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Home My WebLink AboutNCD980602163_19940727_Warren County PCB Landfill_SERB C_Soil Analysis-OCRI"'•---y-•····-··· -· --·•-- I lcallh, l.. :-.-a1ur2I Rc:s.ourcc~ Solie Was1c !'-bnai;cmcn: Division r.o. !)ox 2&'.).!-• ·. Wilmini;ton Sll'l::l ~lc,gn, Nonh C..rolina :!7Gi l Site Number -----------------Field Sample Number WL-~oG"-S:5 Name of Site WA-1<.i2.e.J Gor.JN PG"'B lr,FL Site Location A F"To t-.J NC,. --'--'--..C....:::......:....:=---___:--=;;..._----------- Collected By (;. l'v 1c.H.01...6Q~ Dale Collected ;z_ -:f-;JU LY 9-4 Time I b 15 Agency: Hazardous Waste X Sol.id Waste _· _Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Results (mg/I) Environ mental Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Sol.id (5) WE";.T' ~ ,pt; L"DFL Cadmium ----Chromium --__ Surface water (2) _ Liquid (6) ::::5Ec:P Lead --__ Mercury ~ Soil (3) _ Sludge (1) Sc.lenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul ls (mg/I) (mg/~) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ---- _x_. ~fr?T <(:I, I(? £JPN.. · Cadmium chlordane ----Chloride chlorobcnzcne --// C:iroroium chloroform ------ --__ Copper o-cresol --Fluoride rn-crcsol ------ ·-Iron p-c.rcsol ----Lead cresol ------ --__ Manganese 1, 4-ciich lorobenzcoe -- --__ Mercury 1,2-ciich Io roe.thane -- --Nitrate 1, 1-ciichloroethylcne ----Selenium 2,4-dinitrotolucne ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobcnzenc ----Zinc hexachlorobutadiene Parameti:r ----Results (PCi/1) _pH hcxachloroelhanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta --TDS nitroben1.cnc ----TOC __ pentachlorophcnol -- --__ pyridine Microbiology --__ tetrachlorocthylenc ----trichlorocthylcoe Parameter Results (Col/l00ml) __ 2,4 ,5-lrich loropncnol ----__ 2,4,6-trichlorophenol ----vinyl chloride ----cndrin --lindane -Date Received 7-~-15-:]/I' @eportcd by --__ rncthoxychlor / toxaphcnc 8:-~-?t/1/~ --O;itc Extracted Date Reported 2.~.o -- D.ilc . .\noiyLcd ~-4/-9//1/,P • 942756 __ 2,.~,5-TP (Silvcx) Lab Number DI IS Jl'Jl (llc,iscc :!/91) -- :,;.c.:. Ucpar.mcn1 01 cnvtronmcnt, l lcallh, I,: l\"a1ur.l Rc.s.ourccs Solid Wu1c Manai;cmcnl Division Site Number ----------------Field Sample Number · P.O. Oox ~'--"-" S. Wilmin~on S1rcct Julcii;h, North urolina 2761 l ------------------ Name of Sile WA-1<i2.e.J CborvN Pe,"E, l.DFL Site Location A F"To ~ NC, -~---"-------'--------------- 1 Collected By a. f'v ll.H.01.,..1:;:,0...., Gi ~ s . 'i"E:'PH E..._, Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds --- --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium (;r:'211' 14-3 ---__ Ground waler (1) _ Solid (5) Cadmium --Chromium A IR. 1/cv, --__ Surface water (2) _ Liquid (6) Lead --__ Mercury ){_ Soil (3) Sludge (7) ~l-lT u->/ cC.O Selenium --Silver --_ Other (4) Other (8) :re.-001-$5 -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) .L P&T:GC/MS Arsenic benzene ----Acid:B/N E,,.1. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --F1uoride m-cresol --------Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-di chloroethane --· Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadienc ----Paramett:r Results (PCi/1) pH hex.achlorocthanc ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophcnol -- --__ pyridine Microbiology --__ tetrachlorocthylcne ----trichlorocthylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2.,4,6-trichlorophc:nol ----vinyl chloride --endrin -- '7--:Z. f-f&,P~R c ported by lindane Date Received --__ methoxychlor __ toxaphene Date Extracted Date Reported 2.~-D -- Dale Analyzed 9-!1-94111>£ 942757 __ 2,4.5-TP (Silvex) Lab Number DIIS Jl'Jl (llcviscd 2/91) -- ;--:.C. Dc?~s-mcnl or E.:wironmcnt, I lcalth, k ;s;a1unl Rc.s.ourccs Solid Waste Mana~cmcnl Division SA.MPLE A.1"\ALYSIS REQu'EST Stale L,.t>on1ory or Public Health . P.O. Ik>x 2.SO.li, 306 S. Wilmintton S1n:c1 R.alcii;h, North C.&rolin• 2761 l Site Number Field Sample Number (,L)L -ocJ, _ S.5 ______ ..;;.__.....;;;_ ________ _ ----------------- Name of Site WA-R..2.e..J Cor-JT1 Pc.,"t:, l.DFL Site Location A F"T"o ,-.J NC... --'--'----'--":......:.,_;:::.__---';_:::::._ __________ _ Collected By G. l\J 1c.H.ol,6o~ ID# 3 =f-Date Collected ;2. -=7-:f V L--/ q.4 Time / 4-:£° 3 . ~Te='?H €+.-.) ~ s. Agency: Hazardous Waste X Solid Waste _· _Super fund TCLP Compounds ----- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium 6-t21D 14-3 ---· Ground water (1) _ Solid (5) Cadmium ----Chromium A"~ lJc:JJT --_ Surface water (2) _ Liquid (6) Lead --__ Mercury _){_ Soil (3) _ Sludge (7) ~LIT Lu/ €"CO Selenium --Silver --_ Other (4) _ Other (8) .J. c.-ool-5-S -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul LS(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic bc:.nz.c:.nc:. ----L Acid:B/N E:>..1. Barium carbon tetrachloride:. ----.MTBE Cadmium chlordane:. ------Chloride:. chlorobcnz.~nc ------Chromium chloroform ------ --Copper o-cresol ----Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1, 4-diehlorooenz.eae -- --Mercury 1,2-d i ch 1 oroethane ---- --· Nitrate __ 1,1-dichloroethylene --Selcnium 2,4-dinitrotoluene ----Silver hc:.ptachlor ----Radiochemistry Sulfates hexachlorob~nz.cnc:. ----Zinc hc:.xachlorobutadienc ----Paramdt:r Result.s (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl keton::. --Gross Bela TDS nitrobcnz.enc ------TOC _._ pc:.ntachlorophenol -- --__ pyridine Microbiology ----l ctrachloroeth ylcnc:. trichloroethylcnc ----Parameter Rt:sults (Col /l00ml) __ 2,4,5-trichlorophcnol -- ----__ 2,4,6-t richJorophenol ------vinyl chloride endrin --lind:rnc Date Received 7-2'7-95':~.ilJ-eportcd by --__ mclhm:ychlor D;ite Extracted ,Z~£-j '-f-54/A-13 __ toxaphenc Date Reported 2,.;-D -- D;ite Analyzed Z;-f..-2'-/ ~/J · 942758 __ 2,4,5-TP (S iivex) Lab Nl:mber DI IS Jl'Jl (llc,iscd ..j91) -- I I I i I I ;--;.c Dc?3:":mcn1 o[ E.,,vironmcnl, I lc.alti'I, I,;. ;-.;:i1ur.i i:.uourccs Solie! Waste M.an:a&c:ncn1 Division ~A..'\U'L.t.. ,.,__,Al...,l~l.::, J:U:..~u.c:...::,1. ~1a1c uoorlllory 01 ru01,c 11ca11r, P.O. lk» ~7. 305 S. Wilmini;ion $1r:::: lulci;;i'I, Noni'I urolina ::?7Gl i Sile Number -----------------Field Sa.rn plc NuI:Jbcr __ _:lV:___L __ -..:::o_cJ~..:::b_-_s_S _____ _ Name of Sile WA-Q.;2.e.J Gol'Jrt Pc,"E, l.DFL Site Location A F"To 1'.J NC _..;..__.....;._;;;....;..-=--. __ .;.....:~----------- Collected By 6. f'v 1c.1-to1,.. 6c:n-..l Date Collected ~~ 'JVLY CJ-4 Time /4-£'°3 H Gz 'STEP e,..:>:. Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Rcsults(mg/1) En"irnnmcnt:il Concentr:ite Comments Arsenic --Barium ---· Ground waler (1) _ Solid (5) G-ei:P 14-3 Cadmium ----Chromium A, JZ.. l/eA.JT --Surface waler (2) _ Liquid (6) Lead ----__ Mercury .½_ Soil (3) _ Sludge (7) ;;::,pLIT LL.)/ cCO Selenium --Silver --_ Other (4) _ Other (8) ..l. C. -OOl-$S -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Ori;nnic Compounds Results(mg/1) P&T:GC/MS Arsenic benz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------ x . ~~r< o, /IJ /f!/1/'l-Cadmium chlordane ----Chloride chlorobenzenc ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-crcsol ------ --Iroo __ p-cresol --Lead crcsol ------ --__ Manganese 1, 4-dich I orobenzen e -- ----Mercury 1,2-dich loroethanc -- --Nitrate 1, 1-dichloroethylcne ----Selenium 2, 4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenz.ene ----Zinc hexachlorobutadiene ----Paramelt:r Results (PCi/1) pH hex.achloroethanc ----Gross Alpha --__ Conductivity methyl ethyl ketone --Gross Beta TDS nitroben7.cnc ------TOC pcntachlorcphenol ---- ----pyridine Microbiology ----l etra chloroet hylcne ----trichlorocthylcne Parameter Results (Col/l00ml) __ 2, 4,5-trich lorophcnol ----__ 2,4,6-trichlorophcnol ----vinyl chloride ----endrin -- - Date Received 7-,,,::?9-f fL~&A-cportcd by lind:rne --mcthoxychlor -- ?-~-f0<//~ Date Rcporled --toxaphenc Date Extracted 2,-:!-0 -- '3"-//-9~-Y~. 942759 __ 2,4 ,5-TP (S:l·:cx) Date Analy1.cd Lab Nl!mber DI IS 31'JJ (Rcviscc 2/91) -- I I I I I leallh, t:. 1'a1ural Ruourres Solie Was1e Manai;cment Division Sile Number ---------------- . P.O. D.ox ~7. 306 S , Wilmin'1on Str.:ct R.Alcii;h, North Carolina ::?761 I Field Sam plc Num bcr_---=:...W____:L:__-_:;o___;;;e;__:;7-_-.:....:5_.S~------ Name of. Sile WA-1<.:2..e.J Gor.JT'1 PG"Ei l.DFL Site Location A F".;..o i-.J NC _.:.......;.._...:....=:.....:..:::~-.:...::.-=----------- Collected By G. l'v •LH.ol.6c>)-..) Dale Collected .:Z ~ "JOLY 9 + Time /5 /Z- ~ . $TE"Pf1 e-,-..,S Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---__ Ground water (1) _ Solid (5) (aRID 13-1 Cadmium --Chromium A-112. 1/FJJT --Surface water (2) Liquid (6) Lead ---__ Mercury _5__ Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) _ Other (8) --' -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------ L pa; <O./t:J ,/#1'1\... Chloride chlorobenz.ene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-creso! ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rotolucne ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenz.ene ----Zinc hexachlorobutadiene ----Parameter Resu I ls (?Ci /1) pH hexachloroethane ----__ Gross Alpha --Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenz.ene ------TOC pentachlorophcnol ---- --__ pyridine Microbiology ----t etrachlo roet hylene ----trichloroethylcoe Paramcler Results (Col/lO0ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ------vinyl chloride cndrin -- 7-;'f-f&tJ&J lindane --·Date Received Reported by mcthoxychlor -- Y-~-9¢-Y/J --toxaphene Date Extractccl Date Reported ?.,~-0 -- Dale Analyzed '1?-'l(-991/r?_ Lab Number 942760 ?.,4,5-TP ($ibex) DI IS :l!'JI (Revised ::?/91) -- I I I ! I I i'.C... Uc?ar.mcnl ot .t:.nY1ronmcn1, I lcallh, & 1'a1unl Ru.ourccs Solie! Waste Manai;cmcn1 Division . P.O. Ilox :.50!7, 306 :,.;. Wilmin&"on S1n:c: R.alcii;h, North C:.,rolina 2761 I Sile Number -----------------Field Sample Numbcr_....:;;U:::....·_1.._-_tJ_fJ_~'----::S_S _____ _ Name of. Site WA-RO-e.J C1orJT'1 PG1:, l.DFL Sile Location A F".;..o ,-J NC ·-..!.....:~_:..;::::..:.::::_ _ _:_.:....::::::;_ __________ _ C~llected By a. f\) l(.H.Ol,6,c))...) Dale Collected J. ?-:1 0 LY 9 + Time /~/5" ~ s T~?t1e...::l~ Agency: Hazardous Waste X Solid Waste ___ SuperfUDd TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental· Concentrate Comments Arsenic --Barium ---__ Ground water (1) _ Solid (5) 6R1!) 11-Z. Cadmium --Chromium A1R V£JJ, --Surface water (2) _ Liquid (6) Lead ----__ Mercury L_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --' -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Re.suits (mg/I) (mg/kg) Organic Compounds Rcsul ls (mg/I) P&T:GC/MS Aisenic benz.cne ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------..L Pa; < t7, /I? R_/'nt. Chloride chlorobenzene ----r Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-crcsol ------ --Iron p-crcsol ----Le.ad ere.sol ------ --Manganese 1,4-dichlorobcnzenc ---- --__ Mercury 1,2-dichloroethane ----Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotolucnc ----Silver __ heptachlor --Radiochemistry Sulfates hex.ichlorobcnzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcx.ichloroelhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC pcntachlorophcnol ---- --__ pyridine Microbiology ----tctrachloroethylenc ----trichloroethylcac Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophcnol ----__ 2,4,6-trichlorophcnol ----vinyl chloride ----cndrin -- Dote R~ceived 7-::lf--f9(-f!1clZJRcportcd by lind:rne --mcthoxychlor -- Date Extraclcc.l ~-P<-?L/-v~ __ toxaphene Date Reported 2,4-0 -- Dale Analyzed Y-~91/-Y ,,P . 942761 __ 2,4,5-TP (Sil·.•c:x) Lab Number DI IS J!'Jl (Revised 2/91) -- I lc311h, & r--~1unl Rc.s.ourcc:s Solid Waste Manai;c:mcnt Division P.O. Oo1. 2.50-:7, 306 S . Wilmintion S1r:c1 ~lcii;h, North urotina 27611 Site Number -----------------Field Sample Numbcr __ W;;___L_-_0_().;;;;.._'j-'--• .....;S;......;;;;5 _____ _ Name of Site WA-1<..:2..e.J Cor-JN PGt!:> U,FL Site Location A F".;..o 10 NC . _ _.!.....;_...;...:::;...:_;:__ __ :........;::::...._ __________ _ Collected By a. f\) l(.H.Ol.,6c),-) Dale Collected J. ?-'JOLY 9 + Time /S"Z.o ~ . S'TEPH e-.._,'S Agency: Hazardous Waste X Solid Waste __ Super fund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) G1<1p ID-I Cadmium -- flc;J, Chromium A,R --__ Surface water (2) Liquid (6) Lead --__ Mercury --~ Soil (3) _ Sludge (T) Selenium --·----Silver --·-_ Other (4) Other (8) --' -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resu!Ls (mg/I) (rng/kg) Organic Compounds Resulls(mg/1) P&T:GC/MS A.rsen.ic benz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------L Pa; <P,/~~n'C Chloricie chlorobenzenc ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride rn-cresol ------ --Iron p-crcsol ----Lead cresol ------ --Manganese 1,4-dichlorobenzcoe --------Mercury --1,2-ci ich I oroet hane --Nitrate 1, 1-dichloroct hyicne ----Selenium 2,4-dinitrotoluenc ----Silver hcptachlor ----Radiochemistry Sulfates hexachlorobcnzene ----Zinc hexachlorobutadicne ----Parameter Results (PCi/1) pH hcxachlorocthane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnz.ene ------TOC __ pentachlorophenol -- --__ pp·idine Microbiology ----tctrachloroethylcn e ----trichloroethylcnc Parameter Results (Col /lOOml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ------vinyl chlorid: --cndrin -- o·eitc Received J-,7..f~ftft/;? ,61)_ Reported by lindanc --mcthoxychlor .? -- D:.Jtc Extracted ?-;i-?~# --toxaphenc Date Reported 21~.o -- D.itc Analyzed '5'-¢-9~/2 942762 2,4,5-TP (Sibcx) Lab Number ) I IS J l 'Jl ( llcviscC 2/91) -- ''•"'--_ ... ,.., ...... -, •• ...,, .....i;, .. , ................ . l lc~lth, l: 1':alunl R=urccs Solid Was1c M1nai;cmcn1 Division ....,r,..,;,,.,.a..i. J..JJ..J r-,,...;,,.. ~r,...,_,""' ....,,.,..., •-x ---- . P.O. Oox ::.SO-:i, 306 K WilminG'lon S1r.:c1 ~lcii;:i, North urolin1 :?761 l Sile Number Field Sample Number W L -O I~ -S5 ______ ..;__ _________ _ ---------------- Name of Site WA-'?.i2e.J GorJTY PG°"B U>FL Site Locatioo A F".;-o ,-J NC.. _.;...._ _ __;;;_;_;:'---_;__;_-=----------- Collected By (;. (\) , c. H.o 1,.. 6c>"-' Date Collected :J.~ :JOLY 9+ Time IGZ4 G; $ 5, ,-b"?~E~ Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---_ Ground waler (1) _ Solid (5) G1<1p 9-Z. Cadmium --Chromium A-,R. ilc:A.J T --__ Surface water (2) _ Liquid (6) Lead -- --Mercury _K_ Soil (3) _ Sludge (1) Selenium --Silver --_ Other (4) Other (8) --' -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (rng/k.g) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachioridc ------.MTBE Cadmium chlordane ------_L pa; <~./t?#;rt_ Chloride chlorobcnzenc ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol --------Iroo p-crcsol ----Le.ad cresol ------ --__ Manganese 1, 4-dichl orobenz.eoe -- --__ Mercury --1,2-d ich I orocthane --Nitrate 1, 1-dichloroethyienc ----Selenium 2,4-dinitroloiucnc ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobcnzene ----Zinc hexachlorobu1adiene ----Parameter Results (PCi/1) pH hexachloroethanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzenc ------TOC __ pcntachlorophcnol -- --__ pyridine Microbiology --__ letrachloroethylenc ----trichlorocthylcoc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophcnol --__ vinyl chloride --cndrin -- -Date Received 7-A'? -'1&f Lf'l2 Reported by lindane --methoxychlor -- Dale Extracted "J?-,,;2.. -9~7/~ --toxaphene Dale Reported 2,~-0 -- Dale Analyzed ~-1/-~fi • 942763 2,4,5-TP (Silvex) Lib Number 1)1 IS J!'JI (llcviscd 2/Yl) -- i'.C. Dcpar.mcnt Ol 1::;.n,.,,ronmcnt. 1 lcalth, &: /':atural RC-5-0urccs Soliel Waste Manai;c:mcnt Di,-isior. Site Number V/':\,J,T.L.J. J..JJ,j r,..J, ,r,,...,,..,,,J. ._JJ..t.J •-x ----. P.O . Ilox :!50-li, 306 S. Wilmint1on Strc:ct R.alcii;h, North Carolina 2761 I -----------------Field Sample Numbcr_-'W:;___/.._-_t).....;/_/_-_S_S ______ _ Name of Sile WA-R..:2-e.J CooNn' PG-P, lr,FL Site Location A F".;.-o ~ NC, _..:....;. _ __;__:~::::._ _ __;_;;_:::;__ __________ _ Collccled By ~. (\) tLH.oL6e>._, Dale Collected :Z ?-'JO LY 9+ Time IG2'- ~ s T~i>t(E),.jS. Agency: Hazardous Waste X Sol.id Waste _· __ Supcrfund TCLP Compounds ------ Sample Type Inori,:anic Compounds Results(mg/1) Environmental Concen tra le Comments Arsenic ---Barium ---· _Groundwater (1) ._ Sol.id (5) GRID q-3 Cadmium -- An2 Chromium //~NT --Surface water (2) _ Liquid (6) Lead ---- --Mercury _K_ Soil (3) _. Sludge (7) Selenium --Silver --_ Other (4) _. Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Result.s(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS A.rseruc benz.ene ------ Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------ ..L Pc;::.$ <o,ld #/'K_ Chloride chlorobenzene ----Cruomium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese 1,4-dichlorobenzene -- --Mercury 1,2-di ch l orocthane ---- --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hcxachlorobenz.ene ---- Zinc hexachlorobutadiene ----Paramelt!r Results (PCi/1) _pH hcxachloroelhanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzene ------TOC __ pentachlorophcnol -- --__ p)7idine Microbiology ----t etrachlorocth ylene ----trichlorocthylcnc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichJorophcnol ----__ vinyl chlorid:: cndrin -- -Dale Received 7-.2 9-Wv/ ,4?Rcportcd by lind:inc --__ methoxychlor > Dale Extracted ?-~-f'Y# __ toxaphcne Date Reported 2,~-0 -- Dale AnalyLed "i?-s-9¢-VP 94276l\ __ 2,4 ,5-TP (Sil·:cx) Lab Number DIIS JI')! (Revised 2/Yl) -- ;-.L.. Uc?ar.mcnt 01 .::.,,v,ronmcnt, I lcallh, & 1'atunl R=urccs Solid Was1c Manai;cmcnl Di,-ision Vr>JtJ.J. J..JL:J .M,,..1,r,,,,.,,J,,,J.1-..JA.,..J "'"'-""-'..! _...,....,,..., • . P.O. Box ::S0-:7, 306 S. Wilmin~on Sire:: R.alcii,:h, North Carolina ~7611 Site Number -----------------Fic:ld Sam pie Numbcr_....:W:;_:,_...:L,.;__-__::.t)_/=---=2;_-___,;;;~_S~------ Name of Site WA-R-2.e.J GorJrt PGt;, l..DFL Site Location A F"-;..o"' NC, -..:..--....;...;:c....:..:=_ _ _;_;_a::;_ __________ _ Collected By a. f\) tU•-t.O l.. f:>C)~ Date Collected :2 1-'JO LY 9 + Time. IS-30 ~ :n-e PHE~S Agency: Hazardous Waste X Sol.id Waste _· _Supc.rfund TCLP Compounds --- --- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· _ Ground waler (1) _ Sol.id (5) 61<1D ~ -z. Cadmium -- A1t2 Chromium llt=JJ r --Surface water (2) _ Liquid (6) Lead ---- --Mercury ~ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul ls (mg/l)(rng/kg) Organic Compounds Resul ls (mg/I) P&T:GC/MS Arseruc benzene ------Acid:B/.N E>-1. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------..L. pa; <o,/PL.lhn tt __ Chloride chlorobenzene --,,, Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-crcsol --------Iron __ p-crcsol --Lead ere.sol ------ ----Manganese --1,4-dichlorobenzeoe --__ Mercury 1,2-dichloroelhane -- --Nitrate 1, 1-di chloroeth ylcne ----Selenium 2, 4-di nit rot ol uene ----Silver heptachlor ----Radiochemistry Sulfates he""3chlorobcnzene ----Zinc hc.xachlorobut adiene ----Parameter Results (PCi/1) pH hc""3chloroelh ane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS nilrobenzene ------TOC pcntachlorophenol ---- --__ pyridine Microbiology ----tetrachloroelh ylcne ----trichlorocthylcoc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2, 4,6-l richl oro phenol ----__ vinyl chloride endrin -- Dale R~ccivcd '7 --v< f-'1~ tfi}Rcportcd by lind:inc --mclhoxychlor -- Dille Extracted '?-~-f,¢-Y/J __ toxaphenc Dale Reporled 2,~-D Dille AnalyLcd ~-S-9~1/P --2,4,5-TP (Silvex) Lab Number 942765 DI IS J!'Jl (Revised 2/':11) -- I l lcallh, & l'-atur.al Re.sources Solid Wiste Manatemcnl Division . P.O. rk,x :S.0.:7, 306 ?'-. Wilmin~on ::,1rcci R.alcii;h, North Carolina 2761 I Sile Number _________ ...;.... _____ _ Field Sam pie N umbcr_--=L,U~-=-'---_t)----'-/....::3:::,__-_S_S. _____ _ Name of Site WA-1<.:2.e..J GorJN PC"E, U:,FL Site Location A F".;.-o ,v NC _.:...;....;__...:....:::....:..::::....__..:.....:.-=----------- Collected By c;;. f\) ,u-tol.6o...._, Dale Collected .:'4 ?-'JO LY 9 + Time l5"37.... . '=>T'==?""t ~ ~s. Agency: Hazardous Waste X Solid Waste __ Superfu.nd TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---__ Ground waler (1) Solid (5) GR1!) Z -l Cadmium --Chromium A,R (1£;.J r --Surface water (2) _ Liquid (6) Lead ----__ Mercury _5._ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --' -- .. --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arse::i.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------_L P(k <o./dqR,n Chloride chlorobenzene ----~ Chromium chloroform ------ --Copper o-crcsol --.. --Fluoride m-cresol ------ --Iron p-crcsol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzenc -- --__ Mercury 1,2-dichlorocthane -- --Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) _pH hex.achloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta --TDS nitrobenz.ene ----TOC __ penlachlorophcnol -- --__ pyridine Microbiology ----tetra chloroeth ylcnc ----lrichlorocthyl::nc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichJorophenol ----vinyl chloride --cndrin -- Date Re.ceivcdJ-,?9-f~ll/d. Reported by lind:ine --__ mclhoxychlor T--41-f&,o --toxaphcnc Dale Extracted Date Reported 2,~-D -- Date Analyzed %-S-9t;£"1/p . 942766 _ 2,4,5-TP (Sil..,ex) Lab Number l)IJS Jl'JI (Revised 2/91) -- uc?~~mc.n" 01 .c:,nv,,ronmcn .... :alth, l,:. 1'a1ur.l Rc..s.ourccs j Waste 1',fanai;cmcnt Division : Number ----------------Field Sample Number • r.o. Oox ~,,.JOO ..... n11m101,u,,11 -··--· R.alcii;h, Nonh C.rolina 2761: ----------------- me of Site WA-1<..2.e.J GorJn' · PG"B u,FL Site Location A F'10 ~ NC., -'------"_;_;::'-----=----------- llected By ~. /'v ,u-t.o \... 6c>"'-' ID# ~Ff· Dale Collected .:Z ?-'JO LY 9 + <:. ';, TeP-t-i €.._,S :ency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---_ Ground waler (1) _ Solid (5) 6Rt!) 5-l Cadmium -- A,R Chromium lJeJ..JT --Surface waler (2) _ Liquid (6) Lead --- --Mercury ~ Soil (3) Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) --I -- --Organic Chemistry Inorganic Chemistry -- : 'arameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benz.ene -----Acid:B/N Ext. Barium carbon tetrachloride -----.MTBE Cadmium chlordane -----<o,ltJ4m.. L Pc;& Chloride chlorobenzene --, Chromium chloroform -----__ Copper o-cresol ---F1uoridc m-cresol ----- -Iron __ p-cresol --Lead cresol ----- -Manganese --1, 4-d ichl orobcnzeoe -- -__ Mercury 1)-dichloroethane -- -Nitrate 1.1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor Radiochemistry Sulfates he:x:.:ichlorobenz.ene ----Zinc hexachlorobutadiene ----Jara meter Results (PCi/1) pH he:x:.:ichloroethane ----_ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.ene -----TOC __ pcnlachlorophcnol -- --__ pyridine Microbiology ----tctrachlorocthylcne --__ trichloroethyleoc 'aramcter Results (Col/l00ml) __ 2,4,5-trichlorophenol -----__ 2, 4,6-trichlorophenol -__ vinyl chloride --endrin -- 7 .... ,;zq-f~~Rcportcd by lind:ine )ate Received --__ methoxychlor 45-~-ft/1,/I) __ toxaphcnc ):itc Extracted Date Reported 2,4-D -- ).itc Analyzed ?-S-97'1/17 : Lab Number 942767 __ 2,4,5-TP (Sil'✓cx) llJS J!'Jl (llcviscd 2/91) -- I I I I - ;--.C. Ucpar.mcnl of .l:.:wironmcnt, l lcallh, l,;. 1'a1ur.l Rc:.s.ourccs Solid Waste Manai;cmcnl Division . P.O. 13ox lSD-:i, 306 K Wilmin~on S1~c1 !ulcii;h, North Carolina 2761 I Site Number ----------------Field Sample Number_-'W'---_L._-_0--:/_5_---':S'---S _____ _ Name of. Site WA-R.'2.e.J Go,SN 'PG"B l.DFL Site Location A F".;-o t-J NC -~-..;...;:;c...:..::::___.;_;_..=----------- Collected By ~. f\J •CH.ol,6C>"-' Date Collected :J. ~ JOLY 9 + Time /~30 6i . STEP~~ s. Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compou.nds ----- .• Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· _ Ground water (1) _ Solid (5) G~1D 4-8 Cadmium --Chromium A-112 1/E>.JT -- Surface water (2) _ Liquid (6) Lead ---- --Mercury .K_ Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) --' -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Orgonic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------<o./~m. ...L pa; Chloride chlorobenz.ene ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride rn-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-d i ch lorocthane --Nitrate 1,1-dichloroethylcne ----Selenium 2,4-dinitrotoiuene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzenc ----Zinc hexach lorobut adiene ----Paramett:r Results (PCi/1) pH hexachloroethanc ----__ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC pentachlorophcnol ---- --__ pyridine Microbiology --l etrachloroethylcne --trichloroethykoe P.1r.imcler Results (Col/lOOml) --= 2,4,5-trichlorophenol ----__ 2,4,6-trichJorophcnoi ----vinyl chlorid:: ----endrin -- Dale R::ceived r:Z'l-9~ M Reported by lind:rne --melhoxychlor .,, -- Dal:: Extracted '%~-fl/rt' --toxaphene Date Reported 2,~-D -- Dale Analyzed '5?-S-t}L,/1//!' 942768 __ ::?.,4,5-TP (Silvex) Lab Number DIIS JJ'Jl (Revised 2/YI) --i ·'-uc:.;.,~•.un .. 1u u;. .::.n..,'lronm~n1.. I k2llh, l:. 1'21ural Ru.ou:-cu ,lid W2s1c M2n2i;cmcnt Division ite Number i,,,.Jl"'ll,,J.f.L,L ,lo.J,l,,,.,J ,,_ ··-------"----• . P.O. 11ox 260,:i, J06 S. Wilminpon Street ~lcigh, North Carolina 27611 Field Sample Number W L. -c) I~ -5 S ----------------- ~ame of Sile WA-R..2.€:.J C1or.JN PG'B U,FL Site Localioo A F"To ~ NC, _.:....; _ _;_::...:,;:::__ _ _;_~::;_ __________ _ :ollcctcd By b . f\) 1cH.ol..6C>~ Dale Collected 2 ;z.. · :JULY q4 Time /6~ I ~ . ST~PMeuS. \gency: Hazardous Wasle X Solid Wasle __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concen tr:i le Comments Arsenic --Barium ---· Ground waler (1) _ Solid (5) GJ21D eJ-,JI Cadmium --• --Chromium --/y,vsE Surface waler (2) _ Liquid (6) e~p Lead ----__ Mercury .£_ Soil (3) _ Sludge (7) Selenium --Silver --_ Olher (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Results(mg/1) Parameter Rcsul ts (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arseo.ic benzene ------Acid:B/N E>-1. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ----< (7, /(7,t:J,Mt _x_ Pc.'13 Chloride chlorobenz.ene ----,, Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------ --Iron p-crcsol ----Lead cresol ------ --· --Manganese --1, 4-diehlorobenz.coe ----Mercury --1,2-d ich I oroethane --Nitrate 1, 1-dichloroethylcne ---- Selenium 2,4-dinilrotoluenc ----Silver __ hcptachlor --Radiochemistry Sulfates hex.achlorobenzcnc ----Zinc hcxachlorobutadicne ----Parameter Results (PCi/1) --pH hex.achloroethanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS nitrobenzcne ------TOC pcntachlorophenol ---- --__ pyridine Microbiology ----I elrachloroethylene --__ trichloroethyleoe Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trich.iorophcnol --vinyl chloride ----endrin --lindane Date Received 1-2~-f0t¥'AlJ. --Reporlcd by __ melhoxychlor ,;, loxaphenc ?-//-'/'/{Ill --Dale Extracted Date Repon::d 2.~-0 -- Date Analy,.cd 4Ji: :J"-91,/11/? 942769 __ 2,4,5-TP (Silvcx) Lab Number --DI IS Jl'Jl (llcviscd 2/91) I I ~ uc.p.Jr.mc:u O! .c.:,-.,ronmcnt, lc:)lth, & 1'a1ural R=urccs lid Wasic :-.bnai;cmcnt Division · P.O. flex ~i. 306 1'. Wilmin~on Stn:ct ~lcii;h, North ~roiin• :!7611 le Number -----------------Field Sample Number W L -c) 17 -.S.S amc of Site WA-R.i2e.J Cborvrt PG"B LI)FL Site Location A F"To .-.J NC.. _.:....;. _ __;,_;::....:.,:::._ _ _;_;:_;:::::.._ __________ _ Date Collected 2. ?--:JULY q4 Time /~ob . ~-p H E'i>-:) "S .gcncy: Hazardous Waste X Sol.id Waste _· _Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentr:ite Comments Arsenic --Barium ~ ---· _ Ground water (1) _ Solid (5) 412rp 'ff I 10 Cadmium --Chromium --_ Surface water (2) _ Liquid (6) Lead --__ Mercury X Soil (3) Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistr;· Inorganic Chemistry -- ; Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rtsults(mg/1) P&T:GC/MS Arseo.ic benz.enc ------Acid:B/N Ext. Barium carbon letrachloride ------'MTBE Cadmium chlordane ------...L Pc-a <O·/~,t1,_ Chloride chlorobenz.cne ----Chroc:i i urn chloroform ------ --__ Copper o-crcsol --Fluoride m-cresol --------Iron p-cn:sol ----Lead cresol --------Manganese 1,4-dichlorobenzeoe ---- ----Mercury 1,2-d ichlorocthanc ----Nitrate __ 1,1-dichloroethylcnc --Selenium 2,4-dinilrotolucne ----Silver __ heplachlor --Radiochemistry Sulfates hcx.achlorobenzene ----Zinc hexachlorobutadicnc ----Paramdcr Results (PCi/1) _pH hcx.achlorocthanc --__ Gro~s Alpha __ Conductivi ty --methyl ethyl ketone .. Gross Beta TDS nitrobcnz.cnc ------TOC __ pcnlachlorophcnol -- --__ pyridine Microbiology ----l etra chlorocthylcnc ----trichloroethylcnc Par;imcler Results (Col /l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichiorophcnol ----vinyl chloride ----cndrin -- Date Received J-,l'l-fYt/f .GiJ lindanc --Reported by __ methoxychlor Date Extracted ?-7"-9'/-Y// --loxaphcnc Date Reported 2,4-0 -- Dale Analy1.cd 'i'-S"-90/p 942770 __ 2,•1,5-TP (Silvex) Lab Number DI IS Jl'Jl (llcviml 2/91) -- ulth, l,.:, 1'a1ur.l Ruourccs ii! Was1c M~n:.i;cmcnt Oi,-ision e Number -·-··· --·-··-------..... ----. P.O. Oox ~i. 306 1'. Wilminb'on Su-eel R.alcii;h, North urolin• 17611 Field Sample .Number WL -c) l4S -$S ---------------- 1me of Site WA-R.i:2..e.J Gol'-lTY PC-1:> l.DFL Site Location A F"To >-J NC.., _..:.....;. _ _;_;;:;__:_:::___...:......:.-=----------- :>llcctcd By ~. fv •LHo L 6cn--' ID# 3=?-Date Collected 2. ;i. ::JULY q4 Time / t I 3 G . 'SrcP1-tE>.J.S. gency: Hazardous Waste X Sol.id Waste __ Superfund TCLP Compounds ---- Sample Type Ino~anic Compounds Resulls(mg/1) Enl'ironmcntal Concentrate Comments Arsenic --Barium ---_ Ground water (1) _ Solid (5) GIZ ID 27,o Cadmium --Chromium -- _ Surface water (2) _ Liquid (6) Lead -- --Mercury L Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- --·• --Organic Chemistry Inorganic Chemistry -- ' Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Aisenic benz.ene ------ Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------_x_ Pc..13 <tJ./tJ~ Chloride chlorobenz.cne ----Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobcnzene ----Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexach lcirobutadienc ----Parameter Results (PCi/1) _pH hcxachlorocthanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC pentachlorophenol ---- ----p)'ridine Microbiology ----l ctrachloroeth ylcne ----trichloroethylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trich.iorophcnol ----vinyl chloride ----endrin -- Da1c Received 7-~f:£r/--//(6,a lind:rne --Reported by mcthoxychlor -- Y-'l-f1£11/J --toxaphene Date Exlraclcr.l Date Reported 2,~-0 -- Dale Analyzed S--s-?4L-rP ·. 942771 2,4,5-TP (Silvcx) Lab Number Di IS Jl'Ji (llcviscd 2/91) -- lcallh. l.:. 1'21 .. ral R=urccs ,id W2s1c M2n2i;cmcnt DiV'ision Le Number ----------------- r.O. !>ox 2.SO-:i, 306 K Wilmin~on S1rcct R.alcii;h, North Carolina 27611 Field Sample Number W L -0 I 'l-S .S ame of Site WA-1<.i2..e.J CoorJT'7' Pee, l.DFL Site Location A F"To ~ NC -~--;;,,,,,,,,;,,,.=._ __ ,;,__;::;;.._ __________ _ ollccted By G. f\.) 1CH.Ol,6c,~ Da!.e Collected 2. ?--:JUL 'Y q4 Ti.me It I 9 ~Sit PH c)...)S .gcncy: Hazardous Waste X Soud Waste _· __ Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Solid (5) GR1D 3e;,4 Cadmium ---Chromium --Surface water (2) _ Liquid (6) Lead --- --Mercury )( Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Resu Its (mg/1) Parameter Re.suits (mg/1) (mg/kg) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N fa1. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------_x_ 'PC-13 <P,/~ Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-crcsol ------ --Iron __ p-cresol --Lead crcsol ------ --Manganese --1, 4-dichlorobenz.en::. -- ----Mercury --1,2-dich lorocLhanc --Nitrate 1, 1-dichloroeLhylc:nc ----Selenium 2, 4-dinit rotolucnc ----Silver hcptachlor ----Radiochemistry Sulfates hcX2chlorobenzene ----Zinc he.xach lorobut adicnc ----Paramett:r Resu I ls (PCi /1) _pH hcX2chloroctha_nc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.cnc ------TOC pent achlorophcnol ---- --__ pyr idine Microbiology ----t cLrachlorocth ylcne ----Lrichloroethylcnc Parameter Results (Col/lO0ml) 2,4 ,5-trich lorophcnol ------__ 2,4 ,6-trichiorophcnol --vinyl chloride ----cndrin -- Date Received Z.-~f~.&Rcportcd by lindanc --mcthoxychlor -- 'i'-L/-9'/1!c'__ Date Reported --toxaphcne Dale Extracted 2.~-D -- Dale AnalyLcd 3-S-9~....c?__ LJb Number 942772 __ 2,•1 ,5-TP (Silvcx) I) I IS J l 'Jl ( Revised 2/\Jl) -- lcalth, l,;. 1'a1unl Rc.s.ourccs ,lid Waslc Management Division i1e Number ----------------- P.O. fkix 2SO-:i, 306 S. Wilmini;ton $1rcc1 R.alcigh, Nonh urolina 27611 Field Sample Number W L -c) 2 ~ -!5S fame of Site WA-'2..:2.e..J Gorvn' PC.t:> U,FL Si1e Location A F",o t-J NC. _..!....,.; _ _;;_;:;_;_;:::_ _ _..:....:._..:::::::._ __________ _ :ollecttd By ~. i'v I CH.o \.. 6cn--' Date Collected 2. -:;z.. ~UL Y q4 Time /~ Z I ~ . $-re'PH-EN S. 1.gency: Hazardous Waste X Scud Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· (i ..e JI> 38, lb Ground water (1) _ Solid (5) Cadmium ----Chromium --Surface water (2) _ Liquid (6) Lead ----Mercury --L Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resui ts (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane --<P,717~ ----..x... Pc..'6 Chloride chlorobenz.ene ----Chromium chloroform ------ --__ Coppe~ o-c:-csol --Fluoride m-crcso! ------ --Iron p•crcsol ----Lead cresol ------ --__ Manganese --1,4-dichlorobc:-iz.c..:ic. ----McrCU:)' --1,2-d ich lorocthane --Nitrate 1, 1-ciichloroelhylcnc ----Selenium 2,~-dinit rotol ucnc ----Silve~ __ heptachlor --Radiochemistry Sulfates hex.a ch 1 or obenz.ene ---- Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcxachlorocthane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS nitrobenz.cnc ------TOC __ pcntachlorophcnol -- ----pyridine Microbiology t clrachloroethylene ----trichlorocthylenc ----Parameter Results (CCJl/l00ml) __ 2,4,5 -trichlorophenol ----__ 2,4,6-trichiorophenol ----vinvl chloride ----cndrin -- Date R::.ccivcd 7-_tf'-77'1/.f,.ij2 Reported by lind3nc --mcthoxycnlor -- Oat=. Exlraclcc.l ?-,I -ff ""J/,f) --tox.:iphenc Date Report::.d 2,~-D -- Dale Analy,:cd j'-S-9~V,.O __ 2,4,5-TP (Silvcx) Lab Number 942773 DI IS Jl'Ji (ltcviscd 2/91) -- 3Jlh, l,:. l',:~1ural Ruourccs P.O. nox lS,l.),,., • .)l.J;J '"· YTJIIH• .. b·-·· --- ! Was1c M~n~i;c:mc:nt Di,-i.sion lulcii;h. North urolin• 2761 i : Number Field Sample Number WL -c) Z 1-S~ ----------------- me of Site WA-1<.2.e.J C,o,.JT't PG'"B l.DFL Site Location A FTo ~ NC _.!.....,;,_....:....;=-.:..::::__....:....;.:........::=------------- llected By a. I\) IC,HOL,'6C)).,.) Date Collected 2 ?-:JULY q4 Time / l, Z b ~ . 5TEPMe,..::,.~ ;ency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· -Ground waler (1) Solid (5) G121P 42, zg Cadmium --Chromium --Surface water (2) _ Liquid (6) Lead --- --Mercury ~ Soil (3) _ Sludge (7'; Selenium --Silver --_ Other (4) Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benz.cne ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------<o./P#.M _L Pc.13 Chloride chlorobenz.ene ---- Cb.romiux chloroform ------__ Copper o-cresol ----Fluorid:: rn-crcsol ------ --Iroo __ p-crcsol --Lead crcsol ------ --__ Manganese --1, 4-d ich I orobcnz.coc ----Mercury --1,2-d i ch loroethane --Nitrate 1, 1-dichloroethylcnc ----Selenium 2,4-dinilrotoluene ----Silver hc:ptachlor ----Radiochemistry Sulfates hex;ichlorobenz.ene ----Zinc hexachlorobutadicnc ----Parameter Results (PCi/1) pH hcx;ichloroethaoc ----__ Gruss Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnz.cne ------TOC __ pc:nlachlorophenol --pyridine ----Microbiology ----t ctr a chlorocth ylcnc ----trichloroethylcnc Parameter Results (Col/lO0ml) · __ 2,4,5-trichlorophc:nol ------__ 2, 4,6-trich.iorophenol --vin!•I chlorid:: ----cndrin --lind:rne Date Received 7-,.,1 ';-9//t/(8/J Reported by --__ mcthoxychlor Z-L/-t&e --toxaphcne Dale Extracted Dale Reported 21~ .. o -- Date AnalyLcd__!i::,_"g'-91f'1/p · 94277•-'l __ 2,4.5-TP (Si!vex) Lab Number I DI I.S Jl'Ji (ltcvis::d 2/91) -- _ uc;,~:;.mcn. Ul C..'"l'-1ronmcn:.. lc::;llh, /.. 1'a1unl RC-'Ourccs lid Waste Manai;cmcnt Di~-ision le Number V/'1,,..lTA.J. J,,..,o;,,..,. r-,,Jo.J..J....,_, • ......, ,,._, ---,_ . P.O . l1ox :ZSO.:i, 306 1'. Wilmintion S1ri::c1 R.alcii;h, North Carolina 2761 I Fidd Sample Number WL -c) Z Z. -SS ----------------- ame of Sile WA-R..:2.-e..J Gor.Jrt PCB l.DFL Sile Location A F'To iv NC.. -~-_:....;::....:..;~_....:....;:......::::::;._ __________ _ ollcctcd By b. /\.) •LH.o\...60~ Date Collected 2. ?--~UL Y q4 Time /~ Z9 ~ . STePHtlv'=> ,gcncy: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· Ground waler (1) _ Solid (5) GJZ ID "3~, ZI Cadmium ---Chromium --Surface water (2) _ Liquid (6) Lead --- --Mercury £ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) Organic Compounds Rcsults(mg/1) P&T:GC/MS A.rseo..ic bcnz.enc ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------_x_ Pc..-.3 <: O ./ 0 -/JR01 Chloride chlorobenz.cne ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichiorobenzc::ic --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylcne ----Selenium 2, 4-dinil rolol uene ----Silver heplachlor ----Radiochemistry Sulfates hex.ichlorobenzene ----Zinc hexachlorobu1adiene ----Paramt:lt:r Results (PCi/1) _pH hex.ichloroet hanc --__ Grass Alpha __ Conductivity __ methyl ethyl ketone Cross Bera --TDS nitrobenz.ene ----TOC __ penlachlorophenol -- ----pyridine Microbiology ----I eLrachloroet h ylene ----lrichloroeLhylcnc Parameter Resulls (Col/lOOml) __ 2,4,5-trichlorophenol ----__ 2,4,6-lrichiorophenol ------vinyl chloride --cndrin -- 7-/2r-9Yt1f 6ZJ Reported by lindanc --D;;te Received mcthoxychlor -- ?-41-'1~1/~ __ loxaphenc Date Extracted Date Reported 2.~-0 -- Dale AnalyLcd '&"'-<j?-9'//j/,P ·. 942775 2,·U-TP (Silvcx) Lab Number DI I!:: ]l'Jl (llcviscd '.!/91) --! lc~llh, /,; 1'alunl Resources 1id Waste lshrui;cmcnl Di~-ision le Number t,,.Jr1,,,J,,t4,1,. --·-·---------....., ----r.o. nox ::so,:;, 306 r--:. Wilmin~on Slrt:Ct R.alcii;h, North Carolina 2761 i Field Sample Number W L -c) Z3 -SS ----------------- amc of Site WA-'<i2..e.J GorJn' PG'E:, u,FL Site Location A F'To ~ NC --"--'--...,;,_::......:...;=-----;_,;;:;;,__ __________ _ 'ollecled By ~. fv •l.Ho 1,... 6cn-..., Dale Collected 2. -:;z... -:JULY q4 Time /~ 5 3 Gt . SrePt-1&.lS .gency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· _ Ground waler (1) _ Solid (5) 'i,12 l"D It> I Z4 Cadmium --Chromium --_ Surface water (2) _ Liquid (6) Lead -- --Mercury L_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Orgnnic Compounds Rcsul ts (mg/I) P&T:GC/MS Arsen.ic be:nene ------Acid:B/N fa1. Barium carbon tetrachloride ------MTBE Cadmium chiorcianc ------...L Pc..13 <o,Lo~ Chloride chlorobenzene r ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride rn-cresol ------ --Iron __ p-cresol --Lead crcsol ------ --Manganese l ,c.-dichlorobenzene ---- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-ciichloroethylenc --Selenium 2, c.-di nil rot oiucne ----Silver heptachlor ----Radiochemistry Sulfates h ex.achlo r obcnzene ----Zinc hcx3chlorobutadienc ----Parameter Results (PCi/1) pH hex.achloroelhane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobcnzcnc ------TOC pent a chlorophcnol ---- --__ pyridine Microbiology --tetra chloroelh yl enc --trich lorocthylenc ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4 ,6-tricruorophenol \invl chloride ------cndrin --lind:rne Date Received 7-,lf-f'c/-p~,6,.l) --Reported by mcthoxychlor .> ---I D:it:: Extracted ?-9'---f&P --loxaphcnc Date Reported 2,c.-D --I D:iic AnalyLcd ~-'ff'-fL/1/J° ·. __ 2,.!.5-TP (Silvcx) Lab Number 942776 I l)J !S Jl'Ji (1,cviscd ~/91) --I ....,r.a.....••• --·-••-------....__---. ~Ith. l,:. 1'•tu;-.I Ruourccs r.o. !lox~'· .:,,..,0 "· ~ ........... _ .. - l Waste M•nai;cmcn: Division Raleigh. North urolina 1i6J: ; Number -----------------Field Sample Number WL. -c) Z4-S!S me of Site WA-R.~e.J C,orJN PG"B u,FL Site Location A F"To ,-.J NC ·-..:-..:.~....:....:~::::_-~:....;:~----------- llected By ~. fv t('..H.ol,6c,~ DateCollceted 2.?-::JULY q4-Time /i.34 G . S,'EPHeµ.S ;ency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environm.enlal Concentrate Comments Arsenic --Barium ---· z~ _ Ground water (1) _ Solid (5) G.r.z ID 3, Cadmium --Chromium --Surface water (2) _ Liquid (6) Lead -----Mercury ~ Soil (3) _ Sludge (7) Selenium --Silver -- -Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resu!Ls(mg/1) (mg/k.g) Organic Compounds Rcsul ts (mg/I) P&T:GC/MS Arsenic bcnz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane -------:::-o./~;,r ..L Pc..g Chloride chlorobcnzenc ----Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-crcsol ------Iroo p-cresol ------Lead cresol ------ --__ Mang2.ncse --1. 4-dichl orobenz.eo c --__ MerCUl)' --1,2-dich lorocthane --Nitrate 1, 1-dichloroethylenc ----Selenium 2,4-dinilrotoluenc ----Silver heptachlor ----Radiochemistry Sulfates hex.ich !or obcnz.cne ----Zinc hexachlorobutadicnc ----Parameter Results (PCi/1) pH hex.ichloroethane ----__ Gru5s Alpha __ Conductivity __ methyl ethyl ketone Gross Bela TDS nitrobenz.ene ------TOC __ penlachlorophenol -- ----pyridine Microbiology ----tetrachloroeth ylenc ----trichloroethylc:nc Parameter Results (Col/l00ml) 2,4 ,5-t richlorophcnol ----'. --__ 2,4,6-trichiorophenol -- --vinyl chlorid:: ----cndrin -- Date Received 7-.,-Zf-f'Y"f/'/' /J..l} lind:ine --Reported by mcthoxychlor ✓ -- ~-~-ft:/1/JO --toxaphenc Dal:: Ext;aclec.l Date Reported 2,4-0 -- ?-7-?~1//7 942777 __ 2,4.5-TP (Silvex) Dale Analyzed Lab Number I) I IS JI 'Jl ( llcviscd 2/Y:) -- :-,:.C. Dcpar.mcnl o( E.-,vironmcnl, 1 lcahh, l,;. 1'a1un.l R=urccs Solid Waste M.anai;cmcnl Division SAMPLE A..""-iALYSIS REQUEST ;)la&< '-AVV••·-·, - Sile Number ---------------- . P.O. Dox ~i. 306 K Wilmini;ton s,~ct ~lcigh, North urolina ::?7Gl 1 Field Sample Number W L -t) Z 5' -~ S Name of Sile WA-1<i2.e.J Coot.JT't PC-"B lI,FL Site Location A F"To 1'..l NC, -~-....:.-=~:...__-~-=----------- Dale Collected Z ?---=,u LY q4 Time /{. 39 bi, '5TePtt~~ Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---_ Ground waler (1) _ Solid (5) f.,IZID 27-, ID Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- --Mercury £ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B /N E>..1. Bariur:::i carbon tetrachloride ------"MTBE Cadmium chlordane ----< tJ. I °"7R,f!.h1 _L Pc.'6 Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-crcsol --Lead crcsol ------ ----Mangancse --1,4-dichlorobenzenc --__ Mercury --1,2-dichloroerhane --Nitrate 1, 1-dichloroelhylene ----Selenium 2,4-dinitrololuene ----Silver hcplachlor ----Radiochemistry Sulfates hex.achlorobcnzcnc ----Zinc hexachlorobutadicne ----Paramett:r Results (PCi/1) _pH hex.achloroethanc --__ Gru~s Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzenc ------TOC pent a chlorophenol ---- --__ pyridine Microbiology ----letrachloroeth ylene ----trichlorocthylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trich.iorophcnol ------vinyl chloride cndrin --lind:ine Date Rcccived 7--lf-f~~Lf~Reported by --__ methoxychlor Date Extracted S-S"-9(,L1/I' __ loxaphenc Date Rcport:d 2,~-0 -- 3-?-9f/1//" 942778 2,4,5-TP (Silvex) Dale Analy-Led Lab Number I) I IS JI 'JI ( llcviscd 2/Yl) -- cpar.mcnl o( En""ronmcnt, h, .t 1'a1ural Re.sources Vastc Manai;cmcnt Division 0n...1~·.1.r Lt rlJ\r,,.J,.., • .., __ l .v ... ,__ - '-lumber Field Sam pie N um bcr_...:W::;__:_~L::.__-_0:::::_:2=•-----=:..$_.:$::.__ _____ _ e of Sile WA-1<i2.E:.J GorJT'1 PGt;, l.DFL Site Location A F"T"o "-.l N (_ --'---___;;;;__;,_;:___..;....:.-=----------- ccted By ~. /'v 1l.H.01_,6C>),.,..) Date Collected .:Z ?-'JO LY 9 + Time /5:,8 bi . :{;}Te?+tEe..:l~ .ncy: Haz.ardous Waste X Solid Waste ___ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) :nvironmcntal· Concentrate Comments Arsenic --Barium ---- _ Ground water (1) _ Solid (5) G1<1D ..q-3 Cadmium --Chromium A-,.e 1/tJJ T -- Surface water (2) _ Liquid (6) Lead --- --Mercury f_ Soil (3) _ Sludge (7) Selenium --Silver -- _ Other (4) _ Other (8) -- ---- Organic Chemistry Inorganic Chemistry -- _Jarameter Results(mg/1) Parameter Results (mg/I) (mg/~) O~anic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic -benz.ene ----- Acid:B/N Ext. Barium carbon lelrachloride ------ "MTBE Cadmium chlordane ------ L Pa; <0,/1) tpnt Chloride chlorobenz.ene ----r-Chromium cblorof orm ------ --__ Copper o-cresol -- Fluoride rn-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenzeoe ----Mercury 1,2-dichloroet hane -- --Nitrate 1, 1-dichloroethylene ---- Seknium 2, 4-dinitrot oiuene ---- Silver heptachlor ---- Radiochemistry Sulfates hexachlorobenzene ---- Zinc hexachlorobutadiene ---- Parameter Results (PCi/1) pH hcx.achlorocthane ---- __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta --TDS nitrobenz.ene ---- TOC __ pentachlorophenol -- --__ pyridine Microbiology ----t etrachloroeth ylene --__ trichloroethylcoe Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol -- ----__ 2,4,6-trichlorophcnol ----vinyl chloride --endrin --lind:rne 7-e:?9-'.?¥J.t?@Rcportcd by Date Received --mclhoxychlor -- 1-S:-9~-Y;O __ toxaphenc D.il:: Exlraclecl Date Reported 2,.:!.Q -- ~-?-94rr1 ·-942779 __ 2,4,5-TP (Sil'✓t:X) Date Analyzed Lab Number DIIS J?'JI (ltcviscd 2/91) -- :-,:.C Dcpar.mcnt of Environment, 1 lealth, & 1'atur.il Re.sources Solid Waste Management Division SAMPLE ANALYSIS REQUEST State uboratory of Public Health . P.O. 13ox :S0:7, 306 S. Wilmini;,on Str=ct Raleigh, North Carolina 2761 I Site Number Field Sample Numbcr_--=W:.....__;_L._-_0_..,:2;:_,_+_----'-5_S _____ _ ---------------- Name of Site WA-1<..:2-e.J CborJN PC.t> u,FL Site Location A F'To 10 NC -.<.....:..-..:....:;...:.;:::...__.c....:...-=.----------- Collected By ~. fv •l.HOL6c>..._, ID# 3 :f-Date Collected .:Z ~ JO LY 9 + Time /~ 89 ~-<$ TE'f>t-t €7v> Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ---- Sample Type Incrganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---_ Ground water (1) Solid (5) (a~l!) Z-1-I ID Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- --Mercury _5_ Soil (3) _ Sludge (T) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------ L f>G& < t>, LP-fl?DJ. Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-crcsol ----Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzeoe --__ Mercury 1,2-dichlorocthane --Nitrate = 1,1-dichloroethylcne --Selenium 2,4-dinitroloiucne ----Silver __ heplachlor --Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadiene ----Paramett:r Results (PCi/1) _pH hcxachlorocthanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzcne ------TOC pentachlorophcnol ---- --__ pyridine Microbiology ----l etrachloroeth ylene ----trichloroethylcoe Par.imcler Results (Col/lOOml) __ 2,4,5-trichlorophenol ------'\ __ 2, 4,6-trichlorophenol ------vinyl chloride endrin -- Date Received 7-.:Z.f-f¥t//Lu!J Reported by lind:ine --methoxychlo~ ✓ -- Date Extracted 9-s=-9¢1(11 __ toxaphenc Date Reporled 21~-D -- Dale AnalyLed 'i-?-7',;/-y ,J!' . 942780 __ 2,4,5-TP (Sil•1ex) Lab Number DI IS 3191 (Revised 2/91) -- t,:.C. Depar.ment of Environment, l lc:allh, &. 1'a1ur.al Re.source$ Solid Waste Manai;emcnt Division SAMPLE ANALYSIS REQUEST State Laboratory of Public Health . P.O. D,ox 280,:7, :l06 S. Wilminpon S1r.:e1 R.alcigh, North Carolina 2761 l Site Number ----------------Field Sample Number __ w::...=-..:::L..:.....-__:6):::........,Zo:=....,,$"------'s~s _____ _ Name of Site WA-R.iLe.J GorJTY Pee, l.DFL Site Location A F"To ,-J N (., --~_;._..:..-=~:___.:....:....=.----------- Collected By 6 . f\) rc.Ho\..60"'-' Date Collected Z9 ✓Vl 'Y 94' L, R.e~c Agency: Hazardous Waste X Solid Waste _·_supcrfund TCLP Compounds ---- Sample Type Inorganic Compounds Rcsu lls (mg/I) Environmental Concentrate Comments Arsenic --Barium Po)..) '"D ---__ Ground water (1) _ Sol.id (5) LEdCH ,,.~ Cadmium --Chromium l-1 1..7"1!" ,z_ Ovn:-A LL --_ Surface water (2) _ Liquid (6) Ar Lead --Mercury _K_ Soil (3) Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Resulls(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane X Pc:a,e~~J l~ ----Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-dich loroethanc --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethahe --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ penlachlorophenol -- --__ pyridine Microbiology ----t etrachloroeth ylene --__ trichloroethyleoc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol --vinyl chloride ----endrin -- Date Received 7-:29-f',LP(dl) Reported by lindane --methoxychlor -- '7-S--f&f, __ toxaphene Dale Extracted Dale Reported '2,4-D -- Dale Analyzed ~--ffL'r/J Lab Number 942781 __ 2,4,5-TP (Silvex) DI 15 31~1 (llcvised 2/91) -- 1'.C. Dcpa:-:mc:nt o( Environmc:nt, 1 lcahh, &:. 1'a1ural Rc.wurccs Solid Waste Managc:mc:nt Division SAMPLE ANALYSIS REQUEST State ubOntory or ru011c 11c:a11n -P.O. l>ox 2S0-:7, 306 S. Wilmin!;'On S1~ct Raleigh, North Carolina 27611 Site Number ----------------Field Sample Number __ tu_L_-_t>_.2_'9_-_S_S ______ _ Name of Site WA-1<>2.e..J G,o,,rrt PG"B lDFL Site Location A F"10 ,v NC -!....:...~.:....:::~:__-:....:...=.----------- Collected By a. f\) ll.H.Ol,60....., ID# 3=f--Dale Collected 2 7-;fl) LY '14 Time 14-Z..S- ~ -~~l)H-0...)6 Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ---- Sample Type Inorganic Com!)ounds Resulls (mg/I) Environmental Concen tr:i te Comments Arsenic --Barium ---__ Ground water (1) _ Solid (5) £AST S,i>E t.X>FL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead -- --Mercury £ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane x Pc~Rlfi_ '7, ,:l!:J ~nm ----Chloride chlorobenzene ----, , Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-di chlorocthanc --Nitrate __ 1,1-dicnloroethylcnc --Selenium 2,4-dinitrotolucne ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexach lorobutadiene ----Paramett:r Results (PCi/1) _pH hcxachloroethane --__ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS nitroben7..cne ------TOC __ penlachlorophcnol -- ----pyridine Microbiology ----l etrachlorocthylene ----lrichlorocthylc::ne Par.imcler Rt:sults (Col/l00ml) __ 2,4,S~trichlorophcnol -- ----__ 2,4,6-trichlorophcnol ------\inyl chloride endrin -- 1-,Z f-t:/"f£1/,1)6'J}Rcportcd by lindanc Dale R::ccived --methoxychlor --/ O;.ile Exlractcc.l f'-S-'1¢ -VP --toxaphenc Date Reported --2,~-0 Date Analyzed ..S..-9-91/ yP 942782 2,4 ,5-TP (Silvex) Lab Number --DIIS 3l'Jl (Revised 2/91) ' 1'.C Dcpu~mcnl o! Environment, I icallh, l,:, /':alunl Ruourccs Solid Waste Mana,cmcnl Di,-ision ..:>t-UYJ.I: J..J,L., .t1tJ,.M,,.,,j.,,JJ....J.L.._,., .-...'-'. '-"'.,.__,,,,.,. P.O. Oox 280,:7, 306 K Wilminpon Sa~c: Ralcir;h, North Carolina :7Gll Site Number -----------------Field Sample Numbcr_..,;:W_:_.;;,.L;_----'0::;_.;e:J'--/_•_:5_u...J~----- Name of Site WA-1<.:2.e.J CoorJT'I PC.t, l.DFL Site Location A F"T'o ~ NC.. _.!...:,__;_..:..:,::..:.:::::....__....:...,:c...=::;.__----------- Collected By ~. f\) 1c.H.01,..-6C>~ Dale Collected Z.,fJ :JVL '/ ~ 4 Time I Z-1)5' #1. P., n_,r;,e~ r~.e. Agency: Hazardous Waste X Solid Waste ___ Super fund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· elc..1-'ft-Jee.~ __ Ground water (1) Solid (5) V~T@e)\M. Cadmium --Chromium --_ Liquid (6) Ct2.e e K" _lL Surface water (2) Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --' ----Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------.1L PC-5 <o. t1ot1/ Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ hcptachlor --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnz.cne ------TOC __ penlachlorophcnol -- ----pyridine Microbiology ----tclr achloroct h ylcne trich lorocthylene ----Parameter Results (Col/lO0ml) __ 2,4 ,5-trichlorophcnol ------__ 2,4,6-trichJorophenol --vinyl chloride ----cndrin --lind:rnc Date Received '7-;2.'1-'Jf(t/f'M Reported by --methoxychlor -- D:itc Extracted~ /-ff ::W: Bb --toxaphcne Date Reported 2,.!-D -- Date Analyzed ~-/-'99"11{!:' 942783 __ 2,<:,5-TP (Si lvex) Lab Number l)IJS 31')1 (llc,iscd 2/91) -- I I [ ~-C. Dcp~r.mcnt o( E:wironmcnt, I icalth, l,:. /'sa1ural Rel.Ou recs Solid Was1c Ma.na.,cmcnt Di,;sion .:)A,,.lY.lC" J..J~ rU ,.M,,,...J,.,JJ. ..;J .tr..--.J ,,.._._'-'. '"""A-.,1...., ,._ Site Number ----------------- r.o. !kn ~i. 306 s. Wilminttor. Stn:cl fulcith, North Carolina :?7611 Field Sample Number Lu L -00 l -~ 'D Name of Sile WA-~.2.e..J GorJN PCB l.DFL Sile Location A F"To t-..J NC _.<-.;._~::....:..::=-------'-':-::;._ __________ _ Collected By G. {\), l.H.o 1,.. 6c>~ Dale Collected 2 ~ :r l,) L '/ Gt 4 Time / ze,f;' A. Pco..J~~n;.,e Agency: Hazardous Waste X Solid Waste __ Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic --Barium ----__ Ground water (1) _ Solid (5) 5Ep1Ml=JI...J1 Cadmium --Chromium _ Liquid (6) V/J~TIZB't/11 ~lc.Htv(EC.)< --Surface water (2) Lead ---- C£EkK --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_K_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul t.s (mg/1) (mg/kg) Organic Compounds Rcsul ts (mg/I) P&T:GC/MS Arsen.ic benzene ------ Acid:B/N Ext. Barium carbon lclrachloridc ------"MTBE Cadmium chlordane ------<(,),/()#DJ _x__ :Pc..:B Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-cresol ------ --Iron __ p-crcsol --Lead crcsol ------ --__ Manganese --1, t.-dichlorobcnzcoe --__ Mercury --1,2-dichlorocthane --Nitrate 1, 1-dichloroelhylenc ---- Selenium 2,t.-dinilrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hcx.achlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) --pH hcx.achlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----l ctr a chlorocth yl enc --__ lrichlorocthylcnc Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichJorophenol ----__ vinyl chloride --cndrin --lind:rne 7-;2. '1-9¥Yf ,di) R c ported by --Date Received mcthoxychlor -- r:-S:?4' 1# --toxaphcne Date Extracted Dale Reported 2.~-D -- D.ite Analyzed 'lf-9-9'4L--V.I' 942784 __ 2,4,5-TP (Silvex) Lab Number DI IS 31'J1 (Rc,iscd 2/'>'1) -- ' I I I ;,:.c Ucpar:mc:nt or l:.nY1ronmc:n1. I lc:ai1h, &.:. 1'21u~I Rc:sourccs Solie! W2s1c M•n2i;cmcn1 Di--ision Site Number ..:>nJ.Y.1.I: .L.,~ /"1r...i. ,n,..,J,..,,.&. ..)A._, •"'-'~ '--'6-...,J .... P.O. l>ox 2.so.:7, J06 S. Wilmini;ion S1n:c1 Raleigh, Nonh C.rolina nGJ l -----------------Field Sam pie Numbcr __ _;_LU_::_L=-...-_..;;;;o_o_..:;;z_-_s___;w:;__ ____ _ . Name of Site WA-Q.;2..c:.J GorJrt PG"B lr,FL Site Location A F"To ~ NC.. _.!......:._:_...!...!~~-....:.....::....:::::__ __________ _ I Collected By 6. /\,) 1c.H.0L6c:>\,,..) Date Collected 2 t3 ::f l)L Y Cf 4-Time /O~D M . PP, A./Pe "'-r,:?112. Agency: Hazardous Waste X Solid Waste ____ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium .PO?&:' ,v.Sr,e 1:/1,111( ---· __ Ground water (1) _ Solid (5) Cadmium -- (:/2E£k Chromium _ Liquid (6) ~Ch'IV~Ck --_L Surface water (2) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/kg) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------ _2$._ PC . .'B <t;J. OOIJ/ Chloride chlorobenzene ----Chromii.:.m chloroform ------ --__ Copper o-cresol --Fluoride rn-crcsol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-d ich loroet hane -- --Nitrate 1, 1-dichloroet hylcne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadienc ----Param~tr.:r Results (PCi/1) _pH hexachlorocthane --__ Gross Alr,ha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnz.ene. ------TOC __ pe.nlachlorophenol -- ----pyridine Microbiology --__ tctrachloroethylene ----trichloroethylenc Parameter Results (Col/l00ml) __ 2, 4 ,5-trich lorophenol ----__ 2,4,6-trichJorophcnol ----__ vinyl chloride --endrin -- 7-2-?'/-//~;5'Z}Rcported by lind:!nc Date Received --__ methoxychlor ;;, Dale Extracted ~ -/-9L/VljM --toxaphcnc Date Reported 2,~-D -- Dale Analyzed ~-l-?¢t//' 942785 __ 2,4,5-TP (Silvex) Lab Numbc~ I) II S 31 'JI ( Jtcviscd 2/91) -- I lc.ilth, ,!.; i'->1unl R=ul't'CS Solid WH:: )-.lanai;cmcn: Division Site Number ---------------- R..aicii;h, North urolina ~761 l Field Sample Num bcr __ W_L:.----..::0_0.....:Z=----~=---p=-------- Name of Site WA-g.:z.e:..J CorJTY PG"'i!> U)FL Site Location A F'-To >--J NC _.:..__....:...:::c...:.;::__ _ __.;.-=----------- Collected By (; . t0 t l. H.o l. 6c,)-..) Dale Collected Z. 'z3 ':[ V LY '14 Time /05S- ;U. pc,/~Pe'><-~,e Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ----j Sample Type Inorganic Compounds Resulls(mg/1) I Environmental , Concentrate Comments Arsenic --Barium 6~/ t?7 Gµ -r ----_ Ground water (1) _ Solid (5) Cadmium --Chromium __ Liquid (6) ~µ .=s-✓-72e,4/V\. --Surface water (2) Lead ---- _ Sludge (7) hCHl()ec.~ CR i£".E" --Mercury _ Soi·! (3) Selenium --Silver L Other (4) wL~c.() --_ Other (8) ..SP~t r --I I Z-C. -t:> o I -:.Se:I:> -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resu I Ls (mg/I) (mg/kg) O~anic Compounds Rcsul ts (mg/I) P&T:GC/MS Arse.nic benzene ------Acid:B/N E,,.1. Barium carbon lelrachloridc ---MTBE ----Cadmium chlordane v~E5T <O./l)IP"4------Chloride chlorobenzene ----; Chromium chloroform ------__ Copper o-crcsol ----Fluoride ro-cresol --------Iroo p-cresol ----Lead cresol ------ --__ Manganese --1, 4-dichlorobenz.eoe --__ Mercury --1,2-d ich loroet hane --Nitrate 1, 1-dichloroethylcne ----Selenium 2, 4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroelhane ----__ Gross Alpha __ Conductivity --meth)'I ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC __ penlachlorophenol -- ----pyridine Microbiology lelrachloroeth ylene ---- ----Lrichloroethylcoc Para meter Results (Col/l00rnl) 2, 4 ,5-Lrichlorophcnol ---- ----__ 2, 4 ,6-trichJorophenol --vinyl chloride ----endrin --lind:rne 7-...1.. 9-9,/-p/ LfZ) Reported by --Date Received mcthoxychlor --- J'-S-91(-UO Date Reported --loxaphenc Dale Extracted 2,~-D ! --I D<.1te Analyzed 'fl-9_-9¢-VP 942786 __ 2,4,5-TP (Silvex) I Lab Number ' I) I IS j l 'JI (llcviscd 2/9 l) --I I 1 lc;ahh, l:. ~21unl ~c.:.ourrcs Solie Was:c M~natcmcn: D"~sion ~lcii;h, North C.rolina 27Gl 1 Site Number ----------------Field Sam pie Nurn bcr __ W_..;,..l_-__;e>::..._o--=z=----...:.->:..._:'J:>:...._ _____ _ Name or Site WA-1<..2.e..J GorvTY PC""t:> l.DFL Site Location A F"-,o iv NC _.!....:._...;....::;....:...::::..._ __ -=----------- G:ollccted By ~. fv 1(.H.Ol,6.::,\.-.) DateCollected 2-S -:/vL'Y <r'4 Time /t:>55" fi'2 . p.,,,,11::>e-'l{.re'-R_ . TCLP Compounds Agency: Hazardous Waste X Solid Waste __ Supcrfund ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium 6e:z,,.../7?G;,(.) -r ---· __ Ground water (1) _ Solid (5) Cadmium --Chromium ~µ .=S ~eAJ'V\. --Surface water (2) _ Liquid (6) Lead ---- _ Sludge (7) J3 CHl<.Jec.x <3z£.E/c::"" --Mercury _ Soil (3) Selenium --Silver £ Other (4) w/cc.o --__ Other (8) . .:5,01..1 r --' I .:re::. -oo I -SET> -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Resu I ts(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ---- _£ Acid :B/N Ex1. Barium carbon tetrachloride ----.MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1, 4-d ich Io robenz.en e --__ Mercury --1,2-dich loroethane --Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rotol uene ----Silve~ __ heptachlor --Radiochemistry Su If ates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Paramctl!r Results (PCi/1) --pH hex.achloroctha ne --__ Gross Alpha __ Conductivity --methyl ethyl ketonc Gross Beta TDS nitrobenz.cne ------TOC __ pcntachlorophcnol -- ----pyridine Microbiology t ctrachloroet hylcne ---- --__ trichlorocthylcoe Para rn ctcr Results (Col/l00ml) __ 2,4 ,5-lrichloropncnol ----__ 2, 4 ,6-trichlorophcnol ----vin yl chloride ----cndrin --lind:rnc 7~.z9A Y~11/M Date Received --Reported by mc:hm;ychlor ;,, -- O;itc Extracted <&"-5"-~ lf. ~,1LAB --toxaphene Date Reported 2,~.o I -- Dale Analy-1..cd <J-f?-9</-sill-942787 __ :?.,t..5-TP (Silve.x) Lab Number 1)1 IS Jl'JI (llcviscG :?./91) -- I I I 1,·.L-~cp~r.mcnl oc .t:..nY'\ronnn:::n,. llcallh, & 1':alunl Rc.wurrcs Solid Waste Manai;cmcn: D,vision VF"),,,J.,.&.l ,._,,,_, ,.-••-------x_ __ _ . r.o. 13ox 280-l7, 306 K Wilmini;ton Stn:Cl R.tlcigh, North Carolina 27Gl l Sile Number --------Field Sample Numbcr __ W___:l=----~;:;:_0---=Z:....-~>--=-D _____ _ Name of Site WA-1<i2.e..J Cor.JN PGt:> l.DFL Si1e Ll)calion A F",o iv NC _...c.....; _ _.:....;=-..:..:::::._ __ c......;::::;.... __________ _ Collected By G . f\,) , c H.o L. 6o~ Dale Collected ZS :/uL Y '14 Time /t:>5S' /l'l. Pc r/..Jv€x ,eR Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Resu I ls (mg/I) Environmental Concentrate Comments Arsenic --Barium 6ce:P✓ A? G".A..J -r----· __ Ground water (1) _ Solid (5) Cadmium --Chromium ~,<..J ::S 7'2eA.IV\. --Surface water (2) _ Liquid (6) Lead ---- _ Sludge (T) £!u:.Hl()ecx ~£.E-"'" --Mercury _ Soil (3) Selenium --Silver Ji_ Other (4) ~/_£Cf) --_ Other (8) .Sl'~IT --' I'C.-001-~ED -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) ✓ P&T:GC/MS Aisenic benzene ----Acid:B/N Ext. Barium carbon telrachloride -.MTBE --Cadmium chlordane ------Chloride chlorobenzene ------Chromium cblorof orm ------ --__ Copper o-cresol --Fluoride rn-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1, 4-dichl orobenz.ene -- --__ Mercury 1,2-di ch loroethane -- --Nitrate __ l,l-dichloroe1hylene --Selenium 2,4-dinilrololuene ----Silver __ heplachlor --Radiochemistry Sulfa1es hexachlorobenz.ene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conduc1ivity --methyl e1hyl kelonc Gross Bela TDS nitrobenz.cne ------TOC __ pcntachlorophenol -- --__ pyridine Microbiology --__ tclrachlorocthylene ----trichloroethylenc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ----__ 2,4,6-lrichlorophenol --------vinyl chloride endrin -- 7-,Z'l-f/L/l,,P&i) lind:rne Dale Received --Reported by __ methoxychlor .,, __ toxaphcnc Dale Extracted Dale Reported 2,-:!-D -- Dale Analy-1.cd g-5 -g_'-f-'ilU. t 942788 __ 2,4 .5-TP (Silvex) Lab Number DI IS Jl'JI (Revised :!/91) -- :--;,C Dcpar.mcnt of E,,,,,.;ronmcnt, I lcalth. & 1','atur.l Rc.sourcc1 Solid Waste Manai;cmcn: Oi,ision .::,AJVH' Lt A.l'\A.Ll ;)J...:) ru.,\...l.. UL..;J .L . P.O. lk>x 280-:7, 306 S. Wilmin~on Strc:: RAieigh, North urolina 27Gi: Sile Number ----------------Field Sam pie N umbcr _ _.:..tv-=-=L_-____;0;;;.,_;;0--=3_-____;_-sc.........;:u_Jc...= ____ _ Name of Site WA-R.i::2..e.J GorvTY PG"'E:, U,FL Sile Loc:alioc A F--ro ~ NC, _..:......;__....:....::~::__-~-=----------- Collected By a, f\.) ll.H.0\_.'6o~ Dale Coilected 28 :7lll. Y 9,+ Time O 9/b fi1 , pe, IA,l'C,6-](.~ Agency: Hazardous Waste X Solid Waste __ Su perfu.cd TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground waler (1) _ Solid (5) (J,P~TL2E/1-A1 Cadmium --Chromium --£_ Surface waler (2) Liquid (6) V,u/4/AM-c=z> //c:../ B . Lead --Mercury _ Soil (3) _ Sludge (7) --Selenium --Silver --_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- ; Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benz.ene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------..L pC..13 <d, OfJ'7 I Cb..loride chlorobenz.ene ----Chromium chloroform --· ---- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzece --__ Mercury 1,2-dichloroethane -- --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinilrololuene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Paramett:r Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC __ pentachlorophcno! -- --__ pyridine Microbiology ----tetra chloroeth ylenc ----trichloroelhylenc Parameter Resulls (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichJorophenol ----vinyl chloride ----endrin --lind:rnc Date Received 7-29-7¢'tf..6_tjReported by --methoxychlor -- Datc Extracted -g;.-. /-~1/4Ad._ Date Reported __ toxaphene 2,~-0 -- Date Analyzed 2,.-/-9¥1//J 942789 2,4,5-TP (Silvex) Lab Number 1)1 IS Jl'Jl (llcviscd :./91) -- I I I ! N.C. Dcpar.mcnt o( E.nvu,:,nmcnt, 1 lcalth, & :--:a1ural Rc.s.ourccs Solid Waste Manai;cmcnl Division ~AM.t'L.t., Al'\A.Ll..:>l.:> .K..C.\..!_UL~.l. . P.O. 11ox ~7. J06 S. Wiimini;ton Strec! Raleigh, North Carolina 2761 J Site Number ----------------Field Sample Number __ W~-=Lc:...."'----3(9"""-"'6~'!>::;.._-_:5_1>:.._ ____ _ Name of Site WA-R.i2..E:.J GorvN PG"B l.DFL Site Loc.atioo A F"To ~ NC.., --'---'--...c._::;_..c.:,:._ _ __;_-=----------- Collected By a. I\J IC::.H.01,..6c>~ Dale Collected 2 e :.rv LY 9'1: Time OCf Zo /JI/ . Pt1 , ~-;:, ex re'< >( _· _Superfund TCLP Compounds Agency: Hazardous Waste Solid Waste ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· 5eZJrm EAi r Ground water (1) _ Solid (5) Cadmium ----Chromium --_ Liquid (6) l,/p.5rg,GIHYJ Surface water (2) Lead ---- _ Sludge (7) aA./A& EX> /..c2-..-B --Mercury _ Soil (3) Selenium --Silver --JL Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Organic Compounds Resul ls (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------<: o. I ti ,12j2.m .lL Pc.e Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --!roe __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobcnzeoe --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylcnc ----Selenium 2,4-dinitrotolucne ----Silver __ heptachlor --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethanc ----__ Gruss Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nil robcnzenc ------TOC penlachlorophenol ---- ----pyridine Microbiology ----t ctrachloroct hylcnc ----trichlorocthyleoc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride --cndrin -- 7-~?-f'~£/t&Rcported by lind:rne Date Received --methoxychlor -- Y-s-94(-w, --toxaphenc Date Extracted Dale Reported 2,4-D -- D..ile Analyzed 5'-9-~-r,/,;P ~ 942790 __ 2,4,5-TP (Silvex) Lab Number l)J{S Jl'JI (Revised 2/91) -- I I I i i I I lcalth, l,:. 1'a1ur.l Rc.wurccs Solit1 W.is1c ~bnai;cmcnt Division -,-,,,,,.. ....... --·-·------__ "'<.. ___ . P.O. &ix :ZS0.:7, 306 S. Wilmini;ton Street ~lcigh, North Carolina ~7611 Site Number ----------------Field Sample Num bcr __ tu_..;_1._-_0----=0_4~---=:[;,::...-=.U,J-=. ____ _ Name of Site WA-R~e..J Coo,,:rrt PG"t> l.DFL Site Location A F"T"o >J NC.. -.!....:..-...:...::~~-.:.__:_-=----------- Collected By a. f\) ll.H.Ol,6c,)...) Dale Collected Z.'fs -:TVLY ~4 Time OS-40 /11. Pc--,,._, DE:)!,e-R.. Agency: Hazardous Waste X Sol.id Waste __ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compounds Rcsulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ----Ground water (1) _ Solid (5) .£bc.cJ,u.,t;reE~""" Cadmium ---- ~B Chromium Ut.h(.M# n:> --£ Surface water (2) _ Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) --' -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) O~anic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------L ~c..B <P. OOP/ Chloride chlorobenz.cne ----Chromium chloroform ------__ Copper o-crcsol ----Fluoride rn-crcsol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1, 4-d ichlorobenz.ene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylcne ----Selenium 2,4-dini1ro1oluene ----Silver __ hcptachlor --Radiochemistry Sulfates hexachlorobenz.ene ----Zinc hexachlorobutadiene ----Paramelt:r Results (PCi/1) _pH hcxachlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS ni1robenz.cne ------TOC pen{achlorophenol ---- ----pyridine Microbiology ----l ctrachlor octh ylenc ----trichloroethylcoc Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ------vinyl chloride endrin -- 7-~-f'-7~J/l'~cportcd by lindanc Dale Received --mcthoxychlor _,, -- D:itc Exlraclc<l$_-/-9// YI;,£,$_ Date Reponed __ loxaphenc '2,.!-0 -- Date Analyzed ~2.-f~~ 942791 __ 2,4 ,5-TP (Silvex) Lab Number DIIS 31')1 (Revised ~/91) -- ;-,.:.C. Dcp31':mcnl of Environment, i lcallh, &. 1"a1u:.I Ruourccs Solid Was1c M•n•tcmcnt Division ~AlYl.t' Lr, J-1...1 ,J-'>J..JJ. ..)J..,J "'-'--'..:'. u,_..., .i.. . r .o. nox 28047, 306 K Wilmin~on Slr~Cl lulci~. Nor1h Caro!ina 27611 Sile Number -----------------Field Sample Numbcr_---=--W~::;_;J.~---0_0_4_-_S_:P ____ _ Name of Sile WA-R..2..e..J Go,.JTY PG'B l.DFL Site Location A F",o .t--..J N (_ ·_..t......:.....:........:....:::::...!.:~-....:....;:....;:::;,.._ __________ _ Collecled By a. (\) ll.H.Ol,6'.::>~ Dale Collected ze .:.Jvt. y Cl~ Time C)-g5"0 M , Pc., ,1vr>e-xre~ Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium SeX>/H?E/4/ r ---__ Ground water (1) _ Solid (5) Cadmium --Chromium 7Jou,.,.u.5TR ~,qm --Surface water (2) _ Liquid (6) Lead ---- {)/4/A,//11/17 El? ---Mercury Soil (3) _ Sludge (7) /!QB. Selenium ----Silver --__b_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- : Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benz.ene ------Acid:B /N fat. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ----<&J,/17-".,..,,.,. ...2L Pc.B Chloride chlorobenz.ene .... ,___ --// Chromium chloroforr.: ------__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1, 4-dichlorobenz.eoe -- --__ Mercury --1,2-dich loroethane --Nitrate 1,1-dichloroethylcnc ----Selenium 2,4-dinitroioluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadienc ----Pararnelcr Results (PCi/1) _pH hexachlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC pentachlorophenol ---- ----pyridine Microbiology ----tetrachloroeth ylene ----trichloroethylcne Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----vinyl chloride ----endrin --lind:rnc Date Received 7-...l'1-'l/lpt.62JReportcd by --__ methoxychlor Date Exlracletl '5'-S:-99'-v,o __ 1oxaphene Date Reported 2,~-D -- Dale Analyzed J'-9-~1//> 942792 __ 2,4,5-TP (Silvcx) Lib Number DI !S 31~1 (llc,isccl 2/\11) -- J lcalth, l:. !',:a1ur2I Rcwurccs Solid Was:c Manai;cmcnt Di--i.sion Sile Number ----------------- P.O. !'lox ~7. 306 ?'-. Wilmini;ton Stn:.:t Raleigh, North Carolina ~7G 1 l Field Sample Number t,,U,,t. -~DS-~.:Z:, Name of Site WA-1<.:2.e...J GotJN PG""f3, l.DFL Site Location A F"T"o t.J N (_ _..:.....;._....;...:::......:.;:...._ __ ;_:=::;;__ __________ _ 'Collected By ~. /\) •c.H.o l. 6c>._, ID# 3=?-Dale Collected ZfB .JI/LY 9--? /4. Po1,-.J1:>e)[.Tt=-"'s?. Agency: Hazardous Waste X Solid Waste ___ Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium 5e::z:>/,nf7,(_) r ---· _ Ground water (1) _ Solid (5) Cadmium --Chromium 2);xv.us5recr,m --__ Surface water (2) _ Liquid (6) Lead -- V&,,ur1 M..m 7~b', --Mercury Soil (3) Sludge (7) Selenium ----Silver . X Other (4) _ Other (8) -- -- -- --Organic Chemistry· Inorganic Chemistry -- : Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B/N Ex1. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------< tJ. I tl LJLJffi.. _x_ Pc..F> Chloride chlorobenzene --,, Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------Lead crcsol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-ciich loroethane --Nitrate 1, 1-dichloroelhylcne ----Sc:.lenium 2,4-dinilrololuenc ----Silver hcplachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) --pH hcx.achloroet h. ane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS ni1roben1.ene ------TOC pcnlachlorophenol ---- --__ pyridine Microbiology ----lelrachloroet hylene ----trichloroethylenc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichJorophcnol ----vinyl chloride ----cndrin -- Date Received 7-:2f-ffyt ,81) Reported by lind:rne --methoxychlor -- ?-i-9fi'1(0 __ toxaphene Oat:: Extracted Dale Reported 2,~-D -- Dal:: Analyzed "y-f_-f!i....-PI:/ 942793 __ 2,4,5-TP (Silvcx) Lab Number Dl!S Jl'Jl (Revised 2/91) -- l lcalth, &: 1'a1unl Rc.s.ourccs Solid Wasic 1'hnatcmcnl Di,-ision Sile Number ---------------- . P.O. 11ox ~7. 306 K Wilmini;ton Sir-cc: Raleigh, North Carolina 2761 l Field Sample Number U,.,,) L -Oe5 -;5,UJ Name of Sile WA-R.2.e.J G,otJN PCt:> l.DFL Sile Localion A F"To "-.l NC _.!....;.._....:..-=:....:..:::::...__.:...,:....= __________ _ Collected By ~. fv •LH.o L. 6c,)-) ID# 3-=r-, Dale Collecled _:2f3 Jt//. Y '?4-Time O~+o /)1 . Po I A.JV E',(7c'"12. X TCLP Compounds Agency: Hazardous Waste Solid Waste __ Superfund ---- Sample Type Inorganic Compounds Resulls(mg/1) Envirnnmenlal Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Solid (5) .DQ1..,vAJSr.efiA-/J? Cadmium ----Chromium --J5.._ Surface water (2) _ Liquid (G) 0..U..UA,#~ 772, JS. Lead -- --Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Olhcr (4) _ Other (8) --' -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsul ts (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------ <&:1. d "" I 2L. R=.s Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-crcsol ----Fluoride m-cresol ------ --Iron __ p-crcsol --Lead crcsol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dich lorocthane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadienc ----Parameter Resu I ls (PCi /1) _pH hcx.achloroclh_anc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzcne ------TOC pentachlorophcnol ---- ----pyridine Microbiology ----t ctr a chloroet hylene ----trichlorocthyleoe Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ----__ vinyl chloride cndrin --lind:rne Date Received 7-,.29-f$''J//!al)Reported b:,, --mcthoxychlor ;;, -- ?-L-9¢1(eJe.. Dale Report::d --toxaphene O;ite Extracted 2,4-0 -- Dute Analyzed 2_-.2-9J;L'1/P 942794 __ 2,11,5-TP (Silvex) Lab Number l)f IS Jl'JI (llcviscd :!/YI) -- I I I I ;<.C. Dcp3r.mcn1 of Environmcnl. S~1PL£ ANALYSIS REQUEST S1a1c Labon1ory or Public J-lcallh I lcalth, I,; ,-.:a1ur.l R=urccs Sc,li<l Was1c M.anai;cmc:11 Division Site Number ---------------- P.O. Ilox 280-:7, 306 S. Wilmintton S1~c1 Raleigh, North Carolin• :?7611 Field Sample Number lu-L-(5)0 2 -LC. Name of Sile WA-R.i2.e.J CbotvN PCt> l.nFL Site Location A F"To ~ NC.. -~---=--=:....:..:::~-..:......:.-=----------- Collected By 6. (\) 1c.Hol,6c:>~ Date Collected # 7?, :JvLY t:::t-4 Time / :;5"oO C.. Si" c 'P+-i. e=l--J 5- Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resul ls (mg/I) Environmental Concen tr:i te Comments Arsenic --Barium ---· --Ground water (1) X Solid (5) tveT LA-ru"Z> f:J LL Cadmium --Chromium --Surface water (2) _ Liquid (6) <:,.p-ur~ Lead ----__ Mercury _ Soil (3) _ Sludge (7) ~,o~,r tvl p;O Selenium --J Silver -::,:: C.. -(!;03 -~ L --_ Other (4) _ Other (8) C>o~ ro..e. ECO -- :X:-<:::. -~o~-LC -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Resulls(mg/!) Parameter Results(mg/1) (mg/kg) Organic Compounds Resulls(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------~ Cadmium chlordane ----ISL~5!,o/21'1J. Chloride chlorobenz.ene ----'=5 Chromium chloroform ---- --__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-crcsol --Lead cresol ------ ----Manganese --1,4-dichlorobcnzene --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --hexachloroelhane pH --__ Gross Alpha --Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenz.enc ------TOC __ pentachlorophenol -- ----pyridine Microbiology ----t etrachlorocthylene ----trichlorocthyleoe Parameter Results (Col/l00ml) __ 2,4 ,5-trichlorophenol ------__ 2,4,6-trichlorophenol ------vinyl chloride endrin -- 7-d{?-9¥~.2> lindane --Date Received Reported by __ methoxychlor Date Extracted ~ ?-9¥1/P __ toxaphenc Date Reported 2,-'.!-0 -- Date Analyzed ~-~~$?1(JO 942799 __ 2,4,5-TP (Silvcx) Lab Number l)IIS 3191 (llcviscd 2/91) -- I I I l I J',.".1... uepar.mc:n1 01 cnvuunmoc;m, I lc:ahh, & l'-alural Ruourccs Solid Waste 1',b.nagcmc:nl Division Site Number """ ............. --·-··-------~ · P.O. &,x 280:7, 306 S. Wilmintton Stn:et Raleigh, North Carolina ::?7Gl I Field Sample Number ltJL-(5)0 2 -LC. ---------------- .NameofSile WA-R.iLe..J Gorvrt PG"t> u,FL Site Location AF"Tr>J,.J NC _..:......;__...:..-=~:__-~-=------------ Collected By c;;. f\) •U-to\...60"'-' Dale Collected # ,7.'1, :JVC/ ~4 Time / S-oo c.. . STc'P+-t e-)J s. Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds RcsuHs(mg/1) Environmcnlal Concentrate Comments Arsenic --Barium ---· __ Ground water (1) X Solid (5) l-VE"T /.A-A.17> f:J LL Cadmium --Chromium --_ Surface water (2) _ Liquid (6) u.ur~ Lead --__ Mercury Soil (3) Sludge (7) .:SP~tr (,,c_,)I ECO Selenium ----' Silver _ Other (4) :re-&03 -~~ --_ Other (8) &,v/J ro£ e-c..o -- %"'~ -~o "Z!:. -L c-_ ----Organic Chemistry Inorganic Chemistry -- Parameter Results(rng/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) X P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-eresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenz.ene --__ Mercury --1,2-dich loroethane --Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulfates hexachlorobenz.ene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----lclrachloroethylcne ----trichlorocthylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ----__ vinyl chloride endrin --lindane Date Received 7-..2~ -?fc"f// ,6J) Reported by --__ methoxychlor ;; __ toxaphene Date Extracted Date Reported 2,4-D -- fr-5-91-nA.l.JLab Number __ 2,4,5-TP (Silvcx) Dale Analyzed 942797 DI IS 31'Jl (Revised 2/91) -- ~-C Dcpa:-tment of Environment, I icallh, t:. r--:a1unl R=urcc1 Solid Was1c Management Division .:>t-U,-l.rJ.....,~ l"')..J.,r,,...,,...,,1.._,._, •-x---- Site Number ----------------- · P.O. !>ox 260-:7, 306 :--:. Wilmini;ton S1:-ce1 R.akigh, North Carolin• 2761 J Field Sample Number WL-t5>0 2 -LC. Name of Sile WA-R.i2.e.J CorSN Pc:e, l.DFL Sile Location A F'To ,-J N c.. __ ..!..,..;._....:....::::....:.;~-__:....:.....::::;__ __________ _ Collected By 6. (\J tl.H.Ol,6o~ Dale Collected # ,6.?, :JVL'/ ~4 Time / S"'oO C.. S,c'P-H~l-JS Agency: Hazardous Waste X Solid Waste _·_superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concen tr::i te Comments Arsenic --Barium ---Ground water (1) X Solid (5) ~ET ~"l> I="/ LL.. Cadmium ----Chromium --__ Surface water (2) _ Liquid (6) u...u rcJ.,.TT5:. Lead ----Mercury _ Soil (3) _ Sludge (7) .::SPL /'r' tvl FCO Selenium --J Silver -:re. -603 -~t:.. --_ Other (4) _ Other (8) eco --&>OP ro.e. ::r-c:::. -~o '?:. -L c-_ -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ----_x_ Acid:B/N Ext. Barium carbon tetrachloride ----.MTBE Cadmium chlordane ------ChJoride chlorobenzene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride m-crcsol ------ ---Iroo __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dich loroelhanc --Nitrate 1, 1-dichloroethylene ----2,4-dinitrotoluene Selenium ----Silver heplachlor ----Radiochemistry Sulf ales hex.achlorobenzene ----Zinc hexachlorobutadiene ----Paramelt!r Resu I ts (PCi /1) pH hex.achloroelhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS nitrobcnz.cne ------TOC pcntachlorophenol ---- --__ pyridine Microbiology ----t etrachloroeth ylcnc trichlorocthylene ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin -- Date Reccivcd7-..;??-f'<i{~41J lindanc --Reported by methoxychlor --e>J~ toxaphenc D:ite Extracted Y-s-9'17/P --Date Reported 2,~-0 -- ?-2-9</,8Q 942798 __ 2,4,5-TP (Silvcx) Dale AnalrLed Lab Nt:rnbcr --I) 11 S 31 'Jl ( llcviscd 2/Y l) I I I KC Dcpar.mcnt or Envirunmcnt. l lcalth, I,;. 1'aLunl Re.sources Solid Waste Manatcmcnt Division SAMPLE ANALYSIS K.tl.J u.t...:, 1 :,111c uoonuory 01 ruouc ncaun · r.o. Oox :ZSO.:i, 306 s. Wilmin~on Str:CI R.Alcith, North Carolina ::?7Gl 1 Sile Number ----------------Field Sample Numbcr_-..:W=...:::/..,;:;..._-....:;t?'---0...;;./_-_1.._C. ______ _ Name of Site WA-1<..2.e.J Gorvrt PC"B U,FL Site Location A F"To ~ NC.. -~_;__....:....:::....:..::::...__~~----------- Collected By a. f\) l(.H.0\.,6c>-...J Date Collected 2.'il' 7t!t..?' q4-Time l.9oQ ~ . ~Te-PH.~ 5 Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds -- - - Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium L Solid (5) ---· __ Ground water (1) Q.ey L1MJ'l>t:11.-<-Cadmium --Chromium Co A..J r ~.,u-r..s -- __ Surface water (2) _ Liquid (6) Lead -- w/1ec.a --Mercury _ Soil (3) _ Sludge (7) ~ PJ..17 Selenium --Silver --...J-C-ooi-J...C... _ Other (4) _ Other (8) -- -- -- Organic Chemistf}' Inorganic Chemistry -- : Parameter Resu Its (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _LP&T:GC/MS Arsenic benzene ---- Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-d ich loroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrololuene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Paramett:r Results (PCi/1) --pH hexachloroethanc --__ Gross Alpha --Conductivity __ methyl ethyl ketone Gross Beta TDS ni1robenzcne ------TOC __ pcnlachlorophenol -- --__ pyridine Microbiology ----I etrachloroethylene ----trichloroethyleoc Parameter Results (Col/lOOml) __ 2, 4 ,5-Lrich lorophc:nol -- ----__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lindane Dale Received 7-.,,..."' f-,9,"1f .&Reported by --methoxychlor --__ toxaphene Dote Extracted Date Reported 2,4-D -- 8-5-q4--n ur __ 2,4,5 -TP (Silvex) Date Analyzed Lab Number 942795 DI IS 3191 (llcviscd 2/91) -- I kalth, & 1'.a1ural R=urccs Solie W.astc Management Division Si1e Number ---------------- J'.U. l.>OX ~ , • .)lf,,,,Q i"'. "11m1n1;1un .,>1TT;.t:l R.alcigh, North Carolina 2761 I Field Sample Numbcr_....:W::..=...:.J.....:;__-_cJ_0...:./_-_1-_C ______ _ Name of Site WA-Ri::2..e..J GarJT'i PG"E, U)FL Site Location A F'To l...J NC _.!.,..;.~....:....:::....:..::~-_;_:_~----------- 'Collected By ~. f0 tl.H.o l. 6c,I-,..) Dale Collected Z.'3" 7(!L.)' Gy4-Time / Si'o Q ~ . ~TeF> H. -eu S Agency: Hazardous Waste )( Solid Waste _· __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium L Solid (5) ---__ Ground waler (1) Q,ey LA:N'i:>,:::=1LL. Cadmium --Chromium Co A.Jr €=.UT..5 --__ Surface water (2) _ Liquid (6) Lead -- w/~c.a --Mercury _ Soil (3) _ Sludge (7) -:5PJ..IT Selenium --Silver --..:re -oo I-1-c.,. _ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) O~anic Compounds Results (mg/I) P&T:GC/MS Arsen.ic benzene ------ Acid:B/N Ext. Barium carbon tetrachloride ------~ Cadmium chlordane .3 () /, ',l 9""' ----Chloride ehlorobenzene =~ ----7 Chromium chloroform ---- --__ Copper o-cresol --Fluoride rn-crcsol ------ --Iron __ p-cresol --Lead crcsol ------ --__ Manganese 1,4-dichlorobenzeoe -- --__ Mercury --1,2-dich loroethane Nitrate 1, 1-dichloroelhylene ------Selenium 2,4-dinil rotoluenc ----Silver __ hcplachlor --Radiochemistry Sulfates hexachlorobenzenc ----Zinc hcxachlorobutadicne ----Paramelt:r Results (PCi/1) pH hexachloroethanc ----__ GrCJ5S Alpha __ Conductivity __ methyl ethyl ketone Gross Bela TDS nitrobcnzcne ------TOC __ pcnlachlorophenol -- ----pyridine Microbiology --__ telrachloroethylenc ----Lrichloroethylenc Parameter Results (Col/l00ml) __ 2,4 ,5-trichlorophcnol -- ·-__ 2,4,6-lrichlorophcnol --------vinyl chloride cndrin -- 7-..Z.tj-f~.i)Reported by lindanc --D<1te Re.ccived methoxychlor -- D:itc Extracted ~-S-9 ~-VJJ __ toxaphene Dale Reported 2,4-0 -- D.ilc Analyzed ~-9-9'~-V,O 942796 __ 2,4,5-TP (Silvex) Lab Number DI IS 3l'Jl (llcviscd 2/Yl) -- I I I ! I t-.C. Depar.ment of Environment, I lcalth, & 1'a1ur.l Re.sources Solid Waste Management Division Si1e Number SAM.l-' LJ::., A.NALl .::,J..::, .K.L\,l u.c...:, J. . P.O. Oox :?SO-:i, 306 K Wilmini;,on Street Raleigh, North Cuolina 27611 ----------------Field Sample Number __ W_L_-_O_C>_I_-_F_L _____ _ Name of Site WA-1<.i2.e.J CorJT'i PG"B l.DFL Site Location A F"To t-J NC _::..._._.;...:;;_...;....;:; ___ =------------- Collected By a. f0 ll.H0\,..6o~ Date Collected Z"B .::TPL.. Y '14-Time 09Z6 L. l2esE Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls (mg/I) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) :f,,P-A.f];:) ,t:°i '-TE,'?:.. --Cadmium Chromium --//1 El:>/ V,s.,L __ Surface water (2) _ Liquid (6) Lead -- --Mercury Soil (3) Sludge (7) Selenium ----Silver --_£ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Ori;;anic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N E>..1. Barium carbon tetrachloride ------.MTBE Cadmium chlordane --< tJ. 7 t' /f?l!..M.. ----L ?C.'B Chloride chlorobenzene --Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol --------Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichlorocthylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Paramelt:r Results (PCi/1) _pH hcx.achloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----tetrachloroethylcne ----trichloroethyleoe Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trich.lorophenol ----vinyl chloride --endrin -- 7-,,,?9-?'71/~& Reported by lindane Date Received --mcthoxychlor -" -.- Dale Extracted 3'-j'-r(/1/f' __ toxaphene Date Reported 2,4-D -- Dale Analyzed '3"'-'l._-f'// 1/,L) 942600 2,4,5-TP (Sil·,cx) Lab Number DI IS 3191 (llcviscd 2/91) -- l',:.C Dc:pa:-:ment of Environment, I lc:alth, &. l\'alunl Resource~ Solid Waste Manabemc:ni Division SAMPLE ANALYSIS REQUEST State Labontory of Public Health Site Number ---------------- · P.O. l3ox 2.SO,:i, 306 S. Wilminpon Str.:cl Raleigh, North Carolina 27Gl I Field Sample Number W L-eo 2 -F'L_ Name of Site WA-Ri2.e..J GorJTY PG"E> l.DFL Site Location A F"To ,v NC... _.,:._;__....:....::;._;_:::..._ _ __:..-=.----------- Collected By a . /\) ll.H.Ol,6C))o..) ID# 3=1--Dale Collected 2 g :TVL "I c:; 4 Time <9q r 5 L./2z::>6e Agency: Hazardous Waste X Solid Waste __ Supcrfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium C1--1Al:?CJ0AL. h1...r£12 ---Ground waler (1) _ Solid (5) Cadmium ----Chromium t/,1F'DIVA'l --__ Surface water (2) _ Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Sc:lenium ----Silver --£ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resu I ts (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane --PCB <p.70 ~/T\... ----.lL Chloride chlorobenz.ene ----Chromium chloroform ------ --__ Copper o-cresol --F1uoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ ----Manganese --1,4-dichlorobenz.ene --__ Mercury --1,2-dichloroethanc --Nitrate 1, 1-dichloroethylene ----2,4-dinitrololuene Selenium ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hexachloroethanc --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenz.ene ------TOC __ penlachlorophcnol -- --__ pyridine Microbiology ----tetrachloroeth ylenc --__ trichloroethylcnc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ------vinyl chloride endrin -- 7-2._'7-f tf,Jl;:,d2} Reported bv lindane --Date Received mcthoxychlor , ' -- <f--K--9¢ 1/,P --toxaphene Date Exlractcc.l Dale Reported 2,4-D -- Y-9-9¢1/f) 942801 __ 2,4 ,5-TP (Silvcx) Dale Analyzed Lab Number DIIS 3191 (Revised 2/Yl) -- ,S:.C. Dcpar.mcnl o{ Environment. I lc•llh, l.. 1'•tural Resources Solid Waste M•nai;emcnl Di,-ision .::,AMt' Lt A.J'\n....L.,.l .::,1;:;, r,..,J:.,\,l UJ.J.J J. -·-·----·-·-·; -·. -------- P.O. Ika 280-:7, 306 S. Wilmint1or. Street Raleigh, North urolina 27611 Sile Number -----------------Field Sample Numbcr ___ W;;;__:__t.'-----=(!:)~CJ_l_-____.8=...:L::::;_ ___ _ Name of Site WA-R.~e.J C:ior.JT'I PC.r:, /...DFL Site Location A F"To >0 NC _.<,...;.._....:....::....:....::<--_;,_;c....-=::,__ __________ _ Collected By 6 . fv, C.H.o l. 6c>'-' ID# 3-=t-Dale Collected Zt> ::f V LY 9 4 Time /t:J20 ~ S,€PH lt?"6-.)":::» Agency: Hazardous Waste X Solid Waste ___ Supcrfund TCLP Compounds ------ Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Groundwater (1) _ Solid (5) 4E p(/,47t.,€_ Cadmiuru --Chromium --_ Surface water (2) _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Seknium --Silver --~ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) ]5_P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --F1uoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzeoe -- --__ Mercury 1,2-dichloroethane -- --Nitrate __ 1,1-dichloroethylcnc --Selenium 2,4-dinitrotoluenc ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) _pH hcxachloroelhanc --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobcnz.cne ------TOC __ pcntachlorophenol -- ----pyridine Microbiology ----t etrachloroethylcne --__ trichloroethylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ----__ 2,4,6-trichlorophcnol -- ----__ vinyl chloride cndrin --lind:!ne 7-e?f'-f&5',6..L)Reportcd by Date Received --__ methoxych_lor --toxaphcnc D..itc Extracted Date Reported '.?.,4-D -- D.ilc Analy1.ed ~-J -q4 :ztu.c Lab Number 942802 DI IS Jl'Ji (Revised 2/Yl) __ 2,4,5-TP (Silvcx) -- ! i ! I I I ! l I I :S:.C. Dc?3r.mcn1 of Environment. 1 lcalth. l:. 1'a1unl R=urcc:s Solid Was1c Manai;cm~nl Division ::>ANl.t' Lt A..:,A.L1 ::,L.::, rv...,'-l VJ...-..J,. -------------; --. ---------···· r.o. Dol 280-:7, 306 s. WilminJ;lOn S1rcc1 R.alcii;h, North C.arolina 27GJ J Sile Number Field Sample Number W L -~ 0 2 -f3 L -------'----CC.--=------------------------ Name of Sile WA-R.2-c.J GorST'i PG"B l.DFL Sile Loc.a1ioo A F"To >--J NC _..:......;__....:....::....:...::,:__ _ _;._;:......:::;.._ __________ _ Collected By G;. fv 1c.H.0L.6c>-,...J Dale Collected ZB -:IV-L. Y ~4 Time / l-10 G ~ . s.re-Pf-te->--.:> Agency: Hazardous Waste X Solid Waste ___ Super fund TCLP Compounds --- - - - Sample Type Inorganic Compounds Resu I ls (mg/I) Environmental Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Solid (5) l>. I-. to A T-c-R.. Cadmium ----Chromium -- Surface water (2) _ Liquid (6) Lead ----__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --L Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/!) (mg/kg) Organic Compounds Results(mg/1) .x_P&T:GC/MS Arsenic benzene ---- Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iroo p-cresol ----Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-d ich loroet hane --Nitrate 1, 1-dichloroet hylcne ----Selenium 2,4-dinilrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcxachlorocthanc ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitroben7.ene ------TOC pentachlorophenol ---- --__ pyridine Microbiology --__ tctrachlorocthylcne ----trichlorocthylcnc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol -- --__ 2,4 ,6-trichlorophcnol ----vinyl chloride ----endrin -- 7-,?9-l_<f 'f//', g.ZJ Reported by lind;rnc D1:1tc Received --me:hoxychlor ... -- D:i.tc Extraclcc..l __ toxaphenc Date Reported 2,.!-0 -- Date Analy-1.cd c;,-1 -q'-1---nur-942803 2,4,5-TP (Silvcx) Lab Number DI IS JJ'JI (llcviscd 2/Yl) -- I I I llcalth, & 1'a1ural Ruourccs Solid Waste Manatcmcnl Division Site Number ---------------- · P.O. Oox ~7. 306 S. Wilminpon S1rcc1 R.alcigh, North Carolina 2761 l Field Sample Numbcr _ _;tu~_L_---=t!J_;0::;....;:3=---__;;;B=--L ____ _ Name of Site WA-R.iLe,.J GorvT't PG'B l.DFL Site Location A F"To ~ NC.. _:,__;__.:....:::~~-:.....:...=------------ Collected By (;;;. f\) rcH.o l, 6c>),,.,) Dale Collected 25 :TtlL Y 9+ Time /:/-4-S- ~ . ~TE:? H -e)v ~ Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) t>.F. tvArc~ Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium --Silver --_K_ Other (4) Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _LP&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ---- --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-crcsol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol -- --__ pyridine Microbiology --__ tetrachlorocthylcne ----trichloroethyleoe Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol ------vinyl chloride endrin --lind:rne Date Received 7-2.'1-f'fpt@Rcported by --__ methoxychlor __ toxaphcne O;itc Extracted Date Reported 2.~-D -- Dale Analyzed '?-.:1-94--nu..,_:, 942804 __ 2,4,5-TP (Silvex) Lab Number --DI IS 31')1 (Revised 2/91) 1'.C. Dcpar.mcnt o! Environmcn[, l lcalth, &; 1'a1ural Re.sources Solid Was1c Manai;cmcnt Division SA.M:PLE ANALYSIS REQUEST Stale uboratory o( Public Health · P.O. Oox ~i. 306 K Wilminpon S1rcct Julc:igh, North Carolina 27611 Site Number ----------------Field Sample Number_......:::;.W-=-L..;..:._-_,<2~~:;.....i4_-_,,B"'--L _____ _ Name of Site WA-R.~e.J GorvT't PCB l.DFL Site Location A F"To~ NC l -.<....:..-..:.....=~:____:...:....=.----------- Collected By a . fv I l. H.o \.,..1!:,C)),,..) ID# 3-=t-Dale Collected fl JtJl:f t::/4- ~-ST-EPtt a:>-" Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ---- · Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic --Barium ---__ Ground waler (1) _ Solid (5) 0. I=": Wttf~"R. Cadmium --Chromium A-1R Hos~ --__ Surface water (2) _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --.Js._ Other (4) _ Other (8) -- -- --Organic Chemistry· Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) _x_P&T:GC/MS Arsenic benzene ----Acid:B /N Ext. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --F1uoride m-cresol --------Iron __ p-cresol --Le.ad -cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Paramelt:r Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnzcne ------TOC __ pentachlorophenol -- --__ pyridine Microbiology ----telrachlorocthylcne --__ trichloroethylenc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophcnol --__ vinyl chloride --endrin -- ?-,;l..tj-f~fl/ d..iJReportcd by lindane Date R::c:!ived --__ melhoxychlor .,/ __ Loxaphene Date Extracted Date Reported 2,4-D -- Dale Analy-~ed CJ' 1,_-9J..J 1]1J.[: Lab Number 942805 __ 2,4,5-TP (Silvex) DI IS 31'/1 (Revised :?./Yl) -- l lc:illh, l,; 1'•1ur.l Ru.ourccs Solid Was1c :,,{anai;cmcn1 Division Site Number ----------------- P.O . Dox 280,:i, 306 t,;. Wilmini;,on Street R.alcii;h, North urolin1 2761 J Field Sample Numbcr_---=:..W __ L_-_O_.::;O_/_-_t;,-'---w _____ _ Name o( Site WA-R..2.ei-J CborJT'i PGb l.DFL Sile Location A F"To i-.J NC.. _,!....;.._....:....:::..:_::::..__~:....;::=-------------- Collected By (;. f\) 1(.H.OL.6c:n-J Dale Collected C. € 'J t>L-/ '1 ~ Time /I 3£° T. V.JA1-K:EI::- Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium t± ---· ..JS,._ Ground water (1) _ Solid (5) WELL I Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- ; Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) ~ P&T:GC/MS Arsenic benz.ene ----Acid:B/N Ext. Barium carbon letrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-crcsol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese 1, 4-dichlorobenz.enc -- --__ Mercury --1,2-dichloroethane --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinilrotoluenc ----Silver hcptachlor ---- Radiochemistry Sulfates hexachlorobenzenc ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) --pH hcxachlorocthane --__ Gro5s Alpha __ Conductivity __ methyl ethyl kelonc Gross Bela TDS nitrobenzene ------TOC __ penlachlorophcnol -- --__ pyridine Microbiology ----l clrachloroethylene --__ lrichloroclhylcnc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol -- --__ 2,4,6-lrichlorophcnol ----,inyl chloride ----endrin --lind:rnc 7-..27-l'lf? &Reported by Dale R::ccived --__ mcthoxychlor --toxaphenc Dale Exlraclec.l Dale Reported 2,-:!-D -- Dale Analyzed 'ef'-~-9'-f 7U,IT Lab Number 942806 __ 2,4 ,5-TP (Si!vex) 1)1 IS Jl'Jl (llcviscc 2/Yl) -- , ... -. ...,,, .. ~-·····-··· -· -,-.. _. ............ , llcahh, & 1'a1ur.l Rc.l.Ourccs Solie Wa\tc ~bnai;c:ncnt Division -·-·-... --·-··-------....... ----. P.O. !>Ox 260,:i, 306 ?-,;. Wilminf;'On Str:c: R.&lcii;h, Nonh urolina :?7GJ J Site Number -----------------Field Sample Numbcr_..-:...W...:__L_-_cJ__,;:0~/_-_c;,,_w _____ _ Name of Site WA-R.>2-e.J GorvTY PG"B l.DFL Site Location A F"101'J N (._ ·_.:....;.....:..._....:....::::..:.::~-~:_.:::::_. __________ _ Collected By a. {'v ru--t.01,,..6o'-' ID# 3 =?-Date Collected Z 'B :JI.} L-/ q 4t Time /13£" T. t,,LJF1t..kER..... Agency: Hazardous Waste X Solid Waste __ Super fund TCLP Compounds ------ Sample Type Inoq;anic Compounds Rcsulls(mg/1) Environmental Concentrate Comments Arsenic --Barium tt ---· ~ Ground waler (1) _ Solid (5) WE L.L l Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mercury Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) 011:anic Compounds Rcsulls(mg/1) P&T:GC/MS Aisco..ic benz.enc ----· --Acid:B/N E>..t. Barium carbon tetrachloride -.MTBE ----Cadmium chlordane ~ ?GB IP1:sT <o. ooo / ----Chloride chlorobcnz.ene 7 ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride rn-cresol ------ --Iron __ p-crcsol --Lead ere.sol ------ --__ Manganese 1,4-dichlorobcnzcne -- --__ Mercury 1,2-dichlorocthane -- --Nitrat~ 1, 1-ciichlorocthylcnc ----Selenium 2,4-dinitrotolucnc ----Silver heptachlor ----Radiochemistry Sulfates hcxach lorobenz.ene ----Zinc hexachlorobutadicnc ----Paramt!lcr Results (PCi/1) pH hcxachlorocthanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcn1.cne ------TOC __ pcntachlorophcnol -- --__ pyridine Microbiology ----t e lrachloroet h yl enc ----trichloroethylcne Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophenol --vinyl chloride ----endrin -- Date R=ccived 1--2 ?-'l7(f!j,,6.J) Reported by lind;inc --mcthoxychlor -- Dale Exlractcd j'-/-~Y/j'At!3 --toxaphcnc Dale Reported '.2,~-D -- Dale AnalrLcd ~-~-91/7/,,0 942807 ::?.,4,5-TP (Silvcx) Lab Number DI IS 3J'JI (ltcviscd 2/YI) --I . I lcalth, l,:. t'-alvnl Rc.sour~cs Solid Was1e Manai;cmcnl Division Site Number ---------------- P.O. l>o1 ~i. 306 S. Wilmin~on Str::cl Raleigh, North Carolina 2761 I Field Sample Numbcr _ __:_W_L_-_o__;;o;;.__l_-_~_w _____ _ Name of Site WA-1<.;2.e..J GorJN PGT!:, lr,FL Site Location A F"To ,-,J NC _!....:.....:....__;__::....:..:::...:....__.;....;...=.----------- 1Coilecled By G;. /\) 10-to l. 6cn-J Date Collected c ~ ':J l.}L-/ C\ 1-Time /13~ T WALkE:R.. Agency: Hazardous Waste X Solid Waste __ Supcrfund TCLP Compounds ----- Sample Type Inoq;anic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium tl: ---· _lL Ground waler (1) _ Solid (5) WELL I Cadmium --Chromium --__ Surface waler (2) _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge C0 Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results(mg/l)(mg/~) Organic Compounds Rcsul ts (mg/I) P&T:GC/MS Arsenic benz.ene ------~ Acid:B/N Ext. Barium carbon tetrachloride ----"MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-diehlorobcnzene --__ Mercury --1,2-dichloroelhane Nitrate 1, 1-dichloroelhylcne ------Selenium 2,4-di nil rotoluene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethanc __ Gross Alpha ----__ Conductivity __ methyl ethyl k~tone Gross Bela TDS nitrobenz.cne ------TOC __ penlachlorophcnol -- ----pyridine Microbiology --__ telrachloroclhylcne ----trichlorocthylcoc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophcnol ------\inyl chloride endrin -- 7-.z-r-1ffta; lind:rnc D.itc R::ceivcd --Reported by __ mcthoxychlor - O;itc Extractcd]rJ-qi/ b4 lVft: __ toxaphcnc.: Date Reported 2,4•0 -- D;itc Analyt.c.:d <J.._-;J..-7<-/ aEJ. 942808 __ 2,4,5-TP (Silvex) Lab Number DI IS :ll'Jl (llcviscJ 2/91) -- 1,_.._ i,Jc.;,J.r..n,c.nt or l..:.nvuo,,mc.nt, I leallh, &.:. /':alur.l Re.sources Solid Waste Manai;ement Division . P.O. fk>x ~i. 306 S. Wilmin~O!'I s,~cl Ralcii;h, North Drolina 27GI I Sile Number -----------------Field Sam pie Numbcr_....;Wc...:;._.::.'-_---=t)'--l):........:::Z=-----"~=-W--=------ Name of Site WA-1<;::2.c:.J Gol'JT'1 PG'?;, l.DFL Site Location A F',o i,..J N (_ ·_.:....;._;_....:...;::::....:..:,:::_ _ _;_~=------------- I Collected By G;;. (\) 1CH.ol,.6cn•--' Date Collected Z<g -:J (.) L--/ 9"4 Tune /"f 3~ T. t.,.,U,:,J.-k, ER Agency: Hazardous Waste X Soud Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concen tra le Comments Arsenic --Barium L Ground water (1) :Hz ---· _ Saud (5) W~I..L Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- --Mercury _Soil (3) _ Sludge (7) ,Sp~ I "T tAJ/ ~Co Selenium . --Silver --_ Other (4) _ Other (8) re-001-fiw -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride -.~ ----Cadmium chlordane ----Chloride chlorobenzene ~E5T <o. ooo/ ----Chromium chloroform --· ---- --__ Copper o-cresol --Fluoride ro-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobcnzcne -- --__ Mercury 1,2-dichloroethanc ----Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Z inc hexachlorobutadienc ----Parameltr Resu I ts (PCi /1) pH hcx.achloroclhane ----__ Gross Alpha --Conductivit y --methyl ethyl ketone Gross Beta TDS nit robcn zene ------TOC pcntachlorophcnol ---- --__ p)'ridine i\1 i cro biology --__ tetrachlorocthylcne --__ tri chlorocthylenc Parameter Results (Col/lO0ml) __ 2,4 ,5-trichlorophenol ----__ 2,4,6-trichlorophcnol ----\inyl chloride ----cndrin -- 7-.,Z.'l_-f//-Jl/~cported by lindanc Dare Received --mcthoxychlor .,, -- D.il:: Extraclec.l 'K._-/-9//1/P,A.i --toxaphcnc Date Reported 2.~-0 ;; -- Dale A naly'Lcd ~-;i-'l._¢'1/p · 942809 __ :?.,4,5-TP (Silvex) Lab Number l)IJS 3191 (Revised 2/91) --. r-:.c Ucp~r.mcnt or tnYH~nmcnt. llc~llh, I,. ;--;~lunl Rc..s.ourccs Solid Waste l'-bnai;cmcnt Division Sile Number ----------------- P.O. Oox 280-l7, 306 S. Wilmin~on Str,::ct Raleigh, North Carolina 2761 I Field Sam pie N um bcr_....::.W-=:........:t.;;.;__-__,0:...:::lJ~Z=----~=-.::..W-=------ Name of Sile WA-1<..2.e.J CborJT'l' PG"t> l.DFL Site Loc.alion A F"T"o ls.J NC.. _...:.....; _ _;_;:;_;_=-... __ .;......;:=------------- Collected By 6 . fv 1c..HoL.6c>~ Date Collected . Z'8 :Ju L--/ q4 Time /7-3~ I. ~"' t->'-e.e... Agency: Hazardous Wasle X Solid Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ~2. ---L Ground water (1) _ Solid (5) W~LL Cadmium --Chromium --Surface waler (2) _ Liquid (6) Lead ---- --Mercury _ Soil (3) _ Sludge (7) .:Sp~ I 7' IA.J/ ,/:"GO Selenium --Silver --_ Other (4) _ Other (8) :re-oo ,_ 'i w -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Resulls(mg/1) P&T:GC/MS Arsenic benz.ene ----..:i_ Acid:B/N Ext. Barium carbon tetrachloride ----.MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride rn-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese --1,4-diehlorobenzene --__ Mercury --1,2-dichloroethane --Nitrale 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachl orobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hcxachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pentachlorophcnol -- --__ pyridine Microbiology ----tctrachloroclhylene ----trichloroethylene Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichlorophenol ----vinyl chloride --cndrin -- 7-~f-9f(-r/f .tf{2)Rcporlcd by lind:rne Date R::c::ivcd --methoxychlor -- <:J-oJ-q¥ Af>;Wv.. Date Reported __ toxaphcne Date Exlractcc.l 2,4-D -- 9-r;). -'1 t.f B~ 94281.0 __ 2,4,5-TP (Silvcx) Dale Analyt.cd Lab Number DIIS Jl'Jl (Revised 2/YI) -- I lc:al:h, /,.:. ;-.;a1unl Rc.s.ourcc:s Solie Was:c Management Di,-isior, Raleigh, North C&rolina :?7Gl l Sile Number Field Sample Number WI--0 lJ Z -~ W ---------------- Name of Site WA-R.:2.e.J GorJN PGt;, U,FL Site Location A F"101'..l NC.. _:_;__....:....=;....:..;::<---~-=------------ Coll,ecled By a ' tv IC.H.Ol,6c,)-J Dale Collected Z'S ':IL) L '/ 9' 4 Time /°f 35 T. lAJ ,H .. k: E le!. Agency: Hazardous Waste X Solid Waste _· _Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concentrate Comments Arsenic --Barium Ji_ Ground water (1) d:lz ---_ Solid (5) w~1.L. Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury _ Soil (3) _ Sludge (7) .5P~J 7' tAJ/ /:CO --Selenium • --Silver --_ Other (4) _ Other (8) re-oo ,_ 'i u.1 ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Organic Compounds Results(mg/1) ..£_P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----"MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dich loroethane -- --Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-dinitro1olucnc ----Silver __ heplachlor --Radiochemistry Sulfates hex.a ch lorobenz.ene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzenc ------TOC __ penlachlorophcnol -- --__ pyridine l\1 icro biology --__ tctrachlorocthylene --__ lrichloroethylene Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol -- --__ 2,4,6-lrich.Jorophcnol ----__ vinyl chloride --endrin -- 7-e,lf-f f/'1//Jdfd Reported bv lindanc Dale Received --__ melhoxychlor ;> • __ toxaphcnc Date Extracted Date Reported 2,4-D -- Date J..nalyzcd ?-;J_ -C/Lfw;r __ 2,4,5-TP (Silvex) Lab Numbc~ 9'12811 DI IS 3i')I (Rcvisc:c :?/Yl) -- I 1 ·,c~:th, &. 1'a1unl Rc.s.ourccs SoliJ \l,'astc Manai;cmcnl Di,-uion P.O. !lox ~,. 306 S. Wilmini;ton S1rcc: R.tlcigh, North Carolina 27GI 1 Site Number -----------------Field Sample Nwnbcr_---=.tu...:........:t..:___-_0--'O;......::3::__-.....;::~::t....::W--=------ Name of Site WA-R.i2.e.J GorJn' PC-"'B l.DFL Site Location A F"To >0 NC -~-....;...::;_;_;::__ __ c......;:=:;.._ __________ _ Collected By ~. f0 rc.H.o L 6cnJ Dale Collected 2"1 :::i UL. Y CJ4 Time /too L.. ,QoSE Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concen lrate Comments Arsenic -- '#3 Barium ---· L Ground water (1) _ Soiid (5) lUELI.-Cadmium --Chromium --_._ Surface water (2) _ Liquid (6) Lead -- --Mercury Soil (3) _ Sludge (T) Selenium ----Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/1) (mg/kt;) Organic Compounds Resulls(mg/1) P&T:GC/MS Arsenic benz.ene ------ Acid:B/N Ext. Barium carbon tetrachloride -.MTBE /4 ----Cadmium chlordane ---- X ~§7_ <"O.OOP/ Chloride chlorobenzcne ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m -cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzene --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoiucne ----Silver __ heptachlor --Radiochemistry Sulfates hcx.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH --hcx.achlorocthane __ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Bela TDS nitrobenz.cne ------T0C __ pentachlorophcnol -- ----pyr idine Microbiology ----t e trachlorocthylcne --__ trichlorocthylenc Parameter Results (Col/lOOml) 2,4 ,5-trichlorophcnol ----__ 2,4 ,6-trichlorophcnol ----\inyl chloride ----cndrin --lind:inc 7-Af-fY"t/,t~J)Rcportcd by Diitc R~ccivcd --mcthoxychlor -- Date Extracted ~-:;;,-ft/ :V~alc Reported --toxapncnt: 2,~ .. o -- Dale Analyzed 8-~-9~Jp::> · 91.\2812 __ 2,-1 .5-TP (Silvex) Lab Number 1)1 IS 31'JI (Revised 2/Yl) -- llcahh . .t l',;a1ur.! Ru.ourccs Solid W.s1c Man•i;cmcn1 Di,isior, D R.alcii;n, North Carolina 27GJ l Site Number -----------------Fic:.ld Sample Numbcr_~t-v..;......;L'-----0_O--='3~--.:::~:!..-l-U _____ _ Name of Site WA-'<.2.e.J GorvTY PGt, l.DFL Site Location A F"'To ~ N (_ _..:......;,._....;....:;:...c..=-. __ --=:;..._----------- Collected By G . fv , c H. o 1.., 6::::n--' ID# 3-=f-Dale Collected 2,: ::JV LY '94 Time / t, o O L 12 e>t:,E Agency: Hazardous Waste X Solid Waste ___ SuperfUDd TCLP Compounds ------ Sample Type Inorganic Compounds Rcsults(mg/1) Environmental Concen tr:i le Comments Arsenic -- #3 Barium ---· £ Ground waler (1) Solid (5) lUEJ..L Cadmium --Chromium --Surface water (2) Liquid (6) Lead ----Mercury --Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/~) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ----L Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobe.nzcnc ------Chromium chloroform --·-----__ Copper o-cre.sol --Fluoride m-crcsol --------Iron __ p-cresol --Lead ere.sol ------ --__ Manganese. --1,4-dichlorobenzene --__ Mercury --1,2-dichlorocthanc --Nitrate 1, 1-dichlorocthylcnc ----Selenium 2,4-dinitrotolucnc ----Silver __ he.ptachlor --Radiochemistry Sulfates hcxachlor obenze.ne ----Zinc he.xach lorobut ad iene ----Parameter Resu I ls (PCi /1) _pH hexachloroethanc --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC __ pcntachlorophcnol -- --__ pyridine Microbiology ----tetrachlorocthylcnc lrichlorocthylcnc ----Parameter R~sulls (Col /lOOml) 2, 4 ,5 • l rich I orophcnol --------__ 2,4 ,6-trichlorophcnol --\inyl chloride ----cndrin -- .7--e:lr-?ft!ytLf.2JRcportcd by lind:rnc Date R:ccived --mcthoxychlor -- D..itc Extracted ~-f-C/'f A; vVb' __ toxaphc:ic Date Reported 2,~-0 -- Dale f...nalyzcd g'-rJ.-1c./ t3£) 94281.3 _ 2,4,5-TP (Sil'ICX) Lab Number I) l IS 31 'Jl ( Rcvi~cd 2/91) -- I ic3lth, l:. l'-'•lur.l Ruourccs Solie Waste M•n•i;cmcn1 Di,ision r·.u . 1.>0x ~, • ..)UC) f'. w11m1nb10n =>ni:c• rulcii;h, North C.rolina 27Gl i Site Number -----------------Field Sam pie Numbcr _ __::..?U~t._-_0..:0'--=3=----<=v=-..::u.,/-=------ Name of Sile LUA-1<..2.c.J GorvT'1 PGr, U,FL Site Location A F",o "-.l NC.. _..:....;._...;_::...,;..:=--------'-=:;__----------- Collected By a. f'v ll.H.0\_.6:::,~ Dale CollecLed 2:l ::JULY C/4 Time / &. o o /_. /2~£ Agency: Hazardous Waste X Solid Waste __ Super fund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Enl'ironmcntal Concentrate Comments Arsenic -- "#3 Barium ---· L Ground water (1) Solid (5) ll/EJ..L Cadmium --Chromium --Surface water (2) Liquid (6) Lead ------Mercury Soil (3) _ Siudgc (7) Selenium ----Silver --_ Other (4) _ Other (8) --' -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (rng/k&) Organic Compounds Results (mg/I) _x_ P&T:GC/MS Arseo.ic benz.cne ----Acid:B/N Ex1. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzcne ------Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol ------ --Iron p-crcsol ----Lead crcsol ------ ----Manganese --1,4-dichlorobenzcne --__ Mercury --1,2-dichloroethanc --Nitrate 1, 1-dichlorocthylene ----Selenium 2, 4-dinit rol olu::ne ----Silver __ heptachlor --Radiochemistry Sulfates hcx.achlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hcx.achloroethane ----__ Gross Alpha --Conductivity __ methyl ethyl k::ione Gross Bela TDS ni1robenz.ene ------T0C __ pcnt.ichlorophenol -- --__ pyridine Microbiology ----tetra ch lor octh ylene ----trichlorocthylcnc Parameter Rt:sulls (Col/lOOml) __ 2,4,5-trichlorophenol ------__ 2,4,6-trichJorophenol ----\inyl chloride --cndrin -- 7-e:2.3-1¥'/I/J~cportcd by lind:ine Date R:ccived --methoxychlor 7 --_._ toxaph::nc Date Extracted Date Reported 2,.:.0 -- Date Analylcd ? ., J.-94 111,Lt_ Lab Number _ :?.,4.5-TP (Sil-lex) 942814 1)1 IS 3l'Jl (ltc,iscd 2/91) -- I lcalth, l,; ;-,,'atunl Ruourccs Solid Waste ;\ian•&cmcnt Division Sile Number ---------------- P.Q. [}OX W,)-, I, .:;.JO I'\, w11m1n~on .-:)ll"CC. lulcig:h, Nor1h Carolina 2761: Field Sample Numbcr_----=-W~L=-----=0;.......;...0_4_-----"bL..:;..;..W _____ _ Name of Site WA-R.:2.e..J GorvT'i PGb lnFL Site Location A F"To 10 NC _.:......:......:.........:....::::....:..::::____.:....=...=----------- Collected By 6. /'v 1c.H.01,...6C>~ ID# 3-=f-. Date Colk.ctcd ..2~ :TUL't' q-4 Time (4-0D 1 . t,,,vl4L-k€R Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- WELL .#4 Barium ---· L Ground waler (1) _ Solid (5) Cadmium --Chromium --Surface water (2) _ Liquid (6) Lead ---- wl --Mercury Soil (3) _ Sludge (7) SPLIT ec..o Selenium --• --Silver --:I"C-002--ee.,VJ Other (4) _ Other (8) --I ---- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/1) (mg/kt) Organic Compounds Results (mg/I) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride -.-.MTBE ----Cadmium chlordane X ~6:,r ----<o. ooo/ Chloride chlorobenzene ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iroo __ p•cresol --Lead cresol ------ --__ Manganese --1,4-dichlorobenzeoe --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotol ucne ----Silver heptachlor ----Radiochemistry Sulfates hex..achlorobenzene ----Zinc hexachlorobutadiene ----Pararnelt:r Results (PCi/1) _pH hex..achloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzenc ------TOC pcntachlorophcnol ---- --__ pyridine i\1icrobiology --l ctr a chlo roe th ylen c -- ----trichlorocthylcnc Param~ter Results (Col/lOOml) --__ 2,4,5-trichlorophcnol --__ 2,4,6-trichlorophcnol ------vinyl chloride --cndrin -- Dale Received 7-;) '1--f¥rtJ l1JP-eponed by lindanc --__ mcthoxychlor Dale Extracted ~-;/.-9¢J/P,/3])oate Reported __ toxaphenc 2,4-0 ., --_ 2,4 ,5-TP (Silvcx) Dale Anal:,-Led F'-~-9'9"1/P 9 .. 1281.5 Lab Number DI IS J!'Jl (llcviscd 2/91) -- ' I I I :--:.C Dc?a:-:mcnt o( E:wironmc:nt, I lc:alth, l..:. :--a1ural Rc..s.ourccs Solid Waste Manai;c:mc.nt Division . P.O. Dox 250-:7, 306 1'. Wilmingion S1rcct R.alc:igh, North Carolina 27Gl l Si1c Number Field Sample Number W L-004 -bt.W _ ___;:..___;__:..__ ___ :;:.::_-=-------------------------- Name of Site WA-Ri'.2.e...J GotJTY PG"P:, U,FL Site Location A F",o >-J NC -'-'----'-=-.;:...:::_ _ __;_:;~---------- Collected By G; . I\) I('.. Ho l. 6C>~ Dale Collected ..2~ :f(.)C)I' q4 Time 14-0D T-U-'~l-1<.€:R. Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic -- WELL .#4 Barium ---L Ground water (1) _ Sol.id (5) Cadmium --Chromium --_ Surf ace water (2) _ Liquid (6) Lead -- w} --Mercury _ Soil (3) Sludge (7) SPLIT e c.o Selenium • --Silver --_ Other (4) _ Other (8) I"C -DO Z.-«.;,UJ -- -- --Organic Chemist11· Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Resu I ts (mg/I) P&T:GC/MS Arsenic benzene ----L Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------ --Iron p-crc:.sol ----Lead cresol ------ --__ Manganese --1, 4-dichlorobenz.ene --__ Mercury --1,2-dichlorocthanc --Nitrate 1, 1-dichloroc:.thylcnc ----Selenium 2,4-dinitrotoluc:.ne ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadienc:. ----Parameter Resu I ts (PCi /1) _pH hexachloroelhane --__ Gruss Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobcnz.cne ------TOC __ pcnlachlorophenol -- ----pyridine i\1icrobiology ----t e lrachloroeth ylcnc trichloroethylene ----Parameter Results (Col /lO0ml ) __ 2,4,5-trichlorophcnol ----__ 2,4,6-trichlorophenol ----vinyl chloride ----cndrin -- 7-a2!7-ft/rf'6'.1J Reported by lindanc Date R:ceived --__ methoxychlor ✓ __ toxaphene Date Extracted~.-{-qV ~4 W&-' Date Reported --2,4-D 9-;i. -9 'I 13£) 942816 __ 2,4,5-TP (Silvex) Dale AnalyLcd L.ib Number --l)IIS Jl'JI (ltc:visc:d·2/Yl) I I I ;-,:.c Dc?ar.mcnl or Environment. I lcallh, l.:. 1'alural R=urccs Solid Waste ~hn•i;cmcnt Di,-ision ~A.1''1,LL ~,;;J...,.1::,.1...:, ~'-.,('-'....,..,A . P.O. !)ox 280-:7, 306 t-:. Wilmini;,on St~ct R..alcigh, North Carolina 2761 J Sile Number Field Sample Number WL-004 -~W _ __;_....:.,___;;:.._ ___ ....::;_ _______ _ ----------------- Name of Site WA-R-2.e..J G:,orJT'i PC"B l.DFL Site Location A F"10 >v NC, _..:......;._....:....;::::-..:..::::..._ _ _;_~::c...,_----------- ID# 3-=t-Time 14-0D I . (,,(..,?.AL..J<''E/?... Agency: Haurdous Waste X Solid Waste ___ Superfund TCLP Compounds ------ _ Sample Type Inorganic Compounds Rcsulls(mg/1) Environmental Concentrate Comments Arsenic -- WELL .#4 Barium ---X,_ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead -- w/ --Mercury _ Soil (3) _ Sludge (7) SPuT ec.o Selenium • --Silver --Other (4) _ Other (8) IC-DO 2.-ee.,u.J -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/l)(mg/kg) Ori;nnic Compounds Results (mg/I) _LP&T:GC/MS Arsenic benz.c:ne ----Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzenc: ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride rn-cresol ------ --Iron __ p-cresol --Lead cresol ------ --__ Manganese: 1,4-dichlorobenzeoe ----__ Mercury 1,2-d i ch 1 oroethane -- --Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dini t rotolucnc ----Silver __ heptachlor --Radiochemistry Sulfates hex.:ichlorobenz.ene ----Zinc hexachlorobutadiene ----Paramett:r Results (PCi/1) _pH hex.:ichloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenz.cne ------TOC __ pentachlorophcnol -- ----pyridine l\1 icro biology ----tetra chlorocth ylenc: --__ trichloroethylcne Parameter Results (Col /l00ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-trichlorophcnol ------vinyl chloride cndrin --lindanc 7-;1..f-z.f.£1{t..~cported by Dc1tc Received --__ methoxychlor Date Extracted __ toxa phenc Date Reported 2,~-0 --__ 2,t:;,5-TP (Sil·,ex) Dale AnalyLcd y-;:)_-'3._!f 7ULr 942817 Lab Number DI IS 3191 (ltcviscd 2/91) -- I I I i I J lc:allh, l,:. Satunl R=un:c:s Solid Waste :,-{anai;c:mcn, Division Si1e Number ----------------- P.O. !3ox 2.SOn, 306 S . Wilmini;,on S1r:c1 R.alcii;h, North Carolin• :,G l l Field Sample Number W L -e>O 5 -Gt uJ Name of Site WA-1<.2..e.J GorJN PG"B l.DFL Site Location A F"10 ~ NC.. -~-....:.....:::....:.;~ _ _;_:.......:=:;__ __________ _ Collected By ~ . t0 , c. H.o l. 6c>,._, Dale Collected Zea :JVL Y q4 Time / 40 o ~ t.A--'A J..k e:e.. Agency: Hazardous Waste X Soud Waste ___ Su perfu.nd TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic -- . .:I¾ 4 Barium ---· L Ground water (1) _ Solid (5) WE.LL Cadmium --Chromium --Surface water (2) _ Liquid (6) Lead ---- --Mercury _ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) 0rtanic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ---- xdl~k. Cadmium chlordane ----r<o. 01?0/ Chloride chlorobenzenc ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride rn-cresol ------ --Iron __ p-eresol --Lead cresol ------ --__ Manganese --1,4-dichlorobcnzece ----Mercu:y· --1,2-d ich loroc1hanc --Nitrate 1, 1-dichlorocthylcnc ----Selenium 2,4-diniirotolucnc ----Silver hcptachlor ----Radiochemistry Sulfates hex..achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex..achloroet hane ----__ Gross Alrha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzcnc ------TOC __ penlachlorophcnol -- --__ pyridine Microbiology ----t ctr a ch I orocth yl enc ----trichlorocthylenc Parameter Results (Col/lOOml) 2,4,5-1 richlorophcnol ------__ 2,4,6-trichlorophenol --vinyl chloride ----cndrin -- 7-2_9-f¢yt',d'b_epor1cd by lind:rnc Dale R::ccivcd --methoxychlor -- 'ff?-;l.-9f/1/I'~ Dale Reported --toxaphcne 0;.itc Extracted 2.~-D -- D.ilc Analyzed ~.R-99'VP · 94ZS1.8 __ :?.,-i,5-TP (Silvcx) Lab Number 1)1 IS Jl'JI (Rc:visc:c 2/Yl) --I I I I I ! I ! I i I lcalth, & 1'atunl Ruourccs Solid w~stc :Slanagcmcn: Division . r.o. 11vx 2W7, 306 S. Wilmin~on Strt:.Cl RAieigh, North urolina :7Gl 1 Site Number Field Sample Number W L -f:>O 5 -G, uJ ----------------- Name of Site WA-1<.i2.e.J CorvT1 PG"'B l.DFL Site Location A F"To ,-J NC., ._..!..,.;._....:.._:~::::__....:....;:......:::::...._ __________ _ Collected By ~. f\) u:.H.o l-6C>..._, ID# 3-=t-Date Collected Z <i3 -:T'l) L '/ q4 Time /40 o /. U/AL.kt:~ Agency: Haurdous \Vaste X Sol.id Waste _·_superfund TCLP Compounds ------ Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium .:!¼ 4 ---· ~ Ground water (1) _ Solid (5) WE.LL Cadmium --Chromium --Surface water (2) _ Liquid (6) Lead ---- --Mercury Soil (3) _ Sludge (T) Selenium ----Silver --_ Other (4) _ Other (8) -- -- -- Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kt) Organic Compounds Resu I ts (mi;:/1) P&T:GC/MS Arsen.ic benzene ------_x_ Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE Cadmium chlordane ------Chloride chlorobenzenc ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride rn -cresol ------ --Iron p-cresol ----Lead ere.sol ------ --__ Manganese --1, 4-dichlorobcnz.cnc --__ Mercury --1,2-d i ch loroethane --Nitrate 1, 1-ciichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobcnzcne ----Zinc hcxachlorobutadicne ----Parameter Results (PCi/1) --pH hex.achloroethane --__ Gro~s Alpha __ Conductivity --methyl ethyl ketone Gross Beta TDS nitrobenzene ------TOC penlachlorophenol ---- ----pyridine Micro biology ----tetra chloroet h ylcn c --__ trichloroethylcnc Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----2, 4,6-trichlorophcnol ---- ----\inyl chloride --endrin -- 7-:Zf'-f~(#' ~eportcd by lind:rne Dote Received --methoxychlor ,/ -- D:.ite Extracted ~-1-'f~ k8, Wi.:f' --toxaphene Date Reported 2,4-D 7 -- Dale An.dyzcd '7,). ,CJ<f8[)_ 942819 __ 2,t..5-TP (Silvex) Lab Number 1)1 IS Jl'Jl (llcviscd 2/91 ) -- 1 lcalth, I,:. :-:aiunl Re.sources Solid Was1c :-.lan•i;cmcn: Division r .o. Dox 26047, 306 N. Wilmington Slr<:CI RAlcii;h, North C.rolina :7Gl 1 Si1c Number Field Sample Number W L -E>O 5 -G, W ----------------- Name of Sile WA-1<.2..e..J C1orJTY PG"E:> l.DFL Site Locatioo A F"To iv N (_ _.:....;. _ _;_;::....;_;::.__...:...;c....:::;._ __________ _ Collected By 6 . fv 1c.Hol,6e>-....> Time / 40 o r: ~"''-kt?R.. Agency: Hazardous Waste X Soud Waste _· _Super fund TCLP Compounds ------ Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic -- . .±t 4 Barium ---· L Ground water (1) _ Soud (5) WE.LL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul ls (mg/I) (mg/kt) Organic Compounds Rcsults(mg/1) L P&T:GC/MS Aiseruc benz.ene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-crcsol ------ --Iroo __ p-eresol --Lead cresol ------ --__ Mangaoese 1, 4-dichlorobenz.eoe -- --__ Mercury 1,2-dichloroethane --Nitrate = 1,1-dichlorocthylene --Selenium 2,4-dinitrotoluenc ----Silver heptachlor ----Radiochemistry Sulfates hex.ichlorobenz.ene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hex.ichloroethane --__ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS ni1robenz.ene ------TOC __ pentachlorophcnol -- --__ pyridine Microbiology ----tetra chloroet h ylene trichloroethylene ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol -- ----__ 2,4,6-1richlorophenol --vinyl chloride ----cndrin --lindane Date Received 7--29-f'/1//IJJ'Reponed by --__ mcthoxychlor 7 --toxaphenc Date Extractd Date Reported 2,~-0 -- Dale Analyzed 9'-:2..-9'-/-7](J}"'-Lab Number · 942820 __ 2,4,5-TP (Si!vex) --1)1 IS Jl'JI (ltcviscd 2/Yl) I 1 t ;s:.C. Dcpar.ment o( Environment, l lc:alth, /,.: 1'alur.il Ruourccs Solid Waste Manai;emcnt Division SA.M:PLE ANALYSl.S K.EQ U.t...Yl. Smc uboratory o( Public Health Site Number ---------------- . P.O. Oox 26().17, 306 K Wilmin~on Strcci Raleigh, North C.rolina :?761 I Field Sample Number W L-6> t;> '--3 uJ Name of Site WA-R.i2.e.J Cborv"N PG'B U:,FL Site Location A F",o ,-J NC, -'-------'-----=------------ Collected By a. fv l('..H.Ol,6C))...) Date Collected .2 9 :J'c, L 'I 9 4 Time IG 30 br ."::>TEPH~~ Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· L Ground water (1) _ Solid (5) c°Al<L L1M~e WtLL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury _Soil (3) _ Sludge (7) ::SPLI, w/ E"GO --Selenium --Silver --_ Other (4) _ Other (8) re -003, -c;Ju.J -- -- --Organic Chemistry Inorganic Chemistry -- ' Parameter Result.s(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B /N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane -----:'t?, O CN7/ _x_ ?C.'e, Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol --------Iron __ p-cresol --Lead cresol ------ --__ Manganese 1,4-dichlorobenzene ----__ Mercury --1,2-dichlorocthanc --Nitrate 1, 1-dichloroethylenc --\ --Selenium 2,4-dinitrotolucnc ----Silver __ heplachlor --Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadiene ----Parametu Results (PCi/1) pH hcxachloroethane ----__ Gro~s Alpha __ Conductivity __ methyl ethyl ketone Gross Bela TDS nitrobenz.e:ie ------TOC __ pentachlorophcnol -- --__ pyridine Microbiology ----tetrachloroethylene --__ trichloroethylcnc Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----vinyl chloride ----endrin -- Date Rm;ved 7-.:Z f-~@epo,ted ~ / /4,r:;.P ~ lindanc __ mcthoxychlor __ toxaphene D.itc Extractc<l.¥'-oi7-9'/-J/f'B.QDatc Rep r=~ 2-'Z--9 Y --2.~-D .., ?"-.:?-~'°: 942821. __ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number DI IS Jl'JJ (Revised 2/Yl) -- •"·"--,._,. .. ,·-·····-··· ..... -·····-·····-···· 1 lcallh, l:. :--.:aiur.l Resources Solid w.~tc M•n•&cmcnt Di,ision Site Number l'.0 . fk>x ~i. J06 S. Wilmini;ton Str-ccl RA:cir;h, North urolin• 1761 l -----------------Field Sample Nurnbcr __ W __ J..._-__ o_c> __ I_-_L_.I=::'_-_____ _ Name of Site WA-R..:2.E..J CorJT't PGt;, l.DFL Site Location A F"To t--.l NC ·_..t....:,_;_....:....:::...:.:~-....:.....::.....::::::;_ __________ _ ID# 3-=f-Dale Collected ,,2 "zS -:J' VL 7 Gf'Lf Time /120 L.., i20S'E Agency: Hazardous Waste X Soud Waste ___ Superfund TCLP Compounds ----- Sample Type Inorganic Compounds Results(mg/1) Environ men ta I Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Soud (5) HL.T~-,e 6 YS Te.,+'\. Cadmium ----Chromium --Surface water (2) Liquid (6) /A..JLe T -LEACHA-7e;---Lead ----Mercury _ Soil (3) _ Sludge (7) SPt.../ Z: k..,)/ FC.o Selenium . --Silver --_ Other (4) _.?5_ Other (8) -;J:C-00I-Le:..H . ' -- --., -- Organic Chemistry Inorganic Chemistry -- Results(mg/1) I Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds K P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobenz.ene ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iroo __ p-crcsol --L::.ad cresol ------ --__ Manganese 1,4-dichlorobenzene I -- --__ Mercury --1,2-dich loroet hane --Nitrate 1, 1-dichloroel hylenc ----Selenium . 2,4-d init rot oluene ----Silver heptachlor ----Radiochemistry Su if ates hexa ch lo robe :1zene ----Zinc hcxachlorobutadicne ----Paramett:r Results (PCi/1) _pH hcxachloroethane --__ Gross Alrha __ Conductivity --methyl ethyl ketone Gross Beta TDS ni1robenz.cnc ------TOC pcnlachlorophenol ---- ----pyridine Microbiolo£Y !ctr achloroeth ylenc . 1::-.. ---- --__ trichloroethylcoc Paramclt:r R~sults (Col/l00ml) __ 2.,'1,5-trichlorophenol ----__ 2,4,6-trichJorophenol ----vinyl chloride ----endrin -- 7-~9-9¢V.P6ZJReportcd by lind:rne Date Received --mcthoxychlor ✓ -- D:.itc Extracted --loxarhenc Date Rcportcd 2,4.Q -- 0..tle Analy,.cd 'J--;;J..-9'-J--nur . 942822 __ 2.,t.,5-TP (Silvcx) Lab Numbc:r l)IIS J!'JI (Hcvi.c.:l 2/\11) --i ' I i I : I : ' I I lc:alth, le 1'"a1unl R=urccs Solie! Wasic l\i>n•ccmcni Di,ision Sile Number --------·---------Field Sample Number r .v . ,.,..,., .... ~,. JVQ ,,. n11m1n&1on .::>1rcc1 ~lci&h, North Carolina 27GJ l WJ..-001-L.£' ------------------ Name of Site WA-'<;2..e..J CorJT'i Pe,r::, l.DFL Site Locatioo A i=-·,--o >v NC. ._!,_;_.:...._:....:::....:..:::L. _ _;__:-=:.__--------- Collected By 6 . fv l('..H.o l-~...._, Dale Collected ;2. "iS -=I' VL 7 t::tLJ-Time /I 2o L.., '20SE. Agency: Hazardous Waste X Solid Waslc __ Supcrfund TCLP Compounds ------•' Sample Type Inorganic Compounds Resu l ls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Solid (5) Fit...T€,€. 6YS,e""'-Cadmium ----Chromium --Surface water (2) _ Liquid (6) /AJLe 7 -LEA-CHA7e:-Lead ---- --Mercury _ Soil (3) _ Sludge (7) :f,P(../ T k-J_/£C.O Selenium --Silver --__K_ Other (8) -;re.-OC>I-L~H Other (4) ,, ---- --.. --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Resul ls (mg/I) (mg/~) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arseo.ic bcnz.cne. ----...$.._ Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE Cadmium chlordane. ------Chloride chlorobe.nzcne. ------Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iroo p-cresol ----Lead cresol ------ --__ Manganese --1, 4-d ichl orobenzen e --__ Mercury 1,2-d i ch I oroet hane -- --Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-di nil rotol uene ----Silver heplachlor ----Radiochemistry Sulfates hcxach lorobenze.ne ----Zinc hcxachlorobutadiene ----Paramelt.'.r Results (PCi/1) _pH hcxachloroethanc --__ Gro5s Alrha __ Conductivity --methyl ethyl ketone G ross Beta --TD S nitrobenz.cnc ----TOC pcntachlorophenol ---- --__ pyrid ine Microbiology ----tctr achloroethylene ----trichloroethyieoe Paramcler Results (Col/l00ml) __ 2,4 ,5-trichl orophcnol ----2, 4 ,6-trichJororhcnol ----------vin yl chlo ride cndrin -- Date R~ccived 7-:Z'?-f~pt'.ii}p_cportcd by lind :rnc --mcthoxychlor -- D:itc Extracted /!tlA g'-~1'f fl4 ~ale Rcport::d --loxarhene 2,.!-D -- Dute Analy,.cd f_ ... ;;. -qt/&£) 9,12823 __ 2,li,5-TP (S il vcx) L;1b Number l)J IS :l!'JI (llcviscd 2/91) -- ' I i i ! : i I lolth, ~ 1'>1ur.l Rc..s.ourcc:s Solid W,sic M•n•&cmcn: Oi,-ision Site Number ----------------- l'.0 . n.._..,, 2£0.:7, 306 S . Wilmin1:1on S1~,: R.Alci&h, North Carolina '.?7GJ i Field Sam pie Numbcr __ W __ J.._-_o_c:>_I_-_L_~_-_____ _ Name of Sile WA-R..:2..C:..J CorJN PCt::> l..DFL Site Location A F"10 >--J N (_ ·-..!....:.~--!...!::...:.:::::...... _ __:__::....;:::=...... __________ _ 'Collected By 6 . f\) rc.H.01,..~)...) Date Collected ..2"iS :J VL 7 Cf'L/ Time /120 /.., "20SE. Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ------ Sample Type Inorganic Compounds Rcsulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) Fit..,€,€. 6 Ysre.,+'\ Cadmium --Chromium --__ Surface water (2) _ Liquid (6) /IJLGT -LEA-CHA7e;-Le.ad --__ Mercury _ Soil (3) _ Sludge (1) :{>P<,.✓ T k,)/ FC.o Selenium . --Silver --_ Other (4) ~ Other (8) ;:re-. 001-L <:.H ,, "f i -- --.. --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Rcsul ts (mg/I) (rng/kf:) Organic Compounds Rcsults(mg/1) P&T:GC/MS Arsenic benzene ------Acid:B/N Ex1. Barium carbon tetrachloride --~-----Cadmium chlordane ----Chloride chlorobenzene _L J-><;.Bfoc::,."f" <1:7. OOD/ ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride rn-crcsol ------ --Iron p-crcsol ----Lead crcsol ------ --__ Manganese 1,4-dichlorobenzene -- --__ Mercury 1,2-dichioroethane -- --Nitrate __ 1.1-dichloroethylene --Selenium 2, 4-di nil ro1oluenc ----Silver heplachlor ----Radiochemistry Sulfates hcx;ichlorobenzene ----Zinc hexachlorobutadiene ----Parametr.:r Resu I ts (PCi/1) pH hcx;ichloroethanc ----__ Gross Alrha __ Conductivity --methyl ethyl ketone Gross Beta --TDS nitrobenzenc ----TOC pentachlorophenol ---- --__ pyridine Microbiology ----t ctr achlorocth ylene ----trichloroethyleoe Paramctr.:r Resulls (Col /l00ml) __ 2,4 ,5 -t richlorophcnol ----__ 2,4 ,6-trichlororhcnol --------vin yl chloride endrin --lind:rne Date Received Z-d9-.9~~eportcd by --met hoxych lor -- O;ile Extracted f:--Z .. 9L/Y1IJD:>atc Reported --1oxarhenc 2,~-D -- Dole Anc1ly1.cd j'-.;l-9'9"7/,P . 942824 __ 2,t.,5-TP (Silvex) Lab Number 1)I IS 31'JI (llcvi:.cd :?/YI) -- j I I I I: I' I I I I ; ! l lc~ll!'I, l.:. ,-,;,aur.,I RCl.Ourccs Soiic WHlc ~l•n•i;cmcnt Di,ision Sile Number ----------------- ~ Rilcigh, Nort~. Carolina 2761 I Field Sample Number t,,ul--c>o Z -LE Name of Site WA-1<;2..e..J GorJT'1 PGt:> l.DFL Site Location A F",o >-J NC _..:......:._....:.....:::.....:...;"------''--=::,_----------- Collected By ~ . I\) , c::. H.o l-6::))o....) Date Collected 2.'8 -:!UL Y 9-4 Time /+:so L. . Re:>$£ Agency: Hazardous Waste X Solid Waste Supcrfu.nd TCLP Compounds ------ Sample Type Inorganic Com pounds Rcsu Its (mg/I) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) FIC...1t'/:!_ ..5VSreft1 Cadm ium --Chromium --_ Surface water (2) Liquid (6) 0v-rLE:t-L~-tt~ Lead --Mercury --_ Soil (3) _ Sludge (7) Selenium --Silver --Other (4) ~ Other (8) --' -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1) ..L P&T:G C/MS Arsen.ic benzene ----Acid:B/N Ex1. Barium carbon lclrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobcn1.cne ------Chromium chloroform ------ --__ Copper o-crc:;ol -- Fluoride rn-cresol ------ --Iron p-cresol ----Lead cresol ------ --__ Manganese l,~-dichlorobcnzenc -- --__ Mercury 1,2-dich lorocl hanc -- --Nitrate __ 1,1-dichloroethylcnc --Selenium 2,4-di nil rotol ucne ----Silver heptachlor ----Radiochemistry Sulfates hcx.achlorobenzenc ----Z inc hexachlorobutadiene ----Paramdcr Results (PCi/1) _pH hcxachloroclhane --__ Gro~s Alpha __ Conductivity methyl ethyl ketone --Gross Bela TDS nitroben7.ene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --__ letrachloroelhylene --__ trichloroethylenc Parameter Ri:sults (Col /l00ml) __ 2,<l,5-tr ichlorophcnol ------__ 2,<l,6-trichJorophenol --vinyl chloride ----cndrin --lind:ine Date Received 7-c:z(9'-99'-)(t~eported by --__ meth oxych lor D:1tc Extraclec.J --toxaphenc Dale Reported 2,~-D -- Date A nc1ly1.c d '?(-3..q'-f-nu. ~ 942825 __ 2,4,5-TP (Silvcx) Lab Number DI IS 3:"Ji (llcvi~cd 1/'Jt) -- ! I ieallh, l.. 1'a1unl Resources Solie WHlc 1-,bn•tcmcnl Oi,~sion R.llc:igh, North C..rolina ~761; Site Number Field Sample Number t,,u '--t> O Z -i. E ---------------- Name of Site WA-R..:Z.e..J GotJT'I PG"'B l.DFL Site Location A F"10 ,-__J N (_, _.:....;.._....:....;::....:....::::....__~--=----------- Collected By G . N 1c.H.ol,6C>)...) Dale Collected 2.'8 -:!VL Y 9-4 Time /+:So L. R.eht Agency: Hazardous Waste X Solid Waste Supcrfund TCLP Compounds ---- Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _. Solid (5) Ft L. Tt/2... :5V5refl'? Cadmium --Chromium 0VTL£T -Lb4-C.rt ~ --__ Surface water (2) Liquid (6) Lead --__ Mercury _ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _)(_ Other (8) --I '. -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsea.ic benzene ------~ Acid:B/N E>..1. Barium carbon tetrachloride ----.MTBE · Cadmium chlordane ------Chloride chlorobenz.cnc ------Chromium chloroform --· ----__ Copper o-cresol ----Fluoride rn-crcsol ------Iron p-crcsol ------Lead crcsol ------__ Manganese 1, 4-d ich lorobcnz.ene ---- --__ Mercury --1,2-d ich l oroct h ane Nitrate 1,1-dichloroethylene ------Selenium 2,4-dinitrotoluene ----Silver hcptachlor ----Radiochemistry Sulfates hex.a ch lorobcnz.cne ----Zinc hexachlorobutadiene ----Pararnf!ler Resu I ls (PCi /1) _pH hcx.achloroel bane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobcn7.ene ------TOC pentachlorophenol ---- ----pyridine Microbiology --tctrachlor oc th yl enc --trichloroethylene ----Para meter Rtsults (Col/l00ml) __ 2,4,5-trichlorophenol -- ----__ 2, 4,6-trichJorophenol --vinyl chloride ----endrin --lind2ne ~ ~9-f¢yt'&JRcpor~cd by Date Received --met hoxych lor --__ toxaphene D:Jlc Extraclctl !JNA f-2-'i<f Ns"'~e Reported 2.~-D 7 -- O.itc Analy,.cd f ~j -11 ':/_.,Bi/)_·. 942826 __ 2,ti.5-TP (Silvex) Lab Number DI IS ::il'Ji (Revised 2/91) -- l ! i I i I I I I I I I I I I i: :I I I I ! i: 1: i' 1: : i I lcallr., ,.:. ,,~1u:-.1 1'c..s.ourc"1 Solie WH:c M•n•&cmcnt Di,isior. Site Number ---------------- -R.alcii;h, North Carolina :!7Gl ! Field Sample Number ~'--~ o Z -LE Name of Site W.crQ.>2.c.J GorJT'I PG"B l.DFL Site Location A F"To >-.J NC _.:,___.,;_::;;....:...:::;,__ _ _;_..= __________ _ Collected By (;;. (\) u:.Hc l. 6c>),....) Date Collected 2.'8 :Tvt... Y 9-4 Time /+3o L. R~5E Agency: Hazardous Waste X Sol.id Waste ____ Supcrfund TCLP Compounds ----- Sample Type Inorganic Compounds Resul ls (mg/I) Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _. Solid (5) Ft l-Tt"I:?_ ..:SY.Sreft? Cadmium --Chromium --0tTTLE:7 -L ~M ,ne __ Surface water (2) _ Liquid (6) Lead --Mercury --_ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) __l(_ Other (8) --I -- --Organic Chemistry Inorganic Chemistry -- Parameter Results(mg/1) Parameter Result.s (mg/I) (mg/~) Organic Compounds Rcsulls(mg/1) P&T:GC/MS Arsenic benzene ------ Acid:B/N Ext. Barium carbon tetrachloride ------~ Cadmium chlordane ----T <t?,006/ Chloride chlorobcnzcne ----Chromium chloroform ------ --__ Copper o-crcsol --Fluoride rn -crcsol ------ --Iroo p-crcsol ----Lead cresol ------__ Manganese 1,4-ciichlorobenzcne ---- --Mercury 1,2-ciich loroethane ---- --Nitrate __ 1,1-ciichloroethylcne --Selenium 2,4-din it rotolucnc ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadicnc ----Pararnelt:r Results (PCi/1) _pH hexachloroctbanc --__ Gross Alrha Conductivity methyl ethyl ketone ----Gross Beta TDS nitrobcn1.ene ------TOC __ pentachlorophenol -- ----pyridine Microbiology --__ tetrachlorocthylene --__ trichloroethylcoc Para meter Results (Col/l00ml) __ 2,4,5-trichlorophenol ----__ 2,4 ,6-trichJorophenol ----vinyl chloride ----endrin --lind:rne Date Received 7-e?'f-Gt}t'6.£JRcported by --__ mcthoxychlor ,P~~ __ toxaphenc O;.il:: Extraclcd Y-5~"/1/t@ Date Reported '2,4-0 -- D.ilc A n,dyzc.:d 5'-.3-9~1/P 942827 __ 2,ti ,S-TP (Sil vcx) Lab Number --1)1 IS 3l'Ji (llcviscd :!/91 ) I J I : I ! i ! ! I ' I : I I I ! I : I ! I I : i i I I i ' I ' I ! ; ! : I : I I lcann. ~ J.,..,lur•• r.~u,i..~~ Solid WHlc M•nii;cmcnl Di,;sion lulcig:h, Nor1h Carolina :!7(,J : Site Number ----------------Field Sample Numbcr ___ W __ L_-_::..,0_0--=2"-----f3=-_:L::..;__ ___ _ t✓ame of Site LUA-R.;:2..e,.J CborJTY PGt:> l.DFL Site Location A F,o ,.,J NC. "_.!....:.._...:.....:::.=::__ _ _;_:_-=;__. _________ _ Collected By ~. /'v I l. H.o 'v 6c>'-' Date Collected ze ;J'VL 'f '74 Time / r/ D 6t s.. . S.T€'i>He>--:> Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ---- Sample Type Inorganic Compounds Resu Its (mg/I) Environmentlll Concentrate Comments Arsenic --Barium ---· Ground waler (1) _ Solid (5) 0. F. WA-T€'"R., Cadmium ---Chromium --Surface water (2) _ Liquid (6) Le.ad ---- --Mercury Soil (3) _ Sludge (T) Selenium ' ----Silver ' --£ Other (4) _ Other (8) -- -- --Organic Chemistry Inorganic Chemistry -- : Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds Rcsults(mg/1) I P&T:GC/MS Arsen.ic benzene ----_x._ Acid:B/N Ext. Barium carbon tetrachloride ----~ Cadmium chlordane ----Chloride chlorobenzcne >< yc;ai/4,6,-< o -o o o I ----Chromium chloroform ------ --__ Copper o-cresol --Fluoride m-cresol ------ --Iron p-cresol ----Lead crcsol ------ --__ Manganese --1, 4-d ich lorobenz.co e --__ Mercury --1,2-dichloroethane --Nitrate 1, 1-dichloroct hylcne ----Selenium 2,4-dinitrol ol uene ----Silvu heptachlor ----Radiochemistry Sulfates hex.a ch lorobcnzene ----Zinc hcxachlorobutadiene ----Parameter Results (PCi/1) pH hcxachloroelhanc ------Gross Alrha __ Conductivity methyl ethyl ketone --Gros:; Beta TDS nitroben7.ene ------TOC penlachlorophenol ---- ----pyridine Microbiology let rachloroethylcne ----trichlorocl hylenc ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ----__ 2.,4,6-trichJorophcnol ----vinyl chloride ----cndrin --lind:!nc Date Received 1 :--~--yt/-1//J.il) --Reported by methoxychlor --Pif8 j-/, BNA .? to xaphcnc O;itc Extracted f-3.::ll..i-2./11/, M,IM,-0:itc Reported --2,~-0 --r1a1 · ,8JJ,f' . __ 2,t.,5-TP (Silvcx) .:r ~ 942828 Date Analyze 3-3-ff(YJP S'-j..q </ Lah Number 1)1 IS Jl'Jl (t-cvi:;cd 2/91) t)(;) -- I I ! ! I ' ' ' ; : i ii ' ! l ; ; ' ' ; i : I 1'.C. Dcp3r.menl or l::.:,v,ronment, I icallh, /;:. r--~1vr.l Resources Soli~ W;isic Management Division ..)LA\C: 1..,.aoon1ory Ul r "UJI\,. ru. ...... l · P.O. Oox ~,. 306 t-,;. Wilmintton Strec1 R.tlcitJI, North urolina 2761 l Sile Number ----------------Field Sam pie Numbcr _ ____;_tu...;c...__L.._-_C2'-'(2""-4L-----=&:;__L _____ _ Name of Site WA-'<a..e..J Gor.JT'i Pc:& u,FL Sile Location A F"To 1-J N (_ --'-'--_;_:::-.:...=;___,;__:_.= __________ _ ' Collected By a. f\) 1cH.01...,6c:>,_, ID# 3-=t-Dale Collected---=:.._:n __ .=..;fi_tl...:L:::.,'Y_...:q'-4-'--_ Time /~~5 ~-ST-EPt-l~.!;. Agency: Hazardous Waste X Sol.id Waste _· __ Superfund . Sample Type Environmental Concentrate Comments Ground water (1) Sol.id (5) Surface water (2) Liquid (6) A IR. /10$ ~ _ Soil (3) .):{_ Other (4) _ Sludge (T) __________ _ _ Other (8) __________ _ Organic Chemistry Parameter P&T:GC/MS X Acid:B/N Ext. ~l-o· Results(mg/1) 0, 0 Oi.J:2.ff1 Radiochemistry Inorganic Chemistry Parameter Results (mg/!) (mg/kg) Arsenic Barium Cadmium Chloride Chromium __ Copper Fluoride Iron Lead __ Manganese __ Mercury Nitrate Selenium Silver Sulfates Parameter Zinc Results (PCi/1) _ pH __ Gross Alpha ______ _ __ Conductivity ______ _ Gross Bela TDS TOC Microbiology Parameter Results (Col/l00ml) TCLP Compounds Inorganic Compounds Arsenic Barium Cadmium Chromium Lead __ Mercury Selenium Silver Organic Compounds bc:nz.c:nc: carbon tetrachloride: Resulls(mg/1) Results(mg/1) chlordane: ------- ch lorobc:nz.c:ne chloroform o-crcsol m-cresol __ p-crc:sol crc:sol 1,4-dichlorobcnzc:nc: 1,2-d i ch lorocthane ------- __ 1,1-dichloroc:thylcnc ______ _ 2,4-dinitrotolucne heplachlor hcxachlorobenz.ene hc:xach lorobutadic:nc hcxachloroclhanc methyl ethyl ketone nitrobc:nz.cne pentachlorophcnol pyridine l cl ra chlorocth yl cne lrichlorocthylcne __ 2,4,5-trichlorophcnol __ 2,4,6-trichJorophcnol vinyl chloride endrin lindanc methoxychlor __ toxaphcnc 2,4-D __ 2,4 ,5-TP (Silvcx) ------- -:---:--::=:::.-::..:·· ·...:·..;;.;·· -~--=· -----.. -______ ====== -..... ·----·------"'.':""::"~~------------------·--.. ·--... ·•• (!) s:cA.'.IE LABORA:I'ORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST_ RALEIGH. NC 27611 ORGAN.l'C CHEMICAL ANALYSIS .PORGEA.BLE COMPODNDS LAB NO Cl'-lJ.'l'fl q41 a754-q'--1-;;.?57 lq'-+;27<?~ q'-f~?q5 lq4-J7C17 I P'IELD NO u..;L-ocJ -5511-t..1L-00S-~ 1.ei. •co,-5~ l))J..-oD;i.-sol o.;L-CCJ-U!-wL-DD.2-LC... COMPOOlYD -. TYPE I ( .3 ) I ( 3 ) I ( 3) I ( '-f-) ( 5) I ( 5 ) UNI'l'S w~I w~ w~I µg/1~ ·w1~ µg/l~, ::3:-0ROKZ:TBAlOC IJoop.b I LL i.)._ I I J.. -I LL LL.. ll?ITL CILORIDZ: JO I I IRQl(OKJ:rBAKE :J..() I I cn.0R0!:TlL\ffll: 1n I ,. JO .. I nuc:m.oROn.I101l0KEt'BAll!: J.C:TOIIZ 50 I I 1· l.l•DlCHLOJl0z:na::11E 15 lODOaa:rBAZQ!! I 10 I I ... / ,1 ,v ~ cn.oa.mz: I ,s I 8::516 '? .), B g:r;6 I CAllBOlf D~CU'lDZ: I \ I I u_ I l LL I ntAlr.5-z..:t.t>lc:m.aROJ:TB:?::fl: I '1,; I ACX:rLCll'lT2IU: I ;z::o I l.!-DICl:LOJlOz:n!Aln: 15 I '\ 1/ I \I I :::-BCTMO!fE I~ I +-rarP I +rnrP J C:S-i.;..DICHLORCl:TH:C'r?: 15 ~ I "v ,/ LA I CBLOJlOJl'QRM I I I +,af'io J -h-nro +rar11 l.l.l•TIUCILOROr:TBAZrl: I J-I I l,L u. LL I CAllBO!f T?::'KACm.ORIDZ: 10 I ,v B!:.'l%Z:2'IJ: ,, I +cnrP - i..::-t1rc:m.oao~ TRlCHLOROEl'llEl(J: U•Dlcm.oROPROP.Alf!: I -v I BROMODICM.ORO~ I 10 I ¥ ciher Co1t1Dout~ (£)/c-J N I f MDLf e-D!la.t:r~~o PRE.:scl'lli" 1N L.A0 ~>-1)::5. J -J:stimaced .....iu■ I I \v F) 1--Actual Talu■ i• lccu:,wu to b■ l••• thaA Talu• gi"YeA. L • ..lctu&l. 't'al.u■ i• lccu:,wu to b■ gr.acar thaA Talu■ gi-niD. . I I \/ I ·J I G I (=) I I t7 -X&Cari&l --aualy,r;ed tor !:Ne DOC d■c-~ed-'rh• i:nmbar is ::!l■ Kin.umm. Detec::!ca. Ladt. D. -11101: aualy,r;■d. l/ -Taa.t:at::i,.,.. idaa.~acica.. ]/ -Ou mux: r.J.ac o~ Prioc.t:y i'ollucaa.cs. H -CO,_PoUND R!:UABL)I' bE'1cQ",q~ ONLV AT HIG-H C.ONCENTCRTiclli~ • C • f'o.:)S1BLE -LI:\& C:ONT"At.141~AT"Jc1J. )!:Bl'[R 3085-0 (10 /93) LL ,v {-f-) I u_ I I I I I I I I \v I B :I I ~ I +rf"lrP . I I LA--I I I ;;_ ..J LL- I I I \f I I fF) I PORGCOM-ORt I ----· -----··----..:a. .. ----·-····-----"-.;__----:--------------··-------.. ·--.;. su:rE LABORATORY OF POBLIC HEALTH PO BOX28047-306 N. WII..MINGTON ST~ RALEIGH. NC 27611 ORGANIC CHEMICAL ANAL'YSlS P'URGEA.BLE COMPOONDS LAB NO 9'-l~'74 i 9~75'-f qqd.757 q4~7 ii Q4J 7q!5 q',-~7q 7 -. FIELD NO WL-oo 1-SS WL-C05-5S I LuL.-CC{D-j5 COMPOmYD TYPE I ( 3 ) I ( 3 ) I ( 3 ) UNITS w~ I µg/1~! w"i~ DIJ!RO:WOlll:TRAJ(?: I . ; f'lr"\b LL ~:Z.n:zru!COIQ: .s/' . n OS-u-titc:m.ollOP1LO~ .5 TOUICm TJLVl'S-t..:S-tltc:m.ollOP1t0PSZ'I% \V l.l • .:..:i-'T'Z:'nlACm.ORO~ I JO l.l~TIUc:m.oROr::I1L\lf?: 15 I :Z. H?::L\ff ON?: .!5n I n:ntAC:m.OROr:na:?B 15 I DIJSR.O:Woc:m..oROKJ:TIIAK?: 110 z:nrn.:aa: DCSROMIDZ: I __, cn.oROBz:::cz:arz: IJ-I l.l.l.:•T?:'TRA.CBLO'ROz:T'RA!f]'; I Jo I ?:Tl{TI.]5!:lfn:r?: Is I ::cr:u:. "f?:3 JO I ~ 15 I BROWOrOJUC I 10 I TRA.!nS-l.4--lllc:m.ollO-:Z.B'1t%l'rz: ~o I l.:l.~TIUc:m.oROPRCPAKJ: ;JOO 1.4--Dlc:m.oROB~ )0 1.:1.•Dlc:m.oROB~ J/ 1.:1.•DtB'ROlil~ROPROPAN?: .JnO I VINTLACz:TAT?: IJr \✓ I 1-MDLf 5 -~Ck.6-~ C> PJi:E.Sa-IT I >-1 LA 6 81..A N li:'S. J -Xat:ilu.tad Ta.lua U- I I I I I I I I I I I I I I I v I lC -A.ctual T&l.ua i• lc=wn to be l••• th.Im .....iua gi..-.n. L -.>.ctual "'t'al.ue i• lc=wn to b• i:n:-eater th&l:I. "'l"al.ua gi-re.c.. I ~ I I I I I I I I ·,/ (.>)i.--CD;l. -SD ol:J-• CCI -l-c.. I w L -CXJ;l-L{:_ I ( 'i ) I ( 5 ) ( 5 ) µg/1~ µg/1~, µg/1~ I (.A.-I (A_ I 1 I . I· I I I I --I I I ! i I I I I I I I I \v I \/ I ~;;)_ I l.oO I I J. I ( J. I I ¥ I +race - I +rocP-I +rare - I I { 1 I LL- I I I ,/ ,v I ~3 Lf-~ I 4:r +r-a.Le,... I l-L I LL ,/ ~ I I/ I I .. I I I tr -X&terial waa a.=a..ly:ad tor but =ot detac:1:ed. Th• number i• the •1n:lmm I>etac:ion Liait. m. -Jl1ot azi&l.y:ed. 1:,1 -'%'•Dt&ti-1dene1tication. J:.I -OD mux: U.t ot P:iorlt:y Pollutanta. H -CoMR>llNb Reu~a.y DETEcTRBlE C>NLY RT >-416-1-( CDNCfNT"J!AT)Ot\r.:). C -?~~18'.E u:10 COr-tTA,..lKAi'"loN DEB?m. 3068-0 (10/93) . ------·---··" - PURGCOH..ORC I I ·---·-··----.. ---------=-a-----~ . . .......... __________ ·:~---···· ·• . ·•. ·-----------~~~--------........ ...._ ------------.. ---.. ·•• S'I:A.TE LABORA:I'ORY OF PUBLIC BEAL 'm PO BOX 28047 -306 N. WILMINGTON ST-RALEIGH. NC 27611 ORGANIC CHEMTC'.AL ANAL:YSlS q'-f d'?O~ 9~u3 qL./-~?o4 q-1 ().jD5 I PURGEABLE COMPOUNDS LAB NO q 4;;;_9:z> t" 9<./J.S/f. I l'IEI.DNO U)L-COI -6t-LuL ·Oc~-sLI o;L-ocs-6L WL -00"{-BL 11...,L -c,o I -C--u.~ wL-co~-&W COMPOUND --TYPE I ( 4 ) I ( -t ) I ( 4) ( -+ ) ( I J I ( ; ) I UNITS ,~~kg 6v]µg/xg I ~1wq {Pgi~µgjkg ~wq l~wki CBLOROw:rmAffZ )oop.b I il Vllfn. CBLORmE IO I BROMOaa:rHAJU.: :J.() I cm.oROr::mAIIZ 1n " nac:m.oR0n.t10JtOJa:nU.ff!: 10 ~IQ: I .5o I l.1-Dlc:m.oROETBz:mC .5 I IODOaa:nL\l'r!: I 10 I '\ V j :ia:raTI.Z:I'!: CBLOaIDE I -~ 3J;B I C..UU,01{ Dl3lJLnDE \ I A. ~~Ic:m.oROr:na:::fE ,~ I ACX:rt.OznTIUI.Z: ;;co I l.l•Olc:a::rAROz:nL\ll'I!: I .5 I :-a C'T.Jllf Olf?: I ...:;a I c::,..i;.orcu.oROr::na::n: 15 I "'v CBLORCP"ORK I I +ro.{'_e l.1.1• TJUc:m.oROr:TBAZYE \/ I l,L c.utBOIJ n:tXACm..ORIDE JO I .BC'l%2:2'?: ;:, l.;i.OICBLOROETIL\lfE TlUCBLOROE:TllElflC I I l.3•01CILOROPROPAN!: I -v I BROWODICRLOROICE"I'XAN!: I JO ,I/ fJ : !-~v-/"';'"I rYl ,)'; / l n,-k I G::l (-j (-) I f MDLf e, -caeJ:G-~,-)0 P~l:NT IN L.A6 Buu,n:~. J -Zstilllatad Tal.ue ( 1 I I ,1 I ~:r,B I.A. I I I \ I +ro.c.e_ I u._ I ,V (-j ~ -ktua.l Tal.U• i• lcaawu to be l••• t!1aA 'YILl.u• gi...-.zi.. L -J.c:tua.l 'YILl.ue i• lcaawu to be gr9acer than 'YILl.ua gi,,.... l i 1 I LL I I I I . I I I ,V I ,/ I I 15"J";°B I +r-oce-:r. BI I l_;__ I u_ I I I I I I I I I ·:/ I I 33" I I ,V I LL I I ca ::r I 14 I I LA_ I LL I I I ~ +r-aC'e. L(_ . ,.I/ ..I/ I A (:") I 11 -Xacez:-'..al •-&Dal.y:■d for buc aoc decec:ced. Th• amaber i.s th• Mini-I>etec::!au Lilaie. D. -lloc &D&l.yzed. l/ -Tent&d....-idazitificadou. 2/ -On lilt.DC r.iae ot Pr.1.orlty Pol1utam:a. H _ COIWPoul"fD R!:UABLY bETECl"'ABU! CNLV AT HIG-H CDNc:£NT~T1e.N~ • C. • ?O.::-S1B&..E -LR& CON"l'"'P.Mt~A'r°lclJ. DEBlllt 3065-0 (10/93) ( J. I I I I -I .i -I I I I I I I I I I \ I E) I 1 I I I I I I I I I I I I I I I I .,v I <3 I i PORGCOK.OR:I ·····-····------------------------•·-----·•·.· .. rn:rE LABORATORY' OF POBLIC 'HEALTH PO BOX 28047 -306 N. WILMINGTON ST-. RALEIGH.. NC 27611 ORGANIC CHEMJf"'.AL ANAL'YSIS PORGEA.BLE CO.MPOl7.NDS LAB NO ql-j .;iioa q4;:&D3 q4~-go'-f 9"-l~eo5 9'-f J.00{() I q4-d <o'l f .. FlEIJ) NO lwL-001-BL I WL-oca-BL CO.MPOOM> TYPE I (4 ) ( 4-) UNITS ~n)izg/kg I ~~kg DIBROKO~ _ r; n, .. J-, LL ~L -C.-lfXTX?l..:Z.P'Effl'.A!fOlf!: si'' , ...:n CIS-1.3-DlCBLOROPJlOPEKZ .5 TO~ nAlfa.l.!1-DlCBLOJlOPROPEm: '\V l.l~•T?:TJtACm.OR0rnrAK?: JO I I 1.1;.nuc:xr..oROE:TBAm: 5 I I 2-u::c:z:Al'I Ora: 5n I I T?:TRACm.OROz:ntz:ffZ 15 I I DCIROKocm.oROKrnLUfl: I JO I ~ DDIROKD>r; I ._,-I I CHL0R0Bz::a::z:::rr?: I J-I I l.l.l.:-Tl:T'RI\.Cm..OROrntA:f?: I Jo I I ?:T1!TL B:r:m:%l'll: Is I I :rn.z:~ I JO I I ~ 15 I I BROKOFORJii I 10 I I ntAlf&-l.4-ll1cm.0RO-:Z.BCT%ffJ: io I l.:t~TJUCBLOROPROPAKE ;;Jf)Q I 1 1.-c.-oroa..oaoa~ Jo I I l..:t•DICBLOROBU(ZZl'{!; J/ I I I l.:t-DrBROM0-3-CBLOROPROPAM?: I ::>no I I I VINTI. .AC:T.A.n: Jr I "I ,v I I I I l+MDLf I 13 -o.:IC);fr~C Pli:'E-SENT t>-l L.A8 B~ N'K~. J -X•t:!lia&t•d iralu• ~ -1.c:tual ..-.lu• i• bowu to be l••• t.h&D T&l.u• giTaA. L -ktu&l. iralu• i• bowu to b■ greater tbaA T&l.u• giTaA. Wi...-C03-BL wL-Wf-BL ~l---rol-&~)j i.J'-·Q'.>o1 -6l<l ( J/. ) I ( t/ ) ( / ) r r ) ~pg/kg 1~l µg/kg ~/kg,~kg I .l,(... I (.)._. L,L, I u I ·• ,j L_ -l r, 11 r I u.-. . I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I '\ I/ +-n1N:1 I Ll.- I \ I I ,;/ ' I I \ V I I I I I I I I I t1 -htari&l. ..,.. az1.al:y:■d for but D.Ot d•t•ct■d.. Th• number ia tha •1n:1wm I>et•~.ion Lia:Lt. la -JJot an&l.y:ad.. 1/ -~•nt&ti?a i~ica.tion. "'i:/ -0Zl mux:: Li.•t o! P:c:1.o:d.ty Pollutants. I I I I 'ii -CoM~llN b Reu~ i,_y l>ETECTRSLE oNLY RT Hl6-M CoNCfNTJ!.RTiot.,S. C. -?~SIBLE. u:10 CONT&U,HMAT\oN DEBNR 3068-0 (10/93) . I PtJR.GCOM.ORC I I .... ::-: ... -:.---:-. -:-:. ::=.;=:·:::.:·· ·_;·..:.;,;·. ·::..:· -= -. -. -.. --------=----------····· ·__::......;:..:._-~-- ST.ATE IABORA:I'ORY OF PUBLIC HEALTH PO BOX 28047 -306 N. WILMINGTON ST-RALEIGH. NC 2761.1 ORGANIC CHEMICAL ANALYSIS .PURGEA.BLE C!JMPOUNDS L\BNO (jLJcig'Jt.f q LQ.g 11 I q '-J;).C?~.v q '+~...,-, q4,:,~.:;c; FIELD NO WL-003-<i-W wi...-DDLf-&~I WL-005-&lvt bJL-Ool -LE. WL-00~-lE, I COMPOmYD --TYPE I ( i ) I ( ( ) I ( ) ) ( 8' ) I ( ~) I I UNITS I ~l)g/kg (µg;yµg1kg ~kg ~µg/kg ~kg I CIUJR0aa:ra,u(1; Joop.b I l..1-lJ.-I U-I u__ I U- I l I I vtNTL CXLORIDZ: JO I I BR0M0Ja:TBA1ff; ::1() CXLOR0E'IEAK1C 1n ,. nacm.oaoruroJtOia:nLUn: 10 I I I.So . ..t.erreffZ l.l•Dlc:m..oROrrxarz 15 I I I IODOM%TilAlf?: I !O I I I I I :ia:rxn.z::n: C!LOIIUDZ: I ~ I I I I I CAJUSOlf D~tJU'IDZ: \ I I I I I TltJ\1'S-L:-tllcm.oRO= I J; I I I I I - AOl::rI.OlfTI'lUU: lo:co I I I I I l.l•t1lc:m..oR0!:TIIAlf!: 15 I I I I I y/" I ::.a llT.All'Olf!: ,~ I I I I +r--(}f't° I C:S-l.Z.OICHLOR0!:T'B!::n: 15 I I I I i1 I CIUIROP'ORM I l I I I I I l.l.l•TRlcm.oROET'HAll'z: ~ I I I I I CARlS()lf n:TltN:m.ORmZ: I 10 I I -1 I ,.r llcrz:cn: ti a::r 1.:-01cm.oaoP:I"11Am: u_ . TIUcm.oROz:ntEZ'E I I I I l l.z.tllcm.oROPROP J\ffl!: I -v I / I I / BROMOtllcm.oROaa:TllAlf!: /0 \V I / I ,V ' -w ·, of h,er Co M1)our-dS {£)Jr-) F .) F) I c-=-) r-;·~ +, (-) I 1MDLf e, -~a.G-Aou...io PRl::51:NT IN LA8 8'-A>.i):;'5. J • Zathat■d "l"UU■ I ~ -Actual Tal.ue i• laJawu to b• l••• than Talu• g:!.,ren. I. -Actual Tll.l.ue i• k:Dawn to b• g:r:■•t■r th&n T&l.u• gi,ren. I 11 -ll&ter..&l. •-&D&lyzad !or but 110c d■c ■ccad. Th• ZlUZllbe.r ia :!1■ •~ Dec■ce.:!.on r..1.m.:ic. lQ. -llot an.lyzed. J:.I -T■ncaei,... idan~:icaeion. 2/ -011 lllJUX: I.iac ot! ~o:c:!.ty Pollutanc•-H -COtcPaUND RcUABLY Z>En:CrA~ ONLV A"i HIG-H CDNc£NTt:,,rncN~. C. -po=,s,Bl.E . LA& CONT"P.~ l~A"t"lc"1. DEB?rR 3065-0 (10/93) I I I I I I I I I I I I I I I I ( l I µg/lJIVkg I I I I I I I I I I I I I I I I I I I I I I I i P"[JRGCOK.Oi _-·_-··. :::~--::::_ ......... _ -=~-=--=-------·-"----. -.. -.... -... -. .-. -------;....,;__-__ -=..-=------~------·---'------.. · · .. STATE IABORATORY OF POBUC BEAi.TR PO BOX 28047 -306 N. WILMINGTON ST .. RALEIGH. NC 27611 ORGANIC CHEMICAL ANAL'YSIS PURGEA.BIE COMPOUNDS LAB NO C/4;l?J4 q'-J;,g-(7 q'-1,;lf;;;il) q4J'6# lq4Q8;;6 I --FIELD NO WL·co3-G-w tvl. -{J0'/-6W IOL -oc6-<..rv.J u..'l. --00 J-Le. bJL-Ql!;!-LE I COMPOUND TYP'E I C I ) C I ) ( f ) I ( ~) ( 1 ) UNITS l~yg/kg (µg,tyn/ki n1i)µg,tkg ~/kg :~ DmROMOICCTllAN?: I . i; lir"\h u- I I 4-la:TXTI,-;i.n:lfT.A.!fO!a: . .Sn CS-1..3-DICBLOROPRC~ ..5 TOUJDm ntAffll-1..3-Dtcm.oaoPKOn:n: ,~ l.l~n:TIUCBLOROC'RAlC% I JO I l.l..:l-TJUcm.oRO!:T'BAlff: 15 I :;:... BJ!:X.\1' 0 ra: I 5n I Tr:ltACl!LORO~ 15 DmROMocm..oRO~ 110 rnau:;m: DlllllOMIIlf: .::5 QII.OROBca:?:lf?: IJ-I l.l.U•T?:TlUICm.OROrntAJ\'?: I Jo I ?:'THTL Bz:::rz:?::f?: Is I :rn.z:."f%3 I JO I :rrnu::cz: 15 I BROWOFOJUC 10 ntAffll-l.4-Dtcm.oRO-:i-Btr?%10: io I I..:~TJUCBL0ROPROPAJa: ;JDQ l .4-DICBL0ROB~ )0 I U•Dlcm.oROBZ::NZEN% J/ . I l.:2-DlllROM0-3-CBIDROPROPANz:: I :Joo I vnrn. AC:TA.TZ: I Ji. I "\/ I I I I ; MDL f 6 -~Q.:.lr~ C> P£ESEN7 I ).1 LA 6 B~ N l(S. J -Zatimated -ral.ue I Ll...- I I I I I I I I I I I I ' V I ~ -keual ,,.J.ue i• lr:::Dawn to be le•• than ,,.J.ue gi"l'WA. L -J..ctual -ral.ue i• COW1:1 to b• c,raater than ?e.J,ue gi"l'WA. I ·u~ I +rn£P.,, . u it' I :r I I ( 1 . . I I I I I I I I I I I I I I I . I -v I I I +mr~~ I I I .J I I I +rcH'P I I I ;i-:s I ' I I LL I I I ,v -h-t1no I I U- I ' V I ,:/ I I I 'O' -Jlata:r:ial •-&D,a.l:y:ed for l::nlt :u.ot detected. fll• number ia t:ha X1 uiwm Patec::ion Lia.it. m. -Bot &D&l~ed.-1:./ -Tent&ti.,,.. 1dene4 ~ic:ation. 'J./ -On :mu:x: Li•t of P:::iorlt"J" :tol.lutanea. M -CDM'PllllN b REL.I~ BLY DETEC~SLE cNt.Y RT Hl(;,J,( CoNC.t:~no~, C -?c.,~18l.c. LA0 CONT'Al-ttNA"'i"\oN DEBNR 3068-0 (10/93) ' U- . ·V I I I I I I I I I I I I I I I I I I ( ) -pg/1 pg/kg I I PURGCOM.ORC- BASE/NEUTRAL ANO ACID EXTRACT ABLES COf'1PCXJND ~-nitrosodirrethvlamine )is(2-chloroethvl)ether 2-ch 1 orooheno 1 )henol l 3-dichlorobenzene l 4-dichlorobenzene 1.2-dichlorobenzene :ii s (2-ch loroi ~-----1 )ether hexachloroethane N-nitroso-di-n~roovlamine nitrobenzene isoohorone 2-nitroohenol 2. 4-dirrethvloheno 1 bis(2-chloroethoxv)rrethane 2.4-dichloroohenol 1.2.4-trichlorobenzene naohthalene hexachlorobutadiene 4-ch 1 oro-m-creso 1 hexachlorocvclOOf>ntadiene 2 4.6-trichloroohenol 2-chloronaohthalene acenaohthylene dirrethvl ohthalate 2.6-dinitrotoluene acenaohthene 2 4-dinitroohenol 2 4-dinitrotoluene 4-n i trooheno l fluorene 4-chloroohenylohenylether diethvl ohthalate 4 6-dinitro-o-cresol diphenvlamine azobenzene 4-braroohenvlohenvlether hexachlorobenzene ~ntachloroohenol ohenanthrene anthracene dibutvl phthalate fl uoranthene J -Estimated value. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUNAN RESOURCES P. 0. BOX 2804 7 -306 N. ,wr L11INGTON, ST. , RALEIGH, N. C. 2 76 11 ORGANIC CHE11ICAL ANALYSIS LAB NO '1¥-,< 71.f't' C!l/.J.. 7S.S Y,'7,l 7_..:;-y C/ 1./ ;?7,J(r / FIELD# tuL-001-.~<:, WL-oos-S<:, /Li... -o~--.S. ~ I..JIL-tJ02 -_s:;, TYPE ( 3) ( .3) (...3) ( 'I) UNITS ~ua/ka' ~/µ a I k a ' ~ua/ka ~ua/kq~ /rd :?3" IA-U.-l A: I.A..-- -- '-V S0/1&,So /t}/ 3_~0 i.so/11..,;o 10/~o -v 1501 ~{,,,;'[) /0/330 I 'V 50//tt,SO /tJ/33D / / / , " ,. .....,, \I \/ \V K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. ~</;). /Y,Y kJL-tJ02-Jt" C.,--) ~(µq/ka v<- / \I =?-?ol< 3~ol< LA- / ,1 U -11aterial was analyzed for but not detected. The nuroer NA -Not analyzed. is the Hi ninun Detect ion Limit. m ']) L ---1/ -Tentative identification. £1 -On NRDC List of Priority Pollutants. ~. C. V-<.v-<.o,i.on 06 He.a.Uh SVLv-<.c.e.6 OHS 3068-0 (4/86 L~boJta.to~y) - C!) '-11/2POX" hll-00/-6,. LU < I ) rua/1 \........, LA- , ,1 STATE LABORATORY OF PUBLIC HEAL TH DIVISION OF HEALTH SERVICcS, N.C. DEPARTMENT OF HUMN RESCXJRCES P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL ANO AClO LAB NO qq;i.7._;q q <./.:? 1.'<., qy,J..75,v q~.2'71<7 CJ'-/,:J7C/JI EXTRACTABLES FIELD# /.oL-OOJ-<.5 IIDL-ooS-< <; i.J.,l -oot,,--s ~ wL-Oo2 -<h WL -C)t>2. -Le. C0!'1POONO TYPE ( :? ) ( -? ) ( 3) (~ l CS) UNITS ~uq/lcci) ~~".:u/lco} ~uq/lco 1 ,~uo/ka) ' ~IQ /le 0 ovrene II0/.330 , , -1~ I,< -l-<.-U'- benzidine _,s-,1/1160 -- butvl benzvl phthalate J0/.3.:10 benz(a)anthracene chrysene J, 3 3-dichlorobenzidine .soltb.'i'/J bis(2-ethvlhexvl)ohthalate /()/330 di-n-octvl ohthalate ltJ/.s~o benzo(b)fluoranthene so/11no benzo(k)fluoranthene benzo(a)ovrene i ndeno ( 1 2 3-cd) pyrene dibenzo(a h)anthracene , , benzo(q h i)oervlene \/ ,/ '/ ' I \ V ,v aniline '.S' CJ /J J., ,rQ ,~ I-A-I.A.--LA.-\A- benzoic acid benzvl alcohol 4-ch loroani 1 i ne ' / dibenzofuran i/() /~I) 2-n-ethylnaphthalene 2-n-ethylohenol j ~thvlohenol "" 2-nitroani 1 ine S"ol!t.."i"o 3-ni troani 1 ine 4-ni troani 1 ine / / / 2 4.5-trichloroohenol ~I' ,v "'\ I/ ...._ I 'V \V --------~ f-'(_IP, (tot)FJhfllfT10AJ J +!-,-J ,-J (-J r-J r+J -'---"' --~ m1H .. J -Estimated value. H"OI Sal'- I( -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. u -~terial was analyzed for but not detected. The nurber is the Mini~ Detection Limit . m:z>t.. NA -Hot analyzed. ----1/ -Tent.itive identification. fl -On NROC List of Priority Pollutants. rv. C. V..i.v..i..6..i.on 05 He..a.Lth SVt.v-ic.u OHS 3068-0 (4/86 La.boltiLt.011.q I '-IL./;J.%0 )I /JJl --o o /-C')L;. C / l Juo/1~ LA- \ I/ t.--<-- . \ I/ " I -l { -) I I i j BASE/NEUTRAL AND ACID EXTRACT ABLES COMPOJND nitrosodimethvlamine is(2-chloroethvl)ether -ch 1 orooheno 1 henol 3-dichlorobenzene 4-dichlorobenzene 2-dichlorobenzene ,is(2-chloroi---nether exachloroethane :-nitroso-di-n...nrnnvlamine . i trobenzene $.OOhorone : -o i t rooheno 1 ' 4-d i methv 1 oheno 1 ,is(2-chloroethoxv)methane '. 4-dichloroohenol 2 4-trichlorobenzene 1-1nhtha 1 ene 1exachlorobutadiene 1-chloro~resol 1exachlorocvclooentadiene : 4 6-trichloroohenol :-chloronaohthalene 3.cenaohthvlene forethvl ohtha late 2 6-dinitrotoluene 1cenaohthene 2 4-dinitroohenol 2 4-dinitrotoluene 4-oitroohenol fluorene 4-chloroohenvlohenvlether diethvl ohthalate 4.6-dinitro-o-cresol ::liohenvlamine uobenzene 4-branoohenvlohenvlether hexachlorobenzene :>entachloroohenol :>henanthrene ,mthracene ::libutvl ohthalate fluoranthene J -Estimated value. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES. N.C. DEPARTMENT OF 1-AJHAN RESOORCES P.O. BOX 28047 -306 N •. WILMINGTON. ST., RALEIGH, N.C. 27611 ORGANIC ~EHICAL ANALYSIS LAB NO q4,,J.J1 I 0 C/Y.221 ~ qy.,2..YJ IA 9'1.2.JI/C:, FIELD# wL-oo-i-t.w IAJl.,-00..3-(nli. ilK... "()DI./-/' ,, ill/ -()0 .5-./:.. IL TYPE < I ) < I ) < I > < I ) UNITS V lJQ/1~, UQ/1 \rnttt,e I .,.. uQ/ l lHFr'tl "uq/1~ /l'l/2~ .... LA-IA -IA-u_ -- 'V SO/Jl,50 /tJ/330 so/11~'-o 10/Bo I J, 5o/Jt,,5o I0/33a I "4/ s-0/11,,so JIJ/_'g3t} / / I / ":, '\, \I Y' \' K -Actual value is known to be less than value given. '1'1--"2~~ 1/.l)L-a:Jl-t.E' 1 ?) µg/_V L,.,l- \ V L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. The nurber ~ -Not analyzed. is the 11inim.Jn Detection Limit. m])L ---1/ -Tentative identification. ~I -On NROC List of Priority Pollutants. I. C. Vi..vi...o,i..on 06 HeaLth SeJtvic.u >HS 3068-0 14/86 L~bolfJLto~y) - 9</,,ll'/h 1111/ -1)07_-I J: ?°) ( ) uo/1 ~ I,,( . "\. V BASE/NEUTRAL ANO ACID EXTRACT ABLES C0'1POOND ovrene benzidine butvl benzvl phthalate benz(a)anthracene chrvsene 3.3-oichlorobenzidine bis(2-ethvlhexyl)phthalate di-n--0etvl ohthalate benzo(b)fluoranthene benzo(k)fluoranthene benzo(a)ovrene i ndeno( 1. 2 .3--cd)ovrene dibenzo(a.h)anthracene benzo(a.h. i)perylene aniline benzoic acid benzvl a 1 coho 1 4-<:hloroaniline di benzofuran 2-4rethvlnaohthalene 2--4'1'1E!thvloheno1 ~thylphenol 2-nitroani 1 ine 3-nitroaniline 4-nitroani line 2 4 5-trichloroohenol K'J3( CcJ.Jf-i Rlnlf-no A.) _J STATE LABORATORY OF PUBLIC HEAL TH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGAHIC ~EMICAL ANALYSIS LAB NO (./t./217/0 q(/-251 /3 q '/-2.f?/h q'/.).;, Jq FIELD# lllL-oD2-C.u... Wl -Q:J3 -lnu. ) ".JL -OOY-6,u. l))L.. -oos-r;, u... TY?€ (/ ) C I ) CI l c I l UNITS /µq/1~ i(µq/1 ~ (uq/ 1l . ....au, ruo/f)ua:&o. I0/330 I A ----LA-IA-lA- -""/J/60 -- /0/~:/30 J, .so/11:,.~11 /tJ/Eo /()/.s~O S()//Af'°O I , , ,., ,v "\ V \. I \I/ IS a /1 h_'i'D UL-1/l-v<-v<- '" I/ 1/t:J /_z.:lll '4' S'oh t,.',o / / '-1:t ,, ,1 '\,, \.v -----,,,--.....,_ -+J-(-J '--) (-_) ( -) -- mnt.. J -Estimated value. H2.0/ SCIL K -Actual value is known to be less than value given. 't<./J-22: ~ l<.,l/.,-00/-t..G ( ~) V"ucitv~ 1/4.- '\ I/ v<- / \I -----(-) ~ L -Actual value is known to be greater than value given. U -tiaterial was analyzed for but not detected. The nurt>er is the Minirrun Detection Limit. m~t.. NA -Hot analyzed. -1/ -Tentative identification. fl -On NROC List of Priority Pollutants. N.C. 0-i.v-w-i.on 06 He.a.Uh SVt.v-i.c.e.o DHS 3068-0 14186 LaboJLJLto~ul IC/ Sl.2.J21~ Wl---00 2-li. ( .R) lruo/1 ~ 1/4.- I ; ' ' I i i ,1 v(_ / \V ~ ( -) - i l I j STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF 1-lJHAN RESCXJRCES P.O. BOX 28047 -306 N. WILHINGTOH, ST., RALEIGH, N.C. 27611 ORGANIC CHEMICAL ANALYSIS \ASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD# COl'1POOND TYPE UNITS ii trosocHmethvlami ne JI\/ :i':J,t') ; (2-chloroethvl )ether :h 1 orooheno l !llOl 3-<lichlorobenzene t-<lichlorobenzene ~-<lichlorobenzene s (2-ch loroi 1 )ether xachloroethane n i troso-<li -n-oroov 1 amine trobenzene oohorone nitl'alhenol 4-<limethvloheno 1 s<2-chloroethoxv)methane 4-<lichloroohenol 2.4-trichlorobenzene vhthalene ·xach 1 orobutad i ene -ch 1 oro-m--creso 1 · xach 1 orocvc l ooen tad i ene 4.6-trichloroohenol -chloron~nhthalene :enaoh thv 1 ene methvl ohthalate 6-<linitrotoluene ;enaohthene ,v .4-<linitroohenol S0//&,,50 4-<linitrotoluene /tJ/330 -n i t rooheno l so/11~,;o luorene 10/.Eo -chloroohenvlohenvlether I iethvl ohthalate J, 6-<linitro-o-cresol l5o/Jt,,5o iohenvlamine /0/330 zobenzene I -bramnhenvlohenvlether exachlorobenzene 'I/ entachloroohenol sol10so henanthrene Jtj/."::/_'~r) nthracene ibutvl ohthalate luoranthene ~:, -Estimated value. m-:D L H-z..0/.SO/L- Qt.JdgJ9 Qt.;,J P.1q h11... -ooJ.. _12; i, •{.,-oc,t./~ ( LJ ) ( 4-) ,.....µa/1~ ""'ua/1~ ',( --, ,( - ,. \" ,. ~ .::i nn D \v 71.A- Actual value is known to be less than value given. -Actual value is known to be greater than value given. ( ) 110/l 110/ka ( ) ua/1 ua/lca -- ( ) ua/1 ua/lca --Material was analyzed for but not detected. The nlffber ~ -Not analyzed. is the f'lininun Detection Limit. mIJL --- I -Tentative identification. I -On NROC List of Priority Pollutants • . C. Vivi...ti.i..on 06 He.aLth Se1t.v-<'..c.e.1.1 fS 3068-0 (4/86 L~boJULto~yl - ( ) ua/1 ua/lca STATE LABORATORY OF PUBLIC HEAL TH OIVISIOH OF HEALTH SERVIO::S, N.C . DEPARTMENT OF HUMN RESOURCES P.O. BOX 28047 -306 N. WILMINGTOH, ST., RALEIGH, N.C. 27611 ORGANIC ~EMICAL ANALYSIS BASE/NEUTRAL ANO ACID LAB NO 19</-,Jx' ,)_J? 7<.f,:)..~~9 EXTRACTABLES FIELD II /Jll-00.2-AG WL-7'}0'/-~L COt1PCXJNO . TYPE ( L/,,) ( t.J) ( . ) ( ) UNITS ruo/1~ 'uq/lAt~ uo/1 uQ/lcq uQ/1 uQ/lcq ovrene IJo/~~{j -,.A._ IA- benzidine S't1/JASO -- butvl benzvl ohthalate /0/.3~0 benz(a)anthracene I chrvsene J, I 3 3-dichlorobenzidine 'lbStJ SOI '\ I bis(2-ethvlhexvl)ohthalate Jo/:t::J.o ~-, =? ~ di-n-octvl ohthalate II0/.3~o , I ,e__ benzo(b)fluoranthene so/,~ benzo(lc)fluoranthene benzo(a)ovrene indeno(l.2.3-cd)ovrene dibenzo(a.h)anthracene , , benzo(o.h. i)oervlene ,~ ,1 , 1 aniline ls" a /1 ~.til, I.A-~ benzoic acid benzvl a 1 coho 1 4-chloroaniline "-,.,. dibenzofuran ii() J '=r.:?ll 2~thvlnaohthalene 2~thvlohenol ' 4--4Tethvlohenol "' 2-ni troani line S"o/,t.~o 3-nitroaniline I 4-nitroani 1 ine , 2.4 5-trichloroohenol 'V ,v \. I .-..-.. ,....--,.... f/16 r C.o,JAIW'JATJo;JJ +-I-(-) t+) , - m1H .. J -Estimated value. H"O/ Se;l'- K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Katerial was analyzed for but not detected. The nurt>er is the Mininun Detection Limit. NA -Not analyzed. 1/ -Tentative identification. fl -On NROC List of Priority Pollutants. N. C. V.i..v.u.i.i..o n o 6 H e.a..Uh Se1t.v.i..c.e.6 DH~ ~Oh8-0 (4/8h LaboJULto~u) ( ) ( ) uo/1 uo/lco uo/1 ua/lco REGION: IV REG I ON: IV : WARREN CT Y lQ J. LEA~ER: GROVE R NICHON COMPANY: 1,JARR EN CTY ACiIVITY : SPILi.. ID: CHA IN-OF-CUSTODY RECORD :•RO!:CT ID : SIT E NAME : ~!rr en County L~ndii li !Tl , STATE: Afton /W~rr en , NC T~ SHIPPED: 07/:~!94 CARRIER: AIR8 ILL: SH IP PED re: US -EPA, R~GION IV LAaO~ATORY ENVIRONME NTAL SERVICES DIV COLLEGE STATI ON ROAD • ATHENS, GA 30613 -7799 ATTN: DESSIE COLO U!TT PHONE: 406/546 -3:1! -MPLE ID STAT ION D:S:P.IPTION EXT /PE S i(:) \J L -001 -LE LEACH ~TE ( 1 ·1 WL -PE Si /HER( 1) . ' 63 WL-001-55 SURFACE SOI L t 1) 1,/L-33 EXT /P EST( 1) WL-002-6\.1 GROUND WATER ( 1) WL-102 PEST /HER( 1) WL-002-LC [ANDFILL CONTENTS 1 ) WL -82 · -EXT /PEST(!) l,/L-002-LE LEACHATE ( 1) WL ~ 68 PEST /HER( 1) WL-002-SD SEDIMEN1 ( 1) ~L -53 EXT/PEST (l ) WL-003-GW GROUND WATER . (i.) WL -89 PEST/HER(i ) WL-004-GW GROUND WATER . ( 1) ~L-73 PEST /HER( 1) WL -005-GlJ GRO UND WATER . ( 1) WL -78 PEST /HER( 1 J United Stales Environmental Protection Agency NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Superfund Section Contract Laboratory Program Sample Management Office P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 Mh TP.I X Ground \J3t e~ :.at fr Soil/Std i111ent Ground ~at er Waste Water $efonent Grou nd ~ater Gr ound Wa ter Sr ou nd Water DATE /TIHE SAMPLE R G7-28/11 3S r . WALKER 07-28/13C,C, G. SffDi ,."( 07-28/11 20 L. ROSE 07-2810837 L. ROSE 07 -28/1735 T. WALKER 07-28/1500 G. STEPHENS 07-28 /1430 L. ROSE 07 -28 /1055 M. POINDE XTER 07 -28/1600 L. ROSE 07 -28/1~00 T. WA~KER 07 -28/1400 T. WALKER PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 . I ,. FORM NO. 01083 _ ..... -~•'-• I Al"'I "•-•• £._ ,.__ ... _____ L _,,. \~~ ,: !-:.· r.~,, .. ::~ A~i!ViTY: $::'ILL IO: PROJECT IC: SITE NAME: Warren Count y Landfil l c:T Y, ST ATE: Afto n/~arren, NC 'ATE SHIPPED: 07/29/94 CARRI ER: AIRBILL: SHIP~~~ TO: JS-EP A. REGION IV LA30RA10R ~ ENVIRON~ENTAL SERVICES DIV COLLEGE STATION ROAD .A2 AiHENS, 6~ 30613-77 99 ATTN: DEBB IE COLQUITT PHONE : 404/54~-31!1 ,AMPLE ID ST ATIO~ (1ESC~IPTION ~iLTER•MttHA--"· !. It -001 -FL 0c6( 1) ~~-001 -SD PCS( 1) w~-001-s.i PCB( 1) WL -002 -FL PCB{ i, WL 9€~ SB ~ WL -002-SS PCB( 1) WL-002-SW PCS( 1 \ WL -003-SD PCB( 1 i WL-003 -SS PC'B( i) WL-003-SW PCB( 1) WL -004-SD t,,l )W~"-46 srn1~::NT i 1) \,/L -4, SURFACE ~ATEP ( ! ) WL -4S F:LTER t!:Di?. (;)~L-4i \•I 'N,-. SURFACE SOIL ( 1 ) iJL -41 SURFACE WATER ( 1 ) WL -SO SED!MHH ( 1) \.IL - SURFACE SOE. 1. ! ) HL -4 2 SURFACE WATER (l)w~-3S 5EQIMENT ( 1) WL -33 . /.~-,:.~~ WARREN CTY CHAIN-OF-CUSTODY RECORD NC Department of Environment Health & Natural Resources Division of Solid Waste ManagemenVSuperfund Section Unrted States Environmental Protection Agency Contract Laboratory Program Sample Management Office P.O. Box 27687 Raleigh, NC 27611-7687 PO Box 818 Alexandria, VA 22313 Telephone (919) 733-2801 Fax (919) 733-4811 703-557-2490 FTS 557-2490 DATE!iIME SA~P~ER Soil !Sed i~ent 07 -2810926 L. ROSE Sedir-~nt 0~-2P,.'1205 M. Surf ac€ Wate r 07 -28 /1205 ~. Soi l/Sediir.er,t 07-23/(19:~ ~. ROSE bQGi;ent Oi-~P 'Jl\5r ~ ~INDEXTE Soil/Sedimf'rit 07-28/0920 L. ROSE Surf ace Water 07-28/1040 H. POINOEXTE Sed iment 07 -2910920 r .. POINDEXTE Soi if Sediment ,)i-28/09 30 L. ROSE Surf ,ce lhler Sediment 07-28/0850 ~\. POINDEXTE ~.oil/Sediment (,7 -2810938 L. ROS E Surf ace IJater SediPient FORM NO. 01078 White -LAB Copy for Return to Samplers Yellow -LAB Coov Pink -5a toler'~ Coov Goin -,~trrl r.oov REGION :!\' REGION: IV 0RGJ. L~ADER : 6Q0VEP MICHON COHPANY: WARREN CTY A:i IVITY : SPILL iD: 0ROJE Ci ID: •: · SITE NAME: ~ar ren .County Landfi ll (J P , ST ATE.~.;:Hooillif.ten, NC . ~ ·'. ,. ,t " ~-~-- DATE S~IPPEC : 07/29/~4 CARRIER: LAB Al RB ILL: ENVIRONMENTAL SERVICES DIV COLLEGE STATION ROAD ATHENS, GA 30613-7 ?99 ATTN: DEBBIE COLQUI TT PHONE : 404l54t -3i!l SAMDLE ID STriTI ON DESCRIPTION WARREN CTY CHAIN-OF-CUSTODY RECORD NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Superfund Section P.O. Box 27687 Raleigh, NC 27611 • 7687 Telephone (919) 733-2801 Fax (919) 733-4811 MATRIX jATE/TIME SAMPLER United States Environmental Protection Agency Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 ================~================-=-----------------------==----------------W~-005-3~ SURFA~E WATE R Sur face ~at~r 07-29/0840 ~- r 1 ) J!~ -31 PCB( 1; WL-028-SS SilR FACE SOIL Soil /Sediment 07 -28/093e L. pocc '· i ) WL ~ . 4 ~ FORM NO. 01079 Whi te -LAB Copy for Return to Samplers Yell ow -LAB Copy Pin k -$3~~ler 's Cony G0l d - E xtra Copy . ; I REGION: IV ~CJ. LEAD ER: &ROVER hICHO~ REGION: IV CO~PANY : WARREN CTY AC7IVITY : PR02ECT ID: SITE NA~E : Wa~re~ Coun~y ~a ndfil l :IT Y, STATE: Afto~/~arr e~, NC ~TE SHIPPED : 07 /29/Q~ CARRIER: /.,;PS ILL: SPILL IO: ENVIRONMENTAL SERVICES DIV COLLE GE STATIO N ROAD ATHE NS, 6A 30613-7799 ATTN: DEB BI~ COLOUiiT ~8 ~AMPLE ID STATION O~SCRIPTION WARREN CTY CHAIN-OF-CUSTODY RECORD NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Supertund Section P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 MATRI X DATE/TIME SAMPLER United States Environmental Protection Agency Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703·557-2490 FTS 557-2490 ======================================== =============~= =====---------=------= WL-007-5S PCE'I 1 i WL -OO<l-S) P,'B i 1 \ WL-010-S: Pee( i ) WL-011-SS PCB(l ) wL-012-ss PCB(l) WL-013-$$ PCB( 1) SURFACE SOIL I 1) wL-b SURfACE SOI L { i ) WL - 5llRFACE SOI~ ( 1) WL - SURFACE SOIL 6 { l ) WL -10 SURFACE SOIL ( 1) WL -11 SURFACE SOIL ( 1 ) WL -12 ~IL -014 -55 '' SURFACE son PCB( 1 \ WL-015-SS PC~( 1) IJL-017-S:, PCB( 1) WL-018-SS PCB( 1) (i;WL -12 SURFACE SO!!_ (1) WL -i 4 ("R-"• so1 1 u rHt._ - l )WL-20 SURFACE SOIL (l )WL-21 SURF ~CE SO IL ( 1) WL-22 WL-01 9-55 SURFACE SOIL ( 1) WL--23 PC B( 1 } ~-• WL~o~o -ss: 1~URFACE SOIL PC B( 1) . ( 1) WL -24 Sril!Sediaier.t 07-27 Ii 51t G. $(, i l/S~d i a,e nt C7-~7/i:,1: (.' J . 5Gil/Sed!m ent Seil 'Sediir.~nt C·i -271'! ~2, ' Q , Soil/Sediment Soi l/Sediillent Soil/Sediment 07-27 /1 532 6. Soil.'Sediment Q7-27/153E, G. Soil/Sediment 0>27/1538 G. Sod/Sediment Soil/Sediment (,7-27 /1606 6. Soil/Sediment 07-27/161:{ G. STEPHENS Soil/Sediment 07-27/1 619 G. Soi l/Se diment FORM NO. White -LA~ Copy fer Return to Samplers Yellow -LAB Cop1 Pi nk -Scmplcr's Cc~y Gold -Extra Copy _ 01081 i ~ t: ' . ,, " 1; r I REGION : IV ~oJ . LEADER: GROVE 0 ~!CHON REGION : IV :OMPANY : WARRE~ CT Y ACTI VITY : PROjECT ID: SI TE NAME: ~arr e& Coun~y ~andf ill :m J STATE: Afton/Yafrer,, N( :JE SHIPPf D: 07 /24 1~4 CARRIER: AIRBILL: SPILL H•: ENVIRONMENTAL SERVICES DIV COLLEGE STAT ION ROAD ATHENS, GA 3061:-1799 ?;8 ATJ~: DEBB!E CCLCUITT PHONE: 4041546-2:1: -AMPLE ID SiATION . DESCR!PTION ======== it-021 -~~ PCB( 1) IJL-022-~~ PCB( l) ~L-023-SS PCB( 1) WL-024 -SS PCB( 1) WL-025-S~ PCB( 1) WL-026-SS PCB( 1) WL-027-SS PCB( 1) WL-02(l-S5 PCB( 1) SUP.FA(~ :-0 TL (:' w> SuR ~ACc SOI~ /_ : .· w~- SURFACE 50:L ( 1) ~L- SURFACE SOIL ( : ) 1./L- SURFACE SOIL ( l ) 1-!i. - SURFACE SOIL ( 1) WL- (URFACE SOIL 1) i-lL - SURFACE SOI~ (•' . I ./ wL - 25 ~[ 2i 28 29 15 30 ~ ~ WARREN CTY CHAIN-OF-CUSTODY RECORD United States Environmental Protection Agency NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Superfund Section Contract Laboratory Program Sample Management Office \ P.O. Box 27687 Raleigh, NC 27611-7687 PO Box 818 Alexandria, VA 22313 Telephone (919) 733-2801 Fax (919) 733-4811 703-557-2490 FTS 557-2490 MTRI X DATEiT I~E SAMPLER S0i l/Sedi11~nt -"J7 -n n;,n I;, ~c,il/Sedi11"-nt 07 -27 :'i,29 G. SC'il/S~d ime~t 07·27ii.l23 6. So~l.'Sedifl!ent Q7 -27 .'i63~ G. STEPHENS Soi l/Sedin;e n~ 07 -27/1639 ' Si EPHENS \:, Soil/Sediment 07-2711538 G. STEPHENS Soil/Sedi1mt Oi-27 /1639 G. STEPHENS S0il/Sedime nt 07-271142~ G. STEPHENS FORM NO. 01082 White -LAB Cppy for Return to Sample r::; Yellow -LAB Coo r Vi nk. -;~11oler 's r.oov tir:lrl -;:1tr .. t'/\o v I 1:. ,,. I.~ ,, __ I:_,~ . 1~,. (.'! I• I RE6IOH: IV REGION: IV WARREN CTY 1J. LEADER: GROVER NICHON COMPANY: WARREN ClY ACTIVITY: SPILL ID: ., CHAIN-OF-CUSTODY RECORD 0RCJECT ID: ~ITE NAME: ~arren County Land'ill :TY, SiATE : Afton/Warren , NC -S~IPPED: O7/29 /9C C~RRIER : A!RBILL: ENVIRONMENTAL SERVICES DIV CO~LEGE STATION ROAD ATHENS , GA 30&13-7799 ATTN: DEBBI£ COLOU!iT PHONE: coa/54f-311l KPLE ID STATION NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Superfund Section P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 ~~~~-- ✓ United States Environmental Protection Agency Contract Laboratory Program Sample Management Offtce PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 ~L-O06 -GW GROUND~AlE R IIAiPIX Ground I.later C7-29/193O G. ST EPHENS ( ! ) ~L -10 S FORM NO. 01085 ACiIVITY: PROJECT IC: SITE NAME: ~a r~e~ County Landfi '.l :In . ST4TE: Afton/Warr en, NC ✓~ 4-t-f➔HHl-P.fo.;. ~7 /19/9-4--tARRIER.:... AIRS ILL: SPILL I:,: ENVIRONHENT~L SERVICES DIY COLLEGE STATION ROAD ATHENS, GA 30623 -7799 ~8 ATTN: DESSIE COLQUITT PHOHE: 404/54~-2111 -A~PLE ID STATJO~ · DESCRIPTION ·-...... WARREN CTY CHAIN-OF-CUSTODY RECORD NC Department of Environment Heahh & Natural Resources Division of Solid Waste Management/Supertund Section . P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 MA RI X DATE/T IME SAMPLER So 1,s~di1ent United States Environmental Protection Agency Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 FORM NO.· 01080 Whi te -LAB Copy for Return to Samplers Yellow -LAB Copy Pink -$amPler's COPY Gold -Extra toDY REGIQN: IV · REG I ON: IV ~RO J. LtADER: GROVER NICHON COMPANY: ~ARREN CTY WARREN CTY ACTIVITY : j-:. SPI-LL IC: CHAIN-OF-CUSTODY RECORD • ' .< • .•• ,, PROJECT IC: SITE HA~E : Werren Co~nty Landf ill CITY, STATE: Aft0n/1Jarr~n, NC . 1 • :.! JATE SHIPPED : 07/29/9l (ARRIER: AIRBIL~: SHIPPE D TO: ~5-EPA. REGION IV LA90RATOP" ENVIRONMENTAL SERVICES DIV COLLEGE STATION ROAD LAB ATHENS, GA 30613-7799 ATTN : DEBBIE COLQUITT PHONE: 404/546-3111 SAMPLE ID ST ATION -DESCRIPTI ON IJL-001-GW GROUND IJAT:R '. 1) \.I~ -SP DES i !HER( l 1 IJL -001 -LE -! ~ArH,;F fI / \.IL -- PES i /HER( l ) ~L-002 -GW 6ROUHD WAT ER 1: 1) k · 10 2 PEST /HER( 1 \ •l-002 -LE LEA:HAT: ( 1 ) ioll - PEST /HER( 1) IJL-003 -GIJ GROUND WATER &8 PEST /HER( 1) ( 1 ) WL -39 WL-004-GW GROUND WATE R PEST /HER( 1) ( 1) WL -73 WL-005-G IJ GROUND WATER PEST /HER( l ) ( 1) w~ -78 United States Environmental Protection Agency NC Department of Environment Heatth & Natural Resources Division of Solid Waste ManagemenVSuperfund Section, Contract Laboratory Program Sample Managemem Office P.O. Box 27687 Raleigh, NC 27611-7687 PO Box 818 Alexandria, VA 22313 Telephone (919) 733-2801 Fax (919) 733-4811 703-557-2490 FTS 557-2490 MATRI X DATE/TIME SAHPLER Gr ~und ~~te~ 07 -28/il35 7 . IJALKER Water 07-28 /li ~0 L. R05E G,ouns ~ate, 07 -28/;735 T. WALKER Wat~r 07-28/1430 ~-?.OSE ·jround wa ter 07-28 11600 L. POSE Ground IJater 07-28/1 400 T. WALKER Ground wate r 07-28/1400 T. wALKER FORM NO. 01076 ~hite -LAB Copy for Return to Samplers Yellow -LAB Copy Pink -Sa ~Pl er 's Copy Geld -Extra Copy , l ►.' L ~ t .\ REGION: IV 'RE GI ON : IV -~~J. LEADER: GP.OVER MJC~ON COM?ANY: WARREN CTY WARREN CT Y ACTI VITY : 0POJECT IO: 5Plll ID: CHAIN -OF-CUST OD Y RE C ORD SiT~ N.AM~: ~arrEn ~ount y Landfil l ·~!TY , STATE: Afton/limen, NC ~/ ·AT E SHIPPED : 07129/Q( CARRIER: AIRBILL: SHIPPED TO: ~S-EPA , RE~ION IV LA80RATGRY ENVIRONMENTAL SERvICES DIV COLLEGE STATI ON ROAD .118 -AMPLE ATHENS, GA . 30613 -7799 ATTN : DEBBIE COLQUITT PHONE: 404/54 e-3111 ID STATION DESCP.IPTION NC Department of Environment Health & Natural Resources Division of Solid Waste Management/Superfuncf Section , ; P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 MATRIX DA TE/T:ME United States Environmental Protection Agency Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 AMPLER ·-----------------------------------------------------------------------------------UL-001-6~ GROUND IJAER G'ou~d Uate r 07-28 'ii 35 IJA~K ER ( l) lJL-57 EXT ORG( 1) ~L -001 -L: LEACHATE ~ater 01 -28 t L2'J L. pocr ( 1) U> &2 EXi ORG( 1 ) WL -0 0: -~-S SURF.ACE SOIL ~.0il /Sedin1ent 0i-~8 /'0837 L. ROSE ( 1) w~ -~~ J, EXT ORGi' 1) Rinseate 0t h~, 1;7-28/1710 G. SiEP~EN5 ~l.-00~-ol ( 1 ) WL -9-t ,, EXT ORG( 1 ; WL -,)02-GW GROUND WATER Ground Water 07-28/1'735 T. WALKER (\\Ill ~ ·" . i j fiL -l 'J' EXT ORG( 1) 07-28/1500 G. ST EPHENS WL-002-LC LANDFILL CONTENTS Waste ( 1) WL -81 EXT ORu( 1 ) WL-002-LE LEACHATE WQter 07-28/1430 L. ROSE ( 1) WL -67 EXi ORG( 1) IIL-002-SD SEDIMENT s~ciment 07-2?./1055 M. POINDEXT ( l ) W!_-52 EXT ORG( 1 ) WL-003-GW GROUND WATER Ground ~ater 07-28/1600 L. ROSE ( 1 ) l·ll -l;" ~~ EXi ORG(l) WL-004-BL fi) Hose Rinseate Blan~ Other EXT ORG( 1) , 1 WL -98 WL-004-GW GROUNll WATER G~ound Water 07 -28/1400 T. WALKER EXT ORG(l ) ( 1 ) WL -72 UL-005-GW GROUND WATEK 1;ro1Jnd Water 07-28 /1400 T. WALKER EXT ORG( 1) ( 1) UL -77 FORM NO. 01075 ~hite -LAB Copy for Return to Samplers Yellow -LAa Coby -Pinl -Sa~oler's Coor Gcid -Extra CoPY f:; 1.1 r~ I• .mun~ ... : REGION: IV PR0J. LEADER : &P8VE~ NICHON I REGION: IV COMPAN Y: WAR~EN CTY ~-WARREN CTY ACTIVI''.Y: . PROJECT in: ,SPILL.ID: CHA IN-OF-CUSTODY RECORD Sl?E NA~E : Ua:ren County Landfill CIT_:,~ STATE : Af to n/Warre.I'f~c DATE SHIPPED: 07 /29/9~ CARRIER: AIRBILL: ,-., ,•-1:j . 5HIP0ED TO : US-EPA , REGION IV LABORATORY ENVIRONMENTAL SERVICES DIV COLLEGE STATION ROAD ATHENS , GA 30613-7799 ATTN: DEBBIE COLQUITT PHONE : 404 !546·3lli LA8 SAMPLE ID STA TION ----------------------------IIL-001-BL VGA( l ) WL-OOl·GI. VOA( 1) W~-001 -LC 'JOAi :) iolL-OC• 1 -LE VOA( 1) WL-OO i-55 VOA~l ) WL-02-BL VOA( 1) WL-002-GW VOA( l \ WL -002-LC VOA( 1) UL-002-LE VOA( l) WL-002-SD VOA( 1) WL -003-BL VOA( l) WL-003-GW VOA( 1) WL-004 -BL VOA( 1) WL-004-GW VOA( 1) DESCRIPTION. Trip Blank (l )~L-45 GRCUN.D WAER I_ 1) I,!~ -5~ ~EA~HAiE ( l ) WL - SURFACE SOIL 61 ( 1) WL -31 Rinseate (1) WL -92 GROUND WATER ( 1 ) WL -100 LANDF ILL CON TENTS ( 1: WL -8·~ LE~CHATE ( 1) I.IL -g SEDIMENT ( l) ~L -51 Post Pr eservative Blank ( 1 ) WL -95 GROUND WATER ( 1 ) wL -87 A~~ Hose Rinseate Blank ( 1 J WL -97 GROUND WATER . ( 1 ) WL -71 NC Department of Environment Health & Na1ural Resources Division of Solid Waste ManagemenVSuperfund Sec1ion4 I, P.O. Box 27687 Raleigh, NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 Uni1ed Stales Environmental Protection Agency Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 MATRIX Other DAiE/TIME SAMPLER Ground Water Waste Wate r Soil!Sedite;it Other Ground Wat~r ~aste Water Sediment Other Ground Water Other Ground Water FORM NO. White -LAB Copy for Returr to Sa~plers Yellow· LA~ CQpy Pi nk · Sa~ple~•s Co~y Gold -Ext ra CQPY REGION: IV REG I ON: I V WARREN C TY P~OJ. LEADER: GROVER NICHON COMPANY: WARREN CTY ACT1VITY : SViLL ID: CHA IN-OF-CUSTODY RECORD PROJECT !D: SIT~ NAH~: Wa rrep Count y Landf ill CITY. STATE: Af ton/lilarren . NC DATE SHI PPED: 07/29'94 CARRIER : AIRBILL : S~IPPED TC: US-EPA. R~GION :v LABORATD~Y ENv!ROHMEHTAL SERVICES DI V COLLEGE STATION ROAD ATHENS, GA 30613-7799 ATTN: DEBBIE COLQUITT PHONE : 404/546-3111 -------------------------------------------------· ,.,. LAE SAMPLE ID STATIC~ ·. D~SCRIPT!ON NC Department of Environment Health & Natural 'Resources Division of Solid Waste ManagemenVSuperfund Section P.O. Box 27687 Raleigh. NC 27611-7687 Telephone (919) 733-2801 Fax (919) 733-4811 SAMPLERS (Signature) ~~- \ \( ... .:\.-.\"~ '\ '- MATRIX ~}TE/TIME wL -005 -Gil VGA( i) GROUNC WATER Ground ~ater ' :, '': . ..i .• · . I l '; ~> 7b ! ./ ! ,.. / l ~ ., Uhite -LAB ~;~ f~r te.turr.\o SamP,lers ,,, Unrted States Environmental Protection Agency "- Contract Laboratory Program Sample Management Office PO Box 818 Alexandria, VA 22313 703-557-2490 FTS 557-2490 FORM NO. · 0107.4 . Gold -Extra Copy