NCD980602163_19940728_Warren County PCB Landfill_SERB C_Soil Analysis II-OCR

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'j\.'_.:. Dcp::irtmcr.t er Environment,
11t~I~• J:. 1'4flur-:..I ~c..s.ourccs
$.:)Ii~ .':./a,i!c. ;\{a.nagi:mc.nt Divisio!'
,i,) !
Site Number -----------------
P.O. Dox 2SO-l7. 306 1':. Wilmini;,on s,~ct
lulcigh, North Carolina 27611
Field Sample Number {,,u-L-<:5>0 2 -t.. C...,
Name of Si~c Wo\-R.i2E:J . .} Gor-YN PC.b l.nFL Site Location A F",o ~ NC -~-_:_.::::....:_c:::c..._ __ ;......;;:;c.._ ___________ _
Coilccted By G . f0 1 c H.~ \,, 6c>'l---l ID# 3-=t--Date Collected # ,l..'?, ::Jvc/ ~4 Time / S-oo c... s,e-'P+i e'H s. • TCLP Compounds Agency: Hazardous Waste X Solid Waste $upcrfu.nd ---------
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Sample T-Jpe Inorganic Compounds Resulls(mg/1) I
_K_ Arsenic <' o, Q ( i Environmental Con cen tra t e .Comments
_){_ Barium _o ... "-\ g.__ !
__ Ground water (1) X Solid (5) w~-r ~'"l> FILL-. ± Cadmium ~o.5 !
Chromium L.. o _ c5 I
__ Surface water (2) _ Liquid (6) ~..ur~ _2{_ Lead 0 .. 1~
tvl ,;-eO
L Mercury ...:..o.,c.1
Soil (3) _ Sludge (7) .:SP~tr ~ Selenium < D_.,.Qa.( --' Silver re-eo3 -~c:.. L..O.Q'::i
_ Other (4) _ Other (8) Co~ ro12. eco --
:r-c::::. -~o-z:. -LC --
--Organic Chemistry Inorganic Chemistry I --
F.irameter Results(mg/1) Parameter Results --(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS _x_ A.rsenic 'Q benzene I ----
--· Aci<l:B/N Ext. 1_ Barium J,3 carbon tetrachloride
I --'MTBE l Cadmium -L..9.'B chlordane ----Chloride chlorobenz.ene I -------I ~ Chromium ) a. chloroform ----I __ Copper o-cresol I ----Fluoride m-cresol ------
--Iron __ p-cresol --
--LLead 35 cresol --__ Manganese .. 1, 4-dichlorobenz.eoe ----
--L Mercury ~o-s3 --1,2-dich lorocthane
Nitrate -__ 1,1-dichlorocthylcne ----<I ..:£_ Selenium --2,4-dinitrotoluene
_x_ Silver ~5"'8 --hcptachlor
Radiochemistry Sulfates hexachlorobcnz.ene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------TOC __ pentachlorophenol --
----pyridine
Microbiology ----t etrachloroeth ylcne
----trichloroethylenc
Parameter Results (Col/lO0ml) 2,4 ,5-trich lorophenol --
----__ 2,4,6-trichlorophcnol
------\~ nyl chloride
cndrin --lindanc --Date Received Reported by --methoxychlor
--toxaphcne
Date Exlracled Date Repij13 2,4-0 --919 JUL 29 94 __ 2,4,5-TP (S il vex)
Date An alyzed Lab Number --1)1 IS 3l'JI (Rcvi~cd 2/91)
I lc~ith, l.:. ,,a1ural >-.cu.ivrccs
• Solid Waste /..fanai;cmcnl Di,~sion ... ~.
,,,Sile Number ------------------
J .v . lX • .J.X: ,J,.OV--41, .:,,..JO l''I. l""llflll;lLH.lrl -l\r-:.C.l
R.alcigh, North Carolina :76i ·
Field Sam pie Numbcr __ W _ _:_l_-_~_O_Z=---.5-_;:__r> ______ _
Name of Sile WA-1<;2.e:,-J GorvT'I PGt:, · l.nFL Site Location Ar=--,o >--J NC _.L..:._;__~::....:..=--~.:.,..:=------------
Collected By G _ (\J u:H.01,..6o~ ID# 3=?-Dale CoUected Zea -::J v Ly '14 Time It:> 5S'
/11. p,, 1,JX>e-~~
__ ,Superfllild TCLP Compounds Agency: Hazardous Waste Solid Waste ------
Sample Type Inorganic Compounds Rcsulls(mg/1.
EnYironmcntal ~ Concentrate Comments X Arsenic ('Q,O[
)( Barium o .. 38
__ Ground water (1) _ Solid (5) .::5'~V/A? G;(..) "/ __}C Cadmium ~c.o.5
_K_ Chromium 40.G!:)
__ Surface water (2) Liquid (6) Zk+,µ ~ 7r.::'eA.M. LLcad .L..a.\O --.
Sludge (7) hCHNec.k. ~££-"
_x:__ Mercury ~o.o\
_ Soil (3) )( Selenium ('l).004---1(. Silver ..L... O -Q ;:i
)S_ Other (4) --Other (8) .:SP~1, u,/ £e::.o --' re-&>~/-:SEX> --
--Organic Chemistry Inorganic Chemistry --
Par-a meter Resu I ts (mg/l) Parameter Resulls .... (mg/~) Organic Compounds Rcsul ts (mg/I)
P&T:GC/MS L Arsenic <a benzene ----Acid:B/N Ext. ')( Barium \ls carbon tetrachloride ------'MTBE .L Cadmium . ~9.-0 chlordane ----Chloride chlorobenzene --------L Chromium .L....<::\_8 chloroform --
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----
--_x_Lcad L... :,...o cresol --
--__ Manganese 1, 4-d ich l orobenzene --
--_K__ Mercury ""-o.o<=\ 1,2-dich loroethane --
--Nitrate.· __ 1,1-dichloroethylene --'K Selenium I 2,4-di nit rotoluene
T --Silver 4-C,_e, heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----Zinc hexachlorobutadiene ----Parameter Resulls (PCi/1) _pH • hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone.
Gross Bela TDS nitrobenzene ------TOC __ pentachlorophcnol --
----p)'ridine
Microbiology --__ letrachloroelhylene
--__ trichloroethylenc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-trichlorophenol ----vinyl chloride ----endrin --lind:rnc --Date Received Reported by --methoxychlor
__ toxaphene
Dale Extracted
Date R{jfJ§2Q JUL 29 94 2,.;-D --__ 2,4 ,5-TP (S il vex)
Date Amily,.cd Lab Number --Il l IS 31'JI (ltcviscd 2/91)
N.C. Dcpar:ment of Environment,
·, I lc«lh, & l',;atural Resources
Solid Waste Management Division
Site Number
SAMPLE A.t'\'A.LYSIS REQUEST State Labonitory of Public Health
· P.O. Oox 28047, 306 S. Wilmingion Street
Raleigh, North Carolina 27611
----------------Field Sam pie Number_-'W=--=-.....:L:;:,._-_o_o__;,l_-.....:S____::.!::> _____ _
Name of Site WA-R.i2.€:..J Gorv'T'i PG"'B U,FL Site Location A F'To ,._., NC -~-...:.....=c....:..::::::...._._,;,__:__-=. __________ _
ID# 3:f-Date Collected 2£, ::1V L. "I <2r '1-Time e:, 'BS:f-
L . £~&
Agency: Hazardous Waste X --Solid Waste __ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments L Arsenic < o. o I
'( Barium _o • .L4L-,
__ Ground water (1) _ Solid (5) LeAc...t11tTE P~t-,l''i:> L Cadmium L..c .Q5
\<A-VI >Je
_L Chromium L..o.o5
__ Surface water (2) Liquid (6) Di.,rt-E 7 £._Lead .C.. 0-\0
w IEe-o
_x_ Mercury LO~Q} £ Soil (3) _ Sludge (7) ~Pt-17" .L Selenium < O,oo...r
J _L Silver ,.z_o.o!:ia
_ Other (4) _ Other (8) rc-oo'3--$.S ----
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results--(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS L_ Arsenic ·<~ benzene ----
Acid:B/N Ext. )( Barium ee carbon tetrachloride ------MTBE ~ Cadmium .L..':L8 chlordane ----Chloride chlorobenzene ----~
~ Chromium \ 4' chloroform ----
--__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol ----_!__ Lead ~;;).O cresol --
--__ Manganese --1, 4-dichlorobenzene
--~ Mercury <.o .. o<=\ --1,2-d i ch I oroethane . Nitrate __ 1,1-dichloroethylene ----'I( Selenium I 2,4-dinitrotoluene --_!_Silver -"--9 .. 6 __ hepcachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parametl!r Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pcntachlorophcnol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichJorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by __ methoxychlor
__ toxaphene
Date Extractc<l Date RQorted 2,4-D
13921 JUL 29 94 --2,4,5-TP (Silvex)
Date Analyzed Lab Number --1)1 I.S Jl'JI (llcviscd 2/91)
\.
N.C. Dcpar.mcnt of Environment,
· I lc~ljh, & ;--.:a1ur2I Resources
.5o1;d Waste Manai;cmcnt Division
~f\..LVJ.I:L.L'.., 1'"1...i.'~J.V.lt.V '4"-"-\-l'-'L-.._,A -·--------
Site Number
P.Q, 13ox 2.son, 306 S. Wilmini;ion Street
Raleigh, Nor1h Carolina 276i l
-----------------Field Sample Number WL -~o ~-S:5
Name of Site WA-R.i2.e.J C1orJN Pe,"E, l.DFL Site Location A F"To 10 NC -.!.....:.--'...::::...:..::::c,_ _ __:_~::;...._-----------
ID# 3=/-Date Collected ;z_-:;,_ ;JUL-Y °r4 Time I~ 15
Hazardous Waste X Solid Waste Superfund TCLP Compounds Agency: ---------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments ~Arsenic < <?,i;~ l ,. Barium _0-~8
__ Ground water (1) _ Solid (5) WE!:>T' :tS~PE LX>FL L Cadmium .L_o.o5
_)(_ Chromium .L... o. o.S
__ Surface water (2) Liquid (6) ;5€£::P ~ Lead .L...o • \O
,c Mercury "'-o.c}
_.K. Soil (3) _ Sludge (7) ..L Selenium <a,.oor-
__L Silver .J....o,.c-5
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
:
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Parameter Results(mg/1) Parameter Results ..... (mg/kg) Organic Compounds Results(mg/1) I ! P&T:GC/MS )( Arsenic ·a benzene ----!
Acid:B /N Ext. x Barium Si carbon tetrachloride I ------i
'MTBE _L Cadmium .L_9.8 chlordane ' ----Chloride chlorobenzcne I ------__x_ Chromium \J._ chloroform ----
--__ Copper o-cresol --Fluoride m-cresol : ------i
--Iron p-cresol i ----I
-1L I..cad .J....:J..o cresol I
----'
--__ Manganese --1,4-dichlorobenzene
--~ Mercury ~ Q,. Q~ --1,2-dichloroethane
--Nitrate __ 1,1-dichlorocthylenc x Selenium /,i{ 2,4-dinilrotoluene --
~Silver -'-9 .. 6 __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobuladiene ----Parametl!r Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha __ Conductivity methyl ethyl ketone I
I --I
Gross Bela TDS nitrobenz.ene I ------TOC penlachlorophenol ----
----pyridine
Microbiology --__ tetrachloroethylene '
----lrichloroethylcnc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ! --
----__ 2,4,6-trichJorophenol
--__ vinyl chloride --cndrin --lindane --Date Received Reported by --mctho:>:ychlor
--toxaphenc
Dole Extracted
Dale Reljf~922 JUL 2994 2,4-0 --2,4,5-TP (Silvex)
Dole AnalyLed Lab Number --l)i IS 3l'Jl (ltcviscd 2/91}
N .. C Dr.par.ment of Environment,
llca~(h, & 1','atural Rc.:;ourccs
Solid Waste Management Division
SA.MPLE ANALYSIS REQlJEST State Labontory of Public Health
P.O. 13o, 2SO-l7, 306 N. Wilming,on Street
Raleigh, North Carolina 27611
,.
Site Number -----------------Field Sample Number U-JL. -oo, _ .SS ______ ...;;._ _ _;::_ ________ _
Name of Site WA-1<i2..t.J Gal'JTY PC."B l.DFL Site Location A F"101'J N (__ _..::.....;_ _ _;_;::....,_:::c___.....:......~:::...._-----------
Collected By G. f\) rcH.o\.,60.,.__, ID# 3-=f-Date Collected ;2.-:;.. JULY q4 Time /4-£;3
~ .s . SrePHEJJ
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments X Arsenic Cos!al
X Barium _0.10
__ Ground water (1) Solid (5) c;. t2. ID 14-3 x Cadmium L.o_ a5 x Chromium 4-o. D!S A112. IIEAJT
--
__ Surface water (2) Liguid (6) _K_ Lead 4-0.}0
..2£_ Mercury -Lo.a\
_½_ Soil (3) _ Sludge (7) ~LIT l.L-)Leco L Selenium <o.~a.s.-
~ Silver .L._ Cl ~ Q :5
_ Other (4) __ Other (8) -L c.-DOl-$S --
--
--Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Result:11 #)(-:ng/kg) Organic Compounds Results(mg/1)
P&T:GC/MS X Arsenic . < g__ benzene ----
Acid:B/N Ext. X Barium '"\:b,, carbon tetrachloride ------"MTBE L Cadmium .-(.'3.8 chlordane ----Chloride chlorobenzene ------
--· _K_ Chromium \~ chloroform --
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-crcsol ----
--..1:._Lcad .J..;J.D cresol --
--__ Manganese --1,4-dichlorobenzcne
--..£!._ Mercury '-0 .. 05 --1,2-dichlorocthanc
---Nitrate 1, 1-dichloroethylcne
T <t --Selenium 2,4-dinitrotolucnc
)C --Silver ...L...C\.8 heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadicnc ----Paramefl!r Results (PCi/1) pH hexachloroelhanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nit robcnzen e ------TOC pentachlorophenol ----
----pyridine
Microbiology ----tetr achloroethylcne
----trichloroethylenc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindanc --Date Received Reported by --methoxychlor
__ toxaphcne
Dale Extracted Date Re()orled 2,4-D
13923 JUL 29 94 --__ :?.,4,5-TP (Silvex)
Date AnalyLcd Lab Number --l)J IS 3!'Jl (ltcviscd 2/91)
'LAB o <?A-ToR.Y CHA/Al 0£ C VITO DY Re:ca R D
~PLE LABal2A:T1RY dlu&<lleR (s) ; /']q/9 ==> 177 ?,__]
~•LIDt .
:xTRAcre::vfo 1Cec:wo lJ Y ·
R~L~~ [2A TE.. ID IA F;, Fe R. I
{P//fy /t/y?cJ ~z: /,\ ; 10'.-5~ ~~-~ / I I 11:00 Alt~/5 . ·iJ.:. ... \\ ,, I ~' . ..5Q ~s1 e:e:oct:-:
,,;. q A I c a , Q 9:o-+.:..C: _,
.;.~ ..
?f_,~
• . .:.l =k~L dz.c;-/4~ {_L :oJ /Air -6-<,
0.,f/:sl.u'1~ :J :'{',r (;:,"2-fvv -I
1----~
·t AB o <? ATo(?.Y C HA{AJ a£ C UITO DY Re:ca f2 D
(4 ):2;:;vv e "--•
>AMPLE LABar2A-n,Ry d/UM 3lffR (s) :
DA:TE ID IA E3. i
8-3-9'( lj//:/0
'4,----------~ ;:----------
B:SrC-,M!Y!':::
HAZARDOUS WASTE METAL ANALYSIS
LABORATORY NUMBER:
TOTAL~
REMARKS:
:r~~tt=-
IJ9t9
EXTRACTABLE □
.SW
Ru ui.u
As
lppm)
s; Q_
(9 b .01 <0-005
?.o < o. o I
L.. o. 0 (
N.C. Dept. of Environment, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
0 .ooJ,-
HAZARDOUS WASTE METAL ANALYSIS
DATE: \\ B "f1 5 '-f
SAMPLE NAME: w 2:::"Y',,a-;t; ~ P<'., l B
LABORATORY NUMBER: _\;..;:0;:;;_',~\9.._-_d-.=--0.;;,__ _________ _
TOTAL □
REMARKS:
~ ti?smrf 5?,,st,,J
< 0 .0 t
t'
EXTRACTABLE Q--
Ruuft-6 ( ppm l
< D-O d.:>-
N.C . Dept . of Environment, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
HAZARDOUS WASTE METAL ANALYSIS
DATE : \ a,_ A u • 9 ;4 <S
SAMPLE NAME : (.J.,_) 9-0-0, &m1 ~ PS: I ~ .L 'F
LABORATORY NUMBER:
TOTAL □
REMARKS:
~
<9~
< {).C> I
EXTRACTABLE~
Ru ui.;t.t, I ppm l
< s .ooS-
N.C. Dept. of Environment, Health & Natural Resources
}068-C (Rev. 8/90) Laboratory Services
HAZARDOUS WASTE METAL ANALYSIS
DATE : \ ) g. .• ~ c., -4
SAMPLE NAME:_Y::J=-awn~D-2--a':::'.-=~>9>J=..__f?1,_.,_$,,.,.;;a;_§~--------
LABORATORY NUMBER:
TOTAL □
REMARKS:
135 )5 -
EXTRACTABLE~
~ Ru LJ.i.,u I ppm I
N.C. Dept. of Environ111ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
<o,O {
_,,,, _,.,,.
HAZARDOUS WASTE METAL ANALYSIS
DATE: --1\:hiQ..._R=--i·.c.t11;,1,&_-~..;.'"4'_.:..,. ____________ _
SAMPLE NAME: W 9::c:N:av >g. J.....F
LABORATORY NUMBER:
TOTAL □
REMARKS:
EXTRACTABLE~
~
Ao~
R~ui.,a, ( ppm l
N.C. Dept. of Envirolllllent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
-<o cO I
< O· 0 I
. ,···
-~ ._ ..... -
/
-~---___,___/_·_ ---·-~· ---·---··-----·------~-----
HAZARDOUS WASTE METAL ANALYSIS
DATE:
SAMPLE NAME: .... vJ~...;:jS\i,.;ODS~-a-,-~G~_'V,!::Gs;;;.,..1::2:c... ______ _
LABORATORY NUMBER:
TOTAL □
REMARKS:
fi -cs
o,,tf-2-
0,12-
<o.o5
EXTRACTABLE~
S...__,._J
Ruu.Lu (ppm)
o.38
<._ o, I 0
<o,o5
N.C. Dept. of Environ111ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
. . . . .
. . . . . . ·.. ,._ , , ~ .... ··-
HAZARDOUS WASTE METAL ANALYSIS
SAMPLE NAME: ½,,,)9>£>os co,, w 'fl Sa,?;,
LABORATORY NUMBER: \ ~°''""' '\ --~...;.~d"\ __ _:l-'3.;;;i..:S:l.::l...:=:::.:3:2.. _____ _
TOTAL □
REMARKS:
EXTRACTABLE~
Ruu.U.6 ( ppm I
<o.oE::"
<o,o5
<o. 10
N.C. Dept. of Environnient, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
HAZARDOUS WASTE METAL ANALYSIS
DATE: ½{ l(y q Cj'C( , I
SAMPLE NAME: C--i) ~ ...,..r c:. 1.-Ls;;,. L E
LABORATORY NUMBER: (:J 9 r9 ~ 1 J 9 -;;l .:J
TOTAL~
REMARKS:
EXTRACTABLE □
N.C. Dept. of Environment, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
<.o,o~-
<o.os-
·.,,/,.,,_ ·t•· .. .. . . .
~ f
.. .. . .. ·. '· .· · .. · -~'. ,. . . . . .
DA1
SAl-
LAE ~
T01 \ oa
Q,~
7 -oo
~
'b ~
N.C
306
7 .00
5 -cc
C\.oc,
: ,·· . .-..
·.· . ..:· ... ·.
HAZARDOUS WA~TE METAL ANALYSIS
DATE:
SAMPLE NAME:
LABORATORY NUMBER:
TOTAL~
REMARKS:
4-E
EXTRACTABLE □
5tJ
Ru u.i..u I ppm I
N.C. Dept. of Environ111ent, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
<o-/
_/
HAZARDOUS WASTE METAL ANALYSIS
.-·· "-.-·•:
DATE: --~lf--!-&,~1-9.L.C(:L--_____ _
SAMPLE NAME:_......;;.U~o~r~v~e~._,__==::._~~:::::::_:-:_~L~~/-:_ ___ _
LABORATORY NUMBER: (] '1 (7 ::::7 1 'J p .2 ;J
TOTAL a---EXTRACTABLE □
REMARKS:
-J SLJ
~~]}Ef Ru u.Lu ( ppm )
-zs.~ C J. C ..,_ --
I /9 0.12-<o.o5 o.o~
'Jo -o.og <_o.o5 <o,o5
(~( 0,'/-5 <::_o.o5 o,o~
( o. '-18 <_o,o5 0.06
J_, -
"'-
I d--] -0,37 <o.ot;; 0,08
N.C. Dept. of Environment, Health & Natural Resources
3068-C (Rev. 8/90) Laboratory Services
-6\J
<o,t>~
<0,05"
<0,05
<0,0.5"
<_o.o5
, .
L>....J ~ ~ 'Pc.. 5
-A~ ~
~
IOC \3<\ \9
ao
c~ ~
~ '-6
"'-i .. 87
('.!_,~
1 .DO
qAt::l
. . . . . ·····---· ··-·----····. -----·· ____ _... ______ _....._ ___ _ SOLID WASTE & SHELLFISH WORKSHEET
q (0 /(
~JL _____ 1_1<.....>,<.;.J'-4-----H--"'--'---'::..:......:.::+----jL-=<--=---'-t--
Tare+
Wet Sample
Dry Wt., I
Tota_l __ --------t----1----l---_J ___ __,__ ___ _.._ ___ +--___ _
Ashed Wt., I I
Total I I ___,;;;..;;....;;;..=-----+-----'-----1----;--------,-------'---·--+---~---+---
Tare Weight i i I
-------+----~----------t--------t--·----'------
0, S ( l O,S i !D~~t I Wet Sample
Dry Sample
Wei ht
Ashed Sample
Weight
ed.
C
Pf;
_(e-
I l !
( (),O (
,.d l
c:,,.o
ll<2
lo-....:+d I0~-'40
i 8 s · I C,l.1
10-37
' f-L-<O-C-5 1 l -4-9,S I
rzo-o.5 --l..o..oS j !""-o-a5
! -Z'7~ S ..L..9 -8 1 ! -<-~
!0-C>~ I I I I J__ I
[o-o(Q jo -O<Ja. l llo-os
l I j 1a.. i \(g 10-15 I I 3~ I <o-~<1
r-0-l ~=-1 I 1-<.o-I I
I .L...,)..Q i <.;;;..,c:, I -'-~O ! ----rt) ,OO_J __ -;-1---..,....1-()-.00-~ -'r--+-1 ---,t--1 <_D_.C)o_1-.-
~=-c.S I
1-L._~.e !
! I I I
1 1 i
l
l I I . ,. : ------...--------+----+----+----+----------'--------,--I.
~
l'L. 'J Ct re; i j9J J9 ~o;
I l3 1-1 ,4-!
l I t I I I !o.s-1 I o.~3 i 0,50 -~3 I 0 10,S-/ a.s-c;-io. I'-
I ' I ko_o i I
!~o-cS "'-.0-0':::i -'-.O-c <...e-oS -<..0-05 .l..Cl-C5
I l t
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.L..o_ o ~o ... c ::.-c:--I .L..O_Q "7 .L... -C".9 Lo_c
I I
..... ~ . -·. ·-·· ·---···----··•··•·-· ·-.. . ---·--···-···-··--·••······
LABa@AToRY CHAI.& oF CuITODY Re:caf2 D
>"AtuPLE LABaRtfn,Ry d/rwae=e (s) ; I~ 9/9 ) 11'7 :J.. :J
DA-TE /-0 .LA E:. Fa &
g/1J;i 7:30 adZi7d~~(/
__
1
_1_/_, ___ e_-....... ;:-=-d-__ ~Ad4r,f I a
~~:
'"I·• .l~,------------
•.;f_
. :-r-'1!""'l'·-=---..~ .. ~-. .... '•l ..... ,... : .·:, ~
. REG.t1l~ IV ~. · 'REGIO,N: IV
PROJ,. LEAD-ER: G~OVER NI CHON •. COMPANY l WARREN CTY
.,ACTIVITY,: ', SPILL ID:
PROJECT IO:
SITE NAHE: Warren County Landfill
CITY, STATE: Afton/War re n, NC
DATE SHIPPE D: 07/29/94 CARRIER:
AIRBILL:
~HIPPED TO: US-EPA . REGION IV LABORATORY
ENVIRONME~TAL SERVIC~S DIV
COLLEGE STATION ROAD
LAB
ATHENS, GA 30613-7799
ATTN: DEBBIE COLQUITT
?HONE: 404 /546 -Jili
SAMPLE ID STATION DESCRIPTI ON
WARREN CTY
CHAIN-OF-CUSTODY RECORD
NC Department of Environment Health & Natural Resources
Division of Solid Waste Management/Supertund Section
P.O. Box 27687 Raleigh, NC 27611-7687
Telephone [phone] Fax [phone]
United States Environmental Protection Agency .
Contract Laboratory Program Sample Management Office
PO Box 818 Alexandria, VA 22313
703-557-2490 FTS 557-2490
MATRIX OAT /TIH E AMPLE~
-------------------==================-======-==----------------------------------.-= WL-00 1-Gic GROUND ~ATER Gro und W3ter 07-Bi ll?~ . WALKER
( 1) \.il -,~
METALS(l) wL-001-LE LEACHATE Water
METALS( 1) WL-001-SS
( 1) ~L -64
SURFACE SOIL Soil !Sedise nt i7 -28/0ij37 L. R~S E
METAL5(1) WL-002-BL
(1) WL-34
Rinseate Ot her
~ETALS( 1)
( l) wL ~ 94
WL-002-GW GROUND IIATER Groun d ~ater 07 -28/i~35 T. WALKrn
METALS(lJ WL-002-L
(li Ill· '.0 3
LANDFILL CO NTENTS Waste 07 -28/1500 G. S7EPHENS
METALS( 1)
( : ) !.4L -83
WL-002-LE LEACHATE ~ater 07-28/1430 L. ROSE
HETALS( 1)
\.IL-002-SD
( 1) WL~. 69
SEDIMENT Sedi~ent 07 -28/1055 H. PO INDEXT
METALS( 1) ~L-003-SL
. ( 1) WL -S•
Post Pre~!r1a tive 2lank
~ETALSI i) '..IL -001:,;1,1
( 1 1 Ill -9t
GROU ND :.IATER Sr0und Water 07-28 11600 L. ROSE
11ETALS ( 1) \JL-004-SL
( l ) WL -90
Air Hose Rinseat~ 3lank Oth~r
MEiALS( l) WL-004-SW
( 1) WL · 9q
GROUND \JAT~R Gr~und Water 07 -23/\400 !. ~ALKER
METALS( 1) t.iL-005-6\.1
i , 1 WL -7 4
GROUND ~ATER ~round ~a ter 07-28/1400 !. WALKER
MET~LS( 1) ( 1; WL -79
FORM NO. 01077
·• A'"?-'-s_•.......-,... t ...,,. -•
REGIOW:'vV REGION: IV
1 PROJ. LEAIER: GROVER NICHON COMPANY: WARREN CTY
QITIVITY: ', SPILL ID:
PROJECT ID :
SITE NAME: Warre n Count y La ndfill
CITY, STATE: Af ton/War ren , NC
DATE SHIPP ED: 07/29/Q4 CARRIER:
AIRBILL :
~HI0PED TC : US-E?4. REGIO N IV l~BOR ATORY
LAB
ENVIRONMENTAL SERVI CES DI~
COLL~GE STATION ROAD
~THENS, GA 30613-7799
ATTN: DEBBIE COLQUITT
?HGNE: 404/546-3111
~MMPLE iD SiAT !ON DESCRIPT:~N
WL-005-S~
~ETALS(:) WL-006-SS
METALS( I )
~URFACE SOI L
{ ! ) wL -19
SURF~CE ~O IL
(:) ~L -5
white -LAB Ccov for ~etur ~ :o S3 mole r~
WARREN CTY
CHAIN-OF-CUSTODY RECORD
NC Department of Environment Health & Nalllral Resources
Division of Solid Waste Management/Supertund Section
P.O. Box 27687 Raleigh, NC 27611-7687
Telephone [phone] Fax [phone]
MATR!X
~0 il /Sefraent.
'· ,:._1.:=: --::;.t..:. .c....,... . '~ .\. -----------
United States Environmental Protection Agency
Contract Laboratory Program Sample Management Office
PO Box 818 Alexandria, VA 22313
703-557-2490 FTS 557-2490
c..,:: .. ~7 '--'.:".c .,--:·1 ~ . .:.:,_,\
FORMNO. ---01084
:•E AA
ll072
3E1
~4/08/30
l2:22:07
~4/08/30
l2:22:07
~-King
fl:HDR
ll009
Zl000000
itDATA
~.King
:'.0
1. 0
Zl=g
1
1=1.tL
1. 0E-6
!t,5.0 ck,,
5, Blk,,
::-, Spike,,
7, 14172u,, 2
3, 14172s,, 2
~, 14173u,, 2
10, 14173s,, 2
11,14174u,,2
12, 14174s,, 2
13, 14175u,,2
HGA
14, 14175s,, 2
15,tot 13643u,,2
16, 13643s,, 2
17, 13644u,,2
18, 13644s,, 2
19, 136451.1,,2
::0, 13645s,, 2
21, 13646u,,2
::2, 13646s,, 2
23, 13647u,,2
::4, 13647s,, 2
::5, 13735u,, 2
::6, 13735s,, 2
::7, 13919u,, 2
::8, 139 1 9 s, , 2
::9, 139201.1,, 2
30, 13920s,,2
31, 139211.1,, 2
32, 13921s,, 2
33, 139221.1,, 2
34, 13922s,, 2
35, 13923u,, 2
36, 13923s,, 2
IDWT ASCII 5100 PC 7. 10
~lement File: SE1.GEL
Date: 08/30/94
Element: Se
Time: 12:49
Wavelength: 196.0
Slit: 2.0 L
Data Fi 1 e:
Technique: HGA
ID/Wt Fi le: SEL IDW
Calib. Type: Nonlinear
Lamp Current: 0
Energy: 55
:le ID: Std. Bl k Seq. No.: 00001 A/S Pos.: 40
Replicate 1
::ieak Area (A-s): -0.001
Background Pk Area <A-s): 0.004
Blank Corrected Pk Area (A-s): -0.001
~uto-zero performed.
Time: 12:49
Peak Height <A>: 0.011
Background Pk Height <A>
:le ID: Std 1 Seq. No. : 00002 A/S Pas. : 1
~eplicate 1
='eak Area <A-s): 0. 001
Background Pk Area (A-s): -0.001
Blank Corrected Pk Area <A-s): 0.003
Time: '12:52
Peak Height <A>: 0.12111
Background Pk Height <A>
~xpansion }100 is not allowed. No calibration has occurred.
Date: 08/30/94
0.010
Date: 08/30/94
0.009
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
3e ID: Std. Blk Seq. No.: 00004 A/S Pos.: 40 Date: 08/30/94
~eplicate 1
::ieak Area (A-s): 0.001
Background Pk Area (A-s): 0.023
Blank Corrected Pk Area <A-s): 0.002
~uto-zero performed.
Ti me: 12: 58
Peak Height (A): 0.011
Background Pk Height (A) 0.022
3e ID: Std 1 Seq. No.: 00005 A/S Pas. : 1 Date: 08/30/94
~epl icat e 1
::ieak Area <A-s): 0.052
Background Pk Area (A-s): 0.038
Blank Corrected Pk Area <A-s): 0.051
3tandard number 1 applied. [30.0]
:orrelation coefficient: 1.00000
Time: 13:01
Peak Height <A>: 0. 059
Background Pk Height (A): 0.021
Slope: 0.0017
:le ID: Std 2 Seq. No.: 00006 A/S Pas.: 2 Date: 08/30/94
~eplicate 1
::ieak Area (A-s): 0.090
Background Pk Area (A-s): 0.042
Blank Corrected Pk Area <A-s): 0.089
:ancentration (ug/L ) : 52. 1
3tandard number 2 applied. [50.0]
:arrelation coefficient: 1.00000
Ti me: 13: 03
Peak Height <A>: 0.098
Background Pk Height <A>: 0.021
Slope: 0.0016
3e ID: Lab QC Check Seq. No.: 00007 A/S Pas.: 3
Replicate 1
Peak Area (A-s): 0.020
Background Pk Area <A-s)
Blank Corrected Pk Area
Concentration (ug/L ) :
0.027
< A-s) : 0. 019
11. 7
QC sample is within range 7.5 -12.5
Ti me: 13: 05
Peak Height (A): 0.025
Background Pk Height (A)
Se ID: 5.0 ck Seq. No.: 00008 A/S Pas.: 4
Replicate 1
Peak Area (A-s) 0.012
Background Pk Area (A-s>: 0.02&
Blank Corrected Pk Area (A-s): 0.011
Concentration (ug/L ) : 6.4
Ti me: 13: 08
Peak Height <A>: 0.017
Background Pk Height (A)
Se ID: Blk Seq. No.: 00009 A/S Pas.: 5
Replicate 1
Peak Area <A-s): 0.001
Background Pk Area <A-s) 0.023
Blank Corrected Pk Area <A-s): 0.000
Concentration (ug/L ): 0.0
Time: 13:10
Peak Height <A>: 0. 010
Background Pk Height (A)
Se ID: Spike Seq. No.: 00010 A/S Pas.: 6
Replicate 1
Peak Area <A-s): 0.035
Background Pk Area <A-s)
Blank Corrected Pk Area
Concentration (ug/L ) :
0.027
<A-s) : 0. 034
20.2
Time: 13:12
Peak Height <A>: 0. 044
Background Pk Height <A>
Se ID: 14172u Seq. No. : 00011 A/S Pos.: 7
Replicate 1
Peak Area (A-s) -0.001
Background Pk Area (A-s) 0.088
Time: 13:15
Peak Height (A): 0. 010
Background Pk Height <A>
Date: 08/30/94
0.019
Date: 08/30/94
0.019
Date: 08/30/94
0.019
Date: 08/30/94
0.017
Date: 08/30/94
0. 175
Blank Corrected Pk Area (A-s): -0.002
Concentration (ug/L ): -1.4 Corrected Cone (ug/L >: -2.7
Se ID: 14172s
Replicate 1
Peak Area <A-s): 0.030
Seq. No.: 00012 A/S Pos.: 8
Time: 13:17
Peak Height (A): 0.037
Background Pk Height <A>
Date: 08/30/94
0. 166 Background Pk Area <A-s> 0.09&
Blank Corrected Pk Area (A-s): 0.029
Concentration (ug/L ) : 17.3 Corrected Cone (ug/L ) : 34.6
' ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Se ID: 14173u Seq. No.: 00013 A/S Pos. : 9 Date: 08/30/94
Replicate 1
Peak Area <A-s>: -0.002
Background Pk Area <A-s): 0.105
Blank Corrected Pk Area (A-s>: -0.003
Concentration (ug/L ) : -2.0
Time: 13:19
Peak Height <A> : 0. 010
Background Pk Height <A>: 0. 191
Corrected Cone (ug/L ): -3.9
Se ID: 14173s Seq. No. : 00014 A/S Pas. : 10 Date: 08/30/94
Replicate 1
Peak Area <A-s): 0.031
Background Pk Area <A-s): 0. 113
Blank Corrected Pk Area (A-s>: 0.031
Concentration (ug/L ): 18.2
Ti me: 13: 22
Peak Height <A>: 0.040
Background Pk Height (A): 0. 174
Corrected Cone (ug/L > : 36. 4
Se ID: 14174u Seq. No.: 00015 A/S Pas. : 11 Date: 08/30/94
Replicate 1
Peak Area (A-s): 0.000
Background Pk Area <A-s): 0.108
Blank Corrected Pk Area (A-s>: -0.001
Concentration (ug/L ) : -0.5
Time: 13: 24
Peak Height <A>: 0.010
Background Pk Height <A>: 0.176
Corrected Cone (ug/L ) : -0.9
Se ID: 14174s Seq. No. : 00016 A/S Pas. : 12 Date: 08/30/94
Replicate 1
Peak Area (A-s): 0.029
Background Pk Area (A-s): 0. 105
Blank Corrected Pk Area (A-s>: 0.028
Concentration (ug/L ): 16.7
Ti me: 13: 27
Peak Height <A) : 0. 044
Background Pk Height (A): 0. 165
Corrected Cone (ug/L ) • 77 C"' • ,_,...,. ,_J
Se ID: 14175u Seq. No.: 00017 A/S Pos.: 13 Date: 08/30/94
Replicate 1
Peak Area (A-s): -0.006
Background Pk Area (A-s): 0. 103
Blank Corrected Pk Area <A-s): -0.007
Concentration (ug/L >: -4.5
Ti me: 13: 29
Peak Height (A): 0.009
Background Pk Height <A>: 0. 168
Corrected Cone (ug/L ) : -8.9
Se ID: 14175s Seq. No.: 00018 A/S Pas.: 14 Date: 08/30/94
Replicate 1
Peak Area <A-s>: 0.030
Background Pk Area <A-s>: 0. 103
Blank Corrected Pk Area (A-s): 0.029
Concentration (ug/L ) : 17.4
Time: 13:31
Peak Height <A>: 0.036
Background Pk Height (A): 0. 170
Corrected Cone (ug/L >: 34.7
Se ID: tot 13643u Seq. No.: 00019 A/S Pos. : 15 Date: 08/30/94
Replicate 1
Peak Area (A-s>: 0.005
Background Pk Area <A-s>: 0.034
Blank Corrected Pk Area (A-s>: 0.004
Concentration (ug/L ) : 2.7
Ti me: 13: 34
Peak Height <A>: 0.011
Background Pk Height (A): 0.021
Corrected Cone (ug/L > : 5. 3
ID: 13643s Seq. No.: 00020 A/S Pas. : 16
~pl icat e 1
~ak Area (A-s) 0.040
1ckground Pk Area (A-s>: 0.040
lank Corrected Pk Area <A-s): 0.039
)ncentration (ug/L ) : 22.8
Ti me: 13: 36
Peak Height CA): 0.052
Background Pk Height <A>
Corrected Cone (ug/L ) :
ID: 13644u Seq. No. : 00021 A/S Pas.: 17
eplicate 1
eak Area (A-s): 0.004
ackground Pk Area <A-s): 0.030
Ti me: 13: 38
Peak Height (A) : 0. 011
Background Pk Height <A>
Date: 08/30/94
0.021
45.6
Date: 08/30/94
0.019
lank Corrected Pk Area (A-s): 0.003
oncentration (ug/L ) : 1.6 Corrected Cone (ug/L ): 3.3
e ID: 13644s Seq. No.: 00022 A/S Pas. : 18 Date: 08/30/94
Time: 13:41 eplicate 1
eak Area (A-s) 0.040
ackground Pk Area (A-s): 0.033
Peak Height <A>: 0.049
Background Pk Height <A>: 0.019
lank Corrected Pk Area (A-s): 0.039
oncentration (ug/L ) : 23.0 Corrected Cone (ug/L ) : 45.9
e ID: 13645u Seq. No.: 00023 A/S Pas.: 19
eplicate 1
eak Area (A-s): 0.006
ackground Pk Area (A-s): 0.037
lank Corrected Pk Area <A-s>: 0.005
oncentration (ug/L ): 3.2
Ti me: 13: 43
Peak Height (A): 0. 015
Background Pk Height (A)
Corrected Cone (ug/L ) :
e ID: 13645s Seq. No.: 00024 A/S Pos.: 20
eplicate
eak Area
1
<A-s> 0.039
ackground Pk Area (A-s): 0.043
lank Corrected Pk Area <A-s): 0.038
oncentration <ug/L ) : 22.7
Time: 13:45
Peak Height <A>: 0.054
Background Pk Height CA)
Corrected Cone (ug/L ) :
e ID: 13646u Seq. No.: 00025 A/S Pas. : 21
eplicate 1
eak Area <A-s): 0.003
ackground Pk Area (A-s)
lank Corrected Pk Area
oncentration (ug/L ) :
e ID: 13646s
eolicate 1
0.031
<A-s): 0.002
1. 3
Ti me: 13: 48
Peak Height (A) : 0. 012
Background Pk Height <A>
Corrected Cone (ug/L ) :
Seq. No.: 00026 A/S Pas.: 22
Time: 13: 50
Date: 08/30/94
0.028
6.4
Date: 08/30/94
0.024
45.4
Date: 08/30/94
0.020
2.7
Date: 08/30/94
3ackground Pk Area <A-s): 0.035
3lank Corrected Pk Area <A-s): 0.042
:oncentration (ug/L ) : 25.0
Background Pk Height (A): 0.019
Corrected Cone (ug/L ) : 50.0
:le ID: 13647•.t Seq. No.: 00027 A/S Pos.: 23 Date: 08/30/94
~eplicate 1
'eak Area <A-s): 0.003
3ackground Pk Area <A-s): 0.030
3lank Corrected Pk Area <A-s): 0.002
:oncentrat ion < ug/L ) : 1. 5
Time: 13:53
Peak Height <A>: 0. 012
Background Pk Height <A>: 0.019
Corrected Cone (ug/L > : 3. 0
:le ID: Lab QC Check Seq. No.: 00028 A/S Pos.: 3 Date: 08/30/94
~eplicat e 1
=•eak Area <A-s) : 0. 019
3ackground Pk Area <A-s): 0.026
3lank Corrected Pk Area (A-s): 0.018
:oncentration (ug/L ) : 11. 0
~C sample is within range 7.5 -12.5
Ti me: 13: 55
Pe a k He i g ht (A) : 0. 02 3
Background Pk Height (A) 0.019
3e ID: 13647s Seq. No.: 00029 A/S Pas.: 24 Date: 08/30/94
~eplicate 1
leak Area (A-s): 0.042
3ackground Pk Area <A-s): 0.035
3lank Corrected Pk Area <A-s): 0.041
:oncentration (ug/L ) : 24.0
Ti me: 13: 57
Peak Height <A>: 0.053
Background Pk Height <A>: 0.019
Corrected Cone (ug/L > : 48. 1
:le ID: 13735u Seq. No.: 00030 A/S Pos.: 25 Date: 08/30/94
~eplicate 1
leak Area <A-s): 0.004
3ackground Pk Area <A-s): 0.036
3lank Corrected Pk Area <A-s): 0.003
:oncentration (ug/L ): 1.8
Ti me: 14: 00
Peak Height (A): 0. 014
Background Pk Height <A>: 0.024
Corrected Cone (ug/L ) : 3. E,
3e ID: 13735s Seq. No. : 00031 A/S Pas.: 26 Date: 08/30/94
~eplicate 1
'eak Area <A-s): 0.042
3ackground Pk Area <A-s): 0.042
3lank Corrected Pk Area (A-s): 0.041
:oncent ration ( ug /L ) : 24. 3
Ti me: 14: 02
Peak Height CA): 0.053
Background Pk Height CA): 0.023
Corrected Cone (ug/L >: 48.7
:le ID: 13919u Seq. No.: 00032 A/S Pos.: 27 Date: 08/30/94
~epl icat e 1
leak Area (A-s): 0.005
3ackground Pk Area (A-s): 0.041
3lank Corrected Pk Area <A-s): 0.004
:oncentration (ug/L ): 2.4
Ti me: 14: 05
Peak Height <A>: 0. 014
Background Pk Height (A): 0.025
Corrected Cone (ug/L > : 4. 7
Se ID: 13919 s Seq. No.: 00033 A/S Pos.: 2B Date: 0B/30/94
Replicate 1
Peak Area (A-s> 0.041
Background Pk Area <A-s): 0.046
Blank Corrected Pk Area <A-s>: 0.040
Concentration (ug/L ): 23.5
Ti me: 14: 07
Peak Height <A>: 0.052
Background Pk Height <A>: 0.024
Corrected Cone (ug/L ): 47.0
Se ID: 13920u Seq. No.: 00034 A/S Pos. : 29 Date: 08/30/94
Replicate 1
Peak Area <A-s>: 0.007
Background Pk Area <A-s): 0.032
Blank Corrected Pk Area (A-s): 0.006
Concentration (ug/L ) : 3.7
Ti me: 14: 09
Peak Height <A>: 0. 016
Background Pk Height (A) 121.022
Corrected Cone (ug/L > : 7. 4
Se ID: 13920s Seq. No.: 00035 A/S Pos.: 30 Date: 0B/30/94
Replicate 1
Peak Area <A-s): 0.043
Background Pk Area <A-s>: 0.041
Blank Corrected Pk Area <A-s) 0.042
Concentration (ug/L >: 24.7
Time: 14:12
Peak Height <A>: 0.049
Background Pk Height (A)
Corrected Cone (ug/L ) :
0.022
49.3
Se ID: 13921u Seq. No.: 00036 A/S Pos. : 31 Date: 08/30/94
Replicate 1
Peak Area <A-s>: 0.005
Background Pk Area (A-s)
Blank Corrected Pk Area
Concentration (ug/L ) :
0.056
<A-s > : 0. 004
2.7
Time: 14:14
Peak Height CA): 0.012
Background Pk Height CA): 0.032
Corrected Cone Cug/L ) : 5. 5
Se ID: 13921s Seq. No.: 00037 A/S Pos.: 32 Date: 08/30/94
Replicate 1
Peak Area (A-s) 0.036
Background Pk Area <A-s) 0.066
Blank Corrected Pk Area CA-s): 0.035
Concentration Cug/L >: 20.8
Time: 14:17
Peak Height <A> : 0. 049
Background Pk Height CA) 0.032
Corrected Cone Cug/L >: 41. 7
Se ID: 13922u Seq. No.: 00038 A/S Pos.: 33 Date: 08/30/94
Replicate 1
Peak Area CA-s): 0.007
Background Pk Area CA-s): 0.064
Blank Corrected Pk Area CA-s): 0.006
Concentration Cug/L ): 3.8
Time: 14:19
Peak Height CA> : 0. 012
Background Pk Height <A> 0.032
Corrected Cone Cug/L > : 7. 6
Se ID: 13922s Seq. No.: 00039 A/S Pos.: 34 Date: 08/30/94
Replicate 1 Time: 14:21
Pe k . Ctl-c. • _q D M ·o t -<A~:-0.050 '"I
Background Pk Area <A-s): 0.069
Blank Corrected Pk Area <A-s): 0.038
Concentration (ug/L ) : 22.4
Background Pk Height (A): 0.032
Corrected Cone (ug/L ): 44.8
Se ID: 13923u Seq. No.: 00040 A/S Pos.: 35 Date: 08/30/94
Replicate 1
Peak Area <A-s): 0.003
Background Pk Area CA-s): 0.054
Blank Corrected Pk Area CA-s>: 0.002
Concentration <ug/L ) : 1. 1
Time: 14: 24
Peak Height <A>: 0.011
Background Pk Height CA): 0.029
Corrected Cone Cug/L > : 2. 1
Se ID: 13923s Seq. No.: 00041 A/S Pos.: 36 Date: 08/30/94
Replicate 1
Peak Area <A-s): 0.043
Background Pk Area <A-s): 0.057
Blank Corrected Pk Area (A-s): 0.042
Concentration (ug/L >: 24.8
Time: 14: 26
Peak Height <A> : 0. 051
Background Pk Height (A): 0.030
Corrected Cone (ug/L ): 49.6
Se ID: Lab QC Check Seq. No.: 00042 A/S Pos.: 3 Date: 08/30/94
Replicate 1
Peak Area <A-s>: 0.017
Background Pk Area CA-s): 0.030
Blank Corrected Pk Area CA-s): 0.016
Concentration (ug/L ): 9.9
QC sample is within range 7.5 -12.5
Time: 14:28
Peak Height CA) : 0. 023
Background Pk Height (A): 0.020
Se ID: Lab QC Check Seq. No.: 00043 A/S Pas.: 3 Date: 08/30/94
Replicate 1
Peak Area CA-s): 0.023
Background Pk Area (A-s): 0.029
Blank Corrected Pk Area <A-s): 0.022
Concentration (ug/L ) : 13.3
QC sample is out of range 7.5 -12.5
Ti me: 14: 50
Peak Height <A> : 0. 02&
Background Pk Height (A): 0.019
Se ID: Std. Blk Seq. No.: 00044 A/S Pos.: 40 Date: 08/30/94
Replicate 1
Peak Area <A-s>: 0.004
Background Pk Area (A-s)
Blank Corrected Pk Area
Concentration (ug/L ) :
Auto-zero performed.
Se ID: Std 1
Replicate 1
: 0.023
(A-s>: 0.003
1.6
Ti me: 14: 53
Peak Height <A>: 0.010
Background Pk Height CA)
Seq. No.: 00045 A/S Pas. : 1
Ti me: 14: 55
0.01&
Date: 08/30/94
PE AA
0072
SE1
94/08/2&
12:30:01
94/08/2&
12:30:01
M.King
#HOR
0009
0000000
#DATA
M.King
20
1.0
0=g
1
l=uL
1. 0E-6
4,5.0 ck,,
5, Blk,,
HGA
6, Spike,,
7,ext 13735u,,
8, 13735s,,
9, 139081J,,
10, 13908s,,
11,139191J,,
12, 139 19 s, ,
13, 139201J,,
14, 13920s,,
15, 13921u,,
16, 13921s,,
17, 139221J,,
18, 13922s,,
19, 139231J, ,
20, 13923s,,
21, 14171u,,
22, 14171s,,
23, 14172•J,,
24, 14172s,,
25, 141731J,,
26, 14173s,,
27, 141741J,,
28, 14174s,,
29, 14175u,,
30, 14175s,,
31, tot 13643u, ,
32, 13643s,,
33, 13644u,,
34, 13644s, ,
35, 13645•J, ,
36, 13645s,,
37, 13646u,,
38, 13646s,,
39, 13647u,,
IDWT ASCII 5100 PC 7.10
Element File: SETEST.GEL
Date: 08/26/94
Element: Se
Ti me: 14: 23
Wavelength: 196.0
Slit: 2.0 L
Data File:
Technique: HGA
ID/Wt File: SEl.IDW
Calib. Type: Nonlinear
Lamp Current: 0
Energy: 58
Se ID: Std. Blk Seq. No.: 00046 A/S Pas.: 40
Replicate 1
Peak Area (A-s): 0.003
Background Pk Area <A-s): 0.022
Blank Corrected Pk Area (A-s): 0.002
Concentration (ug/L ) : 1. 2
Auto-zero performed.
Ti me: 14: 23
Peak Height (A): 0. 011
Background Pk Height (A)
Se ID: Std 1 Seq. No.: 00047 A/S Pas. : 1
Replicate 1
Peak Area (A-s): 0.032
Background Pk Area <A-s): 0.029
Blank Corrected Pk Area (A-s): 0.029
Concentration (ug/L ) : 21.9
Standard number 1 applied. (30.0]
Correlation coefficient: 1.00000
Ti me: 14: 26
Peak Height (A): 0.087
Background Pk Height (A)
Slope: 0.0010
Se ID: Std 2 Seq. No.: 00048 A/S Pas.: 2
Replicate 1
Peak Area (A-s): 0.053
Background Pk Area <A-s): 0.031
Blank Corrected Pk Area (A-s>: 0.050
Concentration (ug/L ) : 51.8
Standard number 2 applied. (50. 0]
Correlation coefficient: 1.00000
Ti me: 14: 29
Peak Height <A>: 0. 149
Background Pk Height (A)
Slope: 0.0009
Se ID: Lab QC Check Seq. No.: 00049 A/S Pas.: 3
Replicate 1
Peak Area <A-s): 0.014
Background Pk Area (A-s): 0.021
Blank Corrected Pk Area (A-s): 0.011
Concentration (ug/L ) : 12.0
QC sample is within range 7.5 -12.5
Time: 14:31
Peak Height <A>: 0.035
Background Pk Height <A>
Se ID: 5. 0 ck Seq. No.: 00050 A/S Pas.: 4
Replicate 1
Peak Area <A-s>: 0.009
Background Pk Area (A-s>: 0.022
Ti me: 14: 34
Peak Height (A): 0.029
Background Pk Height (A)
Date: 08/26/94
0.022
Date: 08/26/94
0.027
Date: 08/26/94
0.031
Date: 08/26/94
0.024
Date: 08/26/94
0.023
..
Concentration Cug/L ) : 5. 9
Se ID: Blk Seq. No.: 00051 A/S Pos.: 5
Replicate 1
Peak Area CA-s>: 0.006
Background Pk Area CA-s)
Blank Corrected Pk Area
Concentration Cug/L ) :
0.019
CA-s): 0.003
3.121
Ti me: 14: 36
Peak Height CA): 0.012
Background Pk Height CA>
Se ID: Spike Seq. No.: 00052 A/S Pos. : 6
Replicate 1
Peak Area CA-s): 0.023
Background Pk Area CA-s): 0.024
Blank Corrected Pk Area (A-s): 0.020
Concentration Cug/L ) : 21.3
Time: 14:39
Peak Height CA) : 0. 071
Background Pk Height CA)
Se ID: ext 137351.1 Seq. No.: 00053 A/S Pas. : 7
Replicate 1
Peak Area <A-s): 0.003
Background Pk Area CA-s): 0.293
Blank Corrected Pk Area CA-s>: -0.000
Concentration (ug/L ): -0.2
Time: 14:41
Peak Height CA) : 0. 016
Background Pk Height CA>
Se ID: 13735s Seq. No.: 00054 A/S Pos.: 8
Replicate 1 Ti me: 14: 44
Date: 08/26/94
0.022
Date: 08/26/94
0.023
Date: 08/26/94
0.279
Date: 08/26/94
Peak Area (A-s): 0.017
Background Pk Area (A-s): 0.293
Blank Corrected Pk Area (A-s>: 0.014
Concentration (ug/L ): 15.0
Peak Height <A>: 0.050
Background Pk Height CA): 0.281
Se ID: 13908u Seq. No.: 00055 A/S Pas.: 9
Replicate 1
Peak Area <A-s>: 0.002
Background Pk Area <A-s> 0.288
Blank Corrected Pk Area (A-s): -0.001
Concentration Cug/L ): -1.0
Ti me: 14: 46
Peak Height CA) : 0. 012
Background Pk Height CA)
Se ID: 13908s Seq. No.: 00056 A/S Pos.: 10
Replicate 1
Peak Area CA-s): 0.019
Background Pk Area CA-s): 0.299
Blank Corrected Pk Area CA-s): 0.016
Concentration C ug/L ) : 16. 5
Time: 14: 49
Peak Height CA>: 0.059
Background Pk Height CA>
Se ID: 139191.1 Seq. No.: 00057 A/S Pos.: 11
Date: 08/26/94
0.273
Date: 08/26/94
0.271
Date: 08/26/94
Replicate 1
Peak Area <A-s): 0.000
Background Pk Area (A-s): 0.290
Blank Corrected Pk Area (A-s): -0.003
Concentration (ug/L ): -3.2
Time: 14:51
Peak Height <A> : 0. 012
Background Pk Height (A): 0.268
Se ID: 13919s Seq. No.: 00058 A/S Pos. : 12 Date: 08/26/94
Replicate 1
Peak Area <A-s): 0.023
Background Pk Area CA-s): 0.293
Blank Corrected Pk Area (A-s): 0.020
Concentration (ug/L ): 20.8
Ti me: 14: 54
Peak Height <A>: 0.062
Background Pk Height CA): 0.282
,Se ID: 13920u Seq. No.: 00059 A/S Pos. : 13 Date: 08/26/94
Replicate 1
Peak Area CA-s): 0.000
Background Pk Area <A-s): 0.296
Blank Corrected Pk Area CA-s): -0.003
Concentration Cug/L ): -3.0
Ti me: 14: 56
Peak Height CA): 0.011
Background Pk Height <A>: 0.281
Se ID: 13920s Seq. No.: 00060 A/S Pos. : 14 Date: 08/26/94
Replicate 1
Peak Area (A-s): 0.022
Background Pk Area <A-s): 0.297
Blank Corrected Pk Area (A-s): 0.019
Concentration (ug/L ): 19.5
Ti me: 14: 59
Peak Height CA) : 0. 059
Background Pk Height <A>: 0.270
Se ID: 13921 u Seq. No.: 00061 A/S Pos. : 15 Date: 08/2&/94
Replicate 1
Peak Area CA-s): -0.002
Background Pk Area <A-s): 0.308
Blank Corrected Pk Area (A-s): -0.005
Concentration (ug/L ): -5.2
Time: 15:01
Peak Height (A) : 0. 012
Background Pk Height CA): 0.266
Se ID: 13921 s Seq. No.: 00062 A/S Pas. : 16 Date: 08/26/94
Replicate 1
Peak Area CA-s): 0.024
Background Pk Area (A-s): 0.311
Blank Corrected Pk Area <A-s): 0.021
Concentration Cug/L ): 21.9
Ti me: 15: 04
Peak Height CA): 0.053
Background Pk Height (A): 0.267
Se ID: 13922u Seq. No.: 00063 A/S Pas.: 17 Date: 08/2&/94
Replicate 1
Peak Area <A-s>: 0.001
Background Pk Area <A-s): 0.304
Blank Corrected Pk Area CA-s): -0.002
Concentration (ug/L ): -1.9
Ti me: 15: 06
Peak Height <A>: 0.011
Background Pk Height <A>: 0.261
e ID: 13922s Seq. No.: 00064 A/S Pas.: 18
epl icat e 1
eak Area <A-s): 0.023
ackground Pk Area <A-s): 0.305
lank Corrected Pk Area (A-s): 0.019
oncentration (ug/L ) : 20.3
Ti me: 15: 09
Peak Height CA): 0. 056
Background Pk Height <A>
e ID: 13923u Seq. No.: 00065 A/S Pos.: 19
eplicate 1
'eak Area <A-s) : -0. 002
ackground Pk Area (A-s) 0.307
,lank Corrected Pk Area <A-s): -0.005
:oncentrat ion ( ug/L ) : -5. 4
Time: 15:12
Peak Height (A): 0.011
Background Pk Height ·(A)
ID: 13923s Seq. No.: 00066 A/S Pos.: 20
:eplicate 1
'eak Area ( A-s) : 0. 020
,ack ground Pk Area ( A-s)
,lank Corrected Pk Area
:oncentrat ion ( ug/L ) :
0.309
<A-s>: 0.017
17.4
Time: 15:14
Peak Height (A): 0. 051
Background Pk Height (A)
ie ID: 141711.1 Seq. No.: 00067 A/S Pos. : 21
:eplicate 1
'eak Area (A-s) : 0. 000
1ackground Pk Area <A-s): 0.279
1lank Corrected Pk Area (A-s): -0.003
:oncentrat ion < ug/L > : -2. 9
Time: 15:17
Peak Height CA}: 0.017
Background Pk Height CA)
ie ID: 14171s Seq. No.: 00068 A/S Pos.: 22
:eplicate 1
•eak Area (A-s): 0.021
iackground Pk Area (A-s>: 0.289
ilank Corrected Pk Area <A-s): 0.018
:oncentration (ug/L ): 18.6
Time: 15: 19
Peak Height (A): 0.055
Background Pk Height <A>
ID: 141721.1 Seq. No.: 00069 A/S Pas.: 23
teplicate 1
)eak Area (A-s): 0.000
1ackground Pk Area <A-s>: 0.279
!lank Corrected Pk Area <A-s}: -0.003
:oncentration Ct.tg/L >: -3. 0
Ti me: 15: 22
Peak Height <A>: 0.015
Background Pk Height (A}
ID: Lab QC Check Seq. No.: 00070 A/S Pos.: 3
teplicate 1
•eak Area <A-s} 0.009
Ti me: 15: 24
Peak Heiqht (A} 0.038
Date: 08/26/94
0.275
Date: 08/26/94
0.267
Date: 08/26/94
0.282
Date: 08/26/94
0.270
Date: 08/26/94
0.254
Date: 08/26/94
0.244
Date: 08/26/94
F·E AA
0072
AS2
94/07/06
<)7: 33: 32
94/07/06
()7: 33: 32
#HDR
0009
0000000
#DATA
100
1.0
O=,;i
1
l=mL
1.0E-3
4, 15206, ,
5, 15207, ,
6, 15208, ,
HGA
7, e:-: t 13T.::5u, , 2
8, 13735s, , 2
·~, 13908u , , 2
10, 13908s, , 2
11 , 1391 9u, , 2
12, 13919s, , 2
13, l 3920u, , 2
14, 13920s, , 2
15 , 13921 Ll , , 2
16, 13921s, ,2
1 7, 13922u , , 2
18, 13922s , , 2
1 9, 13923u, , 2
20, 13923s,, 2
21,14171u,,2
22, 141 71 s, , 2
23, 141 72u , , 2
24, 141 72s, , 2
25, 141 73u , , 2
26, 141 73s , , 2
27 , 14174u , , 2
28, 14174s, ,2
29 , 141 75u, , 2
30, 141 7'.=j9 , , 2
31,tot 13034u, ,2
32, 13034s, , 2
33, 13643u , , 2
34, 13643s, , '.;,~
35, 13644u , , 2
36, 13644s , , 2
37, 13645u , , 2
38, 13645s , , 2
39, 13646u , , 2
IDWT ASCII 5100 F'C 7. 10
F'E AA
· 0072'
AS3
94/07/06
08:21:00
.94/07 /06
08:21:00
#HDR
0009
0000000
tl'DATA
100
1.0
O=g
1
l=mL
1.0E-3
4, 13646s , , 2
5, 13647u, ,2
6, 1364 7 s, , 2
7, 13735u , , 2
8, 13735s, , 2
9, 1391 9u, , 2
10, l 3919s, , 2
11 , 13920Ll, , 2
12 , 13920s , , 2
13 , 13921 LI , , 2
14, 13921 s, , 2
15, 13922u, , 2
16, l 3922s, , 2
1 7 , 13923u , , 2
18, l 3923s, , 2
HGA IDWT ASCII 5100 F'C 7 . 10
~----~-------------------------------------------------------------------------
As ID: Std Blk Seq. No.: 00017 A/S Pos .: 40 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.002
Background Pk Area (A-s): 0.053
Blank Corrected Pk Area (A-s): -0.007
Concentration (ug/L ): -1.8
Auto-zero performed.
Time: 10:26
Peak Height (A): 0.026
Background Pk Height (A): 0.041
As ID: Std 1 Seq. No.: 00018 A/S Pos.: 1 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.129
Background Pk Area (A-s): 0.059
Blank Corrected Pk Area (A-s): 0.127
Concentration (ug/L ): 29.6
Time: 10:29
Peak Height (A): 0 .249
Background Pk Height (A): 0 .041
Standard number 1 applied. [30.0]
Correlation coefficient: 1.00000 Slope: 0.0042
-------------------------------------------------------------------------------
As ID: Std 2 I Seq. No.: 00019 A/S Pos.: 2 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.215
Background Pk Area (A-s): 0.068
Blank Corrected Pk Area (A-s): 0.213
Concentration (ug/L ): 50.4
Standard number 2 applied. [50.0]
Correlation coefficient: 1.00000
Time: 10:31
Peak Height (A): 0.384
Background Pk Height (A): 0.048
Slope: 0.0042
As ID: Lab QC Check Seq. No. : 00020 A/S Pos.: 3 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.096
Background Pk Area (A-s): 0.056
Blank Corrected Pk Area (A-s): 0.094
Concentration (ug/L ): 22.3
QC sample is within range 17.5 -22.5
Time: 10:34
Peak Height (A): 0.168
Background Pk Height (A): 0.051
As ID: 5.0 ck Seq. No.: 00021 A/S Pos.: 4 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.024
Background Pk Area (A-s): 0.057
Blank Corrected Pk Area (A-s): 0.021
Concentration (ug/L ): 5.1
Time: 10:36
Peak Height (A): 0.056
Background Pk Height (A): 0.046
As ID: Blk Seq. No.: 00022 A/S Pos.: 5 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.004
Background Pk Area (A-s): 0.055
Blank Corrected Pk Area (A-s): -0.006
Concentration (ug/L ): -1.5
Time: 10:39
Peak Height (A): 0.023
Background Pk Height (A): 0.047
As ID: Spike Seq. No.: 00023 A/S Pos.: 6 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.087
Background Pk Area (A-s): 0.063 .
Blank Corrected Pk Area (A-s): 0.085
Concentration (ug/L ): 20.1
Time: 10:41
Peak Height (A): 0.151
Background Pk Height (A): 0.044
As ID: 15176 Seq. No.: 00024 A/S Pos.: 7 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.005
Background Pk Area (A-s): 0.067
Time: 10:44
Peak Height (A): 0.017
Background Pk Height (A): 0.035
-------------------------------------------------------------------------------
As ID: ext 13735u Seq. No.: 00063 A/S Pos.: 7 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.010
Background Pk Area (A-s): 0.075
Blank Corrected Pk Area (A-s): 0.007
Concentration (ug/L ): 1.8
Time: 12:52
Peak Height (A): 0 .022
Background Pk Height (A): 0.045
Corrected Cone (ug/L ): 3.6
As ID: 13735s Seq. No. : 00064 A/S Pos.: 8 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.093
Background Pk Area (A-s): 0.089
Blank Corrected Pk Area (A-s): 0.091
Concentration (ug/L ): 21 .5
Time: 12:55
Peak Height (A): 0 .132
Background Pk Height (A): 0.054
Corrected Cone (ug/L ): 43.1
As ID: 13908u Seq. No. : 00065 A/S Pos.: 9 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.003
Background Pk Area (A-s): 0.081
Blank Corrected Pk Area (A-s): -0 .005
Concentration (ug/L ): -1 .3
Time: 12: 57
Peak Height (A): 0 .021
Background Pk Height (A): 0.051
Corrected Cone (ug/L ): -2.6
As ID: 13908s Seq. No. : 00066 A/S Pos.: 10 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.102
Background Pk Area (A-s): 0.079
Blank Corrected Pk Area (A-s): 0.100
Concentration (ug/L ): 23.7
Time: 13: 00
Peak Height (A): 0.122
Background Pk Height (A): 0.051
Corrected Cone (ug/L ): 47.4
As ID: 13919u Seq. No.: 00067 A/S Pos.: 11 Date : 07/06/94
Replicate 1
Peak Area (A-s): 0.006
Background Pk Area (A-s): 0.078
Blank Corrected Pk Area (A-s): 0.004
Concentration (ug/L ): 1.0
Time: 13:02
Peak Height (A): 0.023
Background Pk Height (A): 0.047
Corrected Cone (ug/L ): 1.9
As ID: 13919s Seq. No. : 00068 A/S Pos.: 12 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.100
Background Pk Area (A-s): 0 .086
Blank Corrected Pk Area (A-s): 0.097
Concentration (ug/L ): 23.1
Time : 13: 05
Peak Height (A): 0.122
Background Pk Height (A): 0.048
Corrected Cone (ug/L ): 46.1
t
As ID: 13920u Seq. No. : 00069 A/S Pos.: 13 Date: 07/06/94
Replicate 1 Time: 13: 07
Peak Area (A-s): 0.003 Peak Height (A): 0 .020
Background Pk Area (A-s): 0.074
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ): 0.1
Background Pk Height (A): 0.049
Corrected Cone (ug/L ): 0.3
'As ID: 13920s Seq. No.: 00070 A/S Pos.: 14 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.094
Background Pk Area (A-s): 0.080
Blank Corrected Pk Area (A-s): 0.091
Concentration (ug/L ): 21.7
Time: 13:09
Peak Height (A): 0.145
Background Pk Height (A): 0.052
Corrected Cone (ug/L ): 43.4
As ID: 13921u Seq. No.: 00071 A/S Pos.: 15 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.000
Background Pk Area (A-s): 0.077
Blank Corrected Pk Area (A-s): -0.003
Concentration (ug/L ): -0.7
Time: 13: 12
Peak Height (A): 0.026
Background Pk Height (A): 0.050
Corrected Cone (ug/L ): -1.3
As ID: 13921s Seq. No.: 00072 A/S Pos.: 16 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.098
Background Pk Area (A-s): 0.079
Blank Corrected Pk Area (A-s): 0.096
Concentration (ug/L ): 22.7
Time: 13:14
Peak Height (A): 0.146
Background Pk Height (A): 0.048
Corrected Cone (ug/L ): 45.5
As ID: 13922u Seq. No.: 00073 A/S Pos.: 17 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.004
Background Pk Area (A-s): 0.069
Blank Corrected Pk Area (A-s): 0.001
Concentration (ug/L ): 0.3
Time: 13:17
Peak Height (A): 0.021
Background Pk Height (A): 0.041
Corrected Cone (ug/L ): 0.7
As ID: 13922s Seq. No.: 00074 A/S Pos.: 18 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.097
Background Pk Area (A-s): 0.076
Blank Corrected Pk Area (A-s): 0.094
Concentration (ug/L ): 22.4
Time: 13:19
Peak Height (A): 0.122
Background Pk Height (A): 0.046
Corrected Cone (ug/L ): 44.9
-------------------------------------------------------------------------------
As ID: 13923u Seq. No.: 00075 A/S Pos.: 19 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.000
Background Pk Area (A-s): 0.073
Blank Corrected Pk Area (A-s): -0.003
Concentration (ug/L ): -0.7
Time: 13:22
Peak Height (A): 0.022
Background Pk Height (A): 0.048
Corrected Cone (ug/L ): -1.4
. . .
~----·· ----~.;,..:~..w,.J,.......l......:..-i...:.~ ....... ~-
-------------------------------------------------------------------------------
As ID: 13923s Seq. No.: 00076 A/S Pos.: 20 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.094
Background Pk Area (A-s): 0.081
Blank Corrected Pk Area (A-s): 0.092
Concentration (ug/L ): 21.8
Time: 13:24
Peak Height (A): 0.139
Background Pk Height (A): 0.051
Corrected Cone (ug/L ): 43.6
As ID: 14171u Seq. No.: 00077 A/S Pos.: 21 Date: 07/06/94
Replicate 1
Peak Area (A-s): -0.001
Background Pk Area (A-s): 0.084
Blank Corrected Pk Area (A-s): -0.004
Concentration (ug/L ): -0.9
Time: 13:27
Peak Height (A): 0.019
Background Pk Height (A): 0.049
Corrected Cone (ug/L ): -1.9
As ID: 14171s Seq. No. : 00078 A/S Pos.: 22 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.090
Background Pk Area (A-s): 0.078
Blank Corrected Pk Area (A-s): 0.087
Concentration (ug/L ): 20.7
Time: 13: 29
Peak Height (A): 0.128
Background Pk Height (A): 0.045
Corrected Cone (ug/L ): 41.5
As ID: 14172u Seq. No.: 00079 A/S Pos.: 23 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.002
Background Pk Area (A-s): 0.076
Blank Corrected Pk Area (A-s): -0.000
Concentration (ug/L ): -0.0
Time: 13: 32
Peak Height (A): 0.020
Background Pk Height (A): 0.045
Corrected Cone (ug/L ): -0.0
As ID: Lab QC Check Seq. No. : 00080 A/S Pos.: 3 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.096
Background Pk Area (A-s): 0.057
Blank Corrected Pk Area (A-s): 0.094
Concentration (ug/L ): 22.3
QC sample is within range 17.5 -22.5
Time: 13: 34
Peak Height (A): 0.192
Background Pk Height (A): 0.033
As ID: 14172s Seq. No. : 00081 A/S Pos.: 24 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.097
Background Pk Area (A-s): 0.087
Blank Corrected Pk Area (A-s): 0.094
Concentration (ug/L ): 22.4
Time: 13:37
Peak Height (A): 0.129
Background Pk Height (A): 0.054
Corrected Cone (ug/L ): 44.7
-------------------------------------------------------------------------------
As ID: 14173u Seq. No. : 00082 A/S Pos.: 25 Date: 07/06/94
~------------------------------------------------------------------------------
As ID: Std 2 Seq. No.: 00101 A/S Pos.: 2 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0 .256
Background Pk Area (A-s): 0.064
Blank Corrected Pk Area (A-s): 0 .259
Concentration (ug/L ): 54.4
Standard number 2 applied. (50.0]
Correlation coefficient: 1.00000
Time: 14:33
Peak Height (A): 0.443
Background Pk Height (A): 0.038
Slope: 0.0042
-------------------------------------------------------------------------------
As ID: Lab QC Check Seq. No.: 00102 A/S Pos .: 3 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.099
Background Pk Area (A-s): 0.059
Blank Corrected Pk Area (A-s): 0.102
Concentration (ug/L ): 22.2
QC sample is within range 17.5 -22.5
Time: 14:35
Peak Height (A): 0.188
Background Pk Height (A): 0.036
As ID: 13646s Seq. No .: 00103 A/S Pos .: 4 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.130
Background Pk Area (A-s): 0.170
Blank Corrected Pk Area (A-s): 0.133
Concentration (ug/L ): 28.2
Time: 14:38
Peak Height (A): 0 .181
Background Pk Height (A): 0.221
Corrected Cone (ug/L ): 56 .3
As ID: 13647u Seq. No.: 00104 A/S Pos.: 5 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.028
Background Pk Area (A-s): 0.205
Blank Corrected Pk Area (A-s): 0 .031
Concentration (ug/L ): 7.2
Time: 14:40
Peak Height (A): 0.042
Background Pk Height (A): 0 .279
Corrected Cone (ug/L ): 14.4
As ID: 13647s Seq. No.: 00105 A/S Pos.: 6 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.126
Background Pk Area (A-s): 0 .217
Blank Corrected Pk Area (A-s): 0.129
Concentration (ug/L ): 27 .3
Time: 14:43
Peak Height (A): 0 .194
Background Pk Height (A): 0.297
Corrected Cone (ug/L ): 54.7
As ID: 13735u Seq. No. : 00106 A/S Pos.: 7 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.025
Background Pk Area (A-s): 0.283
Blank Corrected Pk Area (A-s): 0 .028
Concentration (ug/L ): 6.4
Time: 14: 45
Peak Height (A): 0.050
Background Pk Height (A): 0.373
Corrected Cone (ug/L ): 12.9
As · ID: 13735s Seq. No.: 00107 A/S Pos.: 8 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.114
,Background Pk Area (A-s): 0.315
Blank Corrected Pk Area (A-s): 0.117
Concentration (ug/L ): 25.1
Time: 14:48
Peak Height (A): 0.167
Background Pk Height (A): 0.429
Corrected Cone (ug/L ): 50.2
As ID: 13919u Seq. No.: 00108 A/S Pos.: 9 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.022
Background Pk Area (A-s): 0.442
Blank Corrected Pk Area (A-s): 0.025
Concentration (ug/L ): 5.7
Time: 14:50
Peak Height (A): 0.058
Background Pk Height (A): 0.626
Corrected Cone (ug/L ): 11.4
As ID: 13919s Seq. No.: 00109 A/S Pos.: 10 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.121
Background Pk Area (A-s): 0.455
Blank Corrected Pk Area (A-s): 0.124
Concentration (ug/L ): 26.4
Time: 14:53
Peak Height (A): 0.178
Background Pk Height (A): 0.634
Corrected Cone (ug/L ): 52.8
As ID:· 13920u Seq. No.: 00110 A/S Pos.: 11 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.007
Background Pk Area (A-s): 0.185
Blank Corrected Pk Area (A-s): 0.010
Concentration (ug/1 ): 2.4
Time: 14:55
Peak Height (A): 0.023
Background Pk Height (A): 0.238
Corrected Cone (ug/L ): 4.8
As ID: 13920s Seq. No.: 00111 A/S Pos.: 12 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.101
Background Pk Area (A-s): 0.168
Blank Corrected Pk Area (A-s): 0.104
Concentration (ug/1 ): 22.5
Time: 14: 57
Peak Height (A): 0.149
Background Pk Height (A): 0.210
Corrected Cone (ug/L ): 44.9
As ID: 13921u Seq. No.: 00112 A/S Pos.: 13 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.005
Background Pk Area (A-s): 0.789
Blank Corrected Pk Area (A-s): 0.008
Concentration (ug/L ): 1.9
Time: 15:00
Peak Height (A): 0.047
Background Pk Height (A): 1.023
Corrected Cone (ug/L ): 3.7
As ID: 13921s Seq. No.: 00113 A/S Pos.: 14 Date: 07/06/94
Replicate 1 Time: 15:02
Peak Area (A-s): 0.109 Peak Height (A): 0.161
-... .:P,'°"Wli""h£"91S""'Ailll\li 1A ... 4-•'"'"QJ _ _,_P►-. -.O:.P.4""".\""'·•'"'*'-;c. ____ 4..,.po_;..,.4-u ""'"> ..... .,,,__a,_,--•~---~~-----•
.
Background Pk Area (A-s): 0.876
Blank Corrected Pk Area (A-s): 0.112
Concentration (ug/L ): 24.2
Background Pk Height (A): 1.146
Corrected Cone (ug/L ): 48.3
As ID: 13922u . Seq. No.: 00114 A/S Pos.: 15 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.018
Background Pk Area (A-s): 0.791
Blank Corrected Pk Area (A-s): 0.021
Concentration (ug/L ): 4.8
Time: 15: 05
Peak Height (A): 0.063
Background Pk Height (A): 1.039
Corrected Cone (ug/L ): 9.6
As ID: 13922s Seq. No.: 00115 A/S Pos.: 16 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.099
Background Pk Area (A-s): 0.819
Blank Corrected Pk Area (A-s): 0.102
Concentration (ug/L ): 22.0
Time: 15: 07
Peak Height (A): 0.150
Background Pk Height (A): 1.051
Corrected Cone (ug/L ): 44.1
As ID: 13923u Seq. No.: 00116 A/S Pos.: 17 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.016
Background Pk Area (A-s): 0.766
Blank Corrected Pk Area (A-s): 0.019
Concentration (ug/L ): 4.4
Time: 15: 10
Peak Height (A): 0.056
Background Pk Height (A): 0.994
Corrected Cone (ug/L ): 8.8
As ID: 13923s Seq. No.: 00117 A/S Pos.: 18 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.115
Background Pk Area (A-s): 0.767
Blank Corrected Pk Area (A-s): 0.118
Concentration (ug/L ): 25.3
Time: 15: 12
Peak Height (A): 0 .169
Background Pk Height (A): 0.953
Corrected Cone (ug/L ): 50.5
As ID: Lab QC Check Seq. No.: 00118 A/S Pos.: 3 Date: 07/06/94
Replicate 1
Peak Area (A-s): 0.096
Background Pk Area (A-s): 0.142
Blank Corrected Pk Area (A-s): 0.099
Concentration (ug/L ): 21.5
QC sample is within range 17.5 -22.5
Time: 15: 15
Peak Height (A): 0.179
Background Pk Height (A): 0.157
.-.,r:• ,.--/'3{):H )t,f {sf /373$"'-f,r
-J/uJd--, I , ' 1'3U-13-'UJ · 1-Jq11-;i3/tf Alf
. . . Autosa■pler Worksheet 08/08/134
12:31 pm
Worksheet Name: D1
Sample Descript~on File: Da i ly
Sequence Autosa ■pler Solution Analytical
Numbers Position Method Files
1 1 weal HW1
·=· ·=· blank HW1 .... ....
3 3 Std-HW1 HW1
4 4 Blk-HW1 HW1
5 5 QC-HW1 HW1
6 6 13034 tot HW1
7 7 13643 tot HW1
8 8 13644 tot HW1
9 9 13645 tot HW1
10 10 13646 tot HW1
11 1 1 13647 tot HW1 1 .-, 0::. 1 .-, 0::. 13735 tot HW1
13 13 13735 tot -D HW1
14 14 13735 tot -s spikeHW1 HW1
15 15 13919 tot HWl
16 16 13920 tot HW1
17 17 13921 tot HW1
18 18 13922 tot HWl
19 19 13923 tot HW1
20 4 Blk-HW1 HW1
21 c:-QC-HWl HWl ,_J
Page 1
Data File:
QC Su■■ary Report
data 1. dat
Daily Sample Description File:
Analytical Method File: HW1
QC Standard Time Element ID Result
Blk-HW1 12:53 pm Cr205552 -0.002
Cd214438 0.001
Ba455403 0.000
QC-HW1 12:56 pm Cr205552 1.031
Cd214438 0.981
Ba455403 1. 015
Blk-HW1 1: 37 pm Cr205552 0.002
Cd214438 0.000
Ba455403 0.000
QC-HW1 1: 40 pm Cr205552 0.996
Cd214438 0.962
Ba455403 1. 015
Page 1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
08/08/94
08/08/94
1: 43 pm
"Rec
102.95
98. 10
101. 50
99.45
96.20
101. 45
Within
Li ■its?
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
~~~~~-~lLt1{~-·.:2,'=7'~~~~~g';iiaUl:t':'>'t' . llt.-ll~~,a w· · 16K94 · f' 1,-.-.,,
~ Sa ■ple Su■■ary Report #2
Data File: data!. dat 08/08/94
Sample Description File: Daily 08/08/94
Analytical Method File: HW1 1: 43 pm
13034 tot 12:59 pm
Cone. Units
Cr205552 0.002 mg/L
Cd214438 0.000 mg/L
Ba455403 0.001 mg/L
13643 tot 1: 01 pm
Cone. Units
Cr205552 0. 121 mg/L
Cd214438 0.009 mg/L
Ba455403 0.381 mg/L
13644 tot 1: 04 pm
Cone. Units
Cr205552 0.040 mg/L
Cd214438 0.002 mg/L
Ba455403 0. 148 mg/L
13645 tot 1: 07 pm
Cone. Units
Cr205552 0. 110 mg/L
Cd214438 0.005 mg/L
Ba455403 0.262 mg/L
13646 tot 1: 10 pm
Cone. Units
Cr205552 0.037 mg/L
Cd214438 0.003 mg/L
Ba455403 0.083 mg/L
13647 tot 1: 12 pm
Cone. Units
Cr205552 0.044 mg/L
Cd214438 0.001 mg/L
Ba455403 0.075 mg/L
Page 1
Sa ■ple Su ■■ary Report #2
Data File: data1.dat 08/08/94
Sample Description File: Daily 08/08/94
Analytical Method File: HW1 1:43 pm
13735 tot 1:15 pm
Cone. Units
Cr205552 0.053 mg/L
Cd214438 0.009 mg/L
Bc:1455403 0. 114 mg/L
13735 tot -D D 1: 18 pm
Cone. Units
Cr205552 0.057 mg/L
Cd214438 0.007 mg/L
Bc:1455403 0. 115 mg/L
13735 tot -s s -spikeHW1 1: 21 pm
Cone. Units
Cr205552 0.963 mg/L
Cd214438 0.893 mg/L
Bc:1455403 1. 091 mg/L
13919 tot 1 . ·=•7 • L...--.J pm
Cone. Units
Cr205552 0.055 mg/L
Cd214438 0.008 mg/L
Bc:1455403 0. 115 mg/L
13920 tot 1: 26 pm
Cone. Units
Cr205552 0.042 mg/L
Cd214438 0.006 mg/L
Ba455403 0.076 mg/L
13921 tot 1 :29 pm
Cone. Units
Cr205552 0.062 mg/L
Cd214438 0.018 mg/L
Ba455403 0.447 mg/L
Page 2
Sa ■ple Su■■ary Report #2
Data File:
Sample Description File:
Analytical Method File:
Cr205552
Cd214438
Ba455403
Cr205552
Cd214438
Ba455403
13922 tot
13923 tot
Cone.
0.059
0.018
0.482
Cone.
0.077
0.017
0.372
data 1. dat
Daily
HW1
Units
mg/L
mg/L
mg/L
Units
mg/L
mg/L
mg/L
Page 3
1: 32 pm
1: 34 pm
08/1218/94
08/08/94
1: 43 pm
Autosa■pler Worksheet
Worksheet Name: D1
Sample Description File: Daily
Sequence Auto sampler Solution
Nu ■bers Position
1 1 weal
2 2 blank
3 3 STD-HW2
4 4 BLK-HW2
5 5 QC-HW2
6 6 13034 tot
7 7 13643 tot
8 8 13644 tot
9 9 13645 tot
10 1121 13646 tot
11 11 13647 tot
12 1 ·-· C. 13735 tot
13 13 13735 tot -D
14 14 13735 tot -s
15 15 13g1g tot
16 16 13g20 tot
17 17 13g21 tot
18 18 13g22 tot
19 19 13g23 tot
20 4 BLK-HW2
21 5 QC-HW2
Page 1
1:44 pm
Analytical
Method Files
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
spikeHW2 Agl
Agl
Agl
Agl
Agl
Agl
Agl
Agl
Data File:
QC Su■■ary Report
data 1. dat
Daily Sample Description File:
Analytical Method File: Ag1
QC Standard Ti ■e Element ID Result
BLK-HW2 1: 55 pm Ag328068 0.000
QC-HW2 1: 57 pm Ag328068 0.963
BLK-HW2 2:27 pm Ag328068 0.000
QC-HW2 2:29 pm Ag328068 1.000
Page 1
Units
mg/L
mg/L
mg/L
mg/L
08/08/94
08/08/94
2:31 pm
'¼Rec
96.30
100.00
Within
Li ■its?
Yes
Yes
Yes
Yes
---·---------------·-----···----------
" Sample Su■■ary Report #2
Data i='ile: data 1. dat 08/08/94
Sample Description File: Daily 08/08/94
Analytical Method File: Ag1 2:31 pm
13034 tot 1: 59 pm
Cone. Units
Ag328068 0.002 mg/L
13643 tot 2:01 pm
Cone. Units
Ag328068 -0.001 mg/L
13644 tot 2:03 pm
Cone. Units
Ag328068 0.000 mg/L
13645 tot 2:05 pm
Cone. Units
Ag328068 -0.001 mg/L
13646 tot 2:07 pm
Cone. Units
Ag328068 0.000 mg/L
13647 tot 2:09 pm
Cone. Units
Ag328068 0.000 mg/L
13735 tot 2: 11 pm
Cone. Units
Ag328068 0.000 mg/L
13735 tot -D D 2: 13 pm
Cone. Units
Ag328068 -0.001 mg/L
Page 1
,. -.. Sa■ple Su■■ary Report #2
Data File: datal. dat 08/08/94
Sample Description File: Daily 08/08/94
Analytical Method File: Agl 2:31 pm
13735 tot -s s -spikeHW2 2: 15 pm
Cone. Units
Ag328068 0.900 mg/L
13919 tot 2: 17 pm
Cone. Units
Ag328068 0.000 mg/L
13920 tot 2: 19 pm
Cone. Units
Ag328068 -0.001 mg/L
13921 tot 2:21 pm
Cone. Units
Ag328068 -0.001 mg/L
13922 tot 2:23 pm
Cone. Units
Ag328068 -0.003 mg/L
13923 tot 2:25 pm
Cone. Units
Ag328068 -0.001 mg/L
Page 2
Autosampler Worksheet
Worksheet Name: Dl
Sample Description File: Daily
Sequence Autosa■pler Solution
Nu ■bers Position
1 1 weal
·=· •=I blank '-'-
3 3 STD-HW2
4 4 BLK-HW2
5 5 QC-HW2
6 6 13908 ext
7 7 13735 ext
8 8 13919 ext
9 9 13920 ext
10 10 13920 ext -D
1 1 1 1 13920 ext -s
12 12 13921 ext
1 7 ... ...., 13 13922 ext
14 14 13923 ext
15 15 14171 ext
16 4 BLK-HW2
17 5 QC-HW2
08/11/94
1:28 pm
Analytical
Method Files
HW2
HW2
HW2
HW2
HW2
HW2
HW2
HW2
HW2
HW2
spikeHW2 HW2
HW2
HW2
HW2
HW2
HW2
HW2
. . -~ Sa11ple Su■■ary Report #2
Data File: datal.dat 08/11/94
Sample Description File: Daily 08/11/94
Analytical Method File: HW2 2:53 pm
13922 ext 2:45 pm
Cone. Units
Pb220353 -0.003 mg/L
Ag328068 0.000 mg/L
13923 ext 2:47 pm
Cone. Units
Pb220353 0.000 mg/L
Ag328068 0.000 mg/L
14171 ext 2:49 pm
Cone. Units
Pb220353 0.009 mg/L
Ag328068 0.000 mg/L
Page 2
Sample Su ■■ary Report #2
Data File:
Sample Description File:
Analytical Method File:
13908 ext
Cone.
Pb220353 -0.009
Ag328068 0.000
13735 ext
Cone.
Pb220353 -0.003
Ag328068 0.000
13919 ext
Cone.
Pb220353 0. 121
Ag328068 -0.001
13920 ext
Cone.
Pb220353 0.003
Ag3281Z168 0.000
13920 ext D -
Cone.
Pb22121353 -0.003
Ag328tZl68 -0.001
13920 ext s -
Cone.
J:•b221Zt353 0.971
Ag328068 1.044
13921 ext
Cone.
r:1b220353 -0.006
Ag328068 0.000
D
s
data 1. dat
Daily
HW2
Units
mg/L
mg/L
Units
mg/L
mg/L
Units
mg/L
mg/L
Units
mg/L
mg/L
Units
mg/L
mg/L
-spikeHW2
Units
mg /L
mg/L
Units
mg/L
mg/L
Page 1
2:31 pm
2:33 pm
2:35 pm
2:37 pm
2:39 pm
2:41 pm
2:43 pm
08/11/94
08/11/94
2:53 pm
Data File:
QC Su ■■ary Report
datal. dat
Daily Sample Description File:
Analytical Method File: HW2
QC Standard Time Element ID Result
BLK-HW2 2:27 pm ~•b220353 -0. 006
Ag328068 0. 012,0
QC-HW2 2:29 pm Pb220353 1. 006
Ag328068 0. 988
BLK-HW2 2:51 pm Pb220353 -0.003
Ag328068 0.000
QC-HW2 2:53 pm Pb220353 1. 014
Ag328068 0.940
Page 1
Units
mg/L
mg /I_
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
08/11/94
08/11/94
2:53 pm
%Rec
100.60
98.80
101. 40
94.00
Within
Li ■its?
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Autosa■pler Worksheet
Worksheet Name: D1
Sample Description File: Daily
Sequence Autosampler Solution
Numbers Position
1 1 weal
•=1 ·=· blank '-'-·~ 7 Std-HW1 ,:, ...,
4 4 Blk-HW1
5 5 QC-HW1
6 6 13908 ext
7 7 13735 ext
8 8 13919 ext
9 9 13920 ext
10 10 13920 ext -D
1 1 1 1 13920 ext -s
1 ·-, .::. 12 13921 ext
13 13 13922 ext
14 14 13923 ext
15 15 14171 ext
16 4 Blk-HW1
17 5 QC-HW1
Page 1
08/ 11/94
12:18 pm
Analytical
Method Files
HW1
HW1
HWl
HW1
HW1
HW1
HW1
HW1
HW1
HW1
spikeHWl HW1
HW1
HW1
HW1
HW1
HW1
HW1
Data File:
QC Sum■ary Report
data 1. dat
Daily Sample Description File:
Analytical Method File: HW1
QC Standard Ti ■ e Element ID Result
B11-<-HWl 12:57 pm Cr205552 0. 000
Cd214438 0.000
Ba455403 0. 000
QC-HW1 12:59 pm Cr205552 1. 087
Cd214438 1. 011
Ba.455403 1. 064
Blk-HWl 1: 23 pm Cr205552 0. 000
Cd214438 0. 000
Ba455403 0. 000
QC-HWl 1:25 pm Cr205552 0.983
Cd214438 1. 040
Ba.455403 0. 990
Page 1
Units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
08/11/94
08/11/94
1: 26 pm
;<.Rec
108. 70
101. 10
106.40
98.30
104. 00
99. 00
Within
Li ■its?
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Sa ■ple Su■■ary Report #2
Data File: data 1. dat 1218/11/94
Sample Description File: Daily 1218/11/94
Analy•tical Method File: HW1 1: 26 pm
13908 ext 1 : 1211 pm
Cone. Units
Cr205552 -0.002 mg/L
Cd214438 0.12101 mg/L
Ba455403 0.268 mg/L
13735 ext 1: 03 pm
Cone. Units
Cr21215552 -0.002 mg/L
Cd214438 0. 000 mg/L
Ba455403 0.376 mg/L
13919 ext 1: 06 pm
Cone. Units
Cr205552 0. 002 mg/L
Cd214438 0.000 mg/L
Ba455403 0. 424 mg/L
13920 ext 1: 08 pm
Cone. Units
Cr205552 0. 002 mg/L
Cd214438 0. 000 mg/L
Ba455403 0.376 mg/L
13920 ext -D D 1:10 pm
Cone. Units
Cr205552 0. 000 mg/L
Cd214438 0.000 mg/L
BaL,55403 0.384 mg/L
13920 ext -s s -spikeHWl 1:12 pm
Cone. Units
Cr205552 0.778 mg/L
Cd21L;438 0.749 mg/L
Ba.Li-55403 1.304 mg/L
Page 1
Sample Su ■■ary Report #2
Data File: data 1. dat
Sample Description File: Daily
Analytical Method File: HW1
13921 ext 1:14 pm
Cone. Units
Cr21Z15552 IZI. IZIIZIIZI mg/L
Cd214438 IZI. 000 mg/L
Ba455403 IZl.464 mg/L
13922 ext 1:17 pm
Cone. Units
Cr205552 IZI. tZIIZIIZI mg/L
Cd214438 IZI. IZIIZI IZI mg/L
Ba455403 IZl.585 mg/L
13923 ext 1:19 pm
Cone. Units
Cr205552 IZI. IZIIZl2 mg/L
Cd214438 tZI. IZIIZIIZJ mg/L
Ba455403 IZI. 699 mg/L
14171 ext 1:21 pm
Cone. Units
Cr205552 IZI. 0 tZl0 mg/L
Cd214438 IZI. 12100 mg/L
Ba45541Z13 1.66IZI mg/L
Page 2
08/11/94
08/11/94
1: 26 pm
ID/Weight File: PB. IDW
Sample Volume: 100 mL
Loe.
9
10
11
12
13
14
15
16
17
18
19
20
21
Sample ID
HW 13034
CER 13643
13644
13645
13646
13647
HW 13735
SW 13919
13920
13921
13921 D
13922
13923
. ' .. --·-··••· •··-·-·•··-·--··-·-•-............... ··-···-·' .. -·--..... c...:....:..:.... ..... --~--.... ..;..,....=. ••
Analyst: ALJ
Nominal Weight: 1.0 g
Weight Dilution
L._ -ec1-d
13111-J__J
"IOI,
~er::Lci
,1/o/ff
t!YJ'
If~
/!)s!Jo
. . . . . ............ . _ _._....._._,...""-••--.....--•~-....,. ..... ,....,..-.._,.v_ • .,,..~ •• -~,•:,.,...;.."--o,.__,.;. __ _,..__ •••. _ .. _.. .. :i......-~~•-..... -.__,_,,._.,._._.~,·--,-.--._·-~~---.-............ -.. '-t...'"""...,i..,._-.,-•..._-, ....... "-,,_~__,...,......,..n •«•-.· --••►-----·
Element File: PB1.FEL
Date: 08/09/94
Data File:
Techniq1.1e: Flame
Pb ID: STD BLK
Absorbance: 0.123
Absorbance: 0. 123
Absorbance: 0. 123
Mean Absorbance:
Auto-zero performed.
Pb ID: STD BLK
Absorbance: 0.001
Absorbance: 0.000
Absorbance: 0.001
Mean Absorbance:
Auto-zero performed.
0. 123
0.001
Element: Pb
Time: 10:51
ID/Wt File: PB. IDW
Calib. Type: Nonlinear
Seq. No. : 00001 A/S
Time: 10:51
Time: 10:51
Time: 10:52
SD: 0.0001
Seq. No. : 00002 A/S
Time: 10:53
Time: 10:53
Time: 10:53
SD: 0.0001
Pas. : 1
Pas. : 1
Pb ID: STD 1 Seq. No.: 00003 A/S Pas.: 2
Absorbance: 0.009
Absorbance: 0.009
Absorbance: 0.009
Mean Absorbance: 0.009
Standard number 1 applied. [0. 500]
Correlation coefficient: 1.00000
Pb ID: STD 2 Seq. No. :
Absorbance: 0.017
Concentration <mg/L ) : 0.989
Absorbance: 0.017
Concentration <mg/L ) 1. 013
Absorbance: 0.017
Concentration (mg/L ) : 1. 006
Ti me: 10: 53
Time: 10:54
Ti me: 10: 54
SD: 0.0001
Slope: 0.0172
00004 A/S Pas. : 3
Time: 10:54
Time: 10:55
Time: 10:55
Wavelength: 283.3
Slit: 0.70 H
Lamp Current: 10
Energy: E:,9
Date: 08/09/94
RSD(~) 0.04
Date: 08/09/94
RSD < ¼) : 1 9. 1 9
Date: 08/09/94
RSD(¼) 0.E:,9
Date: 08/09/94
• Mean· Cone (11g/L ) : 1.003
Standard number 2 applied. C 1. 000]
Correlation coefficient: 1.00000
SD: 0.0120
Slope: 0.0171
Pb ID: STD 3 Seq. No.: 00005 A/S Pos.: 4
Absorbance: 0.035
Concentration (mg/L ): 2.033
Absorbance: 0.035
Concentration (mg/L ): 2.009
Absorbance: 0.035
Concentration (mg/L ) : 2.022
Mean Cone (11g/L ) : 2.022
Standard number 3 applied. (2. 000]
Correlation coefficient: 1.00000
Ti me: 10: 55
Ti me: 10: 55
Time: 10:50
SD: 0.0123
Slope: 0.0172
Pb ID: STD 4 Seq. No.: 00000 A/S Pos.: 5
Sample abs. is outside range of the calibration function.
Absorbance: 0.052 Time: 10:56
Concentration (mg/L ): ----------
Sample abs. is outside range of the calibration function.
Absorbance: 0.053 Time: 10:50
Concentration (mg/L ) : ----------
Sample abs. is outside range of the calibration function.
Absorbance: 0.052 Time: 10:57
Concentration (mg/L ) : ----------
Sample abs.
Mean Cone
is outside range of the calibration function.
(mg/L ) : SD:----
S-shaped calibration curve detected. 2-coef. equation used.
Standard number 4 applied. (3. 000]
Correlation coefficient: 0.99995 Slope: 0.0171
Pb ID: STD 5
Absorbance: 0.070
Concentration (mg/L ): 3.948
Absorbance: 0.070
Concentration (mg/L ) : 3.950
Absorbance: 0.0&9
Concentration <mg/L >: 3.927
Seq. No.: 00007 A/S Pos. : 6
Ti me: 10: 57
Ti me: 10: 57
Time: 10: 58
Mean Cone (mg/L ) : 3.944 SD: 0.0151
S-shaped calibration curve detected. 2-coef. equation used.
RSD ("): 1. 20
Date: 08/09/94
RSD ("): 0. 61
Date: 08/09/94
RSDC'1-): ----
Date: 08/09/94
RSD (") : 0. 38
~orrelation coefficient: 0.99995 Slope: 0.0172
M Calibration -C:\JlA USER\JlA FILES\ELENEMT\PB1.FEL ♦
a.a,
Ill .a ..
Nanlinear
Can-. Caef.: 8.99995
Sla e: a. 8172
S5
a.a Canc,ntratian 4.
Pb ID: PB QC Seq. No.: 00008 A/S Pos. : 7
Absorbance: 0.018
Concentration Cmg/L ): 1.043
Absorbance: 0.018
Concentration Cmg/L ) : 1.035
Absorbance: 0.018
Concentration Cmg/L >: 1.030
Mean Cone Cmg/L ) : 1. 036
QC sample is within range 0.89 -1. 11
Ti me: 11: 00
Ti me: 11: 00
Ti me: 11: 00
SD: 0.0067
Date:-08/09/94
RSD c,o 0.65
~~~~~~~~~~~~~~~~~~~~v~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: HW 13034 Seq. No.: 00009 A/S Pos.: 9 Date: 08/09/94
Absorbance: -0.000
Concentration (mg/L >: -0.002
Absorbance: 0.000
Concentration Cmg/L 0.003
Absorbance: -0.000
Concentration Cmg/L ): -0.006
Mean Cone Cmg/L ) : -0.002
T 1"'\. t""C' 0 1
Time: 11:01
Time: 11:01
Time: 11:01
SD: 0.0045 RSD (;() : 219. 77
n, n--n,c.1n, .1 .1
Absorbance: 0.001
Concentration (mg/L
Absorbance: 0.001
Concentration (mg/L
Absorbance: 0.001
Concentration (mg/L
Mean Cone (mg/L ) :
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration <mg/L
Mean Cone <mg/L ) :
Ti me: 11: 02
) : 0. 04&
Ti me: 11: 02
): 0.044
Ti me: 11: 02
0.051
0.047 SD: 0.0036 RSD('¼): 7.&9
Time: 11 :03
0.014
Time: 11:03
0.021
Time: 11:03
0.004
0.013 SD: 0.0082 RSD (") : 63. 3&
~~~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: 13&45 ._/ Seq. No.: 00012 A/S Pos.: 12 Date: 08/09/94
Absorbance: 0.000
Concentration <mg/L
Absorbance: -0.000
Concentration (mg/L
Absorbance: 0.000
Concentration <mg/L
Mean Cone (mg/L ) :
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Mean Cone (mg/L ) :
0.009
-0.000
0.015
0.008
> : 0. 005
> : 0. 007
): 0.012
0.008
Time: 11:04
Time: 11 :04
Time: 11:04
SD: 0.0078
Ti me: 11: 05
Ti me: 11: 05
Ti me: 11: 05
SD: 0.0037 RSD(¼): 48.31
~~~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: 13&47 V Seq. No.: 00014 A/S Pos.: 14 Date: 08/09/94
Absorbance: 0.000
Concentration (mg/L ): 0.008
Ti me: 11: 06
~oncentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone (mg/L ) :
0.001
): -0.011
-0.001
Ti me: 11: 0&
SD: 0.0095 RSD ("): 1396. 34
~~~~~~~~~~~~~~~~~~~~~~r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: HW 13735 / Seq. No.: 00015 A/S Pos.: 15 Date: 08/09/94
Absorbance: 0.001 Time: 11:07
Concentration (mg/L 0.053
Absorbance: 0.001 Time: 11:07
Concentration (mg/L 0.050
Absorbance: 0.001 Time: 11:07
Concentration (11g/L ) : 0.057
Mean Cone (11g/L ) : 0.053 SD: 0.0035 RSD (") : &.&2
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: SW 13919 ~ Seq. No. : 0001& A/S Pos. :
Absorbance: 0.003 Time: 11:08
Concentration (11g/L 0. 179
Absorbance: 0.003 Time: 11:08
Concentration (mg/L 0. 180
Absorbance: 0.003 Time: 11:08
Concentration (mg/L ) : 0. 181
Mean Cone (mg/L ) : 0. 180 SD: 0.0010
Pb ID: 13920 Seq. No. : 00017 A/S Pos. : 17
Absorbance: 0.000
Concentration (mg/L
Absorbance: 0.000
Concentration (mg/L
Absorbance: -0.000
Concentration (mg/L
Mean Cone (mg/L ) :
Ti me: 11: 09
0.005
Ti me: 11: 09
0.004
Ti me: 11: 09
-0.013
-0.001 SD: 0. 0101
Pb ID: 13921 ~ Seq. No.: 00018 A/S Pos. : 18
Absorbance: 0.001
Concentration (mg/L ): 0.040
Absorbance: 0.001
Concentration (mg/L ): 0.040
Time: 11:10
Time: 11:10
Date: 08/09/94
RSD <"-> : 0. 55
Date: 08/09/94
RSD (Y.) : 821. 50
Date: 08/09/94
Absorbance: 0.001
Concentration (mg/L
Mean Cone (mg/L ) :
): 0.031
0.037
Time: 11:10
SD: 0.0057
Pb ID: PB QC Seq. No. : 00019 A/S Pos.: 7
Absorbance: 0.018
Concentration (mg/L
Absorbance: 0.018
Concentration (mg/L )
Absorbance: 0.018
Concentration (mg/L
Mean Cone (mg/L ) :
1. 054
1. 047
1.044
1.048
QC sample is within range 0.89 -1. 11
Time: 11:11
Time: 11:11
Time: 11:11
SD: 0.0051
RSD (;<.) : 15. 32
Date: 08/09/94
RSD (;<.) 0.48
~~~~~~~~~~~~~~~~~~~~~~~y~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: 13921 D / Seq. No.: 00020 A/S Pas.: 19 Date: 08/09/94
Absorbance: 0.000 Time: 11: 12
Concentration Cmg/L 0.026
Absorbance: 0.001 Time: 11:12
Concentration <mg/L . 0.038 .
Absorbance: 0.001 Time: 11:12
Concentration Cmg/L 0.032
Mean Cone (mg/L ) : 0.032 SD: 0.0061 RSD (;{.) : 19. 02
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: 13922 ✓ Seq. No.: 00021 A/S Pos.: 20 Date: 08/09/94
Absorbance: 0.001 Time: 11:12
Concentration (mg/L 0.040
Absorbance: 0.001 Time: 11: 13
Concentration (mg/L ) 0.033
Absorbance: 0.001 Time: 11:.13
Concentration (mg/L ) 0.037
Mean Cone (11g/L ) : 0.037 SD: 0.0038 RSD(¼>: 10.22
~~~~~~~~~~~~~~~~~~~r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Pb ID: 13923 1./' Seq. No.: 00022 A/S Pas.: 21 Date: 08/09/94
Absorbance: 0.001 Time: 11:13
Concentration (mg/L ) 0.062
Absorbance: 0.001 Time: 11:14
Concentration <mg/L ) 0.080
~~-.... •-..~\--..._.,.--•,r-- -; --···-..--~•-··~-.. ~_,.., . ..., -coric~rit~ation <~g/L '·>: 0.064
Mean Cone (mg/L ) : 0.069 SD: 0.0098
Pb ID: PB QC Seq. No.: 00023 A/S Pas.: 7
Absorbance: 0.018
Concentration (mg/L
Absorbance: 0.018
Concentration <mg/L
Absorbance: 0.018
Concentration (mg/L
Mean Cone (mg/L ) :
) : 1. 065
) : 1. 068
1. 035
1. 056
QC sample is within range 0.89 -1. 11
Time: 11:14
Time: 11:14
Time: 11:15
SD: 0.0183
RSD (1-): 14. 35
Date: 08/09/94
RSD <~> : 1. 73
•
ID/Weight File: HG2.IDW
Sa•ple Volu■e: 100 ml
Loe. Sample ID
---------------
9 ,00025
10 R 1429&
11 14297
12 14298
13 14299
14 H 14333
15 R 14350
1& 14351
17 14352
18 14353
19 14354
20 14354 SPK
21 HW 14394
22 14395
23 1439&
24 14397
25 R 14428
2& 14429
27 14&19
28 HW 13735 EXT
29 13908 EXT
30 SW 13919 EXT
31 13920 EXT
32 13921 EXT
33 13922 EXT
34 13923 EXT
35 CER 14171 EXT
3& QC CHK
37 HW 13034 A
38 B
39 13643 A
40 B
41 13&44 A
42 B
43 13&45 A
44 B
45 13646 A
46 B
47 13&47 A
48 B
49 HW 13735 A
50 B
51 QC CHK
52 SW 13919 A
53 B
54 13920 A
55 B
5& 13921 A
57 B
58 13922 A
59 B
&0 13923 A
&1 B
&2 HW 13908 A
Analyst: ALJ
Nominal Weight: 1.0 g
Weight Dilution --------------------
l v..f '/ (v1t( ~ ~-)-
I J1l ~ G-,f~
SD;\
20
20
20
20
20
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
-,-----~-----------------------------------------------------------------------
Ele■ent File: HG2.MEL
Date: 08/15/94
Ele ■ent: Hg
Ti ■e: 12:53
Wavelength: 253.7
Slit: 0.70 L • Data File:
Technique: MHS
ID/Wt File':··HG2. IDW
Calib. Type: Linear
La■p Current: 5
Energy: 77
Hg ID: Seq. 00001 Seq. No.: 00001 A/S Pos. : 1
Replicate 1
Peak Area <A-s>: -0.008
Blank Corrected Pk Height (A): 0.001
Auto-zero perfor ■ed.
Hg ID: STD BLK
Replicate 1
Peak Area (A-s): -0.000
Blank Corrected Pk Height
Replicate 2
Peak Area <A-s): 0.000
Blank Corrected Pk Height
Mean Pk Height (A):
Auto-zero perfor■ed.
Hg ID: STD 1
Replicate 1
Peak Area (A-s): 0.054
Blank Corrected Pk Height
Replicate 2
Peak Area <A-s>: 0.055
Blank Corrected Pk Height
Mean Pk Height <A> :
Seq. No. :
<A> : 0.000
(A) : 0.000
0.000
Seq. No. :
(A) : 0.008
<A> : 0.008
0.008
Standard nu ■ber 1 applied. [0.000500]
Ti ■e: 12:53
Peak Height (A): 0.001
00002 A/S Pos. : 1
Ti ■e: 12:55
Peak Height <A> : 0.001
Ti ■e: 12:57
Peak Height CA) : 0.001
SD: 0.0000
00003 A/S Pos. : 2
Ti ■e: 12:58
Peak Height <A> : 0.009
Ti ■e: 13:00
Peak Height <A> : 0. 009
SD: 0.0001
Correlation coefficient: 1.00000 Slope: 15.7504
Hg ID: STD 2 Seq. No.: 00004 A/S Pos.: 3
Replicate 1
Peak Area (A-s): 0.102
Blank Corrected Pk Height <A>: 0.016
Concentration <■g/L ): 0.001000
Replicate 2
Peak Area (A-s): 0.103
Blank Corrected Pk Height (A): 0.01&
Concentration <■g/L ): 0.000987
Ti ■e: 13 :02
Peak Height <A>: 0.017
Ti ■e: 13:03
Peak Height (A): 0.017
Date: 08/15/94
Date: 08/15/94
RSD (") : 0.00
Date: 08/15/94
RSD<">: 0.90
Date: 08/15/94
Mean Core C ■g/L ): 0.000994 SD: 0.0000090
Standard nu■ber 2 applied. (0. 001000J
Correlation coefficient: 1.00000 Slope: 15.6702
Hg ID: STD 3 Seq. No.: 00005 A/S Pos.: 4
Replicate 1
Peak Area <A-s): 0.325
Blank Corrected Pk Height CA>: 0.047
Concentration C ■g/L >: 0.002990
Replicate 2
Peak Area (A-s>: 0.321
Blank Corrected Pk Height CA): 0.047
Concentration C ■g/L ): 0.002971
Mean Cone (■g/L ): 0.002980
Standard nu■ber 3 applied. (0. 003000)
Ti ■e: 13:05
Peak Height CA): 0.048
Ti ■e: 13:0E,
Peak Height <A>: 0.048
SD: 0.000013E,
Correlation coefficient: 0.99999 Slope: 15.5792
Hg ID: STD 4 Seq. No.: 0000E, A/S Pos.: 5
Replicate 1
Peak Area (A-s): 0.531
Blank Corrected Pk Height CA>: 0.078
Concentration · (■g/L ): 0.004991
Replicate 2
Peak Area <A-s>: 0.53E,
Blank Corrected Pk Height CA): 0.078
Concentration (■g/L ): 0.005029
Mean Cone (■g/L ): 0.005010
Standard nu■ber 4 applied. C0.005000J
Ti ■

e
:

13:08
Peak Height CA): 0.079
Ti ■e: 13:09
Peak Height CA): 0.080
SD: 0.0000273
Correlation coefficient: 1.00000 Slope: 15.E,010
Hg ID: STD 5 Seq. No.: 00007 A/S Pos.: 6
Replicate 1
Peak Area <A-s): 0.754
Blank Corrected Pk Height CA): 0.110
Concentration C ■g/L ): 0.007041
Replicate 2
Peak Area <A-s): 0.754
Blank Corrected Pk Height CA>: 0.109
Concentration C ■g/L ): 0.007009
Mean Cone (■g/L ): 0.007025
Standard nu■ber 5 applied. (0.007000]
Ti ■

e
:

13:11
Peak Height CA) : 0. 111
Ti ■e: 13:12
Peak Height CA>: 0.111
SD: 0.0000227
Correlation coefficient: 0.99999 Slope: 15.6338
RSDC"): 0.91
Date: 08/15/94
RSDC"): 0.4E,
Date: 08/15/94
RSD <"> : 0. 55
Date: 08/15/94
RSD(%): 0.32
M Calibratian -C:\AA USER\AA FILE5\ELEIIENT\H62.NEL
8.11 S5
Ill ~
Linear
CaJT. Caef.: 8.99999
a.a Slape: 15.6338
Cnnc,ntratinn B,BB7888
Hg ID: QC STD Seq. No.: 00008 A/S Pos.: 7
Replicate 1
Peak Area <A-s>: 0.199
Blank Corrected Pk Height <A>: 0.029
Concentration (■g/L ): 0.001874
Ti ■

e
:

13:15
Peak Height <A>: 0.031
QC sa■ple is out of range 0.00189 -0.00231
Hg ID: STD BLK Seq. No.: 00009 A/S Pos. : 1
Replicate 1
Peak Area (A-s): 0.004
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000013
Replicate 2
Peak Area (A-s): 0.001
Blank Corrected Pk Height CA>: 0.000
Concentration C ■g/L >: 0.000006
Mean Cone C ■g/L ): 0.000010
Auto-zero perfor■ed.
Ti ■e: 13:17
Peak Height CA>: 0.002
Ti ■e: 13: 18
Peak Height (A): 0.002
SD: 0.0000045
Hg ID: STD 4 Seq. No.: 00010 A/S Pos.: 5
Replicate 1
Peak Area <A-s): 0.535
Blank Corrected Pk Height <A>: 0.078
Concentration (■g/L ): 0.004964
Ti ■e: 13:20
Peak Height CA): 0.079
Date: 08/15/94
Date: 08/15/94
RSD C,C,) : 47. 14
Date: 08/15/94
♦
-.;::.~-_:.:::: . ...::;.:-..... :.-;;,•====-==--~~?AM> Ai 4JQJPJP-fob'"'4h':t:4(4•.t:t4:S:4fP .... fiQli_f)1:Y Flff?P.S.WWW7l&W.C¥KOP':? MAC.W
!• : , • '. • :.1· .. • ~ • '., '•: • ~ • l
Concentration <■g/L ): 0.000126
Hg ID: Seq. 00015 Seq. No.: 00015 A/S Pos.: 7
Replicate 1
Peak Area <A-s): 0.228
Bfank Corrected Pk Height <A>: 0.032
Concentration <■g/L ): 0.002042
Ti ■ e: 13:49
Peak Height (A): 0.033
Hg ID: QC STD Seq. No.: 00016 A/S Pos.: 7
Replicate 1
Peak Area <A-s>: 0.226
Blank Corrected Pk Height <A>: 0.032
Concentration (■g/L ) : 0.002068
Ti ■e: 13:51
Peak Height (A): 0.034
QC sa ■ple is within range 0.00189 -0.00231
Hg ID: • 00025 Seq. No.: 00017 A/S Pos.: 9
Replicate 1
Peak Area <A-s): 0.031
Blank Corrected Pk Height <A>: 0.004
Concentration (■g/L ): 0.000255
Replicate 1
Peak Area (A-s): 0.004
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000003
Ti ■e: 13:53
Peak Height (A): 0.006
Ti ■e: 13:55
Peak Height (A): 0.002
Date: 08/15/94
Date: 08/15/94
Date: 08/15/94
~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 14297 Seq. No.: 00019 A/S Pos.: 11 Date: 08/15/94
Replicate 1 Ti ■ e: 13:57
Peak Area (A-s): 0.002 Peak Height (A): 0.001
Blank Corrected Pk Height <A>: -0.000
Concentration <■g/L ) : -0.000016
~~~~~~~~~~~~~~~~~~~~~L~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 14298 / Seq. No.: 00020 A/S Pos.: 12 Date: 08/15/94
Replicate 1
Peak Area <A-s>: 0,000
Blank Corrected Pk Height (A): -0.000
Concentration (■g/L ): -0.000010
Ti ■e: 13: 59
Peak Height (A): 0.001
~~~~~~~~~~~~~~~~~~7~ ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 14299 Seq. No.: 00021 A/S Pos.: 13 Date: 08/15/94
Replicate 1
Peak Area <A-s): -0.002
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ): 0.000003
Ti ■ e: 14:01
Peak Height <A>: 0.002
Repl icah 1 Ti ■e: 14:30
Peak Area <A-s>: -0.002 Peak Height (A): 0.002
Blank Corrected Pk Height <A>: 0.000
Concentration <■g/L >: 0.000003 ~~~~~~~~~~~~~~~~~~~~~~~~~~~L~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: HW 13735 EXT ✓-~eq. No.: 00037 A/S Pos.: 28 Date: 08/15/94
Replicate 1 Ti ■e: 14:32
Peak Area (A-s): 0.001 Peak Height <A>: 0.002
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ): 0.000003 Corrected Cone <■g/L ): 0.00006
Hg ID: QC STD Seq. No.: 00038 A/S Pos.: 7
Replicate 1
Peak Area <A-s>: 0.229
Blank Corrected Pk Height (A): 0.032
Concentration (■g/L ): 0.002074
Ti ■e: 14:34
Peak Height (A): 0.034
QC sa■ple is within range 0.00189 -0.00231
Date: 08/15/94
~~~~~~~~~~~~~~~~~~~~~~~~~t~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 13908 EXT U Seq. No.: 00039 A/S Pos.: 29 Date: 08/15/94
Replicate 1
Peak Area <A-s): -0.002
Blank Corrected Pk Height (A): 0.000
Concentration (■g/L ) : 0.000003
Ti ■e: 14: 36
Peak Height <A>: 0.002
Corrected Cone (■g/L ): 0.00006
Replicate 1 Ti ■e: 14:38
Peak Area (A-s>: -0.005 Peak Height <A>: 0.002
Blank Corrected Pk Height (A): -0.000
Concentration (■g/L ): -0.000003 Corrected Cone (■g/L ): -0.00006
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 13920 EXT V Seq. No.: 00041 A/S Pos.: 31 Date: 08/15/94
Replicate 1
Peak Area (A-s>: 0.004
Blank Corrected Pk Height <A): 0.000
Concentration (■g/L ): 0.000010
Hg ID: 13921 EXT / Seq. No.:
Replicate 1
Peak Area (A-s): 0.003
Blank Corrected Pk Height <A>: -0.000
Concentration (■g/L >: -0.000016
Replicate 1
Ti ■e: 14:40
Peak Height <A>: 0.002
Corrected Cone <■g/L >: 0.00019
00042 A/S Pos.: 32 Date: 08/15/94
Ti ■e: 14:42
Peak Height <A>: 0.001
Corrected Cone <■g/L ): -0.00032
Ti ■e: 14:44
P~ak Aiea <A-s): 0.003 Peak Height (A): 0.001
Blank Corrected Pk Height <A>: -0.000
Concentration <■g/L ): -0.000010 Corrected Cone (■g/L ): -0.00019
Replicate 1
Peak Area (A-s): 0.014
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000010
Replicate 1
Peak Area <A-s): ,0. 023
Blank Corrected Pk Height CA): 0.000
Concentration <■g/L ): 0.000029
Ti ■e: 14:46
Peak Height <A>: 0.002
Corrected Cone C ■g/L ) : 0.00019
Ti ■e: 14:48
Peak Height CA>: 0.002
Corrected Cone C ■g/L ): 0.00058
Hg ID: QC CHK Seq. No.: 00046 A/S Pos.: 36 Date: 08/15/94
Replicate 1 Ti ■e: 14:50 {) 1 /) 0.L2..
Peak Area CA-s): 0.209
Blank Corrected Pk Height (A): 0.029
Concentration C ■g/L ): 0.001835
Peak Height CA>: 0.030 ',.., Ii·,_-<._ IA..r'
Replicate 1
Peak Area CA-s): 0.004
Blank Corrected Pk Height CA): -0.000
Ti ■e: 14:52
Peak Height <A>: 0.001
,.~
t4 .L) ,
Concentration;z■g/L ): -0.000010 Corrected Cone~ ): -0.0010 ?-f"
~~~~~~~~~~~~~~~~ ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: B Seq. No.: 00048 A/S Pos.: 38 Date: 08/15/94
Replicate 1 Ti ■e: 14:54
Peak Area <A-s): 0.007 Peak Height <A>: 0.002
Blank Corrected Pk Height CA>: 0.000
Concentration C ■g/L ): 0.000003 Corrected Cone <~ >: 0.0003
Hg ID: QC STD Seq. No.: 00049 A/S Pos.: 7
Replicate 1
Peak Area <A-s): 0.235
Blank Corrected Pk Height <A>: 0.032
Concentration C ■g/L ): 0.002029
Ti ■e: 14:56
Peak Height CA>: 0.033
QC sa■ple is within range 0.00189 -0.00231
Hg ID: 13643 A'--./
Replicate 1
Peak Area <A-s): 0.006
Seq. No.: 00050 A/S Pos.: 39
Ti ■e: 14:58
Peak Height <A>: 0.003
Date: 08/15/94
Date: 08/15/94
~~~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
H9 Ib: 13647 A V Seq. No.: 00058 A/S Pos.: 47 Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.001
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000010
Ti ■e: 15: 14
Peak Height <A>: 0.002
Corrected Cone (ag+-6 ): 0.0010
Replicate 1 Ti ■ e: 15:16
Peak Area <A-s): 0.006 Peak Height (A): 0.002
Blank Corrected Pk Height (A): -0.000
Concentration (■g/L ): -0.000003 Corrected Cone (~ ): -0.0003 ?f
Hg ID: QC STD Seq. No.: 00060 A/S Pos.: 7 Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.238
Blank Corrected Pk Height <A>: 0.032
Concentration C ■g/L ): 0.002055
Ti ■e: 15:18
Peak Height CA): 0.034
QC sa■ple is within range 0.00189 -0.00231
~~~~~~~~~~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: HW 13735 A ✓ Seq. No.: 00061 A/S Pos.: 49 Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.011
Blank Corrected Pk Height CA): 0.001
Concentration C ■g/L ): 0.000081
Ti ■e: 15:19
Peak Height (A): 0.003
Corrected Cone (atg+t:-): 0.0081
~~~~~~~~~~~~~~~7~~~~~~~~~~~~~~-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: B Seq. No.: 00062 A/S Pos.: 50 Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.007
Blank Corrected Pk Height (A): 0.001
Concentration (■g/L ): 0.000055
Ti ■e: 15:21
Peak Height (A): 0.002
Corrected Cone ~ ) : 0. 0055 /-/
Hg ID: QC CHK Seq. No.: 00063 A/S Pos.: 51 Date: 08/15/94
Replicate 1
Peak Area <A-s): 0.209
Blank Corrected Pk Height <A>: 0.028
Concentration (■g/L ): 0.001829
Ti ■e: 15:23 0 1()
Peak Height CA): 0.030
~~~~~~~~~~~~~~~~~~~~~~~i~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: SW 13919 A ✓ Seq. No.: 00064 A/S Pos.: 52 Date: 08/15/94
Replicate 1
Peak Area CA-s): 0.012
Blank Corrected Pk Height (A): 0.001
Concentration <■g/L ): 0.000061
Ti ■e: 15:25
Peak Height <A>: 0.003
Corrected Cone c.a.g-Ar ) : 0. 0061
Replicate 1
Peak Area (A-s): 0.016
~lank Corrected Pk Height <A>: 0.001
Concentration (■g/L ): 0.000087
Ti ■e: 15:27
Peak Height (A): 0.003
Corrected Cone (.-g-ft: ): 0.0087
Hg ID: 13920 A Seq. No.: 00066 A/S Pos.: 54 Date: 08/15/94
Replicate 1
Peak Area <A-s>: 0.005
Blank Corrected Pk Height <A>: 0.000
Concentration C ■g/L ): 0.000023
Replicate 1
Peak Area (A-s): 0.002
Blank Corrected Pk Height <A>: 0.000
Concentration C ■g/L >: 0.000003
Ti ■e: 15:29
Peak Height CA): 0.002
Corrected Cone (~ >: 0.0023
Ti ■e: 15:31
Peak Height CA): 0.002
Corrected Cone ~ ): 0.0003
~~~~~~~~~~~~~~~~~~~~~r~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Hg ID: 13921 A / Seq. No.: 00068 A/S Pos.: 56 Date: 08/15/94
Replicate 1
Peak Area CA~s>: 0.026
Blank Corrected Pk Height CA>: 0.003
Concentration C ■g/L ): 0.000171
Replicate 1
Peak Area CA-s): 0.024
Blank Corrected Pk Height CA): 0.002
Concentration C ■g/L ): 0.000158
Ti ■e: 15:33
Peak Height CA): 0.004
Corrected Cone (■.gi.1.-->: 0.0171
Ti ■e: 15:35
Peak Height CA>: 0.004
Corrected Cone ~ ): 0.0158
Hg ID: 13922 A Seq. No.: 00070 A/S Pos.: 58 Date: 08/15/94
Replicate 1 Ti ■ e: 15:37
Peak Area CA-s>: 0.011 Peak Height CA>: 0.003
Blank Corrected Pk Height CA): 0.002
Concentration C ■g/L ): 0.000106 Corrected Cone (,a.g-,'e ) : 0. 0106
Hg ID: QC STD Seq. No.: 00071 A/S Pos.: 7
Replicate 1
Peak Area <A-s): 0.235
Blank Corrected Pk Height CA): 0.032
Concentration C ■g/L ): 0.002029
Ti ■e: 15: 39
Peak Height CA>: 0.033
QC sa■ple is within range 0.00189 -0.00231
Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.016
Blank Corrected Pk Height <A>: 0.002
Concentration (■g/L ): 0.000100
Ti ■e: 15:41
Peak Height CA): 0.003
Corrected Cone (ag..th--): 0.0100
Hg ID: 13923 A ✓-Seq. No. : 00073 A/S Pos.: 60 Date: 08/15/94
Replicate 1
Peak Area (A-s): 0.011
Blank Corrected Pk Height <A>: 0.002
Concentration <■g/L ): 0.000126
Replicate 1
Peak Area (A-s): 0.017
Blank Corrected Pk Height <A>: 0.002
Concentration <■g/L ): 0.000139
Ti ■e: 15:43
Peak Height <A>: 0.004
Corrected Cone (~ ): 0.0126
Ti ■e: 15:45
Peak Height <A>: 0.004
Corrected Cone (~ ): 0.0139
Hg ID: HW 13908 A Seq. No.: 00075 A/S Pos.: 62 Date: 08/15/94
Replicate 1 Ti ■e: 15:47
Peak Area <A-s): 0.007 Peak Height (A): 0.002
Blank Corrected Pk Height <A>: 0.001
Concentration <■g/L ): 0.000048 Corrected Cone (~ ): 0.0048
Hg ID: B Seq. No.: 00076 A/S Pos.: &3 Date: 08/15/94
Replicate 1 Ti ■e: 15:49
Peak Area <A-s): 0.001 Peak Height <A>: 0.002
Blank Corrected Pk Height <A>: 0.000
Concentration (■g/L ): 0.000029 Corrected Cone <.ag+t: ) : 0. 0029 / ~
Hg ID: QC STD Seq. No.: 00077 A/S Pos.: 7
Replicate 1
Peak Area (A-s): 0.241
Blank Corrected Pk Height <A>: 0.032
Concentration (■g/L ): 0.002048
Ti ■e: 15:51
Peak Height <A>: 0.033
QC sa■ple is within range 0.00189 -0.00231
Date: 08/15/94