WS-6358_24039_CA_RMR_20221223

GROUNDWATER MONITORING REPORT

JERRY’S AMOCO-B
1411 SOUTH MAIN STREET
GRAHAM, NORTH CAROLINA
INCIDENT NO. 24039

PREPARED FOR:
MR. MICHAEL TOMPKINS
MIDWAY OIL AND GAS COMPANY, INC.
PO BOX 100
MEBANE, NORTH CAROLINA 27302

PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285

DECEMBER 23, 2022
PILOT PROJECT NO. G-8830

SITE INFORMATION

Site Name and Location Jerry’s Amoco-B
1411 South Main Street
Graham, Alamance County, North Carolina

Incident No. 24039

Facility ID: Unknown

Latitude and Longitude: 36.040758; 79.393959

Land Use Category: Commercial

Contacts
Owner of UST: Mr. Michael Tompkins
Midway Oil and Gas Company, Inc.
PO Box 100
Mebane, North Carolina 27302
[phone]

Primary Contact: Mr. Michael Tompkins
Midway Oil and Gas Company, Inc.
[phone]

Consultant: Pilot Geological, PLLC
PO Box 128
Kernersville, North Carolina 27285
[phone]

Laboratory: Pace Analytical
1377 South Park Drive
Kernersville, North Carolina 27284
[phone]
Laboratory I.D. # Various

Release information: In January 1994, a release was identified at the site. The source of the release was stated
to be from a gasoline UST and dispenser. The estimated quantity of the release is unknown.

Table of Contents
1.0 SITE HISTORY ................................................................................................................... 1
1.1 UST Information ......................................................................................................................................... 3
2.0 SITE GEOLOGY AND HYDROGEOLOGY ............................................................................... 3
3.0 FIELD ACTIVITIES .............................................................................................................. 4
3.1 Monitoring Well Sampling .......................................................................................................................... 4
3.2 Groundwater Modeling .............................................................................................................................. 5
3.3 Free Product Investigation and Recovery ................................................................................................... 5
4.0 LABORATORY ANALYTICAL RESULTS ................................................................................. 5
4.1 Groundwater Sample Analysis .................................................................................................................... 5
5.0 CONCLUSIONS ................................................................................................................. 5
6.0 RECOMMENDATIONS ....................................................................................................... 6
7.0 QUALIFICATIONS OF REPORT ........................................................................................... 6
8.0 STATEMENTS AND CERTIFICATIONS ................................................................................. 7

DRAWINGS

Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 Sample Location Map
Drawing 4 Potentiometric Surface Map
Drawing 5 Water Supply Well Location Map
Drawing 6 Benzene Isoconcentration Map
Drawing 7 MTBE Isoconcentration Map
TABLES

Table 1 UST Information
Table 2 Monitoring Well Construction Information
Table 3 Water Supply Well Information
Table 4 Summary of Groundwater Analytical Results

APPENDICIES

Appendix A Monitoring Well Sampling Sheets
Appendix B Laboratory Data Sheets and Chain of Custody Record
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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1.0 SITE HISTORY

The site is located at 1411 South Main Street in Graham, North Carolina (Drawings 1 and 2). The
site is currently developed with an active automotive service facility. A total of five underground
storage tanks (USTs) have been in use at the site during its operating history. Currently, there are
no known USTs located on the subject site. A release was previously identified by others in the
vicinity of the former UST system.

Apex Environmental, Inc. completed a Corrective Action Plan for the site (Apex Project 510057.001,
report dated December 10, 2003). Progress Environmental, Inc. (Progress) previously completed an
Active Remediation Monitoring Report for the site (Progress Project 1020056.001, report dated
January 11, 2017).

According to the Comprehensive Site Assessment (CSA) prepared by Fuss O’Neil and dated
September 2003, a UST Closure Report was prepared by Nesco, Inc. in January 1994. A 1,000-gallon
diesel UST was removed from the site in December of 1993. A Groundwater Incident No. 11697 was
assigned to the site. On May 30, 1994, the site was designated as a low priority site. On October
11, 2001 a 4,000-gallon gasoline UST was removed. According to the CSA report, soil analytical
results indicated that a release had occurred beneath the dispenser islands.

On July 15, 2002, Ms. Billie Rich, executor of the Clara Lindley estate subcontracted the removal of
one 2,000-gallon and one 6,000-gallon gasoline UST. Soil analytical data indicated that a release had
occurred beneath the dispenser islands. A Notice of Regulatory Requirements (NORR) was issued
to both parties. The NORR requested a Limited Site Assessment (LSA) be performed. Based on
analytical results during the Phase I LSA, separate incident numbers were issued to each party.
Midway Oil & Gas Company negotiated with the North Carolina Department of Environment and
Natural Resources (NCDENR) to combine both incidents into one in order to complete the CSA.
According to the CSA, NCDENR suspended Groundwater Incident No. 30037, which was issued to
the Clara Lindley Estate.

On July 16, 2002, one monitoring well (MW-1) was installed at the site in the vicinity of suspected
contamination. The monitoring well boring was advanced to a depth of 25 feet below ground
surface (bgs). Soil samples were collected every five feet until 20 feet bgs. The soil samples collected
from monitoring well boring (MW-1) were analyzed in the laboratory for volatile organic compounds
(VOCs) using USEPA Method 8260 and volatile petroleum hydrocarbons (VPH) using the
Massachusetts Department of Environmental Protection (MADEP) Method. Results were compared
to the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs) as presented in the
NCDENR, UST Section Guidelines for the Assessment and Corrective Action dated April 2001. MTBE
was the only compound detected above the method detection limit, but at concentration below its
Soil-to-Groundwater MSCC.

As discussed above, one monitoring well (MW-1) was installed to a depth of 25 feet bgs to evaluate
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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the presence or absence of petroleum constituents in the groundwater beneath the site. A
groundwater sample was collected from MW-1 on July 23, 2003. The samples were analyzed for
VOCs by USEPA Methods 601/602 including IPE and MTBE, ethylene dibromide (EDB) by USEPA
Method 504.1, volatile petroleum hydrocarbons (VPH) by the MADEP Method, and lead by Standard
Method 3030C.

The VOC, 1,2-dichloroethane was detected at a concentration which exceeded its 2L Groundwater
Quality Standard as described in Title 15A, Subchapter 2L, Section .0202 of the North Carolina
Administrative Code by a factor of 10. A Phase II LSA was required to be completed at the site. In
order to confirm the presence of 1,2-dichloroethane, the monitoring well was re-sampled on August
9, 2002. The analytical results indicated that the concentration of 1,2-dichloroethane exceeded the
2L Groundwater Quality Standard (2L Standard).

Based on these results, the NCDENR issued a NORR on February 6, 2003 requesting a CSA.

On June 17, 2003, ten soil borings were advanced by others at the site. Soil samples were collected
at depths of 5 feet and 10 feet bgs. The purpose of this investigation was to determine the extent
of soil contamination in the vicinity of the dispenser islands. The soil samples were sent to a North
Carolina-certified laboratory to be analyzed for VOCs by USEPA Method 8260/5035 used for
preparation and VPH using the MADEP method.

The soil analytical results were compared to the Soil-to-Groundwater MSCCs and Residential Soil
Cleanup Levels as presented in the 2001 NCDENR Guidelines. Petroleum constituents were
detected at concentrations which exceeded their respective Soil-to-Groundwater MSCCs in the soil
samples collected from soil Borings B2 and B6. Based on the documentation, the contaminated soil
is located in a relatively small area located proximal to the former gasoline dispenser. The area of
contaminated soil was estimated to be approximately 240 square feet. Assuming that the
contaminated soil thickness is 17 feet beneath the site, Apex asserted that approximately 151 cubic
yards or 225 tons of soil had been impacted.

According to Fuss & O’Neill’s CSA report, nine shallow Type II monitoring wells and one deep Type
III monitoring well were installed from June to August 2003. On June 9, 2003, monitoring wells MW-
1 through MW-5, the deep monitoring well DW-1, and the adjacent water-supply well were sampled
on June 2, 2003. On July 8, 2003, groundwater samples were collected from monitoring wells MW-
6 through MW-8 subsequent to their installation on July 3, 2003. On August 5, 2003, groundwater
samples were collected from monitoring wells MW-9 and MW-10 subsequent to their installation
on August 1, 2003. The groundwater samples were analyzed for VOCs by USEPA Method 601/602
modified to include xylenes and methyl tert-butyl ether (MTBE), EDB by USEPA Method 504.1, VPH
by the MADEP Method, and for lead using Standard Method 3030C. The adjacent water-supply well
was sampled for VOCs by USEPA Methods 601/602.

Several petroleum-related compounds were detected in the groundwater samples collected from
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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the monitoring wells during the completion of the CSA. No petroleum constituents were detected
in the deep monitoring well (DW-1) or the adjacent water-supply well. While 1,2-dichloroethane
was detected in groundwater samples from monitoring well MW-1 at a concentration which
exceeded its 2L Groundwater Quality Standard in the groundwater samples collected during the
LSA, the analyte was not detected in monitoring well MW-1 during the CSA. Benzene was detected
in monitoring wells MW-1 and MW-7 at concentrations, which exceeded its 2L Standard.
Ethylbenzene, toluene, and xylenes were detected in the groundwater samples collected from MW-
7 at concentrations which exceeded their respective 2L Groundwater Quality Standards. MTBE was
detected in the groundwater samples collected from monitoring wells MW-1, MW-2 and MW-7 at
concentrations which exceeded its 2L Standard.

Progress completed multiple mobile multi-phase extraction (MMPE) and groundwater monitoring
events were conducted at the site from 2008 through 2020.

Pilot was requested to provide a groundwater monitoring event related to the Notice of Regulatory
Requirements (NORR) issued by the North Carolina Department of Environmental Quality (NCDEQ)
dated November 14, 2022.

Project information is based on correspondence between NCDEQ personnel, Midway Oil and Gas
Company, Inc. and Pilot and the previously completed activities.

1.1 UST Information

The site consists of an active automotive service facility. Based on the available information four
underground storage tanks (USTs) are associated with the site. The USTs consist of one 1,000-
gallon diesel, one 2,000-gallon gasoline, one 6,000-gallon gasoline, and one 4,000-gallon
gasoline. UST information is summarized in Table 1.

2.0 SITE GEOLOGY AND HYDROGEOLOGY

The United States Geological Survey (USGS) Topographic Map, Burlington and Mebane, North
Carolina Quadrangles depict a structure on the site. The site is located near the top of a ridge,
and the elevation of the site is approximately 600 feet above mean sea level. An unnamed
intermittent tributary of Big Alamance Creek is located approximately 1,200 feet west of the
source area of the release. Based on the review of the USGS topographic map and observations
of the general area and site topography, surface run-off would be expected to flow generally to
the west-southwest across the site.

The subject site is located within the Piedmont Physiographic Province. The Piedmont
Physiographic Province generally consists of hills and ridges which are dissected by a system of
swales and streams. The Piedmont Physiographic Province is predominantly underlain by
metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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directly from molten material). The topography and relief of the Piedmont Province has
developed from differential weathering of the igneous and metamorphic rock. Ridges and hills
have been developed in areas of less weathered rock. Because of the continued chemical and
physical weathering, rock in the Piedmont Physiographic Province is generally covered with a
mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness
and are referred to as residuum or residual soils. The residuum is typically finer grained and has
higher clay content near the surface because of the advanced weathering. Similarly, the soils
typically become coarser grained with increasing depth because of decreased weathering. As the
weathering decreases, the residual soils generally retain the overall appearance, texture and
foliations of the parent rock.

In general, groundwater movement in the Piedmont Physiographic Province is from higher to
lower elevations. As such, the presumed direction of groundwater flow is generally to the west-
southwest across the site. Based on the presumed groundwater flow direction, areas
immediately east and north are potentially up-gradient of the site.

Based on the previously completed reports, soils at the site consists of very stiff to hard clayey
sand, silt and partially weathered rock. Weathered rock was reportedly encountered at
approximately 60 feet below ground surface (bgs).

3.0 FIELD ACTIVITIES

The field activities were completed by Pilot on November 28, 2022. The field activities consisted
of collecting groundwater samples from existing monitoring wells MW-2, MW-7, MW-9, MW-10,
MW-11 and MW-12 (Drawing 3). Monitoring well MW-13 was not sampled based on
approximately 0.01 feet of free product being measured in the well.

3.1 Monitoring Well Sampling

Groundwater samples were collected from the existing monitoring wells listed above that did not
contain free product, using a disposable bailer and new length of nylon string. Prior to sampling,
approximately three well volumes were purged from the monitoring wells. The monitoring wells
were purged to remove silt and sediment from the groundwater and collect a representative
sample of groundwater. After the purging was completed, groundwater samples were collected
in the sample containers provided by the laboratory. Pilot personnel wore a new pair of
disposable nitrile gloves during purging and sampling. Each container was labeled and placed in
a cooler containing ice to maintain the samples at approximately 4 Celsius. The samples were
then transported to Pace Analytical (Pace) for chemical analysis. The groundwater samples
collected were analyzed for volatile organic compounds (VOCs) using Standard Method 6200B.
A chain of custody was maintained and is included in Appendix B. Isoconcentration maps for
benzene and MTBE are included as Drawings 6 and 7, respectively. Copies of the Monitoring Well
Sampling Sheets are included in Appendix A.
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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The depth to the groundwater surface in monitoring wells MW-2, MW-7, MW-9, MW-10, MW-
11, MW-12 and MW-13 was measured using a decontaminated water level indicator. The top of
casing elevation for each well was previously surveyed relative to an arbitrary benchmark with
an assumed elevation above mean sea level. The monitoring well elevations were utilized to
prepare a potentiometric surface map (Drawing 4). The relative groundwater elevations
collected from each monitoring well on November 28, 2022 are provided in Table 4. Based on
data collected during the assessment activities, the groundwater flow direction appears to be
generally toward the west-southwest beneath the site.

3.2 Groundwater Modeling

Groundwater modeling was not completed based on a surface water featuring not being
identified within 500 feet of the source area of the release.

3.3 Free Product Investigation and Recovery

Free product was observed in monitoring well MW-13 during this sampling event. Approximately
0.01 feet of free product was measured. MMPE events were previously completed in an effort
to remove the free product and decrease the dissolved phase concentrations. Free product was
historically detected in monitoring well MW-3 on December 30, 2009.

4.0 LABORATORY ANALYTICAL RESULTS

4.1 Groundwater Sample Analysis

Laboratory analysis of the groundwater samples collected from monitoring wells MW-2, MW-9,
MW-10, MW-11 and MW-12 did not detect targeted compounds above their respective 2L
Standards. Laboratory analysis of the groundwater sample collected from monitoring well MW-
7 detected targeted compounds above their respective 2L Standards, but below their respective
GCLs. A summary of the groundwater analytical results is presented in Table 4. The laboratory
data sheets are included in Appendix B.

5.0 CONCLUSIONS

Based on the activities, Pilot concludes the following:

 Monitoring well MW-13 was not sampled since 0.01 feet of free-product was measured in the
well.

 Laboratory analysis of the groundwater samples collected from monitoring wells MW-2, MW-
9, MW-10, MW-11 and MW-12 did not detect targeted compounds above their respective 2L
Standards. Laboratory analysis of the groundwater sample collected from monitoring well
Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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MW-7 detected targeted compounds above their respective 2L Standards, but below their
respective GCLs.

 The groundwater flow was calculated to be to be generally to the west-southwest.

 Several water supply wells were identified within 1,000 feet of the source area of the release
by others.

 The majority of the plume of impacted groundwater appears to be confined to the site. Pilot
recommends an AFVR event to remove the free product from the vicinity of monitoring well
MW-13 and aid in decreasing the dissolved phase concentrations.

6.0 RECOMMENDATIONS

Pilot recommends that the current property owner/responsible party submit a copy of this
Groundwater Monitoring Report to the NCDEQ, UST Section for their review. A Notice of Residual
Petroleum (NORP) is required to be recorded prior to a property transaction occurring.

7.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during
our field activities.

Groundwater Monitoring Report
Jerry’s Amoco-B
1411 South Main Street
Pilot Project G-8830
December 23, 2022

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8.0 STATEMENTS AND CERTIFICATIONS

1 Enter the date the monitoring report was due. Not Established Will this report be
submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
3 If applicable, will any of the proposed attenuation milestones under the schedule
approved in the Corrective Action Plan not be met? (within a reasonable margin of
error)

N/A
YES NO
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?

Free product was detected in MW-13 but is within the assessment area.
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?

YES NO

Certification:
I, Jason T. Ricks, a Licensed Geologist for Pilot Geological, PLLC, do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Pilot Geological, PLLC is licensed to practice geology in North Carolina. The certification number of
the company is C-542.

DRAWINGS
SITE
USGS Topographic Map
Jerry’s Amoco
1411 South Main Street
Graham, Alamance County, NC
Pilot Project G-8830
Drawing 1
USGS Topographic Map
Burlington and Mebane, NC
Quadrangles
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
Jerry’s Amoco
1411 South Main Street
Graham, Alamance County, NC
Pilot Project G-8830
Drawing 2
Google Earth
Interactive Mapping Software
Scale : 1”= 100’
LEGEND
Site BoundaryU. Former UST System
U
Water Supply Well Location Map
Jerry’s Amoco
1411 South Main Street
Graham, Alamance County, NC
Pilot Project G-8830
Drawing 5
Google Earth
Interactive Mapping Software and
Alamance County GIS
Scale : 1”= 300’
LEGEND
Site Boundary
Approximate Water Supply Well Location
Information obtained from previous reports by others.
500’
1,000’
7
6
4
5
1
3 2
8
9

TABLES
UST ID NumberOwner Last ContentsPrevious ContentsCapacity (in Gallons)Construction DetailsTank DimensionsInstallation DateStatus Release4Gasoline Gasoline 4,000 UnknownMidway Oil & Gas Company (1/69 to 10/1/01)Clara Neil Lindle C/o Bille C. Rich (1/1/64 to 7/15/02Unknown 1/1/1964Closed 10/22/01UnknownGasolineUnknown3Gasoline Gasoline 6,000 Unknown Unknown 1/1/1964Closed 7/15/02Unknown2,000 Unknown Unknown 1/1/1964Closed 7/15/02Clara Neil Lindle C/o Bille C. Rich (1/1/64 to 7/15/02Midway Oil & Gas Company (4/29/80 to 12/6/93)Table 1 - UST InformationJerry's AmocoGraham, North Carolina1Diesel Diesel 1,000 Unknown Unknown 4/29/1980Closed 12/6/93Unknown2Gasoline
Monitoring Well IDWell Diameter (Inches)Date Installed Elevation (TOC)Static Water Level (11/28/22)Groundwater ElevationTotal DepthScreened Interval (feet)Sand IntervalBentonite IntervalMW-1 2 7/16/2002 549.04 NM N/A 25 10-25 N/A N/AMW-2 2 6/2/2003 549.37 19.50 529.87 30 10-30 N/A N/AMW-3 2 6/2/2003 547.83 NM N/A 30 10-30 N/A N/AMW-4 2 6/3/2003 549.54 NM N/A 30 10-30 N/A N/AMW-5 2 6/3/2003 549.39 NM N/A 30 10-30 N/A N/AMW-6 2 7/3/2003 548.90 NM N/A 30 10-30 N/A N/AMW-7 2 7/3/2003 546.55 17.39 529.16 30 10-30 N/A N/AMW-8 2 7/3/2003 549.20 NM N/A 30 10-30 N/A N/AMW-9 2 8/1/2003 547.47 18.49 528.98 30 10-30 N/A N/AMW-10 2 8/1/2003 547.00 19.71 527.29 30 10-30 N/A N/AMW-11 2 10/18/2010 549.44 18.76 530.68 30 10-30 N/A N/AMW-12 2 2/3/2011 547.33 17.56 529.77 30 10-30 N/A N/A*MW-13 2 3/16/2013 548.95 19.32 (0.01' FP) 529.64 30 10-30 N/A N/ADW-1 2 6/2/2003 549.56 NM N/A 76 71-76 N/A N/ATable 2 - Monitoring Well Construction InformationJerry's AmocoGraham, North Carolina*If free product is present the groundwater elevation is calculated by (TOC Elevation - Static) + (free product thickness x 0.8581)
Well ID
Number Owner Information Property Address Well Depth (feet) Well Use
Approximate Distance
from the Source Area
Is the Property Connected
to Municipal Water
Information was obtained from previous reports completed by others and updated as available.
Unknown Unknown
585 Unknown
6 Glenn Tyndall
880 Unknown
8 Terry Hutchen 1532 Swepsonville Rd. Unknown Unknown 625 Unknown
9 Dewey Brown 1612 Swepsonville Rd.
7 Amy Hodgin 129 Nicks St. Unknown Not Used
118 Glenn Dr. Unknown Potable 575
Unknown
1405 S. Main St. Unknown Closed
Unknown
260 Unknown
1401 S. Main St. Unknown Unknown 350
5 Uwharrie Bank
160 Nicks St. Unknown Unknown2 Florentino Aguilar and Maria Navarrette
3 Robert Swink Revocable Trust
880
4 Michael Harris
Unknown1324 S. Main St. Unknown Occasional Vehicle
Washing
Unknown
350
Table 3 - Water Supply Well Information
Jerry's Amoco
Graham, North Carolina
1 Glenn and Tina Patterson 1318 S. Main St. Unknown Not Used 550 Unknown
Sample ID Approximate Water
Level (ft. BGS)
Groundwater
Elevation (ft.)
Date
Collected BenzeneEthylbenzeneChloroform1,2-DichloroethaneBromodichloromethaneIsopropylbenzenen-Propylbenzenep-IsopropyltolueneIsopropyl etherMTBENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesLead C5-C8 AliphaticsC9-C18 AliphaticsC9-C22 AromaticsN/A N/A 7/23/2002 <10 <10 <1 15 <1 NA NA NA <10 198 NA NA NA NA <10 NA NA <30 15 141 <100 <100
N/A N/A 8/9/2002 NA NA <1 21 <1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
N/A N/A 6/9/2003 30 <50 <1 <1 <1 NA NA NA <25 821 NA NA NA NA <50 NA NA <150 <5 NA NA NA
N/A N/A 10/29/2008 1.3 <1 <1 23.1 <1 NA NA NA 13.5 225 NA NA NA NA 1.6 NA NA <1 NA NA NA NA
N/A N/A 3/23/2009 <1 <1 <1 <1 <1 NA NA NA <5 6.7 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/11/2009 <1 <1 <1 1.89 <1 NA NA NA <5 7.25 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 2.96 <1 NA NA NA <5 15.1 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/28/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.4 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL 1.62 BQL BQL BQL BQL 0.39J 9.73 BQL BQL 0.59 0.10J BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL 0.1J 2.8 BQL BQL 0.2J BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL 3.2 BQL BQL 0.5 BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 6/9/2003 <1 <1 <1 <1 <1 NA NA NA <50 2,837 NA NA NA NA <1 NA NA <3 6 1,540 <100 <100
N/A N/A 10/29/2008 1.3 <1 <1 3.6 <1 NA NA NA <5 63.7 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 3/23/2009 <1 <1 <1 5.9 <1 NA NA NA <5 27.9 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/11/2009 <1 <1 <1 15.2 <1 NA NA NA <5 43.7 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 4.56 <1 NA NA NA <1 43.2 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/7/2009 <1 <1 <1 9.86 <1 <1 31.8 NA NA <1 <1 <1 <1 <1 NA NA NA NA NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 67.9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 4.6 <0.5 <0.5 <0.5 <0.5 1.4 3.1 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA <0.5 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL 5.56 BQL BQL BQL BQL 0.76 5.41 0.13J BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL 6.7 BQL BQL BQL BQL 0.7 7.5 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL 0.9 BQL BQL BQL BQL BQL 2.4 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 17.8 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL 0.8 BQL BQL BQL BQL BQL 2.7 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL 1.09 BQL BQL BQL BQL BQL 2.34 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 2/11/2016 BQL BQL BQL BQL BQL BQL BQL BQL BQL 3.4 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 12/8/2016 BQL BQL BQL 0.51 BQL BQL BQL BQL BQL 3.56 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/7/2018 BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.23 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
16.78 532.59 3/27/2020 BQL BQL BQL BQL BQL BQL BQL BQL BQL 3.8 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
19.50 529.87 11/16/2022 ND ND ND ND ND ND ND ND ND 3.8 ND ND ND ND ND ND ND ND NA NA NA NA
N/A N/A 6/9/2003 <1 <1 <1 <1 <1 NA NA NA <1 6.8 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/29/2008 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
N/A N/A 4/19/2010 <10 115 <10 <10 <10 NA NA NA <50 <50 NA NA NA NA 21.2 NA NA 431 NA NA NA NA
N/A N/A 5/17/2010 <2 28.3 <2 <2 <2 NA NA NA <10 <10 NA NA NA NA 7.83 NA NA 86.2 NA NA NA NA
N/A N/A 6/8/2010 <0.5 1.7 <0.5 <0.5 <0.5 0.8 2.8 2.9 <0.5 <0.5 <0.5 <0.5 3.4 <0.5 1.2 35.0 12.3 7.9 NA NA NA NA
N/A N/A 8/2/2012 BQL 0.34J BQL BQL BQL 1.68 2.18 4.09 BQL BQL BQL 2.47 4.35 BQL BQL 4.78 0.40J BQL NA NA NA NA
N/A N/A 10/3/2013 0.5 0.7 BQL BQL BQL 0.9 1.5 1.6 0.2J BQL BQL 4.3 8.5 BQL 0.7 1.7 0.2J 1.0 NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL 0.9 2.0 BQL 0.2J 0.5 BQL 9.5 22.2 BQL 3.0 1.5 BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL 0.64 BQL BQL BQL BQL 2.18 3.68 BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.4 BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.00 2.59 BQL BQL BQL BQL NA NA NA NA
N/A N/A 6/9/2003 <1 <1 <1 <1 <1 NA NA NA <1 <1 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/30/2008 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 6/9/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
MW-3
MW-4
MW-1
MW-2
Table 4 - Summary of Groundwater Analytical Results
Graham, North Carolina
Jerry's Amoco
Targeted Compounds VOCs Methods 601/602/6210D/6200B VPH
Sample ID Approximate Water
Level (ft. BGS)
Groundwater
Elevation (ft.)
Date
Collected BenzeneEthylbenzeneChloroform1,2-DichloroethaneBromodichloromethaneIsopropylbenzenen-Propylbenzenep-IsopropyltolueneIsopropyl etherMTBENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesLead C5-C8 AliphaticsC9-C18 AliphaticsC9-C22 AromaticsTargeted Compounds VOCs Methods 601/602/6210D/6200B VPH
N/A N/A 6/9/2003 <1 <1 <1 <1 <1 NA NA NA <1 <1 NA NA NA NA <1 NA NA <3 NA NA NA NA
N/A N/A 10/29/2008 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL 0.1J BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 7/8/2003 <1 <1 <1 <1 <1 NA NA NA <1 <1 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/30/2008 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 6/9/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 7/8/2003 3,805 1,220 <1 <500 <1 NA NA NA <500 30,650 NA NA NA NA 13,930 NA NA 3,390 41 38,300 4,290 4,690
N/A N/A 10/29/2008
N/A N/A 3/23/2009 875 1,180 <100 <100 <100 NA NA NA <100 1,310 NA NA NA NA 2,160 NA NA 4,080 NA NA NA NA
N/A N/A 5/11/2009 726 242 <100 <100 <100 NA NA NA <100 2,520 NA NA NA NA 1,150 NA NA 1,520 NA NA NA NA
N/A N/A 5/29/2009 808 176 <50 <50 <50 NA NA NA <50 8,860 NA NA NA NA 1,070 NA NA 1,300 NA NA NA NA
N/A N/A 12/7/2009 824 423 <20 <20 <20 <20 1,730 NA NA 302 1,050 NA NA NA NA NA NA NA NA NA NA NA
N/A N/A 12/30/2009 808 188 <25 <25 <25 <25 4,870 164 562 306 762 NA NA NA NA NA NA NA NA NA NA NA
N/A N/A 4/19/2010 816 201 <40 <40 <40 NA NA NA <200 3,510 NA NA NA NA 332 NA NA 909 NA NA NA NA
N/A N/A 5/17/2010 859 205 <100 <100 <100 NA NA NA <500 3,130 NA NA NA NA 357 NA NA 1,040 NA NA NA NA
N/A N/A 6/8/2010 936 224 <12.5 <12.5 <12.5 19.5 44.2 <12.5 159 1,970 200 <12.5 <12.5 <12.5 451 611 240 759 NA NA NA NA
N/A N/A 8/2/2012 286 120 BQL BQL BQL 6.75J 10.3J 13.8 25.3 1,190 77.8 BQL BQL BQL 101 403 287 600 NA NA NA NA
N/A N/A 10/3/2013 224 153 BQL BQL BQL BQL 17.0J BQL 42.0J 2,050 119 BQL BQL BQL 99.0 340 233 465 NA NA NA NA
N/A N/A 5/21/2014 280 140 BQL BQL BQL 9.0J 22.5J BQL 54.0 3,720 64.0 BQL BQL BQL 85.5 163 224 258 NA NA NA NA
N/A N/A 1/2/2015 103 102 BQL BQL BQL 9.80 28.4 BQL 31.7 2,220 51.5 BQL BQL BQL 38.8 107 229 139 NA NA NA NA
N/A N/A 4/24/2015 6.3 11.9 BQL BQL BQL 1.7 4.9 BQL 1.4 802 7.0 0.7 BQL BQL 2.2 12.2 10.8 13.9 NA NA NA NA
N/A N/A 9/24/2015 49.5 102 BQL BQL BQL 13.3 31.0 BQL 11.9 516 44.6 4.15 5.60 BQL 17.5 85.4 87.6 101 NA NA NA NA
N/A N/A 2/11/2016 BQL 69.8 BQL BQL BQL BQL BQL BQL BQL 447 59.2 BQL 41.0 BQL BQL 116 144 53.2 NA NA NA NA
N/A N/A 12/8/2016 8.39 39.3 BQL BQL BQL 11.4 18.7 BQL 2.03 52.8 27.5 BQL 4.76 BQL 2.35 27.1 30.6 24.7 NA NA NA NA
N/A N/A 9/7/2018 2.96 11.70 BQL BQL BQL 8.76 9.58 BQL 1.46 115 18.7 BQL 4.52 0.50 0.98 2.47 12.3 7.53 NA NA NA NA
14.93 531.62 3/27/2020 2.4 4.9 BQL BQL BQL 10.3 21.0 BQL BQL 118 43.5 2.9 4.7 0.6 2.30 32.8 BQL 4.8 NA NA NA NA
17.39 529.16 11/16/2022 1.1 0.83 ND ND ND 5.5 11.6 ND 1.0 41.5 14.6 ND 5.2 0.76 0.89 ND ND 1.1 NA NA NA NA
N/A N/A 7/8/2003 <1 <1 <1 9.2 <1 NA NA NA 9.2 <1 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/29/2008 <1 <1 <1 2.3 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 2.09 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 1.0 <0,5 <0.5 <9,5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 8/5/2003 <1 <1 <1 <1 <1 NA NA NA <1 5.6 NA NA NA NA 5.6 NA NA <3 <5 <100 <100 <100
N/A N/A 10/29/2008 <1 <1 <1 <1 <1 NA NA NA <5 9.3 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.6 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL 2.39 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL BQL 0.52 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.01 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 6.4 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 0.96 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/7/2018 BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.39 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
16.36 531.11 3/27/2020 BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.6 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
18.49 528.98 11/16/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA
MW-8
MW-5
MW-6
MW-9
MW-7
Dry
Sample ID Approximate Water
Level (ft. BGS)
Groundwater
Elevation (ft.)
Date
Collected BenzeneEthylbenzeneChloroform1,2-DichloroethaneBromodichloromethaneIsopropylbenzenen-Propylbenzenep-IsopropyltolueneIsopropyl etherMTBENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesLead C5-C8 AliphaticsC9-C18 AliphaticsC9-C22 AromaticsTargeted Compounds VOCs Methods 601/602/6210D/6200B VPH
N/A N/A 8/5/2003 <1 <1 <1 <1 <1 NA NA NA <1 56 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/29/2008 <1 <1 <1 <1 <1 NA NA NA <5 44.5 NA NA NA NA 1.1 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 <1 <1 NA NA NA <5 31.4 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 57.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA
N/A N/A 6/8/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 16.4 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL 0.13J 26.2 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL 0.12J 22.5 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 9.56 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 6.26 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/7/2018 BQL BQL BQL BQL BQL BQL BQL BQL BQL 5.53 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
17.5 529.5 3/27/2020 BQL BQL BQL BQL BQL BQL BQL BQL BQL 4.1 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
19.71 527.29 11/16/2022 ND ND ND ND ND ND ND ND ND 1.2 ND ND ND ND ND ND ND ND NA NA NA NA
N/A N/A 10/21/2010 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 29.9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 NA NA NA NA
N/A N/A 8/2/2012 BQL BQL BQL BQL BQL BQL BQL BQL BQL 36.6 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 10/3/2013 BQL BQL BQL BQL BQL BQL BQL BQL 0.10J 34.3 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 5/21/2014 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 1/2/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 4/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/24/2015 BQL BQL BQL BQL BQL BQL BQL BQL BQL 2.66 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 2/11/2016 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
N/A N/A 9/7/2018 BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
16.06 533.38 3/27/2020 BQL BQL BQL BQL BQL BQL BQL BQL BQL 1.3 BQL BQL BQL BQL BQL BQL BQL BQL NA NA NA NA
18.76 530.68 11/16/2022 ND ND ND ND ND ND ND ND ND 2.6 ND ND ND ND ND ND ND ND NA NA NA NA
N/A N/A 2/10/2011 2,860 962 BQL BQL B 80.0J 232 BQL 134 3,590 302 BQL BQL BQL 1,690 1,480 502 1,960 NA NA NA NA
N/A N/A 8/2/2012 894 780 BQL 52.7 BQL 59.5 172 10.0 27.6 645 247 BQL BQL BQL 3,740 871 363 1,920 NA NA NA NA
N/A N/A 10/3/2013 377 430 BQL BQL BQL 58.0 223 71.0 41.0J 1,340 456 152 67.0 BQL 525 1,130 526 838 NA NA NA NA
N/A N/A 5/21/2014 250 105 BQL BQL BQL 15.5J 52.0 BQL 21.5J 890 39.0 27.5 13.0J BQL 86.5 259 219 180 NA NA NA NA
N/A N/A 1/2/2015 596 114 BQL BQL BQL BQL BQL BQL BQL 1,100 63.0 BQL BQL BQL 134 320 286 468 NA NA NA NA
N/A N/A 4/24/2015 93.9 94.9 BQL BQL BQL 14.7 35.3 7.3 8.8 202 33.0 12.8 BQL BQL BQL 305 105 121 NA NA NA NA
N/A N/A 9/24/2015 157 72.2 BQL BQL BQL 11.8 19.6 6.40 21.7 656 37.4 13.1 11.1 BQL 7.2 224 108 138 NA NA NA NA
N/A N/A 2/11/2016 17.6 34.9 BQL BQL BQL 7.3 17.0 BQL 5.0 156 10.9 BQL 7.5 BQL BQL 191 936 19.5 NA NA NA NA
N/A N/A 12/8/2016 1.61 3.31 BQL BQL BQL 2.19 5.01 BQL 3.32 125 1.33 7.75 2.96 BQL BQL 2.14 BQL BQL NA NA NA NA
N/A N/A 9/7/2018 BQL BQL BQL BQL BQL BQL 1.66 BQL 1.38 5.73 BQL BQL 5.48 BQL BQL BQL BQL BQL NA NA NA NA
N/A NM 3/27/2020 0.9 BQL BQL BQL BQL 1.4 2.0 BQL 1.2 24.4 BQL 2.0 6.9 0.7 BQL 0.5 BQL BQL NA NA NA NA
17.56 528.21 11/16/2022 ND ND ND ND ND 0.67 ND ND ND 6.5 ND ND 5.1 0.56 ND ND ND ND NA NA NA NA
N/A N/A 4/24/2015 53.8 224 BQL BQL BQL 29.0 138 29.8 21.8 1,140 197 30.0 BQL BQL 825 945 309 994 NA NA NA NA
N/A N/A 9/24/2015 69.7 301 BQL BQL BQL 14.8 44.4 BQL 13.2 722 142 7.40 BQL BQL 338 858 137 749 NA NA NA NA
N/A N/A 12/8/2016 BQL 119 BQL BQL BQL BQL 68.8 BQL BQL 126 155 21.0 BQL BQL 424 546 254 648 NA NA NA NA
N/A N/A 12/8/2016 71.5 252 BQL BQL BQL 27.9 108 BQL 11.3 407 183 BQL 10.9 BQL 318 504 250 723 NA NA NA NA
N/A N/A 9/7/2018 16.4 22.1 BQL BQL BQL 7.32 20.5 BQL 2.92 267 16.0 BQL BQL BQL 2.0 58.4 24.7 19.2 NA NA NA NA
N/A NM 3/27/2020 5.2 9.6 BQL BQL BQL 2.9 7.6 BQL 2.0 73.9 4.2 2.1 2.5 BQL BQL 14.8 2.9 8.0 NA NA NA NA
19.32 529.64 11/16/2022
N/A N/A 6/9/2003 <1 <1 <1 <1 <1 NA NA NA <1 <1 NA NA NA NA <1 NA NA <3 <5 <100 <100 <100
N/A N/A 10/29/2008 1.0 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA 1.2 NA NA <1 NA NA NA NA
N/A N/A 5/29/2009 <1 <1 <1 <1 <1 NA NA NA <5 <5 NA NA NA NA <1 NA NA <1 NA NA NA NA
N/A N/A 12/30/2009 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.0 NA NA NA NA NA NA NA NA NA NA NA
N/A N/A 10/3/2013
N/A N/A 5/21/2014
N/A N/A 1/2/2015
1 600 70 0.4 NS 70 70 25 70 20 6 70 70 70 600 400 400 500 15 400 700 200
5,000 80,000 70,000 400 NS 30,500 26,100 11,700 70,000 20,000 6,000 5,900 8,800 14,750 260,000 28,500 24,100 50,000 15,000 NE NE NE
= Concentration Exceeds the 2L Standard
GCL = Gross Contamination Level
NA = Not Analyzed
BQL = Below Quantitation Limits
ND = Non Detect
FP = Free Product
NS = No Standard
NE = Not Established
Free Product 0.01'
DW-1
Not Sampled
Not Sampled
Not Sampled
MW-11
MW-12
MW-13
2L Standard (ug/L)
GCLs (ug/L)
MW-10

APPENDIX A

APPENDIX B
#=CL#
December 16, 2022
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92639464
92639464
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
Jerrys Amoco-B G-8830
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Lab ID Sample ID Matrix Date Collected Date Received
92639464001 MW-2 Water 12/02/22 09:15 12/02/22 11:45
92639464002 MW-7 Water 12/02/22 10:45 12/02/22 11:45
92639464003 MW-9 Water 12/02/22 09:30 12/02/22 11:45
92639464004 MW-10 Water 12/02/22 11:00 12/02/22 11:45
92639464005 MW-11 Water 12/02/22 09:52 12/02/22 11:45
92639464006 MW-12 Water 12/02/22 10:20 12/02/22 11:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92639464001 MW-2 SM 6200B 64 PASI-CCL
92639464002 MW-7 SM 6200B 64 PASI-CSAS
92639464003 MW-9 SM 6200B 64 PASI-CCL
92639464004 MW-10 SM 6200B 64 PASI-CCL
92639464005 MW-11 SM 6200B 64 PASI-CSAS
92639464006 MW-12 SM 6200B 64 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-2 Lab ID:92639464001 Collected:12/02/22 09:15 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/10/22 11:11 71-43-20.50 1
Bromobenzene ND ug/L 12/10/22 11:11 108-86-10.50 1
Bromochloromethane ND ug/L 12/10/22 11:11 74-97-50.50 1
Bromodichloromethane ND ug/L 12/10/22 11:11 75-27-40.50 1
Bromoform ND ug/L 12/10/22 11:11 75-25-20.50 1
Bromomethane ND ug/L 12/10/22 11:11 74-83-95.0 1
n-Butylbenzene ND ug/L 12/10/22 11:11 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/10/22 11:11 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/10/22 11:11 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/10/22 11:11 56-23-50.50 1
Chlorobenzene ND ug/L 12/10/22 11:11 108-90-70.50 1
Chloroethane ND ug/L 12/10/22 11:11 75-00-31.0 1
Chloroform ND ug/L 12/10/22 11:11 67-66-30.50 1
Chloromethane ND ug/L 12/10/22 11:11 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/10/22 11:11 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/10/22 11:11 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/10/22 11:11 96-12-81.0 1
Dibromochloromethane ND ug/L 12/10/22 11:11 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/10/22 11:11 106-93-40.50 1
Dibromomethane ND ug/L 12/10/22 11:11 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/10/22 11:11 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/10/22 11:11 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/10/22 11:11 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/10/22 11:11 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/10/22 11:11 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/10/22 11:11 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/10/22 11:11 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/10/22 11:11 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/10/22 11:11 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/10/22 11:11 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/10/22 11:11 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/10/22 11:11 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/10/22 11:11 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/10/22 11:11 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/10/22 11:11 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/10/22 11:11 108-20-30.50 1
Ethanol ND ug/L 12/10/22 11:11 64-17-52001
Ethylbenzene ND ug/L 12/10/22 11:11 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/10/22 11:11 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/10/22 11:11 98-82-80.50 1
Methylene Chloride ND ug/L 12/10/22 11:11 75-09-22.0 1
Methyl-tert-butyl ether 3.8 ug/L 12/10/22 11:11 1634-04-40.50 1
Naphthalene ND ug/L 12/10/22 11:11 91-20-32.0 1
n-Propylbenzene ND ug/L 12/10/22 11:11 103-65-10.50 1
Styrene ND ug/L 12/10/22 11:11 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/10/22 11:11 630-20-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-2 Lab ID:92639464001 Collected:12/02/22 09:15 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/10/22 11:11 79-34-50.50 1
Tetrachloroethene ND ug/L 12/10/22 11:11 127-18-40.50 1
Toluene ND ug/L 12/10/22 11:11 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/10/22 11:11 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/10/22 11:11 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/10/22 11:11 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/10/22 11:11 79-00-50.50 1
Trichloroethene ND ug/L 12/10/22 11:11 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/10/22 11:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/10/22 11:11 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/10/22 11:11 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/10/22 11:11 108-67-80.50 1
Vinyl chloride ND ug/L 12/10/22 11:11 75-01-41.0 1
m&p-Xylene ND ug/L 12/10/22 11:11 179601-23-11.0 1
o-Xylene ND ug/L 12/10/22 11:11 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %12/10/22 11:11 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %12/10/22 11:11 460-00-470-130 1
Toluene-d8 (S)100 %12/10/22 11:11 2037-26-570-130 1
Sample:MW-7 Lab ID:92639464002 Collected:12/02/22 10:45 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1.1 ug/L 12/14/22 18:17 71-43-20.50 1
Bromobenzene ND ug/L 12/14/22 18:17 108-86-10.50 1
Bromochloromethane ND ug/L 12/14/22 18:17 74-97-50.50 1
Bromodichloromethane ND ug/L 12/14/22 18:17 75-27-40.50 1
Bromoform ND ug/L 12/14/22 18:17 75-25-20.50 1
Bromomethane ND ug/L 12/14/22 18:17 74-83-95.0 1
n-Butylbenzene ND ug/L 12/14/22 18:17 104-51-80.50 1
sec-Butylbenzene 5.2 ug/L 12/14/22 18:17 135-98-80.50 1
tert-Butylbenzene 0.76 ug/L 12/14/22 18:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/14/22 18:17 56-23-50.50 1
Chlorobenzene ND ug/L 12/14/22 18:17 108-90-70.50 1
Chloroethane ND ug/L 12/14/22 18:17 75-00-31.0 1
Chloroform ND ug/L 12/14/22 18:17 67-66-30.50 1
Chloromethane ND ug/L 12/14/22 18:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/14/22 18:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/14/22 18:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/22 18:17 96-12-81.0 1
Dibromochloromethane ND ug/L 12/14/22 18:17 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/22 18:17 106-93-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-7 Lab ID:92639464002 Collected:12/02/22 10:45 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromomethane ND ug/L 12/14/22 18:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/14/22 18:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/14/22 18:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/14/22 18:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/14/22 18:17 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/14/22 18:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/14/22 18:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/14/22 18:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/14/22 18:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/14/22 18:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/14/22 18:17 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/14/22 18:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/14/22 18:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/14/22 18:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/14/22 18:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/14/22 18:17 10061-02-60.50 1
Diisopropyl ether 1.0 ug/L 12/14/22 18:17 108-20-30.50 1
Ethanol ND ug/L 12/14/22 18:17 64-17-52001
Ethylbenzene 0.83 ug/L 12/14/22 18:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/14/22 18:17 87-68-32.0 1
Isopropylbenzene (Cumene)5.5 ug/L 12/14/22 18:17 98-82-80.50 1
Methylene Chloride ND ug/L 12/14/22 18:17 75-09-22.0 1
Methyl-tert-butyl ether 41.5 ug/L 12/14/22 18:17 1634-04-40.50 1
Naphthalene 14.6 ug/L 12/14/22 18:17 91-20-32.0 1
n-Propylbenzene 11.6 ug/L 12/14/22 18:17 103-65-10.50 1
Styrene ND ug/L 12/14/22 18:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/22 18:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/14/22 18:17 79-34-50.50 1
Tetrachloroethene ND ug/L 12/14/22 18:17 127-18-40.50 1
Toluene 0.89 ug/L 12/14/22 18:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/14/22 18:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/14/22 18:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/14/22 18:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/14/22 18:17 79-00-50.50 1
Trichloroethene ND ug/L 12/14/22 18:17 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/14/22 18:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/14/22 18:17 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/14/22 18:17 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/14/22 18:17 108-67-80.50 1
Vinyl chloride ND ug/L 12/14/22 18:17 75-01-41.0 1
m&p-Xylene 1.1 ug/L 12/14/22 18:17 179601-23-11.0 1
o-Xylene ND ug/L 12/14/22 18:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %12/14/22 18:17 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/14/22 18:17 460-00-470-130 1
Toluene-d8 (S)100 %12/14/22 18:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-9 Lab ID:92639464003 Collected:12/02/22 09:30 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/10/22 11:29 71-43-20.50 1
Bromobenzene ND ug/L 12/10/22 11:29 108-86-10.50 1
Bromochloromethane ND ug/L 12/10/22 11:29 74-97-50.50 1
Bromodichloromethane ND ug/L 12/10/22 11:29 75-27-40.50 1
Bromoform ND ug/L 12/10/22 11:29 75-25-20.50 1
Bromomethane ND ug/L 12/10/22 11:29 74-83-95.0 1
n-Butylbenzene ND ug/L 12/10/22 11:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/10/22 11:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/10/22 11:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/10/22 11:29 56-23-50.50 1
Chlorobenzene ND ug/L 12/10/22 11:29 108-90-70.50 1
Chloroethane ND ug/L 12/10/22 11:29 75-00-31.0 1
Chloroform ND ug/L 12/10/22 11:29 67-66-30.50 1
Chloromethane ND ug/L 12/10/22 11:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/10/22 11:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/10/22 11:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/10/22 11:29 96-12-81.0 1
Dibromochloromethane ND ug/L 12/10/22 11:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/10/22 11:29 106-93-40.50 1
Dibromomethane ND ug/L 12/10/22 11:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/10/22 11:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/10/22 11:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/10/22 11:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/10/22 11:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/10/22 11:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/10/22 11:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/10/22 11:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/10/22 11:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/10/22 11:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/10/22 11:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/10/22 11:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/10/22 11:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/10/22 11:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/10/22 11:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/10/22 11:29 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/10/22 11:29 108-20-30.50 1
Ethanol ND ug/L 12/10/22 11:29 64-17-52001
Ethylbenzene ND ug/L 12/10/22 11:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/10/22 11:29 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/10/22 11:29 98-82-80.50 1
Methylene Chloride ND ug/L 12/10/22 11:29 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/10/22 11:29 1634-04-40.50 1
Naphthalene ND ug/L 12/10/22 11:29 91-20-32.0 1
n-Propylbenzene ND ug/L 12/10/22 11:29 103-65-10.50 1
Styrene ND ug/L 12/10/22 11:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/10/22 11:29 630-20-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-9 Lab ID:92639464003 Collected:12/02/22 09:30 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/10/22 11:29 79-34-50.50 1
Tetrachloroethene ND ug/L 12/10/22 11:29 127-18-40.50 1
Toluene ND ug/L 12/10/22 11:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/10/22 11:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/10/22 11:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/10/22 11:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/10/22 11:29 79-00-50.50 1
Trichloroethene ND ug/L 12/10/22 11:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/10/22 11:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/10/22 11:29 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/10/22 11:29 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/10/22 11:29 108-67-80.50 1
Vinyl chloride ND ug/L 12/10/22 11:29 75-01-41.0 1
m&p-Xylene ND ug/L 12/10/22 11:29 179601-23-11.0 1
o-Xylene ND ug/L 12/10/22 11:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %12/10/22 11:29 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %12/10/22 11:29 460-00-470-130 1
Toluene-d8 (S)99 %12/10/22 11:29 2037-26-570-130 1
Sample:MW-10 Lab ID:92639464004 Collected:12/02/22 11:00 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/10/22 11:47 71-43-20.50 1
Bromobenzene ND ug/L 12/10/22 11:47 108-86-10.50 1
Bromochloromethane ND ug/L 12/10/22 11:47 74-97-50.50 1
Bromodichloromethane ND ug/L 12/10/22 11:47 75-27-40.50 1
Bromoform ND ug/L 12/10/22 11:47 75-25-20.50 1
Bromomethane ND ug/L 12/10/22 11:47 74-83-95.0 1
n-Butylbenzene ND ug/L 12/10/22 11:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/10/22 11:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/10/22 11:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/10/22 11:47 56-23-50.50 1
Chlorobenzene ND ug/L 12/10/22 11:47 108-90-70.50 1
Chloroethane ND ug/L 12/10/22 11:47 75-00-31.0 1
Chloroform ND ug/L 12/10/22 11:47 67-66-30.50 1
Chloromethane ND ug/L 12/10/22 11:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/10/22 11:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/10/22 11:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/10/22 11:47 96-12-81.0 1
Dibromochloromethane ND ug/L 12/10/22 11:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/10/22 11:47 106-93-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-10 Lab ID:92639464004 Collected:12/02/22 11:00 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromomethane ND ug/L 12/10/22 11:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/10/22 11:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/10/22 11:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/10/22 11:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/10/22 11:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/10/22 11:47 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/10/22 11:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/10/22 11:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/10/22 11:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/10/22 11:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/10/22 11:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/10/22 11:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/10/22 11:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/10/22 11:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/10/22 11:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/10/22 11:47 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/10/22 11:47 108-20-30.50 1
Ethanol ND ug/L 12/10/22 11:47 64-17-52001
Ethylbenzene ND ug/L 12/10/22 11:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/10/22 11:47 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/10/22 11:47 98-82-80.50 1
Methylene Chloride ND ug/L 12/10/22 11:47 75-09-22.0 1
Methyl-tert-butyl ether 1.2 ug/L 12/10/22 11:47 1634-04-40.50 1
Naphthalene ND ug/L 12/10/22 11:47 91-20-32.0 1
n-Propylbenzene ND ug/L 12/10/22 11:47 103-65-10.50 1
Styrene ND ug/L 12/10/22 11:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/10/22 11:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/10/22 11:47 79-34-50.50 1
Tetrachloroethene ND ug/L 12/10/22 11:47 127-18-40.50 1
Toluene ND ug/L 12/10/22 11:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/10/22 11:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/10/22 11:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/10/22 11:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/10/22 11:47 79-00-50.50 1
Trichloroethene ND ug/L 12/10/22 11:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/10/22 11:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/10/22 11:47 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/10/22 11:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/10/22 11:47 108-67-80.50 1
Vinyl chloride ND ug/L 12/10/22 11:47 75-01-41.0 1
m&p-Xylene ND ug/L 12/10/22 11:47 179601-23-11.0 1
o-Xylene ND ug/L 12/10/22 11:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/10/22 11:47 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %12/10/22 11:47 460-00-470-130 1
Toluene-d8 (S)100 %12/10/22 11:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-11 Lab ID:92639464005 Collected:12/02/22 09:52 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/14/22 17:05 71-43-20.50 1
Bromobenzene ND ug/L 12/14/22 17:05 108-86-10.50 1
Bromochloromethane ND ug/L 12/14/22 17:05 74-97-50.50 1
Bromodichloromethane ND ug/L 12/14/22 17:05 75-27-40.50 1
Bromoform ND ug/L 12/14/22 17:05 75-25-20.50 1
Bromomethane ND ug/L 12/14/22 17:05 74-83-95.0 1
n-Butylbenzene ND ug/L 12/14/22 17:05 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/14/22 17:05 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/14/22 17:05 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/14/22 17:05 56-23-50.50 1
Chlorobenzene ND ug/L 12/14/22 17:05 108-90-70.50 1
Chloroethane ND ug/L 12/14/22 17:05 75-00-31.0 1
Chloroform ND ug/L 12/14/22 17:05 67-66-30.50 1
Chloromethane ND ug/L 12/14/22 17:05 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/14/22 17:05 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/14/22 17:05 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/22 17:05 96-12-81.0 1
Dibromochloromethane ND ug/L 12/14/22 17:05 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/22 17:05 106-93-40.50 1
Dibromomethane ND ug/L 12/14/22 17:05 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/14/22 17:05 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/14/22 17:05 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/14/22 17:05 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/14/22 17:05 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/14/22 17:05 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/14/22 17:05 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/14/22 17:05 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/14/22 17:05 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/14/22 17:05 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/14/22 17:05 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/14/22 17:05 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/14/22 17:05 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/14/22 17:05 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/14/22 17:05 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/14/22 17:05 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/14/22 17:05 108-20-30.50 1
Ethanol ND ug/L 12/14/22 17:05 64-17-52001
Ethylbenzene ND ug/L 12/14/22 17:05 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/14/22 17:05 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 12/14/22 17:05 98-82-80.50 1
Methylene Chloride ND ug/L 12/14/22 17:05 75-09-22.0 1
Methyl-tert-butyl ether 2.6 ug/L 12/14/22 17:05 1634-04-40.50 1
Naphthalene ND ug/L 12/14/22 17:05 91-20-32.0 1
n-Propylbenzene ND ug/L 12/14/22 17:05 103-65-10.50 1
Styrene ND ug/L 12/14/22 17:05 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/22 17:05 630-20-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-11 Lab ID:92639464005 Collected:12/02/22 09:52 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 12/14/22 17:05 79-34-50.50 1
Tetrachloroethene ND ug/L 12/14/22 17:05 127-18-40.50 1
Toluene ND ug/L 12/14/22 17:05 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/14/22 17:05 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/14/22 17:05 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/14/22 17:05 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/14/22 17:05 79-00-50.50 1
Trichloroethene ND ug/L 12/14/22 17:05 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/14/22 17:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/14/22 17:05 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/14/22 17:05 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/14/22 17:05 108-67-80.50 1
Vinyl chloride ND ug/L 12/14/22 17:05 75-01-41.0 1
m&p-Xylene ND ug/L 12/14/22 17:05 179601-23-11.0 1
o-Xylene ND ug/L 12/14/22 17:05 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %12/14/22 17:05 17060-07-070-130 1
4-Bromofluorobenzene (S)103 %12/14/22 17:05 460-00-470-130 1
Toluene-d8 (S)99 %12/14/22 17:05 2037-26-570-130 1
Sample:MW-12 Lab ID:92639464006 Collected:12/02/22 10:20 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 12/14/22 17:23 71-43-20.50 1
Bromobenzene ND ug/L 12/14/22 17:23 108-86-10.50 1
Bromochloromethane ND ug/L 12/14/22 17:23 74-97-50.50 1
Bromodichloromethane ND ug/L 12/14/22 17:23 75-27-40.50 1
Bromoform ND ug/L 12/14/22 17:23 75-25-20.50 1
Bromomethane ND ug/L 12/14/22 17:23 74-83-95.0 1
n-Butylbenzene ND ug/L 12/14/22 17:23 104-51-80.50 1
sec-Butylbenzene 5.1 ug/L 12/14/22 17:23 135-98-80.50 1
tert-Butylbenzene 0.56 ug/L 12/14/22 17:23 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/14/22 17:23 56-23-50.50 1
Chlorobenzene ND ug/L 12/14/22 17:23 108-90-70.50 1
Chloroethane ND ug/L 12/14/22 17:23 75-00-31.0 1
Chloroform ND ug/L 12/14/22 17:23 67-66-30.50 1
Chloromethane ND ug/L 12/14/22 17:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/14/22 17:23 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/14/22 17:23 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/14/22 17:23 96-12-81.0 1
Dibromochloromethane ND ug/L 12/14/22 17:23 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 12/14/22 17:23 106-93-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Sample:MW-12 Lab ID:92639464006 Collected:12/02/22 10:20 Received:12/02/22 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromomethane ND ug/L 12/14/22 17:23 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/14/22 17:23 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/14/22 17:23 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/14/22 17:23 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/14/22 17:23 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/14/22 17:23 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/14/22 17:23 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/14/22 17:23 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/14/22 17:23 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/14/22 17:23 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/14/22 17:23 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/14/22 17:23 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/14/22 17:23 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/14/22 17:23 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/14/22 17:23 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/14/22 17:23 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/14/22 17:23 108-20-30.50 1
Ethanol ND ug/L 12/14/22 17:23 64-17-52001
Ethylbenzene ND ug/L 12/14/22 17:23 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/14/22 17:23 87-68-32.0 1
Isopropylbenzene (Cumene)0.67 ug/L 12/14/22 17:23 98-82-80.50 1
Methylene Chloride ND ug/L 12/14/22 17:23 75-09-22.0 1
Methyl-tert-butyl ether 6.5 ug/L 12/14/22 17:23 1634-04-40.50 1
Naphthalene ND ug/L 12/14/22 17:23 91-20-32.0 1
n-Propylbenzene ND ug/L 12/14/22 17:23 103-65-10.50 1
Styrene ND ug/L 12/14/22 17:23 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/14/22 17:23 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/14/22 17:23 79-34-50.50 1
Tetrachloroethene ND ug/L 12/14/22 17:23 127-18-40.50 1
Toluene ND ug/L 12/14/22 17:23 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/14/22 17:23 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/14/22 17:23 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/14/22 17:23 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/14/22 17:23 79-00-50.50 1
Trichloroethene ND ug/L 12/14/22 17:23 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/14/22 17:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/14/22 17:23 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/14/22 17:23 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/14/22 17:23 108-67-80.50 1
Vinyl chloride ND ug/L 12/14/22 17:23 75-01-41.0 1
m&p-Xylene ND ug/L 12/14/22 17:23 179601-23-11.0 1
o-Xylene ND ug/L 12/14/22 17:23 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %12/14/22 17:23 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %12/14/22 17:23 460-00-470-130 1
Toluene-d8 (S)102 %12/14/22 17:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
741836
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92639464001, 92639464003, 92639464004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3859137
Associated Lab Samples:92639464001, 92639464003, 92639464004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/10/22 03:55
1,1,1-Trichloroethane ug/L ND 0.50 12/10/22 03:55
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/10/22 03:55
1,1,2-Trichloroethane ug/L ND 0.50 12/10/22 03:55
1,1-Dichloroethane ug/L ND 0.50 12/10/22 03:55
1,1-Dichloroethene ug/L ND 0.50 12/10/22 03:55
1,1-Dichloropropene ug/L ND 0.50 12/10/22 03:55
1,2,3-Trichlorobenzene ug/L ND 2.0 12/10/22 03:55
1,2,3-Trichloropropane ug/L ND 0.50 12/10/22 03:55
1,2,4-Trichlorobenzene ug/L ND 2.0 12/10/22 03:55
1,2,4-Trimethylbenzene ug/L ND 0.50 12/10/22 03:55
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/10/22 03:55
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/10/22 03:55
1,2-Dichlorobenzene ug/L ND 0.50 12/10/22 03:55
1,2-Dichloroethane ug/L ND 0.50 12/10/22 03:55
1,2-Dichloropropane ug/L ND 0.50 12/10/22 03:55
1,3,5-Trimethylbenzene ug/L ND 0.50 12/10/22 03:55
1,3-Dichlorobenzene ug/L ND 0.50 12/10/22 03:55
1,3-Dichloropropane ug/L ND 0.50 12/10/22 03:55
1,4-Dichlorobenzene ug/L ND 0.50 12/10/22 03:55
2,2-Dichloropropane ug/L ND 0.50 12/10/22 03:55
2-Chlorotoluene ug/L ND 0.50 12/10/22 03:55
4-Chlorotoluene ug/L ND 0.50 12/10/22 03:55
Benzene ug/L ND 0.50 12/10/22 03:55
Bromobenzene ug/L ND 0.50 12/10/22 03:55
Bromochloromethane ug/L ND 0.50 12/10/22 03:55
Bromodichloromethane ug/L ND 0.50 12/10/22 03:55
Bromoform ug/L ND 0.50 12/10/22 03:55
Bromomethane ug/L ND 5.0 12/10/22 03:55
Carbon tetrachloride ug/L ND 0.50 12/10/22 03:55
Chlorobenzene ug/L ND 0.50 12/10/22 03:55
Chloroethane ug/L ND 1.0 12/10/22 03:55
Chloroform ug/L ND 0.50 12/10/22 03:55
Chloromethane ug/L ND 1.0 12/10/22 03:55
cis-1,2-Dichloroethene ug/L ND 0.50 12/10/22 03:55
cis-1,3-Dichloropropene ug/L ND 0.50 12/10/22 03:55
Dibromochloromethane ug/L ND 0.50 12/10/22 03:55
Dibromomethane ug/L ND 0.50 12/10/22 03:55
Dichlorodifluoromethane ug/L ND 0.50 12/10/22 03:55
Diisopropyl ether ug/L ND 0.50 12/10/22 03:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3859137
Associated Lab Samples:92639464001, 92639464003, 92639464004
Matrix:Water
Analyzed
Ethanol ug/L ND 200 12/10/22 03:55
Ethylbenzene ug/L ND 0.50 12/10/22 03:55
Hexachloro-1,3-butadiene ug/L ND 2.0 12/10/22 03:55
Isopropylbenzene (Cumene)ug/L ND 0.50 12/10/22 03:55
m&p-Xylene ug/L ND 1.0 12/10/22 03:55
Methyl-tert-butyl ether ug/L ND 0.50 12/10/22 03:55
Methylene Chloride ug/L ND 2.0 12/10/22 03:55
n-Butylbenzene ug/L ND 0.50 12/10/22 03:55
n-Propylbenzene ug/L ND 0.50 12/10/22 03:55
Naphthalene ug/L ND 2.0 12/10/22 03:55
o-Xylene ug/L ND 0.50 12/10/22 03:55
sec-Butylbenzene ug/L ND 0.50 12/10/22 03:55
Styrene ug/L ND 0.50 12/10/22 03:55
tert-Butylbenzene ug/L ND 0.50 12/10/22 03:55
Tetrachloroethene ug/L ND 0.50 12/10/22 03:55
Toluene ug/L ND 0.50 12/10/22 03:55
trans-1,2-Dichloroethene ug/L ND 0.50 12/10/22 03:55
trans-1,3-Dichloropropene ug/L ND 0.50 12/10/22 03:55
Trichloroethene ug/L ND 0.50 12/10/22 03:55
Trichlorofluoromethane ug/L ND 1.0 12/10/22 03:55
Vinyl chloride ug/L ND 1.0 12/10/22 03:55
1,2-Dichloroethane-d4 (S)%93 70-130 12/10/22 03:55
4-Bromofluorobenzene (S)%96 70-130 12/10/22 03:55
Toluene-d8 (S)%100 70-130 12/10/22 03:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3859138LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.950 106 60-140
1,1,1-Trichloroethane ug/L 52.150 104 60-140
1,1,2,2-Tetrachloroethane ug/L 50.050 100 60-140
1,1,2-Trichloroethane ug/L 52.750 105 60-140
1,1-Dichloroethane ug/L 46.150 92 60-140
1,1-Dichloroethene ug/L 52.650 105 60-140
1,1-Dichloropropene ug/L 54.250 108 60-140
1,2,3-Trichlorobenzene ug/L 53.950 108 60-140
1,2,3-Trichloropropane ug/L 49.250 98 60-140
1,2,4-Trichlorobenzene ug/L 54.450 109 60-140
1,2,4-Trimethylbenzene ug/L 49.250 98 60-140
1,2-Dibromo-3-chloropropane ug/L 48.750 97 60-140
1,2-Dibromoethane (EDB)ug/L 50.850 102 60-140
1,2-Dichlorobenzene ug/L 51.650 103 60-140
1,2-Dichloroethane ug/L 48.750 97 60-140
1,2-Dichloropropane ug/L 49.750 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3859138LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 50.250 100 60-140
1,3-Dichlorobenzene ug/L 52.350 105 60-140
1,3-Dichloropropane ug/L 49.850 100 60-140
1,4-Dichlorobenzene ug/L 50.650 101 60-140
2,2-Dichloropropane ug/L 44.850 90 60-140
2-Chlorotoluene ug/L 49.550 99 60-140
4-Chlorotoluene ug/L 48.850 98 60-140
Benzene ug/L 48.250 96 60-140
Bromobenzene ug/L 51.250 102 60-140
Bromochloromethane ug/L 50.350 101 60-140
Bromodichloromethane ug/L 49.050 98 60-140
Bromoform ug/L 53.450 107 60-140
Bromomethane ug/L 48.050 96 60-140
Carbon tetrachloride ug/L 52.650 105 60-140
Chlorobenzene ug/L 51.150 102 60-140
Chloroethane ug/L 39.850 80 60-140
Chloroform ug/L 49.150 98 60-140
Chloromethane ug/L 47.150 94 60-140
cis-1,2-Dichloroethene ug/L 47.250 94 60-140
cis-1,3-Dichloropropene ug/L 50.350 101 60-140
Dibromochloromethane ug/L 50.650 101 60-140
Dibromomethane ug/L 54.350 109 60-140
Dichlorodifluoromethane ug/L 60.250 120 60-140
Diisopropyl ether ug/L 43.850 88 60-140
Ethanol ug/L 16502000 83 60-140
Ethylbenzene ug/L 51.150 102 60-140
Hexachloro-1,3-butadiene ug/L 54.550 109 60-140
Isopropylbenzene (Cumene)ug/L 49.950 100 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 45.750 91 60-140
Methylene Chloride ug/L 45.250 90 60-140
n-Butylbenzene ug/L 52.350 105 60-140
n-Propylbenzene ug/L 49.350 99 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 50.150 100 60-140
sec-Butylbenzene ug/L 48.850 98 60-140
Styrene ug/L 51.050 102 60-140
tert-Butylbenzene ug/L 41.650 83 60-140
Tetrachloroethene ug/L 50.050 100 60-140
Toluene ug/L 50.050 100 60-140
trans-1,2-Dichloroethene ug/L 49.650 99 60-140
trans-1,3-Dichloropropene ug/L 49.850 100 60-140
Trichloroethene ug/L 55.350 111 60-140
Trichlorofluoromethane ug/L 53.550 107 60-140
Vinyl chloride ug/L 50.850 102 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3859138LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3861506MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92639802016
3861507
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12012760-140151 17 3020ND25.5 30.1
1,1,1-Trichloroethane ug/L M12013060-140149 14 3020ND25.9 29.8
1,1,2,2-Tetrachloroethane ug/L 20 119 60-140136 13 3020ND23.7 27.1
1,1,2-Trichloroethane ug/L 20 122 60-140139 13 3020ND24.4 27.8
1,1-Dichloroethane ug/L 20 110 60-140127 15 3020ND21.9 25.4
1,1-Dichloroethene ug/L M12012860-140145 13 3020ND25.5 29.0
1,1-Dichloropropene ug/L M12013360-140152 13 3020ND26.5 30.3
1,2,3-Trichlorobenzene ug/L M12013160-140149 13 3020ND26.1 29.8
1,2,3-Trichloropropane ug/L 20 116 60-140133 13 3020ND23.3 26.6
1,2,4-Trichlorobenzene ug/L M12013860-140156 13 3020ND27.5 31.2
1,2,4-Trimethylbenzene ug/L M12012860-140141 9 3020ND25.6 28.1
1,2-Dibromo-3-
chloropropane ug/L 20 115 60-140131 13 3020ND23.0 26.1
1,2-Dibromoethane (EDB)ug/L 20 120 60-140137 13 3020ND24.0 27.4
1,2-Dichlorobenzene ug/L M12012860-140146 13 3020ND25.7 29.2
1,2-Dichloroethane ug/L 20 114 60-140131 14 3020ND22.9 26.2
1,2-Dichloropropane ug/L 20 117 60-140135 14 3020ND23.4 26.9
1,3,5-Trimethylbenzene ug/L M12013060-140148 13 3020ND26.0 29.5
1,3-Dichlorobenzene ug/L M12013260-140150 13 3020ND26.5 30.0
1,3-Dichloropropane ug/L 20 119 60-140137 14 3020ND23.8 27.4
1,4-Dichlorobenzene ug/L M12012760-140145 13 3020ND25.4 29.1
2,2-Dichloropropane ug/L M12012960-140149 14 3020ND25.9 29.7
2-Chlorotoluene ug/L M12012660-140143 13 3020ND25.2 28.6
4-Chlorotoluene ug/L M12012560-140142 12 3020ND25.0 28.3
Benzene ug/L 20 118 60-140135 13 3020ND23.6 27.0
Bromobenzene ug/L M12012860-140145 12 3020ND25.6 29.0
Bromochloromethane ug/L 20 116 60-140133 14 3020ND23.1 26.6
Bromodichloromethane ug/L 20 115 60-140133 14 3020ND23.0 26.6
Bromoform ug/L 20 121 60-140140 15 3020ND24.1 28.0
Bromomethane ug/L M12012760-140147 14 3020ND25.4 29.3
Carbon tetrachloride ug/L M12013560-140156 14 3020ND26.9 31.1
Chlorobenzene ug/L M12012860-140147 14 3020ND25.6 29.4
Chloroethane ug/L 20 119 60-140134 11 3020ND23.9 26.7
Chloroform ug/L 20 120 60-140130 8 3020ND23.9 25.9
Chloromethane ug/L 20 98 60-140113 15 3020ND19.6 22.7
cis-1,2-Dichloroethene ug/L 20 111 60-140128 14 3020ND22.3 25.5
cis-1,3-Dichloropropene ug/L 20 119 60-140138 15 3020ND23.7 27.6
Dibromochloromethane ug/L 20 118 60-140138 15 3020ND23.7 27.5
Dibromomethane ug/L M12012560-140146 15 3020ND25.1 29.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3861506MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92639802016
3861507
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 20 115 60-140131 13 3020ND23.1 26.2
Diisopropyl ether ug/L 20 97 60-140111 14 3020ND19.3 22.3
Ethanol ug/L 800 93 60-140109 16 30800ND746875
Ethylbenzene ug/L M12013160-140148 13 3020ND26.1 29.6
Hexachloro-1,3-butadiene ug/L M12014760-140169 14 3020ND29.4 33.8
Isopropylbenzene
(Cumene)ug/L M12012860-140145 13 3020ND25.5 29.0
m&p-Xylene ug/L M14013160-140150 13 3040ND52.4 59.8
Methyl-tert-butyl ether ug/L 20 99 60-140114 14 3020ND19.9 22.8
Methylene Chloride ug/L 20 105 60-140121 14 3020ND21.0 24.2
n-Butylbenzene ug/L M12014260-140159 11 3020ND28.4 31.9
n-Propylbenzene ug/L M12013560-140148 10 3020ND26.9 29.7
Naphthalene ug/L M12015960-140151 5 3020ND32.3 30.7
o-Xylene ug/L M12012560-140145 15 3020ND24.9 29.0
sec-Butylbenzene ug/L M12013060-140148 13 3020ND26.1 29.7
Styrene ug/L M12012460-140144 15 3020ND24.7 28.9
tert-Butylbenzene ug/L 20 107 60-140123 13 3020ND21.5 24.6
Tetrachloroethene ug/L M12013060-140148 13 3020ND26.0 29.5
Toluene ug/L M12012460-140141 13 3020ND24.7 28.2
trans-1,2-Dichloroethene ug/L 20 119 60-140138 14 3020ND23.8 27.5
trans-1,3-Dichloropropene ug/L 20 117 60-140135 14 3020ND23.4 26.9
Trichloroethene ug/L M12013660-140157 14 3020ND27.2 31.4
Trichlorofluoromethane ug/L M12013760-140157 14 3020ND27.4 31.3
Vinyl chloride ug/L 20 115 60-140130 12 3020ND22.9 26.0
1,2-Dichloroethane-d4 (S)%94 70-13093
4-Bromofluorobenzene (S)%96 70-13096
Toluene-d8 (S)%96 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
743441
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92639464002, 92639464005, 92639464006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3867874
Associated Lab Samples:92639464002, 92639464005, 92639464006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/14/22 16:28
1,1,1-Trichloroethane ug/L ND 0.50 12/14/22 16:28
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/14/22 16:28
1,1,2-Trichloroethane ug/L ND 0.50 12/14/22 16:28
1,1-Dichloroethane ug/L ND 0.50 12/14/22 16:28
1,1-Dichloroethene ug/L ND 0.50 12/14/22 16:28
1,1-Dichloropropene ug/L ND 0.50 12/14/22 16:28
1,2,3-Trichlorobenzene ug/L ND 2.0 12/14/22 16:28
1,2,3-Trichloropropane ug/L ND 0.50 12/14/22 16:28
1,2,4-Trichlorobenzene ug/L ND 2.0 12/14/22 16:28
1,2,4-Trimethylbenzene ug/L ND 0.50 12/14/22 16:28
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/14/22 16:28
1,2-Dibromoethane (EDB)ug/L ND 0.50 12/14/22 16:28
1,2-Dichlorobenzene ug/L ND 0.50 12/14/22 16:28
1,2-Dichloroethane ug/L ND 0.50 12/14/22 16:28
1,2-Dichloropropane ug/L ND 0.50 12/14/22 16:28
1,3,5-Trimethylbenzene ug/L ND 0.50 12/14/22 16:28
1,3-Dichlorobenzene ug/L ND 0.50 12/14/22 16:28
1,3-Dichloropropane ug/L ND 0.50 12/14/22 16:28
1,4-Dichlorobenzene ug/L ND 0.50 12/14/22 16:28
2,2-Dichloropropane ug/L ND 0.50 12/14/22 16:28
2-Chlorotoluene ug/L ND 0.50 12/14/22 16:28
4-Chlorotoluene ug/L ND 0.50 12/14/22 16:28
Benzene ug/L ND 0.50 12/14/22 16:28
Bromobenzene ug/L ND 0.50 12/14/22 16:28
Bromochloromethane ug/L ND 0.50 12/14/22 16:28
Bromodichloromethane ug/L ND 0.50 12/14/22 16:28
Bromoform ug/L ND 0.50 12/14/22 16:28
Bromomethane ug/L ND 5.0 12/14/22 16:28
Carbon tetrachloride ug/L ND 0.50 12/14/22 16:28
Chlorobenzene ug/L ND 0.50 12/14/22 16:28
Chloroethane ug/L ND 1.0 12/14/22 16:28
Chloroform ug/L ND 0.50 12/14/22 16:28
Chloromethane ug/L ND 1.0 12/14/22 16:28
cis-1,2-Dichloroethene ug/L ND 0.50 12/14/22 16:28
cis-1,3-Dichloropropene ug/L ND 0.50 12/14/22 16:28
Dibromochloromethane ug/L ND 0.50 12/14/22 16:28
Dibromomethane ug/L ND 0.50 12/14/22 16:28
Dichlorodifluoromethane ug/L ND 0.50 12/14/22 16:28
Diisopropyl ether ug/L ND 0.50 12/14/22 16:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3867874
Associated Lab Samples:92639464002, 92639464005, 92639464006
Matrix:Water
Analyzed
Ethanol ug/L ND 200 12/14/22 16:28
Ethylbenzene ug/L ND 0.50 12/14/22 16:28
Hexachloro-1,3-butadiene ug/L ND 2.0 12/14/22 16:28
Isopropylbenzene (Cumene)ug/L ND 0.50 12/14/22 16:28
m&p-Xylene ug/L ND 1.0 12/14/22 16:28
Methyl-tert-butyl ether ug/L ND 0.50 12/14/22 16:28
Methylene Chloride ug/L ND 2.0 12/14/22 16:28
n-Butylbenzene ug/L ND 0.50 12/14/22 16:28
n-Propylbenzene ug/L ND 0.50 12/14/22 16:28
Naphthalene ug/L ND 2.0 12/14/22 16:28
o-Xylene ug/L ND 0.50 12/14/22 16:28
sec-Butylbenzene ug/L ND 0.50 12/14/22 16:28
Styrene ug/L ND 0.50 12/14/22 16:28
tert-Butylbenzene ug/L ND 0.50 12/14/22 16:28
Tetrachloroethene ug/L ND 0.50 12/14/22 16:28
Toluene ug/L ND 0.50 12/14/22 16:28
trans-1,2-Dichloroethene ug/L ND 0.50 12/14/22 16:28
trans-1,3-Dichloropropene ug/L ND 0.50 12/14/22 16:28
Trichloroethene ug/L ND 0.50 12/14/22 16:28
Trichlorofluoromethane ug/L ND 1.0 12/14/22 16:28
Vinyl chloride ug/L ND 1.0 12/14/22 16:28
1,2-Dichloroethane-d4 (S)%96 70-130 12/14/22 16:28
4-Bromofluorobenzene (S)%98 70-130 12/14/22 16:28
Toluene-d8 (S)%103 70-130 12/14/22 16:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3867875LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.250 114 60-140
1,1,1-Trichloroethane ug/L 53.450 107 60-140
1,1,2,2-Tetrachloroethane ug/L 52.750 105 60-140
1,1,2-Trichloroethane ug/L 52.350 105 60-140
1,1-Dichloroethane ug/L 46.650 93 60-140
1,1-Dichloroethene ug/L 50.650 101 60-140
1,1-Dichloropropene ug/L 57.250 114 60-140
1,2,3-Trichlorobenzene ug/L 58.350 117 60-140
1,2,3-Trichloropropane ug/L 48.650 97 60-140
1,2,4-Trichlorobenzene ug/L 54.250 108 60-140
1,2,4-Trimethylbenzene ug/L 52.950 106 60-140
1,2-Dibromo-3-chloropropane ug/L 57.350 115 60-140
1,2-Dibromoethane (EDB)ug/L 56.650 113 60-140
1,2-Dichlorobenzene ug/L 54.950 110 60-140
1,2-Dichloroethane ug/L 49.750 99 60-140
1,2-Dichloropropane ug/L 54.350 109 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3867875LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 54.250 108 60-140
1,3-Dichlorobenzene ug/L 54.950 110 60-140
1,3-Dichloropropane ug/L 54.850 110 60-140
1,4-Dichlorobenzene ug/L 50.250 100 60-140
2,2-Dichloropropane ug/L 51.350 103 60-140
2-Chlorotoluene ug/L 57.350 115 60-140
4-Chlorotoluene ug/L 54.050 108 60-140
Benzene ug/L 49.450 99 60-140
Bromobenzene ug/L 54.950 110 60-140
Bromochloromethane ug/L 49.450 99 60-140
Bromodichloromethane ug/L 52.150 104 60-140
Bromoform ug/L 57.850 116 60-140
Bromomethane ug/L 44.350 89 60-140
Carbon tetrachloride ug/L 53.650 107 60-140
Chlorobenzene ug/L 53.150 106 60-140
Chloroethane ug/L 41.250 82 60-140
Chloroform ug/L 45.050 90 60-140
Chloromethane ug/L 45.550 91 60-140
cis-1,2-Dichloroethene ug/L 49.350 99 60-140
cis-1,3-Dichloropropene ug/L 55.550 111 60-140
Dibromochloromethane ug/L 50.150 100 60-140
Dibromomethane ug/L 55.150 110 60-140
Dichlorodifluoromethane ug/L 39.350 79 60-140
Diisopropyl ether ug/L 52.850 106 60-140
Ethanol ug/L 19702000 99 60-140
Ethylbenzene ug/L 51.550 103 60-140
Hexachloro-1,3-butadiene ug/L 54.450 109 60-140
Isopropylbenzene (Cumene)ug/L 51.350 103 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 47.550 95 60-140
Methylene Chloride ug/L 42.450 85 60-140
n-Butylbenzene ug/L 54.550 109 60-140
n-Propylbenzene ug/L 53.750 107 60-140
Naphthalene ug/L 60.950 122 60-140
o-Xylene ug/L 52.350 105 60-140
sec-Butylbenzene ug/L 52.450 105 60-140
Styrene ug/L 53.050 106 60-140
tert-Butylbenzene ug/L 44.650 89 60-140
Tetrachloroethene ug/L 54.150 108 60-140
Toluene ug/L 49.250 98 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 52.550 105 60-140
Trichloroethene ug/L 57.550 115 60-140
Trichlorofluoromethane ug/L 40.850 82 60-140
Vinyl chloride ug/L 44.950 90 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3867875LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3867876MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92641049001
3867877
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 124 60-140131 6 304000ND49605250
1,1,1-Trichloroethane ug/L 4000 117 60-140131 12 304000ND46805250
1,1,2,2-Tetrachloroethane ug/L 4000 111 60-140113 2 304000ND44304520
1,1,2-Trichloroethane ug/L 4000 110 60-140119 7 304000ND44104750
1,1-Dichloroethane ug/L 4000 105 60-140112 7 304000ND41804500
1,1-Dichloroethene ug/L 4000 115 60-140125 9 304000ND46005020
1,1-Dichloropropene ug/L 4000 124 60-140132 6 304000ND49605290
1,2,3-Trichlorobenzene ug/L 4000 107 60-140124 15 304000ND42904970
1,2,3-Trichloropropane ug/L 4000 108 60-140111 3 304000ND43204440
1,2,4-Trichlorobenzene ug/L 4000 109 60-140120 9 304000ND43704780
1,2,4-Trimethylbenzene ug/L 4000 113 60-140121 5 304000243069507280
1,2-Dibromo-3-
chloropropane ug/L 4000 114 60-140117 3 304000ND45704700
1,2-Dibromoethane (EDB)ug/L 4000 120 60-140126 4 30400029951105330
1,2-Dichlorobenzene ug/L 4000 114 60-140122 7 304000ND45404880
1,2-Dichloroethane ug/L 4000 110 60-140117 6 30400020145904880
1,2-Dichloropropane ug/L 4000 119 60-140125 5 304000ND47405010
1,3,5-Trimethylbenzene ug/L 4000 114 60-140121 5 30400072953105580
1,3-Dichlorobenzene ug/L 4000 117 60-140123 5 304000ND46904910
1,3-Dichloropropane ug/L 4000 113 60-140120 6 304000ND45404810
1,4-Dichlorobenzene ug/L 4000 109 60-140118 8 304000ND43704710
2,2-Dichloropropane ug/L 4000 114 60-140126 10 304000ND45405020
2-Chlorotoluene ug/L 4000 108 60-140121 12 304000ND43104830
4-Chlorotoluene ug/L 4000 115 60-140121 6 304000ND45804850
Benzene ug/L 4000 109 60-140119 3 30400075001190012300
Bromobenzene ug/L 4000 115 60-140123 7 304000ND46104930
Bromochloromethane ug/L 4000 114 60-140125 9 304000ND45804990
Bromodichloromethane ug/L 4000 109 60-140117 7 304000ND43604680
Bromoform ug/L 4000 118 60-140121 2 304000ND47404850
Bromomethane ug/L 4000 68 60-14083 19 304000ND27303320
Carbon tetrachloride ug/L 4000 117 60-140127 8 304000ND46905070
Chlorobenzene ug/L 4000 115 60-140125 8 304000ND46005000
Chloroethane ug/L 4000 100 60-140113 12 304000ND39904520
Chloroform ug/L 4000 101 60-140109 7 304000ND41004410
Chloromethane ug/L 4000 89 60-14099 11 304000ND35803980
cis-1,2-Dichloroethene ug/L 4000 109 60-140119 9 304000ND43704760
cis-1,3-Dichloropropene ug/L 4000 113 60-140125 10 304000ND45204990
Dibromochloromethane ug/L 4000 105 60-140112 7 304000ND42004480
Dibromomethane ug/L 4000 116 60-140124 6 304000ND46604960
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3867876MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92641049001
3867877
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 4000 75 60-14083 10 304000ND30103340
Diisopropyl ether ug/L 4000 104 60-140113 8 30400013443104660
Ethanol ug/L 160000 102 60-140106 3 30160000ND163000169000
Ethylbenzene ug/L 4000 113 60-140120 4 304000206065906870
Hexachloro-1,3-butadiene ug/L 4000 116 60-140129 11 304000ND46405170
Isopropylbenzene
(Cumene)ug/L 4000 113 60-140121 7 30400011346404970
m&p-Xylene ug/L 8000 113 60-140125 5 30800093701840019300
Methyl-tert-butyl ether ug/L 4000 98 60-140103 4 30400075646704870
Methylene Chloride ug/L 4000 96 60-140106 9 304000ND38404220
n-Butylbenzene ug/L 4000 118 60-140124 5 304000ND47004950
n-Propylbenzene ug/L 4000 113 60-140122 7 30400022847605090
Naphthalene ug/L 4000 114 60-140124 7 30400081653805760
o-Xylene ug/L 4000 115 60-140126 5 304000433089509370
sec-Butylbenzene ug/L 4000 112 60-140121 8 304000ND44704830
Styrene ug/L 4000 115 60-140122 6 30400010846904980
tert-Butylbenzene ug/L 4000 97 60-140104 7 304000ND38704150
Tetrachloroethene ug/L 4000 118 60-140126 7 304000ND47105040
Toluene ug/L 4000 70 60-14099 4 304000251002790029100
trans-1,2-Dichloroethene ug/L 4000 109 60-140122 11 304000ND43704900
trans-1,3-Dichloropropene ug/L 4000 111 60-140118 6 304000ND44304720
Trichloroethene ug/L 4000 122 60-140130 7 304000ND48605210
Trichlorofluoromethane ug/L 4000 92 60-140102 10 304000ND36804060
Vinyl chloride ug/L 4000 98 60-140108 10 304000ND39304330
1,2-Dichloroethane-d4 (S)%97 70-13097
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92639464
Jerrys Amoco-B G-8830
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92639464001 741836MW-2 SM 6200B
92639464002 743441MW-7 SM 6200B
92639464003 741836MW-9 SM 6200B
92639464004 741836MW-10 SM 6200B
92639464005 743441MW-11 SM 6200B
92639464006 743441MW-12 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2022 03:54 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 28
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