WS-9395_44615_CA_RPTS_20151027_PhaseIIIESA

Phase III Environmental Site
Assessment
Old Greensboro Road
Proposed SunCap Property
Kernersville, North Carolina

October 27, 2015

Prepared For:
SunCap Property Group
ATTN: Jonathan Greene
The Carnegie Building
6101 Carnegie Blvd, Suite #180
Charlotte, NC 28209
704.579.4311

Submitted By:
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, Virginia 24540
434.797.4497

FIGURE 1
USGS Project Location Map

Figure 1: USGS Project Location Map Old Greensboro Road, Kernersville, NCUSGS Topographic Quadrangle Map, Kernersville, NC 20132014 Google Map Data551 Piney Forest Rd. Danville VA 24540434.797.4497ArchitectsEngineersPlannersSurveyorsProject Location36°06'27.9"N 80°02'27.6"WAreas of Interest1328 Old Greensboro Rd1404 Old Greensboro Rd
FIGURE 2
Sample Locations

Figure 2: Soil Sample Locations
Old Greensboro Road, Kernersville, NC
2014 Google Map Data
551 Piney Forest Rd.
Danville VA 24540
434.797.4497
Architects
Engineers
Planners
Surveyors
1328 Old Greensboro Rd 1404 Old Greensboro Rd
Soil sample locations are approximate
= Soil Sample (SS) location
Legend:
= Approximate perimeter of UST
1
2
3
1
2
4
1

APPENDIX A
Site Photographs

1. The UST before removal.
Appendix A: Phase III Site Photographs
1328 Old Greensboro Rd., Kernersville, NC
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
2. The UST is oriented perpendicular to the house.
3. Pumping out the contents of the UST.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
4. The UST after removal.
Appendix A: Phase III Site Photographs
1328 Old Greensboro Rd., Kernersville, NC
5. The UST after removal.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
Appendix A: Phase III Site Photographs
1328 Old Greensboro Rd., Kernersville, NC
6. Inside the UST after removal.
7. Excavating the UST. The UST parallels the house.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
8. Pumping out the contents of UST.
Appendix A: Phase III Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
9. Removing the UST.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
10. The removed UST.
Appendix A: Phase III Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
11. Obvious staining on the removed UST.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
12. Picture of inside the UST. Note the pinprick hole in the tank.
Appendix A: Phase III Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
13. Removed soil.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
14. The excavated pit.
Appendix A: Phase III Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
15. The excavated pit.
P:\50065050\Adm\Reports\Phase 3\Appendix A –Site Photos.pptx
Appendix A: Phase III Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
APPENDIX B
Laboratory Analytical Results

#=CL#
September 02, 2015
LIMS USE: FR - TROY SHELTON
LIMS OBJECT ID: 92264629
92264629
Project:
Pace Project No.:
RE:
Troy Shelton
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, VA 24540
SUNCAP 1328 OLD GREENSBORO RD
Dear Troy Shelton:
Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Lab ID Sample ID Matrix Date Collected Date Received
92264629001 SS-1 (8.5 FT)Solid 08/21/15 08:52 08/24/15 13:00
92264629002 SS-2 (6 FT)Solid 08/21/15 09:09 08/24/15 13:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92264629001 SS-1 (8.5 FT)EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92264629002 SS-2 (6 FT)EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 36
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92264629001 SS-1 (8.5 FT)
Diesel Range Organics(C10-C28)65.2 mg/kg 08/30/15 06:395.9EPA 8015 Modified
Gas Range Organics (C6-C10)15.6 mg/kg 08/25/15 16:368.0EPA 8015 Modified
Methylene Chloride 12.8J ug/kg 08/28/15 01:45 B27.1EPA 8260
Percent Moisture 14.6 %08/25/15 12:540.10ASTM D2974-87
92264629002 SS-2 (6 FT)
Methylene Chloride 9.6J ug/kg 08/28/15 02:05 B23.7EPA 8260
Percent Moisture 12.5 %08/25/15 12:550.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-1 (8.5 FT)Lab ID: 92264629001 Collected: 08/21/15 08:52 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)65.2 mg/kg 08/30/15 06:3908/27/15 16:305.9 5.3 1
Surrogates
n-Pentacosane (S)60 %08/30/15 06:39 629-99-208/27/15 16:3041-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/26/15 21:57 N208/24/15 15:1811.7 11.7 1
Aliphatic (C19-C36)ND mg/kg 08/26/15 21:57 N208/24/15 15:1811.7 11.7 1
Aromatic (C11-C22)ND mg/kg 08/27/15 05:26 N208/24/15 15:1811.7 11.7 1
Surrogates
Nonatriacontane (S)70 %08/26/15 21:57 7194-86-708/24/15 15:1840-140 1
o-Terphenyl (S)61 %08/27/15 05:26 84-15-108/24/15 15:1840-140 1
2-Fluorobiphenyl (S)68 %08/27/15 05:26 321-60-808/24/15 15:1840-140 1
2-Bromonaphthalene (S)59 %08/27/15 05:26 580-13-208/24/15 15:1840-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)15.6 mg/kg 08/25/15 16:3608/25/15 11:038.0 8.0 1
Surrogates
4-Bromofluorobenzene (S)104 %08/25/15 16:36 460-00-408/25/15 11:0370-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/01/15 22:31 N208/31/15 09:223.9 3.9 1
Aliphatic (C09-C12)ND mg/kg 09/01/15 22:31 N208/31/15 09:223.9 3.9 1
Aromatic (C09-C10)ND mg/kg 09/01/15 22:31 N208/31/15 09:223.9 3.9 1
Surrogates
4-Bromofluorobenzene (FID) (S)107 %09/01/15 22:31 460-00-408/31/15 09:2270-130 1
4-Bromofluorobenzene (PID) (S)107 %09/01/15 22:31 460-00-408/31/15 09:2270-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 08/28/15 19:47 83-32-908/26/15 09:35387 89.0 1
Acenaphthylene ND ug/kg 08/28/15 19:47 208-96-808/26/15 09:35387 91.4 1
Aniline ND ug/kg 08/28/15 19:47 62-53-308/26/15 09:35387 104 1
Anthracene ND ug/kg 08/28/15 19:47 120-12-708/26/15 09:35387 86.7 1
Benzo(a)anthracene ND ug/kg 08/28/15 19:47 56-55-308/26/15 09:35387 71.5 1
Benzo(a)pyrene ND ug/kg 08/28/15 19:47 50-32-808/26/15 09:35387 73.8 1
Benzo(b)fluoranthene ND ug/kg 08/28/15 19:47 205-99-208/26/15 09:35387 66.8 1
Benzo(g,h,i)perylene ND ug/kg 08/28/15 19:47 191-24-208/26/15 09:35387 98.4 1
Benzo(k)fluoranthene ND ug/kg 08/28/15 19:47 207-08-908/26/15 09:35387 76.2 1
Benzoic Acid ND ug/kg 08/28/15 19:47 65-85-008/26/15 09:351930 70.3 1
Benzyl alcohol ND ug/kg 08/28/15 19:47 100-51-608/26/15 09:35773 77.3 1
4-Bromophenylphenyl ether ND ug/kg 08/28/15 19:47 101-55-308/26/15 09:35387 70.3 1
Butylbenzylphthalate ND ug/kg 08/28/15 19:47 85-68-708/26/15 09:35387 82.0 1
4-Chloro-3-methylphenol ND ug/kg 08/28/15 19:47 59-50-708/26/15 09:35773 79.7 1
4-Chloroaniline ND ug/kg 08/28/15 19:47 106-47-808/26/15 09:351930 108 1
bis(2-Chloroethoxy)methane ND ug/kg 08/28/15 19:47 111-91-108/26/15 09:35387 90.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-1 (8.5 FT)Lab ID: 92264629001 Collected: 08/21/15 08:52 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 08/28/15 19:47 111-44-408/26/15 09:35387 98.4 1
bis(2-Chloroisopropyl) ether ND ug/kg 08/28/15 19:47 108-60-108/26/15 09:35387 103 1
2-Chloronaphthalene ND ug/kg 08/28/15 19:47 91-58-708/26/15 09:35387 76.2 1
2-Chlorophenol ND ug/kg 08/28/15 19:47 95-57-808/26/15 09:35387 105 1
4-Chlorophenylphenyl ether ND ug/kg 08/28/15 19:47 7005-72-308/26/15 09:35387 79.7 1
Chrysene ND ug/kg 08/28/15 19:47 218-01-908/26/15 09:35387 51.5 1
Dibenz(a,h)anthracene ND ug/kg 08/28/15 19:47 53-70-308/26/15 09:35387 82.0 1
Dibenzofuran ND ug/kg 08/28/15 19:47 132-64-908/26/15 09:35387 63.3 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 19:47 95-50-108/26/15 09:35387 103 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 19:47 541-73-108/26/15 09:35387 87.9 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 19:47 106-46-708/26/15 09:35387 109 1
3,3'-Dichlorobenzidine ND ug/kg 08/28/15 19:47 91-94-108/26/15 09:351930 84.4 1
2,4-Dichlorophenol ND ug/kg 08/28/15 19:47 120-83-208/26/15 09:35387 84.4 1
Diethylphthalate ND ug/kg 08/28/15 19:47 84-66-208/26/15 09:35387 59.8 1
2,4-Dimethylphenol ND ug/kg 08/28/15 19:47 105-67-908/26/15 09:35387 152 1
Dimethylphthalate ND ug/kg 08/28/15 19:47 131-11-308/26/15 09:35387 78.5 1
Di-n-butylphthalate ND ug/kg 08/28/15 19:47 84-74-208/26/15 09:35387 63.3 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/28/15 19:47 534-52-108/26/15 09:35773 77.3 1
2,4-Dinitrophenol ND ug/kg 08/28/15 19:47 51-28-508/26/15 09:351930 63.3 1
2,4-Dinitrotoluene ND ug/kg 08/28/15 19:47 121-14-208/26/15 09:35387 72.6 1
2,6-Dinitrotoluene ND ug/kg 08/28/15 19:47 606-20-208/26/15 09:35387 80.8 1
Di-n-octylphthalate ND ug/kg 08/28/15 19:47 117-84-008/26/15 09:35387 80.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/28/15 19:47 117-81-708/26/15 09:35387 105 1
Fluoranthene ND ug/kg 08/28/15 19:47 206-44-008/26/15 09:35387 56.2 1
Fluorene ND ug/kg 08/28/15 19:47 86-73-708/26/15 09:35387 79.7 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 19:47 87-68-308/26/15 09:35387 66.8 1
Hexachlorobenzene ND ug/kg 08/28/15 19:47 118-74-108/26/15 09:35387 49.2 1
Hexachlorocyclopentadiene ND ug/kg 08/28/15 19:47 77-47-408/26/15 09:35387 71.5 1
Hexachloroethane ND ug/kg 08/28/15 19:47 67-72-108/26/15 09:35387 102 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/28/15 19:47 193-39-508/26/15 09:35387 79.7 1
Isophorone ND ug/kg 08/28/15 19:47 78-59-108/26/15 09:35387 86.7 1
1-Methylnaphthalene ND ug/kg 08/28/15 19:47 90-12-008/26/15 09:35387 101 1
2-Methylnaphthalene ND ug/kg 08/28/15 19:47 91-57-608/26/15 09:35387 83.2 1
2-Methylphenol(o-Cresol)ND ug/kg 08/28/15 19:47 95-48-708/26/15 09:35387 117 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/28/15 19:4708/26/15 09:35387 152 1
Naphthalene ND ug/kg 08/28/15 19:47 91-20-308/26/15 09:35387 94.9 1
2-Nitroaniline ND ug/kg 08/28/15 19:47 88-74-408/26/15 09:351930 120 1
3-Nitroaniline ND ug/kg 08/28/15 19:47 99-09-208/26/15 09:351930 105 1
4-Nitroaniline ND ug/kg 08/28/15 19:47 100-01-608/26/15 09:35773 109 1
Nitrobenzene ND ug/kg 08/28/15 19:47 98-95-308/26/15 09:35387 105 1
2-Nitrophenol ND ug/kg 08/28/15 19:47 88-75-508/26/15 09:35387 93.7 1
4-Nitrophenol ND ug/kg 08/28/15 19:47 100-02-708/26/15 09:351930 69.1 1
N-Nitrosodimethylamine ND ug/kg 08/28/15 19:47 62-75-908/26/15 09:35387 125 1
N-Nitroso-di-n-propylamine ND ug/kg 08/28/15 19:47 621-64-708/26/15 09:35387 73.8 1
N-Nitrosodiphenylamine ND ug/kg 08/28/15 19:47 86-30-608/26/15 09:35387 115 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-1 (8.5 FT)Lab ID: 92264629001 Collected: 08/21/15 08:52 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 08/28/15 19:47 87-86-508/26/15 09:351930 70.3 1
Phenanthrene ND ug/kg 08/28/15 19:47 85-01-808/26/15 09:35387 64.4 1
Phenol ND ug/kg 08/28/15 19:47 108-95-208/26/15 09:35387 116 1
Pyrene ND ug/kg 08/28/15 19:47 129-00-008/26/15 09:35387 65.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 19:47 120-82-108/26/15 09:35387 75.0 1
2,4,5-Trichlorophenol ND ug/kg 08/28/15 19:47 95-95-408/26/15 09:35387 120 1
2,4,6-Trichlorophenol ND ug/kg 08/28/15 19:47 88-06-208/26/15 09:35387 85.5 1
Surrogates
Nitrobenzene-d5 (S)42 %08/28/15 19:47 4165-60-008/26/15 09:3523-110 1
2-Fluorobiphenyl (S)39 %08/28/15 19:47 321-60-808/26/15 09:3530-110 1
Terphenyl-d14 (S)55 %08/28/15 19:47 1718-51-008/26/15 09:3528-110 1
Phenol-d6 (S)40 %08/28/15 19:47 13127-88-308/26/15 09:3522-110 1
2-Fluorophenol (S)41 %08/28/15 19:47 367-12-408/26/15 09:3513-110 1
2,4,6-Tribromophenol (S)48 %08/28/15 19:47 118-79-608/26/15 09:3527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/28/15 01:45 67-64-1136 13.6 1
Benzene ND ug/kg 08/28/15 01:45 71-43-26.8 2.2 1
Bromobenzene ND ug/kg 08/28/15 01:45 108-86-16.8 2.7 1
Bromochloromethane ND ug/kg 08/28/15 01:45 74-97-56.8 2.3 1
Bromodichloromethane ND ug/kg 08/28/15 01:45 75-27-46.8 2.6 1
Bromoform ND ug/kg 08/28/15 01:45 75-25-26.8 3.1 1
Bromomethane ND ug/kg 08/28/15 01:45 74-83-913.6 3.4 1
2-Butanone (MEK)ND ug/kg 08/28/15 01:45 78-93-3136 3.9 1
n-Butylbenzene ND ug/kg 08/28/15 01:45 104-51-86.8 2.4 1
sec-Butylbenzene ND ug/kg 08/28/15 01:45 135-98-86.8 2.2 1
tert-Butylbenzene ND ug/kg 08/28/15 01:45 98-06-66.8 2.7 1
Carbon tetrachloride ND ug/kg 08/28/15 01:45 56-23-56.8 3.5 1
Chlorobenzene ND ug/kg 08/28/15 01:45 108-90-76.8 2.6 1
Chloroethane ND ug/kg 08/28/15 01:45 75-00-313.6 3.3 1
Chloroform ND ug/kg 08/28/15 01:45 67-66-36.8 2.2 1
Chloromethane ND ug/kg 08/28/15 01:45 74-87-313.6 3.3 1
2-Chlorotoluene ND ug/kg 08/28/15 01:45 95-49-86.8 2.3 1
4-Chlorotoluene ND ug/kg 08/28/15 01:45 106-43-46.8 2.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/28/15 01:45 96-12-86.8 4.9 1
Dibromochloromethane ND ug/kg 08/28/15 01:45 124-48-16.8 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/28/15 01:45 106-93-46.8 2.4 1
Dibromomethane ND ug/kg 08/28/15 01:45 74-95-36.8 3.4 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 01:45 95-50-16.8 2.6 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 01:45 541-73-16.8 2.7 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 01:45 106-46-76.8 2.3 1
Dichlorodifluoromethane ND ug/kg 08/28/15 01:45 75-71-813.6 4.9 1
1,1-Dichloroethane ND ug/kg 08/28/15 01:45 75-34-36.8 2.0 1
1,2-Dichloroethane ND ug/kg 08/28/15 01:45 107-06-26.8 3.0 1
1,1-Dichloroethene ND ug/kg 08/28/15 01:45 75-35-46.8 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-1 (8.5 FT)Lab ID: 92264629001 Collected: 08/21/15 08:52 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 08/28/15 01:45 156-59-26.8 1.9 1
trans-1,2-Dichloroethene ND ug/kg 08/28/15 01:45 156-60-56.8 2.6 1
1,2-Dichloropropane ND ug/kg 08/28/15 01:45 78-87-56.8 2.3 1
1,3-Dichloropropane ND ug/kg 08/28/15 01:45 142-28-96.8 2.6 1
2,2-Dichloropropane ND ug/kg 08/28/15 01:45 594-20-76.8 2.3 1
1,1-Dichloropropene ND ug/kg 08/28/15 01:45 563-58-66.8 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/28/15 01:45 10061-01-56.8 2.4 1
trans-1,3-Dichloropropene ND ug/kg 08/28/15 01:45 10061-02-66.8 2.0 1
Diisopropyl ether ND ug/kg 08/28/15 01:45 108-20-36.8 2.3 1
Ethylbenzene ND ug/kg 08/28/15 01:45 100-41-46.8 2.4 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 01:45 87-68-36.8 2.7 1
2-Hexanone ND ug/kg 08/28/15 01:45 591-78-667.8 5.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/28/15 01:45 98-82-86.8 2.6 1
p-Isopropyltoluene ND ug/kg 08/28/15 01:45 99-87-66.8 2.3 1
Methylene Chloride 12.8J ug/kg 08/28/15 01:45 75-09-2 B27.1 4.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/28/15 01:45 108-10-167.8 5.0 1
Methyl-tert-butyl ether ND ug/kg 08/28/15 01:45 1634-04-46.8 2.0 1
Naphthalene ND ug/kg 08/28/15 01:45 91-20-36.8 1.6 1
n-Propylbenzene ND ug/kg 08/28/15 01:45 103-65-16.8 2.3 1
Styrene ND ug/kg 08/28/15 01:45 100-42-56.8 2.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/28/15 01:45 630-20-66.8 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/28/15 01:45 79-34-56.8 2.6 1
Tetrachloroethene ND ug/kg 08/28/15 01:45 127-18-46.8 2.3 1
Toluene ND ug/kg 08/28/15 01:45 108-88-36.8 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/28/15 01:45 87-61-66.8 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 01:45 120-82-16.8 2.2 1
1,1,1-Trichloroethane ND ug/kg 08/28/15 01:45 71-55-66.8 2.4 1
1,1,2-Trichloroethane ND ug/kg 08/28/15 01:45 79-00-56.8 2.8 1
Trichloroethene ND ug/kg 08/28/15 01:45 79-01-66.8 2.8 1
Trichlorofluoromethane ND ug/kg 08/28/15 01:45 75-69-46.8 3.0 1
1,2,3-Trichloropropane ND ug/kg 08/28/15 01:45 96-18-46.8 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/28/15 01:45 95-63-66.8 2.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/28/15 01:45 108-67-86.8 2.4 1
Vinyl acetate ND ug/kg 08/28/15 01:45 108-05-4 L267.8 11.9 1
Vinyl chloride ND ug/kg 08/28/15 01:45 75-01-413.6 2.4 1
Xylene (Total)ND ug/kg 08/28/15 01:45 1330-20-713.6 4.9 1
m&p-Xylene ND ug/kg 08/28/15 01:45 179601-23-113.6 4.9 1
o-Xylene ND ug/kg 08/28/15 01:45 95-47-66.8 2.6 1
Surrogates
Toluene-d8 (S)101 %08/28/15 01:45 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %08/28/15 01:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/28/15 01:45 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %08/25/15 12:540.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-2 (6 FT)Lab ID: 92264629002 Collected: 08/21/15 09:09 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/30/15 06:3908/27/15 16:305.7 5.1 1
Surrogates
n-Pentacosane (S)77 %08/30/15 06:39 629-99-208/27/15 16:3041-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/26/15 22:29 N208/24/15 15:1811.4 11.4 1
Aliphatic (C19-C36)ND mg/kg 08/26/15 22:29 N208/24/15 15:1811.4 11.4 1
Aromatic (C11-C22)ND mg/kg 08/27/15 05:58 N208/24/15 15:1811.4 11.4 1
Surrogates
Nonatriacontane (S)61 %08/26/15 22:29 7194-86-708/24/15 15:1840-140 1
o-Terphenyl (S)75 %08/27/15 05:58 84-15-108/24/15 15:1840-140 1
2-Fluorobiphenyl (S)85 %08/27/15 05:58 321-60-808/24/15 15:1840-140 1
2-Bromonaphthalene (S)87 %08/27/15 05:58 580-13-208/24/15 15:1840-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/25/15 17:2108/25/15 11:038.0 8.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/25/15 17:21 460-00-408/25/15 11:0370-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/01/15 23:01 N208/31/15 09:223.8 3.8 1
Aliphatic (C09-C12)ND mg/kg 09/01/15 23:01 N208/31/15 09:223.8 3.8 1
Aromatic (C09-C10)ND mg/kg 09/01/15 23:01 N208/31/15 09:223.8 3.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)106 %09/01/15 23:01 460-00-408/31/15 09:2270-130 1
4-Bromofluorobenzene (PID) (S)107 %09/01/15 23:01 460-00-408/31/15 09:2270-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 08/28/15 20:15 83-32-908/26/15 09:35377 86.9 1
Acenaphthylene ND ug/kg 08/28/15 20:15 208-96-808/26/15 09:35377 89.2 1
Aniline ND ug/kg 08/28/15 20:15 62-53-308/26/15 09:35377 102 1
Anthracene ND ug/kg 08/28/15 20:15 120-12-708/26/15 09:35377 84.6 1
Benzo(a)anthracene ND ug/kg 08/28/15 20:15 56-55-308/26/15 09:35377 69.7 1
Benzo(a)pyrene ND ug/kg 08/28/15 20:15 50-32-808/26/15 09:35377 72.0 1
Benzo(b)fluoranthene ND ug/kg 08/28/15 20:15 205-99-208/26/15 09:35377 65.2 1
Benzo(g,h,i)perylene ND ug/kg 08/28/15 20:15 191-24-208/26/15 09:35377 96.0 1
Benzo(k)fluoranthene ND ug/kg 08/28/15 20:15 207-08-908/26/15 09:35377 74.3 1
Benzoic Acid ND ug/kg 08/28/15 20:15 65-85-008/26/15 09:351890 68.6 1
Benzyl alcohol ND ug/kg 08/28/15 20:15 100-51-608/26/15 09:35755 75.5 1
4-Bromophenylphenyl ether ND ug/kg 08/28/15 20:15 101-55-308/26/15 09:35377 68.6 1
Butylbenzylphthalate ND ug/kg 08/28/15 20:15 85-68-708/26/15 09:35377 80.0 1
4-Chloro-3-methylphenol ND ug/kg 08/28/15 20:15 59-50-708/26/15 09:35755 77.8 1
4-Chloroaniline ND ug/kg 08/28/15 20:15 106-47-808/26/15 09:351890 105 1
bis(2-Chloroethoxy)methane ND ug/kg 08/28/15 20:15 111-91-108/26/15 09:35377 88.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-2 (6 FT)Lab ID: 92264629002 Collected: 08/21/15 09:09 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 08/28/15 20:15 111-44-408/26/15 09:35377 96.0 1
bis(2-Chloroisopropyl) ether ND ug/kg 08/28/15 20:15 108-60-108/26/15 09:35377 101 1
2-Chloronaphthalene ND ug/kg 08/28/15 20:15 91-58-708/26/15 09:35377 74.3 1
2-Chlorophenol ND ug/kg 08/28/15 20:15 95-57-808/26/15 09:35377 103 1
4-Chlorophenylphenyl ether ND ug/kg 08/28/15 20:15 7005-72-308/26/15 09:35377 77.8 1
Chrysene ND ug/kg 08/28/15 20:15 218-01-908/26/15 09:35377 50.3 1
Dibenz(a,h)anthracene ND ug/kg 08/28/15 20:15 53-70-308/26/15 09:35377 80.0 1
Dibenzofuran ND ug/kg 08/28/15 20:15 132-64-908/26/15 09:35377 61.7 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 20:15 95-50-108/26/15 09:35377 101 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 20:15 541-73-108/26/15 09:35377 85.8 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 20:15 106-46-708/26/15 09:35377 106 1
3,3'-Dichlorobenzidine ND ug/kg 08/28/15 20:15 91-94-108/26/15 09:351890 82.3 1
2,4-Dichlorophenol ND ug/kg 08/28/15 20:15 120-83-208/26/15 09:35377 82.3 1
Diethylphthalate ND ug/kg 08/28/15 20:15 84-66-208/26/15 09:35377 58.3 1
2,4-Dimethylphenol ND ug/kg 08/28/15 20:15 105-67-908/26/15 09:35377 149 1
Dimethylphthalate ND ug/kg 08/28/15 20:15 131-11-308/26/15 09:35377 76.6 1
Di-n-butylphthalate ND ug/kg 08/28/15 20:15 84-74-208/26/15 09:35377 61.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/28/15 20:15 534-52-108/26/15 09:35755 75.5 1
2,4-Dinitrophenol ND ug/kg 08/28/15 20:15 51-28-508/26/15 09:351890 61.7 1
2,4-Dinitrotoluene ND ug/kg 08/28/15 20:15 121-14-208/26/15 09:35377 70.9 1
2,6-Dinitrotoluene ND ug/kg 08/28/15 20:15 606-20-208/26/15 09:35377 78.9 1
Di-n-octylphthalate ND ug/kg 08/28/15 20:15 117-84-008/26/15 09:35377 78.9 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/28/15 20:15 117-81-708/26/15 09:35377 103 1
Fluoranthene ND ug/kg 08/28/15 20:15 206-44-008/26/15 09:35377 54.9 1
Fluorene ND ug/kg 08/28/15 20:15 86-73-708/26/15 09:35377 77.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 20:15 87-68-308/26/15 09:35377 65.2 1
Hexachlorobenzene ND ug/kg 08/28/15 20:15 118-74-108/26/15 09:35377 48.0 1
Hexachlorocyclopentadiene ND ug/kg 08/28/15 20:15 77-47-408/26/15 09:35377 69.7 1
Hexachloroethane ND ug/kg 08/28/15 20:15 67-72-108/26/15 09:35377 99.5 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/28/15 20:15 193-39-508/26/15 09:35377 77.8 1
Isophorone ND ug/kg 08/28/15 20:15 78-59-108/26/15 09:35377 84.6 1
1-Methylnaphthalene ND ug/kg 08/28/15 20:15 90-12-008/26/15 09:35377 98.3 1
2-Methylnaphthalene ND ug/kg 08/28/15 20:15 91-57-608/26/15 09:35377 81.2 1
2-Methylphenol(o-Cresol)ND ug/kg 08/28/15 20:15 95-48-708/26/15 09:35377 114 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/28/15 20:1508/26/15 09:35377 149 1
Naphthalene ND ug/kg 08/28/15 20:15 91-20-308/26/15 09:35377 92.6 1
2-Nitroaniline ND ug/kg 08/28/15 20:15 88-74-408/26/15 09:351890 117 1
3-Nitroaniline ND ug/kg 08/28/15 20:15 99-09-208/26/15 09:351890 103 1
4-Nitroaniline ND ug/kg 08/28/15 20:15 100-01-608/26/15 09:35755 106 1
Nitrobenzene ND ug/kg 08/28/15 20:15 98-95-308/26/15 09:35377 103 1
2-Nitrophenol ND ug/kg 08/28/15 20:15 88-75-508/26/15 09:35377 91.5 1
4-Nitrophenol ND ug/kg 08/28/15 20:15 100-02-708/26/15 09:351890 67.5 1
N-Nitrosodimethylamine ND ug/kg 08/28/15 20:15 62-75-908/26/15 09:35377 122 1
N-Nitroso-di-n-propylamine ND ug/kg 08/28/15 20:15 621-64-708/26/15 09:35377 72.0 1
N-Nitrosodiphenylamine ND ug/kg 08/28/15 20:15 86-30-608/26/15 09:35377 112 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-2 (6 FT)Lab ID: 92264629002 Collected: 08/21/15 09:09 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 08/28/15 20:15 87-86-508/26/15 09:351890 68.6 1
Phenanthrene ND ug/kg 08/28/15 20:15 85-01-808/26/15 09:35377 62.9 1
Phenol ND ug/kg 08/28/15 20:15 108-95-208/26/15 09:35377 113 1
Pyrene ND ug/kg 08/28/15 20:15 129-00-008/26/15 09:35377 64.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 20:15 120-82-108/26/15 09:35377 73.2 1
2,4,5-Trichlorophenol ND ug/kg 08/28/15 20:15 95-95-408/26/15 09:35377 117 1
2,4,6-Trichlorophenol ND ug/kg 08/28/15 20:15 88-06-208/26/15 09:35377 83.5 1
Surrogates
Nitrobenzene-d5 (S)41 %08/28/15 20:15 4165-60-008/26/15 09:3523-110 1
2-Fluorobiphenyl (S)38 %08/28/15 20:15 321-60-808/26/15 09:3530-110 1
Terphenyl-d14 (S)52 %08/28/15 20:15 1718-51-008/26/15 09:3528-110 1
Phenol-d6 (S)37 %08/28/15 20:15 13127-88-308/26/15 09:3522-110 1
2-Fluorophenol (S)39 %08/28/15 20:15 367-12-408/26/15 09:3513-110 1
2,4,6-Tribromophenol (S)40 %08/28/15 20:15 118-79-608/26/15 09:3527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/28/15 02:05 67-64-1119 11.9 1
Benzene ND ug/kg 08/28/15 02:05 71-43-25.9 1.9 1
Bromobenzene ND ug/kg 08/28/15 02:05 108-86-15.9 2.4 1
Bromochloromethane ND ug/kg 08/28/15 02:05 74-97-55.9 2.0 1
Bromodichloromethane ND ug/kg 08/28/15 02:05 75-27-45.9 2.3 1
Bromoform ND ug/kg 08/28/15 02:05 75-25-25.9 2.7 1
Bromomethane ND ug/kg 08/28/15 02:05 74-83-911.9 3.0 1
2-Butanone (MEK)ND ug/kg 08/28/15 02:05 78-93-3119 3.4 1
n-Butylbenzene ND ug/kg 08/28/15 02:05 104-51-85.9 2.1 1
sec-Butylbenzene ND ug/kg 08/28/15 02:05 135-98-85.9 1.9 1
tert-Butylbenzene ND ug/kg 08/28/15 02:05 98-06-65.9 2.4 1
Carbon tetrachloride ND ug/kg 08/28/15 02:05 56-23-55.9 3.1 1
Chlorobenzene ND ug/kg 08/28/15 02:05 108-90-75.9 2.3 1
Chloroethane ND ug/kg 08/28/15 02:05 75-00-311.9 2.8 1
Chloroform ND ug/kg 08/28/15 02:05 67-66-35.9 1.9 1
Chloromethane ND ug/kg 08/28/15 02:05 74-87-311.9 2.8 1
2-Chlorotoluene ND ug/kg 08/28/15 02:05 95-49-85.9 2.0 1
4-Chlorotoluene ND ug/kg 08/28/15 02:05 106-43-45.9 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/28/15 02:05 96-12-85.9 4.3 1
Dibromochloromethane ND ug/kg 08/28/15 02:05 124-48-15.9 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/28/15 02:05 106-93-45.9 2.1 1
Dibromomethane ND ug/kg 08/28/15 02:05 74-95-35.9 3.0 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 02:05 95-50-15.9 2.3 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 02:05 541-73-15.9 2.4 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 02:05 106-46-75.9 2.0 1
Dichlorodifluoromethane ND ug/kg 08/28/15 02:05 75-71-811.9 4.3 1
1,1-Dichloroethane ND ug/kg 08/28/15 02:05 75-34-35.9 1.8 1
1,2-Dichloroethane ND ug/kg 08/28/15 02:05 107-06-25.9 2.6 1
1,1-Dichloroethene ND ug/kg 08/28/15 02:05 75-35-45.9 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Sample: SS-2 (6 FT)Lab ID: 92264629002 Collected: 08/21/15 09:09 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 08/28/15 02:05 156-59-25.9 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/28/15 02:05 156-60-55.9 2.3 1
1,2-Dichloropropane ND ug/kg 08/28/15 02:05 78-87-55.9 2.0 1
1,3-Dichloropropane ND ug/kg 08/28/15 02:05 142-28-95.9 2.3 1
2,2-Dichloropropane ND ug/kg 08/28/15 02:05 594-20-75.9 2.0 1
1,1-Dichloropropene ND ug/kg 08/28/15 02:05 563-58-65.9 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/28/15 02:05 10061-01-55.9 2.1 1
trans-1,3-Dichloropropene ND ug/kg 08/28/15 02:05 10061-02-65.9 1.8 1
Diisopropyl ether ND ug/kg 08/28/15 02:05 108-20-35.9 2.0 1
Ethylbenzene ND ug/kg 08/28/15 02:05 100-41-45.9 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 02:05 87-68-35.9 2.4 1
2-Hexanone ND ug/kg 08/28/15 02:05 591-78-659.3 4.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/28/15 02:05 98-82-85.9 2.3 1
p-Isopropyltoluene ND ug/kg 08/28/15 02:05 99-87-65.9 2.0 1
Methylene Chloride 9.6J ug/kg 08/28/15 02:05 75-09-2 B23.7 3.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/28/15 02:05 108-10-159.3 4.4 1
Methyl-tert-butyl ether ND ug/kg 08/28/15 02:05 1634-04-45.9 1.8 1
Naphthalene ND ug/kg 08/28/15 02:05 91-20-35.9 1.4 1
n-Propylbenzene ND ug/kg 08/28/15 02:05 103-65-15.9 2.0 1
Styrene ND ug/kg 08/28/15 02:05 100-42-55.9 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/28/15 02:05 630-20-65.9 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/28/15 02:05 79-34-55.9 2.3 1
Tetrachloroethene ND ug/kg 08/28/15 02:05 127-18-45.9 2.0 1
Toluene ND ug/kg 08/28/15 02:05 108-88-35.9 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 08/28/15 02:05 87-61-65.9 2.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 02:05 120-82-15.9 1.9 1
1,1,1-Trichloroethane ND ug/kg 08/28/15 02:05 71-55-65.9 2.1 1
1,1,2-Trichloroethane ND ug/kg 08/28/15 02:05 79-00-55.9 2.5 1
Trichloroethene ND ug/kg 08/28/15 02:05 79-01-65.9 2.5 1
Trichlorofluoromethane ND ug/kg 08/28/15 02:05 75-69-45.9 2.6 1
1,2,3-Trichloropropane ND ug/kg 08/28/15 02:05 96-18-45.9 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 08/28/15 02:05 95-63-65.9 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 08/28/15 02:05 108-67-85.9 2.1 1
Vinyl acetate ND ug/kg 08/28/15 02:05 108-05-4 L259.3 10.4 1
Vinyl chloride ND ug/kg 08/28/15 02:05 75-01-411.9 2.1 1
Xylene (Total)ND ug/kg 08/28/15 02:05 1330-20-711.9 4.3 1
m&p-Xylene ND ug/kg 08/28/15 02:05 179601-23-111.9 4.3 1
o-Xylene ND ug/kg 08/28/15 02:05 95-47-65.9 2.3 1
Surrogates
Toluene-d8 (S)100 %08/28/15 02:05 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %08/28/15 02:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %08/28/15 02:05 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.5 %08/25/15 12:550.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9780
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1540631
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/25/15 16:13
4-Bromofluorobenzene (S)%104 70-167 08/25/15 16:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1540632LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 50.450 101 70-165
4-Bromofluorobenzene (S)%102 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1540633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
Gas Range Organics (C6-C10)mg/kg 68.167 78 47-18715.6
4-Bromofluorobenzene (S)%93 70-167
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264629002
1540634SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%98 3101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9791
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1544876
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/01/15 16:30
Aliphatic (C09-C12)mg/kg ND 2.5 N209/01/15 16:30
Aromatic (C09-C10)mg/kg ND 2.5 N209/01/15 16:30
4-Bromofluorobenzene (FID) (S)%101 70-130 09/01/15 16:30
4-Bromofluorobenzene (PID) (S)%102 70-130 09/01/15 16:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544877LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1544878
Aliphatic (C05-C08)mg/kg 14.6 N2159770-1309614.5 1 25
Aliphatic (C09-C12)mg/kg 16.1 N21510730-13011116.7 4 25
Aromatic (C09-C10)mg/kg 4.9 N259870-130974.9 1 25
4-Bromofluorobenzene (FID) (S)%103 70-130101
4-Bromofluorobenzene (PID) (S)%103 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33141
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1542838
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,1-Trichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,2-Trichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2,3-Trichloropropane ug/kg ND 5.0 08/27/15 19:28
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/27/15 19:28
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/27/15 19:28
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/27/15 19:28
1,2-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2-Dichloroethane ug/kg ND 5.0 08/27/15 19:28
1,2-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/27/15 19:28
1,3-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,3-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
1,4-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
2,2-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
2-Butanone (MEK)ug/kg ND 100 08/27/15 19:28
2-Chlorotoluene ug/kg ND 5.0 08/27/15 19:28
2-Hexanone ug/kg ND 50.0 08/27/15 19:28
4-Chlorotoluene ug/kg ND 5.0 08/27/15 19:28
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/27/15 19:28
Acetone ug/kg ND 100 08/27/15 19:28
Benzene ug/kg ND 5.0 08/27/15 19:28
Bromobenzene ug/kg ND 5.0 08/27/15 19:28
Bromochloromethane ug/kg ND 5.0 08/27/15 19:28
Bromodichloromethane ug/kg ND 5.0 08/27/15 19:28
Bromoform ug/kg ND 5.0 08/27/15 19:28
Bromomethane ug/kg ND 10.0 08/27/15 19:28
Carbon tetrachloride ug/kg ND 5.0 08/27/15 19:28
Chlorobenzene ug/kg ND 5.0 08/27/15 19:28
Chloroethane ug/kg ND 10.0 08/27/15 19:28
Chloroform ug/kg ND 5.0 08/27/15 19:28
Chloromethane ug/kg ND 10.0 08/27/15 19:28
cis-1,2-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
cis-1,3-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
Dibromochloromethane ug/kg ND 5.0 08/27/15 19:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1542838
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.0 08/27/15 19:28
Dichlorodifluoromethane ug/kg ND 10.0 08/27/15 19:28
Diisopropyl ether ug/kg ND 5.0 08/27/15 19:28
Ethylbenzene ug/kg ND 5.0 08/27/15 19:28
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/27/15 19:28
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/27/15 19:28
m&p-Xylene ug/kg ND 10.0 08/27/15 19:28
Methyl-tert-butyl ether ug/kg ND 5.0 08/27/15 19:28
Methylene Chloride ug/kg 6.0J 20.0 08/27/15 19:28
n-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
n-Propylbenzene ug/kg ND 5.0 08/27/15 19:28
Naphthalene ug/kg ND 5.0 08/27/15 19:28
o-Xylene ug/kg ND 5.0 08/27/15 19:28
p-Isopropyltoluene ug/kg ND 5.0 08/27/15 19:28
sec-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
Styrene ug/kg ND 5.0 08/27/15 19:28
tert-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
Tetrachloroethene ug/kg ND 5.0 08/27/15 19:28
Toluene ug/kg ND 5.0 08/27/15 19:28
trans-1,2-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
trans-1,3-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
Trichloroethene ug/kg ND 5.0 08/27/15 19:28
Trichlorofluoromethane ug/kg ND 5.0 08/27/15 19:28
Vinyl acetate ug/kg ND 50.0 08/27/15 19:28
Vinyl chloride ug/kg ND 10.0 08/27/15 19:28
Xylene (Total)ug/kg ND 10.0 08/27/15 19:28
1,2-Dichloroethane-d4 (S)%104 70-132 08/27/15 19:28
4-Bromofluorobenzene (S)%97 70-130 08/27/15 19:28
Toluene-d8 (S)%101 70-130 08/27/15 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.750 97 74-137
1,1,1-Trichloroethane ug/kg 50.450 101 67-140
1,1,2,2-Tetrachloroethane ug/kg 37.550 75 72-141
1,1,2-Trichloroethane ug/kg 46.350 93 78-138
1,1-Dichloroethane ug/kg 54.350 109 69-134
1,1-Dichloroethene ug/kg 56.150 112 67-138
1,1-Dichloropropene ug/kg 52.550 105 69-139
1,2,3-Trichlorobenzene ug/kg 46.050 92 70-146
1,2,3-Trichloropropane ug/kg 48.550 97 69-144
1,2,4-Trichlorobenzene ug/kg 44.550 89 68-148
1,2,4-Trimethylbenzene ug/kg 49.550 99 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 47.350 95 65-140
1,2-Dibromoethane (EDB)ug/kg 49.950 100 77-135
1,2-Dichlorobenzene ug/kg 48.550 97 77-141
1,2-Dichloroethane ug/kg 48.650 97 65-137
1,2-Dichloropropane ug/kg 47.750 95 72-136
1,3,5-Trimethylbenzene ug/kg 50.550 101 76-133
1,3-Dichlorobenzene ug/kg 48.750 97 74-138
1,3-Dichloropropane ug/kg 47.550 95 71-139
1,4-Dichlorobenzene ug/kg 46.850 94 76-138
2,2-Dichloropropane ug/kg 49.050 98 68-137
2-Butanone (MEK)ug/kg 96.0J100 96 58-147
2-Chlorotoluene ug/kg 46.550 93 73-139
2-Hexanone ug/kg 90.5100 91 62-145
4-Chlorotoluene ug/kg 49.050 98 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 100100 100 64-149
Acetone ug/kg 90.8J100 91 53-153
Benzene ug/kg 50.250 100 73-135
Bromobenzene ug/kg 50.250 100 75-133
Bromochloromethane ug/kg 50.250 100 73-134
Bromodichloromethane ug/kg 50.250 100 71-135
Bromoform ug/kg 44.850 90 66-141
Bromomethane ug/kg 43.650 87 53-160
Carbon tetrachloride ug/kg 50.450 101 60-145
Chlorobenzene ug/kg 49.350 99 78-130
Chloroethane ug/kg 45.350 91 64-149
Chloroform ug/kg 52.550 105 70-134
Chloromethane ug/kg 41.850 84 52-150
cis-1,2-Dichloroethene ug/kg 52.050 104 70-133
cis-1,3-Dichloropropene ug/kg 48.950 98 68-134
Dibromochloromethane ug/kg 48.050 96 71-138
Dibromomethane ug/kg 48.350 97 74-130
Dichlorodifluoromethane ug/kg 42.750 85 40-160
Diisopropyl ether ug/kg 54.150 108 69-141
Ethylbenzene ug/kg 48.650 97 75-133
Hexachloro-1,3-butadiene ug/kg 44.450 89 68-143
Isopropylbenzene (Cumene)ug/kg 52.850 106 76-143
m&p-Xylene ug/kg 97.9100 98 75-136
Methyl-tert-butyl ether ug/kg 47.450 95 68-144
Methylene Chloride ug/kg 47.150 94 45-154
n-Butylbenzene ug/kg 47.850 96 72-137
n-Propylbenzene ug/kg 48.950 98 76-136
Naphthalene ug/kg 47.950 96 68-151
o-Xylene ug/kg 50.050 100 76-141
p-Isopropyltoluene ug/kg 48.750 97 76-140
sec-Butylbenzene ug/kg 51.250 102 79-139
Styrene ug/kg 49.650 99 79-137
tert-Butylbenzene ug/kg 44.150 88 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 45.650 91 71-138
Toluene ug/kg 48.750 97 74-131
trans-1,2-Dichloroethene ug/kg 52.050 104 67-135
trans-1,3-Dichloropropene ug/kg 48.150 96 65-146
Trichloroethene ug/kg 54.250 108 67-135
Trichlorofluoromethane ug/kg 48.350 97 59-144
Vinyl acetate ug/kg 33.3J L010033 40-160
Vinyl chloride ug/kg 45.650 91 56-141
Xylene (Total)ug/kg 148150 99 76-137
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543838MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
1,1,1,2-Tetrachloroethane ug/kg 25.426.7 95 70-130ND
1,1,1-Trichloroethane ug/kg 25.926.7 97 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 28.026.7 105 70-130ND
1,1,2-Trichloroethane ug/kg 27.126.7 101 70-130ND
1,1-Dichloroethane ug/kg 28.226.7 106 70-130ND
1,1-Dichloroethene ug/kg 33.426.7 125 49-180ND
1,1-Dichloropropene ug/kg 30.526.7 114 70-130ND
1,2,3-Trichlorobenzene ug/kg 23.826.7 89 70-130ND
1,2,3-Trichloropropane ug/kg 24.326.7 91 70-130ND
1,2,4-Trichlorobenzene ug/kg 22.326.7 83 70-130ND
1,2,4-Trimethylbenzene ug/kg 27.326.7 101 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 26.426.7 99 70-130ND
1,2-Dibromoethane (EDB)ug/kg 27.026.7 101 70-130ND
1,2-Dichlorobenzene ug/kg 26.926.7 101 70-130ND
1,2-Dichloroethane ug/kg 26.126.7 98 70-130ND
1,2-Dichloropropane ug/kg 29.326.7 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 27.826.7 104 70-130ND
1,3-Dichlorobenzene ug/kg 27.326.7 102 70-130ND
1,3-Dichloropropane ug/kg 27.626.7 103 70-130ND
1,4-Dichlorobenzene ug/kg 26.626.7 99 70-130ND
2,2-Dichloropropane ug/kg 25.726.7 96 70-130ND
2-Butanone (MEK)ug/kg 57.1J53.5 107 70-130ND
2-Chlorotoluene ug/kg 27.426.7 102 70-130ND
2-Hexanone ug/kg 51.4J53.5 96 70-130ND
4-Chlorotoluene ug/kg 28.126.7 105 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 57.8J53.5 108 70-130ND
Acetone ug/kg 76.9J53.5 120 70-130ND
Benzene ug/kg 29.826.7 111 50-166ND
Bromobenzene ug/kg 27.826.7 104 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543838MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
Bromochloromethane ug/kg 29.226.7 109 70-130ND
Bromodichloromethane ug/kg 25.826.7 96 70-130ND
Bromoform ug/kg 21.626.7 81 70-130ND
Bromomethane ug/kg 33.426.7 125 70-130ND
Carbon tetrachloride ug/kg 25.826.7 97 70-130ND
Chlorobenzene ug/kg 27.426.7 103 43-169ND
Chloroethane ug/kg 31.126.7 116 70-130ND
Chloroform ug/kg 28.226.7 106 70-130ND
Chloromethane ug/kg 28.126.7 105 70-130ND
cis-1,2-Dichloroethene ug/kg 29.826.7 111 70-130ND
cis-1,3-Dichloropropene ug/kg 27.126.7 101 70-130ND
Dibromochloromethane ug/kg 23.826.7 89 70-130ND
Dibromomethane ug/kg 26.926.7 100 70-130ND
Dichlorodifluoromethane ug/kg 25.126.7 94 70-130ND
Diisopropyl ether ug/kg 28.026.7 105 70-130ND
Ethylbenzene ug/kg 27.626.7 103 70-130ND
Hexachloro-1,3-butadiene ug/kg 18.926.7 71 70-130ND
Isopropylbenzene (Cumene)ug/kg 29.526.7 110 70-130ND
m&p-Xylene ug/kg 55.053.5 103 70-130ND
Methyl-tert-butyl ether ug/kg 26.626.7 100 70-130ND
Methylene Chloride ug/kg 42.126.7 109 70-13012.8J
n-Butylbenzene ug/kg 26.526.7 99 70-130ND
n-Propylbenzene ug/kg 28.626.7 107 70-130ND
Naphthalene ug/kg 27.226.7 98 70-130ND
o-Xylene ug/kg 27.026.7 101 70-130ND
p-Isopropyltoluene ug/kg 26.226.7 98 70-130ND
sec-Butylbenzene ug/kg 28.726.7 107 70-130ND
Styrene ug/kg 27.826.7 104 70-130ND
tert-Butylbenzene ug/kg 24.026.7 90 70-130ND
Tetrachloroethene ug/kg 24.626.7 92 70-130ND
Toluene ug/kg 28.626.7 106 52-163ND
trans-1,2-Dichloroethene ug/kg 31.026.7 116 70-130ND
trans-1,3-Dichloropropene ug/kg 25.326.7 95 70-130ND
Trichloroethene ug/kg 25.626.7 96 49-167ND
Trichlorofluoromethane ug/kg 26.626.7 99 70-130ND
Vinyl acetate ug/kg 37.6J53.5 70 70-130ND
Vinyl chloride ug/kg 31.126.7 116 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg 52.9J 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 359 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 7.6J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%112 2299
4-Bromofluorobenzene (S)%95 897
Toluene-d8 (S)%104 15100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37366
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1543159
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 08/30/15 06:16
n-Pentacosane (S)%85 41-119 08/30/15 06:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1543160LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 52.766.7 79 49-113
n-Pentacosane (S)%89 41-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543161MATRIX SPIKE SAMPLE:
MSSpike
Result
92264630001
Diesel Range Organics(C10-C28)mg/kg 45.278.9 56 10-146ND
n-Pentacosane (S)%58 41-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264863008
1543162SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 29300 3 3028500
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37328
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1541631
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/28/15 17:03
1,2-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1,3-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1,4-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1-Methylnaphthalene ug/kg ND 330 08/28/15 17:03
2,4,5-Trichlorophenol ug/kg ND 330 08/28/15 17:03
2,4,6-Trichlorophenol ug/kg ND 330 08/28/15 17:03
2,4-Dichlorophenol ug/kg ND 330 08/28/15 17:03
2,4-Dimethylphenol ug/kg ND 330 08/28/15 17:03
2,4-Dinitrophenol ug/kg ND 1650 08/28/15 17:03
2,4-Dinitrotoluene ug/kg ND 330 08/28/15 17:03
2,6-Dinitrotoluene ug/kg ND 330 08/28/15 17:03
2-Chloronaphthalene ug/kg ND 330 08/28/15 17:03
2-Chlorophenol ug/kg ND 330 08/28/15 17:03
2-Methylnaphthalene ug/kg ND 330 08/28/15 17:03
2-Methylphenol(o-Cresol)ug/kg ND 330 08/28/15 17:03
2-Nitroaniline ug/kg ND 1650 08/28/15 17:03
2-Nitrophenol ug/kg ND 330 08/28/15 17:03
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/28/15 17:03
3,3'-Dichlorobenzidine ug/kg ND 1650 08/28/15 17:03
3-Nitroaniline ug/kg ND 1650 08/28/15 17:03
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/28/15 17:03
4-Bromophenylphenyl ether ug/kg ND 330 08/28/15 17:03
4-Chloro-3-methylphenol ug/kg ND 660 08/28/15 17:03
4-Chloroaniline ug/kg ND 1650 08/28/15 17:03
4-Chlorophenylphenyl ether ug/kg ND 330 08/28/15 17:03
4-Nitroaniline ug/kg ND 660 08/28/15 17:03
4-Nitrophenol ug/kg ND 1650 08/28/15 17:03
Acenaphthene ug/kg ND 330 08/28/15 17:03
Acenaphthylene ug/kg ND 330 08/28/15 17:03
Aniline ug/kg ND 330 08/28/15 17:03
Anthracene ug/kg ND 330 08/28/15 17:03
Benzo(a)anthracene ug/kg ND 330 08/28/15 17:03
Benzo(a)pyrene ug/kg ND 330 08/28/15 17:03
Benzo(b)fluoranthene ug/kg ND 330 08/28/15 17:03
Benzo(g,h,i)perylene ug/kg ND 330 08/28/15 17:03
Benzo(k)fluoranthene ug/kg ND 330 08/28/15 17:03
Benzoic Acid ug/kg ND 1650 08/28/15 17:03
Benzyl alcohol ug/kg ND 660 08/28/15 17:03
bis(2-Chloroethoxy)methane ug/kg ND 330 08/28/15 17:03
bis(2-Chloroethyl) ether ug/kg ND 330 08/28/15 17:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1541631
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/28/15 17:03
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/28/15 17:03
Butylbenzylphthalate ug/kg ND 330 08/28/15 17:03
Chrysene ug/kg ND 330 08/28/15 17:03
Di-n-butylphthalate ug/kg ND 330 08/28/15 17:03
Di-n-octylphthalate ug/kg ND 330 08/28/15 17:03
Dibenz(a,h)anthracene ug/kg ND 330 08/28/15 17:03
Dibenzofuran ug/kg ND 330 08/28/15 17:03
Diethylphthalate ug/kg ND 330 08/28/15 17:03
Dimethylphthalate ug/kg ND 330 08/28/15 17:03
Fluoranthene ug/kg ND 330 08/28/15 17:03
Fluorene ug/kg ND 330 08/28/15 17:03
Hexachloro-1,3-butadiene ug/kg ND 330 08/28/15 17:03
Hexachlorobenzene ug/kg ND 330 08/28/15 17:03
Hexachlorocyclopentadiene ug/kg ND 330 08/28/15 17:03
Hexachloroethane ug/kg ND 330 08/28/15 17:03
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/28/15 17:03
Isophorone ug/kg ND 330 08/28/15 17:03
N-Nitroso-di-n-propylamine ug/kg ND 330 08/28/15 17:03
N-Nitrosodimethylamine ug/kg ND 330 08/28/15 17:03
N-Nitrosodiphenylamine ug/kg ND 330 08/28/15 17:03
Naphthalene ug/kg ND 330 08/28/15 17:03
Nitrobenzene ug/kg ND 330 08/28/15 17:03
Pentachlorophenol ug/kg ND 1650 08/28/15 17:03
Phenanthrene ug/kg ND 330 08/28/15 17:03
Phenol ug/kg ND 330 08/28/15 17:03
Pyrene ug/kg ND 330 08/28/15 17:03
2,4,6-Tribromophenol (S)%80 27-110 08/28/15 17:03
2-Fluorobiphenyl (S)%78 30-110 08/28/15 17:03
2-Fluorophenol (S)%75 13-110 08/28/15 17:03
Nitrobenzene-d5 (S)%80 23-110 08/28/15 17:03
Phenol-d6 (S)%73 22-110 08/28/15 17:03
Terphenyl-d14 (S)%98 28-110 08/28/15 17:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13901670 83 36-120
1,2-Dichlorobenzene ug/kg 12901670 77 41-120
1,3-Dichlorobenzene ug/kg 12601670 76 66-120
1,4-Dichlorobenzene ug/kg 13001670 78 42-120
1-Methylnaphthalene ug/kg 13701670 82 40-120
2,4,5-Trichlorophenol ug/kg 13801670 83 37-120
2,4,6-Trichlorophenol ug/kg 14001670 84 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 13501670 81 33-120
2,4-Dimethylphenol ug/kg 13601670 82 36-120
2,4-Dinitrophenol ug/kg 84008330 101 22-121
2,4-Dinitrotoluene ug/kg 14901670 89 60-120
2,6-Dinitrotoluene ug/kg 14701670 88 54-120
2-Chloronaphthalene ug/kg 13201670 79 41-120
2-Chlorophenol ug/kg 13001670 78 39-120
2-Methylnaphthalene ug/kg 13001670 78 26-120
2-Methylphenol(o-Cresol)ug/kg 12001670 72 41-120
2-Nitroaniline ug/kg 27403330 82 45-120
2-Nitrophenol ug/kg 14001670 84 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 11601670 69 35-120
3,3'-Dichlorobenzidine ug/kg 26503330 79 16-125
3-Nitroaniline ug/kg 27303330 82 45-120
4,6-Dinitro-2-methylphenol ug/kg 32303330 97 46-120
4-Bromophenylphenyl ether ug/kg 13101670 79 36-120
4-Chloro-3-methylphenol ug/kg 29503330 89 37-120
4-Chloroaniline ug/kg 23903330 72 35-120
4-Chlorophenylphenyl ether ug/kg 13401670 81 30-120
4-Nitroaniline ug/kg 28403330 85 48-120
4-Nitrophenol ug/kg 77408330 93 43-120
Acenaphthene ug/kg 13301670 80 46-120
Acenaphthylene ug/kg 13701670 82 46-120
Aniline ug/kg 11201670 67 33-120
Anthracene ug/kg 14001670 84 63-120
Benzo(a)anthracene ug/kg 14101670 84 61-120
Benzo(a)pyrene ug/kg 12601670 76 59-120
Benzo(b)fluoranthene ug/kg 12301670 74 55-120
Benzo(g,h,i)perylene ug/kg 11901670 71 57-120
Benzo(k)fluoranthene ug/kg 15301670 92 56-120
Benzoic Acid ug/kg 58708330 70 13-120
Benzyl alcohol ug/kg 24603330 74 34-120
bis(2-Chloroethoxy)methane ug/kg 12801670 77 21-120
bis(2-Chloroethyl) ether ug/kg 11201670 67 25-120
bis(2-Chloroisopropyl) ether ug/kg 11501670 69 13-120
bis(2-Ethylhexyl)phthalate ug/kg 15001670 90 56-123
Butylbenzylphthalate ug/kg 15301670 92 57-120
Chrysene ug/kg 13801670 83 64-120
Di-n-butylphthalate ug/kg 15101670 91 58-120
Di-n-octylphthalate ug/kg 13501670 81 47-121
Dibenz(a,h)anthracene ug/kg 12001670 72 56-120
Dibenzofuran ug/kg 13701670 82 43-120
Diethylphthalate ug/kg 14501670 87 55-120
Dimethylphthalate ug/kg 14001670 84 54-120
Fluoranthene ug/kg 15001670 90 61-120
Fluorene ug/kg 14201670 85 51-120
Hexachloro-1,3-butadiene ug/kg 14301670 86 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15001670 90 53-120
Hexachlorocyclopentadiene ug/kg 14401670 86 18-150
Hexachloroethane ug/kg 13001670 78 39-120
Indeno(1,2,3-cd)pyrene ug/kg 12001670 72 58-120
Isophorone ug/kg 12301670 74 38-120
N-Nitroso-di-n-propylamine ug/kg 11701670 70 30-120
N-Nitrosodimethylamine ug/kg 11401670 69 32-120
N-Nitrosodiphenylamine ug/kg 13101670 79 50-120
Naphthalene ug/kg 13001670 78 38-120
Nitrobenzene ug/kg 12601670 76 37-120
Pentachlorophenol ug/kg 29803330 89 10-120
Phenanthrene ug/kg 13301670 80 62-120
Phenol ug/kg 14001670 84 37-120
Pyrene ug/kg 14601670 88 63-120
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%82 23-110
Phenol-d6 (S)%79 22-110
Terphenyl-d14 (S)%90 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
1,2,4-Trichlorobenzene ug/kg 10701900 56 18-119ND
1,2-Dichlorobenzene ug/kg 11501900 61 50-110ND
1,3-Dichlorobenzene ug/kg 11001900 58 27-110ND
1,4-Dichlorobenzene ug/kg 11301900 60 28-110ND
1-Methylnaphthalene ug/kg 10701900 57 24-116ND
2,4,5-Trichlorophenol ug/kg 11001900 58 28-110ND
2,4,6-Trichlorophenol ug/kg 10801900 57 17-117ND
2,4-Dichlorophenol ug/kg 10201900 54 21-128ND
2,4-Dimethylphenol ug/kg 10101900 53 10-120ND
2,4-Dinitrophenol ug/kg 20809460 22 10-107ND
2,4-Dinitrotoluene ug/kg 12701900 67 36-109ND
2,6-Dinitrotoluene ug/kg 11901900 63 32-110ND
2-Chloronaphthalene ug/kg 10001900 53 30-107ND
2-Chlorophenol ug/kg 11201900 59 14-106ND
2-Methylnaphthalene ug/kg 10301900 54 10-135ND
2-Methylphenol(o-Cresol)ug/kg 9981900 53 10-124ND
2-Nitroaniline ug/kg 22103780 58 26-116ND
2-Nitrophenol ug/kg 10701900 56 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 9841900 52 10-109ND
3,3'-Dichlorobenzidine ug/kg 23403780 62 10-150ND
3-Nitroaniline ug/kg 23603780 62 22-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
4,6-Dinitro-2-methylphenol ug/kg 22203780 59 13-121ND
4-Bromophenylphenyl ether ug/kg 11101900 58 31-109ND
4-Chloro-3-methylphenol ug/kg 23803780 63 13-128ND
4-Chloroaniline ug/kg 1870J3780 49 18-102ND
4-Chlorophenylphenyl ether ug/kg 11101900 58 29-112ND
4-Nitroaniline ug/kg 25103780 66 16-111ND
4-Nitrophenol ug/kg 61009460 64 14-135ND
Acenaphthene ug/kg 10301900 55 26-114ND
Acenaphthylene ug/kg 10501900 55 32-108ND
Aniline ug/kg 9511900 50 10-107ND
Anthracene ug/kg 11801900 62 32-111ND
Benzo(a)anthracene ug/kg 12301900 65 25-117ND
Benzo(a)pyrene ug/kg 10301900 54 25-106ND
Benzo(b)fluoranthene ug/kg 10401900 55 24-110ND
Benzo(g,h,i)perylene ug/kg 9601900 51 19-112ND
Benzo(k)fluoranthene ug/kg 12701900 67 24-114ND
Benzoic Acid ug/kg ND M194600 10-110ND
Benzyl alcohol ug/kg 21203780 56 24-106ND
bis(2-Chloroethoxy)methane ug/kg 9591900 51 13-119ND
bis(2-Chloroethyl) ether ug/kg 9511900 50 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 9961900 53 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 13101900 69 10-125ND
Butylbenzylphthalate ug/kg 13501900 71 18-110ND
Chrysene ug/kg 12001900 64 30-110ND
Di-n-butylphthalate ug/kg 12501900 66 19-112ND
Di-n-octylphthalate ug/kg 12201900 65 17-105ND
Dibenz(a,h)anthracene ug/kg 9751900 52 23-111ND
Dibenzofuran ug/kg 10801900 57 35-103ND
Diethylphthalate ug/kg 12401900 65 27-113ND
Dimethylphthalate ug/kg 11701900 62 26-111ND
Fluoranthene ug/kg 12701900 67 33-109ND
Fluorene ug/kg 11501900 61 32-113ND
Hexachloro-1,3-butadiene ug/kg 10601900 56 16-116ND
Hexachlorobenzene ug/kg 12501900 66 27-120ND
Hexachlorocyclopentadiene ug/kg 9991900 53 10-108ND
Hexachloroethane ug/kg 11401900 60 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 9361900 49 10-122ND
Isophorone ug/kg 9401900 50 28-114ND
N-Nitroso-di-n-propylamine ug/kg 10601900 56 27-113ND
N-Nitrosodimethylamine ug/kg 9661900 51 10-109ND
N-Nitrosodiphenylamine ug/kg 11001900 58 10-128ND
Naphthalene ug/kg 10101900 54 25-110ND
Nitrobenzene ug/kg 9661900 51 18-114ND
Pentachlorophenol ug/kg 24303780 64 10-122ND
Phenanthrene ug/kg 11101900 59 30-114ND
Phenol ug/kg 11701900 62 11-102ND
Pyrene ug/kg 13101900 67 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%50 30-110
2-Fluorophenol (S)%60 13-110
Nitrobenzene-d5 (S)%54 23-110
Phenol-d6 (S)%59 22-110
Terphenyl-d14 (S)%69 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264553001
1541634SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264553001
1541634SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%45 3564
2-Fluorobiphenyl (S)%39 2148
2-Fluorophenol (S)%39 2751
Nitrobenzene-d5 (S)%40 2551
Phenol-d6 (S)%42 1548
Terphenyl-d14 (S)%49 3973
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37282
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1540309
Associated Lab Samples:92264629001, 92264629002
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N208/26/15 00:49
Aliphatic (C19-C36)mg/kg ND 10.0 N208/26/15 00:49
Aromatic (C11-C22)mg/kg ND 10.0 N208/25/15 16:14
2-Bromonaphthalene (S)%81 40-140 08/25/15 16:14
2-Fluorobiphenyl (S)%80 40-140 08/25/15 16:14
Nonatriacontane (S)%77 40-140 08/26/15 00:49
o-Terphenyl (S)%68 40-140 08/25/15 16:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1540310LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1540311
Aliphatic (C09-C18)mg/kg ND N2107440-14071ND 50
Aliphatic (C19-C36)mg/kg 11.2 N213.3 84 40-1407910.6 5 50
Aromatic (C11-C22)mg/kg 22.4 N228.3 79 40-1409226.0 15 50
2-Bromonaphthalene (S)%80 40-14089
2-Fluorobiphenyl (S)%86 40-14095
Nonatriacontane (S)%81 40-14079
o-Terphenyl (S)%74 40-14088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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Page 31 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8286
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92264629001, 92264629002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264629001
1540420SAMPLE DUPLICATE:
Percent Moisture %15.8 8 2514.6
REPORT OF LABORATORY ANALYSIS
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Eden, NC 27288
[phone]
Page 32 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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Eden, NC 27288
[phone]
Page 33 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92264629
SUNCAP 1328 OLD GREENSBORO RD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92264629001 OEXT/37366 GCSV/22429SS-1 (8.5 FT)EPA 3546 EPA 8015 Modified
92264629002 OEXT/37366 GCSV/22429SS-2 (6 FT)EPA 3546 EPA 8015 Modified
92264629001 OEXT/37282 GCSV/22403SS-1 (8.5 FT)MADEP EPH MADEP EPH
92264629002 OEXT/37282 GCSV/22403SS-2 (6 FT)MADEP EPH MADEP EPH
92264629001 GCV/9780 GCV/9781SS-1 (8.5 FT)EPA 5035A/5030B EPA 8015 Modified
92264629002 GCV/9780 GCV/9781SS-2 (6 FT)EPA 5035A/5030B EPA 8015 Modified
92264629001 GCV/9791 GCV/9799SS-1 (8.5 FT)MADEP VPH MADEP VPH
92264629002 GCV/9791 GCV/9799SS-2 (6 FT)MADEP VPH MADEP VPH
92264629001 OEXT/37328 MSSV/11156SS-1 (8.5 FT)EPA 3546 EPA 8270
92264629002 OEXT/37328 MSSV/11156SS-2 (6 FT)EPA 3546 EPA 8270
92264629001 MSV/33141SS-1 (8.5 FT)EPA 8260
92264629002 MSV/33141SS-2 (6 FT)EPA 8260
92264629001 PMST/8286SS-1 (8.5 FT)ASTM D2974-87
92264629002 PMST/8286SS-2 (6 FT)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 34 of 36
Page 35 of 36
Page 36 of 36
#=CL#
September 02, 2015
LIMS USE: FR - TROY SHELTON
LIMS OBJECT ID: 92264630
92264630
Project:
Pace Project No.:
RE:
Troy Shelton
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, VA 24540
SUNCAP 1404 Old Greensboro Rd
Dear Troy Shelton:
Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Lab ID Sample ID Matrix Date Collected Date Received
92264630001 SS-3 (14FT)Solid 08/21/15 12:16 08/24/15 13:00
92264630002 SS-4 (14FT)Solid 08/21/15 11:34 08/24/15 13:00
REPORT OF LABORATORY ANALYSIS
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Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92264630001 SS-3 (14FT)EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92264630002 SS-4 (14FT)EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 36
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92264630001 SS-3 (14FT)
Methylene Chloride 9.6J ug/kg 08/28/15 02:25 B27.7EPA 8260
Percent Moisture 15.5 %08/25/15 12:550.10ASTM D2974-87
92264630002 SS-4 (14FT)
Diesel Range Organics(C10-C28)24.5 mg/kg 08/30/15 07:275.7EPA 8015 Modified
Aliphatic (C09-C18)19.2 mg/kg 08/26/15 23:33 N211.4MADEP EPH
Methylene Chloride 10.9J ug/kg 08/28/15 02:45 B24.1EPA 8260
Percent Moisture 12.6 %08/25/15 12:550.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-3 (14FT)Lab ID: 92264630001 Collected: 08/21/15 12:16 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/30/15 07:0308/27/15 16:305.9 5.3 1
Surrogates
n-Pentacosane (S)79 %08/30/15 07:03 629-99-208/27/15 16:3041-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/26/15 23:01 N208/24/15 15:1811.8 11.8 1
Aliphatic (C19-C36)ND mg/kg 08/26/15 23:01 N208/24/15 15:1811.8 11.8 1
Aromatic (C11-C22)ND mg/kg 08/27/15 06:30 N208/24/15 15:1811.8 11.8 1
Surrogates
Nonatriacontane (S)63 %08/26/15 23:01 7194-86-708/24/15 15:1840-140 1
o-Terphenyl (S)71 %08/27/15 06:30 84-15-108/24/15 15:1840-140 1
2-Fluorobiphenyl (S)80 %08/27/15 06:30 321-60-808/24/15 15:1840-140 1
2-Bromonaphthalene (S)81 %08/27/15 06:30 580-13-208/24/15 15:1840-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/25/15 18:0508/25/15 11:037.9 7.9 1
Surrogates
4-Bromofluorobenzene (S)96 %08/25/15 18:05 460-00-408/25/15 11:0370-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/01/15 23:31 N208/31/15 09:223.7 3.7 1
Aliphatic (C09-C12)ND mg/kg 09/01/15 23:31 N208/31/15 09:223.7 3.7 1
Aromatic (C09-C10)ND mg/kg 09/01/15 23:31 N208/31/15 09:223.7 3.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %09/01/15 23:31 460-00-408/31/15 09:2270-130 1
4-Bromofluorobenzene (PID) (S)109 %09/01/15 23:31 460-00-408/31/15 09:2270-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 08/28/15 20:42 83-32-908/26/15 09:35391 90.0 1
Acenaphthylene ND ug/kg 08/28/15 20:42 208-96-808/26/15 09:35391 92.3 1
Aniline ND ug/kg 08/28/15 20:42 62-53-308/26/15 09:35391 105 1
Anthracene ND ug/kg 08/28/15 20:42 120-12-708/26/15 09:35391 87.6 1
Benzo(a)anthracene ND ug/kg 08/28/15 20:42 56-55-308/26/15 09:35391 72.2 1
Benzo(a)pyrene ND ug/kg 08/28/15 20:42 50-32-808/26/15 09:35391 74.6 1
Benzo(b)fluoranthene ND ug/kg 08/28/15 20:42 205-99-208/26/15 09:35391 67.5 1
Benzo(g,h,i)perylene ND ug/kg 08/28/15 20:42 191-24-208/26/15 09:35391 99.4 1
Benzo(k)fluoranthene ND ug/kg 08/28/15 20:42 207-08-908/26/15 09:35391 76.9 1
Benzoic Acid ND ug/kg 08/28/15 20:42 65-85-008/26/15 09:351950 71.0 1
Benzyl alcohol ND ug/kg 08/28/15 20:42 100-51-608/26/15 09:35781 78.1 1
4-Bromophenylphenyl ether ND ug/kg 08/28/15 20:42 101-55-308/26/15 09:35391 71.0 1
Butylbenzylphthalate ND ug/kg 08/28/15 20:42 85-68-708/26/15 09:35391 82.9 1
4-Chloro-3-methylphenol ND ug/kg 08/28/15 20:42 59-50-708/26/15 09:35781 80.5 1
4-Chloroaniline ND ug/kg 08/28/15 20:42 106-47-808/26/15 09:351950 109 1
bis(2-Chloroethoxy)methane ND ug/kg 08/28/15 20:42 111-91-108/26/15 09:35391 91.1 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-3 (14FT)Lab ID: 92264630001 Collected: 08/21/15 12:16 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 08/28/15 20:42 111-44-408/26/15 09:35391 99.4 1
bis(2-Chloroisopropyl) ether ND ug/kg 08/28/15 20:42 108-60-108/26/15 09:35391 104 1
2-Chloronaphthalene ND ug/kg 08/28/15 20:42 91-58-708/26/15 09:35391 76.9 1
2-Chlorophenol ND ug/kg 08/28/15 20:42 95-57-808/26/15 09:35391 107 1
4-Chlorophenylphenyl ether ND ug/kg 08/28/15 20:42 7005-72-308/26/15 09:35391 80.5 1
Chrysene ND ug/kg 08/28/15 20:42 218-01-908/26/15 09:35391 52.1 1
Dibenz(a,h)anthracene ND ug/kg 08/28/15 20:42 53-70-308/26/15 09:35391 82.9 1
Dibenzofuran ND ug/kg 08/28/15 20:42 132-64-908/26/15 09:35391 63.9 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 20:42 95-50-108/26/15 09:35391 104 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 20:42 541-73-108/26/15 09:35391 88.8 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 20:42 106-46-708/26/15 09:35391 110 1
3,3'-Dichlorobenzidine ND ug/kg 08/28/15 20:42 91-94-108/26/15 09:351950 85.2 1
2,4-Dichlorophenol ND ug/kg 08/28/15 20:42 120-83-208/26/15 09:35391 85.2 1
Diethylphthalate ND ug/kg 08/28/15 20:42 84-66-208/26/15 09:35391 60.4 1
2,4-Dimethylphenol ND ug/kg 08/28/15 20:42 105-67-908/26/15 09:35391 154 1
Dimethylphthalate ND ug/kg 08/28/15 20:42 131-11-308/26/15 09:35391 79.3 1
Di-n-butylphthalate ND ug/kg 08/28/15 20:42 84-74-208/26/15 09:35391 63.9 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/28/15 20:42 534-52-108/26/15 09:35781 78.1 1
2,4-Dinitrophenol ND ug/kg 08/28/15 20:42 51-28-508/26/15 09:351950 63.9 1
2,4-Dinitrotoluene ND ug/kg 08/28/15 20:42 121-14-208/26/15 09:35391 73.4 1
2,6-Dinitrotoluene ND ug/kg 08/28/15 20:42 606-20-208/26/15 09:35391 81.7 1
Di-n-octylphthalate ND ug/kg 08/28/15 20:42 117-84-008/26/15 09:35391 81.7 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/28/15 20:42 117-81-708/26/15 09:35391 107 1
Fluoranthene ND ug/kg 08/28/15 20:42 206-44-008/26/15 09:35391 56.8 1
Fluorene ND ug/kg 08/28/15 20:42 86-73-708/26/15 09:35391 80.5 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 20:42 87-68-308/26/15 09:35391 67.5 1
Hexachlorobenzene ND ug/kg 08/28/15 20:42 118-74-108/26/15 09:35391 49.7 1
Hexachlorocyclopentadiene ND ug/kg 08/28/15 20:42 77-47-408/26/15 09:35391 72.2 1
Hexachloroethane ND ug/kg 08/28/15 20:42 67-72-108/26/15 09:35391 103 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/28/15 20:42 193-39-508/26/15 09:35391 80.5 1
Isophorone ND ug/kg 08/28/15 20:42 78-59-108/26/15 09:35391 87.6 1
1-Methylnaphthalene ND ug/kg 08/28/15 20:42 90-12-008/26/15 09:35391 102 1
2-Methylnaphthalene ND ug/kg 08/28/15 20:42 91-57-608/26/15 09:35391 84.0 1
2-Methylphenol(o-Cresol)ND ug/kg 08/28/15 20:42 95-48-708/26/15 09:35391 118 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/28/15 20:4208/26/15 09:35391 154 1
Naphthalene ND ug/kg 08/28/15 20:42 91-20-308/26/15 09:35391 95.9 1
2-Nitroaniline ND ug/kg 08/28/15 20:42 88-74-408/26/15 09:351950 121 1
3-Nitroaniline ND ug/kg 08/28/15 20:42 99-09-208/26/15 09:351950 107 1
4-Nitroaniline ND ug/kg 08/28/15 20:42 100-01-608/26/15 09:35781 110 1
Nitrobenzene ND ug/kg 08/28/15 20:42 98-95-308/26/15 09:35391 107 1
2-Nitrophenol ND ug/kg 08/28/15 20:42 88-75-508/26/15 09:35391 94.7 1
4-Nitrophenol ND ug/kg 08/28/15 20:42 100-02-708/26/15 09:351950 69.8 1
N-Nitrosodimethylamine ND ug/kg 08/28/15 20:42 62-75-908/26/15 09:35391 127 1
N-Nitroso-di-n-propylamine ND ug/kg 08/28/15 20:42 621-64-708/26/15 09:35391 74.6 1
N-Nitrosodiphenylamine ND ug/kg 08/28/15 20:42 86-30-608/26/15 09:35391 116 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-3 (14FT)Lab ID: 92264630001 Collected: 08/21/15 12:16 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 08/28/15 20:42 87-86-508/26/15 09:351950 71.0 1
Phenanthrene ND ug/kg 08/28/15 20:42 85-01-808/26/15 09:35391 65.1 1
Phenol ND ug/kg 08/28/15 20:42 108-95-208/26/15 09:35391 117 1
Pyrene ND ug/kg 08/28/15 20:42 129-00-008/26/15 09:35391 66.3 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 20:42 120-82-108/26/15 09:35391 75.8 1
2,4,5-Trichlorophenol ND ug/kg 08/28/15 20:42 95-95-408/26/15 09:35391 121 1
2,4,6-Trichlorophenol ND ug/kg 08/28/15 20:42 88-06-208/26/15 09:35391 86.4 1
Surrogates
Nitrobenzene-d5 (S)42 %08/28/15 20:42 4165-60-008/26/15 09:3523-110 1
2-Fluorobiphenyl (S)34 %08/28/15 20:42 321-60-808/26/15 09:3530-110 1
Terphenyl-d14 (S)46 %08/28/15 20:42 1718-51-008/26/15 09:3528-110 1
Phenol-d6 (S)41 %08/28/15 20:42 13127-88-308/26/15 09:3522-110 1
2-Fluorophenol (S)42 %08/28/15 20:42 367-12-408/26/15 09:3513-110 1
2,4,6-Tribromophenol (S)37 %08/28/15 20:42 118-79-608/26/15 09:3527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/28/15 02:25 67-64-1139 13.9 1
Benzene ND ug/kg 08/28/15 02:25 71-43-26.9 2.2 1
Bromobenzene ND ug/kg 08/28/15 02:25 108-86-16.9 2.8 1
Bromochloromethane ND ug/kg 08/28/15 02:25 74-97-56.9 2.4 1
Bromodichloromethane ND ug/kg 08/28/15 02:25 75-27-46.9 2.6 1
Bromoform ND ug/kg 08/28/15 02:25 75-25-26.9 3.2 1
Bromomethane ND ug/kg 08/28/15 02:25 74-83-913.9 3.5 1
2-Butanone (MEK)ND ug/kg 08/28/15 02:25 78-93-3139 4.0 1
n-Butylbenzene ND ug/kg 08/28/15 02:25 104-51-86.9 2.5 1
sec-Butylbenzene ND ug/kg 08/28/15 02:25 135-98-86.9 2.2 1
tert-Butylbenzene ND ug/kg 08/28/15 02:25 98-06-66.9 2.8 1
Carbon tetrachloride ND ug/kg 08/28/15 02:25 56-23-56.9 3.6 1
Chlorobenzene ND ug/kg 08/28/15 02:25 108-90-76.9 2.6 1
Chloroethane ND ug/kg 08/28/15 02:25 75-00-313.9 3.3 1
Chloroform ND ug/kg 08/28/15 02:25 67-66-36.9 2.2 1
Chloromethane ND ug/kg 08/28/15 02:25 74-87-313.9 3.3 1
2-Chlorotoluene ND ug/kg 08/28/15 02:25 95-49-86.9 2.4 1
4-Chlorotoluene ND ug/kg 08/28/15 02:25 106-43-46.9 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/28/15 02:25 96-12-86.9 5.0 1
Dibromochloromethane ND ug/kg 08/28/15 02:25 124-48-16.9 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/28/15 02:25 106-93-46.9 2.5 1
Dibromomethane ND ug/kg 08/28/15 02:25 74-95-36.9 3.5 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 02:25 95-50-16.9 2.6 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 02:25 541-73-16.9 2.8 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 02:25 106-46-76.9 2.4 1
Dichlorodifluoromethane ND ug/kg 08/28/15 02:25 75-71-813.9 5.0 1
1,1-Dichloroethane ND ug/kg 08/28/15 02:25 75-34-36.9 2.1 1
1,2-Dichloroethane ND ug/kg 08/28/15 02:25 107-06-26.9 3.0 1
1,1-Dichloroethene ND ug/kg 08/28/15 02:25 75-35-46.9 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-3 (14FT)Lab ID: 92264630001 Collected: 08/21/15 12:16 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 08/28/15 02:25 156-59-26.9 1.9 1
trans-1,2-Dichloroethene ND ug/kg 08/28/15 02:25 156-60-56.9 2.6 1
1,2-Dichloropropane ND ug/kg 08/28/15 02:25 78-87-56.9 2.4 1
1,3-Dichloropropane ND ug/kg 08/28/15 02:25 142-28-96.9 2.6 1
2,2-Dichloropropane ND ug/kg 08/28/15 02:25 594-20-76.9 2.4 1
1,1-Dichloropropene ND ug/kg 08/28/15 02:25 563-58-66.9 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/28/15 02:25 10061-01-56.9 2.5 1
trans-1,3-Dichloropropene ND ug/kg 08/28/15 02:25 10061-02-66.9 2.1 1
Diisopropyl ether ND ug/kg 08/28/15 02:25 108-20-36.9 2.4 1
Ethylbenzene ND ug/kg 08/28/15 02:25 100-41-46.9 2.5 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 02:25 87-68-36.9 2.8 1
2-Hexanone ND ug/kg 08/28/15 02:25 591-78-669.3 5.4 1
Isopropylbenzene (Cumene)ND ug/kg 08/28/15 02:25 98-82-86.9 2.6 1
p-Isopropyltoluene ND ug/kg 08/28/15 02:25 99-87-66.9 2.4 1
Methylene Chloride 9.6J ug/kg 08/28/15 02:25 75-09-2 B27.7 4.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/28/15 02:25 108-10-169.3 5.1 1
Methyl-tert-butyl ether ND ug/kg 08/28/15 02:25 1634-04-46.9 2.1 1
Naphthalene ND ug/kg 08/28/15 02:25 91-20-36.9 1.7 1
n-Propylbenzene ND ug/kg 08/28/15 02:25 103-65-16.9 2.4 1
Styrene ND ug/kg 08/28/15 02:25 100-42-56.9 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/28/15 02:25 630-20-66.9 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/28/15 02:25 79-34-56.9 2.6 1
Tetrachloroethene ND ug/kg 08/28/15 02:25 127-18-46.9 2.4 1
Toluene ND ug/kg 08/28/15 02:25 108-88-36.9 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/28/15 02:25 87-61-66.9 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 02:25 120-82-16.9 2.2 1
1,1,1-Trichloroethane ND ug/kg 08/28/15 02:25 71-55-66.9 2.5 1
1,1,2-Trichloroethane ND ug/kg 08/28/15 02:25 79-00-56.9 2.9 1
Trichloroethene ND ug/kg 08/28/15 02:25 79-01-66.9 2.9 1
Trichlorofluoromethane ND ug/kg 08/28/15 02:25 75-69-46.9 3.0 1
1,2,3-Trichloropropane ND ug/kg 08/28/15 02:25 96-18-46.9 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/28/15 02:25 95-63-66.9 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/28/15 02:25 108-67-86.9 2.5 1
Vinyl acetate ND ug/kg 08/28/15 02:25 108-05-4 L269.3 12.2 1
Vinyl chloride ND ug/kg 08/28/15 02:25 75-01-413.9 2.5 1
Xylene (Total)ND ug/kg 08/28/15 02:25 1330-20-713.9 5.0 1
m&p-Xylene ND ug/kg 08/28/15 02:25 179601-23-113.9 5.0 1
o-Xylene ND ug/kg 08/28/15 02:25 95-47-66.9 2.6 1
Surrogates
Toluene-d8 (S)101 %08/28/15 02:25 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %08/28/15 02:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %08/28/15 02:25 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.5 %08/25/15 12:550.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-4 (14FT)Lab ID: 92264630002 Collected: 08/21/15 11:34 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)24.5 mg/kg 08/30/15 07:2708/27/15 16:305.7 5.1 1
Surrogates
n-Pentacosane (S)57 %08/30/15 07:27 629-99-208/27/15 16:3041-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)19.2 mg/kg 08/26/15 23:33 N208/24/15 15:1811.4 11.4 1
Aliphatic (C19-C36)ND mg/kg 08/26/15 23:33 N208/24/15 15:1811.4 11.4 1
Aromatic (C11-C22)ND mg/kg 08/27/15 07:02 N208/24/15 15:1811.4 11.4 1
Surrogates
Nonatriacontane (S)78 %08/26/15 23:33 7194-86-708/24/15 15:1840-140 1
o-Terphenyl (S)88 %08/27/15 07:02 84-15-108/24/15 15:1840-140 1
2-Fluorobiphenyl (S)94 %08/27/15 07:02 321-60-808/24/15 15:1840-140 1
2-Bromonaphthalene (S)104 %08/27/15 07:02 580-13-208/24/15 15:1840-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/25/15 18:2708/25/15 11:039.3 9.3 1
Surrogates
4-Bromofluorobenzene (S)102 %08/25/15 18:27 460-00-408/25/15 11:0370-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/02/15 00:01 N208/31/15 09:224.0 4.0 1
Aliphatic (C09-C12)ND mg/kg 09/02/15 00:01 N208/31/15 09:224.0 4.0 1
Aromatic (C09-C10)ND mg/kg 09/02/15 00:01 N208/31/15 09:224.0 4.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)105 %09/02/15 00:01 460-00-408/31/15 09:2270-130 1
4-Bromofluorobenzene (PID) (S)106 %09/02/15 00:01 460-00-408/31/15 09:2270-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 08/28/15 21:09 83-32-908/26/15 09:35377 86.9 1
Acenaphthylene ND ug/kg 08/28/15 21:09 208-96-808/26/15 09:35377 89.2 1
Aniline ND ug/kg 08/28/15 21:09 62-53-308/26/15 09:35377 102 1
Anthracene ND ug/kg 08/28/15 21:09 120-12-708/26/15 09:35377 84.6 1
Benzo(a)anthracene ND ug/kg 08/28/15 21:09 56-55-308/26/15 09:35377 69.8 1
Benzo(a)pyrene ND ug/kg 08/28/15 21:09 50-32-808/26/15 09:35377 72.0 1
Benzo(b)fluoranthene ND ug/kg 08/28/15 21:09 205-99-208/26/15 09:35377 65.2 1
Benzo(g,h,i)perylene ND ug/kg 08/28/15 21:09 191-24-208/26/15 09:35377 96.1 1
Benzo(k)fluoranthene ND ug/kg 08/28/15 21:09 207-08-908/26/15 09:35377 74.3 1
Benzoic Acid ND ug/kg 08/28/15 21:09 65-85-008/26/15 09:351890 68.6 1
Benzyl alcohol ND ug/kg 08/28/15 21:09 100-51-608/26/15 09:35755 75.5 1
4-Bromophenylphenyl ether ND ug/kg 08/28/15 21:09 101-55-308/26/15 09:35377 68.6 1
Butylbenzylphthalate ND ug/kg 08/28/15 21:09 85-68-708/26/15 09:35377 80.0 1
4-Chloro-3-methylphenol ND ug/kg 08/28/15 21:09 59-50-708/26/15 09:35755 77.8 1
4-Chloroaniline ND ug/kg 08/28/15 21:09 106-47-808/26/15 09:351890 105 1
bis(2-Chloroethoxy)methane ND ug/kg 08/28/15 21:09 111-91-108/26/15 09:35377 88.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-4 (14FT)Lab ID: 92264630002 Collected: 08/21/15 11:34 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 08/28/15 21:09 111-44-408/26/15 09:35377 96.1 1
bis(2-Chloroisopropyl) ether ND ug/kg 08/28/15 21:09 108-60-108/26/15 09:35377 101 1
2-Chloronaphthalene ND ug/kg 08/28/15 21:09 91-58-708/26/15 09:35377 74.3 1
2-Chlorophenol ND ug/kg 08/28/15 21:09 95-57-808/26/15 09:35377 103 1
4-Chlorophenylphenyl ether ND ug/kg 08/28/15 21:09 7005-72-308/26/15 09:35377 77.8 1
Chrysene ND ug/kg 08/28/15 21:09 218-01-908/26/15 09:35377 50.3 1
Dibenz(a,h)anthracene ND ug/kg 08/28/15 21:09 53-70-308/26/15 09:35377 80.0 1
Dibenzofuran ND ug/kg 08/28/15 21:09 132-64-908/26/15 09:35377 61.7 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 21:09 95-50-108/26/15 09:35377 101 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 21:09 541-73-108/26/15 09:35377 85.8 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 21:09 106-46-708/26/15 09:35377 106 1
3,3'-Dichlorobenzidine ND ug/kg 08/28/15 21:09 91-94-108/26/15 09:351890 82.3 1
2,4-Dichlorophenol ND ug/kg 08/28/15 21:09 120-83-208/26/15 09:35377 82.3 1
Diethylphthalate ND ug/kg 08/28/15 21:09 84-66-208/26/15 09:35377 58.3 1
2,4-Dimethylphenol ND ug/kg 08/28/15 21:09 105-67-908/26/15 09:35377 149 1
Dimethylphthalate ND ug/kg 08/28/15 21:09 131-11-308/26/15 09:35377 76.6 1
Di-n-butylphthalate ND ug/kg 08/28/15 21:09 84-74-208/26/15 09:35377 61.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/28/15 21:09 534-52-108/26/15 09:35755 75.5 1
2,4-Dinitrophenol ND ug/kg 08/28/15 21:09 51-28-508/26/15 09:351890 61.7 1
2,4-Dinitrotoluene ND ug/kg 08/28/15 21:09 121-14-208/26/15 09:35377 70.9 1
2,6-Dinitrotoluene ND ug/kg 08/28/15 21:09 606-20-208/26/15 09:35377 78.9 1
Di-n-octylphthalate ND ug/kg 08/28/15 21:09 117-84-008/26/15 09:35377 78.9 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/28/15 21:09 117-81-708/26/15 09:35377 103 1
Fluoranthene ND ug/kg 08/28/15 21:09 206-44-008/26/15 09:35377 54.9 1
Fluorene ND ug/kg 08/28/15 21:09 86-73-708/26/15 09:35377 77.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 21:09 87-68-308/26/15 09:35377 65.2 1
Hexachlorobenzene ND ug/kg 08/28/15 21:09 118-74-108/26/15 09:35377 48.0 1
Hexachlorocyclopentadiene ND ug/kg 08/28/15 21:09 77-47-408/26/15 09:35377 69.8 1
Hexachloroethane ND ug/kg 08/28/15 21:09 67-72-108/26/15 09:35377 99.5 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/28/15 21:09 193-39-508/26/15 09:35377 77.8 1
Isophorone ND ug/kg 08/28/15 21:09 78-59-108/26/15 09:35377 84.6 1
1-Methylnaphthalene ND ug/kg 08/28/15 21:09 90-12-008/26/15 09:35377 98.3 1
2-Methylnaphthalene ND ug/kg 08/28/15 21:09 91-57-608/26/15 09:35377 81.2 1
2-Methylphenol(o-Cresol)ND ug/kg 08/28/15 21:09 95-48-708/26/15 09:35377 114 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/28/15 21:0908/26/15 09:35377 149 1
Naphthalene ND ug/kg 08/28/15 21:09 91-20-308/26/15 09:35377 92.6 1
2-Nitroaniline ND ug/kg 08/28/15 21:09 88-74-408/26/15 09:351890 117 1
3-Nitroaniline ND ug/kg 08/28/15 21:09 99-09-208/26/15 09:351890 103 1
4-Nitroaniline ND ug/kg 08/28/15 21:09 100-01-608/26/15 09:35755 106 1
Nitrobenzene ND ug/kg 08/28/15 21:09 98-95-308/26/15 09:35377 103 1
2-Nitrophenol ND ug/kg 08/28/15 21:09 88-75-508/26/15 09:35377 91.5 1
4-Nitrophenol ND ug/kg 08/28/15 21:09 100-02-708/26/15 09:351890 67.5 1
N-Nitrosodimethylamine ND ug/kg 08/28/15 21:09 62-75-908/26/15 09:35377 122 1
N-Nitroso-di-n-propylamine ND ug/kg 08/28/15 21:09 621-64-708/26/15 09:35377 72.0 1
N-Nitrosodiphenylamine ND ug/kg 08/28/15 21:09 86-30-608/26/15 09:35377 112 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-4 (14FT)Lab ID: 92264630002 Collected: 08/21/15 11:34 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 08/28/15 21:09 87-86-508/26/15 09:351890 68.6 1
Phenanthrene ND ug/kg 08/28/15 21:09 85-01-808/26/15 09:35377 62.9 1
Phenol ND ug/kg 08/28/15 21:09 108-95-208/26/15 09:35377 113 1
Pyrene ND ug/kg 08/28/15 21:09 129-00-008/26/15 09:35377 64.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 21:09 120-82-108/26/15 09:35377 73.2 1
2,4,5-Trichlorophenol ND ug/kg 08/28/15 21:09 95-95-408/26/15 09:35377 117 1
2,4,6-Trichlorophenol ND ug/kg 08/28/15 21:09 88-06-208/26/15 09:35377 83.5 1
Surrogates
Nitrobenzene-d5 (S)49 %08/28/15 21:09 4165-60-008/26/15 09:3523-110 1
2-Fluorobiphenyl (S)42 %08/28/15 21:09 321-60-808/26/15 09:3530-110 1
Terphenyl-d14 (S)55 %08/28/15 21:09 1718-51-008/26/15 09:3528-110 1
Phenol-d6 (S)41 %08/28/15 21:09 13127-88-308/26/15 09:3522-110 1
2-Fluorophenol (S)45 %08/28/15 21:09 367-12-408/26/15 09:3513-110 1
2,4,6-Tribromophenol (S)50 %08/28/15 21:09 118-79-608/26/15 09:3527-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 08/28/15 02:45 67-64-1120 12.0 1
Benzene ND ug/kg 08/28/15 02:45 71-43-26.0 1.9 1
Bromobenzene ND ug/kg 08/28/15 02:45 108-86-16.0 2.4 1
Bromochloromethane ND ug/kg 08/28/15 02:45 74-97-56.0 2.0 1
Bromodichloromethane ND ug/kg 08/28/15 02:45 75-27-46.0 2.3 1
Bromoform ND ug/kg 08/28/15 02:45 75-25-26.0 2.8 1
Bromomethane ND ug/kg 08/28/15 02:45 74-83-912.0 3.0 1
2-Butanone (MEK)ND ug/kg 08/28/15 02:45 78-93-3120 3.5 1
n-Butylbenzene ND ug/kg 08/28/15 02:45 104-51-86.0 2.2 1
sec-Butylbenzene ND ug/kg 08/28/15 02:45 135-98-86.0 1.9 1
tert-Butylbenzene ND ug/kg 08/28/15 02:45 98-06-66.0 2.4 1
Carbon tetrachloride ND ug/kg 08/28/15 02:45 56-23-56.0 3.1 1
Chlorobenzene ND ug/kg 08/28/15 02:45 108-90-76.0 2.3 1
Chloroethane ND ug/kg 08/28/15 02:45 75-00-312.0 2.9 1
Chloroform ND ug/kg 08/28/15 02:45 67-66-36.0 1.9 1
Chloromethane ND ug/kg 08/28/15 02:45 74-87-312.0 2.9 1
2-Chlorotoluene ND ug/kg 08/28/15 02:45 95-49-86.0 2.0 1
4-Chlorotoluene ND ug/kg 08/28/15 02:45 106-43-46.0 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/28/15 02:45 96-12-86.0 4.3 1
Dibromochloromethane ND ug/kg 08/28/15 02:45 124-48-16.0 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 08/28/15 02:45 106-93-46.0 2.2 1
Dibromomethane ND ug/kg 08/28/15 02:45 74-95-36.0 3.0 1
1,2-Dichlorobenzene ND ug/kg 08/28/15 02:45 95-50-16.0 2.3 1
1,3-Dichlorobenzene ND ug/kg 08/28/15 02:45 541-73-16.0 2.4 1
1,4-Dichlorobenzene ND ug/kg 08/28/15 02:45 106-46-76.0 2.0 1
Dichlorodifluoromethane ND ug/kg 08/28/15 02:45 75-71-812.0 4.3 1
1,1-Dichloroethane ND ug/kg 08/28/15 02:45 75-34-36.0 1.8 1
1,2-Dichloroethane ND ug/kg 08/28/15 02:45 107-06-26.0 2.6 1
1,1-Dichloroethene ND ug/kg 08/28/15 02:45 75-35-46.0 2.2 1
REPORT OF LABORATORY ANALYSIS
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Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Sample: SS-4 (14FT)Lab ID: 92264630002 Collected: 08/21/15 11:34 Received: 08/24/15 13:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 08/28/15 02:45 156-59-26.0 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/28/15 02:45 156-60-56.0 2.3 1
1,2-Dichloropropane ND ug/kg 08/28/15 02:45 78-87-56.0 2.0 1
1,3-Dichloropropane ND ug/kg 08/28/15 02:45 142-28-96.0 2.3 1
2,2-Dichloropropane ND ug/kg 08/28/15 02:45 594-20-76.0 2.0 1
1,1-Dichloropropene ND ug/kg 08/28/15 02:45 563-58-66.0 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/28/15 02:45 10061-01-56.0 2.2 1
trans-1,3-Dichloropropene ND ug/kg 08/28/15 02:45 10061-02-66.0 1.8 1
Diisopropyl ether ND ug/kg 08/28/15 02:45 108-20-36.0 2.0 1
Ethylbenzene ND ug/kg 08/28/15 02:45 100-41-46.0 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 08/28/15 02:45 87-68-36.0 2.4 1
2-Hexanone ND ug/kg 08/28/15 02:45 591-78-660.2 4.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/28/15 02:45 98-82-86.0 2.3 1
p-Isopropyltoluene ND ug/kg 08/28/15 02:45 99-87-66.0 2.0 1
Methylene Chloride 10.9J ug/kg 08/28/15 02:45 75-09-2 B24.1 3.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/28/15 02:45 108-10-160.2 4.5 1
Methyl-tert-butyl ether ND ug/kg 08/28/15 02:45 1634-04-46.0 1.8 1
Naphthalene ND ug/kg 08/28/15 02:45 91-20-36.0 1.4 1
n-Propylbenzene ND ug/kg 08/28/15 02:45 103-65-16.0 2.0 1
Styrene ND ug/kg 08/28/15 02:45 100-42-56.0 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/28/15 02:45 630-20-66.0 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/28/15 02:45 79-34-56.0 2.3 1
Tetrachloroethene ND ug/kg 08/28/15 02:45 127-18-46.0 2.0 1
Toluene ND ug/kg 08/28/15 02:45 108-88-36.0 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 08/28/15 02:45 87-61-66.0 2.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/28/15 02:45 120-82-16.0 1.9 1
1,1,1-Trichloroethane ND ug/kg 08/28/15 02:45 71-55-66.0 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/28/15 02:45 79-00-56.0 2.5 1
Trichloroethene ND ug/kg 08/28/15 02:45 79-01-66.0 2.5 1
Trichlorofluoromethane ND ug/kg 08/28/15 02:45 75-69-46.0 2.6 1
1,2,3-Trichloropropane ND ug/kg 08/28/15 02:45 96-18-46.0 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 08/28/15 02:45 95-63-66.0 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 08/28/15 02:45 108-67-86.0 2.2 1
Vinyl acetate ND ug/kg 08/28/15 02:45 108-05-4 L260.2 10.6 1
Vinyl chloride ND ug/kg 08/28/15 02:45 75-01-412.0 2.2 1
Xylene (Total)ND ug/kg 08/28/15 02:45 1330-20-712.0 4.3 1
m&p-Xylene ND ug/kg 08/28/15 02:45 179601-23-112.0 4.3 1
o-Xylene ND ug/kg 08/28/15 02:45 95-47-66.0 2.3 1
Surrogates
Toluene-d8 (S)101 %08/28/15 02:45 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %08/28/15 02:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %08/28/15 02:45 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.6 %08/25/15 12:550.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9780
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1540631
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/25/15 16:13
4-Bromofluorobenzene (S)%104 70-167 08/25/15 16:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1540632LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 50.450 101 70-165
4-Bromofluorobenzene (S)%102 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1540633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
Gas Range Organics (C6-C10)mg/kg 68.167 78 47-18715.6
4-Bromofluorobenzene (S)%93 70-167
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264629002
1540634SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%98 3101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9791
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1544876
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/01/15 16:30
Aliphatic (C09-C12)mg/kg ND 2.5 N209/01/15 16:30
Aromatic (C09-C10)mg/kg ND 2.5 N209/01/15 16:30
4-Bromofluorobenzene (FID) (S)%101 70-130 09/01/15 16:30
4-Bromofluorobenzene (PID) (S)%102 70-130 09/01/15 16:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544877LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1544878
Aliphatic (C05-C08)mg/kg 14.6 N2159770-1309614.5 1 25
Aliphatic (C09-C12)mg/kg 16.1 N21510730-13011116.7 4 25
Aromatic (C09-C10)mg/kg 4.9 N259870-130974.9 1 25
4-Bromofluorobenzene (FID) (S)%103 70-130101
4-Bromofluorobenzene (PID) (S)%103 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33141
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1542838
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,1-Trichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/27/15 19:28
1,1,2-Trichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloroethane ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
1,1-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2,3-Trichloropropane ug/kg ND 5.0 08/27/15 19:28
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/27/15 19:28
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/27/15 19:28
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/27/15 19:28
1,2-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,2-Dichloroethane ug/kg ND 5.0 08/27/15 19:28
1,2-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/27/15 19:28
1,3-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
1,3-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
1,4-Dichlorobenzene ug/kg ND 5.0 08/27/15 19:28
2,2-Dichloropropane ug/kg ND 5.0 08/27/15 19:28
2-Butanone (MEK)ug/kg ND 100 08/27/15 19:28
2-Chlorotoluene ug/kg ND 5.0 08/27/15 19:28
2-Hexanone ug/kg ND 50.0 08/27/15 19:28
4-Chlorotoluene ug/kg ND 5.0 08/27/15 19:28
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/27/15 19:28
Acetone ug/kg ND 100 08/27/15 19:28
Benzene ug/kg ND 5.0 08/27/15 19:28
Bromobenzene ug/kg ND 5.0 08/27/15 19:28
Bromochloromethane ug/kg ND 5.0 08/27/15 19:28
Bromodichloromethane ug/kg ND 5.0 08/27/15 19:28
Bromoform ug/kg ND 5.0 08/27/15 19:28
Bromomethane ug/kg ND 10.0 08/27/15 19:28
Carbon tetrachloride ug/kg ND 5.0 08/27/15 19:28
Chlorobenzene ug/kg ND 5.0 08/27/15 19:28
Chloroethane ug/kg ND 10.0 08/27/15 19:28
Chloroform ug/kg ND 5.0 08/27/15 19:28
Chloromethane ug/kg ND 10.0 08/27/15 19:28
cis-1,2-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
cis-1,3-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
Dibromochloromethane ug/kg ND 5.0 08/27/15 19:28
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1542838
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.0 08/27/15 19:28
Dichlorodifluoromethane ug/kg ND 10.0 08/27/15 19:28
Diisopropyl ether ug/kg ND 5.0 08/27/15 19:28
Ethylbenzene ug/kg ND 5.0 08/27/15 19:28
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/27/15 19:28
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/27/15 19:28
m&p-Xylene ug/kg ND 10.0 08/27/15 19:28
Methyl-tert-butyl ether ug/kg ND 5.0 08/27/15 19:28
Methylene Chloride ug/kg 6.0J 20.0 08/27/15 19:28
n-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
n-Propylbenzene ug/kg ND 5.0 08/27/15 19:28
Naphthalene ug/kg ND 5.0 08/27/15 19:28
o-Xylene ug/kg ND 5.0 08/27/15 19:28
p-Isopropyltoluene ug/kg ND 5.0 08/27/15 19:28
sec-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
Styrene ug/kg ND 5.0 08/27/15 19:28
tert-Butylbenzene ug/kg ND 5.0 08/27/15 19:28
Tetrachloroethene ug/kg ND 5.0 08/27/15 19:28
Toluene ug/kg ND 5.0 08/27/15 19:28
trans-1,2-Dichloroethene ug/kg ND 5.0 08/27/15 19:28
trans-1,3-Dichloropropene ug/kg ND 5.0 08/27/15 19:28
Trichloroethene ug/kg ND 5.0 08/27/15 19:28
Trichlorofluoromethane ug/kg ND 5.0 08/27/15 19:28
Vinyl acetate ug/kg ND 50.0 08/27/15 19:28
Vinyl chloride ug/kg ND 10.0 08/27/15 19:28
Xylene (Total)ug/kg ND 10.0 08/27/15 19:28
1,2-Dichloroethane-d4 (S)%104 70-132 08/27/15 19:28
4-Bromofluorobenzene (S)%97 70-130 08/27/15 19:28
Toluene-d8 (S)%101 70-130 08/27/15 19:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.750 97 74-137
1,1,1-Trichloroethane ug/kg 50.450 101 67-140
1,1,2,2-Tetrachloroethane ug/kg 37.550 75 72-141
1,1,2-Trichloroethane ug/kg 46.350 93 78-138
1,1-Dichloroethane ug/kg 54.350 109 69-134
1,1-Dichloroethene ug/kg 56.150 112 67-138
1,1-Dichloropropene ug/kg 52.550 105 69-139
1,2,3-Trichlorobenzene ug/kg 46.050 92 70-146
1,2,3-Trichloropropane ug/kg 48.550 97 69-144
1,2,4-Trichlorobenzene ug/kg 44.550 89 68-148
1,2,4-Trimethylbenzene ug/kg 49.550 99 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 47.350 95 65-140
1,2-Dibromoethane (EDB)ug/kg 49.950 100 77-135
1,2-Dichlorobenzene ug/kg 48.550 97 77-141
1,2-Dichloroethane ug/kg 48.650 97 65-137
1,2-Dichloropropane ug/kg 47.750 95 72-136
1,3,5-Trimethylbenzene ug/kg 50.550 101 76-133
1,3-Dichlorobenzene ug/kg 48.750 97 74-138
1,3-Dichloropropane ug/kg 47.550 95 71-139
1,4-Dichlorobenzene ug/kg 46.850 94 76-138
2,2-Dichloropropane ug/kg 49.050 98 68-137
2-Butanone (MEK)ug/kg 96.0J100 96 58-147
2-Chlorotoluene ug/kg 46.550 93 73-139
2-Hexanone ug/kg 90.5100 91 62-145
4-Chlorotoluene ug/kg 49.050 98 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 100100 100 64-149
Acetone ug/kg 90.8J100 91 53-153
Benzene ug/kg 50.250 100 73-135
Bromobenzene ug/kg 50.250 100 75-133
Bromochloromethane ug/kg 50.250 100 73-134
Bromodichloromethane ug/kg 50.250 100 71-135
Bromoform ug/kg 44.850 90 66-141
Bromomethane ug/kg 43.650 87 53-160
Carbon tetrachloride ug/kg 50.450 101 60-145
Chlorobenzene ug/kg 49.350 99 78-130
Chloroethane ug/kg 45.350 91 64-149
Chloroform ug/kg 52.550 105 70-134
Chloromethane ug/kg 41.850 84 52-150
cis-1,2-Dichloroethene ug/kg 52.050 104 70-133
cis-1,3-Dichloropropene ug/kg 48.950 98 68-134
Dibromochloromethane ug/kg 48.050 96 71-138
Dibromomethane ug/kg 48.350 97 74-130
Dichlorodifluoromethane ug/kg 42.750 85 40-160
Diisopropyl ether ug/kg 54.150 108 69-141
Ethylbenzene ug/kg 48.650 97 75-133
Hexachloro-1,3-butadiene ug/kg 44.450 89 68-143
Isopropylbenzene (Cumene)ug/kg 52.850 106 76-143
m&p-Xylene ug/kg 97.9100 98 75-136
Methyl-tert-butyl ether ug/kg 47.450 95 68-144
Methylene Chloride ug/kg 47.150 94 45-154
n-Butylbenzene ug/kg 47.850 96 72-137
n-Propylbenzene ug/kg 48.950 98 76-136
Naphthalene ug/kg 47.950 96 68-151
o-Xylene ug/kg 50.050 100 76-141
p-Isopropyltoluene ug/kg 48.750 97 76-140
sec-Butylbenzene ug/kg 51.250 102 79-139
Styrene ug/kg 49.650 99 79-137
tert-Butylbenzene ug/kg 44.150 88 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1542839LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 45.650 91 71-138
Toluene ug/kg 48.750 97 74-131
trans-1,2-Dichloroethene ug/kg 52.050 104 67-135
trans-1,3-Dichloropropene ug/kg 48.150 96 65-146
Trichloroethene ug/kg 54.250 108 67-135
Trichlorofluoromethane ug/kg 48.350 97 59-144
Vinyl acetate ug/kg 33.3J L010033 40-160
Vinyl chloride ug/kg 45.650 91 56-141
Xylene (Total)ug/kg 148150 99 76-137
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543838MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
1,1,1,2-Tetrachloroethane ug/kg 25.426.7 95 70-130ND
1,1,1-Trichloroethane ug/kg 25.926.7 97 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 28.026.7 105 70-130ND
1,1,2-Trichloroethane ug/kg 27.126.7 101 70-130ND
1,1-Dichloroethane ug/kg 28.226.7 106 70-130ND
1,1-Dichloroethene ug/kg 33.426.7 125 49-180ND
1,1-Dichloropropene ug/kg 30.526.7 114 70-130ND
1,2,3-Trichlorobenzene ug/kg 23.826.7 89 70-130ND
1,2,3-Trichloropropane ug/kg 24.326.7 91 70-130ND
1,2,4-Trichlorobenzene ug/kg 22.326.7 83 70-130ND
1,2,4-Trimethylbenzene ug/kg 27.326.7 101 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 26.426.7 99 70-130ND
1,2-Dibromoethane (EDB)ug/kg 27.026.7 101 70-130ND
1,2-Dichlorobenzene ug/kg 26.926.7 101 70-130ND
1,2-Dichloroethane ug/kg 26.126.7 98 70-130ND
1,2-Dichloropropane ug/kg 29.326.7 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 27.826.7 104 70-130ND
1,3-Dichlorobenzene ug/kg 27.326.7 102 70-130ND
1,3-Dichloropropane ug/kg 27.626.7 103 70-130ND
1,4-Dichlorobenzene ug/kg 26.626.7 99 70-130ND
2,2-Dichloropropane ug/kg 25.726.7 96 70-130ND
2-Butanone (MEK)ug/kg 57.1J53.5 107 70-130ND
2-Chlorotoluene ug/kg 27.426.7 102 70-130ND
2-Hexanone ug/kg 51.4J53.5 96 70-130ND
4-Chlorotoluene ug/kg 28.126.7 105 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 57.8J53.5 108 70-130ND
Acetone ug/kg 76.9J53.5 120 70-130ND
Benzene ug/kg 29.826.7 111 50-166ND
Bromobenzene ug/kg 27.826.7 104 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
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Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543838MATRIX SPIKE SAMPLE:
MSSpike
Result
92264629001
Bromochloromethane ug/kg 29.226.7 109 70-130ND
Bromodichloromethane ug/kg 25.826.7 96 70-130ND
Bromoform ug/kg 21.626.7 81 70-130ND
Bromomethane ug/kg 33.426.7 125 70-130ND
Carbon tetrachloride ug/kg 25.826.7 97 70-130ND
Chlorobenzene ug/kg 27.426.7 103 43-169ND
Chloroethane ug/kg 31.126.7 116 70-130ND
Chloroform ug/kg 28.226.7 106 70-130ND
Chloromethane ug/kg 28.126.7 105 70-130ND
cis-1,2-Dichloroethene ug/kg 29.826.7 111 70-130ND
cis-1,3-Dichloropropene ug/kg 27.126.7 101 70-130ND
Dibromochloromethane ug/kg 23.826.7 89 70-130ND
Dibromomethane ug/kg 26.926.7 100 70-130ND
Dichlorodifluoromethane ug/kg 25.126.7 94 70-130ND
Diisopropyl ether ug/kg 28.026.7 105 70-130ND
Ethylbenzene ug/kg 27.626.7 103 70-130ND
Hexachloro-1,3-butadiene ug/kg 18.926.7 71 70-130ND
Isopropylbenzene (Cumene)ug/kg 29.526.7 110 70-130ND
m&p-Xylene ug/kg 55.053.5 103 70-130ND
Methyl-tert-butyl ether ug/kg 26.626.7 100 70-130ND
Methylene Chloride ug/kg 42.126.7 109 70-13012.8J
n-Butylbenzene ug/kg 26.526.7 99 70-130ND
n-Propylbenzene ug/kg 28.626.7 107 70-130ND
Naphthalene ug/kg 27.226.7 98 70-130ND
o-Xylene ug/kg 27.026.7 101 70-130ND
p-Isopropyltoluene ug/kg 26.226.7 98 70-130ND
sec-Butylbenzene ug/kg 28.726.7 107 70-130ND
Styrene ug/kg 27.826.7 104 70-130ND
tert-Butylbenzene ug/kg 24.026.7 90 70-130ND
Tetrachloroethene ug/kg 24.626.7 92 70-130ND
Toluene ug/kg 28.626.7 106 52-163ND
trans-1,2-Dichloroethene ug/kg 31.026.7 116 70-130ND
trans-1,3-Dichloropropene ug/kg 25.326.7 95 70-130ND
Trichloroethene ug/kg 25.626.7 96 49-167ND
Trichlorofluoromethane ug/kg 26.626.7 99 70-130ND
Vinyl acetate ug/kg 37.6J53.5 70 70-130ND
Vinyl chloride ug/kg 31.126.7 116 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg 52.9J 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 359 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264903003
1543837SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 7.6J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%112 2299
4-Bromofluorobenzene (S)%95 897
Toluene-d8 (S)%104 15100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37366
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1543159
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 08/30/15 06:16
n-Pentacosane (S)%85 41-119 08/30/15 06:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1543160LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 52.766.7 79 49-113
n-Pentacosane (S)%89 41-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1543161MATRIX SPIKE SAMPLE:
MSSpike
Result
92264630001
Diesel Range Organics(C10-C28)mg/kg 45.278.9 56 10-146ND
n-Pentacosane (S)%58 41-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264863008
1543162SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 29300 3 3028500
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37328
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1541631
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 08/28/15 17:03
1,2-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1,3-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1,4-Dichlorobenzene ug/kg ND 330 08/28/15 17:03
1-Methylnaphthalene ug/kg ND 330 08/28/15 17:03
2,4,5-Trichlorophenol ug/kg ND 330 08/28/15 17:03
2,4,6-Trichlorophenol ug/kg ND 330 08/28/15 17:03
2,4-Dichlorophenol ug/kg ND 330 08/28/15 17:03
2,4-Dimethylphenol ug/kg ND 330 08/28/15 17:03
2,4-Dinitrophenol ug/kg ND 1650 08/28/15 17:03
2,4-Dinitrotoluene ug/kg ND 330 08/28/15 17:03
2,6-Dinitrotoluene ug/kg ND 330 08/28/15 17:03
2-Chloronaphthalene ug/kg ND 330 08/28/15 17:03
2-Chlorophenol ug/kg ND 330 08/28/15 17:03
2-Methylnaphthalene ug/kg ND 330 08/28/15 17:03
2-Methylphenol(o-Cresol)ug/kg ND 330 08/28/15 17:03
2-Nitroaniline ug/kg ND 1650 08/28/15 17:03
2-Nitrophenol ug/kg ND 330 08/28/15 17:03
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 08/28/15 17:03
3,3'-Dichlorobenzidine ug/kg ND 1650 08/28/15 17:03
3-Nitroaniline ug/kg ND 1650 08/28/15 17:03
4,6-Dinitro-2-methylphenol ug/kg ND 660 08/28/15 17:03
4-Bromophenylphenyl ether ug/kg ND 330 08/28/15 17:03
4-Chloro-3-methylphenol ug/kg ND 660 08/28/15 17:03
4-Chloroaniline ug/kg ND 1650 08/28/15 17:03
4-Chlorophenylphenyl ether ug/kg ND 330 08/28/15 17:03
4-Nitroaniline ug/kg ND 660 08/28/15 17:03
4-Nitrophenol ug/kg ND 1650 08/28/15 17:03
Acenaphthene ug/kg ND 330 08/28/15 17:03
Acenaphthylene ug/kg ND 330 08/28/15 17:03
Aniline ug/kg ND 330 08/28/15 17:03
Anthracene ug/kg ND 330 08/28/15 17:03
Benzo(a)anthracene ug/kg ND 330 08/28/15 17:03
Benzo(a)pyrene ug/kg ND 330 08/28/15 17:03
Benzo(b)fluoranthene ug/kg ND 330 08/28/15 17:03
Benzo(g,h,i)perylene ug/kg ND 330 08/28/15 17:03
Benzo(k)fluoranthene ug/kg ND 330 08/28/15 17:03
Benzoic Acid ug/kg ND 1650 08/28/15 17:03
Benzyl alcohol ug/kg ND 660 08/28/15 17:03
bis(2-Chloroethoxy)methane ug/kg ND 330 08/28/15 17:03
bis(2-Chloroethyl) ether ug/kg ND 330 08/28/15 17:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1541631
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 08/28/15 17:03
bis(2-Ethylhexyl)phthalate ug/kg ND 330 08/28/15 17:03
Butylbenzylphthalate ug/kg ND 330 08/28/15 17:03
Chrysene ug/kg ND 330 08/28/15 17:03
Di-n-butylphthalate ug/kg ND 330 08/28/15 17:03
Di-n-octylphthalate ug/kg ND 330 08/28/15 17:03
Dibenz(a,h)anthracene ug/kg ND 330 08/28/15 17:03
Dibenzofuran ug/kg ND 330 08/28/15 17:03
Diethylphthalate ug/kg ND 330 08/28/15 17:03
Dimethylphthalate ug/kg ND 330 08/28/15 17:03
Fluoranthene ug/kg ND 330 08/28/15 17:03
Fluorene ug/kg ND 330 08/28/15 17:03
Hexachloro-1,3-butadiene ug/kg ND 330 08/28/15 17:03
Hexachlorobenzene ug/kg ND 330 08/28/15 17:03
Hexachlorocyclopentadiene ug/kg ND 330 08/28/15 17:03
Hexachloroethane ug/kg ND 330 08/28/15 17:03
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/28/15 17:03
Isophorone ug/kg ND 330 08/28/15 17:03
N-Nitroso-di-n-propylamine ug/kg ND 330 08/28/15 17:03
N-Nitrosodimethylamine ug/kg ND 330 08/28/15 17:03
N-Nitrosodiphenylamine ug/kg ND 330 08/28/15 17:03
Naphthalene ug/kg ND 330 08/28/15 17:03
Nitrobenzene ug/kg ND 330 08/28/15 17:03
Pentachlorophenol ug/kg ND 1650 08/28/15 17:03
Phenanthrene ug/kg ND 330 08/28/15 17:03
Phenol ug/kg ND 330 08/28/15 17:03
Pyrene ug/kg ND 330 08/28/15 17:03
2,4,6-Tribromophenol (S)%80 27-110 08/28/15 17:03
2-Fluorobiphenyl (S)%78 30-110 08/28/15 17:03
2-Fluorophenol (S)%75 13-110 08/28/15 17:03
Nitrobenzene-d5 (S)%80 23-110 08/28/15 17:03
Phenol-d6 (S)%73 22-110 08/28/15 17:03
Terphenyl-d14 (S)%98 28-110 08/28/15 17:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13901670 83 36-120
1,2-Dichlorobenzene ug/kg 12901670 77 41-120
1,3-Dichlorobenzene ug/kg 12601670 76 66-120
1,4-Dichlorobenzene ug/kg 13001670 78 42-120
1-Methylnaphthalene ug/kg 13701670 82 40-120
2,4,5-Trichlorophenol ug/kg 13801670 83 37-120
2,4,6-Trichlorophenol ug/kg 14001670 84 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 13501670 81 33-120
2,4-Dimethylphenol ug/kg 13601670 82 36-120
2,4-Dinitrophenol ug/kg 84008330 101 22-121
2,4-Dinitrotoluene ug/kg 14901670 89 60-120
2,6-Dinitrotoluene ug/kg 14701670 88 54-120
2-Chloronaphthalene ug/kg 13201670 79 41-120
2-Chlorophenol ug/kg 13001670 78 39-120
2-Methylnaphthalene ug/kg 13001670 78 26-120
2-Methylphenol(o-Cresol)ug/kg 12001670 72 41-120
2-Nitroaniline ug/kg 27403330 82 45-120
2-Nitrophenol ug/kg 14001670 84 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 11601670 69 35-120
3,3'-Dichlorobenzidine ug/kg 26503330 79 16-125
3-Nitroaniline ug/kg 27303330 82 45-120
4,6-Dinitro-2-methylphenol ug/kg 32303330 97 46-120
4-Bromophenylphenyl ether ug/kg 13101670 79 36-120
4-Chloro-3-methylphenol ug/kg 29503330 89 37-120
4-Chloroaniline ug/kg 23903330 72 35-120
4-Chlorophenylphenyl ether ug/kg 13401670 81 30-120
4-Nitroaniline ug/kg 28403330 85 48-120
4-Nitrophenol ug/kg 77408330 93 43-120
Acenaphthene ug/kg 13301670 80 46-120
Acenaphthylene ug/kg 13701670 82 46-120
Aniline ug/kg 11201670 67 33-120
Anthracene ug/kg 14001670 84 63-120
Benzo(a)anthracene ug/kg 14101670 84 61-120
Benzo(a)pyrene ug/kg 12601670 76 59-120
Benzo(b)fluoranthene ug/kg 12301670 74 55-120
Benzo(g,h,i)perylene ug/kg 11901670 71 57-120
Benzo(k)fluoranthene ug/kg 15301670 92 56-120
Benzoic Acid ug/kg 58708330 70 13-120
Benzyl alcohol ug/kg 24603330 74 34-120
bis(2-Chloroethoxy)methane ug/kg 12801670 77 21-120
bis(2-Chloroethyl) ether ug/kg 11201670 67 25-120
bis(2-Chloroisopropyl) ether ug/kg 11501670 69 13-120
bis(2-Ethylhexyl)phthalate ug/kg 15001670 90 56-123
Butylbenzylphthalate ug/kg 15301670 92 57-120
Chrysene ug/kg 13801670 83 64-120
Di-n-butylphthalate ug/kg 15101670 91 58-120
Di-n-octylphthalate ug/kg 13501670 81 47-121
Dibenz(a,h)anthracene ug/kg 12001670 72 56-120
Dibenzofuran ug/kg 13701670 82 43-120
Diethylphthalate ug/kg 14501670 87 55-120
Dimethylphthalate ug/kg 14001670 84 54-120
Fluoranthene ug/kg 15001670 90 61-120
Fluorene ug/kg 14201670 85 51-120
Hexachloro-1,3-butadiene ug/kg 14301670 86 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1541632LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15001670 90 53-120
Hexachlorocyclopentadiene ug/kg 14401670 86 18-150
Hexachloroethane ug/kg 13001670 78 39-120
Indeno(1,2,3-cd)pyrene ug/kg 12001670 72 58-120
Isophorone ug/kg 12301670 74 38-120
N-Nitroso-di-n-propylamine ug/kg 11701670 70 30-120
N-Nitrosodimethylamine ug/kg 11401670 69 32-120
N-Nitrosodiphenylamine ug/kg 13101670 79 50-120
Naphthalene ug/kg 13001670 78 38-120
Nitrobenzene ug/kg 12601670 76 37-120
Pentachlorophenol ug/kg 29803330 89 10-120
Phenanthrene ug/kg 13301670 80 62-120
Phenol ug/kg 14001670 84 37-120
Pyrene ug/kg 14601670 88 63-120
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%80 13-110
Nitrobenzene-d5 (S)%82 23-110
Phenol-d6 (S)%79 22-110
Terphenyl-d14 (S)%90 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
1,2,4-Trichlorobenzene ug/kg 10701900 56 18-119ND
1,2-Dichlorobenzene ug/kg 11501900 61 50-110ND
1,3-Dichlorobenzene ug/kg 11001900 58 27-110ND
1,4-Dichlorobenzene ug/kg 11301900 60 28-110ND
1-Methylnaphthalene ug/kg 10701900 57 24-116ND
2,4,5-Trichlorophenol ug/kg 11001900 58 28-110ND
2,4,6-Trichlorophenol ug/kg 10801900 57 17-117ND
2,4-Dichlorophenol ug/kg 10201900 54 21-128ND
2,4-Dimethylphenol ug/kg 10101900 53 10-120ND
2,4-Dinitrophenol ug/kg 20809460 22 10-107ND
2,4-Dinitrotoluene ug/kg 12701900 67 36-109ND
2,6-Dinitrotoluene ug/kg 11901900 63 32-110ND
2-Chloronaphthalene ug/kg 10001900 53 30-107ND
2-Chlorophenol ug/kg 11201900 59 14-106ND
2-Methylnaphthalene ug/kg 10301900 54 10-135ND
2-Methylphenol(o-Cresol)ug/kg 9981900 53 10-124ND
2-Nitroaniline ug/kg 22103780 58 26-116ND
2-Nitrophenol ug/kg 10701900 56 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 9841900 52 10-109ND
3,3'-Dichlorobenzidine ug/kg 23403780 62 10-150ND
3-Nitroaniline ug/kg 23603780 62 22-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/02/2015 04:21 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
4,6-Dinitro-2-methylphenol ug/kg 22203780 59 13-121ND
4-Bromophenylphenyl ether ug/kg 11101900 58 31-109ND
4-Chloro-3-methylphenol ug/kg 23803780 63 13-128ND
4-Chloroaniline ug/kg 1870J3780 49 18-102ND
4-Chlorophenylphenyl ether ug/kg 11101900 58 29-112ND
4-Nitroaniline ug/kg 25103780 66 16-111ND
4-Nitrophenol ug/kg 61009460 64 14-135ND
Acenaphthene ug/kg 10301900 55 26-114ND
Acenaphthylene ug/kg 10501900 55 32-108ND
Aniline ug/kg 9511900 50 10-107ND
Anthracene ug/kg 11801900 62 32-111ND
Benzo(a)anthracene ug/kg 12301900 65 25-117ND
Benzo(a)pyrene ug/kg 10301900 54 25-106ND
Benzo(b)fluoranthene ug/kg 10401900 55 24-110ND
Benzo(g,h,i)perylene ug/kg 9601900 51 19-112ND
Benzo(k)fluoranthene ug/kg 12701900 67 24-114ND
Benzoic Acid ug/kg ND M194600 10-110ND
Benzyl alcohol ug/kg 21203780 56 24-106ND
bis(2-Chloroethoxy)methane ug/kg 9591900 51 13-119ND
bis(2-Chloroethyl) ether ug/kg 9511900 50 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 9961900 53 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 13101900 69 10-125ND
Butylbenzylphthalate ug/kg 13501900 71 18-110ND
Chrysene ug/kg 12001900 64 30-110ND
Di-n-butylphthalate ug/kg 12501900 66 19-112ND
Di-n-octylphthalate ug/kg 12201900 65 17-105ND
Dibenz(a,h)anthracene ug/kg 9751900 52 23-111ND
Dibenzofuran ug/kg 10801900 57 35-103ND
Diethylphthalate ug/kg 12401900 65 27-113ND
Dimethylphthalate ug/kg 11701900 62 26-111ND
Fluoranthene ug/kg 12701900 67 33-109ND
Fluorene ug/kg 11501900 61 32-113ND
Hexachloro-1,3-butadiene ug/kg 10601900 56 16-116ND
Hexachlorobenzene ug/kg 12501900 66 27-120ND
Hexachlorocyclopentadiene ug/kg 9991900 53 10-108ND
Hexachloroethane ug/kg 11401900 60 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 9361900 49 10-122ND
Isophorone ug/kg 9401900 50 28-114ND
N-Nitroso-di-n-propylamine ug/kg 10601900 56 27-113ND
N-Nitrosodimethylamine ug/kg 9661900 51 10-109ND
N-Nitrosodiphenylamine ug/kg 11001900 58 10-128ND
Naphthalene ug/kg 10101900 54 25-110ND
Nitrobenzene ug/kg 9661900 51 18-114ND
Pentachlorophenol ug/kg 24303780 64 10-122ND
Phenanthrene ug/kg 11101900 59 30-114ND
Phenol ug/kg 11701900 62 11-102ND
Pyrene ug/kg 13101900 67 25-116ND
REPORT OF LABORATORY ANALYSIS
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Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1541633MATRIX SPIKE SAMPLE:
MSSpike
Result
92264553001
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%50 30-110
2-Fluorophenol (S)%60 13-110
Nitrobenzene-d5 (S)%54 23-110
Phenol-d6 (S)%59 22-110
Terphenyl-d14 (S)%69 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264553001
1541634SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264553001
1541634SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%45 3564
2-Fluorobiphenyl (S)%39 2148
2-Fluorophenol (S)%39 2751
Nitrobenzene-d5 (S)%40 2551
Phenol-d6 (S)%42 1548
Terphenyl-d14 (S)%49 3973
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37282
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1540309
Associated Lab Samples:92264630001, 92264630002
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N208/26/15 00:49
Aliphatic (C19-C36)mg/kg ND 10.0 N208/26/15 00:49
Aromatic (C11-C22)mg/kg ND 10.0 N208/25/15 16:14
2-Bromonaphthalene (S)%81 40-140 08/25/15 16:14
2-Fluorobiphenyl (S)%80 40-140 08/25/15 16:14
Nonatriacontane (S)%77 40-140 08/26/15 00:49
o-Terphenyl (S)%68 40-140 08/25/15 16:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1540310LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1540311
Aliphatic (C09-C18)mg/kg ND N2107440-14071ND 50
Aliphatic (C19-C36)mg/kg 11.2 N213.3 84 40-1407910.6 5 50
Aromatic (C11-C22)mg/kg 22.4 N228.3 79 40-1409226.0 15 50
2-Bromonaphthalene (S)%80 40-14089
2-Fluorobiphenyl (S)%86 40-14095
Nonatriacontane (S)%81 40-14079
o-Terphenyl (S)%74 40-14088
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8286
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92264630001, 92264630002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264629001
1540420SAMPLE DUPLICATE:
Percent Moisture %15.8 8 2514.6
REPORT OF LABORATORY ANALYSIS
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Page 32 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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Page 33 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92264630
SUNCAP 1404 Old Greensboro Rd
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92264630001 OEXT/37366 GCSV/22429SS-3 (14FT)EPA 3546 EPA 8015 Modified
92264630002 OEXT/37366 GCSV/22429SS-4 (14FT)EPA 3546 EPA 8015 Modified
92264630001 OEXT/37282 GCSV/22403SS-3 (14FT)MADEP EPH MADEP EPH
92264630002 OEXT/37282 GCSV/22403SS-4 (14FT)MADEP EPH MADEP EPH
92264630001 GCV/9780 GCV/9781SS-3 (14FT)EPA 5035A/5030B EPA 8015 Modified
92264630002 GCV/9780 GCV/9781SS-4 (14FT)EPA 5035A/5030B EPA 8015 Modified
92264630001 GCV/9791 GCV/9799SS-3 (14FT)MADEP VPH MADEP VPH
92264630002 GCV/9791 GCV/9799SS-4 (14FT)MADEP VPH MADEP VPH
92264630001 OEXT/37328 MSSV/11156SS-3 (14FT)EPA 3546 EPA 8270
92264630002 OEXT/37328 MSSV/11156SS-4 (14FT)EPA 3546 EPA 8270
92264630001 MSV/33141SS-3 (14FT)EPA 8260
92264630002 MSV/33141SS-4 (14FT)EPA 8260
92264630001 PMST/8286SS-3 (14FT)ASTM D2974-87
92264630002 PMST/8286SS-4 (14FT)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 34 of 36
Page 35 of 36
Page 36 of 36
#=CL#
September 08, 2015
LIMS USE: FR - TROY SHELTON
LIMS OBJECT ID: 92265117
92265117
Project:
Pace Project No.:
RE:
Troy Shelton
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, VA 24540
SUN CAP 1404 OLD GREENSBORO RD
Dear Troy Shelton:
Enclosed are the analytical results for sample(s) received by the laboratory on August 26, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
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Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Lab ID Sample ID Matrix Date Collected Date Received
92265117001 SS-1 (17')Solid 08/25/15 10:24 08/26/15 16:25
92265117002 SS-2 (16')Solid 08/25/15 13:55 08/26/15 16:25
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92265117001 SS-1 (17')EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92265117002 SS-2 (16')EPA 8015 Modified 2 PASI-CRES
MADEP EPH 7 PASI-CSWB
EPA 8015 Modified 2 PASI-CBFW
MADEP VPH 5 PASI-CBFW
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92265117001 SS-1 (17')
Percent Moisture 10.9 %08/27/15 13:020.10ASTM D2974-87
92265117002 SS-2 (16')
Percent Moisture 10.5 %08/27/15 13:020.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-1 (17')Lab ID: 92265117001 Collected: 08/25/15 10:24 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/02/15 03:4908/31/15 13:295.6 5.1 1
Surrogates
n-Pentacosane (S)84 %09/02/15 03:49 629-99-208/31/15 13:2941-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 08/31/15 23:05 N208/28/15 15:4211.2 11.2 1
Aliphatic (C19-C36)ND mg/kg 08/31/15 23:05 N208/28/15 15:4211.2 11.2 1
Aromatic (C11-C22)ND mg/kg 08/31/15 23:05 N208/28/15 15:4211.2 11.2 1
Surrogates
Nonatriacontane (S)89 %08/31/15 23:05 7194-86-708/28/15 15:4240-140 1
o-Terphenyl (S)86 %08/31/15 23:05 84-15-108/28/15 15:4240-140 1
2-Fluorobiphenyl (S)103 %08/31/15 23:05 321-60-808/28/15 15:4240-140 1
2-Bromonaphthalene (S)110 %08/31/15 23:05 580-13-208/28/15 15:4240-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/02/15 14:0209/02/15 11:177.8 7.8 1
Surrogates
4-Bromofluorobenzene (S)117 %09/02/15 14:02 460-00-409/02/15 11:1770-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/04/15 17:06 N209/03/15 12:113.7 3.7 1
Aliphatic (C09-C12)ND mg/kg 09/04/15 17:06 N209/03/15 12:113.7 3.7 1
Aromatic (C09-C10)ND mg/kg 09/04/15 17:06 N209/03/15 12:113.7 3.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %09/04/15 17:06 460-00-409/03/15 12:1170-130 1
4-Bromofluorobenzene (PID) (S)108 %09/04/15 17:06 460-00-409/03/15 12:1170-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/03/15 16:01 83-32-908/31/15 17:30370 85.3 1
Acenaphthylene ND ug/kg 09/03/15 16:01 208-96-808/31/15 17:30370 87.6 1
Aniline ND ug/kg 09/03/15 16:01 62-53-308/31/15 17:30370 99.9 1
Anthracene ND ug/kg 09/03/15 16:01 120-12-708/31/15 17:30370 83.1 1
Benzo(a)anthracene ND ug/kg 09/03/15 16:01 56-55-308/31/15 17:30370 68.5 1
Benzo(a)pyrene ND ug/kg 09/03/15 16:01 50-32-808/31/15 17:30370 70.7 1
Benzo(b)fluoranthene ND ug/kg 09/03/15 16:01 205-99-208/31/15 17:30370 64.0 1
Benzo(g,h,i)perylene ND ug/kg 09/03/15 16:01 191-24-208/31/15 17:30370 94.3 1
Benzo(k)fluoranthene ND ug/kg 09/03/15 16:01 207-08-908/31/15 17:30370 73.0 1
Benzoic Acid ND ug/kg 09/03/15 16:01 65-85-008/31/15 17:301850 67.3 1
Benzyl alcohol ND ug/kg 09/03/15 16:01 100-51-608/31/15 17:30741 74.1 1
4-Bromophenylphenyl ether ND ug/kg 09/03/15 16:01 101-55-308/31/15 17:30370 67.3 1
Butylbenzylphthalate ND ug/kg 09/03/15 16:01 85-68-708/31/15 17:30370 78.6 1
4-Chloro-3-methylphenol ND ug/kg 09/03/15 16:01 59-50-708/31/15 17:30741 76.3 1
4-Chloroaniline ND ug/kg 09/03/15 16:01 106-47-808/31/15 17:301850 103 1
bis(2-Chloroethoxy)methane ND ug/kg 09/03/15 16:01 111-91-108/31/15 17:30370 86.4 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-1 (17')Lab ID: 92265117001 Collected: 08/25/15 10:24 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 09/03/15 16:01 111-44-408/31/15 17:30370 94.3 1
bis(2-Chloroisopropyl) ether ND ug/kg 09/03/15 16:01 108-60-108/31/15 17:30370 98.8 1
2-Chloronaphthalene ND ug/kg 09/03/15 16:01 91-58-708/31/15 17:30370 73.0 1
2-Chlorophenol ND ug/kg 09/03/15 16:01 95-57-808/31/15 17:30370 101 1
4-Chlorophenylphenyl ether ND ug/kg 09/03/15 16:01 7005-72-308/31/15 17:30370 76.3 1
Chrysene ND ug/kg 09/03/15 16:01 218-01-908/31/15 17:30370 49.4 1
Dibenz(a,h)anthracene ND ug/kg 09/03/15 16:01 53-70-308/31/15 17:30370 78.6 1
Dibenzofuran ND ug/kg 09/03/15 16:01 132-64-908/31/15 17:30370 60.6 1
1,2-Dichlorobenzene ND ug/kg 09/03/15 16:01 95-50-108/31/15 17:30370 98.8 1
1,3-Dichlorobenzene ND ug/kg 09/03/15 16:01 541-73-108/31/15 17:30370 84.2 1
1,4-Dichlorobenzene ND ug/kg 09/03/15 16:01 106-46-708/31/15 17:30370 104 1
3,3'-Dichlorobenzidine ND ug/kg 09/03/15 16:01 91-94-108/31/15 17:301850 80.8 1
2,4-Dichlorophenol ND ug/kg 09/03/15 16:01 120-83-208/31/15 17:30370 80.8 1
Diethylphthalate ND ug/kg 09/03/15 16:01 84-66-208/31/15 17:30370 57.2 1
2,4-Dimethylphenol ND ug/kg 09/03/15 16:01 105-67-908/31/15 17:30370 146 1
Dimethylphthalate ND ug/kg 09/03/15 16:01 131-11-308/31/15 17:30370 75.2 1
Di-n-butylphthalate ND ug/kg 09/03/15 16:01 84-74-208/31/15 17:30370 60.6 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/03/15 16:01 534-52-108/31/15 17:30741 74.1 1
2,4-Dinitrophenol ND ug/kg 09/03/15 16:01 51-28-508/31/15 17:301850 60.6 1
2,4-Dinitrotoluene ND ug/kg 09/03/15 16:01 121-14-208/31/15 17:30370 69.6 1
2,6-Dinitrotoluene ND ug/kg 09/03/15 16:01 606-20-208/31/15 17:30370 77.4 1
Di-n-octylphthalate ND ug/kg 09/03/15 16:01 117-84-008/31/15 17:30370 77.4 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/03/15 16:01 117-81-708/31/15 17:30370 101 1
Fluoranthene ND ug/kg 09/03/15 16:01 206-44-008/31/15 17:30370 53.9 1
Fluorene ND ug/kg 09/03/15 16:01 86-73-708/31/15 17:30370 76.3 1
Hexachloro-1,3-butadiene ND ug/kg 09/03/15 16:01 87-68-308/31/15 17:30370 64.0 1
Hexachlorobenzene ND ug/kg 09/03/15 16:01 118-74-108/31/15 17:30370 47.1 1
Hexachlorocyclopentadiene ND ug/kg 09/03/15 16:01 77-47-408/31/15 17:30370 68.5 1
Hexachloroethane ND ug/kg 09/03/15 16:01 67-72-108/31/15 17:30370 97.7 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/03/15 16:01 193-39-508/31/15 17:30370 76.3 1
Isophorone ND ug/kg 09/03/15 16:01 78-59-108/31/15 17:30370 83.1 1
1-Methylnaphthalene ND ug/kg 09/03/15 16:01 90-12-008/31/15 17:30370 96.5 1
2-Methylnaphthalene ND ug/kg 09/03/15 16:01 91-57-608/31/15 17:30370 79.7 1
2-Methylphenol(o-Cresol)ND ug/kg 09/03/15 16:01 95-48-708/31/15 17:30370 112 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/03/15 16:0108/31/15 17:30370 146 1
Naphthalene ND ug/kg 09/03/15 16:01 91-20-308/31/15 17:30370 90.9 1
2-Nitroaniline ND ug/kg 09/03/15 16:01 88-74-408/31/15 17:301850 114 1
3-Nitroaniline ND ug/kg 09/03/15 16:01 99-09-208/31/15 17:301850 101 1
4-Nitroaniline ND ug/kg 09/03/15 16:01 100-01-608/31/15 17:30741 104 1
Nitrobenzene ND ug/kg 09/03/15 16:01 98-95-308/31/15 17:30370 101 1
2-Nitrophenol ND ug/kg 09/03/15 16:01 88-75-508/31/15 17:30370 89.8 1
4-Nitrophenol ND ug/kg 09/03/15 16:01 100-02-708/31/15 17:301850 66.2 1
N-Nitrosodimethylamine ND ug/kg 09/03/15 16:01 62-75-908/31/15 17:30370 120 1
N-Nitroso-di-n-propylamine ND ug/kg 09/03/15 16:01 621-64-708/31/15 17:30370 70.7 1
N-Nitrosodiphenylamine ND ug/kg 09/03/15 16:01 86-30-608/31/15 17:30370 110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-1 (17')Lab ID: 92265117001 Collected: 08/25/15 10:24 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 09/03/15 16:01 87-86-508/31/15 17:301850 67.3 1
Phenanthrene ND ug/kg 09/03/15 16:01 85-01-808/31/15 17:30370 61.7 1
Phenol ND ug/kg 09/03/15 16:01 108-95-208/31/15 17:30370 111 1
Pyrene ND ug/kg 09/03/15 16:01 129-00-008/31/15 17:30370 62.9 1
1,2,4-Trichlorobenzene ND ug/kg 09/03/15 16:01 120-82-108/31/15 17:30370 71.8 1
2,4,5-Trichlorophenol ND ug/kg 09/03/15 16:01 95-95-408/31/15 17:30370 114 1
2,4,6-Trichlorophenol ND ug/kg 09/03/15 16:01 88-06-208/31/15 17:30370 81.9 1
Surrogates
Nitrobenzene-d5 (S)63 %09/03/15 16:01 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)71 %09/03/15 16:01 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)94 %09/03/15 16:01 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)83 %09/03/15 16:01 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)75 %09/03/15 16:01 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)78 %09/03/15 16:01 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 09/01/15 21:03 67-64-1144 14.4 1
Benzene ND ug/kg 09/01/15 21:03 71-43-27.2 2.3 1
Bromobenzene ND ug/kg 09/01/15 21:03 108-86-17.2 2.9 1
Bromochloromethane ND ug/kg 09/01/15 21:03 74-97-57.2 2.4 1
Bromodichloromethane ND ug/kg 09/01/15 21:03 75-27-47.2 2.7 1
Bromoform ND ug/kg 09/01/15 21:03 75-25-27.2 3.3 1
Bromomethane ND ug/kg 09/01/15 21:03 74-83-914.4 3.6 1
2-Butanone (MEK)ND ug/kg 09/01/15 21:03 78-93-3144 4.2 1
n-Butylbenzene ND ug/kg 09/01/15 21:03 104-51-87.2 2.6 1
sec-Butylbenzene ND ug/kg 09/01/15 21:03 135-98-87.2 2.3 1
tert-Butylbenzene ND ug/kg 09/01/15 21:03 98-06-67.2 2.9 1
Carbon tetrachloride ND ug/kg 09/01/15 21:03 56-23-57.2 3.7 1
Chlorobenzene ND ug/kg 09/01/15 21:03 108-90-77.2 2.7 1
Chloroethane ND ug/kg 09/01/15 21:03 75-00-314.4 3.4 1
Chloroform ND ug/kg 09/01/15 21:03 67-66-37.2 2.3 1
Chloromethane ND ug/kg 09/01/15 21:03 74-87-314.4 3.4 1
2-Chlorotoluene ND ug/kg 09/01/15 21:03 95-49-87.2 2.4 1
4-Chlorotoluene ND ug/kg 09/01/15 21:03 106-43-47.2 2.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/01/15 21:03 96-12-87.2 5.2 1
Dibromochloromethane ND ug/kg 09/01/15 21:03 124-48-17.2 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/01/15 21:03 106-93-47.2 2.6 1
Dibromomethane ND ug/kg 09/01/15 21:03 74-95-37.2 3.6 1
1,2-Dichlorobenzene ND ug/kg 09/01/15 21:03 95-50-17.2 2.7 1
1,3-Dichlorobenzene ND ug/kg 09/01/15 21:03 541-73-17.2 2.9 1
1,4-Dichlorobenzene ND ug/kg 09/01/15 21:03 106-46-77.2 2.4 1
Dichlorodifluoromethane ND ug/kg 09/01/15 21:03 75-71-814.4 5.2 1
1,1-Dichloroethane ND ug/kg 09/01/15 21:03 75-34-37.2 2.2 1
1,2-Dichloroethane ND ug/kg 09/01/15 21:03 107-06-27.2 3.2 1
1,1-Dichloroethene ND ug/kg 09/01/15 21:03 75-35-47.2 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-1 (17')Lab ID: 92265117001 Collected: 08/25/15 10:24 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 09/01/15 21:03 156-59-27.2 2.0 1
trans-1,2-Dichloroethene ND ug/kg 09/01/15 21:03 156-60-57.2 2.7 1
1,2-Dichloropropane ND ug/kg 09/01/15 21:03 78-87-57.2 2.4 1
1,3-Dichloropropane ND ug/kg 09/01/15 21:03 142-28-97.2 2.7 1
2,2-Dichloropropane ND ug/kg 09/01/15 21:03 594-20-77.2 2.4 1
1,1-Dichloropropene ND ug/kg 09/01/15 21:03 563-58-67.2 2.2 1
cis-1,3-Dichloropropene ND ug/kg 09/01/15 21:03 10061-01-57.2 2.6 1
trans-1,3-Dichloropropene ND ug/kg 09/01/15 21:03 10061-02-67.2 2.2 1
Diisopropyl ether ND ug/kg 09/01/15 21:03 108-20-37.2 2.4 1
Ethylbenzene ND ug/kg 09/01/15 21:03 100-41-47.2 2.6 1
Hexachloro-1,3-butadiene ND ug/kg 09/01/15 21:03 87-68-37.2 2.9 1
2-Hexanone ND ug/kg 09/01/15 21:03 591-78-671.8 5.6 1
Isopropylbenzene (Cumene)ND ug/kg 09/01/15 21:03 98-82-87.2 2.7 1
p-Isopropyltoluene ND ug/kg 09/01/15 21:03 99-87-67.2 2.4 1
Methylene Chloride ND ug/kg 09/01/15 21:03 75-09-228.7 4.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/01/15 21:03 108-10-171.8 5.3 1
Methyl-tert-butyl ether ND ug/kg 09/01/15 21:03 1634-04-47.2 2.2 1
Naphthalene ND ug/kg 09/01/15 21:03 91-20-37.2 1.7 1
n-Propylbenzene ND ug/kg 09/01/15 21:03 103-65-17.2 2.4 1
Styrene ND ug/kg 09/01/15 21:03 100-42-57.2 2.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/01/15 21:03 630-20-67.2 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/01/15 21:03 79-34-57.2 2.7 1
Tetrachloroethene ND ug/kg 09/01/15 21:03 127-18-47.2 2.4 1
Toluene ND ug/kg 09/01/15 21:03 108-88-37.2 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 09/01/15 21:03 87-61-67.2 3.2 1
1,2,4-Trichlorobenzene ND ug/kg 09/01/15 21:03 120-82-17.2 2.3 1
1,1,1-Trichloroethane ND ug/kg 09/01/15 21:03 71-55-67.2 2.6 1
1,1,2-Trichloroethane ND ug/kg 09/01/15 21:03 79-00-57.2 3.0 1
Trichloroethene ND ug/kg 09/01/15 21:03 79-01-67.2 3.0 1
Trichlorofluoromethane ND ug/kg 09/01/15 21:03 75-69-47.2 3.2 1
1,2,3-Trichloropropane ND ug/kg 09/01/15 21:03 96-18-47.2 2.3 1
1,2,4-Trimethylbenzene ND ug/kg 09/01/15 21:03 95-63-67.2 2.9 1
1,3,5-Trimethylbenzene ND ug/kg 09/01/15 21:03 108-67-87.2 2.6 1
Vinyl acetate ND ug/kg 09/01/15 21:03 108-05-4 L271.8 12.6 1
Vinyl chloride ND ug/kg 09/01/15 21:03 75-01-414.4 2.6 1
Xylene (Total)ND ug/kg 09/01/15 21:03 1330-20-714.4 5.2 1
m&p-Xylene ND ug/kg 09/01/15 21:03 179601-23-114.4 5.2 1
o-Xylene ND ug/kg 09/01/15 21:03 95-47-67.2 2.7 1
Surrogates
Toluene-d8 (S)101 %09/01/15 21:03 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %09/01/15 21:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/01/15 21:03 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.9 %08/27/15 13:020.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-2 (16')Lab ID: 92265117002 Collected: 08/25/15 13:55 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/02/15 04:1208/31/15 13:295.6 5.0 1
Surrogates
n-Pentacosane (S)85 %09/02/15 04:12 629-99-208/31/15 13:2941-119 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/02/15 18:03 N209/01/15 16:5011.2 11.2 1
Aliphatic (C19-C36)ND mg/kg 09/02/15 18:03 N209/01/15 16:5011.2 11.2 1
Aromatic (C11-C22)ND mg/kg 09/02/15 18:03 N209/01/15 16:5011.2 11.2 1
Surrogates
Nonatriacontane (S)76 %09/02/15 18:03 7194-86-709/01/15 16:5040-140 1
o-Terphenyl (S)103 %09/02/15 18:03 84-15-109/01/15 16:5040-140 1
2-Fluorobiphenyl (S)116 %09/02/15 18:03 321-60-809/01/15 16:5040-140 1
2-Bromonaphthalene (S)105 %09/02/15 18:03 580-13-209/01/15 16:5040-140 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/02/15 15:0209/02/15 11:177.4 7.4 1
Surrogates
4-Bromofluorobenzene (S)121 %09/02/15 15:02 460-00-409/02/15 11:1770-167 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/04/15 17:36 N209/03/15 12:113.8 3.8 1
Aliphatic (C09-C12)ND mg/kg 09/04/15 17:36 N209/03/15 12:113.8 3.8 1
Aromatic (C09-C10)ND mg/kg 09/04/15 17:36 N209/03/15 12:113.8 3.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)105 %09/04/15 17:36 460-00-409/03/15 12:1170-130 1
4-Bromofluorobenzene (PID) (S)104 %09/04/15 17:36 460-00-409/03/15 12:1170-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 09/03/15 16:29 83-32-908/31/15 17:30369 84.9 1
Acenaphthylene ND ug/kg 09/03/15 16:29 208-96-808/31/15 17:30369 87.2 1
Aniline ND ug/kg 09/03/15 16:29 62-53-308/31/15 17:30369 99.5 1
Anthracene ND ug/kg 09/03/15 16:29 120-12-708/31/15 17:30369 82.7 1
Benzo(a)anthracene ND ug/kg 09/03/15 16:29 56-55-308/31/15 17:30369 68.2 1
Benzo(a)pyrene ND ug/kg 09/03/15 16:29 50-32-808/31/15 17:30369 70.4 1
Benzo(b)fluoranthene ND ug/kg 09/03/15 16:29 205-99-208/31/15 17:30369 63.7 1
Benzo(g,h,i)perylene ND ug/kg 09/03/15 16:29 191-24-208/31/15 17:30369 93.9 1
Benzo(k)fluoranthene ND ug/kg 09/03/15 16:29 207-08-908/31/15 17:30369 72.6 1
Benzoic Acid ND ug/kg 09/03/15 16:29 65-85-008/31/15 17:301840 67.1 1
Benzyl alcohol ND ug/kg 09/03/15 16:29 100-51-608/31/15 17:30738 73.8 1
4-Bromophenylphenyl ether ND ug/kg 09/03/15 16:29 101-55-308/31/15 17:30369 67.1 1
Butylbenzylphthalate ND ug/kg 09/03/15 16:29 85-68-708/31/15 17:30369 78.2 1
4-Chloro-3-methylphenol ND ug/kg 09/03/15 16:29 59-50-708/31/15 17:30738 76.0 1
4-Chloroaniline ND ug/kg 09/03/15 16:29 106-47-808/31/15 17:301840 103 1
bis(2-Chloroethoxy)methane ND ug/kg 09/03/15 16:29 111-91-108/31/15 17:30369 86.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-2 (16')Lab ID: 92265117002 Collected: 08/25/15 13:55 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
bis(2-Chloroethyl) ether ND ug/kg 09/03/15 16:29 111-44-408/31/15 17:30369 93.9 1
bis(2-Chloroisopropyl) ether ND ug/kg 09/03/15 16:29 108-60-108/31/15 17:30369 98.4 1
2-Chloronaphthalene ND ug/kg 09/03/15 16:29 91-58-708/31/15 17:30369 72.6 1
2-Chlorophenol ND ug/kg 09/03/15 16:29 95-57-808/31/15 17:30369 101 1
4-Chlorophenylphenyl ether ND ug/kg 09/03/15 16:29 7005-72-308/31/15 17:30369 76.0 1
Chrysene ND ug/kg 09/03/15 16:29 218-01-908/31/15 17:30369 49.2 1
Dibenz(a,h)anthracene ND ug/kg 09/03/15 16:29 53-70-308/31/15 17:30369 78.2 1
Dibenzofuran ND ug/kg 09/03/15 16:29 132-64-908/31/15 17:30369 60.4 1
1,2-Dichlorobenzene ND ug/kg 09/03/15 16:29 95-50-108/31/15 17:30369 98.4 1
1,3-Dichlorobenzene ND ug/kg 09/03/15 16:29 541-73-108/31/15 17:30369 83.8 1
1,4-Dichlorobenzene ND ug/kg 09/03/15 16:29 106-46-708/31/15 17:30369 104 1
3,3'-Dichlorobenzidine ND ug/kg 09/03/15 16:29 91-94-108/31/15 17:301840 80.5 1
2,4-Dichlorophenol ND ug/kg 09/03/15 16:29 120-83-208/31/15 17:30369 80.5 1
Diethylphthalate ND ug/kg 09/03/15 16:29 84-66-208/31/15 17:30369 57.0 1
2,4-Dimethylphenol ND ug/kg 09/03/15 16:29 105-67-908/31/15 17:30369 145 1
Dimethylphthalate ND ug/kg 09/03/15 16:29 131-11-308/31/15 17:30369 74.9 1
Di-n-butylphthalate ND ug/kg 09/03/15 16:29 84-74-208/31/15 17:30369 60.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/03/15 16:29 534-52-108/31/15 17:30738 73.8 1
2,4-Dinitrophenol ND ug/kg 09/03/15 16:29 51-28-508/31/15 17:301840 60.4 1
2,4-Dinitrotoluene ND ug/kg 09/03/15 16:29 121-14-208/31/15 17:30369 69.3 1
2,6-Dinitrotoluene ND ug/kg 09/03/15 16:29 606-20-208/31/15 17:30369 77.1 1
Di-n-octylphthalate ND ug/kg 09/03/15 16:29 117-84-008/31/15 17:30369 77.1 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/03/15 16:29 117-81-708/31/15 17:30369 101 1
Fluoranthene ND ug/kg 09/03/15 16:29 206-44-008/31/15 17:30369 53.6 1
Fluorene ND ug/kg 09/03/15 16:29 86-73-708/31/15 17:30369 76.0 1
Hexachloro-1,3-butadiene ND ug/kg 09/03/15 16:29 87-68-308/31/15 17:30369 63.7 1
Hexachlorobenzene ND ug/kg 09/03/15 16:29 118-74-108/31/15 17:30369 46.9 1
Hexachlorocyclopentadiene ND ug/kg 09/03/15 16:29 77-47-408/31/15 17:30369 68.2 1
Hexachloroethane ND ug/kg 09/03/15 16:29 67-72-108/31/15 17:30369 97.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/03/15 16:29 193-39-508/31/15 17:30369 76.0 1
Isophorone ND ug/kg 09/03/15 16:29 78-59-108/31/15 17:30369 82.7 1
1-Methylnaphthalene ND ug/kg 09/03/15 16:29 90-12-008/31/15 17:30369 96.1 1
2-Methylnaphthalene ND ug/kg 09/03/15 16:29 91-57-608/31/15 17:30369 79.4 1
2-Methylphenol(o-Cresol)ND ug/kg 09/03/15 16:29 95-48-708/31/15 17:30369 112 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/03/15 16:2908/31/15 17:30369 145 1
Naphthalene ND ug/kg 09/03/15 16:29 91-20-308/31/15 17:30369 90.5 1
2-Nitroaniline ND ug/kg 09/03/15 16:29 88-74-408/31/15 17:301840 114 1
3-Nitroaniline ND ug/kg 09/03/15 16:29 99-09-208/31/15 17:301840 101 1
4-Nitroaniline ND ug/kg 09/03/15 16:29 100-01-608/31/15 17:30738 104 1
Nitrobenzene ND ug/kg 09/03/15 16:29 98-95-308/31/15 17:30369 101 1
2-Nitrophenol ND ug/kg 09/03/15 16:29 88-75-508/31/15 17:30369 89.4 1
4-Nitrophenol ND ug/kg 09/03/15 16:29 100-02-708/31/15 17:301840 65.9 1
N-Nitrosodimethylamine ND ug/kg 09/03/15 16:29 62-75-908/31/15 17:30369 120 1
N-Nitroso-di-n-propylamine ND ug/kg 09/03/15 16:29 621-64-708/31/15 17:30369 70.4 1
N-Nitrosodiphenylamine ND ug/kg 09/03/15 16:29 86-30-608/31/15 17:30369 110 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Page 11 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-2 (16')Lab ID: 92265117002 Collected: 08/25/15 13:55 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pentachlorophenol ND ug/kg 09/03/15 16:29 87-86-508/31/15 17:301840 67.1 1
Phenanthrene ND ug/kg 09/03/15 16:29 85-01-808/31/15 17:30369 61.5 1
Phenol ND ug/kg 09/03/15 16:29 108-95-208/31/15 17:30369 111 1
Pyrene ND ug/kg 09/03/15 16:29 129-00-008/31/15 17:30369 62.6 1
1,2,4-Trichlorobenzene ND ug/kg 09/03/15 16:29 120-82-108/31/15 17:30369 71.5 1
2,4,5-Trichlorophenol ND ug/kg 09/03/15 16:29 95-95-408/31/15 17:30369 114 1
2,4,6-Trichlorophenol ND ug/kg 09/03/15 16:29 88-06-208/31/15 17:30369 81.6 1
Surrogates
Nitrobenzene-d5 (S)66 %09/03/15 16:29 4165-60-008/31/15 17:3023-110 1
2-Fluorobiphenyl (S)68 %09/03/15 16:29 321-60-808/31/15 17:3030-110 1
Terphenyl-d14 (S)89 %09/03/15 16:29 1718-51-008/31/15 17:3028-110 1
Phenol-d6 (S)82 %09/03/15 16:29 13127-88-308/31/15 17:3022-110 1
2-Fluorophenol (S)76 %09/03/15 16:29 367-12-408/31/15 17:3013-110 1
2,4,6-Tribromophenol (S)79 %09/03/15 16:29 118-79-608/31/15 17:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 09/01/15 21:23 67-64-1136 13.6 1
Benzene ND ug/kg 09/01/15 21:23 71-43-26.8 2.2 1
Bromobenzene ND ug/kg 09/01/15 21:23 108-86-16.8 2.7 1
Bromochloromethane ND ug/kg 09/01/15 21:23 74-97-56.8 2.3 1
Bromodichloromethane ND ug/kg 09/01/15 21:23 75-27-46.8 2.6 1
Bromoform ND ug/kg 09/01/15 21:23 75-25-26.8 3.1 1
Bromomethane ND ug/kg 09/01/15 21:23 74-83-913.6 3.4 1
2-Butanone (MEK)ND ug/kg 09/01/15 21:23 78-93-3136 3.9 1
n-Butylbenzene ND ug/kg 09/01/15 21:23 104-51-86.8 2.4 1
sec-Butylbenzene ND ug/kg 09/01/15 21:23 135-98-86.8 2.2 1
tert-Butylbenzene ND ug/kg 09/01/15 21:23 98-06-66.8 2.7 1
Carbon tetrachloride ND ug/kg 09/01/15 21:23 56-23-56.8 3.5 1
Chlorobenzene ND ug/kg 09/01/15 21:23 108-90-76.8 2.6 1
Chloroethane ND ug/kg 09/01/15 21:23 75-00-313.6 3.3 1
Chloroform ND ug/kg 09/01/15 21:23 67-66-36.8 2.2 1
Chloromethane ND ug/kg 09/01/15 21:23 74-87-313.6 3.3 1
2-Chlorotoluene ND ug/kg 09/01/15 21:23 95-49-86.8 2.3 1
4-Chlorotoluene ND ug/kg 09/01/15 21:23 106-43-46.8 2.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/01/15 21:23 96-12-86.8 4.9 1
Dibromochloromethane ND ug/kg 09/01/15 21:23 124-48-16.8 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 09/01/15 21:23 106-93-46.8 2.4 1
Dibromomethane ND ug/kg 09/01/15 21:23 74-95-36.8 3.4 1
1,2-Dichlorobenzene ND ug/kg 09/01/15 21:23 95-50-16.8 2.6 1
1,3-Dichlorobenzene ND ug/kg 09/01/15 21:23 541-73-16.8 2.7 1
1,4-Dichlorobenzene ND ug/kg 09/01/15 21:23 106-46-76.8 2.3 1
Dichlorodifluoromethane ND ug/kg 09/01/15 21:23 75-71-813.6 4.9 1
1,1-Dichloroethane ND ug/kg 09/01/15 21:23 75-34-36.8 2.0 1
1,2-Dichloroethane ND ug/kg 09/01/15 21:23 107-06-26.8 3.0 1
1,1-Dichloroethene ND ug/kg 09/01/15 21:23 75-35-46.8 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Page 12 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Sample: SS-2 (16')Lab ID: 92265117002 Collected: 08/25/15 13:55 Received: 08/26/15 16:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
cis-1,2-Dichloroethene ND ug/kg 09/01/15 21:23 156-59-26.8 1.9 1
trans-1,2-Dichloroethene ND ug/kg 09/01/15 21:23 156-60-56.8 2.6 1
1,2-Dichloropropane ND ug/kg 09/01/15 21:23 78-87-56.8 2.3 1
1,3-Dichloropropane ND ug/kg 09/01/15 21:23 142-28-96.8 2.6 1
2,2-Dichloropropane ND ug/kg 09/01/15 21:23 594-20-76.8 2.3 1
1,1-Dichloropropene ND ug/kg 09/01/15 21:23 563-58-66.8 2.0 1
cis-1,3-Dichloropropene ND ug/kg 09/01/15 21:23 10061-01-56.8 2.4 1
trans-1,3-Dichloropropene ND ug/kg 09/01/15 21:23 10061-02-66.8 2.0 1
Diisopropyl ether ND ug/kg 09/01/15 21:23 108-20-36.8 2.3 1
Ethylbenzene ND ug/kg 09/01/15 21:23 100-41-46.8 2.4 1
Hexachloro-1,3-butadiene ND ug/kg 09/01/15 21:23 87-68-36.8 2.7 1
2-Hexanone ND ug/kg 09/01/15 21:23 591-78-667.8 5.3 1
Isopropylbenzene (Cumene)ND ug/kg 09/01/15 21:23 98-82-86.8 2.6 1
p-Isopropyltoluene ND ug/kg 09/01/15 21:23 99-87-66.8 2.3 1
Methylene Chloride ND ug/kg 09/01/15 21:23 75-09-227.1 4.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/01/15 21:23 108-10-167.8 5.0 1
Methyl-tert-butyl ether ND ug/kg 09/01/15 21:23 1634-04-46.8 2.0 1
Naphthalene ND ug/kg 09/01/15 21:23 91-20-36.8 1.6 1
n-Propylbenzene ND ug/kg 09/01/15 21:23 103-65-16.8 2.3 1
Styrene ND ug/kg 09/01/15 21:23 100-42-56.8 2.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/01/15 21:23 630-20-66.8 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/01/15 21:23 79-34-56.8 2.6 1
Tetrachloroethene ND ug/kg 09/01/15 21:23 127-18-46.8 2.3 1
Toluene ND ug/kg 09/01/15 21:23 108-88-36.8 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 09/01/15 21:23 87-61-66.8 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/01/15 21:23 120-82-16.8 2.2 1
1,1,1-Trichloroethane ND ug/kg 09/01/15 21:23 71-55-66.8 2.4 1
1,1,2-Trichloroethane ND ug/kg 09/01/15 21:23 79-00-56.8 2.8 1
Trichloroethene ND ug/kg 09/01/15 21:23 79-01-66.8 2.8 1
Trichlorofluoromethane ND ug/kg 09/01/15 21:23 75-69-46.8 3.0 1
1,2,3-Trichloropropane ND ug/kg 09/01/15 21:23 96-18-46.8 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 09/01/15 21:23 95-63-66.8 2.7 1
1,3,5-Trimethylbenzene ND ug/kg 09/01/15 21:23 108-67-86.8 2.4 1
Vinyl acetate ND ug/kg 09/01/15 21:23 108-05-4 L267.8 11.9 1
Vinyl chloride ND ug/kg 09/01/15 21:23 75-01-413.6 2.4 1
Xylene (Total)ND ug/kg 09/01/15 21:23 1330-20-713.6 4.9 1
m&p-Xylene ND ug/kg 09/01/15 21:23 179601-23-113.6 4.9 1
o-Xylene ND ug/kg 09/01/15 21:23 95-47-66.8 2.6 1
Surrogates
Toluene-d8 (S)100 %09/01/15 21:23 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %09/01/15 21:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/01/15 21:23 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.5 %08/27/15 13:020.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9800
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1546893
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 09/02/15 13:33
4-Bromofluorobenzene (S)%114 70-167 09/02/15 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1546894LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 50.650 101 70-165
4-Bromofluorobenzene (S)%105 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1546895MATRIX SPIKE SAMPLE:
MSSpike
Result
92265117001
Gas Range Organics (C6-C10)mg/kg 78.065 118 47-187ND
4-Bromofluorobenzene (S)%114 70-167
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265117002
1546896SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%115 5121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/9811
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1548030
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/03/15 16:14
Aliphatic (C09-C12)mg/kg ND 2.5 N209/03/15 16:14
Aromatic (C09-C10)mg/kg ND 2.5 N209/03/15 16:14
4-Bromofluorobenzene (FID) (S)%99 70-130 09/03/15 16:14
4-Bromofluorobenzene (PID) (S)%95 70-130 09/03/15 16:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1548031LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1548032
Aliphatic (C05-C08)mg/kg 14.2 N2159570-1309213.8 3 25
Aliphatic (C09-C12)mg/kg 16.1 N21510730-13010816.2 1 25
Aromatic (C09-C10)mg/kg 4.7 N259470-130924.6 1 25
4-Bromofluorobenzene (FID) (S)%101 70-130102
4-Bromofluorobenzene (PID) (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/33209
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1546006
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.7 09/01/15 13:44
1,1,1-Trichloroethane ug/kg ND 4.7 09/01/15 13:44
1,1,2,2-Tetrachloroethane ug/kg ND 4.7 09/01/15 13:44
1,1,2-Trichloroethane ug/kg ND 4.7 09/01/15 13:44
1,1-Dichloroethane ug/kg ND 4.7 09/01/15 13:44
1,1-Dichloroethene ug/kg ND 4.7 09/01/15 13:44
1,1-Dichloropropene ug/kg ND 4.7 09/01/15 13:44
1,2,3-Trichlorobenzene ug/kg ND 4.7 09/01/15 13:44
1,2,3-Trichloropropane ug/kg ND 4.7 09/01/15 13:44
1,2,4-Trichlorobenzene ug/kg ND 4.7 09/01/15 13:44
1,2,4-Trimethylbenzene ug/kg ND 4.7 09/01/15 13:44
1,2-Dibromo-3-chloropropane ug/kg ND 4.7 09/01/15 13:44
1,2-Dibromoethane (EDB)ug/kg ND 4.7 09/01/15 13:44
1,2-Dichlorobenzene ug/kg ND 4.7 09/01/15 13:44
1,2-Dichloroethane ug/kg ND 4.7 09/01/15 13:44
1,2-Dichloropropane ug/kg ND 4.7 09/01/15 13:44
1,3,5-Trimethylbenzene ug/kg ND 4.7 09/01/15 13:44
1,3-Dichlorobenzene ug/kg ND 4.7 09/01/15 13:44
1,3-Dichloropropane ug/kg ND 4.7 09/01/15 13:44
1,4-Dichlorobenzene ug/kg ND 4.7 09/01/15 13:44
2,2-Dichloropropane ug/kg ND 4.7 09/01/15 13:44
2-Butanone (MEK)ug/kg ND 93.5 09/01/15 13:44
2-Chlorotoluene ug/kg ND 4.7 09/01/15 13:44
2-Hexanone ug/kg ND 46.7 09/01/15 13:44
4-Chlorotoluene ug/kg ND 4.7 09/01/15 13:44
4-Methyl-2-pentanone (MIBK)ug/kg ND 46.7 09/01/15 13:44
Acetone ug/kg ND 93.5 09/01/15 13:44
Benzene ug/kg ND 4.7 09/01/15 13:44
Bromobenzene ug/kg ND 4.7 09/01/15 13:44
Bromochloromethane ug/kg ND 4.7 09/01/15 13:44
Bromodichloromethane ug/kg ND 4.7 09/01/15 13:44
Bromoform ug/kg ND 4.7 09/01/15 13:44
Bromomethane ug/kg ND 9.3 09/01/15 13:44
Carbon tetrachloride ug/kg ND 4.7 09/01/15 13:44
Chlorobenzene ug/kg ND 4.7 09/01/15 13:44
Chloroethane ug/kg ND 9.3 09/01/15 13:44
Chloroform ug/kg ND 4.7 09/01/15 13:44
Chloromethane ug/kg ND 9.3 09/01/15 13:44
cis-1,2-Dichloroethene ug/kg ND 4.7 09/01/15 13:44
cis-1,3-Dichloropropene ug/kg ND 4.7 09/01/15 13:44
Dibromochloromethane ug/kg ND 4.7 09/01/15 13:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1546006
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 4.7 09/01/15 13:44
Dichlorodifluoromethane ug/kg ND 9.3 09/01/15 13:44
Diisopropyl ether ug/kg ND 4.7 09/01/15 13:44
Ethylbenzene ug/kg ND 4.7 09/01/15 13:44
Hexachloro-1,3-butadiene ug/kg ND 4.7 09/01/15 13:44
Isopropylbenzene (Cumene)ug/kg ND 4.7 09/01/15 13:44
m&p-Xylene ug/kg ND 9.3 09/01/15 13:44
Methyl-tert-butyl ether ug/kg ND 4.7 09/01/15 13:44
Methylene Chloride ug/kg ND 18.7 09/01/15 13:44
n-Butylbenzene ug/kg ND 4.7 09/01/15 13:44
n-Propylbenzene ug/kg ND 4.7 09/01/15 13:44
Naphthalene ug/kg ND 4.7 09/01/15 13:44
o-Xylene ug/kg ND 4.7 09/01/15 13:44
p-Isopropyltoluene ug/kg ND 4.7 09/01/15 13:44
sec-Butylbenzene ug/kg ND 4.7 09/01/15 13:44
Styrene ug/kg ND 4.7 09/01/15 13:44
tert-Butylbenzene ug/kg ND 4.7 09/01/15 13:44
Tetrachloroethene ug/kg ND 4.7 09/01/15 13:44
Toluene ug/kg ND 4.7 09/01/15 13:44
trans-1,2-Dichloroethene ug/kg ND 4.7 09/01/15 13:44
trans-1,3-Dichloropropene ug/kg ND 4.7 09/01/15 13:44
Trichloroethene ug/kg ND 4.7 09/01/15 13:44
Trichlorofluoromethane ug/kg ND 4.7 09/01/15 13:44
Vinyl acetate ug/kg ND 46.7 09/01/15 13:44
Vinyl chloride ug/kg ND 9.3 09/01/15 13:44
Xylene (Total)ug/kg ND 9.3 09/01/15 13:44
1,2-Dichloroethane-d4 (S)%94 70-132 09/01/15 13:44
4-Bromofluorobenzene (S)%93 70-130 09/01/15 13:44
Toluene-d8 (S)%100 70-130 09/01/15 13:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1546007LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.352.2 98 74-137
1,1,1-Trichloroethane ug/kg 48.352.2 93 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.252.2 88 72-141
1,1,2-Trichloroethane ug/kg 49.852.2 95 78-138
1,1-Dichloroethane ug/kg 48.752.2 93 69-134
1,1-Dichloroethene ug/kg 50.652.2 97 67-138
1,1-Dichloropropene ug/kg 51.152.2 98 69-139
1,2,3-Trichlorobenzene ug/kg 55.352.2 106 70-146
1,2,3-Trichloropropane ug/kg 54.552.2 104 69-144
1,2,4-Trichlorobenzene ug/kg 51.652.2 99 68-148
1,2,4-Trimethylbenzene ug/kg 55.452.2 106 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1546007LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.252.2 98 65-140
1,2-Dibromoethane (EDB)ug/kg 53.452.2 102 77-135
1,2-Dichlorobenzene ug/kg 54.952.2 105 77-141
1,2-Dichloroethane ug/kg 48.552.2 93 65-137
1,2-Dichloropropane ug/kg 50.352.2 96 72-136
1,3,5-Trimethylbenzene ug/kg 55.552.2 106 76-133
1,3-Dichlorobenzene ug/kg 55.352.2 106 74-138
1,3-Dichloropropane ug/kg 49.952.2 96 71-139
1,4-Dichlorobenzene ug/kg 53.952.2 103 76-138
2,2-Dichloropropane ug/kg 49.952.2 96 68-137
2-Butanone (MEK)ug/kg 97.0J104 93 58-147
2-Chlorotoluene ug/kg 60.652.2 116 73-139
2-Hexanone ug/kg 114104 109 62-145
4-Chlorotoluene ug/kg 53.752.2 103 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 113104 108 64-149
Acetone ug/kg 95.8J104 92 53-153
Benzene ug/kg 50.852.2 97 73-135
Bromobenzene ug/kg 57.552.2 110 75-133
Bromochloromethane ug/kg 49.352.2 94 73-134
Bromodichloromethane ug/kg 50.952.2 98 71-135
Bromoform ug/kg 50.252.2 96 66-141
Bromomethane ug/kg 56.652.2 108 53-160
Carbon tetrachloride ug/kg 48.852.2 93 60-145
Chlorobenzene ug/kg 52.152.2 100 78-130
Chloroethane ug/kg 48.552.2 93 64-149
Chloroform ug/kg 51.652.2 99 70-134
Chloromethane ug/kg 46.652.2 89 52-150
cis-1,2-Dichloroethene ug/kg 50.852.2 97 70-133
cis-1,3-Dichloropropene ug/kg 51.652.2 99 68-134
Dibromochloromethane ug/kg 52.552.2 101 71-138
Dibromomethane ug/kg 49.252.2 94 74-130
Dichlorodifluoromethane ug/kg 42.152.2 81 40-160
Diisopropyl ether ug/kg 51.952.2 99 69-141
Ethylbenzene ug/kg 51.852.2 99 75-133
Hexachloro-1,3-butadiene ug/kg 54.452.2 104 68-143
Isopropylbenzene (Cumene)ug/kg 57.952.2 111 76-143
m&p-Xylene ug/kg 105104 100 75-136
Methyl-tert-butyl ether ug/kg 50.852.2 97 68-144
Methylene Chloride ug/kg 52.652.2 101 45-154
n-Butylbenzene ug/kg 54.552.2 104 72-137
n-Propylbenzene ug/kg 54.252.2 104 76-136
Naphthalene ug/kg 56.752.2 109 68-151
o-Xylene ug/kg 54.152.2 104 76-141
p-Isopropyltoluene ug/kg 55.152.2 106 76-140
sec-Butylbenzene ug/kg 57.152.2 109 79-139
Styrene ug/kg 54.952.2 105 79-137
tert-Butylbenzene ug/kg 50.452.2 97 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Page 18 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1546007LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 46.752.2 89 71-138
Toluene ug/kg 51.452.2 99 74-131
trans-1,2-Dichloroethene ug/kg 51.752.2 99 67-135
trans-1,3-Dichloropropene ug/kg 52.152.2 100 65-146
Trichloroethene ug/kg 52.852.2 101 67-135
Trichlorofluoromethane ug/kg 41.852.2 80 59-144
Vinyl acetate ug/kg 35.7J F3,L010434 40-160
Vinyl chloride ug/kg 47.052.2 90 56-141
Xylene (Total)ug/kg 159157 101 76-137
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1546645MATRIX SPIKE SAMPLE:
MSSpike
Result
92265516005
1,1,1,2-Tetrachloroethane ug/kg 24.023.9 100 70-130ND
1,1,1-Trichloroethane ug/kg 22.023.9 92 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 28.123.9 118 70-130ND
1,1,2-Trichloroethane ug/kg 24.423.9 102 70-130ND
1,1-Dichloroethane ug/kg 22.123.9 93 70-130ND
1,1-Dichloroethene ug/kg 22.023.9 92 49-180ND
1,1-Dichloropropene ug/kg 23.523.9 98 70-130ND
1,2,3-Trichlorobenzene ug/kg 25.423.9 106 70-130ND
1,2,3-Trichloropropane ug/kg 26.723.9 112 70-130ND
1,2,4-Trichlorobenzene ug/kg 24.023.9 101 70-130ND
1,2,4-Trimethylbenzene ug/kg 25.823.9 108 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 26.423.9 111 70-130ND
1,2-Dibromoethane (EDB)ug/kg 26.823.9 112 70-130ND
1,2-Dichlorobenzene ug/kg 25.723.9 108 70-130ND
1,2-Dichloroethane ug/kg 23.523.9 98 70-130ND
1,2-Dichloropropane ug/kg 23.123.9 97 70-130ND
1,3,5-Trimethylbenzene ug/kg 25.723.9 108 70-130ND
1,3-Dichlorobenzene ug/kg 25.723.9 108 70-130ND
1,3-Dichloropropane ug/kg 24.323.9 102 70-130ND
1,4-Dichlorobenzene ug/kg 25.323.9 106 70-130ND
2,2-Dichloropropane ug/kg 22.123.9 92 70-130ND
2-Butanone (MEK)ug/kg 49.8J47.7 104 70-130ND
2-Chlorotoluene ug/kg 25.323.9 106 70-130ND
2-Hexanone ug/kg 57.1J47.7 120 70-130ND
4-Chlorotoluene ug/kg 25.223.9 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 55.4J47.7 116 70-130ND
Acetone ug/kg 69.9J47.7 114 70-1300.015J mg/kg
Benzene ug/kg 24.123.9 101 50-166ND
Bromobenzene ug/kg 25.923.9 108 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Eden, NC 27288
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Page 19 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1546645MATRIX SPIKE SAMPLE:
MSSpike
Result
92265516005
Bromochloromethane ug/kg 24.023.9 100 70-130ND
Bromodichloromethane ug/kg 23.823.9 100 70-130ND
Bromoform ug/kg 22.423.9 94 70-130ND
Bromomethane ug/kg 21.123.9 88 70-130ND
Carbon tetrachloride ug/kg 22.823.9 95 70-130ND
Chlorobenzene ug/kg 24.823.9 104 43-169ND
Chloroethane ug/kg 22.023.9 92 70-130ND
Chloroform ug/kg 23.123.9 97 70-130ND
Chloromethane ug/kg 18.923.9 79 70-130ND
cis-1,2-Dichloroethene ug/kg 23.123.9 97 70-130ND
cis-1,3-Dichloropropene ug/kg 23.923.9 100 70-130ND
Dibromochloromethane ug/kg 23.223.9 97 70-130ND
Dibromomethane ug/kg 24.123.9 101 70-130ND
Dichlorodifluoromethane ug/kg 14.3 M123.9 60 70-130ND
Diisopropyl ether ug/kg 24.123.9 101 70-130ND
Ethylbenzene ug/kg 24.823.9 104 70-130ND
Hexachloro-1,3-butadiene ug/kg 24.323.9 102 70-130ND
Isopropylbenzene (Cumene)ug/kg 28.023.9 117 70-130ND
m&p-Xylene ug/kg 50.647.7 106 70-130ND
Methyl-tert-butyl ether ug/kg 24.523.9 103 70-130ND
Methylene Chloride ug/kg 28.723.9 99 70-1300.0049J mg/kg
n-Butylbenzene ug/kg 26.123.9 109 70-130ND
n-Propylbenzene ug/kg 26.023.9 109 70-130ND
Naphthalene ug/kg ND M123.9 1 70-130ND
o-Xylene ug/kg 25.323.9 106 70-130ND
p-Isopropyltoluene ug/kg 25.823.9 108 70-130ND
sec-Butylbenzene ug/kg 26.923.9 113 70-130ND
Styrene ug/kg 25.323.9 106 70-130ND
tert-Butylbenzene ug/kg 23.523.9 98 70-130ND
Tetrachloroethene ug/kg 23.323.9 97 70-130ND
Toluene ug/kg 23.923.9 99 52-163ND
trans-1,2-Dichloroethene ug/kg 23.323.9 97 70-130ND
trans-1,3-Dichloropropene ug/kg 24.223.9 101 70-130ND
Trichloroethene ug/kg 22.023.9 92 49-167ND
Trichlorofluoromethane ug/kg 20.723.9 87 70-130ND
Vinyl acetate ug/kg 60.747.7 127 70-130ND
Vinyl chloride ug/kg 20.323.9 85 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265287001
1546644SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30<8.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Eden, NC 27288
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Page 20 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265287001
1546644SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30<8.1
1,1,2,2-Tetrachloroethane ug/kg ND 30<8.1
1,1,2-Trichloroethane ug/kg ND 30<8.1
1,1-Dichloroethane ug/kg ND 30<8.1
1,1-Dichloroethene ug/kg ND 30<8.1
1,1-Dichloropropene ug/kg ND 30<8.1
1,2,3-Trichlorobenzene ug/kg ND 30<8.1
1,2,3-Trichloropropane ug/kg ND 30<8.1
1,2,4-Trichlorobenzene ug/kg ND 30<8.1
1,2,4-Trimethylbenzene ug/kg ND 30<8.1
1,2-Dibromo-3-chloropropane ug/kg ND 30<8.1
1,2-Dibromoethane (EDB)ug/kg ND 30<8.1
1,2-Dichlorobenzene ug/kg ND 30<8.1
1,2-Dichloroethane ug/kg ND 30<8.1
1,2-Dichloropropane ug/kg ND 30<8.1
1,3,5-Trimethylbenzene ug/kg ND 30<8.1
1,3-Dichlorobenzene ug/kg ND 30<8.1
1,3-Dichloropropane ug/kg ND 30<8.1
1,4-Dichlorobenzene ug/kg ND 30<8.1
2,2-Dichloropropane ug/kg ND 30<8.1
2-Butanone (MEK)ug/kg ND 30<161
2-Chlorotoluene ug/kg ND 30<8.1
2-Hexanone ug/kg ND 30<80.5
4-Chlorotoluene ug/kg ND 30<8.1
4-Methyl-2-pentanone (MIBK)ug/kg ND 30<80.5
Acetone ug/kg 138 3033.8J
Benzene ug/kg ND 30<8.1
Bromobenzene ug/kg ND 30<8.1
Bromochloromethane ug/kg ND 30<8.1
Bromodichloromethane ug/kg ND 30<8.1
Bromoform ug/kg ND 30<8.1
Bromomethane ug/kg ND 30<16.1
Carbon tetrachloride ug/kg ND 30<8.1
Chlorobenzene ug/kg ND 30<8.1
Chloroethane ug/kg ND 30<16.1
Chloroform ug/kg ND 30<8.1
Chloromethane ug/kg ND 30<16.1
cis-1,2-Dichloroethene ug/kg ND 30<8.1
cis-1,3-Dichloropropene ug/kg ND 30<8.1
Dibromochloromethane ug/kg ND 30<8.1
Dibromomethane ug/kg ND 30<8.1
Dichlorodifluoromethane ug/kg ND 30<16.1
Diisopropyl ether ug/kg ND 30<8.1
Ethylbenzene ug/kg ND 30<8.1
Hexachloro-1,3-butadiene ug/kg ND 30<8.1
Isopropylbenzene (Cumene)ug/kg ND 30<8.1
m&p-Xylene ug/kg ND 30<16.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
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Page 21 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265287001
1546644SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30<8.1
Methylene Chloride ug/kg 95.4 C93020.1J
n-Butylbenzene ug/kg ND 30<8.1
n-Propylbenzene ug/kg ND 30<8.1
Naphthalene ug/kg 1.7J 30<8.1
o-Xylene ug/kg ND 30<8.1
p-Isopropyltoluene ug/kg ND 30<8.1
sec-Butylbenzene ug/kg ND 30<8.1
Styrene ug/kg ND 30<8.1
tert-Butylbenzene ug/kg ND 30<8.1
Tetrachloroethene ug/kg ND 30<8.1
Toluene ug/kg ND 30<8.1
trans-1,2-Dichloroethene ug/kg ND 30<8.1
trans-1,3-Dichloropropene ug/kg ND 30<8.1
Trichloroethene ug/kg ND 30<8.1
Trichlorofluoromethane ug/kg ND 30<8.1
Vinyl acetate ug/kg ND 30<80.5
Vinyl chloride ug/kg ND 30<16.1
Xylene (Total)ug/kg ND 30<16.1
1,2-Dichloroethane-d4 (S)%107 29107
4-Bromofluorobenzene (S)%96 2895
Toluene-d8 (S)%102 IS28100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37430
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1545248
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 09/01/15 10:41
n-Pentacosane (S)%90 41-119 09/01/15 10:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545249LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1545259
Diesel Range Organics(C10-C28)mg/kg 56.066.7 84 49-1138254.8 2 30
n-Pentacosane (S)%91 41-11985
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37442
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1545554
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 09/02/15 09:31
1,2-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1,3-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1,4-Dichlorobenzene ug/kg ND 330 09/02/15 09:31
1-Methylnaphthalene ug/kg ND 330 09/02/15 09:31
2,4,5-Trichlorophenol ug/kg ND 330 09/02/15 09:31
2,4,6-Trichlorophenol ug/kg ND 330 09/02/15 09:31
2,4-Dichlorophenol ug/kg ND 330 09/02/15 09:31
2,4-Dimethylphenol ug/kg ND 330 09/02/15 09:31
2,4-Dinitrophenol ug/kg ND 1650 09/02/15 09:31
2,4-Dinitrotoluene ug/kg ND 330 09/02/15 09:31
2,6-Dinitrotoluene ug/kg ND 330 09/02/15 09:31
2-Chloronaphthalene ug/kg ND 330 09/02/15 09:31
2-Chlorophenol ug/kg ND 330 09/02/15 09:31
2-Methylnaphthalene ug/kg ND 330 09/02/15 09:31
2-Methylphenol(o-Cresol)ug/kg ND 330 09/02/15 09:31
2-Nitroaniline ug/kg ND 1650 09/02/15 09:31
2-Nitrophenol ug/kg ND 330 09/02/15 09:31
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 09/02/15 09:31
3,3'-Dichlorobenzidine ug/kg ND 1650 09/02/15 09:31
3-Nitroaniline ug/kg ND 1650 09/02/15 09:31
4,6-Dinitro-2-methylphenol ug/kg ND 660 09/02/15 09:31
4-Bromophenylphenyl ether ug/kg ND 330 09/02/15 09:31
4-Chloro-3-methylphenol ug/kg ND 660 09/02/15 09:31
4-Chloroaniline ug/kg ND 1650 09/02/15 09:31
4-Chlorophenylphenyl ether ug/kg ND 330 09/02/15 09:31
4-Nitroaniline ug/kg ND 660 09/02/15 09:31
4-Nitrophenol ug/kg 127J 1650 09/02/15 09:31
Acenaphthene ug/kg ND 330 09/02/15 09:31
Acenaphthylene ug/kg ND 330 09/02/15 09:31
Aniline ug/kg ND 330 09/02/15 09:31
Anthracene ug/kg ND 330 09/02/15 09:31
Benzo(a)anthracene ug/kg ND 330 09/02/15 09:31
Benzo(a)pyrene ug/kg ND 330 09/02/15 09:31
Benzo(b)fluoranthene ug/kg ND 330 09/02/15 09:31
Benzo(g,h,i)perylene ug/kg ND 330 09/02/15 09:31
Benzo(k)fluoranthene ug/kg ND 330 09/02/15 09:31
Benzoic Acid ug/kg ND 1650 09/02/15 09:31
Benzyl alcohol ug/kg ND 660 09/02/15 09:31
bis(2-Chloroethoxy)methane ug/kg ND 330 09/02/15 09:31
bis(2-Chloroethyl) ether ug/kg ND 330 09/02/15 09:31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1545554
Associated Lab Samples:92265117001, 92265117002
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 09/02/15 09:31
bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/02/15 09:31
Butylbenzylphthalate ug/kg ND 330 09/02/15 09:31
Chrysene ug/kg 57.8J 330 09/02/15 09:31
Di-n-butylphthalate ug/kg ND 330 09/02/15 09:31
Di-n-octylphthalate ug/kg ND 330 09/02/15 09:31
Dibenz(a,h)anthracene ug/kg ND 330 09/02/15 09:31
Dibenzofuran ug/kg ND 330 09/02/15 09:31
Diethylphthalate ug/kg ND 330 09/02/15 09:31
Dimethylphthalate ug/kg ND 330 09/02/15 09:31
Fluoranthene ug/kg ND 330 09/02/15 09:31
Fluorene ug/kg ND 330 09/02/15 09:31
Hexachloro-1,3-butadiene ug/kg ND 330 09/02/15 09:31
Hexachlorobenzene ug/kg ND 330 09/02/15 09:31
Hexachlorocyclopentadiene ug/kg ND 330 09/02/15 09:31
Hexachloroethane ug/kg ND 330 09/02/15 09:31
Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/02/15 09:31
Isophorone ug/kg ND 330 09/02/15 09:31
N-Nitroso-di-n-propylamine ug/kg ND 330 09/02/15 09:31
N-Nitrosodimethylamine ug/kg ND 330 09/02/15 09:31
N-Nitrosodiphenylamine ug/kg ND 330 09/02/15 09:31
Naphthalene ug/kg ND 330 09/02/15 09:31
Nitrobenzene ug/kg ND 330 09/02/15 09:31
Pentachlorophenol ug/kg ND 1650 09/02/15 09:31
Phenanthrene ug/kg ND 330 09/02/15 09:31
Phenol ug/kg ND 330 09/02/15 09:31
Pyrene ug/kg ND 330 09/02/15 09:31
2,4,6-Tribromophenol (S)%94 27-110 09/02/15 09:31
2-Fluorobiphenyl (S)%75 30-110 09/02/15 09:31
2-Fluorophenol (S)%76 13-110 09/02/15 09:31
Nitrobenzene-d5 (S)%79 23-110 09/02/15 09:31
Phenol-d6 (S)%76 22-110 09/02/15 09:31
Terphenyl-d14 (S)%101 28-110 09/02/15 09:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14901670 89 36-120
1,2-Dichlorobenzene ug/kg 13501670 81 41-120
1,3-Dichlorobenzene ug/kg 12901670 77 66-120
1,4-Dichlorobenzene ug/kg 12901670 78 42-120
1-Methylnaphthalene ug/kg 14501670 87 40-120
2,4,5-Trichlorophenol ug/kg 13401670 81 37-120
2,4,6-Trichlorophenol ug/kg 14801670 89 40-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
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Page 25 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 15201670 91 33-120
2,4-Dimethylphenol ug/kg 14501670 87 36-120
2,4-Dinitrophenol ug/kg 76108330 91 22-121
2,4-Dinitrotoluene ug/kg 15901670 95 60-120
2,6-Dinitrotoluene ug/kg 15101670 91 54-120
2-Chloronaphthalene ug/kg 13501670 81 41-120
2-Chlorophenol ug/kg 13301670 80 39-120
2-Methylnaphthalene ug/kg 14001670 84 26-120
2-Methylphenol(o-Cresol)ug/kg 12201670 73 41-120
2-Nitroaniline ug/kg 24103330 72 45-120
2-Nitrophenol ug/kg 14801670 89 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 11801670 71 35-120
3,3'-Dichlorobenzidine ug/kg 28503330 85 16-125
3-Nitroaniline ug/kg 28003330 84 45-120
4,6-Dinitro-2-methylphenol ug/kg 33003330 99 46-120
4-Bromophenylphenyl ether ug/kg 14701670 88 36-120
4-Chloro-3-methylphenol ug/kg 30303330 91 37-120
4-Chloroaniline ug/kg 25003330 75 35-120
4-Chlorophenylphenyl ether ug/kg 14801670 89 30-120
4-Nitroaniline ug/kg 30303330 91 48-120
4-Nitrophenol ug/kg 80508330 97 43-120
Acenaphthene ug/kg 13401670 81 46-120
Acenaphthylene ug/kg 14001670 84 46-120
Aniline ug/kg 10601670 64 33-120
Anthracene ug/kg 14901670 90 63-120
Benzo(a)anthracene ug/kg 14901670 90 61-120
Benzo(a)pyrene ug/kg 16001670 96 59-120
Benzo(b)fluoranthene ug/kg 16201670 97 55-120
Benzo(g,h,i)perylene ug/kg 14701670 88 57-120
Benzo(k)fluoranthene ug/kg 19101670 115 56-120
Benzoic Acid ug/kg 52508330 63 13-120
Benzyl alcohol ug/kg 25003330 75 34-120
bis(2-Chloroethoxy)methane ug/kg 12901670 77 21-120
bis(2-Chloroethyl) ether ug/kg 10601670 64 25-120
bis(2-Chloroisopropyl) ether ug/kg 10201670 61 13-120
bis(2-Ethylhexyl)phthalate ug/kg 15501670 93 56-123
Butylbenzylphthalate ug/kg 15401670 93 57-120
Chrysene ug/kg 14101670 85 64-120
Di-n-butylphthalate ug/kg 16501670 99 58-120
Di-n-octylphthalate ug/kg 14101670 85 47-121
Dibenz(a,h)anthracene ug/kg 15901670 95 56-120
Dibenzofuran ug/kg 14201670 85 43-120
Diethylphthalate ug/kg 15601670 94 55-120
Dimethylphthalate ug/kg 14701670 88 54-120
Fluoranthene ug/kg 16601670 100 61-120
Fluorene ug/kg 14901670 90 51-120
Hexachloro-1,3-butadiene ug/kg 15501670 93 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545555LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 16901670 102 53-120
Hexachlorocyclopentadiene ug/kg 13801670 83 18-150
Hexachloroethane ug/kg 13201670 79 39-120
Indeno(1,2,3-cd)pyrene ug/kg 15601670 94 58-120
Isophorone ug/kg 12301670 74 38-120
N-Nitroso-di-n-propylamine ug/kg 11601670 70 30-120
N-Nitrosodimethylamine ug/kg 11101670 67 32-120
N-Nitrosodiphenylamine ug/kg 13401670 80 50-120
Naphthalene ug/kg 13501670 81 38-120
Nitrobenzene ug/kg 12501670 75 37-120
Pentachlorophenol ug/kg 31303330 94 10-120
Phenanthrene ug/kg 14001670 84 62-120
Phenol ug/kg 13901670 83 37-120
Pyrene ug/kg 14901670 89 63-120
2,4,6-Tribromophenol (S)%98 27-110
2-Fluorobiphenyl (S)%77 30-110
2-Fluorophenol (S)%84 13-110
Nitrobenzene-d5 (S)%83 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%95 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
1,2,4-Trichlorobenzene ug/kg 13801880 74 18-119ND
1,2-Dichlorobenzene ug/kg 12401880 66 50-110ND
1,3-Dichlorobenzene ug/kg 12001880 64 27-110ND
1,4-Dichlorobenzene ug/kg 12201880 65 28-110ND
1-Methylnaphthalene ug/kg 14901880 80 24-116ND
2,4,5-Trichlorophenol ug/kg 13301880 71 28-110ND
2,4,6-Trichlorophenol ug/kg 13101880 70 17-117ND
2,4-Dichlorophenol ug/kg 13001880 69 21-128ND
2,4-Dimethylphenol ug/kg 5551880 30 10-120ND
2,4-Dinitrophenol ug/kg 82509360 88 10-107ND
2,4-Dinitrotoluene ug/kg 16001880 85 36-109ND
2,6-Dinitrotoluene ug/kg 15101880 80 32-110ND
2-Chloronaphthalene ug/kg 12801880 68 30-107ND
2-Chlorophenol ug/kg 11601880 62 14-106ND
2-Methylnaphthalene ug/kg 14501880 77 10-135ND
2-Methylphenol(o-Cresol)ug/kg 7781880 42 10-124ND
2-Nitroaniline ug/kg 23603740 63 26-116ND
2-Nitrophenol ug/kg 13401880 71 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 8431880 45 10-109ND
3,3'-Dichlorobenzidine ug/kg 385J3740 10 10-150ND
3-Nitroaniline ug/kg 24903740 67 22-110ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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Eden, NC 27288
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
4,6-Dinitro-2-methylphenol ug/kg 33303740 89 13-121ND
4-Bromophenylphenyl ether ug/kg 14701880 78 31-109ND
4-Chloro-3-methylphenol ug/kg 27403740 73 13-128ND
4-Chloroaniline ug/kg 1550J3740 41 18-102ND
4-Chlorophenylphenyl ether ug/kg 14901880 80 29-112ND
4-Nitroaniline ug/kg 26103740 67 16-111ND
4-Nitrophenol ug/kg 76309360 79 14-135ND
Acenaphthene ug/kg 13201880 70 26-114ND
Acenaphthylene ug/kg 13401880 72 32-108ND
Aniline ug/kg 225J1880 12 10-107ND
Anthracene ug/kg 14501880 77 32-111ND
Benzo(a)anthracene ug/kg 14701880 74 25-117ND
Benzo(a)pyrene ug/kg 15101880 78 25-106ND
Benzo(b)fluoranthene ug/kg 16101880 86 24-110ND
Benzo(g,h,i)perylene ug/kg 13901880 74 19-112ND
Benzo(k)fluoranthene ug/kg 18601880 99 24-114ND
Benzoic Acid ug/kg 56909360 61 10-110ND
Benzyl alcohol ug/kg 23003740 61 24-106ND
bis(2-Chloroethoxy)methane ug/kg 12201880 65 13-119ND
bis(2-Chloroethyl) ether ug/kg 225J1880 12 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 9521880 51 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 15301880 78 10-125ND
Butylbenzylphthalate ug/kg 15701880 80 18-110ND
Chrysene ug/kg 14201880 71 30-110ND
Di-n-butylphthalate ug/kg 15401880 79 19-112ND
Di-n-octylphthalate ug/kg 14801880 79 17-105ND
Dibenz(a,h)anthracene ug/kg 14301880 76 23-111ND
Dibenzofuran ug/kg 14201880 76 35-103ND
Diethylphthalate ug/kg 15401880 82 27-113ND
Dimethylphthalate ug/kg 14501880 77 26-111ND
Fluoranthene ug/kg 15701880 79 33-109ND
Fluorene ug/kg 15001880 80 32-113ND
Hexachloro-1,3-butadiene ug/kg 14701880 78 16-116ND
Hexachlorobenzene ug/kg 16701880 89 27-120ND
Hexachlorocyclopentadiene ug/kg 11901880 64 10-108ND
Hexachloroethane ug/kg 12501880 67 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 14701880 78 10-122ND
Isophorone ug/kg 12001880 64 28-114ND
N-Nitroso-di-n-propylamine ug/kg 11101880 59 27-113ND
N-Nitrosodimethylamine ug/kg 9291880 50 10-109ND
N-Nitrosodiphenylamine ug/kg 9491880 51 10-128ND
Naphthalene ug/kg 13201880 71 25-110ND
Nitrobenzene ug/kg 11501880 61 18-114ND
Pentachlorophenol ug/kg 30803740 80 10-122ND
Phenanthrene ug/kg 14001880 73 30-114ND
Phenol ug/kg 10401880 56 11-102ND
Pyrene ug/kg 14401880 72 25-116ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1545556MATRIX SPIKE SAMPLE:
MSSpike
Result
92265315005
2,4,6-Tribromophenol (S)%74 27-110
2-Fluorobiphenyl (S)%63 30-110
2-Fluorophenol (S)%54 13-110
Nitrobenzene-d5 (S)%65 23-110
Phenol-d6 (S)%56 22-110
Terphenyl-d14 (S)%80 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265315008
1545557SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg 69.3J 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265315008
1545557SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 57.0J 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%64 1876
2-Fluorobiphenyl (S)%61 1571
2-Fluorophenol (S)%41 2352
Nitrobenzene-d5 (S)%61 1370
Phenol-d6 (S)%46 2861
Terphenyl-d14 (S)%78 1288
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37399
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92265117001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1544326
Associated Lab Samples:92265117001
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N208/30/15 13:53
Aliphatic (C19-C36)mg/kg ND 10.0 N208/30/15 13:53
Aromatic (C11-C22)mg/kg ND 10.0 N208/30/15 13:53
2-Bromonaphthalene (S)%104 40-140 08/30/15 13:53
2-Fluorobiphenyl (S)%99 40-140 08/30/15 13:53
Nonatriacontane (S)%76 40-140 08/30/15 13:53
o-Terphenyl (S)%84 40-140 08/30/15 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1544327LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1544328
Aliphatic (C09-C18)mg/kg ND N2105740-14071ND 50
Aliphatic (C19-C36)mg/kg ND N213.3 66 40-1407910.6 50
Aromatic (C11-C22)mg/kg 20.7 N228.3 73 40-1409526.9 26 50
2-Bromonaphthalene (S)%83 40-140101
2-Fluorobiphenyl (S)%82 40-140107
Nonatriacontane (S)%69 40-14080
o-Terphenyl (S)%68 40-14093
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 31 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/37438
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92265117002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1545530
Associated Lab Samples:92265117002
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N209/01/15 13:55
Aliphatic (C19-C36)mg/kg ND 10.0 N209/01/15 13:55
Aromatic (C11-C22)mg/kg ND 10.0 N209/01/15 13:55
2-Bromonaphthalene (S)%109 40-140 09/01/15 13:55
2-Fluorobiphenyl (S)%106 40-140 09/01/15 13:55
Nonatriacontane (S)%85 40-140 09/01/15 13:55
o-Terphenyl (S)%96 40-140 09/01/15 13:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1545531LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1545532
Aliphatic (C09-C18)mg/kg ND N2108340-14076ND 50
Aliphatic (C19-C36)mg/kg 12.2 N213.3 91 40-1408411.2 9 50
Aromatic (C11-C22)mg/kg 32.2 N228.3 114 40-14011532.6 1 50
2-Bromonaphthalene (S)%109 40-140138
2-Fluorobiphenyl (S)%117 40-140139
Nonatriacontane (S)%90 40-14082
o-Terphenyl (S)%106 40-140106
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 32 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8294
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92265117001, 92265117002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92264014001
1542434SAMPLE DUPLICATE:
Percent Moisture %20.9 6 2522.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92265117002
1542435SAMPLE DUPLICATE:
Percent Moisture %10.9 3 2510.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/08/2015 04:28 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 33 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
The internal standard response is below criteria. Results may be biased high.IS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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Eden, NC 27288
[phone]
Page 34 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92265117
SUN CAP 1404 OLD GREENSBORO RD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92265117001 OEXT/37430 GCSV/22458SS-1 (17')EPA 3546 EPA 8015 Modified
92265117002 OEXT/37430 GCSV/22458SS-2 (16')EPA 3546 EPA 8015 Modified
92265117001 OEXT/37399 GCSV/22442SS-1 (17')MADEP EPH MADEP EPH
92265117002 OEXT/37438 GCSV/22469SS-2 (16')MADEP EPH MADEP EPH
92265117001 GCV/9800 GCV/9807SS-1 (17')EPA 5035A/5030B EPA 8015 Modified
92265117002 GCV/9800 GCV/9807SS-2 (16')EPA 5035A/5030B EPA 8015 Modified
92265117001 GCV/9811 GCV/9814SS-1 (17')MADEP VPH MADEP VPH
92265117002 GCV/9811 GCV/9814SS-2 (16')MADEP VPH MADEP VPH
92265117001 OEXT/37442 MSSV/11169SS-1 (17')EPA 3546 EPA 8270
92265117002 OEXT/37442 MSSV/11169SS-2 (16')EPA 3546 EPA 8270
92265117001 MSV/33209SS-1 (17')EPA 8260
92265117002 MSV/33209SS-2 (16')EPA 8260
92265117001 PMST/8294SS-1 (17')ASTM D2974-87
92265117002 PMST/8294SS-2 (16')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 35 of 37
Page 36 of 37
Page 37 of 37