WS-9395_44615_CA_RPTS_20150109_PhaseIIESA

NOTICE

This ASTM Phase II Environmental Site Assessment report is provided for the exclusive
use of the client and his/her agents as specified within the contract. Dewberry Engineers
Inc. authorizes no party other than those specified in the contract to rely on this
instrument of professional service provided by Dewberry Engineers Inc.

Dewberry Engineers Inc. will meet with third parties as authorized by the client to
discuss the information contained in this report. All third parties wishing to rely on this
instrument of professional service must first enter into a contractual agreement with
Dewberry Engineers Inc. subject to the same Scope of Services, Limitations, and
Standard Terms and Conditions as the original contract with appropriate fees to be
negotiated at the time of the request for third party reliance.

Proposed SunCap Property Phase II Environmental Site Assessment

TOC-1 January 9, 2015
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TABLE OF CONTENTS

1. INTRODUCTION ............................................................................................. 1
2. SITE DESCRIPTION ....................................................................................... 1
3. SITE INVESTIGATION ................................................................................... 1
4. SAMPLING RESULTS ..................................................................................... 2
5. CONCLUSION .................................................................................................. 3
6. REFERENCES .................................................................................................. 4
7. PROFESSIONAL STATEMENT AND SIGNATURES .................................. 5

List of Figures

Figure 1 USGS Project Location Map
Figure 2 Boring Locations

List of Tables

Table 1 1328 Old Greensboro Rd Analytical Soil and PID Results Summary
Table 2 1404 Old Greensboro Rd Analytical Soil and PID Results Summary

List of Appendices

Appendix A Site Photographs
Appendix B Laboratory Analytical Results
Proposed SunCap Property Phase II Environmental Site Assessment

1 January 9, 2015
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1. INTRODUCTION

Dewberry Engineers Inc. (Dewberry) performed a Phase II Environmental Site Assessment (ESA)
on the southern side of two (2) houses located along Old Greensboro Road in Kernersville, NC
(Figure 1: USGS Project Location Map). The Phase II ESA was conducted based on information
compiled from the Phase I ESA report dated May 8, 2014. During the Phase I ESA site
reconnaissance conducted April 4, 2014, Dewberry personnel identified two (2) recognized
environmental conditions (RECs) located at 1328 Old Greensboro Road and 1404 Old Greensboro
Road in Forsyth and Guilford counties, respectively (Figure 2: Boring Locations). The RECs
consist of one (1) underground storage tank (UST) located on the southern side of each house.

2. SITE DESCRIPTION

The areas of interest include the southern side of two (2) vacant residential houses in Kernersville,
North Carolina. The houses are east-southeast of the intersection of Route 66 and I-40/Business.
Accesses to the sites are from Old Greensboro Road via East Mountain Street.

The UST at 1328 Old Greensboro Road is adjacent to the southeastern corner of the house. It is
rectangular in shape and parallels the house in an east-west direction. The UST is located east of
a central air conditioning unit and west of an unmaintained garden. The UST is covered with soil.

The UST at 1404 Old Greensboro Road is adjacent to the southeastern corner of the house. It is
rectangular in shape and parallels the house in an east-west direction. The UST is located between
a central air conditioning unit and the southeastern corner of the house. The UST is covered with
soil.

3. SITE INVESTIGATION

On September 2, 2014, Dewberry personnel measured the approximate depth of the UST below
ground surface (bgs) by measuring from the top of the fill pipe to the bottom of the tank. Dewberry
personnel verified that both USTs were not empty. The UST located at 1328 Old Greensboro Road
is approximately 6 feet (72 inches) bgs; the UST located at 1404 Old Greensboro Road is
approximately 4.5 feet (54 inches) bgs.

On September 2, 2014, Dewberry and Bedford Well Drilling performed Geoprobe® services at
the site. As Figure 2 and Appendix A: Site Photographs illustrates, Dewberry personnel gathered
three (3) soil samples around each of the USTs at 1328 and 1404 Old Greensboro Road.

Based on the Geoprobe® soil borings, three (3) soil types were observed at the subject property.
Soil types are identified in order of depth, with the shallow soil layer identified first:

1. Red Clay
2. Micaceous red silty clay with fine to coarse grained sand
3. Saprolite (parent material) biotite gneiss, fine to coarse grained sand

A four foot Shelby tube sampler was used in the Geoprobe®. The Shelby tube was advanced to a
maximum depth of 8 feet. The soil borings were logged by Dewberry personnel. At a minimum, a
Proposed SunCap Property Phase II Environmental Site Assessment

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soil sample was collected every 4 feet from the boring and placed into sealable gallon sized bags
where the soil was massaged to release any volatile organic compounds (VOCs) into the headspace
of the bag. An in-field photo-ionization detector (PID) meter was used to measure the presence of
VOCs (units in parts per million) in the headspace of the bag. If a noticeable petroleum staining
or odor was present, the odorous and/or stained soil was placed into sample collection containers
(after a PID measurement was taken) and sent to Pace Analytical (PACE), a North Carolina
licensed laboratory, for analysis.

To avoid damaging the USTs, a hand auger was used to collect a fourth soil sample (SS-4) around
the fill pipe of each UST. Each soil sample was analyzed for VOCs. A positive PID reading from
the hand augered soil sample was collected from the UST at 1328 Old Greensboro Road and sent
to PACE for further analysis.

If a soil boring visually appeared to be clean and determined to have very little measurable amounts
of VOCs (less than 10 ppm) during PID analysis, then a sample was taken at approximately 8 feet
bgs and sent to the lab for analysis.

All soil samples were analyzed for total petroleum hydrocarbons: gasoline range organics (GRO),
diesel range organics (DRO), oil range organics (ORO), and oil and grease. The samples were also
analyzed for percent moisture.

4. SAMPLING RESULTS

The laboratory analysis revealed that areas around the USTs contain contamination for GRO and
DRO above the maximum soil contaminant concentration (MSCC) levels for residential soil
cleanup for the North Carolina Department Environmental Natural Resources (NC DENR) and/or
the regional screening levels (RSL) for residential soil for the United States Environmental
Protection Agency (US EPA) (Appendix B: Laboratory Analytical Results).

At 1328 Old Greensboro Road, contamination above the RSLs for DRO was found in the soil
surrounding the fill pipe of the UST (identified as SS-4) (Figure 2 and Table 1).

At 1404 Old Greensboro Road, soil contamination was found above the RSLs and the MSCC
levels for GRO and DRO at the southeast corner of the UST (identified as SS-1) (Figure 2 and
Table 2). Soil contamination was discovered at approximately 5.6 feet bgs, approximately 1 foot
below the estimated depth of the UST.

Proposed SunCap Property Phase II Environmental Site Assessment

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5. CONCLUSION

Dewberry recommends a Phase III Environmental Site Assessment which involves the draining
and disposal of USTs at 1328 and 1404 Old Greensboro Road. The Phase III ESA would also
involve the removal of contaminated soil through excavation. Soil samples would be collected at
various intervals during the excavation process and analyzed for VOCs using the PID meter. Based
on the PID results, soil samples will be collected and sent to PACE for analysis. Dewberry
recommends that samples are analyzed for constituents as per NC DENR: NC Division of Waste
Management’s guidelines for UST sampling. The collection of soil samples at various intervals
during the excavation process will ensure that the contamination plume has been completely
remediated (removed). The excavated contaminated soil will be properly disposed off site at an
appropriate disposal facility.

Dewberry has not notified the EPA or NC DENR concerning the leaking UST at 1404 Old
Greensboro Road. Effective December 1988, EPA has issued federal regulations which delegates
UST regulatory authority to approved state programs (i.e. NC DENR’s Division of Waste
Management (DWM)). According to the EPA and NC DENR regulations, it is not Dewberry’s
responsibility to notify the NC DWM of the leaking UST. Rather, it is the responsibility of the
owner or operator of the UST to notify the NC DWM (919-707-8200) of the release. The NC
DWM must be notified of the release within 24 hours of receiving this report. The owner or
operator will need to take corrective action to properly dispose of the contaminated soil and follow
up with a report providing the actions they plan on taking or have taken to correct the damage
caused by the USTs. They will need to report their progress and any information they have
collected to the NC DWM no later than 20 days after confirming the release.

If the owner or operator decides to close the USTs, Dewberry recommends that the USTs are
properly closed per NC DENR: NC Division of Waste Management’s UST Program procedures.
The owner or operator will need to notify the appropriate DWM regional office by submitting a
UST-3 form within five (5) working days prior to closure if the closure is performed by a
Professional Engineer (P.E.) or a Licensed Geologist (L.G.). If closures of the USTs are not
performed by a P.E. or a L.G., then the form must be completed and returned to the DWM thirty
(30) days prior to closure. Records of the actions taken to close the USTs and remediate the sites
should be retained for three (3) years.

Proposed SunCap Property Phase II Environmental Site Assessment

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6. REFERENCES

Environmental Data Resources, Inc. (2014). The EDR Radius MapTM Report with GeoCheck®
(Inquiry # 3898740.2s). Shelton, CT: Environmental Data Resources, Inc.

Google Maps (2014). [Interactive digital map viewed September 2014].
Retrieved from https://maps.google.com/.

Innocent Landowners, Standards for Conducting All Appropriate Inquiries, 40CFR §312 (2013).

NCDENR: N.C. Division of Waste Management. Underground Storage Tank Program. Retrieved from:
http://portal.ncdenr.org/web/wm/ust/ustmain

NCDENR: N.C. Division of Waste Management. (April 2012). Maximum Soil Contaminant
Concentration Levels (MSCCs). Retrieved from:
http://portal.ncdenr.org/c/document_library/get_file?uuid=ad84a424-64a3-423c-a34c-
8faeb9ffc27b&groupId=38361

Standard Practice for Environmental Site Assessments: Phase I Environmental Site Assessment Process
(E1527-13), American Society for Testing Materials (2013). West Conshohocken, PA.

United States Environmental Protection Agency (May 2014). Regional Screening Level (RSL) Summary
Table. Retrieved from: http://www.epa.gov/reg3hwmd/risk/human/rb-
concentration_table/Generic_Tables/docs/master_sl_table_01run_MAY2014.pdf

United States Environmental Protection Agency (May 2014). Regional Screening Levels (Formerly
PRGs). Retrieved from: http://www.epa.gov/region9/superfund/prg/.

U.S Geological Society (USGS). (2013). [Map of Kernersville, NC Quadrangle, 7.5-Minute Series from
USGS website viewed April 2014]. Retrieved from http://www.usgs.gov/pubprod/.

FIGURE 1
USGS Project Location Map

Figure 1: USGS Project Location Map Old Greensboro Road, Kernersville, NCUSGS Topographic Quadrangle Map, Kernersville, NC 20132014 Google Map Data551 Piney Forest Rd. Danville VA 24540434.797.4497ArchitectsEngineersPlannersSurveyorsProject Location36°06'27.9"N 80°02'27.6"WAreas of Interest1328 Old Greensboro Rd1404 Old Greensboro Rd
FIGURE 2
Boring Locations

Figure 2: Boring LocationsOld Greensboro Road, Kernersville, NC2014 Google Map Data551 Piney Forest Rd. Danville VA 24540434.797.4497ArchitectsEngineersPlannersSurveyors1328 Old Greensboro Rd1404 Old Greensboro RdBoring locations are approximate= Boring location and SS numberLegend:= Approximate perimeter of UST123123441
TABLE 1
1328 Old Greensboro Road
Analytical Soil and PID Results Summary

P:\50065050\Adm\Reports\Phase 2\Table 1.docx
Table 1: 1328 OLD GREENSBORO RD Analytical Soil and PID Results Summary
Constituent
US EPA RSL
for
Residential
Soil1
(mg/kg)
NC DENR
MSCC Levels
for Residential
Soil Cleanup2
(mg/kg)
Sample
Location3
Soil Sample
Depth
(ft bgs)
PID
Reading
(ppm)
Analytical Results4
GRO
(mg/kg)
DRO
(mg/kg)
ORO
(mg/kg)
Oil and
Grease
(mg/kg)
GRO 52 939 1
3.4-3.8 0 -- -- -- --
6.6-7.4 -- ND ND ND ND
7.4-7.8 0 -- -- -- --
2
3.4-4.2 0.2 ND ND ND ND
DRO 9.6 1500 6.7-7.4 -- ND ND ND ND
7.4-7.8 0.2 -- -- -- --
ORO 23000 31000 3
3.4-3.8 0 -- -- -- --
6.7-7.4 -- ND ND ND ND
7.4-7.8 0 -- -- -- --
4 0-1 0.1 ND 63.1 51.5 ND

1As per the US EPA Regional Screening Level (RSL) Summary Table for Residential Soils (revised May 2014)
(http://www.epa.gov/reg3hwmd/risk/human/rb-concentration_table/Generic_Tables/docs/master_sl_table_01run_MAY2014.pdf)

2As per the NC DENR Maximum Soil Contaminant Concentration Levels (revised April 2012)
(http://portal.ncdenr.org/c/document_library/get_file?uuid=ad84a424-64a3-423c-a34c-8faeb9ffc27b&groupId=38361)

3All sample locations were bored to a minimum depth of 8’ (or 96”) except SS-4 which was hand augured to 1’ due to site limitations

4Soil samples were collected on September 2, 2014

Bold = exceeds EPA and/or NC DENR soil contamination levels
-- = not measured/analyzed
bgs = below ground surface
DRO = diesel range organics
GRO = gas range organics
MSCC = maximum soil contamination concentration
NC DENR = North Carolina Department of Environment and Natural Resources
ND = not detected
ORO = oil range organics
PID = photo-ionization detector
ppm = parts per million
RSL = regional screening level
US EPA = United States Environmental Protection Agency

TABLE 2
1404 Old Greensboro Road
Analytical Soil and PID Results Summary

P:\50065050\Adm\Reports\Phase 2\Table 1.docx
Table 2: 1404 OLD GREENSBORO RD Soil Sample Analytical and PID Results Summary
Constituent
US EPA RSL
for
Residential
Soil1
(mg/kg)
NC DENR
MSCC Levels
for Residential
Soil Cleanup2
(mg/kg)
Sample
Location3
Soil Sample
Depth
(ft bgs)
PID
Reading
(ppm)
Analytical Results4
GRO
(mg/kg)
DRO
(mg/kg)
ORO
(mg/kg)
Oil and
Grease
(mg/kg)
GRO 52 939 1
1.8-2 0 -- -- -- --
2.9-3.8 0.3 ND ND ND ND
5.5-6.4 105 647 28300 60.0 44900
7.1-7.8 44.8 61.9 20100 55.9 24800
2
1.7-2 0.8 -- -- -- --
DRO 9.6 1500
3.4-3.8 0.9 -- -- -- --
5.8-6.1 1.1 -- -- -- --
6.7-7.4 -- ND ND ND ND
7.4-7.8 0.9 -- -- -- --
ORO 23000 31000
3
3.3-3.8 0.7 -- -- -- --
5.7-6.2 0.4 -- -- -- --
6.8-7.4 -- ND ND ND ND
7.4-7.8 0.6 -- -- -- --
4 0-0.8 8.3 -- -- -- --
0.8-1 5.0 -- -- -- --

1As per the US EPA Regional Screening Level (RSL) Summary Table for Residential Soils (revised May 2014)
(http://www.epa.gov/reg3hwmd/risk/human/rb-concentration_table/Generic_Tables/docs/master_sl_table_01run_MAY2014.pdf)

2As per the NC DENR Maximum Soil Contaminant Concentration Levels (revised April 2012)
(http://portal.ncdenr.org/c/document_library/get_file?uuid=ad84a424-64a3-423c-a34c-8faeb9ffc27b&groupId=38361)

3All sample locations were bored to a minimum depth of 8’ (or 96”) except sample location 4 which was hand augured to 1’ due to site
limitations

4Soil samples were collected on September 2, 2014

Bold = exceeds EPA and/or NC DENR soil contamination levels
-- = not measured/analyzed
bgs = below ground surface
DRO = diesel range organics
GRO = gas range organics
MSCC = maximum soil contamination concentration
NC DENR = North Carolina Department of Environment and Natural Resources
ND = not detected
ORO = oil range organics
PID = photo-ionization detector
ppm = parts per million
RSL = regional screening level
US EPA = United States Environmental Protection Agency

APPENDIX A
Site Photographs

1. Approximate soil sample locations on southern side of residential house. Numbered locations
correspond to soil sample locations presented in Table 1.
Appendix A: Phase II Site Photographs
1328 Old Greensboro Rd., Kernersville, NC
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2. Location of SS-4. Distance between fill pipe and capped pipe is approximately 1 foot.
1
2
3
4
Fill Pipe Approximate perimeter of UST
4
1
3. Approximate soil sample locations on southern side of residential house. Numbered
locations correspond to soil sample locations presented in Table 2.
Appendix A: Phase II Site Photographs
1404 Old Greensboro Rd., Kernersville, NC
23
Approximate perimeter of UST
Fill Pipe 4
P:\50065050\Adm\Reports\Phase 2\Appendix A –Site Photos.pptx
APPENDIX B
Laboratory Analytical Results

#=CL#
September 10, 2014
LIMS USE: FR - TROY SHELTON
LIMS OBJECT ID: 92215911
92215911
Project:
Pace Project No.:
RE:
Troy Shelton
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, VA 24540
50065050 SunCap 1328 Old Green
Dear Troy Shelton:
Enclosed are the analytical results for sample(s) received by the laboratory on September 03, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Lab ID Sample ID Matrix Date Collected Date Received
92215911001 1 (6.6'-7.4')Solid 09/02/14 10:45 09/03/14 18:51
92215911002 2 (3.4'-4.2')Solid 09/02/14 11:16 09/03/14 18:51
92215911003 2 (6.7'-7.4')Solid 09/02/14 11:13 09/03/14 18:51
92215911004 3 (6.7'-7.4')Solid 09/02/14 11:45 09/03/14 18:51
92215911005 4 (0'-1')Solid 09/02/14 11:53 09/03/14 18:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92215911001 1 (6.6'-7.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215911002 2 (3.4'-4.2')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215911003 2 (6.7'-7.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215911004 3 (6.7'-7.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215911005 4 (0'-1')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 19
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92215911001 1 (6.6'-7.4')
Percent Moisture 19.1 %09/08/14 13:150.10ASTM D2974-87
92215911002 2 (3.4'-4.2')
Percent Moisture 17.1 %09/08/14 13:160.10ASTM D2974-87
92215911003 2 (6.7'-7.4')
Percent Moisture 14.8 %09/08/14 13:160.10ASTM D2974-87
92215911004 3 (6.7'-7.4')
Percent Moisture 16.9 %09/08/14 13:160.10ASTM D2974-87
92215911005 4 (0'-1')
Diesel Range Organics(C10-C28)63.1 mg/kg 09/05/14 16:475.9EPA 8015 Modified
Oil Range Organics (C28-C40)51.5 mg/kg 09/05/14 16:4717.7EPA 8015 Modified
Percent Moisture 15.2 %09/08/14 13:170.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Sample: 1 (6.6'-7.4')Lab ID: 92215911001 Collected: 09/02/14 10:45 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 15:1109/04/14 09:176.2 5.6 1
Surrogates
n-Pentacosane (S)61 %09/05/14 15:11 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 15:1109/04/14 09:1718.5 13.6 1
Surrogates
n-Pentacosane (S)61 %09/05/14 15:11 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1586.6 86.6 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 14:5109/04/14 14:187.2 7.2 1
Surrogates
4-Bromofluorobenzene (S)84 %09/06/14 14:51 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.1 %09/08/14 13:150.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Sample: 2 (3.4'-4.2')Lab ID: 92215911002 Collected: 09/02/14 11:16 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 15:3509/04/14 09:176.0 5.4 1
Surrogates
n-Pentacosane (S)59 %09/05/14 15:35 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 15:3509/04/14 09:1718.1 13.3 1
Surrogates
n-Pentacosane (S)59 %09/05/14 15:35 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1684.4 84.4 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 15:1409/04/14 14:187.3 7.3 1
Surrogates
4-Bromofluorobenzene (S)85 %09/06/14 15:14 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.1 %09/08/14 13:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Sample: 2 (6.7'-7.4')Lab ID: 92215911003 Collected: 09/02/14 11:13 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 15:5909/04/14 09:175.9 5.3 1
Surrogates
n-Pentacosane (S)62 %09/05/14 15:59 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 15:5909/04/14 09:1717.6 12.9 1
Surrogates
n-Pentacosane (S)62 %09/05/14 15:59 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1682.2 82.2 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 15:3709/04/14 14:186.4 6.4 1
Surrogates
4-Bromofluorobenzene (S)83 %09/06/14 15:37 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.8 %09/08/14 13:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Sample: 3 (6.7'-7.4')Lab ID: 92215911004 Collected: 09/02/14 11:45 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 16:2309/04/14 09:176.0 5.4 1
Surrogates
n-Pentacosane (S)69 %09/05/14 16:23 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 16:2309/04/14 09:1718.0 13.2 1
Surrogates
n-Pentacosane (S)69 %09/05/14 16:23 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1684.2 84.2 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 16:0009/04/14 14:186.2 6.2 1
Surrogates
4-Bromofluorobenzene (S)80 %09/06/14 16:00 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.9 %09/08/14 13:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Sample: 4 (0'-1')Lab ID: 92215911005 Collected: 09/02/14 11:53 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)63.1 mg/kg 09/05/14 16:4709/04/14 09:175.9 5.3 1
Surrogates
n-Pentacosane (S)54 %09/05/14 16:47 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)51.5 mg/kg 09/05/14 16:4709/04/14 09:1717.7 13.0 1
Surrogates
n-Pentacosane (S)54 %09/05/14 16:47 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1782.5 82.5 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 16:2209/04/14 14:187.8 7.8 1
Surrogates
4-Bromofluorobenzene (S)85 %09/06/14 16:22 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.2 %09/08/14 13:170.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/18759
9071B
9071B
9071 Oil and Grease
Associated Lab Samples: 92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1278197
Associated Lab Samples:92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Matrix: Solid
Analyzed
Oil and Grease mg/kg ND 70.0 09/05/14 09:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1278198LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/kg 12201330 92 78-114
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1278199MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215459009
1278200
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Oil and Grease mg/kg 1690 91 78-11494 3 201690ND1580 1630
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8509
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1278003
Associated Lab Samples:92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 09/06/14 14:06
4-Bromofluorobenzene (S)%81 70-167 09/06/14 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1278004LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 45.149.7 91 70-165
4-Bromofluorobenzene (S)%86 70-167
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1278005MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215555002
1278006
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Gas Range Organics (C6-
C10)mg/kg 39.4 115 47-187113 239.4ND 45.7 45.0
4-Bromofluorobenzene (S) %86 70-16783
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29754
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1277910
Associated Lab Samples:92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 09/05/14 14:22
n-Pentacosane (S)%79 41-119 09/05/14 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1277911LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 55.266.7 83 49-113
n-Pentacosane (S)%83 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1277931MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215414006
1277932
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 82.4 79 10-14678 2 3082.4ND 65.9 64.8
n-Pentacosane (S)%82 41-11981
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29755
EPA 3546
EPA 8015 Modified
8015 Solid GCSV ORO
Associated Lab Samples: 92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1277914
Associated Lab Samples:92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Matrix: Solid
Analyzed
Oil Range Organics (C28-C40) mg/kg ND 15.0 09/05/14 13:58
n-Pentacosane (S)%78 41-119 09/05/14 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1277915LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1277928
Oil Range Organics (C28-C40) mg/kg 81.583.3 98 50-15010386.0 5 30
n-Pentacosane (S)%85 41-11985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7007
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92215911001, 92215911002, 92215911003, 92215911004, 92215911005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92215018011
1280271SAMPLE DUPLICATE:
Percent Moisture %15.2 12 2513.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92216289003
1280272SAMPLE DUPLICATE:
Percent Moisture %19.0 6 2517.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92215911
50065050 SunCap 1328 Old Green
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92215911001 OEXT/29754 GCSV/187871 (6.6'-7.4')EPA 3546 EPA 8015 Modified
92215911002 OEXT/29754 GCSV/187872 (3.4'-4.2')EPA 3546 EPA 8015 Modified
92215911003 OEXT/29754 GCSV/187872 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215911004 OEXT/29754 GCSV/187873 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215911005 OEXT/29754 GCSV/187874 (0'-1')EPA 3546 EPA 8015 Modified
92215911001 OEXT/29755 GCSV/187881 (6.6'-7.4')EPA 3546 EPA 8015 Modified
92215911002 OEXT/29755 GCSV/187882 (3.4'-4.2')EPA 3546 EPA 8015 Modified
92215911003 OEXT/29755 GCSV/187882 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215911004 OEXT/29755 GCSV/187883 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215911005 OEXT/29755 GCSV/187884 (0'-1')EPA 3546 EPA 8015 Modified
92215911001 GCSV/18759 GCSV/187771 (6.6'-7.4')9071B 9071B
92215911002 GCSV/18759 GCSV/187772 (3.4'-4.2')9071B 9071B
92215911003 GCSV/18759 GCSV/187772 (6.7'-7.4')9071B 9071B
92215911004 GCSV/18759 GCSV/187773 (6.7'-7.4')9071B 9071B
92215911005 GCSV/18759 GCSV/187774 (0'-1')9071B 9071B
92215911001 GCV/8509 GCV/85121 (6.6'-7.4')EPA 5035A/5030B EPA 8015 Modified
92215911002 GCV/8509 GCV/85122 (3.4'-4.2')EPA 5035A/5030B EPA 8015 Modified
92215911003 GCV/8509 GCV/85122 (6.7'-7.4')EPA 5035A/5030B EPA 8015 Modified
92215911004 GCV/8509 GCV/85123 (6.7'-7.4')EPA 5035A/5030B EPA 8015 Modified
92215911005 GCV/8509 GCV/85124 (0'-1')EPA 5035A/5030B EPA 8015 Modified
92215911001 PMST/70071 (6.6'-7.4')ASTM D2974-87
92215911002 PMST/70072 (3.4'-4.2')ASTM D2974-87
92215911003 PMST/70072 (6.7'-7.4')ASTM D2974-87
92215911004 PMST/70073 (6.7'-7.4')ASTM D2974-87
92215911005 PMST/70074 (0'-1')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
September 10, 2014
LIMS USE: FR - TROY SHELTON
LIMS OBJECT ID: 92215910
92215910
Project:
Pace Project No.:
RE:
Troy Shelton
Dewberry Engineers Inc.
551 Piney Forest Road
Danville, VA 24540
Suncap 1404 Old Greensboro Rd
Dear Troy Shelton:
Enclosed are the analytical results for sample(s) received by the laboratory on September 03, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Eden, NC 27288
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Lab ID Sample ID Matrix Date Collected Date Received
92215910001 1 (2.9'-3.8')Solid 09/02/14 12:43 09/03/14 18:51
92215910002 1 (5.5'-6.4')Solid 09/02/14 13:04 09/03/14 18:51
92215910003 1 (7.1'-7.8')Solid 09/02/14 13:00 09/03/14 18:51
92215910004 2 (6.7'-7.4')Solid 09/02/14 13:35 09/03/14 18:51
92215910005 3 (6.8'-7.4')Solid 09/02/14 14:02 09/03/14 18:51
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92215910001 1 (2.9'-3.8')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215910002 1 (5.5'-6.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215910003 1 (7.1'-7.8')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215910004 2 (6.7'-7.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
92215910005 3 (6.8'-7.4')EPA 8015 Modified 2 PASI-CJDW1
EPA 8015 Modified 2 PASI-CJDW1
9071B 1 PASI-CCLW
EPA 8015 Modified 2 PASI-CGAW
ASTM D2974-87 1 PASI-CACS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Eden, NC 27288
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Page 4 of 19
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92215910001 1 (2.9'-3.8')
Percent Moisture 22.0 %09/08/14 13:170.10ASTM D2974-87
92215910002 1 (5.5'-6.4')
Diesel Range Organics(C10-C28)28300 mg/kg 09/05/14 19:35629EPA 8015 Modified
Oil Range Organics (C28-C40)60.0 mg/kg 09/05/14 17:3518.9EPA 8015 Modified
Oil and Grease 44900 mg/kg 09/05/14 09:1588.19071B
Gas Range Organics (C6-C10)647 mg/kg 09/06/14 18:398.5EPA 8015 Modified
Percent Moisture 20.6 %09/08/14 13:170.10ASTM D2974-87
92215910003 1 (7.1'-7.8')
Diesel Range Organics(C10-C28)20100 mg/kg 09/05/14 19:58614EPA 8015 Modified
Oil Range Organics (C28-C40)55.9 mg/kg 09/05/14 17:5918.4EPA 8015 Modified
Oil and Grease 24800 mg/kg 09/05/14 09:1586.09071B
Gas Range Organics (C6-C10)61.9 mg/kg 09/06/14 19:017.8EPA 8015 Modified
Percent Moisture 18.6 %09/08/14 13:170.10ASTM D2974-87
92215910004 2 (6.7'-7.4')
Percent Moisture 21.8 %09/08/14 13:180.10ASTM D2974-87
92215910005 3 (6.8'-7.4')
Percent Moisture 19.3 %09/08/14 13:180.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Sample: 1 (2.9'-3.8')Lab ID: 92215910001 Collected: 09/02/14 12:43 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 17:1109/04/14 09:176.4 5.8 1
Surrogates
n-Pentacosane (S)76 %09/05/14 17:11 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 17:1109/04/14 09:1719.2 14.1 1
Surrogates
n-Pentacosane (S)76 %09/05/14 17:11 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1789.7 89.7 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 18:1609/04/14 14:186.2 6.2 1
Surrogates
4-Bromofluorobenzene (S)82 %09/06/14 18:16 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.0 %09/08/14 13:170.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Sample: 1 (5.5'-6.4')Lab ID: 92215910002 Collected: 09/02/14 13:04 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)28300 mg/kg 09/05/14 19:3509/04/14 09:17629 567 100
Surrogates
n-Pentacosane (S)0 %09/05/14 19:35 629-99-2 S409/04/14 09:1741-119 100
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)60.0 mg/kg 09/05/14 17:3509/04/14 09:1718.9 13.8 1
Surrogates
n-Pentacosane (S)332 %09/05/14 17:35 629-99-2 S509/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease 44900 mg/kg 09/05/14 09:1509/05/14 07:1888.1 88.1 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)647 mg/kg 09/06/14 18:3909/04/14 14:188.5 8.5 1
Surrogates
4-Bromofluorobenzene (S)214 %09/06/14 18:39 460-00-4 S109/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.6 %09/08/14 13:170.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Sample: 1 (7.1'-7.8')Lab ID: 92215910003 Collected: 09/02/14 13:00 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)20100 mg/kg 09/05/14 19:5809/04/14 09:17614 553 100
Surrogates
n-Pentacosane (S)0 %09/05/14 19:58 629-99-2 S409/04/14 09:1741-119 100
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)55.9 mg/kg 09/05/14 17:5909/04/14 09:1718.4 13.5 1
Surrogates
n-Pentacosane (S)196 %09/05/14 17:59 629-99-2 S509/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease 24800 mg/kg 09/05/14 09:1509/05/14 07:1886.0 86.0 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)61.9 mg/kg 09/06/14 19:0109/04/14 14:187.8 7.8 1
Surrogates
4-Bromofluorobenzene (S)116 %09/06/14 19:01 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.6 %09/08/14 13:170.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Sample: 2 (6.7'-7.4')Lab ID: 92215910004 Collected: 09/02/14 13:35 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 18:2309/04/14 09:176.4 5.8 1
Surrogates
n-Pentacosane (S)81 %09/05/14 18:23 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 18:2309/04/14 09:1719.2 14.1 1
Surrogates
n-Pentacosane (S)81 %09/05/14 18:23 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1989.5 89.5 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 19:2409/04/14 14:186.8 6.8 1
Surrogates
4-Bromofluorobenzene (S)85 %09/06/14 19:24 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.8 %09/08/14 13:180.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Sample: 3 (6.8'-7.4')Lab ID: 92215910005 Collected: 09/02/14 14:02 Received: 09/03/14 18:51 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 09/05/14 18:4709/04/14 09:176.2 5.6 1
Surrogates
n-Pentacosane (S)69 %09/05/14 18:47 629-99-209/04/14 09:1741-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 09/05/14 18:4709/04/14 09:1718.6 13.6 1
Surrogates
n-Pentacosane (S)69 %09/05/14 18:47 629-99-209/04/14 09:1741-119 1
Analytical Method: 9071B Preparation Method: 9071B9071 Oil and Grease
Oil and Grease ND mg/kg 09/05/14 09:1509/05/14 07:1986.8 86.8 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 09/06/14 19:4709/04/14 14:187.1 7.1 1
Surrogates
4-Bromofluorobenzene (S)82 %09/06/14 19:47 460-00-409/04/14 14:1870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.3 %09/08/14 13:180.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCSV/18759
9071B
9071B
9071 Oil and Grease
Associated Lab Samples: 92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1278197
Associated Lab Samples:92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Matrix: Solid
Analyzed
Oil and Grease mg/kg ND 70.0 09/05/14 09:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1278198LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/kg 12201330 92 78-114
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1278199MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215459009
1278200
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Oil and Grease mg/kg 1690 91 78-11494 3 201690ND1580 1630
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8509
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1278003
Associated Lab Samples:92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 09/06/14 14:06
4-Bromofluorobenzene (S)%81 70-167 09/06/14 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1278004LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 45.149.7 91 70-165
4-Bromofluorobenzene (S)%86 70-167
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1278005MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215555002
1278006
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Gas Range Organics (C6-
C10)mg/kg 39.4 115 47-187113 239.4ND 45.7 45.0
4-Bromofluorobenzene (S) %86 70-16783
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29754
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1277910
Associated Lab Samples:92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 09/05/14 14:22
n-Pentacosane (S)%79 41-119 09/05/14 14:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1277911LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 55.266.7 83 49-113
n-Pentacosane (S)%83 41-119
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1277931MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92215414006
1277932
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/kg 82.4 79 10-14678 2 3082.4ND 65.9 64.8
n-Pentacosane (S)%82 41-11981
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/29755
EPA 3546
EPA 8015 Modified
8015 Solid GCSV ORO
Associated Lab Samples: 92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1277914
Associated Lab Samples:92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Matrix: Solid
Analyzed
Oil Range Organics (C28-C40) mg/kg ND 15.0 09/05/14 13:58
n-Pentacosane (S)%78 41-119 09/05/14 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1277915LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1277928
Oil Range Organics (C28-C40) mg/kg 81.583.3 98 50-15010386.0 5 30
n-Pentacosane (S)%85 41-11985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7007
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92215910001, 92215910002, 92215910003, 92215910004, 92215910005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92215018011
1280271SAMPLE DUPLICATE:
Percent Moisture %15.2 12 2513.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92216289003
1280272SAMPLE DUPLICATE:
Percent Moisture %19.0 6 2517.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Surrogate recovery outside laboratory control limits (confirmed by re-analysis).S1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92215910
Suncap 1404 Old Greensboro Rd
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92215910001 OEXT/29754 GCSV/187871 (2.9'-3.8')EPA 3546 EPA 8015 Modified
92215910002 OEXT/29754 GCSV/187871 (5.5'-6.4')EPA 3546 EPA 8015 Modified
92215910003 OEXT/29754 GCSV/187871 (7.1'-7.8')EPA 3546 EPA 8015 Modified
92215910004 OEXT/29754 GCSV/187872 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215910005 OEXT/29754 GCSV/187873 (6.8'-7.4')EPA 3546 EPA 8015 Modified
92215910001 OEXT/29755 GCSV/187881 (2.9'-3.8')EPA 3546 EPA 8015 Modified
92215910002 OEXT/29755 GCSV/187881 (5.5'-6.4')EPA 3546 EPA 8015 Modified
92215910003 OEXT/29755 GCSV/187881 (7.1'-7.8')EPA 3546 EPA 8015 Modified
92215910004 OEXT/29755 GCSV/187882 (6.7'-7.4')EPA 3546 EPA 8015 Modified
92215910005 OEXT/29755 GCSV/187883 (6.8'-7.4')EPA 3546 EPA 8015 Modified
92215910001 GCSV/18759 GCSV/187771 (2.9'-3.8')9071B 9071B
92215910002 GCSV/18759 GCSV/187771 (5.5'-6.4')9071B 9071B
92215910003 GCSV/18759 GCSV/187771 (7.1'-7.8')9071B 9071B
92215910004 GCSV/18759 GCSV/187772 (6.7'-7.4')9071B 9071B
92215910005 GCSV/18759 GCSV/187773 (6.8'-7.4')9071B 9071B
92215910001 GCV/8509 GCV/85121 (2.9'-3.8')EPA 5035A/5030B EPA 8015 Modified
92215910002 GCV/8509 GCV/85121 (5.5'-6.4')EPA 5035A/5030B EPA 8015 Modified
92215910003 GCV/8509 GCV/85121 (7.1'-7.8')EPA 5035A/5030B EPA 8015 Modified
92215910004 GCV/8509 GCV/85122 (6.7'-7.4')EPA 5035A/5030B EPA 8015 Modified
92215910005 GCV/8509 GCV/85123 (6.8'-7.4')EPA 5035A/5030B EPA 8015 Modified
92215910001 PMST/70071 (2.9'-3.8')ASTM D2974-87
92215910002 PMST/70071 (5.5'-6.4')ASTM D2974-87
92215910003 PMST/70071 (7.1'-7.8')ASTM D2974-87
92215910004 PMST/70072 (6.7'-7.4')ASTM D2974-87
92215910005 PMST/70073 (6.8'-7.4')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 09/10/2014 03:32 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 19
Page 18 of 19
Page 19 of 19