NCD980602163_19940701_Warren County PCB Landfill_SERB C_Binder No. 3 - Sampling Plan Data, July 1994-OCR

WARREN COUNTY
SAMPLING PLAN
JULY 1994
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PCB LF
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DIOXINS ANALYSIS
Fuel
Hexane
Water
Soil/Sediment/Filter
INORGANIC CHEMICALS
ORGANIC CHEMICALS
WARREN COUNTY 1994
BINDER NO. 3
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STATE LABORATORY OF PUBLIC HEAL TH
WARREN COUNTY PCB LANDFILL
ORGANICS AND INORGANICS
LAB NOS. 013909-013923
;s.·.c. Ocpar.mcnt o( Environment,
l lcallh, & .--,·,.ur:il Resources
Solid Waste Manai;cmcnt Di,ision
Si te Number -----------------field Sample Number
P.O . Box 2SO-l7, 306 ~-Wilming,on Strccl
Raleigh, North Carolina 2761 J
/ ------------------
Name of Site WA-1<i2.e.J GorJTY PCt:> l..DFL Site Location A F"To iv NC, _..:.......c._....:...,:::_,_:_;::;__ __ .....-e=C--------------
Collected By 6 . N , u-to l-6C:>..,_, ID# 3 =t-Time /120
I.. , i20SE.
Agency: Hazardous Waste X Solid Waste ___ Supcrfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
En-,,ironmcntal Concentrate Comments Arsenic --Barium ----__ Ground water (1) _ Solid (5) FtLT€12 6Y~7""E""---Cadmium
Chromium --__ Surface water (2) Liquid (6) /AJLe.7 -LE.t4CHA7e---Lead
Mercury --Soil (3) _ Sludge (T) £>PL ✓ Z: k,)/ FC..o Selenium --. --Silver
-2i._ Other (8) ;:re-001-L <!.H --_ Other (4) ' --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)1es;'.1 ~ Organic Compounds Results(mg/1)
P&T:GC/MS ~ Ars C D.l C .L._Q.G) benzene ----Acid:B/N Ext. L Barium c.a3 carbon tetrachloride ----"MTBE 'Y Cadmium .L... O. 0Cd-. chlordane ------Chloride chlorobenz.ene ------_x_ Chromium LO.o I chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-crcsol ----,c Lead 1-0.005 cresol ------
--__ Manganese --1, 4-d ichlorobcnz.ene
----1!:__ Mercury -<..0.0005 --1,2-dichloroethane
--Nitrate 1, 1-di chloroeth ylcne ----
)(: Selenium L..o. coS 2,4-dinitrotolucnc ---1:._ Silver L__o ,.05 --heptachlor
Radiochemistry Sulfates hexach lorobenzene ----Zinc hexachlorobutadicnc ----Parameter Results (PCi/1) pH hcxachloroethanc ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenz.cne ------TOC pcnlachlorophcnol ----
----pyridine
Microbiology ----lelr achloroethylene
----trichloroethylcoc
Parameter Results (Col/l0Oml) __ 2,4,5-trichlorophcnol --
------2, 4,6-t ri chl orophcnol
--vi nyl chloride ----endrin --lind:rnc --Date Received Report ed by methoxychlor --
--toxaphcne
D:.itc Extracted Date Reported · 2,4-0
013909 JUL 2 9 9 4 --__ 2,4 ,5-TP (Silvcx)
Dale Analyzed Lab Number --DI IS 3l 'J I (llcviscd 2/'Jl)
I !c,allh, !,:. l'>atur.il Re.sources
Solid Waste Management Di,ision
Sile Number -----------------
P.O. 13ox 2.SO-l7, 306 K Wilmini;ion Street
Raleigh, North C.roiin• 27611
Field Sample Number tut..-~O 2 -J. € /
Name of Site WA-Q.>2-c..J GarJTY PC"B l.DFL Site Location A F"To.-J NC _.L.:._...:_..!...!:::...!.:~-....:.....:.:......:::::::._ __________ _
Collected By G. {\) 1c.H.o\..,6Qi,.J ID# 3-=l-Date Collected 2€ ;JVL Y 9-4 Time /+3c
L. f2_osE
Agency: Hazardous Waste X Solid Waste Supcrfund TCLP Compounds ------
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) FIL.Te/:!?_ ~vsre#J Cadmium --Chromium
t?VtLeT-LI=ACM ~ --__ Surface water (2) Liquid (6) Lead --Mercury --_ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _l(_ Other (8) --'
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)(--" ~' -Organic Compounds Results(mg/1)
P&T:GC/MS _)(_ Arsenic .L..a.c:.1 benzene ----
--Acid:B/N Ext. ~ Barium o.o7 carbon tetrachloride --"MTBE 1-_ Cadmium L.o. aoa chlordane ----Chloride chlorobenzene ------_:f::_ Chromium ..l..0.01 chloroform ---
--__ Copper o-cresol --F1uoride m-cresol ------
--Iron __ p-crcsol --£ Lead L._O. oo!:S cresol ----
--__ Manganese --1,4-dichlorobenzene
--__2;__ Mercury L..o-0005 --1,2-dichloroethanc
--Nitrate 1,1-dichloroethylenc --_L Selenium 4.0. c, o,:j --2,4-di nit rot ol uene
.J::_ Silver .z.c.o5 --heptachlor
Radiochemistry Sulfates hex.a ch l orobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hex.achloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobcn7.ene ------TOC penl achlorophcnol ----
--__ pyridine
Microbiology ----tetra chloroet h ylcne
----lrichloroethylcoc
Parameter Results (Col/l00ml) __ 2,4,5-lrichlorophcnol --
----__ 2,4,6-trichJorophcnol
------vinyl chloride
cndrin --lind:rne --Dale Received Reported by --methoxychlor
--toxaphcne
Date Extracted Dale Repdt1 · 2,4-D --910 JUL 29 94 --2,4,5-TP (Sil vex)
Dale Anc1l y1.cd Lab Number --I)! IS Jl'Ji (IZcvi scd 2/'.11 )
I I I i I I
J lcalth, l,:. :S:at ur.l Re.sources
Sol;d Waste Management D i,;sion
Site Number -----------------
!'.U. Do;i; ~,._"'JC.,. ,,,·11m1nr,ton Jtrc:ct
lulcigh, Nor1h Carolina 27611
Field Sample Number W L -c) 0 '2 -(i3 L / ----------"':.._--=-----=----
Name of Sile W A-R.i2.c..J Ga1'lT;,' PGt, l.nFL Si te Location A F"T"o >--J NC. _..c._:. _ _:_::::.....:c"'------'-"::;__-----------
Collected By 6 . f0 tl.H.o l, 6c,1--> Date Collected 2'8 dVL Y "74 Time / 1-ID
c;, ~ . S:.r€"Pt-t e>--.:>
Agency: Hazardous Waste X Solid Waste Superfu.od TCLP Compounds ------
Sample Type Inorganic Compounds Rcs ulls (mg/1)
Environmental Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) _ Solid (5) o. F. LA.J,+TeR., Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (T) Selenium ----Silver --L OLhcr (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)<& /II@) Orgnnic Comp ounds Rcsults(mg/1 )
P&T:GC/MS ...L Arsenic L. Cl-CI ben2cne ----
--Acid:B/N E xt. _J£_ Barium L.O.C\ carbon tetrachloride --'MTBE ',( Cadmium <. <!::l • Gog-chlordane ------Chloride chlorobcn2ene ------
--~ Chromium ..t.....0.01 chloroform ----
--__ Copper o-cresol --Fluoride m-crcsol ------
--Iroo p-crcsol ----
--,<_ Lead L.o. oo'.:::i cresol --
--Manga nese 1,4-dichlorobenzcnc ----
--_zs_ Mercury L... o.coa.5 1,2-dich lorocthanc --
--Nitra te 1, 1-dichloroet hylene
7 Selenium --
-4-0. 0 C>~ 2, 4-di nit rot ol uene --1_ Silver L._D.o,3 --heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadicne ----
I
!
I I I I I
I
I I
I I I
I Parameter Results (PCi/1) pH hex.achloroet hanc ----~I __ Gross Alpha __ Cond uctivity --methyl ethyl ketone
Gross Beta TDS nitrobcn7.cne ------I
TOC pent a ch loropheno! I
----I
----pyridine
M icrobiology t ctrachloroet h ylcnc ----trichloroethylcne ----Parameter Results (Col/l00ml) 2, 4, 5-trich I orophcnol ----
--2, 4,6-t rich] orophenol ----
--\~n yl chloride I ----endrin i --lind:ine l --Date Received Reported by --methoxychlor I
toxaphcnc I
--I
O;;te ExtractccJ Date Rcp 'ljld 2 · 2,-'--D ! i --3911 JUL 9 94 2,·\5-TP (S ilvcx) '' --Dale A nal yzed Lab Nu mber --·-1)/ IS 31')1 (ltcviscd 2/'Jl )
N.c; Dcpar.mcnt of Environment,
i lcallh, & l',;a1ural Resources
Solid Waslc Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Heal1h
· P.O. 13ox ~7. 306 S. Wilmini;1on S1rcct
Raleigh, North Carolina 2761 I
Site Number -----------------Field Sam pie Numbcr_.....:t,u::...=.....:J_c....-_-.....:~:;...._t,--=3'---.....:8==--L-'------.i,6,£/_,,._
Name of Site WA-R.i2E:..J GorvTY PC,t!:, U,FL Site Location A F'To ~ N (_
Collected By a . fv IC.Ho\,.. 6c)-......> Dale Collected 2'Z Jt.Jt.:f q1, Time_/L....:..=?....:-/_5'_· __
4 . $fE'Ptt?-,.J~
Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) -· Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Results (mg/I)(~) Organic Compounds Results(mg/1)
P&T:GC/MS .1.. Arsenic L..O-wl benzene ----
--Acid:B/N Ext. ____K_ Barium L.. o .a I carbon tetrachloride --"MTBE ..:;,5__ Cadmium ~o.oca... chlordane ----Chloride chlorobenzene --------~ Chromium .t...o_ol chloroform --
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --.)( Lead .L...o.co5 cresol ------
--__ Manganese 1,4-dichlorobenzene --
--~ Mercury L....o. oo c.!5 1,2-dichloroethane --.. Nitrate 1, 1-dichloroethylcne --T Selenium --
.t...C). 005 2,4-dinitrotoluene --~ Silver .t...o.a5 --heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcxachloroethanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC __ penlachlorophenol --
----pyridine
i\·1 icro biology ----tetrachloroeth ylene
----trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophcnol ------__ 2,4,6-triehJorophcnol
----vinyl chloride --endrin --lindane --Date Received Reported by --methoxychlor
--toxaphene
Date Extracted Dale Reported 2,4-0
013912 JUL 29 94 --
--2,4,5-TP (S ilvex)
Dale AnalyLed Lab Number --DI IS 31')1 (Revised 2/91)
:-:.c. Dcpar.mcnt O( l:.nV\ronmcnc.
iicalth, & Natural Resources
Solid Waste Management Division
~.)f'UlJ.J. J....1-L, ~ 'l4}J...,,J.. ...J.1,.U A . ..........,'-(.......,,.._,....,.._
P.O . 13-ox 2.SO-n, 306 N. Wilmin[:lon Street
RAieigh, North C•rolin• 27611
Site Number -----------------Field Sam plc Numbcr_--=-W=--L._-_,0"°-"'?)'----"4_-...:::B==--L ____ . ..:..✓ __
Name of Site WA-1<.i2.e..J Go,,JTY PGr::, U>FL Site Location A F",o i--J NC _..:.._:. _ __:_:::.....:.._::,c__ __ -..c=e------------
Collected By G;. f\), CH.o L. 6o"'-' ID# ';3 =(--Date Collected ;:?<; -;{{)Cf 44-
~-ST-EPH. ~.S:..
Agency: Hazardous Waste X Solid Waste ___ Superfllild TCLP Compounds ------
Sample Type Inori;anic Compounds Rcsu Its (mg/I)
Environmental Concentrate Comments Arsenic --Q~(l,L .F{~e Barium ---· __ Ground water (1) _ Solid (5) . I=": Wttr c "ie Cadmium --Chromium
A-1R 1-to,5E --__ Surface water (2) Liquid (6) Lead --Mercury --Soil (3) _ Sludge (7) Selenium ----Silver --_){_ Other (4) _ Other (8) --
--
--Organic Chemist11· Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I: <Mt (J g) Organic Compounds Results (mg/I)
P&T:GC/MS __x_ Arseuic L...0_01 benzene ----
--Acid:B/N Ext. l Barium o.o<.sz. carbon tetrachloride --"MTBE _x_ Cadmium .t..O-OOd-.. chlordane ----Chloride chlorobenz.ene ----~-i__ Chromium ,<_D-o\ chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----
--_x_Lcad 0.0\...\l cresol --
--__ Manganese --1,4-dichlorobenzene
--L Mercury ~o-ooo...5 --1,2-d i ch I oroethane
--Nitrate 1, 1-dich I oroeth ylcne ----± Selenium L.D.Oo5 2,4-dinitrotol.uene --Silver -L....a. o 5 heptachlor --Radiochemistry Sulfates hexach lorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hcxachloroclhane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------TOC pent achlorophenol ----
----pyridine
Microbiology ----le tra chloroeth ylene
----trichloroethylene
Parameter Results (Col/l00ml) __ 2,'1,5-trichlorophenol --
------2, 4,6-trichlorophenol
----vinyl chloride --endrin --lindanc --Date Received Reported by --methoxychlor
toxaphenc --Date Extracted
Date ReptYfj91J JUL f 9 94 2,4-D --__ 2,4,5-TP (Silvex)
Dole A nalyzcd Lab Number --I) I I .S JI 'J; ( H.cviscd 2/9 I )
I I
t-:.C Depar::nent of Environment,
i lcalth, &: /'satural Resources
Solid Waste Management Division
SAMPLE ANALYSIS Kt(,l Ut.Yl State ubontory or i-uotic Hcann
P.O. Oox 2.80-l7, 306 1'. Wi!mini;1on Street
Raleigh, North Carolir,a 27611
Site Number -----------------
./
Field Sample Numbcr_~W.:..._L_-_t9---=0~/_-_t;,.:..._w _____ _
Name of Site WA-R.i2e.J Cborvn' PC-""B U,FL Site Location A F"10 I..J NC _.!.....:._...;_:::__:_::"---~--='-------------
Collected By a. f,J ll.HOL.6c)),,..) Dale Collected Z ~ :] V-L-/ C\ ~ Time /13£"
T-tAJA Lkl=-R..
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inor6anic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
-1:t J
---· ~ Ground water (1) _ Solid (5) We '-t. Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium --. --Silver --_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)(~) Organic Compounds Results(mg/1)
P&T:GC/MS _L Arsenic .L.....o .c, I benzene ----Acid:B/N Ext. L Barium o.o5 carbon tetrachloride ----MTBE L Cadmium L..c, -C,<:,d--chlordane ----Chloride chlorobenzene ------X Chromium .L.....o. o \ chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------Iron __ p-crcsol -----_x_ Lead L__o.coS cresol ----
--__ Manganese --1,4-dichlorobenzeoe
--L Mercury L..o-ooQ.5 --1,2-dichloroethanc
Nitrate 1, 1-dichloroethylene ------L Selenium .L.o-oo;S 2,4-dinit rotoluene --..J5._ Silver L..Q.O => --heptachlor
Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hcxachlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzenc ------TOC __ pentachlorophenol --
----pyridine
Microbiology ----t etrachloroeth yl cne
--__ trichloroethyleoc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichJorophenol
------vinyl chloride
cndrin --lindanc --Date Received Reported by methoxychlor --
--toxaphcne
D.ilc Extracted Date Reparted 2 2,4-D --13914 JUL 9 9 4 __ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --DI IS 31')1 (l~cviscd 2/91)
'
1'.C. Dcpar.mcnt of Environment,
I lcallh, l,;. 1'alural Resources
Solid Waste Management Oi,ision
SAMPLE A.i"-(ALYSIS .Kl:..<..,.! u.t...::, 1 Stale Laboratory of Public Hcallh
P.O. Ik>x 2SO-l7, 306 1'. Wilminpon Street
R.alci&h, Nor.h Carolina 2761 I
,/
Site Number -----------------Field Sample Number Wt. -~ l> Z-~ lAJ
"-fame of Site WA-R.i2.e..J CorvT't PG"B l.DFL Site Location A F",o iv NC, --'------'-'=----~------------
Collected By (;. /'v 1~Ho 1.,. 6c>l-J Date Collected Z'S ;/cJ L--/ «=t4 Time /135
/. R_ U .. .u+Lk£,
Agency: Hazardous Waste X Soud Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium L Ground water (1) :Hz ---· Soud (5) W~J.L Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) .SP/. I 1" tAJ/ ;:GO Selenium . --Silver --_ Other (4) _ Other (8) re-001-'i w --
--
--Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Results(mg/1) (t mP ~ Organic Compounds Results(mg/1)
P&T:GC/MS >( Arsenic .,{_CJ. o I benzene ------Acid:B/N Ext. X Barium .1_0.0\ carbon tetrachloride ----'MTBE 1-Cadmium L.ci,oo:;.._ chlordane ----Chloride chlorobenz.ene ------~ Chromium .L.o.ol chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------
--Iron __ p-cresol --
--~ Lead ~c.co5 cresol --
--__ Manganese --1,4-dichlorobenzene
---L Mercury L..0.0005 --1,2-dich lorocthanc
--Nitrate __ 1,1-dichloroethylcne --_½_ Selenium .L.... CJ. OQ5 --2,4-dinitrotolucne
){ Silver -<..0,.9=5 __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hcxachloroclhane --__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobcnz.ene ------TOC __ pcntachlorophenol --
----pyridine
Microbiology --__ tetrachlorocthylene
--__ lrichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol --
----__ 2, 4,6-trichlorophcnol
------vinyl chloride
endrin --lindane --Date Received Reported by --methoxychlor
--toxaphene
Dale Extracted Date Reported 2,4-0
013915 JUL 29 94 --__ 2,4,5-TP (Silvex)
Dale A nalyzed Lab Number --DIIS 31')1 (Revised 2/91)
:--.c;. Dcpar.ment of Environment,
1 lcalth, & Natural Resources
Solid Waste Management Di,~sion
SAMPLE ANALYSIS K.l::\l Ut~T State Labontory o( Public Heallh
· P 0 . 13ox 280-l7, 306 K Wilmini;1on Street
Raleigh, North Carolina 2761 I
Site Number Field Sample Number tut. -00 '3 -~ u..J -------"-----'--------------------------
Name of Site WA-1<i2.e..J Coor-JN PG"t> l.r,FL Site Location A F'To ,-J N l, --'-------''-----------------
Collected By a. f\) t(.H0\_.6CH•-> Dale Collected 2j' ::JULY q4 Time /1.oo
L. Rose
Agency: Hazardous Waste X Solid Waste ___ Super fund TCLP Compounds ------
Sample Type Inorganic Compounds Resuits (mg/I)
Environmental Concentrate Comments Arsenic --
#3 Barium ---· L Ground water (1) _ Solid (5) lUELL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) __ Sludge (T) _ Selenium ----Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)(~) Or~anic Compounds Results(mg/1)
P&T:GC/MS X Arsenic -i...o.o I benzene ------Acid:B/N Ext. X Barium L.. D.a \ carbon tetrachloride ------.MTBE X Cadmium -'-o-=oJ,,, chlordane --· ----Chloride chlorobenz.ene --------_L Chromium ..t._a.o I chloroform --__ Copper o-cresol ----Fluoride m-cresol ------
--Iron __ p-cresol --_x_ Lead L.o.ooS cresol ----
--__ Manganese --1,4-dichlorobenzene
--~ Mercury L.o.ooo...5 --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylene ----)( Selenium L. 0-oo !:l 2,4-dinitrotoluene --1._Silver .L.. o. o5 __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parametl!r Results (PCi/1) _pH hexachlorocthane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nilrobenzene ------TOC __ pentachlorophenol --
--__ pyridine
J\1icrobiology ----tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-lrichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Date R:ceivcd Reported by --melhoxychlor
--toxaphenc
Dale Extracted Date Reported 2,~-0 --013916 JUL 29 94 2,4 ,5-TP (Silvex)
Date Analyzed Lab Number · --DI I.S Jl'Jl (Revised 2/'11)
N.c;:. Dcpar.mcnt of E:wironmcnt,
I leallh, l,.:. ~;alural Resources
Solid Waslc :--.!anagcmcnl Di,-ision
SAMPLE ANALYSIS REQUEST Slalc ubonuory of Public Hcallh
· P.O. 13ox 2S047, 306 K Wilmington Slrce:
R.tlciyi, North Carolina 2761 l
J
Site Number Field Sample Number W L-004 -~u.J _ __: _______ __;::_ _______ _ -----------------
Name of Site WA-R.i2e.J GorvT'I PC"B lr,FL Site Location A F"To iv NC.. _.!....:.__;_____:_::~:::.......-...:....:--=:..__-----------
Collected By ~ . fv I u-1.0 \... 6.c>l--J ID# 3-=/-Date Collected .2"B :fVL~ q4 Time l'tOD
I , t,U~ L. K' El<..
Agency: Hazardous Waste X Solid Waste Supcrfund TCLP Compounds --- ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
WEt..L ":1-¾4
Barium ---· X Ground water (1) Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
wl --Mercury
_ Soil (3) _ Sludge (7) SPL.lT ec.o Selenium • --Silver --_ Other (4) Other (8) :re -o~ 2.-c.;,w --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)~) Organic Compounds Results(mg/1)
P&T:GC/MS ..K._ Arsenic L..o. O I benzene ----Acid:B/N Ext. )( Barium q.08 carbon tetrachloride ------"MTBE "t( Cadmium .<:_o_ cca.. chlordane ------Chloride chlorobenzene ------X Chromium L..O.Cll chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --
--L Lead L.o. ooS cresol --
--__ Manganese --1,4-dichlorobenzeoe
--~ Mercury ~a.GOOS --1,2-dichlorocthane
--Nitrate 1, 1-dichloroethylene ----)( Selenium ~CJ.605 2,4-dinitrotoluene --_lL Silver L.c,_0'5 __ heptachlor
Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Paramelt:r Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC penlachlorophenol ----
----pyridine
i\1icrobiology ----tetrachloroethylcne
--__ trichloroethylenc
Parameter Results (Col /l00ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichiorophenol
------vin yl chloride
endrin --lindane --Date Received Reported by methoxychlor --
--toxaphene
Date Extracted Date Reported 2,4-0
013917 JUL 29 94 --
--2,4 ,5-TP (Silvcx)
Dale Analyzed Lab Number --DI IS 3191 (llcviscd 2/91)
:S:.C Dcpar:mcnl of Environment.
l l·calth, &. 1"atural Resources
Solid Waste Management Division
SAMPLE Al'\'.ALY.Sl.S .K..t.{J U.t:,::,T State Labonitory of Public Health
P.O. !>Ox 260-l7, 306 N. Wilmington Street
Raleigh, North Carolina 2761 l
Site Number -----------------F ield Sample Number W L -eo 5 -G, uJ /
l\iame of Site WA-1<i2..€:.J Gor.JT't PGt> l..I>FL Site Location A F"To ,-J NC., _.!......:._;_....:.....::::...:..::~-...:......:.-=::__-----------
Collected By a. {\) ICH.o L. 6c:>...., Date Collected Zto -:f'VL '/ 9-4 Time / 40 o
7? t,,VA Lk e-R..__
Agency: Hazardous Waste X Solid Waste ___ Su perfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
WE.LL ~4
Barium ---· L Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)~) Organic Compounds Results(mg/1)
P&T:GC/MS ~ Arsenic z6.01 benzene ----Acid:B/N Ext. ~ Barium o.oe carbon tetrachloride ----'MTBE 'Ji Cadmium ..t..o. oa.;J... chlordane ----Chloride chlorobenz.ene ------
---~ Chromium -'-0-0\ chloroform --
--__ Copper o-cresol --Fluoride rn-cresol --------Iron p-cresol ----
--__½_Lead L_o .oc.5 cresol --
--__ Manganese --1,4-dichlorobenzene
--L Mercury L.0-000~ --1,2-dich loroethane
--Nitrate 1,1-dichloroethylene -------2£_ Selenium .L....c:,, co5 --2,4-dinitrotoluene
...:£_Silver L..o,.o:S --heptachlor
Radiochemistry Sulfates hexachlorobenz.ene ----
Zinc hexach lorobutadienc ----Parameti:r Results (PCi/1) pH hcxachlorocthanc ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------TOC pentachlorophcnol ----
----pyridine
Microbiology ----tetrachlorocthylene
----trichloroethylene
Parameter Results (Coi/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
----vinyl chloride --endrin --lindane --Date Received Reported by methoxychlor --to xaphenc --Date Extracted Date Reported 2,~-D
013918 JUL 2 9 9 4 --__ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --1)1 IS Jl'Jl (llcviscd 2/91)
)':.C. Depar1ment of Environment,
i l~alth, & l'sl!ur::.I Rc.s.ou:ccs
Solid Waste Management Di,isio"
~Al',l!'Lt i\.J'iAJ....I.:>l.::i I"\..L\,lUL.J.I. ...,~-~--...,_..,',J ••• ..,., ....... --··-----....
P.O. Gox 280--0, 306 S. Wilminpon S1n:e!
Raleigh, North Carolina 2761 J
Sile Number -----------------Field Sample Number lu-L-e>O 2 -t.. C.
"iame of Sile WA-Q.i2e.J GorJN PC"B l.DFL Site Location A F"To ~ NC.. -'-------''-----------------
Collected By G. f',J 1cH.o\.,6o)-..) Date Collected # 7'l> :JVL'/ <q-4 Time I S-oo
C. s . STE"'P+-le-N
Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental· Concentrate .Comments _LArsenic <o.Q l
L Barium _o-'-\ g.__
__ Ground water (1) X Solid (5) b.JeT ~2> f:"J LL.. ± Cadmium L_ Q.Q,5
Chromium ~O-C.5
__ Surface water (2) _ Liquid (6) o.ur~ 2_Lcad O,.)d... L Mercury .£..O.,GI
Soil (3) _ Sludge (7) .:SP~tr t.ol ,E"CO -i=. Selenium <D.,Q~ --J Silver ~c::. -t!X:.>3 -~ c.. ..C:...o.c.•5
I
I _ Other (4) _ Other (8) t;,o /J ro~ ECO -----,
:r-c -£90 '?:. -LC. --. I
I --I
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results .... (mg/kg) Organic Compounds Rcsults(mg/!)
P&T:GC/MS _¼_ Arsenic ·9, ben2ene ----Acid:B/N Ex1. iBarium d,3 --carbon tetrachloride --.MTBE i Cadmium ...c(_°i.'6 chlordane ----Chloride chloroben2enc ------~ Chromium ) a. chloroform ----__ Copper o-cresol ----Fluoride m-crcsol ------Iron p-cresol ------2--Lead 35 crcsol ----
----Manganese --1,4-dichloroben2enc
--L Mercury .,c._c,_c3 1,2-d i ch loroethane --Nitrate 1, 1-dichloroethylene ----<l --..$.._ Selenium --2,4-dinitrotoluene
.JL Silver ...(._5w.8 --heptachlor
Radiochemistry Sulfates hcxachlorobcnzene ----Zinc hexachlorobutadiene ----Parameter Resu I Ls (PCi /!) pH hcxachlorocthane ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitroben2ene ! ------TOC __ penlachlorophenol I --
--__ pyridine
Microbiology ----telrach loroethylene
----trichloroethyleoc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --2, 4,6-trichlorophcnol ' ------I ------vinyl chloride I
endrin --lindane --Date Received Reported by methoxych lor --toxaphcnc --Date Ex!raclc<l Date Rep~i~S 29 2,4-0 --
I 19 JUL 94 2,4,5-TP (Si lvcx) --, Dale Anaiy-1.cd Lab Number I --1)1 IS JJ'JI (ll cviscd 2/91) I
I lcalth, t-: ;,atural H.c'-".lurccs
.so:-ic! Waste M,n.&cmcn: Di,;sion
'-''-'A .,_.,,,..._, • J f -.i',.r,J I •• •' I l<l••••r.,• ._..,, ~••, --. •
R.aici&h , Nort h Carolina c7GJ 1
Sile Number Field Sample Number vV L -C)t:J Z -.5:.D ---------='----------------------------
Name of Site WA-1<i2.e..J CoNN PC""i:, l.DFL Site Location A F -101--J N (__ --'-------'-------------------
.:2olleclcd By 6 . N r c. H.o l. 1!:>Qi-...> Dale Collected Z<a ~VL Y <t'4
/11 . Pc 1AJX>e-~~ TCLP Compounds Agency: Hazardous Waste X Solid Waste ___ Superfllild ------
Sample Type Inorganic Compounds Resuits (mg/1)
Environmental , Concentrate Comments X Arsenic <Q,O[
)( Barium _o. ::>8
6cP/&? i£.,(..) r --Ground water (1) __ Solid (5) 1-Cadmium ...(_ C • c.5 --_L Chromium 4c.a5
--Surface water (2) _ Liquid (6) ~,tU :S 77.?eA/V\. ::L_Lcad .L..O,.iO
_ Sludge (7) kJC/fl()f3C_J,c Ll££" _x:_ Mercury ~o.o\
Soil (3) X Selenium <lJ.()O.j---]( Silver .L..Q-Q;:;;i Js._ Other (4) _ Other (8) ::S,D~/T u.,/ £t::O --• .re-6>~1-:SEX> --
--Organic Chemistry Inorganic Chemistry --
Parameter Resu I ts (mg/I) Parameter Results .... (mg/kg) Organic Compounds Results(mg /1)
P&T:GC/MS L Arsenic ·<a bcni cne ----Acid:B/N Ext. ')( Barium \l, carbon tetrachloride ------'MTBE ~ Cadmium L. 9,.8 chlordane ----Chloride chlorobeniene ----~-
L Chromium .L...~-8 chloroform ----__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------_x_ Lead L... :,._q cresol ----
----Manganese --1,4-d ichlorobenzcne
--...1L Mercury L..o.o<=\ --1,2-dich lo roet hane
Nitrate 1, 1-dichloroethylcne ------'IC Selenium I 2, 4-di nit rotol uene
T --Silver ..L..9.e, __ heptachlor --Radiochemistry Sulfates hexach lorobcnz.ene ----Zinc hexach lorobu tad iene ----Parameter Results (PCi/1) pH hexachloroet h ane ----
--Gross Alrha --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
Microbiology lclrach loroet h ylcne ----trichloroethylcne ----Parameter Results (Col /lO0ml) 2, 4 ,5-trich lorophenol ----
--2, 4,6-trichJo rophcno l ----
----vinyl chloride --cndrin --li nd:rne --Date Rece ived Reported by --mclho xych!o r
--loxaphene
D:.ilc Extracted
D ale R{jfJ~ JUL 29 94 2,~-0 --2,4.5 -TP (S ilvcx) --Da le Analy1.c.:d La b Num ber --Ill IS ::il'JI (!1.cvi scd 2/91)
-
J',:.C. Dcpar:ment of Environment,
't Icalth, l:. 1'atural Resources
Solid Waste Management Di,-ision
SAMPLE A.NA.LYSl~ K.1:,(J_ U.t..'::l 1 State l.Abontory or t'ullhc Hcsi!h
P.O. l3ox ~7. 306 :--. Wilmini;ton ~trccl
luleigh, North Carolina 2761 l
Site Number -----------------Field Sample Numbcr __ W __ L_-_O_O_/ _-_S_S _____ __,1.._/_
Name of Sile WA-1<i2.€:.J CorJT':r PC."B l.DFL Site Location A F",o "-' NC.. _.::._c._....:....:::_.:...;:c._ _ ___;--=;__-----------
Collected By a. f\,) ll.HO\.., 6C))...) Date Collected '2£, :IV l-"j C2r f
L . J2~t£
Agency: Hazardous Waste X Solid Waste ___ Superfu.nd TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments L Arsenic < o. o I
~ Barium _0.-4~
__ Ground water (1) _ Solid (5) LeAc..tt~Te P~>-.}'l:> L Cadmium ~c.QS
R~v, >Jr:
1-_ Chromium L...o.o5
__ Surface water (2) _ Liquid (6) DtJrL.ET .2{_Lcad .L... C, -\0
w IEC-0
_x_ Mercury LO.Q} L Soil (3) _ Sludge (7) !5Pt-l'T" L Selenium < o.oo_r J ___!__ Silver ..,(__c.Q=i
_ Other (4) _ Other (8) rc-oo"3-:s.S --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results __ (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS X Arsenic ·<a benzene ----Acid:B /N Ext. )t Barium sei carbon tetrachloride ------MTBE ~ Cadmium .L...9.8 chlordane ----Chloride chlorobenzene --------_L_ Chromium \ ::h chloroform ----__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --_L Lead 4-d\0 cresol ----
--__ Manganese --1,4-dichlorobenzene
--~ Mercury <-o-oC\ --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylcne ----
)( Selenium I 2,4-dinitrotoluene --
...L Silver ~'9-8 __ heptachlor
Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroelhanc ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pcntachlorophenol --
--__ pyridine
Microbiology ----tetra chloroeth ylcne
--__ lrichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by --methoxychlor
__ toxaphcne
Date Extraclec..l Date RQorted '2,~-D
13921 JUL 29 94 --:?.,4,5-TP (Silvcx)
Dale Analyzed Lab Number --DI I.S 3191 (Revised 2/91)
!
I '.callh, &. 1',°alural Resources
Solid Wasle Managcmenl Di,~sion
P 0. nox ~7. 306 ~-Wilmini;,on Slrcel
RAieigh, North urolin1 276i 1
Site Number -----------------Field Sample Number WL -~D €-S:5
Name of Site WA-1<.i2e.J Cbor-JTY PC.t> l.DFL Site Location A FT'o 1'J NC -~---~---------------
Collected By G. (\J, l'..Ho I... 6::)1-,..) Date Collected ;z-:;. JULY q4 Time I'=, 15
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments ___x_ Arsenic <<?,al
}( Barium _o.~e,
__ Ground water (1) _ Solid (5) Wc~r :t;.,z:>c LI>FL .L Cadmium .L_c::, .05
_)(_ Chromium ..L.... D ~ o.5
__ Surface water (2) Liquid (6) ~eE::P 1-Lead ..t....o • \C)
X: Mercury '--0.C \ --~ Soil (3) Sludge (7) L_ Selenium < Q,. {!Xjj
_L Silver 4-C._ c5
_ Other (4) Other (8) --
--
--Organic Chemist!)' Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results----(mg/kg) Organic Compounds Resu I ts (mg/!)
P&T:GC/MS X Arsenic ol benzene ----C\j Acid:B/N Ext. X: Barium ca rbon lelrachioride ------MTBE L Cadmium L..'3 • .e, chlordane ----Chloride chlorobenz.ene ------_x__ Chromium \J.. chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ------L Lead ...t_,ao cresol --
--__ Manganese 1, 4-d ich I orobenz.ene --
--~ Mercury '-0,.Qj --1,2-d ichlo roethan e
--Nitrate 1, 1-dichlorocthylenc x ;,q --Selenium 2,4-dinit rotol uene ---1:.._ Silver .L..9J6 --heptachlor
Radiochemistry Sulfates hexachlorobenz.enc ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroeth.ane ----__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------TOC pentachlorophenol ----
--__ pyridine
i\1 icro biology l c tra chlo roet h ylcne ----
----trichloroethyleoe
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichlorophenol
--vinyl chloride ----cndrin --lindane --Date Received Reported by methoxychlor --toxaphenc --D.itc Extracted
Dale Rcof~922 JUL 29 94 2,4-D --__ '2,4,5-TP (Silvc:x)
D.ilc Anal:,.:zcd Lab Number --Di IS 3J'Jl (ltc,·iscd 2/91)
I
I i i
N.C Dcpar.mcnt o( Environment,
I !cailh, & /'.'.a,ural RGSOurccs
Solid Was:c Management Oi,ision
SAJ\1PLE A.I\'ALYSIS REQu'"EST Stale ubontory of Public Health
P.O. !3ox 2W7, 306 N. Wilmini;1on Street
R.alcigh, North 0rolin• 2761 l
Site Number -----------------Field Sampic Numbcr ___ L.V __ /.. __ -_o_D_(,_;__ __ 5_5 ____ _L_
✓ame of Site WA-R.i2e.J CoorvT't PC"E:i l.nFL Site Location A FTo J,,J -~---~---------------NC
Collected By G. fv 1cH.o \.., 6,o-....> Dale Collected ;.2.':1--JULY q4 Time /4-£"3
<;;, s :µ.S TE"PHE.
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Rcs ulls(mg/1)
Environmental Concentrate Comments X Arsenic ( ot!.al
X Barium _c.""\o
__ Ground waler (1) _ Solid (5) 6-t211) 14-3 x Cadmium L..o-0.5 x Chromium "'-0 -D!:i A,R. 111:A.Jr --__ Surface waler (2) _ Liquid (6) _K__ Lead .L..0 .. 10
._X_ Mercury <-Q.c,\
_){_ Soil (3) _ Sludge (7) ~LIT (_L,)L e:-c.o L Selenium <o.aDJ-
X: Silver L...o!J!.o:S
_ Other (4) _ Other (8) -1. C. -DOl-$S --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Para meter Resul 1s111 #)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS X Arsenic <9-. benzene ----Acid:B/N Ext. X Barium J:h. carbon tetrachloride ------"MTBE L Cadmium -Z'.9.8 chlordane ----Chloride chlorobenzene ------___K_ Chromium \ lg chloroform ----__ Copper o-crcsol ----Fluoride m-crcsol ------
--Iron __ p-crcsol --_&_Lead .L...;).D cresol ----
----Manganese --1,4-dichlorobenzcoe
--~ Mercury '-c,o'.:j 1,2-dichlorocthane --
---Nitrate 1, 1-dichloroethylcne
7 <t --Selenium 2,4-dinitrotolucne
T --Silver -'-°'-8 __ heptachlor
Radiochemistry Sulfates hexachlorobenzcne ----
Zinc hcxachlorobutadicnc ----Parameter Resu I ts (PCi /!) pH hexachlorocthanc ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------TOC pcntachlorophcnol ----
----pyridine
Microbiology ----te trachloroeth ylcne
trichloroethylenc ----Parameter Results (Col/l00ml) 2,4,5-trichlorophcnol ----
--2, 4,6-trichlorophenol ----
------vinyl chloride
cndrin --lindane --Dale Received Reported by --methoxychlor
__ toxaphene
D.ilc Extracted Date Reoorled ?.,4-D
013923 JUL 29 94 --__ 2,4,5-TP (S ilvex)
Date Analyzed Lab Number --DI IS J!'Jl (H.cviscd 2/91)
STATE LABORATORY OF PUBLIC HEAL TH
WARREN COUNTY PCB LANDFILL
ORGANICS AND INORGANICS
LAB NOS. 942748 -942829
I lca!th, & t--:atur•I Resource,
Sol id W aste Manai;cmcnt Oi,~sion
~Jr)._llJ..J. J... .. :J..-' £),,.._,_ \r:,....J....,,l ..l.. V .L LJ A'-.-'--_.'-(.._,,.,___,._) ,L. .. , ........... .-..,,.....,, _,...,. J ..., .............. , •.••...•.
P.O . Gox 260-17, 306 1'. Wilrr.in[;lon Street
Raleigh, North G rolin• 27611
Sit e Number -----------------F ield Sam pk Numbcr_~W-=-L=---_O_D__:./_-_S=---=:3=,=--------
Name of Site WA-R.i2..E:.J Got0T'7' PC.:6 l.DFL Site Location A F,o 10 NC -~..:._....:....:::....:.:::c..__..:.....c--==-------------
Dale Collected 2£ :.1l) L 'Y a, 4-Time D'B'3:f-
j,.. e.#~c
Agency: Haz.ardous Waste X Solid Waste ___ Superfund TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
LeAl-tt 11-n P~>-.)i:> ---·
__ Ground water (1) _ Solid (5) Cadmium --
Chromium
R-'t-v, >v e --
__ Surface water (2) _ Liquid (6) 01)rLET Lead --
wlEc..O --Mercury x Soil (3) _ Sludge (7) SPL-IT Selenium --1 --Silver
rC•003-SS --
_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1)
P&T:GC/MS Arsen.ic benz.ene ------L Acid:B/N Ext. Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------Chloride chlorobenz.ene ----~-
Chromium chloroform ------
--· __ Copper o-cresol --
Fluoride m-cresol ------Iron p-cresol ------
Lead cresol ------
---__ Manganese 1,4-dichlorobenz.ene --
--__ Mercury 1,2-dich loroethane --Nitrate 1, 1-dich lorocthylene ------Selenium 2,4-di n itrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a chlorobenzene ----
Zinc hex a ch I orobu lad iene ----Parameter Results (PCi/1) pH hexachloroelh a ne ----Gross Alrha ----Conductivity __ methyl ethyl ketone
(Jross Beta TDS nitrobenz.e ne ·------
TOC __ pentachlo rophcn ol --pyr idi ne ----J'\1icrobiology ----lelr ach l oroelh yl en e
trichloroethylcnc ----Parameter Results (Col/lO0ml) 2,4,5-l rich lorophcnol ----
----__ 2,4,6-trichJorophenol
--vinyl chloride ----endrin --
lindane
Date Recei ved 7 -,;;lf-~dJ}Keporte d by
--methoxychlor ---
Dille Extracted ~-5-<j_'j_ 5/tL/lt?J
__ toxa phene
D ate R epo rted --2,4-D
I __ 2,4 ,5-TP (Silvex)
Dale A nalyLcci!L:f-9'-f B fl. 942749 Lab Number --l)J IS 31 '}1 (!,cviscd 2/91)
'--Jl"),.J,l..l.l A..J.k.-' ~..._..,~~.A..._.,.,.._,.,............,'-(_'-".,._..__...,,,_ _____ ,,_ ..__...,...,,.,_.,.,.J -· .
I lea Ith, & 0atural Resources
Solid Waste Ma na&ement Division
Site Number -----------------
P.O . Gox 280J7, 306 !',;. Wilminb'10n Street
Raleigh, North Carolin• 27611
Field Sample Nurnbcr _ _.::..W..::......._L_-_O_O_I_-_S_::; ______ _
Name of Sile WA-R.i2.E:.J GorvT'l' PC.t:> U,FL Site Location A F",o ,-J NC -.!.....'..-'----...:..-=::__:_::::......... _ ___;-=:;__-----------
Collected By 6. fv 1<'.'..HOl,60)..J ID# 371--Dale Collected 2'6 ::JULY <2r 1-
L. Rose
Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ---·--
Sample Type Inorganic Compounds Resulls(mg/1)
Enviro11mentt1l Concentrate Comments Arsenic --
Barium
LeAc..tt 1rn P~i-.)i:> ---·
__ Ground waler (1) _ Solid (5) Cadmium --Chromium R-'rv, >ve --
__ Surface waler (2) _ Liquid (6) OtJrL.ET Lead --
w/Ec..O --Mercury x Soil (3) Sludge (7) :5PL-IT Selenium --I --Silver
rc ... 00::1-ss --
Other (4) _ Other (8) ----
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ----
·~
Cadmium chlordane
~ 6 PEST-<t:1.-/d~ --
Chloride chlorobenzene .. ~-
Chromium chloroform ------__ Copper o-cresol ----
Fluoride m-creso l ------
--Iron p-cresol ----
Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroclhanc
--Nitrate 1, 1-di ch loroethylcnc ----
Selenium 2,4-di nit rotolucnc ----
Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobcnzenc ----
Zinc hexach lorobul adicne ----Parameter Results (PCi/I) pH hex;,chloroel hane ----__ Gross Alpha --Conductivity m ethyl e thyl keton::, --Gross Beta TDS nitrobcnzene ------TOC pcntachlorophcnol ----
--__ pyridine
Microbiology ----l etra chloroet h yl enc
--__ trichlorocthylenc
Parameter Results (Col/l00ml) 2,4,5-l rich loropknol ----
------2, 4,6-trichJorophcnol
----vinyl chlo ride --endrin --lin d:rne
Date Rcceivcd 7:3f-f¥--Jlt 1/2) Reported by
--
--mcthoxychlor
Date Extracted ,Y-;;?-?',!__1//J --toxaphenc
Date Reported --2,4-D
Dc1tc Analyn:d Y,-4L-'l__¥1/P 942750 __ 2,4,5 -TP (Silvcx)
Lab N umber --1)1 IS 31')1 (1,cviscd 2/91 )
r-,.:.C Depanment of Environment,
I lcalth, & l','.atural Resources
Solid Waste Manai;cment Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
Site Number ----------------
. P.O. lklx 2S0-17, 306 N. Wilmin!,'.lon Street
Raleigh, North urolin• 27611
Field Sample Number W L -0 0 Z -SS
Name of Site WA-1<.i:2.€:.J Cbor.JT't PC-"B l.DFL Site Location A F"To ,-J NC., -~-..c....;::.-'-"'--_.;_-=-----------
Collected By a. f\) 1u-1.0L6C>"-' Time 0Gf 2 0
t 12 . DSt:=
Agency: Hazardous Waste X --Solid Waste ___ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium ----
L '° A-u-, "'1't __ Ground water (1) _ Solid (5) fb...s::r, Cadmium --Chromium --_ Liquid (6) IJ~Ae 0vrFALL Surface water (2) Lead --Mercury --£ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------<d ./d#AL, ..LL PCS Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --__ Mercury 1,2-dich loroethane --
--Nitrate __ 1,1-dichloroethylene --Selenium 2, 4-di ni trotol uene ----Silver __ heptachlor --Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hcxachlorocthanc --__ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobe.nzcne ------TOC __ pentachlorophcnol --
----p)'ridinc
Microbiology ----tetrachloroethylcne
trichloroethylene ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichl orophcnol
----vinyl chlori de --endrin --lindanc
Date Received 7-:l/-~ ci1JReported by --
--meth oxychlor
7 -
D.ile ExtractccJ ~~-?¥1//J --toxaphcne
Date Reported --2,4-D
Dale Anal yzed ?-~-9{/-p'~ 942751 _ 2,4 ,5-TP (Silvex)
Lab Number --1)1 IS 3191 (Revised 2/91)
~.C Dcpanment of Environment,
I lcalth, & 1'atural Rcs.ources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Lat>oratory of Public Health
P.O. nox ~7. 306 K Wilming10n Street
Raleigh, Nonh Carolina 27611
Site Number Field Sample Number IAJ 1..-DO 3 -SS -----------------
Name of Site WA-R.i2e.J GarvTY PGt!:> U,FL Site Location A F"To ,-J NC... _.:.......;__....:.....::--'-':;__ _ ____.:.-='------------
Collected By ~ . fv , LHo L. 6cn•-.l Dale Collected Zf3 :TVL.. Y 9 4 Time CJC/3o
J,.. • /2t)SE_
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Cor.1pounds Rcsulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· LEACH If-TE Ground water (1) _ Solid (5) tpA)J:::> Cadmium --Chromium --__ Surface water (2) _ Liquid (6) M ,r,-r:>1.t!!: Lead --Mercury --L Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/l)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane --PC.B(L~J o, 53~ ----x_ Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --
--Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-di ni trotol uene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadi ene ----Parameter Results (PCi/1) pH hcxachlorocthane ----__ G ross A lpha __ Conductivity meth yl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC pcntachlorophcnol ----
----pyridine
l\1icro biology ----telr achloroclh ylene
--__ trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichl orophcnol
----vin yl chloride --endrin --lindane
7 -~'f-f.¥1/,f&Jz e ported by
--Date R eceived mcthoxych lor --
S"--2-?.Y-YP
__ loxaphene
O;i te Extracted Date Report ed 2,4-D --
T -~-?fr///-1 942752 __ 2,4,5-TP (S i!vex)
Dat e Analyzed Lab Number --DI IS Jl'Jl (l~cviscd 2/91 )
N.C Depar.ment of Environment,
1 lcallh, &. Natural Rewurces
Solid Waste Management Division
SAlviPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 280-l7, 306 N. Wilmington Stn:et
RAieigh, North Carolina 27611
Site Number Field Sample Number IA.J t. -0 04 -$.S ----------------
Name of Site WA-R.i2.€:.J GorvT"t PC."B u,FL Site Location A F",o ,v NC _..,_;__.....:....::::....:...:,c__ _ ___;c.......=::.._.... _________ _
Collected By a. fv ,u-to l-6c,)J ID# :3-=t-DateColiected Z~ -::7VL.Y t:14-Time ~C/30
J,.. eo5e
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
1,IFACHH~
----__ Ground water (1) _ Solid (5) Pe>~]:> Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Ar 17t-Ti?/?. Ot,JTFAI..L Lead --Mercury --_x_ Soil (3) _ Sludge (7) Selenium --Silver --
--Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride
--MTBE ----Cadmium chlordane
,< Pc..Be~t-PJ l,IS'~hl ----Chloride chlorobenzene --~-,-Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichlorocthane
Nitrate -1, 1-di chloroethylcne ------Selenium 2,4-dinitrotolucne ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch l orobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
--__ pyridine
Microbiology ----tetrachloroeth ylene
----trichloroethylene
Parameter Results (Col/lO0ml) 2, 4 ,5 -trich lorophenol ----
------2, 4,6-trichlorophenol
------vinyl chloride --endrin --lindane
Date Received ;'-,2'1-99:'tg'a2R.eported by --
--methoxychlor
~-dl.-9W/' --toxaphene
Dale Extracted Date Reported 2,4-D --
Date AnalyLcd ~-f'-fL/J/'P 942753
_ 2,4,5-TP (S il vex)
Lab Number --DI IS Jl'Jl (Revised 2/91)
N.C Depar.ment of Environment,
I Jcalth, & Natural Resources
Solid Waste Management Di,~sion
S~1PLE ANALYSIS REQUEST State Laboratory of Public Health
Site Number ----------------
P.O. Box 280-l7, 306 N. Wilmington Stree t
Raleigh, North urolina 27611
Field Sample Num ber WL -tJo€-S:5
Name of Site WA-R.i2.tiJ C1arJTY PG"B u,FL Site Location A F'To ,v NL _..<.....:._....:....::c....:....::~-__:.-='------------
Collected By a . f\,) I l.H.O L 6C)),.,.) Date Collected 2, 1--.JV L->' q 4 Time I '-, I 5"
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) Wc:~r :5 ,z:,e-1..r:>FL Cadmium --Chromium --__ Surface water (2) Liquid (6) :5E:c:P Lead --
--M ercury
_K Soil (3) _ Sludge (7) Selenium --Silve r --
_ O ther (4) _ Other (8) --
--
--
Organic Chemist11' Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
L P&T:GC/MS Arsenic benzene ----A cid:B/N Ext. Barium carbon tetrachloride ------'MTBE · Cadmium chlordane ------Chloride chlorobenzene ----~
Chromium chloroform ------__ Copper o-cresol ----Fluoride m -cresol ------
--Iron p-cresol ----Lead cresol ------
--__ M anganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
Nitrate -1, 1-dichloroethylene ------
Selenium 2,4-din it rotol uene ----Silver heptachl or ----Ra diochemistry Sulfates hexachlorobenzene ----· Zinc hexachlo robut adiene ----Parameter Results (PCi/1) pH hexachl oroethane ----
--Gross Alp ha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC penta chl orophenol ----
----pyridine
J\1icrobiology ---------tetra chloroethyl ene
trichloroeth ylene ----Para meter Res ults (Col /l00ml) 2,4,5-trichlorophcnol --
----__ 2,4,6-trichJo rophenol
------vinyl chlori de
endrin --lindane
Date Receive d 7-$-ff/11/;@ Reported by
--
--methoxychlo r
--toxaphcnc
Dille E xtracted Date Reported 2,4-D --
i-5-9~ n1j r 942754 __ 2,4,5 -TP (Si lvex)
Dille Analyzed Lab Number --DI IS 3191 (IZcviscd 2/91)
;--:.C. Depar.ment of Environment,
I lcaith, & ~atural Rcs.ources
Solid Waste Management Di,~sion
.'::>A.MJ-' Lt, Al'\ALl :::,1~ K.t,I...!_ Ut~ 1 .:-.tatc LM C>on.tory 01 r·uo11c ttC!iltn
l'.0. 11ox 2SO-:,, 306 N. Wilmington Street
Raleigh, North Cuolin• :!761 l
Site Number -----------------Field Sample Number WL -~O 5 ... .S~
Name of Site WA-R.i2.e.J Cbor.JTY Pc,1!:, l.DFL Site Location A F",o ,__; NC _.:_:_ _ __:_::_;_=----c.....:::;c__ __________ _
Collected By b. (\J 1c.Ho\..6o~ ID# 3 =?-Date Collected ,Z 1-;JULY q4 Time I~ I 5
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) _ Solid (5) w~~r :!!,,Pc Lr>FL Cadmium --Chromium --
__ Surface water (2) Liquid (6) ~ec:P Lead --Mercury --_K_ Soil (3) Sludge (7) Selenium --Silver --
_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/1 )
P&T:GC/MS Arsenic benzene ----_x_ Acid:B/N Ext. Barium carbon tetrachloride ----
"MTBE · Cadmium chlordane ------
Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --
Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
----Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-d ichloroethane --
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rot ol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
Zinc hexach I orobutad ienc ----Parameti:r Results (PCi/1) pH hcxachloroethanc ----
--Gross Alpha __ Conductivity --meth yl ethyl ketone
Gross Beta TDS nitrobcnzene ------
TOC pcntachlorophenol ----
----pyridine
Microbiology ----tetra chlorocth ylcnc
trichloroethylcnc ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichlorophenol
----\~nyl chl orid e --endrin --lind:rnc
Date Received 7-,,;?f'-f?'~l'/ZJP-eportcd by
--
--mcthoxych lor
z.-~ --1191/A:6 --toxaphene
OJlc Extracted Dale Reported 2,4-D
7 --
</-R-9L/ t3ll 942755 __ 2,4,5-TP (S il vex)
D<1tc Analy-Lcd Lab Number --1)1 IS 31')1 (IZcviscd 2/91)
;-.;.C. Dcpar.mcnl of Environment,
l lcal1h, & j',:a1ural Rc.wurces
Solid Was1c Management Di,~sion
0A1Ylt' L.C, f\...l 'if-U..,1 .:> l.::> .tu:.,'-.,'. UCO .l .,_l!.4!."--L..AVVl AlV l ; v, < .,.V II'-I>'-"''''
l'.O. fk>x ~7. 31)6 ,,-,;_ Wilming-ton S1rcc1
Raleigh, North Carolina 2761 l
Site Number Field Sample Number W L -OD C-S:5
Name of Site WA-Q.i2e..J C1or..:iT'i PCB l.DFL Si te Location A F"To 10 NC _.!......:. _ _:_::::.._:_:"------'-='-------------
Collected By a. f\) I CHO l-6C>'-' Date Collected 2-1-JVL->' q4 Time I'=, I 5
Agency: Hazardous Waste X Solid Waste Superf1111d TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments / a,,Jf.tl Arsenic --Barium ---·
__ Ground water (1) Solid (5) Wc:t;,r :6 , PE LX>FL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) ::5ec:P Lead --Mercury --X_ Soil (3) Sludge (7) Selenium --Si lver --
--Other (4) --Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------
-~
· Cadmium chlordane ----Chloride chlorobenzene ~ ~ft?T <,:,, IP LUl-'M. --~-,, Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m-cresol ------
·-Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4 -dichlo robenzeoe --
--__ Mercury 1,2-d ichloroethane --Nitrate -1,1-dichloroethylene ------Selenium 2,4-dini t rot oluene ----Silver heptachlor ----
Radiochemistry Sulfates hexach lorobenzene ----Zinc hex a ch I orob u tad ien e ----Para meter Res ults (PCi/1) pH hexachloroethane ----
--· Gross Alpha __ Conductivity methyl ethyl ketone --Ciross Beta TDS nitr obcn7_cne ------T OC pentachlorophcnol ----
----pyridine
Microbiology ----tetra chloroet h ylen e
----trichloroethylcne
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophenol
--\~n yl ch loride ----endrin --lin dane
Date Received 7 -al'f-f~/J' ~eported by --methoxychlor
7 --
8:-t2-9 t/1/I' --toxaphene
D;ilc Extract ed Date Reported 2,4-D --
Date ;-\nc.tlyzcd 2-:::_5!_-9¢'1/,f) _ Lab Number 942756
__ 2:1 ,5-TP (Silvcx)
--DI IS Ji'Jl (IZcviscd 2/91)
N.C Depanment or Environment,
I lcalth, & J\'.atura\ Rewurces
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
P.O. Box 280-17, 306 N. Wilmingion Street
Raleigh, North Carolina 2761 1
Site Number Field Sample Number lVt. -oo b-.S5 ---------------------------------
Name of Site WA-R.i2-e.J GorJT1 PG'B u,FL Site Location A FTo t-.J NC.... _..c.....:.~....:....:::.....:..::,c___....:.....::_:::::::...._ _________ _
Collected By a. f\) l(.HOL,6c:)l--> ID# 3-=t-Date Collected ;2.?-::fVL-Y CJ4 Time /4-£:'3
c;. · ~TEPHEUS
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium
6-e11> 14-3 ---· Ground water (1) Solid (5) Cadmium --Chromium
A IR. l/G"A.J-r --__ Surface water (2) Liquid (6) Lead --
--Mercury
.1{_ Soil (3) Sludge (7) ~LIT LL>/ €-CO Selenium --Silver --_ Other (4) :re.-_ Other (8) C>Ol-$S --
--
--Organic Chemistry Inorganic Chemistry --
' Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
...L P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
-Nitrate 1, 1-dichloroethylene ------Selenium 2,4-dinitrotoluene ----Silver heptachlo r ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroeth ane ----
--Gross A lpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
Microbiology ----tetrachlorocthylcne
----trichloroethylenc
Parameter Results (Col/lO0ml) 2,4,5-trichlorophcnol --
----__ 2,4,6-trichJ orophcnol
------vinyl chl oride
endrin --lindane
Date Received 7-:Z.,.f i'7(,P~Rcport ed by --
--meth oxychlor
toxaphene --Date Extracted Date R eported 2,4-D --
Date Analyzed 9-6-9"-J 111.AJ 942757 _ 2,4,5-TP (Silvex)
Lab Number
I)\ IS 3191 (Revised 2/91) --
N.C Dcpar.mcnl o( Environment,
1 lcalth, & 1'atur.l Re.sources
Solid Waste Management Division
SA1'.1PL£ ANALYSIS REQlTEST Stale u bon.tory o( Public l-lc•lth
· P.O. Box 280-17, 306 N. Wilming10n Street
Raleigh, North Carolin• 27611
Site Number Field Sample Number UJL. -OD b -.SS ----'-----=----=---'-=--------------------------
Name of Site WA-R.i2.e.J CorJTY Pc,r:, lr,FL Site Location A F,o ,-J NC -~__:__:_:::....:...:"'-... _ _:_:......::::...._ __________ _
Collected By a. f\) IC.HOL,6c)~ ID# 3-=f--Dale Collected ;;z=,. J(.}L'Y q4 Time /4-£°3
. ~Te'PH €-.J G;: ~
Agency: Hazardous Waste X Sol.id Waste Superfund TCLP Compounds --------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
(it211) 14-3 ---· __ Ground water (1) Solid (5) Cadmium --Chromium A,R IIEJJT
--__ Surface water (2) _ Liquid (6) Lead --
--Mercury
){_ Soil (3) Sludge. (7) ~LIT ~Jcco Selenium ----Silver --Other (4) _ Other (8) :re. .. OC>l-SS ----
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul ls (mg/1) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ----__x_ Acid:B/N Ext. Barium carbon tetrachloride ----"MTBE Cadmium chlordane ------Chloride. chlorobenz.ene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron p-cresol ------Lead cresol ------
--__ Manganese --1, 4-dichlorobenz.ene
--__ Mercury --1,2-dich loroethane
-Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-dini t rotol uene ----Silver heptachlor ----Radiochemistry Sulfates hcxachlo robe.nz.ene ----Zinc hex a ch I orobu tad i en e ----Parameter Results (PCi/1) pH hcxachlo roethane ----
--Gross Alpha --Conductivity --methyl eth yl keton e
Gross Beta TDS nitrobcnz.e ne ------TOC penlachlorophenol ----
----pyridine
Microbiology ----t elrachloroeth ylcne
----trichloroethylcne
Parameter Results (Col/l00ml) 2,4,5-trichlorophcnol ----
------2, 4,6-tri chJ orophen ol
------vin yl chloride
endrin --lind ;rne
Date Rcccived 7-,29-9'/Y~eportcd by --
--methoxychlor
~di-!~ --toxaphenc
Date Extracted $-£-j<-f Date Reported --2,4 -D
I __ 2,4,5-T P (Silvex)
Dale Analyzed g;-f-2'+ ~d) · 942758 Lab Number --I)! IS Jl'Jl (!Zcviscd ../91) I I
;-,:.C. Dcpar.ment of Environment,
l lcalth, & 1','atura l Rcwurces
Solid Waste Management Di,~sion
SA..MPLE ANALYSIS REQUEST State Labontory of Public Health
P.O. !kn 2S0-17, 306 N. Wilmini;,on S1rcc:
R..alcigh, North Carolina 2761 i
Site Number -----------------Field Sample Num bcr __ _:lV __ ~_---=-C>_CJ_b=----=-S_S _____ _
Name of Site W A-R.i2-e.J GorvTY PCB U>FL Si te Location A FTo ,.J NC --'---'--_:_:::.....:...:,c___---'---'C---"===-------------
Collected By G. f\) u:.Ho L, 6c:,)....) ID# 3-+ Date Collected ~ ":?-7 V LY C/4 Time / 4-£; 3
H Gz 'STEP a-.,!=-
Agency: Hazardous Waste X Soud Waste Superfund TCLP Compounds --------
Sample Type Inorganic Compounds Rcsulls(mg/1)
Environmcnt;il Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) Solid (5) G-t21l) 14-3 Cadmium --
Chromiu m A-, 12!... 1/eAJT --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
_){_ Soil (3) _ Sludge (7) .;;;:,pLIT t..u/ t:CO Selenium --
Silver --
_ Other (4) _ Other (8) :re.-DOI-SS --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Resulls(mg/1) Parameter Results (mg/!) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsen.ic benzene ------Acid:B/N fat. Barium carbon tetrachloride ------
-~
Cadmium chlordane ----_x_ ~VFE~T< C1, /IJ /?/JA Chloride chlorobenzene --~-
Chromillill chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1, 4-d ichl orobenzene
--__ Mercury --1,2-di chloroethane
· N it rate 1, 1-dichloroethylene ------
Selenium 2,4-din i trotol uene ----
Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
Z inc hexachlorobutadiene ----Pa rameter Results (PCi/1) pH hexachloroelhane ----
--Gross Alpha __ Conductivity methyl ethyl ketone --Gross Bela TDS nitrobenzene ------TOC pentachlorophe nol ----
----pyridine
Microbiology ----tetra chloroet hylcne,
trichloroethylcnc ----Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichl o rophenol
------vin yl chlori de
endrin --lind;rne
Date Received 7-.;;??-fp!V<&J?.-eportcd by --
--methoxychlor
'tf'-~-f$?1//J Dale Report ed
--toxaphene
Date Extracted 2,4-D --
?-//-9{/-yp 942759
_ 2,4,5-TP (S:lve-x)
Dulc A nalyzed Lab Number --l)I IS J l'Jl (l\cviscd 2/91)
/',:.C. Uepar.mcnt ol 1:.nVJronmcnt.
l lcalth, & r---:atural Resources
Solid Waste Management Di,ision
Site Number -----------------
..)LALC L-KLXJr».iury Ul ruv11c nc11H n
r.o. !}ox 2S047, 305 N. Wilmin&lOn Strcel
RB\cigh, North C..rolin• 2761 l
Field Sample Number W L -t) tJ "i--:SS _______ ....;:__:..........=--------
Name of.Site WA-Ri2.E:..J ~orJTY PGb U)FL Site Location A F"10 ,.J NC --'---'----'---=;_.:...;"------'--=:..__-----------
Collected By a. f'v ,u--t.o \... 6o"-' Date Collected J.. ?-J () LY 9+ Time /5 J z_
c;. ,-..>'S. · $T«cP-f1 e
Agency: Hazardous Waste X ---Solid Waste ___ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
13-l ---· __ Ground water (1) _ Solid (5) 6f<!tD Cadmium --Chromium
A-112 1/cAJT --__ Surface water (2) _ Liquid (6) Lead --Mercury --_lf_ Soil (3) Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --I
--' --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
~ Pc& <O./t'#11L Chloride chlorobenz.ene ----Chromium chloroform -· ----
--__ Copper o-crcsol --
Fluoride m-creso! ------
--Iron p-crcsol ----Lead cresol ------
----Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --Nitrate 1, 1-dichloroethylene ------
Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Su If ales hcx.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha --Conductivity --me thyl ethyl ketone
Gross Beta TDS nitrobenz.ene ------
TOC pentachlorophcnol ----
----pyridine
Microbiology ----t etrachloroet hylene
trichloroethylenc ----P;iramcter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
----__ vinyl chloride
endrin --
7 -~f-f&tfd.LJ
lind:rne
Date Received --
Reported by methoxychlor ---
Y-;?--9#1//J --toxaphene
Dale Ext racted Date Reported 2,4-D --
'1r-s/-9<,t-VP 942760
__ 2,4 ,5 -TP (Silvex)
Dale Anct!yzcd Lab Number
DI IS ]!'JI (H.cviscd 2/91) --
r--;.C. Dcpar.mcnl o [ Environment,
I lcalth, & Natural Rc.s.ources
Solid Waslc Management Division
.'.:>ANlt' Lt, A.NALl .'.:>l.) Kcl...,l UL.) 1 St>lc l.J<t>on.tory-o( Public H u lt h
P.O. Box 2SO-l7, 306 N. Wilmini;ton Slr\:cl
R.alcigh, North C.Arolina 27611
Sit e N umber Field Sample Number WL -t) [) ~ -~ 5 -----------------------------------
Name of.Site WA-R.i2.t..J Go,,J"N PGt> l.DFL Site Location A F-ro-,..J NC _ _,___;__......:....:=-..:..::c__ __ :........=::..._ __________ _
Collected By G;. fv re.Ho L.. 6:::))-...) Date Collected :Fr JOLY 9+
~ $, "Sa. Tt;? +-, E...:)
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) (al<l!) II-z. Cadmium --Chromium A,R 1/eJJ, --__ Surface water (2) _ Liquid (6) Lead --
--M ercury
~ Soil (3) Sludge (7) Selenium --Silver --
_ O ther (4) _ Other (8) --'
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
-1L PG& <t:7,/'WA(_ Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylene ----
Selenium 2,4-dinitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobcnzene ----Zinc hexach I orobu tad iene ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross A lpha --Conducti vity --methyl eth yl ketone
Gross Beta TDS nitrobenzene ------TOC pcntachlorophcnol ----
----pyridine
Microbiology ----tetr achloroet h ylene
trichloroeth ylene ----Parameter Results (Col/l0Oml) 2,4 ,5-trich I orophenol ----
------2, 4,6-trichJ orophcnol
------vinyl chloride
endrin --
7 -,:2f--f"if 1(f, Li'l)R e ported by
lind:rne
Date Received --rnelhoxychlor --
~--l-?L/-v~ --toxaphcnc
Dale Extracted Dale Reported 2,4-D --
Y-¥-91/-Y/J 942761 __ 2,4,5-TP (S ilvex)
Dale Analyzed Lab Number --DI IS Jl'Jl (Revised 2/91)
·-
J'.'.L Ucpar,mcnl or 1:..."lvuonmcnt,
l leallh, &: Natural Resources
Solid Waste Managcmcnl Di,~sion
Sile Number ------------------
..)lAlC. L.AVVJAi.'Jl/ UL j UUIIL Jll..l'l\il
P.O. 13o~ 2SO-l7, 306 N. Wilmi1'!;1Dn Str::cl
Raleigh, North C.rolin• 2761 l
Field Sam pie N um bcr_-'W=----_L._-_O_CJ.::__~-=----_$_5=----------
Name of Site WA-1<i2E:.J CborJT1 PCB l.DFL Site Location A F,o ,-J NC _-'----'.. _ __:_::::__:_::,c__ _ ___:c......=::.._ __________ _
Collected By 6. fv ,u-1.0 L. 6c:>"-' Date Collected J.. 1-JV LY 9 + Time /SZ.o
<:. . $'T£PH f:t,..)'S
Agency: Hazardous Waste >( Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) 61<1D /l)-1 Cadmium --
(/E)..)T
Chromium A,R --__ Surface water (2) _ Liquid (6) Lead --Mercury --~ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --I
--.•
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/!)
P&T:GC/MS Arsenic ben2ene ------
Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------<P,/t?#n'L ..1'L Pc.,.B, Chloride chloroben2ene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
---Iron p-cresol ------Lead cresol ------
--__ Manganese --1, 4-d ichl orobenzen e
--__ Mercury --1,2-dichloroethane
--Nitrate 1,1-dichloroethylcnc ----Selenium 2,4-dinitrotol uene ----Silver hcptachlor ----Radiochemistry Sulfates hex,ichlorobenzene ----Zinc hexach lorobutadiene ----Parameter Results (PCi/1) pH hex.achlo roethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitroben2cne ------TOC pentachlorophenol ----
----pyridine
Microbiology ----tetrachloroethylene
----trichloroethylene
Pc1ramcter Results (Col/lO0ml) 2, 4 ,5-t rich I orophen ol ----
----2, 4,6-trichlorophenol --
----vinyl chloride --endrin --lindane
Date Received 1-~'1~f tf t//! t3l) Reported by --
--methoxychlor .,, tox aphcnc ?-;i-?$1'-w:, --D;ite Extracted Date Reported ?,4-D --
'9'-¢-9¢1/~ 942762
__ 2,4,5-TP (Silvex)
Dol e Analyzed Lab Number
I)! IS Jl'JI (Revised 2/91) --
~,:. C. Uc par. rnc n t ot 1:.nvuon n\c n L
1 lcalth, /,: ~~atural Rc.s.ourcc<
Solid Waste Management Di,~sion
.:lf-1..JY!r L.C, J-U'(f\.J...,l ~.1.0 J:\.J.:.,~ UL.:l .I. ~UllC LJll>Or&lOI)' 0 { IUOIJC l"1C!ll0
P.O. llox 280-n, 306 N. Wilmini;,on Street
Raleigh, North Carolina '7cil 1
Site Number Fie.id Sample Number WL. -0 I I!> -SS. -----------------------------------
Name of Site WA-1<.i2.e.J GarST'I PG°"B l.DFL Si te Location A F.;.-o ,.J NC --'-"-_;_;:_:_::c._. __ __c=ce-__________ _
Collected By G. (\J 1c.H.ol,60)-) Date Collected J.1-JO LY 9+ Time IG'Z4
~ . STb-P "°' E\.JS,
Agency: Hazardous Waste X Sol.id Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground waler (1) Sol.id (5) (al<tD '1-Z. Cadmium --Chromium
A-11< 11,;;-AJ T --__ Surface water (2) _ Liquid (6) Lead --Mercury --X. Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --I
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul Ls (mg/I) (mg/kg) Organic Compounds Results (mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
L Pc,,& <~-/tl#M._ Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d i ch 1 oroeth ane
Nitrate 1, 1-dichloroethylene ------
Selenium 2,4-dini trotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----tetra ch loroet hylcne
trichloroethylene ----Parameter Results (Col/l00ml) __ 2,4 ,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
------vi nyl ch loride
endrin --
Da te Received 7~ ,d1 -f°it,//.1Lll) Reported by
lindane --
--methoxychlor
_;,, toxaphene
D;itc Extracted 51--2.. -9//"'/l)J --Dale Reported --2,4-D
DcJl c Analyzed ~-1/-91/1/,P · 942763 __ 2,4 ,5-TP (Silvex)
Lab Number --1)1 IS 31'!! (ltcviscd 2/91)
i\.C. Ucpanmcnl ol l:,nvuonmcnt,
I lcalth, & Natur.d Rcs.ourcr.s
Solid Waste Management Di,isior.
uiU\'l.1L!c, Al'<ALJ.010 L'.L\.,l_UL.:>1 .:>UllC uoora1ory Oi IUOIIC fiC!Hn
· P.O. !)ox 2SO--l7, 306 N. Wilmin&1on S1n:c1
RAieigh, North C.rolin• 2761 I
Sile Number FiddSamplcNumber WL-t)//-~S -----------------------------------
Nameof.SiteWA-R.i2.t..J GorJT'i PCb l.I,FL SiteLocation AF"Tot-J NC --'-'-_:_::~:,c_ __ :__:=;:.._ __________ _
Collected By b . (\) 1 £'..Ho L 6c::))....) Date Collected J.. ':I-'JO LY 9+
~ s Tli:;:>t-t~"S:.
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental· Concentrate Comments Arsenic --Barium ---· __ Ground water (1) . Solid (5) 6f<t!) q-3 Cadmium --
A ,,2
Chromium
1/,;;a,.JT --__ Surface water (2) Liquid (6) Lead --
--Mercury
_£ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride
-.MTBE ----Cadmium chlordane ------<e7,/4#/K_ _2L_ Pc,& Chloride chlorobenzene --~-
Ch1omium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --
--Nitrate 1,1-dichloroethylcne ----Selenium 2,4 -dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene -----· Zinc hexachlorobutadiene ----Parameter Resu I ts (PCi/1) pH hexachloroethanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnzene ------TOC pcntachlorophenol ----
--__ pyridine
Microbiology tetrachloroe th ylene ----
----trichl oroethylenc
Parameter Results (Col/l0Oml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-trichJorophcnol --
----vinyl ch loride --endrin --
Dale Received 7-,2 9-Wv/ ~eported by
lindanc --
--methoxychlor _,
Dille Extracted 2_-~-~"J;I!!._ --toxaphcne
Date Reported --2,4-0
"i?-5-9¢-v,,o 942764
_ 2,4,5-TP (Si lvex)
DJ!e Analyzed Lab Number --DI IS 3!'J1 (H.cviscd 2/91)
·-
;--;.C. Dcpar.ment o f Environmenc,
1 lealth, & Natural Res.ourccs
Solid Waste Management Di,ision
Site Num ber -----------------
:>talc Lab-Oratory 01 J-'ubllc l!o lth
P.O. 13ox 2S047, 305 N. Wilmini;,on Street
Raleigh, North Carolina 2761 I
Fiel d Sam ple Number W L. -012 -5 5 ------------------
Name of. Site WA-R.i2.E:.J Cbo,-JT)' PG'B l.DFL Si te Locatio n A F,o 10 NL _-<--..:. _ _:_::c...:...::,c__ __ :.......=c_ __________ _
Collected By a. f\) tl.HOL,6c,)-..) ID# 3-=f-Date Collected :2. ~ JO L >' 9 f Time IS3o
~ !rre PH E..:>S
Agency: Hazardous Waste X Solid Waste SuperfUIJd TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· ,-2 __ Ground water (1) Soli d (5) (a~I!) Cad mium --
A,,, Chromium
Ve=J.Jr --__ Surface water (2) Liquid (6) Lead --
--Mercury
X Soil (3) _ Sl udge (7) Selenium --Silver --
--Oth er (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B /N E xt. Barium carbon tetrachlorid e ------'MTBE Cadmium chlordane ------
_2L PG& <::0 1/P~ ..... Chlorid e ch lorobenzene ,, ' ~-Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-di ch I oroet h ane
--Nitrate 1,1 -dich loroethylcne ----Selenium 2,4-dinitrotol ue ne ----Silver heptachlor ----R ad iochemistry Sul fa tes hex.achlorobenzene ----Zinc hexachl orobutadiene ----Pa rame ter Results (PCi/1) pH hex.a ch Io roe than c ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nit robenzene ------TOC pent ach lorophenol ----
----pyridine
Micro biology ----tetra ch loroet hylene
trichloroeth ylenc ----Parameter Res ults (Col/l 0Om l) 2,4,5-trich lo rophcnol ----
----2, 4,6-trichl orophcnol --
------vinyl chloride
endrin --
Date Received 7 ,,..~f-'J~l.!f.l}R.eported by
lindane --
--methoxychlor
Dc1tc Ex!raclc<l "fl-V-1j'1/;t} --toxaphene
Date Reported --'.2,4-D
Y-S-9~1/P
__ '.2,4,5-T P (Silvex)
Dc1lc Analyzed Lab Number 942765 D I IS 31 ')1 (H.cviscd 2/91) --
·-
0 .C. Uepar.mcnt ot l:.nv,ronmcnt,
I lcalth, & 1','atural Rcs.ourccs
Solid Waste Management Di,~sion
wf\Jn.r Lr, f\J'\JU...-1 0i..:, RL\L ur:,0 J. .. )UHC LllOOr&lOf)' 01 ruo11c liC!.ltn
P.O. Gox 2S0-17, 305 N. Wilmini;,on Street
Raleigh, North C..rolin• 2761 l
Site Number Field Sample Number W/.. -0 13 -SS ---=------'-=----'------------------------------
Name of.Site WA-R.i2e.J Gor.JT'1 PC"B l.DFL Site Location A F,o ,v NC., -~-.....:....:::....:....:,c___....:._::......=:;__ __________ _
Collected By G;. fv 1cH.ol,6o"-' ID# 3-+ Date Collected J. ~ JO LY 9+ Time /5"3 'Z..
. $T-.;'P-4-t ~ ,a.'.)S
Agency: Hazardous Waste X ---Solid Waste ___ Superfund TCLP Compounds
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ----
Ground water (1) _ Solid (5) (a~I!) Z-1 Cadmium --Chromium A11~ lle:JJt: --
__ Surface water (2) _ Liquid (6) Lead --__ Mercury
~ Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) Other (8) --I
--' --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
.L_ Pc,,.& <o,/~;rl.. Chloride chlorobenzene --~
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----
Le.ad cresol ------
----Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --Nitrate 1, 1-di chloroeth ylene ------Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachl orobenzene ----
Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----
__ Gross Alpha __ Conductivity me thyl ethyl ketone --Gross Bela TDS nitrobenzenc ------TOC __ pcntachlorophe nol --
----pyridine
Microbiology ----tetra chloroet h ylene
trichlorocthylene ----Parameter Results (Col/lO0ml) __ 2,4 ,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
--vin yl chloride ----endrin --lin dane
Date Rece ivc.d?-;!9-f~(/./) Reported by --methoxychlor --
T-//-?&/J --toxa phe ne
OJte Extracted Date R e ported 2,4-0 --
DJ!e Analyzed 3'-S-9¢1/P 942766 __ 2,4,5-TP (Sil vex)
Lab Number --1)1 IS 3l'Jl (IZcviscd 2/91 )
·-
1'.C De pa r\ment of Environment,
1 lealth, & 1'.'a tural Rcs.ourccs
Solid Waste Management Division
Site Number -----------------
:,tate l...JlC>Ontory 01 ruDIIC lic•lth
P.O. !}ox 2S0-17, 306 N. Wilmin&1on Street
Raleigh, North urolina 2761 l
Field Sample Numbcr __ L,U=---_l.._-_0_/_4_-_~_S ______ _
Name of Site WA-1<.i2.E:.J G,orvT'I PC:B l.DFL Site Location A F"To,v NC --'----'--.....:.....::=-:...c::::...._ __ =-=;:....__-----------
Collected By ~. fv •c.H.oL6c::::>'l----l ID# 3-={-Dale Collected :2. "1-JO LY 9+ Time /5"3{:,
C:. . -e.,e-Pt-t €.._,S
Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental· Concentrate Comments Arsenic --Barium ---· __ Ground waler (1) Sol.id (5) 6~1D 5-1 Cadmium --
A,R Chromium
/)EJJT --__ Surface water (2) Liquid (6) Lead --Mercury --_Jf_ Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --I
--·,
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Exi. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ----<o,/P# "-L Pc& Chloride chlorobenzene ~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotol ucne ----Silver heptachlor --, --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexach lorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethane ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----te trachlorocth ylene
trichlorocthylcnc ----Parameter Results (Col/l00ml) 2, 4, 5-trich I orophenol ----
----2, 4,6-trichlorophcnol --
------vinyl chloride
endrin --
Date R eceived z-;zr -NU1t1'JJRcported by
lindane --
--mcthoxychlor
~-//-2VJ(/) --toxaphenc
DJtc Extracted Date Reported 2,4-D --
Y-S-9~-Y,P ·· 9'-\2767
__ 2,4,5-TP (Sil ve.x)
Date AnalyLcd Lab Number
DI IS 3!')1 (l,cviscd 2/91) --
;--,;.C. Ocpar.mcnl of Environment,
I lcallh, & 1','~lural Rcwurccs
Solid Waste Management Oi,~sion
Site Number -----------------
c,l&{C Ult>Oratory ol rubl1C lic>llh
P.O. 8ox 2SN7, 306 N. Wilmini;ton Street
R..alcigh, North urolin• 27611
Field Sam pie N um bcr __ W=---_L._-_0----=-/--=5=----__,:S:::::.......cS=------
Name of-Site WA-R.i2.c.J Got'JT'i PC.t;, l.DFL Si te Location A FTo i-_J NC _.!......:......:__...:....c::.__:_::,<__ _ __c._::c_:::::..__ __________ _
Collected By G;. f\,) ,u--t.o \... 6c:>)J ID# 3-=t-Date Collected :J.1--:JOLY 9+ Time /!,30
6i . S~Pl-\eN s.
Age ncy: Hazardous Waste X Solid Waste ___ Superfllild TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Grou nd water (1) Solid (5) (;il<t!) 4-8 Cadmium --Chromium A-112 Ve>JT --__ Su rface wa ter (2) _ Liquid (6) Lead --
--Mercury
_K_ Soi l (3) Sludge (7) Selenium --Si lve r --_ Other (4) _ Other (8) --I
--' --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsen.ic benzene ------Acid:B/N Ex1:. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------<o~/~11t. L PG& Chloride chlorobenzene ----Chromium chlornform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d i ch I oroethane
--Nitrate 1,1-dichloroethylcne ----Selenium 2,4-dinit roto\ uene ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexach lorobutadiene ----Parameter Results (PCi/1) pH hcxachlorocthane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pent a ch lorophenol ----
----pyridine
M icrobiolo gy ----tetra chloroeth ylene
----trichloroethylcne
P.iramcter Results (Col/lO0ml) 2, 4 ,5-t rich I orophenol ----
------2, 4 ,6-trichl orophen ol
------vinyl chloride
endrin --
Date Received 7-;l.f-9r,£ 'JI/ Az> Reported by
lindane --
--mcthoxychlor ;,, toxaphc.ne ~-~-1Vr? --Date Ex tracleu Dale Report ed :?.,4-D --
"f?-S-9¥~ Lab Number 942768
__ :?.,4,5-TP (Silvex)
Dale Analyzed --DI IS 31')1 (ll.cviscd 2/91)
-
r,:.l-ucp-anmcnt 0: t n"1ronmcnt,
J lcalth, & /':atur.il Rc.wu~ccs
Solid Waste Management Division
0/-UYll" L.L'.., f-) ... J ,~.1. J.l.tJ nL\,l UL..);_ -..H 41"-L ~vv1 ,1nury u1 ruu11c 11c:21.1tn
Sile Number -----------------
P.O. Box 2Sl)-17, 306 N. Wilmin!;lon Street
R..alcigh, North C. rolin• 27611
Field Sample Number W L -0 I~ -$ S
Name of Sile WA-R.i2-c.J Gor-.J"N PGt:> l.DFL Sile Location A F"To .10 NC _..,__ _ _:_._:::...__:__.:=:_ __ ~c..._-----------
Collected By a. /\) 1c.H.0L6oµ Dale Collected 2 ?-;/UL 'Y q4 Time /6t>I
~ . ST~PHEU~
Agency: Hazardous Waste X Sol.id Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground waler (1) Solid (5) (i.12 I J) tJ-,11 Cadmium .. --Chromium --&,-,,P /lousE __ Su rface water (2) Liquid (6) Lead --Mercury --1L Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Pt1rameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsul ts (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------<0,/0~,P/lt __x_ 'PC-1i3 Chloride chlorobenzene --~-,, Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol --· ----
--· __ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichlorocthane --
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rotol uene ----Silver heptachlor ----Radiochemistry Su lfates hexachlorobenzene ----Zinc hexach I orobu lad icn c ----Parameter Results (PCi/1) pH hexachloroethanc ----
--Gross Alpha __ Conductivity methyl ethyl kctonc --Gross Beta TDS nilrobenzenc -------TOC pcnlachlorophcnol ----
----pyridine
Microbiology ----l elr achloroelh ylen e
----trichloroelhyleoc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-tridJorophcnol
vinvl chloride --------endrin --lindanc
Date Received 1-.2.r-?-f0¥' AJJ --Reported by melhoxychlor
✓ --
Y-,-1/-fj!J!/' Dale Reported --toxaphcnc
Dale Ext racted 2,4-D --
~ s-9~11/J 942769 __ 2,4,5-TP (Silvcx)
Dole A nalyzed La b Num be r --DI IS JI'}! (ltcviscd 2/91)
i<.C [,sq;~r.mc:ll of Environment,
l lea Ith,&. r--.·a tur.d Re.sources
Solid Waste Management Di,~sion
..)lAi-: 1. .. .Jn>On.~ory o.l .t'ut;i ,c 11c31ln
P.O. [kx ~'7. 306 N. Wilmini;ion Street
R..alcigh, North Carolin• 2761 l
Sile Number Field Sample Number WL -() 17-S.S -----------------------------------
Name of Site WA-1<.i2..e,,.J Gar-.)TY PCt!:> U)FL Site Location A Fro i-J NC --'-----~---------------
Coilccted By (;. (\) 1c.H.0L6c:::),,_, ID# 3-+ Date Collected 2-:/--::JULY q4
Q -~~PHE"....:)~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --Barium ~ ---· __ Ground water (1) _ Solid (5) 'iR.rp ~, 10 Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
1L Sui! (3) _ Sludge (7) Selenium --Silver --___ 0 ther ( 4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic ; benzene ------Acid:B/N Ext. Barium carbon tetrachloride --· ----'MTBE Cadmium chlordane ------<(;I•/~ _)(_ Pe-13 Chloride chlorobenze ne --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride rn-cresol ------Iron __ p-cresol ----Lead cresol ------
·-----Manganese 1,4-dichlorobenzene --
--· --Mercury 1,2-d i ch I oroethane --
Nitrate 1,1-dichloroethylcne -------Selenium 2,4-dinitrotol uen e ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----··----·--Zinc hexach lorobu tad iene ----Pararnetl'.r Resulls (PCi/1) pH hex.achloroethane ----Cross A lph a --__ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pen tachlorophenol ----
----pyridine
Microbiology tetra chloroethylcne ----
----trichloroethyleoc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trich.iorophenol
--vinyl chloride ----cndrin --
Date Received 1-,/9-'l_Y1!efJ..tfli) lindane --Reported by --methoxychlor
2-£/-?'lr/J --toxaphene
Date Extracted Date Reported 2,4 -D --
~-s--9{/rp 9427 7 0 __ 2,•1,5-TP (Silvcx)
Dale Analyzed Lab Number --1)1 IS 31')! (IZcviscd 2/91)
-
1,.1......* 1...,·._y_,,,,,,-.·,, v, ..__,, .. ,,v,1111._,,,,
; lcolth, !, ls.'atur.l\ Re.sources
So,ic Was1c Management Di,~sion
Sile Numbe'. -----------------
P.O. fk>x 2.S0-17, 306 1'. Wilmin[:lon Stn:ci
Raleigh, North C:..rolin, 2761 l
Field Sample Number WL -0 /<$ -SS
Name of Site W,H?.i2.c.J CorJT'i PC-t> u,FL Site Location A F",o ,-J NC _.:._c. _ _;_::;_.:...;=------'--='--------------
Collected By 6. f\) tCHo L 6c>""-' ID# 3=/-Date Collected 2. ?--;JULY q4 Time //, / 3
Gr .'Sr-E-P,-,E"A.JS
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds -----
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---·
Ground waler (1) _ Solid (5) GRID 21-, o Cadmium --. --Chromium --Surface water (2) _ Liquid (6) Lead --Mercury --_&_ Soil (3) _ Sludge. (7) Selenium --Silver --_ Other (4) Other (8) --
--
' --
Organic Chemistry Inorganic Chemistry --
P;irameter Results(mg/1) Parameter Results (mg/I)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------__x_ Pc..13 <P./P~ Chloride chlorobenzene ----Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
, __ __ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dich loroethane --
--Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-di nitrotolucne ----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzene ----
Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gro<,s A lpha --Conductivity methyl ethyl ketone --
Gross Bna TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
Microbiology ----tetra chi orocth ylene
trichloroethylenc ----------Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-tri ch.iorophenol
----vinyl chloride --endrin --
lindane
Date Received 7-.fl. '1-?._r/,-y/'54_ --
Reported by --methoxychlor
;;, toxaphene
Dale Extracted -~!i.::_f~1//J --Date Reported --2,4-D
Dole Analyzed %-S-?~-J/,.P ·. 942771.
__ 2,4,5-TP (S ilvex)
Lab Number --
1)1 IS JJ'Jl (IZcvi scd 2/91)
1, .. l ...... ucpanmcrH Ol t:.nv1ronmcnl,
J lcallh, l,:. J\:alvrol Rc:.,-.ourccs
Solid Waslc Management Division
0/-Ul'.ll J,._.,J, . .'~ /·)._l \f ),. .LJJ.. ..J Jt..~-' .l'l.,J...,~ UJ.-V A ...,,_,..,_ .._,_,.,......, .• ,....,,] v• 1 ~...,,,._ • ,,_..,,,,,
Site Number -----------------
P.O. Box 2SO-l7, 306 1':. Wilmini;1on Stn:cl
Raleigh, North Carolin• 2761 l
Field Sample Number WL -t> I 'I-.:5S
Name of Site UJA-R.i2.e.J Go,-SN PCt:i l.DFL Site Location A F",o ,.J NC -.!.......'..-'---....:....:::.....:..::,:___-'-':.......==-------------
Collected By ~. {\) tLHo L 6c:,)-..) Time /6 19
<=t ST E"Pt-t E.)...)S
Agency: Hazardous Waste X Solid Waste _· __ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) GR1D 3~,4 Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
.L_ Soil (3) _ Sludge (7) Selenium --Silver --
--Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul t.s (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B /N E>,t. Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------..¼_ Pe,13 <t:?1/~ Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m -crcsol ------
--Iron __ p-cresol --
Lead ere.sol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d i ch loroctha.nc
--Nitrate 1, 1-dichlorocthylcne ----Selenium 2,4-dinit ro toluene ----
Silver heptachlor ----Radiochemistry Sulfates hex.a ch lo robenzene ----Zinc hexach lorobutadiene ----Parameter Results (PCi/1) pH hcx.a chloroelhanc ----__ Gross Alph a --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzcnc ------TOC pentachlorophenol ----
----pyridine
M icrobiology ----te lr a chloroeth ylene
trichlorocthyleoe ----Parameter Results (Col/l00ml) 2,4 ,5-trich lorophenol --
----__ 2,4,6-trich.io rophenol
------vinyl chloride
endrin --
Date Received 7:-...,q;..f~a7t?Report ed by
lindanc --
--melhoxychlor
'F-L/-91/1!L!_ Date Reported --toxaphene
Dale Extracted 2,4-D --
3-S-9,'~ Lab Number 9427 7 2 __ 2,4,5-TP (Silvex)
Date Analyzed --1)1 IS Jl'Jl (l~cviscd 2/91)
l lcalth, & 1','atural Resources
Solid Waste Management Division
Site Number -----------------
P.O. fki x ?-8()4 7, 306 '"· Wilrnini;,on Street
R.alcigh, North Carolina 2761 1
Field Sample Number W L. -tJ 2 0 -55
Name of Site WA-R.i2..E:.J GorvTY PG'B li:,FL Site Location A F"10 ,.J NC _L.....:__:__:...::::....:..:~---'--':.......::::::c__ __________ _
Collected By a . f0 ll.HO L 60~ Date Collected 2. ':/--:JULY q4 Time /~ Z I
Gt . $-re'PH-EN ~
Agency: Hazardous Waste X Solid Waste ___ Supcrfund TCLP Compounds ------
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· 4,e IX> 313, lb __ Ground waler (1) Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury --1L Soil (3) Sludge (7) Selenium ----Silver --
--Other (4) --Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane. --<I?,/ d #A'i ----_x_ Pc..0 Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-crcsol ----Fluoride m-creso! ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzeoe
--__ Mercury --1,2-dich loroethane
Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-di nitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hcXachlorobenzene ----Zinc hexach lorobu tad iene ----Parameter Results (PCi/1) pH hcx.achloroet hanc ----
--Gross Alpha --Conducti vity --methyl ethyl keton e
Gross Beta TDS nitrobenze ne ------TOC pcntachlorophenol ----
----pyridine
Microbiology ----tetrachl oroclh yl ene
trichloroethylene ----Parameter Results (Col /l00ml) 2,4,5-t ri ch loroph enol ----
------2, 4 ,6-t richJ o roph en ol
------vinyl chloride
cndrin --
Date Receive d 7-ol?-'lW/!Bi> Reported by
lin dan e --
--methoxych lor ..
Dc1lc Ex tr ac ted 'f?-y'-,Yt/__1/,{) --toxaphenc
Date Reported --?.,4 -D
D<1te Analy1.cd _2_-5-9~JAP
__ 2,4,5-TP (S il vex)
Lab N umber __ !)ll27 7 3 --DI IS 31 ')1 (l,eviscd 2/91)
i"-'--ucp..11 ,111c 11 l Ul cn"1runmcnc,
: !callh, &. 1'alurai Rc..<ourccs
Solid Waslc Management Division
Site Number -----------------
.J~ ...... ~vvi•1·VJJ ·v, I \JlJIII. I l L Ailll
P.O. 13ox 2S0-17, 306 N. Wilmini;ion S1rccl
RAieigh, North Carolina 2761 1
Ficld Sample Number W l -tJ Z I-S ~
Name of Site WA-R.i2e.J CborvTY PCr:, l.DFL Si te Location A F"1010 NC _,L.:,_....:__~::....:..:~-~:......:::::::..._ __________ _
Collected By c;; . (\) 1 C.Ho L 6c:>~ Date Collect::.d 2 ?-:JUL "'1' q4 Time I I., Z. l,
~ 5-r eP tt El,.::)~
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concen tra le Comments Arsenic --Barium ---· (q 12 I.I> 42, ze Ground water (1) Solid (5) Cadmium ----Chromium --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
1L Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/!) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:G C/MS Arsen.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium. chlordane ------<P,/P~M_ _x_ Pc.~ Chloride chlorobenzene ----Chromiun, chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----
Lead cresol ------
--__ Manganese --1,4-dichlorobenzenc
--__ Mercury --1,2-d ich lorocthane
--Nitrate 1, 1-dichlorocthylcne ----Selenium 2,4-di nitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hcxachlorocthane ----
--Gross A lpha __ Conduct ivity methyl ethyl ketone --Gross Beta TDS nitrobcnz.ene ------TOC pcntachlorophcnol ----
----pyridine
Microbiology ----tetra chloroethyl enc
----trichloroethyl cnc
Parameter Results (Col/l00ml) 2,4 ,5-trichlo rophcnol ----
------2, 4 ,6-trichJ oroph cnol
------vinyl chloride
cndrin --lindane
7-;lf-9//t/(&;Reported by --Date Received mcthoxychlor --
?-L/-t&e --toxaphene
Date Extracted Date Reported 2,4-D --
Date Anal'[Lcd--5l.::_'9'-91/1/;:' 9427 7 4 __ 2,4 ,5-TP (Si!vex)
Lab Number --1)1 IS JJ 'JJ (llcviscd 2/91)
I
i'-,'.L. u cpar;.mcnl 01 t nvu c rim cnt,
i lc;;llh, & 1\'a lural Rc.s.ourcc:s
Solid '.1/aslc Management Di,ision
0f-l..J.\''.l!' LJ...', r\..1 'r'J,,,.J....JJ,. J l.U 1'-.J_.,\..L_ VL..J J,. ~'~4 ~'-L-£VV!AlUJ)' Ul f UUIIL f1 '-ll1111
Sile Number -----------------
P.O. 11ox 2W7, 306 N. Wilmini;ion S1n:c1
Raleigh, North Carolina 2761 J
Fie.Id Sample Number WL -0 2 Z. -~S
Name of Sile WA-1<.i2€:.J GoNT'I PG"B U,FL Site Locati on A F,o 10 NC _..:........:,_-"--':......:;._;::__ __ __c=C-..-__________ _
Coll ected By 6 . l'v I LHo L 6C>~ Dale Coll ected 2. ?-:JV LY q4 Time /~ Z 9
c;; . SrePH-E1'J'=»
Agency: H azardous Waste X Sol.id Waste Superfund T CLP Compounds ---------
Sample Type Inorganic Compounds Rcs ulls(mg/1)
Environmental C oncentrate Comments A rsenic --Barium ----
__ Gro und water (1) Sol.id (5) G,12 ID 3~, ZI Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --M e rcury --_L Soil (3) _ Sludge (7) Seleniu m --
Silver --
--Other (4) _ O ther (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Par ameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Orga nic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
A cid:B/N Ext. Barium carbon te trachl oride ------'M T BE Cadmium chlordane -------15__ Pc..0 <" 0 ,10-/PM' Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-crcsol ----F luoride m -cresol ------
--Iron p-crcsol ----Lead ere.sol ------
--__ Manganese --1,4-dichlorobcnzene
--__ Mercury --1,2-dichlorocthanc
N itrate 1, 1-dichloroethylcne ------Selenium 2,4-di nilrotolucnc ----Silver hcplachlor ----
Rad ioc hemistry Sulfates hex.a ch I orobenze ne ----
Zinc hexachlorobul adienc ----Parameter Results (PCi/1) --pH hcx.achloroc thane --__ Gruss Alpha __ Conductivit y --methyl e thyl ketone
C ross Bela TDS ni trobcnzene ------
TOC pcntachlorophenol ----
----pyridine
M icrobiology ----t ctr ach lorocthylcnc
trichloroe thylenc ----Pa rameter Res ults (Col/l00ml) 2,4,5-tri ch lorophcnol ----
------2, 4,6-tri chforophenol
------vinyl chlo ri de
cndrin --
7 -1l.l/-'Jzkt/tf 6ZJ Reporte d by
lindanc
Date Received --
--methoxychl or
?-//-rzLv,,a --toxaphene
Date Extracted Dale R eported 2,4-D --
Dole A nc1i yLcd &"'-~-9¢J/,;::J ·. 942775 __ 2,4,5-TP (Silvex)
Lab N umber --D I IS Jl'Jl (!Zcviscd 2/91)
I
-
0.L Ucpanmcnt or 1:.nvuon mcnt,
l lcalth, & r--:a1ural Re.sources
Solid Waste Management Di,ision
0A.J.Y.trL£.; ,u,A.J..J;.JJ..U I\...L\.l_U~...JJ.. ,.H4lL 1.,A;,-.._n ,1 \•.)ryo, r uu11c 11c11,1ln
Site Number -----------------
· P.O. Box 280-17, 306 N. Wilminb10n Street
Raleigh, North Carolin• 2761 l
Field Sample Number WL -c) Z3 •$S
Name of Si le WA-R.i2.e.J Gor.J"N PGt> l.DFL Site Location A F"To 1'J NC _..:___c _ __;_::.__:.._::c.._ __ --=c ___________ _
Col lected By G . (\J •LHo L. 60.,_., ID#~-={-Dale Collected 2., ?---;/UL Y q4 Time /(, 3 3
a. . SrePH-0-lS
Agency: Hazardous Waste X Soud Waste ___ Super fund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground waler (1) _ Soud (5) 'f,IZ ID I I) I Z4 Cadmium --Chromium --__ Surface wa ter (2) Liquid (6) Lead --Mercury --Ji_ Soil (3) Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Resulls(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Res ults(mg/1)
P&T:GC/MS A.rsen.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------_x_ Pe-13 <t?, /() QfNlL Chloride chlorobcnzene r ----Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------.
Iron p-cresol ------Lead cresol ------
·-__ Manganese --1, 4-d ich lorobenzeoe
--__ Mercury --1,2-dich lo roet hane
--Nitrate 1, 1-dichloroethylcnc ----Selenium 2,4-dinitrololuene ----Silver heplachlor ----Radiochemistry Sulfates hexach lorobenzene ----Zin c hexa ch lo robu tad ien e ----Parameter Results (PCi/1) pH hexac hl oroelhanc ----Gross Alpha --__ Conductivi ty --methyl ethyl ketone --
Gross Beta TDS nit robenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----tetra ch loroeth ylcne
trichloroethylcne ----Parameter Results (Col/l00ml ) __ 2,4,5-trichlorophenol --
----------2, 4 ,6-tridJ oroph en ol
------\~n yl chloride
endrin --lindane
Date R eceived ;7-,lf-f'c/1//;Lf lJ --
Reported by --methoxychlor
;,, toxaphene ?-t/-f&.f? --·--Date Exlractc<l Date Report ed 2,4-0 --
11-?-9L/1//' .
__ 2,4,5-TP (S il vex)
Dille Analyzed Lab Number 942776
1)I IS 31')1 (llcviscd 2/91) --
1"\-.L. ucpanmcnl O[ t.:.nvuonmcnt,
! lea Ith, c,: Nalu,ol Rc..<0urccs
Solid Waste Managcmcn, Divi~ion
Site Number -----------------
P.O. !1ox 1S0-17, 306 N. Wilmin[;Jon Street
RAieigh, North Carolin• 27611
Field Sample Number Wt. -c) Z.4-S.5
Name of Site WA-R.i2€:.J CborJTY PCB l.DFL Site Location A F"To 10 NC -~---~---------------
Collected By a. f\) IC.HOL6c:>)-..J Date Collected 2-:,... ;/UL Y q-4 Time /1,$4
G s .s . -r'EPHE:,._,
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· 3 1 ZG" __ Ground water (1) _ Solid (5) G1Z1D Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury --1L Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Resu I ts (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane -------<0,/~ .L Pc..6 Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------Lead ere.sol ------
----Manganese 1,4-dichlorobenzene --
----Mercury 1,2-d i ch I orocth ane --
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Si lver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobu tad iene ----Parameter Results (PCi/1) pH hexachloroethanc ----__ Gross Alpha --Conductivity --methyl ethyl keton e
Gross Beta TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
Microbiology ----t etr achlorocth yl ene
----trichlorocthylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol ---
----__ 2,4,6-trichlorophenol
------\~nyl chloride
endrin --lindane
Date Received 7-,,l_f -f'Y/// ,6.1) --Reported by --methoxychlor
.,I toxaphcne 8'-~-f~# --O;ilc Ext racted Dale Reported 2,4-D --
Y-S-9;;/1/.,d 942777
__ 2,4,5-TP (Silvex)
O;itc Analyzed Lab Number --DI IS Jl'Jl (ltcviscd 2/91)
N.C Dcpanmcnt of Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAJ¥1PLE ANALYSIS REQUEST State Laboratory of Public Health
Site Number -----------------
P.O. Box 28047, 306 N. Wilmington S1n::c1
lulcigh, North Carolina 2761 J
Field Sample Number W L -t) Z 5' · :5 S
Name of Site WA-R.i2.€:.J Gor.JT't PC"B l.I,FL Site Location A F"To ,v NC.--.!......'...-'--_;__:::....:...::"'----'-"-='------------
Collected By c;;. f\) tC.Ho L 6C>"--' ID# 3-=f-Date Collected 2. ?-:JVL Y q4 Time It 39
6oz. 5,E"Ptte,.:) 5:.
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) {i,IZID 21-' It:> Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --£ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------__x_ Pc.0 <()./(}#hf Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dich loroelhane
--Nitrate 1,1-dichloroethylcne ----Selenium 2, 4-di nil rotol u ene ----Silver __ heplachlor --Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achl oroelhane ----
--G ross A lpha __ Conducti vit y --methyl ethyl ketone
G ross Beta TDS nitrobenzene ------TOC penta chl o rophenol ----
----pyridine
Microbiology ----tetr achloroethylene
----trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichl orophenol --
------2, 4,6-trich.i orophen ol
------vinyl chloride
endrin --lindane
D ate R eceived 7-,,1f-f9"tts'AL,Reporled by
--
--meth oxych lor
Dale Extracted 3-S-9<./-1/1' --toxa phe ne
Dale Reported --2,4-D
3 -?-2f/1(,;4 " 942778 __ 2,4,5-TP (Silvex)
Date A nalyzed Lab Number --DI IS 31 91 (IZcviscd 2/91)
1'.C Dcpar,mcnt of Environment,
l lcalth, & l','atural Re.sources
Solid Waste Management Di,~sion
Site Number -----------------
.:)UllC UDOra.tory 0[ I UDllC liC!i\n
P.O. Gox 2W7, 306 I','. Wilmin&1on Street
Raleigh, North urolin• ~761 1
Fie.Id Sample Number WL -o:z" -:S$ _ _..::;. ___ ....:::.._ ___________ _
Name of.Site WA-R.i2.t.J Cor-JT't PC."f!:, l.DFL Site Location A F,o,i.J NC _.c._.:._....:.....:::....:.;"--..--'-=:;__-----------
Collected By c;;. fv 1cHo\..,6o"-' DateCollected :Z1-JOLY 9f Time /5$8
~. ~"TE'P+t E~ g.
Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---__ Ground water (1) Solid (5) 6J<tD ~ -3 Cadmium --Chromium
A-,~ /)~µ T --__ Surface water (2) Liquid (6) Lead --Mercury --~ Soil (3) _ Sludge (7) Selenium --Silver --
--Ot her (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachlorid e ------"MTBE Cadmium ch lordane ------
....L Pc,& < t1>, LO-fP11 Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
----Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d ich loroet h ane
Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-dinitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch l orobenzene ----Zinc hexach lorobu tadiene ----Parameter Results (PCi/1) pH hexach loroethanc ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pen tachlorophenol ----
----pyridine
Microbi olo gy ----tetra chlorocth ylene
trichlorocth ylenc ----Parameter Resu lts (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6 -trichJorophcnol
------vinyl chloride
endrin --lin d:rnc
Date Received Z-e<9-9'¥J/t&Reported by --
--methoxychlor
1-S-9~-Yr' --toxaphene
D<1tc Extracted Date Reported 2,4-D --
'i'-?-%/rjP 942779 __ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --I)/ IS Jl'Jl (llcviscd 2/91)
1'.C. Dcpanmcnt of Environment,
l lcalth, & Natural Resources
Solid Waslc Management Di,~sion
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
· P.O. Box 2S047, 306 N. Wilmini;ion Street
RAieigh, Nonh Carolina 27611
Site Number ----------------Field Sample Numbcr_~LA):___L._-_l)----'2=-....,7-_---=S_.S _____ _
Name of Site WA-R.i2.E:.J <l>or.Jrt Pc,"E, /_oFL Site Location A F'To ,v NC _..<......:._c__....:...:::....:...:,<_.__---'..-'c_:=:_ _________ _
Collected By a. fv l('..H.OL,6C)).J ID# 3-=/-DateCollected j?-JULY 9-t Time It 89
~ . '5TEPH£1v>
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Incrganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) 6R1!) Z.-1-l ID Cadmium --• Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --__K_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------A cid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------L PG& < t?. L d-fP21, Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1,1-dichloroeth ylc ne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1 ) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ke tone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----tetrachloroethylene ---
----trichloroethylene
Parameter Results (Col/l00ml) 2,4,5-trichlorophenol --
----'\ __ 2,4,6-trichlorophenol
------vinyl chloride
endrin --
Date Received 7-,:/.f-W///IL!L) Reported by
lindane --methoxychlor --.,, toxaphene
Dale Extracted 9-S--9¢1/1' --Date Reported --2,4-D
'i-?-9~-r/J 942780
2,4,5-TP (Silvex)
Date Analyzed Lab Number --J)IIS 31')1 (Revised 2/91)
N.C. Dcpanmcnt of Environment,
l lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
· P.O. 13ox 280-47, 306 N. Wilminpon Street
Raleigh, North Carolina 27611
Site Number Field Sample Number W L -(9 Z cg" -S S ------~~--------------------------
Name of Sile WA-1<.i2.E:.J GarJTY PG""B u,FL Site Location A F"To ~ N (__ --'---'---'--=--=-='--__;_--=-----------
Collected By G;. f\) 1cHoL.6C>"'--' ID# 3=/-Date Collected Z.€ ✓tlL >' 9., Time 6) 9 $'B'
L, ,e e~c
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
LEdLHlf-TE ~lv'D
---· __ Ground waler (1) _ Solid (5) Cadmium --Chromium
~ LrE'iZ.-Ov~ALL --__ Surface waler (2) _ Liquid (6) Ar Lead --
--Mercury
__){_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride
-.MTBE ----Cadmium chlordane
X Pe-'?£~NJJ /,~ ----Chloride chlorobenzene --~-Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d i ch loroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC penlachlorophenol ----
----pyridine
Microbiology ----telrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
------vinyl chloride
endrin --
D ate Received 7-:2'?-f</P( (1j} Reported by
lindanc --
--methoxychlor
~S--9¥1/P --toxaphene
Dale Extracted Date Reported 2,4-0 --
Dale AnalyLed~~f~j//-7 Lab Number 942781 2,4,5-TP (Silvex)
--l)J IS J J'JI (Revised 2/91)
l\'.C Dcpar.mcnt of Environment,
l lcalth, & 1'atural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
· P.O. 13-ox 28047, 306 1'. Wilmington Street
Raleigh, North Carolina 27611
Site Number ----------------Field Sample Numbcr __ lu __ L_-_t>_:Z_Cf_-_S_S ______ _
Name of Site WA-R.i2.t.J Cborvn' PC.'B l.r,FL Site Location A F'To ,v NC, _.r......:.~....:....::::....:..::,,c___...;__:-=:.__----------
Collected By a . fv ll'. .. H.O l. 6c:>"'-' ID# 3=/-Date Collected 2 ?---;JULY '1"'1 Time 14-ZS-
~ -~~:{)Ha...)E,
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ----
__ Ground water (1) _ Solid (5) £AST S,l>E Lx,FL --Cadmium
Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
_Jf__ Soil (3) Sludge (7) Selenium --Silver --
_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsul ts (mg/I)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane --PC'B~-J'lf!). 0,.:2:2 ~nm. ----
X Chloride chlorobenzene --~-,, Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-di ch I orocthane
--Nitrate 1, 1-dicnloroethylene ----Selenium 2, 4-d i nit rot ol ucne ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenz.ene ----
Zinc hex a ch I orobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
G ross Beta TDS nitrobenzene ------TOC pentachlorophcnol ----
--__ pyridine
Microbiology ----tetr achloroethylcne
----trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trich lorophenol --
------2, 4,6-t ri chl orophenol
------vinyl chlo ride
endrin --
1-_..t ?-'f 93/t~...lJReported by
lindane --Date Received rnethoxychlor --
O;ite Extracted $'-S'-'1¢ 1!,{) --toxaphene
Date Reported --2,4-D
Dale Analyzed ....3....-9...-91/ J/,P 942782 __ 2,4,5-TP (Silvex)
Lab Number --DI IS 3191 (Revised 2/91)
,..,:.C. Dcpanmenl o[ Environment,
I lea Ith, & Natura\ Rcu,urces
Solid Waste Management Di,~sion
~AMP Lr, ANAf,i:::, 1~ Kl:.,'--2 Ut.,:::, l St•lc Laboratory of Public Holth
P.O. !}ox 2SC-47, 306 N. Wilmint;1on Stn:ct
R.alcigh, North Carolina 2761 l
Site Number -----------------Field Sample Numbcr __ W __ L_-........,c._O_o_/ __ ._:5_W-----'-------
Name of Site WA-R.;2.e.J ~or-.)N PG"B u,FL Site Location A F'To ,v NC _.!....C,. _ __:__:::....:_::,___ _ __.c......=;__ __________ _
Date Collected 29 :JVL 'I Cf 4 Time I Z-()5
/111 . P,, ,A..-'-oe,c.. rtP,,e
Agency: Hazardous Waste X Solid Waste ____ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· '21ctfNEC.K: __ Ground water (1) Solid (5) V r,T@il' M. Cadmium --Chromium --
_ Liquid (6) C'2.E EK" _lL Surface water (2) Lead --Mercury --Soil (3) Sludge (7) Selenium ----Silver --
--Other (4) _ Other (8) --'
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) Organic Compounds Rcsults(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium car.ban tetrachloride ------'MTBE Cadmium chlordane ------L Pc..B <O, tJOO/ Chloride chlorobenz.ene ----Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
----Mercury --1,2-dich loroethane
Nitrate -1,1-dichloroethylcne ------Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulf ales hexachlorobenz.enc ----Zinc hex a ch Io robu lad i cne ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenz.ene ------TOC penlachlorophenol ----
----pyridine
Microbiology ----l etrachl oroet hylene
trichloroethylenc -----·-Parameter Results (Col/l0Oml) 2, 4 ,5-trich I orophcnol ----
------2, 4,6-t richJ orophenol
------vinyl chloride
endrin --lindane
Date Received '7-;2.f-9¢-t/,1'.ii) Reported by --
--methoxychlor
.J toxaphcne
Date Ex!rac[cJ <?'-/-ff::V~ Bb --
Date Reported --2,4-D
__ 2,4,5-TP (Silvex)
Dale Analyzed 5'-/-'f9"J//I Lab Numbe r 942783
I)\ IS Jl'Jl (/Zcviscd 2/Yl) --
i
1','.C Dcpar.ment of Environmcnl.,
I kalth, & Na tural Re.sources
Solid Waste Management Di,ision
2,A.Nlr' Lt, J\l'U; . ..Ll ~1.::, K..t.,"-,L U.t.,::, 1 ::,talc L->t>o ntory O! l'utJl1~ !le>ith
Site Number ------------------
P.O. l}o, 280-l,, YJ6 S. Wilmini;1on Street
RAieigh, North Carolin• 2761 l
Field Sample Number L0 L -00 I -5 'D
Name of Site WA-1<.i2.E.:10 CborvT'i PC"B l.DFL Site Location A F,o ,-J NC --'--'--....:....:::....:..::,__ _ _.:--=:__ __________ _
Collected By a. f\) 1 U-to \.. 6o"t-> Dale Collected 2.~ Jl>L '/ Gt4 Time /Zct;'
M.. Pc ,~r:>EJCT'ti-R
Agency: Hazardous Waste X Solid Waste ___ ,Su per fund TCLP Compounds ------
Sample Type Inorganic Compounds Rcsu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---·
5~:PIME.iUT" __ Ground water (1) _ Solid (5) Cadmium --Chromium
Liquid (6) t},P~rteat-Jff J2/CH/VEC.-l< --__ Surface water (2) Lead --
CJ2.E~K --Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --_lL Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Resu Its (mg/1) Parameter Results (mg/I) (tng/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arseruc benzene ------Acid:B/N Ext Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------<. o , Io llf2tll _x__£__c..:B Chloride ch lorobenzene
1 --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1)-dichloroethylcne ----Selenium 2,4-di nit rotol u ene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobu l adiene ----Parameter Results (PCi/1) pH hcx.achloroelhane ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----l etra chloroeth ylene
----lrichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane
Date Received ?-;2.f-'11/P~,ti,J)Rcporlcd by --
--methoxychl or
.7 toxaphene
'i-S:?//1/P --Dole Extraclc c.l Dale Report ed 2,4-D --
'5'-9-2~11/J 942784
__ 2,4,5-TP (Sil ve x)
D<.1t e A na lyzed Lab Nurn bcr --J)I IS J l9l (Revised 2/91 )
;,:.C. Ocpar:mcnl of Environment,
I lcaith, & 1'.'atural Resources
Solid Waste /'-.fanagcmcrll Division
Si te Number -----------------
'.>t•tc LJ<txlntury o'. r'ubl,c !iolth
P.O . fkix 2.W7, 306 1'. Wilmini;ion Strut
R.alcig.h, Nonh Carolin• 27611
Field Sample Number W L-00 Z -SW ------------------
Name of Site UJA-Qi2e...J Gor.JT't PGt:, l.DFL Site Location A FT"~ 10 /\JC _..:.......:. _ __;_::......:...;"-------'='------------
Collected By G;. f',J t CH.o L. 6Q)-..) Date Collected 2 t3 JtJL Y Cf 4-Time /04-0
M . p,., 1 AJPe,c ,~
Agency: Hazardous Waste >< Solid Waste ___ ,Superfund TCLP Compounds ---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· P<2?VNSne E:A-~ __ Ground water (1) _ Solid (5) Cadmium --
<?12e.£1<
Chromium
Liquid (6) ~c.HIV~C.k --__}{_ Surface water (2) Lead --Mercury --Soil (3) _ Sludge (T) Selenium ----Silver --
--Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium car,bon tetrachloride ------'MTBE Cadmium chlordane ----x PCB <t:),OOIJ/ Chloride chlorobenzene ----Chrornit:m chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------.. Lead cresol ------
--__ Manganese --1, 4-d ichlorobenzene
--__ Mercury --1,2-d ich loroet h ane
--Nitrate 1, 1-dichloroethylene ----Selenium 2,4-di nitrolol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexach lorobu tadiene ----Parameter Results (PCi/1) pH hexachloroethane ----
--Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC penlachlorophenol ----
----pyridine
Microbiology ----t etr achloroeth ylene
----trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophenol
------vinyl chloride
endrin --
7-2 -f'f//P,6'.L)Reported by
lin dane --Date Received methoxych lor .,,, --
O;itc Extracted 4i-/-9¥1//jlJ!L_ Dale Reported --toxaphrnc
--2,4-D
~-l-?¢1/~-94Z785
__ 2,4,S-TP (S il vex)
Dc.Jtc Analy1.cd Lab Number
I)I IS 3191 (H.cviscd 2/91) --
I lea Ith,,.<:.: ;'.°at,,ral Rcsourc~s
Solid Waste Ma na gement Di,ision
Sile Number ------------------
f'.O. !,ox 280-17, 306 ~,. W,lm,ni;ton Strut
R.Jilc igh , North Carolin• 27Gl l
Field s am pie N um bc r __ w_.:_l_-__:0'----0-=Z:_-___;__5,.__:_-P _____ _
Name of Sile WA-1<..2.e:.J GorJT'/ PC"B l.DFL Site LllC2 tion A F"10 J\..l NC _.,!.......C._~::.....:_"'---__ _.:cC---__________ _
Collected By 6 , (\) 1 <'.'.. H.o l-6o"-' DateColl ected 2-S :JvLY "?4 Time /t:, 55"
;U. PtP ✓.UPex~.e..
Agency: Hazardous Waste >( Solid Waste Superfllil d T CLP Compounds ------
Sample Type In organic Compounds Resu I ts (mg/I)
Environmental , Concentrate Comments A rs enic --Barium
:5e:P/,&?E,,U -r ---· Ground water (1) Solid (5) Cadmium ----Chromium
~;U :$ 77'2eA,IV\.
--__ Surface water (2) _ Liquid (6) Lead --
_ Slu dge (7) hCfll(.)ec_J.., <?££Fl<: --Mercury
Soil (3) Seleniu m ----Silve r
~ Other (4) wL1rco --
--Other (8) .5P~I T --I
I
:Z:C. -0 e:> I -::5£I:> --
--
Organic Chemistry Inorganic Ch emi stry --
Param eter Res ults (mg/I) Parameter Res ul ls (mg/I) (mg/~) Organi c Co mpounds Res ults(mg/1)
P &T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium . ch lordane
v~E6T <". I IJ ,111),m, ----Chloride chlorobenzene ----Ch.romium chloroform ------__ Copper o-cresol ----Fluori de m-cresol ------Iron p-cresol ------Lead cresol ------
----Manganese --1,4-d ich lorobenzene
--__ Mercury --1,2-dich lo roethanc
Nitrate · -1, 1-d ich loroeth ylcne ------Seleni um 2,4-d in itrotol u enc ----Silvu hcptachlor ----
Radiochemi st ry Su If ates hex.a ch lorobcnzene ----Zinc hexach lorobu t adienc ----Para meter Results (PCi/1) pH hex.achloroet h ane ----
--G ross Alpha --Conductivity --methyl ethyl ke tone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----pyr:d ine ----M icro bi ology ----tetrachloroeth ylcne
----trichloroethylenc
Pa rameter Results (Co l/l00ml ) 2,4,5-trich lo rophcnol ----
------2, 4,6-trichJorophenol
----vinyl ch loride --cndrin --lind:rne
7-.A 9-9';/''Jl~Lll) Reported by --Date Received melhoxychlor --:;., toxaphcne J'--S-91(1//!__ Dale Reported --Dale Extracted 2,~-D --
Date Analy,.cd '$'-(J-9 //Y/!!.__ Lab Number 942786 __ 2,4,5-TP (Si!vex)
--Ill IS Jl'JI (:Zcviscd 2/91)
I lcalth, /.:. ~a1urdl Rc.-«,urccs
SoJ;d \J./as:c i\~ anagcmcnt Di,·ision
Si te N umber ------------------
1'.U. !lox 280-1 7, 306 ~-Wilm,ni;-ton ~txcl
Raleigh, North Carolin• 2761 l
Field Sample Number W l -~OZ-~"P --------=-----------
Na me of Site WA-R.,2..t"1 G>o rvTi PC""B lnFL Site Location A F10 ,0 NC ---'-'--_:_:::......:.._::c_ __ c.......=c.___ __________ _
Collected By G . (\J tCH.Ol,6o~ ID# 3-=?--DateCollccled 2'8 -:/vLY <f4 Time It:> 55"
fi1. . P.,nvE>e-"-re'R.. . TCLP Compounds Agency: Hazardous Waste X Solid Waste Supcrfund ---
Sample Type Ino11;anic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium
.6'ez;,,.. /1? ~ -r ---· __ Ground water (1) _ Solid (5) Cadmium --Chromium
~µ !S 772eA.,vt
--__ Surface water (2) _ Liquid (6) Lead --
- Sludge (7) hCHNeck (:Q£E~ --Mercury
_ Soil (3) Selenium --Silver
£ Other (4) u., /_s:c:.o --
Other (8) , .S/DLI T --'
.i-~-001-sET> --I
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul ls(mg/1) (mg/kg) Organic Compounds Resu lts(mg/1)
P&T:GC/MS Arsenic benzene ------x_ Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE Cadmium . chlordane ------Chloride chlorobenz.ene ----~-
Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m-crcsol ------Iron p-cresol ------Lead crcsol ------
--__ Manganese 1, 4-d ich I orobenz.ene --
--Mercury 1,2-d ich lorocthanc ----Nitrate · -1, 1-dichloroeth ylcnc ------Selenium 2, 4-d i nit rotol u enc ----
Silver heptachlor ----Radiochemistry Sulfates hex.a ch I or obe nz.cne ----Z in c hexach lorobu tad icnc ----Paramell'.r Results (PCi/1) pH hcx;ichloroethane ----__ Gross Alpha __ Conductivit y methyl ethyl ketone --Gross Beta TDS nitrobcnz.cne ------TOC pcntachlorophcnol ----pyridine ----Microbiology ----t etrachloroct h ylcne
trichl orocthyleoc ----Parameter Re sult s (Col/lO0m l) 2, 4 ,5-trich lorophcnol ----
--__ 2, 4,6-trichl orophcnol --
--vin yl ch loride ----cndrin --lind:rn e
7~,,29-f</tl/!&J --Da te Received Reported by mcthoxychlor
;,, --tox aphcne --Dale Extracted <t-5:~9 '-f. s=_,1/ AB Dale Reported 2,4-0
( --
Dc1l c Analyzed H_,-9</-&£J 942787 __ 2,4,5-TP (Silvex)
Lab Number --1)1 IS Jl'JI (P,cviscd 2/91)
i''.C. !.JcpJr-.mcnt of Environment,
I lea Ith, & Na tu cal Rcs.c.urccs
Solid Waste Management D"ision
.:)UllC LllGOr1lOf)' 01 ruo11c l1C!.lln
P.O. Box 2S0-17, 306 N. Wilmington Street
RJilcigh, North C.rolin• 2761:
Site Numbu Field Sample Number W l • ~OZ-.$."]:> -------~------------------
Name of Site WA-Ri2E:..J CorJT'/ PCt::> l.nFL Site Location A FTo t,J NC ---'----'--....:.....:'-'-'"'-----'-='-------------
Collected By ~. (\) 1 CH.o \.. 60"-' ID#~-=/--Date Collected Z-8 -:/vL 'Y <(4 Time /055"
/11. Pc r~Pt"X reR
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
6°cP/A?E"/4J r ---· __ Ground water (1) Solid (5) Cadmium --Chromium
~;CJ :S 772eAft,'\_
--
__ Surface water (2) _ Liquid (6) Lead --
Sludge (7) JZc1-t1<Jec~ <?R£E"° --Mercury
Soil (3) Sdenium ----Silver
£ Other (4) lVfEC.O
--
_ Other (8) $1't-lT --I
IC.~ 00 I-:SED --
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds Results (mg/I)
✓ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------
Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----Zinc hexachl orobutadiene ----Parameter Results (PCi/1) pH hex.achloroeth ane ----__ Gross Alpha __ Conductivity methyl ethyl keton e --Gross Beta TDS nitrobenzene ------TOC pcntachlorophe nol ----
----pyridine
Microbiology ----tetra chloroet h ylene
--__ trichloroethylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-tricWorophcnol
----vinyl chloride --endrin --lind anc 7-~9-f/Lt/,.t',$) --Date Received Reported by methoxychlor --.,
toxaphcne --Date Extracted Dale Reported 2,4-D --
Dale Analyzed ~5-94--fl,ti t'. 942788
_ 2,4.5-TP (Silvex)
Lab Number
1)1 IS Jl'Jl (l~cviscd 2/91) ---
~;.c. Dcpar.mcnt of E nvironment.
I lcalth, l,;. 1','atu,-a! Resources
Solid Waste Management Division
.:::iA.l\'ll' L.t, Al'iALl :)10 K.t...V. U.t,:) .L ~tate L.Mt>o:-•tory or r'ubl,, Holth
P.O. 13ox 2S[)•17, 306 /',;, Wilmini;ton Strcc:
Raleigh, No rth C,,rolin• 2761 l
Site Number Fie.Id Sample Numl:x.r WI.. -00:3-.:SuJ --=-----=----=;____c---=c_-=c___::=-=:__----------------------
Name of Site WA-R.i2t.J GorvTY PGt> /...DFI-Site Location A FTo ,-J NC -~---'--....:....:::....:...:"'-------'-'---==-------------
Collected By a. /\) 1U-t.ol,6c>.,_, Date Coilecled 28 ::!Vt Y 9+ Time O ?lb
fl1 • pe; I A.I 'PG-]( TffZ__
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Con cen tra te Comments Arsenic --Barium ---· __ Ground waler (1) _ Solid (5) (JISTte£A-/J1 Cadmium --Chromium --£ Surface water (2) _ Liquid (6) lJAIA-IAMc=Z> 7e..t '8 . Lead --Mercury --Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) Other (8) --'
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Resu I ts (mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Resulls(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachl orid e ------'MTBE Cadmium chlo rdane ------<"• (JIJO/ x_PC,'B Chloride chl orobenz.ene ----Chromium chl oroform --· ----__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------Lead cresol ------
--__ Manganese --1, 4-d ichl orobenz.e ne
----Mercury --1,2-dich loroethane
--Nitrate 1, 1-di chloroethylcne ----Selenium 2,4-di nitr ololuen e ----Silver heplachl or ----Radiochemistry Sulfates hex.a ch lo robe nz.ene ----Zinc hexachlorobut adi ene ----Parameter Results (PCi/1) pH hcx.ac hloroelh ane ----__ Gross A lpha __ Condu ctivi ty ·--methyl ethyl ketone
Gross Bet a TDS nitrobenz.ene. ------T OC pen lachl orophenol ----
----pyr idine
Microbiology ----tetra chl o roe th yl cne
----trichloroelhylene
Parameter Re sults (Co l/l 00 ml ) 2, 4, 5-trich l orop henol ----
------2, 4 ,6-tric hJ o ro phenol
------vi nyl chl oride
cndri n --lin dane
Date Received J-:29-7'~,6'.,PReporl cd by
--
--methoxychlor
D:ilc Extr acted <g:.-J-94/7/4Ati Dale Report ed --toxaphene
--2,4-D
Dale Analyzed 2._-/-9¥1/r' 942789
_ 2,4,5 -TP (S il ve.x)
Lab Number
1)1 IS 31')1 (H.cviscd 2/91) --
I
r--:.C. Ocpar.mcnt of Environment,
J lcalth, & l\'atural Resources
Solid Waste Management Division
Site Number -----------------
St•tc ubon.tory o [ Public Holth
· l'.O. Box ~7, 306 N. Wilmington Strcc!
R.Blcigh, North Cuolina 2761 J
Field Sam pie N um bcr_~W-=--=L.=--•_,(9"""-'6=-....:~"'----~__:._X> _____ _
Name of Site WA-R.'2.E:.J CotvT'7' PC-t, l.DFL Site Location A F,o ,..J NC _..,_;__....c....;:::,__:_;::::__ _ ______c_c=c....,_ __________ _
Collected By ~. fv rc.H.ol,6c>~ ID# 3-=l--Date Collected 20 :JVL Y Gt'i-
/fl. Pt1,~;:,~,el!..
X TCLP Compounds Agency: Hazardous Waste Solid Waste ___ Supe.rfund -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---·
5E:'l)r m EAi r __ Ground water (1) _ Solid (5) Cadmium --Chromium
_ Liquid ( 6) l/2D.:S T/2.~ --__ Surface water (2) Lead --
l/A).V,4,11( EX> /,e..,13 --Mercury
Soil (3) Sludge (T) Selenium ----Silver --lL Other (4) _ Other (8) --I
) --~
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:G C/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane -------<::o-lll pPrK . L Pc.e Chloride chloroben2ene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --l,4-dichloroben2ene
--__ Mercury --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylcnc ----Selenium 2,4-dinitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
Zinc hexachlorobut adiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS ni1robe.n2cne ------TOC pent ach lorophcnol ----
----pyridine
Microbiology ----t ctr achloroet h ylen e
trichloroethylenc ----Parameter Results (Col/l00ml) 2, 4 ,5-trich lorop henol ----
------2, 4,6-trichJorophenol -
----vinyl chloride --endrin --
1-..l..'/-f~//t&Rcportcd by
lind:rne
Date Received --
--methoxychlor
"i-S-9¢-w> --toxaphen e
Date Extracted Date Reported 2,4-D --
Dat e Analy,.cd -2._-9-9¢'1/;P · 942790 __ 2,ti,5-TP (Silvex)
Lab Numbe r --1)1 IS 3191 (IZeviscd 2/91)
-
N.C. Dcpar.mcnt of Environrnc.n t,
I lc.allh, & Natural RC..1-0urces
Solid Waste Management Di,ision
~l4lC L;.,.b,on.lory oi Puol1c r1·ctirlh ___ _
P.O. fk,x 280-l7, 306 N. Wilmini;,or, Strut
Raleigh, North Carolin• 27611
Site Number Field Sample Number tuJ. -00 4,.. :/;;:,UJ -------=--'----'----=------------------------
Name of Site WA-Ri2.e.J GorvT'I PCB l.DFL Site Location A F'10 t--J NC _..!......:. _ _;__:::_;__:::c_ _ ___;c......=::...._ __________ _
Collected By (;. (\J, c.Ho L. 6c'.:::>,._, ID# 3-=i--Date Collected Z.'8 -:TVLY <::/'4 Time 084-t:J
/J1. P,:,,,NDE'tlr~-R
Agency: Hazardous Waste X Solid Waste _· __ Superfllild TCLP Compounds ---
Sample Type Inorganic Compounds Resu Its (rng/1)
Environmental Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) _ Solid (5) .t:bc.uAJ.sreEA-.,...., Cadmium --
VvVA# n> ~6
Chromium
;<._ Surface water (2) --Liquid (6) Lead --Mercury --Soil (3) Sludge (T) Selenium ----Silver --
Other (4) --_ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) Organic Compounds Results(mg/1)
P&T:GC/MS Arsen.ic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------1-Pc::..B <P. OQ P/ Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol --------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
--· Nitrate 1, 1-dichloroethylcne ----
Selenium 2,4-di nit rotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobut adiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC pentachlorophenol ----
----pyridine
Microbiology tetra chloroet h ylene ----
----trichloroethylene
Parameter Results (Col/l00ml) 2, 4,5-tri ch loroph cnol ----
--2, 4,6-trichl oro phenol ----
--vinyl chloride ----endrin --lind:rne
7 _,~;f • Yf?f//'.&xzeported by --Date Received methoxychlor --..,, toxaphene
D<itc Extracted$_-/-9 L/ Yf) ~6!_ Date Reported --
--2,4-D
7 __ 2,4,5-TP (S il vex)
Dale Analyzed K-2.-f#~ _ Lab Number 9li2791. --DI IS 31')1 (Revised 2/91 )
t~.C. Dcpar.mcnt of Environment,
I lca lth, & 1','atucal RC-.\.Ourccs
Solid Waste Management Di,ision
~AiVU' L .t, A l\ALl ::,1.::, .K...t..\,L UL.) 1 :O.l&le Uit>on.tory Ol l'ubl•r li e>lth
P.O. Bo x 28047, 306 N. Wilmini;,on Street
Raleigh, North Carolin• 2761 l
Site Number Field Sample Num ber tu J. .. 004-SP ----'---------------------------------
Name of Site WA-R.i2-t.J GorJT'i PGr:, l.DFL Site Location A FT"o 10 N (_ _,.c____,:, _ _:_:;___:_;"-------='--------------
Collect ed By a. t0, CHO 1..-~),...) ID# ;3-=f, Date Collect ed Z 0 :/vi. Y '1~ Time OZ5'o
M , Pe,;,AJ1:>e1<Tc~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds -----
Sample Type Inorganic Co mpounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium
Se-z:>onEAJr ----__ G round wa ler (1) _ Solid (5) Cadmium --Chrom ium
720 LLJA.} .5 'Tl2 £ 19 /Yl
--__ Surfa ce wa ter (2) Liquid (6) Lead --
{)µA/,JA?£l:::> ---Mercury
Soil (3) _ Sludge (T) I/Z,-B . Seleniu m ----Silver --L Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1 ) (mg/kg) Organic Comp ounds Res ults(mg/1)
P&T:GC/MS Arseni c benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------< d ,I" .,..,..'! ... , -2{__ PcB Chloride chlorobenzene
~ --/~ Chromium chloroforr,1 ------
--__ Copper o-cresol --Fluoride m-creso l ------
--Iron p-cresol ----Le.ad cresol ------
--__ Manganese --1,4-d ichlorobenzene
--__ Mercury --1,2-d i ch I oroelh ane
--Nitrate 1, 1-dich loroel h ylc nc ----Selenium 2,4-dinitrotoluene ----Silver hcptachlor ----R adi ochemi stry Sul fates hex.a ch lorobenzene ----Zinc hexachlorobutadiene ----Pa ra meter Res ults (PCi/1 ) pH hexachloroctha ne ----
---· Gross Alpha __ Cond uc tivity --methyl ethyl ketone
Gross Bela TDS nitrobcnz.ene ------TOC pentach lorophenol ----
----pyri dine ·--Microbi olo gy ----telr achloroel h ylene
----lrichloroclhylcne
Parameter Res ults (Col/l 0Oml ) 2,4 ,5-tr ichl orophcnol ----
----2, 4,6-trichlorophenol --
----vinyl chloride --endrin --lindane
Date Received 7 -~'J'-7'/'f//61J Rcpor ted by --
--mcthoxychlor
"i'-S:-9~ 7/P --loxaphcne
DJte Extract ed Date Report ed 2,4 -D --
:?-9-~¥YP 942792 __ 2,4,5-TP (Silve.x)
Dc1tc A nalyzed Lab Number ---DI IS 31')1 (P.cviscd 2/91)
I lcailh, &. Natural Resources
Solid Waste Management Di,;sion
P.O. Sox 2W7, 306 N. Wilming,on Street
Raleigh, North Carolini 2761 J
Site Number Field Sample Number t,,,UL. -t:>C>S-:!:,.:Z:, -----------------
Na me of Site WA-1<.i2E:i-J CorJT't PC"B l.DFL Site Location A F,o 10 l\J C _.!..,_:,___:.___:_:::....:...:,c__ _ __c_:-==-------------
Collected By a. ('v I c.Ho L. 6c;>)...) Date Collected Zt!B .:ZVLY 9...,
A. Po,,..,7:>E)t.Tt-'S!, .
Agency: Hazardous Waste X Solid Waste. ____ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium
5e-Z> /~ 6 A.J r ---· __ Ground water (1) _ Solid (5) Cadmium --Chromium
2J:x.v,u'5r.ecr,/Y1 --
__ Surface water (2) _ Liquid (6) Lead --
VAJ,Uri M..FD ~P, --Mercury
Soil (3) _ Sludge (T) Selenium ----Silver --X Other (4) _ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS A.rsen.ic benzene ------Acid:B/N Ext. Barium ca rbon tetrachloride ------'MTBE Cadmium chlordane ------< p. / (J flLJffi.. _x_ pc:e, Chloride chlorobenzene ~-,, Chromium chloroform ------__ Copper o-cresol ----Fluoride m -cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichlorocthanc
Nitrate -1,1-dichloroeth ylenc ------
Selenium 2,4-dinitrotol ucnc ----Silver heptachlor ----
Radiochemistry Sulfates hex.a ch lorobenzenc ----Zinc hexach lorobutadiene ----Parameter Results (PCi /1) --pH hcxachloroeth ane --
--Gross Alpha __ Conductivity --methyl ethyl ketone
G ross Beta TDS nit robenzcne ------TOC penlachlorophenol ----pyridi ne ----Microbiology ----tetra chloroct hylcne
trichloroethylcne ----Parameter Results (Col/l00ml) __ 2,4,5 -trichlorophenol --
------2, 4,6-trichJorophenol
------vin yl chlori de
endrin --lindwe
Date Received 7-,:lf-ff~ "31) Reported by --
--methoxychlor
?-i-?fi'11/' --toxaphcne
Da te Extracted Dale Reported 2,4-D --
Dale A nalyzed '7--f-f4'---pf} 942793 --2,4,5-TP (Silvex)
Lab Number
DI IS Jl'Jl (!Zeviscd 2/91) --
I
'"'·'--uepar.ment of l:.nvironmcfft,
I icalth, & 1','a1 ·"ra\ Rc.<0urccs
Solid Waste Management Di,ision
~A.JY1r1.::...r; J-\..1"""7\..-L1 .. ,·10· "I"\J........\l_ u -r..:;....)· 1 ---;.3u1n:· 1....,&vunnury UI I UUIH . .-nc.111111
Site Number -----------------
· P.O. !}ox 28047, 306 N. Wilmin£10n Street
RAieigh, North C..rolin• 2761 l
Field Sample Number tvL -06>5 -,:5l,,(}
Name of Site WA-R.i2.t.J GorvTY PCt, l.DFL Site Location A F",o ,0 NC _..<......:._...:...::::....C..:"-...---=--=c__-----------
Collected By G;. {'v 1c.H.0L.6o"1J ID# ;3-={-Date Collected ,:::lf3 Jtlt. Y C?4-Time 0841--o
hi. Po,~v~rt-R X TCLP Compounds Agency: Hazardous Waste Solid Waste ___
0
S uperfund -----
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) £)vw~5-r.eE,J/J? Cadmium --Chromium --J5.._ Surface water (2) _ Liquid (6) O'..U/4/...9#~ 772115. Lead --Mercury --Soil (3) Sludge (1) Selenium ----Silver --_ Other (4) _ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
<e:,. """/ ~ R:..B Chloride chlorobenzene ----Chromium chloroform ------__ Copper o-crcsol ----Fluoride m-cresol ------
--Iron p-cresol ----Le.ad cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dich loroethane --
--Nitrate 1, 1-dichloroet hylene ----Selenium 2,4-dinitrotolucne ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hcx.achloroethane ----
--Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzcne ------TOC pentachlorophenol ----
----pyridine
Microbiology ----t etrachlorocth ylen e
----trichloroethylene
Parameter Re sults (Col/l00ml) __ 2,4,5-trichlorophenol -------·-
----2,4,6-trichl orophcnol --
--vinyl chloride ----endrin --lind;rne
7-;i_r-r~l/lf!dl)Rcpo rted by --Date Received methoxychlor --;,,, toxap hene
O<.1lc Exlraclcu --2::.L_-9//7/~Jd Date Reported --
--2,4-0
O<.1lc Analyzed ~2._-9¢;/,f? 942794 _ 2,4,5-TP (Silvex)
Lab Number --DI IS 3191 (!Zcviscd 2/91)
N.C. Depar.ment or Environment,
l lcalth, & l',atural Resources
Solid Waste Management Di,ision
SAMPLE ANALYSIS REQUEST State Laboratory or Public Health
· P.O. 13ox 2.S0-:7, 306 N. Wilmingion Street
RAieigh, North Carolina 2761 I
Site Number ----------------Field Sam pie N urn bcr_-'W==--=-...c/......;..._-_(!:)_0-'/_-_/..._d ______ _
Name of Site WA-R.i2.€:..J Gat.Jn' PGt, U,FL Site Location A F"To ,v N (_ -.L..:.--'-.....:....::::....:...:,:__ _ __c.._;-='------------
Collected By a. ('\) IU·tO I.,. 6c>~ ID# 3=1--Date Collected 2-'iJ' 7tJL. Y q4 Time I.Boo
~-~TePH.e,...,5
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentra te Comments Arsenic --Barium
X_ Solid (5) L!'M.J'i>,: IL'-
---· __ Ground water (1) Q,ey Cadmium --Chromium
C!oA.J rE"AJT..S
--__ Surface water (2) Liquid (6) Lead --
w/1:cD --Mercury
_ Soil (3) _ Sludge (7) :5/DJ..IT Selenium --Silver --_ Oth er (4) .rc-ool-1-C _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_x_P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
Nitrate 1,1-dichloroethylene -
------Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Su lfates hexachlorobenzene ----Zinc hexachlorobut adiene ----Parameter Results (PCi/1) pH hcxachloroelhane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----I etr achloroeth ylene
trichloroeth ylene ----Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophcnol
------vinyl chloride
endrin --lin dane
Date Received 7 -,?f-,?'?('~,&Reported by --
--methoxychlor
--toxaphcne
D.itc Extracted Dale Reported 2,4-D --
8 -5 -q 4---n w--__ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number 942795 DI IS Jl'JJ (Revised 2/91) --
j'\,.'-~ UC}JJJ ,1111..Jll Ul J..-IIVIIVIIIJ1(..Jll,
I k alth, & Natural Res.ource,
Solid Waste Management Di,~sion
U~l,A...1-.L...J.L; r,...J, ,_.,._,.__.,,J.. '-',11,..'--' A'--'"--"'-.(_.._.,....._,,~_,..-..
P.O. &,x 260-:7, 306 N. Wilming1on S1rcc1
R..alcigh, North Carolini 2761 I
Site Number Field Sample Number WJ...-cJOI-J..,C _ __;::.....:;......c..._ _____________ _ -----------------
Name of Sile WA-'2.i2.t ~ GarvTi PGt;, l.D FL Site Location_LA...:....:..F_T...:....:::0:...:,-J:.=.. _ _:__N~C::.._ _________ _
Collected By G . f\) 1 LH.o l-6c;>)-..) Dale Collected Z"iJ' 7tJt-'/ Cf-4-Time / .I:i'Ot)
<;.. ::.Tel>He-.JS
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
)( Solid (5) ---· __ Ground waler (1) {2,ey LtMJ'i>PIL<-Cadmium --Chromium
Co A.Jr E;A.JT.5 --__ Surface waler (2) Liquid (6) Lead --
w/t=ca --Mercury
Soil (3) _ Sludge (7) SPJ..17 Selenium ----Silver --
_J,.. c. -oo I-t...C-Other (4) _ Other (8) ' ----
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ----
~o)T
Cadmium chlordane
.3 0 /,'I¥''"
----Chloride chlorobenzene --~-7-Chromium chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1, 4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rotol uene ----Silver heptachlor ----Radiochemistry Sul fates hexachlorobenzene ----Zinc hexach I orobu tad iene ----Parameter Resu I ts (PCi/1) pH hexachloroelhane ----
--Gross Alpha __ Conductivity --methyl ethyl keton e
G ross Beta TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
Microbiology ----· t e tr achloroet h ylene
trichloro ethyl eo e ----Parameter Results (Col/l00ml) 2,4,5-trich lorophenol ----
------2, 4,6 -tri chl orophcnol
------vinyl ch loride
endrin --
1-,L'f-f~Rcportc d by
lind ane
Date Received --
--methoxych lor
~-S -9¢11/J --tox aphene
Dote Extract ed Date Reported '2,4-D --
Dale AnalyLcd ~-9-?~-V/J) 9,12796 2,4,5-TP (Silvex)
Lab Number --DI IS 31'}1 (IZcviscd 2/Yl)
t,:.C. Dcpanment of Environment,
l lcalth, & Natural Resources
Solid Waste Management Division
SA.11PLE ANALYSIS REQUEST State Laboratory of Public Health
Site Number ----------------
-P.O. I3ox 2SO-l7, 306 K Wilmington Street
R.alc:igh , North Carolina 27611
Field Sample Number WL-eo 2 -/,.. C.
Name of Site WA-R.i2.e.J C1ot-JT'1 PGt, u,FL Site Location A F"To ,-J NC.., -~-....:.....:::....:....::,c__ _ ___:.--='------------
Collected By a . (\) 1 U-to L. e,o"-,) Date Collected# ,,7..?, :JvLY ~4-Time / S-oO
C. s. . SfcP-Hel-J
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds RcsuHs(mg/1)
Environmental Concentrate Comments Arsenic --Barium ----
Ground water (1) X Solid (5) t<JET ~7> f:"'/ LL-Cadmium --Chromium --__ Surface water (2) Liquid (6) (!,eA...1r~ Lead --
--Mercury
Soil (3) _ Sludge (7) $P~1r tvl ECO Selenium ----' Silver
_ Other (4) -::,:c. -603 -~~ --
Other (8) &,o/J re~ ~t:> --
TC:::. -60~-LC --
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/~) Organic Compounds Results(mg/1)
X P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
Nitrate -1,1-dichloroethylcne ------Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexach I orobutad iene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC __ pentachlorophenol --
----pyridine
Microbiology ----tetrachloroethylene
----trichloroethylene
Parameter Results (Col/l00ml) 2,4 ,5-trich lorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane
Date Received 7 -.;:l?-?fZ't//J&.J) Reported by --melhoxychlor
;;;, --
--toxaphene
O;ite Extracted Dale Reported 2,4-D --
~-5--q-'-{ ~Lab Number
__ 2,4,5-TP (Silvex)
Dale Analyzed 942797 DI IS 3191 (Revised 2/91) --
N.C. Depa:-tmenl of Environment,
J lcallh, & ,-.;atural Rcs.ourcc~
Solid Wa~te Management Di,ision
SA.?\1PLE A.i~ALYSIS REQUEST Stale Labontort of Public Health
Sit e Number -----------------
P.O. !'k,x 280-17, 306 N. Wilmi nt;ton St:--cc1
Raleigh, Nonh Carolin• 2761 J
Field Sample Number WL-00 2 -"-=C..~-----
Name of Sile WA-R.i2.e.J Cborvrt PC"B l.DFL Site Location A FTo t-J NC -'--'---'-=:.....:....:"----'-..:.--='-------------
Collected By a. rv ll.H.OL,6c,~ ID# 3-=f--Date Collecled # 2.-?, :JVLY c=t4 Time / S-oO
~ . Sf c 'P-H el-' s
Agency: Hazardous Waste X Solid Waste ___ 5uperfund TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental· Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) X Solid (5) t<J~T ~-Z, Fl LL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) t:RA.J rcJ.,..rT5;. Lead --Mercury
tvl ECO --_ Soil (3) Sludge (7) .:Sl't.1r Selenium ,, --
-:J:: C.. -'903 -~ L Silver
_ Oth er (4) --Other (8) /PVP ro12. e'CO --
TC. -t!i>O '?. -LC. --
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds Results (mg/1)
P&T:GC/MS Arsenic benzene ----..J(_ Acid:B/N Ext. Barium carbon tetrachl oride ----'MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fl uoride m-cresol ------
---Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichl oroeth ane --Nitrate . 1, 1-dichloroethylcne ----·· ----Selenium 2, 4-di n i trotol uen e ----Si lver __ heplachlor --Radiochemistry Sul fa tes hex.ach lorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1 ) pH hex.achloroelhane ----__ Gross Alpha --Conductivit y meth yl ethyl ketone --· Gross Beta TDS nitrobenzenc ------TOC penlachlorophcnol ----
----pyridine
Microbiology ----t etrachloroeth ylcnc
--__ trichloroethylenc
Parameter Resu lts (Col/l00nil) 2, 4 ,5-trich loroph enol --
----__ 2,4,6-trichJorophcnol
--vinyl chloride ----endrin --lindane
D ate Received7-;:l?-/?f/'fttL!,2) --Reported by methoxychlor --
{JAi~ --toxaphenc
D:ite Extracted Y-S'-.1/l/t/P Date Repo rted 2,4-D --
?-JJ-1-</ .,6£l 942798 __ 2,4,5 -TP (Silvex)
Date Analyzed Lab Number --1)1 IS J J'JJ (IZcviscd 2/91)
~,'.C.. Dcpar:mcnt o[ Environment,
l lcalth, & t-:a tural R=urccs
Svlid Waste Management Division
SAMPLE ANALYSIS REQUEST State ubontory of Public Hcolth
P.O. Box 7..80-17, 306 S. Wilmingion Street
Raleigh, North Carolina 2761 J
Site Number -----------------Field Sample Num bcr_...c;W_.=:;__L_-_e=--co=---_2 _ ___..L,..____,,,C.. ______ _
Name of Sile. WA-R.i2..e..J CborJT'i PGb l.DFL Site l.oLl.tion A F,o ,.J NC --'----'--__;__::....:...=-----'---'=;c.__-----------
Coilecled By a . (\_) fC.H.Ol,6c)......, ID #_3_-=f--__ Date Collected----'#,,,.__,,7;=~=--~=V~LJ.Y_q-=-------4-Time I S-o 0
C: . S'fei!>-Hel-JS
Agency: Hazardous Waste X Sol.id Waste __ $uperfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ----__ Groundwater (1) X Sol.id (5) toET ~"l> f:°/ LL Cadmium --Chromium --__ Surface waler (2) Liquid (6) u.vr~ Lead --Mercury --Soil (3) _ Sludge (7) .:SP~tr t-vl ECO Selenium --I --
~C.. -C03 -LC Silver
_ O ther (4) --Other (8) t;,o/J ,-C/2. e-c.o --
re::. -6>0 "Z. -LC --
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------~ Cadmium chlordane
LS L~ K.#01. ----
Chloride chlorobenzene --~-~
Chromium chloroform ----
--· __ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1, 4-dich I orobenzeoe
--__ Mercury --1,2-dichloroethane
Nitrate -1, 1-dichloroethylcne ------
Selenium 2,4-di nitrotol uene ----Silver hcptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hexachloroelhanc ----Gross Alpha ----Conductivity methyl ethyl ketone --Gross Beta TDS nitrobe nzene ------TOC pentachlorophenol ----
--__ pyridine
Microbiology ----tetrachloroclh ylcne
trichloroethylcoe ----Parameter Results (Col/l 00ml) 2,4,5-trich lorophenol --
----__ 2,4,6-trichlorophcnol
--vinyl chloride ----endrin --lindane 7-~9-tJt/llt,d-P --Date Received Reported by methoxychlor --
DJte Extracted ~ ';11-9~1/P --toxaphene
Date Reported --2,4-D
Dale Analyzed 'j{_-9'9'~1!,f) 942799 __ 2,4,5-TP (S ilvex)
Lab Number
1)/ IS 3191 (!Zcviscd 2/91) --
t-:.C Depanment of Environment,
l lcalth, & t-:atural Res.ources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box :2S047, 306 t-:. Wilmingion Street
Raleigh, North Carolina 27611
Site Number Field Sample Number W L -0~ I -FL -----'--------'-------------------------
Name of Site WA-gi2€:.J Cbor.JT'I PG"B l.DFL Site Location A F"Te> ,-.J NC ._.L..:._;__....:....=::::....=..=,:___...:.....:-=:____----------
Collected By a. N l(.HOL,6c>~ ID# 3=/-Dale Collected 2'8 .::TPL Y 'f-f Time 09Z6
L 12 e5E
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ---
Sample Type Inorganic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) :s~A.Jr:> NLTbC:... --Cadmium
Chromium --/J1 Er>✓ ,_..A-'L. __ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --_K_ Other ( 4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane --< d . 7 t' 4J,(J,1A._ ----_K_ PC.'B Chloride chlorobenzene ~-,,, . Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex,ichlorobenzene ----
Zinc hexa chlo robutadiene ----Parameter Results (PCi/1) pH hex,i chlo roethane ----
--Gross A lpha __ Conductivity --me thyl ethyl ketone
G ross Beta TDS nitrobenzene ------TOC pentachloro phenol ----
----pyridine
Microbiology ----te tra chloroethylene
----trichlorocthylene
Parameter Results (Col/l00ml) 2,4,5-trichlorophenol ----
------2, 4,6-tri chl orophen ol
------vin yl chloride
endri n --
7 ... ,?f-f~,P~dl) Reported by
lindane
Date R eceived --methoxychlor ., --
D<Jtc Extract c<l~,Y-f///--Vf' --toxaphene
Dale Report ed --2,4-D
D ale Analyzed Y'-{j_·~'JL/ 1//J 942800 _ 2,4,5-TP (Silvcx)
Lab Number --DI IS 31'}1 (Revised 2/91)
N.C Dcpar:mcnt of Environment,
I lcalth, & Natural Resources
Solid Waste Managemeni Division
SAMPLE ANALYSIS REQUEST State Lal>oratory of Public Health
Site Number ----------------
P.O. &ix 2SO-l7, 306 N. Wilminpon Strut
RAieigh, North Carolina 27611
Field Sample Number W L.-00 2 -F'L.
Name of Site WA-R.i:2-€:..J Go,SN PC"B l.I,FL Site Location A F"To t-J NC _.!......:._....:....:::.....:....::,__ _ ___:.-=c...__----------
Collected By a. f\,) ICHOL,6c))..) ID# :3-+ Date Collected 2 0 7VL 'Y '14
L./Zt:>se
Agency: Hazardous Waste X Solid Waste ___ Superf1111d TCLP Compounds -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
C1--1A/.2CJ0AL, FiLrE:12
---· __ Ground water (1) _ Solid (5) Cadmium --Chromium
/f4Fl:>/V.M
--__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) Sludge (7) Selenium ----Silver --~ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsen.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane --PCS <p.7(7 Q._"'-----
~ Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulfates hcx.achlorobenzene ----
Zinc hexachlorobutadicne ----Parameter Results (PCi/1) pH hcx.achlorocthanc ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC pentachlorophcnol ----
--__ pyridine
Microbiology ----tetrachloroeth ylene
----trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----2, 4,6-trichJ orophenol --
------vinyl chloride
endrin --lindane
7 -2_1j -f </-J1/;L/2> Reported by Date Received --
--methoxychlor .. toxaphene 'i'--3--'1¢ 11 p --O;ile Extracted Date Reported 2,4-D --
Dale Analyzc:d_2_-f -f ¢1(/' 942801.
_ 2,4,5-TP (Silvex)
Lab Number --1)11.S 31'Jl (IZcviscd 2/91)
t-,:.C D cpar.mcnt of Environment,
J lcalth, & i':atural Rcs.ourccs
Solid Waste Mandgcrncnt Di,~sion
0AJYH' L.t, AJ'iALl .)L'.) .K.L'xl ur~.::, 1 :-.t •tc LJlD-Oratory 01 l'u Ot1c li c>llh
P.O. Box 2.S0-17, 306 I':. Wilmingion Strccl
RAieigh, North Carolin• 27611
Site Number -----------------Field Sam pie N um bcr __ .....:W::.....=.......:"-::....:.......----.!::t!>~CJ-'-/_-~B~L=-----
Name of Site WA-Ri2.e..J GotJTY Pee, l.DFL Site Location A F"10 ,-J N (_, -~-__:_:c....:...c=--------='-------------
Collected By (;;. f\,), U--t.o \.. 6c,l-,..) Date Collected Z15 ::TVL-Y 94 Time /cJ20
~-$,€PH e,-..._-,S
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Solid (5) aF. W;l'?t"t'i!, Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (7) Selenium ----Silver --x__ Other (4) _ Other (8) --'
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
15._P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachl orid e ------"MTBE Cadmium chlo rd ane ------Chloride chl orobenze ne ----~-
Chromium chl orofo rm ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichl orobenzeoe
--__ Mercury --1,2-dichl orocth ane
Nitrate -1,1-di ch loroet h ylcne ------Selenium 2,4-d i nitrotol ucne ----Silver heptac hl or ----
Radiochemistry Sulfates hex.a ch lorobenzene ----Zin c hexac h lorobut ad iene ----Parameter Results (PCi/1) pH hex.ac hloroethane ----__ Gross Alpha __ Conducti vity --methyl et hyl ketone
Gross Beta TDS nitrobenzene ------TOC pen tac hl orophenol ----
----pyr idin e
Microbiology ----tetra chloroeth yl ene
tri chl oroethyle oc ----Parameter Results (Col/lO0ml) 2,4,5-trich lorophenol ----
----2, 4 ,6-t ri chJ oro phenol --
------vi nyl chl ori de
endrin --lin d,rne
Date R eceived 7 -e:/j'-ff(J/f&LJRe portcd by
--
--meth oxych_lor
toxaphene --DJtc Extracted Da le Reported 2,4-D --
D<Jlc Analyzed ~-/ -q4 7lMJ: Lab Nu mber 9 ,\2802 2,4,5 -TP (Silvex)
--DI IS Jl'Jl (H.cviscd 2/91)
;-,-.l... ucpar.mcnl 0( tn"lronnlcnl,
l lcalth, & J';aiural Rc.s.ourccs
Solid Waste Management Di,-ision
UH,..Jl'.ll. LA.'J r1...1 ,/""),..J._J.l. ..JJ..U J..'-..J.....,,'..t.. V..L...,J ..l
P.O. Box 280-l7, 306 J';. Wilmini;ion Street
Raleigh, North Cllroli n• 2761 I
Site Number Field Sample Number W L -0 O 2 -i3 L -----------~-----------------------
Name of Site WA-1<.i2E:.J CborJT'I PCt:i lr,FL Site Location A F',o t-J NC, --'-------''-----------------
Collected By a. (\) 1 l.H.O l-6c>)-..) Date Collected 2B -;;J'C)l Y -==,4 Ti.me / l-10
a, p ~ . S.Tt t-t~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Rcsulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· l>. I-. __ Ground water (1) Solid (5) tuATrR Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) Selenium --Si lver --L Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
_x_ P&T:GC/MS Arsenic benzene ----Acid:B/N fat Barium carbon tetrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
----Mercury 1,2-dichloroethanc --Nitrate -1, 1-dichloroet hylene ------Selenium 2,4-di nitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobenzenc ----Z inc h cxa ch lo robu lad iene ----Parameter Results (PCi/1) pH hex;ichlo roethane ----__ Gross Alpha __ Conductivity --meth yl ethyl ketone
Gross Beta TDS nitroben7,ene ------TOC __ pentach lorophenol --
----pyridine
Microbiology ----tetra chloroeth ylene
----trichlorocthylcne
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophcnol --
------2, 4 ,6-l richJ orophenol
------\~nyl ch loride
cndrin --lind:rne
Date Received 7-,,l9-ft/ ti/, BLJ Reported by --melhoxychlor ;;, --
--toxaphcne
D:ile Extracted Date Reported 2,4-D --
c;,-, _q'f ·nur 942803 __ 2,4 ,5-TP (Silvex)
Date Analyzed Lab Number --I)I IS 3191 (l(cviscd 2/91)
N.C Department of Environment,
I lcalth, & Natural Resources
Solid Waste Management Di,~sion
SAMPLE ANALYSIS REQUEST State L&bontory of Public He1lth
· P.O. Box 2&0-l7, 306 N. Wilmington Street
RAieigh, North C.rolin1 27611
Site Number Field Sample Number tuL -~03-BL ------~---------------------------
Name of Site WA-R.i2.€:..J C1orvN PC.'B u,FL Site Location A F"To ,.J NC _.:......:__...c....:;:__.:....:::;.__ _ ___;;_-=-----------
Collected By a. f\,) ll.H.OL,6c>"'-> Date Collected zg -:TtlL 'I 91-Time /-14-5'"
~ .S~He>v~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· Ground water (1) _ Solid (5) t>. F. /.UATe~ --Cadmium
Chromium --Surface water (2) _ Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --Ji_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
L P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese 1,4-dichl orobenzene --
--__ Mercury 1,2-dichloroethane --Nitrate -__ 1,1-dichloroethylcne ----Selenium 2, 4-d i ni trotol u ene ----Silver heptachlor ----Radiochemistry Sulfates hex.ach lorobenzene ----Zinc hex a chlorobu t adiene ----Parameter Results (PCi/1) --pH hex.achloroelhane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC __ pentachl o rophenol --
----pyridine
Microbiology ----tetrachloroeth ylene
trichloroethylene ----Parameter Res ults (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane
Date Received Z-.2.r-t<frt@Rcported by
--
--methoxychlor
__ toxaphene
Dc1tc Extracted Date Reported 2,4-D --
'?-;1-9'-/-~ Lab Number 942804
_ 2,4,5-TP (Silvex)
Dc1lc Analyzed --DI IS 31')1 (Revised 2/91)
N.C Depanment of Environment,
l lcalth, & l','.atural Resources
Solid Waste l\fanagement Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
· P.O. 13ox 280-l7, 306 N. Wilmingt0n Street
Raleigh, North Carolina 2761 I
Site Number ----------------Field Sam pie Nurn bcr_---=-tlJ=-.::.c:L._-......,O,,-,:.,,t)~4,....._-_,B=-_L ____ _
Name of Site WA-g;2.e...J Gor..:irt PG"& U>FL Site Location A F",o ,v NC _.L.:......:.._....:....!:~~-...:......:C-='------------
Collected By ~ . f\,) 1 U-to \.. 6::::,)-.) Date Collected ;1$ Jtll.'f 4+
~ , STEP tt e:,.::>.C.
Agency: Hazardous Waste X Sol.id Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) _ Sol.id (5) t). ,c:-: Wtf116:°ie Cadmium --Chromium
__ Surface water (2) A-tR /-(-('),$~ --Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (T) Selenium ----Silver --A Other (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/ki) Organic Compounds Results(mg/1)
..x_P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------
Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Lead ,cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1,1-dichloroethylene ----Selenium 2,4-di ni trotol uene ----Silver heptachlor ----Radiochemistry Su If ates hex.achlorobenzene ----Zinc hexachlorobutadienc ----Parameter Results (PCi/1) pH hcx.achloroethanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pcntachlorophenol --
----pyridine
Microbiology ----tetrachloroeth ylene
----trichloroethylcne
Parameter Results (Col/l00ml) 2,4 ,5-trich lorophenol --
----__ 2,4,6-trichlorophcnol
------vinyl chloride
endrin --lindane
1-;l..'t-f ~fl/ L/.LJReported by Date Received --methoxychlor
.7 --
--toxaphcne
O;.ite Extractec.l Date Reported 2,4-0 --
Dute Analyzed ?f' -:J,..-91-/ ,UJr Lab Number 942805 _ 2,4 ,5-TP (Silvex)
DI IS 3191 (ll.cviscd 2/91) --
·-
I leallh, &. /',°atural Resources
Solid Waste Management Di,~sion
..J~Q,._. ~.._...._,, .. ,v,, Vl J VUl1 ... J 11..(ll~JI
P.O. Box 280--17, 306 ts:. Wilming10n St n:ct
Rlilcigh, North Carolin• 27611
Sile Number -----------------Field Sam pie Numbcr _ ___::,W __ L_-_O----=O=---l_-_t;,,--=-VJ ____ _
Name of Sit e WA-1<i2e.J CoNTY PC.t> lr,FL Site Location A FTo ,-J N (., _..!._C_....:_....:...,:::.....:..:::,__ _ __c_c--==-------------
Date Collected e, 'c3 :J t.>L-/ C\ 1-Time /13£"
T. U-J/41...KE:/e..
Agency: Hazardous Waste X Solid Waste ___ Supcrfu.nd TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
ti ----
~ Ground water (1) Solid (5) Wet..L I Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --
Soil (3) Sludge (7) Sdenium ------Si lve r --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resu!Ls (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_x_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride rn-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroeth ane
--Nitrate 1, 1-dichloroethylene ----Seleniu m 2,4-dini t rotol uene ----Si lver heptachlor ----Rad ioc hemistry Sulfat es hex.achlorobenzene ----Z in c hex a ch I orobu tad iene ----Parameter Results (PCi/1) pH hex.achloroethanc ----
--Gross Alpha __ Condu ctivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophcnol ----
----pyridine
M icrobi ology ----tctrachloroeth ylene
trich loroeth ylcne ----Parameter Results (Col/l00ml) 2,4,5 -t rich lorophcnol ----
------2, 4,6-l richlorophenol
------vinyl chloride
endrin --lind:rne
7-.,2!1-ftltt LIL)Rcportcd by
--Dale R(:ccived met hoxych lor --toxaphenc --· Dote Extracted Date Reported '.2/i-D --
<? -~ -C/ 4-711.J,J 942806
__ 2,'1,5 -TP (Silvex)
Dole Anc1ly1.cd Lab Number --DI IS Jl'Jl (!Zcvised 2/91)
I lcalth, l-:. /\:alural Rcwurccs
Solid Wa~lc Management Division
Site Number -----------------Field Sample Number
P.O. Gox 2.80-17, 306 /\:. Wilminpon S1rcc1
lukigh, Nor1h Carolin• 2761 l
WL-001-<;,w ------------------
Name of Si te WA-R.i2.e.J GorvT'l' PCt:> U)FL Site Location A FTo 10 NC -~---~---------------
Collected By G;. {\) tCHo L 6Q)...) Date Collected G 'c3 :J U-L-/ ~ 1-Time /13£"
T (,,U"'> l--k !:le....
Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic • --Barium tt ---· _l{_ Ground waler (1) _ Solid (5) WEL.L I Cadmium --
Chromium --
Surface water (2) Liquid (6) Lead ----Mercury --
Soil (3) _ Sludge (7) Selenium ----Silver --
__ Oth er (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/J) (mg/kg) Organic Compounds Resul ts(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------'MTBE Cadmium chlordane
A-PC.B IPt:E>T <:e,, OQt:1 I ----Chloride chlorobenzene r --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Le.ad cresol ------
----Manganese 1,4-dichlorobenzcne --
----Mercury 1,2-dichloroethane --
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinit rotol uenc ----
Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----
Zinc hexach lorobutadienc ----Paramell'.r Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha __ Cond uctivit y --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophen ol ----
----pyridine
Microbiology ----tetra chloroeth yl en e
----trichlorocthylenc
Parameter Resu lts (Col/l00ml) __ 2,4,5-trichlorophcnol --
----__ 2,4,6-trichlorophcnol
------\~nyl chloride
cndrin -----
Date Received 1-,,2 ?-'/')(1'~ t!,_j) Reported by
lind:rne --
--mcthoxychlor ,,
toxaphenc
f'-/-9L/1//jAd --0;,ile Exlrac(cc.l Date Reported 2,4-D --
Y-~ -9(/7/,::, 942807 __ 2,4,5-TP (Silvex)
Date AnaltLcd Lab Number --DI IS 31~1 (IZcvis cd 2/91)
..
l lcalth, & Satural Re~urccs
Solid Waste Management Division
~--· .,.._,.,. ........ ,,.. ........ .,, ......... ~., ... ...., .......... 8'..........._..x ..._,.,,.__,._..,,.,. -.;, ............... v-v,a ,vJ.,' VI I u v 1, ... I 1"-0l~Jl
P.O. Gox 2S0-17, 306 S. Wilmini;,on Str::ct
Raleigh, North urolin• 27611
Site Number -----------------Field Sam plc Numbcr_--=-W-'-_L_-_0---=0:........:./_-_(;,_.:_W _____ _
Name of Site · WA-R.>2.E:.J Gor--iTY PC.t> l.DFL Si te Location A FTo "-..) NC, _..<.....:._:___:_:~:,:__ _ _:_:_=::::.___ __________ _
Collected By 6. {\) tU-to L 6c:>..._, Date Collected G 'c3 :I VL-/ q 1-Time /13£"
T W~LkE/<.
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Enviro nmental Concentrate Comments Arsenic --Barium
-1:t. ---· ~ Ground water (1) Solid (5) WEt..L ' Cadmium --
Chromium --
__ Su rface water (2) Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arseruc benzene ----_x_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------
Chloride chlorobenz.ene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenz.ene
--__ Mercury --1,2-d ich loroethane
Nitrate 1, 1-dichloroethylcne ------Seleni um 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch I orobenz.ene ----
Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroeth ane ----__ Gross Alpha __ Conductivity --methyl ethyl ket one
Gross Beta TDS nitrobenz.ene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----t e t r ach loroelh yl ene
trich loroelhylenc ----Parameter Results (Col/lOOml) 2,4,5-trich lorophcnol --
----__ 2,4,6-trichl orophenol
----vi nyl chloride --endrin --
7-.2/t-ffft&J lind:rne
Date Received --Reported by --mcthoxychlor
U;.ite Extractcd]r-J-ql./ k4 --toxaphene
W&-Dale Reported --2,4-0
D;.i!c AnalrLcd <i__-J.-7</ al) 942808
__ 7.,4,5-TP (Silvex)
Lab Number --DI IS 31~1 (lscviscd 2/91)
I lcallh, & /':atu ra\ Rc.s.ourccs
Solid Waste Manai;cmcnt Division
Site Number -----------------
--------·-·-·-·) ~·. --··· ...... .. · P.O. Box 2.W7, 306 N. Wilmini,:ton Street
Raleigh, North C.,,ro\in• 2761 l
Field Sample Numbcr_....:Wc...::......:c.../.._---=O:.....l>_:__,,Z,,__-_'1=1.-._W-'-------
Na me of Sile WA-R.i2E:..J Cbor0r-t PC"B l.DFL Site Location A F"To ,-.J NC --'--'--...:....::::....:..::::__ _ __;c....=::........-----------
Collected By 6 . (\) 1 c.H.o L 6o.._, Dale Collected Z~ :/ cJ L '/ 9-4 Time /135
T. lA..,1,:,1-JcER
Agency: Hazardous Waste X Solid Waste ___ Su perfu.od TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
JS_ Ground water (1) Hz ---· Solid (5) WE 1.L Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --Soil (3) _ Sludge (7) .5P~J r t-<J/ /:Co Selenium --. --Silver --
--Other (4) _ Other (8) re-001--c;;w --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (m g/kg) Organic Co mpou nds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride
-.~ ----Cadmium chlordane ----A-e;, <o. ooo/ Chlorid e chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylen e ----Selenium 2,4 -dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----Zinc hexach lorobutadiene ----Parameter Resu I ts (PCi /1) pH hcx.ac hloroclhane ----
--Gross A lpha __ Conductivit y --methyl ethyl ketone
Gross Be ta TDS nitrobenzene ------TOC pent achlorophenol ----
----pyridine
J\·1 icro bi ology ----tetrachloroeth ylene
----tri chloroelhylene
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----vinyl chl oride --endri n --
7-;l.'f-fr/-Jlt,&!Keported by
lindanc
Date Received --
--metho;,;ychlor
O;ilc Extracle<l "K_-/-9//1/,P.,A.i --toxaphcne
Date Report ed --2,4-0
7 __ 2,4,5-TP (Si lvex)
Dale Analyzed ~ -;;/._ -2¢1/ p . Lab Number 9 42809
D I IS 3l 'Jl (ll cviscd 2/91) --
J'"'\.l-. U CJJJ il!llCIH UI cnvirunmcnl,
l lcalth, t.:. ~atural Re.s.ourccs
Solid Waste Management Di,ision
t,Jr)....lf.&...I. J,,......J4...-, r),..J. ,r>,..J..J..L .J.LL.I ............... \,,,l VJ......,..J .l.
P.O. Gox 280-17, 306 )';_ Wilmini;ton Street
Raleigh, North C..rolin• 27611
Sile Number -----------------Field Sample Numbcr __ W_L __ -~O_lJ~ZC.....-----'~~-VJ _____ _
Name of Site WA-Q.i2.E:.J Gorvrt PC."B l.oFL Site Location A FTo,v NC --'----~---'-''------=------------
Collected By a . {\) IC.H.Ol,6c:>-.....> Dale Collected Z'8 :J L) L "'1 9'4 Time /135
-r. C,,LJ A '-~ e,e_
Agency: Haurdous Waste X Soud Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concen tra le Comments Arsenic --Barium
~ Ground waler (1) .Hz ---· _ Solid (5) We 1.L-Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) Sludge (7) .SP~1r t-v/ ./:Co Selenium ----Silver --
--Other (4) _ Other (8) re-001--'i w --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pa.rameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ----__x_ Acid:B/N Ext. Barium carbon tetrachloride ----"MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform -------__ Copper o-cresol ----Fluoride m-cresol ------Iron p-cresol ------Lead cresol ------
----Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethane --Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch lorobenzene ----
Zinc hexach lorobuladiene ----Parameter Results (PCi/1) pH hex.achloroelhanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzenc ------TOC __ pcnlachlorophcnol --
----pyridine
i\1icrobiolo gy ----lctrachloroethylcne
----trichloroethylenc
Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophcnol
------vin yl chloride
endrin --
7-~3/-9fl///~Reported by
lindanc
Date Received --
--methoxychlor
.7 toxaphcne <l -oJ -q¥ AB;Wv D ate Reported
--Dole Extract ed 2,4-D --
9, r:J. -CJ tf 8i9 942810 _ 2,4,5-TP (Silvex)
Dole A mdyLcd Lab Number --DI IS Jl'JI (ltcviscd 2/91)
i'-.l....-ucp3r----.mcnt o: tnvironmcnt,
I lcai,h, &. r-;atur.il Rcs.ourccs
Solid Waste Management Division
Sile Number -----------------
..)ldlC: LllL'-Uf"Ill)f""j l)l r UU\ll r-iCZlllll
P.O . Box 2.SO-l7, 306 K Wilminpon Street
Raleigh, North Carolin• 27611
Fi cl d sample N um bcr _ _.:W:...=:....-=-L,."---------=t)==--=l)'-"'z'------'G~-=-VJ-=------
Name of Sile WA-k2.i2.E:.J Gor0T'I PCB U)FL Site Location A F"To 1'.) NC _..:..._ _ _:_.::......;_::::_ __ _ccc...._ __________ _
Collected By 6 . f\) t U-1.0 L 6o)....) Dale Collected Z'S :I l.) L--/ q4 Time /135
T. WA l-tc E= ,a
Agency: Hazardous Waste X Solid Waste Superfund TCLP Compounds ---------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium L Ground waler (1) .Hz ---· _ Solid (5) w~1.L. Cadmium --Chromium --__ Surface waler (2) _ Liquid (6) Lead --Mercury --Soil (3) _ Sludge (7) .5P~I, tA..J/ FC..o Selenium --. --Silver --_ Other (4) _ Other (8) re-001-'iw --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pa.rameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
LP&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------
MTBE Cadmium chlordane ------
Chloride chlorobenzene ------Chromium chlorof 0rm ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dich lorobenzene --
--__ Mercury 1,2-dich loroethane --
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinilrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity methyl ethyl ketone --G ross Beta TDS nitrobenzene -------TOC pentachlorophenol ----
----pyridine
i\1icro biology ----tetra chloroeth ylene
----trichloroethylene
Parameter Results (Col/lOOrnl) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichJorophenol
--vinyl chloride ----endrin --
7-~//-Y ~'P/!J6JJ Reported by
lindane
Dale Received --
methoxychlor ;, --
--toxaphene
O;itc Extracted Dale Reported 2,4-D --
? -~ -q '-1 '-fl.llf' __ 2,4,5-TP (Silvex)
D;ilc Analyzed Lab Number 942811 DI IS 3l'JI (1,cviscd 2/91) --
..
I ka:1h, & /\';,tural Re.sources
SoliJ Waste Management Di,ision
Site Number ---,----------------
P.O. !}ox 28-0-17 , 306 N. Wilmini;,on Strcc:
R.idcigh, Nonh urolin• 27611
Field Sample N um bcr_---=.tu....:__t.'----0_0'---='3==-----"~=--W'-------
Name of Si te WA-R.i2.e..J Cbor..:>T':>' Pc:i) lr,FL Site Location A F",o l's) N (_ -~...:.___:_::::....:....::::...._ _ _c_::......=::..__ __________ _
Collected By a' N ll.H.OL6(::n-.J ID# :3-=/--Date Collected 21! ::JULY q-4 Time /&OO
L.. /2oSE
Agency: Hazardous Waste X Solid Waste Supcrfu.nd TCLP Compounds ---------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
'#3 Barium ---· Ji_ Ground water (1) _ Solid (5) WELL Cadmium --Chromium --_. __ Su rface water (2) _ Liquid (6) Lead --Mercury --Soi l (3) Sludge (7) Selenium ----Silver --_ Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsen.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------
'MTBE /4 Cadmium chlordane ----
X ~t=:?7 <"0. 0 "" I Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead crcsol ------
--__ Manganese 1,4-d ichlorobenzene --
--__ Mercury 1,2-dichloroethane --
--Nitrate 1, 1-dich loroethylene ----Selenium 2,4-dinil rotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexach lorobenze ne ----Zinc hexach lorobu tad ienc ----Parameter Res u I ts (PCi/1) pH hcx.achloroethane ----
--Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobcnzene ------TOC pentach loroph enol ----
----pyridine
i\1icrobiology ----tetrachlo roeth yle ne
----trichloroethylen e
Parameter Resul ts (Col/l0Oml) __ 2,4,5-trich lorophenol --
----__ 2,4,6-trichJorophcnol
----vinyl chloride --endrin --lin dan e
7-el{f-[W ,d--2)Reported by --Date Received mcthoxychl or --
Dale Extracted '%'-~-N J/P..BJ)Ja le Reported --toxaphene
--?.,4-D
7 __ 2,4 ,5 -TP (S ilvex)
Date Analyzed '3-~-9$/~ · Lab Number 9,\2812
I)! IS 3\'JI (l,cviscd 2/91) --
..
I lealth. & Natura! Resources
Solid W;;ste Management Oi,-ision
Sit e Number ---,----------------
P.O. f3ox 2S0-47, 305 N. W ilmini;1o n Street
R.alc igh , Nonh Carolina 2761 l
Field Sample Numbcr __ tu_l-_-_0_0--='3=-----=~'-'--W _____ _
Nam e of Site WA-R.i2.e.J GorJTY PG"B l.DFL Site 1-Dcation A F"10 "-.J NC --'----'---'--_:_:::....:....:::c.__ _ __;,-=:.__-----------
Collected By b. fv ll'...Ho L 6Q),...) Dale Collected 2~ ::JV L. Y CJ4 Time /1,oo
L 12 D$E
Agency: Hazardous Waste X Sol.id Waste ___ SuperfUDd TCLP Compounds ------
Sample Type Inorganic Compounds Rcsu I ts (mg/I)
En vironmental Concentrate Comments Arsenic --
#3
Barium ---· L Ground water (1) Sol.id (5) WELL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --Soil (3) _ Sludge (7) Selenium ----Silver --_ O ther (4) Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ----L A cid:B/N Ext. Barium carbon tetrachlo ri de ----'MTBE Cadmium chl ordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --
Fluoride m-cresol ------
--Iron __ p-creso l --Lead cresol ------
--__ Manganese 1, 4-d ichl orobenzene --
--__ Mercury 1,2-di chlor,oethane --
--Nitrate 1,1-dichl oroethylene ----Selenium 2,4-din itrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hexa ch lorobutad iene ----Parameter Resu I ts (PCi /1) pH hexachloroeth anc ----
--Gross Al pha __ Condu ctivity --meth yl eth yl ketone
Gross Beta T DS nit robrnzene ------T OC prnlachlorophcnol ----
----pyridin e
Microbiology ----tetr ach lor oethylen e
----tri chlo roeth ylenc
Parame ter Res ults (C ol /lO0ml ) __ 2,4,5-tr ichl orophcnol --
----__ 2,4,6-tri chJo rophcnol
--vinyl chloride ----endrin --lin d:rn e
?--i/t/-?f£1(1.d..2JRc porlcd by --Date R e.ceivcd methoxyc hlor --
DJle Extracted ~-l -g}/_ AE Wl::I --toxaphenc
D3 lc Reported --2,4-D 'j __ 2,'1 ,5 -TP (S ilvex)
D al e A nalyzed ~-r:J--9'-/ t3£) Lab Number 942813 --I)! IS 3l'Jl (IZevised 2/9\)
..
I icaltr., & 1'-'atural Rcw urccs
Solid \l,';;stc Management Di,ision
Site Number -----------------
f'.0 . 11ox ?.-S0-17, 306 1','. Wilrnin~o n Street
Raleigh, North C. rolina 27611
Field Sam pie Num bcr __ W __ /.._-_0_0--="3--_~--"--l.A...) _____ _
Name of Sile !J.)A-1<_i2.E:.J C1arvT'1 Per:, lr,FL Site Location A F"To ,._j N (_ --'-----~---------------
Collc.cted By G. f\) 1c.HoL6:::::>""-' Dale Colleclcd 2~ ::J l) LY CJ4 Time /t,oo
I-. /2&>'$1:.
Agency: Haz.ardous Waste X Solid Waste ___ Superfund TCLP Compounds -----
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
'#3 Barium ---· L Ground water (1) _ Solid (5) WELL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium ----Silver --_ Other (4) _ Other (8) --I
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_x_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium car.ban tetrachloride ------'MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------__ Copper o-cresol ----
Fluoride m-cresol ------Iron __ p-cresol ----Lead cresol ------
----Manganese --1, 4-d ichl orobenzene
--__ Mercury --1,2-dichloroethanc
Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-dinit rotoluene ----
Silver heptach lor ----Radiochemistry S ulfates hex,ichlorobenzene ----
Zinc hexach lorobutadienc ----Parameter Results (PCi/1) pH hexachloroelhane ----
--Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentach lorophcnol ----
----pyridine
Microbiology ----lelrachloroeth ylcne
--__ trichlo roethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
--vinyl chloride ----
endrin --lind:rne
Date Received ~-fc/fl/J /1Jkeporled by --
--methoxychlor :;, toxaphcne --Dc1te Extracted Date Reported 2,4-D --
1( _, J -q '+ 'lw.r
__ 2,4,5-TP (Silvex)
Dc1 tc Analyzed Lab Number 942814 1)1 IS JJ'Jl (l(cviscd 2/91) ---
r-,.·.c Dcpa:~mcnt of Environment.
1 lcalth, & ,..;atural Resource<
Solid Waste Management Di,~sion
SAMPLE ANALYS IS K.l:,(JU.t:.')T St,te Laboratory of Pubk Hal,h
P.O. !}ox 2.SO-l7, 306 1'. Wilrnin!;Jon Strce,
R.alcigh, North u.rolina 2761 i
Site Number Field Sample Number W L-004 -~W -----'----------=---------------------------
Name of Site WA-R.i2c..J Gor.JT)' Pct!:> l.DFL Site Location A F,o 10 N (__ _.r.....:.__:__.....:....::::....:..:~-....:.....::....c:::::_._ __________ _
Collected By ~. f\) t<'.'..HOL6C>)-...) Date Collected ..21' :f(.)L,," q4 Time 14-0D
T • t,,t,, 14 L-E k R
Agency: Haurdous Waste X Solid Waste _Superfund TCLP Compounds ------
Sample Type Inorga nic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
WEL.L #4
Barium ---· 1L.._ Ground water (1) Solid (5) Cadmium --
Chromium --__ Surface water (2) Liquid (6) Lead --
w/ --Mercury
Soil (3) Sludge (7) SPt...lT eGo Selenium ----Silver --_ Other (4) :re-002-ee,w _ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsenic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------. 'MTBE Cadmium chlordane
>( @-ftf•6"tiT ----<O. ooo/ Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron __ p-cresol --Le.ad cresol ------
--__ Manganese --1,4-dichlorobenzeoe
--__ Mercury --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylcne ----
Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Su If ates hexachlorobenzene ----Zinc hexach lorobutadiene ----Parameter Results (PCi/1) pH hex,ichloroethane ----
--Gross Alph a __ Conductivit y --methyl ethyl ketone
Gross Beta TDS nitrobenzene -------TOC penlachlorophenol ----
--__ pyridine
Microbiology ----tetra chloroeth ylcne
trichloroethylene ----Parameter Results (Col/l00ml) 2, 4, 5-t rich lorophcno l ----
------2, 4 ,6-lrichl orophcno l
----vinyl chloride --endrin --lin dane
7 -e:l'J-fs/rtg@-eported by
--Date Received methoxychlor --
D;ite Extracted ?-;1..-9//-vf!/:!l)Datc Reported --toxaphene
--2,4-0 ... _ 2,4,5-TP (Silvcx)
D;itc Analyzed g'-.::?-9 ~-r,:' 942815 Lab Number --I)! IS 31')1 (!Zcviscd 2/91)
1'.C. Dcpar.mcnt of Environment,
I lcalth, &. ~alural Rc.s.ources
Solid Waste Management Di,-ision
SAMPLE ANALYSIS REQUEST St•tc ul>ontorf of Public He.Ith
P.O. f3ox 280-17, 306 K Wilmingion Street
Raleigh, North Carolin• 2761 J
Site Number -----------------Field Sam pie N um bcr_-=-W-'--'L=------=0_0_4_---=bt,::..:::....::W'---------
Name of Site WA-Ri2e.J Cbor.JTY PC-t:, /...DFL Site Location A F"1010 NC --'-'--'--....:....:::.....:...:::::...._ _ __:_:~c.__-----------
Collected By C;. ('v IC.HOL,60~ ID# 3-=l-Dale Collected .2~ :f<..)Ly q4 Time {1-0D
T {,,V i&I J,.. I<. t? R.
Agency: Hazardous Waste X Solid Waste --~Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
Wct...L .#4
Barium ---· L Ground water (1) Solid (5) Cadmium --Chromium --__ Surface waler (2) Liquid (6) Lead --
w/ --Mercury
Soil (3) _ Sl udge (7) SPt.1 T e(.,o Selenium ----Silver --_ Other (4) :rC-DOZ.-<e,W _ Other (8) ' --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul t.s (mg/I) (mg/kg) Organic Compounds Results (mg/I)
P&T:GC/MS Arsen.ic benzene ----_2L Acid:B/N Ext. Barium carbon tetrachloride ----.MTBE Cadmium chlordane ------Chloride chlorobenz.ene ----~-Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethanc
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-dinitrotol ucne ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Zinc hex a ch I orob u tad iene ----Parameter Results (PCi/1) pH hexachloroethane ----Gross Alpha --__ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenz.ene ------TOC __ pcntachlorophenol --
----pyridine
J\1 icro biology ----tetra chloroeth yl ene
----trichl oroeth ylenc
Parameter Results (Col /l0Oml) 2, 4 ,5-t rich lorop h cnol ----
----2, 4,6-trichlorophcnol --
----vinyl chloride --endrin --
7 -;;l._'f-fr./-r/J/S..1) Reported by
lindanc --Date Received melhoxychlor
✓ --
DJ le Exlraclcc.l ~ ,.. [-qy b!4 W&-' --toxaphcne
Dale Report ed --2,4-0
7-;i -9'/JJD 942816 _ 2,4 ,5-TP (S il vex)
DJle AnalyLcd Lab Number --DI IS JJ'Jl (!Zc viscd 2/91 )
i','.C Ocp3r.mcnl of Environment,
I lcalth, &. i','a tu ral Rc.s.ourccs
Solid Waste Management Di~ision
Site Number -----------------
::,talc ut>oatory 01 ruo11c tic•lth
P.O. IJ.ox 28(}.17, 306 N. Wilmingrnn Street
RAieigh, North Carolina 2761 I
Fie.Id Sam plc N urn bcr_----=-W-'-'L=---_,:0=--0_4_-__;bt.=--=W=--------
Name of Site WA-1<.i2.e.J CborJTI PCb U)FL Site Location A F"10 ,v NC -.!......:.~_:_._::::...:...,::c__ _ __c__::.....:::=------------
Collected By a . t,J I c.H.o L 6c::::)j,,...) ID# :3-=t-Dale CoU ccted .2~ :ft)Ly q4 Time 11-0D
I . t,,UAL.k'E~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
WE l-L .# 4
Barium ---· ]L_ Ground water (1) _ Solid (5) Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
w} --Mercury
Soil (3) _ Sludge (7) SPuT ec.o Selenium --, --Silve r --_ Other (4) :rc-002-~w Other (8) ' --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
1_ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane ------Chloride chlorobe nzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1, 4-d ichl orobcnzene
--__ Mercury --1,2-dichloroethanc
--Nitrate 1,1-dichlo rocthylene ----Selenium 2,4-dini trotol uene ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutad icne ----Parameter Results (PCi/1) pH hexachloroelhane ----
--Gross A lph a __ Conductivity m eth yl ethyl ketone --G ross Bela T DS nitrobenzenc ------T OC __ pentachl o rophenol --
----pyridine
l\1 icro biology ----tetrachloroeth ylcne
----lrichloroethylenc
Parameter Res ults (C ol/l00ml) __ 2,4,5-trichlo rophenol --
----__ 2,4,6-trichJ o rophenol
----vinyl chloride --e ndrin --lindanc
Date Received 7 -,;J...f -f </pto'beported by --
--meth oxych lor
--toxa phene
Dale Extracted D3lc Reported 2,4-D --
Dale Analyzed~ Lab Number 942817 __ 2,4 ,5-TP (Silvex)
--l)IIS J l'J I (IZcviscd 2/91)
..
1'.C. Ocpar.mcnt of En,1ronmcnt,
I lea Ith, & 1','atural Re.sources
Solid Waste Management Division
.:)i-\...lY.l.r LJ:, A.J'IA.LI ;:,.1..::, I',..L\.l_ UL..) .l C>latc uoor.1ory 01 ruo11c nca11n
Site Number -----------------
P.O. Go, 2SO-l7, 306 1',;. Wilmini;,on S1rcc1
Raleigh, North C:,,rolina 27611
Field Sample Number W L -l::>O 5 -Gz uJ
Name of Site WA-~i2t.J CborvTY PCb U)FL Site Location A F,o 10 NC _..c._:'---......,:_=-...:..::<_ __ _;__=-------------
Collected By C;. f\.) 1c.HoL6c>).J Dale Collected Z~ :1(.)L Y q4 Time / 4D O
-,; ~ A 1,. k e -e_
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
.±1:4 ----£Groundwater (1) _ Solid (5) WELL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --Mercury --
Soil (3) Sludge (7) Selenium ----Silver --
--Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1)
P&T:GC/MS Arsenic benzene ------Acid:B/N E>-i. Barium carbon tetrachloride ----xd!B~J~ Cadmium chlordane ----r<o. """I Chloride chlorobenzene --~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-crcsol ----Le.ad cresol ------
--__ Manganese --1, 4-d ichlorobenzene
--__ Mercury --1,2-d ich loroethane
--Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dini trotolucne ----Silver heptachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexach lorobutad iene ----Parameter Results (PCi/1) pH hex.achloroethane ----
--Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobcnzenc. ------TOC __ penlachlorophe nol --
----pyridine
Microbiology ----t e tr ach loroeth ylene
----trichloroelhylcne
Parameter Results (Col/lO0ml) 2,4 ,5-trich lorophenol ----
----2,4,6-trichl orophcnol --
----vinyl chloride --endrin --
7-,,,Z9-f¢ytl.5'b-cpo rted by
lindane
Date Received --
--mcthoxychlor
5'-:l.-9ffljB12Date Reported
--tox aphene
O;ite Ext rac ted 2,4-D --
D<itc AnCJlyzcd 8"--.R-9~ · Lab Number 9 1.\Z81.8
__ ?.,-1,5-TP (Silvc.x)
--I)! IS 31 ')1 (llcviscd 2/9i )
N.C. Dcpar.mcnt of Environment,
l lcalth, & Natural Rc..s.ourccs
Solid Waste Managcmcn: Division
:'.:>i\.JYl.t' Lt AJ\A.LX .::,1.::, .K.C\..,L UL.:) l .:,tuc U.lX>n.tory 01 t·uo11c r,onn
Site Number -----------------
P.O. Gvx 280-47, 306 K Wilming10n Street
Raleigh, North C..rolin• :!761 l
Field Sample Number W L -E>O 5 -G, uJ
Name of Site WA-Q.i2.E::i.J Gor..JT'I PGt!:> l.DFL Site Location A F,o 10 NC -~-___:_=--.:...:::c._ __ ..:......;=-.. ___________ _
Collected By a. f\j I U--lO \.. 6c,l-J ID# 3-+ Date Collected Z ~ -:f () L '/ '1'4 Time / 40 o
(. ~I'll-kt~
Agency: Hazardous Waste X Solid Waste __ Superfund TCLP Compounds --- ---
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium
.;i¼ 4 ---· Ji_ Ground water (1) _ Solid (5) WE.LL Cadmium --Chromium --
__ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) Sludge (7) Selenium ----Silver --
--Other (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------_t._ Acid:B/N Ext. Barium carbon tetrachloride ----.MTBE Cadmium chlordane ------
Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--· Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichloroethanc --
--Nitrate 1, 1-dichloroethylcne ----
Selenium 2,4-di nitrotol uene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch I orobenzene ----Zinc hexachlorobutad iene --. --Parameter Resulls (PCi/1) pH hex.achloroethane ----Gross Alpha --__ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ------TOC __ penlachlorophenol --
----pyridine
Microbiology ----tetra chloroet hylene
----trichloroethylene
Parameter Results (Col/lO0ml) 2,4,5-trich lorophenol ----
----2, 4,6-trichlorophenol --
--vinyl chloride ----endrin --
7-:lP-f¢(# 8.}faeported by
lindane --Date Received methoxychlor --.,I toxaphene
O;.ilc Ex!raclcd K-l-c.J~ l\,P,, ,J/(:1' --Date Reported --2,4-0
7 __ 2,4,5-TP (Silvex)
O<1lc Anc1ly1.cd <] ... ). -CJ </___89 Lab Number 91\2819
I)\ IS 31')1 (IZcviscd 2/91) --
;-,:_c Dcpar.mcnl of En,ironmcnl,
J lcallh, & ;--:alural Rcs.ourccs
Solid Waste Management Oi,~sion
.'.:>AJYl.t' L.t, AJ\ALX :)1:) .K.C\..L UL.:) 1 :,talc ut>On.tory 01 r u o11c 11crnn
Si te Number -----------------
· P.O. lk>x 280--17, 306 N. Wilmington Street
Raleigh, North urolin• 2761 l
Field Sample Number W L -eo 5 -G, uJ
Name of Site WA-Ri2.e..J GorvN PCt:> lo FL Site Location A FTo ,-J NC _.!.....:._~_:___;:::__:_::,c___ _ ___:_:__:::::::...._ __________ _
Coll ected By ~. f\) tC.Ho \... 6C))...) ID# :3-=t----Date Collected Z'a :1VL -Y q4 Time / 40 o
-r. t,u;,J-Jc't?R.
Age ncy: Hazardous Waste X Solid Waste Superfllild TCLP Compounds ------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
.:I¾ 4 ----_15_ Ground water (1) _ Solid (5) WE.LL Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (7) Selenium ----Si lver --
_ Oth er (4) Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (m g/I) (mg/kg) Organic Compounds Results (mg/I)
L P&T:GC/MS Arsen.ic benzene ----
Acid:B/N Ext. Barium carbon tetrachlorid e ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m-cresol ------
--Iron p-crcsol ----
Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury 1,2-dichlo roethanc --Nitrate 1, 1-dichloroethylcne ------Selenium 2,4-dinitrotol ucne ----
Silver heptachlor ----
Radiochemistry Sulfates hcxachlorobenzene ----Zinc hex a ch Io robu tad icnc ----Parameter Results (PCi/1) pH hcxachlorocthane ----Gross Alpha ----Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene -------TOC __ pentachlorophenol --pyridine ----
Microbiology ----tetr achloroeth ylene
trichlorocth ylene ----Parameter Results (Col/l00ml) __ 2,4,5-trichlorophenol --
----__ 2,4 ,6-trichl orophenol
----vinyl chloride --cndrin --lindane
Date Received '7--29-f¢'1//~eported by --methoxychlor
✓ --toxaphcnc --DJle Extracted Dale. Reported 2,4-D --
'2._-,:}_-CJ..'f 7'1 u]-Lab Number 9,12s20 __ 2,4,5 -TP (Silvcx)
D,!lc Analyzed --1)1 IS Jl'Jl (IZcviscd 2/91 )
1'.C Department of Environment,
l lealth , & 1'a1ural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
. P.O. 13ox 280-47, 306 N. Wilmin&1on Street
Raleigh, North Carolina 2761 l
Site Number -----------------Field Sample Numbcr __ W"--_L_-_<9_(;)=--'-=----<;_-"--v.J'--'------
Name of Site WA-~;2.e...J Gor.JT"t PC"B l...DFL Site Location A F"To ,.J N (__ _..:......:._..c....;::_.:_:::;__ _ _.;.-=-----------
Collected By a. {\) ll.HOL,6c>)J Dale Collected 2 B :rt, L '/ ~ 4 Time IG 30
br . ';:>TEPH ~~
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Rcsulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· L Ground waler (1) _ Solid (5) EARL L1M'=2 WELL Cadmium --Chromium --__ Surface water (2) Liquid (6) Lead --
--M ercury
Soil (3) Sludge (7) ::SPLlr w/ E:GO Selenium ----Silver --
_ Other (4) Other (8) re::::-003• '-JW --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------.MTBE Cadmium chlordane -------<o, OOQ/ _x_ pc.:e, Chloride chlorobenzene ----Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dich loroethane
Nitrate 1, 1-dichloroethylcne -
------Selenium 2,4-dinitrotoluene ----Silver heplachlor ----Radiochemistry Sulfates hex.achlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC pentachlorophenol ----
----pyridine
Microbiology ----telr achloroethylene
----trichloroethylene
Parameter Results (Col/lO0ml ) __ 2,4,5-lrichlorophenol --
------2, 4,6-trichlorophenol
------vinyl chlori de
endrin --
Dmc Rm;v,d 2-.:l.'/-f'P1'?@ cpO'lcd ~//le~ 17 lindanc
__ methoxychlor
--toxaphene
O;itc ExtractccJ~-~-9'/-Jl/'8l)Dalc Rep ned~ t. -Z. ~ 9y --2,4-D
;;, 2,4,5-TP (Silvex)
D;itc Analyzed 'ir-~-W1/,,L' ·. Lab Number 94Z821. --DI IS 31')1 (Revised 2/91)
,''.L. ucp:i:--:r;~,cnt o! i:.n,.,1r\Jnm.:-nt,
I lcalth, L :-.:Jtural Rcwurces
Snlid Waste Management Di,-ision
Sile Number -----------------Field Sa.rnplc Number
l'.O. Dox 2.S0-17, J06 ~-Wilmingion Street
R.,:cigh, Norn, C.r.Jlin• 2701 1
Wi.. -Ot!!J I-L£
Name of Site WA-'<i2E:.J Gar-JT;,' Pct':> l.DFL Site LoCJl!OD A F,o 1--J NC --'--'-__;__:=-:...::,c__ __ ~C......-------------
Collected By (;. f\) 1cH.ol,6'::::n--' ID# 3-=i-Date Collected .:2-'<zs :J' VL Y Cf~ Time / / Z.o
t., /20S'E.
Agency: Hazardous Waste X Solid Waste ___ Superfund TCLP Compounds ------
Sample Type In organic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Groundwater (1) _ Solid (5) Ft l-T€R.. 6Y::5,E""'-Cadmium --Chromium --
_._ Surface water (2) _ Liquid (6) /AJLe7 -L E"1Ch'A7e:---Lead
Mercury --
Soil (3) _ Slud ge (7) :5PLI T k,,J/ £C.O Selenium --. --Silver --__X Other (8) ::re-001-L <!.H Other (4) 'I ----
--..
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul ts(mg/1) (mg/kg) Organic Compounds Rcsults(mg/1)
'/( P&T:GC/MS Arsenic benzene ----
Acid:B/N Ext. Barium carbon tetrachloride ------"MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----Le.ad cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-d ich loroet hane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2,4-di nitrotolucne ----Silver heptachlor ----Radiochemistry Su if ates h exa ch Io robe n zene ----
Zinc hcxachlorobutadicne ----Parameter Results (PCi/1) pH hcx.achloroeth ane ----___ Gross Alpha __ Conductivity methyl ethyl kc.tone --Gross Beta TDS nitrobenzene -------TOC pcntachlorophcnol ----
----pyridine
Microbiology l el r a chloroet h ylen c ----
tr i chi oroethylcoc. ----Parameter Results (Col/l00ml) 2,4 ,5-trich lorophcnol ----
----2, 4,6-t richJ orophenol --
--vinyl chloride --·--cndrin --
7-;J.'J-'J</-V/!IJZ)Reportcd by
lindane --Date Received methoxychlor
7 --toxaphc.nc --O;itc Exlractcd Date Re.p ort ed 2,4-D --
g,. ~ -9 'i. 111.u-942822 __ 2,4,5-TP (Silvex)
Dale Analy1.cd Lab Number --1)1/S 31 ')1 (l~cviscd 2/91)
i",'.C. Ucp:·!1~mcnt ot l:,nv1ronmc.nl,
J ir,alth, & <'Jtural Rcs.ourccs
Solid Waste Management Di,ision
l'.O. Gox 2&').17, 306 N. Wilming,on Street
R.1dei&h, North C.&rol in• ~7Gi l
Site Number ------------------Field Sample Numb<:r __ W __ t.._-_0--'-0_1_-_L_t:-_-_____ _
Na me of Site WA-~i2.c.J GorvT'I PGt> l.DFL Site Location A F,o >-J NC _ _:_: _ _:_=-:.=----'-=-------------
Collected By (;; . (\J I U-to l, ~)-....) ID# 3-=/-Date CoUected ,,,2 'iS -::J VL -Y <=tLf Time / I z.o
l. /2osE
Agency: Hazardous Waste X Solid Waste Super fund TCLP Compounds ---------,,
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) Hl-T€R.. 6 Y::s re,n. --Cadmium
Chromium --
_._ Surface water (2) _ Liquid (6) /AJLe.T -LEACHA7e:-Lead --Mercury --Soil (3) _ Sludge (7) £>Pt.Ir k// ./?C..O Selenium --' --Sil ver --_ Other (4) ~ Other (8) ;:re-00I-L <!.H --i I
--..
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Co mpounds Results(mg/1)
P&T:GC/MS Arsenic benzene ---->( Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE Cadmium chlordane ------Chloride chlorobenzcne ----~-
Chromium chloroform ------
--__ Copper o-crcsol ---Fluoride m-crcsol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-di ch lorobenzene --
--__ Mercury 1,2-d ich lorocth ane --Nitrate .. 1, 1-dichloroeth ylcnc ------Selenium 2,4-d i ni trotol u enc ----Silver heptachlor ----Radiochemistry Sulfates hcx,ichlorobenzene ----
Z inc hexach lorobutad icne ----Parameter Res ults (PCi/1) pH hcx,ichlorocthanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnz.cnc ------TOC pentachlorophcnol ----
----pyridine
Microb iology tctr achloroeth ylcne ----
trichlorocthylcne ----Parameter Results (Col/lO0rril) 2,4 ,5-trich lorophcnol ----
--2, 4,6-trichlorophcnol ----
--vinyl chloride ----endrin --
Date Received 7-:l'?-f~pt'.it}rzcport cd by
lind:rne --
--mclhoxychlor
Dale Exlraclcd /kA. g'-"k1'f ~ ijgJatc Reported --toxaphcnc
---2,4-D
f ~,_J _,CJ t./ 8/J 9,12823 __ 2,4,5-TP (Si!vex)
OJtc A nalyzcd Lab Number --I)! IS 31')1 (!lcviscd 2/91)
i"'-.l~-LJ':_;J.!i~n,c nt .-1,.l{ 1:.nv•,:-unn,cr,l,
I ieollh, & i','a tural Rcwurccs
Solid Waste Management Division
l'.0 . Box 7..80-17, 306 1'. WilminQo n Str-~ct
lulcigh, North u rolin, 2761)
Sile Number -----------------Field Sam pie Num bcr __ W __ t.._-_o_O __ I_-_L_£ ______ _
Name of Site WA-1<.i2.e.J Gor-YN PGb l.DFL Site Location A F10 ,-,J NC _ _L_:__~~::...:..::"------'-'--===--------------
Collected By 6 . t0 1 C.Ho l-~)-...) ID# 3-=f-. Date Collected ;2 ~ -::J VL "r Cf'Lf Time /120
L.., l2oS'E
Agency: Hazardous Was te X Solid Waste Superfund TCLP Compounds ------,,
Sample Type Inorganic Compounds Rcsulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium ----__ Ground water (1) Solid (5) HL.T€i€. 6 Y!?TE.,v\. Cadmium --Chromi um --___ Surface water (2) Liquid (6) /,VLE.7 -L-£"1CHA7e:---Lead
--Mercury
Soil (3) _ Sludge (7) SPt..1 T tv/£c..o Selenium ----Silver --_ Other (4) _K Other (8) -;re-00I-L <!.H I I "f , --
' --·,·.
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Resul ls (mg/I) (mg/kg) Organic Compounds Rcsults(mg/1)
P&T:GC/MS Arsen.ic benzene ------Acid:B/N Ext. Barium carbon tetrachloride ------
-~
Cadmium chlordane ----Chloride chlorobenzene L ~VE::,'f <t:1. ooo/ --~-
Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron p-cresol ----.. Lead cresol ------
--__ Manganese --1,4-dichlorobenzeoe
--__ Mercury --1,2-dichloroethane
--Nitrate 1,1-dichloroethylcne ----Selenium 2,4-d i nit rotol uene ----Silver heptachlor ----
Radiochemistry Su Hates hex.a ch I orobenzcne ----Zinc hcxachlorobutadiene ----Parameter Results (PCi/1) pH hex;ichloroethanc ----
---Gross Alph a __ Conductivity --methyl ethyl ketone
Gross Bela TDS nitrobenzene ------TOC __ pentachlorophenol --pyridine ----Microbiology tetr achloroethylcne ----trichloroethylcne ----Parameter Results (Col /l00rril) 2,4,5-trich lorophenol ----
--___ 2,4,6-trichlorophenol --
--vin yl chloride ----cn drin --lindanc
~eJf/-. 7t/Jf',5peported by --Date Received methoxychlor --
f-~ -9 fJ/§B})J atr:. Reported
--loxap hene
Dat e Extracted 2,4-0 --
Dol e Anal ylcd ?-3-9'~,,,0 · 942824 2,'1,5 -TP (S il ve.x)
Lab Num ber --J)JJS 31 ')1 (lkvi,cd 2/91)
l lcalth, & i<Jtu r:il R<:sources
Solid W aste Management [)i,ision
Site Number -----------------
!'.0 . f.lo, 280-47, 306 1<. Wilmir.[1on S1c-c:e1
Riilcigh, North Grolin• 27611
Field Sample Number t,ul...-0 OZ -J. E
Name of Site WA-Qi2..e..J GorJTi PCb lr,FL Site Location A F,o >s.J /\) L -~__;__.....:....:::....:..:"---..:.__:._-;::..__ __
Date Collected 2.'8 -:IVL Y 9-4 Time /+.So
L.. . Re:>~£
Agency: Haz.ardous Waste X: Solid Waste Supcrfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---·
__ Ground water (1) _ Solid (5) Ft l-it:e_ ~V.Sreft? Cadmium --Chromium --tJ>VtLE'T-L I:A-CM ,tTt __ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) Sludge (7) Selenium ----Silver --_ Other (4) _k_ Other (8) ---I
I
--
--Organic Chemistry Inorganic Chemistry --
Parameter Res ults (mg/I) Parameter Resul Ls (mg/I) (mg/k.g) Organic Compounds Results(mg/1)
_L P&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium car.ban tetrachloride ------'MTBE Cadmium chl ordane, ------Chloride chlorobenzene ----~-
Chromium chloroform ------
--__ Coppu o-cre,sol --Fluoride m-cre,sol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1, 4-d ichl orobenzene, --
--Me,rcury 1,2-dich loroeth ane ----Nitrate 1,1-dichloroeth ylcne ------Selenium 2,4-di nit rotol ucne ----Silver __ heptachlor --Radiochemistry Sulfates h cxa ch Io robe n ze n e, ----Zinc hexach lorobut adienc ----Parameter Resu lts (PCi/1) pH hexachloroelhane ----__ G ro5s Alpha __ Conductivity methyl ethyl ketone --Gross Be ta TDS nitrobenz.ene. ------TOC pcntach loroph cnol ----pyridine ----Microbiology ----tetra chloroet h yl en e.
trichloroethylenc ----Parameter Resu lts (Col/l00ml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-trichlorophcnol --
--vinyl chloride ----endrin --lind:rnc
Date Received 2.::d._f-9¢-rt'lf!L}rzepo rtcd by --
--melhoxychlor
toxa phene, --Da te Exlraclcd Dale Re.ported 2,4-D --
O<Jlc Analy1,cd __ ?(-3 R~ Lab Number 942825 __ 2,4,5 -TP (Silvex)
--1)1 IS Jl'Ji (!Zr.vised 2/91)
I I I
1 lcallh, & /\.'alural Rcrourccs
Solid Waste 1'-lanagcmcnl Di,-ision
Site Number -----------------
P.O. fk n 2&}17, 306 N. Wilmini,.,on S1 n::c1
Rlilcigh, North C...n:ilina 27.'.Jl l
Field Sample Number t,,uJ..-~OZ -J. E
Name of Site WA-R.i2e.J CorvTi PCB U)FL Site Location A F'10 t-J NC _..!........:. _ _:_:::...:...:::c.._ _ ___;c.....=c..__ __________ _
Collected By G . (\) 1 c. H.o l-~l---.l ID# 3-=l-Dale Collected 2'8 :/UL Y 94
L. Reht
Agency: Hazardous Waste X Soud Waste SuperfuJJd TCLP Compounds ---
Sample Type Inorganic Co mpounds Rcsu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) . Solid (5) FtL.'f'tE'~ ;,Y.S,e#> Cadmium --Chromium --t9VTLE.t -L £A-CM ,ne; __ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (7) Selenium ----Silver --_ O th er (4) __k_ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Resu I ts (mg /1) (mg/~) Organic Compoun ds Results(mg/1)
P&T:GC/MS Arseuic benzene ----A Acid:B/N Ext. Barium carbon tetrachloride ----'MTBE · Cadmium chlordane ------
Chloride ch lorobenzcnc ----~-
Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dich lorocthane
--Nitrate 1, 1-dichloroeth ylenc ----Selenium 2,4-dinit rotoluene ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch I orobc nzene ----Zinc hexachl orobutadicne ----Para meter Resu lts (PCi/1) pH hcx.a chl oroet h ane ----
--G ross Alpha __ Conductivity --meth yl eth yl ketone
G ross Be.ta TDS nitrobc.nz.enc. ------TOC pent ach lor ophenol ----
----pyridine
Microbiology ----tetr ach loroethylcne
----trichlorocthylcoe
Parameter Resu lt s (Col /l00ml) 2, 4 ,5-t ri ch lo ro phenol ----
--2, 4,6-trichJoro phenol ----
--vin yl ch lori de ----cndrin --lind:rn e J--p(?· f¢~&}Reported by
--D at e R eceived methoxychl or --
/!;NA f -2-'jt/~"'~c Reported
--toxaphene
Date Extracted 2,4-0
7 --
Do le A ncJly1.cd f ,J-"J ':/_ ,J?,/j}__ 942826
2,4,5-TP (Silvex)
Lab Number
l)IIS 31'JI (IZcviscd 2/91 ) --i
l lcaltb, l.:. l''<atu :-·~.d Reso urces
Solid Was:c. i',lanagcrncnl Di,isior.
Site Number -----------------
l'.0. Box 2.80-17, 306 I',;. Wilmin[;10 n Strcc1
Raleigh, North Cuolina 2761 J
Field Sample Number t,,uJ..-0 0 Z. -1. E
Name of Site WA:R.i2..t.J Ll>orvTi PC"B l.DFL Site Location A F'To 1'.J NC _..c._:_ _ _c__::::__:__::::._ _ __c__:=:;.__ __________ _
Collected By 6. N tCH.o l-6Q},,..) ID# 3~ Dale Collected 2,g ";JULY 9-4 Time /+:so
L. R E>5E
Agency: Hazardous Waste X: Solid Waste Supcrfund TCLP Compounds ------
Sample Type Inorganic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---·
__ Ground wa ler (1) _. Solid (5) Ftl-Tt-1?_ .:5V.Sre/Y? Cadmium --Chromium --t)vn£T-L~ACft~ __ Surface waler (2) _ Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (7) Se.le.nium ----Sil ver --
_ Other (4) _)(_ Other (8) --I
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Resu 1 ts (mg/1) Parameter Resul Ls (mg/!) (mg/kg) Organic Co mpounds Rcsulls(mg/1)
P&T:GC/MS Arsen.ic benzene ------
Acid:B/N Ext. Barium carbon tetrachloride ------~ Cadmium chlorda ne. ----T <t?,006/ Chlori de chloroben2e.ne --~-
Chromium chloroform --· ----
--__ Copper o-creso l --
Fluoride m-crcsol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese l ,4 -dichloroben2ene --
--__ Mercury 1,2-d ich loroethanc --Nitrate 1, 1-dichloroethylcne ------
Selenium 2,4-di nitrotoluene ----Silver hept achl or ----Radiochemistry Sulfates hexach lorobenzene ----
Zinc hexach lorob u tad iene ----Parameter Results (PCi/1) pH hexachloroet ha ne ----__ Gross Alrha --Conductivity methyl eth yl keton e --Gross Beta T DS nit robenn ne ------T OC pent a ch lo rophcnol ----
----pyrid in e
Mi crobiology ----tetra chl o roet hylene
trich loroethylco e ----Parameter Res ults (Col/l0Oml) __ 2,4,5-t richl orophcnol --
--2, 4 ,6-Lrich.lorophcn ol ----
--vi nyl chl ori de ----endr in --lind;,ne
D at e Receivcd _Z_::el_.'f -~ 4..iJRcported by
--methoxych lor --P~!fr --toxaphene
D.itc Exlr aclcu Y-3_"ifvt8£J Dale Report ed --2 ,4-D
D at e Analyzed 3-..3-'J:'f/_1,(e___ Lab Number 942827
__ 2,4,5 -TP (S il ve x)
-------·-----1)1 IS J l'JI (IZcviscd 2/91)
I
I
I lcalth, & i','atvr,,! Resources
Solid Waste Management Di,ision
Site Number -----------------
1'.U. Uox 1..ou-• i , Y-J0 0. ½'1!m1npon ~tree\
RAieigh , Nonh Carolin• 2761 l
Field Sample Number W L -0 0 2 -f3 L ---------'-'---=-------
l'-./ame of Site WA-1<.i2..e:..J Cx>rvT'I PCB l.DFL Sit e Location A FTo ,-J NC
Collected By ~. f\) U'..Ho l. 60)-..) ID# 3-q.. Date Collected 28 -;;TVL 'I ~4 Time / f!O
a, S:,. . S.,tPt-l €")-...:>
Agency: Hazardous Waste X Solid Waste Superfu.nd TCLP Compounds ------
Sample Type Inorganic Compounds Resu I ts (mg/I)
Environmental Concentrate Comments Arsenic --Barium ---·
--Ground wa ter (1) Solid (5) o. F'. WA-,t-R.. --Cadmium
Chromium --Surface water (2) Liquid (6) Lead ----Mercury --Soil (3) _ Sludge (T) Seleniu m ----Silver --L Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/!) Parameter Resu I ts (mg/I) (mg/kg) Organic Co mpounds Results(mg/1)
P&T:GC/MS Arsenic benzene ----___x_ Acid:B/N Ext. Barium carbon tetrachloride ----
~BE Cadmium chlordane
'I< ~PE!>,<'o,ooo/
----Chloride chlorobenzene --~-
Chromium chloroform ------__ Copper o-cresol ·----Fluoride m-cresol ------Iron p-cresol ------Lead cresol ------
----Manganese 1,4-dichlorobenzene --
----Mercury 1,2-d ich loroethane --
--Nitrate 1, 1-dichloroeth ylcne ----Selenium 2, 4-di nit ro tol uene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----Z inc hexach lorobut ad ie ne ----Paramete r Results (PCi/1) pH }1ex;ichloroet h ane ----G ro ss Alpha ----Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC penlach lorophenol ----pyridine ----Microbiology tel ra chloroct h ylene ----trichloroct hylcoe ----Pt1rameter Resu lt s (Col/l00rnl) 2, 4 ,5-lrich lorophcnol ----
--__ 2,4,6-triehlorophcnol --
--vinyl ch loride ----endrin --lind wc
Date Received 1-~-ft/--tl/Jtt!l} --Reported by --melhoxychlor
~.t~ BNA 7 toxaphenc --Dale Extracled~ate Reported --2,4-0
/'('LJ; ~T f3AJ,I./ . 942828
__ 2,<'l,5-TP (Silvcx)
Dole Analy1,ed3!:~J!.1/P S7~3..q '/ Lab Number --1)1 IS 31')1 (1,cviscd 2/91) lJl} I I
t<.C Dcpanmcnt of Environment,
J lcalth, &. Natural Resources
Solid Waste Management Division
SA.MP LE ANALYSIS REQUEST State ubon.tory of Public Hui:~
P.O. Gox 2S0--17, 306 N. Wilmin&1on Street
Raleigh, North Carolin• 27611
Site Number -----------------Field Sam plc Numbcr_~tu-=-_L'-----..,.,O:::..ttJ""'_4_.___-_,,&=-L _____ _
Name of Site WA-R.i2..E:.J Gor-JTY PC"B l.DFL Site Location A F,o t--.J NC _L.....:....:.._....:....:::....:...::::'....__...:._::.....:::::..__ __________ _
Collected By a . rv , c H.o L-6C>'-' Dale Collected ;2$ -;fOCj 44-
~-ST-EPt-l ~.s;._
Agency: Haz.ardous Waste X Solid Waste Superfund TCLP Compounds --------,
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium ---· __ Ground water (1) Solid (5) o.;:: WNcle Cadmium --Chromium
AIR Hos~ --__ Surface water (2) _ Liquid (6) Lead --Mercury --
Soil (3) _ Sludge (7) Selenium ----Silver --A Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results (mg/I) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsen.ic benzene ------L Acid:B /N Ext. Barium car.bon tetrachloride ----~1~ Cadmium chlordane ----
0, 00'/-::L.pp ""--Chloride chlorobenzene ~-Q' Chromium chloroform ------__ Copper o-cresol ----Fluoride m-cresol ------
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylcne ----Selenium 2, 4-di nit rotol u enc ----Silver heptachlor ----Radiochemistry Sulfates hex.a ch Io robenzene ----
Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hex.achloroeth ane ----
--Gross A lpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzen e ------
TOC pentachlorophenol ----
----pyridine
Microbiology ----tetra chloroeth ylene
trichloroethylene ----Parameter Results (Col/l00ml) __ 2,4 ,5-trichlorophcnol --
----__ 2,4,6-trichJorophenol
------vinyl chloride
cndrin --
Date Received .Z:::c:lf/#&J Reported by
lindane --
--methoxychlor
f t!8Yr It"' ~,) i\t {,-----toxaphene
D"c fatmtc"1-3:ff::'/!': Date Rcponcd --2,4-D
tPr;j-!Jl# ~JJI}-. 942829 --2,4,5-TP (Silvex)
Date AnalyLcd LV1/P c;/-.3-91/Lab Number --l)J IS JJ'J l (l,cviscd 2/91) 8S.
h· e le) SIJ/11 p le ;(;s
-----···· .. ·· ..... _-.
STA7E IABORA:I'ORY OF POBLIC BEALTB
PO BOX 28047 -306 11. WILJmrGTOll ST .. RALEIGH. NC 27611
ORGANIC' CREMTCAL ANAL'YSIS
.PtmGEABLE COIIPOmYDS UBNO Cl'-IJ'?Oa q'+c'ND3 q'-1.;li'oLI-961 f).'?D5 Qlf;;J9:Z>{tJ
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tJN1TS (Nlyii,Jq (N;yµg1q ~~llifq (iig/~µgJq {Piij)NJq
cm.01t0MET1LVIZ Joopl, l 1.
vurn. cm.oamg 10
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cm.01t0ICTILVIS 1n .. 10 nuc:m.oaon.uoa0XB'T1L\l'l'E
.a.c:rron 50
1.1-Dlc:m.ollU)l:nlZ2fS 5
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D. -Jlot uaal~ad-1/ • T■Dt&ti,,. idaatificatioa.
l/ • 0D JIJtDC Li•t of Priority l'ollutaat•-H • COMPou,,u, REUABLY 2>ETECrA~ CNLV AT 1UG-1t t'.oNCE~TeATicNl •
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STATE LABORATORY' OF PDBLIC BEALTB
PO BOX 28047-306 l!I'. WILIIINGTON ST •. RAJ,EJr,a NC 27611
ORGANIC CHEMICAL ANALl'SlS
~GE4Bl.E CO.IIPOl7NDS IABNO q~ ;i<l{)~ qL.J~03 lq'-lJio'-1 9'-IJ605 Cf/~CXD
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• 8Act.6~C> P'RIUa.JT IN LA8 81..ANIC'S.
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L -Actual T&l.u• i• bowu to be graater tbaA T&l.ue giTCI..
ti' • ll&t•rial waa wlyzed for !Nt DOt detected. Tb• 11.uaber i• the •1n:fwm l>atectioD Liait.
--:.Ct &Dal~ed-1/ -TeDtati.,.. idezltificatioD. 2/ -OD JIJUlC List of hiority Pollutam:•.
ii -CoM~llNb ReUJ:\9,.Y DETECTRSLE ONLY RT Hl6-... c.oNCf~RT)O~.
C -?~51BLE i-A0 C.0...sTAMlMA710N. DEBl'm 3068-0 (10/93)
q4~'8'I I
..,i . (lJJ -6W
c I )
~/'q
u
\ /
PORGCOILORC
M
---___ .., ...... _. ·-· __ ...,_
-------'·'· ... ·-----·
STATE LABORATORY OF PUBLIC BEAi.TB
PO BOX 28047-3061'. WIUmfGTOlf ST-RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
.PDRGE&.BlZ CO.IIPOUNDS LAB NO q~g,11-
FIELD NO WL-cc3-&-w ..
COJIPOC'ND -· TYPE C I )
t7NlTS ~/kg
CBLOROICETBAl'IZ Joop.b u.-
"11Jfft.CBLOIUDI: 10
.ut0110KZTBAKZ :l()
c:m.oaosnu.zn: 1n
" 10 TJIICBL0R0~
.ACSTOR .50
Ll.Z)lc:m.0ROsna:lm 'J
10DOIIIIZT1IAlff: lO
~ cm.oam1: .'5
c:.umolf DISCUml: \
IIIARS-i.:z.DICBL0R011!:T11EffZ J;
ACntOinntZU: ;J:::C)
Ll•Dlc:m.oROl:TBAJf!: .5
:1-BITr'NIO!fl: .:;o
CS-1.:-DICHLOltOl:TBl:ffZ ,Ii
c:m.0ROPORK
Ll.l•TmCBLOIIOEnlAJl'Z \ v
CAJUM)lf n:ntN:BLORrDI: /0
~ Ii
1.Z-D1c:m.oaoEn1AKS
nucm.oaor:nun
U-DICBL01t0Pll0PMZ ,I /
D0110D[CBL0ll0Kl:T!IAlfE /0 'I
ofh~r Co Mi)ourd.5 ®IF) F) ,
fMDLf
e,-?IAekG-~,-l0 PRE:SEl'IT'" IN I.AB &,u,n:~.
J -Zat.iaated Tal.ue
q"lJ_g I 1
w 1---00'f-&t.:"
( ' )
~pg/kg
U--
" I/
F )
I: -Actual. 'Yalu• i• k::aowii to b• l••• t:b&D 'ftLl.11• gi-.
:C. • Actual·....iue i• k::aowii to be si:•at:er t:b&D Tal.11• gi'Y9D.
q'-l~~~D
l>)L-005-l-w
( ) )
(N/i')P&lkl
U-
I
,V
r--)
q'f~...,::, q 4,.:) 9._., r:;
WL-Ool -LE i)Jl..·00;1-U,
( 8' ) ( 13"">
(1igij)wkg ~
t -U-
.
,I
+-t'"tll'P
u
v .....
~:r
u._ .
/
'\/
' (+) (-)
'O' -llat:erial •-analysed for bile DOC det:ec:ced. ft• Duaber i• th••~ Detec:cioll :C..1.ait. a. -:aoc analysed.
1/ • Tellt:ati.,.. idalltificatiOll.
°ii -Oil IIJt.DC Liat of Priority Poll111:aAt•• H • COMPoU,.U) REUABLY l>ETEaABl.e DN&.V AT HICilt CoNc£NTEAT"JCNj •
C. • po.:,s,BLE -LR& CONT'P.~1~1=r~tctJ,
Dl!:Bl'IR. 3085-0 (10/93)
( ) I
pg/1 ll&/kg
I
I
I
I
POJUiCOM.OP
-····. ·-·-··------"-···········-'-------. -. -----------------··-·
STATE IABORATORr OF PDBLIC HEALTH
PO BOX 28047 -306 K. WILJIINGTOK ST .. Rt\TEif"dL NC 27611
ORGANIC CBEMTl"'-AL ANALl"SlS
.PC1RG&Ul[Z CO.IIPOmvDS LAB NO q4~l!f q'-l (;Yo/7 qmx, q4J~;i;l q4;;ig;J5
-. FIELD NO WL·oo3--6-u.J tvt.. ·b0'1-61J.) 11.)L -ocf,-<.. ...,_,,...' U-CO/-L.t iJl-OC;;2.-Le
COIIPOmvD TYPE C I ) C I ) ( f ) ( ~) ( ? )
t1NlTS ~]l&/q ('Pt! 'PtlkC ~'pt/q ~ ~ ,
DDlltOMOID:TBAl'IZ ~ ri""h u-u..-. t . ..' ~ frnrP LL.
I I -
+MZTBn,.:&-n:lff.UIOIQC . ---~n t.1 ~
C.l>Dlau.oa0PIIOPEIU 5 t'
't0UJZlq t:r
'TMff8-1.S-11lcm.o1tOP1t0PSKZ H.-11 . .
1.1.2.2-n:ntACBZ.ollOE'r1!Aln JO
1...1~nucm.oaor:TBAl'rZ 5
::1-BJ:L\IIOJa: !5n
n:ntACm.OllOETBE!m .5
DDIROMOCBl.01l0ta:T1L\lfZ IQ
'tn.ZJfZ DDROKD>E .!5 ·V
J.OllO~ J.,, i"mf'f-)
1.1.1.2-TZT1lACm.01l0~ Jo l1
rnrn.•~ 5 +rarie
ZTl.Z."fES JO ;ij
ft STT1lDE 15 u
.,
JlllOIIOFOllK 10
TaAZ1a-1.4-Drcm.oao-:a-aarzn ~o
1.2~T1UCBLOltOPKOPAIOC ;;J1)Q
1.4,-DICBLOllOIIEIIZZl'IZ ID
1.2•DICBLOROII~ J/
1.2-DDllOMo-s.cBLOllOPllOP.ANZ :JoO
VDffL ACZTATZ ~ ,I
i-MDLf
e -8Act.6~1> Pee.sa-rr IN LAB 81..AN)C~.
J -Zatiaated Yalu•
,I
• Actual Talue i• 11::m:Nn to be l••• t.!aaD -111• c,1-..m.
-Actual ""11.l.u• i• bown to be g,:water tbazl. -111e tri..-.n.
\if
+rnno
(..A-
,v ,v
J . -Matarial waa wl.yzed for :bat 110t detected. flle :auaber i• the M1niem l)etection :t.iait.
ID. -Jrot wl.ysed.
1/ -Tentati-idelltification. 2/ -on mux: %.iat of hiorit:y ~Uut&Zlta. ii -CcM'J"llN b REl.l ~ a,y C>ETECTRSLE oNLY RT H 1.6'1-t CoNCf"1T"&ATIO~.
C • ?~51&.E u:18 CON'T'AMlMA"TloN. l>EBNll 3088-0 (10/95)
,v
( )
N/1 pg/q
PCRGCOK.ORG
L 8ASE/NEUTRAL AND ACID
EXTRACTABLES
COf1PWND
N-nitrosodimethvlanine
bis(2-chloroethvl)ether
2-ch 1 orooheno 1
ohenol
1.3-dichlorobenzene
1.4-dichlorobenzene
1,2-dichlorobenzene
bis(2-chloroi nether
hexachloroethane
N-nitroso-di-n~mDvlanine
nitrobenzene
isoohorone
2-ni troohenol
2 4-dimethvlohenol
bisC2-chloroethoxv)methane
2 4-dichloroohenol
1 2 4-trichlorobenzene
nanhthalene
hexachlorobutadiene
!: oro...ffi-Creso 1
.chlorocvclooentadiene
,,6-trichloroohenol
2-chloronaohthalene
acenanhthvlene
dimethvl ohthalate
2 6-dinitrotoluene
acen.mhthene
2 4-dinitroohenol
2 4-dinitrotoluene
4-nitroohenol
fluorene
4-chloroohenvlohenvlether
diethvl Dhthalate
4.6-dinitro-<>-cresol
diohenvlanine
azobenzene
4--0raroohenvlohenvlether
hexachlorobenzene
oentachloroohenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
~ -Estimated value.
STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARHENT OF HJNAN RESOORCES P.O. BOX 28047 -306 N. WIUUNGTON, ST., RALEIGH, N.C. 27611
ORGANIC ri.:MICAL ANALYSIS
LAB NO qq~Jt'/O c.., i./ .].RI ~ qv.LYJtA vYJ..JIJq
FIELD# t,.JL, -(JO '2-6, ii, IIJ(.,-00.3-<nu.:.. i~L -(X)lJ _t, u JJJL-()0~11
TYPE < I l < I > ( ) c / >
UNITS uo/1~ uo/1'\~ 1 \JQ/1~ rua/11nm!ka
IIV.c'"" IA.-&A.-1,,,L_ IA -
--
,,
So//ia-~O
JtJ/330
S0//~50
10/~o
.,j,
-~o, ~/,,~()
/()/330 ,
~.,
.$"()//I,, S"{J
/t'J/~3{}
/ / / I
\j , '\ '\ I ,, \
-Actual value is known to be less than value given.
f;/C/~Y~
,/M-a,/-(.1£
1 V'>
"ua/lJia;aq
lA-
\ I
-Actual value is known to be greater than value given.
u -"'1terial ..as analyzed for but not detected. The nlll'ber is the Mininun Detection Limit. m'J)L
NA -Not analyzed. ----1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
N. C. V.i.v..i.6.i.on 06 He.ai..th SeAv.i.c.e.6
VHS 3068-0 (4/86 Labolt.ato~y)
~ V ,,,ll' 7 /,-,
111£-1.>02-I J:
( -')
\JQ/1 ~
IA -
' V
STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. OEPARTl'1ENT Of HUl'\AN RESOORCES
P.O. BOX 28047 -306 N. WILHINGTOH, ST ., RALEIGH, N.C. 27611
ORGAHIC DiEHICAL ANALYSIS
LAB NO BASE/NEUTRAL AHO ACID
EXTRACT ABLES FIELD# /ul-(){) 2-6. u.. W l -o:, 3 -lnu. ) luL ·OtJ'/-6>11. tpL--OOS-6, u:. WI.--ool-1..i W{.,-COZ -U
<XlNPQJNO TYPE < L l < I l < I > < I l C ~l 1 Kl
UNITS
ovrene 1/IJ/~~l'J
benzidine
butvl benzvl ohthalate 110/Jl~0
benz(a)anthracene l
chrvsene J,
3 3-dichlorobenzidine StJJ'IMIJ
bis(2~thvlhexvl)ohthalate
di-n-«tvl ohthalate /()/.J~o
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)ovrene
indeno(l 2.3-cd)ovrene
dibenzo(a.h)anthracene / ,
benzo(a h. i)oervlene \I/ ,/
aniline l$°tJ//h_'iO lJL-vL,
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2~thylnaohthalene
2~thvlphenol j
4-ffl!thvlohenol
2-nitroani line
3-nitroaniline
4-nitroani 1 ine
2 4 5-trichloroohenol \. I
~ +J-(-J \..-J { -J
"11)1-
J -Estimated value. H2.0/ .SOIL
K -Actual value is known to be less than value given.
l -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The m.l'l'ber
NA -Not analyzed.
1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
N. C. 0-<.v-W-<.O n o 6 H e.a..Uh SVtv-<.cu
OHS 3068-0 (4/86 Labolt.a.,(:o~q )
is the Hininun Detection Limit. n,J)t.., -
vL
"I/
STATE LABORATORY OF PUBLIC ~LTH
DIVISION OF HEALTH SERVICES, N.C. OEPARTfENT OF K11AN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C . 27611
-' UNEUTRAL ANO ACID LAB NO
EXTRACTABLES FIELD I
a>MPOONO TYPE
UNITS
N-nitrosodimethvlamine /('J/;/~
bisl2-chloroethvllether
2-chloroohenol
ohenol
1.3-dichlorobenzene
l 4-dichlorobenzene
l 2-dichlorobenzene
bis<2-chloroi .. J lether
hexachloroethane
N-ni troso-di-n-l)mnvlami ne
nitrobenzene
i~horone
2-ni tmnheno l
2. 4-d imethv 1 rwono l
bis(2-chloroethoxv)methane
2.4-dichlomnhenol
1.2.4-trichlorobenzene
nanhthalene
hexachlorobutadiene
4-ch 1 oro~reso 1
hexachlorocvclnn,,ntadiene
)-trichloroohenol
.. ,..loronanhthalene
acen;mhthvlene
dimethvl ohthalate
2.6-dinitrotoluene
acenaohthene ' If'
2.4-dinitrmhenol I.S'2n'»SO
2.4-dinitrotoluene I Jt,/3.'~0
4-n i tmnheno l ~0/tt.~O
fluorene 10/~tJ
4-chloroohenvlohenvlether I
diethvl ohthalate J,
4.6-dinitro-o-cresol l5D/ ~t,,StJ
diohenvlamine '"/'.33tJ
azobenzene I
4-bramohenvlohenvlether
hexachlorobenzene " rwontachlomnhenol ~()//t,,.51",
ohenanthrene ~A/ :J~/\
anthracene
dibutvl Dhthalate
fl uoranthene ' if
J -Estimated value.
ml)L
Hz.O/SOIL-
ORGANIC OEPHCAL ANALYSIS
Cl:1 ..,0 ..J9 'IY,,lY:J.q
,· .. , _,.,., :!.. -Ai_ in/_•, ,f ,.., ,
cu} _J_ ,., } ( }
ruo/1~ "'"ua/1 hzlmi ua/1 ua/kg
I I( --1.,c__
, ,,
, ~:1. DDD
\II' 'LA-
~ -Actual value is lcna,,n to be less than value given.
( }
uo/1 ua/kQ
--
( )
ua/1 uo/ka
Actual value is kna,,n to be greater than value given.
Material was analyzed for but not detected. The nlJT'ber is the 11ininun Detection Limit. m'])L .. -Not analyzed. ---_ 1/ -Tentative identification. i1 -On NROC List of Priority Pollutants.
N. C. V.i.v,i..t,-i.orr. 06 Health SVLv-<.c.e..6
VHS 3068-0 (4/86 Labolt.a..to~y)
( )
uo/1 uo/ka
BASE/NEUTRAL AHO ACID
EXTRACTABLES
QlNFOONO
0vrene
benzidine
butvl benzvl Dhthalate
benz(a)anthracene
chrvsene
3.3-dichlorobenzidine
bis(2-ethvlhexv1)0hthalate
di-n--0etvl ohthalate
benzo(blfluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
i ndeno ( 1 2 3-cd) 0vrene
dibenzo(a h)anthracene
benzo(Q h i )nPrvlene
aniline
benzoic acid
benzvl alcohol
4-ch 1 oroan i 1 i ne
dibenzofuran
2-nethvlnaohthalene
2-nethvlohenol
4-fflethvlohenol
2-nitroani tine
3-nitroani 1 ine
4-ni troani 1 ine
2.4 5-trichlOl"OPhenol
Yt'l!,(C.o,.JFJ~ATJDAJJ
STATE LABORATORY OF PUBLIC HEAL TH
DIVISION Of HEALTH SERVICES, N.C. OEPART~NT Of 1-fJAAN RESOJRCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO ~'/~).}? o/'1.,,;..i'e)..9
FIELD I 11.Jl-002-AL w L-tiLJ t/ 7'U_
TYPE C Lil ( I.I) ( ) ( )
UNITS j 'u o/ 1 l.a:l:l!!tll ruQ/1),,~ uo/1 uo/kQ \Ja/1 uQ/kQ
M/~:fl'J I.A -.~
s11/JIISO --
IJ()/J1.:JO
J, I
Sft/lLl(',i ,1
JIJ/~~D UJ .. ~ ~
/()/.J~o '1A-
.S-0/JM'n
,
\, 1 / ,,
l,<~/:~-.~ IA-LA-
'-i,
'"/=r.:ui
~
"' ~o/Jt..<"o
,
~;' ,1 \.,
--,,--,.,..
.+,/-(-} { + J . --
"11>L..
J -Estimated value. Hz.0/ SOIL.
K -Actual value is known to be less than value given.
( )
uQ/1 uQ/kQ
L -Actual value is known to be greater than value given.
U -Platerial was analyzed for but not detected. The nurber
NA -Not analyzed.
is the Minim.In Detection Limit. fl'lJ)t..,.
1/ -Tentative identification. ii -On NROC List of Priority Pollutants.
N. C. V-i.v-i.6-i.on o 6 He.a.U:h SVt.v-tc~
VHS 3068-0 (4/86 Labolt.a..to~y)
-
( )
uQ/1 ua/lcQ
~ C!!IJin
YOUR
YIICAL
SOURCE
September 29, 1994
Pauline,
The data package attached is a result of a special analysis done on an
existing sample from the original sampling event. You will recall that we had
a rinsate blank sample (WL-002-BL) for the equipment used in collecting
water from the monitoring wells. That sample was run by Method 8081 and
showed ND on organochlorines. Because the Method 8290 gave us some
inexplicable results near the detection limit of ppq (and for which we had not
run a blank), we transferred the original equipment blank over from the
Health Services Lab to Triangle Labs;still under chain of custody1and had
them run it by Method 8290 (the sample number 942828 results from the
interlaboratory transfer, the second number being the number assigned
internally by the Health Sciences Lab as shown on their results sheet).
The enclosed data are a copy of those results. Clearly this is not an
"ideal" control, but the presence of trace levels of dioxins and furans
(coupled with your ND data at the PPT level) gives us some confidence that
the amounts present in the samples could be from sample collection or
glassware preparation in spite of our having used standard Superfund-quality
preparation methods.
CASE NARRATIVE
Analysis of Samples for the Presence of
Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans by
High-Resolution Gas Chromatography/ High-Resolution Mass Spectrometry
METHOD 8290
Date:
Client ID:
P.O. Number :
TLI Project Number :
September 26, 1994
State of North Carolina, NCDEHNR
Contract # 28928
29600
This report should only be reproduced in full. Any reproduction of this report requires permission from Triangle
Laboratories of RTP, Inc.
Rev. 12/17/93
Triangle Laboratories of RTP, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713 Research Triangle Park, NC 27709
919-544-5729 Fax# [phone]
Triangle Laboratories of RTP, Inc.
Case Narrative
Overview
September 26, 1994
29600
The sample was extracted and analyzed according to procedures described in the Triangle
Laboratories Data User's Manual (Rev. 12/92-LLW-7-AH-2/93). Any particular diffi-
culties encountered during the sample's handling by Triangle Labs will be discussed in
the QC Remarks section below. Results reported relate only to the items tested.
Quality Control Samples
A laboratory method blank --identified as the TLI Water Blank --was prepared along
with the sample.
oc Remarks
The release of this particular set of State of North Carolina, NCDEHNR analytical data
by Triangle Labs was authorized by the Quality Control Chemist who has reviewed each
sample data package individually following a series of inspections/reviews. When appli-
cable, general deviations from acceftable QC reguirements are identified below and
comments are made on the effect o these deviations upon the validity and reliability of
the results. Please consult Trian~le Laboratories' Data User's Manual for further details.
Specific QC issues associated with this particular project are:
Sample Receipt: One water sample was received from State of North Carolina,
NCDEHNR m good condition on September 14, 1994 at ambient temperature and was
stored in a refrigerator at 4°C until extraction. The client's chain-of-custody did not
indicate whether or not the sample was preserved prior to shipment.
Sample Preparation Laboratory: The sample had only 175 mLs of sample for extraction.
Per client request, TLI was instructed to extract the volume received.
Mass Spectrometry: None
Data Review: Results for mono-, di-, or tri-chlorinated Dibenzo Dioxins or furans are
included in this data package. Triangle Laboratories does not have QC criteria for these
analytes other than the +/-15% isotope ratio criterion. Precision and accuracy of results
for these analytes have not been certified or verified. Detection limits may be systemati-
cally underestimated. As stated in the Data User's Manual (section 2.8), Triangle Labo-
ratories cannot defend the validity or accuracy of these lower congeners. Contrary to
version yt-6 of the Data User's Manual, continuing calibration response factors are used
to calculate results for these analytes.
Other Comments: Any analytes found in the TLI Water Blank are detected at a level
equal to or less than the Target Detection Limit. This level of contamination is accept-
able as per TLI Guidelines. OCDD is not subject to blank contamination criteria as per
TLI Gmdelines.
2
Triangle Laboratories of RTP, Inc.
Case Narrative
Sample Calculations:
Analyte Concentration
September 26, 1994
29600
The concentration or amount of any analyte is calculated using the following expression.
where:
C(6) is the concentration or amount of a given analyte,
A6 is the integrated current for the characteristic ions of the analyte,
AB is the integrated current of the characteristic ions of the corresponding internal
standard,
QB represents the amount of internal standard added to the sample before extrac-
tion,
RRF(6) is the mean analyte relative response factor from the initial calibration
(ICal) and,
W is the sample weight or volume
Detection Limits
The detection limit reported for a target analyte that is not detected or presents an analyte
response that is less than 2.5 times the background level is calculated by using the follow-
ing expression. The area of the analyte is replaced by the noise level measured in a
region of the chromatogram clear of senuine GC signals multiplied by an empirically
determined factor. The detection lirmts represent the maximum possible concentration of
a target analyte that could be present without being detected.
2 * 2.5 * (F * H) * QB
where:
DL(6) is the estimated detection limit for a target analyte,
3
~ Triangle Laboratories of RTP, Inc.
Case Narrative
2.5 is the minimum response required for a GC signal,
September 26, 1994-
29600
F is an empirical number that approximates the area to height ratio for a GC sig-
nal. This number is 5 for the DB-5 column and 3.5 for the DB-225 column,
H is the height of the noise,
AB is the integrated current of the characteristic ions of the corresponding internal
standard,
QB represents the amount of internal standard added to the sample before extrac-
tion,
RRF(6) is the mean analyte relative response factor from the initial calibration
(Ical) and,
W is the sample weight or volume
Other sample calculations may be found in Triangle Laboratories' Data User's Manual.
Data Flags
A "B" flag is used to indicate that an analyte has been detected in the laboratory method
blank as well as in an associated field sample. The "B" flag will be used only when the
concentration of analyte found in the sample is less than 20 times that found in the asso-
ciated blank. This flag denotes possible contribution of background laboratory contami-
nation to the concentration or amount of that analyte detected in the field sample. Under
Triangle Laboratories of RTP guidelines, a laboratory blank is acceptable if one of the
following conditions is satisfied: 1) the tetra through hepta CDD/CDF levels are all
below the target detection limits (TDLs), 2) the analyte levels found are all below 1/3 the
theoretical method detection limit (TMQL), or 3) the contamination levels are less than
5% of the levels detected in the associated field samples. If these conditions are satisfied
or if the blank is unable to be reextracted, the interpretation of the contamination levels
relative to the samples should be as follows: 1) analyte quantitations should be consid-
ered valid if the level of blank contamination is less than five percent of the level detected
in the field sample, 2) analyte quantitations should be considered estimated if the analyte
level in the sample is five to twenty times the level of the analyte in the blank, or 3)
analytes whose level in a sample is the same as or less than five times the level detected
in the associated blank should be considered present likely due to laboratory contamina-
tion and not native to the sample.
A ''V'' flag is used to indicate that, although the percent recovery of a labeled standard
may be below a specific QC limit, the signal-to-noise ratio of the peak is greater than
10:1. The standard is considered reliably quantifiable. All quantitations derived from the
standard are considered valid as well.
4
. Triangle Laboratories of RTP, Inc.
Case Narrative
September 26, 1994
29600
By our interpretation, the analytical data in this project are valid based on the guidelines
of EPA Method 8290 (Rev. 0) and Triangle Laboratories' Method 8290 Data User's
Manual. Any specific QC concerns or problems have been discussed in the QC
REMARKS section with emphasis on their affect on the data. Should State of North
Carolina, NCDEHNR have any questions or comments regarding this data package,
please feel free to contact Edwm Marti, Technical Director, at [phone].
For Triangle Laboratories of RTP, Inc.,
Report Preparation Quality Control
Sheila A. Lee-Lewis
Report Preparation Chemist Report Preparation Chemist
Total pages in report:_q_t __ 5
•
-· r
TRIANGLE lABORATORIES OF RTP, INC.
Rev. AH -9/93
DOCUMENT
CONTROL
6
•
State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
TLI Contract No. 28928 See Ed Marti, if any questions
September 13, 1 994
Sample No. 942828
Warren County PCB Landfill Sampling Program July 28, 1994
Rinsate Blank Sample ID WL-002-BL
to be analyzed by EPA Method 8290X:M-O
if sufficient sample is available to achieve detection limit of 50 ppq or less.
Turnaround time 14 days
Contact: Sharron Rogers
Division of Solid Waste Management
NC Dept. of Environment, Health, and Natural Resources
401 Oberlin Road, Suite 150
Raleigh, NC 27605
919-733-4996
·• 7
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone] FAX [phone]
50% recycled/ 10% post-consumer paper An Equal Opportunity Affirmative Action Employer
~C-D£H.'\K
~i\'i!-ion of Solid Waste Management
::J Superfund Section
'.J Hazardous W,1ste Section
7 Solid Waste Section
Jrg:rn1c:. i...au: ---lnorganics Lab: ---
CHAIN OF CUSTODY RECORD
Project Name: Warre,t'.\ Cr2./t:J.;LA-Nf2 f;J/
Site ID# (NCD#) ________ _
Location: Wo...r~ (!,.J..,., ~c
,4 -{J
Address:'f.k.o NC J
Sampled by: b. S-.J~e_l-L~S
Sampler ID fjj <;J_, ~
Telephone:_('91'7) 733 -730g ?Jr R:3er mc!Jc,,,,'c(
Date Sampled :_7..___.-,2=----g-_-~9.___.._y _______ _
Time Sampled: 7 .' / c)
Sample Types: Soil ------Water -----Waste -----Other_!
Remarks: SR1 Ovl-/4. c.0_ cY I /1 [&c.ln-i ,s~-1-I
Field Sample
Numbers
A
Relin~uished bL .a.A l'l /J. '-ff/ o d f M. Date: cj/; ~)9f Time: /,: 1~0111 I
NCDEJhU ,v · -.__, / 7 ~
Hu-(.~'e,,,.a. ~47' S1gna ture) '--.
Rece~:d?~:; ----?-~±--/-;er-____________________ Date:-qh/Jt/ ___ Tirne:--/ Z :;re> ________
-) (Signature) I
Relinquished by: Date: Time:
(Signature)
------------------------------------------------------------------------------------------------------------------------------------------------
Received by: Date: Time:
(Signature)
Relinquished by : Date: Time:
(Signature)
------------------------------------------------------------------------------------------------------------------------------------------------
Received by: Date: Time:
(Signature) i
Results Reported: D3te: ___ _ Time: -----(Signature)
8
A:\COCR.FRM)
PAGE l OF l
·-----------------------------------------------------------------+--------------------+------------------------------------+------+
Custody Seal Present/Intact : TLI Project Nu■ber : 29600 Book 1
Chain of Custody Present +--------------------+------------------------------------+
Sa1ple Tags Present : Client: DSWOl : STATE OF HORTH CAROLINA, NCDEHHR 88
Sa1ole Tag Numbers : Listed +--------------------+------------------------------------+------+
SNO Forms : Absent Date Received 1 09/14/94 By Li L ~: Page '
+------------------------------------------------------------------+--------------------+-----------+---:~------+
Box HO ICE Carrier and Hu■ber SHARRON ROGERS 36
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
' TLI Number Matrix : To LAB : To STORAGE: To LAB : To STORAGE: To LAB : To STORAGE: To LAB : To STORAGE:
mR/H Client ID Location : Date/Init : Date/Init : Date/Init': Date/Init : Date/Init : Date/Init : Oate/Init : Date/Init :
;·aa-i,-1······::;:;:······coo:::::·;1~Y.j·~:-·:::::::;:::::::::::;:::::::::::;:::::::::::;:::::::::::;::::::::::::
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
I
I I
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
I
I
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
I I
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
I
I
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
, I
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
+-----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
I
I
I
I
I
+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
----------------------------------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+-----------+
Receiving Remarks: WATER INSIDE A GALLON JAR.IT APPEARS TO BE 8 TO 10 OZ OF WATER.
\
I i 9
I :~ t
I *"" . ' i Archive Remarks: i. --:
+------------------------------TRIANGLE LABORATORIES OF RTP, IHC.--CHAIH OF CUSTODY--REVISED 06/20/94-------------------------------+
TRIANGLE LABORATORIES OF RTP, INC.
HIGH RESOLUTION SAMPLE TRACKING AND PROJECT MANAGEMENT FORM
--;~~-;;~;~~-;;~;;-------::!~!~~~TIVE ~~:=~~~~-~~tts~--------------
PROD CODE: D03001 TYPE ... : B HOLD TIME .. : 0 DAY(S)
MATRIX ... : WATER
DETECT LM: 50 PPQ
RPT REQ .... : Report Option II
RPT FORMAT.: 8290
METHOD ....... : 8290X MONO -OCTA
CLIENT PROJ .. : WARREN CO. PCB LANDFILL SAMPLE ORIGIN:
CLIENT ....... : STATE OF NORTH CAROLINA, NCDEHNR (DSW0l)
P.O. NO ...... : CONTRACT# 28928 COLLECT DATE.: 07/28/94
CONTACT ...... : SHARON ROGERS PHONE ........ : [phone]
PROJ. MGR .... : Edwin (Ed) Marti ORIGINATOR ... : MCM
-----------------------------PROJECT TIMETABLE------------------------------
UNIT IN DATE
RECEIVING 09 /14/94
WET LAB 09 /15/94
HRMS LAB 0'11.i-i(trq,o 9 /2 3 / 911
HR RPT PR 0113~~ Q.9 /2 9 / 9-4'
SHIPPING o~/)i,rf 1-G / 0 3 / ~11
Due To Client
ACTUAL OUT DATE
09 /15 /94 ~r:14{e-t4o 9 /2 3 / 9 4
oq/,23fl/O 9 /2 9 / 94
c?Ci/J..~tf 10 ,' 0 3 ;' 9,t
04/2b~'f10 / 03 ;' 94
o"l/'2-8~'(0/0~/94-
ACTUAL
----------------QUALITY ASSURANCE/ QUALITY CONTROL SAMPLES-----------------
TLI BLANKS ... : 1
-------------------SPECIAL INSTRUCTIONS / QA REQUIREMENTS-------------------
WET LAB .... : Low Level PRESPIKE STANDARD: NA
ANALYTE CONC UNIT: PPQ
Needed: Confirms
The TLI Chain-of-Custody IDs match client Chain-of-Custody IDs where
present, or in cases where they do not match, see the Project
Communication Form for reconciliation.
SPECIAL INSTRUCTIONS:
Completed by:
Reviewed by:
~~DATE ~ DATE:
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
q /14-[qf
9/r(fl 'f ( PMGTH0794)
-1 '"' . ._
Printed: 14:44 09/14i94
TRIANGLE LABORATORIES OF ATP, INC.
PROJECT· COMMUNICATION TRACKING FORM page_/_ of
i TLI Project Number: J_CJ~QO
I
Use this form to record all exchanges of information between production units as well as personnel
handling this project. Decisions, corrective actions and recommendations must also appear on this
tracking document.
Date Name Comment I Decision I Resolution / Action / Observation
~-\ br-r-, u\~ (91'\;\ _)_ .l t't~~ ~ ~--~
~~I---., ..J...._ -~' L-, \ k . Wt \ J 1->-vr-
0.7K k.~
1 1
SOP No. CGN t26 RIIVISIOl'I 2. t ATTAOtllSfT' I to November 1993 page 3 of 4
! . I , PROJECT COMMUNICATION TRACKING FORM page_ of_
TLI Project Numbet: 'l-9GOO
Use this form to record all exchanges of information between production units as well as personnel
handling this project. Decisions, corrective actions and recommendations must also appear on this
tracking document.
Date Name Comment I Decision I R~solution / ~ion / Observation
-1l1t l~Y (lN\ ~~~s (tJ; ) ~ ()1 I~ r.Aiw t:4~ o-1~,5 rA-vU~?
I V '--"'. 1
,;t
Ii
I
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'
...
I
.
I
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· .. : 1 2
SO!' No. CGN126 Revision 2. 1 ATTACHMENT I 10 November 1993 page 3 of •
+--------------------------------------------------------------------------------------------------------------------------+ I TRIANGLE LABORATORIES OF RTP, INC. PAGE 1 OF 1 I PCDD/PCDF/PBDD/PBDF Sample Preparation Tracking & Management Form +,-~g~f~::~1~g~~'.~::;;:;~;~------------------------~;::::-::::::--_;;_-;~~=~=i;;~~NO~_=_~_-;A_-_~_~;M_=N_~-~~~~-~-~-~r_9_o_i;M_~_~_~~~~-;;;TA-+I WL Spike: 20 ul, cone: 0.100 ng/ul +1::~:::+1-:j~~:----~1----:::::,:-------+l------~~g~i-------+l-s~~~LE-+l~f;:-1~~--+l-~~~-~A-15-+l-~!~g:-------+l-~~~~-------+l-~~~1~-+I ID I SAMPLE ID Before After g / 1 ~tials IniO~Jl 'ut Initials Initials Yesnro1 +------+------------------------------+---------+---------+------+-------------+-------------+-------------+-------------+----~v + I I TLI BLANK 1xxxxxxxxx1xxxxxxxxx1 I I I I I 1'4 I ooo TLI wATER BLANK xxxxxxxxx xxxxxxxxx ;).oo P?R C-l,U)1\_) Nr. +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+---T----+ 1001 I 88-36-1 942828 l~~~~~l~~~~~I r75 I nrR I ~/ I I I j I +------+------------------------------+---------+---------+--------+--L----------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I i i i i i i i i i i i +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ I I I I I I I I I I I +------+------------------------------+---------+---------+--------+-------------+-------------+-------------+-------------+--------+ Gross weight of sample container+ sample before/after aliquot removal Indicate below the TLI Identification Number of the Sample Fortification Solutions: LABORATORY ID: LOW USF-AIS: COMMENTS: USF-I:~1__,_1/Ja_1r:3.·7/7/9S USF-A: USF-MX: _________ _ USF-C: GAf 1\/1tj/h5 Other: +----------------------------------------------------------+ +1-INITIAi~-OF-BOTH-THE-SPIKER_AND_OBSE::::i:~:a::-ENTERED. ___ l_/ __ 1, ::: :x:::~::::s),~~~50~ (XXXXX = Gross Weight not provided for WATER Samples.) +-----------------------------------------------------------------------------------------------------------REV 08/09/94 (PSTMF 7)--+ ---31 (_,-J Triangle Laboratories of ATP, Inc. 801 Capitola Drive • Durham, North Carolina 27713 Phone: [phone] • Fax: [phone] Printed: 14:58 09/14/94
PAGE 1 OF 1 TRIANGLE LABORATORIES OF RTP, INC. SAMPLE EXTRACTION and CLEANUP TRACKING FORM TLI Project: 29600 HROMATOGRAPHIC CLEANU_ \'f~\~'\ Ext S#.crd Spike Extr. SWr Acid Big Escltd and bev. / a er Base Fish Sil~ TLI Number Ex . Extr. Ge. 000 g1t ~' ~ TLI BLANK 001 88-36-1 ~ J <9~,✓ ~/ ~av? .11v I/' Jt, 1, ~·u t'f\ M~ I\ -v~\V'\' \\J~ ~(~~ (6l~~nt Exch e Add Tri Comments ; ~ ~ Triangle Laboratories of RTP, Inc. 801 Capitola Drive • Durham, North Carolina 27713 Phone: (919} 544-5729 • Fax: (919} 544-5491 Acid Flor-Carbon T~: Alm~ isil Co~ fer 6 gm \ ~ ~1~ l/ qh_;i ~ . ,,,,., y1 v-V 1 I \·,\Jc \ ~ ' '--< qi cwr~~ r'\ JJt-0~~ mbine Divide Sox --Rev 08/09/94 (PSTMF 4)= Printed: 14:58 09/14/94
PAGE 1 OF 1 +-----------------------------------------------------------------------------------------------------------------------------------+ TRIANGLE LABORATORIES OF RTP, INC. I PCDD/PCDF/PBDD/PBDF SAMPLE TRACKING & MANAGEMENT FORM +--------------------+ !PROJECT: 29600 I SAMPLE EXTRACT INFORMATION +--------------------+ Extract Chain of Custody I +------+------------+--------------------+-----------+-------------------+---------+------------------------------------------------+ I I TLI I FROM WET LAB I I TO MASS SPEC LAB I I I S#.crd SAMPLE ID DATE AND TIME INITIALS DATE AND TIME INITIALS COMMENTS SAMPLE RELEASED SAMPLE ACCEPTED I 000 ~~] TLI ~ BLANK ~~]9~it4 ~ ~ Y' ,LL) I OL ~~~~~]~Cf l ~. °' ~~~~~]~[~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~j loo1 ___ 188-36-1 _____ 1 _________ ~ _______ lv ________ 1 ____ ) _____________ 1 __ 1 _____ 1 ________________________________________________ 1 I I I I I I I I i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i ----i i i i i i i i i i i i i i i i ----i i i i i i i i ----i i i i i i i i -----i +------+------------+--------------------+-----------+-------------------+---------+------------------------------------------------+ I I +-----------r~---------..\, <..n Triangle Laboratories of RTP, Inc. 801 Capitola Drive• Durham, North Carolina 27713 Phone: [phone] • Fax: [phone] ----------------REV 01/21/94 (PSTMF 9)--+ Printed: 14:58 09/14/94
PAGE 1 OF 1 +-----------------------------------------------------------------------------------------------------------------------------------+ I TRIANGLE LABORATORIES OF RTP, INC. I Method: 8290X MONO -OCTA HR GC/HRMS ANALYSIS +-------------------+ Required Detection Limit: 50 PPQ !PROJECT: 29600 I +--------------------------------------------------------------------· --------------------------------------------------------------+ I SAMPLE INFORMATION RS Cone I 1ST COLUMN 2ND COLUMN 20 ul @ 100. 0 PG/ul +-----------------------------------------------------------------------------------------------------------------------------------+ I I TLI / I GC/MS FII,._EW.1}?1E !CONFIRM !CONFIRM F~E IUSF-RS IUSF-RS !ANALYSIS I S#.crd SAMPLE ID / CLIENT COLUMN: ~ COLUMN: D VOLUME INIT. COMMENTS / SAMPLE ID SOLN ID DATE +-----------------------------------------------------------------------------------------------------------------------------------+ I 000 I TLI BLANK TLI WATER BLANK I ~fNS'tP\ I NO I --I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I 001 I 88-36-1 942828 I :Yf'-15~ I "'Jb I -I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +--------.--------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ I I I I I I I I I +-----------------------------------------------------------------------------------------------------------------------------------+ Comments: Type: B Spike File: SPM2372S .. Amt of Extract: 100% +-----------------------------------------------------------------------------------------------------------REV 07/06/94 (PSTMF 6)--+ -..1 °' Triangle Laboratories of RTP, Inc. 801 Capitola Drive• Durham, North Carolina 27713 Phone: [phone] • Fax: [phone] Printed: 14:58 09/14/94
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TL-RTP Project: 29600
Client Sample: TLI WATER BLANK
Method 8290 PCDD/PCDF Analysis (b)
Analysis File: S945801
Client Project:
Sample Matrix:
TLRTPID:
Sample Size:
Dry Weight:
GC Column:
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4,7,8-HxCDD
1,2,3,6,7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3, 7,8-PeCDF
2,3,4, 7,8-PeCDF
1,2,3,4,7,8-HxCDF
1,2,3,6,7,8-HxCDF
2,3,4,6, 7,8-HxCDF
1,2,3,7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4, 7 ,8,9-HpCDF
1,2,3,4,6, 7,8,9-OCDF
TotalMCDD
TotalDCDD
Total TriCDD
Total TCDD
Total PeCDD
Total HxCDD
Total HpCDD
TotalMCDF
Total DCDF
Total TriCDF
Total TCDF
Total PeCDF
Total HxCDF
n/a
WATER
TLIBLANK
0.200 L
n/a
DB-5
Triangle Laboratories of RTP, Inc.
ND
ND
ND
ND
ND
13.8
EMPC
EMPC
ND
ND
6.3
ND
EMPC
ND
EMPC
11.8
EMPC
ND
ND
ND
EMPC
ND
ND
13.8
EMPC
ND
41.3
EMPC
ND
6.3
Date Received: I I
Date Extracted: 09/20/94
Date Analyzed: 09/25/94
Dilution Factor: n/a
Blank File: S945801
Analyst: JW
5.4
8.9
6.7
5.6
6.1
30.0
7.9
5.1
4.9
3.1
16.0
4.2
9.5
28.8
3.5
5.3
12.4
7.4
8.9
6.1
1
46.7
7.9
1 55.1
7.9
5.0
1 22.3
Continued on next page
Page 1 of2
801 Capitola Drive• Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Spike File:
ICAL:
CONCAL:
SPM2372S
SF53254
S945800
% Moisture:
% Lipid:
n/a
n/a
n/a % Solids:
1.09 36:09
1.41 32:16
1.11 36:36
2 2
M237_PSR v:1.09, LARS 5.13.12
Printed: 15:47 09/26/94
TL-RTP Project: 29600
Client Sample: TLI WATER BLANK
Method 8290 PCDD/PCDF Analysis (b)
Analysis File: S945801
Total HpCDF
13Ci2-2,3,7,8-TCDF
13Ci2-2,3,7,8-TCDD
13C12-1,2,3,7,8-PeCDF
13C12-l,2,3,7,8-PeCDD
13C 12-1,2,3,6, 7,8-HxCDF
13C 12-1,2,3,6, 7,8-HxCDD
13C12-l,2,3,4,6,7,8-HpCDF
13C12-l,2,3,4,6, 7,8-HpCDD
13Ci2-l,2,3,4,6, 7,8,9-OCDD
37C4-2,3,7,8-TCDD
13C1r2,3,4, 7,8-PeCDF
13Ci2-l,2,3,4, 7,8-HxCDF
13C12-l,2,3,4, 7 ,8-HxCDD
13C 12-1,2,3,4, 7 ,8,9-HpCDF
13Ci 2-l,2,3,7,8,9-HxCDF
13Ci 2-2,3,4,6, 7,8-HxCDF
13C12-l,2,3,4-TCDD
13C12-l,2,3, 7,8,9-HxCDD
11.8
5130
5160
5960
5420
8280
8070
7370
8280
16060
395
6210
6460
7430
9490
7780
8880
1
51.3
51.6
59.6
54.2
82.8
80.7
73.7
82.8
80.3
39.5
62.1
64.6
74.3
94.9
77 .8
88 .8
21.3
0.77
0.82
1.56
1.43
0.50
1.22
0.44
1.02
0.84
1.54
0.51
1.20
0.44
0.51
0.51
0.82
1.19
Data Reviewer: --~'-'--'--=~'---L_~=-<--~,.;,~'4:~~ ____ 09/26/94
Triangle Laboratories of RTP, Inc.
801 Capitola Drive• Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Page 2 of2
24:06
24:57
28:32
29:41
32:21
33:04
35:10
36:08
39:27
24:58
29:18
32:15
32:59
36:34
33 :36
32:52
24:43
33:22
2 3
✓
M237_PSR v:1.09, LARS 5.13.12
Printed: 15:47 09/26/94
\..
~
1-
•'•:;-••"-•A••
Initial .... Date ...
B-File/Header Changes 9L, 9-1.~# Calculated Noise Area: 9,J/
Manual Integrations f -'i-Channel: Jj,J
Transcription _/ /_ Initials: W
dBASE Corrections _/_/_ Date: 1b--~f1'1
Page No. 1 Listing of S945801B.dbf
09/25/94 Matched GC Peaks I Ratio / Ret. Time
Compound/
M_Z .... omit Ratio .. RT. Total.Peak.Area ..
MonoCDF
202-204 3.84 8:56 . 510.56
3.81 9: 09: 151.19
202-204 Peaks 7~v 661.75
MonoCDD
218-220 ON 0 .68 7:19 20.51
DC 2 .81 16 :09 261.54
218-220 Peaks 0 0.00
DiCDF
238-240 D 3. 11 11: 58 96.92
238-240 Peaks 1 96.92
DiCDD
252-254 ON 3.18 7:40 18.82
ON 7.26 8 :11 39.03
ON 4.12 13:15 21. 87
.0 1.47 16 :10 128.37
ON 2.46 18:22 22.38
252-254 Peaks 1 128.37
TriCDF
270-272 ON 0 .59 15:55 22. 71
0.80 16:39• 55 .13
1.06
16,~
164.13
DC 1.05 17: t~ 25.60
270-272 Peaks ,.r 219.26
TCDF
304-306 c~.55 24: 09 J(... 43.75
304-306 Peaks /q_;I 43 .75
13Cl2-TCDF
316-318 DC 0.59 22:53 105.73
DC 0.54 23:36 135.05
0.77 24:06 56,094.44
DC 0.93 24:37 282 .32
DC 0.70 26:05 113.12
Triangle Laboratories of RTP, Inc~
801 Capitola Drive • Durham, North Carolina 2n13
Phone: (919} 544-5729 • Fax: [phone]
Match Match
Rat RT.
F T
F F
*** Total ***
F F
T F
*** Total ***
F F
*** Total ***
F F
F F
F F
T F
F F
*** Total ***
F F
F F
T T
T F
*** Total ***
0 T
***Total***
F F
F F
T T
F F
T F
Who/ ID
Rel.RT Why Identification .. Code
0.371 FR
0.380 FR
0.293 SN
0.647 WH
0.497 w-sµ
0.307 SN
0.328 WL
0.531 FR
0.648 5rJ
0.736 SN
0.660 SN
0 .691 FR
0 .698 Total TriCDF AN
0 . 721 SN
1. 002 ~FR 2378-TCDF AN
0.950 WL
0.979 WL
1. 000 -13C12-2378-TCDF ISO
1.021 WH
1.082 WH
24
Printed: 09:14 09/25/94
\
Page No . 2 Listing of S945801B.dbf
09/25/94 Matched GC Peaks I Ratio / Ret. Time
Compound/
M_Z .... omit Ratio .. RT . Total.Peak.Area ..
DC 0.78 28:33 1,295 .21
DC 0.83 29:19 1 ,291.07
316-318 Peaks 1 56,094.44
TCDD
~Ho.64 320-322 24:43 32.17
DC 0.56
283~
81.55
DC 0 .81 29 :19 100.94
320-322 Peaks .Jo 0.00
37Cl-TCDD
328 DC 0 .00 21:18 171.16
0.00 23:20 258.02
0 .00 24:58 2,666.19
DC 0.00 25:25 25.84
DC 0 .00 28 :41 145 .71
328 Peaks 2 2,924 .21
13Cl2-TCDD
332-334 0 .61 23 :35 102 .45
0.82 24:43 61,039 .70
0.82 24:57 36,440.09
0.87 25:19 895.92
DC 1.16 29:41 710.26
DC 0.82 30:03 106.49
332-334 Peaks 4 98,478.16
13C 12 -PeCDF
352-354 DC 1. 39 28:09 165.57
1. 56 28 :32 40,509.51
1.49 28:52 599.46
1. 54 29 :18 45,972 .26
DC 1.17 30:20 78.47
352-354 Peaks 3 87,081.23
13C12-PeCDD
368-370 1.43 29:41 22,570.80
1.44 29:50 3,562.51
368-370 Peaks 2 26,133.31
HxCDF
~1(v.f_41 374-376 32:16 1 38.59
DC 1.11 32:22 30 .90
c"-0.96
32~
101.18
DC 1.07 3 3 : 3 ,_,,.vc., 14.54
374-376 Peaks ld 101 .18
13C12-HxCDF
384-386 DC 0 .49 31:15 157.75
DC 0.59 31:24 87.22
0.51 32:15 41,541.78
0.50 32 :21 55,104 .49
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Match Match
Rat RT.
T F
T F
*** Total***
F F
F F
T F
*** Total ***
T F
T F
T T
T F
T F
*** Total ***
F F
T T
T T
T F
F F
T F
*** Total ***
T F
T T
T F
T T
F F
*** Total ***
T T
T F
*** Total ***
T T
€) T
T
T T
*** Total ***
T F
T F
T T
T T
Who/ ID
Rel.RT Why Identification .. Code
1.185 WH
1.216 WH
0.991 SN
1.144 WH
1.175 WH
0.854 WL
0.935
1.001-37Cl-TCDD SURl
1.019 SN
1 .150 WH
0 .945 FR
0 . 991 -13Cl2-1234-TCDD RSl
1.000 ,_, 13Cl2-2378-TCDD ISl
1. 015
1.190 WH
1.204 WH
0.987 WL
1. 000-13Cl2-PeCDF 123 IS2
1 .012
1.027-13Cl2-PeCDF 234 SUR2
1.063 WH
1. ooo-13Cl2-PeCDD 123 IS3
1 .005
0.997 ~
1. 001 SN
l.016~FR 234678-HxCDF AN
1.039 SN
0.966 WL
0 .971 WL
0 . 997 _ 13C12-HxCDF 478 SUR3
1. 000 -13C12-HxCDF 678 IS4
~ Page No. 3 Listing of S945801B.dbf
09/25/94 Matched GC Peaks I Ratio / Ret. Ti.me
Compound/
M_Z .... omit Ratio .. RT. Total.Peak.Area ..
0.51 32:52 57,594.96
0.51 33:36 42,133.27
384-386 Peaks 4 196,374.50
13Cl2-HxCDD
402-404 1.20 32:59 32,655.91
1.22 33:04 38,744.26
1.19 33:22 47,618.93
402-404 Peaks 3 119,019.10
HpCDF
408-410 0-1.46 35:10 54. 71
_y {l vf 1. 11 36 ,~
41.44
DC 1. 63 39:2 t ~ 124.97
408-410 Peaks 54.71
13Cl2-HpCDF
418-420 0.44 35:10 34,301.13
0.44 36:34 32,401.63
418-420 Peaks 2 66,702.76
HpCDD ~ 424-426 1. 09 36:09 39.48
424-426 Peaks ;[) 0.00
13C12-HpCDD
436-438 DC 1.31 35:27 45 .45
1. 02 36:08 29 ,372.87
1.21 36:33 84.75
1.01 39:28 3,806.74
436-438 Peaks 3 33,264.36
OCDF
442-444 (!_,~0. 66 39:38 ~ 71.45
442-444 Peaks 1 {r 71.45 /
OCDD
458-460 u-o .56 39:28 ~ 62.99
458-460 Peaks /q} 62.99
13Cl2-0CDD
470-472 0.84 39:27 39,696.05
DN 0 .64 40:17 22 .31
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Match Match
Rat RT.
T T
T T
*** Total***
T T
T T
T T
*** Total ***
€) T
T T
F F
*** Total***
T T
T T
*** Total***
T T
*** Total***
F F
T T
F F
T F
*** Total ***
(i) T
*** Total ***
€) T
*** Total ***
T T
F F
Who/ ID
Rel.RT Why Identification .. Code
1.016-13C12-HxCDF 234 ALT2
1.039 -13C12-HxCDF 789 ALTl
0. 997 -13Cl2-HxCDD 478 SUR4
1. 000-13C12-HxCDD 678 IS5
1.009., 13Cl2-HxCDD 789 RS2
1.0oo'9FR 1234678-HpCDF AN
l.041~
1.122 WH
1.000 ..... 13Cl2-HpCDF 678 IS6
1.0401.. 13Cl2-HpCDF 789 SUR5
1. 000 ~
0.981 WL
1.000-13C12-HpCDD 678 IS7
1.012 FR
1. 092
1. 005Q1/FR OCDF AN
1. oooi,9FR OCDD AN
1. 000 -13Cl2-0CDD IS8
1.021 SN
26
Printed: 09:14 09/25/94
Page No.
09/25/94
4 Listing of S945801B.dbf
Matched GC Peaks/ Ratio/ Ret . Time
Match Match Who/ ID Compound/
M_Z .... Omit Ratio .. RT. Total.Peak.Area .. Rat RT . Rel .RT Why Identification .. Code
Column.. . Description ........... .
M_Z -Nominal Ion Mass(es)
RT . -Retention Time
Match Rat -Ratio Match True/False
Match RT -Time Match True/False
Rel RT -Relative Retention Time
*** End of Report***
Triangle Laboratories of RTP, Inc.
"Why" Code Description
WL -Below Retention Time Window
WH -Above Retention Time Window
SN -Below Signal to Noise Level
<M -Below Method Detection Limit
FR -Cale based on theoretical ratio
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
27
Printed: 09:14 09/25/94
S94el1 25-SEP-94 03:16 78S (EI•) Sijs:tmm·
Ii 2 F: 319,8$5 G: 321.SU H: 327,8847 I: 3:1,9792 J: 331,918
Text:TLI m WK TLil9
• F S1,11,lc
0~ __ ...,....... ___ ..._._...,._ ___ _,,_ _ __,..,
100 G S1 ,11 ,Le
0"'-__ ...,....... ___ ..._. _______ .....,.. __
1.00
6.162
1.00
8.6473
2 8
594ml1 25-IP-94 03: 16 78S CEI •) 9$: tll6.IS
Ii 2 F: 319,835 G: 321,8936 H= 327.884, I= 3:1.9792 J: 331.918
Tct=TLI m llfl« TLIIB
1 J S1,I1,G2
I
88
78
60
58
48
JJ
28
10
e ........................ ~~..::.;.. .......... ....-i~..-Clliil .....
28=00 22=00 24=00 26:00 28:00 JJ :00
100.00
6429
29
~1 25-E>-94 03=16 78S CEI•) ~:tlJBS
ri 4 F= 425."37 G: 41.9729 H= ~.8169 I= 437.8148 J: 442.9728
Text=TLI m llM TLil9
0....._..._.. _______ ..,.._ ______ __
100 ~--!I
0....._ ___________ __
100 ~,._,.......,.......,""""'8,i~ ..... .,,..,..~..........-i.....,....~~
!I
8......., ___________ _
100.00
29
100.00
479
100.00
1133
100.00
1677
3 0
594811 25-m,-94 03: 16 78S CEI +) 81$: tmilS
Ii 2 F: 319,8935 G: 321,891 H: 327 .884, I : 3:1.9'92 J: 331.9!8
Text:TLI m flIK TLil2$88
1,
58
8
198
58
8
198
58
8
28:98 22:98 24:98 26:00 28:98 38:(t
198.98
47!}
8.8453
198.98
47!}
16.1113
198.98
47!} s.m
198.98
4737
5.0768
31
894m91 25-m,-94 03=16 70S (El•) &,5=1«6.S
I 4 F= e;,7737 G: ~.9729 H= ~.8169 I= 437.8140 J: 442.9728
Text:TLI m llJH( TLil2$00 · ·
l ...
i.-...,r,~,..._.,,,.,,,.,,vw,.,itii-
51
0~--------------1• i ..... ~~,.....~~t'la
Ei0 ~.,..,.lllflJI
0....._ ____ ......., _________ _
lctli,wi._.~...,..,.......,........,....,;r.,.,.~.......,.......,........,...__...,
51
51
0 ________________ _
let.ct
1133
22,5639
1ct.ct
1133
7.2893
let.ct
1677
29.4721
1ct.ct
1677
9,J,81
32
8946981 25~-94 83: 16 i'8S CEI •) 51$: tlBiS
~ 2 F: 319,8$5 G: !1.89"£ H: 327 ,8847 I: 31,9792 J: 331.9JS
Text :llI m llff« llll2$l\l
8
111
I
8
111
I
8
111
I
8
28:11 22 =11 24:88 26:80 28:11 J :88
111.11
47!)
5125
188.88
47!)
6429
111,88
47!)
8329
111,11
47!)
!-14
33
5945801 25-QJ-94 03: 16 78S CEI •) Sus= tll6S
Ii 3 f: 391.8127 G: 392.9760 H: 481.ffl I: 483.~ J: GJ.9729
Text:TLI m II.fl« TLil9
58
e .............................. ~...i.-.:~ ...... ~ ...................... 111 J S1
11.ce
1133
~
11.ce
1133
8674
34
ssmtl 25-f:P-94 83: 16 70S (EI•) &!s:tmm
Ii 4 f: 425.7737 G: ut.9729 H: UJ.8169 I: 437 .8140 J: 442.9728
Text:TLI m lJ1I( TLil9
50
e~ ............................ ,......~ ....... ~ ..................... ~
J:80 J;:80 3]:80 J:80 39:80 48:98 41:80
180.80
1677
3192
180.80
1677
4111
180.80
1677
4375
35
, S945801 25-SEP-94 Sir=Voltage 70S Sys= NOB5US
SaRple 1 Injectton 1 Group 1 "ass.202.0186
Text:TLI WATER BLANK TLil29608
1 i,0 NorR = 63
A l. ·--; '-~ ' ... :--t ~"': • ·-:;-:. ~ .. ~"'""".7"'
8=80 9=28 18 =48 12 =88 13=28 14 =48 16=88 17=28 18:48
5945801 25-SEP-94 Sir=Voltage 70S Sys = NOB5US
SaRple 1 Injection 1 Group 1 ftass 204.0157
Text=TLI WATER BLANK TLil29608
l:1_.. _ _,.., -.,.:=, ,,f\,.:.!:::::;,-......,.._.,., --.....-,:q,-..-,-:i-. ----.-... -...... --.-•...... --•N-or_R...,: -.~-..21-3
8=88 9=28 18=48 12=88 13=20 14=40 16 =00 17=20 18=40
5945801 25-SEP-94 5ir =Voltage 705 Sys = NOB5U5
SaRple 1 Injection 1 Group 1 ftass 218.0135
Text=TLI WATER BLANK TLll29600
11--... --;·-·-,-:-=-~ ........ ----:::------;-~-*-: ... -·-;---.. -.. :;--·---··-,"-••-.. ~-----:-"~',:r•~-~ 1:6~
8=00 9=20 10=40 12 =00 13=20 14 =40 16 =00 17=20 18=40
5945801 25-5EP-94 5ir=Voltage 705 Sys = NOB5US
5aRple 1 Injection 1 Group 1 ftass 220.0106
Text =TLI WATER BLANK TLil29600
l:L~':""~-;----~ :··"-; .... _. .. :·~--=---~~~ ~
8=00 9=28 10 =40 12 =00 13 =20 14=40 16 =00 17 =20 18 =40
S945801 25-SEP-94 5ir =Voltage 705 Sys = NOBSUS
SaRple 1 Injection 1 Group 1 ftass 271.9562
Text=TLI WATER BLANK TLil29600
36
' S945801 25-SEP-94 SLr =Uoltage }0S Sys= NDB5US
Sa~ple l InjectLon l Group l ftass.237.9767
Text =TLI WATER BLANK TLll29600
Nor~= 69
....
8=08 9=28 18 =48 12 =88 13 =20 14 =40 16 :80 17 =20 18 =40
S945801 25-SEP-94 SLr =Voltage }0S Sys = NDB5US
Sa•ple 1 lnjectLon 1 Group 1 "ass 239.9738
Text =TLI WATER BLANK TLil29600
100 Nor•= 50
A ~ ..,.::'--'-w,'"~~°t~
8=00 9=20 10 =40 12 =00 13 =20 14 =40 16 =00 1}=20 18 =48
S945801 25-SEP-94 SLr =Voltage 70S Sys = NDB5US
Sa•ple 1 lnjectLon 1 Group 1 "ass 251.9745
Text=TLI WATER BLANK TLil29600
10~ Nor•' 36
0 ~
8=00 9=20 10 =40 12 =00 13=20 14 =40 16=00 1}=20 18 =40
5945801 25-SEP-94 SLr =Voltage 70S Sys : NDB5US
Sa•ple 1 InjectLon 1 Group 1 ftass 253.9716
Text=TLI WATER BLANK TLil29600
I~:-'""::"'"~ :""""'.'~:N•o:.\I<~
8=00 9=20 10=40 12 =00 13=20 14=40 16 =00 17 =20 18=40
S945801 25-SEP-94 SLr =Uoltage 70S Sys = NDBSUS
Sa•ple 1 InjectLon 1 Group 1 ftass 305.9173
Text =TLI WATER BLANK TLil29600
37
, 5945801 25-SEP-94 SLr =Voltage 705 Sys = NDB5US
Sa111ple 1 lnjectLon 1 Group 1 "ass .269.9406
Text =TLI WATER BLANK TLil29688
100 Nor111= 20 J--:; .---~-:7 :-·•:. ·;·..,:· ::'";"'""'" --;:--~---~ --:: .. -
8=88 9=28 18 =48 12=88 13=28 14 =48 16 =88 17 =28 18 =48
5945801 25-SEP-94 SLr =Voltage 70S Sys = NDB5US
Sa111ple 1 lnjectLon 1 Group 1 "ass 271.9377
Text=TLI WATER BLANK TLil29688
!:) .... _~. --~---~-~~~:
8=88 9=28 18 =48 12=88 13=28 14=48 16 =88 17=28 18=48
5945801 25-SEP-94 SLr =Voltage 70S Sys = NDB5US
Sa111ple 1 InjectLon 1 Group 1 "ass 285.9355
Text =TLI WATER BLANK TLil29600
100 Nor111= 7
A~•:-::::~~~~:~
8=00 9=20 10 =40 12 =00 13 =20 14 =40 16=00 17 =20 18=40
5945801 25-SEP-94 SLr=Voltage 70S Sys = NDBSUS
Sa111ple 1 lnjectLon 1 Group 1 "ass 287.9326
Text=TLI WATER BLANK TLil29600
10~ Hor111= 6 Ar:~~:,~.,~~~~
8=09 9=20 19=40 12 =00 13=20 14 =40 16=00 17 =20 18 =40
5945801 25-SEP-94 SLr=Voltage 705 Sys : NDB5US
Sa111ple 1 InjectLon 1 Group 1 "ass 339.8783
Text=TLI WATER BLANK TLil29600
38
., . •
· S945801 25-S[P-94 Sir=Uoltage 70S Sys= NDB5US
Sa11ple 1 Injection 1 Group 2 ftass303.9016
Text=TLI WRT[R BLANK TLil29688
IH~ Nor11= 8
At':~~=~ 19=58 21 =88 22=18 23=28 24=38 25=48 26=58 28=88 29=18 38=28
S945801 25-S[P-94 Sir =Voltage 70S Sys= NDBSUS
Sa11ple 1 Injection 1 Group 2 ftass 305.8987
Text=TLI WATER BLANK TLil29608
':b-~~~~-:~
19=58 21 =08 22=18 23:28 24=38 25 =48 26=58 28=88 29=18 38=28
S945801 25-S[P-94 Sir=Voltage 70S Sys= NDB5US
Sa11ple 1 Injection 1 Group 2 ftass 315.9419
Text=TLI WATER BLANK TLil29600
':1 ! Nor11= 5125
I I I I I I I I .. I I 19=50 21 =00 22= 10 23=20 24 =30 25 =40 26=50 28=00 29= 10 30=20
S945801 25-S[P-94 Sir =Voltage 70S Sys= NDB5US
Sa11ple 1 Injection 1 Group 2 ftass 317.9389
Text=TLI WRT[R BLANK TLil29600
':1 l
Nor11= 6541
I I I I I I I I .. I • I j
19=50 21 =00 22 = 10 23=20 24=30 25 =40 26 =50 28 =00 29 = 10 30=20
S945801 25-S[P-94 Sir =Voltage 70S Sys= NDB5US
Sa11ple 1 Injection 1 Group 2 ftass 375.8364
Text=TLI WATER BLANK TLil29600
I:
£.1:50 21=00 22=10 23:20 24=30 25 =40 26=50 28=00 29=10 3~2~
, S945801 · 25-SEP-94 SLr =Uoltage 70S Sys = NDBSUS
Sa111ple 1 InjectLon 1 Group 2 "ass319.8965
Text =TLI WATER BLANK TLll29600
l:b:-:--::;-.-··;·::::.: -~·--::--:--·"·:--:;:-·~ : .... I.~:
19 =50 21 =80 22 =10 23 =20 24 =30 25=48 26 =58 28 =08 29 =18 38=28
5945801 25-S[P-94 SLr =Uoltage 705 Sys = NDB5US
Sa111ple 1 lnjectLon 1 Group 2 "ass 321.8936
Text=TLI WATER BLANK TLil29600
1l-: -; -:· ... ;· -----;~--:~--;-"'.7"" :· ... _. •• :. u ""'';:::
19 = 50 21 = 00 22 = 10 23: 20 24 = 30 25 = 40 26 = 50 20 = 00 29 = 10 30 = 20
S945801 25-SEP-94 SLr=Uoltage 70S Sys = NDB5US
Sa111ple 1 lnjectLon 1 Group 2 "ass 327.8847
Text :TLI WATER BLANK TLil29600
] L
Nor111= 554
I .:::ll, I I .;i. I I I I ~ I I
19 =50 21 =00 22= 10 23=20 24 =30 25 =40 26 =50 28 =00 29 = 10 30=20
S945801 25-SEP-94 SLr =Uoltage 70S Sys = NDBSUS
Sa111ple 1 lnjechon 1 Group 2 "ass 331.9368
Text:TLI WATER BLANK TLil29600
IJ .h Nor111 = 6429
I I I I I I I I 19=50 21 :00 22 = 10 23 :20 24=30 25=40 26 =50 28 =00 29: 10 30=20
5945801 25-SEP-94 SLr =Uoltage 70S Sys = NDB5US
Sa111ple 1 Injechon 1 Group 2 "ass 333.9338
Text=TLI WATER BLANK TLil29600
1:1
I I I .h I I I
Nor111 = 7688
I I &J:50 21 =00 22 = 10 23 =20 24 =30 25=40 26=50 28 =00 29 = 10 30=20
40
'S945801 25-SEP-94 SLr=Voltage 70S Sys = NDB5US
Sa•ple 1 InjectLon 1 Group 2 "ass 339.8597
Text:TLI WATER BLANK TL1129688
18 j__ ···-.AL 1,. ··~ Jo,. ••• .a ..... Jl, u.A1.~
0r1 ... 1.
7
0 (:':~
19 : 58 21 : 88 22 : 18 23: 28 24 : 38 · 25 : 48 26 : 58 28 : 88 29 = 18 38 : 28
S945801 25-SEP-94 SLr=Uoltage 70S Sys: NDB5US
Sa•ple 1 lnjectLon 1 Group 2 "ass 341.8567
Text=TLI WATER BLANK TLil29688
1:
19=58 21 :88 22 :18 23:28 24 :38 25=48 26=58 28=88 29 :18 38 :28
S945801 25-SEP-94 SLr:Voltage 70S Sys : NDB5US
Sa•ple 1 InjectLon 1 Group 2 "ass 351.9000
Text =TLI WATER BLANK TLil29600
1
:1 I I I I I 19 =50 21 :00 22=10 23:20 24 =30 25 =40
S945801 25-SEP-94 SLr :Voltage 70S Sys = NDB5US
Sa•ple 1 lnjectLon 1 Group 2 "ass 353.8970
Text :TLI WATER BLANK TLil29600
1
:1 I I I I I
19 =50 21 =00 22=10 23:20 24 =30 25 :40
S945801 25-SEP-94 SLr :Voltage 70S Sys= NDB5US
Sa•ple 1 lnjectLon 1 Group 2 "ass 409.7974
Text =TLI WATER BLANK TLil29600
1
I 26 :50
I 26=50
No1
I ! I
28=00 29: 10
I 28 :00
8329
I 30 =20
5386
I 30 =20
, J : 50 21 : 00 22 = 10 23: 20 24 = 30 25 = 40 26 = 50 28 : 00 29 : 10 30 : 20
41
-5945991 25-SEP-94 SLr:Uoltage 705 Sys: NDB5US
Sa"ple 1 InjectLon 1 Group 2 "ass.355.8546
Text=TLI WATER BLANK TLll29688
Nor": 5
0
19=50 21 =00 22 = 10 23=20 24 :30 25=40 26:50 28:00 29: 10 30=20
S945801 25-SEP-94 SLr=Uoltage 705 Sys: NDB5US
Sa,iiple 1 lnjechon 1 Group 2 "ass 357,8516
Text=TLI WATER BLANK TLil29600
10 Nor,ii = 28
0----------------------------------19=50 21 =00 22 =10 23:20 24:30 25=40 26 =50 28=00 29=10 30 =20
5945881 25-SEP-94 SLr :Uoltage 78S Sys= NDB5US
Sa,iiple 1 lnjectLon 1 Group 2 ftass 367.8949
Text=TLI WRTER BLANK TLil29600
10 Nor,ii= 3844
0
19=50 21 :00 22 = 10 23 =20 24:30 25=40 26 =58 28 :00 29 = 10 30=20
5945801 25-SEP-94 SLr =Uoltage 705 Sys= NDB5US
Sa,iiple 1 Injechon 1 Group 2 ftass 369.8919
Text =TLI WATER BLANK TLil29600
10 Nor,ii= 2669
19=50 21 =00 22=10 23:20 24 =30 25 :40 26=50 28=00 29 =10 30 =28
42
I
-5945B01 25-SEP-94 SLr=Voltage 70S Sys = NOB5US
SaRple 1 InjectLon 1 Group 3 ftass 373.B208
Text =TLI WATER BLANK TLil29688
u1~ NorR = 23
A~::;::~-;~
31=88 31 =28 31=48 32 =88 32 =28 32 =48 33=88 33=28 33=48 34=88 34=28 34=48
5945B01 25-SEP-94 SLr =Voltage 70S Sys = NOB5US
SaRple 1 InjectLon 1 Group 3 ftass 375.817B
Text =TLI WATER BLANK TLl129688
191 Nor•' 23
H r: , :'.".;:'.":: ~ ;-;-; . ~ ~;' . ; . '.;:: •; :'.";-:-, ' . ::; . ; ::::---;-:-
31 = 88 31=28 31 =48 32 =88 32 =28 32 =48 33=88 33 =28 33=48 34=88 34 =28 34 =48
S945B01 25-SEP-94 SLr =Voltage 70S Sys = NOB5US
SaRple 1 lnjectLon 1 Group 3 ftass 3B3.9639
Text =TLI WATER BLANK TLil29600
10~ NorR =
A~ • I I I .M.. I fl. I .L I I
6564
I 31=00 31 =20 31 =40 32 =00 32 =20 32 :40 33 =00 33=20 33=40 34 =00 34 =20 34 :40
S945901 25-SEP-94 SLr :Uoltage 70S Sys = NDBSUS
SaRple 1 lnjectLon 1 Group 3 ftass 385.8610
Text=TLI WATER BLANK TLil29600
12728
I 31 =00 31 :20 31=40 32 :00 32=20 32 =40 33=00 33=20 33=40 34 =00 34=20 34:40
S945801 25-SEP-94 SLr =Voltage 70S Sys = NDB5US
SaRple 1 InjectLon 1 Group 3 ftass 445.7555
Text=TLI WATER BLANK TLil29600
I I I I I O I I I I I 31 :40 32 =00 32 :20 32=40 33 =00 33=20 33 =40 34=00 34 =20 34 :40
43
\
-S945801 25-SEP-94 SLr :Voltage 70S Sys: NDB5US
SaRple 1 InjectLon 1 Group 3 "ass389.8156
Text:TLI WATER BLANK TLil29600
0 -....--------.---.----.--....---.--......------.-----.----.---....--......----.-----,-----,.--,..--31 :00 31 :20 31 :40 32:00 32:20 32 :40 33 :00 33:20 33:40 34 :00 34:20 34:40
S945801 25-SEP-94 SLr:Voltage 70S Sys : NDB5US
SaRple 1 lnjectLon 1 Group 3 "ass 391.8127
Text=TLI WATER BLANK TLil29600
100 NorR = 6
0+--....----.-----.---.----.---...--.-------.---.---.----.--.......----.----.---.----.-
31 :00 31 :20 31=40 32=00 32 =20 32 =40 33 :00 33 =20 33=40 34 =00 34 =20 34=40
S945881 25-SEP-94 SLr =Voltage 705 Sys : NDBSUS
SaRple 1 lnjectLon 1 Group 3 "ass 401.8558
Text=TLI WATER BLANK TLil29600
10 NorR = 8574
B-1----~--------..L...,--_::,,,,~___::::.-----~---31 :00 31 =20 31 =40 32 =00 32=20 32 =40 33 :00 33 =20 33 =40 34=00 34=20 34=40
S945801 25-SEP-94 SLr =Voltage 70S Sys : NDB5US
SaRple 1 InjectLon 1 Group 3 "ass 403.8529
Text=TLI WATER BLANK TLil29600
10 NorR: 7201
31 :00 31 :20 31 =40 32 :00 32=20 32:40 33=00 33 =20 33=40 34=00 34:20 34=40
44
..
_ S945801 25-SEP-94 SLr=Uoltage 70S Sys = NDB5US
SaRple 1 InjectLon 1 Group 4 ftass.407.7818
Text =TLI WRTER BLANK TLil29600
•:~ -· • ·::--::-:": -: ·; -_. . 7 ---::-:-::::;; . ~ :··----:=··:-;""
0
Nor:_ ;
29
35=20 36=00 36 =40 37=20 38 =00 38 =40 39 =28 40 =00 40=40 41=28
S945801 25-SEP-94 SLr=Uoltage 70S Sys= NDB5US
SaRple l InjectLon 1 Group 4 ftass 409.7789
Text =TLI WRTER BLRNK TLil29600
!:~-;-~. ; , "7 ;-··,-·•~-,-~ ;N: ·;-•:~
35 =20 36:00 36=40 37 =20 38 =00 38 =40 39 =20 48=80 40 =40 41 =28
S945801 25-SEP-94 SLr=Uoltage 70S Sys = NDB5US
SaRple 1 InjectLon 1 Group 4 ftass 417.8253
Text =TLI WRTER BLANK TLil29600
NorR = 3192
I I 35 =20 36 =00 36 =40 37 =20 38 =00 38 =40 39 =20 40 =00 40=40 41 =20
5945801 25-SEP-94 SLr =Uoltage 70S Sys = NDB5US
SaRple 1 InjectLon 1 Group 4 ftass 419.8220
Text=TLI WRTER BLRNK TLil29600
] ~ I I I ~ I I I I I
NorR= 7058
I I I 35 =20 36 =00 36 =40 37 =20 38=00 38 =40 39 =20 40=00 40 =40 41 =20
S945801 25-SEP-94 SLr =Uoltage 705 Sys= NDBSUS
SaRple 1 InjectLon 1 Group 4 ftass 479.7165
Text =TLI WRTER BLANK TLil29600
I:
35 =20 36 =00 36 =40 37 =20 38=00 38 =40 39=20 40=00 40 =40 41 =20
45
· 5945801 25-SEP-94 Si.r:Uoltage 705 Sys: NDB5US
Sa11ple 1 Injecti.on 1 Group 4 "ass.423.7766
Text =TLI WATER BLANK TLil29688
Ut0 Nor11 = 9
0
35=20 36=00 36=40 37 =20 38 =00 38=40 39 =20 40=00 40=40 41 =20
5945801 25-SEP-94 Si.r=Uoltage 705 Sys = NDBSUS
Sa11ple 1 Injecti.on 1 Group 4 "ass 425.7737
Text=TLI WATER BLANK TLil29600
10 Nor11= 9
0
35=20 36 =00 36 =40 37:20 38 =00 38 =40 39 =20 40=00 40 =40 41 =20
S945881 25-SEP-94 Si.r =Voltage 78S Sys = NDB5US
Sa11ple 1 lnjecti.on 1 Group 4 "ass 435.8169
Text=TLI WATER BLANK TLll29600
10 Nor11= 4111
0
35=20 36=00 36:40 37=20 38 =00 38 :40 39=20 40 =00 40 =40 41 =20
5945801 25-SEP-94 Si.r :Voltage 70S Sys = NDBSUS
Sa11ple 1 lnjecti.on 1 Group 4 "ass 437.8140
Text=TLI WATER BLANK TLil29600
10 Nor11= 4110
35=20 36:00 36 =40 37:20 38=00 38 :40 39=20 40 =00 40 =40 41 =20
46
lH
00
69
49
29
-S945891 25-SEP-94 SLr :Uoltage 795 Sys: NDB5US
SaRple l Injection l Group 4 ftass.441.7428
Text:TLI WATER BLANK TLil29600
HorR= 12
0---.---.---------------------......---------~---
19
00
40
35 :29 36 :90 36 =49 37 =29 30 =99 30 =49 39 =29 49 =00 40 =49 41 =20
S945891 25-SEP-94 SLr =Uoltage 79S Sys = NDB5US
SaRple 1 Injection 1 Group 4 "ass 443.7399
Text =TLI WATER BLANK TLil29600
Nor,-:
29 V""~lf'Wlll'IJ..,...1"'Wll"W~"Vl/n,#"'4A1PV'Vo,.,..,.V...
13
BJ--.-----.-..---.----.---..---.-------.------...--------------
00
69
40
20
35 =20 36 =99 36 =40 37=29 30=00 30=40 39 =20 40 =00 40=40 41 =20
S945001 25-SEP-94 SLr=Uoltage 70S Sys = HDB5US
SaRple 1 lnjectLon 1 Group 4 "ass 513.6775
Text =TLI WATER BLANK TLil29690
35=20 36=09 36=49 3]:20 30 =00 30=49 39 =20 40 =90 40 =40 41 =20
47
-S945801 25-SEP-94 SLr :Uoltage 70S Sys : NDB5US
Sa,iple 1 lnjectLon 1 Group 4 "ass-457.7377
Text :TLI WATER BLANK TLil29600
10 Nor,i: 11
e
35:20 36 :00 36:40 3]:20 38:00 38=40 39:20 40:00 40 =40 41 :20
S945801 25-SEP-94 SLr :Uoltage 70S Sys : NDB5US
Sa,iple 1 lnjecti.on 1 Group 4 "ass 459 .7348
Text:TLI WATER BLANK TLil29600
10 Nor,i : 16
0
35 =20 36 :00 36=40 3]:20 38:00 38:40 39:20 40 :00 40=40 41 =20
S945881 25-SEP-94 Si.r:Uoltage 78S Sys : NDB5US
Sa,iple 1 lnjecti.on 1 Group 4 "ass 469 J]]9
Text:TLI WATER BLRNK TLil29600
10 Nor,i = 43]5
0
35 :20 36:00 36 :40 3]:20 38 :00 38:40 39=20 40:00 40:40 41 :20
S945801 25-SEP-94 SLr=Uoltage 70S Sys : NDB5US
Sa,iple 1 Injecti.on 1 Group 4 "ass 471,]]50
Text =TLI WATER BLANK TLil29600
10 Nor,i= 5284
35=20 36=00 36 =40 3]=20 38 :00 38 =40 39=20 40 =00 40 =40 41 :20
48
z Ref. aass 292.m Peac t~
Hei.gt -1.39 IJC!ts Spil al ~
~• Ille na tmm
Dta flle naae A:S945891
Resollt i.oo 1118
~ rurber 2
Iool2at i.oo aode EI•
Swi.tch~ Wl.Tflt
Ref I aasses 292 Im J 416.9760
5 A 293 J 332 s JS
B 14 K 334 T 370
CB L 3i U 376
D 316 ~ 340 Y 410
E 318 H 342 r 320 0 ~
G ~ p~
H ~ Q 356
I 331 R 358
Chnel I 3Jl.9792 Peac t~
5 HelJt .i IJC!ts Spil al~
49
~1 25-IP-94 03: 16 i'8S (EI•) &,s: tmilS
Ii 2 F: 319.8$5 G: 321.8936 H= 327.8847 J: 3:1.9792 J: 331.918
Text: lll m lfll TLI12931
r
~~ii8iEl.5iii!ll!!l"Bl.5~~~~~~~
c 1 ~ al: C.J o)'... i. 'I
=58 ~~~~~~~~~~~~~ ~l)lL/q~
1.08
6429
23:(1 23:J 24:(1 24=1 25:(1 25:J 26=08 26:J 2]:(I 2]:J
' \
50
S9458a1 '5-SEP-94 83:16 i'8S CEI•) ~:tmm
Ii 1 A: 282.8186 8: 284.815i C: 284.!88 D: 218.81~ £: 228.81E
Text:llI ~lER lft« llll9
ta,• A Sl,11,Gl
58
188 B S1 ,11 ,61
58
8"""'-----------------7:98 8:1 9:i 18:i 11:i 12:i
51
59&31 25-IP-94 03:16 70S CEI+) St,s:f116.S
II 2 B: J:3.~16 C: JPj,817 O: 315,9419 E: 317,99 f: 319,815
Text:TLI m aJK TLil2Rl
100 B S1,I1,fx! 1.00
8.8453
1.00
12.2188
1,00
5125
52
5945301 25-11-94 03:16 78S (EI•) StJs:tlmS
Ii 2 B: 13,9316 C: !5,a7 O: 315,9419 E: 317,SlJS f: 319,85
Text : TLI IITER flftl TLI129J
11 B S1,11,tc A= 21,$
A= 1.21
= 0.6835
Ul.P1
0~~ ............ ..-1-~.....-,~~ ............ ~ ..........
1,1
8.0453
1,1
12,21~
1.00
5125
53
5945Ei31 25-IP-94 03:16 70S CEI•) S1Js:t06.6
ti 3 ff: 373.8208 B: 375.8178 C: 13.139 O: !5.110 £: J9,81!i
Text:TLI mW TLil9
1001 A S1 ,11 ,G3 1.00
14.3713
1.00
11.5249
1.00
511
54
59459i1 25-IP-94 83:16 78S CEI•) &1s:tll6S
Ii 3 A: 373.8288 B: ~.8178 C: !3.8639 O: 15.118 E: JS.81$
Text: TLI llTER II.ff« TLil9
188 A S1,11,63
58
1':24 i:J i:J i:42 i:48 i:54 33:fl 33:'3 33:12 33:18
1.88
22.5639
1.88
22.!44
1.88
6$4
55
~1 25-SEP-94 83:16 ilS CEI•) ~:tmi.6
Ii 4 ff: 407.7818 B: 409.7789 C: 417.8253 O: 419.8228 E= 423.7766
Text:TLI m llft« TLI12$1
108 A Sl9 = 38.91
1081 B S19 = 29,34
50
= 1.m
(IIP1
1.08
15.~
1.1)
12.8322
1,1)
3192
56
• S945831 25-SEP-94 83:16 i'8S CEI•) ~:t05S
i 4 A: 487,7818 B: 489,7789 C: 417,&:53 O: 419,8228 £: 423,ms
Text :TLI m llJR TLil9
tll•A S1,11,64
111 B S1,11,
180 C S1 ,I1 ,64
0~ ..... ....-i ................. .......i~;::,,,.. ................. .....-i.-.
1,11
10,2423
1,00
2fi87
57
-
~1 25-IP-94 03:16 785 (El•) &,s:tlJm
(I 4 K: 441,7428 L: 443,7399 ~: 4oJ,rJTJ H: 459,7348 O: 469,7779
Text:TLI m IIJ1I TLitaae
100 K S1 ,It ,64
1001 L S1 ,11 ,64
A= 34.~
= 48,71
= 0,7165
ltlo)
1,00
U,7832
1.00
13,0343
1.00
4375
58
5945f.et 25-IP-94 03:16 785 CEI•) b:flll!iS
II 4 R: '61.'TIJJ H: 459.7348 O: 469.7779 P: 471,i'i!Al Q: 479,7165
Tct:TLI m llfK TLil29Iil
11 R S1,11,64
1(181 N S1 , 11 ,c.t A= 53,74
= 0.6a14 c~,
1,(18
11,3393
1.08
15.9194
1.08
43'5
59
TRIANGLE IABORATORIES OF RTP, INC.
Rav. AH -9/93
SAMPLE
DATA
19
;'fl!'llrsi,tp,-~
'" ~ ::.~ ,' '
Data File
Sample ID
Units
Analytes
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
234678-HxCDF
123789-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
Total MCDD
Total DCDD
Total TriCDD
TOTAL TCDD
TOTAL PeCDD
TOTAL HxCDD
TOTAL HpCDD
Total MCDF
Total DCDF
Total TriCDF
TOTAL TCDF
TOTAL PeCDF
TOTAL HxCDF
TOTAL HpCDF
Other Standards
37Cl-TCDD
13Cl2-PeCDF 234
13Cl2-HxCDF 478
13Cl2-HxCDD 478
13C12-HpCDF 789
Other Standards
13C12-HxCDF 789
13Cl2-HxCDF 234
TRIANGLE LABORATORIES OF RTP, INC .
Sample Result Summary for Project 29600
Method 8290X Fllll Screen Analyses (DB-5)
S945801
TLI WATER BLANK
ppq
(5 .4)
(8. 9)
(6. 7)
(5.6)
(6 .1)
13 .8
{30 .0}
{7 .9}
(5 .1)
(4. 9)
6 .3
(3 .1)
{16.0}
(4 .2)
{9 .5}
11.8
{28.8}
(3 . 5)
( 5. 3)
(12 .4)
{7 .4}
(8 . 9)
(6 .1)
13 .8
{46.7}
(7. 9)
41.3
{7 .9}
(5 . 0)
6 .3
11 .8
Percent Recovery
39 .5
62.1
64.6
74.3
94.9
Percent Recovery
77.8
88.8
S945802
942828
ppq
( 6 . 3)
(9 . 2)
(8. 2)
(6.8)
(7.4)
13 .5
69 .7
(4. 5)
(5 . 6)
(5. 4)
(4 . 9)
(3 . 9)
18 .0
(5.2)
5 .6
(8 .5)
{12.9}
(4 .1)
( 6 .1)
(14 .3)
8 .8
( 9. 2)
(7 .4)
13.5
{21.5}
(8. 3)
18.5
(4 . 5)
(5 . 5)
18 .0
5.6
Summary (%
45.5
63.8
60.7
71. 7
89.1
B
B
B
B
B
Rec)
Summary (% Rec)
72.9
79 .3
Internal Standards Percent Recovery Summary (% Rec)
13C12-2378-TCDF 51.3
13Cl2-23 7 8-TCDD 51.6
13C12-PeCDF 123 59 .6
Triangle Laboratories of ATP, Inc.
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
52 .8
48.3
58.4
Page 1
09/26/94
20
Printed: 15:54 09/26/94
TRIANGLE LABORATORIES OF RTP, INC.
Sample Result Summary for Project 29600
Method 8290X F"ull Screen Analyses (DB-5)
S945801 Data File
Sample ID TLI WATER BLANK
S945802
942828
Units
Internal Standards
13Cl2-PeCDD 123
13Cl2-HxCDF 678
13C12-HxCDD 678
13Cl2-HpCDF 678
13Cl2-HpCDD 678
13Cl2-OCDD
ppq
Percent
54.2
82 .8
80 .7
73 .7
82 .8
80 .3
ppq
Recovery Summary
56.4
72 .4
71.8
64 .0
72.7
74 .2
(% Rec)
{Estimated Maximum Possible Concentration}, (Detection Limit).
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Page 2
09/26/94
2 1
Printed: 15:54 09/26/94
TL-RTP Project: 29600
Client Sample: 942828
Method 8290 PCDD/PCDF Analysis (b)
Analysis File: S945802
Client Project:
Sampie Matrix:
lLRTPID:
Sample Size:
Dry Weight:
GCColumn:
2,3,7,8-TCDD
1,2,3,7,8-PeCDD
1,2,3,4, 7,8-HxCDD
1,2,3,6, 7,8-HxCDD
1,2,3,7,8,9-HxCDD
1,2,3,4,6,7,8-HpCDD
1,2,3,4,6,7,8,9-OCDD
2,3,7,8-TCDF
1,2,3, 7,8-PeCDF
2,3,4,7,8-PeCDF
1,2,3,4, 7 ,8-HxCDF
1,2,3,6, 7 ,8-HxCDF
2,3,4,6, 7,8-HxCDF
1,2,3, 7,8,9-HxCDF
1,2,3,4,6,7,8-HpCDF
1,2,3,4, 7 ,8,9-HpCDF
1,2,3,4,6,7,8,9-OCDF
TotalMCDD
TotalDCDD
Total TriCDD
TotalTCDD
Total PeCDD
Total HxCDD
TotalHpCDD
TotalMCDF
TotalDCDF
Total TriCDF
Total TCDF
Total PeCDF
Total HxCDF
WARREN CO. PCB LANDFILL
WATER Date Received: ·09/14/94
88-36-1 Date Extracted: 09/20/94
Date Analyzed: 09/25/94
0.175 L
n/a
DB-5
ND
ND
ND
ND
ND
13.5
69.7
ND
ND
ND
ND
ND
18.0
ND
5.6
ND
EMPC
ND
ND
ND
8.8
ND
ND
13.5
EMPC
ND
18.5
ND
ND
18.0
Dilution Factor: n/a
Blank File: S945801
Analyst: JW
1
1
1
1
6.3
9.2
8.2
6.8
7.4
4.5
5.6
5.4
4.9
3.9
5.2
8.5
12.9
4.1
6.1
14.3
9.2
7.4
21.2
21.5
8.3
4.5
5.5
Continued on next page
Page 1 of2
Triangle Laboratories of RTP, Inc.
801 Capitola Drive• Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Spike File:
ICAL:
CONCAL:
SPM2372S
SF53254
S945800
% Moisture: n/a
% Lipid: n/a
% Solids: n/a
1.03
0.84
1.19
1.06
60
36:08
39:27
32:52
35:10
B_
B_
B_
B_
B_
M237_PSR v:1.09, LARS 5.13.12
Printed: 15:47 09/26/94
TL-RTP Project: 29600
Client Sample: 942828
TotalHpCDF 5.6
0030
5520
6670
6450
8270
8210
7310
8310
13C12-2,3,7,8-TCDF
13C12-2,3,7,8-TCDD
13C12-1,2,3, 7,8-PeCDF
13C12-l,2,3, 7,8-PeCDD
13C12-l,2,3,6, 7,8-HxCDF
13C12-1,2,3,6, 7 ,8-HxCDD
13C12-1,2,3,4,6, 7,8-HpCDF
13C12-1,2,3,4,6, 7,8-HpCDD
13C12-1,2,3,4,6, 7,8,9-0CDD 16960
37CI.--2,3,7,8-TCDD
13C12-2,3,4, 7,8-PeCDF
13C12-l,2,3,4, 7,8-HxCDF
13C12-1,2,3,4, 7,8-HxCDD
13C12-1,2,3,4, 7,8,9-HpCDF
13C12-1,2,3, 7 ,8,9-HxCDF
13C12-2,3,4,6, 7,8-HxCDF
13C12-l,2,3,4-TCDD
13C12-1,2,3,7,8,9-HxCDD
521
7290
6930
8200
10180
8330
9060
1
Method 8290 PCDD/PCDF Analysis (b)
Analysis File: S945802
52.8
48.3
58.4
56.4
72.4
71.8
64.0
72.7
74.2
45.5
63.8
00.7
71.7
89.1
72.9
79.3
0.78
0.80
1.50
1.55
0.51
1.22
0.44
1.02
0.85
1.53
0.51
1.21
0.44
0.50
0.51
0.80
1.22
24:05
24:56
28:31
29:40
32:20
33:03
35:09
36:07
39:26
24:57
29:18
32:14
32:59
36:34
33 :35
32:51
24:41
33:22
Data Reviewer: --~....l.l.!..> ... ~-.::-..:.:4'-u=='!,1:g·:___ ____ 09/26/94
61
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 2n13
Phone: [phone] • Fax: [phone]
Page 2 of2 M237_PSR v:1.09. LARS 5.13.12
Printed: 15:47 09/26/94
B-File/Header Changes
Manual Integrations
Transcription
dBASE Corrections
Page No. 1
09/25/94
Compound/
M_Z .... Omit Ratio
MonoCDF ~ltY 4 .02 202-204
Q2.36
202-204 Peaks
MonoCDD
218-220 DN 0.81
DN 2.49
218-220 Peaks
DiCDF
238-240 DN 0 . 72
238-240 Peaks
DiCDD
252-254 DC 5.42
252-254 Peaks
TriCDF
270-272 DN 1.43
1.14
270-272 Peaks
TriCDD
286-288 DC 0 .97
286-288 Peaks
TCDF
304-306 DC 0.69
304-306 Peaks
13Cl2-TCDF
316-318 DC 1.10
DC 0.67
0.78
DC 0.88
DC 0 .94
DC 0 .87
DC 0.89
316-318 Peaks
Initial .... Date ...
~ 3_1 ~1 't<+
± _Ill_
_I I_
_/ I_
Calculated Noise Area: /0,&:;...
Channe 1 : 3}()
Initials:~
Date: C/(~/tlt.1
Listing of S945802B.dbf
Matched GC Peaks I Ratio / Ret. Time
Match Match Who/
. . RT. Total.Peak.Area .. Rat RT . Rel .RT Why Identification ..
8:54• 249.67 F T 0 .370 .:s~ llA~(/ 54.57 F F 0.464
304.24 *** Total***
12 :31 12. 08 F F 0.502 SN
16 :09 30.71 F F 0 .648 WH
0 0.00 *** Total***
12:50 11. 79 F F 0.533 SN
0 0.00 *** Total ***
8:10 31. 74 F F 0 .328 WL
0 0 .00 *** Total ***
16:38 30 .19 p F 0 .691 PR
16c!J 78.37 T p 0.698
78.37 ***Total***
16:39 16 .42 T F 0.668 SN
0 0.00 *** Total ***
24:06 25 .72 T T 1.001 SN
0 0 .00 *** Total***
22:50 116. 40 F F 0 .948 WL
23:35 199.06 T F 0.979 WL
24:05 68,177.83 T T 1.000-l3Cl2-2378-TCDF
24:35 470.08 T F 1. 021 WH
26:04 109.74 F F 1.082 WH
28 :32 1 ,386.63 T F 1 .185 WH
29:18 1,503.67 T F 1.217 WH
1 68,177.83 ***Total***
Triangle Laboratories of ATP, Inc.
ID
Code
ISO
I)
801 Capitola Drive• Durham, North Carolina 2n13
Phone: [phone] • Fax: [phone]
Printed: 09:15 09/25/94
'·'
Page No. 2 Listing of S945802B.dbf
09/25/94 Matched GC Peaks I Ratio / Ret. Time
Compound/
M_Z .... omit Ratio .. RT . Total.Peak.Area ..
TCDD ( 320-322 0.68 24 : 41 ' 37.30
0 .70 25 :07 25 .65
DC 0.73 28:32 127 .64
DC 0.65 29(Y 150.49
320-322 Peaks 37 .30
37Cl-TCDD
328 DC 0.00 21:17 2 16.42
0.00 23:19 180.43
0.00 24:57 3,629.68
DC 0 .00 28:41 33 .47
328 Peaks 2 3,810.11
13Cl2-TCDD
332-334 0 .95 23:34 116.31
0.80 24:41 72,048.50
0.80 24:56 40,287.14
0.79 25:18 968.62
DC 1.06 29:41 691.10
332-334 Peaks 4 113,420.57
13C12-PeCDF
352-354 DC 1.42 27 :34 77 .25
DC 1.56 28 :08 204.00
1.50 28 :31 46 ,850.34
1.48 28:50 699 .55
1.53 29:18 55,690.52
DC 1. Bl 30:19 100 .57
352-354 Peaks 3 103,240.41
13Cl2-PeCDD
368-370 1. 55 29:40 27,716 .29
1. 55 29:48 4,211.46
368-370 Peaks 2 31,927.75
HxCDF
374-376 1.19 328' 102 .14
374-376 Peaks 1 · 102.14
13Cl2-HxCDF
384-386 DC 0.52 31:13 192 .04
DC 0.62 31:22 104.52
0 .51 32:14 45,653.79
0.51 32 :20 56,413.13
0.51 32:51 60,153.59
0.50 33:35 46,218.43
384-386 Peaks 4 208,438.94
13Cl2-HxCDD
402-404 1.21 32:59 36,916 .53
1.22 33:03 40,353 .87
Triangle Laboratories of RTP, Inc.
801 Capitola Drive • Durham, North Carolina 2n13
Phone: [phone] • Fax: [phone]
Match Match
Rat RT.
T F
T F
T F
T F
*** Total ***
T F
T F
T T
T F
***Total***
F F
T T
T T
T F
F F
***Total***
T F
T F
T T
' T F
T T
F F
*** Total***
T T
T F
***Total***
T T
*** Total ***
T F
F F
T T
T T
T T
T T
***Total***
T T
T T
Who/ ID
Rel.RT Why Identification .. Code
0 .990
1.007 SN
1.144 WH
1.175 WH
0.854 WL
0.935
1.001 -37Cl-TCDD SURl
1.150 WH
0 .945 FR
0. 990 -13C12-1234-TCDD RSl
1.000 -13Cl2-2378-TCDD ISl
1. 015
1.191 WH
0 .967 WL
0.987 WL
1 . ooo-13Cl2-PeCDF 123 IS2
1.011
1.027 _. 13C12-PeCDF 234 SUR2
1.063 WH
1. 000,.... 13Cl2-PeCDD 123 IS3
1.004
1.016 -234678-HxCDF AN
0.965 WL
0.970 WL
0 . 997 -13Cl2-HxCDF 478 SUR3
1. ooo-13C12-HxCDF 678 IS4
1.016-13C12-HxCDF 234 ALT2
1. 039 ~ 13Cl2-HxCDF 789 ALTl
0.998-13Cl2-HxCDD 478 SUR4
1. 000 -13C12-HxCDD 678 IS5
Printed: 09:15 09/25/94
'·'
Page No.
09/25/94
3 Listing of S945802B.dbf
Matched GC Peaks/ Ratio/ Ret. Time
Compound/
M_Z.... Omit
Match Match Who/ ID
Ratio . . RT . Total.Peak.Area .. Rat RT. Rel.RT Why Identification .. Code
1.22 33 :22
402-404 Peaks 3
HpCDF .-, ~r 408-410 () 1 . 06 35:10
DC 2.30 39:27
408-410 Peaks t0
13C12-HpCDF
418-420 0 .44 35 :09
0 .44 36:34
418-420
HpCDD
424-426
424-426
Peaks 2
13C12-HpCDD
436-438 DC 0.90 35:26
1.02 36:07
1.05 39:27
436-438 Peaks 2
OCDP
442-444 ~C'-' 1 .03 39 :w 442-444
OCDD
458-460
458-460
13Cl2-0CDD
470-472
Column ...
M_Z
RT .
Match Rat
Match RT
Rel RT
Peaks
0.84 39cf) Peaks 1.
0.85 39:26
DC 1.34 40 :09
DC 0.95 40:18
Description ........... .
-Nominal Ion Mass(es)
-Retention Time
Ratio Match True/False
-Time Match True/False
-Relative Retention Time
*** End of Report***
Triangle Laboratories of RTP, Inc.
55,732.31 T T 1.010-13C12-HxCDD 789
133,002 .71
28.82
110.39
0.00
34,881.12
35,588.01
70,469.13
19.82
.;1.68
0.00
58.05
***Total***
T T
p p
***Total***
T T
T T
***Total***
-(i)r p
T
***Total***
T F
1.000 ✓
1.122 WH
1 .000 -
1.040 -
0.981
1.000
0.981 WL
13C12-HpCDP
13Cl2-HpCDP
678
789
30,184.33 T T 1 .000-13C12-HpCDD 678
3,791.12 T F 1.092
33,975 .45 *** Total ***
30.16 t:) T efJ 1 .005-FR
0.00 ***Total***
138.49 T T 1.000 -OCDD
138.49 *** Total***
42,914.16 T T 1.000 .,,,,. 13Cl2-0CDD
35.51 F F 1.018 WH
28.94 T F 1.022 SN
"Why" Code Description
WL -Below Retention Time Window
WH -Above Retention Time Window
SN Below Signal to Noise Level ,.
<M -Below Method Detection Limit
PR -Cale based on theoretical ratio
RS2
IS6
SUR5
IS7
AN
IS8
64
801 Capitola Drive • Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Printed: 09:15 09/25/94
S5fAIE !-IP-94 84= 81 78S CEI •) &,s=tmm
12 F: 319,&5 6= :11,891 H= :£',884] I= 3:1.9'92 J: 331.918
Text. =942828 n.11588
• r s1,11,~
,..._ ____________ _
188 G s1,11,~
23:1 24=88 24=1 25:88 25:1 26:88
1,88
8,211
1,88
8.!i22
65
~ 25-IP-94 84:81 78S CEI•) Qs:tll6JS
112 F: 319,&5 G: 321,891 H= 327,8847 I= 3:1,9792 J: 331,918
Text :9428Z8 1Lil9
J S1 ,11 ,~ 188,88
II
,e
68
I
48
I
28
18
8-.......-.~ ...... ~~~ .................. ~.-o-. ..... 28:88 22:88 24:88 26:88 28:88 J:88
7535
66
S94Ea!2 !-IP-94 84:81 '8S CEI•) &,s:tm.S
Ii 4 F: e.m; G: ~.9'29 H: ai.8169 I: W.8148 J: 442.9728
Text: 942828 n.11293
·~---------------188
2.NUI~,,~~,.,._~
i
8~-------------188 ...... ~~,........~-~
i
8........,........, _____________ _
J:88 J:88 3]:88 38:89 39:88 48:89 41:88
188.88
4631
188.88
1857
188.88
1624
67
stM6882 25-!P-94 84=01 '8S CEI•) 9.is=tll!i6
I 2 F= 319.815 G= 321.891 H= £'.8847 I= 31.9'92 J: 331.918
Text:942828 1LI&00
L_
58
8
108
58
8
108
58
8
108
58
0
29=08 22=80 24:08 26:08 28=80 J:80
100.00
4531
6.2191
100.00
4531
21.4847
108.08
4531
6.W5
108.08
4531
5.2588
68
:-'
S9458E 25-IP-94 04:81 7E CEI•> &,s:tll5JS
Ii 4 r: e.7737 G: 41.9729 H: ai.8169 I: 43],8148 J: ~.9728
Text :942828 TLiall
!i8 ,~...,...,...~ ..... ,,...,..~...., ........ ~~~ .......... ~
188
~~~~,,,,...,_ilf"'l"'Wv.rv,/
!i8 ~~~~ , ........ ____ ...._,_..,_.....,_,...._....,.... __ _
188 ....... ~~ ....... ,,,...,,,.-~
!i8
!i8 e...._ _____________ _
188.88
1857
1.1281
188.88
1857 ,.ss
188.88
1624
i.~11
188.88
1624
9.6698
69
5845& 25-IP-94 84:81 70S (£!+) &,s:tm.,S
Ii 2 F: 319.8$5 G: 321.891 H: 327.8847 I: 31.9'92 J: 331.918
Text :942828 n.112R1
1
I
8
111
I
8
180
I
8
111
I
8
28:80 22:80 24:80 26:80 28:IJ 38:IJ
111.11
4631
6126
111.80
4631
,sj66
111.80
4631
8888
111.80
4631
191
70
S945802 25-11-94 84: 81 '8S CEI •) &,s: tl:6!m
Ii 3 r: !1.8127 G: 392 .9'60 H: 481.8558 I : 483 .8529 J: 41 .9729
Text =942828 TLil2!08
Ul,88
1E7
6726
Ul.88
1E7
11141
71
S9458E 25-El-94 84:81 78S CEI•) &,s:tmilS
ti 4 F= 425.7T!) G= G.9729 H= ~.8169 I= 437.8148 J: 442.9728
Tct :942828 TLll2$88
e ............................................................................ _.. ....
J;:88 J:88 37:88 38:89 39:88 48:89 41=88
188.88
1624
3442
188.88
1624
~
188.88
1624
4768
72
S945B82 25-SEP-94 SLr =Uoltage JBS Sys : NDB5US
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Text =942B28 TLil29600
l:L~~ .. b, ~~~ .. ~;~~~
8=88 9=28 18=48 12=88 13 =28 14=48 16 =88 17 =28 18 =48
S945802 25-SEP-94 SLr :Uoltage J0S Sys : NDB5US
SaRple 1 lnjectLon 1 Group 1 ftass 284.8157
Text=94282B TLil29688
I:)_.__ ... , -,--=---::m:r::i.,.,-o---.,-~-.. • .....,_....,, _.....,._, _____ , _______ ,N_or-R=,..._ .. ,_2_15-
8:88 9:28 18 :48 12=88 13 :28 14:40 16 =88 1J=20 10 =48
S945802 25-SEP-94 SLr =Uoltage J0S Sys : NDB5US
SaRple 1 InjectLon 1 Group 1 ftass 21B.0135
Text=942828 TLll29600
1:1 _ -, . ; -' . --;• ' . : ; -: . ;: ·;· . ~ NorR : 157
• v,, ..
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8=08 9:20 10:48 12=00 13:20 14 =40 17 =20 18 =40
S945802 25-SEP-94 Str =Uoltage JBS Sys: NDBSUS
SaRple 1 lnjectton 1 Group 1 ftass 220.0106
Text=942B28 TLil29600
11 . ., ~ :::--'" : ·--:---; ; -: •·· ; , ·:--• =7'::; ... ~ """.":":" -~ "•: • ;r~:-• ' -: ...
8=00 9=20 10 =40 12 =00 13:20 14 =40 16 =00 17 =20 18 =40
S945802 25-SEP-94 Str =Uoltage 70S Sys = NDB5US
SaRple 1 Injectton 1 Group 1 ftass 271.9562
Text=942829 TLil29600 19b Non, 9
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8=00 9=20 10:40 12 =00 13 =20 14=40 16 =00 17 =20 18 =40
73
5945802 25-SEP-94 Sir=Uoltage 70S Sys = NDB5US
Sa~ple 1 Injection 1 Group 1 ftass.237.9767
Text =942828 TLll29600
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8=88 9=20
5945802 25-SEP-94
Sa~ple 1 Injection 1
Text=942828 TLil29600
. ,. • .,_.., e ·-,.: r % , : ' ' 18=48 12 =88 13=28 14 =48
Sir=Uoltage 70S Sys= NDB5US
Group 1 "ass 239.9738
Nor~= 69
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1:L--: .. :::--;""" .. ~~·~ ·--. ";:•. :-'""~~·.,.. --.~
8=80 9=20 18=40 12=00 13=28 14=48 16 =88 17 =28 18 =48
S945802 25-SEP-94 Sir =Uoltage 70S Sys = NDB5US
Sa~ple 1 Injection 1 Group 1 "ass 251.9745
Text=942828 TLil29600
lH~ . ! . ,
1
Nor~= 35 A~~= 8=00 9=20 10 =40 12 =00 13=20 14=40 16=00 17=20 18=40
S945802 25-SEP-94 Sir=Uoltage 70S Sys= NDB5US
Sa~ple 1 Injection 1 Group 1 ftass 253.9716
Text=942828 TLil29600
1:k ~. :~~-•-:::~--~---=-•-;: ... ~
8=00 9=2H 10=40 12=00 13=20 14 =40 16=00 17=20 18=40
5945802 25-SEP-94 Sir=Uoltage 70S Sys = NDB5US
Sa~ple 1 Injection 1 Group 1 "ass 305.9173
Text=942828 TLil29600
10 6
8=00 9=20 10 =40 12=00 13=20 14=40 16 =00 1}=20 18=40
74
S945802 25-SEP-94 Sir =Uoltage 70S Sys = NDBSUS
sa-ple 1 Injection 1 Group 1 "ass 269.9406
Text=942828 TLll29688
1:k,w: ; :-'•:~M-~ I:& o~r~: ~4,;~
8:88 9=20 18 =48 12=88 13=28 14 =48 16=88 17:28 18=40
S945802 25-SEP-94 Sir :Uoltage JHS Sys: NDBSUS
sa-ple l Injection 1 Group 1 "ass 271.9377
Text=942828 TLil29600
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8=00 9=20 10 =40 12=00 13 =28 14=48 16:88 17 =28 18:48
S945B02 25-SEP-94 Sir =Uoltage 70S Sys : NDBSUS
sa-ple 1 Injection 1 Group 1 "ass 285.9355
Text =942B28 TLil29600
Nor-=
0 --~ -. _______,..., --. -.---....-, --. --,---.......-, ---.--..--, --8=00 9=20 10=40 12 =00 13=20 14 =40 16:00 17 =20 18 =40
S945B02 25-SEP-94 Sir=Uoltage 70S Sys : NDBSUS
sa-ple 1 Injection 1 Group 1 "ass 287.9326
Text=942828 TLil29600
10~ NorR : 6
af"r'=·~~~~-:~
8=00 9:20 10 =40 12:00 13:20 14:40 16 =00 17=20 18 =40
S945802 25-SEP-94 Sir=Uoltage 70S Sys: NDBSUS
Sa•ple 1 Injection 1 Group 1 "ass 339.8783
Text =942828 TLil29600
10 Nor-= 5
8=00 9=20 10=40 12:00 13:20 14:40 16:00 17 =20 18=40
75
S945802 25-SEP-94 SLr=Uoltage J0S Sys= NDB5US
SaRple 1 lnjectLon 1 Group 2 ftass303.9016
Text=942828 TLil29688
10\" NorR= 6 ar ~
19 =58 21 =88 22 = 18 23:28 24=38 25:48 26=58 28=88 29 = 18 38=28
S945802 25-SEP-94 SLr=Uoltage JBS Sys= NDB5US
SaRple 1 InjectLon 1 Group 2 ftass 305.8987
Text =942928 TLll29688
18 -Nor11 , J
B
19=58 21 =88 22: 18 23=28 24=38 25=48 26=58 28=88 29= 18 38=28
S945802 25-SEP-94 SLr=Uoltage J0S Sys= NDB5US
SaRple 1 lnjectLon 1 Group 2 ftass 315.9419
Text=942828 TLil29600
108, ~ Nor,-= 6126
a~ I I I I I I I I • I e I ;
19=50 21 =00 22= 10 23 =20 24 =30 25=40 26=50 28 =00 29 : 10 30=20
S945802 25-SEP-94 SLr=Uoltage J0S Sys= NDB5US
SaRple 1 lnjechon 1 Group 2 ftass 317.9389
Text=942828 TLil29600
1:1 ~ Nor,-= 7952
I I I I I I I :tJ, e I I 19=50 21 =00 22= 10 23 =20 24=30 25=40 26=50 28=00 29 : 10 30=20
S945802 25-SEP-94 SLr=Uoltage J0S Sys : NDB5US
Sa,-ple 1 lnjechon 1 Group 2 ftass 375.8364
Text=942828 TLil29600
10
1:,:50 21 =00 22=10 23:20 24=30 25=40 26=50 28 =00 29=10 30 =20
76
._,
S945802 25-SEP-94 Sir=Uoltage ]HS Sys = NDB5US
5aaple 1 Injection 1 Group 2 "ass319.8965
Text=942828 TLil29688
19=58 21 =88 22= 18 23:28 24=38 25=48 26=58 28 =88 29 = 18 38 =28
5945802 25-5EP-94
Saaple 1 Injection 1
Text=942828 TLil29688
5ir =Uoltage ]HS Sys = NDB5US
Group 2 "ass 321.8936
] : ~ -:~ I ;~,•
19=58 21=88 22 =18
S945802 25-SEP-94
Saaple 1 Injection 1
Text =942828 TLll29600
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S945802 25-SEP-94
Saaple 1 Injection 1
Text=942828 TLil29600
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I I 19:50 21 =00 22 = 10
5945802 25-SEP-94
5aaple 1 lnjecti.on 1
Text=942828 TLll29600
1:1
I I •• r50 21 =00 22 : 10
23:28 24=38 25 =48
Sir =Uoltage ]HS Sys= NDB5US
Group 2 "ass 327.8847
qi, I l I 23 :20 24=30 25 :40
Sir =Uoltage JBS Sys = NOB5US
Group 2 "ass 331.9368
I I h I I 23 =20 24=30 25 =40
Sir =Uoltage JBS Sys = NOB5US
Group 2 "ass 333.9338
I I h I I 23 =20 24=30 25 =40
; -= --::;:--LI-:::---.-_:_
26=58 28 =88 29 =18 38 =28
Nora = ]66
I I I I 26 =50 28 =00 29 : 10 30 =20
Nora = ]565
I I I I 26 =50 28 :00 29: 10 30=20
Nora= 9577
I I I I 26=50 28 =00 29 = 10 30=20
77
5945B02 25-SEP-94 SLr=Voltage 70S Sys: NDBSUS
Sa•ple 1 lnjectLon 1 Group 2 ftass 339.B597
Text:942828 TLll29688
IH~•~ ac=::==-~..,=
19=58 21:88 22:18 23:28 24=38 25=48 26 =58 28=88 29=18 38=28
S945B02 25-SEP-94 SLr:Voltage JBS Sys: NDB5US
Sa•ple 1 InjectLon 1 Group 2 ftass 341.8567
Text:942828 TLil29688
I:
19=58 21=88 22 =18 23=28 24=38 25 =48 26 =58 28 =88 29=18 38=28
S945802 25-SEP-94 SLr =Voltage 70S Sys= NDB5US
Sa•ple 1 lnjectLon 1 Group 2 ftass 351.9000
Text =942828 TLil29600
IJ , ,
19:50 21:00 22 =10
S945B02 25-SEP-94
Sa•ple 1 lnjectLon 1
Text=942828 TLll29600
1:1 . '
19=50 21 =00 22: 10
S945802 25-5EP-94
Sa•ple 1 lnjectLon 1
Text=942828 TLil29600
I I I I 23 =20 24=30 25 =40 26=50
5Lr =Voltage 705 Sys= NDB5US
Group 2 ftass 353.8970
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SLr=Voltage 705 Sys : NDBSUS
Group 2 ftass 409.7974
Nol . ! ' 28:00 29 : 10
B808
I 30 :20
I 30=20
19=50 21=00 22 =10 23=20 24 =30 25=40 26=50 28=00 29=10 30 =20
78
S945802 25-SEP-94 SLr =Uoltage 70S Sys = NDB5US
SaRple 1 lnjectLon 1 Group 2 ftass355.8546
Text:942828 TLil29688
100 NorR= 5
0--------------------------------------19 =50 21 =00 22= 10
10
S945802 25-SEP-94
SaRple 1 InjectLon 1
Text=942828 TLil29600
23 =20 24=30 25 =40 26=50
SLr =Uoltage 70S Sys= NOB5US
Group 2 ftass 357.8516
28 =00 29 : 10 30 =20
HorR = 13
0 +------.--...----r-----..-------.---------..--.......... ----.--......---r----..---1s=50 21 =00 22 =10
10
S945882 25-SEP-94
SaRple 1 lnjectLon 1
Text =942828 TLil29600
23 =20 24 :30 25 :40 26=50
SLr=Uoltage 785 Sys = NDB5US
Group 2 ftass 367.8949
28 =00 29 = 10 30 =20
Nor,i = 5091
e+-----,.-------------..----------------....&....;-------19 :50 21 =00 22 =10
10
S945802 25-SEP-94
SaRple 1 lnjectLon 1
Text =942828 TLil29600
23 =20 24 =30 25 =40 26=50
SLr =Uoltage 70S Sys : NDBSUS
Group 2 ftass 369.8919
28 =00 29 : 10 30=20
NorR = 3281
--+------------,,__ __________ ,,__ _ _,,. _____ .......... ~.,.._-
19 = 50 21 :00 22=10 23:20 24=30 25 =48 26 =50 28 =00 29 =10 30 =20
79
S945802 25-SEP-94 Sir:Uoltage 70S Sys: NDBSUS
SaRple 1 Injection 1 Group 3 "ass373.9209
Text=942828 TLil29688
'L.-:-~;~-~ ~~~-:
31=88 31:28 31=48 32 =88 32 =28 32=48 33=88 33=28 33 =48 34 :88 34:28 34 =48
S945902 25-SEP-94 Sir=Uoltage 70S Sys: NDBSUS
SaRple 1 Injection 1 Group 3 "ass 375.8178
Text =942928 TLil29688
'L. ;: -= ·; ~ ~ ... -; :~= . :;: ":'_ ~ -;~
31 =88 31=28 31=48 32 =88 32=28 32=48 33=88 33 =28 33 =48 34 =80 34 =28 34 =48
S945802 25-SEP-94 Sir=Uoltage 70S Sys= NDB5US
Sa•ple 1 Injection 1 Group 3 "ass 383.8639
Text=942829 TLil29600
Nor•=
I 31=00 31=20 31=40 32=00 32=20 32=40 33=00 33=20 33:40 34=00 34 =20
S945802 25-SEP-94 Sir=Uoltage 70S Sys = NDBSUS
SaRple 1 Injection 1 Group 3 ftass 385.8610
Text=942828 TLil29600
I~ ' ' '
nA A .. NorR
O ,/R, I I'L, • I ,A. • I • I
31 =00 31=29 31 =40
S945802 25-SEP-94
SaRple 1 Injection 1
Text =942828 TLil29600
32 =99 32 =20 32=40 33=90 33=20 33=40 34=09 34=20
Sir =Uoltage 79S Sys = NDB5US
Group 3 "ass 445.7555
191 ' '
I I I I I I ' I I I I I 31 =00 31 =20 31=40 32=00 32=20 32=40 33=00 33=20 33=40 34=00 34 =20
6726
I 34=40
13167
I 34=49
I 34=40
80
S945B02 25-SEP-94 Str =Uoltage JBS Sys = NDBSUS
Sa•ple 1 lnjectton l Group 3 Rass3B9.B156
Text =942B2B TLil29688
100 Nor•= 8
e +-----------------"T""""-------.-----"T""""--.....----------.--31 = e e 31 =20 31 =40 32 =00 32 =20 32 =40 33=00 33=20 33=40 34 =00 34=20 34=40
S945802 25-SEP-94 Str=Uoltage 70S Sys = NDBSUS
Sa•ple 1 Injectton 1 Group 3 Rass 391.8127
Text=94282B TLl129600
10 Nor•= 6
0---------------------------------31 =00 31 =20 31=40
10
S945882 25-SEP-94
Sa•ple 1 Injectton 1
Text =942828 TLil29600
32=00 32=20 32 =40 33 =00 33 =20
Sir =Uoltage 78S Sys = NDBSUS
Group 3 Rass 401.8558
33:40 34=00 34=20 34=40
Nor•= 10641
0 ........ _____ --"l-____ .,._ _____ ....._~-.._.;:a-...------"1----
31:ee 31 =20 31=40 32 =00 32 =20 32 =40 33 =00 33=20 33=40 34=00 34=20 34=40
10
S945802 25-SEP-94 Sir=Uoltage 705 Sys= NDB5US
Sa•ple 1 Injection 1 Group 3 "ass 403.8529
Text=942828 TLll29600
Nor•= 8590
31 =00 31=20 31=40 32 =00 32=20 32=40 33=00 33 =20 33=40 34=00 34 =20 34=40
81
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Sa11ple 1 Injection 1 Group 4 ftassA0].]818
Text=942829 TLil29688
]J\\~::~r ;· •; :; :: ~ ;:-· ~ -, ; .J:-" •' ~ ::;,-~-or_•_:--;:-:-~:...._~
35=28 36=88 36 =48 37 =28 39:88 38 =48 39=28 48=88 48=48 41 =28
S945802 25-SEP-94 Sir=Uoltage 70S Sys: NDB5US
Sa11ple 1 Injection 1 Group 4 ftass 409.7789
Text =942928 TLil29688
1:b-;: =--::-~--: --:-:::::"=--~ .. -~ ;" 7:
35 =28 36 =80 36 =48 37 =28 38=88 38 =48 39 =28 48 =88 48 =48 41=28
S945902 25-SEP-94 Sir =Uoltage 705 Sys : NDB5US
Sa11ple 1 Injection 1 Group 4 ftass 417.8253
Text :942829 TLl129600
]L
I I 35=20 36 =00
S945902 25-SEP-94
Sa11ple 1 Injection 1
Text=94282B TLil29600
k I I I 36 =40 3]=20 39 =00 38 :40
Sir :Uoltage 705 Sys = NDB5US
Group 4 ftass 419.8220
I 39 :20
]L
I I .k . . .. 35=20 36 =00
S945802 25-SEP-94
Sa11ple 1 Injection 1
Text=942829 TLil29600
36 :40 37=20 38=00 38 =40 39=20
Sir =Uoltage 70S Sys : NDB5US
Group 4 ftass 479.7165
Nor11 = 3442
I I I
40:00 40 =40 41 =20
Nor11: 7765
I I I
40 =00 40 =40 41 =20
teb Nor~, e
-~~
35:20 36=00 36:40 37=20 38 :00 38=40 39=20 40 :00 40:40 41=29
82
. ·' S945B92 25-SEP-94 Sir=Uoltage JBS Sys= NDB5US
SaAple 1 Injection 1 Group 4 ftass .423.]]66
Text =942B2B TLil29600
10 Nor•= 10
0
35:20 36 =00 36 =40 3]=20 38=00 38 =40 39 =20 40 =00 40 =40 41 =20
S945802 25-SEP-94 Sir=Voltage ]0S Sys: NDBSUS
SaAple 1 Injection 1 Group 4 ftass 425,773]
Text=942B2B TLil29600
10 Nor•= 9
e ~-------T""---..-------------,...--------,--.--,__----
10
35=20 36=00
S945882 25-SEP-94
SaAple 1 Injection 1
Text:942928 TLil29600
36 =40 37=20 39=00 38=40 39=20
Sir =Uoltage JBS Sys: NDBSUS
Group 4 ftass 435.B169
40 =00 40 =40 41 =20
Nor•= 435]
0-----""""-=--------------.-...:.-.....------"P-'"--
10
35=20 36=00
S945802 25-SEP-94
SaAple 1 Injection 1
Text=94282B TLl129600
36=40 3]=20 39=00 38=40 39 =20
Sir=Voltage 705 Sys = NDBSUS
Group 4 ftass 43].8140
40 =00 40 =40 41 =20
Nor•= 4243
35=20 36=00 36=40 3]=20 38 =00 38=40 39 =20 40=00 40=40 41 =20
83
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60
40
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5945B02 25-SEP-94 SLr=Uoltage JBS Sys= NDBSUS
SaRple 1 InjectLon 1 Group 4 "ass.441.742B
Text=942B2B TLil29680
NorR= 9
0...._____,_,..._ _____ __,. ____ --------r----......---------T---
10
BB
40
20
35=20 36=00
S945B02 25-S[P-94
SaRple 1 InjectLon 1
Text=942B2B TLll29600
36=40 3]=20 38=00 38 =40 39 =20
SLr=Uoltage 70S Sys= NDBSUS
Group 4 "ass 443.7399
40=00 40=40 41 =20
NorR= 9
8 .,__---------------------------------...---.---
18
80
60
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20
35 =20 36=00 36 =40 3]:20 38 =00 38 =40 39=20 40=00 40 =40 41=20
5945802 25-S[P-94 SLr=Uoltage JBS Sys: NDB5US
SaRple 1 lnjectLon 1 Group 4 "ass 513.6775
Text=942B28 TLll29600
NorR=
35 =20 36=00 36 =40 3]:20 38 =00 38 =40 39=20 40=00 40 =40 41:20
4
84
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Text=942828 TLil296B8
10 Nora= 18
B
35:20 36 =00 36:40 3]:28 38 =00 38=40 39=20 40=80 48 =40 41 =20
S945802 25-SEP-94 SLr=Uoltage JBS Sys = NDBSUS
Saaple 1 lnjechon 1 Group 4 ftass 459.7348
Text=94282B TLil29600
10 Nora= 24
0
35=20 36:00 36 :40 37=20 38=00 38 =40 39=20 40=00 40 =40 41 =20
S945B82 25-SEP-94 SLr =Uoltage JBS Sys = NDB5US
Saaple 1 lnjechon 1 Group 4 ftass 469 .7779
Text=942828 TLil29600
18 Nora = 4760
0----,--------.----------,pL.....:~--------
10
35=28 36 =08
S945802 25-SEP-94
Saaple 1 lnjectLon 1
Text=942828 TLll29600
36 =40 3]=28 38=00 38=40 39=20
SLr=Uoltage 70S Sys= NDB5US
Group 4 ftass 4]1.J750
40=00 40 =40 41 =20
35=20 36=00 36 =40 37=20 38=00 38=40 39=20 40=00 40=40 41=20
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$945982 25-IP-94 84:81 '8S CEI•) 9$:tlllS..S
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Tm :942828 TLil293
lav· r S1 ,11 ,rx!
58
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5945882 25-IP-94 84:81 785 CEI•) St,s:tlffl
I 1 ft: 21,81'3 8: 284,8157 C: 284,!188 O: 218,81~ E: 228,811
TM:942828 TLIBa
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S94Ei882 !-IP-94 84:81 78S CEI•) Sus:f116S
14 ft: 487J818 S: 489J789 C: 4V.8253 D: 419.8229 E: eJ.7766
Text :942828 TLil9
1,88
6,618]
1.88
8.!13
1.88
3442
89
-~
5945882 25-!IP-94 94:81 '8S CE!•) ~:tam
114 [: 423.~ f: e.713] G: ~.9'29 H: e.816S I: 437.8148
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foul. :942828 1Lil2&\l
11 E S1,Il,64
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A= 17.69
= 17.11
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$94912 !i·!P-94 84:81 :,IS CEI•) ~:t06JS
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e..._....,........-i,..... ..... .....i::~~~ ..........................
1.88
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92
/
·'
TRIANGLE LABORATORIES OF RTP, INC.
Rav. AH -9/93
CALIBRATION
DATA
93
~..,
• I
Date: 09/25/94 TRIANGLE LABORATORIES, INC.
continulng Calibration for S945800
Analysis Date .... : 09/25/94 Method ...... : M237
Jperator ......... : JW Instrument .. : s
Init Calibration.: SF53254 Std.Cone .... : 50.00
ICal Date .••..•.. : 03/25/94
Analyte Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
Total MCDF 1.947 3.32 4:08 8:57 0.3709 1.860 0.087 4.7%
15:08
Total MCDD 1.850 2.98 4:58 9:35 0.3838 1.789 0.061 3.4%
15:58
Total DCDF 0.536 6.30 11:08 12:12 0.5055 0.570 -0.034 -6.0%
16:08
Total DCDD 1.239 1.51 11:58 12:54 0.5167 1. 394 -0.155 -11.1%
16:58
Total TriCDF 0.709 0.98 15:08 16:54 0.7003 0.972 -0.263 -27.0%
20:08
Total TriCDD 0.527 1.00 16:58 16:58 0.6796 0.931 -0.404 -43.4%
20:58
2378-TCDF 0.963 0.77 20:04 24:09 1.0007 0.987 -0.024 -2.4%
26:17
TOTAL TCDF 0.963 0.77 o. 9·a1 -0.024 -2.4%
2378-TCDD 0.995 a.as 21:48 25:00 1.0013 1.201 -0.206 -17.2%
26:16
TOTAL TCDD 0.995 a.as 1.201 -0.206 -17.2%
12378-PeCDF 1.012 1.58 26:13 28:33 1.0000 1.152 -0.140 -12.1%
30:36
23478-PeCDF 1.139 1.59 29:19 1.0269 1.194 -0.055 -4.6%
TOTAL PeCDF 1.076 1.59 1.173 -0.097 -8.3%
12378-PeCDD 1.310 1.64 27:36 29:42 1.0006 1.188 0.122 10.2%
30:23
TOTAL PeCDD 1.310 1.64 1.188 0.122 10.2%
123478-HxCDF 0.990 1.12 31:06 32:16 0.9969 1.104 -0.114 -10.4%
33:52
123678-HxCDF 1.328 1.13 32:22 1.0000 1.384 -0.056 -4.0%
234678-HxCDF 1.081 1.12 32:53 1.0160 1.150 -0.069 -6.0%
123789-HxCDF 1.003 1.12 33:37 1.0386 1.031 -0.028 -2.7%
TOTAL HxCDF 1.100 1.12 1.167 -0.067 -5.7%
123478-HxCDD 0.973 1.24 31:38 33:00 0.9975 0.919 0.054 5.9%
33:32
123678-HxCDD 1.137 1.25 33:05 1.0000 1.099 0.038 3.4%
Page l
94
· , Date': 09/25/94 TRIANGLE LABORATORIES, INC.
Continujng Calibration for S945800
123789-HxCDD 1.114 1. 23· 33:23 1.0091 1.014 0.100 9.8%
TOTAL HxCDD 1.074 1.24 1.011 0.063 6.3%
1234678-HpCDF 1.756 1.06 35:01 35:11 1.0005 1.678 0.078 4.7%
36:47
1234789-HpCDF 1.160 1.06 36:36 1.0408 1.024 0.136 13.3%
TOTAL HpCDF 1.458 1.06 1.351 0.107 7.9%
1234678-HpCDD 0.980 1.05 35:18 36:09 1.0005 0.977 0.003 0.3%
36:19
TOTAL HpCDD 0.980 1.05 0.977 0.003 0.3%
OCDF 1.499 0.92 35:27 39:37 1.0042 1. 250 0.249 20.0%
43:27
OCDD 1.186 0.84 39:18 39:28 1.0004 1.058 0.128 12.1%
39:38
Other Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
37Cl-TCDD 0.868 21:47 25:00 1.0013 0.956 -0.088 -9.2%
26:16
13Cl2-PeCDF 234 0.982 1.47 28:25 29:19 1.0269 1.088 -0.106 -9.8%
29:31
13Cl2-HxCDF 478 0.863 0.51 32:16 0.9969 0.966 -0.103 -10.6%
13Cl2-HxCDF 234 0.950 a.so 32:53 1.0160 0.974 -0.024 -2.4%
13Cl2-HxCDF 789 0.800 a.so 33:37 1.0386 0.814 -0.014 -1.7%
13Cl2-HxCDD 478 0.944 1.20 33:00 0.9975 0.916 0.028 3.1%
13Cl2-HpCDF 789 0.833 0.43 35:01 36:36 1.0408 0.733 0.100 13.6%
36:46
Internal Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13Cl2-2378-TCDF 1.844 0.76 23:59 24:08 1.0000 1.793 0.051 2.8%
2.4: 19
13Cl2-2378-TCDD 1.262 0.83 22:58 24:58 1.0000 1.157 0.105 9.1%
26:58
13Cl2-PeCDF 123 1.345 1.48 28:25 28:33 1.0000 1.114 0.231 20.7%
29:31
13Cl2-PeCDD 123 0.652 1.58 29:32 29:41 1.0000 0.682 -0.030 -4.4%
29:57
13Cl2-HxCDF 678 1.598 0.51 32:07 32:22 1.0000 1.398 0.200 14.3%
33:48
13Cl2-HxCDD 678 0.958 1.21 32:05 33:05 1.0000 1.008 -0.050 -5.0%
34:05
Page 2
95
Date: 09/25/94 TRIANGLE LABORATORIES, INC.
Continuing Calibration for S945800
13Cl2-HpCDF 678 1.089 0.44-35:01 35:10 1.0000 0.978 0.111 11.4%
36:46
13Cl2-HpCDD 678 0.856 1.01 35:59 36:08 1.0000 0.745 0.111 14.9%
39:39
13Cl2-OCDD 0.612 0.89 39:18 39:27 1.0000 0.519 0.093 18.0%
39:38
Recovery Standard Summary ICal Delta
Name RF Ratio RT RT Rel. RT RF RF %D
1&2 Lo/High
13Cl2-1234-TCDD 1.000 0.84 24:44 0.9907 1.000 0.000 0.0%
13Cl2-HxCDD 789 1.000 1.20 33:23 1.0091 1.000 0.000 0.0%
QC Front End Check: 1.2868
Page 3
96
~
TRIANGLE LABORATORIES, INC. Date: 03/25/94
Initial Calibration summary for SF53254
A,,alysis Date •••• : 03/25/9-i Method .••••• : M237
Instrument ••••••• : s
Analytes RF SD %BSD RT RT/LO RT/HI Ratiol Ratio2 N
Total MCDF l.860 0.000 0% 9:06 4:21 15:21 3.231 1
Total MCDD l.789 0.000 0% 9:4-l 5:11 16:11 3.086 1
Total DCDF 0.570 0.000 0% 12:23 11:21 16:21 6.586 1
Total DCDD 1.394 0.000 0% 13:06 12:11 17:11 l.569 1
Total TriCDF 0.972 0.000 0% 17:07 15:21 20:21 0.997 l
Total TriCDD 0.931 0.000 0% 17:12 17:ll 21:ll l.005 l
2378-TCDF 0.987 0.052 5% 24:22 20:21 28:21 0. 718 5
TOTAL TCDF 0.987 0.052 5% o. 718 5
2378-TCDD l.201 0.095 8% 25:12 21:11 29:11 0.762 5
TOTAL TCDD l.201 0.095 8% 0.762 5
12378-PeCDF l.152 0.0-i9 "" 28:44 24:43 32:43 l.548 5
23478-PeCDF l.194 0.060 5% 29:29 l.550 5
TOTAL PeCDF l.173 0.051 4% l.548 5
12378-PeCDD l.188 0.023 2% 29:52 25:50 33:50 l.553 5
TOTAL PeCDD l.188 0.023 2% l.553 5
123478-HxCDF l.104 0.043 "' 32:23 28:28 36:28 l.160 5
123678-HxCDF l.384 0.026 2% 32:29 l.166 5
234678-HxCDF l.150 0.048 4% 32:59 l.156 5
123789-HxCDF l.031 0.055 5% 33:43 l.169 5
TOTAL HxCDF l.167 0.038 3% l.163 5
123478-HxCDD 0.919 0.042 5% 33:07 29:ll 37: 11 l.224 5
123678-HxCDD l.099 0.036 3% 33: 11 l.238 5
123789-HxCDD l.Ol4 0.018 2% 33:29 l.230 5
TOTAL HxCDD l.011 0.018 2% l.231 5
1234678-HpCDF l.678 0.040 2% 35:16 31:15 39:15 l.054 5
1234789-HpCDF l.024 0.062 6% 36:41 l.058 5
TOTAL HpCDF l.351 0.043 3% l.055 5
1234678-HpCDD 0.977 0.031 3% 36:15 32:14 40:14 l.030 5
TOTAL HpCDD 0.977 0.031 3% l.030 5
OCDF l.250 0.077 6% 39:44 35:32 43:32 0.903 5
OCDD l.058 0.023 2% 39:33 35:32 43:32 0.840 5
Other Standards RF SD %RSD RT RT/LO RT/HI Ratiol Ratio2 N
37Cl-TCDD 0.956 0.038 4% 25:12 23 :11 27: 11 5
l3Cl2-PeCDF 234 l.088 0.044 4% 29:29 26:43 30:43 l.465 5
13Cl2-HxCDF 478 0.966 0.021 2% 32:22 0.524 5
13Cl2-HxCDF 234 0.974 0.022 2% 32:59 0.522 5 • I
13Cl2-HxCDF 789 0.814 0.042 5% 33:42 0.525 5
13Cl2-HxCDD 478 0.916 0.054 6% 33:06 l.210 5
l3Cl2-HpCDF 789 0.733 0.042 6% 36:41 33:15 39:15 0.439 5
Internal Standards RF SD \RSD RT RT/LO RT/HI Ratiol Ratio2 N
13Cl2-2378-TCDF l.793 0.077 4% 24:21 23:21 25:21 0.779 5
13Cl2-2378-TCDD l.157 0.034 3% 25: 11 23:ll 27: 11 0.806 5
l3Cl2-PeCDF 123 1.114 0.029 3% 28:43 24:43 32:43 l.456 5
Page 1
97
I"
TRIANGLE LABORATORIES, INC.
Initial Calibration SUmmary for SF53254
13Cl2-PeCDD 123 0.682 0.0-&2 n 29:50 25:50 33:50
13Cl2-HxCDF 678 1.398 0.077 n 32:28 28:28 36:28
l3Cl2-HxCDD 678 1.008 0.018 2% 33:ll 29:11 37:11
l3Cl2-HpCDJ!' 678 0.978 0.029 3% 35:15 33:15 39:15
13Cl2-HpCDD 678 0.745 0.064 9% 36 :14 35:14 37:14
13Cl2-OCDD 0.519 0.087 17% 39:32 37:32 41:32 --·-·· -·
Recovery standards RF SD %RSD RT RT/LO RT/HI
l3Cl2-l234-TCDD 1.000 0.000 0% 24:58
l3Cl2-HxCDD 789 1.000 0.000 0% 33:29
*** End of Report *** ----·· .. ·--·-•#-----·---·. .. ···--·· ----·-···--
Page 2
Date: 03/25/94
1.530 s
0.527 5
1.213 5
0.444 5
1.041 5
0.892 s
Ratiol Ratio2 H
0 .806 5
1.207 s
1 r
ENVIRONMENTAL TESTING & CONSUL TING, INC.
WARREN COUNTY PCB LANDFILL
ETC NO. 9407718
ETC NO. 9407718-09 IS MISSING
SOIL/SEDIMENT /FILTER SAMPLES
WATER SAMPLES
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road• Memphi~, TN 3801 • [phone] • FAX [phone]
August 31, 1994
Ms. Pauline Ewold
Environmental Compliance
106 Robinson Street
Ashton, VA 23005
Ref: Analytical Testing
ETC Order#
Project Description
Founded 1972
9407718
Warren County,NC
PCB Landfill
The above referenced project has been analyzed per your
instructions. The analyses were performed in our laboratory
in accordance with Standard Methods 17th Edition; The Solid
Waste Manual SW-846; EPA Methods for the Analysis of Water
and Wastes and/or 40 CFR part 136. The results are shown on
the attached analysis sheet(s).
Within the attached report, some analyte data may be reported
as "Qualified" data indicated by a "Data Flag" next to the
result. The following summarizes the possible ''Data Flags" that
may be associated with this data
Q -Surrogate recovery outside QC Limits.
j -Estimated Value, result outside calibration range.
B Analyte detected in blank.
N -Non-Compliance Report associated with this sample
or project indicating standard protocol was not
followed. Please refer to attached report.
Please do not hesitate to contact our office if you have any
questions.
Sincerely,
~ll~
Randall H. Thomas
Vice-President
General Manager
rt
Attachment
LOGIN
CHAIN-OF-CUSTODY
ENVIRONMENTAL TESTING AND CONSULTING, INC.
MEMPHIS, TN
CASE NARRATIVE
LOGIN/CHAIN-OF-CUSTODY
Client Name
Project Name
Environmental Compliance Organization
: -warren County, NC
-PCB Landfill
ETC Order#
Remarks
9407-718
Samples for the above referenced site arrived at ETC, Inc. on 07/30/94.
The login coordinator noted that the Chain-of-Custody that arrived with
the samples did not correspond to the pre-log information available.
Nathan Pera (ETC, Inc.) contacted Ms. Pauline Ewold (ECO) in order to
confirm the analyses. Per conversation with Ms. Ewold on 07/30/94, the
samples were logged according to the pre-log information.
Summary of Analyses
Soil/Sediment/Filter Samples
voe 8240
BNA 8270 / Pest 8141
RCRA Metals
TCLP -Full List
PEST/PCB 8081
Dioxins/Furans 8280
Water samples
voe
BNA 8270
Pest 8141
RCRA Metals
TCLP -Full List
Pest/PCB 8081
Dioxins/Furans 8280
Analyses for Pesticides/PCBs were subcontracted to Waste Stream
Technology, Inc.
Analyses for Dioxins/Furans were subcontracted to PACE Laboratories.
Please refer to Chain-of-Custodies within each Data Package.
Environmental Testing and consulting, Inc.
2924 Walnut Grove Road -Memphis; TN 38111 -[phone]
Cross Reference Table
Project: Warren County,NC
Sample ID
IC-003-SS
IC-001-SED
IC-001-LC
IC-001-GW
IC-002-GW
IC-001-LCH
IC-003--LC
IC-002-LC
IC-003-GW
rc-001-ss
rc-002-ss
ETC
Laboratory ID
9407-718-01
9407-718-02
9407-718-03
9407-718-04
9407-718-05
9407-718-06
9407-718-07
9407-718-08
9407-718-09
9407-718-10
9407-718-11
ETC Laboratory Order# 9407-718
Pace Lab Order # IK0899
Waste Stream Group # 9401-172
PACE
Laboratory ID
IK0899-1
IK0899-2
Not Analyzed
IK0899-3
IK0899-4
IK0899-5
IK0899-6
IK0899-7
Not Analyzed
IK0899-8
IK0899-9
waste stream
Laboratory ID ·
WS07275
WS07276
WS07277
WS07278
WS07279
WS07280
WS07281
WS07282
WS07283
WS07284
WS07285
ECO TEL N0.804 798 4305 ..... ___,.... 804 798 4305 . 9: 00 P. 03
The following changes/additions to scheduled sampling effort were made in the
field:
ECO SAMPLE
NUMBER
IC -001· SS
IC .. 002 -SS
IC• OOJ .. OW
JC-002 •GW
JC -001 -LC
IC .. 002-LC
IC-001 • SEO
IC -003 -SS
IC -001 -LCH
IC -003 -GW
SAMPLE
MEDIA
Soil
Soil
SAMPLE
LOCATION
sutface soil near air vent
sutface soil from seep
on slope
Groundwater well # 2
Groundwater well # 4
Soi I dry landfill contents
Soil
Soil
Sediment
Soil
duplicate dry landfill
contents
wet landfill contents
downstream sediment
from Richneck Creek
sediment basin outlet
ravine
Leachate filter system inlet
Groundwater Limmer well
FIELD
CHANGES
NONE
NONE
NONE
NONE
ONLY ENOUGH DR\'
MATERIAL
RECOVERED FOR
VOCAND-
ANALYSIS
DUPLICATE WET
LAND FILL
CONTENTS
NONE
NONE
NONE
NONE
ADDED SAMPLE · a:
Unless otherwise noted al! samples are to be analyzed for full voe, BNA,
RCRA metals, TCLP, PCB/pesticides, PCDD/PCDF, specialized PCB.
~c, Inc. Environmental Testing & Consulting, Inc. . 2924 Walnut Grove Rd. Memphis, TN 3811·1 (901 )327-2750 fax [phone] · •CLIENT NAME SITE SAMPLER (sign) SAMPLE I of cont. ID NUMBER -S"'S ~-cw tCH Le_ ~ /·1111gnl LOCATION/ .... ' CHAIN -OF CUSTODY RECORD PHONE #: FAX RESULTS FAX#: RUSH ANALYSES (LIST BELOW) FID# REG. TURN. PO# ICE REMARKS SAMPLE I SAMPLE I SAMPLE TYPE I ... ,... .... I DATE TIME COMP I GRAB . ~ --I ----;</? ~-'~7 4".':J 'I '-I~ 'J lsion)
ETC, Inc. · ,Environmental Testing & Consulting, Inc. i.·,2924 Walnut Grove Rd . .. Memphis, TN 38111 (901 )327-2750 fax [phone] CLIENT NAME (:!.,,d,w,>v-'Al'fn7A;_. /;.~,, •Jl,<J"'ff 0.J?-e.A I:;, ~~.,.J SITE 'IA.} tA,,,. ,.,,*) ~ .. r1u AJI', ?c../!, / /h<J"""'' , PROJECT I I SAMPLER (sign) I of SAMPLE LOCATION/ cont'. ID NUMBER DEPTH ~ zc., ,cm, --ss ":>11fl.l"'ltc ~"' ....... NdAL 4112 ,MAJt ti TC'_ -(){j::l -55 ~<)A,/11'~ $ti/(. 1::--~-, .. ~ dN.<:°L,1'/1.£: '" r--.... . ~ ~ ~ ~ .~ / ~ / ~ / .......... / / ' .,//'.'"") ' 1. R~~HED BY N~. /.., ,--., ~ CHAIN Oi., CUSTODY RECORD -7~r '' V PHONE#: ~o<I-~i -'-;''Jo< FAX RESULTS FAX#: Qn./-5~-72-•I'/ RUSH ANALYSES FID# REG. TURN. PO# ICE REMARKS SAMPLE SAMPLE SAMPLE TYPE MATRIX DATE TIME COMP GRAB AGIDF; SOIL OTHER 7,Z?/9''/ /1/ :<3 x 11~ 1/f~ /S'ja_ X I I / ~ ,...,. ~ ........ ~ """ DATE ~ .L TIME RECt!J-D BY •(sign)/(/ l1_fJ --::4,(6' ~ •. fl -j IJ.u/1~ I TIME '. 2.~~HED-BY l•,~I G .1, 11 !1-.. • , (Ud DAi . le, o1' rl ~:So l~EO BY I~ ~ ' '-~ ~ ~77, 3, RELIN lUISHED BY (print) DAfrE / TIME RF.CEIVED BY LAB (print) I S -U-?Pfman/'l !•ignl (sign) j~~~ -(LIST BELOW) DATE TIME 7A7 3,iffAA ~TE / 2 1 TIME , 2-I~I' o7Jl:,J,y TIME /050
SAMPLE
REPORTS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
·<ercury -TCLP
elenium -TCLP
Silver -TCLP
TCLP Extraction
DL -Detection Limit
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.420
<0.004
<0.007
<0.045
<0 .001
<0.075
<0.007
Leachate
DL
0 .050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:SOIL
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
Project#
Matrix :SOIL
Sample Date :07/28/94
DETECTION TIME DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 76.3 \ 0 1030 07/31/94 PM
Silver <1. 75 mg/Kg 1. 75 0935 08/17/94 AB
Arsenic <12.5 mg/Kg 12.5 0935 08/17/94 AB
Barium 122 mg/Kg 1.00 0935 08/17/94 AB
irnium <1.00 mg/Kg 1.00 0935 08/17/94 AB
comium 23 .7 mg/Kg 3.50 0935 08/17/94 AB
Mercury 0.041 mg/Kg 0.020 1540 08/08/94 JF
Lead <11.3 mg/Kg 11.3 0935 08/17/94 AB
Selenium <18.8 mg/Kg 18 .8 0935 08/17/94 AB
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
6010A
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dlchloropropene
Ethyl benzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/08/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren county,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
llinyl Chloride
Xylenes
surrogate standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-d8
S3 -4-Bromofluorobenzene
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
109
83
87
8240
08/08/94 08/08/94 LS
5.00
5.00
5.00
5.00 so.a
5.00
5.00
oc Limits
70 121
81 117
74 121
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson Street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile Organics
Benzene ND
carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate Standard % Recovery
S1 -1,2-Dichloroethane-d4 107
S2 -Toluene-dB 93
S3 -4-Bromofluorobenzene 91
DL
0.005
0.005
0.005
0.050
0.005
0.005
0.005
0.050
0.005
0.005
0.005
DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
a.so a.so
100
6.00
7.50 a.so
0.70
200
0.70 a.so
0.20
QC Limits
76 114
88 110
86 115
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
08/11/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENf AL TESTING & CONSULTING INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
Endrin ND
Methoxychlor ND
Toxaphene ND
surrogate Standard % Recovery
Sl -Dibutyl Chlorendate 115
S2 -Tetrachloro-m-xylene 104
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0
0.50
QC Limits
25 125
25 125
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab IO 9407718-01
Sample ID: IC-003-SS
Project#
FIO #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-o
Demeton-S
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Herphos
Hevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
8141
08/10/94 08/26/94 DC
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ND ug/Kg 35.0
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
rrogate standard
__,l -2,4,5-T
RESULT
UNITS: {mg/L)
Leachate
ND
ND
% Recovery
59
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
REGULATORY
DL LEVEL: {mg/L)
0.080 10.0
0.008 5.00
QC Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND -Not De~ted DL -Detection Limit
AIAA?tt~
LABORATORY MANAGER
BY METHOD
TL 1311
6640-B
cc cc
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST
TCLP Extraction Organics
TCLP Semivolatiles
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
2-Methylphenol
3&4-Methylphenol
Nitrobenzene
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Pyridine
surrogate standard
Sl -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
S4 -Phenol-d6
S5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
RESULT
UNITS: (mg/L)
Leachate
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
% Recovery
63
73
88
31
73
40
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
DL -Detection Limit
aBORATORY MANAGER
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
REGULATORY DATE
LEVEL: (mg/L) ANALYZED
08/04/94
0.13 08/19/94
0.13 08/19/94
0.50 08/19/94
3.00 08/19/94
200 08/19/94
200 08/19/94
2.00 08/19/94
100 08/19/94
400 08/19/94
2.00 08/19/94
5.00 08/19/94
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND -Not D~7'fted
.J!All:1 i~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/19/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-01
Sample ID: IC-003-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate standard
Sl -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-dl4
'4 -Phenol-d6
5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
59
61
85
67
77
61
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/19/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
oc Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
Project#
Matrix
Sample
DETECTION TIME
:SOIL
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 75.6 % 0 1030 07/31/94 PM
Silver <0.700 mg/Kg 0.700 1250 08/12/94 AB
Arsenic <5.00 mg/Kg 5.00 1250 08/12/94 AB
Barium 12.3 mg/Kg 0.200 1250 08/12/94 AB
Cadmium <0.400 mg/Kg 0.400 1250 08/12/94 AB
-:-omium 14.7 mg/Kg 0.700 1250 08/12/94 AB
ccury <0.020 mg/Kg 0.020 1540 08/08/94 JF
Lead <4.50 mg/Kg 4.50 1250 08/12/94 AB
Selenium <7.50 mg/Kg 7.50 1250 08/12/94 AB
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
-elenium -TCLP
ilver -TCLP
1'CLP Extraction
DL -Detection Limit
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.419
<0.004
0.008
0.048
<0.001
<0.075
<0.007
Leachate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
LO
5.0
:SOIL
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A ·
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl benzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Hethyl-2-pentanone (MIBK)
Methyl Ethyl Ke tone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not Det_r;ted
A~11~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
NO ug/Kg
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/08/94
100 so.a so.a
S.00
S.00
S.00
S.00 so.a
S.00 s.oo
S.00 s.oo so.a
S.00
S.00 s.oo
20.0
S.00 s.oo
S.00
S.00 s.oo s.oo
S.00
S.00
S.00
S.00
S.00
5.00 so.a so.a
5.00
50.0
50.0
20.0
5.00
S.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate Standard
Sl -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
113
92
89
8240
08/08/94 08/08/94 LS
5.00
5.00
5.00
5.00
50.0
5.00
5.00
QC Limits
70 121
81 117
74 121
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate standard % Recovery
Sl -l,2-Dichloroethane-d4 108
S2 -Toluene-dB 92
S3 -4-Bromofluorobenzene 96
DL
0.005
0.005
0.005
0.050
0.005
0.005
0.005
0.050
0.005
0.005
0.005
ND -Not Detnted DL -Detection Limit
AAAYt I~ LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
a.so a.so
100
6.00
7.50 a.so
0.70
200
0.70 a.so
0.20
QC Limits
76 114
88 110
86 115
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING INC.
2924 Walnut Grove Road -Memphis, TN 38111-(901)327~2750
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST
TCLP Extraction Organics
TCLP Pesticides
Chlordane
Heptachlor
Lindane
Endrin
Methoxychlor
roxaphene
surrogate standard
Sl -Dibutyl Chlorendate
s~ -Tetrachloro-m-xylene
RESULT
UNITS: (mg/L)
Leachate
ND
ND
ND
ND
ND
ND
% Recovery
88
78
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.010
0.001
0.001
0.001
0.040
0.100
0.03
0.008
0.40
0.02
10.0 a.so
oc Limits
25 125
25 125
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
DL -Detection Limit
LABORATORY MANAGER
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST RESULT UNITS
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-0
Demeton-S
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/10/94 08/26/94
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
BY METHOD
8141
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
surrogate standard
·t -2, 4, 5-T
RESULT
UNITS: (mg/L)
Leachate
ND
ND
% Recovery
26
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE -
ANALYZED
08/04/94
08/12/94
08/12/94
ND -Not D7tefY-ed DL -Detection Limit dA»i ~.,~
LABORATORY MANAGER
BY METHOD
TL 1311
6640-B
cc cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
1924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Methylphenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
Surrogate Standard % Recovery
Sl -Nitrobenzene-d5 70
S2 -2-Fluorobiphenyl 79
S3 -4-Terphenyl-dl4 102
S4 -Phenol-d6 5 Q
S5 -2,4,6-Tribromophenol 5 Q
S6 -2-Fluorophenol 6 Q
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
ND -Not Der,cted DL -Detection Limit
1l»t44 ~' LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13
0.50
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
lenzo(b)fluoranthene
denzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibe nzo(a,h)anthracene
Dibe nzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylpheno l
Dime thyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND -Not De~ted d.MY!✓~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-02
Sample ID: IC-001-SED
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
[sophorone
2-Hethylnaphthalene
2-Hethylphenol (o-cresol)
3&4-Hethylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate Standard
Sl -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
S4 -Phenol-d6
, -2,4,6-Tribromophenol
_6 -2-Fluorophenol
%
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg ·
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Recovery
44
50
73
50
73
40
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
QC Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,Nc
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-03
Sample ID: IC-001-LC
TEST RESULT
Percent Solids 79.7
UNITS
Project#
Matrix :SOIL
Sa~ple Date : 07/28/94
DETECTION TIME DATE
LIMIT ANALYZED ANALYZEDBY METHOD
0 1115 08/09/94 PM 160.3
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road-Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-03
Sample ID: IC-001-LC
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichlor o-2-butene
Dichlorofluoromethane
1,2-Dichlor obenzene
1,3-Dichlor obenzene
1,4-Dichlor obenzene
1,1-Dichlor oethane
1,2-Dichlor oetha ne
1,1-Dichlor oethe ne
trans-1,2-Dichlo roethene
1,2-Dichlor opropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacryla te
2-Hexanone (MBK)
Iodomethane
4-Me thyl-2-penta none (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tet rachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -No~ D4rrcted
)/011~
76.3j ug/Kg
ND ug/Kg
ND ug/Kg
1. 98j ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
108 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
10.6 ug/Kg
25.3 ug/Kg
63.1 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/08/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-03
Sample ID: IC-001-LC
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate Standard
Sl -l,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Brornofluorobenzene
ND -Not De~~ted
)JAAJ{ i lA~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
111
95
90
8240
08/08/94 08/08/94 LS
5.00
5.00
5.00
5.00 so.a
5.00
5.00
oc Limits
70 121
81 117
74 121
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
Project#
Matrix
Sample
DETECTION TIME
:AQUEOUS
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Silver <0.007 mg/L 0.007 1038 08/08/94 AB
Arsenic <0.050 mg/L 0.050 1038 08/08/94 AB
Barium 0.034 mg/L 0.002 1038 08/08/94 AB
Cadmium <0.004 mg/L 0.004 1038 08/08/94 AB
Chromium <0.007 mg/L 0.007 1038 08/08/94 AB
"-,rcury <0.001 mg/L 0 .001 0830 08/10/94 JF
ad <0.045 mg/L 0.045 1038 08/08/94 AB
Selenium <0.075 mg/L 0.075 1038 08/08/94 AB
Metal results are dry weight mg/Kg_
W1r.~ -----------J _______ _
METHOD
6010A
6010A
6010A
6010A
6010A
7470
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
-~lenium -TCLP
lver -TCLP
.l'CLP Extraction
DL -Detection Limit
µkl~
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.176
<0.004
0.010
<0.045
<0.001
<0.075
<0.007
Filtrate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
c i s-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-He xanone (MBK)
Iodomethane
4 -Methyl-2-pentanone (HIBK)
Methyl Ethyl Ketone (MEK)
Me thylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/09/94 08/09/94
100
50.0 so.a
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00 so.a
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
20.0
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate Standard
S1 -l,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND -Not DetiJted
pAA>f 1 ~
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
% Recovery
110
98
93
08/09/94
5.00
5.00
5.00
5.00
50.0
5.00
5.00
oc Limits
76 114
88 110
86 115
8240
08/09/94 LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Filtrate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene 0.005
Trichloroethene ND
Vinyl Chloride ND
surrogate standard % Recovery
S1 -1,2-Dichloroethane-d4 109
S2 -Toluene-dB 91
S3 -4-Bromofluorobenzene 96
DL
0.005
0.005
0.005
0.050
0.005
0.005
0.005
0.050
0.005
0.005
0.005
ND -Not De1/Jted DL -Detection Limit
)/AAY/ i~
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
a.so a.so
100
6.00
7.50
0.50
0 .70
200
0.70 a.so
0.20
QC Limits
76 114
88 110
86 115
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING INC.
2924 Walnut Grove Road -Memphis, TN 38111-(901)327~i7SO
-ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
Organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
,;;ndrin ND
lethoxychlor ND
Toxaphene ND
Surrogate Standard % Recovery
S1 -Dibutyl Chlorendate 123
S2 -Tetrachloro-m-xylene 108
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
BORATRY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0 a.so
QC Limits
25 125
25 125
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
· 2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST RESULT UNITS
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-0
Demeton-S
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND -Not "J~d
_)/AA>(</-
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
DETECTION DATE
:AQUEOUS
Date : 07/28/94
DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/26/94
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
BY METHOD
8141
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
~Qrrogate Standard
-2,4,5-T
RESULT
UNITS: (mg/L)
Filtrate
ND
ND
% Recovery
42
Project#
FID #
Matrix :AQUEOUS
Sample Date : 07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND -Not Dete~ed DL -Detection Limit
cYdxf I~ LABORATORY MANAGER
BY METHOD
TL 1311
6640-B cc cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP Semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Hethylphenol ND
3&4-Hethylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
surrogate standard % Recovery
Sl -Nitrobenzene-d5 78
S2 -2-Fluorobiphenyl 79
S3 -4-Terphenyl-d14 96
S4 -Phenol-d6 30
S5 -2,4,6-Tribromophenol 80
S6 -2-Fluorophenol 40
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
ND -Not Deto/)ted DL -Detection Limit
».MXJ 1~
tffi..BORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13
0.50
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3"-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND -Not Detrr-ed
AIM:Jli<fu
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/18/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-04
Sample ID: IC-001-GW
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
1ndeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
Surrogate Standard
S1 -Nitrobenzene-dS
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
S4 -Phenol-d6
~5 -2,4,6-Tribromophenol -rs6 -2-Fluorophenol
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
% Recovery
66
76
44
27
58
36
Project#
FID #
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/18/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10 .0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
QC Limits
35 114
43 116
33 141
10 94
10 123
21 100
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
Project#
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION TIME DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Silver <0.007 mg/L 0.007 1038 08/08/94 AB
Arsenic <0.050 mg/L 0.050 1038 08/08/94 AB
Barium 0.045 mg/L 0.002 1038 08/08/94 AB
Cadmium <0.004 mg/L 0.004 1038 08/08/94 AB
r"romium <0.007 mg/L 0.007 1038 08/08/94 AB
:.cury <0.001 mg/L 0.001 0830 08/10/94 JF
Lead <0.045 mg/L 0.045 1038 08/08/94 AB
Selenium <0.075 mg/L 0.075 1038 08/08/94 AB
Metal results are dry weight mg/Kg.
METHOD
6010A
6010A
6010A
6010A
6010A
7470
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road• Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
Project#
Matrix
Sample
DETECTION TIME
:AQUEOUS
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Silver <0.007 mg/L 0.007 1038 08/08/94 AB
Arsenic <0.050 mg/L 0.050 1038 08/08/94 AB
Barium 0.045 mg/L 0.002 1038 08/08/94 AB
Cadmium <0.004 mg/L 0.004 1038 08/08/94 AB
:omium <0 .007 mg/L 0.007 1038 08/08/94 AB
.. ..:rcury <0.001 mg/L 0.001 0830 08/10/94 JF
Lead <0.045 mg/L 0.045 1038 08/08/94 AB
Selenium <0.075 mg/L 0.075 1038 08/08/94 AB
Metal results are dry weight mg/Kg.
METHOD
6010A
6010A
6010A
6010A
6010A
7470
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
ircury -TCLP
alenium -TCLP
Silver -TCLP
TCLP Extraction
DL -Detection Limit
RYMANAGER
RESULT
UNITS: (mg/L)
<0.050
0.158
<0.004
0.008
<0.045
<0.001
<0.075
<0.007
Filtrate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:AQUEOUS
Date : 07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
~ethylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not Det_e2ted . j {J ,j A"/}' .//-:A,~
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
:AQUEOUS
Date : 07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/09/94 08/09/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00 so.a
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00 so.a
50.0
20.0
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS .
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
Surrogate standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND -Not Deo/7ted
JvWJ~
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
% Recovery
108
96
94
8240
08/09/94 08/09/94 LS
5.00
5.00
5.00
5.00 so.a
5.00
5.00
oc Limits
76 114
88 110
86 115
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Filtrate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene 0.005
Trichloroethene ND
Vinyl Chloride ND
surrogate standard % Recovery
Sl -l,2-Dichloroethane-d4 109
S2 -Toluene-dB 91
S3 -4-Bromofluorobenzene 96
DL
0.005
0.005
0.005
0.050
0.005
0.005
0.005
0.050
0 .005
0.005
0.005
ND -Not ted DL - De tection Limit
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.50
0.50
100
6.00
7.50
0 .50
0.70
200
0.70 a.so
0.20
QC Limits
76 114
88 110
86 115
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
1ndrin ND
Methoxychlor ND
Toxaphene ND
Surrogate standard % Recovery
Sl -Dibutyl Chlorendate 96
S2 -Tetrachloro-m-xylene 88
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0
0.50
QC Limits
25 125
25 125
:AQUEOUS
Date : 07/28/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST RESULT UNITS
0rganphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifoa
Coumaphos
Demeton-o
Demeton-S
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fenaulfothian
Fenthion
Malathion
Merphos
Mevinphoa
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
:AQUEOUS
Date : 07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/26/94
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
BY METHOD
8141
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
106 Robinson Street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
r-•rrogate Standard
-2,4,5-T
RESULT
UNITS: (mg/L)
Filtrate
ND
ND
% Recovery
47
Project#
FID #
Matrix :AQUEOUS
Sample Date : 07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080
0.008
10.0
5.00
oc Limits
25 125
DATE
ANALYZED BY METHOD
08/04/94 TL 1311
6640-B
08/12/94 cc
08/12/94 cc
ND -Not DetecfJd DL -Detection Limit »vWt1~
LABORATORY MANAGER
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP Semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Methylphenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
Surrogate standard :1§ Recovery
S1 -Nitrobenzene-dS 61
S2 -2-Fluorobiphenyl 63
S3 -4-Terphenyl-d14 84
S4 -Phenol-d6 25
S5 -2,4,6-Tribromophenol 54
S6 -2-Fluorophenol 34
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
DL -Detection Limit
LABORATORY MANAGER
(___
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13 a.so
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,Nc
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/20/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Waln1,1t Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,Nc
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-05
Sample ID: IC-002-GW
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate Standard
Sl -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
,4 -Phenol-d6
,5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
%
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
61
56
38
20
43
33
Project#
·pro#
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/20/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
QC Limits
35 114
43 116
33 141
10 94
10 123
21 100
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
Project#
Matrix
Sample
DETECTION TIME
:AQUEOUS
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Silver <0.007 mg/L 0.007 1038 08/08/94 AB
Arsenic <0.050 mg/L 0.050 1038 08/08/94 AB
Barium 0.224 mg/L 0.002 1038 08/08/94 AB
Cadmium <0.004 mg/L 0.004 1038 08/08/94 AB
~,romium <0.007 mg/L 0.007 1038 08/08/94 AB
rcury <0.001 mg/L 0.001 0830 08/10/94 JF
Lead <0.045 mg/L 0.045 1038 08/08/94 AB
Selenium <0.075 mg/L 0.075 1038 08/08/94 AB
Metal results are dry weight mg/Kg.
METHOD
6010A
6010A
6010A
6010A
6010A
7470
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
,1enium -TCLP
.lver -TCLP
TCLP Extraction
DL -Detection Limit
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.216
<0.004
<0.007
<0.045
<0.001
<0.075
<0.007
Filtrate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,Nc
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
,romodichloromethane
Jromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not Dey;ted
»NG11 ~~
ND ug/L
ND ug/L
ND ug/L
2. 58.j ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/09/94 08/09/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
20.0
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
TO: Bill Meyer Mike Kelly Brenda Rivers Pat Williamson Grover Nicholson Dexter Matthews RichardBarefoot -J/ / Routing Slip Jerry RhQtles I / Jack~utler / / ,Pat DeRosa /" Lee Crosby , CharlotteJesneck ~~ms Pierre~fer \ Date: ______ _
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate Standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
4.76j ug/L
% Recovery
112
105
95
08/09/94
5.00
5.00
5.00
5.00
50.0
5.00
5.00
oc Limits
76 114
88 110
86 115
8240
08/09/94 LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Filtrate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene 0.005
Trichloroethene ND
Vinyl Chloride ND
Surrogate standard % Recovery
Sl -1,2-Dichloroethane-d4 109
S2 -Toluene-dB 88
S3 -4-Bromofluorobenzene 94
DL
0.005
0.005
0.005
0.050
0.005
0.005
0.005
0.050
0.005
0.005
0.005
ND -Not De~ted DL -Detection Limit
.YAIPt {h
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.50
0.50
100
6.00
7.50
0.50
0.70
200
0.70
0.50
0.20
QC Limits
76 114
88 110
86 115
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENT AL TESTING & CONSULTING INC.
2924 Walnut Grove Road-Memphis, TN 38111-(901)327~1750
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
Endrin ND
lethoxychlor ND
Ioxaphene ND
surrogate standard % Recovery
Sl -Dibutyl Chlorendate 104
S2 -Tetrachloro-m-xylene 96
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0
0.50
QC Limits
25 125
25 125
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
,emeton-0
,emeton-s
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Herphos
Hevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion{Protothiofos)
Trichloronate
ND -Not Detj6Jed
».M)f-1-~
8141
08/04/94 08/26/94 DC
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ND ug/L 1.00
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-0
Silvex
P•,rrogate standard
-2,4,5-T
RESULT
UNITS: (mg/L)
Filtrate
ND
ND
% Recovery
44
Project#
FID #
Matrix :AQUEOUS
Sample Date :07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND;;~D?tt DL -Detection Limit
LABORATORY MANAGER
BY METHOD
TL 1311
6640-B cc cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Filtrate
TCLP semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
~exachloroethane ND
-Methyl phenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
surrogate standard ~ Recovery
S1 -Nitrobenzene-d5 65
S2 -2-Fluorobiphenyl 73
S3 -4-Terphenyl-d14 79
S4 -Phenol-d6 29
S5 -2,4,6-Tribromophenol 62
S6 -2-Fluorophenol 36
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
DL -Detection Limit
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13
0.50
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:AQUEOUS
Date :07/28/94
DATE
ANALYZED
08/04/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3"-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Project#
FID #
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/20/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-06
Sample ID: IC-001-LCH
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate standard
S1 -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-dl4
S4 -Phenol-d6
:5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
ND -Not De'fl'ted
.~MXf,:f_~_
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
% Recovery
59
59
37
29
52
42
Project#
FID #
Matrix
Sample
:AQUEOUS
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/04/94 08/20/94
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
QC Limits
35 114
43 116
33 141
10 94
10 123
21 100
BY METHOD
8270
DC
. ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
bate Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
Project#
Matrix
Sample
DETECTION TIME
:SOIL
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 83.6 \ 0 1030 07/31/94 PM
Silver <1.75 mg/Kg 1.75 0935 08/17/94 AB
Arsenic <12.5 mg/Kg 12.S 0935 08/17/94 AB
Barium 26.7 mg/Kg 0.200 0935 08/17/94 AB
Cadmium <1.00 mg/Kg 1.00 0935 08/17/94 AB
-comium 17.0 mg/Kg 3.50 0935 08/17/94 AB
rcury 0.025 mg/Kg 0.020 1540 08/08/94 JF
Lead 46.9 mg/Kg 11.3 0935 08/17/94 AB
Selenium <18.8 mg/Kg 18.8 0935 08/17/94 AB
Metal results are dry weight mg/Kg.
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
60i0A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
"'C!lenium -TCLP
lver -TCLP
~.;LP Extraction
Limit
RESULT
UNITS: (mg/L)
<0.050
0.335
<0.004
0.167
0.167
<0.001
<0.075
<0.007
Leachate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:SOIL
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren county,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not o7t~cted
.A·'»Wd~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
132 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
12.3 ug/Kg
211 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/08/94
100
50.0
50.0
5.00
5 .00
5.00
5.00
50.0
5.00
5.00
5.00
5 .00
50.0
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Tinyl Chloride
Xylenes
surrogate standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND ~ Not oer,cted
A44~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
108
99
89
8240
08/08/94 08/08/94 LS
5.00
5.00
5.00
5.00
50.0
5.00
5.00
QC Limits
70 121
81 117
74 121
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
.,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate standard ~ Recovery:
S1 -1,2-Dichloroethane-d4 108
S2 -Toluene-dB 90
S3 -4-Bromofluorobenzene 96
DL
0.050
0.050
0.050
0 .500
0.050
0.050
0.050
0.500
0.050
0.050
0.050
DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.50 a.so
100
6.00
7.50
0.50
0.70
200
0 .70 a.so
0.20
QC Limits
76 114
88 110
86 115
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING INC.
2924 Walnut Grove Road-Memphis, TN 38111-(901)327~11s0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren county,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST
TCLP Extraction Organics
TCLP Pesticides
Chlordane
Heptachlor
Lindane
Endrin
lethoxychlor
Toxaphene
surrogate standard
S1 -Dibutyl Chlorendate
S2 -Tetrachloro-m-xylene
RESULT
UNITS: (mg/L)
Leachate
ND
ND
ND
ND
ND
ND
% Recovery
100
96
DL
0.010
0.001
0.001
0.001
0.040
0.100
")/;/ J~Yled DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0
0.50
oc Limits
25 125
25 125
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST RESULT UNITS
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-0
Demeton-S
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND -Not Detefld
dA>t1~11 _, __ -----------·---·--
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/10/94 08/26/94
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
BY METHOD
8141
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
... ••rrogate standard
L -2,4,5-T
RESULT
UNITS: (mg/L)
Leachate
ND
ND
% Recovery
57
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND -Not Det!Jted DL -Detection Limit
.dM>tf~ LABORATORY MANAGER
BY METHOD
TL 1311
6640-B cc cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST
TCLP Extraction Organics
TCLP Semivolatiles
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
~-Methylphenol
J&4-Methylphenol
Nitrobenzene
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Pyridine
surrogate standard
S1 -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
S4 -Phenol-d6
S5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
RESULT
UNITS: (mg/L)
Leachate
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
% Recovery
76
69
51
31
55
41
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
DL -Detection Limit
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
REGULATORY
LEVEL: (mg/L)
0.13
0.13
0.50
3.00
200
200
2.00
100
400
2.00
5.00
oc Limits
34 114
43 116
33 141
10 94
10 123
21 100
DATE
ANALYZED
08/04/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9 4 o 7 718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND -Not Det~ed
,dl.A/tsd 4: ~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
388 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-07
Sample ID: IC-003-LC
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylarnine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate standard
S1 -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
S4 -Phenol-d6
:5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
%
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
NO ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Recovery
7 Q
10 Q
11 Q
5 Q
9 Q
6 Q
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
QC Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
Project I
Matrix
Sample
DETECTION TIME
:SOIL
Date :07/28/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 79.8 \ 0 1030 07/31/94 PM
Silver <1.75 mg/Kg 1. 75 0935 08/17/94 AB
Arsenic <12. 5 mg/Kg 12.5 0935 08/17/94 AB
Barium 28.8 mg/Kg 0.200 0935 08/17/94 AB
Cadmium <1.00 mg/Kg 1.00 0935 08/17/94 AB
r1-tromium 15.6 mg/Kg 3.50 0935 08/17/94 AB
rcury 0.026 mg/Kg 0.020 1540 08/08/94 JF
Lead 61.8 mg/Kg 11.3 0935 08/17/94 AB
Selenium <18.8 mg/Kg 18.8 0935 08/17/94 AB
Metal results are dry weight mg/Kg.
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9 4 o 7 718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
,_elenium -TCLP
ilver -TCLP
.i'CLP Extraction
. ,.,.
DL -Detection Limit
µ/uli,tc
Ll\.BORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.385
<0.004
0.170
0.170
<0.001
<0.075
<0.007
Leachate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:SOIL
Date :07/28/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
,Bromodichloromethane
Jromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1 ,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not Detnted
-)}#/ ✓-lb --
82.7j ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
252 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
23.9 ug/Kg
420 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/08/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5 .00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0 so.a
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET ·
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
Project#
FID #
Matrix :SOIL
Sample Date :07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
111
95
85
8240
08/08/94 08/08/94 LS
5.00
5.00
5.00
5.00
50.0
5.00
5.00
QC Limits
70 121
81 117
74 121
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate standard :Ii Recovery:
Sl -l,2-Dichloroethane-d4 108
S2 -Toluene-dB 91
SJ -4-Bromofluorobenzene 94
DL
0.050
0.050
0.050
0.500
0.050
0.050
0.050
0.500
0.050
0.050
0.050
DL -Detection Limit
BORAORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.50
0.50
100
6.00
7.50
0.50
0.70
200
0.70
0.50
0.20
QC Limits
76 114
88 110
86 115
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENf AL TESTING & CONSULTING INC.
2924 Walnut Grove Road -Memphis, TN 38111-(901)327~17S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
Endrin ND
Methoxychlor ND
roxaphene ND
surrogate standard % Recovery:
S1 -Dibutyl Chlorendate 88
S2 -Tetrachloro-m-xylene 92
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL:(mg/L)
0.03
0.008
0.40
0.02
10.0 a.so
QC Limits
25 125
25 125
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Organphosphor Pesticide
Azinphos .Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-0
Demeton-s
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8141
08/10/94 08/26/94 DC
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35 .0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35 .0
ug/Kg 35 .0
ug/Kg 35 .0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ug/Kg 35.0
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
surrogate standard
\ -2,4,5-T
RESULT
UNITS: (mg/L)
Leachate
ND
ND
% Recovery
53
Project#
FID #
Matrix :SOIL
Sample Date : 07/28/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
DL -Detection Limit
BY METHOD
TL 1311
6640-B
cc
cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Methylphenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,S-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
surrogate standard ~ Recovery
S1 -Nitrobenzene-dS 74
S2 -2-Fluorobiphenyl 71
S3 -4-Terphenyl-d14 102
S4 -Phenol-d6 24 ss -2,4,6-Tribromophenol 59
S6 -2-Fluorophenol 29
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
ND -Not Det,,ted DL -Detection Limit
~{~ EABORATRY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13 a.so
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:SOIL
Date :07/28/94
DATE
ANALYZED
08/04/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
08/19/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren county,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
NO -Not Oetned A~1✓~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
474 ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-08
Sample ID: IC-002-LC
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadlene
Indeno{l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroanlllne
3-Nltroanlllne
4-Nltroanlllne
2-Nitrophenol
4-Nitrophenol
N-Nitrosodlmethylamine
N-Nitrosodiphenylamine
N-Nitrosodlpropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trlchlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazlne
Surrogate Standard
S1 -Nitrobenzene-dS
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d14
4 -Phenol-d6
JS -2,4,6-Tribromophenol
S6 -2-Fluorophenol
%
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Recovery
8 Q
113
134
8 Q
116
7 Q
Project#
FID #
Matrix
Sample
:SOIL
Date :07/28/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
oc Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
Project#
Matrix
Sample
DETECTION TIME
:SOIL
Date :07/27/94
DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 88.5 % 0 1030 07/31/94 PM
Silver <1.75 mg/Kg 1.75 0935 08/17/94 AB
Arsenic <12.5 mg/Kg 12.5 0935 08/17/94 AB
Barium 81.4 mg/Kg 0.200 0935 08/17/94 AB
Cadmium <1.00 mg/Kg 1.00 0935 08/17/94 AB
~hromium 26.7 mg/Kg 3.50 0935 08/17/94 AB
Mercury 0 .040 mg/Kg 0.020 1540 08/08/94 JF
Lead 26.4 mg/Kg 11.3 0935 08/17/94 AB
Selenium <18.8 mg/Kg 18.8 0935 08/17/94 AB
Metal results are dry weight mg/Kg.
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environ.mental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
Selenium -TCLP
Silver -TCLP
TCLP Extraction
DL -Detection Limit
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.768
<0.004
<0.007
<0.045
<0.001
<0.075
<0.007
Leachate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:SOIL
Date :07/27/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not De~ected
)!~{/ ~J
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
l.89j ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/09/94 08/09/94
100 so.a
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00 so.a
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00 so.a so.a
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
Project#
FID #
Matrix :SOIL
Sample Date :07/27/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate standard
Sl -l,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND -Not Detrted
Al -~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
112
81
78
08/09/94
5.00
5.00
5.00
5.00 so.a
5.00
5.00
QC Limits
70 121
81 117
74 121
8240
08/09/94 LS
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road-Memphis, TN 38111-(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate standard % Recovery
Sl -l,2-Dichloroethane-d4 104
S2 -Toluene-dB 93
S3 -4-Bromofluorobenzene 93
DL
0.050
0.050
0.050
0.500
0.050
0.050
0.050
0.500
0.050
0.050
0.050
ND -Not De~r,-ed DL -Detection Limit
j)Alfi/{M
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.50 a.so
100
6.00
7.50 a.so
0.70
200
0.70 a.so
0.20
QC Limits
76 114
88 110
86 115
:SOIL
Date : 07/27/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
Endrin ND
Methoxychlor ND
Toxaphene ND
surrogate standard i Recovery
S1 -Dibutyl Chlorendate 104
S2 -Tetrachloro-m-xylene 96
DL
0.010
0.001
0.001
0.001
0.040
0.100
DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.03
0.008
0.40
0.02
10.0
0.50
QC Limits
25 125
25 125
:SOIL
Date :07/27/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST RESULT UNITS
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-0
Demeton-s
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/10/94 08/26/94
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
BY METHOD
8141
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
Organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST
TCLP Extraction Organics
TCLP Herbicides
2,4-D
Silvex
~urrogate standard
S1 -2,4,5-T
RESULT
UNITS: (mg/L)
Leachate
ND
ND
% Recovery
47
Project#
FID #
Matrix :SOIL
Sample Date : 07/27/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
oc Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND -Not Dete~d DL -Detection Limit
J/.MX/1~
LABORATORY MANAGER
BY METHOD
TL 1311
6640-B
cc
cc
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
Organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Semivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Methylphenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,S-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
surrogate Standard \ Recovery:
Sl -Nitrobenzene-dS 70
S2 -2-Fluorobiphenyl 77
S3 -4-Terphenyl-dl4 75
S4 -Phenol-d6 31
S5 -2,4,6-Tribromophenol 68
S6 -2-Fluorophenol 43
DL
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
ND -Not De~.tted DL -Detection Limit
)!0&/1✓~
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13 a.so
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:SOIL
Date :07/27/94
DATE
ANALYZED
08/04/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environ.mental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren county,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road-Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-10
Sample ID: IC-001-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (rn&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodirnethylamine
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
Surrogate Standard
Sl -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-dl4
S4 -Phenol-d6
S5 -2,4,6-Tribrornophenol
S6 -2-Fluorophenol
ND -Not Dett9ted
~NOl.f ~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
43
52
72
48
63
37
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
QC Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
INORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
Project#
Matrix :SOIL
Sample Date :07/27/94
DETECTION TIME DATE
TEST RESULT UNITS LIMIT ANALYZED ANALYZED BY
Percent Solids 47.8 % 0 1030 07/31/94 PM
Silver <1. 75 mg/Kg 1.75 0935 08/17/94 AB
Arsenic <12. 5 mg/Kg 12.5 0935 08/17/94 AB
Barium 136 mg/Kg 0.200 0935 08/17/94 AB
Cadmium <1.00 mg/Kg 1.00 0935 08/17/94 AB
~hromium 24.4 mg/Kg 3.50 0935 08/17/94 AB
Mercury 0.018 mg/Kg 0.020 1540 08/08/94 JF
Lead <11.3 mg/Kg 11.3 0935 08/17/94 AB
Selenium <18.8 mg/Kg 18.8 0935 08/17/94 AB
Metal results are dry weight mg/Kg.
METHOD
160.3
6010A
6010A
6010A
6010A
6010A
7471
6010A
6010A
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -(901)327-27S0
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST
Arsenic -TCLP
Barium -TCLP
Cadmium -TCLP
Chromium -TCLP
Lead -TCLP
Mercury -TCLP
Selenium -TCLP
Silver -TCLP
TCLP Extraction
DL -Detection Limit
LABORATORY MANAGER
RESULT
UNITS: (mg/L)
<0.050
0.519
<0.004
<0.007
<0.045
<0.001
<0.075
<0.007
Leachate
DL
0.050
0.002
0.004
0.007
0.045
0.001
0.075
0.007
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
5.0
100
1.0
5.0
5.0
0.2
1.0
5.0
:SOIL
Date :07/27/94
DATE
ANALYZED
08/08/94
08/08/94
08/08/94
08/08/94
08/08/94
08/09/94
08/11/94
08/08/94
08/04/94
BY METHOD
AB 6010A
AB 6010A
AB 6010A
AB 6010A
AB 6010A
JF 7470
AB 6010A
AB 6010A
TL 1311
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST RESULT UNITS
Volatile Organics
Acetone
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
Dibromomethane
1,4-Dichloro-2-butene
Dichlorofluoromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl Methacrylate
2-Hexanone (MBK)
Iodomethane
4-Methyl-2-pentanone (MIBK)
Methyl Ethyl Ketone (MEK)
Methylene Chloride
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
ND -Not Det~ted ,;lviY 1 ~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
4.08j ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/09/94 08/09/94
100
50.0
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
5.00
50.0
5.00
5.00
5.00
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
50.0
50.0
5.00
50.0
50.0
20.0
5.00
5.00
5.00
5.00
5.00
BY METHOD
8240
LS
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
Project#
FID #
Matrix :SOIL
Sample Date :07/27/94
DETECTION DATE DATE
TEST RESULT UNITS LIMIT EXTRACTED ANALYZED BY METHOD
Volatile Organics
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl Acetate
Vinyl Chloride
Xylenes
surrogate standard
S1 -1,2-Dichloroethane-d4
S2 -Toluene-dB
S3 -4-Bromofluorobenzene
ND ~. Not Derted
A/\AY{ <I ~fj
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
108
87
87
8240
08/09/94 08/09/94 LS
5.00
5.00
5.00
5.00 so.a
5.00
5.00
QC Limits
70 121
81 117
74 121
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
RESULT
TEST UNITS: (mg/L)
TCLP Zero Headspace Leachate
TCLP Volatile Organics
Benzene ND
Carbon Tetrachloride ND
Chlorobenzene ND
Chloroform ND
1,4-Dichlorobenzene ND
1,2-Dichloroethane ND
1,1-Dichloroethene ND
Methyl Ethyl Ketone ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl Chloride ND
surrogate standard ~ Recovery
S1 -1,2-Dichloroethane-d4 108
S2 -Toluene-dB 93
S3 -4-Bromofluorobenzene 97
DL
0.050
0.050
0.050
0.500
0.050
0.050
0.050
0.500
0 .050
0.050
0.050
N:v;;; ✓Y!ted DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
a.so a.so
100
6.00
7.50 a.so
0.70
200
0.70 a.so
0 .20
QC Limits
76 114
88 110
86 115
:SOIL
Date :07/27/94
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
08/12/94
BY METHOD
TL 1311
8240
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
DG
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road-Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Pesticides
Chlordane ND
Heptachlor ND
Lindane ND
Endrin ND
Methoxychlor ND
Toxaphene ND
surrogate standard % Recovery:
Sl -Dibutyl Chlorendate 100
S2 -Tetrachloro-m-xylene 100
DL
0.010
0.001
0.001
0.001
0.040
0.100
ND -Not Dented DL -Detection Limit
~AMf~
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL:(mg/L)
0.03
0.008
0.40
0.02
10.0 a.so
QC Limits
25 125
25 125
:SOIL
Date : 07/27/94
DATE
ANALYZED
08/04/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
08/16/94
BY METHOD
TL 1311
8080
DC
DC
DC
DC
DC
DC
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson Street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST RESULT UNITS
Organphosphor Pesticide
Azinphos Methyl
Bolstar
Chlorpyrifos
Coumaphos
Demeton-o
Demeton-s
Diazinon
Dichlorvos
Dimethoate
Disulfoton
EPN
Ethoprop
Fensulfothian
Fenthion
Malathion
Merphos
Mevinphos
Naled
Parathion ethyl
Parathion methyl
Phorate
Ronnel
Sulfotep
TEPP
Stirophos(Tetrachlorovinphos)
Tokuthion(Protothiofos)
Trichloronate
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date : 07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/10/94 08/26/94
35.0
35.0
35.0
35.0
35.0
35.0
35 .0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35.0
35 .0
35.0
35.0
35.0
35.0
35.0
35.0
BY METHOD
8141
DC
ENVIRONMENf AL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental compliance
organization
106 Robinson street
Ashton, VA 23005
Site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST
TCLP Extraction organics
TCLP Herbicides
2,4-0
Silvex
,urrogate Standard
Sl -2,4,5-T
RESULT
UNITS: (mg /L)
Leachate
ND
ND
% Recovery
54
Project#
FID #
Matrix :SOIL
Sample Date : 07/27/94
REGULATORY
DL LEVEL: (mg/L)
0.080 10.0
0.008 5.00
QC Limits
25 125
DATE
ANALYZED
08/04/94
08/12/94
08/12/94
ND/4ot Dete#d DL -Detection Limit
~f~
LABORATORY MANAGER
BY METHOD
TL 13 11
6640-B
cc
cc
ENVIRONl\1ENfAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road-Memphis, TN 38111-[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
106 Robinson Street
Ashton, VA 23005
site ID Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
RESULT
TEST UNITS: (mg/L)
TCLP Extraction Organics Leachate
TCLP Sernivolatiles
2,4-Dinitrotoluene ND
Hexachlorobenzene ND
Hexachlorobutadiene ND
Hexachloroethane ND
2-Methylphenol ND
3&4-Methylphenol ND
Nitrobenzene ND
Pentachlorophenol ND
2,4,5-Trichlorophenol ND
2,4,6-Trichlorophenol ND
Pyridine ND
surrogate standard ~ Recovery
S1 -Nitrobenzene-d5 66
S2 -2-Fluorobiphenyl 64
S3 -4-Terphenyl-dl4 35
S4 -Phenol-d6 20
S5 -2,4,6-Tribrornophenol 42
S6 -2-Fluorophenol 27
DL
0.050
0.050
0.050
0.050
0.050
0.050
0 .050
0.050
0.050
0.050
0.050
DL -Detection Limit
LABORATORY MANAGER
Project#
FID #
Matrix
Sample
REGULATORY
LEVEL: (mg/L)
0.13
0.13
0.50
3.00
200
200
2.00
100
400
2.00
5.00
QC Limits
34 114
43 116
33 141
10 94
10 123
21 100
:SOIL
Date :07/27/94
DATE
ANALYZED
08/04/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
08/21/94
BY METHOD
TL 1311
8270
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Benzoic Acid
Benzidine
Benzyl Alcohol
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
4-Chloroaniline
2-Chloronaphthalene
4-Chloro-3-methylphenol
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
ND -Not De~d
))MY/1~
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
BY METHOD
8270
DC
ENVIRONMENTAL TESTING & CONSULTING, INC.
2924 Walnut Grove Road -Memphis, TN 38111 -[phone]
ORGANIC ANALYSIS DATA SHEET
Client Name Environmental Compliance
organization
Site ID
106 Robinson street
Ashton, VA 23005
Warren County,NC
PCB Landfill
Date Arrived 07/30/94
ETC Order Number 9407718
ETC Lab ID 9407718-11
Sample ID: IC-002-SS
TEST RESULT UNITS
Base/Neutral & Acid Ext
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Indeno(l,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol (o-cresol)
3&4-Methylphenol (m&p-cresol)
Naphthalene
Nitrobenzene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylami ne
N-Nitrosodiphenylami ne
N-Nitrosodipropylami ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorphenol
2,4,6-Trichlorophenol
Hexachloroethane
Hexachlorocyclopentadiene
1,2-Diphenylhydrazine
surrogate standard
S1 -Nitrobenzene-d5
S2 -2-Fluorobiphenyl
S3 -4-Terphenyl-d 14
S4 -Phenol-d6
S5 -2,4,6-Tribromophenol
S6 -2-Fluorophenol
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
ND ug/Kg
% Recovery
55
66
78
65
68
54
Project#
FID #
Matrix
Sample
:SOIL
Date :07/27/94
DETECTION DATE DATE
LIMIT EXTRACTED ANALYZED
08/08/94 08/18/94
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
330
QC Limits
23 120
30 115
18 137
24 113
19 122
25 121
BY METHOD
8270
DC
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOUS Contract:
Lab Code: Case No.: IK0899
Matrix:
IN049
SOIL (SoiVWater/Waste/Ash)
Sample wt/vol: 10.04 (g/mL) g
Water Sample Prep: (Sepf/Cont)
Concentrated Extract Volume: 50 (uL)
Injection Volume: 2 (uL) % Solids:
GC Column: DB-5 ID: 0.25 (mm)
SDG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
940TT18-01E I
IK0899-1
0501006.D
08/02/94
08/06/94
08/24/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306
12378-PeCDF 340/342
12378-PeCDD 356/358
23478-PeCDF 340/342
123478-HxCDF 374/376
123678-HxCDF 374/376
123478-HxCDD 390/392
123678-HxCDD 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376
123789-HxCDF 374/376
1234678-HpCDF 408/410
1234678-HpCDD 424/426
1234789-HoCDF 408/410
ocoo 458/460 40.35 0.92 1.1889
OCDF 442/444
NOTE: Concentrations,· EMPC's, and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCDD
13C-123678-HxCDD
13C-1234678-HpCOF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.80
332/334 19.01 0.80
402/404 28.33 1.25
420/422 32.51 1.08
470/472 40.35 0.92
328/NA 19.01 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
u 0.0145
u 0.0069
u 0.0062
u 0.0110
u 0.0059
u 0.0086
u 0.0071
u 0.0089
u 0.0079
u 0.0076
u 0.0083
u 0.0090
u 0.0083
u 0.0131
u 0.0100
J
u 0.0212
% RECOVERY
REC # LIMITS
76.0 25-150
74.0 25-150
74.0 25-150
64.9 25-150
49.6 25-150
70.2 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code:
Matrix:
IN049
SOIL
Sample wt/vol: 10.02
Case No.: IK0899
(Soil/Water/Waste/Ash)
(g/mL) g
Water Sample Prep: (Sepf/Cont)
Concentrated Extract Volume: 50 (uL)
Injection Volume: 2 (uL) % Solids:
GC Column: DB-5 ID: 0.25 (mm)
SDG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
940n1a-02e I
1 c -o o \ -s E-n __,
IK0899-2
0601007.0
08/02/94
08/06/94
08/24/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306
12378-PeCDF 340/342
12378-PeCDD 356/358
23478-PeCDF 340/342
123478-HxCOF 374/376
123678-HxCOF 374/376
123478-HxCDD 390/392
123678-HxCOO 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376
123789-HxCOF 374/376
1234678-HpCDF 408/410
1234678-HcCDD 424/426
1234789-HpCDF 408/410
OCDD 458/460 40.35 0.90 0.2774
OCDF 442/444
NOTE: Concentrations, EMPC's, and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCDD
13C-123678-HxCDD
13C-1234678-HpCDF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.81
332/334 19.01 0.86
402/404 28.33 1.25
420/422 32.53 1.08
470/472 40.33 0.93
328/NA 19.03 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1 .01
NA
u 0.0151
u 0.0070
u 0.0061
u 0.0122
u 0.0058
u 0.0085
u 0.0070
u 0.0081
u 0.0072
u 0.0070
u 0.0082
u 0.0089
u 0.0074
u 0.0118
u 0.0089
J
u 0.0148
% RECOVERY
REC # LIMITS
76.6 25-150
76.9 25-150
81.1 25-150
75.5 25-150
60.0 25-150
70.7 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code: IN049 Case No.: IK0899
Matrix: WATER {SoiVWater/Waste/Ash)
Sample wt/vol: 1050 {g/ml) ml
Water Sample Prep: SEPF {Sepf/Cont)
Concentrated Extract Volume:
Injection Volume: 2
GC Column: DB-5
50 {ul)
{ul) % Solids:
ID: 0.25 {mm)
SDG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
9407718-04E I
IK0899-3
0501006.D
08/02/94
-ae~-i~
08/23/94
1
Concentration Units: (ng/L or ug/Kg) ng/L
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306
12378-PeCDF 340/342
12378-PeCDD 356/358
23478-PeCDF 340/342 ..
123478-HxCDF 374/376
123678-HxCDF 374/376
123478-HxCDD 390/392
123678-HxCDD 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376
123789-HxCDF 374/376
1234678-HpCDF 408/410
1234678-HpCDD 424/426
1234789-HpCDF 408/410
OCDD 458/460
OCDF 442/444
NOTE: Concentrations, EMPC's, 'and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
1 SC.2378-TCDF
130.2378-TCDD
1 SC.123678-HxCDD
13C-1234678-HoCDF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.41 0.80
332/334 19.01 0.80
402/404 28.33 1.24
420/422 32.53 0.98
470/472 40.35 0.91
328/NA 19.01 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
u 0.1447
u 0.1054
u 0.1089
u 0.2011
u 0.1047
u 0.1455
·u 0.1198
u 0.1833
u 0.1TT6
u 0.1640
u 0.1415
u 0.1505
u 0.1626
u 0.1326
u 0.1912
u 0.2858
u 0.2936
% RECOVERY
REC # LIMITS
66.7 · 25-150
62.7 25-150
61.9 25-150
53.1 25-150
40.9 25-150
73.1 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name:
lab Code:
PACE-INDIANAPOUS Contract:
IN049 Case No.: IK0899
Matrix: WATER (SoiVWater/Waste/Ash)
Sample wt/vol: 1070
Water Sample Prep: SEPF
Concentrated Extract Volume:
(g/mL) ml
(Sept/Cont)
SDG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Data Received:
EPA SAMPLE NO.
940TT18-05E I
IK0899-4
0601007.D
08/02/94
Injection Volume: 2
50 (ul)
(ul) % Solids: 0.0 Date Extracted: ~~ 't·<11-<li4
GC Column: 08-5 ID: 0.25 (mm) Date Analyzed: 08/23/94
Dilution Factor: 1
Concentration Units: (ng/L or ug/Kg) ng/L
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322 u 0.1554
2378-TCDF 304/306 u 0.1092
12378-PaCDF 340/342 u 0.1183
12378-PaCDD 356/358 u 0.1912
23478-PaCDF 340/342 u 0.1137
123478-HxCDF 374/376 u 0.1448
123678-HxCDF 374/376 u 0.1191
123478-HxCDD 390/392 u 0.1580
123678-HxCDD 390/392 u 0.1530
123789-HxCDD 390/392 u 0.1413
234678-HxCDF 374/376 u 0.1408
123789-HxCDF 374/376 u 0.1497
1234678-HDCDF 408/410 u 0.1466
1234678-HpCDD 424/426 u 0.1366
1234789-HpCDF 408/410 u 0.1724
OCDD 458/460 u 0.2892
OCDF 442/444 u 0.2980
NOTE: Concentrations, EMPC's, and EDL's are caJculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCDD
130-123678-HxCDD
130-1234678-HoCDF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.80
332/334 19.01 0.83
402/404 28.34 1.26
420/422 32.51 0.98
_470/472 40.34 0.91
328/NA 19.03 NA
# Column to be used to flag vaJues outside QC fimits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
% RECOVERY
REC # LIMITS
75.9 25-150
73.2 25-150
73.0 25-150
65.3 25-150
54.3 25-150
79.9 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code: IN049 Case No.: IK0899 SDG No.:
Matrix: WATER (Soil/Water/Waste/Ash) SAS No:
Sample wt/vol: 1070 (g/ml) ml Lab Sample ID:
Water Sample Prep: SEPF (Sepf/Cont) Lab File ID:
Concentrated Extract Volume: 50 (ul) Date Received:
Injection Volume: 2 (ul) % Solids: 0.0 Date Extracted:
GC Column: DB-5 ID: 0.25 (min) Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
940n1B-06E I
IK0899-5
0701008.D
08/02/94
g:t:,!?J u~
08/23/94
1
Concentration Units: (ng/L or ug/Kg) ng/L
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306
12378-PeCDF 340/342
12378-PeCDD 356/358
23478-PeCDF 340/342
123478-HxCDF 374/376
123678-HxCDF 374/376
123478-HxCDD 390/392
· 123678-HxCDD 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376
123789-HxCDF 374/376
1234678-HpCDF 408/410
1234678-HoCDD 424/426
1234789-HpCDF 408/410
OCDD 458/460
OCDF 442/444
NOTE: Concentrations, EMPC's, and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCDD
13C-123678-HxCDD
13C-1234678-HpCDF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.80
332/334 19.01 0.79
402/404 28.34 1.24
420/422 32.53 0.99
470/472 40.34 0.93
328/NA 19.03 NA
# Column to be used to flag values outside QC limits.
FORM I PCOD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
u 0.1354
u 0.0960
u 0.1009 u 0.1815
u 0.0970
u 0.1129
u 0.0929
u 0.1416
u 0.1372
u 0.1267
u 0.1098
u 0.1168
u 0.1108
u 0.1223
u 0.1303
u 0.2174
u 0.2248
% RECOVERY
REC # LIMITS
85.4 · 25-150
83.9 25-150
87.7 25-150
82.6 25-150
69.5 25-150
80.1 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code:
Matrix:
IN049
SOIL
Sample wt/vol: 10.05
Case No.: IK0899
(Soil/Water/Waste/Ash)
(g/ml) g
Water Sample Prep: {Sepf/Cont)
Concentrated Extract Volume: 50 {uL)
Injection Volume: 2 (uL) % Solids:
GC Column: DB-5 ID: 0.25 (mm)
SDG No.:
SAS No:
Lab Sample ID:
Lab F"ile ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
OUution Factor:
EPA SAMPLE NO.
940n18-07E
7 C. -oo]-LC .,:.-
IK0899-6
0701008.0
08/02/94
08/06/94
08/24/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306 18.49 0.75 0.1133
12378-PeCDF 340/342 22.49 1.47 0.0329
12378-PeCDD 356/358 23.81 0.17 *
23478-PeCDF 340/342 23.22 1.75 0.1188
123478-HxCDF 374/376 27.09 1.24 1.1452
123678-HxCDF 374/376 27.27 1.17 0.1712
123478-HxCDO 390/392
123678-HxCDO 390/392
123789-HxCDD 390/392
234678-HxCOF 374/376 28.03 1.24 0.1010
123789-HxCDF 374/376 29.59 1.90 *
1234678-HpCOF 408/410 32.55 1.07 0.8958
1234678-HpCDO 424/426
1234789-HpCOF 408/410 35.07 1.03 0.5491 ocoo 458/460 40.37 0.93 0.3237
OCDF 442/444 40.64 0.82 4.2072
NOTE: Concentrations, EMPC'a, and EDL'a are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
130-2378-TCDD
13C-123678-HxCDD
13C-1234678-HoCDF
13C-OCDD
3701-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.47 0.80
332/334 19.09 0.68
402/404 28.35 1.25
420/422 32.53 1.07
470/472 40.35 0.92
328/NA 19.09 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1:0S-1.43
0.88-1.20
0.76-1.01
NA
H 0.0164
J
J
H 3.6552
J
J
J
u 0.0214 ..
u 0.0191
u 0.0184
J
0.2926
J
u 0.0113
J
J
J
% RECOVERY
REC # LIMITS
60.7 25-150
72.8 H 25-150
84.3 25-150
74.9 25-150
51.9 25-150
57.1 H 25-150
10/90
1DFA
PCDD/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code:
Matrix:
IN049
SOIL
Sample wt/vol: 10.01
Case No.: IK0899
(Soil/Water/Waste/ Ash)
(g/mL} g
Water Sample Prep: (Sepf/Cont}
Concentrated Extract Volume: 50 (uL)
Injection Volume: 2 (uL) % Solids:
GC Column: DB-5 ID: 0.25 (mm)
SDG No.:
SAS No:
Lab Sample ID:
Lab File 10:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
940TT18-0SE I
IK0899-7
0801009.0
08/02/94
08/06/94
08/24/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDD 320/322
2378-TCDF 304/306 18.49 0.74 0.5214
12378-PeCDF 340/342 22.44 1.48 0.1171
12378-PeCDD 356/358 23.81 0.18 •
23478-PeCDF 340/342 23.22 1.49 0.4418
123478-HxCDF 374/376 27.09 1.24 4.7069
123678-HxCDF 374/376 27.27 1.25 0.5958
123478-HxCDO 390/392
123678-HxCDD 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376 28.05 1.16 0.3657
123789-HxCDF 374/376 29.59 1.91 •
1234678-HpCDF 408/410 32.55 1.07 3.0825
1234678-HpCDO 424/426
1234789-HoCDF 408/410 35.09 1.07 1.7253
OCDO 458/460
OCDF 442/444 40.64 0.83 14.4435
NOTE: Concentrations, EMPC's, and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCDO
13C-123678-HxCDO
13C-1234678-HpCDF
13C-OCOO
37Cl-2378-TCDO
SELECTED PEAK ION
IONS: RT RATIO #
316/318 18.49 0.82
332/334 19.11 0.66
402/404 28.37 1.26
420/422 32.55 1.07
470/472 . 40.37 0.90
328/NA 19.11 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
H 0.0111
J
J
H 5.5604
J
J
u 0.0405
u 0.0362
u 0.0349
J
0.8831
u 0.0231
J
u 0.0975
% RECOVERY
REC # LIMITS
60.0 25-150
72.2 H 25-150
84.9 25-150
65.8 25-150
32.6 25-150
61.2 H 25-150
10/90
1DFA
PCOO/PCDF SAMPLE DATA SUMMARY
Lab Name: PACE-INDIANAPOLIS Contract:
Lab Code:
Matrix:
IN049
SOIL
Sample wt/vol: 10.08
Case No.: IK0899
(Soil/Water/Waste/ Ash)
(g/mL) g
Water Sample Prep: (Sepf/Cont)
Concentrated Extract Volume: 50 (uL)
Injection Volume: 2 (uL) % Solids:
GC Column: DB-5 ID: 0.25 (mm)
SOG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
EPA SAMPLE NO.
940ma.,oe I
IK0899-8
0901010.0
08/02/94
08/06/94
08/25/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/EDL
2378-TCDO 320/322
2378-TCDF 304/306
12378-PeCDF 340/342
12378-PeCOO 356/358
23478-PeCOF 340/342
123478-HxCOF 374/376
123678-HxCOF 374/376
123478-HxCDO 390/392
123678-HxCOO 390/392
123789-HxCDO 390/392
234678-HxCDF 374/376
123789-HxCOF 374/376
1234678-HpCOF 408/410
1234678-HpCOO 424/426
1234789-HpCOF 408/410 ocoo 458/460 40.37 0.95 2.9478
OCDF 442/444
NOTE: Concentrations, EMPC's, and EOL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
13C-2378-TCDF
13C-2378-TCOO
13C-123678-HxCDD
13C-1234678-HpCOF
13C-OCOO
37Cl-2378-TCDO
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.81
332/334 19.01 0.79
402/404 28.33 1.24
420/422 32.53 1.09
470/472 40.35 0.93
328/NA 19.01 NA
# Column to be used to flag values outside QC limits.
FORM I PCD0-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
u 0.0242
u 0.0252
u 0.0214
u 0.0313
u 0.0204
u 0.0309
u 0.0257
u 0.0413
u 0.0369
u 0.0356
u 0.0301
u 0.0324
u 0.0235
u 0.0181
u 0.0283
J
u 0.0807
% RECOVERY
REC # LIMITS
51 .9 25-150
50.5 25-150
73.9 25-150
61.1 25-150
32.4 25-150
48.7 25-150
10/90
1DFA
PC00/PCDF SAMPLE DATA SUMMARY
Lab Name:
lab Code:
PACE-INDIANAPOUS Contract:
Matrix:
IN049
SOIL
Sample wt/vol: 10.05
Water Sample Prep:
Case No.: IK0899
{Soil/WaterfNaste/Aah)
(g/mL) g
{Sepf/Cont)
Concentrated Extract Volume: 50 (uL)
Injection Volume: 2 (uL) % Solids:
GC Column: 08-5 ID: 0.25 {mm)
SOG No.:
SAS No:
Lab Sample ID:
Lab File ID:
Date Received:
0.0 Date Extracted:
Date Analyzed:
Dilution Factor:
-----·--·----· --· ---·------
EPA SAMPLE NO.
940TT18-11E I
IK0899-9
1001011.0
08/02/94
08/06/94
08/25/94
1
Concentration Units: (ng/L or ug/Kg) ug/Kg
SELECTED PEAK ION
ANALYTE IONS RT RATIO # CONCENTRATION Q EMPC/E0L
2378-TCDD 320/322
2378-TC0F 304/306
12378-PeCDF 340/342
12378-PeCDD 356/358
23478-PeCDF 340/342
123478-HxCDF 374/376
123678-HxCDF 374/376
123478-HxCD0 390/392
123678-HxCDD 390/392
123789-HxCDD 390/392
234678-HxCDF 374/376
123789-HxCDF 374/376
1234678-HpCDF 408/410
1234678-HpCDD 424/426
1234789-HpCDF 408/410
OCDD 458/460 40.39 0.97 0.5782
OCDF 442/444
NOTE: Concentrations, EMPC's, and EDL's are calculated on a wet weight basis.
INTERNAL
STANDARDS
130-2378-TCDF
130-2378-TCDD
130-123678-HxCDD
130-1234678-HoCDF
13C-OCDD
37Cl-2378-TCDD
SELECTED PEAK ION
IONS RT RATIO #
316/318 18.43 0.80
332/334 19.01 0.80
402/404 28.33 1.24
420/422 32.55 1.07
470/472 40.37 0.94
328/NA 19.01 NA
# Column to be used to flag values outside QC limits.
FORM I PCDD-1
ION RATIO
LIMITS
0.65-0.89
0.65-0.89
1.05-1.43
0.88-1.20
0.76-1.01
NA
u 0.0163
u 0.0108
u 0.0097
u 0.0234
u 0.0092
u 0.0192
u 0.0160
u 0.0226
u 0.0202
u 0.0195
u 0.0188
u 0.0202
u 0.0198
u 0.0123
u 0.0239
J
u 0.0495
% RECOVERY
REC # LIMITS
83.8 25-150
80.2 25-150
88.0 25-150
72.5 25-150
39.5 25-150
75.8 25-150
10/90
Site : ECC
Date Sampled : 7 /28/94
Waste Stream Technology Inc
Pesticide & PCB Report
Method 8081
Date Received : 8/2/94 @ 1200
Compound
al ha-BHC
beta-BHC
amma-BHC Lindane
delta-BHC
He tachlor
Aldrin
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4' -DOD
Endrin Aldeh de
Endosulfan Sulfate
4,4' -DDT
Endrin Ketone
Metho chlor
Chlordane
Toxa hene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Detection Limit Multiplier
Lab ID Number
Client ID
Date Extracted
Date Analyzed ·
Detection
Limit
0.003
0.003
0.001
0.002
0.008
0.003
0.022
0.003
0.002
0.009
0.005
0.003
0.004
0.015
0.010
0.004
0.010
0.010
0.040
0.040
0.136
0.130
0.141
0.115
0.038
0.019
0.027
Surrogate Percent Recovery
T etrachloro-m-lene
Decachlorobiphenyl
WS07275 WS07276
01F 02F
8/10/94 8/10/94
8/12/94 8/12/94
Result Result
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u u u
u u
u u
u u
u u
u u
u u
1 1
80 88
92 94
Group Number :9401-172
Report Units : mg/Kg
Matrix: Soil
Analyst's Initials: RJW
WS07277 WS07277
038 038
8/10/94 8/10/94
8/16/94 8/16/94
Result Result
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
u NAF
146 NAF
u NAF
880 E 1000
1000 5000
Diluted Out Diluted Out
Diluted Out Diluted Out
NAF denotes Not Analyzed For. Only "E" flagged values reported in diluted sample.
Site: ECC
Date Sampled : 7 /28/94
Waste Stream Technology Inc
Pesticide & PCB Report
Method 8081 ·
Date Received : 8/2/94@ 1200
Lab ID Number WS07278
Client ID 04F
Date Extracted 8/4/94
Date Analyzed 8/17/94
Detection
Compound Limit Result
alpha-BHC 0.044 u
beta-BHC 0.046 u
gamma-BHC (Lindane) 0.016 u
delta-BHC 0.023 u
Heptachlor 0.12 u
Aldrin 0.048 u
Heptachlor Epoxide 0.32 u
Endosulfan I 0.048 · u
Dieldrin 0.028 u
4,4'-DDE 0.13 u
Endrin 0.080 u
Endosulfan II 0.041 u
4,4' -DOD 0.057 u
Endrin Aldehyde 0.23 u
Endosulfan Sulfate 0.16 u
4,4' -DDT 0.064 u
Endrin Ketone 0.054 u
Methoxychlor 0.14 u
Chlordane 0.60 u
Toxaphene 0.60 u
Aroclor 1016 2.0 u
Aroclor 1221 2.0 u
Aroclor 1232 2.1 u
Aroclor 1242 1.7 u
Aroclor 1248 0.57 u
Aroclor 1254 0.29 u
Aroclor 1260 0.41 u
Detection Limit Multiplier 1
Surrogate % Recovery QC Limits
Tetrachloro-m-xylene 60-150
Decachlorobiphenyl 60 -150 87
Group Number: 9401-172
Report Units : ug/L
Matrix : Aqueous
Analyst's Initials: RJW
WS07279 WS07280
05F 06F
8/4/94 8/4/94
8/17/94 8/17/94
Result Result
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
u u
1 1
83 76
~ite: ECC
Waste Stream Technology Inc
Pesticide & PCB Report
Method 8081
Date Sampled : 7 /28 & 7 /27 /94
Date Received : 8/2/94 @ 1200
Group Number: 9401-172
Report Units : mg/Kg
Matrix : Soil
1 / _ #1(,,,1_55 ,.... Analyst's Initials: RJW ~-v ;/-{ C-c,oJ-5$ ,...
Lab ID Number WS07281 WS07282 WS07284 WS07285
Client ID 07F 08F 10F 11F
Date Extracted 8/10/94 8/10/94 8/10/94 8/10/94
Date Analyzed 8/16/94 8/16/94 8/16/94 8/16/94
Detection
Compound Limit Result Result Result Result
alpha-BHC 0.003 U U U U
beta-BHC 0.003 U U U U
loamma-BHC (Lindane) 0.001 U U U U
delta-BHC 0.002 U U U U
Heotachlor 0.008 U U U U
Aldrin 0.003 U U U U
Heotachlor Eooxide 0.022 U U U U
Endosulfan I 0.003 U U U U -------------+-------+-----+-----+-------+------11
4,4'-DDE
Endrin
Endosulfan II
4,4' -DOD
Endrin Aldehyde
Endosulfan Sulfate
4,4' -DDT
Endrin Ketone
Methoxvchlor
Chlordane
Toxaphene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Detection Limit Multiplier
Surrogate Percent Recovery
1 fetrachloro-m-xvlene
I Decachlorobiphenyl
0.002 U U U U
0.009 U U U U
0.005 U U U U
0.003 U U U U
0.004 U U U U
0.015 U U U U
0.010 U U U U
0.004 U U U U
0.010 U U U U
0.010 U U U U
0.040 U U U U
0.040 U U U U
0.136 U U U U
0.130 U U U U
0.141 U U U U
0.115 U U U U
0.038 60 63 U U
0.019 U U U U
0.027 303 303 0.008 J 0.004 J
1000 1000 1 1
Diluted Out Diluted Out 88
Diluted Out Diluted Out 63
85
61
wasTESl"REdlTI ---T ECH NOL w
-.. Site: ECC
Date Sampled: 7/28/94
Waste Stream Technology Inc
Pesticide & PCB Report
Method 8081
Date Received : 8/2/94 @ 1200
Compound
alpha-BHC
beta-BHC
gamma-BHC (Lindane)
delta-BHC
Heptachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4' -DOD
Endrin Aldehyde
Endosulfan Sulfate
4,4' -DDT
Endrin Ketone
Methoxychlor
Chlordane
Toxaphene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Detection Limit Multiplier
Surrogate % Recovery
Tetrachloro-m-xylene
Decachlorobiphenyl
MB denotes Method Blank.
NA denotes Not Applicable.
Lab ID Number WS07283
Client ID 09A
Date Extracted 8/4/94
Date Analyzed . 8/17/94
Detection
Limit Result
0.044 u
0.046 u
0.016 u
0.023 u
0.12 u
0.048 u
0.32 u
0.048 u
0.028 u
0.13 u
0.080 u
0.041 u
0.057 u
0.23 u
0.16 u
0.064 u
0.054 u
0.14 u
0.60 u
0.60 u
2.0 u
2.0 u
2.1 u
1.7 u
0.57 u
0.29 u
0.41 u
1
QC Limits
60-150
60-150 74
Group Number : 9401 -172
Report Units: ug/L
Matrix : Aqueous
Analyst's Initials : RJW
MB94216
NA
8/4/94
8/17/94
Result Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1
83