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HomeMy WebLinkAboutNCD980602163_19900515_Warren County PCB Landfill_SERB C_Superfund Sampling - 1990-OCR15 May 1990 MEMORANDUM: To: From: Re: File Charlotte J esneck, Hydrogeologist Superfund Section PCB Landfill, Warren County Trip Summary and Laboratory Data For 18 April 1990 Sampling On 18 April 1990, Bruce Nicholson and I traveled to the PCB landfill in Warren County to conduct sampling of grass and soil on the landfill cap. The purpose of the sampling was to assist the Solid Waste Section in obtaining background information on the landfill cap before leachate extraction, treatment, and spray irrigation recommences. The landfill was staked at 50 feet intervals as depicted in the attached sketch. The landfill was then divided into four quadrants. Samples of grass and surface soil were collected near each staked point and composited within quadrants. This approach yielded four grass composite samples and four soil composite samples. In addition to these samples, samples were collected from the leachate collection pond sediment and the charcoal filter. The leachate collection pond did not have enough liquid to take a water sample. The soil samples form the landfill cap were collected using stainless steel scoops and composited in a precleaned stainless steel bucket. The bucket was decontaminated between composites by washing with alconox and deionized water, rinsing with deionized water, rinsing with isopropyl alcohol, and again rinsing with deionized water. The scoops were discarded between quadrants. The grass samples were composited in a bucket lined with aluminum foil. The foil was discarded between composites. Polyvinyl chloride gloves were worn while collecting samples. The gloves were discarded between quadrants and the other samples collected. All samples we placed in glass jars precleaned for organic samples. The samples were stored on ice until delivered to the laboratory the next morning. All of the samples were analyzed for PCBs and Base/Neutral and Acid Extractables. '- The table below identifies the field sample numbers, the Superfund Section identification numbers, the laboratory identification numbers, and the time of collection for each sample location: Field# Superfund # Lab# Location Time Collected A-G-1 12064 905009 Quadrant A 11 :50 -12: 10 Composite, Grass A-S-1_ 12065 905010 Quadrant A 11:50 -12: 10 Composite, Soil B-G-1 12066 905011 Quadrant B 11:15 -11:30 Composite, Grass B-S-1 12067 905012 Quadrant B 11:15 -11:30 Composite, Soil C-G-1 12068 905013 Quadrant C 15:00 -15:15 Composite, Grass C-S-1 12069 905014 Quadrant C 15:00 -15:15 Composite, Soil D-G-1 12070 905015 Quadrant D 14:40 -14:55 Composite, Grass D-S-1 12071 905016 Quadrant D 14:40 -14:55 Composite, Soil 2 12072 905017 Leachate Pond 15:30 Sediment 3 12073 905018 Charcoal Filter 15:30 The analytical data sheets are attached. Sample 2, the sediment from the leachate pond, was the only sample with a detectable concentration of PCBs. PCBs ( # 1260 PCB) were detected at a level of 0.27 ppm in t~is sample. attachments cc: Lee Crosby Bobby Lufty cv/jo/Memos.cv 'x. + >< I V\ 71 0 ,: ,., ( 3 ., ~ J:' -f ~ (" ) 0 :> 0 ::s ::, + + () (A - ' "' "' ~ V' I 7 r I ;1-11 -1--+- :, r (' + + .L + ----l-1..J-. .J--1-I -x-x-x-x-'t--x -x -x-x- $> -+-... L ..L + + .0 + '7-.L- I --1- +-X + l + -+- -+ .,.. +- + ..,_ -1--1- _J 0 C 9 s... ~ 75 0 'f ~ ::s ,;::, ~ ~ --I-""" "' 0 D C5 X. ~ t---(1l ~ " r-p -+-(':> -0 0 ~ v Q /'-\ ..., ......__ <:' ..., I ::, r> ~ .:'> c:,,Q_ -", I r--_ -....£) '.; D C ::, l./\ ...,_ 0 -c j --.:::, ::s L'> N. C. Department of Human Resources Division of Health Services 53 f >l 5 V vi -Pi' l',Jfl J SAMPLE ANALYSES REQUEST ttf {;filMelllic Health M P. ~ox 28047 AY 3~1J-mBington Street '"' ...,tt'aleigh, 2 7 611 Site Number _<....:;jv:...._'e,'='' :...._Q,.__,___,,.,_'1?)(=-· o'-· -~-~o_,='l,,.__li=-t_, --;; __ > __ Field Sample Number I ~ 0 <cSUmmtND SEc:TION Name of Site ___,_f----"(:::...L:/3:::..· _.::,L"'-...:::.r-A.:._u_r\..i..C.)""-1.C_,_,_,· /___,_} _______ Site Loc,tion ~-5 G v la_" f Collected By . Lic~ ( /:,--5 /2 /r ,' (\ ID# __ 4-!......J../ __ Date Collected ~ J) 8' / <j_o Mrre r7for1 ic,~/:) Time AM Type of Sample: .4 :_.. b .._; / Environmental __ Groundwater ( 1) __ Surface Water (2) __ Soil (3)- --Other (4) c7nce trate s-5 Cj r-o __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments Pleo.s Q Jl O l e l\ o 1a(/ ly s is I £ ; c ,: + , I f:. f he 1 P / s 9 t2 Ui So m;/e_ ) Q { + , q n a J <1 -z...,e fo r f h e__ o f ~ e rs 1 INORGANIC CHEMISTRY Extractables Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury __ Selenium __ Silver -- -- ---· ·- -- -- Parameter Results mg/1 ~T:GC/MS d:B/N Ext. z= TOX . J r J--.. ) () r o hr c 20 , c. u c ,· L r /\ lor o b~nl.-Ou!+'~rM ,L c, l,·cA ,/ c,vc, ~-,., r--11, · / C.; n u o ), e ,.-c o rv,OCv n,I < ·,,J h I(."' ,..,.,, / h Parameter __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/l00mls APR 1 9 1990 Reported By Total Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride . ------- __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter ~B __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ 1 <o,. LO pP-""'--~ Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ 1 __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS __ TOC .. -- -- -- -- -- -- Parameter Results mg/1 __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 I ! * ➔/' f (' J N. C. Department of Human Resources Division of Health Services ,5 u 1P -P r r-v 11 SAMPLE ANALYSES REQUEST Seate Laboratory of Public Health P. 0 . Box 28047 306 N. Wilmington Street Raleigh, 276 I 1 Site Number _...L/2....::.Vi---'0"""':c_.,:_OL,__(.7,_1 ~;::_· .=..,o_~-~-· _"•_O..c;:l=---'--/l=.~-?_> __ Field Sample Number _.;_/_~_-6_----'0'---S _________ _ Name of Site ----'f~..:::.(:.....· !....:/~=::...........::(=.-.:.:.:<:.....···._,'...:.,\-'-,..:.:.)_,;_'":_'.1../--'''-l ____ 0 _ 1 _ 1 ___ 0 aStiet~CL 0 o 11 ceacttieodn :~. ,)· ,J.51...'; ,);/ ~,(:: Collected By //e,, Ir/:,·> Ji/, , r\ ID#--~---~ __ Q_ _ I_, I I I Type of Sample: A -S -j_ Environmental Groundwater ( 1) Cons~ntran,. C Comments II,/' ,-,. '--l \ r I ;-i -,;.' -1 _, : ✓ Surface Water (2) __ Soil (3)- ~(5) __ Liquid (6) __ Sludge (7) __ Other (8) _l (-f h (' 1 p -C ' , 0 I . / f ; \'.'_ o }J. e rs --Other (4) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury . __ Selenium __ Silver -- -- •. ---· ....... -- -- Parameter Results mg/1 ~T:GC/MS d:B/N Ext. TOX . . 1/ ( J'\ i o r u bi'l!-Z.c,, c. ,, ,icl L r /,/orob fnl-O vH..:,r.;,c t(l,1!1 ,/ <1 ,., Q ~ °t I t-/f, I C, n u o ), t ,.-c c r,1:',:·J "'/ < __ (MF) Coliform Colonies/l OO mls __ (MPN) Coliform Colonies/lOOmls Date Received APR 1 g jggQ Bl) __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _TDS __ Fluoride . --·-----__ Toe ---- __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB'.s __ Petroleum __ Endrin __ Lindane Results mg/ 1 Parameter Results mg/1 __ Methoxychlor < ol 10 ff/'YI..__~ __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter Results PCi/1 __ Gross Alpha __ Gross Beta Date Reported 71 ~@~ Date Extracted L/--23·-<JQ-VP (WA lf--J_S"-C/0 AA . PC/3-'s t3µn DateAnalyzed l/-;{3-'1<21(p 5-J-9of>j) Reported By 9(15010 Lab Number __________________ _ DHS3l91 (Revised7/85) N. C. Department of Human Resources Division of Health Services -S§Zp ►' ,Su I°~ r /'cH1J SAMPLE ANALYSES REQUEST State Laboratory of Public Healt P. 0. Box 2804 306 N. Wilmington Strei Site Number ---'-/l-"--V_,e,='' __,()"-'---_·_'1----=K--'c_> _~_-_,o.....,;=, ~li=t-~ _?_> __ Raleigh, 2 761 Field Sample Number __ \ _-;}_-_CJ_&:J_tJ _______ _ Name of Site -)_/..--'f--'',;_-..:::~:..._--'---'.-..=:.~'-i__:C""''_ '--'--',_:.:..._, ..f_/',.__;-. ,,.L.)"---. ..L.f'-'-'-·L;-'J-I_D_i; _______ t'~ '~~/~~~~-DaStieteCLoollceacftieodn ~~-/1/. ,1\~ ,-J,//191 ~('. ',l Collected By ":'qr/a '5 /1/1 (\ tt _ I f I(\ ---- Type of Sample: 8 ,.-b ,-. j h/, r r " /) .i n r.\ 1 "' 7 tJ -. g_, Time A. M Environmental ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (3)_ __ Other (4) Concentrate c I c_ ·r-c, S-> ~~(S) __ Liquid (6) __ Sludge (7) __ Other (8) Comments , I --, I ( / ·-~ , .. / y'i ~1 ~ 1./ ·:.; / } Q { f . er fl a J l/ '2--e fo r I ' --) I, e_ 0 11! ,} (.J' i )11' ·(_;) i '). INORGANIC CHEMISTRY Extractables Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury · __ Selenium __ Silver -- --- -----· ,. -- -- Parameter Results mg/1 ~T:GC/MS Acid:B/N Exe. 1/ ~~~ioroh,,,--z..o ;co <,·J ,/ ( /\ /oro Ot n Z-O L,./.fc rr1 ,'c c, c,·J ,,--1 vc,, ·1, FY,· -I _ (',;/\Li C· (Ac 1,-C Crv,['"c-111/ < -. ' v.-' , I(. r\ M / U /' / I Q Y ,, ;~/ ,, ,,t:i i"'"/1r .,J,(\,},1ICROBI LOG } I , L{ I ~-_) ) ~ Parameter __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lO0mls Total Parameter Results mg/ 1 Parameter Results mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Cond uctivity __ Copper _TOS __ Fluoride -------__ TOC __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter ~B __ PCB'.s __ Petroleum __ Endrin __ Lindane Results mg/ 1 <O.10:pp/l'y Parameter __ Gross Alpha __ Gross Beta -- -- -- -- -- -- Parameter Results mg/1 __ Methoxychlor __ T oxaphene _2,4-0 __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 APR 1 9 1990 B ,/"\ Date Received ~~-,---------=~/JI _________ _ Date ExcractedPff.13-9oyp Date Reported,....,.....,=-----~..-.--~--------1' Cl3 ~ 8;() fl 4-JS--90 .4A Date Analyzed LJ-23-1/0i/P 5-J-CJpBf)_ Reported By Lab Number OHS 3191 ( Re vised 7185) N. C. Department of Human Resources Division of Health Services . l Su t> + r /v 11 J State Labo ratory of Public Hcalc: SAMPLE ANALYSES REQUEST P. 0. Box 2804' 306 N. Wilmington Scree Raleigh, 2761 Site Number Field Sample Number _ _c\_8-_·----'-"C)------11~.,.,__.,_] ______ _ Name o f Site _f'-1 ___:::(:.._;_r"_):='., -.-:'-'0: 1 ~l:.:._, _!_''u• 1c.c--::...)...1..f'....,_,_·.L;-')'----------Site Location ,--cf--'--'-'-'-'"cc..··_· -=-s--.-~· ..:;.."'+/_,_),'--'-'-,:--·r_r _)·-'-V--'-:·_, -'-'-'-'-" -'''--'-'--;-'· ,_·. '-'1:..__ __ _ ID# __ 4....,___,_/ __ Date Collected . =/ / ) 8' / CJ() Time ID -I °J It -1it Collected By l{q):,-_<, rJr , ! r\ Type of Sample: 0-S -.j En vi ronmen ta! ___ Groundwater ( 1) . -/Surface Water (2) _V_ S 'oil (3)_ __ Other (4) Concentrate Solid (5 ) __ Liquid (6) __ Sludge (7) __ Other (8) Comments f ; () o -'> Q cfl c. / c ;-:z , , ,; j ., I C 'i/2 !: 0 ' I I ,· r , d ; c r,{ l P cJ , INORGANIC CHEMISTRY Extractables Total Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TOS __ Selenium • __ Fluoride -------__ Toe __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury --··~-.. --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 ~T:GC/MS Acid:B/N Ext. _TOX . J ~ ( J'\ i or e h,,f.-z.c., c. a<; L r l\lor o b~nZ-o :,,/-1 ,,r r,;,c C(l,·J ,/ r, .,.. '-~ -,-' ~If. . I C-i"/\u c,, Ac1rc c.:~N-;0,./, -' , I. I I L-l \ 1../ / ... .-_) / _:., Parameter ·' __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colo nies/lO0mls APR 1 9 1990 {3 f) Parameter XB __ PCB's __ Petroleum __ Endrin __ Lindane Date Receiver! Date Ex tracten._3-C/()1./p:......_...L..=:.--L--'----'-"~"-'!IJCL.L~-lf_,__--'--:J..-'-5'--__,C/c..::D~/fu:.'9.1--- R e ported By DHS 3191 (Revised 7/85) Results mg/ 1 < 0, / 0 .pp.rr,.__,, Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/1 __ Methoxychlor __ T oxaphene _2,4-0 __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 Date Reported -:-:,-------------------1Gf3 S l3NA Date Analyzed l/-;23 -C/01/p -:f ~ 1---CJO f3l) Q. ,n,, l::;'. n 'M rry t...~"-l , ... ..J1V ..... tf.lll Lab Number %Zp ?s,>; /) Svvi.+r r-vt1J SAMPLE ANALYSES REQUEST N. C. Department of Human Resources Division of Health Services State Laboratory of Public Health P. 0 . Box 28047 306 N. Wilmington Street / Raleigh, 27611 _L...:;V::.__:,.(_,,""---"-Q_,___°l_v,=-..~'--=-n-~_-_-·O_,,=·l,._______;ft-=0'--, _?_> __ Field Sample Number _l~J. __ O_· _({J_f ________ _ Site Number f C r' :1) / · ) ,r--' / s· L · c./ . -I) f )/\ ,". ."·. ,l ('.· ~ Name O Sire ---''--='-:....· .c..:!'--.=:..)_L,=-.c:...C-_< .,:_YI'"-'·'""'-,·-'--. ___ ,_._._·--'-----)-_-11/ ___ DatleteCoolcleacrtteodn . ~~"n. !) )~;; ";? o ,(·.,, v :, r ,T,,im .. e 1 : ~ /? N\ Collected By i{\l'/t, ..5 !i /1 ,-(\ ID#--~-'--'-----_ _ ~ _ (__ J t-1" I I I Type of Sample: ~ _ b .-/ Environmental Concentrate "" ___ Groundwater ( l) ___ Surface Water (2) __ Soil (3)- --Other (4) J r:-:. ,uS-' . I • --s-ci'ti& ( 5) __ Liquid (6) __ Sludge (7) __ Other (8) INORGANIC CHEMISTRY Extractables Parameter Results mg/1 ___ Arsenic __ Barium __ Cadmium 1--Chrnmium ____ Lead __ Mercury __ Selenium ___ Silver -- -- ---· -- -- Parameter Results mg/1 ~T:GC/MS Acid:B/N Ext. _TOX . . / . . i ·J \L_ (.,/'"'/o r o 1:'0-Z.c,cuc, L ( /, lore-b,:n7-o.__,f.f-'~rr,11c c1 t,-c A ', ..... '; ..... " 0\ ., I Fr: . / (-1 n 1_. of i e. ,.-ccmf!<'c'n.,/< ., .J__ -.N, I'. -"' ": · cl h I MICROBIOLOGY ,'.. ,,,... 1 .,./ 1 ) ti 1 h. Jt : ,· ) ' ({. i ,.{ .... . , I . I L-t '"-I..( I~-...) ,'_:;, Parameter __ (MF) Coliform Colonies/l00mls --(MPN) Coliform Colonies/l00mls Date Received Date Extract=~-90\/P APR 1 9 1900 (30 Reported By DHS 319 I ( Revised 7/85) Total Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _TDS __ Fluoride -------__ TOC __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB's __ Petroleum __ Endrin __ Lindane l/-2.5-90 14/t Results rng/1 Parameter Results mg/ 1 __ Methoxychlor < 0 t LO -Pfl-~' __ Toxaphene ,- _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter Results PCi/1 __ Gross Alpha __ Gross Beta Date Reported -.=-,---------~--------?c.(3, J t:3 ,v It Date Analyzed 'l -;&~9oyp 5-/--CJoM Lab Number ::-tg;ry ?»,' 5 /\ .r l) fl J N. C. Department of Human Resources Division of Health Services " u 1J> ·-P , , Seate Laboratory of Public Heal cf SAMPLE AN AL YSES REQUEST P. 0. Box 2804; 306 N. Wilmington Scree Site Number Raleigh, 2761 • _.L/1-"...V_,,C,.,:,___!o:__J___0 _1_;::_K-=-o-~_,_~l~7,=)--........c..li=0'--, -~-~--Field Sample Number __ l _d_' _C='--=0=--_,9 ______ _ /;,-'J ; //"';] .?! . I' Name.: of Site --'f_-·_.:::;'--'-i...:c/._"'-)--'-C='--'1-'-:,-'rC'-\..1-.· '-'-''.-L--·__,_-',~--------Site Loca,ion 7 /l"f'\. S o v _/ .A ('. 'r '(,, ) ' .. Collected By /, (, /.Ir;_·...::> /, 11 ; f\ Type of Sample: Environmental __ Groundwater ( 1) --:-T Surface Water (2) _V __ Soil (3)- --Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Date Collected . cJ J ) t< ) CJ() I I 1 Comments , ~ , Time \-3 P /11 I ,,. c· ·, , I _ / \_ r , ·, · :7 i ./ '.~ / . -/'1 } /\ .. ,; I Q i-,-, er ,. a . <-1 2--e ro r f /2 (:'_ o 1/2 r:-r.s INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/1 Paran1eter Results mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Seler1i um __ Fluoride . -------__ TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury --~--.. --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter -,,B& T:GC/MS ~ Acid:B/N Ext. Results mg/1 _TOX . --~-----L ( J'\ i () I' o b I',~ -Z.c, '-;c-t, -'--'( '--=· J'-----,,--- L_ ( /\ } (; ( 0 b t' 11 Z-0 LJI-~ ir,!, L Ci , , , ,\ c,vcc "·t• Fw ; , ./ ('.',{ i\ I 1 0 /r). c 1r C <.:.r,1/l,:!-._:n . ../, ••• ~-'-1--.. TY\ ' 9 1' t MICROBIOLOGY •·•, r• ..._ ,,/ I) r) ; ,..,• )t : ,•) t A. i ,, _,. , j ··,'1 !...·t 1\L/!'7'-·1;_:::,, Parameter · __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/l00mls Parameter _ _f,DB _\_,,/""'_pprcB's __ Petroleum __ Endrin __ Lindane Date Received APR 1 9 l990 {3!) ~c.8~ Date Extracted q-E-C/0-yp NJ/A · 4-2$-10 ,4A Reported By DHS319 1 (Rcvised7/85) Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Parameter __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) Results mg/1 RADIOCHEMISTRY Results PCi/1 Dace Reported p...-,at),.,.,-,-~------,i1,=N.-::,. . .,.-,lf------ Date Analyzed L/-.;?3-t:JOVP S-/ -CJa61) Qf:)~:f\'~ i◄ Lab Number t..Jt'-· '..JJ'U ~-~ st p--,.;," Sv(>-Pr f..)~J Scace Laboratory of Public Hcahh N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST P. 0 . Box 28047 306 N. Wilmingt0n Street Raleigh, 2 761 1 Site Number Field Sample Number -+) _fh"-'-'-_,_{J-<--' ---'7'-----'cJ=---------- fJ ,,. .. --:i / • .). I'_, . I ,1 Na me o f Site ---'''---='-'-'-''=-..)-'-0:a~'---.C-c._1 ..:...,-1"""' . ...C....C.-'---'--'-----'----------Site Loca;ion -'--/-',, .. ---'/'..:.....,.,"-' :_.=5_,c_; ..c..v..,../-'-Ji'--"-c--'-f __ )½~::,'-. _:_r_,._r.1_1'~.Yc..c.:__:f__,· (..:_) '--(l'------1 / ) <;J ) 9C Time /-3 f fY\ Collected By l{, ( r; .5 )J, ,' (\ Type o( Sample: En vironmen ta! ID# __ 4...,__,_/ __ ~Da)e Collecte.d D-<; , Comments / ( )\ 1 1 , ; :I // ., I ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (3)- Concen~r,;a;e) 5 _5 ~~(S) __ Liquid (6) __ Sludge (7) __ Other (8) £ ;c,_.f , L (-f}fy;, ) Q f-+ , c.i r, o l i; "Z--e f'o r I. . );, e.. oh e rs --Other (4) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ C h romium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride. -------__ TOC __ Si lv er __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury --..... ,. --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/I ~T:GC/MS Acid:B/N Ext. LL_ ~Of;/ n ru Ln.c, c. u (,·J .!L_ ( /, / 0r O [)~ 1: Z-o;_,,/+c ((,), l C( c, j ,/ '/VI.;,,.,, ~,7'. I C, nu c, , ), c ,.-c cm,,,,,1,,,/ < · J h 'L 'r-.. f"X: ' +- __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lO0mls Parameter ~B _PCB'.s __ Petroleum __ Endrin __ Lindane Date Received __,.-r-__ AP_R_1_9_1_990_--'-'d=-t) ______ _ Date Extract~~-90--VP 6,,vi t.f-2s-qo AA Reported By Results mg/ I <n,/Onn-,.,..._ I I Parameter __ Gross Alpha __ Gross Beta Lab Number Parameter Results mg/I __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 N. C. Deparcmenr of Human Resources Division of Health Services ~?s/ 5v r° -P r f'..; f1 J SAMPLE ANALYSES REQUEST State Laboratory of Public Hcaltl P. 0 . Box 2804' 306 N. Wilmington Scree Site Number Name of Sire / . Raleigh, 2761 _L...:Jt/::...__:,,.G""--"-0-'---'"_, ~=-· a-'--· -~-..i.-_··l----'7;=l,------'-li=~--, _~_: __ Field Sample Number _ _.l_;} __ O_l ________ _ '.{J ,' .. ,/->·' /. c·., ·,,. ,·_.,) .,r'. , ,I ,) / I r -~ · Site location S .~. · -Sc;~'/ A .::. / 10# __ 4~. ~/ __ Date Collected . w ) ) ?{ ) 90 )'!/c, rr;> ,, /nri 1./.. l i ' . Collected By · ,::, r I:'., .5 /1 /: , f\ Time _____ _ Type of Sample: -f I . I 0-5-1. Environmental ___ Groundwater ( 1) ~ Surface Water (2) __ Soil (3)- --Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) I I Q ( + , q i' o } u c..--e fo r J. }, <: o -J /2 e o / -p ., I. ; . [) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates ___ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph ___ Lead __ Chromium __ Conductivi ty __ Mercury __ Copper _TDS __ Selenium __ Fluoride -------__ TOC __ Silve r __ Iron -- --__ Lead -- ---__ Manganese -- ---__ Mercury --........ --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 ~T:GC /MS d:B/N Ext. -,-TOX , . J ~ cJ'\lnrUh,c/1-Z.c,,c_u c,· L ( /\ /oro brr.Z-01.){~rr.:,c c, r, rA ,/ C.?1~~1~1c,?f), c 1r c~.~f!<'c•n,/< __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/l00mls APR 1 9 1900 Rf)_ Parameter ~B _PCB's __ Petroleum __ Endrin __ Lindane Date Received '/-,I · Date Extracte~3-901/p /ii/A //~2S-'10 All Reported By OHS 3191 (Revised 7185) Results mg/1 -<a,LO :ppm-,, Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ 1 __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 Date Reporte~ Date Analyzed ~#°-901/p ¥-:t<to/W Lab Number Of0.C."016• ~'-I:..iJ , :=§Z?f >l 5uf>-Pr /'v11J N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hcalt~ P. 0. Box 2804, 306 N. Wilmington Scree, Raleigh, 27611 Sire Number Field Sam pie Number _ ____,_\--.....:::3':....:'----=(J"'--_7=---& _______ _ /} I ., ! -I .('' , I 1 / / f S ,___ . -( . . s· L . .:::_; <., ,··.,· ,.,./ l_ .. • .,.r )A~ i Na me o ire __,,_'-.::::-'--L="-·, --'-'=--=-(-'-.\-''-'-\ .,..' ,,~, _,1~1__,__,.__________ 1 re ocapon ---'.'-''--'-'"''-' --"'-'--'-"-~-'-'"~-'--·~ V.'c1.'-'-r ,_r ~" _,_()-'--· ·-'--r:'--'-r1--'----- ID# __ 4-'---'-/_' __ Dare Collected . cj / ) <;{) 9C Time3f#tf1-"'-'m'----Collected By /,;j, (It;_-<, /1 /r , . (\ Type of Sample: Environmental Concentrate ___ Groundwater (1) ___ Solid (5) ___ Surface Water (2) ___ Liquid (6) J.L_ ~) 5 cc.( mb t+ Sludge (7) __ Other ( 4) Other (8) ·'· Jl c:( C- INORGANIC CHEMISTRY Comments ~ /' / ,·> I i. I '-. r, ·, ·, j Extractables Total Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chromium ___ Lead __ Mercury __ Selenium __ Silver -- -- ---.,, .. -- -- Parameter Results mg/1 ~T:GC/MS Acid:B/N Ext. Z ~0(1 n ro ,~en,_c, ;c. [; (,·J ,/ ( /,/or o bf nl-0 ,__,/{~rr,,,L ciL ,·sA ,/ ci..·,,~,~i~-,c,\l()l C v~· c.c,~.1/lt!•.:n,./ < . ' ' ,', L-~-~ '-1 / 1_,-_',, / .::::, Parameter / - __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lO0mls Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ Fluoride ·--------- __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY Parameter ~B __ PCWs __ Petroleum __ Endrin __ Lindane Results mg/ 1 o, ::t.2 :( PPIYL :k{#/ ;J,.{:,O -PeA 1 Paran\eter __ Gross Alpha __ Gross Bera Dare Receive~ APR 1 9 1900 JJJ)._ Dare Extracted ~ii--1ow IMM l/,25-t?o All Reported By Lab Number DHS 3 I 9 I (R~vised 7185) Parameter Results mg/1 __ Silver __ Sulfates __ Zinc _Ph __ Cond uc tivity _TDS __ TOC - -- -- -- -- -- -- Parameter Results mg/1 __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 N. C. Department o f Human Resources Division of Health Services Sb t >.~ ,5 \.) 1J>-P (' State Laboratory of Public Healer P. 0. Box 28041 306 N. Wilmington Scree, SAMPLE ANALYSES REQUEST Site Number . I I i I Collected By I!.,:,, I' I,;~' /1 /1 T ype of Sa mple: E nvironmental ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (3)- (\ _d_ Ot-hcr ( 4) c.Jc,, r u Qr C oncentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Raleigh, 2 761 1 -:;l_, 0 7 "3 Field Sample Number _________________ _ Co mments (. "'.\ ; / (_ /\ // l" ;/ / Time 3 ;? JV1 I i Q ( f-, o i1 a J l/ -z._.e I fo r -J-h e_ o /). e r.s , I ,· n , ) ; r o J e J. INORGANIC CHEMISTRY Extractables Parameter Results mg/1 __ Arsenic __ Barium ___ Cadmium __ Chromium ___ Lea d ___ Mercury __ Seleni um ___ Sil ver -- -- ---· ...... _ -- -- Parameter Results mg/ 1 ~T:GC/MS Acid: B/N Ext. _TOX . J L ( .f'\ i o t' u h:F7-o ,c 11 r; · L ( l\ lo r o b-:n Z..OvN~ rr,1, c c, t,· J ,··✓r ~1 v ,; "·1 1 Fr, I G{ n ,_; 0 i A (. I' CC MN c' /\.-/ < . ' _ ,,.,.,· r-. ·c 1--I'':: '.:i 1~ r . " MICROBIOLOGY ·-, r,.~ • ,_, ,) () 1 ,-... i 1, ,1.J • ,, 1,.,,,. • . '-,,, '-·t '-i..l /1.._· -> /_> Parameter 7 __ (MF) Coli fo rm Colonies/lO0mls __ (MPN) Coliform Colonies/lO0mls Total Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chloride __ C hromium __ Copper __ Fluoride . ------- __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Sel enium ORGANIC CHEMISTRY Parameter ~B __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 < {_ I Q .pprvt~ P arameter __ G ross Alpha __ Gross Beta Parameter Results mg/ 1 __ Silver __ Sulfates __ Zinc _Ph __ Conductivity - _TDS __ TOC -- -- -- -- -- -- -- Parameter Results mg/I __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,S-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 Dare Received APR 1 g 1990 t3D . . Date Reported :;;;:--;;;c=-r-------:;;--a---------- ~;y 8/VA- Date Analyzed, L.f-,3tJ-qtrlJ> 5-.2.-9~8~ Reported By Lab Number S0,:::;01a oc2:icJ of S2.mpling: Cnain of Cus::oci'-" Reco-r-d B2zardous ~aste Materials Generator Storage Facility Other: T~ansnorter Trea~~nt Faci.J..i Disposal ?2cility {bandfi.11 --------------------------f I ~ , t ~p2ny I s N 2..IDe __ _,_--"'C----'-{-"--)_C_ll~l'l~cJ"--'----,_f~1~t+· _______ I elepnon et ___ ) __ -· ______ _ dciress \~w~~~ : oll e c: or ' s N 2..me_-=--"'=~--'-'---+--'a..-='--'~=-'-"'-"--'----T el e~'Oho:) e( __ _,e) ________ _ . rignat:ure late Szspled y / ) <d 9 () .: . .. . Time S2.illpled _____ _,___+-, .......-----,1------------ yp e o:: ?rocess Gener2.ting '\,,12.ste ? CD J l sf)() c) C{ ( --+-!L~-'-"'-----'-<---vft--'~--L--+-------------- L 2 . 3. S0-:nple Ne. I J,() Cc ~ I \~011 c: Possession: signature sign2..:ure -/lO{c5 \.)07~ ,a-O~b 1cJiJ73 .:itle tit1.e inclusive d2. tes iI:1clusive dates 0 c:: e lns::-uc;::io;-is: Complete 2.11 applica·ole infcr.:c..::i.o., inclucin6 signatures, 2nd submit \..'ith ·.2n2.lysis :c-eaues:: fo:T:s. STATE LABORATORY OF PUBLIC HEALTH DIVIS IOO OF HEALTH SERVICES, N. C. DEPARTMENT OF HUMAN RESOORCES P.O. BOX 28047 -306 N. WILHINGTOO, ST., RALEIGH, N.C. 27611. ORGANIC CHEHICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # COMPOOND TYPE UNITS N-nitrosodimethvlamine Jnl :?3c bis (2--ch 1 oroethyl) ether 2-ch 1 orooheno 1 phenol 1 3-<lichlorobenzene 1 4-<lichlorobenzene 1 2-<lichlorobenzene bis (2--ch loroi :;__,,__,, ~, l)ether hexachloroethane - N-nitroso-<li-n-proovlamine nitrobenzene i s.oohorone 2-n i t rooheno 1 2 4-<limethylphenol bis(Z--chloroethoxy)methane 2 4-<lichloroohenol 1 2 4-trichlorobenzene nanhthalene hexachlorobutadiene 4--chloro-m--cres.ol hexachlorocyclooentadiene 2,4 6-trichloroohenol 2--chloronaohthalene acenaohthvlene dimethyl ohthalate 2 6-<linitrotoluene acenaohthene ,v 2 4-<linitroohenol SO/irt,So 2 4-<linitrotoluene !O/330 4-ni troohenol 'iSO/;t..50 fl uorene /0/E3o 4--chloroohenylphenvlether I diethyl phthalate -J., 4 6-<linitro-o---cres.ol So/J~C::O diohenvlamine l azobenzene ~ 4-braroohenvlohenvlether !rJ/..330 hexachlorobenzene I0/330 pentachloroohenol S0//05"0 phenanthrene JtJ/330 anthracene dibutyl phthalate fl uoranthene 'i ~ J -Estimated value. ffil)L flz.0/.50/ 1- C?o5oo9 CJ 05°?:> Io l~O(pt./ 1..;i., o(pS (.,) (3) ~(µq/kq' ~(µq/kqJ Ji -/,I - \/ \I/ K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. 90501 I 1..i.o~f.o ( ')) ~uq/ko LI \v qt>~'J0/,;2. /~t>b7 ( ? ) ~ µ q / k q) . /,,( \/ C/050/ =? I..J..o(p 9 (S-) ~µq/kq /~ \/ U -Katerial was analyzed for but not detected. The nurber NA -~t analyzed. is the 11ininun Detection Limit. m'J)L ---- 1/ -Tentative identification. ~/ -On NRDC List of Priority Pollutants . ,'-.!. C. V-<.V,</2,{,0Yl. 06 He.aLth SV!.V,{,C.e/2 VHS 3068-0 (4/86 Laboltato~y) - CD ( ) uq/1 µq/kq STATE LABORATORY OF f->UBLlC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESCXJRCES P.O. BOX 28047 -306 N. WILMINGTON, ST ., RALEIGH, N.C. 27611 ORGANIC D-lEMICAL ANALYSIS BASE/NEUTRAL ANO ACIO LAB NO qosooq 90S010 y'oSol I 9oso1.;i_ 9oSoJ_? EXTRACT ABLES FIELD# / ;J, o& t./ l~O(;:J I ~()f.o0 1.::i.oto7 CXJMPOONO TYPE ( 5) (3) ( S) (3) UNITS ~µ Q / k Q' u.c;it:l /uq/kq J .l-Gll1('uq/kQ .--J..l(µo/kQJ pyrene /0/3~n IA u_ IA u__ benzidine so/1160 butyl benzvl oht halate J0/330 benz(a)anthracene chrysene J, 3 3--dichlorobenzidine so//b.'io bis(2-ethvlhexvl)phthalate /()/330 di-n-octyl phthalate /0/.130 benzo(b)fluoranthene so/11:Do benzo(k)fluoranthene benzo(a)ovrene i ndeno ( 1 2 3---cd) pyrene dibenzo(a h)anthracene benzo(q h i )perylene \1/ \/ \I ,; ,v aniline ISo/1,t,,,;o L;{___. vL-I), -L,{__.. benzoic acid benzvl alcohol 4---ch 1 oroan i 1 i ne '-;' di benzofuran IO/Z.:M 2-methvl naohthd l ene 2-methylpheool j 4-methylpheool ~ 2-nitroaniline s-ol!lo5o 3-ni troani 1 i ne 4-nitroaniline 2 4 5-trichlorooheool 'lj/ \I \/ \I ,I n,1) L. J -Estimated value . H2.0/ So/1... K -Actual value is known to be less than value given . L -Actll<ll value is known to be greater than value given. U -Material was analyzed for but not detected. The nurber 1s the Minim..rn Detection Limit. NA -Not analyzed. 1/ -Tentative ide ntification. ~/ -On NROC Li s t of Priori ty Pollutants. N.C. 0-<..v..u,-<..on 06 He.a.Lth SVtv-<..c.U> OHS 306 8-0 (4/86 LabotuLto~y) Jc:!. olPR (-5) ~lC\JQ/kq' l,(__ \.V U- ,I 0 ( ) uo/1 µq/kQ STATE LABORATORY OF PUBLIC HEALTH DIVIS ION OF HEAL TH SERVICES, N. C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH , N.C. 27611 ORGANIC Q-lEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD# COMPOUND TYPE UNITS N-nitrosodimethvlamine /fl/ ~30 bis(2--<:hloroethvl)ether 2-chloroohenol ohenol 1 3--<:i ichlorobenzene l 4--<:iichlorobenzene l 2--<:iichlorobenzene bis(2--<:hloroi"'--",. A ,l)ether hexachloroethane - N-nitroso--<:li-n--oroovlamine nitrobenzene i soohorone 2-n i t rooheno l 2 4--<:iimethvlohenol bis(2--<:hloroethoxv)methane 2 4--<:iichloroohenol l 2 4-trichlorobenzene naohthalene hexachlorobutadiene 4--<:hl oro-m-cresol hexachlorocvclooentadiene 2,4 6-trichloroohenol 2--<:hloronaphthalene acenaohthvlene dimethyl ohthalate 2.6--<:iin i trotoluene acenaohthene 'V 2,4--<:iinitroohenol S0//hSO 2 4--<:iinitrotoluene !0/330 4-ni troohenol 'S°O/tt.,50 fl uorene 10/~30 4--<:hloroohenvlohenvlether diethyl phthalate J, 4 6--<:iinitro-o-cresol SOI ,t.i;o diohenylamine J azobenzene \V 4-braroohenylohenylether I o/.330 hexachlorobenzene /n/.33D oe ntachloroohenol so/Jto5"o ohenanthrene JIJ/.:no anthracene dibutvl phthalate fl uoranthene \j-" J -Estimated value. ,n1) L H2..0/.SOIL- CJ05ol '-I qo--,o;s /e,{O ft:,CJ /o?07O ( 3) ( "1) ~µq/kq" ~µq/kq) IA. LL \I \( K -Actual value is known to be less than value given . L -Actual value is known to be greater than value given . C/OSO/fa l-<07 I ( ~) ~Y~q/kQ) IA \v 9 r')_ "lD I 7 /~07cJ.. L3') ~6q/kq) I/ \/ 9o c;o!K /~D73 ( 41) ~ (µq/kq-... u_ / \V U -Katerial was analyzed for but not detected. The nu-rber NA -Not analyzed. is the Minirrun Detection Limit. m1JL .... -- 1/ -Tentative identification. ~I -On NRDC List of Priority Pollutants. J.C. V~v,<.,6 ~on 06 Healih SVtv~~e/2 JHS 3068-0 (4/86 LaboJta.to~y) - ( ) D µq/l µq/kq STATE LABORATORY OF f>UBUC HEAL TH DIVISION OF HEALTH SERVICf:S, N.C. DEPARTMENT OF HUMAN. RESOUfiCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 OOGNHC ~EMICAL ANALYSIS BASE/NEUTRAL AAD ACID LAB NO 9 rJ 5 n It..) qo..c;oI ., 9'oso1ta Y'O. ,017 EXTRACT ABLES FIELD# /~()/, q /col07rJ /_)_071 /oln7C:Z roMPOOND TYPE (-3) (.::J-) ( ..3) (3) UNITS -t1!11'.J.('uq/kq ~~(Gqik:q ~ 7uq/kq' ,.ad.✓uo/kal ovrene /0/~~n II -vL l,,!.._-l,{__ benzidine .~tJ/JhSO butyl benzyl phthal ate J0/330 benz(a)anthracene l chrvsene J, · 3 3-dichlorobenzidine 'lh..'itJ SOI bis(2-ethylhexyl)phthalate :/()/330 di-n-octvl ohthalate IO/.l~o benzo(b)fluoranthene s-0/11-50 benzo(k)fluoranthene benzo(a)pyrene indeno( 1 2 3-<:d)pyrene dibenzo(a h)anthracene benzo( q h i) oerv 1 ene ,!/ ,v \V \/ \I/ aniline tsol1t.,;--o IA...-IA--U-/A._ benzoic acid benzvl alcohol 4-ch 1 oroan i 1 i ne " ~ dibenzofuran 10/Z-/IJ 2-irethyl naphtha 1 ene 2-roethvl oheno 1 j 4-methylphenol \V 2-n i troan i 1 i ne S"o/Jta5o 3-n i troani 1 i ne 4-ni troani 1 i ne 2 4 5-trichloroohenol ~/ \V \v ,v \V m1H .. J -Estimate<l value. H:z.OI Soll.. to be less than value given . K -Actual value is known L -Actual value is known U -Katerial was analyzed NA -Not analyzed. to be greater than value given . for but not detected. The nuroer 1s the Hininun Detection Limit. 1/ -Tentative identification. ~/ -On NRDC List of Priority Pollutants . N. C. D-<..v-<..6-<..o 11 o 6 H ea.Lth s Vtv-<..c.e/2 VHS 306&-O (4 /&6 Labott.a.to~y l 90,0/ R /-2073 ( 'I) ( ) .....a:t::J (uq/kq uq/ 1 uq/kq t,( \V LL \/