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Home My WebLink AboutWS-5930_21402_CA_IAR_2014110706/17/14 Technical Report for Terraquest Environmental Quality Mart 7; Winston-Salem, NC 04198 Accutest Job Number: FA15409 Sampling Dates: 05/28/14 - 05/29/14 Report to: Terra Quest Environmental mwebster@terraquestpc.com ATTN: Megan Webster Total number of pages in report: Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001) DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177), AK, AR, GA, KY, MA, NV, OK, UT, WA This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Heather Wandrey 407-425-6700 Harry Behzadi, Ph.D. Laboratory Director Southeast 06/17/14 e-Hardcopy 2.0 Automated Report 208 Accutest Laboratories is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. 1 of 208 FA15409 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................4 Section 2: Summary of Hits ....................................................................................................7 Section 3: Sample Results ........................................................................................................16 3.1: FA15409-1: B1 8-10 .....................................................................................................17 3.2: FA15409-2: B2 8-10 .....................................................................................................20 3.3: FA15409-3: B3 8-10 .....................................................................................................23 3.4: FA15409-4: B4 8-10 .....................................................................................................27 3.5: FA15409-5: B5 8-10 .....................................................................................................31 3.6: FA15409-6: B6 8-10 .....................................................................................................34 3.7: FA15409-7: B7 8-10 .....................................................................................................37 3.8: FA15409-8: B8 13-15 ...................................................................................................40 3.9: FA15409-9: B9 13-14 ...................................................................................................44 3.10: FA15409-10: B10 8-10 ...............................................................................................48 3.11: FA15409-11: B11 8-10 ................................................................................................52 3.12: FA15409-12: B12 8-10 ...............................................................................................59 3.13: FA15409-13: B13 8-10 ...............................................................................................65 3.14: FA15409-14: B14 13-15 .............................................................................................71 3.15: FA15409-15: B15 13-15 .............................................................................................77 3.16: FA15409-16: B16 13-15 .............................................................................................79 3.17: FA15409-17: B17 13-15 .............................................................................................80 3.18: FA15409-18: G1 0-5 ...................................................................................................81 3.19: FA15409-19: G2 0-5 ...................................................................................................84 3.20: FA15409-20: D16 3-4 .................................................................................................85 3.21: FA15409-21: K16 1.5 .................................................................................................87 3.22: FA15409-22: TRIP BLANK .......................................................................................89 3.23: FA15409-23: GW 1 .....................................................................................................92 3.24: FA15409-24: MW 1 ....................................................................................................95 3.25: FA15409-25: MW 4 ....................................................................................................103 3.26: FA15409-26: MW 5 ....................................................................................................106 3.27: FA15409-27: TRIP BLANK .......................................................................................109 Section 4: Misc. Forms ............................................................................................................112 4.1: Chain of Custody ...........................................................................................................113 Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................117 5.1: Method Blank Summary ................................................................................................118 5.2: Blank Spike Summary ...................................................................................................135 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................152 Section 6: GC/MS Semi-volatiles - QC Data Summaries .....................................................166 6.1: Method Blank Summary ................................................................................................167 6.2: Blank Spike Summary ...................................................................................................174 6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................180 Section 7: GC Volatiles - QC Data Summaries .....................................................................184 7.1: Method Blank Summary ................................................................................................185 123456782 of 208 FA15409 Table of Contents -2- Sections: 7.2: Blank Spike Summary ...................................................................................................189 7.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................190 7.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................193 7.5: Duplicate Summary .......................................................................................................194 Section 8: GC Semi-volatiles - QC Data Summaries ............................................................197 8.1: Method Blank Summary ................................................................................................198 8.2: Blank Spike Summary ...................................................................................................202 8.3: Blank Spike/Blank Spike Duplicate Summary ..............................................................203 8.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................206 8.5: Duplicate Summary .......................................................................................................207 123456783 of 208 FA15409 Accutest LabLink@151826 11:13 17-Jun-2014 Sample Summary Terraquest Environmental Job No:FA15409 Quality Mart 7; Winston-Salem, NC Project No: 04198 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA15409-1 05/28/14 12:22 JL 05/30/14 SO Soil B1 8-10 FA15409-2 05/28/14 12:07 JL 05/30/14 SO Soil B2 8-10 FA15409-3 05/28/14 11:52 JL 05/30/14 SO Soil B3 8-10 FA15409-4 05/28/14 11:44 JL 05/30/14 SO Soil B4 8-10 FA15409-5 05/28/14 10:43 JL 05/30/14 SO Soil B5 8-10 FA15409-6 05/28/14 10:50 JL 05/30/14 SO Soil B6 8-10 FA15409-7 05/28/14 10:55 JL 05/30/14 SO Soil B7 8-10 FA15409-8 05/28/14 12:17 JL 05/30/14 SO Soil B8 13-15 FA15409-9 05/28/14 11:37 JL 05/30/14 SO Soil B9 13-14 FA15409-10 05/28/14 12:27 JL 05/30/14 SO Soil B10 8-10 FA15409-11 05/28/14 12:32 JL 05/30/14 SO Soil B11 8-10 FA15409-12 05/28/14 11:19 JL 05/30/14 SO Soil B12 8-10 FA15409-13 05/28/14 11:12 JL 05/30/14 SO Soil B13 8-10 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 4 of 208 FA15409 1 Accutest LabLink@151826 11:13 17-Jun-2014 Sample Summary (continued) Terraquest Environmental Job No:FA15409 Quality Mart 7; Winston-Salem, NC Project No: 04198 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA15409-14 05/28/14 11:28 JL 05/30/14 SO Soil B14 13-15 FA15409-15 05/28/14 10:16 JL 05/30/14 SO Soil B15 13-15 FA15409-16 05/28/14 10:26 JL 05/30/14 SO Soil B16 13-15 FA15409-17 05/28/14 10:37 JL 05/30/14 SO Soil B17 13-15 FA15409-18 05/28/14 14:19 JL 05/30/14 SO Soil G1 0-5 FA15409-19 05/28/14 14:27 JL 05/30/14 SO Soil G2 0-5 FA15409-20 05/28/14 14:23 JL 05/30/14 SO Soil D16 3-4 FA15409-21 05/28/14 14:32 JL 05/30/14 SO Soil K16 1.5 FA15409-22 05/28/14 00:00 JL 05/30/14 SO Trip Blank Soil TRIP BLANK FA15409-23 05/28/14 14:00 JL 05/30/14 AQ Ground Water GW 1 FA15409-24 05/29/14 12:35 JL 05/30/14 AQ Ground Water MW 1 FA15409-25 05/29/14 12:38 JL 05/30/14 AQ Ground Water MW 4 FA15409-26 05/29/14 12:40 JL 05/30/14 AQ Ground Water MW 5 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 5 of 208 FA15409 1 Accutest LabLink@151826 11:13 17-Jun-2014 Sample Summary (continued) Terraquest Environmental Job No:FA15409 Quality Mart 7; Winston-Salem, NC Project No: 04198 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA15409-27 05/28/14 00:00 JL 05/30/14 AQ Trip Blank Water TRIP BLANK Soil samples reported on a dry weight basis unless otherwise indicated on result page. 6 of 208 FA15409 1 Summary of Hits Page 1 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA15409-1 B1 8-10 Acetone 0.0702 0.049 0.015 mg/kg SW846 8260B Benzene 0.0384 0.0049 0.00098 mg/kg SW846 8260B n-Butylbenzene 0.0054 0.0049 0.00098 mg/kg SW846 8260B sec-Butylbenzene 0.0055 0.0049 0.00098 mg/kg SW846 8260B Di-Isopropyl ether 0.0085 0.0049 0.0010 mg/kg SW846 8260B Ethylbenzene 0.0307 0.0049 0.00098 mg/kg SW846 8260B Isopropylbenzene 0.0113 0.0049 0.00098 mg/kg SW846 8260B p-Isopropyltoluene 0.0019 J 0.0049 0.00098 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.0266 0.0049 0.00098 mg/kg SW846 8260B Naphthalene 0.0560 0.0049 0.0020 mg/kg SW846 8260B n-Propylbenzene 0.0192 0.0049 0.00098 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 0.0059 0.0049 0.00098 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 0.0023 J 0.0049 0.00098 mg/kg SW846 8260B Toluene 0.0042 J 0.0049 0.00098 mg/kg SW846 8260B Xylene (total)0.0168 0.015 0.0026 mg/kg SW846 8260B m,p-Xylene 0.0124 0.0098 0.0016 mg/kg SW846 8260B o-Xylene 0.0044 J 0.0049 0.0010 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)2.99 J 6.3 2.2 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)3.70 J 6.3 2.2 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)4.01 J 6.3 2.2 mg/kg MADEP VPH REV 1.1 FA15409-2 B2 8-10 Acetone 0.0326 J 0.056 0.017 mg/kg SW846 8260B Di-Isopropyl ether 0.0089 0.0056 0.0011 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.0030 J 0.0056 0.0011 mg/kg SW846 8260B C9- C12 Aliphatics (Unadj.)4.47 J 7.8 2.7 mg/kg MADEP VPH REV 1.1 FA15409-3 B3 8-10 Benzene 0.312 J 0.34 0.068 mg/kg SW846 8260B n-Butylbenzene 5.43 0.34 0.068 mg/kg SW846 8260B sec-Butylbenzene 2.02 0.34 0.068 mg/kg SW846 8260B Ethylbenzene 37.5 3.4 0.68 mg/kg SW846 8260B Isopropylbenzene 4.57 0.34 0.068 mg/kg SW846 8260B p-Isopropyltoluene 1.39 0.34 0.068 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.427 0.34 0.068 mg/kg SW846 8260B Naphthalene 40.9 3.4 1.4 mg/kg SW846 8260B n-Propylbenzene 19.4 3.4 0.68 mg/kg SW846 8260B Styrene 3.95 0.34 0.068 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 164 6.8 1.4 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 51.6 3.4 0.68 mg/kg SW846 8260B Toluene 39.4 3.4 0.68 mg/kg SW846 8260B 7 of 208 FA15409 2 Summary of Hits Page 2 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method Xylene (total)257 10 1.8 mg/kg SW846 8260B m,p-Xylene 173 6.8 1.1 mg/kg SW846 8260B o-Xylene 83.7 3.4 0.73 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)1470 J 3500 1200 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)2800 J 3500 1200 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)7270 3500 1200 mg/kg MADEP VPH REV 1.1 FA15409-4 B4 8-10 Acetone 0.0541 0.049 0.015 mg/kg SW846 8260B Di-Isopropyl ether 0.0105 0.0049 0.0010 mg/kg SW846 8260B Methyl ethyl ketone 0.0265 0.025 0.0074 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.338 0.33 0.067 mg/kg SW846 8260B Naphthalene 0.0022 J 0.0049 0.0020 mg/kg SW846 8260B FA15409-5 B5 8-10 Acetone 0.0230 J 0.053 0.016 mg/kg SW846 8260B FA15409-6 B6 8-10 Acetone 0.0418 J 0.055 0.016 mg/kg SW846 8260B FA15409-7 B7 8-10 Acetone 0.0559 0.051 0.015 mg/kg SW846 8260B FA15409-8 B8 13-15 n-Butylbenzene 6.64 0.53 0.11 mg/kg SW846 8260B sec-Butylbenzene 3.43 0.53 0.11 mg/kg SW846 8260B tert-Butylbenzene 0.293 J 0.53 0.11 mg/kg SW846 8260B Ethylbenzene 0.237 J 0.53 0.11 mg/kg SW846 8260B Isopropylbenzene 4.55 0.53 0.11 mg/kg SW846 8260B p-Isopropyltoluene 3.25 0.53 0.11 mg/kg SW846 8260B Naphthalene 0.841 0.53 0.21 mg/kg SW846 8260B n-Propylbenzene 17.3 0.53 0.11 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 49.6 5.3 1.1 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 17.5 0.53 0.11 mg/kg SW846 8260B m,p-Xylene 0.194 J 1.1 0.17 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)1110 370 130 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)311 J 370 130 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)903 370 130 mg/kg MADEP VPH REV 1.1 8 of 208 FA15409 2 Summary of Hits Page 3 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA15409-9 B9 13-14 Benzene 0.0879 0.0055 0.0011 mg/kg SW846 8260B n-Butylbenzene 0.0601 0.0055 0.0011 mg/kg SW846 8260B sec-Butylbenzene 0.0200 0.0055 0.0011 mg/kg SW846 8260B Di-Isopropyl ether 0.0065 0.0055 0.0011 mg/kg SW846 8260B Ethylbenzene 2.72 0.36 0.073 mg/kg SW846 8260B Isopropylbenzene 0.0545 0.0055 0.0011 mg/kg SW846 8260B p-Isopropyltoluene 0.0149 0.0055 0.0011 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.0629 0.0055 0.0011 mg/kg SW846 8260B Naphthalene 1.68 0.36 0.15 mg/kg SW846 8260B n-Propylbenzene 0.153 0.0055 0.0011 mg/kg SW846 8260B Styrene 0.0432 0.0055 0.0011 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 6.51 0.36 0.073 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 1.90 0.36 0.073 mg/kg SW846 8260B Toluene 13.1 0.36 0.073 mg/kg SW846 8260B Xylene (total)16.4 1.1 0.19 mg/kg SW846 8260B m,p-Xylene 11.0 0.73 0.12 mg/kg SW846 8260B o-Xylene 5.38 0.36 0.078 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)24.2 J 30 11 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)26.6 J 30 11 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)66.7 30 11 mg/kg MADEP VPH REV 1.1 FA15409-10 B10 8-10 Benzene 1.04 0.36 0.073 mg/kg SW846 8260B n-Butylbenzene 1.26 0.36 0.073 mg/kg SW846 8260B sec-Butylbenzene 0.412 0.36 0.073 mg/kg SW846 8260B Di-Isopropyl ether 0.149 J 0.36 0.075 mg/kg SW846 8260B Ethylbenzene 6.46 0.36 0.073 mg/kg SW846 8260B Isopropylbenzene 0.956 0.36 0.073 mg/kg SW846 8260B p-Isopropyltoluene 0.300 J 0.36 0.073 mg/kg SW846 8260B Methyl Tert Butyl Ether 2.01 0.36 0.073 mg/kg SW846 8260B Naphthalene 6.25 0.36 0.15 mg/kg SW846 8260B n-Propylbenzene 3.31 0.36 0.073 mg/kg SW846 8260B Styrene 0.210 J 0.36 0.073 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 24.8 3.6 0.73 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 6.48 0.36 0.073 mg/kg SW846 8260B Toluene 3.77 0.36 0.073 mg/kg SW846 8260B Xylene (total)21.1 1.1 0.19 mg/kg SW846 8260B m,p-Xylene 13.3 0.73 0.12 mg/kg SW846 8260B o-Xylene 7.80 0.36 0.078 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)12.1 7.9 2.8 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)10.3 7.9 2.8 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)17.7 7.9 2.8 mg/kg MADEP VPH REV 1.1 9 of 208 FA15409 2 Summary of Hits Page 4 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA15409-11 B11 8-10 Benzene 0.777 0.32 0.063 mg/kg SW846 8260B n-Butylbenzene 6.80 0.32 0.063 mg/kg SW846 8260B sec-Butylbenzene 2.18 0.32 0.063 mg/kg SW846 8260B tert-Butylbenzene 0.106 J 0.32 0.063 mg/kg SW846 8260B Ethylbenzene 26.2 3.2 0.63 mg/kg SW846 8260B Isopropylbenzene 4.86 0.32 0.063 mg/kg SW846 8260B p-Isopropyltoluene 1.52 0.32 0.063 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.864 0.32 0.063 mg/kg SW846 8260B Naphthalene 43.6 3.2 1.3 mg/kg SW846 8260B n-Propylbenzene 19.6 3.2 0.63 mg/kg SW846 8260B Styrene 0.818 0.32 0.063 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 122 3.2 0.63 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 40.7 3.2 0.63 mg/kg SW846 8260B Toluene 7.99 0.32 0.063 mg/kg SW846 8260B Xylene (total)130 9.5 1.7 mg/kg SW846 8260B m,p-Xylene 90.4 6.3 1.0 mg/kg SW846 8260B o-Xylene 39.6 3.2 0.68 mg/kg SW846 8260B Acenaphthene 0.0333 J 0.21 0.026 mg/kg SW846 8270D Acenaphthylene 0.0391 J 0.21 0.021 mg/kg SW846 8270D Anthracene 0.107 J 0.21 0.021 mg/kg SW846 8270D Benzo(a)anthracene 0.174 J 0.21 0.021 mg/kg SW846 8270D Benzo(a)pyrene 0.121 J 0.21 0.021 mg/kg SW846 8270D Benzo(b)fluoranthene 0.113 J 0.21 0.021 mg/kg SW846 8270D Benzo(g,h,i)perylene 0.0686 J 0.21 0.021 mg/kg SW846 8270D Benzo(k)fluoranthene 0.119 J 0.21 0.023 mg/kg SW846 8270D Chrysene 0.171 J 0.21 0.021 mg/kg SW846 8270D Dibenzofuran 0.0329 J 0.21 0.021 mg/kg SW846 8270D Fluoranthene 0.438 0.21 0.021 mg/kg SW846 8270D Fluorene 0.0840 J 0.21 0.021 mg/kg SW846 8270D Indeno(1,2,3-cd)pyrene 0.0740 J 0.21 0.021 mg/kg SW846 8270D 1-Methylnaphthalene 7.16 1.7 0.17 mg/kg SW846 8270D 2-Methylnaphthalene 16.6 1.7 0.17 mg/kg SW846 8270D Naphthalene 19.4 1.7 0.17 mg/kg SW846 8270D Phenanthrene 0.402 0.21 0.021 mg/kg SW846 8270D Pyrene 0.390 0.21 0.021 mg/kg SW846 8270D C5- C8 Aliphatics (Unadj.)342 J 660 230 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)556 J 660 230 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)1380 660 230 mg/kg MADEP VPH REV 1.1 C11-C22 Aromatics (Unadj.)188 50 38 mg/kg MADEP EPH REV 1.1 C9-C18 Aliphatics 420 50 25 mg/kg MADEP EPH REV 1.1 C19-C36 Aliphatics 27.5 J 50 25 mg/kg MADEP EPH REV 1.1 10 of 208 FA15409 2 Summary of Hits Page 5 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA15409-12 B12 8-10 Acetone 0.0365 J 0.049 0.015 mg/kg SW846 8260B Ethylbenzene 0.0038 J 0.0049 0.00098 mg/kg SW846 8260B Naphthalene 0.0037 J 0.0049 0.0020 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 0.0049 0.0049 0.00098 mg/kg SW846 8260B Toluene 0.0038 J 0.0049 0.00098 mg/kg SW846 8260B Xylene (total)0.0237 0.015 0.0026 mg/kg SW846 8260B m,p-Xylene 0.0152 0.0098 0.0016 mg/kg SW846 8260B o-Xylene 0.0085 0.0049 0.0011 mg/kg SW846 8260B C11-C22 Aromatics (Unadj.)13.0 13 9.5 mg/kg MADEP EPH REV 1.1 C19-C36 Aliphatics 30.4 13 6.3 mg/kg MADEP EPH REV 1.1 FA15409-13 B13 8-10 Acetone 0.218 0.054 0.016 mg/kg SW846 8260B Benzene 0.0127 0.0054 0.0011 mg/kg SW846 8260B Di-Isopropyl ether 0.0038 J 0.0054 0.0011 mg/kg SW846 8260B Ethylbenzene 0.0025 J 0.0054 0.0011 mg/kg SW846 8260B Methyl ethyl ketone 0.0391 0.027 0.0081 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.0109 0.0054 0.0011 mg/kg SW846 8260B Naphthalene 0.0038 J 0.0054 0.0022 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 0.0030 J 0.0054 0.0011 mg/kg SW846 8260B Toluene 0.0024 J 0.0054 0.0011 mg/kg SW846 8260B Xylene (total)0.0056 J 0.016 0.0029 mg/kg SW846 8260B m,p-Xylene 0.0040 J 0.011 0.0017 mg/kg SW846 8260B o-Xylene 0.0017 J 0.0054 0.0012 mg/kg SW846 8260B FA15409-14 B14 13-15 Benzene 1.13 0.35 0.070 mg/kg SW846 8260B n-Butylbenzene 0.524 0.35 0.070 mg/kg SW846 8260B sec-Butylbenzene 0.156 J 0.35 0.070 mg/kg SW846 8260B Ethylbenzene 2.94 0.35 0.070 mg/kg SW846 8260B Isopropylbenzene 0.328 J 0.35 0.070 mg/kg SW846 8260B p-Isopropyltoluene 0.113 J 0.35 0.070 mg/kg SW846 8260B Methylene chloride 0.348 JB 0.70 0.28 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.137 J 0.35 0.070 mg/kg SW846 8260B Naphthalene 2.04 0.35 0.14 mg/kg SW846 8260B n-Propylbenzene 1.19 0.35 0.070 mg/kg SW846 8260B Styrene 0.163 J 0.35 0.070 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 7.32 0.35 0.070 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 2.26 0.35 0.070 mg/kg SW846 8260B Toluene 12.7 0.35 0.070 mg/kg SW846 8260B Xylene (total)17.2 1.1 0.19 mg/kg SW846 8260B 11 of 208 FA15409 2 Summary of Hits Page 6 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method m,p-Xylene 11.7 0.70 0.11 mg/kg SW846 8260B o-Xylene 5.48 0.35 0.075 mg/kg SW846 8260B 1-Methylnaphthalene 0.569 0.21 0.021 mg/kg SW846 8270D 2-Methylnaphthalene 1.26 0.21 0.021 mg/kg SW846 8270D Naphthalene 0.951 0.21 0.021 mg/kg SW846 8270D C5- C8 Aliphatics (Unadj.)47.1 30 11 mg/kg MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)48.2 30 11 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)75.6 30 11 mg/kg MADEP VPH REV 1.1 C11-C22 Aromatics (Unadj.)30.6 13 9.4 mg/kg MADEP EPH REV 1.1 C9-C18 Aliphatics 108 13 6.3 mg/kg MADEP EPH REV 1.1 FA15409-15 B15 13-15 No hits reported in this sample. FA15409-16 B16 13-15 No hits reported in this sample. FA15409-17 B17 13-15 No hits reported in this sample. FA15409-18 G1 0-5 Acetone 0.120 0.045 0.013 mg/kg SW846 8260B Benzene 0.0101 0.0045 0.00090 mg/kg SW846 8260B n-Butylbenzene 0.0061 0.0045 0.00090 mg/kg SW846 8260B sec-Butylbenzene 0.0030 J 0.0045 0.00090 mg/kg SW846 8260B Ethylbenzene 0.104 0.0045 0.00090 mg/kg SW846 8260B Isopropylbenzene 0.0084 0.0045 0.00090 mg/kg SW846 8260B Methyl ethyl ketone 0.0223 0.022 0.0067 mg/kg SW846 8260B Methyl Tert Butyl Ether 0.0037 J 0.0045 0.00090 mg/kg SW846 8260B Naphthalene 0.0570 0.0045 0.0018 mg/kg SW846 8260B n-Propylbenzene 0.0277 0.0045 0.00090 mg/kg SW846 8260B 1,2,4-Trimethylbenzene 0.0706 0.0045 0.00090 mg/kg SW846 8260B 1,3,5-Trimethylbenzene 0.0194 0.0045 0.00090 mg/kg SW846 8260B Toluene 0.0046 0.0045 0.00090 mg/kg SW846 8260B Xylene (total)0.0497 0.013 0.0024 mg/kg SW846 8260B m,p-Xylene 0.0472 0.0090 0.0014 mg/kg SW846 8260B o-Xylene 0.0024 J 0.0045 0.00096 mg/kg SW846 8260B C5- C8 Aliphatics (Unadj.)1.91 J 4.8 1.7 mg/kg MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)4.95 4.8 1.7 mg/kg MADEP VPH REV 1.1 12 of 208 FA15409 2 Summary of Hits Page 7 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA15409-19 G2 0-5 TPH-GRO (C6-C10)16.6 5.8 2.9 mg/kg SW846 8015C FA15409-20 D16 3-4 TPH (C10-C28) a 12.0 5.4 3.2 mg/kg SW846 8015C FA15409-21 K16 1.5 TPH (C10-C28) a 152 27 16 mg/kg SW846 8015C FA15409-22 TRIP BLANK Methylene chloride b 0.0048 JB 0.010 0.0040 mg/kg SW846 8260B FA15409-23 GW 1 Benzene c 57.9 2.5 0.50 ug/l SM 6200B n-Butylbenzene c 0.93 J 2.5 0.50 ug/l SM 6200B sec-Butylbenzene c 0.65 J 2.5 0.50 ug/l SM 6200B Chloroethane c 1.7 J 2.5 0.61 ug/l SM 6200B Di-Isopropyl ether c 10.1 2.5 0.50 ug/l SM 6200B Ethylbenzene c 31.2 2.5 0.50 ug/l SM 6200B Isopropylbenzene c 6.7 2.5 0.50 ug/l SM 6200B Methyl chloride c 0.79 J 2.5 0.50 ug/l SM 6200B Methyl Tert Butyl Ether c 52.4 2.5 0.50 ug/l SM 6200B Naphthalene c 85.2 2.5 0.50 ug/l SM 6200B n-Propylbenzene c 5.9 2.5 0.50 ug/l SM 6200B Styrene c 3.1 2.5 0.50 ug/l SM 6200B 1,2,4-Trimethylbenzene c 13.0 2.5 0.50 ug/l SM 6200B Toluene c 22.6 2.5 0.50 ug/l SM 6200B Xylene (total) c 284 30 4.0 ug/l SM 6200B m,p-Xylene c 9.7 J 20 2.0 ug/l SM 6200B o-Xylene c 274 10 2.0 ug/l SM 6200B FA15409-24 MW 1 Benzene 2000 25 5.0 ug/l SM 6200B n-Butylbenzene 10.5 J 25 5.0 ug/l SM 6200B sec-Butylbenzene 6.9 J 25 5.0 ug/l SM 6200B Di-Isopropyl ether 182 25 5.0 ug/l SM 6200B Ethylbenzene 860 25 5.0 ug/l SM 6200B Isopropylbenzene 29.6 25 5.0 ug/l SM 6200B Methyl Tert Butyl Ether 393 25 5.0 ug/l SM 6200B 13 of 208 FA15409 2 Summary of Hits Page 8 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method Naphthalene 551 25 5.0 ug/l SM 6200B n-Propylbenzene 87.4 25 5.0 ug/l SM 6200B 1,2,4-Trimethylbenzene 66.4 25 5.0 ug/l SM 6200B 1,3,5-Trimethylbenzene 8.4 J 25 5.0 ug/l SM 6200B Toluene 1180 25 5.0 ug/l SM 6200B Xylene (total)644 75 10 ug/l SM 6200B m,p-Xylene 483 50 5.0 ug/l SM 6200B o-Xylene 161 25 5.0 ug/l SM 6200B 2,4-Dimethylphenol 0.78 J 4.8 0.48 ug/l EPA 625 Acenaphthene 0.54 J 4.8 0.48 ug/l EPA 625 Dibenzofuran 1.0 J 4.8 0.51 ug/l EPA 625 bis(2-Ethylhexyl)phthalate 566 38 12 ug/l EPA 625 Fluorene 1.3 J 4.8 0.48 ug/l EPA 625 1-Methylnaphthalene 90.4 4.8 0.48 ug/l EPA 625 2-Methylnaphthalene 155 38 4.1 ug/l EPA 625 Naphthalene 470 38 3.8 ug/l EPA 625 Total TIC, Semi-Volatile 912 J ug/l C5- C8 Aliphatics (Unadj.)6370 1000 350 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.)1930 1000 350 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.)1930 1000 350 ug/l MADEP VPH REV 1.1 C11-C22 Aromatics (Unadj.)1860 190 140 ug/l MADEP EPH REV 1.1 C9-C18 Aliphatics 1200 190 96 ug/l MADEP EPH REV 1.1 FA15409-25 MW 4 Benzene 395 25 5.0 ug/l SM 6200B n-Butylbenzene 11.0 J 25 5.0 ug/l SM 6200B sec-Butylbenzene 12.6 J 25 5.0 ug/l SM 6200B Ethylbenzene 1160 25 5.0 ug/l SM 6200B Isopropylbenzene 129 25 5.0 ug/l SM 6200B p-Isopropyltoluene 19.3 J 25 5.0 ug/l SM 6200B Naphthalene 401 25 5.0 ug/l SM 6200B n-Propylbenzene 268 25 5.0 ug/l SM 6200B Styrene 7.3 J 25 5.0 ug/l SM 6200B 1,2,4-Trimethylbenzene 2070 25 5.0 ug/l SM 6200B 1,3,5-Trimethylbenzene 665 25 5.0 ug/l SM 6200B Toluene 665 25 5.0 ug/l SM 6200B Xylene (total)5110 75 10 ug/l SM 6200B m,p-Xylene 2690 50 5.0 ug/l SM 6200B o-Xylene 2410 25 5.0 ug/l SM 6200B FA15409-26 MW 5 Benzene 53.9 10 2.0 ug/l SM 6200B n-Butylbenzene 8.0 J 10 2.0 ug/l SM 6200B 14 of 208 FA15409 2 Summary of Hits Page 9 of 9 Job Number:FA15409 Account:Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Collected:05/28/14 thru 05/29/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method sec-Butylbenzene 13.4 10 2.0 ug/l SM 6200B Ethylbenzene 786 10 2.0 ug/l SM 6200B Isopropylbenzene 109 10 2.0 ug/l SM 6200B p-Isopropyltoluene 8.5 J 10 2.0 ug/l SM 6200B Naphthalene 308 10 2.0 ug/l SM 6200B n-Propylbenzene 199 10 2.0 ug/l SM 6200B 1,2,4-Trimethylbenzene 233 10 2.0 ug/l SM 6200B 1,3,5-Trimethylbenzene 37.4 10 2.0 ug/l SM 6200B Toluene 16.2 10 2.0 ug/l SM 6200B Xylene (total)382 30 4.0 ug/l SM 6200B m,p-Xylene 345 20 2.0 ug/l SM 6200B o-Xylene 36.6 10 2.0 ug/l SM 6200B FA15409-27 TRIP BLANK Acetone 2.4 J 10 1.0 ug/l SM 6200B (a) Petroleum hydrocarbon pattern extends beyond C28. (b) Suspected laboratory contaminant. (c) Sample vial(s) contained significant headspace; reported results are considered minimum values. 15 of 208 FA15409 2 Accutest LabLink@151826 11:13 17-Jun-2014 Sample Results Report of Analysis Southeast Section 3 16 of 208 FA15409 3 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B1 8-10 Lab Sample ID:FA15409-1 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:81.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064640.D 1 05/30/14 AH n/a n/a VF2135 Run #2 Initial Weight Run #1 6.31 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0702 0.049 0.015 mg/kg 71-43-2 Benzene 0.0384 0.0049 0.00098 mg/kg 108-86-1 Bromobenzene ND 0.0049 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0049 0.0019 mg/kg 75-27-4 Bromodichloromethane ND 0.0049 0.00098 mg/kg 75-25-2 Bromoform ND 0.0049 0.0011 mg/kg 104-51-8 n-Butylbenzene 0.0054 0.0049 0.00098 mg/kg 135-98-8 sec-Butylbenzene 0.0055 0.0049 0.00098 mg/kg 98-06-6 tert-Butylbenzene ND 0.0049 0.00098 mg/kg 108-90-7 Chlorobenzene ND 0.0049 0.00098 mg/kg 75-00-3 Chloroethane ND 0.0049 0.0022 mg/kg 67-66-3 Chloroform ND 0.0049 0.0011 mg/kg 95-49-8 o-Chlorotoluene ND 0.0049 0.00098 mg/kg 106-43-4 p-Chlorotoluene ND 0.0049 0.00098 mg/kg 56-23-5 Carbon tetrachloride ND 0.0049 0.0014 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0049 0.00098 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0049 0.00098 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0049 0.0011 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0049 0.0017 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0049 0.00098 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0049 0.00098 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0049 0.00098 mg/kg 108-20-3 Di-Isopropyl ether 0.0085 0.0049 0.0010 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0049 0.0014 mg/kg 124-48-1 Dibromochloromethane ND 0.0049 0.00098 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0049 0.0012 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0049 0.00098 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0049 0.00098 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0049 0.00098 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0049 0.00098 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0049 0.0011 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0049 0.0013 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 208 FA15409 33.1 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B1 8-10 Lab Sample ID:FA15409-1 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:81.2 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0049 0.00098 mg/kg 64-17-5 Ethyl alcohol ND 0.39 0.065 mg/kg 100-41-4 Ethylbenzene 0.0307 0.0049 0.00098 mg/kg 591-78-6 2-Hexanone ND 0.024 0.0048 mg/kg 98-82-8 Isopropylbenzene 0.0113 0.0049 0.00098 mg/kg 99-87-6 p-Isopropyltoluene 0.0019 0.0049 0.00098 mg/kg J 108-10-1 4-Methyl-2-pentanone ND 0.024 0.0049 mg/kg 74-83-9 Methyl bromide ND 0.0049 0.0018 mg/kg 74-87-3 Methyl chloride ND 0.0049 0.0020 mg/kg 75-09-2 Methylene chloride ND 0.0098 0.0039 mg/kg 78-93-3 Methyl ethyl ketone ND 0.024 0.0073 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.0266 0.0049 0.00098 mg/kg 91-20-3 Naphthalene 0.0560 0.0049 0.0020 mg/kg 103-65-1 n-Propylbenzene 0.0192 0.0049 0.00098 mg/kg 100-42-5 Styrene ND 0.0049 0.00098 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0049 0.0010 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0049 0.00098 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0049 0.0014 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0049 0.0016 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0049 0.0012 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0049 0.0018 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0049 0.0011 mg/kg 95-63-6 1,2,4-Trimethylbenzene 0.0059 0.0049 0.00098 mg/kg 108-67-8 1,3,5-Trimethylbenzene 0.0023 0.0049 0.00098 mg/kg J 127-18-4 Tetrachloroethylene ND 0.0049 0.0012 mg/kg 108-88-3 Toluene 0.0042 0.0049 0.00098 mg/kg J 79-01-6 Trichloroethylene ND 0.0049 0.0010 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0049 0.00098 mg/kg 75-01-4 Vinyl chloride ND 0.0049 0.0010 mg/kg 108-05-4 Vinyl Acetate ND 0.024 0.0078 mg/kg 1330-20-7 Xylene (total)0.0168 0.015 0.0026 mg/kg m,p-Xylene 0.0124 0.0098 0.0016 mg/kg 95-47-6 o-Xylene 0.0044 0.0049 0.0010 mg/kg J CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 91%75-124% 2037-26-5 Toluene-D8 91%75-126% 460-00-4 4-Bromofluorobenzene 100%71-133% 17060-07-0 1,2-Dichloroethane-D4 105%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 208 FA15409 33.1 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B1 8-10 Lab Sample ID:FA15409-1 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:81.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007901.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.09 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)2.99 6.3 2.2 mg/kg J C9- C12 Aliphatics (Unadj.)3.70 6.3 2.2 mg/kg J C9- C10 Aromatics (Unadj.)4.01 6.3 2.2 mg/kg J CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 129%70-130% 460-00-4 BFB 118%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 208 FA15409 33.1 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B2 8-10 Lab Sample ID:FA15409-2 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:70.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064641.D 1 05/30/14 AH n/a n/a VF2135 Run #2 Initial Weight Run #1 6.35 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0326 0.056 0.017 mg/kg J 71-43-2 Benzene ND 0.0056 0.0011 mg/kg 108-86-1 Bromobenzene ND 0.0056 0.0012 mg/kg 74-97-5 Bromochloromethane ND 0.0056 0.0021 mg/kg 75-27-4 Bromodichloromethane ND 0.0056 0.0011 mg/kg 75-25-2 Bromoform ND 0.0056 0.0012 mg/kg 104-51-8 n-Butylbenzene ND 0.0056 0.0011 mg/kg 135-98-8 sec-Butylbenzene ND 0.0056 0.0011 mg/kg 98-06-6 tert-Butylbenzene ND 0.0056 0.0011 mg/kg 108-90-7 Chlorobenzene ND 0.0056 0.0011 mg/kg 75-00-3 Chloroethane ND 0.0056 0.0025 mg/kg 67-66-3 Chloroform ND 0.0056 0.0013 mg/kg 95-49-8 o-Chlorotoluene ND 0.0056 0.0011 mg/kg 106-43-4 p-Chlorotoluene ND 0.0056 0.0011 mg/kg 56-23-5 Carbon tetrachloride ND 0.0056 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0056 0.0011 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0056 0.0011 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0056 0.0012 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0056 0.0020 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0056 0.0011 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0056 0.0011 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0056 0.0011 mg/kg 108-20-3 Di-Isopropyl ether 0.0089 0.0056 0.0011 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0056 0.0016 mg/kg 124-48-1 Dibromochloromethane ND 0.0056 0.0011 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0056 0.0014 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0056 0.0011 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0056 0.0011 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0056 0.0011 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0056 0.0011 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0056 0.0012 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0056 0.0015 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 208 FA15409 33.2 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B2 8-10 Lab Sample ID:FA15409-2 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:70.9 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0056 0.0011 mg/kg 64-17-5 Ethyl alcohol ND 0.44 0.074 mg/kg 100-41-4 Ethylbenzene ND 0.0056 0.0011 mg/kg 591-78-6 2-Hexanone ND 0.028 0.0054 mg/kg 98-82-8 Isopropylbenzene ND 0.0056 0.0011 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0056 0.0011 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.028 0.0056 mg/kg 74-83-9 Methyl bromide ND 0.0056 0.0021 mg/kg 74-87-3 Methyl chloride ND 0.0056 0.0022 mg/kg 75-09-2 Methylene chloride ND 0.011 0.0044 mg/kg 78-93-3 Methyl ethyl ketone ND 0.028 0.0083 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.0030 0.0056 0.0011 mg/kg J 91-20-3 Naphthalene ND 0.0056 0.0022 mg/kg 103-65-1 n-Propylbenzene ND 0.0056 0.0011 mg/kg 100-42-5 Styrene ND 0.0056 0.0011 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0056 0.0012 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0056 0.0011 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0056 0.0016 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0056 0.0018 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0056 0.0013 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0056 0.0021 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0056 0.0013 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0056 0.0011 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0056 0.0011 mg/kg 127-18-4 Tetrachloroethylene ND 0.0056 0.0014 mg/kg 108-88-3 Toluene ND 0.0056 0.0011 mg/kg 79-01-6 Trichloroethylene ND 0.0056 0.0011 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0056 0.0011 mg/kg 75-01-4 Vinyl chloride ND 0.0056 0.0011 mg/kg 108-05-4 Vinyl Acetate ND 0.028 0.0089 mg/kg 1330-20-7 Xylene (total)ND 0.017 0.0030 mg/kg m,p-Xylene ND 0.011 0.0018 mg/kg 95-47-6 o-Xylene ND 0.0056 0.0012 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%75-124% 2037-26-5 Toluene-D8 93%75-126% 460-00-4 4-Bromofluorobenzene 102%71-133% 17060-07-0 1,2-Dichloroethane-D4 100%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 208 FA15409 33.2 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B2 8-10 Lab Sample ID:FA15409-2 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:70.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007902.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.31 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 7.8 2.7 mg/kg C9- C12 Aliphatics (Unadj.)4.47 7.8 2.7 mg/kg J C9- C10 Aromatics (Unadj.)ND 7.8 2.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 127%70-130% 460-00-4 BFB 117%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 208 FA15409 33.2 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B3 8-10 Lab Sample ID:FA15409-3 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:77.6 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064670.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064671.D 1 06/02/14 AH n/a n/a VF2136 Run #3 F0064690.D 1 06/03/14 AH n/a n/a VF2137 Initial Weight Methanol Aliquot Run #1 5.98 g 100 ul Run #2 5.98 g 10.0 ul Run #3 5.98 g 5.0 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 3.4 1.0 mg/kg 71-43-2 Benzene 0.312 0.34 0.068 mg/kg J 108-86-1 Bromobenzene ND 0.34 0.074 mg/kg 74-97-5 Bromochloromethane ND 0.34 0.13 mg/kg 75-27-4 Bromodichloromethane ND 0.34 0.068 mg/kg 75-25-2 Bromoform ND 0.34 0.074 mg/kg 104-51-8 n-Butylbenzene 5.43 0.34 0.068 mg/kg 135-98-8 sec-Butylbenzene 2.02 0.34 0.068 mg/kg 98-06-6 tert-Butylbenzene ND 0.34 0.068 mg/kg 108-90-7 Chlorobenzene ND 0.34 0.068 mg/kg 75-00-3 Chloroethane ND 0.34 0.15 mg/kg 67-66-3 Chloroform ND 0.34 0.077 mg/kg 95-49-8 o-Chlorotoluene ND 0.34 0.068 mg/kg 106-43-4 p-Chlorotoluene ND 0.34 0.068 mg/kg 56-23-5 Carbon tetrachloride ND 0.34 0.095 mg/kg 75-34-3 1,1-Dichloroethane ND 0.34 0.068 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.34 0.068 mg/kg 563-58-6 1,1-Dichloropropene ND 0.34 0.076 mg/kg 106-93-4 1,2-Dibromoethane ND 0.34 0.12 mg/kg 107-06-2 1,2-Dichloroethane ND 0.34 0.068 mg/kg 78-87-5 1,2-Dichloropropane ND 0.34 0.068 mg/kg 142-28-9 1,3-Dichloropropane ND 0.34 0.068 mg/kg 108-20-3 Di-Isopropyl ether ND 0.34 0.070 mg/kg 594-20-7 2,2-Dichloropropane ND 0.34 0.096 mg/kg 124-48-1 Dibromochloromethane ND 0.34 0.068 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.34 0.086 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.34 0.068 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.34 0.068 mg/kg 541-73-1 m-Dichlorobenzene ND 0.34 0.068 mg/kg 95-50-1 o-Dichlorobenzene ND 0.34 0.068 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 208 FA15409 33.3 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B3 8-10 Lab Sample ID:FA15409-3 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:77.6 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 106-46-7 p-Dichlorobenzene ND 0.34 0.077 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.34 0.092 mg/kg 10061-02-6 trans-1,3-Dichloropropene ND 0.34 0.068 mg/kg 64-17-5 Ethyl alcohol ND 27 4.5 mg/kg 100-41-4 Ethylbenzene 37.5 a 3.4 0.68 mg/kg 591-78-6 2-Hexanone ND 1.7 0.33 mg/kg 98-82-8 Isopropylbenzene 4.57 0.34 0.068 mg/kg 99-87-6 p-Isopropyltoluene 1.39 0.34 0.068 mg/kg 108-10-1 4-Methyl-2-pentanone ND 1.7 0.34 mg/kg 74-83-9 Methyl bromide ND 0.34 0.13 mg/kg 74-87-3 Methyl chloride ND 0.34 0.14 mg/kg 75-09-2 Methylene chloride ND 0.68 0.27 mg/kg 78-93-3 Methyl ethyl ketone ND 1.7 0.51 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.427 0.34 0.068 mg/kg 91-20-3 Naphthalene 40.9 a 3.4 1.4 mg/kg 103-65-1 n-Propylbenzene 19.4 a 3.4 0.68 mg/kg 100-42-5 Styrene 3.95 0.34 0.068 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.34 0.072 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.34 0.068 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.34 0.096 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.34 0.11 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.34 0.082 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.34 0.13 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.34 0.079 mg/kg 95-63-6 1,2,4-Trimethylbenzene 164 b 6.8 1.4 mg/kg 108-67-8 1,3,5-Trimethylbenzene 51.6 a 3.4 0.68 mg/kg 127-18-4 Tetrachloroethylene ND 0.34 0.086 mg/kg 108-88-3 Toluene 39.4 a 3.4 0.68 mg/kg 79-01-6 Trichloroethylene ND 0.34 0.070 mg/kg 75-69-4 Trichlorofluoromethane ND 0.34 0.068 mg/kg 75-01-4 Vinyl chloride ND 0.34 0.070 mg/kg 108-05-4 Vinyl Acetate ND 1.7 0.55 mg/kg 1330-20-7 Xylene (total)257 a 10 1.8 mg/kg m,p-Xylene 173 a 6.8 1.1 mg/kg 95-47-6 o-Xylene 83.7 a 3.4 0.73 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits 1868-53-7 Dibromofluoromethane 76%85%88%75-124% 2037-26-5 Toluene-D8 96%91%93%75-126% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 208 FA15409 33.3 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B3 8-10 Lab Sample ID:FA15409-3 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:77.6 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits 460-00-4 4-Bromofluorobenzene 94%97%98%71-133% 17060-07-0 1,2-Dichloroethane-D4 87%81%86%72-135% (a) Result is from Run# 2 (b) Result is from Run# 3 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 208 FA15409 33.3 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B3 8-10 Lab Sample ID:FA15409-3 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:77.6 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007939.D 100 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.89 g 5.1 ml 20.0 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)1470 3500 1200 mg/kg J C9- C12 Aliphatics (Unadj.)2800 3500 1200 mg/kg J C9- C10 Aromatics (Unadj.)7270 3500 1200 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 0% a 70-130% 460-00-4 BFB 0% a 70-130% (a) Outside control limits due to dilution. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 208 FA15409 33.3 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B4 8-10 Lab Sample ID:FA15409-4 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064665.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064669.D 1 06/02/14 AH n/a n/a VF2136 Initial Weight Methanol Aliquot Run #1 6.76 g Run #2 6.68 g 100 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0541 0.049 0.015 mg/kg 71-43-2 Benzene ND 0.0049 0.00099 mg/kg 108-86-1 Bromobenzene ND 0.0049 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0049 0.0019 mg/kg 75-27-4 Bromodichloromethane ND 0.0049 0.00099 mg/kg 75-25-2 Bromoform ND 0.0049 0.0011 mg/kg 104-51-8 n-Butylbenzene ND 0.0049 0.00099 mg/kg 135-98-8 sec-Butylbenzene ND 0.0049 0.00099 mg/kg 98-06-6 tert-Butylbenzene ND 0.0049 0.00099 mg/kg 108-90-7 Chlorobenzene ND 0.0049 0.00099 mg/kg 75-00-3 Chloroethane ND 0.0049 0.0022 mg/kg 67-66-3 Chloroform ND 0.0049 0.0011 mg/kg 95-49-8 o-Chlorotoluene ND 0.0049 0.00099 mg/kg 106-43-4 p-Chlorotoluene ND 0.0049 0.00099 mg/kg 56-23-5 Carbon tetrachloride ND 0.0049 0.0014 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0049 0.00099 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0049 0.00099 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0049 0.0011 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0049 0.0018 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0049 0.00099 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0049 0.00099 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0049 0.00099 mg/kg 108-20-3 Di-Isopropyl ether 0.0105 0.0049 0.0010 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0049 0.0014 mg/kg 124-48-1 Dibromochloromethane ND 0.0049 0.00099 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0049 0.0012 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0049 0.00099 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0049 0.00099 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0049 0.00099 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0049 0.00099 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0049 0.0011 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0049 0.0013 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 208 FA15409 33.4 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B4 8-10 Lab Sample ID:FA15409-4 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0049 0.00099 mg/kg 64-17-5 Ethyl alcohol ND 0.40 0.066 mg/kg 100-41-4 Ethylbenzene ND 0.0049 0.00099 mg/kg 591-78-6 2-Hexanone ND 0.025 0.0048 mg/kg 98-82-8 Isopropylbenzene ND 0.0049 0.00099 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0049 0.00099 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.025 0.0049 mg/kg 74-83-9 Methyl bromide ND 0.0049 0.0018 mg/kg 74-87-3 Methyl chloride ND 0.0049 0.0020 mg/kg 75-09-2 Methylene chloride ND 0.0099 0.0040 mg/kg 78-93-3 Methyl ethyl ketone 0.0265 0.025 0.0074 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.338 a 0.33 0.067 mg/kg 91-20-3 Naphthalene 0.0022 0.0049 0.0020 mg/kg J 103-65-1 n-Propylbenzene ND 0.0049 0.00099 mg/kg 100-42-5 Styrene ND 0.0049 0.00099 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0049 0.0010 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0049 0.00099 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0049 0.0014 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0049 0.0016 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0049 0.0012 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0049 0.0018 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0049 0.0011 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0049 0.00099 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0049 0.00099 mg/kg 127-18-4 Tetrachloroethylene ND 0.0049 0.0012 mg/kg 108-88-3 Toluene ND 0.0049 0.00099 mg/kg 79-01-6 Trichloroethylene ND 0.0049 0.0010 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0049 0.00099 mg/kg 75-01-4 Vinyl chloride ND 0.0049 0.0010 mg/kg 108-05-4 Vinyl Acetate ND 0.025 0.0079 mg/kg 1330-20-7 Xylene (total)ND 0.015 0.0026 mg/kg m,p-Xylene ND 0.0099 0.0016 mg/kg 95-47-6 o-Xylene ND 0.0049 0.0011 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 89%84%75-124% 2037-26-5 Toluene-D8 93%92%75-126% 460-00-4 4-Bromofluorobenzene 101%104%71-133% 17060-07-0 1,2-Dichloroethane-D4 95%83%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 208 FA15409 33.4 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B4 8-10 Lab Sample ID:FA15409-4 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 208 FA15409 33.4 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B4 8-10 Lab Sample ID:FA15409-4 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007906.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.57 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg C9- C12 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg C9- C10 Aromatics (Unadj.)ND 6.9 2.4 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 120%70-130% 460-00-4 BFB 110%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 208 FA15409 33.4 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B5 8-10 Lab Sample ID:FA15409-5 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064702.D 1 06/04/14 AH n/a n/a VF2138 Run #2 Initial Weight Run #1 6.35 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0230 0.053 0.016 mg/kg J 71-43-2 Benzene ND 0.0053 0.0011 mg/kg 108-86-1 Bromobenzene ND 0.0053 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0053 0.0020 mg/kg 75-27-4 Bromodichloromethane ND 0.0053 0.0011 mg/kg 75-25-2 Bromoform ND 0.0053 0.0011 mg/kg 104-51-8 n-Butylbenzene ND 0.0053 0.0011 mg/kg 135-98-8 sec-Butylbenzene ND 0.0053 0.0011 mg/kg 98-06-6 tert-Butylbenzene ND 0.0053 0.0011 mg/kg 108-90-7 Chlorobenzene ND 0.0053 0.0011 mg/kg 75-00-3 Chloroethane ND 0.0053 0.0024 mg/kg 67-66-3 Chloroform ND 0.0053 0.0012 mg/kg 95-49-8 o-Chlorotoluene ND 0.0053 0.0011 mg/kg 106-43-4 p-Chlorotoluene ND 0.0053 0.0011 mg/kg 56-23-5 Carbon tetrachloride ND 0.0053 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0053 0.0011 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0053 0.0011 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0053 0.0012 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0053 0.0019 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0053 0.0011 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0053 0.0011 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0053 0.0011 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0053 0.0011 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0053 0.0015 mg/kg 124-48-1 Dibromochloromethane ND 0.0053 0.0011 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0053 0.0013 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0053 0.0011 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0053 0.0011 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0053 0.0011 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0053 0.0012 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0053 0.0014 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 31 of 208 FA15409 33.5 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B5 8-10 Lab Sample ID:FA15409-5 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg 64-17-5 Ethyl alcohol ND 0.42 0.070 mg/kg 100-41-4 Ethylbenzene ND 0.0053 0.0011 mg/kg 591-78-6 2-Hexanone ND 0.026 0.0052 mg/kg 98-82-8 Isopropylbenzene ND 0.0053 0.0011 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0053 0.0011 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.026 0.0053 mg/kg 74-83-9 Methyl bromide ND 0.0053 0.0020 mg/kg 74-87-3 Methyl chloride ND 0.0053 0.0021 mg/kg 75-09-2 Methylene chloride ND 0.011 0.0042 mg/kg 78-93-3 Methyl ethyl ketone ND 0.026 0.0079 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0053 0.0011 mg/kg 91-20-3 Naphthalene ND 0.0053 0.0021 mg/kg 103-65-1 n-Propylbenzene ND 0.0053 0.0011 mg/kg 100-42-5 Styrene ND 0.0053 0.0011 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0053 0.0011 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0053 0.0011 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0053 0.0015 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0053 0.0017 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0053 0.0013 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0053 0.0020 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0053 0.0012 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0053 0.0011 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0053 0.0011 mg/kg 127-18-4 Tetrachloroethylene ND 0.0053 0.0013 mg/kg 108-88-3 Toluene ND 0.0053 0.0011 mg/kg 79-01-6 Trichloroethylene ND 0.0053 0.0011 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0053 0.0011 mg/kg 75-01-4 Vinyl chloride ND 0.0053 0.0011 mg/kg 108-05-4 Vinyl Acetate ND 0.026 0.0084 mg/kg 1330-20-7 Xylene (total)ND 0.016 0.0028 mg/kg m,p-Xylene ND 0.011 0.0017 mg/kg 95-47-6 o-Xylene ND 0.0053 0.0011 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 94%75-124% 2037-26-5 Toluene-D8 91%75-126% 460-00-4 4-Bromofluorobenzene 103%71-133% 17060-07-0 1,2-Dichloroethane-D4 97%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 32 of 208 FA15409 33.5 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B5 8-10 Lab Sample ID:FA15409-5 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007907.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.88 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 7.5 2.6 mg/kg C9- C12 Aliphatics (Unadj.)ND 7.5 2.6 mg/kg C9- C10 Aromatics (Unadj.)ND 7.5 2.6 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 99%70-130% 460-00-4 BFB 91%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 33 of 208 FA15409 33.5 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B6 8-10 Lab Sample ID:FA15409-6 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 C098558.D 1 05/30/14 AH n/a n/a VC3954 Run #2 Initial Weight Run #1 6.16 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0418 0.055 0.016 mg/kg J 71-43-2 Benzene ND 0.0055 0.0011 mg/kg 108-86-1 Bromobenzene ND 0.0055 0.0012 mg/kg 74-97-5 Bromochloromethane ND 0.0055 0.0021 mg/kg 75-27-4 Bromodichloromethane ND 0.0055 0.0011 mg/kg 75-25-2 Bromoform ND 0.0055 0.0012 mg/kg 104-51-8 n-Butylbenzene ND 0.0055 0.0011 mg/kg 135-98-8 sec-Butylbenzene ND 0.0055 0.0011 mg/kg 98-06-6 tert-Butylbenzene ND 0.0055 0.0011 mg/kg 108-90-7 Chlorobenzene ND 0.0055 0.0011 mg/kg 75-00-3 Chloroethane ND 0.0055 0.0025 mg/kg 67-66-3 Chloroform ND 0.0055 0.0012 mg/kg 95-49-8 o-Chlorotoluene ND 0.0055 0.0011 mg/kg 106-43-4 p-Chlorotoluene ND 0.0055 0.0011 mg/kg 56-23-5 Carbon tetrachloride ND 0.0055 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0055 0.0011 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0055 0.0011 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0055 0.0012 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0055 0.0020 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0055 0.0011 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0055 0.0011 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0055 0.0011 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0055 0.0011 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0055 0.0015 mg/kg 124-48-1 Dibromochloromethane ND 0.0055 0.0011 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0055 0.0014 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0055 0.0011 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0055 0.0011 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0055 0.0011 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0055 0.0012 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0055 0.0015 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 34 of 208 FA15409 33.6 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B6 8-10 Lab Sample ID:FA15409-6 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.3 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg 64-17-5 Ethyl alcohol ND 0.44 0.073 mg/kg 100-41-4 Ethylbenzene ND 0.0055 0.0011 mg/kg 591-78-6 2-Hexanone ND 0.027 0.0054 mg/kg 98-82-8 Isopropylbenzene ND 0.0055 0.0011 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0055 0.0011 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.027 0.0055 mg/kg 74-83-9 Methyl bromide ND 0.0055 0.0020 mg/kg 74-87-3 Methyl chloride ND 0.0055 0.0022 mg/kg 75-09-2 Methylene chloride ND 0.011 0.0044 mg/kg 78-93-3 Methyl ethyl ketone ND 0.027 0.0082 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0055 0.0011 mg/kg 91-20-3 Naphthalene ND 0.0055 0.0022 mg/kg 103-65-1 n-Propylbenzene ND 0.0055 0.0011 mg/kg 100-42-5 Styrene ND 0.0055 0.0011 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0055 0.0011 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0055 0.0011 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0055 0.0015 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0055 0.0018 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0055 0.0013 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0055 0.0020 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0055 0.0013 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0055 0.0011 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0055 0.0011 mg/kg 127-18-4 Tetrachloroethylene ND 0.0055 0.0014 mg/kg 108-88-3 Toluene ND 0.0055 0.0011 mg/kg 79-01-6 Trichloroethylene ND 0.0055 0.0011 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0055 0.0011 mg/kg 75-01-4 Vinyl chloride ND 0.0055 0.0011 mg/kg 108-05-4 Vinyl Acetate ND 0.027 0.0088 mg/kg 1330-20-7 Xylene (total)ND 0.016 0.0029 mg/kg m,p-Xylene ND 0.011 0.0017 mg/kg 95-47-6 o-Xylene ND 0.0055 0.0012 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 119%75-124% 2037-26-5 Toluene-D8 98%75-126% 460-00-4 4-Bromofluorobenzene 95%71-133% 17060-07-0 1,2-Dichloroethane-D4 129%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 35 of 208 FA15409 33.6 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B6 8-10 Lab Sample ID:FA15409-6 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:74.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007908.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.73 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 7.7 2.7 mg/kg C9- C12 Aliphatics (Unadj.)ND 7.7 2.7 mg/kg C9- C10 Aromatics (Unadj.)ND 7.7 2.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 108%70-130% 460-00-4 BFB 100%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 36 of 208 FA15409 33.6 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B7 8-10 Lab Sample ID:FA15409-7 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:72.7 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 C098559.D 1 05/30/14 AH n/a n/a VC3954 Run #2 Initial Weight Run #1 6.72 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0559 0.051 0.015 mg/kg 71-43-2 Benzene ND 0.0051 0.0010 mg/kg 108-86-1 Bromobenzene ND 0.0051 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0051 0.0020 mg/kg 75-27-4 Bromodichloromethane ND 0.0051 0.0010 mg/kg 75-25-2 Bromoform ND 0.0051 0.0011 mg/kg 104-51-8 n-Butylbenzene ND 0.0051 0.0010 mg/kg 135-98-8 sec-Butylbenzene ND 0.0051 0.0010 mg/kg 98-06-6 tert-Butylbenzene ND 0.0051 0.0010 mg/kg 108-90-7 Chlorobenzene ND 0.0051 0.0010 mg/kg 75-00-3 Chloroethane ND 0.0051 0.0023 mg/kg 67-66-3 Chloroform ND 0.0051 0.0012 mg/kg 95-49-8 o-Chlorotoluene ND 0.0051 0.0010 mg/kg 106-43-4 p-Chlorotoluene ND 0.0051 0.0010 mg/kg 56-23-5 Carbon tetrachloride ND 0.0051 0.0014 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0051 0.0010 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0051 0.0010 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0051 0.0011 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0051 0.0018 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0051 0.0010 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0051 0.0010 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0051 0.0010 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0051 0.0011 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0051 0.0014 mg/kg 124-48-1 Dibromochloromethane ND 0.0051 0.0010 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0051 0.0013 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0051 0.0010 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0051 0.0010 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0051 0.0010 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0051 0.0011 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0051 0.0014 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 37 of 208 FA15409 33.7 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B7 8-10 Lab Sample ID:FA15409-7 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:72.7 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg 64-17-5 Ethyl alcohol ND 0.41 0.068 mg/kg 100-41-4 Ethylbenzene ND 0.0051 0.0010 mg/kg 591-78-6 2-Hexanone ND 0.026 0.0050 mg/kg 98-82-8 Isopropylbenzene ND 0.0051 0.0010 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0051 0.0010 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.026 0.0051 mg/kg 74-83-9 Methyl bromide ND 0.0051 0.0019 mg/kg 74-87-3 Methyl chloride ND 0.0051 0.0020 mg/kg 75-09-2 Methylene chloride ND 0.010 0.0041 mg/kg 78-93-3 Methyl ethyl ketone ND 0.026 0.0077 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0051 0.0010 mg/kg 91-20-3 Naphthalene ND 0.0051 0.0020 mg/kg 103-65-1 n-Propylbenzene ND 0.0051 0.0010 mg/kg 100-42-5 Styrene ND 0.0051 0.0010 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0051 0.0011 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0051 0.0010 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0051 0.0014 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0051 0.0016 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0051 0.0012 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0051 0.0019 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0051 0.0012 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0051 0.0010 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0051 0.0010 mg/kg 127-18-4 Tetrachloroethylene ND 0.0051 0.0013 mg/kg 108-88-3 Toluene ND 0.0051 0.0010 mg/kg 79-01-6 Trichloroethylene ND 0.0051 0.0010 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0051 0.0010 mg/kg 75-01-4 Vinyl chloride ND 0.0051 0.0010 mg/kg 108-05-4 Vinyl Acetate ND 0.026 0.0082 mg/kg 1330-20-7 Xylene (total)ND 0.015 0.0027 mg/kg m,p-Xylene ND 0.010 0.0016 mg/kg 95-47-6 o-Xylene ND 0.0051 0.0011 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 116%75-124% 2037-26-5 Toluene-D8 96%75-126% 460-00-4 4-Bromofluorobenzene 90%71-133% 17060-07-0 1,2-Dichloroethane-D4 121%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 38 of 208 FA15409 33.7 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B7 8-10 Lab Sample ID:FA15409-7 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:72.7 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007909.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.30 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 7.4 2.6 mg/kg C9- C12 Aliphatics (Unadj.)ND 7.4 2.6 mg/kg C9- C10 Aromatics (Unadj.)ND 7.4 2.6 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 121%70-130% 460-00-4 BFB 112%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 39 of 208 FA15409 33.7 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B8 13-15 Lab Sample ID:FA15409-8 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:72.6 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064672.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064673.D 1 06/02/14 AH n/a n/a VF2136 Initial Weight Methanol Aliquot Run #1 3.98 g 100 ul Run #2 3.98 g 10.0 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 5.3 1.6 mg/kg 71-43-2 Benzene ND 0.53 0.11 mg/kg 108-86-1 Bromobenzene ND 0.53 0.11 mg/kg 74-97-5 Bromochloromethane ND 0.53 0.20 mg/kg 75-27-4 Bromodichloromethane ND 0.53 0.11 mg/kg 75-25-2 Bromoform ND 0.53 0.11 mg/kg 104-51-8 n-Butylbenzene 6.64 0.53 0.11 mg/kg 135-98-8 sec-Butylbenzene 3.43 0.53 0.11 mg/kg 98-06-6 tert-Butylbenzene 0.293 0.53 0.11 mg/kg J 108-90-7 Chlorobenzene ND 0.53 0.11 mg/kg 75-00-3 Chloroethane ND 0.53 0.24 mg/kg 67-66-3 Chloroform ND 0.53 0.12 mg/kg 95-49-8 o-Chlorotoluene ND 0.53 0.11 mg/kg 106-43-4 p-Chlorotoluene ND 0.53 0.11 mg/kg 56-23-5 Carbon tetrachloride ND 0.53 0.15 mg/kg 75-34-3 1,1-Dichloroethane ND 0.53 0.11 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.53 0.11 mg/kg 563-58-6 1,1-Dichloropropene ND 0.53 0.12 mg/kg 106-93-4 1,2-Dibromoethane ND 0.53 0.19 mg/kg 107-06-2 1,2-Dichloroethane ND 0.53 0.11 mg/kg 78-87-5 1,2-Dichloropropane ND 0.53 0.11 mg/kg 142-28-9 1,3-Dichloropropane ND 0.53 0.11 mg/kg 108-20-3 Di-Isopropyl ether ND 0.53 0.11 mg/kg 594-20-7 2,2-Dichloropropane ND 0.53 0.15 mg/kg 124-48-1 Dibromochloromethane ND 0.53 0.11 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.53 0.13 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.53 0.11 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.53 0.11 mg/kg 541-73-1 m-Dichlorobenzene ND 0.53 0.11 mg/kg 95-50-1 o-Dichlorobenzene ND 0.53 0.11 mg/kg 106-46-7 p-Dichlorobenzene ND 0.53 0.12 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.53 0.14 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 40 of 208 FA15409 33.8 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B8 13-15 Lab Sample ID:FA15409-8 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:72.6 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.53 0.11 mg/kg 64-17-5 Ethyl alcohol ND 42 7.0 mg/kg 100-41-4 Ethylbenzene 0.237 0.53 0.11 mg/kg J 591-78-6 2-Hexanone ND 2.6 0.52 mg/kg 98-82-8 Isopropylbenzene 4.55 0.53 0.11 mg/kg 99-87-6 p-Isopropyltoluene 3.25 0.53 0.11 mg/kg 108-10-1 4-Methyl-2-pentanone ND 2.6 0.53 mg/kg 74-83-9 Methyl bromide ND 0.53 0.20 mg/kg 74-87-3 Methyl chloride ND 0.53 0.21 mg/kg 75-09-2 Methylene chloride ND 1.1 0.42 mg/kg 78-93-3 Methyl ethyl ketone ND 2.6 0.79 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.53 0.11 mg/kg 91-20-3 Naphthalene 0.841 0.53 0.21 mg/kg 103-65-1 n-Propylbenzene 17.3 0.53 0.11 mg/kg 100-42-5 Styrene ND 0.53 0.11 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.53 0.11 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.53 0.11 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.53 0.15 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.53 0.17 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.53 0.13 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.53 0.20 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.53 0.12 mg/kg 95-63-6 1,2,4-Trimethylbenzene 49.6 a 5.3 1.1 mg/kg 108-67-8 1,3,5-Trimethylbenzene 17.5 0.53 0.11 mg/kg 127-18-4 Tetrachloroethylene ND 0.53 0.13 mg/kg 108-88-3 Toluene ND 0.53 0.11 mg/kg 79-01-6 Trichloroethylene ND 0.53 0.11 mg/kg 75-69-4 Trichlorofluoromethane ND 0.53 0.11 mg/kg 75-01-4 Vinyl chloride ND 0.53 0.11 mg/kg 108-05-4 Vinyl Acetate ND 2.6 0.85 mg/kg 1330-20-7 Xylene (total)ND 1.6 0.28 mg/kg m,p-Xylene 0.194 1.1 0.17 mg/kg J 95-47-6 o-Xylene ND 0.53 0.11 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 79%86%75-124% 2037-26-5 Toluene-D8 95%93%75-126% 460-00-4 4-Bromofluorobenzene 97%97%71-133% 17060-07-0 1,2-Dichloroethane-D4 94%84%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 41 of 208 FA15409 33.8 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B8 13-15 Lab Sample ID:FA15409-8 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:72.6 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 42 of 208 FA15409 33.8 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B8 13-15 Lab Sample ID:FA15409-8 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:72.6 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007932.D 10 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.37 g 5.1 ml 20.0 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)1110 370 130 mg/kg C9- C12 Aliphatics (Unadj.)311 370 130 mg/kg J C9- C10 Aromatics (Unadj.)903 370 130 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 0% a 70-130% 460-00-4 BFB 0% a 70-130% (a) Outside control limits due to dilution. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 43 of 208 FA15409 33.8 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B9 13-14 Lab Sample ID:FA15409-9 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.1 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064663.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064691.D 1 06/03/14 AH n/a n/a VF2137 Initial Weight Methanol Aliquot Run #1 6.14 g Run #2 6.11 g 100 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 0.055 0.016 mg/kg 71-43-2 Benzene 0.0879 0.0055 0.0011 mg/kg 108-86-1 Bromobenzene ND 0.0055 0.0012 mg/kg 74-97-5 Bromochloromethane ND 0.0055 0.0021 mg/kg 75-27-4 Bromodichloromethane ND 0.0055 0.0011 mg/kg 75-25-2 Bromoform ND 0.0055 0.0012 mg/kg 104-51-8 n-Butylbenzene 0.0601 0.0055 0.0011 mg/kg 135-98-8 sec-Butylbenzene 0.0200 0.0055 0.0011 mg/kg 98-06-6 tert-Butylbenzene ND 0.0055 0.0011 mg/kg 108-90-7 Chlorobenzene ND 0.0055 0.0011 mg/kg 75-00-3 Chloroethane ND 0.0055 0.0025 mg/kg 67-66-3 Chloroform ND 0.0055 0.0012 mg/kg 95-49-8 o-Chlorotoluene ND 0.0055 0.0011 mg/kg 106-43-4 p-Chlorotoluene ND 0.0055 0.0011 mg/kg 56-23-5 Carbon tetrachloride ND 0.0055 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0055 0.0011 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0055 0.0011 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0055 0.0012 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0055 0.0020 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0055 0.0011 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0055 0.0011 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0055 0.0011 mg/kg 108-20-3 Di-Isopropyl ether 0.0065 0.0055 0.0011 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0055 0.0015 mg/kg 124-48-1 Dibromochloromethane ND 0.0055 0.0011 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0055 0.0014 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0055 0.0011 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0055 0.0011 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0055 0.0011 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0055 0.0012 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0055 0.0015 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 44 of 208 FA15409 33.9 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B9 13-14 Lab Sample ID:FA15409-9 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.1 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg 64-17-5 Ethyl alcohol ND 0.44 0.073 mg/kg 100-41-4 Ethylbenzene 2.72 a 0.36 0.073 mg/kg 591-78-6 2-Hexanone ND 0.027 0.0054 mg/kg 98-82-8 Isopropylbenzene 0.0545 0.0055 0.0011 mg/kg 99-87-6 p-Isopropyltoluene 0.0149 0.0055 0.0011 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.027 0.0055 mg/kg 74-83-9 Methyl bromide ND 0.0055 0.0021 mg/kg 74-87-3 Methyl chloride ND 0.0055 0.0022 mg/kg 75-09-2 Methylene chloride ND 0.011 0.0044 mg/kg 78-93-3 Methyl ethyl ketone ND 0.027 0.0082 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.0629 0.0055 0.0011 mg/kg 91-20-3 Naphthalene 1.68 a 0.36 0.15 mg/kg 103-65-1 n-Propylbenzene 0.153 0.0055 0.0011 mg/kg 100-42-5 Styrene 0.0432 0.0055 0.0011 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0055 0.0012 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0055 0.0011 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0055 0.0015 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0055 0.0018 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0055 0.0013 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0055 0.0021 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0055 0.0013 mg/kg 95-63-6 1,2,4-Trimethylbenzene 6.51 a 0.36 0.073 mg/kg 108-67-8 1,3,5-Trimethylbenzene 1.90 a 0.36 0.073 mg/kg 127-18-4 Tetrachloroethylene ND 0.0055 0.0014 mg/kg 108-88-3 Toluene 13.1 a 0.36 0.073 mg/kg 79-01-6 Trichloroethylene ND 0.0055 0.0011 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0055 0.0011 mg/kg 75-01-4 Vinyl chloride ND 0.0055 0.0011 mg/kg 108-05-4 Vinyl Acetate ND 0.027 0.0088 mg/kg 1330-20-7 Xylene (total)16.4 a 1.1 0.19 mg/kg m,p-Xylene 11.0 a 0.73 0.12 mg/kg 95-47-6 o-Xylene 5.38 a 0.36 0.078 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 84%85%75-124% 2037-26-5 Toluene-D8 89%89%75-126% 460-00-4 4-Bromofluorobenzene 92%97%71-133% 17060-07-0 1,2-Dichloroethane-D4 102%85%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 45 of 208 FA15409 33.9 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B9 13-14 Lab Sample ID:FA15409-9 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:74.1 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 46 of 208 FA15409 33.9 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B9 13-14 Lab Sample ID:FA15409-9 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:74.1 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007933.D 1 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.96 g 5.1 ml 25.0 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)24.2 30 11 mg/kg J C9- C12 Aliphatics (Unadj.)26.6 30 11 mg/kg J C9- C10 Aromatics (Unadj.)66.7 30 11 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 99%70-130% 460-00-4 BFB 92%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 47 of 208 FA15409 33.9 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B10 8-10 Lab Sample ID:FA15409-10 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:73.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064674.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064675.D 1 06/02/14 AH n/a n/a VF2136 Initial Weight Methanol Aliquot Run #1 6.31 g 100 ul Run #2 6.31 g 10.0 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 3.6 1.1 mg/kg 71-43-2 Benzene 1.04 0.36 0.073 mg/kg 108-86-1 Bromobenzene ND 0.36 0.079 mg/kg 74-97-5 Bromochloromethane ND 0.36 0.14 mg/kg 75-27-4 Bromodichloromethane ND 0.36 0.073 mg/kg 75-25-2 Bromoform ND 0.36 0.079 mg/kg 104-51-8 n-Butylbenzene 1.26 0.36 0.073 mg/kg 135-98-8 sec-Butylbenzene 0.412 0.36 0.073 mg/kg 98-06-6 tert-Butylbenzene ND 0.36 0.073 mg/kg 108-90-7 Chlorobenzene ND 0.36 0.073 mg/kg 75-00-3 Chloroethane ND 0.36 0.16 mg/kg 67-66-3 Chloroform ND 0.36 0.082 mg/kg 95-49-8 o-Chlorotoluene ND 0.36 0.073 mg/kg 106-43-4 p-Chlorotoluene ND 0.36 0.073 mg/kg 56-23-5 Carbon tetrachloride ND 0.36 0.10 mg/kg 75-34-3 1,1-Dichloroethane ND 0.36 0.073 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.36 0.073 mg/kg 563-58-6 1,1-Dichloropropene ND 0.36 0.081 mg/kg 106-93-4 1,2-Dibromoethane ND 0.36 0.13 mg/kg 107-06-2 1,2-Dichloroethane ND 0.36 0.073 mg/kg 78-87-5 1,2-Dichloropropane ND 0.36 0.073 mg/kg 142-28-9 1,3-Dichloropropane ND 0.36 0.073 mg/kg 108-20-3 Di-Isopropyl ether 0.149 0.36 0.075 mg/kg J 594-20-7 2,2-Dichloropropane ND 0.36 0.10 mg/kg 124-48-1 Dibromochloromethane ND 0.36 0.073 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.36 0.092 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.36 0.073 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.36 0.073 mg/kg 541-73-1 m-Dichlorobenzene ND 0.36 0.073 mg/kg 95-50-1 o-Dichlorobenzene ND 0.36 0.073 mg/kg 106-46-7 p-Dichlorobenzene ND 0.36 0.081 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.36 0.098 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 48 of 208 FA15409 33.10 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B10 8-10 Lab Sample ID:FA15409-10 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:73.0 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.36 0.073 mg/kg 64-17-5 Ethyl alcohol ND 29 4.8 mg/kg 100-41-4 Ethylbenzene 6.46 0.36 0.073 mg/kg 591-78-6 2-Hexanone ND 1.8 0.36 mg/kg 98-82-8 Isopropylbenzene 0.956 0.36 0.073 mg/kg 99-87-6 p-Isopropyltoluene 0.300 0.36 0.073 mg/kg J 108-10-1 4-Methyl-2-pentanone ND 1.8 0.36 mg/kg 74-83-9 Methyl bromide ND 0.36 0.14 mg/kg 74-87-3 Methyl chloride ND 0.36 0.15 mg/kg 75-09-2 Methylene chloride ND 0.73 0.29 mg/kg 78-93-3 Methyl ethyl ketone ND 1.8 0.55 mg/kg 1634-04-4 Methyl Tert Butyl Ether 2.01 0.36 0.073 mg/kg 91-20-3 Naphthalene 6.25 0.36 0.15 mg/kg 103-65-1 n-Propylbenzene 3.31 0.36 0.073 mg/kg 100-42-5 Styrene 0.210 0.36 0.073 mg/kg J 630-20-6 1,1,1,2-Tetrachloroethane ND 0.36 0.076 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.36 0.073 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.36 0.10 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.36 0.12 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.36 0.087 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.36 0.14 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.36 0.084 mg/kg 95-63-6 1,2,4-Trimethylbenzene 24.8 a 3.6 0.73 mg/kg 108-67-8 1,3,5-Trimethylbenzene 6.48 0.36 0.073 mg/kg 127-18-4 Tetrachloroethylene ND 0.36 0.092 mg/kg 108-88-3 Toluene 3.77 0.36 0.073 mg/kg 79-01-6 Trichloroethylene ND 0.36 0.074 mg/kg 75-69-4 Trichlorofluoromethane ND 0.36 0.073 mg/kg 75-01-4 Vinyl chloride ND 0.36 0.074 mg/kg 108-05-4 Vinyl Acetate ND 1.8 0.58 mg/kg 1330-20-7 Xylene (total)21.1 1.1 0.19 mg/kg m,p-Xylene 13.3 0.73 0.12 mg/kg 95-47-6 o-Xylene 7.80 0.36 0.078 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 86%87%75-124% 2037-26-5 Toluene-D8 91%89%75-126% 460-00-4 4-Bromofluorobenzene 96%97%71-133% 17060-07-0 1,2-Dichloroethane-D4 83%84%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 49 of 208 FA15409 33.10 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B10 8-10 Lab Sample ID:FA15409-10 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:73.0 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 50 of 208 FA15409 33.10 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B10 8-10 Lab Sample ID:FA15409-10 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:73.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007942.D 1 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.81 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)12.1 7.9 2.8 mg/kg C9- C12 Aliphatics (Unadj.)10.3 7.9 2.8 mg/kg C9- C10 Aromatics (Unadj.)17.7 7.9 2.8 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 109%70-130% 460-00-4 BFB 98%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 51 of 208 FA15409 33.10 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064676.D 1 06/02/14 AH n/a n/a VF2136 Run #2 F0064677.D 1 06/02/14 AH n/a n/a VF2136 Initial Weight Methanol Aliquot Run #1 6.26 g 100 ul Run #2 6.26 g 10.0 ul VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 3.2 0.95 mg/kg 71-43-2 Benzene 0.777 0.32 0.063 mg/kg 108-86-1 Bromobenzene ND 0.32 0.069 mg/kg 74-97-5 Bromochloromethane ND 0.32 0.12 mg/kg 75-27-4 Bromodichloromethane ND 0.32 0.063 mg/kg 75-25-2 Bromoform ND 0.32 0.068 mg/kg 104-51-8 n-Butylbenzene 6.80 0.32 0.063 mg/kg 135-98-8 sec-Butylbenzene 2.18 0.32 0.063 mg/kg 98-06-6 tert-Butylbenzene 0.106 0.32 0.063 mg/kg J 108-90-7 Chlorobenzene ND 0.32 0.063 mg/kg 75-00-3 Chloroethane ND 0.32 0.14 mg/kg 67-66-3 Chloroform ND 0.32 0.072 mg/kg 95-49-8 o-Chlorotoluene ND 0.32 0.063 mg/kg 106-43-4 p-Chlorotoluene ND 0.32 0.063 mg/kg 56-23-5 Carbon tetrachloride ND 0.32 0.088 mg/kg 75-34-3 1,1-Dichloroethane ND 0.32 0.063 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.32 0.063 mg/kg 563-58-6 1,1-Dichloropropene ND 0.32 0.070 mg/kg 106-93-4 1,2-Dibromoethane ND 0.32 0.11 mg/kg 107-06-2 1,2-Dichloroethane ND 0.32 0.063 mg/kg 78-87-5 1,2-Dichloropropane ND 0.32 0.063 mg/kg 142-28-9 1,3-Dichloropropane ND 0.32 0.063 mg/kg 108-20-3 Di-Isopropyl ether ND 0.32 0.065 mg/kg 594-20-7 2,2-Dichloropropane ND 0.32 0.089 mg/kg 124-48-1 Dibromochloromethane ND 0.32 0.063 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.32 0.080 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.32 0.063 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.32 0.063 mg/kg 541-73-1 m-Dichlorobenzene ND 0.32 0.063 mg/kg 95-50-1 o-Dichlorobenzene ND 0.32 0.063 mg/kg 106-46-7 p-Dichlorobenzene ND 0.32 0.071 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.32 0.085 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 52 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.32 0.063 mg/kg 64-17-5 Ethyl alcohol ND 25 4.2 mg/kg 100-41-4 Ethylbenzene 26.2 a 3.2 0.63 mg/kg 591-78-6 2-Hexanone ND 1.6 0.31 mg/kg 98-82-8 Isopropylbenzene 4.86 0.32 0.063 mg/kg 99-87-6 p-Isopropyltoluene 1.52 0.32 0.063 mg/kg 108-10-1 4-Methyl-2-pentanone ND 1.6 0.32 mg/kg 74-83-9 Methyl bromide ND 0.32 0.12 mg/kg 74-87-3 Methyl chloride ND 0.32 0.13 mg/kg 75-09-2 Methylene chloride ND 0.63 0.25 mg/kg 78-93-3 Methyl ethyl ketone ND 1.6 0.47 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.864 0.32 0.063 mg/kg 91-20-3 Naphthalene 43.6 a 3.2 1.3 mg/kg 103-65-1 n-Propylbenzene 19.6 a 3.2 0.63 mg/kg 100-42-5 Styrene 0.818 0.32 0.063 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.32 0.067 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.32 0.063 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.32 0.089 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.32 0.10 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.32 0.076 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.32 0.12 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.32 0.073 mg/kg 95-63-6 1,2,4-Trimethylbenzene 122 a 3.2 0.63 mg/kg 108-67-8 1,3,5-Trimethylbenzene 40.7 a 3.2 0.63 mg/kg 127-18-4 Tetrachloroethylene ND 0.32 0.080 mg/kg 108-88-3 Toluene 7.99 0.32 0.063 mg/kg 79-01-6 Trichloroethylene ND 0.32 0.065 mg/kg 75-69-4 Trichlorofluoromethane ND 0.32 0.063 mg/kg 75-01-4 Vinyl chloride ND 0.32 0.065 mg/kg 108-05-4 Vinyl Acetate ND 1.6 0.51 mg/kg 1330-20-7 Xylene (total)130 a 9.5 1.7 mg/kg m,p-Xylene 90.4 a 6.3 1.0 mg/kg 95-47-6 o-Xylene 39.6 a 3.2 0.68 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 84%84%75-124% 2037-26-5 Toluene-D8 92%95%75-126% 460-00-4 4-Bromofluorobenzene 93%97%71-133% 17060-07-0 1,2-Dichloroethane-D4 86%79%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 53 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 54 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X035133.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 Run #2 X035163.D 8 06/06/14 MV 06/03/14 OP51829 SX1646 Initial Weight Final Volume Run #1 30.1 g 1.0 ml Run #2 30.1 g 1.0 ml ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.0 0.21 mg/kg 95-57-8 2-Chlorophenol ND 0.21 0.021 mg/kg 59-50-7 4-Chloro-3-methyl phenol ND 0.21 0.021 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.21 0.022 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.21 0.023 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.0 0.21 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.42 0.084 mg/kg 95-48-7 2-Methylphenol ND 0.21 0.021 mg/kg 3&4-Methylphenol ND 0.21 0.042 mg/kg 88-75-5 2-Nitrophenol ND 0.21 0.021 mg/kg 100-02-7 4-Nitrophenol ND 1.0 0.17 mg/kg 87-86-5 Pentachlorophenol ND 1.0 0.17 mg/kg 108-95-2 Phenol ND 0.21 0.021 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.21 0.021 mg/kg 83-32-9 Acenaphthene 0.0333 0.21 0.026 mg/kg J 208-96-8 Acenaphthylene 0.0391 0.21 0.021 mg/kg J 120-12-7 Anthracene 0.107 0.21 0.021 mg/kg J 56-55-3 Benzo(a)anthracene 0.174 0.21 0.021 mg/kg J 50-32-8 Benzo(a)pyrene 0.121 0.21 0.021 mg/kg J 205-99-2 Benzo(b)fluoranthene 0.113 0.21 0.021 mg/kg J 191-24-2 Benzo(g,h,i)perylene 0.0686 0.21 0.021 mg/kg J 207-08-9 Benzo(k)fluoranthene 0.119 0.21 0.023 mg/kg J 101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.021 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.21 0.042 mg/kg 100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg 91-58-7 2-Chloronaphthalene ND 0.21 0.025 mg/kg 106-47-8 4-Chloroaniline ND 0.21 0.021 mg/kg 218-01-9 Chrysene 0.171 0.21 0.021 mg/kg J 111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.021 mg/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 0.21 0.022 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.031 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 55 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.21 0.024 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.21 0.021 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.21 0.021 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.021 mg/kg 53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.021 mg/kg 132-64-9 Dibenzofuran 0.0329 0.21 0.021 mg/kg J 84-74-2 Di-n-butyl phthalate ND 0.42 0.042 mg/kg 117-84-0 Di-n-octyl phthalate ND 0.21 0.042 mg/kg 84-66-2 Diethyl phthalate ND 0.42 0.042 mg/kg 131-11-3 Dimethyl phthalate ND 0.21 0.042 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.42 0.042 mg/kg 206-44-0 Fluoranthene 0.438 0.21 0.021 mg/kg 86-73-7 Fluorene 0.0840 0.21 0.021 mg/kg J 118-74-1 Hexachlorobenzene ND 0.21 0.021 mg/kg 87-68-3 Hexachlorobutadiene ND 0.21 0.021 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.21 0.021 mg/kg 67-72-1 Hexachloroethane ND 0.21 0.021 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.0740 0.21 0.021 mg/kg J 78-59-1 Isophorone ND 0.21 0.021 mg/kg 90-12-0 1-Methylnaphthalene 7.16 a 1.7 0.17 mg/kg 91-57-6 2-Methylnaphthalene 16.6 a 1.7 0.17 mg/kg 91-20-3 Naphthalene 19.4 a 1.7 0.17 mg/kg 98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg 621-64-7 N-Nitroso-di-n-propylamine ND 0.21 0.021 mg/kg 86-30-6 N-Nitrosodiphenylamine ND 0.21 0.021 mg/kg 85-01-8 Phenanthrene 0.402 0.21 0.021 mg/kg 129-00-0 Pyrene 0.390 0.21 0.021 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.021 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 70%70%40-102% 4165-62-2 Phenol-d5 79%78%41-100% 118-79-6 2,4,6-Tribromophenol 92%86%42-108% 4165-60-0 Nitrobenzene-d5 92%83%40-105% 321-60-8 2-Fluorobiphenyl 84%84%43-107% 1718-51-0 Terphenyl-d14 90%90%45-119% (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 56 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007935.D 10 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.04 g 5.1 ml 10.0 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)342 660 230 mg/kg J C9- C12 Aliphatics (Unadj.)556 660 230 mg/kg J C9- C10 Aromatics (Unadj.)1380 660 230 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 0% a 70-130% 460-00-4 BFB 0% a 70-130% (a) Outside control limits due to dilution. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 57 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B11 8-10 Lab Sample ID:FA15409-11 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:79.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN009267.D 4 06/16/14 NAF 06/10/14 OP51928 GNN403 Run #2 Initial Weight Final Volume Run #1 20.1 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)188 50 38 mg/kg C9-C18 Aliphatics 420 50 25 mg/kg C19-C36 Aliphatics 27.5 50 25 mg/kg J CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 68%40-140% 580-13-2 2-Bromonaphthalene 83%40-140% 84-15-1 o-Terphenyl 68%40-140% 321-60-8 2-Fluorobiphenyl 83%40-140% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 58 of 208 FA15409 33.11 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064664.D 1 06/02/14 AH n/a n/a VF2136 Run #2 Initial Weight Run #1 6.44 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.0365 0.049 0.015 mg/kg J 71-43-2 Benzene ND 0.0049 0.00098 mg/kg 108-86-1 Bromobenzene ND 0.0049 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0049 0.0019 mg/kg 75-27-4 Bromodichloromethane ND 0.0049 0.00098 mg/kg 75-25-2 Bromoform ND 0.0049 0.0011 mg/kg 104-51-8 n-Butylbenzene ND 0.0049 0.00098 mg/kg 135-98-8 sec-Butylbenzene ND 0.0049 0.00098 mg/kg 98-06-6 tert-Butylbenzene ND 0.0049 0.00098 mg/kg 108-90-7 Chlorobenzene ND 0.0049 0.00098 mg/kg 75-00-3 Chloroethane ND 0.0049 0.0022 mg/kg 67-66-3 Chloroform ND 0.0049 0.0011 mg/kg 95-49-8 o-Chlorotoluene ND 0.0049 0.00098 mg/kg 106-43-4 p-Chlorotoluene ND 0.0049 0.00098 mg/kg 56-23-5 Carbon tetrachloride ND 0.0049 0.0014 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0049 0.00098 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0049 0.00098 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0049 0.0011 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0049 0.0018 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0049 0.00098 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0049 0.00098 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0049 0.00098 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0049 0.0010 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0049 0.0014 mg/kg 124-48-1 Dibromochloromethane ND 0.0049 0.00098 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0049 0.0012 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0049 0.00098 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0049 0.00098 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0049 0.00098 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0049 0.00098 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0049 0.0011 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0049 0.0013 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 59 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0049 0.00098 mg/kg 64-17-5 Ethyl alcohol ND 0.39 0.066 mg/kg 100-41-4 Ethylbenzene 0.0038 0.0049 0.00098 mg/kg J 591-78-6 2-Hexanone ND 0.025 0.0048 mg/kg 98-82-8 Isopropylbenzene ND 0.0049 0.00098 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0049 0.00098 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.025 0.0049 mg/kg 74-83-9 Methyl bromide ND 0.0049 0.0018 mg/kg 74-87-3 Methyl chloride ND 0.0049 0.0020 mg/kg 75-09-2 Methylene chloride ND 0.0098 0.0039 mg/kg 78-93-3 Methyl ethyl ketone ND 0.025 0.0074 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0049 0.00098 mg/kg 91-20-3 Naphthalene 0.0037 0.0049 0.0020 mg/kg J 103-65-1 n-Propylbenzene ND 0.0049 0.00098 mg/kg 100-42-5 Styrene ND 0.0049 0.00098 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0049 0.0010 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0049 0.00098 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0049 0.0014 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0049 0.0016 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0049 0.0012 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0049 0.0018 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0049 0.0011 mg/kg 95-63-6 1,2,4-Trimethylbenzene 0.0049 0.0049 0.00098 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0049 0.00098 mg/kg 127-18-4 Tetrachloroethylene ND 0.0049 0.0012 mg/kg 108-88-3 Toluene 0.0038 0.0049 0.00098 mg/kg J 79-01-6 Trichloroethylene ND 0.0049 0.0010 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0049 0.00098 mg/kg 75-01-4 Vinyl chloride ND 0.0049 0.0010 mg/kg 108-05-4 Vinyl Acetate ND 0.025 0.0079 mg/kg 1330-20-7 Xylene (total)0.0237 0.015 0.0026 mg/kg m,p-Xylene 0.0152 0.0098 0.0016 mg/kg 95-47-6 o-Xylene 0.0085 0.0049 0.0011 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 89%75-124% 2037-26-5 Toluene-D8 92%75-126% 460-00-4 4-Bromofluorobenzene 104%71-133% 17060-07-0 1,2-Dichloroethane-D4 93%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 60 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X035134.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 Run #2 Initial Weight Final Volume Run #1 30.4 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.0 0.21 mg/kg 95-57-8 2-Chlorophenol ND 0.21 0.021 mg/kg 59-50-7 4-Chloro-3-methyl phenol ND 0.21 0.021 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.21 0.022 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.21 0.023 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.0 0.21 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.42 0.083 mg/kg 95-48-7 2-Methylphenol ND 0.21 0.021 mg/kg 3&4-Methylphenol ND 0.21 0.042 mg/kg 88-75-5 2-Nitrophenol ND 0.21 0.021 mg/kg 100-02-7 4-Nitrophenol ND 1.0 0.17 mg/kg 87-86-5 Pentachlorophenol ND 1.0 0.17 mg/kg 108-95-2 Phenol ND 0.21 0.021 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.21 0.021 mg/kg 83-32-9 Acenaphthene ND 0.21 0.026 mg/kg 208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg 120-12-7 Anthracene ND 0.21 0.021 mg/kg 56-55-3 Benzo(a)anthracene ND 0.21 0.021 mg/kg 50-32-8 Benzo(a)pyrene ND 0.21 0.021 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.21 0.021 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.21 0.021 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.21 0.023 mg/kg 101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.021 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.21 0.042 mg/kg 100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg 91-58-7 2-Chloronaphthalene ND 0.21 0.025 mg/kg 106-47-8 4-Chloroaniline ND 0.21 0.021 mg/kg 218-01-9 Chrysene ND 0.21 0.021 mg/kg 111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.021 mg/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 0.21 0.022 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.031 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 61 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.21 0.024 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.21 0.021 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.21 0.021 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.021 mg/kg 53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.021 mg/kg 132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg 84-74-2 Di-n-butyl phthalate ND 0.42 0.042 mg/kg 117-84-0 Di-n-octyl phthalate ND 0.21 0.042 mg/kg 84-66-2 Diethyl phthalate ND 0.42 0.042 mg/kg 131-11-3 Dimethyl phthalate ND 0.21 0.042 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.42 0.042 mg/kg 206-44-0 Fluoranthene ND 0.21 0.021 mg/kg 86-73-7 Fluorene ND 0.21 0.021 mg/kg 118-74-1 Hexachlorobenzene ND 0.21 0.021 mg/kg 87-68-3 Hexachlorobutadiene ND 0.21 0.021 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.21 0.021 mg/kg 67-72-1 Hexachloroethane ND 0.21 0.021 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.21 0.021 mg/kg 78-59-1 Isophorone ND 0.21 0.021 mg/kg 90-12-0 1-Methylnaphthalene ND 0.21 0.021 mg/kg 91-57-6 2-Methylnaphthalene ND 0.21 0.021 mg/kg 91-20-3 Naphthalene ND 0.21 0.021 mg/kg 98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg 621-64-7 N-Nitroso-di-n-propylamine ND 0.21 0.021 mg/kg 86-30-6 N-Nitrosodiphenylamine ND 0.21 0.021 mg/kg 85-01-8 Phenanthrene ND 0.21 0.021 mg/kg 129-00-0 Pyrene ND 0.21 0.021 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.021 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 59%40-102% 4165-62-2 Phenol-d5 66%41-100% 118-79-6 2,4,6-Tribromophenol 74%42-108% 4165-60-0 Nitrobenzene-d5 61%40-105% 321-60-8 2-Fluorobiphenyl 68%43-107% 1718-51-0 Terphenyl-d14 76%45-119% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 62 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007914.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.37 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 6.4 2.2 mg/kg C9- C12 Aliphatics (Unadj.)ND 6.4 2.2 mg/kg C9- C10 Aromatics (Unadj.)ND 6.4 2.2 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 123%70-130% 460-00-4 BFB 113%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 63 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B12 8-10 Lab Sample ID:FA15409-12 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:78.9 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN009105.D 1 06/10/14 NAF 06/02/14 OP51816 GNN399 Run #2 Initial Weight Final Volume Run #1 20.1 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)13.0 13 9.5 mg/kg C9-C18 Aliphatics ND 13 6.3 mg/kg C19-C36 Aliphatics 30.4 13 6.3 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 81%40-140% 580-13-2 2-Bromonaphthalene 86%40-140% 84-15-1 o-Terphenyl 65%40-140% 321-60-8 2-Fluorobiphenyl 74%40-140% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 64 of 208 FA15409 33.12 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064649.D 1 05/30/14 AH n/a n/a VF2135 Run #2 Initial Weight Run #1 6.10 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.218 0.054 0.016 mg/kg 71-43-2 Benzene 0.0127 0.0054 0.0011 mg/kg 108-86-1 Bromobenzene ND 0.0054 0.0012 mg/kg 74-97-5 Bromochloromethane ND 0.0054 0.0021 mg/kg 75-27-4 Bromodichloromethane ND 0.0054 0.0011 mg/kg 75-25-2 Bromoform ND 0.0054 0.0012 mg/kg 104-51-8 n-Butylbenzene ND 0.0054 0.0011 mg/kg 135-98-8 sec-Butylbenzene ND 0.0054 0.0011 mg/kg 98-06-6 tert-Butylbenzene ND 0.0054 0.0011 mg/kg 108-90-7 Chlorobenzene ND 0.0054 0.0011 mg/kg 75-00-3 Chloroethane ND 0.0054 0.0024 mg/kg 67-66-3 Chloroform ND 0.0054 0.0012 mg/kg 95-49-8 o-Chlorotoluene ND 0.0054 0.0011 mg/kg 106-43-4 p-Chlorotoluene ND 0.0054 0.0011 mg/kg 56-23-5 Carbon tetrachloride ND 0.0054 0.0015 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0054 0.0011 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0054 0.0011 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0054 0.0012 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0054 0.0019 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0054 0.0011 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0054 0.0011 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0054 0.0011 mg/kg 108-20-3 Di-Isopropyl ether 0.0038 0.0054 0.0011 mg/kg J 594-20-7 2,2-Dichloropropane ND 0.0054 0.0015 mg/kg 124-48-1 Dibromochloromethane ND 0.0054 0.0011 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0054 0.0014 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0054 0.0011 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0054 0.0011 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0054 0.0011 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0054 0.0011 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0054 0.0012 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0054 0.0014 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 65 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0054 0.0011 mg/kg 64-17-5 Ethyl alcohol ND 0.43 0.072 mg/kg 100-41-4 Ethylbenzene 0.0025 0.0054 0.0011 mg/kg J 591-78-6 2-Hexanone ND 0.027 0.0053 mg/kg 98-82-8 Isopropylbenzene ND 0.0054 0.0011 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0054 0.0011 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.027 0.0054 mg/kg 74-83-9 Methyl bromide ND 0.0054 0.0020 mg/kg 74-87-3 Methyl chloride ND 0.0054 0.0022 mg/kg 75-09-2 Methylene chloride ND 0.011 0.0043 mg/kg 78-93-3 Methyl ethyl ketone 0.0391 0.027 0.0081 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.0109 0.0054 0.0011 mg/kg 91-20-3 Naphthalene 0.0038 0.0054 0.0022 mg/kg J 103-65-1 n-Propylbenzene ND 0.0054 0.0011 mg/kg 100-42-5 Styrene ND 0.0054 0.0011 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0054 0.0011 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0054 0.0011 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0054 0.0015 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0054 0.0017 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0054 0.0013 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0054 0.0020 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0054 0.0012 mg/kg 95-63-6 1,2,4-Trimethylbenzene 0.0030 0.0054 0.0011 mg/kg J 108-67-8 1,3,5-Trimethylbenzene ND 0.0054 0.0011 mg/kg 127-18-4 Tetrachloroethylene ND 0.0054 0.0014 mg/kg 108-88-3 Toluene 0.0024 0.0054 0.0011 mg/kg J 79-01-6 Trichloroethylene ND 0.0054 0.0011 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0054 0.0011 mg/kg 75-01-4 Vinyl chloride ND 0.0054 0.0011 mg/kg 108-05-4 Vinyl Acetate ND 0.027 0.0086 mg/kg 1330-20-7 Xylene (total)0.0056 0.016 0.0029 mg/kg J m,p-Xylene 0.0040 0.011 0.0017 mg/kg J 95-47-6 o-Xylene 0.0017 0.0054 0.0012 mg/kg J CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 92%75-124% 2037-26-5 Toluene-D8 88%75-126% 460-00-4 4-Bromofluorobenzene 104%71-133% 17060-07-0 1,2-Dichloroethane-D4 86%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 66 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X035135.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 Run #2 Initial Weight Final Volume Run #1 29.8 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.1 0.22 mg/kg 95-57-8 2-Chlorophenol ND 0.22 0.022 mg/kg 59-50-7 4-Chloro-3-methyl phenol ND 0.22 0.022 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.22 0.023 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.22 0.024 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.1 0.22 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.44 0.088 mg/kg 95-48-7 2-Methylphenol ND 0.22 0.022 mg/kg 3&4-Methylphenol ND 0.22 0.044 mg/kg 88-75-5 2-Nitrophenol ND 0.22 0.022 mg/kg 100-02-7 4-Nitrophenol ND 1.1 0.18 mg/kg 87-86-5 Pentachlorophenol ND 1.1 0.18 mg/kg 108-95-2 Phenol ND 0.22 0.022 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.22 0.022 mg/kg 83-32-9 Acenaphthene ND 0.22 0.028 mg/kg 208-96-8 Acenaphthylene ND 0.22 0.022 mg/kg 120-12-7 Anthracene ND 0.22 0.022 mg/kg 56-55-3 Benzo(a)anthracene ND 0.22 0.022 mg/kg 50-32-8 Benzo(a)pyrene ND 0.22 0.022 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.22 0.022 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.22 0.022 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.22 0.024 mg/kg 101-55-3 4-Bromophenyl phenyl ether ND 0.22 0.022 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.22 0.044 mg/kg 100-51-6 Benzyl Alcohol ND 0.22 0.022 mg/kg 91-58-7 2-Chloronaphthalene ND 0.22 0.026 mg/kg 106-47-8 4-Chloroaniline ND 0.22 0.022 mg/kg 218-01-9 Chrysene ND 0.22 0.022 mg/kg 111-91-1 bis(2-Chloroethoxy)methane ND 0.22 0.022 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.22 0.022 mg/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 0.22 0.023 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.22 0.033 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 67 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 0.22 0.022 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.22 0.025 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.22 0.022 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.22 0.022 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.22 0.022 mg/kg 53-70-3 Dibenzo(a,h)anthracene ND 0.22 0.022 mg/kg 132-64-9 Dibenzofuran ND 0.22 0.022 mg/kg 84-74-2 Di-n-butyl phthalate ND 0.44 0.044 mg/kg 117-84-0 Di-n-octyl phthalate ND 0.22 0.044 mg/kg 84-66-2 Diethyl phthalate ND 0.44 0.044 mg/kg 131-11-3 Dimethyl phthalate ND 0.22 0.044 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.44 0.044 mg/kg 206-44-0 Fluoranthene ND 0.22 0.022 mg/kg 86-73-7 Fluorene ND 0.22 0.022 mg/kg 118-74-1 Hexachlorobenzene ND 0.22 0.022 mg/kg 87-68-3 Hexachlorobutadiene ND 0.22 0.022 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.22 0.022 mg/kg 67-72-1 Hexachloroethane ND 0.22 0.022 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.22 0.022 mg/kg 78-59-1 Isophorone ND 0.22 0.022 mg/kg 90-12-0 1-Methylnaphthalene ND 0.22 0.022 mg/kg 91-57-6 2-Methylnaphthalene ND 0.22 0.022 mg/kg 91-20-3 Naphthalene ND 0.22 0.022 mg/kg 98-95-3 Nitrobenzene ND 0.22 0.022 mg/kg 621-64-7 N-Nitroso-di-n-propylamine ND 0.22 0.022 mg/kg 86-30-6 N-Nitrosodiphenylamine ND 0.22 0.022 mg/kg 85-01-8 Phenanthrene ND 0.22 0.022 mg/kg 129-00-0 Pyrene ND 0.22 0.022 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.22 0.022 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 44%40-102% 4165-62-2 Phenol-d5 52%41-100% 118-79-6 2,4,6-Tribromophenol 65%42-108% 4165-60-0 Nitrobenzene-d5 47%40-105% 321-60-8 2-Fluorobiphenyl 54%43-107% 1718-51-0 Terphenyl-d14 68%45-119% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 68 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007917.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.24 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg C9- C12 Aliphatics (Unadj.)ND 6.9 2.4 mg/kg C9- C10 Aromatics (Unadj.)ND 6.9 2.4 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 111%70-130% 460-00-4 BFB 102%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 69 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B13 8-10 Lab Sample ID:FA15409-13 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:76.2 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN009106.D 1 06/10/14 NAF 06/02/14 OP51816 GNN399 Run #2 Initial Weight Final Volume Run #1 19.9 g 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)ND 13 9.9 mg/kg C9-C18 Aliphatics ND 13 6.6 mg/kg C19-C36 Aliphatics ND 13 6.6 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 61%40-140% 580-13-2 2-Bromonaphthalene 76%40-140% 84-15-1 o-Terphenyl 59%40-140% 321-60-8 2-Fluorobiphenyl 66%40-140% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 70 of 208 FA15409 33.13 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064678.D 1 06/02/14 AH n/a n/a VF2136 Run #2 Initial Weight Methanol Aliquot Run #1 5.82 g 100 ul Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 3.5 1.1 mg/kg 71-43-2 Benzene 1.13 0.35 0.070 mg/kg 108-86-1 Bromobenzene ND 0.35 0.077 mg/kg 74-97-5 Bromochloromethane ND 0.35 0.13 mg/kg 75-27-4 Bromodichloromethane ND 0.35 0.070 mg/kg 75-25-2 Bromoform ND 0.35 0.076 mg/kg 104-51-8 n-Butylbenzene 0.524 0.35 0.070 mg/kg 135-98-8 sec-Butylbenzene 0.156 0.35 0.070 mg/kg J 98-06-6 tert-Butylbenzene ND 0.35 0.070 mg/kg 108-90-7 Chlorobenzene ND 0.35 0.070 mg/kg 75-00-3 Chloroethane ND 0.35 0.16 mg/kg 67-66-3 Chloroform ND 0.35 0.079 mg/kg 95-49-8 o-Chlorotoluene ND 0.35 0.070 mg/kg 106-43-4 p-Chlorotoluene ND 0.35 0.070 mg/kg 56-23-5 Carbon tetrachloride ND 0.35 0.098 mg/kg 75-34-3 1,1-Dichloroethane ND 0.35 0.070 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.35 0.070 mg/kg 563-58-6 1,1-Dichloropropene ND 0.35 0.078 mg/kg 106-93-4 1,2-Dibromoethane ND 0.35 0.13 mg/kg 107-06-2 1,2-Dichloroethane ND 0.35 0.070 mg/kg 78-87-5 1,2-Dichloropropane ND 0.35 0.070 mg/kg 142-28-9 1,3-Dichloropropane ND 0.35 0.070 mg/kg 108-20-3 Di-Isopropyl ether ND 0.35 0.072 mg/kg 594-20-7 2,2-Dichloropropane ND 0.35 0.099 mg/kg 124-48-1 Dibromochloromethane ND 0.35 0.070 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.35 0.089 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.35 0.070 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.35 0.070 mg/kg 541-73-1 m-Dichlorobenzene ND 0.35 0.070 mg/kg 95-50-1 o-Dichlorobenzene ND 0.35 0.070 mg/kg 106-46-7 p-Dichlorobenzene ND 0.35 0.079 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.35 0.094 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 71 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.35 0.070 mg/kg 64-17-5 Ethyl alcohol ND 28 4.7 mg/kg 100-41-4 Ethylbenzene 2.94 0.35 0.070 mg/kg 591-78-6 2-Hexanone ND 1.8 0.34 mg/kg 98-82-8 Isopropylbenzene 0.328 0.35 0.070 mg/kg J 99-87-6 p-Isopropyltoluene 0.113 0.35 0.070 mg/kg J 108-10-1 4-Methyl-2-pentanone ND 1.8 0.35 mg/kg 74-83-9 Methyl bromide ND 0.35 0.13 mg/kg 74-87-3 Methyl chloride ND 0.35 0.14 mg/kg 75-09-2 Methylene chloride 0.348 0.70 0.28 mg/kg JB 78-93-3 Methyl ethyl ketone ND 1.8 0.53 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.137 0.35 0.070 mg/kg J 91-20-3 Naphthalene 2.04 0.35 0.14 mg/kg 103-65-1 n-Propylbenzene 1.19 0.35 0.070 mg/kg 100-42-5 Styrene 0.163 0.35 0.070 mg/kg J 630-20-6 1,1,1,2-Tetrachloroethane ND 0.35 0.074 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.35 0.070 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.35 0.099 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.35 0.11 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.35 0.084 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.35 0.13 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.35 0.081 mg/kg 95-63-6 1,2,4-Trimethylbenzene 7.32 0.35 0.070 mg/kg 108-67-8 1,3,5-Trimethylbenzene 2.26 0.35 0.070 mg/kg 127-18-4 Tetrachloroethylene ND 0.35 0.089 mg/kg 108-88-3 Toluene 12.7 0.35 0.070 mg/kg 79-01-6 Trichloroethylene ND 0.35 0.072 mg/kg 75-69-4 Trichlorofluoromethane ND 0.35 0.070 mg/kg 75-01-4 Vinyl chloride ND 0.35 0.072 mg/kg 108-05-4 Vinyl Acetate ND 1.8 0.56 mg/kg 1330-20-7 Xylene (total)17.2 1.1 0.19 mg/kg m,p-Xylene 11.7 0.70 0.11 mg/kg 95-47-6 o-Xylene 5.48 0.35 0.075 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 86%75-124% 2037-26-5 Toluene-D8 93%75-126% 460-00-4 4-Bromofluorobenzene 102%71-133% 17060-07-0 1,2-Dichloroethane-D4 81%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 72 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X035136.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 Run #2 Initial Weight Final Volume Run #1 30.2 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 1.1 0.21 mg/kg 95-57-8 2-Chlorophenol ND 0.21 0.021 mg/kg 59-50-7 4-Chloro-3-methyl phenol ND 0.21 0.021 mg/kg 120-83-2 2,4-Dichlorophenol ND 0.21 0.022 mg/kg 105-67-9 2,4-Dimethylphenol ND 0.21 0.024 mg/kg 51-28-5 2,4-Dinitrophenol ND 1.1 0.21 mg/kg 534-52-1 4,6-Dinitro-o-cresol ND 0.43 0.086 mg/kg 95-48-7 2-Methylphenol ND 0.21 0.021 mg/kg 3&4-Methylphenol ND 0.21 0.043 mg/kg 88-75-5 2-Nitrophenol ND 0.21 0.021 mg/kg 100-02-7 4-Nitrophenol ND 1.1 0.17 mg/kg 87-86-5 Pentachlorophenol ND 1.1 0.17 mg/kg 108-95-2 Phenol ND 0.21 0.021 mg/kg 88-06-2 2,4,6-Trichlorophenol ND 0.21 0.021 mg/kg 83-32-9 Acenaphthene ND 0.21 0.027 mg/kg 208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg 120-12-7 Anthracene ND 0.21 0.021 mg/kg 56-55-3 Benzo(a)anthracene ND 0.21 0.021 mg/kg 50-32-8 Benzo(a)pyrene ND 0.21 0.021 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.21 0.021 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.21 0.021 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.21 0.023 mg/kg 101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.021 mg/kg 85-68-7 Butyl benzyl phthalate ND 0.21 0.043 mg/kg 100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg 91-58-7 2-Chloronaphthalene ND 0.21 0.025 mg/kg 106-47-8 4-Chloroaniline ND 0.21 0.021 mg/kg 218-01-9 Chrysene ND 0.21 0.021 mg/kg 111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg 111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.021 mg/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 0.21 0.022 mg/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.032 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 73 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8270D SW846 3550C Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg 122-66-7 1,2-Diphenylhydrazine ND 0.21 0.024 mg/kg 541-73-1 1,3-Dichlorobenzene ND 0.21 0.021 mg/kg 106-46-7 1,4-Dichlorobenzene ND 0.21 0.021 mg/kg 91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.021 mg/kg 53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.021 mg/kg 132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg 84-74-2 Di-n-butyl phthalate ND 0.43 0.043 mg/kg 117-84-0 Di-n-octyl phthalate ND 0.21 0.043 mg/kg 84-66-2 Diethyl phthalate ND 0.43 0.043 mg/kg 131-11-3 Dimethyl phthalate ND 0.21 0.043 mg/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 0.43 0.043 mg/kg 206-44-0 Fluoranthene ND 0.21 0.021 mg/kg 86-73-7 Fluorene ND 0.21 0.021 mg/kg 118-74-1 Hexachlorobenzene ND 0.21 0.021 mg/kg 87-68-3 Hexachlorobutadiene ND 0.21 0.021 mg/kg 77-47-4 Hexachlorocyclopentadiene ND 0.21 0.021 mg/kg 67-72-1 Hexachloroethane ND 0.21 0.021 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.21 0.021 mg/kg 78-59-1 Isophorone ND 0.21 0.021 mg/kg 90-12-0 1-Methylnaphthalene 0.569 0.21 0.021 mg/kg 91-57-6 2-Methylnaphthalene 1.26 0.21 0.021 mg/kg 91-20-3 Naphthalene 0.951 0.21 0.021 mg/kg 98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg 621-64-7 N-Nitroso-di-n-propylamine ND 0.21 0.021 mg/kg 86-30-6 N-Nitrosodiphenylamine ND 0.21 0.021 mg/kg 85-01-8 Phenanthrene ND 0.21 0.021 mg/kg 129-00-0 Pyrene ND 0.21 0.021 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.021 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 55%40-102% 4165-62-2 Phenol-d5 62%41-100% 118-79-6 2,4,6-Tribromophenol 71%42-108% 4165-60-0 Nitrobenzene-d5 58%40-105% 321-60-8 2-Fluorobiphenyl 63%43-107% 1718-51-0 Terphenyl-d14 75%45-119% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 74 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007936.D 1 06/03/14 MM n/a n/a GUU392 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.39 g 5.1 ml 25.0 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)47.1 30 11 mg/kg C9- C12 Aliphatics (Unadj.)48.2 30 11 mg/kg C9- C10 Aromatics (Unadj.)75.6 30 11 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 120%70-130% 460-00-4 BFB 94%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 75 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B14 13-15 Lab Sample ID:FA15409-14 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:77.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN009206.D 1 06/13/14 NG 06/10/14 OP51928 GNN402 Run #2 NN009059.D 4 06/06/14 NAF 06/02/14 OP51816 GNN397 Initial Weight Final Volume Run #1 20.6 g 2.0 ml Run #2 20.2 g 2.0 ml MAEPH List CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)30.6 13 9.4 mg/kg C9-C18 Aliphatics 108 13 6.3 mg/kg C19-C36 Aliphatics ND 13 6.3 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 57%40%40-140% 580-13-2 2-Bromonaphthalene 95%27%40-140% 84-15-1 o-Terphenyl 65%40%40-140% 321-60-8 2-Fluorobiphenyl 90%27%40-140% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 76 of 208 FA15409 33.14 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B15 13-15 Lab Sample ID:FA15409-15 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:69.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082023.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.59 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 8.7 4.4 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 100%56-149% 98-08-8 aaa-Trifluorotoluene 102%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 77 of 208 FA15409 33.15 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B15 13-15 Lab Sample ID:FA15409-15 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C SW846 3550C Percent Solids:69.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 WR5667.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 Run #2 Initial Weight Final Volume Run #1 30.1 g 1.0 ml Run #2 CAS No.Compound Result RL MDL Units Q TPH (C10-C28)ND 6.0 3.6 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 84-15-1 o-Terphenyl 96%56-122% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 78 of 208 FA15409 33.15 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B16 13-15 Lab Sample ID:FA15409-16 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:74.8 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082026.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.87 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 7.4 3.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 100%56-149% 98-08-8 aaa-Trifluorotoluene 102%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 79 of 208 FA15409 33.16 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:B17 13-15 Lab Sample ID:FA15409-17 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:73.4 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082027.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.13 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 7.4 3.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 100%56-149% 98-08-8 aaa-Trifluorotoluene 103%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 80 of 208 FA15409 33.17 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 2 Client Sample ID:G1 0-5 Lab Sample ID:FA15409-18 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:88.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064666.D 1 06/02/14 AH n/a n/a VF2136 Run #2 Initial Weight Run #1 6.31 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 0.120 0.045 0.013 mg/kg 71-43-2 Benzene 0.0101 0.0045 0.00090 mg/kg 108-86-1 Bromobenzene ND 0.0045 0.00098 mg/kg 74-97-5 Bromochloromethane ND 0.0045 0.0017 mg/kg 75-27-4 Bromodichloromethane ND 0.0045 0.00090 mg/kg 75-25-2 Bromoform ND 0.0045 0.00097 mg/kg 104-51-8 n-Butylbenzene 0.0061 0.0045 0.00090 mg/kg 135-98-8 sec-Butylbenzene 0.0030 0.0045 0.00090 mg/kg J 98-06-6 tert-Butylbenzene ND 0.0045 0.00090 mg/kg 108-90-7 Chlorobenzene ND 0.0045 0.00090 mg/kg 75-00-3 Chloroethane ND 0.0045 0.0020 mg/kg 67-66-3 Chloroform ND 0.0045 0.0010 mg/kg 95-49-8 o-Chlorotoluene ND 0.0045 0.00090 mg/kg 106-43-4 p-Chlorotoluene ND 0.0045 0.00090 mg/kg 56-23-5 Carbon tetrachloride ND 0.0045 0.0012 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0045 0.00090 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0045 0.00090 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0045 0.0010 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0045 0.0016 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0045 0.00090 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0045 0.00090 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0045 0.00090 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0045 0.00092 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0045 0.0013 mg/kg 124-48-1 Dibromochloromethane ND 0.0045 0.00090 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0045 0.0011 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0045 0.00090 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0045 0.00090 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0045 0.00090 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0045 0.00090 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0045 0.0010 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0045 0.0012 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 81 of 208 FA15409 33.18 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 2 Client Sample ID:G1 0-5 Lab Sample ID:FA15409-18 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:88.3 Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0045 0.00090 mg/kg 64-17-5 Ethyl alcohol ND 0.36 0.060 mg/kg 100-41-4 Ethylbenzene 0.104 0.0045 0.00090 mg/kg 591-78-6 2-Hexanone ND 0.022 0.0044 mg/kg 98-82-8 Isopropylbenzene 0.0084 0.0045 0.00090 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0045 0.00090 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.022 0.0045 mg/kg 74-83-9 Methyl bromide ND 0.0045 0.0017 mg/kg 74-87-3 Methyl chloride ND 0.0045 0.0018 mg/kg 75-09-2 Methylene chloride ND 0.0090 0.0036 mg/kg 78-93-3 Methyl ethyl ketone 0.0223 0.022 0.0067 mg/kg 1634-04-4 Methyl Tert Butyl Ether 0.0037 0.0045 0.00090 mg/kg J 91-20-3 Naphthalene 0.0570 0.0045 0.0018 mg/kg 103-65-1 n-Propylbenzene 0.0277 0.0045 0.00090 mg/kg 100-42-5 Styrene ND 0.0045 0.00090 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0045 0.00094 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0045 0.00090 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0045 0.0013 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0045 0.0014 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0045 0.0011 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0045 0.0017 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0045 0.0010 mg/kg 95-63-6 1,2,4-Trimethylbenzene 0.0706 0.0045 0.00090 mg/kg 108-67-8 1,3,5-Trimethylbenzene 0.0194 0.0045 0.00090 mg/kg 127-18-4 Tetrachloroethylene ND 0.0045 0.0011 mg/kg 108-88-3 Toluene 0.0046 0.0045 0.00090 mg/kg 79-01-6 Trichloroethylene ND 0.0045 0.00092 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0045 0.00090 mg/kg 75-01-4 Vinyl chloride ND 0.0045 0.00092 mg/kg 108-05-4 Vinyl Acetate ND 0.022 0.0072 mg/kg 1330-20-7 Xylene (total)0.0497 0.013 0.0024 mg/kg m,p-Xylene 0.0472 0.0090 0.0014 mg/kg 95-47-6 o-Xylene 0.0024 0.0045 0.00096 mg/kg J CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 91%75-124% 2037-26-5 Toluene-D8 89%75-126% 460-00-4 4-Bromofluorobenzene 100%71-133% 17060-07-0 1,2-Dichloroethane-D4 97%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 82 of 208 FA15409 33.18 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:G1 0-5 Lab Sample ID:FA15409-18 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:88.3 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU007919.D 1 06/02/14 AH n/a n/a GUU391 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 7.05 g 5.1 ml 100 ul Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)1.91 4.8 1.7 mg/kg J C9- C12 Aliphatics (Unadj.)ND 4.8 1.7 mg/kg C9- C10 Aromatics (Unadj.)4.95 4.8 1.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 110%70-130% 460-00-4 BFB 99%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 83 of 208 FA15409 33.18 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:G2 0-5 Lab Sample ID:FA15409-19 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:82.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082028.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 6.45 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)16.6 5.8 2.9 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 99%56-149% 98-08-8 aaa-Trifluorotoluene 101%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 84 of 208 FA15409 33.19 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:D16 3-4 Lab Sample ID:FA15409-20 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:77.7 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082029.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.82 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 7.0 3.5 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 99%56-149% 98-08-8 aaa-Trifluorotoluene 102%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 85 of 208 FA15409 33.20 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:D16 3-4 Lab Sample ID:FA15409-20 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C SW846 3550C Percent Solids:77.7 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 WR5668.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 Run #2 Initial Weight Final Volume Run #1 29.8 g 1.0 ml Run #2 CAS No.Compound Result RL MDL Units Q TPH (C10-C28) a 12.0 5.4 3.2 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 84-15-1 o-Terphenyl 103%56-122% (a) Petroleum hydrocarbon pattern extends beyond C28. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 86 of 208 FA15409 33.20 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:K16 1.5 Lab Sample ID:FA15409-21 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C Percent Solids:76.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 QR082033.D 1 06/03/14 MM n/a n/a GQR3491 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.81 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 8.4 4.2 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 101%56-149% 98-08-8 aaa-Trifluorotoluene 103%66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 87 of 208 FA15409 33.21 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:K16 1.5 Lab Sample ID:FA15409-21 Date Sampled:05/28/14 Matrix:SO - Soil Date Received:05/30/14 Method:SW846 8015C SW846 3550C Percent Solids:76.0 Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 WR5669.D 5 06/03/14 SJL 06/02/14 OP51815 GWR165 Run #2 Initial Weight Final Volume Run #1 30.3 g 1.0 ml Run #2 CAS No.Compound Result RL MDL Units Q TPH (C10-C28) a 152 27 16 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 84-15-1 o-Terphenyl 77%56-122% (a) Petroleum hydrocarbon pattern extends beyond C28. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 88 of 208 FA15409 33.21 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-22 Date Sampled:05/28/14 Matrix:SO - Trip Blank Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 F0064646.D 1 05/30/14 AH n/a n/a VF2135 Run #2 Initial Weight Run #1 5.00 g Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 0.050 0.015 mg/kg 71-43-2 Benzene ND 0.0050 0.0010 mg/kg 108-86-1 Bromobenzene ND 0.0050 0.0011 mg/kg 74-97-5 Bromochloromethane ND 0.0050 0.0019 mg/kg 75-27-4 Bromodichloromethane ND 0.0050 0.0010 mg/kg 75-25-2 Bromoform ND 0.0050 0.0011 mg/kg 104-51-8 n-Butylbenzene ND 0.0050 0.0010 mg/kg 135-98-8 sec-Butylbenzene ND 0.0050 0.0010 mg/kg 98-06-6 tert-Butylbenzene ND 0.0050 0.0010 mg/kg 108-90-7 Chlorobenzene ND 0.0050 0.0010 mg/kg 75-00-3 Chloroethane ND 0.0050 0.0023 mg/kg 67-66-3 Chloroform ND 0.0050 0.0011 mg/kg 95-49-8 o-Chlorotoluene ND 0.0050 0.0010 mg/kg 106-43-4 p-Chlorotoluene ND 0.0050 0.0010 mg/kg 56-23-5 Carbon tetrachloride ND 0.0050 0.0014 mg/kg 75-34-3 1,1-Dichloroethane ND 0.0050 0.0010 mg/kg 75-35-4 1,1-Dichloroethylene ND 0.0050 0.0010 mg/kg 563-58-6 1,1-Dichloropropene ND 0.0050 0.0011 mg/kg 106-93-4 1,2-Dibromoethane ND 0.0050 0.0018 mg/kg 107-06-2 1,2-Dichloroethane ND 0.0050 0.0010 mg/kg 78-87-5 1,2-Dichloropropane ND 0.0050 0.0010 mg/kg 142-28-9 1,3-Dichloropropane ND 0.0050 0.0010 mg/kg 108-20-3 Di-Isopropyl ether ND 0.0050 0.0010 mg/kg 594-20-7 2,2-Dichloropropane ND 0.0050 0.0014 mg/kg 124-48-1 Dibromochloromethane ND 0.0050 0.0010 mg/kg 75-71-8 Dichlorodifluoromethane ND 0.0050 0.0013 mg/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.0050 0.0010 mg/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.0050 0.0010 mg/kg 541-73-1 m-Dichlorobenzene ND 0.0050 0.0010 mg/kg 95-50-1 o-Dichlorobenzene ND 0.0050 0.0010 mg/kg 106-46-7 p-Dichlorobenzene ND 0.0050 0.0011 mg/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.0050 0.0013 mg/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 89 of 208 FA15409 33.22 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-22 Date Sampled:05/28/14 Matrix:SO - Trip Blank Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.0050 0.0010 mg/kg 64-17-5 Ethyl alcohol ND 0.40 0.067 mg/kg 100-41-4 Ethylbenzene ND 0.0050 0.0010 mg/kg 591-78-6 2-Hexanone ND 0.025 0.0049 mg/kg 98-82-8 Isopropylbenzene ND 0.0050 0.0010 mg/kg 99-87-6 p-Isopropyltoluene ND 0.0050 0.0010 mg/kg 108-10-1 4-Methyl-2-pentanone ND 0.025 0.0050 mg/kg 74-83-9 Methyl bromide ND 0.0050 0.0019 mg/kg 74-87-3 Methyl chloride ND 0.0050 0.0020 mg/kg 75-09-2 Methylene chloride a 0.0048 0.010 0.0040 mg/kg JB 78-93-3 Methyl ethyl ketone ND 0.025 0.0075 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.0050 0.0010 mg/kg 91-20-3 Naphthalene ND 0.0050 0.0020 mg/kg 103-65-1 n-Propylbenzene ND 0.0050 0.0010 mg/kg 100-42-5 Styrene ND 0.0050 0.0010 mg/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.0050 0.0011 mg/kg 71-55-6 1,1,1-Trichloroethane ND 0.0050 0.0010 mg/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.0050 0.0014 mg/kg 79-00-5 1,1,2-Trichloroethane ND 0.0050 0.0016 mg/kg 87-61-6 1,2,3-Trichlorobenzene ND 0.0050 0.0012 mg/kg 96-18-4 1,2,3-Trichloropropane ND 0.0050 0.0019 mg/kg 120-82-1 1,2,4-Trichlorobenzene ND 0.0050 0.0012 mg/kg 95-63-6 1,2,4-Trimethylbenzene ND 0.0050 0.0010 mg/kg 108-67-8 1,3,5-Trimethylbenzene ND 0.0050 0.0010 mg/kg 127-18-4 Tetrachloroethylene ND 0.0050 0.0013 mg/kg 108-88-3 Toluene ND 0.0050 0.0010 mg/kg 79-01-6 Trichloroethylene ND 0.0050 0.0010 mg/kg 75-69-4 Trichlorofluoromethane ND 0.0050 0.0010 mg/kg 75-01-4 Vinyl chloride ND 0.0050 0.0010 mg/kg 108-05-4 Vinyl Acetate ND 0.025 0.0080 mg/kg 1330-20-7 Xylene (total)ND 0.015 0.0027 mg/kg m,p-Xylene ND 0.010 0.0016 mg/kg 95-47-6 o-Xylene ND 0.0050 0.0011 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 91%75-124% 2037-26-5 Toluene-D8 90%75-126% 460-00-4 4-Bromofluorobenzene 107%71-133% 17060-07-0 1,2-Dichloroethane-D4 91%72-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 90 of 208 FA15409 33.22 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-22 Date Sampled:05/28/14 Matrix:SO - Trip Blank Soil Date Received:05/30/14 Method:SW846 8260B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 91 of 208 FA15409 33.22 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:GW 1 Lab Sample ID:FA15409-23 Date Sampled:05/28/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0187270.D 5 06/06/14 TD n/a n/a VA1478 Run #2 a E031079.D 20 06/06/14 TD n/a n/a VE1043 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 5.0 ug/l 71-43-2 Benzene 57.9 2.5 0.50 ug/l 108-86-1 Bromobenzene ND 2.5 0.50 ug/l 74-97-5 Bromochloromethane ND 2.5 0.50 ug/l 75-27-4 Bromodichloromethane ND 2.5 0.50 ug/l 75-25-2 Bromoform ND 2.5 0.50 ug/l 104-51-8 n-Butylbenzene 0.93 2.5 0.50 ug/l J 135-98-8 sec-Butylbenzene 0.65 2.5 0.50 ug/l J 98-06-6 tert-Butylbenzene ND 2.5 0.50 ug/l 108-90-7 Chlorobenzene ND 2.5 0.50 ug/l 75-00-3 Chloroethane 1.7 2.5 0.61 ug/l J 67-66-3 Chloroform ND 2.5 0.50 ug/l 95-49-8 o-Chlorotoluene ND 2.5 0.50 ug/l 106-43-4 p-Chlorotoluene ND 2.5 0.50 ug/l 56-23-5 Carbon tetrachloride ND 2.5 0.50 ug/l 75-34-3 1,1-Dichloroethane ND 2.5 0.50 ug/l 75-35-4 1,1-Dichloroethylene ND 2.5 0.50 ug/l 563-58-6 1,1-Dichloropropene ND 2.5 0.50 ug/l 106-93-4 1,2-Dibromoethane ND 2.5 0.50 ug/l 107-06-2 1,2-Dichloroethane ND 2.5 0.50 ug/l 78-87-5 1,2-Dichloropropane ND 2.5 0.50 ug/l 142-28-9 1,3-Dichloropropane ND 2.5 0.50 ug/l 108-20-3 Di-Isopropyl ether 10.1 2.5 0.50 ug/l 594-20-7 2,2-Dichloropropane ND 2.5 0.50 ug/l 124-48-1 Dibromochloromethane ND 2.5 0.50 ug/l 75-71-8 Dichlorodifluoromethane ND 2.5 0.50 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.50 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.50 ug/l 541-73-1 m-Dichlorobenzene ND 2.5 0.50 ug/l 95-50-1 o-Dichlorobenzene ND 2.5 0.50 ug/l 106-46-7 p-Dichlorobenzene ND 2.5 0.50 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.50 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 92 of 208 FA15409 33.23 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:GW 1 Lab Sample ID:FA15409-23 Date Sampled:05/28/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.50 ug/l 100-41-4 Ethylbenzene 31.2 2.5 0.50 ug/l 64-17-5 Ethyl Alcohol ND 500 130 ug/l 591-78-6 2-Hexanone ND 25 2.5 ug/l 98-82-8 Isopropylbenzene 6.7 2.5 0.50 ug/l 99-87-6 p-Isopropyltoluene ND 2.5 0.50 ug/l 108-10-1 4-Methyl-2-pentanone ND 13 2.5 ug/l 74-83-9 Methyl bromide ND 2.5 0.50 ug/l 74-87-3 Methyl chloride 0.79 2.5 0.50 ug/l J 75-09-2 Methylene chloride ND 10 5.0 ug/l 78-93-3 Methyl ethyl ketone ND 13 3.4 ug/l 1634-04-4 Methyl Tert Butyl Ether 52.4 2.5 0.50 ug/l 91-20-3 Naphthalene 85.2 2.5 0.50 ug/l 103-65-1 n-Propylbenzene 5.9 2.5 0.50 ug/l 100-42-5 Styrene 3.1 2.5 0.50 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.50 ug/l 71-55-6 1,1,1-Trichloroethane ND 2.5 0.50 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.50 ug/l 79-00-5 1,1,2-Trichloroethane ND 2.5 0.53 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.50 ug/l 96-18-4 1,2,3-Trichloropropane ND 2.5 0.59 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.50 ug/l 95-63-6 1,2,4-Trimethylbenzene 13.0 2.5 0.50 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 2.5 0.50 ug/l 127-18-4 Tetrachloroethylene ND 2.5 0.50 ug/l 108-88-3 Toluene 22.6 2.5 0.50 ug/l 79-01-6 Trichloroethylene ND 2.5 0.50 ug/l 75-69-4 Trichlorofluoromethane ND 2.5 0.50 ug/l 75-01-4 Vinyl chloride ND 2.5 0.50 ug/l 108-05-4 Vinyl Acetate b ND 25 0.88 ug/l 1330-20-7 Xylene (total)284 c 30 4.0 ug/l m,p-Xylene 9.7 c 20 2.0 ug/l J 95-47-6 o-Xylene 274 c 10 2.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%98%70-130% 2037-26-5 Toluene-D8 101%100%70-130% 460-00-4 4-Bromofluorobenzene 103%105%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 93 of 208 FA15409 33.23 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:GW 1 Lab Sample ID:FA15409-23 Date Sampled:05/28/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Sample vial(s) contained significant headspace; reported results are considered minimum values. (b) Associated BS recovery outside control limits. (c) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 94 of 208 FA15409 33.23 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0187271.D 50 06/06/14 TD n/a n/a VA1478 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 500 50 ug/l 71-43-2 Benzene 2000 25 5.0 ug/l 108-86-1 Bromobenzene ND 25 5.0 ug/l 74-97-5 Bromochloromethane ND 25 5.0 ug/l 75-27-4 Bromodichloromethane ND 25 5.0 ug/l 75-25-2 Bromoform ND 25 5.0 ug/l 104-51-8 n-Butylbenzene 10.5 25 5.0 ug/l J 135-98-8 sec-Butylbenzene 6.9 25 5.0 ug/l J 98-06-6 tert-Butylbenzene ND 25 5.0 ug/l 108-90-7 Chlorobenzene ND 25 5.0 ug/l 75-00-3 Chloroethane ND 25 6.1 ug/l 67-66-3 Chloroform ND 25 5.0 ug/l 95-49-8 o-Chlorotoluene ND 25 5.0 ug/l 106-43-4 p-Chlorotoluene ND 25 5.0 ug/l 56-23-5 Carbon tetrachloride ND 25 5.0 ug/l 75-34-3 1,1-Dichloroethane ND 25 5.0 ug/l 75-35-4 1,1-Dichloroethylene ND 25 5.0 ug/l 563-58-6 1,1-Dichloropropene ND 25 5.0 ug/l 106-93-4 1,2-Dibromoethane ND 25 5.0 ug/l 107-06-2 1,2-Dichloroethane ND 25 5.0 ug/l 78-87-5 1,2-Dichloropropane ND 25 5.0 ug/l 142-28-9 1,3-Dichloropropane ND 25 5.0 ug/l 108-20-3 Di-Isopropyl ether 182 25 5.0 ug/l 594-20-7 2,2-Dichloropropane ND 25 5.0 ug/l 124-48-1 Dibromochloromethane ND 25 5.0 ug/l 75-71-8 Dichlorodifluoromethane ND 25 5.0 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 25 5.0 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 25 5.0 ug/l 541-73-1 m-Dichlorobenzene ND 25 5.0 ug/l 95-50-1 o-Dichlorobenzene ND 25 5.0 ug/l 106-46-7 p-Dichlorobenzene ND 25 5.0 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 25 5.0 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 95 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 25 5.0 ug/l 100-41-4 Ethylbenzene 860 25 5.0 ug/l 64-17-5 Ethyl Alcohol ND 5000 1300 ug/l 591-78-6 2-Hexanone ND 250 25 ug/l 98-82-8 Isopropylbenzene 29.6 25 5.0 ug/l 99-87-6 p-Isopropyltoluene ND 25 5.0 ug/l 108-10-1 4-Methyl-2-pentanone ND 130 25 ug/l 74-83-9 Methyl bromide ND 25 5.0 ug/l 74-87-3 Methyl chloride ND 25 5.0 ug/l 75-09-2 Methylene chloride ND 100 50 ug/l 78-93-3 Methyl ethyl ketone ND 130 34 ug/l 1634-04-4 Methyl Tert Butyl Ether 393 25 5.0 ug/l 91-20-3 Naphthalene 551 25 5.0 ug/l 103-65-1 n-Propylbenzene 87.4 25 5.0 ug/l 100-42-5 Styrene ND 25 5.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 25 5.0 ug/l 71-55-6 1,1,1-Trichloroethane ND 25 5.0 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 25 5.0 ug/l 79-00-5 1,1,2-Trichloroethane ND 25 5.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 25 5.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 25 5.9 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 25 5.0 ug/l 95-63-6 1,2,4-Trimethylbenzene 66.4 25 5.0 ug/l 108-67-8 1,3,5-Trimethylbenzene 8.4 25 5.0 ug/l J 127-18-4 Tetrachloroethylene ND 25 5.0 ug/l 108-88-3 Toluene 1180 25 5.0 ug/l 79-01-6 Trichloroethylene ND 25 5.0 ug/l 75-69-4 Trichlorofluoromethane ND 25 5.0 ug/l 75-01-4 Vinyl chloride ND 25 5.0 ug/l 108-05-4 Vinyl Acetate a ND 250 8.8 ug/l 1330-20-7 Xylene (total)644 75 10 ug/l m,p-Xylene 483 50 5.0 ug/l 95-47-6 o-Xylene 161 25 5.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 105%70-130% 17060-07-0 1,2-Dichloroethane-D4 109%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 96 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 97 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:EPA 625 EPA 625 Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X035118.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 Run #2 X035157.D 8 06/06/14 MV 06/02/14 OP51824 SX1646 Initial Volume Final Volume Run #1 1050 ml 1.0 ml Run #2 1050 ml 1.0 ml ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.5 ug/l 95-57-8 2-Chlorophenol ND 4.8 0.49 ug/l 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.48 ug/l 120-83-2 2,4-Dichlorophenol ND 4.8 0.55 ug/l 105-67-9 2,4-Dimethylphenol 0.78 4.8 0.48 ug/l J 51-28-5 2,4-Dinitrophenol ND 24 5.2 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l 95-48-7 2-Methylphenol ND 4.8 0.48 ug/l 3&4-Methylphenol ND 4.8 1.1 ug/l 88-75-5 2-Nitrophenol ND 4.8 0.57 ug/l 100-02-7 4-Nitrophenol ND 24 4.8 ug/l 87-86-5 Pentachlorophenol ND 24 4.8 ug/l 108-95-2 Phenol ND 4.8 0.48 ug/l 88-06-2 2,4,6-Trichlorophenol ND 4.8 0.53 ug/l 83-32-9 Acenaphthene 0.54 4.8 0.48 ug/l J 208-96-8 Acenaphthylene ND 4.8 0.48 ug/l 120-12-7 Anthracene ND 4.8 0.59 ug/l 56-55-3 Benzo(a)anthracene ND 4.8 0.61 ug/l 50-32-8 Benzo(a)pyrene ND 4.8 0.62 ug/l 205-99-2 Benzo(b)fluoranthene ND 4.8 0.68 ug/l 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.77 ug/l 207-08-9 Benzo(k)fluoranthene ND 4.8 0.49 ug/l 101-55-3 4-Bromophenyl phenyl ether ND 4.8 0.64 ug/l 85-68-7 Butyl benzyl phthalate ND 4.8 0.77 ug/l 100-51-6 Benzyl Alcohol ND 4.8 0.95 ug/l 91-58-7 2-Chloronaphthalene ND 4.8 0.53 ug/l 106-47-8 4-Chloroaniline ND 4.8 0.48 ug/l 218-01-9 Chrysene ND 4.8 0.69 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.52 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.66 ug/l 108-60-1 bis(2-Chloroisopropyl)ether ND 4.8 0.55 ug/l 7005-72-3 4-Chlorophenyl phenyl ether ND 4.8 0.51 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 98 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:EPA 625 EPA 625 Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.64 ug/l 541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l 106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.86 ug/l 53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l 132-64-9 Dibenzofuran 1.0 4.8 0.51 ug/l J 84-74-2 Di-n-butyl phthalate ND 4.8 0.95 ug/l 117-84-0 Di-n-octyl phthalate ND 4.8 0.95 ug/l 84-66-2 Diethyl phthalate ND 4.8 0.95 ug/l 131-11-3 Dimethyl phthalate ND 4.8 0.60 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate 566 a 38 12 ug/l 206-44-0 Fluoranthene ND 4.8 0.67 ug/l 86-73-7 Fluorene 1.3 4.8 0.48 ug/l J 118-74-1 Hexachlorobenzene ND 4.8 0.63 ug/l 87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l 77-47-4 Hexachlorocyclopentadiene ND 4.8 0.95 ug/l 67-72-1 Hexachloroethane ND 4.8 0.48 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.60 ug/l 78-59-1 Isophorone ND 4.8 0.48 ug/l 90-12-0 1-Methylnaphthalene 90.4 4.8 0.48 ug/l 91-57-6 2-Methylnaphthalene 155 a 38 4.1 ug/l 91-20-3 Naphthalene 470 a 38 3.8 ug/l 98-95-3 Nitrobenzene ND 4.8 0.48 ug/l 621-64-7 N-Nitroso-di-n-propylamine ND 4.8 0.48 ug/l 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.51 ug/l 85-01-8 Phenanthrene ND 4.8 0.57 ug/l 129-00-0 Pyrene ND 4.8 0.78 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 4.8 0.48 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 42%40%14-67% 4165-62-2 Phenol-d5 27%26%10-50% 118-79-6 2,4,6-Tribromophenol 93%86%33-118% 4165-60-0 Nitrobenzene-d5 85%78%42-108% 321-60-8 2-Fluorobiphenyl 85%85%40-106% 1718-51-0 Terphenyl-d14 90%87%39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 99 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:EPA 625 EPA 625 Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC ABN List for NC, May 2012 CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q 590-36-3 2-Pentanol, 2-methyl-1.88 56 ug/l JN 77-74-7 3-Pentanol, 3-methyl-1.98 50 ug/l JN 108-88-3 Toluene 2.07 180 ug/l JN 1462-03-9 Cyclopentanol, 1-methyl-2.18 65 ug/l JN 19550-46-0 1,3-Dimethyl cyclopentanol 2.43 65 ug/l JN 100-41-4 Ethylbenzene 2.55 170 ug/l JN 106-42-3 p-Xylene 2.71 72 ug/l JN 108-67-8 Benzene, 1,3,5-trimethyl-3.21 46 ug/l JN 496-11-7 Indane 3.44 140 ug/l JN 141-93-5 Benzene, 1,3-diethyl-3.48 68 ug/l JN Total TIC, Semi-Volatile 912 ug/l J (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 100 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:MADEP VPH REV 1.1 Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UV064384.D 10 06/03/14 MM n/a n/a GUV3417 Run #2 Purge Volume Run #1 5.0 ml Run #2 MADEP VPH List CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)6370 1000 350 ug/l C9- C12 Aliphatics (Unadj.)1930 1000 350 ug/l C9- C10 Aromatics (Unadj.)1930 1000 350 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 106%70-130% 460-00-4 BFB 106%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 101 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 1 Client Sample ID:MW 1 Lab Sample ID:FA15409-24 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:MADEP EPH REV 1.1 SW846 3510C Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN009066.D 1 06/06/14 NAF 06/02/14 OP51822 GNN397 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 MAEPH List CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)1860 190 140 ug/l C9-C18 Aliphatics 1200 190 96 ug/l C19-C36 Aliphatics ND 190 96 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 77%40-140% 580-13-2 2-Bromonaphthalene 92%40-140% 84-15-1 o-Terphenyl 76%40-140% 321-60-8 2-Fluorobiphenyl 88%40-140% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 102 of 208 FA15409 33.24 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:MW 4 Lab Sample ID:FA15409-25 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0187272.D 50 06/06/14 TD n/a n/a VA1478 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 500 50 ug/l 71-43-2 Benzene 395 25 5.0 ug/l 108-86-1 Bromobenzene ND 25 5.0 ug/l 74-97-5 Bromochloromethane ND 25 5.0 ug/l 75-27-4 Bromodichloromethane ND 25 5.0 ug/l 75-25-2 Bromoform ND 25 5.0 ug/l 104-51-8 n-Butylbenzene 11.0 25 5.0 ug/l J 135-98-8 sec-Butylbenzene 12.6 25 5.0 ug/l J 98-06-6 tert-Butylbenzene ND 25 5.0 ug/l 108-90-7 Chlorobenzene ND 25 5.0 ug/l 75-00-3 Chloroethane ND 25 6.1 ug/l 67-66-3 Chloroform ND 25 5.0 ug/l 95-49-8 o-Chlorotoluene ND 25 5.0 ug/l 106-43-4 p-Chlorotoluene ND 25 5.0 ug/l 56-23-5 Carbon tetrachloride ND 25 5.0 ug/l 75-34-3 1,1-Dichloroethane ND 25 5.0 ug/l 75-35-4 1,1-Dichloroethylene ND 25 5.0 ug/l 563-58-6 1,1-Dichloropropene ND 25 5.0 ug/l 106-93-4 1,2-Dibromoethane ND 25 5.0 ug/l 107-06-2 1,2-Dichloroethane ND 25 5.0 ug/l 78-87-5 1,2-Dichloropropane ND 25 5.0 ug/l 142-28-9 1,3-Dichloropropane ND 25 5.0 ug/l 108-20-3 Di-Isopropyl ether ND 25 5.0 ug/l 594-20-7 2,2-Dichloropropane ND 25 5.0 ug/l 124-48-1 Dibromochloromethane ND 25 5.0 ug/l 75-71-8 Dichlorodifluoromethane ND 25 5.0 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 25 5.0 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 25 5.0 ug/l 541-73-1 m-Dichlorobenzene ND 25 5.0 ug/l 95-50-1 o-Dichlorobenzene ND 25 5.0 ug/l 106-46-7 p-Dichlorobenzene ND 25 5.0 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 25 5.0 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 103 of 208 FA15409 33.25 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:MW 4 Lab Sample ID:FA15409-25 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 25 5.0 ug/l 100-41-4 Ethylbenzene 1160 25 5.0 ug/l 64-17-5 Ethyl Alcohol ND 5000 1300 ug/l 591-78-6 2-Hexanone ND 250 25 ug/l 98-82-8 Isopropylbenzene 129 25 5.0 ug/l 99-87-6 p-Isopropyltoluene 19.3 25 5.0 ug/l J 108-10-1 4-Methyl-2-pentanone ND 130 25 ug/l 74-83-9 Methyl bromide ND 25 5.0 ug/l 74-87-3 Methyl chloride ND 25 5.0 ug/l 75-09-2 Methylene chloride ND 100 50 ug/l 78-93-3 Methyl ethyl ketone ND 130 34 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 25 5.0 ug/l 91-20-3 Naphthalene 401 25 5.0 ug/l 103-65-1 n-Propylbenzene 268 25 5.0 ug/l 100-42-5 Styrene 7.3 25 5.0 ug/l J 630-20-6 1,1,1,2-Tetrachloroethane ND 25 5.0 ug/l 71-55-6 1,1,1-Trichloroethane ND 25 5.0 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 25 5.0 ug/l 79-00-5 1,1,2-Trichloroethane ND 25 5.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 25 5.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 25 5.9 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 25 5.0 ug/l 95-63-6 1,2,4-Trimethylbenzene 2070 25 5.0 ug/l 108-67-8 1,3,5-Trimethylbenzene 665 25 5.0 ug/l 127-18-4 Tetrachloroethylene ND 25 5.0 ug/l 108-88-3 Toluene 665 25 5.0 ug/l 79-01-6 Trichloroethylene ND 25 5.0 ug/l 75-69-4 Trichlorofluoromethane ND 25 5.0 ug/l 75-01-4 Vinyl chloride ND 25 5.0 ug/l 108-05-4 Vinyl Acetate a ND 250 8.8 ug/l 1330-20-7 Xylene (total)5110 75 10 ug/l m,p-Xylene 2690 50 5.0 ug/l 95-47-6 o-Xylene 2410 25 5.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 106%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 104 of 208 FA15409 33.25 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:MW 4 Lab Sample ID:FA15409-25 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 105 of 208 FA15409 33.25 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:MW 5 Lab Sample ID:FA15409-26 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0187273.D 20 06/06/14 TD n/a n/a VA1478 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 200 20 ug/l 71-43-2 Benzene 53.9 10 2.0 ug/l 108-86-1 Bromobenzene ND 10 2.0 ug/l 74-97-5 Bromochloromethane ND 10 2.0 ug/l 75-27-4 Bromodichloromethane ND 10 2.0 ug/l 75-25-2 Bromoform ND 10 2.0 ug/l 104-51-8 n-Butylbenzene 8.0 10 2.0 ug/l J 135-98-8 sec-Butylbenzene 13.4 10 2.0 ug/l 98-06-6 tert-Butylbenzene ND 10 2.0 ug/l 108-90-7 Chlorobenzene ND 10 2.0 ug/l 75-00-3 Chloroethane ND 10 2.4 ug/l 67-66-3 Chloroform ND 10 2.0 ug/l 95-49-8 o-Chlorotoluene ND 10 2.0 ug/l 106-43-4 p-Chlorotoluene ND 10 2.0 ug/l 56-23-5 Carbon tetrachloride ND 10 2.0 ug/l 75-34-3 1,1-Dichloroethane ND 10 2.0 ug/l 75-35-4 1,1-Dichloroethylene ND 10 2.0 ug/l 563-58-6 1,1-Dichloropropene ND 10 2.0 ug/l 106-93-4 1,2-Dibromoethane ND 10 2.0 ug/l 107-06-2 1,2-Dichloroethane ND 10 2.0 ug/l 78-87-5 1,2-Dichloropropane ND 10 2.0 ug/l 142-28-9 1,3-Dichloropropane ND 10 2.0 ug/l 108-20-3 Di-Isopropyl ether ND 10 2.0 ug/l 594-20-7 2,2-Dichloropropane ND 10 2.0 ug/l 124-48-1 Dibromochloromethane ND 10 2.0 ug/l 75-71-8 Dichlorodifluoromethane ND 10 2.0 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 10 2.0 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 10 2.0 ug/l 541-73-1 m-Dichlorobenzene ND 10 2.0 ug/l 95-50-1 o-Dichlorobenzene ND 10 2.0 ug/l 106-46-7 p-Dichlorobenzene ND 10 2.0 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 10 2.0 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 106 of 208 FA15409 33.26 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:MW 5 Lab Sample ID:FA15409-26 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 10 2.0 ug/l 100-41-4 Ethylbenzene 786 10 2.0 ug/l 64-17-5 Ethyl Alcohol ND 2000 520 ug/l 591-78-6 2-Hexanone ND 100 10 ug/l 98-82-8 Isopropylbenzene 109 10 2.0 ug/l 99-87-6 p-Isopropyltoluene 8.5 10 2.0 ug/l J 108-10-1 4-Methyl-2-pentanone ND 50 10 ug/l 74-83-9 Methyl bromide ND 10 2.0 ug/l 74-87-3 Methyl chloride ND 10 2.0 ug/l 75-09-2 Methylene chloride ND 40 20 ug/l 78-93-3 Methyl ethyl ketone ND 50 14 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 10 2.0 ug/l 91-20-3 Naphthalene 308 10 2.0 ug/l 103-65-1 n-Propylbenzene 199 10 2.0 ug/l 100-42-5 Styrene ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.0 ug/l 71-55-6 1,1,1-Trichloroethane ND 10 2.0 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.0 ug/l 79-00-5 1,1,2-Trichloroethane ND 10 2.1 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 10 2.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 10 2.4 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 10 2.0 ug/l 95-63-6 1,2,4-Trimethylbenzene 233 10 2.0 ug/l 108-67-8 1,3,5-Trimethylbenzene 37.4 10 2.0 ug/l 127-18-4 Tetrachloroethylene ND 10 2.0 ug/l 108-88-3 Toluene 16.2 10 2.0 ug/l 79-01-6 Trichloroethylene ND 10 2.0 ug/l 75-69-4 Trichlorofluoromethane ND 10 2.0 ug/l 75-01-4 Vinyl chloride ND 10 2.0 ug/l 108-05-4 Vinyl Acetate a ND 100 3.5 ug/l 1330-20-7 Xylene (total)382 30 4.0 ug/l m,p-Xylene 345 20 2.0 ug/l 95-47-6 o-Xylene 36.6 10 2.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 107 of 208 FA15409 33.26 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:MW 5 Lab Sample ID:FA15409-26 Date Sampled:05/29/14 Matrix:AQ - Ground Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 108 of 208 FA15409 33.26 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 1 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-27 Date Sampled:05/28/14 Matrix:AQ - Trip Blank Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0187269.D 1 06/06/14 TD n/a n/a VA1478 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone 2.4 10 1.0 ug/l J 71-43-2 Benzene ND 0.50 0.10 ug/l 108-86-1 Bromobenzene ND 0.50 0.10 ug/l 74-97-5 Bromochloromethane ND 0.50 0.10 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l 75-25-2 Bromoform ND 0.50 0.10 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l 108-90-7 Chlorobenzene ND 0.50 0.10 ug/l 75-00-3 Chloroethane ND 0.50 0.12 ug/l 67-66-3 Chloroform ND 0.50 0.10 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l 56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l 108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l 541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l 95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l 106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 109 of 208 FA15409 33.27 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 2 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-27 Date Sampled:05/28/14 Matrix:AQ - Trip Blank Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l 100-41-4 Ethylbenzene ND 0.50 0.10 ug/l 64-17-5 Ethyl Alcohol ND 100 26 ug/l 591-78-6 2-Hexanone ND 5.0 0.50 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l 108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l 74-83-9 Methyl bromide ND 0.50 0.10 ug/l 74-87-3 Methyl chloride ND 0.50 0.10 ug/l 75-09-2 Methylene chloride ND 2.0 1.0 ug/l 78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l 91-20-3 Naphthalene ND 0.50 0.10 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l 100-42-5 Styrene ND 0.50 0.10 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l 108-88-3 Toluene ND 0.50 0.10 ug/l 79-01-6 Trichloroethylene ND 0.50 0.10 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l 75-01-4 Vinyl chloride ND 0.50 0.10 ug/l 108-05-4 Vinyl Acetate a ND 5.0 0.18 ug/l 1330-20-7 Xylene (total)ND 1.5 0.20 ug/l m,p-Xylene ND 1.0 0.10 ug/l 95-47-6 o-Xylene ND 0.50 0.10 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 110 of 208 FA15409 33.27 Accutest LabLink@151826 11:13 17-Jun-2014 Report of Analysis Page 3 of 3 Client Sample ID:TRIP BLANK Lab Sample ID:FA15409-27 Date Sampled:05/28/14 Matrix:AQ - Trip Blank Water Date Received:05/30/14 Method:SM 6200B Percent Solids:n/a Project:Quality Mart 7; Winston-Salem, NC VOA List for NC, May 2012 CAS No.Compound Result RL MDL Units Q (a) Associated BS recovery outside control limits. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 111 of 208 FA15409 33.27 Accutest LabLink@151826 11:13 17-Jun-2014 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Southeast Section 4 112 of 208 FA15409 4 FA15409: Chain of Custody Page 1 of 4 113 of 208 FA15409 44.1 FA15409: Chain of Custody Page 2 of 4 114 of 208 FA15409 44.1 FA15409: Chain of Custody Page 3 of 4 115 of 208 FA15409 44.1 FA15409: Chain of Custody Page 4 of 4 116 of 208 FA15409 44.1 Accutest LabLink@151826 11:13 17-Jun-2014 GC/MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Southeast Section 5 117 of 208 FA15409 5 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-MB A0187268.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 10 1.0 ug/l 71-43-2 Benzene ND 0.50 0.10 ug/l 108-86-1 Bromobenzene ND 0.50 0.10 ug/l 74-97-5 Bromochloromethane ND 0.50 0.10 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l 75-25-2 Bromoform ND 0.50 0.10 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l 108-90-7 Chlorobenzene ND 0.50 0.10 ug/l 75-00-3 Chloroethane ND 0.50 0.12 ug/l 67-66-3 Chloroform ND 0.50 0.10 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l 56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l 108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l 541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l 95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l 106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l 100-41-4 Ethylbenzene ND 0.50 0.10 ug/l 64-17-5 Ethyl Alcohol ND 100 26 ug/l 591-78-6 2-Hexanone ND 5.0 0.50 ug/l 118 of 208 FA15409 55.1.1 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-MB A0187268.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 CAS No.Compound Result RL MDL Units Q 98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l 108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l 74-83-9 Methyl bromide ND 0.50 0.10 ug/l 74-87-3 Methyl chloride ND 0.50 0.10 ug/l 75-09-2 Methylene chloride ND 2.0 1.0 ug/l 78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l 91-20-3 Naphthalene ND 0.50 0.10 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l 100-42-5 Styrene ND 0.50 0.10 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l 108-88-3 Toluene ND 0.50 0.10 ug/l 79-01-6 Trichloroethylene ND 0.50 0.10 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l 75-01-4 Vinyl chloride ND 0.50 0.10 ug/l 108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l 1330-20-7 Xylene (total)ND 1.5 0.20 ug/l m,p-Xylene ND 1.0 0.10 ug/l 95-47-6 o-Xylene ND 0.50 0.10 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%70-130% 2037-26-5 Toluene-D8 101%70-130% 119 of 208 FA15409 55.1.1 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-MB A0187268.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 103%70-130% 120 of 208 FA15409 55.1.1 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1043-MB E031067.D 1 06/06/14 TD n/a n/a VE1043 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23 CAS No.Compound Result RL MDL Units Q 1330-20-7 Xylene (total)ND 1.5 0.20 ug/l m,p-Xylene ND 1.0 0.10 ug/l 95-47-6 o-Xylene ND 0.50 0.10 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 92%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% 121 of 208 FA15409 55.1.2 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-MB C098546.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 15 ug/kg 71-43-2 Benzene ND 5.0 1.0 ug/kg 108-86-1 Bromobenzene ND 5.0 1.1 ug/kg 74-97-5 Bromochloromethane ND 5.0 1.9 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform ND 5.0 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg 98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.3 ug/kg 67-66-3 Chloroform ND 5.0 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg 56-23-5 Carbon tetrachloride ND 5.0 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 5.0 1.1 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg 108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 5.0 1.4 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 5.0 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg 64-17-5 Ethyl alcohol ND 400 67 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 591-78-6 2-Hexanone ND 25 4.9 ug/kg 122 of 208 FA15409 55.1.3 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-MB C098546.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 CAS No.Compound Result RL MDL Units Q 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg 108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg 74-83-9 Methyl bromide ND 5.0 1.9 ug/kg 74-87-3 Methyl chloride ND 5.0 2.0 ug/kg 75-09-2 Methylene chloride ND 10 4.0 ug/kg 78-93-3 Methyl ethyl ketone ND 25 7.5 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 5.0 1.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.2 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 1.9 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 108-05-4 Vinyl Acetate ND 25 8.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.7 ug/kg m,p-Xylene ND 10 1.6 ug/kg 95-47-6 o-Xylene ND 5.0 1.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 108%75-124% 2037-26-5 Toluene-D8 100%75-126% 460-00-4 4-Bromofluorobenzene 101%71-133% 123 of 208 FA15409 55.1.3 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-MB C098546.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 CAS No.Surrogate Recoveries Limits 17060-07-0 1,2-Dichloroethane-D4 106%72-135% 124 of 208 FA15409 55.1.3 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-MB F0064639.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 15 ug/kg 71-43-2 Benzene ND 5.0 1.0 ug/kg 108-86-1 Bromobenzene ND 5.0 1.1 ug/kg 74-97-5 Bromochloromethane ND 5.0 1.9 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform ND 5.0 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg 98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.3 ug/kg 67-66-3 Chloroform ND 5.0 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg 56-23-5 Carbon tetrachloride ND 5.0 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 5.0 1.1 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg 108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 5.0 1.4 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 5.0 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg 64-17-5 Ethyl alcohol ND 400 67 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 591-78-6 2-Hexanone ND 25 4.9 ug/kg 125 of 208 FA15409 55.1.4 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-MB F0064639.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 CAS No.Compound Result RL MDL Units Q 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg 108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg 74-83-9 Methyl bromide ND 5.0 1.9 ug/kg 74-87-3 Methyl chloride ND 5.0 2.0 ug/kg 75-09-2 Methylene chloride 4.9 10 4.0 ug/kg J 78-93-3 Methyl ethyl ketone ND 25 7.5 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 5.0 1.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.2 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 1.9 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 108-05-4 Vinyl Acetate ND 25 8.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.7 ug/kg m,p-Xylene ND 10 1.6 ug/kg 95-47-6 o-Xylene ND 5.0 1.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 92%75-124% 2037-26-5 Toluene-D8 93%75-126% 460-00-4 4-Bromofluorobenzene 107%71-133% 126 of 208 FA15409 55.1.4 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-MB F0064639.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 CAS No.Surrogate Recoveries Limits 17060-07-0 1,2-Dichloroethane-D4 92%72-135% 127 of 208 FA15409 55.1.4 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-MB F0064661.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 15 ug/kg 71-43-2 Benzene ND 5.0 1.0 ug/kg 108-86-1 Bromobenzene ND 5.0 1.1 ug/kg 74-97-5 Bromochloromethane ND 5.0 1.9 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform ND 5.0 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg 98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.3 ug/kg 67-66-3 Chloroform ND 5.0 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg 56-23-5 Carbon tetrachloride ND 5.0 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 5.0 1.1 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg 108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 5.0 1.4 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 5.0 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg 64-17-5 Ethyl alcohol ND 400 67 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 591-78-6 2-Hexanone ND 25 4.9 ug/kg 128 of 208 FA15409 55.1.5 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-MB F0064661.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 CAS No.Compound Result RL MDL Units Q 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg 108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg 74-83-9 Methyl bromide ND 5.0 1.9 ug/kg 74-87-3 Methyl chloride ND 5.0 2.0 ug/kg 75-09-2 Methylene chloride 6.1 10 4.0 ug/kg J 78-93-3 Methyl ethyl ketone ND 25 7.5 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 5.0 1.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.2 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 1.9 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 108-05-4 Vinyl Acetate ND 25 8.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.7 ug/kg m,p-Xylene ND 10 1.6 ug/kg 95-47-6 o-Xylene ND 5.0 1.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 90%75-124% 2037-26-5 Toluene-D8 91%75-126% 460-00-4 4-Bromofluorobenzene 102%71-133% 129 of 208 FA15409 55.1.5 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-MB F0064661.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 CAS No.Surrogate Recoveries Limits 17060-07-0 1,2-Dichloroethane-D4 88%72-135% 130 of 208 FA15409 55.1.5 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2137-MB F0064689.D 1 06/03/14 AH n/a n/a VF2137 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-9 CAS No.Compound Result RL MDL Units Q 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.7 ug/kg m,p-Xylene ND 10 1.6 ug/kg 95-47-6 o-Xylene ND 5.0 1.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 88%75-124% 2037-26-5 Toluene-D8 93%75-126% 460-00-4 4-Bromofluorobenzene 104%71-133% 17060-07-0 1,2-Dichloroethane-D4 86%72-135% 131 of 208 FA15409 55.1.6 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-MB F0064701.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 CAS No.Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 15 ug/kg 71-43-2 Benzene ND 5.0 1.0 ug/kg 108-86-1 Bromobenzene ND 5.0 1.1 ug/kg 74-97-5 Bromochloromethane ND 5.0 1.9 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform ND 5.0 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg 98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.3 ug/kg 67-66-3 Chloroform ND 5.0 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg 56-23-5 Carbon tetrachloride ND 5.0 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 5.0 1.1 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg 108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 5.0 1.4 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 5.0 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg 64-17-5 Ethyl alcohol ND 400 67 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 591-78-6 2-Hexanone ND 25 4.9 ug/kg 132 of 208 FA15409 55.1.7 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-MB F0064701.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 CAS No.Compound Result RL MDL Units Q 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg 108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg 74-83-9 Methyl bromide ND 5.0 1.9 ug/kg 74-87-3 Methyl chloride ND 5.0 2.0 ug/kg 75-09-2 Methylene chloride ND 10 4.0 ug/kg 78-93-3 Methyl ethyl ketone ND 25 7.5 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 5.0 1.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.2 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 1.9 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 108-05-4 Vinyl Acetate ND 25 8.0 ug/kg 1330-20-7 Xylene (total)ND 15 2.7 ug/kg m,p-Xylene ND 10 1.6 ug/kg 95-47-6 o-Xylene ND 5.0 1.1 ug/kg CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 92%75-124% 2037-26-5 Toluene-D8 89%75-126% 460-00-4 4-Bromofluorobenzene 105%71-133% 133 of 208 FA15409 55.1.7 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-MB F0064701.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 CAS No.Surrogate Recoveries Limits 17060-07-0 1,2-Dichloroethane-D4 85%72-135% 134 of 208 FA15409 55.1.7 Blank Spike Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-BS A0187266.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 67-64-1 Acetone 50 60.3 121 70-130 71-43-2 Benzene 10 11.7 117 70-130 108-86-1 Bromobenzene 10 12.4 124 70-130 74-97-5 Bromochloromethane 10 12.5 125 70-130 75-27-4 Bromodichloromethane 10 10.7 107 70-130 75-25-2 Bromoform 10 10.3 103 70-130 104-51-8 n-Butylbenzene 10 11.4 114 70-130 135-98-8 sec-Butylbenzene 10 12.7 127 70-130 98-06-6 tert-Butylbenzene 10 12.1 121 70-130 108-90-7 Chlorobenzene 10 12.5 125 70-130 75-00-3 Chloroethane 10 10.2 102 60-140 67-66-3 Chloroform 10 12.1 121 70-130 95-49-8 o-Chlorotoluene 10 12.3 123 70-130 106-43-4 p-Chlorotoluene 10 12.6 126 70-130 56-23-5 Carbon tetrachloride 10 11.2 112 70-130 75-34-3 1,1-Dichloroethane 10 12.5 125 70-130 75-35-4 1,1-Dichloroethylene 10 11.7 117 70-130 563-58-6 1,1-Dichloropropene 10 11.8 118 70-130 106-93-4 1,2-Dibromoethane 10 12.4 124 70-130 107-06-2 1,2-Dichloroethane 10 11.9 119 70-130 78-87-5 1,2-Dichloropropane 10 12.3 123 70-130 142-28-9 1,3-Dichloropropane 10 12.3 123 70-130 108-20-3 Di-Isopropyl ether 10 11.3 113 70-130 594-20-7 2,2-Dichloropropane 10 12.7 127 70-130 124-48-1 Dibromochloromethane 10 12.2 122 70-130 75-71-8 Dichlorodifluoromethane 10 8.9 89 60-140 156-59-2 cis-1,2-Dichloroethylene 10 12.7 127 70-130 10061-01-5 cis-1,3-Dichloropropene 10 10.7 107 70-130 541-73-1 m-Dichlorobenzene 10 12.8 128 70-130 95-50-1 o-Dichlorobenzene 10 12.5 125 70-130 106-46-7 p-Dichlorobenzene 10 11.7 117 70-130 156-60-5 trans-1,2-Dichloroethylene 10 11.5 115 70-130 10061-02-6 trans-1,3-Dichloropropene 10 12.9 129 70-130 100-41-4 Ethylbenzene 10 12.5 125 70-130 64-17-5 Ethyl Alcohol 500 409 82 70-130 591-78-6 2-Hexanone 50 59.8 120 70-130 * = Outside of Control Limits. 135 of 208 FA15409 55.2.1 Blank Spike Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-BS A0187266.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 98-82-8 Isopropylbenzene 10 12.5 125 70-130 99-87-6 p-Isopropyltoluene 10 12.4 124 70-130 108-10-1 4-Methyl-2-pentanone 50 64.8 130 70-130 74-83-9 Methyl bromide 10 9.7 97 60-140 74-87-3 Methyl chloride 10 10 100 60-140 75-09-2 Methylene chloride 10 11.4 114 70-130 78-93-3 Methyl ethyl ketone 50 56.9 114 70-130 1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130 91-20-3 Naphthalene 10 10.9 109 70-130 103-65-1 n-Propylbenzene 10 12.7 127 70-130 100-42-5 Styrene 10 11.2 112 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 12.4 124 70-130 71-55-6 1,1,1-Trichloroethane 10 11.1 111 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 12.0 120 70-130 79-00-5 1,1,2-Trichloroethane 10 12.1 121 70-130 87-61-6 1,2,3-Trichlorobenzene 10 12.5 125 70-130 96-18-4 1,2,3-Trichloropropane 10 11.6 116 70-130 120-82-1 1,2,4-Trichlorobenzene 10 12.4 124 70-130 95-63-6 1,2,4-Trimethylbenzene 10 11.4 114 70-130 108-67-8 1,3,5-Trimethylbenzene 10 11.4 114 70-130 127-18-4 Tetrachloroethylene 10 12.6 126 70-130 108-88-3 Toluene 10 12.6 126 70-130 79-01-6 Trichloroethylene 10 12.4 124 70-130 75-69-4 Trichlorofluoromethane 10 9.0 90 60-140 75-01-4 Vinyl chloride 10 9.5 95 60-140 108-05-4 Vinyl Acetate 50 75.9 152*70-130 1330-20-7 Xylene (total)30 35.4 118 70-130 m,p-Xylene 20 23.8 119 70-130 95-47-6 o-Xylene 10 11.6 116 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%70-130% 2037-26-5 Toluene-D8 102%70-130% * = Outside of Control Limits. 136 of 208 FA15409 55.2.1 Blank Spike Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1478-BS A0187266.D 1 06/06/14 TD n/a n/a VA1478 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23, FA15409-24, FA15409-25, FA15409-26, FA15409-27 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 99%70-130% * = Outside of Control Limits. 137 of 208 FA15409 55.2.1 Blank Spike Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1043-BS E031065.D 1 06/06/14 TD n/a n/a VE1043 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 1330-20-7 Xylene (total)30 36.5 122 70-130 m,p-Xylene 20 23.8 119 70-130 95-47-6 o-Xylene 10 12.6 126 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 94%70-130% 17060-07-0 1,2-Dichloroethane-D4 85%70-130% 2037-26-5 Toluene-D8 103%70-130% 460-00-4 4-Bromofluorobenzene 104%70-130% * = Outside of Control Limits. 138 of 208 FA15409 55.2.2 Blank Spike Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-BS C098545.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 67-64-1 Acetone 250 306 122 61-152 71-43-2 Benzene 50 53.3 107 76-126 108-86-1 Bromobenzene 50 53.2 106 76-122 74-97-5 Bromochloromethane 50 51.9 104 77-120 75-27-4 Bromodichloromethane 50 55.2 110 74-130 75-25-2 Bromoform 50 57.0 114 76-127 104-51-8 n-Butylbenzene 50 53.7 107 71-128 135-98-8 sec-Butylbenzene 50 59.5 119 79-135 98-06-6 tert-Butylbenzene 50 62.4 125 77-133 108-90-7 Chlorobenzene 50 56.5 113 81-129 75-00-3 Chloroethane 50 60.5 121 68-133 67-66-3 Chloroform 50 49.5 99 72-123 95-49-8 o-Chlorotoluene 50 57.5 115 77-129 106-43-4 p-Chlorotoluene 50 58.2 116 80-134 56-23-5 Carbon tetrachloride 50 52.5 105 78-133 75-34-3 1,1-Dichloroethane 50 49.5 99 73-125 75-35-4 1,1-Dichloroethylene 50 56.3 113 81-136 563-58-6 1,1-Dichloropropene 50 56.4 113 75-130 106-93-4 1,2-Dibromoethane 50 55.8 112 77-126 107-06-2 1,2-Dichloroethane 50 57.8 116 74-128 78-87-5 1,2-Dichloropropane 50 55.1 110 74-125 142-28-9 1,3-Dichloropropane 50 55.6 111 76-122 108-20-3 Di-Isopropyl ether 50 52.1 104 75-122 594-20-7 2,2-Dichloropropane 50 63.7 127 77-133 124-48-1 Dibromochloromethane 50 56.5 113 76-127 75-71-8 Dichlorodifluoromethane 50 63.7 127 68-168 156-59-2 cis-1,2-Dichloroethylene 50 53.7 107 74-126 10061-01-5 cis-1,3-Dichloropropene 50 54.8 110 80-123 541-73-1 m-Dichlorobenzene 50 57.9 116 81-129 95-50-1 o-Dichlorobenzene 50 58.6 117 80-129 106-46-7 p-Dichlorobenzene 50 52.6 105 76-130 156-60-5 trans-1,2-Dichloroethylene 50 52.9 106 70-127 10061-02-6 trans-1,3-Dichloropropene 50 55.5 111 75-131 64-17-5 Ethyl alcohol 1000 1020 102 53-154 100-41-4 Ethylbenzene 50 52.9 106 77-123 591-78-6 2-Hexanone 250 299 120 72-133 * = Outside of Control Limits. 139 of 208 FA15409 55.2.3 Blank Spike Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-BS C098545.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 98-82-8 Isopropylbenzene 50 56.4 113 80-136 99-87-6 p-Isopropyltoluene 50 59.3 119 77-131 108-10-1 4-Methyl-2-pentanone 250 296 118 76-132 74-83-9 Methyl bromide 50 62.3 125 65-139 74-87-3 Methyl chloride 50 59.9 120 71-144 75-09-2 Methylene chloride 50 63.0 126 74-137 78-93-3 Methyl ethyl ketone 250 278 111 75-137 1634-04-4 Methyl Tert Butyl Ether 50 52.4 105 77-120 91-20-3 Naphthalene 50 55.9 112 79-129 103-65-1 n-Propylbenzene 50 58.9 118 80-135 100-42-5 Styrene 50 55.6 111 78-125 630-20-6 1,1,1,2-Tetrachloroethane 50 56.4 113 78-126 71-55-6 1,1,1-Trichloroethane 50 55.9 112 70-129 79-34-5 1,1,2,2-Tetrachloroethane 50 54.5 109 71-126 79-00-5 1,1,2-Trichloroethane 50 55.1 110 74-124 87-61-6 1,2,3-Trichlorobenzene 50 54.7 109 77-128 96-18-4 1,2,3-Trichloropropane 50 58.4 117 74-127 120-82-1 1,2,4-Trichlorobenzene 50 55.3 111 78-130 95-63-6 1,2,4-Trimethylbenzene 50 55.1 110 74-123 108-67-8 1,3,5-Trimethylbenzene 50 53.9 108 73-122 127-18-4 Tetrachloroethylene 50 53.1 106 79-130 108-88-3 Toluene 50 53.5 107 76-124 79-01-6 Trichloroethylene 50 53.8 108 75-128 75-69-4 Trichlorofluoromethane 50 57.5 115 73-145 75-01-4 Vinyl chloride 50 52.6 105 76-141 108-05-4 Vinyl Acetate 250 227 91 48-164 1330-20-7 Xylene (total)150 162 108 80-129 m,p-Xylene 100 107 107 80-128 95-47-6 o-Xylene 50 55.8 112 80-132 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 98%75-124% 2037-26-5 Toluene-D8 101%75-126% 460-00-4 4-Bromofluorobenzene 100%71-133% * = Outside of Control Limits. 140 of 208 FA15409 55.2.3 Blank Spike Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VC3954-BS C098545.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 CAS No.Surrogate Recoveries BSP Limits 17060-07-0 1,2-Dichloroethane-D4 100%72-135% * = Outside of Control Limits. 141 of 208 FA15409 55.2.3 Blank Spike Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-BS F0064638.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 67-64-1 Acetone 250 233 93 61-152 71-43-2 Benzene 50 51.1 102 76-126 108-86-1 Bromobenzene 50 49.3 99 76-122 74-97-5 Bromochloromethane 50 52.8 106 77-120 75-27-4 Bromodichloromethane 50 54.3 109 74-130 75-25-2 Bromoform 50 46.5 93 76-127 104-51-8 n-Butylbenzene 50 50.9 102 71-128 135-98-8 sec-Butylbenzene 50 47.0 94 79-135 98-06-6 tert-Butylbenzene 50 47.4 95 77-133 108-90-7 Chlorobenzene 50 49.5 99 81-129 75-00-3 Chloroethane 50 64.9 130 68-133 67-66-3 Chloroform 50 49.9 100 72-123 95-49-8 o-Chlorotoluene 50 48.6 97 77-129 106-43-4 p-Chlorotoluene 50 51.4 103 80-134 56-23-5 Carbon tetrachloride 50 59.8 120 78-133 75-34-3 1,1-Dichloroethane 50 51.1 102 73-125 75-35-4 1,1-Dichloroethylene 50 49.9 100 81-136 563-58-6 1,1-Dichloropropene 50 50.7 101 75-130 106-93-4 1,2-Dibromoethane 50 50.1 100 77-126 107-06-2 1,2-Dichloroethane 50 50.0 100 74-128 78-87-5 1,2-Dichloropropane 50 51.1 102 74-125 142-28-9 1,3-Dichloropropane 50 48.2 96 76-122 108-20-3 Di-Isopropyl ether 50 53.9 108 75-122 594-20-7 2,2-Dichloropropane 50 55.8 112 77-133 124-48-1 Dibromochloromethane 50 51.0 102 76-127 75-71-8 Dichlorodifluoromethane 50 47.0 94 68-168 156-59-2 cis-1,2-Dichloroethylene 50 51.9 104 74-126 10061-01-5 cis-1,3-Dichloropropene 50 54.4 109 80-123 541-73-1 m-Dichlorobenzene 50 50.7 101 81-129 95-50-1 o-Dichlorobenzene 50 48.3 97 80-129 106-46-7 p-Dichlorobenzene 50 49.6 99 76-130 156-60-5 trans-1,2-Dichloroethylene 50 50.2 100 70-127 10061-02-6 trans-1,3-Dichloropropene 50 50.8 102 75-131 64-17-5 Ethyl alcohol 1000 1030 103 53-154 100-41-4 Ethylbenzene 50 48.8 98 77-123 591-78-6 2-Hexanone 250 242 97 72-133 * = Outside of Control Limits. 142 of 208 FA15409 55.2.4 Blank Spike Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-BS F0064638.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 98-82-8 Isopropylbenzene 50 48.3 97 80-136 99-87-6 p-Isopropyltoluene 50 49.5 99 77-131 108-10-1 4-Methyl-2-pentanone 250 221 88 76-132 74-83-9 Methyl bromide 50 55.4 111 65-139 74-87-3 Methyl chloride 50 48.6 97 71-144 75-09-2 Methylene chloride 50 55.1 110 74-137 78-93-3 Methyl ethyl ketone 250 239 96 75-137 1634-04-4 Methyl Tert Butyl Ether 50 52.9 106 77-120 91-20-3 Naphthalene 50 52.5 105 79-129 103-65-1 n-Propylbenzene 50 48.8 98 80-135 100-42-5 Styrene 50 50.1 100 78-125 630-20-6 1,1,1,2-Tetrachloroethane 50 50.0 100 78-126 71-55-6 1,1,1-Trichloroethane 50 50.6 101 70-129 79-34-5 1,1,2,2-Tetrachloroethane 50 48.6 97 71-126 79-00-5 1,1,2-Trichloroethane 50 47.9 96 74-124 87-61-6 1,2,3-Trichlorobenzene 50 51.6 103 77-128 96-18-4 1,2,3-Trichloropropane 50 47.9 96 74-127 120-82-1 1,2,4-Trichlorobenzene 50 50.7 101 78-130 95-63-6 1,2,4-Trimethylbenzene 50 49.2 98 74-123 108-67-8 1,3,5-Trimethylbenzene 50 49.0 98 73-122 127-18-4 Tetrachloroethylene 50 42.4 85 79-130 108-88-3 Toluene 50 45.9 92 76-124 79-01-6 Trichloroethylene 50 48.3 97 75-128 75-69-4 Trichlorofluoromethane 50 52.2 104 73-145 75-01-4 Vinyl chloride 50 49.0 98 76-141 108-05-4 Vinyl Acetate 250 233 93 48-164 1330-20-7 Xylene (total)150 144 96 80-129 m,p-Xylene 100 94.8 95 80-128 95-47-6 o-Xylene 50 48.8 98 80-132 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 91%75-124% 2037-26-5 Toluene-D8 87%75-126% 460-00-4 4-Bromofluorobenzene 99%71-133% * = Outside of Control Limits. 143 of 208 FA15409 55.2.4 Blank Spike Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2135-BS F0064638.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 CAS No.Surrogate Recoveries BSP Limits 17060-07-0 1,2-Dichloroethane-D4 84%72-135% * = Outside of Control Limits. 144 of 208 FA15409 55.2.4 Blank Spike Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-BS F0064660.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 67-64-1 Acetone 250 248 99 61-152 71-43-2 Benzene 50 49.7 99 76-126 108-86-1 Bromobenzene 50 47.9 96 76-122 74-97-5 Bromochloromethane 50 50.8 102 77-120 75-27-4 Bromodichloromethane 50 53.4 107 74-130 75-25-2 Bromoform 50 44.3 89 76-127 104-51-8 n-Butylbenzene 50 45.2 90 71-128 135-98-8 sec-Butylbenzene 50 50.7 101 79-135 98-06-6 tert-Butylbenzene 50 48.4 97 77-133 108-90-7 Chlorobenzene 50 51.0 102 81-129 75-00-3 Chloroethane 50 38.3 77 68-133 67-66-3 Chloroform 50 48.6 97 72-123 95-49-8 o-Chlorotoluene 50 50.4 101 77-129 106-43-4 p-Chlorotoluene 50 54.1 108 80-134 56-23-5 Carbon tetrachloride 50 48.4 97 78-133 75-34-3 1,1-Dichloroethane 50 48.1 96 73-125 75-35-4 1,1-Dichloroethylene 50 46.1 92 81-136 563-58-6 1,1-Dichloropropene 50 50.2 100 75-130 106-93-4 1,2-Dibromoethane 50 51.4 103 77-126 107-06-2 1,2-Dichloroethane 50 48.5 97 74-128 78-87-5 1,2-Dichloropropane 50 49.7 99 74-125 142-28-9 1,3-Dichloropropane 50 48.9 98 76-122 108-20-3 Di-Isopropyl ether 50 49.4 99 75-122 594-20-7 2,2-Dichloropropane 50 54.6 109 77-133 124-48-1 Dibromochloromethane 50 51.6 103 76-127 75-71-8 Dichlorodifluoromethane 50 45.3 91 68-168 156-59-2 cis-1,2-Dichloroethylene 50 50.1 100 74-126 10061-01-5 cis-1,3-Dichloropropene 50 53.3 107 80-123 541-73-1 m-Dichlorobenzene 50 53.2 106 81-129 95-50-1 o-Dichlorobenzene 50 51.3 103 80-129 106-46-7 p-Dichlorobenzene 50 46.8 94 76-130 156-60-5 trans-1,2-Dichloroethylene 50 46.9 94 70-127 10061-02-6 trans-1,3-Dichloropropene 50 56.0 112 75-131 64-17-5 Ethyl alcohol 1000 871 87 53-154 100-41-4 Ethylbenzene 50 46.6 93 77-123 591-78-6 2-Hexanone 250 230 92 72-133 * = Outside of Control Limits. 145 of 208 FA15409 55.2.5 Blank Spike Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-BS F0064660.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 98-82-8 Isopropylbenzene 50 51.3 103 80-136 99-87-6 p-Isopropyltoluene 50 50.8 102 77-131 108-10-1 4-Methyl-2-pentanone 250 220 88 76-132 74-83-9 Methyl bromide 50 44.8 90 65-139 74-87-3 Methyl chloride 50 46.5 93 71-144 75-09-2 Methylene chloride 50 50.4 101 74-137 78-93-3 Methyl ethyl ketone 250 242 97 75-137 1634-04-4 Methyl Tert Butyl Ether 50 51.6 103 77-120 91-20-3 Naphthalene 50 48.2 96 79-129 103-65-1 n-Propylbenzene 50 49.5 99 80-135 100-42-5 Styrene 50 49.0 98 78-125 630-20-6 1,1,1,2-Tetrachloroethane 50 50.2 100 78-126 71-55-6 1,1,1-Trichloroethane 50 49.7 99 70-129 79-34-5 1,1,2,2-Tetrachloroethane 50 47.5 95 71-126 79-00-5 1,1,2-Trichloroethane 50 47.6 95 74-124 87-61-6 1,2,3-Trichlorobenzene 50 47.5 95 77-128 96-18-4 1,2,3-Trichloropropane 50 49.3 99 74-127 120-82-1 1,2,4-Trichlorobenzene 50 49.2 98 78-130 95-63-6 1,2,4-Trimethylbenzene 50 47.2 94 74-123 108-67-8 1,3,5-Trimethylbenzene 50 46.4 93 73-122 127-18-4 Tetrachloroethylene 50 44.8 90 79-130 108-88-3 Toluene 50 44.2 88 76-124 79-01-6 Trichloroethylene 50 47.7 95 75-128 75-69-4 Trichlorofluoromethane 50 46.4 93 73-145 75-01-4 Vinyl chloride 50 45.9 92 76-141 108-05-4 Vinyl Acetate 250 177 71 48-164 1330-20-7 Xylene (total)150 147 98 80-129 m,p-Xylene 100 96.4 96 80-128 95-47-6 o-Xylene 50 50.8 102 80-132 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 95%75-124% 2037-26-5 Toluene-D8 89%75-126% 460-00-4 4-Bromofluorobenzene 102%71-133% * = Outside of Control Limits. 146 of 208 FA15409 55.2.5 Blank Spike Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2136-BS F0064660.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 CAS No.Surrogate Recoveries BSP Limits 17060-07-0 1,2-Dichloroethane-D4 89%72-135% * = Outside of Control Limits. 147 of 208 FA15409 55.2.5 Blank Spike Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2137-BS F0064688.D 1 06/03/14 AH n/a n/a VF2137 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-9 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 100-41-4 Ethylbenzene 50 52.2 104 77-123 91-20-3 Naphthalene 50 56.5 113 79-129 95-63-6 1,2,4-Trimethylbenzene 50 51.2 102 74-123 108-67-8 1,3,5-Trimethylbenzene 50 51.9 104 73-122 108-88-3 Toluene 50 50.9 102 76-124 1330-20-7 Xylene (total)150 163 109 80-129 m,p-Xylene 100 108 108 80-128 95-47-6 o-Xylene 50 54.8 110 80-132 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 93%75-124% 2037-26-5 Toluene-D8 90%75-126% 460-00-4 4-Bromofluorobenzene 97%71-133% 17060-07-0 1,2-Dichloroethane-D4 84%72-135% * = Outside of Control Limits. 148 of 208 FA15409 55.2.6 Blank Spike Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-BS F0064700.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 67-64-1 Acetone 250 222 89 61-152 71-43-2 Benzene 50 52.7 105 76-126 108-86-1 Bromobenzene 50 52.8 106 76-122 74-97-5 Bromochloromethane 50 55.5 111 77-120 75-27-4 Bromodichloromethane 50 57.1 114 74-130 75-25-2 Bromoform 50 50.0 100 76-127 104-51-8 n-Butylbenzene 50 53.0 106 71-128 135-98-8 sec-Butylbenzene 50 52.8 106 79-135 98-06-6 tert-Butylbenzene 50 48.7 97 77-133 108-90-7 Chlorobenzene 50 54.7 109 81-129 75-00-3 Chloroethane 50 56.3 113 68-133 67-66-3 Chloroform 50 53.0 106 72-123 95-49-8 o-Chlorotoluene 50 53.2 106 77-129 106-43-4 p-Chlorotoluene 50 57.5 115 80-134 56-23-5 Carbon tetrachloride 50 55.0 110 78-133 75-34-3 1,1-Dichloroethane 50 53.6 107 73-125 75-35-4 1,1-Dichloroethylene 50 50.7 101 81-136 563-58-6 1,1-Dichloropropene 50 54.7 109 75-130 106-93-4 1,2-Dibromoethane 50 54.2 108 77-126 107-06-2 1,2-Dichloroethane 50 52.0 104 74-128 78-87-5 1,2-Dichloropropane 50 53.3 107 74-125 142-28-9 1,3-Dichloropropane 50 49.3 99 76-122 108-20-3 Di-Isopropyl ether 50 52.8 106 75-122 594-20-7 2,2-Dichloropropane 50 63.4 127 77-133 124-48-1 Dibromochloromethane 50 55.0 110 76-127 75-71-8 Dichlorodifluoromethane 50 50.8 102 68-168 156-59-2 cis-1,2-Dichloroethylene 50 55.2 110 74-126 10061-01-5 cis-1,3-Dichloropropene 50 57.0 114 80-123 541-73-1 m-Dichlorobenzene 50 60.2 120 81-129 95-50-1 o-Dichlorobenzene 50 58.3 117 80-129 106-46-7 p-Dichlorobenzene 50 53.0 106 76-130 156-60-5 trans-1,2-Dichloroethylene 50 51.7 103 70-127 10061-02-6 trans-1,3-Dichloropropene 50 57.6 115 75-131 64-17-5 Ethyl alcohol 1000 1030 103 53-154 100-41-4 Ethylbenzene 50 49.1 98 77-123 591-78-6 2-Hexanone 250 224 90 72-133 * = Outside of Control Limits. 149 of 208 FA15409 55.2.7 Blank Spike Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-BS F0064700.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 98-82-8 Isopropylbenzene 50 55.5 111 80-136 99-87-6 p-Isopropyltoluene 50 54.7 109 77-131 108-10-1 4-Methyl-2-pentanone 250 214 86 76-132 74-83-9 Methyl bromide 50 55.7 111 65-139 74-87-3 Methyl chloride 50 50.8 102 71-144 75-09-2 Methylene chloride 50 56.5 113 74-137 78-93-3 Methyl ethyl ketone 250 229 92 75-137 1634-04-4 Methyl Tert Butyl Ether 50 56.6 113 77-120 91-20-3 Naphthalene 50 55.1 110 79-129 103-65-1 n-Propylbenzene 50 53.9 108 80-135 100-42-5 Styrene 50 54.3 109 78-125 630-20-6 1,1,1,2-Tetrachloroethane 50 53.9 108 78-126 71-55-6 1,1,1-Trichloroethane 50 54.5 109 70-129 79-34-5 1,1,2,2-Tetrachloroethane 50 48.4 97 71-126 79-00-5 1,1,2-Trichloroethane 50 50.4 101 74-124 87-61-6 1,2,3-Trichlorobenzene 50 53.8 108 77-128 96-18-4 1,2,3-Trichloropropane 50 49.5 99 74-127 120-82-1 1,2,4-Trichlorobenzene 50 55.8 112 78-130 95-63-6 1,2,4-Trimethylbenzene 50 51.6 103 74-123 108-67-8 1,3,5-Trimethylbenzene 50 48.8 98 73-122 127-18-4 Tetrachloroethylene 50 48.1 96 79-130 108-88-3 Toluene 50 48.9 98 76-124 79-01-6 Trichloroethylene 50 52.7 105 75-128 75-69-4 Trichlorofluoromethane 50 54.2 108 73-145 75-01-4 Vinyl chloride 50 50.6 101 76-141 108-05-4 Vinyl Acetate 250 185 74 48-164 1330-20-7 Xylene (total)150 159 106 80-129 m,p-Xylene 100 103 103 80-128 95-47-6 o-Xylene 50 55.9 112 80-132 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 93%75-124% 2037-26-5 Toluene-D8 87%75-126% 460-00-4 4-Bromofluorobenzene 97%71-133% * = Outside of Control Limits. 150 of 208 FA15409 55.2.7 Blank Spike Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VF2138-BS F0064700.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 CAS No.Surrogate Recoveries BSP Limits 17060-07-0 1,2-Dichloroethane-D4 81%72-135% * = Outside of Control Limits. 151 of 208 FA15409 55.2.7 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15399-7MS E031081.D 200 06/06/14 TD n/a n/a VE1043 FA15399-7MSD E031082.D 200 06/06/14 TD n/a n/a VE1043 FA15399-7 E031078.D 200 06/06/14 TD n/a n/a VE1043 The QC reported here applies to the following samples:Method: SM 6200B FA15409-23 FA15399-7 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 1330-20-7 Xylene (total)21400 6000 31300 165* a 6000 28300 115 10 70-130/20 m,p-Xylene 14400 4000 21000 165* a 4000 19000 115 10 70-130/20 95-47-6 o-Xylene 6940 2000 10300 168* a 2000 9290 118 10 70-130/20 CAS No.Surrogate Recoveries MS MSD FA15399-7 Limits 1868-53-7 Dibromofluoromethane 100%97%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%95%104%70-130% 2037-26-5 Toluene-D8 102%102%101%70-130% 460-00-4 4-Bromofluorobenzene 103%105%103%70-130% (a) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 152 of 208 FA15409 55.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15382-1MS C098554.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1MSD C098555.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1 C098549.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 FA15382-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 67-64-1 Acetone ND 375 510 136 373 375 100 31*61-152/27 71-43-2 Benzene ND 75 74.3 99 74.7 70.5 94 5 76-126/26 108-86-1 Bromobenzene ND 75 78.7 105 74.7 74.5 100 5 76-122/32 74-97-5 Bromochloromethane ND 75 72.0 96 74.7 68.5 92 5 77-120/24 75-27-4 Bromodichloromethane ND 75 76.9 102 74.7 72.8 98 5 74-130/25 75-25-2 Bromoform ND 75 74.9 100 74.7 75.6 101 1 76-127/26 104-51-8 n-Butylbenzene ND 75 78.1 104 74.7 72.7 97 7 71-128/35 135-98-8 sec-Butylbenzene ND 75 83.2 111 74.7 77.4 104 7 79-135/34 98-06-6 tert-Butylbenzene ND 75 84.7 113 74.7 80.6 108 5 77-133/34 108-90-7 Chlorobenzene ND 75 80.5 107 74.7 77.9 104 3 81-129/29 75-00-3 Chloroethane ND 75 114 152*74.7 109 146*4 68-133/29 67-66-3 Chloroform ND 75 70.0 93 74.7 66.3 89 5 72-123/26 95-49-8 o-Chlorotoluene ND 75 82.6 110 74.7 79.0 106 4 77-129/33 106-43-4 p-Chlorotoluene ND 75 85.6 114 74.7 80.2 107 7 80-134/33 56-23-5 Carbon tetrachloride ND 75 73.8 98 74.7 68.9 92 7 78-133/29 75-34-3 1,1-Dichloroethane ND 75 69.7 93 74.7 67.7 91 3 73-125/27 75-35-4 1,1-Dichloroethylene ND 75 100 133 74.7 94.2 126 6 81-136/28 563-58-6 1,1-Dichloropropene ND 75 73.4 98 74.7 70.8 95 4 75-130/28 106-93-4 1,2-Dibromoethane ND 75 73.3 98 74.7 72.3 97 1 77-126/26 107-06-2 1,2-Dichloroethane ND 75 81.2 108 74.7 73.4 98 10 74-128/23 78-87-5 1,2-Dichloropropane ND 75 75.6 101 74.7 72.8 98 4 74-125/25 142-28-9 1,3-Dichloropropane ND 75 74.7 100 74.7 74.9 100 0 76-122/26 108-20-3 Di-Isopropyl ether ND 75 67.9 90 74.7 76.0 102 11 75-122/25 594-20-7 2,2-Dichloropropane ND 75 89.1 119 74.7 79.5 106 11 77-133/28 124-48-1 Dibromochloromethane ND 75 79.0 105 74.7 75.3 101 5 76-127/27 75-71-8 Dichlorodifluoromethane ND 75 78.5 105 74.7 74.9 100 5 68-168/29 156-59-2 cis-1,2-Dichloroethylene ND 75 71.8 96 74.7 70.8 95 1 74-126/26 10061-01-5 cis-1,3-Dichloropropene ND 75 77.7 104 74.7 73.9 99 5 80-123/26 541-73-1 m-Dichlorobenzene ND 75 83.9 112 74.7 81.1 109 3 81-129/33 95-50-1 o-Dichlorobenzene ND 75 83.2 111 74.7 79.0 106 5 80-129/32 106-46-7 p-Dichlorobenzene ND 75 79.1 105 74.7 74.5 100 6 76-130/32 156-60-5 trans-1,2-Dichloroethylene ND 75 96.5 129*74.7 92.5 124 4 70-127/27 10061-02-6 trans-1,3-Dichloropropene ND 75 74.9 100 74.7 73.8 99 1 75-131/28 64-17-5 Ethyl alcohol ND 1500 157 10*1490 333 22*72*53-154/42 100-41-4 Ethylbenzene ND 75 75.6 101 74.7 74.2 99 2 77-123/31 591-78-6 2-Hexanone ND 375 373 99 373 367 98 2 72-133/26 * = Outside of Control Limits. 153 of 208 FA15409 55.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15382-1MS C098554.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1MSD C098555.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1 C098549.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 FA15382-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 98-82-8 Isopropylbenzene ND 75 77.5 103 74.7 74.7 100 4 80-136/32 99-87-6 p-Isopropyltoluene ND 75 84.2 112 74.7 79.4 106 6 77-131/34 108-10-1 4-Methyl-2-pentanone ND 375 375 100 373 364 98 3 76-132/26 74-83-9 Methyl bromide ND 75 110 147*74.7 102 137 8 65-139/31 74-87-3 Methyl chloride ND 75 93.2 124 74.7 95.8 128 3 71-144/27 75-09-2 Methylene chloride ND 75 107 143*74.7 97.6 131 9 74-137/28 78-93-3 Methyl ethyl ketone ND 375 349 93 373 287 77 19 75-137/25 1634-04-4 Methyl Tert Butyl Ether ND 75 86.0 115 74.7 82.5 111 4 77-120/24 91-20-3 Naphthalene ND 75 74.1 99 74.7 68.4 92 8 79-129/33 103-65-1 n-Propylbenzene ND 75 83.9 112 74.7 80.0 107 5 80-135/33 100-42-5 Styrene ND 75 77.9 104 74.7 76.0 102 2 78-125/30 630-20-6 1,1,1,2-Tetrachloroethane ND 75 79.7 106 74.7 75.5 101 5 78-126/27 71-55-6 1,1,1-Trichloroethane ND 75 78.6 105 74.7 77.1 103 2 70-129/27 79-34-5 1,1,2,2-Tetrachloroethane ND 75 74.5 99 74.7 73.9 99 1 71-126/30 79-00-5 1,1,2-Trichloroethane ND 75 73.8 98 74.7 74.9 100 1 74-124/28 87-61-6 1,2,3-Trichlorobenzene ND 75 78.4 104 74.7 70.4 94 11 77-128/35 96-18-4 1,2,3-Trichloropropane ND 75 77.7 104 74.7 77.1 103 1 74-127/27 120-82-1 1,2,4-Trichlorobenzene ND 75 82.9 110 74.7 74.3 100 11 78-130/34 95-63-6 1,2,4-Trimethylbenzene ND 75 80.9 108 74.7 76.8 103 5 74-123/34 108-67-8 1,3,5-Trimethylbenzene ND 75 79.6 106 74.7 75.2 101 6 73-122/33 127-18-4 Tetrachloroethylene ND 75 72.3 96 74.7 72.7 97 1 79-130/31 108-88-3 Toluene ND 75 74.7 100 74.7 75.0 100 0 76-124/30 79-01-6 Trichloroethylene ND 75 74.5 99 74.7 70.8 95 5 75-128/27 75-69-4 Trichlorofluoromethane ND 75 88.9 118 74.7 85.8 115 4 73-145/31 75-01-4 Vinyl chloride ND 75 87.3 116 74.7 87.2 117 0 76-141/27 108-05-4 Vinyl Acetate ND 375 350 93 373 332 89 5 48-164/37 1330-20-7 Xylene (total)ND 225 229 102 224 222 99 3 80-129/30 m,p-Xylene ND 150 151 101 149 147 98 3 80-128/30 95-47-6 o-Xylene ND 75 77.2 103 74.7 75.2 101 3 80-132/30 CAS No.Surrogate Recoveries MS MSD FA15382-1 Limits 1868-53-7 Dibromofluoromethane 100%96%112%75-124% 2037-26-5 Toluene-D8 99%102%102%75-126% 460-00-4 4-Bromofluorobenzene 96%99%94%71-133% * = Outside of Control Limits. 154 of 208 FA15409 55.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15382-1MS C098554.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1MSD C098555.D 1 05/30/14 AH n/a n/a VC3954 FA15382-1 C098549.D 1 05/30/14 AH n/a n/a VC3954 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-6, FA15409-7 CAS No.Surrogate Recoveries MS MSD FA15382-1 Limits 17060-07-0 1,2-Dichloroethane-D4 101%94%109%72-135% * = Outside of Control Limits. 155 of 208 FA15409 55.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-1MS F0064667.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1MSD F0064668.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1 F0064640.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 FA15409-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 67-64-1 Acetone 70.2 337 318 74 344 411 99 26 61-152/27 71-43-2 Benzene 38.4 67.4 60.4 33*68.9 63.2 36*5 76-126/26 108-86-1 Bromobenzene ND 67.4 41.1 61*68.9 47.1 68*14 76-122/32 74-97-5 Bromochloromethane ND 67.4 55.4 82 68.9 56.8 82 2 77-120/24 75-27-4 Bromodichloromethane ND 67.4 44.8 66*68.9 48.5 70*8 74-130/25 75-25-2 Bromoform ND 67.4 31.7 47*68.9 34.3 50*8 76-127/26 104-51-8 n-Butylbenzene 5.4 67.4 50.8 67*68.9 49.4 64*3 71-128/35 135-98-8 sec-Butylbenzene 5.5 67.4 56.8 76*68.9 56.8 74*0 79-135/34 98-06-6 tert-Butylbenzene ND 67.4 39.9 59*68.9 47.9 70*18 77-133/34 108-90-7 Chlorobenzene ND 67.4 48.0 71*68.9 53.5 78*11 81-129/29 75-00-3 Chloroethane ND 67.4 51.9 77 68.9 37.9 55*31*68-133/29 67-66-3 Chloroform ND 67.4 60.3 90 68.9 55.7 81 8 72-123/26 95-49-8 o-Chlorotoluene ND 67.4 39.3 58*68.9 47.7 69*19 77-129/33 106-43-4 p-Chlorotoluene ND 67.4 35.9 53*68.9 45.4 66*23 80-134/33 56-23-5 Carbon tetrachloride ND 67.4 36.6 54*68.9 39.5 57*8 78-133/29 75-34-3 1,1-Dichloroethane ND 67.4 53.4 79 68.9 53.2 77 0 73-125/27 75-35-4 1,1-Dichloroethylene ND 67.4 49.7 74*68.9 51.4 75*3 81-136/28 563-58-6 1,1-Dichloropropene ND 67.4 50.8 75 68.9 53.1 77 4 75-130/28 106-93-4 1,2-Dibromoethane ND 67.4 52.9 79 68.9 54.6 79 3 77-126/26 107-06-2 1,2-Dichloroethane ND 67.4 50.4 75 68.9 50.4 73*0 74-128/23 78-87-5 1,2-Dichloropropane ND 67.4 53.3 79 68.9 55.6 81 4 74-125/25 142-28-9 1,3-Dichloropropane ND 67.4 47.4 70*68.9 51.7 75*9 76-122/26 108-20-3 Di-Isopropyl ether 8.5 67.4 57.0 72*68.9 58.2 72*2 75-122/25 594-20-7 2,2-Dichloropropane ND 67.4 27.3 41*68.9 31.2 45*13 77-133/28 124-48-1 Dibromochloromethane ND 67.4 41.2 61*68.9 45.3 66*9 76-127/27 75-71-8 Dichlorodifluoromethane ND 67.4 38.3 57*68.9 39.1 57*2 68-168/29 156-59-2 cis-1,2-Dichloroethylene ND 67.4 54.0 80 68.9 56.3 82 4 74-126/26 10061-01-5 cis-1,3-Dichloropropene ND 67.4 26.3 39*68.9 30.7 45*15 80-123/26 541-73-1 m-Dichlorobenzene ND 67.4 33.5 50*68.9 41.6 60*22 81-129/33 95-50-1 o-Dichlorobenzene ND 67.4 34.3 51*68.9 43.3 63*23 80-129/32 106-46-7 p-Dichlorobenzene ND 67.4 31.3 46*68.9 39.7 58*24 76-130/32 156-60-5 trans-1,2-Dichloroethylene ND 67.4 48.2 72 68.9 51.2 74 6 70-127/27 10061-02-6 trans-1,3-Dichloropropene ND 67.4 26.4 39*68.9 32.5 47*21 75-131/28 64-17-5 Ethyl alcohol ND 1350 165 12*1380 835 61 134*53-154/42 100-41-4 Ethylbenzene 30.7 67.4 148 174*68.9 90.1 86 49*77-123/31 591-78-6 2-Hexanone ND 337 225 67*344 221 64*2 72-133/26 * = Outside of Control Limits. 156 of 208 FA15409 55.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-1MS F0064667.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1MSD F0064668.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1 F0064640.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 FA15409-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 98-82-8 Isopropylbenzene 11.3 67.4 93.1 121 68.9 72.9 89 24 80-136/32 99-87-6 p-Isopropyltoluene 1.9 J 67.4 42.0 60*68.9 51.1 71*20 77-131/34 108-10-1 4-Methyl-2-pentanone ND 337 266 79 344 244 71*9 76-132/26 74-83-9 Methyl bromide ND 67.4 43.8 65 68.9 41.3 60*6 65-139/31 74-87-3 Methyl chloride ND 67.4 47.5 71 68.9 47.4 69*0 71-144/27 75-09-2 Methylene chloride ND 67.4 56.6 84 68.9 56.2 82 1 74-137/28 78-93-3 Methyl ethyl ketone ND 337 385 114 344 298 87 25 75-137/25 1634-04-4 Methyl Tert Butyl Ether 26.6 67.4 68.4 62*68.9 73.1 68*7 77-120/24 91-20-3 Naphthalene 56.0 67.4 189 197*68.9 115 86 49*79-129/33 103-65-1 n-Propylbenzene 19.2 67.4 143 184*68.9 84.8 95 51*80-135/33 100-42-5 Styrene ND 67.4 38.3 57*68.9 43.8 64*13 78-125/30 630-20-6 1,1,1,2-Tetrachloroethane ND 67.4 47.6 71*68.9 52.2 76*9 78-126/27 71-55-6 1,1,1-Trichloroethane ND 67.4 51.7 77 68.9 55.1 80 6 70-129/27 79-34-5 1,1,2,2-Tetrachloroethane ND 67.4 51.8 77 68.9 51.0 74 2 71-126/30 79-00-5 1,1,2-Trichloroethane ND 67.4 338 502*68.9 195 283*54*74-124/28 87-61-6 1,2,3-Trichlorobenzene ND 67.4 18.1 27*68.9 26.8 39*39*77-128/35 96-18-4 1,2,3-Trichloropropane ND 67.4 52.1 77 68.9 51.0 74 2 74-127/27 120-82-1 1,2,4-Trichlorobenzene ND 67.4 19.6 29*68.9 27.2 39*32 78-130/34 95-63-6 1,2,4-Trimethylbenzene 5.9 67.4 111 156*68.9 118 163*6 74-123/34 108-67-8 1,3,5-Trimethylbenzene 2.3 J 67.4 62.4 89 68.9 67.0 94 7 73-122/33 127-18-4 Tetrachloroethylene ND 67.4 39.9 59*68.9 46.0 67*14 79-130/31 108-88-3 Toluene 4.2 J 67.4 47.4 64*68.9 53.2 71*12 76-124/30 79-01-6 Trichloroethylene ND 67.4 61.5 91 68.9 59.7 87 3 75-128/27 75-69-4 Trichlorofluoromethane ND 67.4 44.3 66*68.9 44.5 65*0 73-145/31 75-01-4 Vinyl chloride ND 67.4 46.0 68*68.9 47.4 69*3 76-141/27 108-05-4 Vinyl Acetate ND 337 14.2 4*344 ND 0*200*48-164/37 1330-20-7 Xylene (total)16.8 202 173 77*207 180 79*4 80-129/30 m,p-Xylene 12.4 135 115 76*138 118 77*3 80-128/30 95-47-6 o-Xylene 4.4 J 67.4 58.3 80 68.9 61.8 83 6 80-132/30 CAS No.Surrogate Recoveries MS MSD FA15409-1 Limits 1868-53-7 Dibromofluoromethane 90%89%91%75-124% 2037-26-5 Toluene-D8 94%92%91%75-126% 460-00-4 4-Bromofluorobenzene 97%98%100%71-133% * = Outside of Control Limits. 157 of 208 FA15409 55.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-1MS F0064667.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1MSD F0064668.D 1 06/02/14 AH n/a n/a VF2135 FA15409-1 F0064640.D 1 05/30/14 AH n/a n/a VF2135 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-1, FA15409-2, FA15409-13, FA15409-22 CAS No.Surrogate Recoveries MS MSD FA15409-1 Limits 17060-07-0 1,2-Dichloroethane-D4 93%77%105%72-135% * = Outside of Control Limits. 158 of 208 FA15409 55.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-14MS F0064680.D 1 06/02/14 AH n/a n/a VF2136 FA15409-14MSD F0064681.D 1 06/03/14 AH n/a n/a VF2136 FA15409-14 F0064678.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 FA15409-14 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 67-64-1 Acetone ND 17600 17100 97 17600 13500 77 24 61-152/27 71-43-2 Benzene 1130 3510 4600 99 3510 4360 92 5 76-126/26 108-86-1 Bromobenzene ND 3510 3280 93 3510 3360 96 2 76-122/32 74-97-5 Bromochloromethane ND 3510 3650 104 3510 3490 99 4 77-120/24 75-27-4 Bromodichloromethane ND 3510 3570 102 3510 3460 99 3 74-130/25 75-25-2 Bromoform ND 3510 3220 92 3510 3030 86 6 76-127/26 104-51-8 n-Butylbenzene 524 3510 3480 84 3510 3460 84 1 71-128/35 135-98-8 sec-Butylbenzene 156 J 3510 3500 95 3510 3450 94 1 79-135/34 98-06-6 tert-Butylbenzene ND 3510 3340 95 3510 3410 97 2 77-133/34 108-90-7 Chlorobenzene ND 3510 3620 103 3510 3550 101 2 81-129/29 75-00-3 Chloroethane ND 3510 718 20*3510 658 19*9 68-133/29 67-66-3 Chloroform ND 3510 3300 94 3510 3200 91 3 72-123/26 95-49-8 o-Chlorotoluene ND 3510 3350 95 3510 3560 101 6 77-129/33 106-43-4 p-Chlorotoluene ND 3510 3360 96 3510 3420 97 2 80-134/33 56-23-5 Carbon tetrachloride ND 3510 3210 91 3510 3070 87 4 78-133/29 75-34-3 1,1-Dichloroethane ND 3510 3330 95 3510 3120 89 7 73-125/27 75-35-4 1,1-Dichloroethylene ND 3510 2930 83 3510 2650 75*10 81-136/28 563-58-6 1,1-Dichloropropene ND 3510 3470 99 3510 3160 90 9 75-130/28 106-93-4 1,2-Dibromoethane ND 3510 3710 106 3510 3560 101 4 77-126/26 107-06-2 1,2-Dichloroethane ND 3510 3400 97 3510 3180 91 7 74-128/23 78-87-5 1,2-Dichloropropane ND 3510 3460 99 3510 3410 97 1 74-125/25 142-28-9 1,3-Dichloropropane ND 3510 3450 98 3510 3180 91 8 76-122/26 108-20-3 Di-Isopropyl ether ND 3510 3420 97 3510 3210 91 6 75-122/25 594-20-7 2,2-Dichloropropane ND 3510 3340 95 3510 3080 88 8 77-133/28 124-48-1 Dibromochloromethane ND 3510 3690 105 3510 3490 99 6 76-127/27 75-71-8 Dichlorodifluoromethane ND 3510 2960 84 3510 2670 76 10 68-168/29 156-59-2 cis-1,2-Dichloroethylene ND 3510 3600 102 3510 3340 95 7 74-126/26 10061-01-5 cis-1,3-Dichloropropene ND 3510 3540 101 3510 3450 98 3 80-123/26 541-73-1 m-Dichlorobenzene ND 3510 3540 101 3510 3560 101 1 81-129/33 95-50-1 o-Dichlorobenzene ND 3510 3600 102 3510 3540 101 2 80-129/32 106-46-7 p-Dichlorobenzene ND 3510 3270 93 3510 3240 92 1 76-130/32 156-60-5 trans-1,2-Dichloroethylene ND 3510 3200 91 3510 3010 86 6 70-127/27 10061-02-6 trans-1,3-Dichloropropene ND 3510 3590 102 3510 3580 102 0 75-131/28 64-17-5 Ethyl alcohol ND 70300 68800 98 70300 58700 84 16 53-154/42 100-41-4 Ethylbenzene 2940 3510 6180 92 3510 5960 86 4 77-123/31 591-78-6 2-Hexanone ND 17600 16300 93 17600 14400 82 12 72-133/26 * = Outside of Control Limits. 159 of 208 FA15409 55.3.4 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-14MS F0064680.D 1 06/02/14 AH n/a n/a VF2136 FA15409-14MSD F0064681.D 1 06/03/14 AH n/a n/a VF2136 FA15409-14 F0064678.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 FA15409-14 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 98-82-8 Isopropylbenzene 328 J 3510 4100 107 3510 3780 98 8 80-136/32 99-87-6 p-Isopropyltoluene 113 J 3510 3390 93 3510 3370 93 1 77-131/34 108-10-1 4-Methyl-2-pentanone ND 17600 16400 93 17600 14900 85 10 76-132/26 74-83-9 Methyl bromide ND 3510 2700 77 3510 2400 68 12 65-139/31 74-87-3 Methyl chloride ND 3510 3170 90 3510 2890 82 9 71-144/27 75-09-2 Methylene chloride 348 JB 3510 3480 89 3510 3290 84 6 74-137/28 78-93-3 Methyl ethyl ketone ND 17600 17500 100 17600 15700 89 11 75-137/25 1634-04-4 Methyl Tert Butyl Ether 137 J 3510 3850 106 3510 3650 100 5 77-120/24 91-20-3 Naphthalene 2040 3510 5740 105 3510 5490 98 4 79-129/33 103-65-1 n-Propylbenzene 1190 3510 4230 87 3510 4360 90 3 80-135/33 100-42-5 Styrene 163 J 3510 3680 100 3510 3560 97 3 78-125/30 630-20-6 1,1,1,2-Tetrachloroethane ND 3510 3750 107 3510 3570 102 5 78-126/27 71-55-6 1,1,1-Trichloroethane ND 3510 3230 92 3510 3090 88 4 70-129/27 79-34-5 1,1,2,2-Tetrachloroethane ND 3510 3270 93 3510 3260 93 0 71-126/30 79-00-5 1,1,2-Trichloroethane ND 3510 4300 122 3510 4090 116 5 74-124/28 87-61-6 1,2,3-Trichlorobenzene ND 3510 3470 99 3510 3340 95 4 77-128/35 96-18-4 1,2,3-Trichloropropane ND 3510 3250 93 3510 3410 97 5 74-127/27 120-82-1 1,2,4-Trichlorobenzene ND 3510 3410 97 3510 3320 95 3 78-130/34 95-63-6 1,2,4-Trimethylbenzene 7320 3510 10200 82 3510 10300 85 1 74-123/34 108-67-8 1,3,5-Trimethylbenzene 2260 3510 5100 81 3510 5400 89 6 73-122/33 127-18-4 Tetrachloroethylene ND 3510 3660 104 3510 3370 96 8 79-130/31 108-88-3 Toluene 12700 3510 16000 94 3510 15100 68* a 6 76-124/30 79-01-6 Trichloroethylene ND 3510 3390 97 3510 3270 93 4 75-128/27 75-69-4 Trichlorofluoromethane ND 3510 1600 46*3510 1580 45*1 73-145/31 75-01-4 Vinyl chloride ND 3510 3280 93 3510 2940 84 11 76-141/27 108-05-4 Vinyl Acetate ND 17600 9180 52 17600 6530 37*34 48-164/37 1330-20-7 Xylene (total)17200 10500 27100 94 10500 25600 80 6 80-129/30 m,p-Xylene 11700 7030 17800 87 7030 16900 74*5 80-128/30 95-47-6 o-Xylene 5480 3510 9310 109 3510 8690 91 7 80-132/30 CAS No.Surrogate Recoveries MS MSD FA15409-14 Limits 1868-53-7 Dibromofluoromethane 91%88%86%75-124% 2037-26-5 Toluene-D8 93%88%93%75-126% 460-00-4 4-Bromofluorobenzene 94%97%102%71-133% * = Outside of Control Limits. 160 of 208 FA15409 55.3.4 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-14MS F0064680.D 1 06/02/14 AH n/a n/a VF2136 FA15409-14MSD F0064681.D 1 06/03/14 AH n/a n/a VF2136 FA15409-14 F0064678.D 1 06/02/14 AH n/a n/a VF2136 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-4, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-12, FA15409-14, FA15409-18 CAS No.Surrogate Recoveries MS MSD FA15409-14 Limits 17060-07-0 1,2-Dichloroethane-D4 79%78%81%72-135% (a) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 161 of 208 FA15409 55.3.4 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-9MS F0064692.D 1 06/03/14 AH n/a n/a VF2137 FA15409-9MSD F0064693.D 1 06/03/14 AH n/a n/a VF2137 FA15409-9 F0064691.D 1 06/03/14 AH n/a n/a VF2137 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-3, FA15409-9 FA15409-9 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 100-41-4 Ethylbenzene 2720 3630 6090 93 3630 6090 93 0 77-123/31 91-20-3 Naphthalene 1680 3630 5690 110 3630 5420 103 5 79-129/33 95-63-6 1,2,4-Trimethylbenzene 6510 3630 9380 79 3630 9380 79 0 74-123/34 108-67-8 1,3,5-Trimethylbenzene 1900 3630 5230 92 3630 5180 90 1 73-122/33 108-88-3 Toluene 13100 3630 15400 63* a 3630 15500 66* a 1 76-124/30 1330-20-7 Xylene (total)16400 10900 26200 90 10900 25000 79*5 80-129/30 m,p-Xylene 11000 7270 17300 87 7270 16400 74*5 80-128/30 95-47-6 o-Xylene 5380 3630 8910 97 3630 8640 90 3 80-132/30 CAS No.Surrogate Recoveries MS MSD FA15409-9 Limits 1868-53-7 Dibromofluoromethane 91%90%85%75-124% 2037-26-5 Toluene-D8 88%88%89%75-126% 460-00-4 4-Bromofluorobenzene 98%99%97%71-133% 17060-07-0 1,2-Dichloroethane-D4 81%82%85%72-135% (a) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 162 of 208 FA15409 55.3.5 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15510-10MS F0064715.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10MSD F0064716.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10 a F0064712.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 FA15510-10 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 67-64-1 Acetone 180 U 1290 1090 84 1290 1300 100 18 61-152/27 71-43-2 Benzene 18 U 258 182 70*259 202 78 10 76-126/26 108-86-1 Bromobenzene 18 U 258 129 50*259 143 55*10 76-122/32 74-97-5 Bromochloromethane 18 U 258 208 81 259 219 85 5 77-120/24 75-27-4 Bromodichloromethane 18 U 258 134 52*259 165 64*21 74-130/25 75-25-2 Bromoform 18 U 258 75.1 29*259 103 40*31*76-127/26 104-51-8 n-Butylbenzene 18 U 258 59.8 23*259 73.9 29*21 71-128/35 135-98-8 sec-Butylbenzene 18 U 258 81.9 32*259 99.8 39*20 79-135/34 98-06-6 tert-Butylbenzene 18 U 258 94.3 37*259 114 44*19 77-133/34 108-90-7 Chlorobenzene 18 U 258 145 56*259 159 61*9 81-129/29 75-00-3 Chloroethane 18 U 258 190 74 259 244 94 25 68-133/29 67-66-3 Chloroform 18 U 258 185 72 259 208 80 12 72-123/26 95-49-8 o-Chlorotoluene 18 U 258 111 43*259 132 51*17 77-129/33 106-43-4 p-Chlorotoluene 18 U 258 117 45*259 136 53*15 80-134/33 56-23-5 Carbon tetrachloride 18 U 258 128 50*259 158 61*21 78-133/29 75-34-3 1,1-Dichloroethane 18 U 258 195 76 259 217 84 11 73-125/27 75-35-4 1,1-Dichloroethylene 18 U 258 205 79*259 227 88 10 81-136/28 563-58-6 1,1-Dichloropropene 18 U 258 173 67*259 193 75 11 75-130/28 106-93-4 1,2-Dibromoethane 18 U 258 170 66*259 193 75*13 77-126/26 107-06-2 1,2-Dichloroethane 18 U 258 201 78 259 227 88 12 74-128/23 78-87-5 1,2-Dichloropropane 18 U 258 188 73*259 210 81 11 74-125/25 142-28-9 1,3-Dichloropropane 18 U 258 178 69*259 199 77 11 76-122/26 108-20-3 Di-Isopropyl ether 18 U 258 196 76 259 228 88 15 75-122/25 594-20-7 2,2-Dichloropropane 18 U 258 203 79 259 225 87 10 77-133/28 124-48-1 Dibromochloromethane 18 U 258 107 41*259 139 54*26 76-127/27 75-71-8 Dichlorodifluoromethane 18 U 258 169 65*259 194 75 14 68-168/29 156-59-2 cis-1,2-Dichloroethylene 18 U 258 186 72*259 193 75 4 74-126/26 10061-01-5 cis-1,3-Dichloropropene 18 U 258 121 47*259 145 56*18 80-123/26 541-73-1 m-Dichlorobenzene 18 U 258 98.0 38*259 119 46*19 81-129/33 95-50-1 o-Dichlorobenzene 18 U 258 95.7 37*259 119 46*22 80-129/32 106-46-7 p-Dichlorobenzene 18 U 258 90.7 35*259 109 42*18 76-130/32 156-60-5 trans-1,2-Dichloroethylene 18 U 258 183 71 259 210 81 14 70-127/27 10061-02-6 trans-1,3-Dichloropropene 18 U 258 137 53*259 160 62*15 75-131/28 64-17-5 Ethyl alcohol 1400 U 5170 3560 69 5180 4940 95 32 53-154/42 100-41-4 Ethylbenzene 18 U 258 133 51*259 148 57*11 77-123/31 591-78-6 2-Hexanone 90 U 1290 954 74 1290 1120 87 16 72-133/26 * = Outside of Control Limits. 163 of 208 FA15409 55.3.6 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15510-10MS F0064715.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10MSD F0064716.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10 a F0064712.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 FA15510-10 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 98-82-8 Isopropylbenzene 18 U 258 112 43*259 128 49*13 80-136/32 99-87-6 p-Isopropyltoluene 18 U 258 76.9 30*259 95.8 37*22 77-131/34 108-10-1 4-Methyl-2-pentanone 90 U 1290 1050 81 1290 1130 87 7 76-132/26 74-83-9 Methyl bromide 18 U 258 172 67 259 205 79 18 65-139/31 74-87-3 Methyl chloride 18 U 258 178 69*259 215 83 19 71-144/27 75-09-2 Methylene chloride 36 U 258 254 98 259 276 107 8 74-137/28 78-93-3 Methyl ethyl ketone 90 U 1290 1020 79 1290 1140 88 11 75-137/25 1634-04-4 Methyl Tert Butyl Ether 18 U 258 209 81 259 235 91 12 77-120/24 91-20-3 Naphthalene 18 U 258 64.0 25*259 87.6 34*31 79-129/33 103-65-1 n-Propylbenzene 18 U 258 114 44*259 127 49*11 80-135/33 100-42-5 Styrene 18 U 258 85.2 33*259 113 44*28 78-125/30 630-20-6 1,1,1,2-Tetrachloroethane 18 U 258 131 51*259 155 60*17 78-126/27 71-55-6 1,1,1-Trichloroethane 18 U 258 184 71 259 197 76 7 70-129/27 79-34-5 1,1,2,2-Tetrachloroethane 18 U 258 188 73 259 202 78 7 71-126/30 79-00-5 1,1,2-Trichloroethane 18 U 258 178 69*259 201 78 12 74-124/28 87-61-6 1,2,3-Trichlorobenzene 18 U 258 39.7 15*259 53.4 21*29 77-128/35 96-18-4 1,2,3-Trichloropropane 18 U 258 197 76 259 211 81 7 74-127/27 120-82-1 1,2,4-Trichlorobenzene 18 U 258 43.6 17*259 57.3 22*27 78-130/34 95-63-6 1,2,4-Trimethylbenzene 18 U 258 103 40*259 118 46*14 74-123/34 108-67-8 1,3,5-Trimethylbenzene 18 U 258 96.3 37*259 117 45*19 73-122/33 127-18-4 Tetrachloroethylene 18 U 258 126 49*259 147 57*15 79-130/31 108-88-3 Toluene 18 U 258 157 61*259 166 64*6 76-124/30 79-01-6 Trichloroethylene 18 U 258 179 69*259 198 76 10 75-128/27 75-69-4 Trichlorofluoromethane 18 U 258 194 75 259 220 85 13 73-145/31 75-01-4 Vinyl chloride 18 U 258 186 72*259 210 81 12 76-141/27 108-05-4 Vinyl Acetate 90 U 1290 57.2 4*1290 66.3 5*15 48-164/37 1330-20-7 Xylene (total)54 U 775 407 53*777 457 59*12 80-129/30 m,p-Xylene 36 U 517 271 52*518 307 59*12 80-128/30 95-47-6 o-Xylene 18 U 258 136 53*259 150 58*10 80-132/30 CAS No.Surrogate Recoveries MS MSD FA15510-10 Limits 1868-53-7 Dibromofluoromethane 93%93%95%75-124% 2037-26-5 Toluene-D8 89%90%94%75-126% 460-00-4 4-Bromofluorobenzene 101%101%107%71-133% * = Outside of Control Limits. 164 of 208 FA15409 55.3.6 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15510-10MS F0064715.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10MSD F0064716.D 1 06/04/14 AH n/a n/a VF2138 FA15510-10 a F0064712.D 1 06/04/14 AH n/a n/a VF2138 The QC reported here applies to the following samples:Method: SW846 8260B FA15409-5 CAS No.Surrogate Recoveries MS MSD FA15510-10 Limits 17060-07-0 1,2-Dichloroethane-D4 94%97%101%72-135% (a) Confirmation run for internal standard areas. * = Outside of Control Limits. 165 of 208 FA15409 55.3.6 Accutest LabLink@151826 11:13 17-Jun-2014 GC/MS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Southeast Section 6 166 of 208 FA15409 6 Method Blank Summary Page 1 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-MB X035110.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 50 10 ug/l 95-57-8 2-Chlorophenol ND 5.0 0.52 ug/l 59-50-7 4-Chloro-3-methyl phenol ND 5.0 0.50 ug/l 120-83-2 2,4-Dichlorophenol ND 5.0 0.58 ug/l 105-67-9 2,4-Dimethylphenol ND 5.0 0.50 ug/l 51-28-5 2,4-Dinitrophenol ND 25 5.4 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l 95-48-7 2-Methylphenol ND 5.0 0.50 ug/l 3&4-Methylphenol ND 5.0 1.2 ug/l 88-75-5 2-Nitrophenol ND 5.0 0.60 ug/l 100-02-7 4-Nitrophenol ND 25 5.0 ug/l 87-86-5 Pentachlorophenol ND 25 5.0 ug/l 108-95-2 Phenol ND 5.0 0.50 ug/l 88-06-2 2,4,6-Trichlorophenol ND 5.0 0.55 ug/l 83-32-9 Acenaphthene ND 5.0 0.50 ug/l 208-96-8 Acenaphthylene ND 5.0 0.50 ug/l 120-12-7 Anthracene ND 5.0 0.62 ug/l 56-55-3 Benzo(a)anthracene ND 5.0 0.64 ug/l 50-32-8 Benzo(a)pyrene ND 5.0 0.65 ug/l 205-99-2 Benzo(b)fluoranthene ND 5.0 0.72 ug/l 191-24-2 Benzo(g,h,i)perylene ND 5.0 0.81 ug/l 207-08-9 Benzo(k)fluoranthene ND 5.0 0.51 ug/l 101-55-3 4-Bromophenyl phenyl ether ND 5.0 0.67 ug/l 85-68-7 Butyl benzyl phthalate ND 5.0 0.81 ug/l 100-51-6 Benzyl Alcohol ND 5.0 1.0 ug/l 91-58-7 2-Chloronaphthalene ND 5.0 0.56 ug/l 106-47-8 4-Chloroaniline ND 5.0 0.50 ug/l 218-01-9 Chrysene ND 5.0 0.72 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.55 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.69 ug/l 108-60-1 bis(2-Chloroisopropyl)ether ND 5.0 0.58 ug/l 7005-72-3 4-Chlorophenyl phenyl ether ND 5.0 0.54 ug/l 95-50-1 1,2-Dichlorobenzene ND 5.0 0.50 ug/l 122-66-7 1,2-Diphenylhydrazine ND 5.0 0.68 ug/l 541-73-1 1,3-Dichlorobenzene ND 5.0 0.50 ug/l 106-46-7 1,4-Dichlorobenzene ND 5.0 0.50 ug/l 167 of 208 FA15409 66.1.1 Method Blank Summary Page 2 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-MB X035110.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 CAS No.Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.90 ug/l 53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.81 ug/l 132-64-9 Dibenzofuran ND 5.0 0.53 ug/l 84-74-2 Di-n-butyl phthalate ND 5.0 1.0 ug/l 117-84-0 Di-n-octyl phthalate ND 5.0 1.0 ug/l 84-66-2 Diethyl phthalate ND 5.0 1.0 ug/l 131-11-3 Dimethyl phthalate ND 5.0 0.63 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.6 ug/l 206-44-0 Fluoranthene ND 5.0 0.70 ug/l 86-73-7 Fluorene ND 5.0 0.50 ug/l 118-74-1 Hexachlorobenzene ND 5.0 0.66 ug/l 87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l 77-47-4 Hexachlorocyclopentadiene ND 5.0 1.0 ug/l 67-72-1 Hexachloroethane ND 5.0 0.50 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.63 ug/l 78-59-1 Isophorone ND 5.0 0.50 ug/l 90-12-0 1-Methylnaphthalene ND 5.0 0.50 ug/l 91-57-6 2-Methylnaphthalene ND 5.0 0.53 ug/l 91-20-3 Naphthalene ND 5.0 0.50 ug/l 98-95-3 Nitrobenzene ND 5.0 0.50 ug/l 621-64-7 N-Nitroso-di-n-propylamine ND 5.0 0.50 ug/l 86-30-6 N-Nitrosodiphenylamine ND 5.0 0.53 ug/l 85-01-8 Phenanthrene ND 5.0 0.60 ug/l 129-00-0 Pyrene ND 5.0 0.82 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.50 ug/l CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 33%14-67% 4165-62-2 Phenol-d5 21%10-50% 118-79-6 2,4,6-Tribromophenol 74%33-118% 4165-60-0 Nitrobenzene-d5 67%42-108% 321-60-8 2-Fluorobiphenyl 69%40-106% 1718-51-0 Terphenyl-d14 83%39-121% 168 of 208 FA15409 66.1.1 Method Blank Summary Page 3 of 3 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-MB X035110.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: FA15409-24 CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q Total TIC, Semi-Volatile a 0 ug/l (a) No TICs detected. 169 of 208 FA15409 66.1.1 Method Blank Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MB X035126.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 830 170 ug/kg 95-57-8 2-Chlorophenol ND 170 17 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 170 17 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 17 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 18 ug/kg 51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg 95-48-7 2-Methylphenol ND 170 17 ug/kg 3&4-Methylphenol ND 170 33 ug/kg 88-75-5 2-Nitrophenol ND 170 17 ug/kg 100-02-7 4-Nitrophenol ND 830 130 ug/kg 87-86-5 Pentachlorophenol ND 830 130 ug/kg 108-95-2 Phenol ND 170 17 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 170 17 ug/kg 83-32-9 Acenaphthene ND 170 21 ug/kg 208-96-8 Acenaphthylene ND 170 17 ug/kg 120-12-7 Anthracene ND 170 17 ug/kg 56-55-3 Benzo(a)anthracene ND 170 17 ug/kg 50-32-8 Benzo(a)pyrene ND 170 17 ug/kg 205-99-2 Benzo(b)fluoranthene ND 170 17 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg 207-08-9 Benzo(k)fluoranthene ND 170 18 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg 85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg 100-51-6 Benzyl Alcohol ND 170 17 ug/kg 91-58-7 2-Chloronaphthalene ND 170 20 ug/kg 106-47-8 4-Chloroaniline ND 170 17 ug/kg 218-01-9 Chrysene ND 170 17 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 17 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 170 17 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 170 25 ug/kg 95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 170 19 ug/kg 541-73-1 1,3-Dichlorobenzene ND 170 17 ug/kg 106-46-7 1,4-Dichlorobenzene ND 170 17 ug/kg 170 of 208 FA15409 66.1.2 Method Blank Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MB X035126.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 CAS No.Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine ND 170 17 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 170 17 ug/kg 132-64-9 Dibenzofuran ND 170 17 ug/kg 84-74-2 Di-n-butyl phthalate ND 330 33 ug/kg 117-84-0 Di-n-octyl phthalate ND 170 33 ug/kg 84-66-2 Diethyl phthalate ND 330 33 ug/kg 131-11-3 Dimethyl phthalate ND 170 33 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg 206-44-0 Fluoranthene ND 170 17 ug/kg 86-73-7 Fluorene ND 170 17 ug/kg 118-74-1 Hexachlorobenzene ND 170 17 ug/kg 87-68-3 Hexachlorobutadiene ND 170 17 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 170 17 ug/kg 67-72-1 Hexachloroethane ND 170 17 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 170 17 ug/kg 78-59-1 Isophorone ND 170 17 ug/kg 90-12-0 1-Methylnaphthalene ND 170 17 ug/kg 91-57-6 2-Methylnaphthalene ND 170 17 ug/kg 91-20-3 Naphthalene ND 170 17 ug/kg 98-95-3 Nitrobenzene ND 170 17 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 170 17 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 17 ug/kg 85-01-8 Phenanthrene ND 170 17 ug/kg 129-00-0 Pyrene ND 170 17 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 170 17 ug/kg CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 66%40-102% 4165-62-2 Phenol-d5 78%41-100% 118-79-6 2,4,6-Tribromophenol 82%42-108% 4165-60-0 Nitrobenzene-d5 68%40-105% 321-60-8 2-Fluorobiphenyl 75%43-107% 1718-51-0 Terphenyl-d14 88%45-119% 171 of 208 FA15409 66.1.2 Method Blank Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MB L0678101.D 1 06/04/14 MV 06/03/14 OP51829 SL3461 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 CAS No.Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 830 170 ug/kg 95-57-8 2-Chlorophenol ND 170 17 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 170 17 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 17 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 18 ug/kg 51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg 95-48-7 2-Methylphenol ND 170 17 ug/kg 3&4-Methylphenol ND 170 33 ug/kg 88-75-5 2-Nitrophenol ND 170 17 ug/kg 100-02-7 4-Nitrophenol ND 830 130 ug/kg 87-86-5 Pentachlorophenol ND 830 130 ug/kg 108-95-2 Phenol ND 170 17 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 170 17 ug/kg 83-32-9 Acenaphthene ND 170 21 ug/kg 208-96-8 Acenaphthylene ND 170 17 ug/kg 120-12-7 Anthracene ND 170 17 ug/kg 56-55-3 Benzo(a)anthracene ND 170 17 ug/kg 50-32-8 Benzo(a)pyrene ND 170 17 ug/kg 205-99-2 Benzo(b)fluoranthene ND 170 17 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg 207-08-9 Benzo(k)fluoranthene ND 170 18 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg 85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg 100-51-6 Benzyl Alcohol ND 170 17 ug/kg 91-58-7 2-Chloronaphthalene ND 170 20 ug/kg 106-47-8 4-Chloroaniline ND 170 17 ug/kg 218-01-9 Chrysene ND 170 17 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 17 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 170 17 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 170 25 ug/kg 95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 170 19 ug/kg 541-73-1 1,3-Dichlorobenzene ND 170 17 ug/kg 106-46-7 1,4-Dichlorobenzene ND 170 17 ug/kg 172 of 208 FA15409 66.1.3 Method Blank Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MB L0678101.D 1 06/04/14 MV 06/03/14 OP51829 SL3461 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 CAS No.Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine ND 170 17 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 170 17 ug/kg 132-64-9 Dibenzofuran ND 170 17 ug/kg 84-74-2 Di-n-butyl phthalate ND 330 33 ug/kg 117-84-0 Di-n-octyl phthalate ND 170 33 ug/kg 84-66-2 Diethyl phthalate ND 330 33 ug/kg 131-11-3 Dimethyl phthalate ND 170 33 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg 206-44-0 Fluoranthene ND 170 17 ug/kg 86-73-7 Fluorene ND 170 17 ug/kg 118-74-1 Hexachlorobenzene ND 170 17 ug/kg 87-68-3 Hexachlorobutadiene ND 170 17 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 170 17 ug/kg 67-72-1 Hexachloroethane ND 170 17 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 170 17 ug/kg 78-59-1 Isophorone ND 170 17 ug/kg 90-12-0 1-Methylnaphthalene ND 170 17 ug/kg 91-57-6 2-Methylnaphthalene ND 170 17 ug/kg 91-20-3 Naphthalene ND 170 17 ug/kg 98-95-3 Nitrobenzene ND 170 17 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 170 17 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 17 ug/kg 85-01-8 Phenanthrene ND 170 17 ug/kg 129-00-0 Pyrene ND 170 17 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 170 17 ug/kg CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 63%40-102% 4165-62-2 Phenol-d5 74%41-100% 118-79-6 2,4,6-Tribromophenol 77%42-108% 4165-60-0 Nitrobenzene-d5 68%40-105% 321-60-8 2-Fluorobiphenyl 68%43-107% 1718-51-0 Terphenyl-d14 85%45-119% 173 of 208 FA15409 66.1.3 Blank Spike Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-BS X035109.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 65-85-0 Benzoic Acid 100 16.4 16 10-69 95-57-8 2-Chlorophenol 50 34.2 68 52-98 59-50-7 4-Chloro-3-methyl phenol 50 33.4 67 54-103 120-83-2 2,4-Dichlorophenol 50 35.6 71 53-103 105-67-9 2,4-Dimethylphenol 50 34.7 69 43-90 51-28-5 2,4-Dinitrophenol 100 87.5 88 44-112 534-52-1 4,6-Dinitro-o-cresol 100 98.4 98 66-121 95-48-7 2-Methylphenol 50 29.2 58 43-90 3&4-Methylphenol 100 48.7 49 36-88 88-75-5 2-Nitrophenol 50 36.8 74 53-102 100-02-7 4-Nitrophenol 100 25.6 26 18-62 87-86-5 Pentachlorophenol 100 96.7 97 61-115 108-95-2 Phenol 50 15.8 32 19-56 88-06-2 2,4,6-Trichlorophenol 50 42.3 85 59-107 83-32-9 Acenaphthene 50 42.4 85 61-107 208-96-8 Acenaphthylene 50 42.2 84 60-104 120-12-7 Anthracene 50 42.5 85 65-108 56-55-3 Benzo(a)anthracene 50 42.1 84 66-111 50-32-8 Benzo(a)pyrene 50 40.7 81 62-107 205-99-2 Benzo(b)fluoranthene 50 40.5 81 65-114 191-24-2 Benzo(g,h,i)perylene 50 44.4 89 66-116 207-08-9 Benzo(k)fluoranthene 50 44.4 89 65-114 101-55-3 4-Bromophenyl phenyl ether 50 36.8 74 65-109 85-68-7 Butyl benzyl phthalate 50 42.7 85 65-112 100-51-6 Benzyl Alcohol 50 29.2 58 46-94 91-58-7 2-Chloronaphthalene 50 40.8 82 57-103 106-47-8 4-Chloroaniline 50 39.7 79 49-105 218-01-9 Chrysene 50 43.7 87 66-111 111-91-1 bis(2-Chloroethoxy)methane 50 36.9 74 51-102 111-44-4 bis(2-Chloroethyl)ether 50 35.0 70 53-100 108-60-1 bis(2-Chloroisopropyl)ether 50 37.2 74 45-106 7005-72-3 4-Chlorophenyl phenyl ether 50 39.1 78 62-105 95-50-1 1,2-Dichlorobenzene 50 32.8 66 48-97 122-66-7 1,2-Diphenylhydrazine 50 40.8 82 61-110 541-73-1 1,3-Dichlorobenzene 50 33.1 66 45-95 106-46-7 1,4-Dichlorobenzene 50 34.3 69 45-98 * = Outside of Control Limits. 174 of 208 FA15409 66.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-BS X035109.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 91-94-1 3,3'-Dichlorobenzidine 50 41.9 84 46-117 53-70-3 Dibenzo(a,h)anthracene 50 44.2 88 66-119 132-64-9 Dibenzofuran 50 42.2 84 61-106 84-74-2 Di-n-butyl phthalate 50 41.7 83 65-107 117-84-0 Di-n-octyl phthalate 50 40.8 82 62-118 84-66-2 Diethyl phthalate 50 41.1 82 64-108 131-11-3 Dimethyl phthalate 50 39.5 79 63-106 117-81-7 bis(2-Ethylhexyl)phthalate 50 42.7 85 61-117 206-44-0 Fluoranthene 50 42.3 85 63-106 86-73-7 Fluorene 50 42.7 85 62-108 118-74-1 Hexachlorobenzene 50 41.4 83 63-108 87-68-3 Hexachlorobutadiene 50 35.0 70 42-102 77-47-4 Hexachlorocyclopentadiene 50 30.4 61 39-102 67-72-1 Hexachloroethane 50 33.2 66 42-100 193-39-5 Indeno(1,2,3-cd)pyrene 50 40.2 80 64-119 78-59-1 Isophorone 50 35.1 70 43-87 90-12-0 1-Methylnaphthalene 50 33.5 67 53-102 91-57-6 2-Methylnaphthalene 50 36.5 73 51-102 91-20-3 Naphthalene 50 35.8 72 47-100 98-95-3 Nitrobenzene 50 36.7 73 50-104 621-64-7 N-Nitroso-di-n-propylamine 50 38.5 77 52-104 86-30-6 N-Nitrosodiphenylamine 50 44.1 88 64-108 85-01-8 Phenanthrene 50 42.6 85 66-110 129-00-0 Pyrene 50 41.7 83 64-113 120-82-1 1,2,4-Trichlorobenzene 50 33.1 66 45-97 CAS No.Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 38%14-67% 4165-62-2 Phenol-d5 24%10-50% 118-79-6 2,4,6-Tribromophenol 88%33-118% 4165-60-0 Nitrobenzene-d5 73%42-108% 321-60-8 2-Fluorobiphenyl 83%40-106% 1718-51-0 Terphenyl-d14 88%39-121% * = Outside of Control Limits. 175 of 208 FA15409 66.2.1 Blank Spike Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-BS X035125.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 65-85-0 Benzoic Acid 3330 2150 65 36-118 95-57-8 2-Chlorophenol 1670 1020 61 48-104 59-50-7 4-Chloro-3-methyl phenol 1670 1090 65 52-108 120-83-2 2,4-Dichlorophenol 1670 1040 62 51-105 105-67-9 2,4-Dimethylphenol 1670 1080 65 43-96 51-28-5 2,4-Dinitrophenol 3330 3070 92 40-119 534-52-1 4,6-Dinitro-o-cresol 3330 3120 94 64-121 95-48-7 2-Methylphenol 1670 1090 65 46-107 3&4-Methylphenol 3330 2120 64 44-111 88-75-5 2-Nitrophenol 1670 999 60 49-104 100-02-7 4-Nitrophenol 3330 2710 81 56-116 87-86-5 Pentachlorophenol 3330 3100 93 61-114 108-95-2 Phenol 1670 1170 70 45-110 88-06-2 2,4,6-Trichlorophenol 1670 1230 74 56-109 83-32-9 Acenaphthene 1670 1220 73 56-109 208-96-8 Acenaphthylene 1670 1210 73 56-106 120-12-7 Anthracene 1670 1280 77 61-110 56-55-3 Benzo(a)anthracene 1670 1310 79 66-111 50-32-8 Benzo(a)pyrene 1670 1270 76 59-104 205-99-2 Benzo(b)fluoranthene 1670 1240 74 67-113 191-24-2 Benzo(g,h,i)perylene 1670 1400 84 67-113 207-08-9 Benzo(k)fluoranthene 1670 1370 82 67-114 101-55-3 4-Bromophenyl phenyl ether 1670 1050 63 62-110 85-68-7 Butyl benzyl phthalate 1670 1340 80 65-113 100-51-6 Benzyl Alcohol 1670 1070 64 53-108 91-58-7 2-Chloronaphthalene 1670 1150 69 53-106 106-47-8 4-Chloroaniline 1670 1140 68 30-115 218-01-9 Chrysene 1670 1370 82 65-112 111-91-1 bis(2-Chloroethoxy)methane 1670 1020 61 48-105 111-44-4 bis(2-Chloroethyl)ether 1670 855 51 46-103 108-60-1 bis(2-Chloroisopropyl)ether 1670 952 57 40-110 7005-72-3 4-Chlorophenyl phenyl ether 1670 1180 71 58-106 95-50-1 1,2-Dichlorobenzene 1670 939 56 44-102 122-66-7 1,2-Diphenylhydrazine 1670 1240 74 58-112 541-73-1 1,3-Dichlorobenzene 1670 947 57 42-100 106-46-7 1,4-Dichlorobenzene 1670 993 60 40-106 * = Outside of Control Limits. 176 of 208 FA15409 66.2.2 Blank Spike Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-BS X035125.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 91-94-1 3,3'-Dichlorobenzidine 1670 1390 83 36-114 53-70-3 Dibenzo(a,h)anthracene 1670 1380 83 68-115 132-64-9 Dibenzofuran 1670 1220 73 57-108 84-74-2 Di-n-butyl phthalate 1670 1300 78 63-108 117-84-0 Di-n-octyl phthalate 1670 1270 76 64-119 84-66-2 Diethyl phthalate 1670 1280 77 61-109 131-11-3 Dimethyl phthalate 1670 1220 73 59-108 117-81-7 bis(2-Ethylhexyl)phthalate 1670 1330 80 64-115 206-44-0 Fluoranthene 1670 1320 79 60-108 86-73-7 Fluorene 1670 1250 75 58-109 118-74-1 Hexachlorobenzene 1670 1250 75 59-111 87-68-3 Hexachlorobutadiene 1670 1000 60 41-108 77-47-4 Hexachlorocyclopentadiene 1670 987 59 49-110 67-72-1 Hexachloroethane 1670 962 58 40-105 193-39-5 Indeno(1,2,3-cd)pyrene 1670 1250 75 66-116 78-59-1 Isophorone 1670 1010 61 42-89 90-12-0 1-Methylnaphthalene 1670 958 57 49-106 91-57-6 2-Methylnaphthalene 1670 1050 63 47-106 91-20-3 Naphthalene 1670 999 60 44-104 98-95-3 Nitrobenzene 1670 983 59 43-108 621-64-7 N-Nitroso-di-n-propylamine 1670 1090 65 48-108 86-30-6 N-Nitrosodiphenylamine 1670 1320 79 62-110 85-01-8 Phenanthrene 1670 1270 76 63-111 129-00-0 Pyrene 1670 1250 75 65-115 120-82-1 1,2,4-Trichlorobenzene 1670 959 58 45-100 CAS No.Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 61%40-102% 4165-62-2 Phenol-d5 68%41-100% 118-79-6 2,4,6-Tribromophenol 80%42-108% 4165-60-0 Nitrobenzene-d5 58%40-105% 321-60-8 2-Fluorobiphenyl 71%43-107% 1718-51-0 Terphenyl-d14 82%45-119% * = Outside of Control Limits. 177 of 208 FA15409 66.2.2 Blank Spike Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-BS L0678100.D 1 06/04/14 MV 06/03/14 OP51829 SL3461 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 65-85-0 Benzoic Acid 3330 2050 62 36-118 95-57-8 2-Chlorophenol 1670 985 59 48-104 59-50-7 4-Chloro-3-methyl phenol 1670 1060 64 52-108 120-83-2 2,4-Dichlorophenol 1670 1020 61 51-105 105-67-9 2,4-Dimethylphenol 1670 1030 62 43-96 51-28-5 2,4-Dinitrophenol 3330 2560 77 40-119 534-52-1 4,6-Dinitro-o-cresol 3330 2850 86 64-121 95-48-7 2-Methylphenol 1670 1020 61 46-107 3&4-Methylphenol 3330 1960 59 44-111 88-75-5 2-Nitrophenol 1670 1000 60 49-104 100-02-7 4-Nitrophenol 3330 2430 73 56-116 87-86-5 Pentachlorophenol 3330 2750 83 61-114 108-95-2 Phenol 1670 1090 65 45-110 88-06-2 2,4,6-Trichlorophenol 1670 1110 67 56-109 83-32-9 Acenaphthene 1670 1110 67 56-109 208-96-8 Acenaphthylene 1670 1100 66 56-106 120-12-7 Anthracene 1670 1190 71 61-110 56-55-3 Benzo(a)anthracene 1670 1230 74 66-111 50-32-8 Benzo(a)pyrene 1670 1230 74 59-104 205-99-2 Benzo(b)fluoranthene 1670 1230 74 67-113 191-24-2 Benzo(g,h,i)perylene 1670 1290 77 67-113 207-08-9 Benzo(k)fluoranthene 1670 1240 74 67-114 101-55-3 4-Bromophenyl phenyl ether 1670 958 57*62-110 85-68-7 Butyl benzyl phthalate 1670 1280 77 65-113 100-51-6 Benzyl Alcohol 1670 1060 64 53-108 91-58-7 2-Chloronaphthalene 1670 1040 62 53-106 106-47-8 4-Chloroaniline 1670 1130 68 30-115 218-01-9 Chrysene 1670 1290 77 65-112 111-91-1 bis(2-Chloroethoxy)methane 1670 1040 62 48-105 111-44-4 bis(2-Chloroethyl)ether 1670 1060 64 46-103 108-60-1 bis(2-Chloroisopropyl)ether 1670 991 59 40-110 7005-72-3 4-Chlorophenyl phenyl ether 1670 1090 65 58-106 95-50-1 1,2-Dichlorobenzene 1670 918 55 44-102 122-66-7 1,2-Diphenylhydrazine 1670 1150 69 58-112 541-73-1 1,3-Dichlorobenzene 1670 924 55 42-100 106-46-7 1,4-Dichlorobenzene 1670 961 58 40-106 * = Outside of Control Limits. 178 of 208 FA15409 66.2.3 Blank Spike Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-BS L0678100.D 1 06/04/14 MV 06/03/14 OP51829 SL3461 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 Spike BSP BSP CAS No.Compound ug/kg ug/kg %Limits 91-94-1 3,3'-Dichlorobenzidine 1670 1290 77 36-114 53-70-3 Dibenzo(a,h)anthracene 1670 1300 78 68-115 132-64-9 Dibenzofuran 1670 1140 68 57-108 84-74-2 Di-n-butyl phthalate 1670 1250 75 63-108 117-84-0 Di-n-octyl phthalate 1670 1280 77 64-119 84-66-2 Diethyl phthalate 1670 1170 70 61-109 131-11-3 Dimethyl phthalate 1670 1150 69 59-108 117-81-7 bis(2-Ethylhexyl)phthalate 1670 1300 78 64-115 206-44-0 Fluoranthene 1670 1230 74 60-108 86-73-7 Fluorene 1670 1160 70 58-109 118-74-1 Hexachlorobenzene 1670 1170 70 59-111 87-68-3 Hexachlorobutadiene 1670 946 57 41-108 77-47-4 Hexachlorocyclopentadiene 1670 944 57 49-110 67-72-1 Hexachloroethane 1670 941 56 40-105 193-39-5 Indeno(1,2,3-cd)pyrene 1670 1180 71 66-116 78-59-1 Isophorone 1670 1030 62 42-89 90-12-0 1-Methylnaphthalene 1670 946 57 49-106 91-57-6 2-Methylnaphthalene 1670 1040 62 47-106 91-20-3 Naphthalene 1670 973 58 44-104 98-95-3 Nitrobenzene 1670 988 59 43-108 621-64-7 N-Nitroso-di-n-propylamine 1670 1060 64 48-108 86-30-6 N-Nitrosodiphenylamine 1670 1230 74 62-110 85-01-8 Phenanthrene 1670 1210 73 63-111 129-00-0 Pyrene 1670 1170 70 65-115 120-82-1 1,2,4-Trichlorobenzene 1670 921 55 45-100 CAS No.Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 59%40-102% 4165-62-2 Phenol-d5 63%41-100% 118-79-6 2,4,6-Tribromophenol 72%42-108% 4165-60-0 Nitrobenzene-d5 59%40-105% 321-60-8 2-Fluorobiphenyl 63%43-107% 1718-51-0 Terphenyl-d14 78%45-119% * = Outside of Control Limits. 179 of 208 FA15409 66.2.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-MS X035112.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 OP51824-MSD X035113.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 FA15334-1 X035111.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 FA15334-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 65-85-0 Benzoic Acid 48 U 190 50.4 26 190 62.6 33 22 10-69/39 95-57-8 2-Chlorophenol 4.8 U 95.2 66.5 70 95.2 69.6 73 5 52-98/25 59-50-7 4-Chloro-3-methyl phenol 4.8 U 95.2 65.9 69 95.2 68.7 72 4 54-103/23 120-83-2 2,4-Dichlorophenol 4.8 U 95.2 65.4 69 95.2 68.5 72 5 53-103/26 105-67-9 2,4-Dimethylphenol 4.8 U 95.2 61.6 65 95.2 65.6 69 6 43-90/27 51-28-5 2,4-Dinitrophenol 24 U 190 171 90 190 172 90 1 44-112/25 534-52-1 4,6-Dinitro-o-cresol 9.5 U 190 189 99 190 191 100 1 66-121/23 95-48-7 2-Methylphenol 4.8 U 95.2 60.8 64 95.2 66.1 69 8 43-90/28 3&4-Methylphenol 4.8 U 190 108 57 190 120 63 11 36-88/28 88-75-5 2-Nitrophenol 4.8 U 95.2 66.4 70 95.2 68.6 72 3 53-102/29 100-02-7 4-Nitrophenol 24 U 190 80.8 42 190 89.9 47 11 18-62/33 87-86-5 Pentachlorophenol 24 U 190 189 99 190 191 100 1 61-115/26 108-95-2 Phenol 4.8 U 95.2 41.7 44 95.2 47.6 50 13 19-56/35 88-06-2 2,4,6-Trichlorophenol 4.8 U 95.2 78.4 82 95.2 79.8 84 2 59-107/23 83-32-9 Acenaphthene 4.8 U 95.2 81.5 86 95.2 82.4 87 1 61-107/22 208-96-8 Acenaphthylene 4.8 U 95.2 80.3 84 95.2 81.2 85 1 60-104/22 120-12-7 Anthracene 4.8 U 95.2 83.0 87 95.2 82.7 87 0 65-108/20 56-55-3 Benzo(a)anthracene 4.8 U 95.2 81.7 86 95.2 83.1 87 2 66-111/22 50-32-8 Benzo(a)pyrene 4.8 U 95.2 78.8 83 95.2 79.1 83 0 62-107/23 205-99-2 Benzo(b)fluoranthene 4.8 U 95.2 79.7 84 95.2 80.3 84 1 65-114/23 191-24-2 Benzo(g,h,i)perylene 4.8 U 95.2 86.3 91 95.2 86.6 91 0 66-116/23 207-08-9 Benzo(k)fluoranthene 4.8 U 95.2 85.7 90 95.2 87.6 92 2 65-114/24 101-55-3 4-Bromophenyl phenyl ether 4.8 U 95.2 71.3 75 95.2 72.2 76 1 65-109/23 85-68-7 Butyl benzyl phthalate 4.8 U 95.2 80.9 85 95.2 82.3 86 2 65-112/24 100-51-6 Benzyl Alcohol 4.8 U 95.2 60.9 64 95.2 65.6 69 7 46-94/27 91-58-7 2-Chloronaphthalene 4.8 U 95.2 77.4 81 95.2 78.7 83 2 57-103/23 106-47-8 4-Chloroaniline 4.8 U 95.2 71.4 75 95.2 73.7 77 3 49-105/27 218-01-9 Chrysene 4.8 U 95.2 85.6 90 95.2 87.0 91 2 66-111/22 111-91-1 bis(2-Chloroethoxy)methane 4.8 U 95.2 66.0 69 95.2 69.6 73 5 51-102/28 111-44-4 bis(2-Chloroethyl)ether 4.8 U 95.2 56.7 60 95.2 61.1 64 7 53-100/27 108-60-1 bis(2-Chloroisopropyl)ether 4.8 U 95.2 65.8 69 95.2 68.9 72 5 45-106/26 7005-72-3 4-Chlorophenyl phenyl ether 4.8 U 95.2 76.3 80 95.2 77.4 81 1 62-105/20 95-50-1 1,2-Dichlorobenzene 4.8 U 95.2 63.8 67 95.2 67.1 70 5 48-97/24 122-66-7 1,2-Diphenylhydrazine 4.8 U 95.2 84.0 88 95.2 78.2 82 7 61-110/24 541-73-1 1,3-Dichlorobenzene 4.8 U 95.2 64.5 68 95.2 69.5 73 7 45-95/25 106-46-7 1,4-Dichlorobenzene 4.8 U 95.2 68.0 71 95.2 73.4 77 8 45-98/25 * = Outside of Control Limits. 180 of 208 FA15409 66.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51824-MS X035112.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 OP51824-MSD X035113.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 FA15334-1 X035111.D 1 06/03/14 MV 06/02/14 OP51824 SX1644 The QC reported here applies to the following samples:Method: EPA 625 FA15409-24 FA15334-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 91-94-1 3,3'-Dichlorobenzidine 4.8 U 95.2 73.2 77 95.2 64.4 68 13 46-117/29 53-70-3 Dibenzo(a,h)anthracene 4.8 U 95.2 85.3 90 95.2 87.6 92 3 66-119/24 132-64-9 Dibenzofuran 4.8 U 95.2 82.9 87 95.2 82.4 87 1 61-106/21 84-74-2 Di-n-butyl phthalate 4.8 U 95.2 80.1 84 95.2 81.9 86 2 65-107/21 117-84-0 Di-n-octyl phthalate 4.8 U 95.2 77.4 81 95.2 78.6 83 2 62-118/24 84-66-2 Diethyl phthalate 4.8 U 95.2 80.7 85 95.2 80.1 84 1 64-108/21 131-11-3 Dimethyl phthalate 4.8 U 95.2 77.3 81 95.2 78.0 82 1 63-106/22 117-81-7 bis(2-Ethylhexyl)phthalate 4.8 U 95.2 81.4 85 95.2 82.8 87 2 61-117/23 206-44-0 Fluoranthene 4.8 U 95.2 82.1 86 95.2 83.8 88 2 63-106/21 86-73-7 Fluorene 4.8 U 95.2 82.2 86 95.2 82.5 87 0 62-108/20 118-74-1 Hexachlorobenzene 4.8 U 95.2 81.7 86 95.2 81.5 86 0 63-108/22 87-68-3 Hexachlorobutadiene 4.8 U 95.2 68.3 72 95.2 73.0 77 7 42-102/28 77-47-4 Hexachlorocyclopentadiene 4.8 U 95.2 57.3 60 95.2 64.4 68 12 39-102/29 67-72-1 Hexachloroethane 4.8 U 95.2 65.9 69 95.2 71.0 75 7 42-100/29 193-39-5 Indeno(1,2,3-cd)pyrene 4.8 U 95.2 77.3 81 95.2 79.9 84 3 64-119/24 78-59-1 Isophorone 4.8 U 95.2 63.2 66 95.2 67.1 70 6 43-87/25 90-12-0 1-Methylnaphthalene 4.8 U 95.2 61.8 65 95.2 65.5 69 6 53-102/27 91-57-6 2-Methylnaphthalene 4.8 U 95.2 68.8 72 95.2 72.1 76 5 51-102/26 91-20-3 Naphthalene 4.8 U 95.2 66.8 70 95.2 71.1 75 6 47-100/29 98-95-3 Nitrobenzene 4.8 U 95.2 66.3 70 95.2 69.6 73 5 50-104/28 621-64-7 N-Nitroso-di-n-propylamine 4.8 U 95.2 68.2 72 95.2 71.2 75 4 52-104/25 86-30-6 N-Nitrosodiphenylamine 4.8 U 95.2 84.7 89 95.2 85.1 89 0 64-108/23 85-01-8 Phenanthrene 4.8 U 95.2 82.6 87 95.2 84.1 88 2 66-110/21 129-00-0 Pyrene 4.8 U 95.2 80.3 84 95.2 81.5 86 1 64-113/23 120-82-1 1,2,4-Trichlorobenzene 4.8 U 95.2 63.9 67 95.2 67.3 71 5 45-97/28 CAS No.Surrogate Recoveries MS MSD FA15334-1 Limits 367-12-4 2-Fluorophenol 51%58%36%14-67% 4165-62-2 Phenol-d5 37%44%23%10-50% 118-79-6 2,4,6-Tribromophenol 89%89%81%33-118% 4165-60-0 Nitrobenzene-d5 69%73%71%42-108% 321-60-8 2-Fluorobiphenyl 83%85%74%40-106% 1718-51-0 Terphenyl-d14 91%91%93%39-121% * = Outside of Control Limits. 181 of 208 FA15409 66.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MS X035128.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 OP51829-MSD X035129.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 FA15386-3 X035127.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 FA15386-3 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 65-85-0 Benzoic Acid 1000 U 4070 476 12*4110 485 12*2 36-118/41 95-57-8 2-Chlorophenol 200 U 2030 1130 56 2050 1140 55 1 48-104/26 59-50-7 4-Chloro-3-methyl phenol 200 U 2030 1280 63 2050 1260 61 2 52-108/21 120-83-2 2,4-Dichlorophenol 200 U 2030 1210 59 2050 1170 57 3 51-105/27 105-67-9 2,4-Dimethylphenol 200 U 2030 1250 61 2050 1220 59 2 43-96/23 51-28-5 2,4-Dinitrophenol 1000 U 4070 2330 57 4110 2180 53 7 40-119/32 534-52-1 4,6-Dinitro-o-cresol 410 U 4070 3330 82 4110 3220 78 3 64-121/29 95-48-7 2-Methylphenol 200 U 2030 1230 60 2050 1210 59 2 46-107/24 3&4-Methylphenol 200 U 4070 2410 59 4110 2360 57 2 44-111/24 88-75-5 2-Nitrophenol 200 U 2030 1140 56 2050 1150 56 1 49-104/27 100-02-7 4-Nitrophenol 1000 U 4070 2900 71 4110 2880 70 1 56-116/23 87-86-5 Pentachlorophenol 1000 U 4070 3350 82 4110 3310 81 1 61-114/23 108-95-2 Phenol 200 U 2030 1300 64 2050 1290 63 1 45-110/24 88-06-2 2,4,6-Trichlorophenol 200 U 2030 1440 71 2050 1370 67 5 56-109/25 83-32-9 Acenaphthene 200 U 2030 1440 71 2050 1400 68 3 56-109/23 208-96-8 Acenaphthylene 200 U 2030 1420 70 2050 1380 67 3 56-106/23 120-12-7 Anthracene 200 U 2030 1470 72 2050 1440 70 2 61-110/21 56-55-3 Benzo(a)anthracene 200 U 2030 1480 73 2050 1450 71 2 66-111/23 50-32-8 Benzo(a)pyrene 200 U 2030 1440 71 2050 1420 69 1 59-104/23 205-99-2 Benzo(b)fluoranthene 200 U 2030 1400 69 2050 1390 68 1 67-113/24 191-24-2 Benzo(g,h,i)perylene 200 U 2030 1570 77 2050 1550 75 1 67-113/21 207-08-9 Benzo(k)fluoranthene 200 U 2030 1550 76 2050 1560 76 1 67-114/22 101-55-3 4-Bromophenyl phenyl ether 200 U 2030 1240 61*2050 1210 59*2 62-110/21 85-68-7 Butyl benzyl phthalate 200 U 2030 1460 72 2050 1420 69 3 65-113/20 100-51-6 Benzyl Alcohol 200 U 2030 1130 56 2050 1190 58 5 53-108/24 91-58-7 2-Chloronaphthalene 200 U 2030 1370 67 2050 1310 64 4 53-106/23 106-47-8 4-Chloroaniline 200 U 2030 1270 62 2050 1320 64 4 30-115/30 218-01-9 Chrysene 200 U 2030 1560 77 2050 1530 74 2 65-112/25 111-91-1 bis(2-Chloroethoxy)methane 200 U 2030 1170 58 2050 1170 57 0 48-105/24 111-44-4 bis(2-Chloroethyl)ether 200 U 2030 922 45*2050 934 45*1 46-103/27 108-60-1 bis(2-Chloroisopropyl)ether 200 U 2030 1050 52 2050 1070 52 2 40-110/25 7005-72-3 4-Chlorophenyl phenyl ether 200 U 2030 1370 67 2050 1350 66 1 58-106/21 95-50-1 1,2-Dichlorobenzene 200 U 2030 993 49 2050 1040 51 5 44-102/28 122-66-7 1,2-Diphenylhydrazine 200 U 2030 1450 71 2050 1320 64 9 58-112/22 541-73-1 1,3-Dichlorobenzene 200 U 2030 994 49 2050 1030 50 4 42-100/30 106-46-7 1,4-Dichlorobenzene 200 U 2030 1050 52 2050 1100 54 5 40-106/29 * = Outside of Control Limits. 182 of 208 FA15409 66.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51829-MS X035128.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 OP51829-MSD X035129.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 FA15386-3 X035127.D 1 06/04/14 MV 06/03/14 OP51829 SX1645 The QC reported here applies to the following samples:Method: SW846 8270D FA15409-11, FA15409-12, FA15409-13, FA15409-14 FA15386-3 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD 91-94-1 3,3'-Dichlorobenzidine 200 U 2030 1550 76 2050 1550 75 0 36-114/28 53-70-3 Dibenzo(a,h)anthracene 200 U 2030 1490 73 2050 1460 71 2 68-115/23 132-64-9 Dibenzofuran 200 U 2030 1390 68 2050 1400 68 1 57-108/22 84-74-2 Di-n-butyl phthalate 410 U 2030 1460 72 2050 1420 69 3 63-108/19 117-84-0 Di-n-octyl phthalate 200 U 2030 1370 67 2050 1360 66 1 64-119/21 84-66-2 Diethyl phthalate 410 U 2030 1470 72 2050 1420 69 3 61-109/20 131-11-3 Dimethyl phthalate 200 U 2030 1420 70 2050 1380 67 3 59-108/20 117-81-7 bis(2-Ethylhexyl)phthalate 410 U 2030 1460 72 2050 1450 71 1 64-115/23 206-44-0 Fluoranthene 200 U 2030 1500 74 2050 1460 71 3 60-108/25 86-73-7 Fluorene 200 U 2030 1480 73 2050 1420 69 4 58-109/21 118-74-1 Hexachlorobenzene 200 U 2030 1460 72 2050 1430 70 2 59-111/21 87-68-3 Hexachlorobutadiene 200 U 2030 1100 54 2050 1130 55 3 41-108/27 77-47-4 Hexachlorocyclopentadiene 200 U 2030 1090 54 2050 1080 53 1 49-110/31 67-72-1 Hexachloroethane 200 U 2030 999 49 2050 1040 51 4 40-105/32 193-39-5 Indeno(1,2,3-cd)pyrene 200 U 2030 1400 69 2050 1380 67 1 66-116/22 78-59-1 Isophorone 200 U 2030 1170 58 2050 1150 56 2 42-89/22 90-12-0 1-Methylnaphthalene 200 U 2030 1100 54 2050 1100 54 0 49-106/26 91-57-6 2-Methylnaphthalene 200 U 2030 1090 54 2050 1180 57 8 47-106/27 91-20-3 Naphthalene 200 U 2030 1130 56 2050 1150 56 2 44-104/27 98-95-3 Nitrobenzene 200 U 2030 1090 54 2050 1100 54 1 43-108/25 621-64-7 N-Nitroso-di-n-propylamine 200 U 2030 1260 62 2050 1210 59 4 48-108/27 86-30-6 N-Nitrosodiphenylamine 200 U 2030 1510 74 2050 1470 72 3 62-110/21 85-01-8 Phenanthrene 200 U 2030 1470 72 2050 1430 70 3 63-111/22 129-00-0 Pyrene 200 U 2030 1440 71 2050 1410 69 2 65-115/25 120-82-1 1,2,4-Trichlorobenzene 200 U 2030 1060 52 2050 1080 53 2 45-100/26 CAS No.Surrogate Recoveries MS MSD FA15386-3 Limits 367-12-4 2-Fluorophenol 56%56%56%40-102% 4165-62-2 Phenol-d5 64%62%65%41-100% 118-79-6 2,4,6-Tribromophenol 76%74%72%42-108% 4165-60-0 Nitrobenzene-d5 56%56%59%40-105% 321-60-8 2-Fluorobiphenyl 70%67%66%43-107% 1718-51-0 Terphenyl-d14 77%75%81%45-119% * = Outside of Control Limits. 183 of 208 FA15409 66.3.2 Accutest LabLink@151826 11:13 17-Jun-2014 GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Southeast Section 7 184 of 208 FA15409 7 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUU391-MB UU007896.D 1 06/02/14 AH n/a n/a GUU391 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-1, FA15409-2, FA15409-4, FA15409-5, FA15409-6, FA15409-7, FA15409-12, FA15409-13, FA15409-18 CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg CAS No.Surrogate Recoveries Limits 460-00-4 BFB 83%70-130% 460-00-4 BFB 77%70-130% 185 of 208 FA15409 77.1.1 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUU392-MB UU007930.D 1 06/03/14 MM n/a n/a GUU392 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-3, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-14 CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg CAS No.Surrogate Recoveries Limits 460-00-4 BFB 80%70-130% 460-00-4 BFB 75%70-130% 186 of 208 FA15409 77.1.2 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3417-MB UV064380.D 1 06/03/14 MM n/a n/a GUV3417 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-24 CAS No.Compound Result RL MDL Units Q C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l C9- C10 Aromatics (Unadj.)ND 100 35 ug/l CAS No.Surrogate Recoveries Limits 460-00-4 BFB 98%70-130% 460-00-4 BFB 101%70-130% 187 of 208 FA15409 77.1.3 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GQR3491-MB QR082022.D 1 06/03/14 MM n/a n/a GQR3491 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-16, FA15409-17, FA15409-19, FA15409-20, FA15409-21 CAS No.Compound Result RL MDL Units Q TPH-GRO (C6-C10)ND 5.0 2.5 mg/kg CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 102%56-149% 98-08-8 aaa-Trifluorotoluene 104%66-132% 188 of 208 FA15409 77.1.4 Blank Spike Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GQR3491-BS QR082021.D 1 06/03/14 MM n/a n/a GQR3491 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-16, FA15409-17, FA15409-19, FA15409-20, FA15409-21 Spike BSP BSP CAS No.Compound mg/kg mg/kg %Limits TPH-GRO (C6-C10)20 18.0 90 74-128 CAS No.Surrogate Recoveries BSP Limits 460-00-4 4-Bromofluorobenzene 99%56-149% 98-08-8 aaa-Trifluorotoluene 101%66-132% * = Outside of Control Limits. 189 of 208 FA15409 77.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUU391-BS UU007894.D 1 06/02/14 AH n/a n/a GUU391 GUU391-BSD UU007895.D 1 06/02/14 AH n/a n/a GUU391 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-1, FA15409-2, FA15409-4, FA15409-5, FA15409-6, FA15409-7, FA15409-12, FA15409-13, FA15409-18 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C5- C8 Aliphatics (Unadj.)12500 14900 119 14500 116 3 70-130/25 C9- C12 Aliphatics (Unadj.)8320 9880 119 9720 117 2 70-130/25 C9- C10 Aromatics (Unadj.)4160 3770 91 3760 90 0 70-130/25 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 88%86%70-130% 460-00-4 BFB 82%80%70-130% * = Outside of Control Limits. 190 of 208 FA15409 77.3.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUU392-BS UU007927.D 1 06/03/14 MM n/a n/a GUU392 GUU392-BSD UU007928.D 1 06/03/14 MM n/a n/a GUU392 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-3, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-14 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C5- C8 Aliphatics (Unadj.)12500 14600 117 14700 118 1 70-130/25 C9- C12 Aliphatics (Unadj.)8320 9470 114 9570 115 1 70-130/25 C9- C10 Aromatics (Unadj.)4160 3670 88 3820 92 4 70-130/25 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 85%85%70-130% 460-00-4 BFB 80%80%70-130% * = Outside of Control Limits. 191 of 208 FA15409 77.3.2 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3417-BS UV064377.D 1 06/03/14 MM n/a n/a GUV3417 GUV3417-BSD UV064378.D 1 06/03/14 MM n/a n/a GUV3417 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-24 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD C5- C8 Aliphatics (Unadj.)240 290 121 296 123 2 70-130/25 C9- C12 Aliphatics (Unadj.)160 167 104 161 101 4 70-130/25 C9- C10 Aromatics (Unadj.)80 80.8 101 81.7 102 1 70-130/25 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 118%111%70-130% 460-00-4 BFB 116%106%70-130% * = Outside of Control Limits. 192 of 208 FA15409 77.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-15MS QR082024.D 1 06/03/14 MM n/a n/a GQR3491 FA15409-15MSD QR082025.D 1 06/03/14 MM n/a n/a GQR3491 FA15409-15 QR082023.D 1 06/03/14 MM n/a n/a GQR3491 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-16, FA15409-17, FA15409-19, FA15409-20, FA15409-21 FA15409-15 Spike MS MS Spike MSD MSD Limits CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD TPH-GRO (C6-C10)ND 34.9 35.5 102 34.9 35.4 101 0 74-128/17 CAS No.Surrogate Recoveries MS MSD FA15409-15 Limits 460-00-4 4-Bromofluorobenzene 98%97%100%56-149% 98-08-8 aaa-Trifluorotoluene 99%99%102%66-132% * = Outside of Control Limits. 193 of 208 FA15409 77.4.1 Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15409-1DUP UU007921.D 1 06/02/14 AH n/a n/a GUU391 FA15409-1 UU007901.D 1 06/02/14 AH n/a n/a GUU391 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-1, FA15409-2, FA15409-4, FA15409-5, FA15409-6, FA15409-7, FA15409-12, FA15409-13, FA15409-18 FA15409-1 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits C5- C8 Aliphatics (Unadj.)2990 J ND 200*50 C9- C12 Aliphatics (Unadj.)3700 J ND 200*50 C9- C10 Aromatics (Unadj.)4010 J ND 200*50 CAS No.Surrogate Recoveries DUP FA15409-1 Limits 460-00-4 BFB 98%129%70-130% 460-00-4 BFB 90%118%70-130% * = Outside of Control Limits. 194 of 208 FA15409 77.5.1 Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15435-2DUP UU007941.D 1 06/03/14 MM n/a n/a GUU392 FA15435-2 UU007940.D 1 06/03/14 MM n/a n/a GUU392 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-3, FA15409-8, FA15409-9, FA15409-10, FA15409-11, FA15409-14 FA15435-2 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits C5- C8 Aliphatics (Unadj.)ND ND nc 50 C9- C12 Aliphatics (Unadj.)ND ND nc 50 C9- C10 Aromatics (Unadj.)ND ND nc 50 CAS No.Surrogate Recoveries DUP FA15435-2 Limits 460-00-4 BFB 118%111%70-130% 460-00-4 BFB 110%104%70-130% * = Outside of Control Limits. 195 of 208 FA15409 77.5.2 Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA15414-9DUP UV064405.D 1 06/04/14 MM n/a n/a GUV3417 FA15414-9 UV064396.D 1 06/03/14 MM n/a n/a GUV3417 The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1 FA15409-24 FA15414-9 DUP CAS No.Compound ug/l Q ug/l Q RPD Limits C5- C8 Aliphatics (Unadj.)ND 67.9 J 200*50 C9- C12 Aliphatics (Unadj.)ND ND nc 50 C9- C10 Aromatics (Unadj.)ND ND nc 50 CAS No.Surrogate Recoveries DUP FA15414-9 Limits 460-00-4 BFB 198%*97%70-130% 460-00-4 BFB 203%*100%70-130% * = Outside of Control Limits. 196 of 208 FA15409 77.5.3 Accutest LabLink@151826 11:13 17-Jun-2014 GC Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Southeast Section 8 197 of 208 FA15409 8 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51822-MB NN009014.D 1 06/05/14 NAF 06/02/14 OP51822 GNN396 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-24 CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)ND 200 150 ug/l C9-C18 Aliphatics ND 200 100 ug/l C19-C36 Aliphatics ND 200 100 ug/l CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 78%40-140% 580-13-2 2-Bromonaphthalene 83%40-140% 84-15-1 o-Terphenyl 77%40-140% 321-60-8 2-Fluorobiphenyl 84%40-140% 198 of 208 FA15409 88.1.1 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51816-MB NN009049.D 1 06/06/14 NAF 06/02/14 OP51816 GNN397 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-12, FA15409-13, FA15409-14 CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)ND 10000 7500 ug/kg C9-C18 Aliphatics ND 10000 5000 ug/kg C19-C36 Aliphatics ND 10000 5000 ug/kg CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 65%40-140% 580-13-2 2-Bromonaphthalene 88%40-140% 84-15-1 o-Terphenyl 62%40-140% 321-60-8 2-Fluorobiphenyl 93%40-140% 199 of 208 FA15409 88.1.2 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51928-MB NN009181.D 1 06/12/14 NG 06/10/14 OP51928 GNN401 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-11, FA15409-14 CAS No.Compound Result RL MDL Units Q C11-C22 Aromatics (Unadj.)ND 10000 7500 ug/kg C9-C18 Aliphatics ND 10000 5000 ug/kg C19-C36 Aliphatics ND 10000 5000 ug/kg CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 70%40-140% 580-13-2 2-Bromonaphthalene 89%40-140% 84-15-1 o-Terphenyl 64%40-140% 321-60-8 2-Fluorobiphenyl 86%40-140% 200 of 208 FA15409 88.1.3 Method Blank Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51815-MB WR5655.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-20, FA15409-21 CAS No.Compound Result RL MDL Units Q TPH (C10-C28)ND 4.2 2.5 mg/kg CAS No.Surrogate Recoveries Limits 84-15-1 o-Terphenyl 99%56-122% 201 of 208 FA15409 88.1.4 Blank Spike Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51815-BS WR5654.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-20, FA15409-21 Spike BSP BSP CAS No.Compound mg/kg mg/kg %Limits TPH (C10-C28)33.3 30.4 91 62-116 CAS No.Surrogate Recoveries BSP Limits 84-15-1 o-Terphenyl 109%56-122% * = Outside of Control Limits. 202 of 208 FA15409 88.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51822-BS a NN009012.D 1 06/05/14 NAF 06/02/14 OP51822 GNN396 OP51822-BSD a NN009013.D 1 06/05/14 NAF 06/02/14 OP51822 GNN396 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-24 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD C11-C22 Aromatics (Unadj.)1700 1650 97 1500 88 10 40-140/30 C9-C18 Aliphatics 600 391 65 344 57 13 40-140/30 C19-C36 Aliphatics 800 743 93 682 85 9 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 88%81%40-140% 580-13-2 2-Bromonaphthalene 92%87%40-140% 84-15-1 o-Terphenyl 80%73%40-140% 321-60-8 2-Fluorobiphenyl 86%82%40-140% Sample Compound Col #1 Col #2 Breakthrough Limit OP51822-BS 2-Methylnaphthalene 67.2 ND 0.0%5.0 OP51822-BS Naphthalene 58.5 ND 0.0%5.0 OP51822-BSD 2-Methylnaphthalene 59.6 ND 0.0%5.0 OP51822-BSD Naphthalene 52.2 ND 0.0%5.0 (a) Insufficient sample for batch duplicate. * = Outside of Control Limits. 203 of 208 FA15409 88.3.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51816-BS NN009047.D 1 06/06/14 NAF 06/02/14 OP51816 GNN397 OP51816-BSD NN009048.D 1 06/06/14 NAF 06/02/14 OP51816 GNN397 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-12, FA15409-13, FA15409-14 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C11-C22 Aromatics (Unadj.)85000 63800 75 66200 78 4 40-140/30 C9-C18 Aliphatics 30000 15700 52 17100 57 9 40-140/30 C19-C36 Aliphatics 40000 27800 70 29400 74 6 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 63%68%40-140% 580-13-2 2-Bromonaphthalene 87%83%40-140% 84-15-1 o-Terphenyl 61%63%40-140% 321-60-8 2-Fluorobiphenyl 85%84%40-140% Sample Compound Col #1 Col #2 Breakthrough Limit OP51816-BS 2-Methylnaphthalene 2600 ND 0.0%5.0 OP51816-BS Naphthalene 2380 ND 0.0%5.0 OP51816-BSD 2-Methylnaphthalene 2760 ND 0.0%5.0 OP51816-BSD Naphthalene 2530 ND 0.0%5.0 * = Outside of Control Limits. 204 of 208 FA15409 88.3.2 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51928-BS NN009179.D 1 06/12/14 NG 06/10/14 OP51928 GNN401 OP51928-BSD NN009180.D 1 06/12/14 NG 06/10/14 OP51928 GNN401 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-11, FA15409-14 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C11-C22 Aromatics (Unadj.)85000 66300 78 62700 74 6 40-140/30 C9-C18 Aliphatics 30000 18100 60 16300 54 10 40-140/30 C19-C36 Aliphatics 40000 30400 76 27400 69 10 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 75%65%40-140% 580-13-2 2-Bromonaphthalene 84%88%40-140% 84-15-1 o-Terphenyl 63%58%40-140% 321-60-8 2-Fluorobiphenyl 77%80%40-140% Sample Compound Col #1 Col #2 Breakthrough Limit OP51928-BS 2-Methylnaphthalene 2750 ND 0.0%5.0 OP51928-BS Naphthalene 2460 ND 0.0%5.0 OP51928-BSD 2-Methylnaphthalene 2550 ND 0.0%5.0 OP51928-BSD Naphthalene 2290 ND 0.0%5.0 * = Outside of Control Limits. 205 of 208 FA15409 88.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51815-MS WR5681.D 1 06/04/14 SJL 06/02/14 OP51815 GWR165 OP51815-MSD WR5657.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 FA15265-12 WR5656.D 1 06/03/14 SJL 06/02/14 OP51815 GWR165 The QC reported here applies to the following samples:Method: SW846 8015C FA15409-15, FA15409-20, FA15409-21 FA15265-12 Spike MS MS Spike MSD MSD Limits CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD TPH (C10-C28)4.9 U 39.3 30.4 77 39.6 32.5 82 7 62-116/35 CAS No.Surrogate Recoveries MS MSD FA15265-12 Limits 84-15-1 o-Terphenyl 97%103%86%56-122% * = Outside of Control Limits. 206 of 208 FA15409 88.4.1 Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51816-DUP NN009060.D 4 06/06/14 NAF 06/02/14 OP51816 GNN397 FA15409-14 NN009059.D 4 06/06/14 NAF 06/02/14 OP51816 GNN397 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-12, FA15409-13, FA15409-14 FA15409-14 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits C11-C22 Aromatics (Unadj.)ND ND nc 30 a C9-C18 Aliphatics 69900 41500 J 51*30 a C19-C36 Aliphatics ND ND nc 30 a CAS No.Surrogate Recoveries DUP FA15409-14 Limits 3386-33-2 1-Chlorooctadecane 19%*40%40-140% 580-13-2 2-Bromonaphthalene 22%*27%*40-140% 84-15-1 o-Terphenyl 16%*40%40-140% 321-60-8 2-Fluorobiphenyl 22%*27%*40-140% (a) Advisory control limits. * = Outside of Control Limits. 207 of 208 FA15409 88.5.1 Duplicate Summary Page 1 of 1 Job Number:FA15409 Account:TQENCM Terraquest Environmental Project:Quality Mart 7; Winston-Salem, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP51928-DUP NN009187.D 1 06/12/14 NG 06/10/14 OP51928 GNN401 FA15618-1 NN009186.D 1 06/12/14 NG 06/10/14 OP51928 GNN401 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 FA15409-11, FA15409-14 FA15618-1 DUP CAS No.Compound ug/kg Q ug/kg Q RPD Limits C11-C22 Aromatics (Unadj.)12000 U ND nc 30 a C9-C18 Aliphatics 12000 U ND nc 30 a C19-C36 Aliphatics 12000 U ND nc 30 a CAS No.Surrogate Recoveries DUP FA15618-1 Limits 3386-33-2 1-Chlorooctadecane 57%73%40-140% 580-13-2 2-Bromonaphthalene 91%104%40-140% 84-15-1 o-Terphenyl 51%71%40-140% 321-60-8 2-Fluorobiphenyl 86%99%40-140% (a) Advisory control limits. * = Outside of Control Limits. 208 of 208 FA15409 88.5.2 Analytical Report 492739 for Terraquest Environmental Consultants, P.C. Project Manager: Ryan Kerins Lisa Parker/Reid Co QM#7 22-SEP-14 03014 6017 Financial Dr., Norcross, GA 30071 Ph:(770) 449-8800 Fax:(770) 449-5477 Xenco-Houston (EPA Lab code: TX00122): Texas (T104704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054) New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610) Xenco-Atlanta (EPA Lab Code: GA00046): Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135) Texas (T104704477), Louisiana (04176), USDA (P330-07-00105) Xenco-Lakeland: Florida (E84098) Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX) Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX) Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757) Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757) Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758) Collected By: Client Page 1 of 69 Final 1.000 Page 2 of 69 Final 1.000 Table of Contents Cover Page 1 Cover Letter 3 Sample ID Cross Reference 4 Explanation of Qualifiers (Flags) 5 Hits Summary 6 Certificate of Analysis (Detailed Report) 11 Summary of Quality control 33 Blank Summary 51 Chain of Custody 67 Sample Receipt Conformance Report 69 Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Project Manager: Ryan Kerins Terraquest Environmental Consultants, P.C. 100 E. Ruffin Street Mebane, NC 27302 Reference: XENCO Report No(s): 492739 Lisa Parker/Reid Co QM#7 Project Address: NC Ryan Kerins: We are reporting to you the results of the analyses performed on the samples received under the project name referenced above and identified with the XENCO Report Number(s) 492739. All results being reported under this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using all other available quality control measures. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise arranged with you. The samples received, and described as recorded in Report No. 492739 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard practices, controlled substances under regulated protocols, etc). We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions concerning this report, please feel free to contact us at any time. Respectfully, 22-SEP-14 Client Services Manager Mike Kimmel Page 3 of 69 Final 1.000 Sample Cross Reference 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 Sample Id K1 2.0 K1 3.0 K2 2.0 K3 2.0 MW1 09-04-14 09:45 09-04-14 09:52 09-04-14 10:00 09-04-14 10:17 09-04-14 11:50 Date Collected Lab Sample Id 492739-001 492739-002 492739-003 492739-004 492739-005 Sample DepthMatrix S S S S W Page 4 of 69 Final 1.000 Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America 4143 Greenbriar Dr, Stafford, TX 77477 9701 Harry Hines Blvd , Dallas, TX 75220 5332 Blackberry Drive, San Antonio TX 78238 2505 North Falkenburg Rd, Tampa, FL 33619 12600 West I-20 East, Odessa, TX 79765 6017 Financial Drive, Norcross, GA 30071 3725 E. Atlanta Ave, Phoenix, AZ 85040 Phone Fax (281) 240-4200 (281) 240-4280 (214) 902 0300 (214) 351-9139 (210) 509-3334 (210) 509-3335 (813) 620-2000 (813) 620-2033 (432) 563-1800 (432) 563-1713 (770) 449-8800 (770) 449-5477 (602) 437-0330 Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Flagging Criteria X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD. B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination. D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference. Dilution factors are included in the final results. The result is from a diluted sample. E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated. F RPD exceeded lab control limits. J The target analyte was positively identified below the quantitation limit and above the detection limit. U Analyte was not detected. L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations. H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the Department Supervisor and QA Director. Data were determined to be valid for reporting. K Sample analyzed outside of recommended hold time. JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated numerical value may not be consistent with the amount actually present in the environmental sample. ** Surrogate recovered outside laboratory control limit. BRL Below Reporting Limit. RL Reporting Limit MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation DL Method Detection Limit NC Non-Calculable + NELAC certification not offered for this compound. * (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation Page 5 of 69 Final 1.000 Hits Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 33.36 Date Received : % Moisture : 09.04.14 09.45 Date Collected : 492739-001Lab Sample Id : SoilMatrix : K1 2.0Sample Id : VOCs by SW-846 8260B Analytical Method :SW5035Prep Method: 09.08.14 06.51 Date Prep: 2-Butanone (MEK) Acetone Toluene Parameter Result Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number 78-93-3 67-64-1 108-88-3 0.047 0.29 0.0013 950108Seq Number Dry WeightBasis : 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 Analysis Date Page 6 of 69 Final 1.000 Hits Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 33.36 Date Received : % Moisture : 09.04.14 09.45 Date Collected : 492739-001Lab Sample Id : SoilMatrix : K1 2.0Sample Id : MADEP EPH SVOCs by SW-846 8270D Analytical Method : Analytical Method : SW3550 SW3545 Prep Method: Prep Method: 09.09.14 11.30 09.09.14 16.00 Date Prep: Date Prep: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics bis(2-ethylhexyl) phthalate Parameter Parameter Result Result J Flag Flag mg/kg mg/kg mg/kg mg/kg Units Units 1 1 1 1 Dil Dil Cas Number Cas Number C11C22 ALHYDRC9C ALHYDRC19 117-81-7 73.8 87.2 71.9 0.104 950483 950332 Seq Number Seq Number Dry WeightBasis : 09.09.14 19.01 09.09.14 18.55 09.09.14 18.55 09.10.14 16.22 Analysis Date Analysis Date Page 7 of 69 Final 1.000 Hits Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 32.42 Date Received : % Moisture : 09.04.14 09.52 Date Collected : 492739-002Lab Sample Id : SoilMatrix : K1 3.0Sample Id : MADEP EPH SVOCs by SW-846 8270D TPH-Diesel Range Organics by SW-846 8015C VOCs by SW-846 8260B Analytical Method : Analytical Method : Analytical Method : Analytical Method : SW3545 SW3545 SW3545 SW5035 Prep Method: Prep Method: Prep Method: Prep Method: 09.18.14 16.00 09.15.14 16.00 09.09.14 14.00 09.18.14 06.43 Date Prep: Date Prep: Date Prep: Date Prep: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics bis(2-ethylhexyl) phthalate TPH-DRO (C10-C28) 2-Butanone (MEK) Acetone Parameter Parameter Parameter Parameter Result Result Result Result J Flag Flag Flag Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units Units 1 1 1 1 1 1 1 Dil Dil Dil Dil Cas Number Cas Number Cas Number Cas Number C11C22 ALHYDRC9C ALHYDRC19 117-81-7 C10C28DRO 78-93-3 67-64-1 32.3 207 234 0.145 90.9 0.037 0.39 951157 950874 950381 950876 Seq Number Seq Number Seq Number Seq Number Dry WeightBasis : 09.22.14 15.00 09.22.14 14.42 09.22.14 14.42 09.17.14 20.01 09.10.14 14.48 09.18.14 09.40 09.18.14 09.40 Analysis Date Analysis Date Analysis Date Analysis Date Page 8 of 69 Final 1.000 Hits Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 26.45 Date Received : % Moisture : 09.04.14 10.17 Date Collected : 492739-004Lab Sample Id : SoilMatrix : K3 2.0Sample Id : MADEP EPH TPH-Diesel Range Organics by SW-846 8015C VOCs by SW-846 8260B Analytical Method : Analytical Method : Analytical Method : SW3545 SW3545 SW5035 Prep Method: Prep Method: Prep Method: 09.18.14 16.00 09.09.14 14.00 09.18.14 06.43 Date Prep: Date Prep: Date Prep: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics TPH-DRO (C10-C28) 2-Butanone (MEK) Acetone Parameter Parameter Parameter Result Result Result Flag Flag Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units 1 1 1 1 1 1 Dil Dil Dil Cas Number Cas Number Cas Number C11C22 ALHYDRC9C ALHYDRC19 C10C28DRO 78-93-3 67-64-1 48.3 18.5 31.8 68.0 0.018 0.41 951157 950381 950876 Seq Number Seq Number Seq Number Dry WeightBasis : 09.22.14 15.36 09.22.14 15.15 09.22.14 15.15 09.10.14 16.57 09.18.14 10.01 09.18.14 10.01 Analysis Date Analysis Date Analysis Date Page 9 of 69 Final 1.000 Hits Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received : % Moisture : 09.04.14 11.50 Date Collected : 492739-005Lab Sample Id : Ground WaterMatrix : MW1Sample Id : SVOCs by EPA 625 + 10 TICs Analytical Method :E625PPrep Method: 09.08.14 13.45 Date Prep: 1-Methylnaphthalene + bis(2-ethylhexyl) phthalate 2-Methylnaphthalene Naphthalene Naphthalene, 1,2,3,4-tetrahydro-5, (TIC) Benzene, 4-ethyl-1,2-dimethyl- (TIC) unknown (TIC) Naphthalene, 1,4-dimethyl- (TIC) 1,3-Dimethylcyclopentanol (TIC) Ethylbenzene (TIC) Benzene, 1,3-diethyl- (TIC) Cyclopentanol, 1-methyl- (TIC) Benzene, 1,4-diethyl- (TIC) Indane (TIC) Parameter Result JN JN JN JN JN JN JN JN JN JN Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 5 5 5 5 5 5 5 5 5 5 5 5 5 5 DilCas Number 90-12-0 117-81-7 91-57-6 91-20-3 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC 68.7 227 97.1 364 83.4 287 67.9 76.9 82.9 183 85.5 94.1 72.0 311 950218Seq Number 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 Analysis Date Page 10 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3550Prep Method: 09.09.14 11.30 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 29.6 14.8 14.8 Result 29.6 14.8 14.8 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 73.8 87.2 71.9 950483Seq Number: RL Dry WeightBasis: MDL 09.09.14 19.01 09.09.14 18.55 09.09.14 18.55 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 55 73 51 09.09.14 18.55 09.09.14 19.01 09.09.14 19.01 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 33.36% Moisture: Page 11 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.09.14 16.00 Date Prep: 5458Tech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0882 0.0807 0.0787 0.0777 0.0916 0.0961 0.0633 0.0906 0.0802 0.0647 0.0906 0.0891 0.0762 0.0697 0.0667 0.0628 0.147 0.0727 0.0687 0.0867 0.0847 0.0712 0.0827 0.0946 0.0757 0.0613 0.0697 0.0847 0.0548 0.0737 0.0807 0.0732 0.0812 0.0822 0.0857 0.0787 0.0747 0.0598 0.0707 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.996 0.498 0.996 2.49 0.498 0.498 0.498 0.249 0.498 0.498 0.498 0.996 0.996 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.996 0.498 0.498 0.249 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950332Seq Number: RL Dry WeightBasis: MDL 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 Analysis Date 33.36% Moisture: Page 12 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.09.14 16.00 Date Prep: 5458Tech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0672 0.0807 0.0662 0.0966 0.0637 0.0802 0.0752 0.0916 0.0827 0.0647 0.0608 0.0832 0.0553 0.0857 0.0772 0.0906 0.0513 0.0797 0.0887 0.0712 0.105 0.0901 0.0827 0.0697 0.0847 0.0946 Result U J U U U U U U U U U U U U U U U U U U U U U U U U 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.498 0.996 0.498 0.498 0.498 0.498 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U 0.104 U U U U U U U U U U U U U U U U U U U U U U U U 950332Seq Number: RL Dry WeightBasis: MDL 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 36 39 41 72 99 39 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 09.10.14 16.22 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 33.36% Moisture: Page 13 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 09.08.14 11.20 Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000926 0.000926 0.000309 Result U U U 0.000926 0.000926 0.000309 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 U U U 950395Seq Number: RL Dry WeightBasis: MDL 09.08.14 13.37 09.08.14 13.37 09.08.14 13.37 Analysis Date Surrogate 70-130 70-130 % Recovery Flag % % 89 102 09.08.14 13.37 09.08.14 13.37 Cas Number 615-59-8 615-59-8 Units Analysis Date 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Limits 33.36% Moisture: Page 14 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.08.14 06.51 Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00088 0.0014 0.00078 0.00093 0.0013 0.00063 0.00067 0.0019 0.0010 0.00084 0.0010 0.0015 0.00069 0.0011 0.00095 0.0012 0.00080 0.00080 0.00070 0.0027 0.00082 0.0013 0.00064 0.00093 0.0038 0.0080 0.00060 0.00099 0.0012 0.00058 0.0011 0.0029 0.00086 0.00067 0.0012 0.0028 0.00086 0.0027 0.00077 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0012 0.0023 0.0012 0.0012 0.0023 0.0012 0.0012 0.0023 0.0012 0.0012 0.0012 0.0023 0.0012 0.0012 0.0012 0.0012 0.0012 0.0012 0.0012 0.012 0.0012 0.012 0.0012 0.0012 0.012 0.012 0.0012 0.0012 0.0023 0.0012 0.0012 0.0058 0.0012 0.0012 0.0012 0.0058 0.0012 0.0058 0.0012 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U U U U U U U U U U U 0.047 U U U U U 0.29 U U U U U U U U U U U U U 950108Seq Number: RL Dry WeightBasis: MDL 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 Analysis Date 33.36% Moisture: Page 15 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.45 Date Collected:492739-001Lab Sample Id: SoilMatrix: K1 2.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.08.14 06.51 Date Prep: MWETech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00063 0.0014 0.033 0.00066 0.0015 0.00088 0.00141 0.00081 0.0025 0.0015 0.0010 0.00091 0.000833 0.00076 0.00086 0.00097 0.0012 0.00068 0.00091 0.00078 0.00082 0.0041 0.00084 0.0023 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0012 0.0023 0.058 0.0012 0.0023 0.0012 0.00233 0.0023 0.0058 0.0023 0.0012 0.0012 0.00116 0.0012 0.0012 0.0012 0.0023 0.0012 0.0012 0.0012 0.0012 0.0058 0.0058 0.0058 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U 0.0013 U U U U U U 950108Seq Number: RL Dry WeightBasis: MDL 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 144 103 99 09.08.14 16.52 09.08.14 16.52 09.08.14 16.52 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 33.36% Moisture: Page 16 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 09.18.14 16.00 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 29.4 14.7 14.7 Result 29.4 14.7 14.7 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 32.3 207 234 951157Seq Number: RL Dry WeightBasis: MDL 09.22.14 15.00 09.22.14 14.42 09.22.14 14.42 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 61 67 68 09.22.14 14.42 09.22.14 15.00 09.22.14 15.00 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 32.42% Moisture: Page 17 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16.00 Date Prep: TUETech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0861 0.0788 0.0769 0.0759 0.0895 0.0939 0.0618 0.0886 0.0783 0.0633 0.0886 0.0871 0.0744 0.0681 0.0652 0.0613 0.144 0.0710 0.0671 0.0847 0.0827 0.0696 0.0808 0.0925 0.0740 0.0599 0.0681 0.0827 0.0535 0.0720 0.0788 0.0715 0.0793 0.0803 0.0837 0.0769 0.0730 0.0584 0.0691 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.973 0.487 0.973 2.43 0.487 0.487 0.487 0.243 0.487 0.487 0.487 0.973 0.973 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.973 0.487 0.487 0.243 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: RL Dry WeightBasis: MDL 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 Analysis Date 32.42% Moisture: Page 18 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16.00 Date Prep: TUETech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0657 0.0788 0.0647 0.0944 0.0623 0.0783 0.0735 0.0895 0.0808 0.0633 0.0594 0.0813 0.0540 0.0837 0.0754 0.0886 0.0501 0.0779 0.0866 0.0696 0.102 0.0881 0.0808 0.0681 0.0827 0.0925 Result U J U U U U U U U U U U U U U U U U U U U U U U U U 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.487 0.973 0.487 0.487 0.487 0.487 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U 0.145 U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: RL Dry WeightBasis: MDL 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 38 40 36 60 100 39 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 09.17.14 20.01 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 32.42% Moisture: Page 19 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: TPH-Diesel Range Organics by SW-846 8015C MADEP VPH TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: CLAR JOL JOL Analyst: Analyst: Analyst: SW3545 SW5030B SW5030B Prep Method: Prep Method: Prep Method: 09.09.14 14.00 09.16.14 14.41 09.09.14 08.15 Date Prep: Date Prep: Date Prep: 5458 JOL JOL Tech: Tech: Tech: TPH-DRO (C10-C28) C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics TPH-GRO Parameter Parameter Parameter 3.78 0.000984 0.000984 0.000328 1.7 Result Result Result U U U U 12.3 0.000984 0.000984 0.000328 3.0 Flag Flag Flag mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units 1 50 50 50 50 Dil Dil Dil Cas Number Cas Number Cas Number C10C28DRO ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 8006-61-9 90.9 U U U U 950381 950789 950391 Seq Number: Seq Number: Seq Number: RL RL RL Dry Weight Dry Weight Dry Weight Basis: Basis: Basis: MDL MDL MDL 09.10.14 14.48 09.16.14 17.16 09.16.14 17.16 09.16.14 17.16 09.09.14 10.22 Analysis Date Analysis Date Analysis Date Surrogate Surrogate Surrogate 32-128 70-130 70-130 57-131 % Recovery % Recovery % Recovery Flag Flag Flag % % % % 85 118 123 89 09.10.14 14.48 09.16.14 17.16 09.16.14 17.16 09.09.14 10.22 Cas Number Cas Number Cas Number 84-15-1 615-59-8 615-59-8 615-59-8 Units Units Units Analysis Date Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene Limits Limits Limits 32.42 32.42 32.42 % Moisture: % Moisture: % Moisture: Page 20 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06.43 Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00078 0.0012 0.00070 0.00083 0.0012 0.00056 0.00060 0.0017 0.00091 0.00075 0.00090 0.0013 0.00062 0.00097 0.00085 0.0010 0.00071 0.00071 0.00062 0.0024 0.00074 0.0012 0.00057 0.00083 0.0034 0.0071 0.00053 0.00089 0.0010 0.00052 0.00100 0.0026 0.00077 0.00060 0.0010 0.0025 0.00077 0.0024 0.00069 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0021 0.0010 0.0010 0.0021 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0052 0.0010 0.0010 0.0010 0.0052 0.0010 0.0052 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U U U U U U U U U U U 0.037 U U U U U 0.39 U U U U U U U U U U U U U 950876Seq Number: RL Dry WeightBasis: MDL 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 Analysis Date 32.42% Moisture: Page 21 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 09.52 Date Collected:492739-002Lab Sample Id: SoilMatrix: K1 3.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06.43 Date Prep: MWETech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00056 0.0012 0.029 0.00059 0.0013 0.00079 0.00126 0.00072 0.0022 0.0014 0.00092 0.00081 0.000744 0.00068 0.00077 0.00087 0.0011 0.00061 0.00081 0.00070 0.00073 0.0037 0.00075 0.0021 Result U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0021 0.052 0.0010 0.0021 0.0010 0.00208 0.0021 0.0052 0.0021 0.0010 0.0010 0.00104 0.0010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0010 0.0052 0.0052 0.0052 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U U 950876Seq Number: RL Dry WeightBasis: MDL 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 148 101 95 09.18.14 09.40 09.18.14 09.40 09.18.14 09.40 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 32.42% Moisture: Page 22 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.00 Date Collected:492739-003Lab Sample Id: SoilMatrix: K2 2.0Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3545 SW5030B Prep Method: Prep Method: 09.09.14 14.00 09.09.14 08.15 Date Prep: Date Prep: 5458 JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.49 1.6 Result Result U U 11.4 2.8 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 U U 950381 950391 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 09.10.14 16.25 09.09.14 10.54 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 40 95 09.10.14 16.25 09.09.14 10.54 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 26.82 26.82 % Moisture: % Moisture: Page 23 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 09.18.14 16.00 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 26.6 13.3 13.3 Result 26.6 13.3 13.3 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 48.3 18.5 31.8 951157Seq Number: RL Dry WeightBasis: MDL 09.22.14 15.36 09.22.14 15.15 09.22.14 15.15 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 52 69 55 09.22.14 15.15 09.22.14 15.36 09.22.14 15.36 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 26.45% Moisture: Page 24 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16.00 Date Prep: TUETech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0798 0.0731 0.0713 0.0704 0.0830 0.0871 0.0573 0.0821 0.0726 0.0586 0.0821 0.0807 0.0690 0.0632 0.0604 0.0568 0.134 0.0659 0.0623 0.0785 0.0767 0.0645 0.0749 0.0857 0.0686 0.0555 0.0632 0.0767 0.0496 0.0668 0.0731 0.0663 0.0735 0.0744 0.0776 0.0713 0.0677 0.0541 0.0641 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.902 0.451 0.902 2.26 0.451 0.451 0.451 0.226 0.451 0.451 0.451 0.902 0.902 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.902 0.451 0.451 0.226 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: RL Dry WeightBasis: MDL 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 Analysis Date 26.45% Moisture: Page 25 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16.00 Date Prep: TUETech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0609 0.0731 0.0600 0.0875 0.0577 0.0726 0.0681 0.0830 0.0749 0.0586 0.0550 0.0753 0.0501 0.0776 0.0699 0.0821 0.0465 0.0722 0.0803 0.0645 0.0947 0.0816 0.0749 0.0632 0.0767 0.0857 Result U U U U U U U U U U U U U U U U U U U U U U U U U U 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.451 0.902 0.451 0.451 0.451 0.451 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: RL Dry WeightBasis: MDL 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 52 54 59 97 125 60 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 09.17.14 20.30 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 26.45% Moisture: Page 26 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: TPH-Diesel Range Organics by SW-846 8015C MADEP VPH TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: CLAR JOL JOL Analyst: Analyst: Analyst: SW3545 SW5030B SW5030B Prep Method: Prep Method: Prep Method: 09.09.14 14.00 09.16.14 14.41 09.09.14 08.15 Date Prep: Date Prep: Date Prep: 5458 JOL JOL Tech: Tech: Tech: TPH-DRO (C10-C28) C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics TPH-GRO Parameter Parameter Parameter 3.46 0.000832 0.000832 0.000277 1.5 Result Result Result U U U U 11.3 0.000832 0.000832 0.000277 2.5 Flag Flag Flag mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units 1 50 50 50 50 Dil Dil Dil Cas Number Cas Number Cas Number C10C28DRO ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 8006-61-9 68.0 U U U U 950381 950789 950391 Seq Number: Seq Number: Seq Number: RL RL RL Dry Weight Dry Weight Dry Weight Basis: Basis: Basis: MDL MDL MDL 09.10.14 16.57 09.16.14 17.47 09.16.14 17.47 09.16.14 17.47 09.09.14 11.26 Analysis Date Analysis Date Analysis Date Surrogate Surrogate Surrogate 32-128 70-130 70-130 57-131 % Recovery % Recovery % Recovery Flag Flag Flag % % % % 75 109 105 90 09.10.14 16.57 09.16.14 17.47 09.16.14 17.47 09.09.14 11.26 Cas Number Cas Number Cas Number 84-15-1 615-59-8 615-59-8 615-59-8 Units Units Units Analysis Date Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene Limits Limits Limits 26.45 26.45 26.45 % Moisture: % Moisture: % Moisture: Page 27 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06.43 Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00079 0.0012 0.00070 0.00084 0.0012 0.00056 0.00060 0.0017 0.00091 0.00075 0.00090 0.0013 0.00062 0.00097 0.00085 0.0010 0.00072 0.00071 0.00063 0.0024 0.00074 0.0012 0.00058 0.00084 0.0034 0.0072 0.00054 0.00089 0.0011 0.00052 0.0010 0.0026 0.00077 0.00060 0.0010 0.0026 0.00077 0.0024 0.00069 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0021 0.0010 0.0010 0.0021 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0052 0.0010 0.0010 0.0010 0.0052 0.0010 0.0052 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U U U U U U U U U U U 0.018 U U U U U 0.41 U U U U U U U U U U U U U 950876Seq Number: RL Dry WeightBasis: MDL 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 Analysis Date 26.45% Moisture: Page 28 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 10.17 Date Collected:492739-004Lab Sample Id: SoilMatrix: K3 2.0Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06.43 Date Prep: MWETech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00056 0.0012 0.029 0.00059 0.0013 0.00079 0.00126 0.00072 0.0023 0.0014 0.00092 0.00082 0.000748 0.00069 0.00077 0.00087 0.0011 0.00061 0.00081 0.00070 0.00074 0.0037 0.00075 0.0021 Result U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0021 0.052 0.0010 0.0021 0.0010 0.00209 0.0021 0.0052 0.0021 0.0010 0.0010 0.00104 0.0010 0.0010 0.0010 0.0021 0.0010 0.0010 0.0010 0.0010 0.0052 0.0052 0.0052 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U U 950876Seq Number: RL Dry WeightBasis: MDL 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 148 106 92 09.18.14 10.01 09.18.14 10.01 09.18.14 10.01 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 26.45% Moisture: Page 29 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 11.50 Date Collected:492739-005Lab Sample Id: Ground WaterMatrix: MW1Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.08.14 13.45 Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene Parameter 9.95 10.9 10.4 9.41 99.3 8.91 7.97 6.93 9.75 8.81 13.4 8.07 9.75 35.2 6.09 9.06 10.5 10.8 15.3 9.06 6.68 7.08 19.2 7.33 6.93 6.19 23.6 8.81 6.14 5.94 6.39 9.01 10.3 9.06 8.12 9.41 9.75 10.3 5.89 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 49.5 248 49.5 49.5 248 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 248 99.0 49.5 49.5 99.0 49.5 49.5 49.5 49.5 99.0 49.5 248 49.5 248 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 99-65-0 50-32-8 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 105-67-9 191-24-2 51-28-5 100-51-6 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 U U U U U U U 68.7 U U U U U U U U U U U U U U U U U U U U U 227 U U U U U U U U 97.1 950218Seq Number: RL MDL 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 Analysis Date % Moisture: Page 30 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 11.50 Date Collected:492739-005Lab Sample Id: Ground WaterMatrix: MW1Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.08.14 13.45 Date Prep: BROTech: di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene 1,3-Dimethylcyclopentanol (TIC) Benzene, 1,3-diethyl- (TIC) Benzene, 1,4-diethyl- (TIC) Benzene, 4-ethyl-1,2-dimethyl- (TIC) Cyclopentanol, 1-methyl- (TIC) Ethylbenzene (TIC) Indane (TIC) Naphthalene, 1,2,3,4-tetrahydro-5, (TIC) Naphthalene, 1,4-dimethyl- (TIC) unknown (TIC) Parameter 6.83 9.90 8.96 12.6 7.72 10.9 8.81 9.26 11.8 9.65 9.26 11.9 6.98 7.52 7.38 6.73 12.4 7.08 11.2 8.12 10.1 8.71 11.9 Result U U U U U U U U U U U U U U U U U U U U U U JN JN JN JN JN JN JN JN JN JN 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 49.5 248 49.5 49.5 49.5 49.5 49.5 49.5 248 49.5 49.5 49.5 49.5 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 DilCas Number 117-84-0 95-48-7 206-44-0 15831-10-4 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC U U U U U U U U U U U U U 364 U U U U U U U U U 82.9 85.5 72.0 287 94.1 183 311 83.4 76.9 67.9 950218Seq Number: RL MDL 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 Analysis Date Surrogate 30-100 44-117 48-117 46-111 50-200 % Recovery Flag % % % % % 61 63 63 76 62 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 09.09.14 15.00 Cas Number 367-12-4 321-60-8 118-79-6 4165-60-0 4165-62-2 Units Analysis Date 2-Fluorophenol 2-Fluorobiphenyl 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Limits % Moisture: Page 31 of 69 Final 1.000 Certificate of Analytical Results 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 09.05.14 09.50 Date Received: 09.04.14 11.50 Date Collected:492739-005Lab Sample Id: Ground WaterMatrix: MW1Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.08.14 13.45 Date Prep: BROTech: 950218Seq Number: Surrogate 46-126 % Recovery Flag %87 09.09.14 15.00 Cas Number 1718-51-0 Units Analysis Date Terphenyl-D14 Limits % Moisture: Page 32 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 492722-001 492739-001 661230-1-BLK 661723-1-BLK Parent Sample Id: Parent Sample Id: MB Sample Id: MB Sample Id: Soil Soil Solid Solid Matrix: Matrix: Matrix: Matrix: Percent Moisture Percent Moisture MADEP EPH MADEP EPH Analytical Method: Analytical Method: Analytical Method: Analytical Method: SW3550 SW3545 Prep Method: Prep Method: 09.09.14 09.18.14 Date Prep: Date Prep: Percent Moisture Percent Moisture C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter Parameter Parameter Parameter %RPD %RPD %RPD %RPD L Flag Flag Flag Flag 20 20 40 40 40 40 40 40 RPD Limit RPD Limit RPD Limit RPD Limit 0 0 38 9 9 2 0 0 950008 950008 950483 951157 Seq Number: Seq Number: Seq Number: Seq Number: 09.05.14 17:00 09.05.14 17:00 09.10.14 17:56 09.11.14 14:06 09.11.14 14:06 09.22.14 11:57 09.22.14 11:58 09.22.14 11:58 Analysis Date Analysis Date Analysis Date Analysis Date Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 LCSD %Rec LCSD %Rec 68 40 68 65 53 73 LCSD Result LCSD Result 115 24.2 54.4 110 31.8 58.2 LCS %Rec LCS %Rec 46 37 62 64 53 73 32.5 33.4 78.5 22.2 49.8 108 31.8 58.2 Spike Amount Spike Amount 170 60.0 80.0 170 60.0 80.0 Parent Result Parent Result MB Result MB Result 32.5 33.4 <20.0 <10.0 <10.0 <20.0 <10.0 <10.0 492722-001 D 492739-001 D 661230-1-BKS 661723-1-BKS MD Sample Id: MD Sample Id: LCS Sample Id: LCS Sample Id: 661230-1-BSD 661723-1-BSD LCSD Sample Id: LCSD Sample Id: % % mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units Units MD Result MD Result LCS Result LCS Result 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Surrogate Surrogate LCSD Flag LCSD Flag 09.11.14 14:06 09.10.14 17:56 09.10.14 17:56 09.22.14 11:58 09.22.14 11:57 09.22.14 11:57 Analysis Date Analysis Date Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 LCSD %Rec LCSD %Rec 54 76 63 66 70 53 LCS %Rec LCS %Rec 52 56 88 70 70 58 MB %Rec MB %Rec 63 49 22 48 73 71 % % % % % % Units Units LCS Flag LCS Flag ** MB Flag MB Flag Page 33 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 492739-001 493361-001 Parent Sample Id: Parent Sample Id: Soil Soil Matrix: Matrix: MADEP EPH MADEP EPH Analytical Method: Analytical Method: SW3550 SW3545 Prep Method: Prep Method: 09.09.14 09.18.14 Date Prep: Date Prep: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter Parameter %RPD %RPD XF XF XF Flag Flag 40 40 40 40 40 40 RPD Limit RPD Limit 2 3 12 51 85 72 950483 951157 Seq Number: Seq Number: 09.09.14 19:37 09.09.14 19:28 09.09.14 19:28 09.22.14 13:47 09.22.14 13:36 09.22.14 13:36 Analysis Date Analysis Date Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 MSD %Rec MSD %Rec 56 51 66 151 159 137 MSD Result MSD Result 216 133 150 420 164 184 MS %Rec MS %Rec 58 47 82 293 502 356 220 129 169 710 407 391 Spike Amount Spike Amount 253 89.4 119 199 70.1 93.4 Parent Result Parent Result 73.8 87.2 71.9 126 54.9 58.9 492739-001 S 493361-001 S MS Sample Id: MS Sample Id: 492739-001 SD 493361-001 SD MSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units MS Result MS Result 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Surrogate Surrogate MSD Flag MSD Flag 09.09.14 19:28 09.09.14 19:37 09.09.14 19:37 09.22.14 13:36 09.22.14 13:47 09.22.14 13:47 Analysis Date Analysis Date Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 MSD %Rec MSD %Rec 58 74 60 62 98 72 MS %Rec MS %Rec 60 75 58 68 81 62 % % % % % % Units Units MS Flag MS Flag Page 34 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661198-1-BLKMB Sample Id: WaterMatrix: SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method: 09.08.14Date Prep: Anthracene 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene Parameter %RPD L Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 6 0 10 5 11 2 1 13 3 11 3 13 3 10 0 0 1 4 1 1 1 0 6 0 3 4 3 9 0 10 11 14 2 6 1 9 1 13 3 9 1 1 5 0 2 0 1 14 11 1 7 2 950218Seq Number: 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 Analysis Date Limits 27-133 65-135 33-143 45-110 17-163 20-124 25-175 24-159 39-135 11-162 32-119 0-219 0-191 30-110 36-120 53-127 22-147 15-110 32-129 25-158 47-145 33-145 10-181 33-184 55-115 12-158 36-166 8-158 60-118 0-152 17-168 0-227 55-105 0-114 0-112 1-118 45-105 0-107 40-110 26-137 30-110 59-121 0-152 24-116 41-125 40-113 29-182 0-171 0-132 21-196 21-133 35-180 LCSD %Rec 83 60 81 80 91 60 73 83 67 93 72 82 100 72 63 79 79 72 61 77 76 81 85 74 88 69 85 86 70 92 79 83 74 80 83 81 70 87 69 84 70 78 80 65 80 63 67 82 71 77 64 68 LCSD Result 41.6 29.8 40.6 40.2 45.5 30.1 36.3 41.4 33.7 46.6 36.1 40.9 50.2 35.8 31.3 39.3 39.7 35.8 30.7 38.5 37.8 40.3 42.4 36.9 44.2 34.6 42.6 43.1 35.2 45.9 39.4 41.6 36.9 39.8 41.5 40.3 35.1 43.5 34.5 42.1 35.0 39.0 40.2 32.4 40.2 31.3 33.6 41.2 35.3 38.5 32.1 33.8 LCS %Rec 89 59 90 84 102 61 73 94 69 84 70 94 97 65 62 78 79 69 62 78 75 81 90 74 91 72 82 94 70 101 88 95 75 84 84 88 71 99 67 92 70 79 84 65 79 63 68 95 79 77 69 69 44.3 29.7 44.9 42.1 50.9 30.6 36.7 47.1 34.7 41.8 35.0 46.8 48.7 32.3 31.2 39.2 39.4 34.4 31.0 39.0 37.3 40.3 45.0 36.8 45.4 36.0 41.2 47.2 35.2 50.7 43.9 47.7 37.5 42.2 42.1 44.2 35.4 49.5 33.4 46.2 35.2 39.5 42.2 32.5 39.3 31.4 33.9 47.3 39.3 38.3 34.3 34.4 Spike Amount 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 MB Result <2.01 <2.11 <1.90 <20.1 <1.80 <1.61 <1.40 <1.97 <1.78 <2.71 <1.63 <1.97 <7.11 <1.23 <1.83 <2.12 <2.18 <3.09 <1.83 <1.35 <1.43 <1.48 <1.40 <1.25 <4.76 <1.78 <1.24 <1.20 <1.29 <1.82 <2.09 <1.83 <1.64 <1.90 <1.97 <2.08 <1.19 <1.38 <2.00 <1.81 <2.55 <1.56 <2.21 <1.78 <1.87 <2.38 <1.95 <1.87 <2.41 <1.41 <1.52 <1.49 661198-1-BKSLCS Sample Id:661198-1-BSDLCSD Sample Id: ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L UnitsLCS Result Page 35 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661198-1-BLKMB Sample Id: WaterMatrix: SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method: 09.08.14Date Prep: n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene Parameter %RPD H Flag 30 30 30 30 30 30 30 30 RPD Limit 4 3 4 2 2 6 0 9 950218Seq Number: 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 Analysis Date Limits 10-230 50-110 44-142 14-76 37-144 54-120 5-112 23-152 LCSD %Rec 82 102 62 86 74 80 68 88 LCSD Result 41.0 50.8 31.2 43.2 36.8 40.1 34.2 44.1 LCS %Rec 79 105 65 88 72 85 68 96 39.5 52.4 32.5 44.1 36.0 42.7 34.1 48.2 Spike Amount 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 MB Result <1.36 <2.50 <1.43 <2.26 <1.64 <2.04 <1.76 <2.40 661198-1-BKSLCS Sample Id:661198-1-BSDLCSD Sample Id: ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L UnitsLCS Result 2-Fluorobiphenyl 2-Fluorophenol 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-D14 Surrogate LCSD Flag 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 09.09.14 14:04 Analysis DateLimits 39-99 33-92 32-129 37-94 50-200 18-133 LCSD %Rec 72 57 83 70 71 91 LCS %Rec 72 61 89 73 72 102 MB %Rec 76 72 80 79 76 107 % % % % % % UnitsLCS Flag MB Flag Page 36 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661256-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 09.09.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 0 4 5 4 11 10 6 8 12 1 2 22 4 18 10 6 22 8 10 5 11 8 6 12 15 5 5 20 5 5 5 3 1 7 7 4 16 9 10 6 3 6 10 8 6 9 7 9 9 9 5 1 950332Seq Number: 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 Analysis Date Limits 35-129 38-122 38-120 37-121 40-135 39-139 36-135 38-133 48-131 42-136 32-138 38-125 36-126 37-128 30-133 33-142 38-126 41-135 30-146 37-140 40-134 34-124 41-131 46-132 21-152 37-131 39-129 33-117 39-139 44-135 43-153 40-153 40-153 33-156 43-145 30-129 33-127 25-124 46-145 42-135 41-155 39-132 45-131 43-132 43-142 34-166 41-138 41-131 36-142 35-129 16-106 36-121 LCSD %Rec 77 84 81 83 81 84 90 93 93 84 79 105 85 108 92 86 106 93 86 85 96 88 84 95 75 85 90 103 92 87 101 106 89 83 91 91 104 114 99 89 91 84 88 90 85 99 94 87 91 74 84 83 LCSD Result 1.29 1.40 1.35 1.38 1.36 1.40 1.51 1.55 1.56 1.41 1.32 1.75 1.42 1.80 1.53 1.43 1.77 1.55 1.43 1.42 1.60 1.47 1.41 1.59 1.26 1.42 1.51 1.72 1.53 1.46 1.69 1.77 1.49 1.38 1.52 1.52 1.74 1.91 1.66 1.49 1.52 1.40 1.47 1.50 1.42 1.66 1.57 1.46 1.52 1.23 1.40 1.38 LCS %Rec 77 80 77 79 73 76 85 86 83 83 78 84 82 90 83 80 85 86 77 81 86 81 80 84 65 81 86 84 87 83 96 102 88 89 85 87 89 104 90 84 88 79 80 83 80 90 88 80 83 81 88 81 1.29 1.34 1.28 1.32 1.22 1.27 1.42 1.43 1.39 1.39 1.30 1.41 1.37 1.51 1.39 1.34 1.42 1.43 1.29 1.35 1.44 1.36 1.33 1.41 1.08 1.35 1.44 1.41 1.45 1.39 1.60 1.71 1.47 1.48 1.42 1.46 1.48 1.74 1.50 1.41 1.47 1.32 1.33 1.38 1.34 1.51 1.47 1.34 1.39 1.35 1.47 1.36 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0590 <0.0540 <0.0527 <0.0520 <0.0613 <0.0643 <0.0423 <0.0607 <0.0537 <0.0433 <0.0607 <0.0597 <0.0510 <0.0467 <0.0447 <0.0420 <0.0987 <0.0460 <0.0580 <0.0567 <0.0477 <0.0553 <0.0633 <0.0507 <0.0410 <0.0467 <0.0567 <0.0367 <0.0493 <0.0540 <0.0490 <0.0543 <0.0550 <0.0573 <0.0500 <0.0400 <0.0473 <0.0450 <0.0540 <0.0443 <0.0647 <0.0427 <0.0537 <0.0503 <0.0613 <0.0553 <0.0433 <0.0407 <0.0557 <0.0370 <0.0573 <0.0517 661256-1-BKSLCS Sample Id:661256-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 37 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661256-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 09.09.14Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 3 8 1 4 18 2 11 7 27 7 17 950332Seq Number: 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 Analysis Date Limits 39-154 36-128 35-128 32-129 34-129 27-155 14-148 37-139 34-127 42-138 30-113 LCSD %Rec 91 92 80 87 110 105 95 90 112 93 108 LCSD Result 1.52 1.53 1.34 1.45 1.84 1.76 1.59 1.51 1.87 1.55 1.81 LCS %Rec 88 84 81 84 92 103 86 84 86 86 91 1.47 1.41 1.35 1.40 1.53 1.72 1.43 1.41 1.43 1.44 1.52 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0607 <0.0343 <0.0533 <0.0593 <0.0477 <0.0700 <0.0603 <0.0553 <0.0467 <0.0567 <0.0633 661256-1-BKSLCS Sample Id:661256-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Surrogate ** LCSD Flag 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 09.10.14 15:26 Analysis Date Limits 25-121 23-120 30-115 19-122 18-137 15-110 LCSD %Rec 108 89 81 89 100 120 LCS %Rec 87 89 80 88 91 85 MB %Rec 85 82 76 80 108 82 % % % % % % UnitsLCS Flag MB Flag Page 38 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661531-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 09.15.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD F Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 1 0 2 2 2 8 1 0 4 4 2 0 2 4 3 2 3 4 1 4 1 2 2 12 11 4 3 10 2 7 9 37 6 11 3 2 2 0 3 9 11 3 7 6 1 4 2 3 1 4 0 2 950874Seq Number: 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 Analysis Date Limits 35-129 38-122 38-120 37-121 40-135 39-139 36-135 38-133 48-131 42-136 32-138 38-125 36-126 37-128 30-133 33-142 38-126 41-135 30-146 37-140 40-134 34-124 41-131 46-132 21-152 37-131 39-129 33-117 39-139 44-135 43-153 40-153 40-153 33-156 43-145 30-129 33-127 25-124 46-145 42-135 41-155 39-132 45-131 43-132 43-142 34-166 41-138 41-131 36-142 35-129 16-106 36-121 LCSD %Rec 68 75 67 69 73 73 85 92 81 80 75 101 78 114 85 80 108 83 45 77 91 81 76 78 53 80 85 105 82 84 96 108 81 101 95 88 98 114 97 82 83 77 78 83 81 96 82 78 78 69 71 75 LCSD Result 1.13 1.25 1.12 1.16 1.22 1.22 1.42 1.53 1.35 1.33 1.26 1.68 1.31 1.90 1.42 1.34 1.80 1.39 0.756 1.28 1.52 1.35 1.27 1.31 0.883 1.33 1.42 1.75 1.37 1.40 1.61 1.81 1.35 1.69 1.59 1.47 1.63 1.91 1.62 1.37 1.38 1.28 1.31 1.39 1.35 1.61 1.37 1.30 1.31 1.15 1.18 1.25 LCS %Rec 67 75 68 68 74 79 84 92 84 83 77 101 80 109 87 78 105 86 45 80 92 83 78 88 48 83 87 95 84 78 88 75 76 90 93 90 99 114 95 75 74 79 84 88 81 92 84 80 79 66 71 77 1.12 1.25 1.14 1.14 1.24 1.32 1.40 1.53 1.41 1.39 1.28 1.68 1.33 1.82 1.46 1.31 1.75 1.44 0.747 1.33 1.54 1.38 1.30 1.47 0.794 1.38 1.46 1.59 1.40 1.30 1.47 1.25 1.27 1.51 1.55 1.50 1.66 1.91 1.58 1.25 1.24 1.32 1.41 1.47 1.36 1.54 1.40 1.34 1.32 1.11 1.18 1.28 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0590 <0.0540 <0.0527 <0.0520 <0.0613 <0.0643 <0.0423 <0.0607 <0.0537 <0.0433 <0.0607 <0.0597 <0.0510 <0.0467 <0.0447 <0.0420 <0.0987 <0.0460 <0.0580 <0.0567 <0.0477 <0.0553 <0.0633 <0.0507 <0.0410 <0.0467 <0.0567 <0.0367 <0.0493 <0.0540 <0.0490 <0.0543 <0.0550 <0.0573 <0.0500 <0.0400 <0.0473 <0.0450 <0.0540 <0.0443 <0.0647 <0.0427 <0.0537 <0.0503 <0.0613 <0.0553 <0.0433 <0.0407 <0.0557 <0.0370 <0.0573 <0.0517 661531-1-BKSLCS Sample Id:661531-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 39 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661531-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 09.15.14Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 10 1 0 2 2 4 3 2 1 2 1 950874Seq Number: 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 Analysis Date Limits 39-154 36-128 35-128 32-129 34-129 27-155 14-148 37-139 34-127 42-138 30-113 LCSD %Rec 85 89 75 84 105 102 68 81 107 90 98 LCSD Result 1.42 1.49 1.25 1.41 1.76 1.70 1.14 1.36 1.78 1.51 1.64 LCS %Rec 77 89 75 83 104 106 70 83 106 89 99 1.29 1.48 1.25 1.38 1.73 1.77 1.17 1.39 1.77 1.48 1.66 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0607 <0.0343 <0.0533 <0.0593 <0.0477 <0.0700 <0.0603 <0.0553 <0.0467 <0.0567 <0.0633 661531-1-BKSLCS Sample Id:661531-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Surrogate LCSD Flag 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 09.17.14 16:43 Analysis Date Limits 25-121 23-120 30-115 19-122 18-137 15-110 LCSD %Rec 105 88 79 79 99 103 LCS %Rec 103 88 80 84 90 100 MB %Rec 83 86 80 77 111 81 % % % % % % UnitsLCS Flag MB Flag Page 40 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 492739-004Parent Sample Id: SoilMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 09.15.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD X F Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 5 8 11 12 9 6 1 12 7 7 2 3 0 6 11 22 2 12 5 10 7 3 6 20 15 2 4 8 12 16 16 10 18 19 17 0 4 1 16 16 20 5 8 6 13 14 13 9 14 5 33 12 950874Seq Number: 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 Analysis Date Limits 31-100 27-97 25-96 27-94 33-110 35-111 33-103 28-109 35-122 35-119 32-108 25-102 22-104 27-104 20-128 30-104 30-111 22-117 3-130 38-115 26-116 4-104 34-114 28-117 12-137 31-111 36-122 20-120 33-118 31-136 44-105 29-120 35-126 37-123 35-122 31-106 24-103 32-103 32-129 34-122 36-124 31-107 34-118 36-115 37-121 35-126 15-135 31-117 38-116 30-98 12-194 27-98 MSD %Rec 39 37 35 35 73 65 52 37 72 63 49 41 44 41 74 25 45 83 9 77 71 53 66 90 69 57 60 43 89 93 101 92 100 92 107 41 40 48 118 93 97 60 76 65 90 126 95 70 84 41 15 34 MSD Result 0.865 0.821 0.781 0.790 1.64 1.46 1.16 0.833 1.61 1.42 1.09 0.924 0.989 0.910 1.66 0.566 1.01 1.86 0.195 1.72 1.59 1.19 1.48 2.02 1.54 1.27 1.35 0.959 1.99 2.08 2.26 2.05 2.25 2.05 2.39 0.926 0.887 1.08 2.65 2.08 2.18 1.34 1.71 1.45 2.01 2.82 2.13 1.57 1.89 0.921 0.333 0.762 MS %Rec 40 39 39 39 66 61 51 42 66 58 47 42 44 43 65 31 46 73 8 69 65 51 62 73 58 55 58 39 78 79 85 82 83 75 89 41 41 48 100 79 79 56 70 60 78 109 83 64 73 43 21 38 0.908 0.890 0.874 0.888 1.50 1.38 1.15 0.944 1.50 1.32 1.07 0.949 0.990 0.968 1.48 0.709 1.03 1.65 0.186 1.55 1.48 1.15 1.40 1.66 1.32 1.24 1.30 0.884 1.76 1.78 1.92 1.85 1.87 1.69 2.02 0.929 0.920 1.09 2.26 1.78 1.79 1.27 1.58 1.36 1.77 2.46 1.87 1.44 1.64 0.967 0.466 0.855 Spike Amount 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 Parent Result <0.0799 <0.0731 <0.0713 <0.0704 <0.0831 <0.0871 <0.0573 <0.0822 <0.0727 <0.0587 <0.0822 <0.0808 <0.0691 <0.0632 <0.0605 <0.0569 <0.134 <0.0623 <0.0785 <0.0767 <0.0646 <0.0749 <0.0858 <0.0686 <0.0555 <0.0632 <0.0767 <0.0497 <0.0668 <0.0731 <0.0664 <0.0736 <0.0745 <0.0776 <0.0677 <0.0542 <0.0641 <0.0609 <0.0731 <0.0600 <0.0876 <0.0578 <0.0727 <0.0682 <0.0831 <0.0749 <0.0587 <0.0551 <0.0754 <0.0501 <0.0776 <0.0700 492739-004 SMS Sample Id:492739-004 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 41 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 492739-004 661234-1-BLK 492739-002 Parent Sample Id: MB Sample Id: Parent Sample Id: Soil Solid Soil Matrix: Matrix: Matrix: SVOCs by SW-846 8270D TPH-Diesel Range Organics by SW-846 8015C TPH-Diesel Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: SW3545 SW3545 SW3545 Prep Method: Prep Method: Prep Method: 09.15.14 09.09.14 09.09.14 Date Prep: Date Prep: Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine TPH-DRO (C10-C28) TPH-DRO (C10-C28) Parameter Parameter Parameter %RPD %RPD %RPD X Flag Flag Flag 30 30 30 30 30 30 30 30 30 30 30 20 20 RPD Limit RPD Limit RPD Limit 20 2 2 4 2 6 8 10 1 18 12 15 15 950874 950381 950381 Seq Number: Seq Number: Seq Number: 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.10.14 13:43 09.10.14 15:20 Analysis Date Analysis Date Analysis Date Limits Limits Limits 30-129 11-139 31-100 27-106 26-122 38-127 14-128 34-115 23-104 33-112 1-106 32-119 32-119 MSD %Rec LCSD %Rec MSD %Rec 95 45 41 37 44 91 83 86 44 96 35 58 27 MSD Result LCSD Result MSD Result 2.13 1.00 0.916 0.833 0.996 2.04 1.87 1.93 0.985 2.16 0.780 19.2 104 MS %Rec LCS %Rec MS %Rec 77 43 41 39 43 85 76 77 44 80 39 67 0 1.74 0.982 0.936 0.871 0.981 1.93 1.72 1.74 0.999 1.81 0.882 22.3 89.5 Spike Amount Spike Amount Spike Amount 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 2.26 33.3 49.2 Parent Result MB Result Parent Result <0.0822 <0.0465 <0.0722 <0.0803 <0.0646 <0.0948 <0.0817 <0.0749 <0.0632 <0.0767 <0.0858 <2.56 90.9 492739-004 S 661234-1-BKS 492739-002 S MS Sample Id: LCS Sample Id: MS Sample Id: 492739-004 SD 661234-1-BSD 492739-002 SD MSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units MS Result LCS Result MS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 o-Terphenyl o-Terphenyl Surrogate Surrogate Surrogate MSD Flag LCSD Flag MSD Flag 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.17.14 21:27 09.10.14 13:43 09.10.14 15:20 Analysis Date Analysis Date Analysis Date Limits Limits Limits 25-121 23-120 30-115 19-122 18-137 15-110 32-128 32-128 MSD %Rec LCSD %Rec MSD %Rec 37 39 47 90 95 43 76 76 MS %Rec LCS %Rec MS %Rec 42 41 47 83 83 47 80 71 MB %Rec 71 % % % % % % % % Units Units Units MS Flag LCS Flag MS Flag MB Flag Page 42 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661366-1-BLK 661612-1-BLK 492739-001 MB Sample Id: MB Sample Id: Parent Sample Id: Solid Solid Soil Matrix: Matrix: Matrix: MADEP VPH MADEP VPH MADEP VPH Analytical Method: Analytical Method: Analytical Method: SW5030B SW5030B SW5030B Prep Method: Prep Method: Prep Method: 09.08.14 09.16.14 09.08.14 Date Prep: Date Prep: Date Prep: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter Parameter Parameter %RPD %RPD %RPD Flag Flag Flag 25 25 25 25 25 25 25 25 25 RPD Limit RPD Limit RPD Limit 2 1 5 2 2 0 1 3 2 950395 950789 950395 Seq Number: Seq Number: Seq Number: 09.08.14 11:51 09.08.14 11:51 09.08.14 11:51 09.16.14 15:43 09.16.14 15:43 09.16.14 15:43 09.08.14 14:34 09.08.14 14:34 09.08.14 14:34 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 LCSD %Rec LCSD %Rec MSD %Rec 84 107 120 82 109 122 105 107 119 LCSD Result LCSD Result MSD Result 6.31 8.04 2.99 6.16 8.15 3.06 9.75 9.89 3.67 LCS %Rec LCS %Rec MS %Rec 86 109 114 81 111 122 105 104 121 6.45 8.15 2.84 6.05 8.31 3.05 9.70 9.61 3.75 Spike Amount Spike Amount Spike Amount 7.50 7.50 2.50 7.50 7.50 2.50 9.26 9.26 3.09 MB Result MB Result Parent Result <0.000750 <0.000750 <0.000250 <0.000750 <0.000750 <0.000250 <0.000926 <0.000926 <0.000309 661366-1-BKS 661612-1-BKS 492739-001 S LCS Sample Id: LCS Sample Id: MS Sample Id: 661366-1-BSD 661612-1-BSD 492739-001 SD LCSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units LCS Result LCS Result MS Result 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Surrogate Surrogate Surrogate LCSD Flag LCSD Flag MSD Flag 09.08.14 11:51 09.08.14 11:51 09.16.14 15:43 09.16.14 15:43 09.08.14 14:34 09.08.14 14:34 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 70-130 70-130 70-130 70-130 LCSD %Rec LCSD %Rec MSD %Rec 86 90 94 90 82 98 LCS %Rec LCS %Rec MS %Rec 91 91 96 91 78 93 MB %Rec MB %Rec 101 99 99 98 % % % % % % Units Units Units LCS Flag LCS Flag MS Flag MB Flag MB Flag Page 43 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 492739-002 661361-1-BLK 492739-002 Parent Sample Id: MB Sample Id: Parent Sample Id: Soil Solid Soil Matrix: Matrix: Matrix: MADEP VPH TPH-Gasoline Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: SW5030B SW5030B SW5030B Prep Method: Prep Method: Prep Method: 09.16.14 09.09.14 09.09.14 Date Prep: Date Prep: Date Prep: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics TPH-GRO TPH-GRO Parameter Parameter Parameter %RPD %RPD %RPD Flag Flag Flag 25 25 25 25 25 RPD Limit RPD Limit RPD Limit 2 10 6 0 2 950789 950391 950391 Seq Number: Seq Number: Seq Number: 09.16.14 18:18 09.16.14 18:18 09.16.14 18:18 09.09.14 08:47 09.09.14 12:29 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 70-130 64-114 64-114 MSD %Rec LCSD %Rec MSD %Rec 93 122 124 92 90 MSD Result LCSD Result MSD Result 9.18 12.0 4.06 46 54 MS %Rec LCS %Rec MS %Rec 95 111 117 92 88 9.33 10.9 3.83 46 53 Spike Amount Spike Amount Spike Amount 9.84 9.84 3.28 50 60 Parent Result MB Result Parent Result <0.000984 <0.000984 <0.000328 <1.5 <1.7 492739-002 S 661361-1-BKS 492739-002 S MS Sample Id: LCS Sample Id: MS Sample Id: 492739-002 SD 661361-1-BSD 492739-002 SD MSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units MS Result LCS Result MS Result 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene Surrogate Surrogate Surrogate MSD Flag LCSD Flag MSD Flag 09.16.14 18:18 09.16.14 18:18 09.09.14 08:47 09.09.14 12:29 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 57-131 57-131 MSD %Rec LCSD %Rec MSD %Rec 99 106 96 98 MS %Rec LCS %Rec MS %Rec 97 101 104 99 MB %Rec 96 % % % % Units Units Units MS Flag LCS Flag MS Flag MB Flag Page 44 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661206-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 09.08.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 8 5 0 6 16 11 0 4 3 7 2 3 2 4 10 7 0 7 12 0 7 0 8 10 0 5 6 4 2 7 4 13 13 6 4 3 6 18 10 4 10 7 7 6 11 4 2 20 0 9 11 3 950108Seq Number: 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 Analysis Date Limits 61-140 68-124 79-117 72-125 78-126 73-134 75-135 63-124 73-136 77-132 81-118 80-124 59-131 81-122 74-138 83-125 81-120 83-118 54-152 61-127 78-133 61-138 78-134 60-144 65-125 60-130 79-122 72-122 73-120 76-126 56-125 61-137 60-142 86-115 74-118 57-148 71-120 49-147 78-121 80-123 34-145 58-125 83-133 80-122 64-140 82-133 68-125 67-136 58-123 64-146 79-140 79-133 LCSD %Rec 118 112 104 94 94 120 110 110 114 118 110 114 106 106 120 112 108 110 122 100 114 98 114 118 100 92 106 106 98 104 98 88 118 104 96 120 104 70 96 102 60 75 112 94 120 114 97 100 100 124 122 107 LCSD Result 0.059 0.056 0.052 0.047 0.047 0.060 0.055 0.055 0.057 0.059 0.055 0.057 0.053 0.053 0.060 0.056 0.054 0.055 0.061 0.10 0.057 0.098 0.057 0.059 0.10 0.092 0.053 0.053 0.049 0.052 0.049 0.044 0.059 0.052 0.048 0.060 0.052 0.035 0.048 0.051 0.030 1.5 0.056 0.047 0.060 0.114 0.097 0.050 0.050 0.062 0.061 0.0534 LCS %Rec 128 118 104 100 110 134 110 114 118 126 112 118 104 110 132 120 108 118 138 100 122 98 124 130 100 97 112 110 100 112 102 100 134 110 100 124 110 84 106 106 66 70 120 100 134 119 99 122 100 136 136 110 0.064 0.059 0.052 0.050 0.055 0.067 0.055 0.057 0.059 0.063 0.056 0.059 0.052 0.055 0.066 0.060 0.054 0.059 0.069 0.10 0.061 0.098 0.062 0.065 0.10 0.097 0.056 0.055 0.050 0.056 0.051 0.050 0.067 0.055 0.050 0.062 0.055 0.042 0.053 0.053 0.033 1.4 0.060 0.050 0.067 0.119 0.099 0.061 0.050 0.068 0.068 0.0550 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.10 0.050 0.10 0.050 0.050 0.10 0.10 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 2.0 0.050 0.050 0.050 0.100 0.10 0.050 0.050 0.050 0.050 0.0500 MB Result <0.00075 <0.0012 <0.00067 <0.00080 <0.0012 <0.00054 <0.00057 <0.0016 <0.00087 <0.00072 <0.00086 <0.0013 <0.00060 <0.00093 <0.00081 <0.0010 <0.00069 <0.00068 <0.00060 <0.0023 <0.00071 <0.0011 <0.00055 <0.00080 <0.0032 <0.0069 <0.00051 <0.00085 <0.0010 <0.00050 <0.00096 <0.0025 <0.00074 <0.00058 <0.00099 <0.0024 <0.00074 <0.0023 <0.00066 <0.00054 <0.0012 <0.028 <0.00057 <0.0013 <0.00076 <0.00121 <0.00069 <0.0022 <0.0013 <0.00088 <0.00078 <0.000716 661206-1-BKSLCS Sample Id:661206-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 45 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661206-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 09.08.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD H Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 11 6 11 11 6 10 2 7 11 6 11 950108Seq Number: 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 Analysis Date Limits 75-137 82-128 61-137 72-140 85-120 76-126 78-115 71-128 51-154 72-124 67-138 LCSD %Rec 124 104 120 104 100 96 100 108 100 96 84 LCSD Result 0.062 0.052 0.060 0.052 0.050 0.048 0.050 0.054 0.050 0.048 0.042 LCS %Rec 138 110 134 116 106 106 102 116 112 102 94 0.069 0.055 0.067 0.058 0.053 0.053 0.051 0.058 0.056 0.051 0.047 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 MB Result <0.00066 <0.00074 <0.00083 <0.0010 <0.00059 <0.00078 <0.00067 <0.00071 <0.0035 <0.00072 <0.0020 661206-1-BKSLCS Sample Id:661206-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate LCSD Flag 09.08.14 08:26 09.08.14 08:26 09.08.14 08:26 Analysis Date Limits 50-150 57-158 50-150 LCSD %Rec 94 100 103 LCS %Rec 92 103 104 MB %Rec 100 108 108 % % % UnitsLCS Flag MB Flag Page 46 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661669-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 09.18.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 0 6 4 4 6 3 4 12 2 2 6 2 2 0 0 0 2 0 5 3 2 8 2 0 8 2 0 0 2 2 9 0 2 2 4 4 0 2 2 2 0 18 2 2 2 4 1 3 7 4 2 2 950876Seq Number: 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 Analysis Date Limits 61-140 68-124 79-117 72-125 78-126 73-134 75-135 63-124 73-136 77-132 81-118 80-124 59-131 81-122 74-138 83-125 81-120 83-118 54-152 61-127 78-133 61-138 78-134 60-144 65-125 60-130 79-122 72-122 73-120 76-126 56-125 61-137 60-142 86-115 74-118 57-148 71-120 49-147 78-121 80-123 34-145 58-125 83-133 80-122 64-140 82-133 68-125 67-136 58-123 64-146 79-140 79-133 LCSD %Rec 116 102 104 100 102 122 98 106 100 114 102 108 98 102 118 108 102 104 124 99 110 94 110 112 100 97 106 104 100 100 90 100 114 102 92 98 104 82 102 96 70 75 108 104 114 110 99 118 86 112 118 111 LCSD Result 0.058 0.051 0.052 0.050 0.051 0.061 0.049 0.053 0.050 0.057 0.051 0.054 0.049 0.051 0.059 0.054 0.051 0.052 0.062 0.099 0.055 0.094 0.055 0.056 0.10 0.097 0.053 0.052 0.050 0.050 0.045 0.050 0.057 0.051 0.046 0.049 0.052 0.041 0.051 0.048 0.035 1.5 0.054 0.052 0.057 0.110 0.099 0.059 0.043 0.056 0.059 0.0553 LCS %Rec 116 96 100 104 108 118 94 94 98 116 96 106 96 102 118 108 100 104 118 96 112 87 112 112 92 95 106 104 102 98 82 100 112 104 88 102 104 84 104 94 70 90 110 106 116 114 98 114 80 116 120 112 0.058 0.048 0.050 0.052 0.054 0.059 0.047 0.047 0.049 0.058 0.048 0.053 0.048 0.051 0.059 0.054 0.050 0.052 0.059 0.096 0.056 0.087 0.056 0.056 0.092 0.095 0.053 0.052 0.051 0.049 0.041 0.050 0.056 0.052 0.044 0.051 0.052 0.042 0.052 0.047 0.035 1.8 0.055 0.053 0.058 0.114 0.098 0.057 0.040 0.058 0.060 0.0562 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.10 0.050 0.10 0.050 0.050 0.10 0.10 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 2.0 0.050 0.050 0.050 0.100 0.10 0.050 0.050 0.050 0.050 0.0500 MB Result <0.00075 <0.0012 <0.00067 <0.00080 <0.0012 <0.00054 <0.00057 <0.0016 <0.00087 <0.00072 <0.00086 <0.0013 <0.00060 <0.00093 <0.00081 <0.0010 <0.00069 <0.00068 <0.00060 <0.0023 <0.00071 <0.0011 <0.00055 <0.00080 <0.0032 <0.0069 <0.00051 <0.00085 <0.0010 <0.00050 <0.00096 <0.0025 <0.00074 <0.00058 <0.00099 <0.0024 <0.00074 <0.0023 <0.00066 <0.00054 <0.0012 <0.028 <0.00057 <0.0013 <0.00076 <0.00121 <0.00069 <0.0022 <0.0013 <0.00088 <0.00078 <0.000716 661669-1-BKSLCS Sample Id:661669-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 47 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 661669-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 09.18.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 2 2 0 6 2 2 4 2 4 2 4 950876Seq Number: 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 Analysis Date Limits 75-137 82-128 61-137 72-140 85-120 76-126 78-115 71-128 51-154 72-124 67-138 LCSD %Rec 120 110 110 106 106 102 94 108 106 104 96 LCSD Result 0.060 0.055 0.055 0.053 0.053 0.051 0.047 0.054 0.053 0.052 0.048 LCS %Rec 122 112 110 112 108 104 90 110 110 102 100 0.061 0.056 0.055 0.056 0.054 0.052 0.045 0.055 0.055 0.051 0.050 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 MB Result <0.00066 <0.00074 <0.00083 <0.0010 <0.00059 <0.00078 <0.00067 <0.00071 <0.0035 <0.00072 <0.0020 661669-1-BKSLCS Sample Id:661669-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate LCSD Flag 09.18.14 07:50 09.18.14 07:50 09.18.14 07:50 Analysis Date Limits 50-150 57-158 50-150 LCSD %Rec 96 102 101 LCS %Rec 98 103 100 MB %Rec 118 108 100 % % % UnitsLCS Flag MB Flag Page 48 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 493454-004Parent Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035APrep Method: 09.18.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter X X Flag 950876Seq Number: 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 Analysis Date Limits 62-137 64-128 61-130 65-136 33-158 42-152 48-135 58-134 43-139 66-134 69-132 71-120 53-140 68-126 67-134 68-127 70-129 72-118 68-151 42-147 68-127 32-142 68-127 64-135 34-149 43-163 65-135 67-121 66-137 60-129 48-147 42-170 71-117 71-117 59-135 44-166 62-127 34-157 41-155 63-128 16-171 23-148 65-139 57-138 62-133 69-130 48-169 17-184 27-157 59-136 67-134 71-124 MS %Rec 123 85 92 108 115 123 92 92 100 115 92 100 100 100 115 108 92 100 123 96 108 84 108 115 92 93 108 100 92 92 85 108 131 100 85 108 108 92 92 85 85 94 108 108 115 118 96 292 77 123 123 110 0.16 0.11 0.12 0.14 0.15 0.16 0.12 0.12 0.13 0.15 0.12 0.13 0.13 0.13 0.15 0.14 0.12 0.13 0.16 0.24 0.14 0.21 0.14 0.15 0.23 0.25 0.14 0.13 0.12 0.12 0.11 0.14 0.17 0.13 0.11 0.14 0.14 0.12 0.12 0.11 0.11 4.7 0.14 0.14 0.15 0.294 0.24 0.38 0.10 0.16 0.16 0.143 Spike Amount 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.25 0.13 0.25 0.13 0.13 0.25 0.25 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 5.0 0.13 0.13 0.13 0.250 0.25 0.13 0.13 0.13 0.13 0.130 Parent Result <0.0019 <0.0030 <0.0017 <0.0020 <0.0029 <0.0014 <0.0014 <0.0041 <0.0022 <0.0018 <0.0022 <0.0032 <0.0015 <0.0023 <0.0020 <0.0025 <0.0017 <0.0017 <0.0015 <0.0057 <0.0018 <0.0028 <0.0014 <0.0020 <0.0081 0.017 <0.0013 <0.0021 <0.0025 <0.0013 <0.0024 <0.0062 <0.0019 <0.0015 <0.0025 <0.0061 <0.0019 <0.0058 <0.0017 <0.0014 <0.0030 <0.070 <0.0014 <0.0032 <0.0019 <0.00304 <0.0017 <0.0054 <0.0033 <0.0022 <0.0020 <0.00180 493454-004 SMS Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 49 of 69 Final 1.000 QC Summary 492739 Terraquest Environmental Consultants, P.C. Lisa Parker/Reid Co QM#7 493454-004Parent Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035APrep Method: 09.18.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter Flag 950876Seq Number: 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 Analysis Date Limits 65-131 50-143 67-131 42-156 13-188 57-143 55-141 39-150 34-179 13-188 40-161 MS %Rec 123 108 108 115 108 108 85 115 131 85 108 0.16 0.14 0.14 0.15 0.14 0.14 0.11 0.15 0.17 0.11 0.14 Spike Amount 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 0.13 Parent Result <0.0017 <0.0019 <0.0021 <0.0026 <0.0015 <0.0020 <0.0017 <0.0018 <0.0088 <0.0018 <0.0051 493454-004 SMS Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate 09.18.14 16:56 09.18.14 16:56 09.18.14 16:56 Analysis Date Limits 50-150 57-158 50-150 MS %Rec 102 100 98 % % % UnitsMS Flag Page 50 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661198-1-BLKLab Sample Id: WATERMatrix: 661198-1-BLK Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.08.14 13:45Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene Benzo(a)pyrene 1,3-Dinitrobenzene 1,4-Dichlorobenzene 1-Methylnaphthalene + Benzo(b)fluoranthene Benzo(k)fluoranthene 2,4-Dichlorophenol Benzo(g,h,i)perylene 2,4-Dimethylphenol Benzyl alcohol 2,4-Dinitrophenol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl Phenyl Ether 1,2-Dichlorobenzene Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane bis(2-chloroethyl) ether 1,2-Diphenylhydrazine bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene di-n-Octyl Phthalate Parameter 2.01 2.21 2.11 1.90 1.80 20.1 1.61 1.40 1.97 2.71 1.78 1.97 1.63 1.23 7.11 1.83 2.12 2.18 3.09 1.35 1.83 1.43 3.88 1.48 1.40 1.25 1.78 4.76 1.24 1.20 1.29 1.82 2.09 1.83 1.64 1.90 1.97 2.08 1.19 1.38 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 10.0 20.0 10.0 10.0 10.0 50.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 20.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 50-32-8 99-65-0 106-46-7 90-12-0 205-99-2 207-08-9 120-83-2 191-24-2 105-67-9 100-51-6 51-28-5 95-57-8 101-55-3 59-50-7 106-47-8 7005-72-3 95-50-1 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 111-44-4 122-66-7 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 117-84-0 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950218Seq Number: MDLRL 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 Analysis Date Page 51 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661198-1-BLKLab Sample Id: WATERMatrix: 661198-1-BLK Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.08.14 13:45Date Prep: BROTech: 2-methylphenol Fluoranthene Fluorene 3&4-Methylphenol Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene 2-Nitrophenol 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine Pentachlorophenol 1,2,4-Trichlorobenzene 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) Parameter 2.00 1.81 1.56 2.55 2.21 1.78 1.87 2.38 1.87 1.95 2.41 1.41 1.52 1.49 1.36 2.50 2.26 1.43 1.64 2.04 1.76 2.40 Result U U U U U U U U U U U U U U U U U U U U U U JN JN JN JN JN 10.0 10.0 10.0 20.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 95-48-7 206-44-0 86-73-7 15831-10-4 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 88-75-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 120-82-1 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC U U U U U U U U U U U U U U U U U U U U U U 5.21 5.77 5.10 4.25 6.03 950218Seq Number: MDLRL 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 09.09.14 13:36 Analysis Date Page 52 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661206-1-BLKLab Sample Id: SOLIDMatrix: 661206-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.08.14 06:51Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Parameter 0.00075 0.0012 0.00067 0.00080 0.0012 0.00054 0.00057 0.0016 0.00087 0.00072 0.00086 0.0013 0.00060 0.00093 0.00081 0.00100 0.00069 0.00068 0.00060 0.0023 0.00071 0.0011 0.00055 0.00080 0.0032 0.0069 0.00051 0.00085 0.0010 0.00050 0.00096 0.0025 0.00074 0.00058 0.00099 0.0024 0.00074 0.0023 0.00066 0.00054 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 0.0050 0.0010 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950108Seq Number: MDLRL 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 Analysis Date Page 53 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661206-1-BLKLab Sample Id: SOLIDMatrix: 661206-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.08.14 06:51Date Prep: MWETech: Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.0012 0.028 0.00057 0.0013 0.00076 0.00121 0.00069 0.0022 0.0013 0.00088 0.00078 0.000716 0.00066 0.00074 0.00083 0.0010 0.00059 0.00078 0.00067 0.00071 0.0035 0.00072 0.0020 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0020 0.050 0.0010 0.0020 0.0010 0.00200 0.0020 0.0050 0.0020 0.0010 0.0010 0.00100 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U 950108Seq Number: MDLRL 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 09.08.14 09:54 Analysis Date Page 54 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661230-1-BLKLab Sample Id: SOLIDMatrix: 661230-1-BLK Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3550Prep Method: 09.09.14 11:30Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 20.0 10.0 10.0 Result U U U 20.0 10.0 10.0 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C1 ALHYDRC19C U U U 950483Seq Number: MDLRL 09.09.14 17:15 09.09.14 17:18 09.09.14 17:18 Analysis Date Page 55 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661234-1-BLKLab Sample Id: SOLIDMatrix: 661234-1-BLK Sample Id: TPH-Diesel Range Organics by SW-846 8015C Analytical Method: CLARAnalyst: SW3545Prep Method: 09.09.14 14:00Date Prep: 5458Tech: TPH-DRO (C10-C28) Parameter 2.56 Result U8.33 Flag mg/kg Units 1 DilCas Number C10C28DRO U 950381Seq Number: MDLRL 09.10.14 13:11 Analysis Date Page 56 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661256-1-BLKLab Sample Id: SOLIDMatrix: 661256-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.09.14 16:00Date Prep: 5458Tech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether Parameter 0.0590 0.0540 0.0527 0.0520 0.0613 0.0643 0.0423 0.0607 0.0537 0.0433 0.0607 0.0597 0.0510 0.0467 0.0447 0.0420 0.0987 0.0487 0.0460 0.0580 0.0567 0.0477 0.0553 0.0633 0.0507 0.0410 0.0467 0.0567 0.0367 0.0493 0.0540 0.0490 0.0543 0.0550 0.0573 0.0527 0.0500 0.0400 0.0473 0.0450 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.667 1.67 0.333 0.333 0.333 0.167 0.333 0.333 0.333 0.667 0.667 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.167 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 39638-32-9 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950332Seq Number: MDLRL 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 Analysis Date Page 57 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661256-1-BLKLab Sample Id: SOLIDMatrix: 661256-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.09.14 16:00Date Prep: 5458Tech: bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0540 0.0443 0.0647 0.0427 0.0537 0.0503 0.0613 0.0553 0.0433 0.0407 0.0557 0.0370 0.0573 0.0517 0.0607 0.0343 0.0533 0.0593 0.0477 0.0700 0.0603 0.0553 0.0467 0.0567 0.0633 Result U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.333 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U 950332Seq Number: MDLRL 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 09.10.14 14:57 Analysis Date Page 58 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661361-1-BLKLab Sample Id: SOLIDMatrix: 661361-1-BLK Sample Id: TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: JOLAnalyst: SW5030BPrep Method: 09.09.14 08:15Date Prep: JOLTech: TPH-GRO Parameter 1.5 Result U2.5 Flag mg/kg Units 50 DilCas Number 8006-61-9 U 950391Seq Number: MDLRL 09.09.14 09:50 Analysis Date Page 59 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661366-1-BLKLab Sample Id: SOLIDMatrix: 661366-1-BLK Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 09.08.14 11:20Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000750 0.000750 0.000250 Result U U U 0.000750 0.000750 0.000250 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C1 HYDC9C10 U U U 950395Seq Number: MDLRL 09.08.14 12:52 09.08.14 12:52 09.08.14 12:52 Analysis Date Page 60 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661531-1-BLKLab Sample Id: SOLIDMatrix: 661531-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16:00Date Prep: TUETech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether Parameter 0.0590 0.0540 0.0527 0.0520 0.0613 0.0643 0.0423 0.0607 0.0537 0.0433 0.0607 0.0597 0.0510 0.0467 0.0447 0.0420 0.0987 0.0487 0.0460 0.0580 0.0567 0.0477 0.0553 0.0633 0.0507 0.0410 0.0467 0.0567 0.0367 0.0493 0.0540 0.0490 0.0543 0.0550 0.0573 0.0527 0.0500 0.0400 0.0473 0.0450 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.667 1.67 0.333 0.333 0.333 0.167 0.333 0.333 0.333 0.667 0.667 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.167 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 39638-32-9 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: MDLRL 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 Analysis Date Page 61 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661531-1-BLKLab Sample Id: SOLIDMatrix: 661531-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 09.15.14 16:00Date Prep: TUETech: bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0540 0.0443 0.0647 0.0427 0.0537 0.0503 0.0613 0.0553 0.0433 0.0407 0.0557 0.0370 0.0573 0.0517 0.0607 0.0343 0.0533 0.0593 0.0477 0.0700 0.0603 0.0553 0.0467 0.0567 0.0633 Result U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.333 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U 950874Seq Number: MDLRL 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 09.17.14 16:15 Analysis Date Page 62 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661612-1-BLKLab Sample Id: SOLIDMatrix: 661612-1-BLK Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 09.16.14 14:41Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000750 0.000750 0.000250 Result U U U 0.000750 0.000750 0.000250 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C1 HYDC9C10 U U U 950789Seq Number: MDLRL 09.16.14 16:45 09.16.14 16:45 09.16.14 16:45 Analysis Date Page 63 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661669-1-BLKLab Sample Id: SOLIDMatrix: 661669-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06:43Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Parameter 0.00075 0.0012 0.00067 0.00080 0.0012 0.00054 0.00057 0.0016 0.00087 0.00072 0.00086 0.0013 0.00060 0.00093 0.00081 0.00100 0.00069 0.00068 0.00060 0.0023 0.00071 0.0011 0.00055 0.00080 0.0032 0.0069 0.00051 0.00085 0.0010 0.00050 0.00096 0.0025 0.00074 0.00058 0.00099 0.0024 0.00074 0.0023 0.00066 0.00054 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 0.0050 0.0010 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 950876Seq Number: MDLRL 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 Analysis Date Page 64 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661669-1-BLKLab Sample Id: SOLIDMatrix: 661669-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 09.18.14 06:43Date Prep: MWETech: Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.0012 0.028 0.00057 0.0013 0.00076 0.00121 0.00069 0.0022 0.0013 0.00088 0.00078 0.000716 0.00066 0.00074 0.00083 0.0010 0.00059 0.00078 0.00067 0.00071 0.0035 0.00072 0.0020 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0020 0.050 0.0010 0.0020 0.0010 0.00200 0.0020 0.0050 0.0020 0.0010 0.0010 0.00100 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U 950876Seq Number: MDLRL 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 09.18.14 09:18 Analysis Date Page 65 of 69 Final 1.000 Blank Summary 492739 Terraquest Environmental Consultants, P.C., Mebane, NC Lisa Parker/Reid Co QM#7 661723-1-BLKLab Sample Id: SOLIDMatrix: 661723-1-BLK Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 09.18.14 16:00Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 20.0 10.0 10.0 Result U U U 20.0 10.0 10.0 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C1 ALHYDRC19C U U U 951157Seq Number: MDLRL 09.22.14 11:20 09.22.14 11:25 09.22.14 11:25 Analysis Date Page 66 of 69 Final 1.000 Page 67 of 69 Final 1.000 Page 68 of 69 Final 1.000 Prelogin/Nonconformance Report- Sample Log-In XENCO Laboratories 492739Work Order #: 09/05/2014 09:50:00 AMDate/ Time Received: Terraquest Environmental Consultants, PClient: Sample Receipt Checklist Checklist completed by: Date: Checklist reviewed by:Date: Mike Kimmel 09/05/2014 09/05/2014 #2 *Shipping container in good condition? #3 *Samples received on ice? #4 *Custody Seals intact on shipping container/ cooler? #5 Custody Seals intact on sample bottles? #6 *Custody Seals Signed and dated? #7 *Chain of Custody present? #8 Sample instructions complete on Chain of Custody? #9 Any missing/extra samples? #10 Chain of Custody signed when relinquished/ received? #11 Chain of Custody agrees with sample label(s)? #12 Container label(s) legible and intact? #13 Sample matrix/ properties agree with Chain of Custody? #14 Samples in proper container/ bottle? #15 Samples properly preserved? #16 Sample container(s) intact? #17 Sufficient sample amount for indicated test(s)? #18 All samples received within hold time? #19 Subcontract of sample(s)? #20 VOC samples have zero headspace (less than 1/4 inch bubble)? #21 <2 for all samples preserved with HNO3,HCL, H2SO4? #22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH? Yes Yes N/A N/A N/A Yes Yes No Yes Yes Yes Yes Yes Yes Yes Yes Yes No N/A N/A N/A #1 *Temperature of cooler(s)?1.2 Acceptable Temperature Range: 0 - 6 degC Air and Metal samples Acceptable Range: Ambient * Must be completed for after-hours delivery of samples prior to placing in the refrigerator Analyst: PH Device/Lot#: Comments Dario Lagunas Temperature Measuring device used : #61 Page 69 of 69 Final 1.000 Analytical Report 493612 for Terraquest Environmental Consultants, P.C. Project Manager: Ryan Kerins Parkers Stop & Shop 26-SEP-14 03014 6017 Financial Dr., Norcross, GA 30071 Ph:(770) 449-8800 Fax:(770) 449-5477 Xenco-Houston (EPA Lab code: TX00122): Texas (T104704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054) New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610) Xenco-Atlanta (EPA Lab Code: GA00046): Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135) Texas (T104704477), Louisiana (04176), USDA (P330-07-00105) Xenco-Lakeland: Florida (E84098) Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX) Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX) Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757) Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757) Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758) Collected By: Client Page 1 of 28 Final 1.000 Page 2 of 28 Final 1.000 Table of Contents Cover Page 1 Cover Letter 3 Sample ID Cross Reference 4 Explanation of Qualifiers (Flags) 5 Hits Summary 6 Certificate of Analysis (Detailed Report) 10 Summary of Quality control 21 Blank Summary 23 Chain of Custody 25 Sample Receipt Conformance Report 28 Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Project Manager: Ryan Kerins Terraquest Environmental Consultants, P.C. 100 E. Ruffin Street Mebane, NC 27302 Reference: XENCO Report No(s): 493612 Parkers Stop & Shop Project Address: NC Ryan Kerins: We are reporting to you the results of the analyses performed on the samples received under the project name referenced above and identified with the XENCO Report Number(s) 493612. All results being reported under this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using all other available quality control measures. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise arranged with you. The samples received, and described as recorded in Report No. 493612 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard practices, controlled substances under regulated protocols, etc). We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions concerning this report, please feel free to contact us at any time. Respectfully, 26-SEP-14 Client Services Manager Mike Kimmel Page 3 of 28 Final 1.000 Sample Cross Reference 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop Sample Id MW1A GW2 MW4 Trip Blank 09-17-14 13:15 09-17-14 14:45 09-17-14 14:45 09-17-14 00:00 Date Collected Lab Sample Id 493612-001 493612-002 493612-003 493612-004 Sample DepthMatrix W W W W Page 4 of 28 Final 1.000 Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America 4143 Greenbriar Dr, Stafford, TX 77477 9701 Harry Hines Blvd , Dallas, TX 75220 5332 Blackberry Drive, San Antonio TX 78238 2505 North Falkenburg Rd, Tampa, FL 33619 12600 West I-20 East, Odessa, TX 79765 6017 Financial Drive, Norcross, GA 30071 3725 E. Atlanta Ave, Phoenix, AZ 85040 Phone Fax (281) 240-4200 (281) 240-4280 (214) 902 0300 (214) 351-9139 (210) 509-3334 (210) 509-3335 (813) 620-2000 (813) 620-2033 (432) 563-1800 (432) 563-1713 (770) 449-8800 (770) 449-5477 (602) 437-0330 Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Flagging Criteria X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD. B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination. D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference. Dilution factors are included in the final results. The result is from a diluted sample. E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated. F RPD exceeded lab control limits. J The target analyte was positively identified below the quantitation limit and above the detection limit. U Analyte was not detected. L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations. H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the Department Supervisor and QA Director. Data were determined to be valid for reporting. K Sample analyzed outside of recommended hold time. JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated numerical value may not be consistent with the amount actually present in the environmental sample. ** Surrogate recovered outside laboratory control limit. BRL Below Reporting Limit. RL Reporting Limit MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation DL Method Detection Limit NC Non-Calculable + NELAC certification not offered for this compound. * (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation Page 5 of 28 Final 1.000 Hits Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received : % Moisture : 09.17.14 13.15 Date Collected : 493612-001Lab Sample Id : Ground WaterMatrix : MW1ASample Id : SVOCs by EPA 625 + 10 TICs Analytical Method :E625PPrep Method: 09.19.14 14.00 Date Prep: 1-Methylnaphthalene + bis(2-ethylhexyl) phthalate 2-Methylnaphthalene Naphthalene Benzene, 1,2,4-trimethyl- (TIC) Indane (TIC) unknown (TIC) unknown (TIC) Ethylbenzene (TIC) unknown (TIC) Cyclopentanol, 1-methyl- (TIC) unknown (TIC) 1,3-Dimethylcyclopentanol (TIC) 1-Methylcyclohexanol (TIC) Parameter Result J D JN JN JN JN JN JN JN JN JN JN Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 5 1 1 1 1 1 1 1 1 1 1 DilCas Number 90-12-0 117-81-7 91-57-6 91-20-3 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC 30.4 3.12 16.9 188 32.3 180 82.1 31.7 242 45.6 103 53.8 99.3 49.9 951294Seq Number 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 09.33 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 Analysis Date Page 6 of 28 Final 1.000 Hits Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received : % Moisture : 09.17.14 14.45 Date Collected : 493612-002Lab Sample Id : Ground WaterMatrix : GW2Sample Id : SVOCs by EPA 625 + 10 TICs Analytical Method :E625PPrep Method: 09.19.14 14.00 Date Prep: Anthracene Benzo(a)anthracene Benzo(a)pyrene 1-Methylnaphthalene + Benzo(g,h,i)perylene bis(2-ethylhexyl) phthalate Chrysene 2-Methylnaphthalene Fluoranthene Fluorene Phenanthrene Pyrene Naphthalene, 2,3-dimethyl- (TIC) Nonane, 3,7-dimethyl- (TIC) Benzene, 1-methyl-3-propyl- (TIC) unknown hydrocarbon (TIC) Benzene, 1-methyl-4-(1-methylethyl (TIC) unknown (TIC) Naphthalene, 1-ethyl- (TIC) Pentadecane (TIC) Heptadecane (TIC) Tetradecane (TIC) Parameter Result J J J D J J J D J J JN JN JN JN JN JN JN JN JN JN Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 100 1 1 1 100 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 56-55-3 50-32-8 90-12-0 191-24-2 117-81-7 218-01-9 91-57-6 206-44-0 86-73-7 85-01-8 129-00-0 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC 8.26 3.62 2.39 1310 2.00 7.87 2.71 3100 7.40 8.06 25.8 10.1 316 163 268 199 282 167 180 255 154 343 951294Seq Number 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 10.30 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 10.30 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 Analysis Date Page 7 of 28 Final 1.000 Hits Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received : % Moisture : 09.17.14 14.45 Date Collected : 493612-003Lab Sample Id : Ground WaterMatrix : MW4Sample Id : SVOCs by EPA 625 + 10 TICs Analytical Method :E625PPrep Method: 09.19.14 14.00 Date Prep: 1-Methylnaphthalene + bis(2-ethylhexyl) phthalate 2-Methylnaphthalene Naphthalene Benzene, 1,2,3-trimethyl- (TIC) Benzene, 1,2,3-trimethyl- (TIC) Benzene, 1-ethyl-2-methyl- (TIC) p-Xylene (TIC) p-Xylene (TIC) Benzene, 1-ethyl-2-methyl- (TIC) Benzene, 1,2,3-trimethyl- (TIC) Indane (TIC) Ethylbenzene (TIC) Benzene, 1-methyl-4-(1-methylethyl (TIC) Parameter Result J D JN JN JN JN JN JN JN JN JN JN Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 5 1 1 1 1 1 1 1 1 1 1 DilCas Number 90-12-0 117-81-7 91-57-6 91-20-3 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC 51.6 6.03 110 208 1220 290 692 925 674 232 345 118 293 131 951294Seq Number 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 10.01 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 Analysis Date Page 8 of 28 Final 1.000 Hits Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received : % Moisture : 09.17.14 00.00 Date Collected : 493612-004Lab Sample Id : Ground WaterMatrix : Trip BlankSample Id : SVOCs by EPA 625 + 10 TICs Analytical Method :E625PPrep Method: 09.19.14 14.00 Date Prep: Benzyl alcohol bis(2-ethylhexyl) phthalate unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) Parameter Result J J JN JN JN JN JN JN JN Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 DilCas Number 100-51-6 117-81-7 TIC TIC TIC TIC TIC TIC TIC 5.65 2.45 5.14 4.75 6.51 5.72 7.31 4.49 4.97 951294Seq Number 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 Analysis Date Page 9 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 13.15 Date Collected:493612-001Lab Sample Id: Ground WaterMatrix: MW1ASample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene Parameter 1.99 2.19 2.09 1.88 19.9 1.78 1.59 1.39 1.95 1.76 2.68 1.61 1.95 7.04 1.22 1.81 2.10 2.16 3.06 1.81 1.34 1.42 3.84 1.47 1.39 1.24 4.71 1.76 1.23 1.19 1.28 1.80 2.07 1.81 1.62 1.88 1.95 2.06 1.18 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U J U U U U U U U U 9.90 49.5 9.90 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 19.8 9.90 9.90 19.8 9.90 9.90 9.90 9.90 19.8 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 99-65-0 50-32-8 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 105-67-9 191-24-2 51-28-5 100-51-6 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 U U U U U U U 30.4 U U U U U U U U U U U U U U U U U U U U U 3.12 U U U U U U U U 16.9 951294Seq Number: RL MDL 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 Analysis Date % Moisture: Page 10 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 13.15 Date Collected:493612-001Lab Sample Id: Ground WaterMatrix: MW1ASample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene 1,3-Dimethylcyclopentanol (TIC) 1-Methylcyclohexanol (TIC) Benzene, 1,2,4-trimethyl- (TIC) Cyclopentanol, 1-methyl- (TIC) Ethylbenzene (TIC) Indane (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) Parameter 1.37 1.98 1.79 2.52 1.54 2.19 1.76 1.85 2.36 1.93 1.85 2.39 1.40 7.52 1.48 1.35 2.48 1.42 2.24 1.62 2.02 1.74 2.38 Result U U U U U U U U U U U U U D U U U U UH U U U U JN JN JN JN JN JN JN JN JN JN 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 5 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-84-0 95-48-7 206-44-0 15831-10-4 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC U U U U U U U U U U U U U 188 U U U U U U U U U 99.3 49.9 32.3 103 242 180 53.8 31.7 45.6 82.1 951294Seq Number: RL MDL 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 09.33 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 Analysis Date Surrogate 44-117 30-100 48-117 46-111 50-200 % Recovery Flag % % % % % 68 68 88 69 76 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 09.23.14 07.10 Cas Number 321-60-8 367-12-4 118-79-6 4165-60-0 4165-62-2 Units Analysis Date 2-Fluorobiphenyl 2-Fluorophenol 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Limits % Moisture: Page 11 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 13.15 Date Collected:493612-001Lab Sample Id: Ground WaterMatrix: MW1ASample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: 951294Seq Number: Surrogate 46-126 % Recovery Flag %87 09.23.14 07.10 Cas Number 1718-51-0 Units Analysis Date Terphenyl-D14 Limits % Moisture: Page 12 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-002Lab Sample Id: Ground WaterMatrix: GW2Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene Parameter 1.99 2.19 2.09 1.88 19.9 1.78 1.59 139 1.95 1.76 2.68 1.61 1.95 7.04 1.22 1.81 2.10 2.16 3.06 1.81 1.34 1.42 3.84 1.47 1.39 1.24 4.71 1.76 1.23 1.19 1.28 1.80 2.07 1.81 1.62 1.88 1.95 2.06 118 Result J U U J U J U D U U U U J U U U U U U U U U U U U U U U U J U U J U U U U U D 9.90 49.5 9.90 9.90 49.5 9.90 9.90 990 9.90 9.90 9.90 9.90 9.90 49.5 19.8 9.90 9.90 19.8 9.90 9.90 9.90 9.90 19.8 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 990 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 100 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 100 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 99-65-0 50-32-8 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 105-67-9 191-24-2 51-28-5 100-51-6 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 8.26 U U 3.62 U 2.39 U 1310 U U U U 2.00 U U U U U U U U U U U U U U U U 7.87 U U 2.71 U U U U U 3100 951294Seq Number: RL MDL 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 10.30 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 10.30 Analysis Date % Moisture: Page 13 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-002Lab Sample Id: Ground WaterMatrix: GW2Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene Benzene, 1-methyl-3-propyl- (TIC) Benzene, 1-methyl-4-(1-methylethyl (TIC) Heptadecane (TIC) Naphthalene, 1-ethyl- (TIC) Naphthalene, 2,3-dimethyl- (TIC) Nonane, 3,7-dimethyl- (TIC) Pentadecane (TIC) Tetradecane (TIC) unknown (TIC) unknown hydrocarbon (TIC) Parameter 1.37 1.98 1.79 2.52 1.54 2.19 1.76 1.85 2.36 1.93 1.85 2.39 1.40 1.50 1.48 1.35 2.48 1.42 2.24 1.62 2.02 1.74 2.38 Result U U J U J U U U U U U U U U U U U U UH U U JN JN JN JN JN JN JN JN JN JN 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-84-0 95-48-7 206-44-0 15831-10-4 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC U U 7.40 U 8.06 U U U U U U U U U U U U U U U 25.8 U 10.1 268 282 154 180 316 163 255 343 167 199 951294Seq Number: RL MDL 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 Analysis Date Surrogate 44-117 30-100 48-117 46-111 50-200 % Recovery ** Flag % % % % % 75 113 106 101 95 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 09.23.14 08.36 Cas Number 321-60-8 367-12-4 118-79-6 4165-60-0 4165-62-2 Units Analysis Date 2-Fluorobiphenyl 2-Fluorophenol 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Limits % Moisture: Page 14 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-002Lab Sample Id: Ground WaterMatrix: GW2Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: 951294Seq Number: Surrogate 46-126 % Recovery Flag %86 09.23.14 08.36 Cas Number 1718-51-0 Units Analysis Date Terphenyl-D14 Limits % Moisture: Page 15 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-003Lab Sample Id: Ground WaterMatrix: MW4Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene Parameter 1.99 2.19 2.09 1.88 19.9 1.78 1.59 1.39 1.95 1.76 2.68 1.61 1.95 7.04 1.22 1.81 2.10 2.16 3.06 1.81 1.34 1.42 3.84 1.47 1.39 1.24 4.71 1.76 1.23 1.19 1.28 1.80 2.07 1.81 1.62 1.88 1.95 2.06 1.18 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U J U U U U U U U U 9.90 49.5 9.90 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 19.8 9.90 9.90 19.8 9.90 9.90 9.90 9.90 19.8 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 99-65-0 50-32-8 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 105-67-9 191-24-2 51-28-5 100-51-6 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 U U U U U U U 51.6 U U U U U U U U U U U U U U U U U U U U U 6.03 U U U U U U U U 110 951294Seq Number: RL MDL 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 Analysis Date % Moisture: Page 16 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-003Lab Sample Id: Ground WaterMatrix: MW4Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene Benzene, 1,2,3-trimethyl- (TIC) Benzene, 1,2,3-trimethyl- (TIC) Benzene, 1,2,3-trimethyl- (TIC) Benzene, 1-ethyl-2-methyl- (TIC) Benzene, 1-ethyl-2-methyl- (TIC) Benzene, 1-methyl-4-(1-methylethyl (TIC) Ethylbenzene (TIC) Indane (TIC) p-Xylene (TIC) p-Xylene (TIC) Parameter 1.37 1.98 1.79 2.52 1.54 2.19 1.76 1.85 2.36 1.93 1.85 2.39 1.40 7.52 1.48 1.35 2.48 1.42 2.24 1.62 2.02 1.74 2.38 Result U U U U U U U U U U U U U D U U U U UH U U U U JN JN JN JN JN JN JN JN JN JN 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 5 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-84-0 95-48-7 206-44-0 15831-10-4 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC TIC TIC TIC TIC TIC U U U U U U U U U U U U U 208 U U U U U U U U U 345 1220 290 232 692 131 293 118 925 674 951294Seq Number: RL MDL 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 10.01 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 Analysis Date Surrogate 30-100 44-117 48-117 46-111 50-200 % Recovery Flag % % % % % 66 69 85 68 72 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 09.23.14 07.38 Cas Number 367-12-4 321-60-8 118-79-6 4165-60-0 4165-62-2 Units Analysis Date 2-Fluorophenol 2-Fluorobiphenyl 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Limits % Moisture: Page 17 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 14.45 Date Collected:493612-003Lab Sample Id: Ground WaterMatrix: MW4Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: 951294Seq Number: Surrogate 46-126 % Recovery Flag %89 09.23.14 07.38 Cas Number 1718-51-0 Units Analysis Date Terphenyl-D14 Limits % Moisture: Page 18 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 00.00 Date Collected:493612-004Lab Sample Id: Ground WaterMatrix: Trip BlankSample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: Anthracene Benzoic Acid 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene Parameter 1.99 2.19 2.09 1.88 19.9 1.78 1.59 1.39 1.95 1.76 2.68 1.61 1.95 7.04 1.22 1.81 2.10 2.16 3.06 1.81 1.34 1.42 3.84 1.47 1.39 1.24 4.71 1.76 1.23 1.19 1.28 1.80 2.07 1.81 1.62 1.88 1.95 2.06 1.18 Result U U U U U U U U U U U U U U J U U U U U U U U U U U U U U J U U U U U U U U U 9.90 49.5 9.90 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 19.8 9.90 9.90 19.8 9.90 9.90 9.90 9.90 19.8 9.90 49.5 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 65-85-0 541-73-1 56-55-3 99-65-0 50-32-8 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 105-67-9 191-24-2 51-28-5 100-51-6 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 U U U U U U U U U U U U U U 5.65 U U U U U U U U U U U U U U 2.45 U U U U U U U U U 951294Seq Number: RL MDL 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 Analysis Date % Moisture: Page 19 of 28 Final 1.000 Certificate of Analytical Results 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 09.19.14 10.05 Date Received: 09.17.14 00.00 Date Collected:493612-004Lab Sample Id: Ground WaterMatrix: Trip BlankSample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14.00 Date Prep: BROTech: di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) Parameter 1.37 1.98 1.79 2.52 1.54 2.19 1.76 1.85 2.36 1.93 1.85 2.39 1.40 1.50 1.48 1.35 2.48 1.42 2.24 1.62 2.02 1.74 2.38 Result U U U U U U U U U U U U U U U U U U UH U U U U JN JN JN JN JN JN JN 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 9.90 9.90 49.5 9.90 9.90 9.90 9.90 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-84-0 95-48-7 206-44-0 15831-10-4 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 88-06-2 85-01-8 108-95-2 129-00-0 TIC TIC TIC TIC TIC TIC TIC U U U U U U U U U U U U U U U U U U U U U U U 7.31 4.97 5.72 5.14 6.51 4.75 4.49 951294Seq Number: RL MDL 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 Analysis Date Surrogate 30-100 44-117 48-117 46-111 50-200 46-126 % Recovery Flag % % % % % % 57 64 82 59 61 94 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 09.23.14 08.07 Cas Number 367-12-4 321-60-8 118-79-6 4165-60-0 4165-62-2 1718-51-0 Units Analysis Date 2-Fluorophenol 2-Fluorobiphenyl 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-D14 Limits % Moisture: Page 20 of 28 Final 1.000 QC Summary 493612 Terraquest Environmental Consultants, P.C. Parkers Stop & Shop 661823-1-BLKMB Sample Id: WaterMatrix: SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method: 09.19.14Date Prep: Anthracene 1,3-Dichlorobenzene Benzo(a)anthracene 1,3-Dinitrobenzene Benzo(a)pyrene 1,4-Dichlorobenzene 1-Methylnaphthalene Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene 2,4-Dimethylphenol Benzo(g,h,i)perylene 2,4-Dinitrophenol Benzyl alcohol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene di-n-Octyl Phthalate 2-methylphenol Fluoranthene 3&4-Methylphenol Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 3 3 1 3 3 1 5 1 8 6 6 1 13 2 1 2 9 9 0 2 3 5 5 5 3 5 3 0 1 1 1 1 4 4 3 2 2 2 10 5 9 5 3 2 5 1 6 2 1 5 1 2 951294Seq Number: 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 Analysis Date Limits 27-133 65-135 33-143 45-110 17-163 20-124 25-175 24-159 39-135 11-162 32-119 0-219 0-191 30-110 36-120 53-127 22-147 15-110 32-129 25-158 47-145 33-145 10-181 33-184 55-115 12-158 36-166 8-158 60-118 0-152 17-168 0-227 55-105 0-114 0-112 1-118 45-105 0-107 40-110 26-137 30-110 59-121 0-152 24-116 41-125 40-113 29-182 0-171 0-132 21-196 21-133 35-180 LCSD %Rec 88 66 83 86 98 65 76 93 75 89 74 86 114 73 67 84 83 65 65 79 81 88 96 75 86 70 81 89 73 92 83 90 79 86 87 78 71 90 64 89 65 82 88 68 78 66 75 91 80 75 70 72 LCSD Result 43.9 32.8 41.5 43.1 48.9 32.3 38.2 46.7 37.5 44.7 37.0 42.8 56.8 36.4 33.6 42.1 41.3 32.3 32.7 39.5 40.4 43.8 48.1 37.7 43.1 35.2 40.6 44.6 36.6 45.9 41.4 44.9 39.6 42.8 43.5 38.9 35.3 45.1 31.9 44.5 32.7 40.8 44.0 34.1 39.2 32.8 37.4 45.5 40.0 37.7 35.1 36.0 LCS %Rec 86 68 82 83 95 65 73 93 69 84 70 87 99 75 67 82 76 71 65 78 78 84 91 72 84 74 84 89 73 91 82 89 76 82 84 76 69 88 70 85 72 78 85 70 75 66 70 89 81 72 70 70 42.8 33.8 41.0 41.7 47.3 32.7 36.5 46.3 34.5 42.1 34.9 43.3 49.7 37.3 33.4 41.1 37.9 35.3 32.7 38.8 39.2 41.8 45.7 35.8 42.0 37.0 42.0 44.6 36.4 45.6 40.8 44.4 38.2 41.2 42.1 38.2 34.5 44.2 35.1 42.4 35.8 38.9 42.7 34.8 37.3 33.1 35.2 44.6 40.5 35.8 34.8 35.2 Spike Amount 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 MB Result <2.01 <2.11 <1.90 <20.1 <1.80 <1.61 <1.40 <1.97 <1.78 <2.71 <1.63 <1.97 <7.11 <1.23 <1.83 <2.12 <2.18 <3.09 <1.83 <1.35 <1.43 <1.48 <1.40 <1.25 <4.76 <1.78 <1.24 <1.20 <1.29 <1.82 <2.09 <1.83 <1.64 <1.90 <1.97 <2.08 <1.19 <1.38 <2.00 <1.81 <2.55 <1.56 <2.21 <1.78 <1.87 <2.38 <1.95 <1.87 <2.41 <1.41 <1.52 <1.49 661823-1-BKSLCS Sample Id:661823-1-BSDLCSD Sample Id: ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L UnitsLCS Result Page 21 of 28 Final 1.000 QC Summary 493612 Terraquest Environmental Consultants, P.C. Parkers Stop & Shop 661823-1-BLKMB Sample Id: WaterMatrix: SVOCs by EPA 625 + 10 TICs Analytical Method:E625PPrep Method: 09.19.14Date Prep: n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol 2,4,6-Trichlorophenol Phenanthrene Phenol Pyrene Parameter %RPD H Flag 30 30 30 30 30 30 30 30 RPD Limit 3 4 5 5 4 4 4 3 951294Seq Number: 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 Analysis Date Limits 10-230 50-110 44-142 14-76 37-144 54-120 5-112 23-152 LCSD %Rec 76 103 71 98 78 88 71 93 LCSD Result 38.2 51.6 35.6 48.8 38.8 43.8 35.5 46.3 LCS %Rec 78 99 68 93 74 84 74 90 39.2 49.4 33.9 46.4 37.2 42.1 37.1 45.0 Spike Amount 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 MB Result <1.36 <2.50 <1.43 <2.26 <1.64 <2.04 <1.76 <2.40 661823-1-BKSLCS Sample Id:661823-1-BSDLCSD Sample Id: ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L UnitsLCS Result 2-Fluorobiphenyl 2-Fluorophenol 2,4,6-Tribromophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-D14 Surrogate LCSD Flag 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 09.23.14 01:54 Analysis DateLimits 39-99 33-92 32-129 37-94 50-200 18-133 LCSD %Rec 76 68 92 77 66 93 LCS %Rec 72 62 88 73 65 89 MB %Rec 70 66 84 67 67 92 % % % % % % UnitsLCS Flag MB Flag Page 22 of 28 Final 1.000 Blank Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 661823-1-BLKLab Sample Id: WATERMatrix: 661823-1-BLK Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14:00Date Prep: BROTech: Anthracene Benzoic Acid Benzo(a)anthracene 1,3-Dichlorobenzene Benzo(a)pyrene 1,3-Dinitrobenzene 1,4-Dichlorobenzene 1-Methylnaphthalene + Benzo(b)fluoranthene 2,4-Dichlorophenol Benzo(k)fluoranthene Benzo(g,h,i)perylene 2,4-Dimethylphenol Benzyl alcohol 2,4-Dinitrophenol 2-Chlorophenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 1,2-Dichlorobenzene 4-Chlorophenyl Phenyl Ether Acenaphthene 3,3-Dichlorobenzidine Acenaphthylene 4,6-dinitro-2-methyl phenol bis(2-chloroethoxy) methane 1,2-Diphenylhydrazine bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate 2-Chloronaphthalene Butyl benzyl phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate 2-Methylnaphthalene di-n-Octyl Phthalate Parameter 2.01 2.21 1.90 2.11 1.80 20.1 1.61 1.40 1.97 1.78 2.71 1.97 1.63 1.23 7.11 1.83 2.12 2.18 3.09 1.83 1.35 1.43 3.88 1.48 1.40 1.25 4.76 1.78 1.24 1.20 1.29 1.82 2.09 1.83 1.64 1.90 1.97 2.08 1.19 1.38 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 10.0 20.0 10.0 10.0 10.0 50.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 20.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-12-7 65-85-0 56-55-3 541-73-1 50-32-8 99-65-0 106-46-7 90-12-0 205-99-2 120-83-2 207-08-9 191-24-2 105-67-9 100-51-6 51-28-5 95-57-8 101-55-3 59-50-7 106-47-8 95-50-1 7005-72-3 83-32-9 91-94-1 208-96-8 534-52-1 111-91-1 122-66-7 111-44-4 39638-32-9 117-81-7 91-58-7 85-68-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 91-57-6 117-84-0 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 951294Seq Number: MDLRL 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 Analysis Date Page 23 of 28 Final 1.000 Blank Summary 493612 Terraquest Environmental Consultants, P.C., Mebane, NC Parkers Stop & Shop 661823-1-BLKLab Sample Id: WATERMatrix: 661823-1-BLK Sample Id: SVOCs by EPA 625 + 10 TICs Analytical Method: VICAnalyst: E625PPrep Method: 09.19.14 14:00Date Prep: BROTech: 2-methylphenol Fluoranthene Fluorene 3&4-Methylphenol Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane 2-Nitrophenol Indeno(1,2,3-c,d)Pyrene 4-Nitrophenol Isophorone Naphthalene Nitrobenzene n-Nitrosodi-n-Propylamine n-Nitrosodiphenylamine 1,2,4-Trichlorobenzene Pentachlorophenol Phenanthrene 2,4,6-Trichlorophenol Phenol Pyrene unknown (TIC) unknown (TIC) unknown (TIC) unknown (TIC) Parameter 2.00 1.81 1.56 2.55 2.21 1.78 1.87 2.38 1.95 1.87 2.41 1.41 1.52 1.49 1.36 2.50 1.43 2.26 2.04 1.64 1.76 2.40 Result U U U U U U U U U U U U U U U U U U U U U U JN JN JN JN 10.0 10.0 10.0 20.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 Flag ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 95-48-7 206-44-0 86-73-7 15831-10-4 118-74-1 87-68-3 77-47-4 67-72-1 88-75-5 193-39-5 100-02-7 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 120-82-1 87-86-5 85-01-8 88-06-2 108-95-2 129-00-0 TIC TIC TIC TIC U U U U U U U U U U U U U U U U U U U U U U 4.03 7.99 5.56 4.86 951294Seq Number: MDLRL 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 09.23.14 01:25 Analysis Date Page 24 of 28 Final 1.000 Page 25 of 28 Final 1.000 Page 26 of 28 Final 1.000 Page 27 of 28 Final 1.000 Prelogin/Nonconformance Report- Sample Log-In XENCO Laboratories 493612Work Order #: 09/19/2014 10:05:00 AMDate/ Time Received: Terraquest Environmental Consultants, PClient: Sample Receipt Checklist Checklist completed by: Date: Checklist reviewed by:Date: Mike Kimmel 09/20/2014 09/20/2014 #2 *Shipping container in good condition? #3 *Samples received on ice? #4 *Custody Seals intact on shipping container/ cooler? #5 Custody Seals intact on sample bottles? #6 *Custody Seals Signed and dated? #7 *Chain of Custody present? #8 Sample instructions complete on Chain of Custody? #9 Any missing/extra samples? #10 Chain of Custody signed when relinquished/ received? #11 Chain of Custody agrees with sample label(s)? #12 Container label(s) legible and intact? #13 Sample matrix/ properties agree with Chain of Custody? #14 Samples in proper container/ bottle? #15 Samples properly preserved? #16 Sample container(s) intact? #17 Sufficient sample amount for indicated test(s)? #18 All samples received within hold time? #19 Subcontract of sample(s)? #20 VOC samples have zero headspace (less than 1/4 inch bubble)? #21 <2 for all samples preserved with HNO3,HCL, H2SO4? #22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH? Yes Yes N/A N/A N/A Yes Yes No Yes Yes Yes Yes Yes Yes Yes Yes Yes No N/A N/A N/A #1 *Temperature of cooler(s)?1.3 Acceptable Temperature Range: 0 - 6 degC Air and Metal samples Acceptable Range: Ambient * Must be completed for after-hours delivery of samples prior to placing in the refrigerator Analyst: PH Device/Lot#: Comments Mike Kimmel Temperature Measuring device used : Page 28 of 28 Final 1.000 Analytical Report 495867 for Terraquest Environmental Consultants, P.C. Project Manager: Jonathan Grubbs Parker's Stop N Shop 06-NOV-14 03014 6017 Financial Dr., Norcross, GA 30071 Ph:(770) 449-8800 Fax:(770) 449-5477 Xenco-Houston (EPA Lab code: TX00122): Texas (T104704215-14-18), Arizona (AZ0765), Florida (E871002), Louisiana (03054) New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610) Xenco-Atlanta (EPA Lab Code: GA00046): Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135) Texas (T104704477), Louisiana (04176), USDA (P330-07-00105) Xenco-Lakeland: Florida (E84098) Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX) Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX) Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757) Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757) Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758) Collected By: Client Page 1 of 77 Final 1.000 Page 2 of 77 Final 1.000 Table of Contents Cover Page 1 Cover Letter 3 Sample ID Cross Reference 4 Explanation of Qualifiers (Flags) 5 Hits Summary 6 Certificate of Analysis (Detailed Report) 14 Summary of Quality control 39 Blank Summary 60 Chain of Custody 75 Sample Receipt Conformance Report 77 Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Project Manager: Jonathan Grubbs Terraquest Environmental Consultants, P.C. 100 E. Ruffin Street Mebane, NC 27302 Reference: XENCO Report No(s): 495867 Parker's Stop N Shop Project Address: NC Jonathan Grubbs: We are reporting to you the results of the analyses performed on the samples received under the project name referenced above and identified with the XENCO Report Number(s) 495867. All results being reported under this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using all other available quality control measures. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise arranged with you. The samples received, and described as recorded in Report No. 495867 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard practices, controlled substances under regulated protocols, etc). We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions concerning this report, please feel free to contact us at any time. Respectfully, 06-NOV-14 Client Services Manager Mike Kimmel Page 3 of 77 Final 1.000 Sample Cross Reference 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop Sample Id K1-SW1 (2.5) K1-SW2 (2.5) K1-SW3 (2.5) K1-SW4 (2.5) K1-BE1 (3.5) K3-SW1 (2.5) K3-SW2 (2.5) K3-SW3 (2.5) K3-SW4 (2.5) K3-BE1 (3.5) 10-22-14 13:12 10-22-14 13:04 10-22-14 13:06 10-22-14 13:08 10-22-14 13:02 10-22-14 11:28 10-22-14 11:30 10-22-14 11:32 10-22-14 11:34 10-22-14 11:25 Date Collected Lab Sample Id 495867-001 495867-002 495867-003 495867-004 495867-005 495867-006 495867-007 495867-008 495867-009 495867-010 Sample DepthMatrix S S S S S S S S S S Page 4 of 77 Final 1.000 Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America 4143 Greenbriar Dr, Stafford, TX 77477 9701 Harry Hines Blvd , Dallas, TX 75220 5332 Blackberry Drive, San Antonio TX 78238 2505 North Falkenburg Rd, Tampa, FL 33619 12600 West I-20 East, Odessa, TX 79765 6017 Financial Drive, Norcross, GA 30071 3725 E. Atlanta Ave, Phoenix, AZ 85040 Phone Fax (281) 240-4200 (281) 240-4280 (214) 902 0300 (214) 351-9139 (210) 509-3334 (210) 509-3335 (813) 620-2000 (813) 620-2033 (432) 563-1800 (432) 563-1713 (770) 449-8800 (770) 449-5477 (602) 437-0330 Recipient of the Prestigious Small Business Administration Award of Excellence in 1994. Certified and approved by numerous States and Agencies. A Small Business and Minority Status Company that delivers SERVICE and QUALITY Flagging Criteria X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD. B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination. D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference. Dilution factors are included in the final results. The result is from a diluted sample. E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated. F RPD exceeded lab control limits. J The target analyte was positively identified below the quantitation limit and above the detection limit. U Analyte was not detected. L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations. H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the Department Supervisor and QA Director. Data were determined to be valid for reporting. K Sample analyzed outside of recommended hold time. JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated numerical value may not be consistent with the amount actually present in the environmental sample. ** Surrogate recovered outside laboratory control limit. BRL Below Reporting Limit. RL Reporting Limit MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation DL Method Detection Limit NC Non-Calculable + NELAC certification not offered for this compound. * (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation Page 5 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 16.63 Date Received : % Moisture : 10.22.14 13.12 Date Collected : 495867-001Lab Sample Id : SoilMatrix : K1-SW1 (2.5)Sample Id : TPH-Diesel Range Organics by SW-846 8015C Analytical Method :SW3550Prep Method: 10.28.14 09.45 Date Prep: TPH-DRO (C10-C28) Parameter Result J Flag mg/kg Units 1 DilCas Number C10C28DRO 8.60 954095Seq Number Dry WeightBasis : 10.29.14 05.52 Analysis Date Page 6 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 14.36 Date Received : % Moisture : 10.22.14 13.04 Date Collected : 495867-002Lab Sample Id : SoilMatrix : K1-SW2 (2.5)Sample Id : TPH-Diesel Range Organics by SW-846 8015C Analytical Method :SW3550Prep Method: 10.28.14 09.45 Date Prep: TPH-DRO (C10-C28) Parameter Result J Flag mg/kg Units 1 DilCas Number C10C28DRO 4.94 954095Seq Number Dry WeightBasis : 10.29.14 06.29 Analysis Date Page 7 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 14.75 Date Received : % Moisture : 10.22.14 13.06 Date Collected : 495867-003Lab Sample Id : SoilMatrix : K1-SW3 (2.5)Sample Id : TPH-Diesel Range Organics by SW-846 8015C Analytical Method :SW3550Prep Method: 10.28.14 09.45 Date Prep: TPH-DRO (C10-C28) Parameter Result Flag mg/kg Units 1 DilCas Number C10C28DRO 54.5 954095Seq Number Dry WeightBasis : 10.29.14 07.05 Analysis Date Page 8 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 15.45 Date Received : % Moisture : 10.22.14 13.08 Date Collected : 495867-004Lab Sample Id : SoilMatrix : K1-SW4 (2.5)Sample Id : TPH-Diesel Range Organics by SW-846 8015C Analytical Method :SW3550Prep Method: 10.28.14 09.45 Date Prep: TPH-DRO (C10-C28) Parameter Result J Flag mg/kg Units 1 DilCas Number C10C28DRO 7.61 954095Seq Number Dry WeightBasis : 10.29.14 07.42 Analysis Date Page 9 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 20.56 Date Received : % Moisture : 10.22.14 13.02 Date Collected : 495867-005Lab Sample Id : SoilMatrix : K1-BE1 (3.5)Sample Id : VOCs by SW-846 8260B Analytical Method :SW5035Prep Method: 10.28.14 06.53 Date Prep: 1,2,4-Trimethylbenzene Acetone Naphthalene Parameter Result J Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number 95-63-6 67-64-1 91-20-3 0.00095 0.044 0.0015 954075Seq Number Dry WeightBasis : 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 Analysis Date Page 10 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 30.35 Date Received : % Moisture : 10.22.14 11.28 Date Collected : 495867-006Lab Sample Id : SoilMatrix : K3-SW1 (2.5)Sample Id : TPH-Diesel Range Organics by SW-846 8015C Analytical Method :SW3550Prep Method: 10.28.14 09.45 Date Prep: TPH-DRO (C10-C28) Parameter Result J Flag mg/kg Units 1 DilCas Number C10C28DRO 4.34 954095Seq Number Dry WeightBasis : 10.29.14 08.54 Analysis Date Page 11 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 14.85 Date Received : % Moisture : 10.22.14 11.25 Date Collected : 495867-010Lab Sample Id : SoilMatrix : K3-BE1 (3.5)Sample Id : MADEP VPH Analytical Method :SW5030BPrep Method: 10.30.14 03.58 Date Prep: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter Result Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C ALHYDRC9C HYDC9C10 3.92 2.67 1.29 954253Seq Number Dry WeightBasis : 10.30.14 09.03 10.30.14 09.03 10.30.14 09.03 Analysis Date Page 12 of 77 Final 1.000 Hits Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 14.85 Date Received : % Moisture : 10.22.14 11.25 Date Collected : 495867-010Lab Sample Id : SoilMatrix : K3-BE1 (3.5)Sample Id : VOCs by SW-846 8260B Analytical Method :SW5035Prep Method: 10.28.14 06.53 Date Prep: 1,2,4-Trimethylbenzene Acetone Naphthalene Parameter Result Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number 95-63-6 67-64-1 91-20-3 0.0020 0.051 0.0023 954075Seq Number Dry WeightBasis : 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 Analysis Date Page 13 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.12 Date Collected:495867-001Lab Sample Id: SoilMatrix: K1-SW1 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.28.14 08.35 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.06 1.3 Result Result J U 9.94 2.2 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 8.60 U 954095 954085 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 05.52 10.29.14 05.38 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 88 95 10.29.14 05.52 10.29.14 05.38 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 16.63 16.63 % Moisture: % Moisture: Page 14 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.04 Date Collected:495867-002Lab Sample Id: SoilMatrix: K1-SW2 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.28.14 08.35 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 2.99 1.3 Result Result J U 9.72 2.2 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 4.94 U 954095 954085 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 06.29 10.29.14 06.09 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 78 88 10.29.14 06.29 10.29.14 06.09 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 14.36 14.36 % Moisture: % Moisture: Page 15 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 11.03.14 09.30 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 23.0 11.5 11.5 Result U U U 23.0 11.5 11.5 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 U U U 954596Seq Number: RL Dry WeightBasis: MDL 11.05.14 00.41 11.04.14 23.33 11.04.14 23.33 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 73 69 77 11.04.14 23.33 11.05.14 00.41 11.05.14 00.41 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 14.75% Moisture: Page 16 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3550Prep Method: 11.04.14 10.00 Date Prep: BROTech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0690 0.0631 0.0616 0.0608 0.0717 0.0752 0.0495 0.0709 0.0627 0.0507 0.0709 0.0698 0.0596 0.0546 0.0522 0.0491 0.115 0.0569 0.0538 0.0678 0.0663 0.0557 0.0647 0.0740 0.0592 0.0479 0.0546 0.0663 0.0429 0.0577 0.0631 0.0573 0.0635 0.0643 0.0670 0.0616 0.0585 0.0468 0.0553 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.779 0.390 0.779 1.95 0.390 0.390 0.390 0.195 0.390 0.390 0.390 0.779 0.779 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.779 0.390 0.390 0.195 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954619Seq Number: RL Dry WeightBasis: MDL 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 Analysis Date 14.75% Moisture: Page 17 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3550Prep Method: 11.04.14 10.00 Date Prep: BROTech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0526 0.0631 0.0518 0.0756 0.0499 0.0627 0.0588 0.0717 0.0647 0.0507 0.0475 0.0651 0.0433 0.0670 0.0604 0.0709 0.0401 0.0624 0.0694 0.0557 0.0818 0.0705 0.0647 0.0546 0.0663 0.0740 Result U U U U U U U U U U U U U U U U U U U U U U U U U 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.390 0.779 0.390 0.390 0.390 0.390 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U U 954619Seq Number: RL Dry WeightBasis: MDL 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 61 69 80 79 84 67 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 11.04.14 19.12 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 14.75% Moisture: Page 18 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C MADEP VPH TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: CLAR JOL JOL Analyst: Analyst: Analyst: SW3550 SW5030B SW5030B Prep Method: Prep Method: Prep Method: 10.28.14 09.45 11.03.14 10.00 10.28.14 08.35 Date Prep: Date Prep: Date Prep: CLAR JOL JOL Tech: Tech: Tech: TPH-DRO (C10-C28) C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics TPH-GRO Parameter Parameter Parameter 2.99 0.000642 0.000642 0.000214 1.2 Result Result Result U U U U 9.73 0.000642 0.000642 0.000214 2.1 Flag Flag Flag mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units 1 50 50 50 50 Dil Dil Dil Cas Number Cas Number Cas Number C10C28DRO ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 8006-61-9 54.5 U U U U 954095 954490 954085 Seq Number: Seq Number: Seq Number: RL RL RL Dry Weight Dry Weight Dry Weight Basis: Basis: Basis: MDL MDL MDL 10.29.14 07.05 11.03.14 12.03 11.03.14 12.03 11.03.14 12.03 10.29.14 06.41 Analysis Date Analysis Date Analysis Date Surrogate Surrogate Surrogate 32-128 70-130 70-130 57-131 % Recovery % Recovery % Recovery Flag Flag Flag % % % % 94 105 105 91 10.29.14 07.05 11.03.14 12.03 11.03.14 12.03 10.29.14 06.41 Cas Number Cas Number Cas Number 84-15-1 615-59-8 615-59-8 615-59-8 Units Units Units Analysis Date Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene Limits Limits Limits 14.75 14.75 14.75 % Moisture: % Moisture: % Moisture: Page 19 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 11.03.14 07.49 Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00058 0.00092 0.00052 0.00062 0.00090 0.00042 0.00044 0.0013 0.00067 0.00056 0.00067 0.00100 0.00046 0.00072 0.00063 0.00077 0.00053 0.00053 0.00046 0.0018 0.00055 0.00087 0.00043 0.00062 0.0025 0.0053 0.00040 0.00066 0.00078 0.00039 0.00074 0.0019 0.00057 0.00045 0.00077 0.0019 0.00057 0.0018 0.00051 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.00077 0.0015 0.00077 0.00077 0.0015 0.00077 0.00077 0.0015 0.00077 0.00077 0.00077 0.0015 0.00077 0.00077 0.00077 0.00077 0.00077 0.00077 0.00077 0.0077 0.00077 0.0077 0.00077 0.00077 0.0077 0.0077 0.00077 0.00077 0.0015 0.00077 0.00077 0.0039 0.00077 0.00077 0.00077 0.0039 0.00077 0.0039 0.00077 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954513Seq Number: RL Dry WeightBasis: MDL 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 Analysis Date 14.75% Moisture: Page 20 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.06 Date Collected:495867-003Lab Sample Id: SoilMatrix: K1-SW3 (2.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 11.03.14 07.49 Date Prep: MWETech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00042 0.00091 0.022 0.00044 0.00098 0.00059 0.000933 0.00053 0.0017 0.0010 0.00068 0.00060 0.000553 0.00051 0.00057 0.00064 0.00080 0.00045 0.00060 0.00052 0.00055 0.0027 0.00056 0.0016 Result U U U U U U U U U U U U U U U U U U U U U U U U 0.00077 0.0015 0.039 0.00077 0.0015 0.00077 0.00154 0.0015 0.0039 0.0015 0.00077 0.00077 0.000772 0.00077 0.00077 0.00077 0.0015 0.00077 0.00077 0.00077 0.00077 0.0039 0.0039 0.0039 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U U 954513Seq Number: RL Dry WeightBasis: MDL 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 121 89 95 11.03.14 11.30 11.03.14 11.30 11.03.14 11.30 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 14.75% Moisture: Page 21 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.08 Date Collected:495867-004Lab Sample Id: SoilMatrix: K1-SW4 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.28.14 08.35 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.03 1.3 Result Result J U 9.86 2.3 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 7.61 U 954095 954085 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 07.42 10.29.14 07.13 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 75 91 10.29.14 07.42 10.29.14 07.13 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 15.45 15.45 % Moisture: % Moisture: Page 22 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 10.28.14 15.30 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 25.0 12.5 12.5 Result U U U 25.0 12.5 12.5 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 U U U 954194Seq Number: RL Dry WeightBasis: MDL 10.29.14 17.16 10.29.14 17.37 10.29.14 17.37 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 51 56 72 10.29.14 17.37 10.29.14 17.16 10.29.14 17.16 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 20.56% Moisture: Page 23 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17.00 Date Prep: 5458Tech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0741 0.0679 0.0662 0.0653 0.0771 0.0808 0.0532 0.0762 0.0674 0.0545 0.0762 0.0750 0.0641 0.0586 0.0561 0.0528 0.124 0.0612 0.0578 0.0729 0.0712 0.0599 0.0695 0.0796 0.0637 0.0515 0.0586 0.0712 0.0461 0.0620 0.0679 0.0616 0.0683 0.0691 0.0721 0.0662 0.0628 0.0503 0.0595 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.838 0.419 0.838 2.09 0.419 0.419 0.419 0.209 0.419 0.419 0.419 0.838 0.838 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.838 0.419 0.419 0.209 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: RL Dry WeightBasis: MDL 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 Analysis Date 20.56% Moisture: Page 24 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17.00 Date Prep: 5458Tech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0566 0.0679 0.0557 0.0813 0.0536 0.0674 0.0633 0.0771 0.0695 0.0545 0.0511 0.0700 0.0465 0.0721 0.0649 0.0762 0.0431 0.0670 0.0746 0.0599 0.0880 0.0758 0.0695 0.0586 0.0712 0.0796 Result U U U U U U U U U U U U U U U U U U U U U U U U U U 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.419 0.838 0.419 0.419 0.419 0.419 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: RL Dry WeightBasis: MDL 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 53 58 70 71 71 57 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 10.29.14 15.26 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 20.56% Moisture: Page 25 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 10.30.14 03.58 Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000698 0.000698 0.000233 Result U U U 0.000698 0.000698 0.000233 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 U U U 954253Seq Number: RL Dry WeightBasis: MDL 10.30.14 09.34 10.30.14 09.34 10.30.14 09.34 Analysis Date Surrogate 70-130 70-130 % Recovery Flag % % 106 101 10.30.14 09.34 10.30.14 09.34 Cas Number 615-59-8 615-59-8 Units Analysis Date 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Limits 20.56% Moisture: Page 26 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06.53 Date Prep: 4148Tech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00064 0.0010 0.00057 0.00069 0.00099 0.00046 0.00049 0.0014 0.00075 0.00062 0.00074 0.0011 0.00051 0.00079 0.00070 0.00085 0.00059 0.00058 0.00051 0.0019 0.00061 0.00097 0.00047 0.00068 0.0028 0.0059 0.00044 0.00073 0.00086 0.00043 0.00082 0.0021 0.00063 0.00050 0.00085 0.0021 0.00063 0.0020 0.00057 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.00086 0.0017 0.00086 0.00086 0.0017 0.00086 0.00086 0.0017 0.00086 0.00086 0.00086 0.0017 0.00086 0.00086 0.00086 0.00086 0.00086 0.00086 0.00086 0.0086 0.00086 0.0086 0.00086 0.00086 0.0086 0.0086 0.00086 0.00086 0.0017 0.00086 0.00086 0.0043 0.00086 0.00086 0.00086 0.0043 0.00086 0.0043 0.00086 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U 0.00095 U U U U U U U U U U U U U U U 0.044 U U U U U U U U U U U U U 954075Seq Number: RL Dry WeightBasis: MDL 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 Analysis Date 20.56% Moisture: Page 27 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 13.02 Date Collected:495867-005Lab Sample Id: SoilMatrix: K1-BE1 (3.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06.53 Date Prep: 4148Tech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00046 0.0010 0.024 0.00048 0.0011 0.00065 0.00103 0.00059 0.0019 0.0011 0.00075 0.00067 0.000612 0.00056 0.00063 0.00071 0.00089 0.00050 0.00067 0.00057 0.00060 0.0030 0.00062 0.0017 Result U U U U U U U U U J U U U U U U U U U U U U U U 0.00086 0.0017 0.043 0.00086 0.0017 0.00086 0.00171 0.0017 0.0043 0.0017 0.00086 0.00086 0.000855 0.00086 0.00086 0.00086 0.0017 0.00086 0.00086 0.00086 0.00086 0.0043 0.0043 0.0043 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U 0.0015 U U U U U U U U U U U U U U 954075Seq Number: RL Dry WeightBasis: MDL 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 118 93 95 10.28.14 11.54 10.28.14 11.54 10.28.14 11.54 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 20.56% Moisture: Page 28 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.28 Date Collected:495867-006Lab Sample Id: SoilMatrix: K3-SW1 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.28.14 08.35 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.67 1.9 Result Result J U 11.9 3.2 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 4.34 U 954095 954085 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 08.54 10.29.14 07.45 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 78 95 10.29.14 08.54 10.29.14 07.45 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 30.35 30.35 % Moisture: % Moisture: Page 29 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.30 Date Collected:495867-007Lab Sample Id: SoilMatrix: K3-SW2 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.31.14 12.01 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.56 1.9 Result Result U U 11.6 3.2 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 U U 954095 954374 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 09.29 10.31.14 14.09 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 72 97 10.29.14 09.29 10.31.14 14.09 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 28.27 28.27 % Moisture: % Moisture: Page 30 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.32 Date Collected:495867-008Lab Sample Id: SoilMatrix: K3-SW3 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.31.14 12.01 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.55 1.8 Result Result U U 11.5 3.0 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 U U 954095 954374 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 03.31 10.31.14 14.41 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 69 97 10.29.14 03.31 10.31.14 14.41 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 28.05 28.05 % Moisture: % Moisture: Page 31 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.34 Date Collected:495867-009Lab Sample Id: SoilMatrix: K3-SW4 (2.5)Sample Id: TPH-Diesel Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: CLAR JOL Analyst: Analyst: SW3550 SW5030B Prep Method: Prep Method: 10.28.14 09.45 10.31.14 12.01 Date Prep: Date Prep: CLAR JOL Tech: Tech: TPH-DRO (C10-C28) TPH-GRO Parameter Parameter 3.71 1.8 Result Result U U 12.0 3.1 Flag Flag mg/kg mg/kg Units Units 1 50 Dil Dil Cas Number Cas Number C10C28DRO 8006-61-9 U U 954095 954374 Seq Number: Seq Number: RL RL Dry Weight Dry Weight Basis: Basis: MDL MDL 10.29.14 10.04 10.31.14 15.13 Analysis Date Analysis Date Surrogate Surrogate 32-128 57-131 % Recovery % Recovery Flag Flag % % 75 92 10.29.14 10.04 10.31.14 15.13 Cas Number Cas Number 84-15-1 615-59-8 Units Units Analysis Date Analysis Date o-Terphenyl 2,5-Dibromotoluene Limits Limits 30.87 30.87 % Moisture: % Moisture: Page 32 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 10.28.14 15.30 Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 23.2 11.6 11.6 Result U U U 23.2 11.6 11.6 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C18 ALHYDRC19C3 U U U 954194Seq Number: RL Dry WeightBasis: MDL 10.29.14 19.04 10.29.14 19.15 10.29.14 19.15 Analysis Date Surrogate 40-140 40-140 40-140 % Recovery Flag % % % 47 45 71 10.29.14 19.15 10.29.14 19.04 10.29.14 19.04 Cas Number 3386-33-2 84-15-1 321-60-8 Units Analysis Date 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Limits 14.85% Moisture: Page 33 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17.00 Date Prep: 5458Tech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether Parameter 0.0687 0.0629 0.0613 0.0605 0.0714 0.0749 0.0493 0.0706 0.0625 0.0505 0.0706 0.0695 0.0594 0.0543 0.0520 0.0489 0.115 0.0567 0.0536 0.0675 0.0660 0.0555 0.0644 0.0737 0.0590 0.0477 0.0543 0.0660 0.0427 0.0574 0.0629 0.0571 0.0633 0.0640 0.0668 0.0613 0.0582 0.0466 0.0551 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.776 0.388 0.776 1.94 0.388 0.388 0.388 0.194 0.388 0.388 0.388 0.776 0.776 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.776 0.388 0.388 0.194 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: RL Dry WeightBasis: MDL 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 Analysis Date 14.85% Moisture: Page 34 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17.00 Date Prep: 5458Tech: bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0524 0.0629 0.0516 0.0753 0.0497 0.0625 0.0586 0.0714 0.0644 0.0505 0.0473 0.0648 0.0431 0.0668 0.0602 0.0706 0.0400 0.0621 0.0691 0.0555 0.0815 0.0702 0.0644 0.0543 0.0660 0.0737 Result U U U U U U U U U U U U U U U U U U U U U U U U U U 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.388 0.776 0.388 0.388 0.388 0.388 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 39638-32-9 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: RL Dry WeightBasis: MDL 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 Analysis Date Surrogate 25-121 23-120 30-115 19-122 18-137 15-110 % Recovery Flag % % % % % % 58 63 74 77 72 59 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 10.29.14 15.54 Cas Number 367-12-4 4165-60-0 321-60-8 118-79-6 1718-51-0 4165-62-2 Units Analysis Date 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Limits 14.85% Moisture: Page 35 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 10.30.14 03.58 Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000831 0.000831 0.000277 Result 0.000831 0.000831 0.000277 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C12 HYDC9C10 3.92 2.67 1.29 954253Seq Number: RL Dry WeightBasis: MDL 10.30.14 09.03 10.30.14 09.03 10.30.14 09.03 Analysis Date Surrogate 70-130 70-130 % Recovery Flag % % 105 102 10.30.14 09.03 10.30.14 09.03 Cas Number 615-59-8 615-59-8 Units Analysis Date 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Limits 14.85% Moisture: Page 36 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06.53 Date Prep: 4148Tech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene Parameter 0.00081 0.0013 0.00072 0.00086 0.0012 0.00058 0.00061 0.0018 0.00093 0.00077 0.00092 0.0014 0.00064 0.00099 0.00087 0.0011 0.00074 0.00073 0.00064 0.0024 0.00076 0.0012 0.00059 0.00086 0.0035 0.0074 0.00055 0.00091 0.0011 0.00054 0.0010 0.0026 0.00079 0.00062 0.0011 0.0026 0.00079 0.0025 0.00071 Result U U U U U U U U U U UX U U U UX U UX U U U U U U U U U U U U U U U U U U U U 0.0011 0.0021 0.0011 0.0011 0.0021 0.0011 0.0011 0.0021 0.0011 0.0011 0.0011 0.0021 0.0011 0.0011 0.0011 0.0011 0.0011 0.0011 0.0011 0.011 0.0011 0.011 0.0011 0.0011 0.011 0.011 0.0011 0.0011 0.0021 0.0011 0.0011 0.0053 0.0011 0.0011 0.0011 0.0053 0.0011 0.0053 0.0011 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 U U U U U U U U U 0.0020 U U U U U U U U U U U U U U U 0.051 U U U U U U U U U U U U U 954075Seq Number: RL Dry WeightBasis: MDL 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 Analysis Date 14.85% Moisture: Page 37 of 77 Final 1.000 Certificate of Analytical Results 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 10.24.14 10.20 Date Received: 10.22.14 11.25 Date Collected:495867-010Lab Sample Id: SoilMatrix: K3-BE1 (3.5)Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06.53 Date Prep: 4148Tech: cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.00058 0.0013 0.030 0.00060 0.0014 0.00081 0.00129 0.00074 0.0023 0.0014 0.00094 0.00084 0.000766 0.00070 0.00079 0.00089 0.0011 0.00063 0.00083 0.00072 0.00076 0.0038 0.00077 0.0021 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0011 0.0021 0.053 0.0011 0.0021 0.0011 0.00214 0.0021 0.0053 0.0021 0.0011 0.0011 0.00107 0.0011 0.0011 0.0011 0.0021 0.0011 0.0011 0.0011 0.0011 0.0053 0.0053 0.0053 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 10061-01-5 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U 0.0023 U U U U U U U U U U U U U U 954075Seq Number: RL Dry WeightBasis: MDL 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 Analysis Date Surrogate 50-150 57-158 50-150 % Recovery Flag % % % 119 93 98 10.28.14 12.19 10.28.14 12.19 10.28.14 12.19 Cas Number 17060-07-0 460-00-4 2037-26-5 Units Analysis Date 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Limits 14.85% Moisture: Page 38 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495860-001 495861-005 495861-016 495867-009 663617-1-BLK Parent Sample Id: Parent Sample Id: Parent Sample Id: Parent Sample Id: MB Sample Id: Soil Soil Soil Soil Solid Matrix: Matrix: Matrix: Matrix: Matrix: Percent Moisture Percent Moisture Percent Moisture Percent Moisture MADEP EPH Analytical Method: Analytical Method: Analytical Method: Analytical Method: Analytical Method:SW3545Prep Method: 10.28.14Date Prep: Percent Moisture Percent Moisture Percent Moisture Percent Moisture C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter Parameter Parameter Parameter Parameter %RPD %RPD %RPD %RPD %RPD Flag Flag Flag Flag Flag 20 20 20 20 40 40 40 RPD Limit RPD Limit RPD Limit RPD Limit RPD Limit 2 1 0 2 7 3 1 953842 953842 953842 953842 954194 Seq Number: Seq Number: Seq Number: Seq Number: Seq Number: 10.24.14 09:00 10.24.14 09:00 10.24.14 09:00 10.24.14 09:00 10.29.14 14:50 10.29.14 15:27 10.29.14 15:27 Analysis Date Analysis Date Analysis Date Analysis Date Analysis Date Limits 40-140 40-140 40-140 LCSD %Rec 79 59 74 LCSD Result 135 35.1 58.8 LCS %Rec 85 57 73 23.7 30.2 35.9 30.4 145 34.1 58.2 Spike Amount 170 60.0 80.0 Parent Result Parent Result Parent Result Parent Result MB Result 23.3 29.9 35.8 30.9 <20.0 <10.0 <10.0 495860-001 D 495861-005 D 495861-016 D 495867-009 D 663617-1-BKS MD Sample Id: MD Sample Id: MD Sample Id: MD Sample Id: LCS Sample Id:663617-1-BSDLCSD Sample Id: % % % % mg/kg mg/kg mg/kg Units Units Units Units Units MD Result MD Result MD Result MD Result LCS Result 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Surrogate LCSD Flag 10.29.14 15:27 10.29.14 14:50 10.29.14 14:50 Analysis DateLimits 40-140 40-140 40-140 LCSD %Rec 57 79 95 LCS %Rec 58 79 98 MB %Rec 68 61 48 % % % UnitsLCS Flag MB Flag Page 39 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663842-1-BLK 495867-005 496360-001 MB Sample Id: Parent Sample Id: Parent Sample Id: Solid Soil Soil Matrix: Matrix: Matrix: MADEP EPH MADEP EPH MADEP EPH Analytical Method: Analytical Method: Analytical Method: SW3545 SW3545 SW3545 Prep Method: Prep Method: Prep Method: 11.03.14 10.28.14 11.03.14 Date Prep: Date Prep: Date Prep: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter Parameter Parameter %RPD %RPD %RPD Flag Flag Flag 40 40 40 40 40 40 40 40 40 RPD Limit RPD Limit RPD Limit 1 2 9 10 21 9 0 6 18 954596 954194 954596 Seq Number: Seq Number: Seq Number: 11.04.14 17:52 11.04.14 17:10 11.04.14 17:10 10.29.14 17:52 10.29.14 18:10 10.29.14 18:10 11.04.14 19:34 11.04.14 18:46 11.04.14 18:46 Analysis Date Analysis Date Analysis Date Limits Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 40-140 40-140 40-140 LCSD %Rec MSD %Rec MSD %Rec 114 66 80 67 49 77 89 62 110 LCSD Result MSD Result MSD Result 194 39.8 63.7 142 36.6 76.6 190 46.8 110 LCS %Rec MS %Rec MS %Rec 113 68 87 60 60 83 90 59 92 192 40.8 69.5 128 45.1 83.7 190 44.0 91.9 Spike Amount Spike Amount Spike Amount 170 60.0 80.0 214 75.5 101 212 74.8 99.8 MB Result Parent Result Parent Result <20.0 <10.0 <10.0 <25.2 <12.6 <12.6 <24.9 <12.5 <12.5 663842-1-BKS 495867-005 S 496360-001 S LCS Sample Id: MS Sample Id: MS Sample Id: 663842-1-BSD 495867-005 SD 496360-001 SD LCSD Sample Id: MSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units LCS Result MS Result MS Result 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl 1-Chlorooctadecane o-Terphenyl 2-Fluorobiphenyl Surrogate Surrogate Surrogate LCSD Flag MSD Flag MSD Flag 11.04.14 17:10 11.04.14 17:52 11.04.14 17:52 10.29.14 18:10 10.29.14 17:52 10.29.14 17:52 11.04.14 18:46 11.04.14 19:34 11.04.14 19:34 Analysis Date Analysis Date Analysis Date Limits Limits Limits 40-140 40-140 40-140 40-140 40-140 40-140 40-140 40-140 40-140 LCSD %Rec MSD %Rec MSD %Rec 85 108 91 50 68 80 96 87 91 LCS %Rec MS %Rec MS %Rec 94 109 96 63 59 74 87 90 91 MB %Rec 80 88 73 % % % % % % % % % Units Units Units LCS Flag MS Flag MS Flag MB Flag Page 40 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663619-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 10.28.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 8 9 7 9 6 2 3 6 1 2 4 7 3 4 1 5 5 3 4 3 3 4 5 4 13 3 4 11 3 1 3 2 3 1 3 4 9 6 0 1 3 4 2 3 0 1 4 3 0 5 13 6 954326Seq Number: 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 Analysis Date Limits 35-129 38-122 38-120 37-121 40-135 39-139 36-135 38-133 48-131 42-136 32-138 38-125 36-126 37-128 30-133 33-142 38-126 41-135 30-146 37-140 40-134 34-124 41-131 46-132 21-152 37-131 39-129 33-117 39-139 44-135 43-153 40-153 40-153 33-156 43-145 30-129 33-127 25-124 46-145 42-135 41-155 39-132 45-131 43-132 43-142 34-166 41-138 41-131 36-142 35-129 16-106 36-121 LCSD %Rec 69 65 63 63 72 68 66 67 87 79 69 62 70 62 65 74 65 80 86 75 72 76 81 74 68 70 77 80 78 78 112 125 102 80 78 65 60 66 86 74 106 68 75 74 75 90 78 72 77 75 60 68 LCSD Result 1.16 1.08 1.05 1.05 1.21 1.14 1.10 1.12 1.45 1.32 1.16 1.04 1.17 1.03 1.08 1.24 1.09 1.33 1.44 1.26 1.20 1.27 1.35 1.24 1.13 1.17 1.28 1.33 1.30 1.30 1.87 2.09 1.70 1.34 1.31 1.08 1.01 1.11 1.43 1.23 1.77 1.14 1.25 1.24 1.26 1.50 1.31 1.21 1.29 1.26 0.997 1.14 LCS %Rec 64 59 59 58 68 67 64 63 86 77 66 58 72 59 64 71 62 77 83 73 69 73 77 71 77 68 74 71 75 77 109 122 99 81 76 62 55 63 86 73 103 66 73 72 75 90 75 70 77 72 53 64 1.07 0.983 0.979 0.961 1.14 1.12 1.07 1.06 1.44 1.29 1.11 0.969 1.20 0.987 1.07 1.18 1.04 1.29 1.38 1.22 1.16 1.22 1.29 1.19 1.29 1.14 1.23 1.19 1.26 1.29 1.82 2.04 1.65 1.36 1.27 1.04 0.923 1.05 1.43 1.22 1.72 1.10 1.22 1.20 1.26 1.51 1.26 1.17 1.29 1.20 0.877 1.07 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0590 <0.0540 <0.0527 <0.0520 <0.0613 <0.0643 <0.0423 <0.0607 <0.0537 <0.0433 <0.0607 <0.0597 <0.0510 <0.0467 <0.0447 <0.0420 <0.0987 <0.0460 <0.0580 <0.0567 <0.0477 <0.0553 <0.0633 <0.0507 <0.0410 <0.0467 <0.0567 <0.0367 <0.0493 <0.0540 <0.0490 <0.0543 <0.0550 <0.0573 <0.0500 <0.0400 <0.0473 <0.0450 <0.0540 <0.0443 <0.0647 <0.0427 <0.0537 <0.0503 <0.0613 <0.0553 <0.0433 <0.0407 <0.0557 <0.0370 <0.0573 <0.0517 663619-1-BKSLCS Sample Id:663619-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 41 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663619-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 10.28.14Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 3 3 5 5 4 3 4 3 6 2 8 954326Seq Number: 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 Analysis Date Limits 39-154 36-128 35-128 32-129 34-129 27-155 14-148 37-139 34-127 42-138 30-113 LCSD %Rec 105 66 64 67 69 83 54 71 60 72 56 LCSD Result 1.75 1.11 1.07 1.12 1.16 1.39 0.899 1.18 0.998 1.21 0.939 LCS %Rec 102 65 61 64 67 81 52 68 56 71 52 1.70 1.08 1.02 1.07 1.12 1.35 0.863 1.14 0.940 1.19 0.870 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0607 <0.0343 <0.0533 <0.0593 <0.0477 <0.0700 <0.0603 <0.0553 <0.0467 <0.0567 <0.0633 663619-1-BKSLCS Sample Id:663619-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Surrogate LCSD Flag 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 10.29.14 13:33 Analysis Date Limits 25-121 23-120 30-115 19-122 18-137 15-110 LCSD %Rec 65 67 75 87 72 66 LCS %Rec 60 66 72 84 69 63 MB %Rec 64 69 79 82 76 63 % % % % % % UnitsLCS Flag MB Flag Page 42 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663909-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3550Prep Method: 11.04.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 2 2 0 1 6 4 1 1 5 1 2 0 2 0 2 3 2 1 2 1 2 1 2 6 9 1 0 1 1 1 2 2 1 7 4 4 1 1 5 0 1 1 6 1 1 5 7 4 1 1 6 1 954619Seq Number: 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 Analysis Date Limits 35-129 38-122 38-120 37-121 40-135 39-139 36-135 38-133 48-131 42-136 32-138 38-125 36-126 37-128 30-133 33-142 38-126 41-135 30-146 37-140 40-134 34-124 41-131 46-132 21-152 37-131 39-129 33-117 39-139 44-135 43-153 40-153 40-153 33-156 43-145 30-129 33-127 25-124 46-145 42-135 41-155 39-132 45-131 43-132 43-142 34-166 41-138 41-131 36-142 35-129 16-106 36-121 LCSD %Rec 77 66 65 64 84 85 78 80 101 90 83 64 86 63 78 77 68 89 82 85 83 86 98 80 65 81 89 78 85 92 94 102 85 79 93 73 63 68 98 84 87 80 94 87 83 102 85 89 87 87 57 69 LCSD Result 1.29 1.10 1.09 1.07 1.41 1.42 1.30 1.33 1.69 1.51 1.38 1.07 1.43 1.06 1.30 1.28 1.13 1.48 1.37 1.42 1.38 1.43 1.63 1.34 1.08 1.36 1.48 1.31 1.42 1.53 1.57 1.71 1.42 1.32 1.56 1.22 1.06 1.13 1.64 1.40 1.46 1.34 1.57 1.46 1.38 1.71 1.42 1.48 1.45 1.45 0.952 1.16 LCS %Rec 78 67 65 65 80 81 77 81 96 91 81 64 84 63 76 74 66 87 80 86 81 86 95 75 59 81 89 79 86 91 92 104 86 74 90 76 64 68 93 84 89 80 89 86 84 98 91 85 86 86 54 70 1.31 1.12 1.09 1.08 1.33 1.36 1.29 1.35 1.61 1.52 1.35 1.07 1.40 1.06 1.27 1.24 1.11 1.46 1.34 1.44 1.35 1.44 1.59 1.26 0.989 1.35 1.48 1.32 1.43 1.52 1.54 1.74 1.43 1.23 1.50 1.27 1.07 1.14 1.56 1.40 1.48 1.33 1.48 1.44 1.40 1.63 1.52 1.42 1.44 1.43 0.899 1.17 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0590 <0.0540 <0.0527 <0.0520 <0.0613 <0.0643 <0.0423 <0.0607 <0.0537 <0.0433 <0.0607 <0.0597 <0.0510 <0.0467 <0.0447 <0.0420 <0.0987 <0.0460 <0.0580 <0.0567 <0.0477 <0.0553 <0.0633 <0.0507 <0.0410 <0.0467 <0.0567 <0.0367 <0.0493 <0.0540 <0.0490 <0.0543 <0.0550 <0.0573 <0.0500 <0.0400 <0.0473 <0.0450 <0.0540 <0.0443 <0.0647 <0.0427 <0.0537 <0.0503 <0.0613 <0.0553 <0.0433 <0.0407 <0.0557 <0.0370 <0.0573 <0.0517 663909-1-BKSLCS Sample Id:663909-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 43 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663909-1-BLKMB Sample Id: SolidMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3550Prep Method: 11.04.14Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 1 1 1 0 1 3 6 2 1 8 2 954619Seq Number: 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 Analysis Date Limits 39-154 36-128 35-128 32-129 34-129 27-155 14-148 37-139 34-127 42-138 30-113 LCSD %Rec 86 75 72 74 74 93 72 78 62 89 66 LCSD Result 1.44 1.26 1.20 1.24 1.23 1.56 1.20 1.30 1.04 1.48 1.10 LCS %Rec 87 75 72 74 74 96 68 79 63 82 67 1.46 1.25 1.21 1.24 1.24 1.60 1.13 1.32 1.05 1.37 1.12 Spike Amount 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 1.67 MB Result <0.0607 <0.0343 <0.0533 <0.0593 <0.0477 <0.0700 <0.0603 <0.0553 <0.0467 <0.0567 <0.0633 663909-1-BKSLCS Sample Id:663909-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Surrogate LCSD Flag 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 11.04.14 13:10 Analysis Date Limits 25-121 23-120 30-115 19-122 18-137 15-110 LCSD %Rec 63 78 87 95 84 69 LCS %Rec 62 77 85 94 75 71 MB %Rec 63 73 81 84 82 64 % % % % % % UnitsLCS Flag MB Flag Page 44 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-010Parent Sample Id: SoilMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 10.28.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD X F Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 19 18 14 20 14 14 18 17 10 13 15 20 12 14 12 18 15 10 16 13 16 14 11 13 9 14 13 16 15 14 16 48 19 5 15 15 20 18 18 15 17 11 11 12 16 20 17 12 14 15 16 20 954326Seq Number: 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 Analysis Date Limits 31-100 27-97 25-96 27-94 33-110 35-111 33-103 28-109 35-122 35-119 32-108 25-102 22-104 27-104 20-128 30-104 30-111 22-117 3-130 38-115 26-116 4-104 34-114 28-117 12-137 31-111 36-122 20-120 33-118 31-136 44-105 29-120 35-126 37-123 35-122 31-106 24-103 32-103 32-129 34-122 36-124 31-107 34-118 36-115 37-121 35-126 15-135 31-117 38-116 30-98 12-194 27-98 MSD %Rec 61 54 55 53 67 66 62 59 85 75 65 53 64 56 63 66 58 76 77 72 65 69 76 69 79 66 72 66 74 76 106 117 95 81 73 59 52 57 80 70 98 65 73 70 73 85 77 70 73 68 46 57 MSD Result 1.18 1.06 1.07 1.03 1.31 1.29 1.20 1.16 1.66 1.47 1.27 1.03 1.25 1.09 1.22 1.28 1.13 1.49 1.51 1.40 1.27 1.35 1.49 1.35 1.55 1.29 1.41 1.28 1.44 1.48 2.06 2.29 1.86 1.57 1.43 1.15 1.01 1.12 1.56 1.36 1.91 1.27 1.42 1.37 1.43 1.66 1.51 1.37 1.43 1.32 0.889 1.11 MS %Rec 73 65 63 64 77 76 73 70 93 86 75 64 72 64 70 79 67 84 90 81 76 79 85 78 72 76 82 77 85 87 123 72 114 76 85 68 63 68 95 81 116 72 81 79 86 104 91 79 84 79 53 69 1.43 1.27 1.23 1.26 1.50 1.49 1.44 1.37 1.83 1.68 1.47 1.26 1.41 1.25 1.37 1.54 1.31 1.64 1.77 1.59 1.49 1.55 1.67 1.53 1.42 1.48 1.61 1.51 1.67 1.70 2.42 1.41 2.24 1.49 1.67 1.34 1.24 1.34 1.87 1.58 2.27 1.42 1.58 1.54 1.68 2.03 1.79 1.54 1.64 1.54 1.04 1.36 Spike Amount 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 Parent Result <0.0693 <0.0634 <0.0618 <0.0610 <0.0720 <0.0755 <0.0497 <0.0712 <0.0630 <0.0509 <0.0712 <0.0700 <0.0599 <0.0548 <0.0524 <0.0493 <0.116 <0.0540 <0.0681 <0.0665 <0.0560 <0.0650 <0.0744 <0.0595 <0.0481 <0.0548 <0.0665 <0.0430 <0.0579 <0.0634 <0.0575 <0.0638 <0.0646 <0.0673 <0.0587 <0.0470 <0.0556 <0.0528 <0.0634 <0.0520 <0.0759 <0.0501 <0.0630 <0.0591 <0.0720 <0.0650 <0.0509 <0.0477 <0.0654 <0.0434 <0.0673 <0.0607 495867-010 SMS Sample Id:495867-010 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 45 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-010Parent Sample Id: SoilMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3545Prep Method: 10.28.14Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 16 13 17 20 14 15 20 15 19 13 21 954326Seq Number: 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 Analysis Date Limits 30-129 11-139 31-100 27-106 26-122 38-127 14-128 34-115 23-104 33-112 1-106 MSD %Rec 97 62 58 58 63 78 55 69 53 69 44 MSD Result 1.89 1.20 1.13 1.14 1.22 1.52 1.08 1.34 1.03 1.34 0.861 MS %Rec 113 70 68 71 71 90 67 79 63 78 54 2.21 1.37 1.34 1.39 1.40 1.76 1.32 1.55 1.24 1.52 1.06 Spike Amount 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 1.96 Parent Result <0.0712 <0.0403 <0.0626 <0.0697 <0.0560 <0.0822 <0.0708 <0.0650 <0.0548 <0.0665 <0.0744 495867-010 SMS Sample Id:495867-010 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 Surrogate MSD Flag 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 10.29.14 16:22 Analysis Date Limits 25-121 23-120 30-115 19-122 18-137 15-110 MSD %Rec 48 56 67 75 62 56 MS %Rec 60 71 77 90 72 67 % % % % % % UnitsMS Flag Page 46 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 496360-001Parent Sample Id: SoilMatrix: SVOCs by SW-846 8270DAnalytical Method:SW3550Prep Method: 11.04.14Date Prep: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Parameter %RPD Flag 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 RPD Limit 1 3 2 4 1 5 0 1 2 1 2 1 3 0 1 10 3 3 16 1 1 1 2 4 10 0 1 0 1 2 3 3 1 9 2 1 1 5 4 2 2 2 1 1 1 3 0 2 1 2 10 2 954619Seq Number: 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 Analysis Date Limits 31-100 27-97 25-96 27-94 33-110 35-111 33-103 28-109 35-122 35-119 32-108 25-102 22-104 27-104 20-128 30-104 30-111 22-117 3-130 38-115 26-116 4-104 34-114 28-117 12-137 31-111 36-122 20-120 33-118 31-136 44-105 29-120 35-126 37-123 35-122 31-106 24-103 32-103 32-129 34-122 36-124 31-107 34-118 36-115 37-121 35-126 15-135 31-117 38-116 30-98 12-194 27-98 MSD %Rec 66 55 54 54 68 65 63 67 85 78 67 54 75 53 65 61 56 75 82 72 69 72 78 67 58 68 73 63 73 80 81 89 74 75 89 64 54 57 88 73 76 66 79 75 76 90 75 71 73 73 48 58 MSD Result 1.37 1.15 1.12 1.12 1.43 1.36 1.31 1.40 1.78 1.63 1.40 1.12 1.57 1.11 1.36 1.27 1.16 1.56 1.72 1.51 1.44 1.50 1.62 1.39 1.21 1.42 1.53 1.32 1.52 1.67 1.69 1.87 1.54 1.57 1.85 1.33 1.12 1.19 1.84 1.53 1.59 1.38 1.66 1.56 1.58 1.88 1.57 1.49 1.52 1.53 1.01 1.22 MS %Rec 66 56 54 55 69 68 62 66 83 79 68 54 73 53 64 67 57 72 70 72 68 70 79 63 52 68 74 63 73 78 78 87 73 69 86 64 54 60 84 71 74 67 78 75 75 87 75 72 72 71 44 60 1.39 1.18 1.14 1.16 1.45 1.43 1.31 1.39 1.75 1.65 1.43 1.13 1.53 1.11 1.34 1.41 1.20 1.51 1.46 1.52 1.43 1.48 1.65 1.33 1.10 1.42 1.55 1.32 1.54 1.63 1.64 1.82 1.53 1.44 1.81 1.34 1.13 1.25 1.77 1.50 1.56 1.41 1.64 1.58 1.57 1.83 1.57 1.52 1.51 1.50 0.915 1.25 Spike Amount 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 Parent Result <0.0742 <0.0679 <0.0663 <0.0654 <0.0772 <0.0809 <0.0533 <0.0763 <0.0675 <0.0545 <0.0763 <0.0751 <0.0642 <0.0587 <0.0562 <0.0528 <0.124 <0.0579 <0.0730 <0.0713 <0.0600 <0.0696 <0.0797 <0.0637 <0.0516 <0.0587 <0.0713 <0.0461 <0.0621 <0.0679 <0.0616 <0.0684 <0.0692 <0.0721 <0.0629 <0.0503 <0.0595 <0.0566 <0.0679 <0.0558 <0.0814 <0.0537 <0.0675 <0.0633 <0.0772 <0.0696 <0.0545 <0.0512 <0.0700 <0.0465 <0.0721 <0.0650 496360-001 SMS Sample Id:496360-001 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 47 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 496360-001 663568-1-BLK 495867-008 Parent Sample Id: MB Sample Id: Parent Sample Id: Soil Solid Soil Matrix: Matrix: Matrix: SVOCs by SW-846 8270D TPH-Diesel Range Organics by SW-846 8015C TPH-Diesel Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: SW3550 SW3550 SW3550 Prep Method: Prep Method: Prep Method: 11.04.14 10.28.14 10.28.14 Date Prep: Date Prep: Date Prep: Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine TPH-DRO (C10-C28) TPH-DRO (C10-C28) Parameter Parameter Parameter %RPD %RPD %RPD Flag Flag Flag 30 30 30 30 30 30 30 30 30 30 30 20 20 RPD Limit RPD Limit RPD Limit 1 3 2 1 1 0 1 1 3 3 5 2 10 954619 954095 954095 Seq Number: Seq Number: Seq Number: 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 10.28.14 22:57 10.29.14 04:06 Analysis Date Analysis Date Analysis Date Limits Limits Limits 30-129 11-139 31-100 27-106 26-122 38-127 14-128 34-115 23-104 33-112 1-106 32-119 32-119 MSD %Rec LCSD %Rec MSD %Rec 75 65 61 63 62 81 68 68 52 75 37 105 101 MSD Result LCSD Result MSD Result 1.57 1.35 1.27 1.31 1.29 1.69 1.43 1.43 1.08 1.57 0.768 35.0 46.5 MS %Rec LCS %Rec MS %Rec 74 62 62 63 62 80 67 68 53 73 38 108 91 1.55 1.31 1.30 1.32 1.30 1.69 1.41 1.42 1.11 1.53 0.806 35.8 41.9 Spike Amount Spike Amount Spike Amount 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 2.10 33.3 46.1 Parent Result MB Result Parent Result <0.0763 <0.0432 <0.0671 <0.0746 <0.0600 <0.0881 <0.0759 <0.0696 <0.0587 <0.0713 <0.0797 <2.56 <3.54 496360-001 S 663568-1-BKS 495867-008 S MS Sample Id: LCS Sample Id: MS Sample Id: 496360-001 SD 663568-1-BSD 495867-008 SD MSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units MS Result LCS Result MS Result 2-Fluorophenol Nitrobenzene-d5 2-Fluorobiphenyl 2,4,6-Tribromophenol Terphenyl-D14 Phenol-d5 o-Terphenyl o-Terphenyl Surrogate Surrogate Surrogate MSD Flag LCSD Flag MSD Flag 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 11.04.14 18:17 10.28.14 22:57 10.29.14 04:06 Analysis Date Analysis Date Analysis Date Limits Limits Limits 25-121 23-120 30-115 19-122 18-137 15-110 32-128 32-128 MSD %Rec LCSD %Rec MSD %Rec 48 64 69 79 71 55 96 88 MS %Rec LCS %Rec MS %Rec 48 65 70 80 70 57 103 80 MB %Rec 77 % % % % % % % % Units Units Units MS Flag LCS Flag MS Flag MB Flag Page 48 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663721-1-BLK 663857-1-BLK 495861-010 MB Sample Id: MB Sample Id: Parent Sample Id: Solid Solid Soil Matrix: Matrix: Matrix: MADEP VPH MADEP VPH MADEP VPH Analytical Method: Analytical Method: Analytical Method: SW5030B SW5030B SW5030B Prep Method: Prep Method: Prep Method: 10.30.14 11.03.14 10.30.14 Date Prep: Date Prep: Date Prep: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter Parameter Parameter %RPD %RPD %RPD Flag Flag Flag 25 25 25 25 25 25 25 25 25 RPD Limit RPD Limit RPD Limit 2 3 2 2 1 0 4 1 2 954253 954490 954253 Seq Number: Seq Number: Seq Number: 10.30.14 04:29 10.30.14 04:29 10.30.14 04:29 11.03.14 10:31 11.03.14 10:31 11.03.14 10:31 10.30.14 11:07 10.30.14 11:07 10.30.14 11:07 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 LCSD %Rec LCSD %Rec MSD %Rec 98 98 113 81 121 128 101 104 117 LCSD Result LCSD Result MSD Result 7.33 7.38 2.82 6.07 9.05 3.19 9.97 10.3 3.87 LCS %Rec LCS %Rec MS %Rec 99 101 115 83 122 127 105 105 115 7.46 7.58 2.87 6.21 9.15 3.18 10.4 10.4 3.79 Spike Amount Spike Amount Spike Amount 7.50 7.50 2.50 7.50 7.50 2.50 9.90 9.90 3.30 MB Result MB Result Parent Result <0.000750 <0.000750 <0.000250 <0.000750 <0.000750 <0.000250 <0.000990 <0.000990 <0.000330 663721-1-BKS 663857-1-BKS 495861-010 S LCS Sample Id: LCS Sample Id: MS Sample Id: 663721-1-BSD 663857-1-BSD 495861-010 SD LCSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units LCS Result LCS Result MS Result 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) Surrogate Surrogate Surrogate LCSD Flag LCSD Flag MSD Flag 10.30.14 04:29 10.30.14 04:29 11.03.14 10:31 11.03.14 10:31 10.30.14 11:07 10.30.14 11:07 Analysis Date Analysis Date Analysis Date Limits Limits Limits 70-130 70-130 70-130 70-130 70-130 70-130 LCSD %Rec LCSD %Rec MSD %Rec 89 87 106 105 99 91 LCS %Rec LCS %Rec MS %Rec 94 90 107 104 89 86 MB %Rec MB %Rec 116 110 103 99 % % % % % % Units Units Units LCS Flag LCS Flag MS Flag MB Flag MB Flag Page 49 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-003 663630-1-BLK 663814-1-BLK 495804-001 Parent Sample Id: MB Sample Id: MB Sample Id: Parent Sample Id: Soil Solid Solid Soil Matrix: Matrix: Matrix: Matrix: MADEP VPH TPH-Gasoline Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: Analytical Method: Analytical Method: Analytical Method: SW5030B SW5030B SW5030B SW5030B Prep Method: Prep Method: Prep Method: Prep Method: 11.03.14 10.28.14 10.31.14 10.28.14 Date Prep: Date Prep: Date Prep: Date Prep: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics TPH-GRO TPH-GRO TPH-GRO Parameter Parameter Parameter Parameter %RPD %RPD %RPD %RPD Flag Flag Flag Flag 25 25 25 25 25 25 RPD Limit RPD Limit RPD Limit RPD Limit 6 3 0 2 0 0 954490 954085 954374 954085 Seq Number: Seq Number: Seq Number: Seq Number: 11.03.14 16:40 11.03.14 16:40 11.03.14 16:40 10.28.14 09:06 10.31.14 12:33 10.28.14 15:14 Analysis Date Analysis Date Analysis Date Analysis Date Limits Limits Limits Limits 70-130 70-130 70-130 64-114 64-114 64-114 MSD %Rec LCSD %Rec LCSD %Rec MSD %Rec 85 113 121 98 104 96 MSD Result LCSD Result LCSD Result MSD Result 5.45 7.24 2.60 49 52 49 MS %Rec LCS %Rec LCS %Rec MS %Rec 80 110 122 100 104 96 5.12 7.03 2.61 50 52 49 Spike Amount Spike Amount Spike Amount Spike Amount 6.42 6.42 2.14 50 50 51 Parent Result MB Result MB Result Parent Result <0.000642 <0.000642 <0.000214 <1.5 <1.5 <1.5 495867-003 S 663630-1-BKS 663814-1-BKS 495804-001 S MS Sample Id: LCS Sample Id: LCS Sample Id: MS Sample Id: 495867-003 SD 663630-1-BSD 663814-1-BSD 495804-001 SD MSD Sample Id: LCSD Sample Id: LCSD Sample Id: MSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units Units Units Units MS Result LCS Result LCS Result MS Result 2,5-Dibromotoluene 2,5-Dibromotoluene (PID) 2,5-Dibromotoluene 2,5-Dibromotoluene 2,5-Dibromotoluene Surrogate Surrogate Surrogate Surrogate MSD Flag LCSD Flag LCSD Flag MSD Flag 11.03.14 16:40 11.03.14 16:40 10.28.14 09:06 10.31.14 12:33 10.28.14 15:14 Analysis Date Analysis Date Analysis Date Analysis Date Limits Limits Limits Limits 70-130 70-130 57-131 57-131 57-131 MSD %Rec LCSD %Rec LCSD %Rec MSD %Rec 98 97 102 103 99 MS %Rec LCS %Rec LCS %Rec MS %Rec 93 91 103 109 97 MB %Rec MB %Rec 96 99 % % % % % Units Units Units Units MS Flag LCS Flag LCS Flag MS Flag MB Flag MB Flag Page 50 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-007Parent Sample Id: SoilMatrix: TPH-Gasoline Range Organics by SW-846 8015C Analytical Method:SW5030BPrep Method: 10.31.14Date Prep: TPH-GRO Parameter %RPD Flag 25 RPD Limit 0 954374Seq Number: 10.31.14 20:32 Analysis Date Limits 64-114 MSD %Rec 100 MSD Result 64 MS %Rec 10064 Spike Amount 64 Parent Result <1.9 495867-007 SMS Sample Id:495867-007 SDMSD Sample Id: mg/kg UnitsMS Result 2,5-Dibromotoluene Surrogate MSD Flag 10.31.14 20:32 Analysis Date Limits 57-131 MSD %Rec 98 MS %Rec 102 % UnitsMS Flag Page 51 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663625-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 10.28.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 2 7 2 11 2 4 2 8 8 8 2 6 0 2 8 6 0 8 2 7 11 0 8 6 1 8 2 7 2 0 4 2 6 0 0 4 2 7 4 0 13 6 2 2 8 1 0 4 2 11 9 1 954075Seq Number: 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 Analysis Date Limits 61-140 68-124 79-117 72-125 78-126 73-134 75-135 63-124 73-136 77-132 81-118 80-124 59-131 81-122 74-138 83-125 81-120 83-118 54-152 61-127 78-133 61-138 78-134 60-144 65-125 60-130 79-122 72-122 73-120 76-126 56-125 61-137 60-142 86-115 74-118 57-148 71-120 49-147 78-121 80-123 34-145 58-125 83-133 80-122 64-140 82-133 68-125 67-136 58-123 64-146 79-140 79-133 LCSD %Rec 106 88 102 88 106 94 102 92 96 92 102 96 110 92 92 92 100 92 106 88 90 100 92 92 93 100 92 86 104 104 104 94 106 98 106 98 100 84 92 104 72 90 98 92 92 99 110 110 102 88 88 99 LCSD Result 0.053 0.044 0.051 0.044 0.053 0.047 0.051 0.046 0.048 0.046 0.051 0.048 0.055 0.046 0.046 0.046 0.050 0.046 0.053 0.088 0.045 0.10 0.046 0.046 0.093 0.10 0.046 0.043 0.052 0.052 0.052 0.047 0.053 0.049 0.053 0.049 0.050 0.042 0.046 0.052 0.036 1.8 0.049 0.046 0.046 0.0991 0.11 0.055 0.051 0.044 0.044 0.0495 LCS %Rec 108 94 100 98 108 98 104 100 104 100 100 102 110 94 100 98 100 100 108 94 100 100 100 98 92 92 94 92 106 104 108 96 112 98 106 102 102 90 96 104 82 85 100 94 100 100 110 106 104 98 96 100 0.054 0.047 0.050 0.049 0.054 0.049 0.052 0.050 0.052 0.050 0.050 0.051 0.055 0.047 0.050 0.049 0.050 0.050 0.054 0.094 0.050 0.10 0.050 0.049 0.092 0.092 0.047 0.046 0.053 0.052 0.054 0.048 0.056 0.049 0.053 0.051 0.051 0.045 0.048 0.052 0.041 1.7 0.050 0.047 0.050 0.0999 0.11 0.053 0.052 0.049 0.048 0.0502 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.10 0.050 0.10 0.050 0.050 0.10 0.10 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 2.0 0.050 0.050 0.050 0.100 0.10 0.050 0.050 0.050 0.050 0.0500 MB Result <0.00075 <0.0012 <0.00067 <0.00080 <0.0012 <0.00054 <0.00057 <0.0016 <0.00087 <0.00072 <0.00086 <0.0013 <0.00060 <0.00093 <0.00081 <0.0010 <0.00069 <0.00068 <0.00060 <0.0023 <0.00071 <0.0011 <0.00055 <0.00080 <0.0032 <0.0069 <0.00051 <0.00085 <0.0010 <0.00050 <0.00096 <0.0025 <0.00074 <0.00058 <0.00099 <0.0024 <0.00074 <0.0023 <0.00066 <0.00054 <0.0012 <0.028 <0.00057 <0.0013 <0.00076 <0.00121 <0.00069 <0.0022 <0.0013 <0.00088 <0.00078 <0.000716 663625-1-BKSLCS Sample Id:663625-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 52 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663625-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 10.28.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 9 2 6 6 2 6 2 6 2 2 2 954075Seq Number: 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 Analysis Date Limits 75-137 82-128 61-137 72-140 85-120 76-126 78-115 71-128 51-154 72-124 67-138 LCSD %Rec 90 102 94 104 90 102 108 94 106 94 98 LCSD Result 0.045 0.051 0.047 0.052 0.045 0.051 0.054 0.047 0.053 0.047 0.049 LCS %Rec 98 104 100 110 92 108 106 100 108 96 100 0.049 0.052 0.050 0.055 0.046 0.054 0.053 0.050 0.054 0.048 0.050 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 MB Result <0.00066 <0.00074 <0.00083 <0.0010 <0.00059 <0.00078 <0.00067 <0.00071 <0.0035 <0.00072 <0.0020 663625-1-BKSLCS Sample Id:663625-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate LCSD Flag 10.28.14 07:40 10.28.14 07:40 10.28.14 07:40 Analysis Date Limits 50-150 57-158 50-150 LCSD %Rec 103 90 100 LCS %Rec 107 99 99 MB %Rec 101 99 93 % % % UnitsLCS Flag MB Flag Page 53 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663911-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 11.03.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 6 0 2 2 0 9 6 2 4 4 15 6 11 9 4 2 11 8 0 13 2 10 2 6 6 16 4 2 2 2 12 2 9 4 0 11 6 2 7 4 2 6 4 0 2 5 2 20 10 4 2 7 954513Seq Number: 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 Analysis Date Limits 61-140 68-124 79-117 72-125 78-126 73-134 75-135 63-124 73-136 77-132 81-118 80-124 59-131 81-122 74-138 83-125 81-120 83-118 54-152 61-127 78-133 61-138 78-134 60-144 65-125 60-130 79-122 72-122 73-120 76-126 56-125 61-137 60-142 86-115 74-118 57-148 71-120 49-147 78-121 80-123 34-145 58-125 83-133 80-122 64-140 82-133 68-125 67-136 58-123 64-146 79-140 79-133 LCSD %Rec 112 82 94 86 102 98 108 90 106 100 98 102 112 92 100 98 96 102 104 90 94 94 94 100 88 100 92 88 98 100 104 90 118 100 100 82 94 86 92 96 94 85 98 82 98 103 100 112 106 96 94 102 LCSD Result 0.056 0.041 0.047 0.043 0.051 0.049 0.054 0.045 0.053 0.050 0.049 0.051 0.056 0.046 0.050 0.049 0.048 0.051 0.052 0.090 0.047 0.094 0.047 0.050 0.088 0.10 0.046 0.044 0.049 0.050 0.052 0.045 0.059 0.050 0.050 0.041 0.047 0.043 0.046 0.048 0.047 1.7 0.049 0.041 0.049 0.103 0.10 0.056 0.053 0.048 0.047 0.0511 LCS %Rec 106 82 92 84 102 90 102 88 102 96 84 96 100 84 96 96 86 94 104 79 92 85 92 94 83 85 88 86 100 98 92 88 108 96 100 92 100 88 86 92 96 80 94 82 96 98 98 92 96 92 92 96 0.053 0.041 0.046 0.042 0.051 0.045 0.051 0.044 0.051 0.048 0.042 0.048 0.050 0.042 0.048 0.048 0.043 0.047 0.052 0.079 0.046 0.085 0.046 0.047 0.083 0.085 0.044 0.043 0.050 0.049 0.046 0.044 0.054 0.048 0.050 0.046 0.050 0.044 0.043 0.046 0.048 1.6 0.047 0.041 0.048 0.0984 0.098 0.046 0.048 0.046 0.046 0.0478 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.10 0.050 0.10 0.050 0.050 0.10 0.10 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 2.0 0.050 0.050 0.050 0.100 0.10 0.050 0.050 0.050 0.050 0.0500 MB Result <0.00075 <0.0012 <0.00067 <0.00080 <0.0012 <0.00054 <0.00057 <0.0016 <0.00087 <0.00072 <0.00086 <0.0013 <0.00060 <0.00093 <0.00081 <0.0010 <0.00069 <0.00068 <0.00060 <0.0023 <0.00071 <0.0011 <0.00055 <0.00080 <0.0032 <0.0069 <0.00051 <0.00085 <0.0010 <0.00050 <0.00096 <0.0025 <0.00074 <0.00058 <0.00099 <0.0024 <0.00074 <0.0023 <0.00066 <0.00054 <0.0012 <0.028 <0.00057 <0.0013 <0.00076 <0.00121 <0.00069 <0.0022 <0.0013 <0.00088 <0.00078 <0.000716 663911-1-BKSLCS Sample Id:663911-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result Page 54 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 663911-1-BLKMB Sample Id: SolidMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 11.03.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 6 4 2 4 5 4 4 4 4 9 8 954513Seq Number: 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 Analysis Date Limits 75-137 82-128 61-137 72-140 85-120 76-126 78-115 71-128 51-154 72-124 67-138 LCSD %Rec 98 100 98 106 90 102 102 94 116 90 100 LCSD Result 0.049 0.050 0.049 0.053 0.045 0.051 0.051 0.047 0.058 0.045 0.050 LCS %Rec 92 96 96 102 86 106 98 90 112 82 92 0.046 0.048 0.048 0.051 0.043 0.053 0.049 0.045 0.056 0.041 0.046 Spike Amount 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.050 MB Result <0.00066 <0.00074 <0.00083 <0.0010 <0.00059 <0.00078 <0.00067 <0.00071 <0.0035 <0.00072 <0.0020 663911-1-BKSLCS Sample Id:663911-1-BSDLCSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsLCS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate LCSD Flag 11.03.14 08:59 11.03.14 08:59 11.03.14 08:59 Analysis Date Limits 50-150 57-158 50-150 LCSD %Rec 106 90 99 LCS %Rec 102 92 96 MB %Rec 109 92 99 % % % UnitsLCS Flag MB Flag Page 55 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-010Parent Sample Id: SoilMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 10.28.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD X X X Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 4 0 2 0 8 2 13 8 9 7 2 12 5 2 10 11 6 8 4 15 2 0 5 5 12 9 7 3 2 6 0 5 2 7 0 7 6 7 0 0 0 9 5 2 5 4 9 7 20 8 5 2 954075Seq Number: 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 Analysis Date Limits 62-137 64-128 61-130 65-136 33-158 42-152 48-135 58-134 43-139 66-134 69-132 71-120 53-140 68-126 67-134 68-127 70-129 72-118 68-151 42-147 68-127 32-142 68-127 64-135 34-149 43-163 65-135 67-121 66-137 60-129 48-147 42-170 71-117 71-117 59-135 44-166 62-127 34-157 41-155 63-128 16-171 23-148 65-139 57-138 62-133 69-130 48-169 17-184 27-157 59-136 67-134 71-124 MSD %Rec 89 84 91 80 89 80 62 64 64 73 93 78 98 84 80 73 91 75 84 86 75 100 75 75 89 63 82 73 91 95 95 76 89 84 95 85 89 71 80 87 64 95 82 82 78 84 100 76 65 69 75 82 MSD Result 0.049 0.046 0.050 0.044 0.049 0.044 0.034 0.035 0.035 0.042 0.051 0.043 0.054 0.046 0.044 0.040 0.050 0.041 0.046 0.095 0.041 0.11 0.041 0.041 0.098 0.12 0.045 0.040 0.050 0.052 0.052 0.042 0.049 0.046 0.052 0.047 0.049 0.039 0.044 0.048 0.035 2.1 0.045 0.045 0.043 0.0927 0.11 0.058 0.038 0.038 0.041 0.0455 MS %Rec 84 82 91 79 95 77 54 68 57 66 89 68 102 80 71 64 95 68 86 100 71 100 70 70 100 54 75 70 91 88 93 79 89 77 93 79 82 75 79 86 63 105 77 79 73 80 109 82 51 63 70 80 0.047 0.046 0.051 0.044 0.053 0.043 0.030 0.038 0.032 0.039 0.050 0.038 0.057 0.045 0.040 0.036 0.053 0.038 0.048 0.11 0.040 0.11 0.039 0.039 0.11 0.11 0.042 0.039 0.051 0.049 0.052 0.044 0.050 0.043 0.052 0.044 0.046 0.042 0.044 0.048 0.035 2.3 0.043 0.044 0.041 0.0891 0.12 0.062 0.031 0.035 0.039 0.0446 Spike Amount 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.11 0.056 0.11 0.056 0.056 0.11 0.11 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 2.2 0.056 0.056 0.056 0.112 0.11 0.056 0.056 0.056 0.056 0.0558 Parent Result <0.00084 <0.0013 <0.00075 <0.00090 <0.0013 <0.00060 <0.00064 <0.0018 <0.00097 0.0020 <0.00096 <0.0014 <0.00067 <0.0010 <0.00091 <0.0011 <0.00077 <0.00076 <0.00067 <0.0025 <0.00079 <0.0013 <0.00062 <0.00089 <0.0036 0.051 <0.00057 <0.00095 <0.0011 <0.00056 <0.0011 <0.0027 <0.00083 <0.00065 <0.0011 <0.0027 <0.00083 <0.0026 <0.00074 <0.00060 <0.0013 <0.031 <0.00063 <0.0014 <0.00085 <0.00135 <0.00077 0.016 0.0023 <0.00098 <0.00087 <0.000799 495867-010 SMS Sample Id:495867-010 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 56 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-010Parent Sample Id: SoilMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 10.28.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 5 9 10 0 5 2 2 5 0 0 2 954075Seq Number: 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 Analysis Date Limits 65-131 50-143 67-131 42-156 13-188 57-143 55-141 39-150 34-179 13-188 40-161 MSD %Rec 73 84 78 89 76 87 93 82 93 25 84 MSD Result 0.040 0.046 0.043 0.049 0.042 0.048 0.051 0.045 0.051 0.014 0.046 MS %Rec 68 75 70 88 71 88 89 77 91 25 80 0.038 0.042 0.039 0.049 0.040 0.049 0.050 0.043 0.051 0.014 0.045 Spike Amount 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 0.056 Parent Result <0.00073 <0.00083 <0.00093 <0.0012 <0.00066 <0.00087 <0.00075 <0.00079 <0.0039 <0.00080 <0.0022 495867-010 SMS Sample Id:495867-010 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate MSD Flag 10.28.14 17:48 10.28.14 17:48 10.28.14 17:48 Analysis Date Limits 50-150 57-158 50-150 MSD %Rec 104 94 101 MS %Rec 111 95 99 % % % UnitsMS Flag Page 57 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-003Parent Sample Id: SoilMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 11.03.14Date Prep: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene Parameter %RPD X XF F XF F Flag 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 2 2 2 2 16 2 9 8 0 4 2 5 3 7 6 10 8 5 2 12 4 10 7 4 4 96 0 7 0 6 6 4 5 0 2 10 4 0 4 2 13 39 2 2 0 3 17 54 21 2 0 3 954513Seq Number: 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 Analysis Date Limits 62-137 64-128 61-130 65-136 33-158 42-152 48-135 58-134 43-139 66-134 69-132 71-120 53-140 68-126 67-134 68-127 70-129 72-118 68-151 42-147 68-127 32-142 68-127 64-135 34-149 43-163 65-135 67-121 66-137 60-129 48-147 42-170 71-117 71-117 59-135 44-166 62-127 34-157 41-155 63-128 16-171 23-148 65-139 57-138 62-133 69-130 48-169 17-184 27-157 59-136 67-134 71-124 MSD %Rec 96 86 88 81 93 82 60 84 63 82 91 75 102 82 88 77 91 75 95 81 81 91 81 82 87 318 82 79 91 91 98 82 95 84 91 88 89 77 81 86 77 100 84 75 86 86 100 456 74 75 81 85 MSD Result 0.055 0.049 0.050 0.046 0.053 0.047 0.034 0.048 0.036 0.047 0.052 0.043 0.058 0.047 0.050 0.044 0.052 0.043 0.054 0.089 0.046 0.10 0.046 0.047 0.096 0.35 0.047 0.045 0.052 0.052 0.056 0.047 0.054 0.048 0.052 0.050 0.051 0.044 0.046 0.049 0.044 2.3 0.048 0.043 0.049 0.0993 0.11 0.26 0.042 0.043 0.046 0.0489 MS %Rec 97 86 88 81 107 83 53 90 62 78 91 71 103 76 81 69 83 71 95 83 76 92 74 78 83 833 81 72 90 84 91 84 98 83 88 95 91 76 83 86 86 148 81 76 84 83 108 776 90 76 79 82 0.056 0.050 0.051 0.047 0.062 0.048 0.031 0.052 0.036 0.045 0.053 0.041 0.060 0.044 0.047 0.040 0.048 0.041 0.055 0.10 0.044 0.11 0.043 0.045 0.10 1.0 0.047 0.042 0.052 0.049 0.053 0.049 0.057 0.048 0.051 0.055 0.053 0.044 0.048 0.050 0.050 3.4 0.047 0.044 0.049 0.0967 0.13 0.45 0.052 0.044 0.046 0.0476 Spike Amount 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.12 0.058 0.12 0.058 0.058 0.12 0.12 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 2.3 0.058 0.058 0.058 0.117 0.12 0.058 0.058 0.058 0.058 0.0583 Parent Result <0.00088 <0.0014 <0.00078 <0.00094 <0.0014 <0.00063 <0.00067 <0.0019 <0.0010 <0.00084 <0.0010 <0.0015 <0.00070 <0.0011 <0.00095 <0.0012 <0.00080 <0.00080 <0.00070 <0.0027 <0.00083 <0.0013 <0.00064 <0.00093 <0.0038 <0.0080 <0.00060 <0.0010 <0.0012 <0.00058 <0.0011 <0.0029 <0.00087 <0.00068 <0.0012 <0.0029 <0.00086 <0.0027 <0.00077 <0.00063 <0.0014 <0.033 <0.00066 <0.0015 <0.00089 <0.00141 <0.00081 <0.0025 <0.0015 <0.0010 <0.00091 <0.000835 495867-003 SMS Sample Id:495867-003 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result Page 58 of 77 Final 1.000 QC Summary 495867 Terraquest Environmental Consultants, P.C. Parker's Stop N Shop 495867-003Parent Sample Id: SoilMatrix: VOCs by SW-846 8260BAnalytical Method:SW5035Prep Method: 11.03.14Date Prep: sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter %RPD Flag 20 20 20 20 20 20 20 20 20 20 20 RPD Limit 4 2 2 6 0 12 0 2 0 0 2 954513Seq Number: 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 Analysis Date Limits 65-131 50-143 67-131 42-156 13-188 57-143 55-141 39-150 34-179 13-188 40-161 MSD %Rec 82 81 86 93 79 93 93 86 104 74 86 MSD Result 0.047 0.046 0.049 0.053 0.045 0.053 0.053 0.049 0.059 0.042 0.049 MS %Rec 78 78 83 86 78 103 91 83 102 72 86 0.045 0.045 0.048 0.050 0.045 0.060 0.053 0.048 0.059 0.042 0.050 Spike Amount 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 0.058 Parent Result <0.00077 <0.00087 <0.00097 <0.0012 <0.00069 <0.00091 <0.00078 <0.00082 <0.0041 <0.00084 <0.0023 495867-003 SMS Sample Id:495867-003 SDMSD Sample Id: mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg UnitsMS Result 1,2-Dichloroethane-D4 4-Bromofluorobenzene Toluene-D8 Surrogate MSD Flag 11.03.14 19:03 11.03.14 19:03 11.03.14 19:03 Analysis Date Limits 50-150 57-158 50-150 MSD %Rec 105 99 98 MS %Rec 111 101 102 % % % UnitsMS Flag Page 59 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663568-1-BLKLab Sample Id: SOLIDMatrix: 663568-1-BLK Sample Id: TPH-Diesel Range Organics by SW-846 8015C Analytical Method: CLARAnalyst: SW3550Prep Method: 10.28.14 09:45Date Prep: CLARTech: TPH-DRO (C10-C28) Parameter 2.56 Result U8.33 Flag mg/kg Units 1 DilCas Number C10C28DRO U 954095Seq Number: MDLRL 10.28.14 22:23 Analysis Date Page 60 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663617-1-BLKLab Sample Id: SOLIDMatrix: 663617-1-BLK Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 10.28.14 15:30Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 20.0 10.0 10.0 Result U U U 20.0 10.0 10.0 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C1 ALHYDRC19C U U U 954194Seq Number: MDLRL 10.29.14 14:14 10.29.14 14:54 10.29.14 14:54 Analysis Date Page 61 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663619-1-BLKLab Sample Id: SOLIDMatrix: 663619-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17:00Date Prep: 5458Tech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether Parameter 0.0590 0.0540 0.0527 0.0520 0.0613 0.0643 0.0423 0.0607 0.0537 0.0433 0.0607 0.0597 0.0510 0.0467 0.0447 0.0420 0.0987 0.0487 0.0460 0.0580 0.0567 0.0477 0.0553 0.0633 0.0507 0.0410 0.0467 0.0567 0.0367 0.0493 0.0540 0.0490 0.0543 0.0550 0.0573 0.0527 0.0500 0.0400 0.0473 0.0450 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.667 1.67 0.333 0.333 0.333 0.167 0.333 0.333 0.333 0.667 0.667 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.167 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 39638-32-9 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: MDLRL 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 Analysis Date Page 62 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663619-1-BLKLab Sample Id: SOLIDMatrix: 663619-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3545Prep Method: 10.28.14 17:00Date Prep: 5458Tech: bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0540 0.0443 0.0647 0.0427 0.0537 0.0503 0.0613 0.0553 0.0433 0.0407 0.0557 0.0370 0.0573 0.0517 0.0607 0.0343 0.0533 0.0593 0.0477 0.0700 0.0603 0.0553 0.0467 0.0567 0.0633 Result U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.333 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U 954326Seq Number: MDLRL 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 10.29.14 13:05 Analysis Date Page 63 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663625-1-BLKLab Sample Id: SOLIDMatrix: 663625-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06:53Date Prep: 4148Tech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Parameter 0.00075 0.0012 0.00067 0.00080 0.0012 0.00054 0.00057 0.0016 0.00087 0.00072 0.00086 0.0013 0.00060 0.00093 0.00081 0.00100 0.00069 0.00068 0.00060 0.0023 0.00071 0.0011 0.00055 0.00080 0.0032 0.0069 0.00051 0.00085 0.0010 0.00050 0.00096 0.0025 0.00074 0.00058 0.00099 0.0024 0.00074 0.0023 0.00066 0.00054 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 0.0050 0.0010 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954075Seq Number: MDLRL 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 Analysis Date Page 64 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663625-1-BLKLab Sample Id: SOLIDMatrix: 663625-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 10.28.14 06:53Date Prep: 4148Tech: Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.0012 0.028 0.00057 0.0013 0.00076 0.00121 0.00069 0.0022 0.0013 0.00088 0.00078 0.000716 0.00066 0.00074 0.00083 0.0010 0.00059 0.00078 0.00067 0.00071 0.0035 0.00072 0.0020 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0020 0.050 0.0010 0.0020 0.0010 0.00200 0.0020 0.0050 0.0020 0.0010 0.0010 0.00100 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U 954075Seq Number: MDLRL 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 10.28.14 09:21 Analysis Date Page 65 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663630-1-BLKLab Sample Id: SOLIDMatrix: 663630-1-BLK Sample Id: TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: JOLAnalyst: SW5030BPrep Method: 10.28.14 08:35Date Prep: JOLTech: TPH-GRO Parameter 1.5 Result U2.5 Flag mg/kg Units 50 DilCas Number 8006-61-9 U 954085Seq Number: MDLRL 10.28.14 10:10 Analysis Date Page 66 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663721-1-BLKLab Sample Id: SOLIDMatrix: 663721-1-BLK Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 10.30.14 03:58Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000750 0.000750 0.000250 Result U U U 0.000750 0.000750 0.000250 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C1 HYDC9C10 U U U 954253Seq Number: MDLRL 10.30.14 06:21 10.30.14 06:21 10.30.14 06:21 Analysis Date Page 67 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663814-1-BLKLab Sample Id: SOLIDMatrix: 663814-1-BLK Sample Id: TPH-Gasoline Range Organics by SW-846 8015C Analytical Method: JOLAnalyst: SW5030BPrep Method: 10.31.14 12:01Date Prep: JOLTech: TPH-GRO Parameter 1.5 Result U2.5 Flag mg/kg Units 50 DilCas Number 8006-61-9 U 954374Seq Number: MDLRL 10.31.14 13:37 Analysis Date Page 68 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663842-1-BLKLab Sample Id: SOLIDMatrix: 663842-1-BLK Sample Id: MADEP EPH Analytical Method: CLARAnalyst: SW3545Prep Method: 11.03.14 09:30Date Prep: 5458Tech: C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics Parameter 20.0 10.0 10.0 Result U U U 20.0 10.0 10.0 Flag mg/kg mg/kg mg/kg Units 1 1 1 DilCas Number C11C22 ALHYDRC9C1 ALHYDRC19C U U U 954596Seq Number: MDLRL 11.04.14 17:17 11.04.14 16:38 11.04.14 16:38 Analysis Date Page 69 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663857-1-BLKLab Sample Id: SOLIDMatrix: 663857-1-BLK Sample Id: MADEP VPH Analytical Method: JOLAnalyst: SW5030BPrep Method: 11.03.14 10:00Date Prep: JOLTech: C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Parameter 0.000750 0.000750 0.000250 Result U U U 0.000750 0.000750 0.000250 Flag mg/kg mg/kg mg/kg Units 50 50 50 DilCas Number ALHYDRC5C8 ALHYDRC9C1 HYDC9C10 U U U 954490Seq Number: MDLRL 11.03.14 11:32 11.03.14 11:32 11.03.14 11:32 Analysis Date Page 70 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663909-1-BLKLab Sample Id: SOLIDMatrix: 663909-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3550Prep Method: 11.04.14 10:00Date Prep: BROTech: 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl-phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether Parameter 0.0590 0.0540 0.0527 0.0520 0.0613 0.0643 0.0423 0.0607 0.0537 0.0433 0.0607 0.0597 0.0510 0.0467 0.0447 0.0420 0.0987 0.0487 0.0460 0.0580 0.0567 0.0477 0.0553 0.0633 0.0507 0.0410 0.0467 0.0567 0.0367 0.0493 0.0540 0.0490 0.0543 0.0550 0.0573 0.0527 0.0500 0.0400 0.0473 0.0450 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.667 1.67 0.333 0.333 0.333 0.167 0.333 0.333 0.333 0.667 0.667 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.167 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 120-82-1 95-50-1 541-73-1 106-46-7 95-95-4 88-06-2 120-83-2 105-67-9 121-14-2 606-20-2 91-58-7 95-57-8 91-57-6 95-48-7 88-74-4 88-75-5 15831-10-4 91-94-1 99-09-2 534-52-1 101-55-3 59-50-7 106-47-8 7005-72-3 100-01-6 100-02-7 83-32-9 208-96-8 62-53-3 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 65-85-0 85-68-7 111-91-1 111-44-4 39638-32-9 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954619Seq Number: MDLRL 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 Analysis Date Page 71 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663909-1-BLKLab Sample Id: SOLIDMatrix: 663909-1-BLK Sample Id: SVOCs by SW-846 8270D Analytical Method: VICAnalyst: SW3550Prep Method: 11.04.14 10:00Date Prep: BROTech: bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Parameter 0.0540 0.0443 0.0647 0.0427 0.0537 0.0503 0.0613 0.0553 0.0433 0.0407 0.0557 0.0370 0.0573 0.0517 0.0607 0.0343 0.0533 0.0593 0.0477 0.0700 0.0603 0.0553 0.0467 0.0567 0.0633 Result U U U U U U U U U U U U U U U U U U U U U U U U U 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.333 0.667 0.333 0.333 0.333 0.333 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 117-81-7 218-01-9 53-70-3 132-64-9 84-66-2 131-11-3 84-74-2 117-84-0 206-44-0 86-73-7 118-74-1 87-68-3 77-47-4 67-72-1 193-39-5 78-59-1 91-20-3 98-95-3 621-64-7 86-30-6 87-86-5 85-01-8 108-95-2 129-00-0 110-86-1 U U U U U U U U U U U U U U U U U U U U U U U U U 954619Seq Number: MDLRL 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 11.04.14 12:42 Analysis Date Page 72 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663911-1-BLKLab Sample Id: SOLIDMatrix: 663911-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 11.03.14 07:49Date Prep: MWETech: 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Parameter 0.00075 0.0012 0.00067 0.00080 0.0012 0.00054 0.00057 0.0016 0.00087 0.00072 0.00086 0.0013 0.00060 0.00093 0.00081 0.00100 0.00069 0.00068 0.00060 0.0023 0.00071 0.0011 0.00055 0.00080 0.0032 0.0069 0.00051 0.00085 0.0010 0.00050 0.00096 0.0025 0.00074 0.00058 0.00099 0.0024 0.00074 0.0023 0.00066 0.00054 Result U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.0010 0.010 0.0010 0.010 0.0010 0.0010 0.010 0.010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0050 0.0010 0.0010 0.0010 0.0050 0.0010 0.0050 0.0010 0.0010 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 71-55-6 79-34-5 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 78-93-3 95-49-8 591-78-6 106-43-4 99-87-6 108-10-1 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 124-48-1 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 954513Seq Number: MDLRL 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 Analysis Date Page 73 of 77 Final 1.000 Blank Summary 495867 Terraquest Environmental Consultants, P.C., Mebane, NC Parker's Stop N Shop 663911-1-BLKLab Sample Id: SOLIDMatrix: 663911-1-BLK Sample Id: VOCs by SW-846 8260B Analytical Method: MLAAnalyst: SW5035Prep Method: 11.03.14 07:49Date Prep: MWETech: Dichlorodifluoromethane Ethanol Ethylbenzene Isopropyl Ether Isopropylbenzene m,p-Xylenes Methyl tert-butyl ether Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Parameter 0.0012 0.028 0.00057 0.0013 0.00076 0.00121 0.00069 0.0022 0.0013 0.00088 0.00078 0.000716 0.00066 0.00074 0.00083 0.0010 0.00059 0.00078 0.00067 0.00071 0.0035 0.00072 0.0020 Result U U U U U U U U U U U U U U U U U U U U U U U 0.0020 0.050 0.0010 0.0020 0.0010 0.00200 0.0020 0.0050 0.0020 0.0010 0.0010 0.00100 0.0010 0.0010 0.0010 0.0020 0.0010 0.0010 0.0010 0.0010 0.0050 0.0050 0.0050 Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg Units 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 DilCas Number 75-71-8 64-17-5 100-41-4 108-20-3 98-82-8 179601-23-1 1634-04-4 75-09-2 91-20-3 104-51-8 103-65-1 95-47-6 135-98-8 100-42-5 98-06-6 127-18-4 108-88-3 156-60-5 10061-02-6 79-01-6 75-69-4 108-05-4 75-01-4 U U U U U U U U U U U U U U U U U U U U U U U 954513Seq Number: MDLRL 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 11.03.14 11:05 Analysis Date Page 74 of 77 Final 1.000 Page 75 of 77 Final 1.000 Page 76 of 77 Final 1.000 Prelogin/Nonconformance Report- Sample Log-In XENCO Laboratories 495867Work Order #: 10/24/2014 10:20:00 AMDate/ Time Received: Terraquest Environmental Consultants, PClient: Sample Receipt Checklist Checklist completed by: Date: Checklist reviewed by:Date: Mike Kimmel 10/24/2014 10/25/2014 #2 *Shipping container in good condition? #3 *Samples received on ice? #4 *Custody Seals intact on shipping container/ cooler? #5 Custody Seals intact on sample bottles? #6 *Custody Seals Signed and dated? #7 *Chain of Custody present? #8 Sample instructions complete on Chain of Custody? #9 Any missing/extra samples? #10 Chain of Custody signed when relinquished/ received? #11 Chain of Custody agrees with sample label(s)? #12 Container label(s) legible and intact? #13 Sample matrix/ properties agree with Chain of Custody? #14 Samples in proper container/ bottle? #15 Samples properly preserved? #16 Sample container(s) intact? #17 Sufficient sample amount for indicated test(s)? #18 All samples received within hold time? #19 Subcontract of sample(s)? #20 VOC samples have zero headspace (less than 1/4 inch bubble)? #21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for samples for the analysis of HEM or HEM-SGT which are verified by the analysts. #22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH? Yes Yes N/A N/A N/A Yes Yes No Yes Yes Yes Yes Yes Yes Yes Yes Yes No N/A N/A N/A #1 *Temperature of cooler(s)?1.2 Acceptable Temperature Range: 0 - 6 degC Air and Metal samples Acceptable Range: Ambient * Must be completed for after-hours delivery of samples prior to placing in the refrigerator Analyst: PH Device/Lot#: Comments Dario Lagunas Temperature Measuring device used : #61 Page 77 of 77 Final 1.000