corrected Pk Area (A-s): 0.496
Concentration (ug/L ): 22.3
QC sample is within range 17.5 -22.5
Time: 01:45
Peak Height (A): 0.261
Background Pk Height (A): 0.011
,s-~rro -,7 l5'6"'3S-3q
JS'-f-OO -o'2... ,~<-i8'1 -o,J
Autosampler Worksheet
I 3qoq -ri s t.J
Worksheet Name: D1
Sample Description Fi le: Dai !y
3equence
Numbers
1
..I .-, -· c_
·I ,.:;_-
2 5
'-'
Autosampler
Position
4
s
7
::.1
9
25
.-,-, C. (
So lution
irJC-:=t -~
::; l a n i<
'3t. d -H\,; 1
QC-l-H•J 1
1531.6
15317
15400
15401
15402
1.548'3
15490
15491
15!S38
15538
15538
15539
13909 -sw
139:!.0 SW
13911 SW
13912 SW
13913 SW
13914 SW
13915 SW
13916 SW
13917 SW
13918· SW
E', l '.-< -rq,.,; 1
:Js-,~~·J 1
-D
-S spikeHW1
Anal y tical
Met h od Files
:3 .:;. ~ ..
7J --; _1,:;• ....
13 .. J. l
q -.. ,._-c::\ -
Data File:
Sa mple Description File:
An alytical Method F ile:
QC Summary Report
data 1. dat
Dai l ;1
E\.s t
GC Standard Time Element ID
i: 36 pm
·::, ., -:, -:,, _. _ _; :-!iii
2 : 2 '.:S p m
Units
iT1 g /) __
2:30 pm
Within
Limits?
Sample Summary Report #2
• Data File:
Sample Descript:on File :
~nalytical Method File:
153!.6
15317
15400
15401
15402
15489
15490
15491
Cor:c.
.,-,.,,··-; 7 ... _ .. ,'.•--· (
oatal .dat 09/0!/94
Daily ~1 /01 /1 4
Bal 2:30 pm
l.J,, it:;
,-_.., -· ' 11,:::;/ ,_
-, ..... ~ .
"':::J ' -
U,, J. ts
l. • .:n it=
:Jr,it:;
ilig/:_
;:J .i1
Sample Summary Report #2
Data F iJ.e :
Sa~ple De scr1 p ti a n F il e:
Anal ytical Method Fi le :
15533
i5538 D
!5538 ,-:·
1553<3
1.3909 SW
13910 SW
13912 SW
c:o nc .
,·-. --.......
-J ,.J 't'-.
1
: G i7 C .
·.'·t,'••--· •,·:.,-,_:,._,
D
data 1. dat
Ds.i ly
T"J --( .1.-•d;.
!_!n j.ts
,_ ..:: .L.. .·-.. ,, ;j
S -spil-<eHW1
-• _ I I
I;_~ J.. -\.,J I l -I_,':,
. ,_..: --_,l ..;. ,_. _:.
'j] g / '......
I 1..-.; ,I-.,_. :~. ! .... ~ .. ~
, _ ,-;,, 7
..._ .. '!'...·'
!t.~'3 / 0 l / c31+
\'.l":;l / :z· 1 / ') ::;.
2: 3~, pii1
Sample Summary Report #2
~ Data Fi l e:
Sample Description File:
Analytical Me t hod File:
13913 SW
Cone.
13914 SW
Cone:.
13915 SW
c:,J1;c: ..
3a45'.:AtZf3 0 . 000
1 3916 S W
Con,=.
82-455403 :21 . 000
13917 SW
Con e.
8 a '+SSL~1i3 0 . :zi,c:-'-..J
13918 SW
C,Jnc.
Ba4'.:J S4li'.l.3 ._, '.ll77 "-'•
dat a 1. dat
Daily
Bai
Units
!iii]/:...
Units
i !-. ; ---ii ~ J ::}
ITi g /~_
· . ..Jn i ·'.; :.:,
:n g /'._
Un i t s
mg /I -
Unit ·;
iiig1 " I-
2: l '3 prn
09 / 1211/9 4.
1,)g /:Zll /9 4
2:30 pm
ID/Weight File: HG2.IDW
Sa■ple Volu■e: 100 ■L
Loe. Sa■ple ID ---------------
9 . 00025
10 SW 13909
11 13910
12 13911
13 13912
14 13913
15 13914
16 13915
17 13916
18 13917
19 13918
20 13918 SPK
21 R 13947
22 13948
23 13949
24 13950
25 14038
26 14131
27 SW 14167
28 14168
29 14169
30 14170
31 14170 D
32 H 14215
33 R 14216
34 14217
35 14218
36 QC CHK
37 CER 13112 EXT
38 13113 EXT
39 13114 EXT
40 13115 XET
41 CER 11529 A
42 11529 -B
43 SW 10994 A
44 10994 B
45 CER 11957 A
46 11957 B
47 11958 A
48 11958 B
49 HW 11959'A
50 11959 B
51 1221& A
52 QC CHK
53 1221& B
54 12217 A
55 12217 B
56 128&2 A
57 128&2 B
58 128&3 A
59 128&3 B
&0 CER 13114 A
E, 1 1~114 '8
..
Analyst: ALJ
No ■inal Weight: 1. 0
Weight Dilution
--------------------
m. ere. v<.. r ';f--
/3Cf o1-tf'
uJ {?e,(!-
20
20
20
20
.2 100
.2 100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
1 OIOI
/1
g
?j<;t/ .aef
P"d
f~c~
tj}?o
DC::
Loe.
63
J.~J. J.;;J H
Sa■ple ID
13115 B
Weight Dilution
100
------------------------------------------·-----~----. ----~-----------~-----Ele■ent File: HG2.MEL
Date: 08/05/94
Ele ■ent: Hg
Ti ■ e: 10:57
Wavelength: 253.7
Slit: 0.70 L
Data Fi le:
Technique: MHS
ID/Wt File: HG2.IDW
Calib. Type: Linear
La■p Current: 5
Energy: 76
--------------------------------------------------------------------------. ----
Hg ID: Seq. 00001 Seq. No.: 00001 A/S Pos. : 1
Replicate 1 Ti ■e: 10:57
Peak Area CA-s): 0.010 Peak Height CA): 0.001
Blank Corrected Pk Height CA>: 0.001
Auto-zero perfor■ed.
Hg ID: STD BLK Seq. No. : 00002 A/S Pos. : 1
Replicate 1 Ti ■e: 10:59
Peak Area CA-s>: 0.00& Peak Height CA> : 0. 001
Blank Corrected Pk Height CA> : -0.000
Replicate 2 Ti ■e: 11:01
Peak Area CA-s): 0.005 Peak Height CA> : 0.001
Blank Corrected Pk Height CA>: -0.000
Mean Pk Height CA): -0.000 SD: 0.0000
Auto-zero perfor■ ed.
Hg ID: STD 1 Seq. No.: 00003 A/S Pos. : 2
Replicate 1 Ti ■e: 11 :03
Peak Area <A-s> : 0.050 Peak Height <A>: 0.009
Blank Corrected Pk Height <A> : 0.008
Replicate 2 Ti ■e: 11:04
Peak Area CA-s): 0.052 Peak Height CA) : 0. 009
Blank Corrected Pk Height CA) : 0.008
Mean Pk Height CA) : 0.008 SD: 0.0000
Standard nu■ber 1 applied. [0. 000500]
Correlation coefficient: 1.00000 Slope: 15.4494
Hg ID: STD 2 Seq. No.: 00004 A/S Pos.: 3
Replicate 1
Peak Area CA-s): 0.101
Blank Corrected Pk Height CA): 0.015
Concentration <■g/L >: 0.000994
Replicate 2
Peak Area CA-s): 0.100
Blank Corrected Pk Height CA>: 0.016
Concentration C ■g/L ): 0.00102&
Ti ■e: 11 :06
Peak Height CA): 0.017
Ti ■e: 11 :07
Peak Height <A>: 0.017
Date: 08/05/94
Date: 08/05/94
RSD<~>: 0.00
Date: 08/05/94
RSD<~>: 0.00
Date: 08/05/94
M Calibration -C:\AA USER\AA FILES\ELENENT\H62.NEL
8.11 55
Linear
Carr. Caef.: 8.99956
B.B
Slape: 16.4375
Cancentratian B.BB78BB
Hg ID: QC STD Seq. No.: 00008 A/S Pos.: 7
Replicate 1
Peak Area (A-s): -0.002
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ): 0.000018
Ti ■e: 11 :20
Peak Height (A): 0.002
QC sa■ple is out of range 0.00189 -0.00231
Hg ID: STD BLK Seq. No.: 00009 A/S Pos. : 1
Replicate 1
Peak Area (A-s): 0.001
Blank Corrected Pk Height (A): -0.000
Concentration <■g/L ): -0.00000&
Replicate 2
Peak Area <A-s): 0.002
Blank Corrected Pk Height (A): 0.000
Concentration <■g/L ) : 0.000000
Mean Cone (■g/L ): -0.000003
Auto-zero perfor■ed.
Ti ■ e: 11 :22
Peak Height (A): 0.001
Ti ■e: 11 :23
Peak Height (A): 0.001
SO: 0.0000043
Hg ID: STD 4 Seq. No.: 00010 A/S Pos.: 5
Replicate 1 Ti ■e: 11 :25
Peak Area (A-s): 0.520 Peak Height (A): 0.085
Blank Corrected Pk Height (A): 0.084
Date:
Date: 08/05/94
RSD ( ~ > : 141. 42
Date: 08/05/94
•
I
....f'~wµ,,_ .... M~~~-H,.,......,},..~__Dl,..DIOIC::J~.,.~~-·-----~---.-•--·-·-·----~··•.-------~-~---~--~-.. ----~~~-·-
Replicate 2
Peak Area (A-s): 0.522
Blank Corrected Pk Height <A>: 0.083
Concentration (■g/L ): 0.005063
Mean Cone (■g/L ): 0.005093
Reslope standard applied. (0.005000]
Ti ■e: 11 :26
Peak Height <A>: 0.084
SD: 0.0000432
Correlation coefficient: 0.99956 Slope: 16.4375
RSD<~>: 0.85
M Calibratian -C:\llA USER\llA FILES\ELENENT\H62.NEL
8,11
Ill -Cl 4=
Unear
Can-. Caef.: 8.99956
Sla e: 16,4375
B,B Canc1ntratian
Hg ID: QC STD Seq. No.: 00011 A/S Pos.: 7
Replicate 1
Peak Area <A-s): 0.202
Blank Corrected Pk Height <A>: 0.032
Concentration (■g/L ): 0.001908
Ti ■e: 11 :29
Peak Height (A): 0.033
QC sa■ple is within range 0.00189 -0.00231
Hg ID: • 00025 Seq. No.: 00012 A/S Pos.: 9
Replicate 1
Peak Area <A-s): 0.027
Blank Corrected Pk Height <A>: 0.004
Concentration (■g/L ): 0.000255
Replicate 1
Peak Area (A-s): -0.001
Ti ■e: 11:31
Peak Height (A): 0.006
Ti ■e: 11 :33
L-1 •
a.
Date: 08/05/94
Date: 08/05/94
S5
888
♦
I
Concentration (1g/L ) : -0.000003
Replicate 1
Peak Area (A-s): 0.010
Blank Corrected Pk Height CA): 0.000
Concentration (1g/L ): 0.000027
Ti ■e: 11 :35
Peak Height (A): 0.002
Replicate 1 Ti ■e: 11:37
Peak Area (A-s): 0.004 Peak Height (A): 0.001
Blank Corrected Pk Height <A>: -0.000
Concentration (■g/L ): -0.000003
Replicate 1
Peak Area (A-s): -0.001
Blank Corrected Pk Height (A>: 0.000
Concentration (1g/L ): 0.000009
Replicate 1
Peak Area <A-s): -0.001
Blank Corrected Pk Height (A): 0.000
Concentration (1g/L ): 0.000003
Replicate 1
Peak Area (A-s): 0.007
Blank Corrected Pk Height <A>: 0.000
Concentration (1g/L ): 0.000021
Replicate 1
Peak Area <A-s): 0.002
Ti ■e: 11 :38
Peak Height (A): 0.001
Ti ■e: 11 :40
Peak Height <A>: 0.001
Ti ■e: 11:42
Peak Height CA>: 0.002
Ti ■e: 11: 44
Peak Height (A): 0.001
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000009 ~~~~~~~~~~~~~~~~~~~+~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 13916 Seq. No.: 00020 A/S Pos.: 17 Date: 08/05/94
Replicate 1
Peak Area <A-s): 0.005
Blank Corrected Pk Height CA): 0.000
Concentration (1g/L ): 0.000009
Ti ■e: 11 :46
Peak Height CA>: 0.001
Replicate 1
Peak Area <A-s): -0.000
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000015
Ti ■e: 11 :48
Peak Height CA>: 0.002
Hg ID: QC STD Seq. No.: 00022 A/S Pos.: 7
Replicate 1
Peak Area <A-s): 0.202
Blank Corrected Pk Height <A>: 0.032
Concentration (■g/L ): 0.001932
Ti ■e: 11:50
Peak Height <A>: 0.034
QC sa■ple is within range 0.00189 -0.00231
Replicate 1
Peak Area <A-s): -0.003
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ): 0.000009
Replicate 1
Peak Area <A-s): 0. 196
Blank Corrected Pk Height CA): 0.031
Concentration <■g/L ): 0.001854
Ti ■e: 11: 52
Peak Height <A>: 0.001
Ti ■e: 11:54
Peak Height <A>: 0.032
Date: 08/05/94
~~~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: R 13947 ✓ Seq. No.: 00025 A/S Pos.: 21 Date: 08/05/94
Replicate 1
Peak Area <A-s): 0.009
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000009
Ti ■e: 11: 56
Peak Height CA): 0.001
Replicate 1 Ti ■e: 11:58
Peak Area <A-s): 0.003 Peak Height <A>: 0.002
Blank Corrected Pk Height (A>: 0.000
Concentration <■g/L ): 0.000021 ~~~~~~~~~~~~~~~~~~~~L~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 13949 ✓--Seq. No.: 00027 A/S Pos.: 23 Date: 08/05/94
Replicate 1
Peak Area <A-s): 0.003
Blank Corrected Pk Height CA): 0.000
Concentration (■g/L ): 0.000027
Ti ■e: 12:00
Peak Height CA): 0.002
~~~~~~~~~~~~~~~~~y~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ . . ~ '. Hg ID: 13950 Seq. No.: 00028 A/S Pos.: 24 Date: 08/05/94
Replicate 1 Ti ■e: 12:01
Peak Area <A-s): 0.002 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.000
Concentration <■g/L ): 0.000009
---------------~--------------------------------------------------------Hg ID: 14038 Seq. No.: 00029 A/S Pas.: 25 Date: 08/05/94
Replicate 1
Peak Area <A-s): 0.004
Blank Corrected Pk Height <A): 0.000
Concentration (■g/L ): 0.000021
Ti ■e: 12:03
Peak Height (A): 0.002
Hg ID: 14131 Seq. No.: 00030 A/S Pas. : 26
Replicate 1
Peak Area <A-s>: 0.002
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ): 0.000015
Ti ■e: 12:05
Peak Height <A>: 0.002
Replicate 1 Ti ■e: 12:07
Peak Area (A-s): -0.002 Peak Height <A>: 0.001
Blank Corrected Pk Height (A): 0.000
Date: 08/05/94
Concentration <■g/L ): 0.000003
------------~------------------------------------··--·-·-------····-Hg ID: 14168 Seq. No.: 00032 A/S Pas.: 28 Date: 08/05/94
Replicate 1
Peak Area <A-s): 0.003
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000027
Ti ■e: 12:09
Peak Height (A): 0.002
Hg ID: QC STD Seq. No.: 00033 A/S Pas.: 7
Replicate 1
Peak Area (A-s): 0.208
Blank Corrected Pk Height <A>: 0.032
Concentration <■g/L ): 0.001932
Ti ■e: 12:11
Peak Height (A): 0.034
QC sa■ple is within ran/0.00189 -0.00231
Date: 08/05/94
~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 14169 Seq. No.: 00034 A/S Pas.: 29 Date: 08/05/94
Replicate 1
Peak Area <A-s>: -0.005
Blank Corrected Pk Height <A>: -0.000
Concentration <■g/L ): -0.000003
Ti ■e: 12:13
Peak Height <A>: 0.001
..,,• ..,__,_ ...... -~••••-••.,•·--.-•••-., r-••--'••-• -••• ••• ••·' ..... •-~ • ••• '••••--" •••_., .,. •••• ••~• • o ·'-•••• ••••• ••--• • •••• ••••• __ ,..___, •• ,,.._, • ,___,,.,. •••"' •--•• • . ._, , ......... ,, •••• •-•~•--••i.--.... -.rJ,t,•.~ .......... J~,.i,•-... ,c.•_, .
ID/Weight File: AG.IDW
Sample Volume: 100 mL
Loe. Sample ID
/ 9 sw13909
10 sw13910
11 sw13911
12
13
14
15
sw13912
sw13913
sw13914
sw13915
16 sw13916
17 sw13917
18 sw13918
19 sw13918
5; l i1~~
11;q(}q-t?
\}JJ<e)-
Analyst: PJC
Nominal Weight: 1.0 g
Weight Dilution
\ \
5; ( {lcf-
o; f Y</
IJC--
/1tc~
/a1'a
Element File: AG1.FEL
Date: 09/02/94
Data File:
Technique: Flame
Ag ID: Seq. 00001
Absorbance: -0.325
Absorbance: -0.325
Absorbance: -0.325
Mean Absorbance:
Ag ID: STD BLK
Absorbance: -0.325
Absorbance: -0.325
Absorbance: -0.325
Mean Absorbance:
Auto-zero performed.
Ag ID: STD BLK
Absorbance: 0.000
Absorbance: 0.000
Absorbance: 0.000
Mean Absorbance:
Auto-zero performed.
Ag ID: std 1
Absorbance: 0.007
Absorbance: 0.007
Absorbance: 0.007
Mean Absorbance:
-121.325
-0.325
0.000
0.007
Element: Ag
Time: 11: 33
ID/Wt File: AG.IDW
Calib. Type: Nonlinear
Seq. No. : 00001 A/S Pas.: 0
Ti me: 11: 33
Time: 11: 33
Time: 11: 33
SD: 0.0002
Seq. No.: 00002 A/S Pas.: 0
Time: 11: 34
Time: 11: 34
Time: 11: 34
SD: 0.0000
Seq. No. : 00003 A/S Pas. : 1
Time: 11:35
Time: 11:35
Time: 11:35
SD: 0.0001
Seq. No.: 00004 A/S Pas. : 2
Time: 11:3tS
Time: 11:3tS
Ti me : 11 : 3tS
SD: 0.0001
Standard number 1 applied. [0.050]
Correlation coefficient: 1.00000 Slope: 0. 14tS3
Wavelength: 328. 1
Slit:0.70H
Lamp Current: 10
Energy: 67
Date: 09/02/94
RSD ('1-): 0. 0tS
Date: 09/02/94
RSD('1-) 0.01
Date: 09/02/94
RSD<'1-) 14.80
Date: 09/02/94
RSD('1-) 1. 41
Ag ID: std 2
Absorbance: 0.047
Concentration (mg/L
Absorbance: 0.047
Concentration (mg/L
Absorbance: 0.047
Concentration (mg/L
Mean Cone (mg/L ) :
Seq. No.: 00005 A/S Pos. : 3
Ti me: 11: 37
0.322
Ti me: 11: 37
0.322
Ti me: 11: 37
0.321
121.322 SD: 0.0001
Standard number 2 applied. [0. 300]
Correlation coefficient: 1.00000 Slope: 0. 1443
Ag ID: std 3
Absorbance: 0.078
Concentration (mg/L
Absorbance: 0.078
Concentration (mg/L
Absorbance: 0.078
Concentration (mg/L
Mean Cone (mg/L ) :
Seq. No. : 00006 A/S Pos. : 4
0.471
0.471
0.471
0.471
Time: 11: 38
Ti me: 11: 38
Ti me: 11: 38
SD: 0.0005
S-shaped calibration curve detected. 2-coef. equation used.
Standard number 3 applied. [0.500]
Correlation coefficient: 0.99956 Slope: 0. 1470
Ag ID: std 4
Absorbance: 0. 109
Concentration (mg/L
Absorbance: 0. 109
Concentration (mg/L
Absorbance: 0. 108
Concentration <mg/L
Mean Cone (mg/L ) :
Seq. No.: 00007 A/S Pos. : 5
Ti me: 11: 39
): 0.672
Ti me: 11: 39
0.675
Ti me: 11: 39
0. 672
0.673 SD: 0.0020
S-shaped calibration curve detected. 2-coef. equation used.
Standard number 4 applied. [0.700]
Correlation coefficient: 0.99966 Slope: 0. 1487
Ag ID: std 5
Absorbance: 0. 153
Co r~ t:Y' t:inn ( n/1
Seq. No.: 00008 A/S Pos. : 6
Ti me: 11: 40
Date: 09/02/94
RSD(1-) 0.04
Date: 09/02/94
RSD (,<.): 0. 10
Date: 09/02/94
RSD (";(.) : 0. 29
Date: 09/02/94
I
Absorbance: 0.153
Concentration (mg/L
Absorbance: 0. 153
Concentration (mg/L
Mean Cone (mg/L ) :
Ti me: 11: 40
0.954
Ti me: 11: 40
0.952
0.953 SD: 0.0010
S-shaped calibration curve detected. 2-coef. equation used.
Standard number 5 applied. [1. 000]
Correlation coefficient: 0.999&0 Slope: 0. 1509
Ag ID: Ag QC
Absorbance: 0.012
Concentration (mg/L
Absorbance: 0.012
Concentration (mg/L
Absorbance: 0.012
Concentration (mg/L
Mean Cone (mg/L ) :
Seq. No.: 00009 A/S Pos. : 7
Time: 11:41
0.080
Time: 11:41
0.078
Time: 11:41
0.078
0.079 SD: 0.0009
QC s ample is within range 0.0&8 0.084
Ag ID: sw13909
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Mean Cone (mg/L ) :
Ag ID: sw13910
Abs o rbance: -0.000
Concentration (mg/L
Abs o rbance: -0.000
Concentration (mg/L
Abs o rbance: -0.000
Concentration (mg/L
Mean Cone (mg/L ) :
On T n • c: i..1 1 -:;:Q 1 1
)
Seq. No. : 00010 A/S Pos.: 9
Time: 11:42
0.000
Time: 11:42
0.002
Time: 11:42
0.000
0.001 SD: 0.0011
Seq. No.: 00011 A/S Pos. : 10
Time: 11:43
-0.002
Time: 11:43
-0.002
Time: 11:43
-0.002
-0.002 SD: 0.0004
!=:on _ l'Jn_ e 12112112112
RSD('¼) 0. 10
Date: 09/02/94
RSD(i<.) 1. 17
Date: 09/02/94
RSD(i<.): 149.75
Date: 09/02/94
RSD (%): 21. 70
Abs1Jrbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Abs 1Jrbance: -0.001
Concentration (mg/L
Mean Cone (mg/L ) :
Ag ID: sw13912
Absorbanee: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone (mg/L ) :
Ag ID: sw13913
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone <mg/L ) :
Ag ID: sw13914
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.001
Concentration (mg/L
Mean Cone (mg/L ) :
Ag ID: sw13915
Absorbance: -0.001
Concentration (m □/L
Time: 11:44
-0.003
Time: 11:44
-0.003
Time: 11:44
-0.004
-0.003 SD: 0.0006 RSD (1-) : 21. 66
Seq. No.: 00013 A/S Pos. : 12 Date: 09/02/94
Time: 11:45
-0.002
Time: 11:45
-0.002
Time: 11:45
-0.001
-0.002 SD: 0.0005 RSD ( 1-> : 25.50
Seq. No.: 00014 A/S Pos. : 13 Date: 09/02/94
Time: 11:46
-0.003
Time: 11 : 4E-
-0.002
Time: 11 : 4E,
-0.003
-0.003 SD: 0.0005 RSD ( 1-> : 21 . 06
Seq. No. : 00015 A/S Po s. : 14 Date: 09/02/94
Time: 11:47
-0.002
Time: 11:47
-0.003
Time: 11 :47
-0.004
-0.003 SD: 0.0007 RSD (1-) : 23.96
Seq. No. : 00016 A/S Pas. : 15 Date: 09/02/94
Ti me: 11: 48
-0.004
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone (mg/L ) :
Ag ID: sw13916
Absorbance: -0.001
Conc entration (mg/L
Absorbance: -0.001
Concentration (mg/L
Absorbance: -0.001
Concentration (mg/L
Mean Cone Cmg/L ) :
Ag ID: sw13917
Absorbance: -0.000
Concentration Cmg/L
Absorbance: -0.000
Concentration Cmg/L
Absorbance: -0.001
Concentration Cmg/L
Mean Cone Cmg/L ) :
Ag ID: sw13918
Absorbance: -0.001
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone Cmg/L ) :
Ag ID: Ag QC
Absorbance: 0.012
Concentration Cmg/L
Abs orbance: 0.012
r l"'\.,.,.,....,l""I,...,,+.,-~+--. ,.,....,, I ... ..,. /I
)
\ .
Ti me: 11: 48
-0.001
Ti me: 11: 48
-0.002
-0.002 SD: 0.0016 RSD ('1■): 68. 22
Seq. No. : 00017 A/S Pos. : 16 Date: 09/02/94
Time: 11:49
-0.005
Time: 11:49
-0.004
Time: 11:49
-0.006
-0.005 SD: 0.0011 RSDC'1■): 23.35
Seq. No. : 00018 A/S Pas. : 17 Date: 09/02/94
Time: 11:50
-0.003
Time: 11:50
-0.003
Time: 11:50
-0.003
-0.003 SD: 0.0004 RSD < '1■ > : 13.27
Seq. No. : 00019 A/S Pos. : 18 Date: 09/02/94
Time: 11: 51
-0.004
Time: 11: 51
-0.002
Time: 11: 51
-0.002
-0.003 SD: 0.0010 RSD (;<.) : 39. 82
Seq. No. : 00020 A/S Po s. : 7 Date: 09/02/94
Time: 11:52
0.079
Time: 11:52
"' 1'11"7.0.
Absorbance: 0.012
Concentration (mg/L
Mean Cone (mg/L >:
0. 079
0.079
QC sample is within range 0.0&8
Ti me: 11: 52
SD: 0.0005 RSD < '¼ > : 0. & 7
0.084