WS-5532_19272_CA_RMR_20230105_CAPR

Speedway, LLC
500 Speedway Drive Enon, Ohio 45323 Phone: [phone]

Corrective Action
Performance Report
Speedway Store No. 6958 653 East Webb Avenue Burlington, North Carolina
Incident No. 19272
Project No. 60686627
January 5, 2023

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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Quality Information

Prepared for:
North Carolina Department of Environmental Quality
Winston-Salem Regional Office
Division of Waste Management – Underground Storage Tank Section
450 West Hanes Mill Road, Suite 300
Winston-Salem, NC 27105
Phone: [phone]
Prepared by:
AECOM Technical Services, Inc,
5438 Wade Park Blvd., Suite 200
Raleigh, North Carolina 27607
Phone: [phone]
aecom.com
Copyright © 2022 by AECOM
All rights reserved. No part of this copyrighted work may be reproduced, distributed, or transmitted in any form or by
any means without the prior written permission of AECOM.
Prepared by Prepared by Reviewed by

Angie Sastoque Ardila
Entry Level Remediation Engineer
[e-mail]
Ian Ros, P.E.
[e-mail]
Remediation Engineer
Marianne Link
Project Manager
[e-mail]

Reviewed by

Marie Treiber [e-mail]
Regional Senior Project Manager
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Table of Contents
Executive Summary ....................................................................................................................................................... 1
1 Introduction ......................................................................................................................................................... 1-1
2 Site Background Information ............................................................................................................................... 2-1
2.1 Site Identification ......................................................................................................................................... 2-1
2.2 Contact Information ..................................................................................................................................... 2-1
2.3 Release Information ..................................................................................................................................... 2-1
3 Site History and Characterization ........................................................................................................................ 3-1
3.1 Site Characteristics ...................................................................................................................................... 3-1
3.2 Site Geology and Hydrogeology .................................................................................................................. 3-1
3.3 Underground Storage Tank Systems ........................................................................................................... 3-1
3.4 Aboveground Storage Tank Systems ........................................................................................................... 3-1
3.5 Historical Releases ...................................................................................................................................... 3-1
3.6 Zoning .......................................................................................................................................................... 3-2
3.7 Receptor Information ................................................................................................................................... 3-2
3.7.1 Public Water Supply Wells .................................................................................................................... 3-2
3.7.2 Private Water Supply Wells .................................................................................................................. 3-2
3.7.3 Public Water Systems ........................................................................................................................... 3-2
3.7.4 Surface Water ....................................................................................................................................... 3-2
3.7.5 Wellhead Protection Areas ................................................................................................................... 3-2
3.7.6 Subsurface Structures .......................................................................................................................... 3-2
3.8 Initial Abatement and Remediation Activities ............................................................................................... 3-3
4 Groundwater Monitoring ..................................................................................................................................... 4-1
4.1 Groundwater Gauging.................................................................................................................................. 4-1
4.2 Groundwater Sampling Methods ................................................................................................................. 4-1
4.3 Groundwater Analytical Results ................................................................................................................... 4-1
5 Corrective Action ................................................................................................................................................. 5-1
5.1 Description ................................................................................................................................................... 5-1
5.2 Objectives .................................................................................................................................................... 5-1
5.3 Operation and Maintenance ......................................................................................................................... 5-1
5.4 Monitoring and Performance ........................................................................................................................ 5-1
6 Conclusions and Recommendations ................................................................................................................... 6-1
7 References.......................................................................................................................................................... 7-1
8 Statements and Certifications ............................................................................................................................. 8-1

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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Figures

Figure 1 Site Location Map
Figure 2 Site Features Map
Figure 3 Zoning Map
Figure 4 Groundwater Elevation Contour Map - November 8, 2022
Figure 5 Estimated Benzene Isoconcentration Map - November 8, 2022
Tables

Table 1 Site History – UST Owner/Operator and Other Responsible Party Information
Table 2 Site History – UST System and Other Release Information
Table 3 Monitoring and Recovery Well Construction Summary
Table 4 Historical LNAPL Thickness and Groundwater Elevation Data
Table 5 November 2022 Groundwater Analytical Results
Table 6 Historical Groundwater Analytical Results
Table 7 Summary of Air Stack Analytical Results and Mass Removal Calculations
Table 8 Summary of Liquid Discharge Flow Data and Analytical Results

Appendices

Appendix A Adjacent Parcel Data
Appendix B Groundwater Monitoring Event Documentation
Appendix C Laboratory Analytical Reports
Appendix D DPE System Drawings and Wastewater Permit
Appendix E System O&M Tracking and Inspection Form
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Acronyms
2L Standard Title 15A North Carolina Administrative Code 2L.0202 Groundwater Quality Standard
AECOM AECOM Technical Services, Inc.
AFVR Aggressive Fluid/Vapor Recovery
AST Aboveground Storage Tank
bls Below Land Surface
CAP Corrective Action Plan
CAPR Corrective Action Performance Report
CoC Contaminant of Concern
CSA Comprehensive Site Assessment
DIPE Diisopropyl ether
DPE Dual-Phase Extraction
DTW Depth to Water
DWM Division of Waste Management
EPA United States Environmental Protection Agency
ft feet
ft/ft feet-per-foot
GCL Gross Contaminant Level
GIS Geopgraphic Information System
gpd gallons per day
gpm gallons per minute
in-Hg inches of mercury
LNAPL light non-aqueous phase liquid
MAA Mid-Atlantic Associates, Inc.
MMPE Mobile Multi-Phase Extraction
MTBE Methyl Tert-Butyl Ether
MTU Mobile Treatment Unit
NCDEQ North Carolina Department of Environmental Quality
NCDENR North Carolina Department of Environment Natural Resources
NTCP New Technology Cleanup Plan
O&M Operation and Maintenance
% Percent
Pace Pace Analytical
PID Photoionization Detector
POTW Publicly Owned Treatment Works
scfm standard cubic feet per minute
Site Speedway Store No. 6958
Speedway Speedway, LLC
SVE/GW Soil Vapor Extraction/Vacuum-Enhanced Groundwater Recovery and Treatment System
SWAP NC’s Source Water Assessment Program
UST Underground Storage Tank
VOC Volatile Organic Compound
VR Vapor Recovery
WilcoHess WilcoHess, LLC

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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Executive Summary
As required by the North Carolina Department of Environmental Quality (NCDEQ), AECOM Technical Services, Inc.
of North Carolina (AECOM), on behalf of Speedway, LLC (Speedway), has prepared this Corrective Action
Performance Report (CAPR) for Speedway Store No. 6958 (Site), located at 653 East Webb Avenue, Burlington,
North Carolina 27217. The Site is an active gas station and convenience store.
On November 6, 1997, a release from the Site’s gasoline underground storage tank (UST) system was reported. As a
result, several environmental assessment activities have been performed on the Site and nearby locations. Currently,
a Dual-Phase Extraction (DPE) system operates at the Site. The DPE system recovers, treats, and discharges
petroleum impacted groundwater and soil vapor.
The DPE system currently operates in 6-month intervals. According to the initial CAPR, submitted by Mid-Atlantic
Associates, Inc. (MAA – Speedway’s former environmental consultant) on December 7, 2021 (MAA, 2021a), the first
operating period occurred from March to September 2021. During that time, the DPE system had a total downtime of
33 days, resulting in a runtime efficiency of 82%. Five air stack samples and five treated liquid discharge samples
were collected during this initial operating period. A total of 187,966 gallons (approximately 1,033 gallons per day) of
groundwater were extracted, and an estimated 710 gallons of petroleum were removed as vapor during the first
operating period. On October 4, 2021, groundwater sampling and gauging activities were performed, and a
Groundwater Monitoring Report was submitted by MAA on December 7, 2021 (MAA, 2021b). The groundwater
sampling results indicated that several Site monitoring wells exhibited constituent concentrations above the Title 15A
NCAC 2L.0202 Groundwater Quality Standard (2L Standard), and monitoring wells MW-19 and MW-21 exhibited
benzene concentrations exceeding the Gross Contaminant Level (GCL). Light non-aqueous phase liquid (LNAPL)
was not detected in any monitoring wells during the October 4, 2021 sampling and gauging event.
The activities conducted during the second DPE system operating period (March 2022 through September 2022) are
summarized as follows:
• AECOM personnel conducted groundwater gauging activities for 11 monitoring wells and groundwater sampling
activities for eight monitoring wells.
• DPE system operation and maintenance (O&M) was conducted on a routine and as-needed basis to maintain
system operation.
• Air stack samples and treated liquid discharge samples were collected from the DPE system on a routine basis.
Based on the observations and results from the second DPE system operating period that are detailed in this report,
AECOM concludes the following:
• Several constituents of concern (CoCs) were detected in groundwater at concentrations exceeding the 2L
Standards.
• Benzene was detected in monitoring well MW-21 at a concentration exceeding the GCL.
• Measurable LNAPL was present in monitoring well MW-19 at a thickness of 0.02 feet.
• The DPE system operated with a runtime efficiency of 92 percent (%).
• The DPE system recovered and treated 120,603 gallons of petroleum impacted groundwater at an average
effective pump rate of 726.3 gallons-per-day (gpd).
• Mass removal calculations estimated 320.39 gallons of petroleum were removed as vapor by the DPE system.
• Mass removal efficiency of the DPE system appears to increase overtime through continuous operation.
• The DPE system may be mobilizing contaminant mass towards the extraction wells from the surrounding
formation.
Based on these conclusions, AECOM, on behalf of Speedway, recommends the following:
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
• Continue operating the DPE system. Extend the operational period from six months to 12 months in order to
further evaluate the increasing trends of mass removal efficiency over time.
• Perform semi-annual groundwater sampling while the DPE system is operating in order to evaluate the effects
of the system on localized groundwater elevations (e.g., radius of influence, groundwater drawdown, and cones
of depression) and groundwater CoC concentrations. The first event should occur after six months of operation
and the second event should occur after 12 months of operation.
• Continue to perform monthly air stack sampling of the DPE system.
• Continue to perform quarterly sampling of the DPE system treated liquid discharge.
• Collect influent liquid samples during the quarterly discharge sampling in order to further evaluate and monitor
mass removal as liquid and air stripper/active carbon treatment efficiency.
• Generate and submit a CAPR after 12 months of operation summarizing the results and conclusions after
implementation of the above recommendations.
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
1 Introduction
As required by the NCDEQ, AECOM has prepared this CAPR, on behalf of Speedway, to document the second
operating period of the DPE system as well as the activities and results of the November 8, 2022 groundwater
monitoring event conducted at the Site. The Site is located at 653 East Webb Avenue, Burlington, North Carolina
27217 (Figure 1). The Site is an active gas station and convenience store. The layout of the facility, Site features, and
surrounding properties are illustrated in Figure 2. Based on the previous remediation activities and historical
assessment data, a New Technology Cleanup Plan (NTCP) (MAA, 2017) was approved by the NCDEQ to implement
a full-scale DPE system at the Site. Construction of the system was initiated on September 17, 2020 and completed
on March 8, 2021 when operation began.

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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
2 Site Background Information
The following sections provide site background and contact information.
2.1 Site Identification
Date of Incident Report: November 6,1997
Incident Number: 19272
Facility ID: 0-004038
Site Rank: High (H180E)
Site Name: Speedway 6958
Site Street Address: 653 East Webb Avenue
City/Town: Burlington Zip Code: 27217 County: Alamance
Latitude/Longitude: 36.08815 / -79.43034
2.2 Contact Information
Property Owner: Speedway, LLC
Address: 500 Speedway Dr., Enon, OH 45323 Telephone: [phone]

Property Occupant: Speedway, LLC
Address: 500 Speedway Dr., Enon, OH 45323 Telephone: [phone]

UST Owner: Speedway, LLC
Address: 500 Speedway Dr., Enon, OH 45323 Telephone: [phone]

UST Operator: Speedway, LLC
Address: 500 Speedway Dr., Enon, OH 45323 Telephone: [phone]

Consultant/Contractor: AECOM
Address: 5438 Wade Park Boulevard, Suite 200, Raleigh, NC 27607 Telephone: [phone]
2.3 Release Information
On November 6, 1997, a release from the gasoline UST system located at the Site was reported. As a result, a soil
vapor extraction and vacuum-enhanced groundwater recovery and treatment (SVE/GW) system was installed in
2001. Shortly after installation, LNAPL and vapors were discovered in the Willowbrook Hosiery facility, located at 413
Tucker Street which is downgradient of the known extent of the release. An emergency vapor recovery (VR) system
was installed to remove vapors from the Willowbrook Hosiery facility; however, the remediation system was
permanently shut down in December 2004 under Session Law 2004-124.
The former Site owner (WilcoHess) renovated the Site in 2005. The renovation consisted of removing and replacing
the USTs, product lines, and dispensers, razing Site buildings, and constructing a new building. The renovation also
involved abandoning former remediation and monitoring wells and removing the former soil vapor extraction/ vacuum-
enhanced groundwater recovery and treatment system (SVE/GW). With the lowering of the Trust Fund “funding bar”
in 2008, the NCDEQ directed the renewal of assessment and remediation activities at the Site.
Based on Site subsurface characterization, the groundwater contaminant plume has migrated off-site, in the direction
of the adjacent residential apartment complex, the Bateman residence, and the Willowbrook facility, where LNAPL
and impacted groundwater have historically been observed in the basement. LNAPL has also been intermittently
present in four off-site monitoring wells (MW-19, MW-21, MW-23, and MW-24), generally located west of the Site
(Figure 2). Passive LNAPL recovery activities (such as absorbent socks) were conducted from February 2009
through December 2009, and a total of seven Mobile Multi-Phase Extraction (MMPE) events were completed at the
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
Site from June 2012 to January 2015. Selected historical Site assessment data was provided in the Groundwater
Monitoring Report dated December 7, 2021 (MAA, 2021b).

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3 Site History and Characterization
The following sections provide information on the Site including USTs operated at the Site and follows the general
outline established in Guidelines for Assessment and Corrective Action for UST Releases (NCDEQ, 2021a) and
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases (NCDEQ, 2021b).
3.1 Site Characteristics
The Site is an active gas station and convenience store located at 653 East Webb Avenue, Burlington, North Carolina
27217 (Figure 1). The layout of the facility, Site features, and surrounding properties are illustrated in Figure 2. The
Site is accessed from East Webb Avenue, east of the Site, and Tucker Street, south of the Site. Commercial and
residential properties surround the Site.
3.2 Site Geology and Hydrogeology
Site geology and hydrogeology were evaluated based on historical and current investigations. The Site is located
within the Piedmont physiographic province. The subsurface generally consists of clayey silts and silty clays
interlayered with medium to coarse sands and quartz lenses. The Site’s geologic profile consists of silty clay in the
first four feet (ft) below land surface (bls) and then becomes tan-light brown clayey silt (saprolitic) to 15 ft bls.
Extremely weathered rock was encountered from 15 to 20 ft bls (MAA, 2021a).
Based on the previous borings advanced at the Site, the lithologic units beneath the Site appear to be laterally
discontinuous (MAA, 2021a). Therefore, a preferential migration pathway (e.g., a former stream bed, fracture zone,
dike, etc.) may exist between the Site and the Willowbrook Hosiery facility, allowing for accelerated transport of
contaminants.
Groundwater has historically been encountered at approximately 12 ft bls. Based on the results of the most recent
gauging event (November 8, 2022), general groundwater flow is to the southwest, which is consistent with historical
groundwater flow.
3.3 Underground Storage Tank Systems
UST owner operator and other responsible party information is provided in Table 1. A summary of the USTs
maintained at the Site is provided below and summarized in Table 2.
Currently, there are four double-walled, steel USTs with fiberglass coating at the Site. There is one 15,000-gallon
regular unleaded gasoline UST, one 8,000-gallon premium unleaded gasoline UST, one 12,000-gallon diesel UST,
and one 10,000-gallon kerosene UST.
3.4 Aboveground Storage Tank Systems
No aboveground storage tank (AST) systems are currently present on-site. Based on available information, no ASTs
have historically been present at the Site.
3.5 Historical Releases
Based on the NCDEQ Incident Management Database (NCDEQ, 2022a), there are two historical releases (UST
incident number 19272 and UST incident number 48221). The UST incident number 19272 is the subject incident,
reported on November 6, 1997. WilcoHess, LLC (WilcoHess) was the responsible party. The UST incident number
48221 was reported on January 20, 2022 when the under-dispenser containment of Dispenser 1/2 failed triennial
hydrostatic testing. Repairs were made and a post-repair hydrostatic test passed. A Site Check Report (MAA, 2022)
concluded that petroleum impacts (benzene and xylenes) were detected above NCDEQ action levels, however, any
impact to groundwater would be commingled with the prior release associated with NCDEQ incident number 19272.
NCDEQ has not responded to this report and the incident is currently open with no risk classification. Speedway was
the responsible party.
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
3.6 Zoning
According to the Burlington Zoning Viewer Map (City of Burlington, 2022), the properties surrounding the Site are
zoned Residential, General Business, and Industrial. The Site is currently zoned as General Business, and the Site’s
adjoining properties are zoned as General Business and Medium Density Residential. The main zones within 1,500 ft
of the Site are Residential, Industrial, Office Institutional, and General Business. Currently, west of the Site are
residential properties, beyond which is East Davis Street; to the north are Davis Street United Methodist Church and
Alamance Funeral Service, beyond which is Cameron Street; to the east is East Webb Avenue, beyond which is
Stillwood Ammunition Systems; to the south of the Site is Friendly Check Cashing, beyond which is DEKRA
Emissions & Safety Station. A zoning map is provided as Figure 3. Adjacent property owners are identified in the
table and drawing that are provided in Appendix A.
3.7 Receptor Information
A receptor survey update was not conducted as part of this reporting period. Receptor information for the Site was
documented in the Comprehensive Site Assessment (CSA) submitted by MAA on October 21, 1998 (MAA, 1998).
3.7.1 Public Water Supply Wells
No water supply wells were identified within 1,500 ft of the Site (MAA, 1998).
3.7.2 Private Water Supply Wells
Based on information obtained from the NCDEQ Division of Water Resources database (NCDEQ Division of Water
Resources, 2021), the municipal water service covers the Site and surrounding area. Therefore, surrounding
properties are expected to be connected to public water.
According to the NC’s Source Water Assessment Program ([SWAP] NCDEQ, 2021c) 2.0 Geographic Information
System (GIS) online mapping application, the nearest registered groundwater community well is approximately 6,200
ft northeast of the Site, located at the Stoney Creek Reservoir.
3.7.3 Public Water Systems
The City of Burlington’s municipal water and sewer are available to the Site and properties surrounding the Site. The
city obtains its water from Lake Macintosh and Stoney Creek Reservoir.
3.7.4 Surface Water
According to the Ground Water Management Branch Map Interface (NCDEQ 2022b), the closest surface water
bodies are the Dye Branch, located approximately 1,400 ft west of the Site, and an unnamed tributary of Haw River
located about 1,000 ft east of the Site. The surface waters around the Site are illustrated in Figure 3.
3.7.5 Wellhead Protection Areas
No wellhead protection areas were identified within 1,500 ft of the Site (NCDEQ, 2021c).
3.7.6 Subsurface Structures
Currently, there are no known subsurface structures (basements, etc.) at the Site that could potentially accumulate
fuel vapors. However, there are several subsurface structures that may have influenced the migration path of
impacted groundwater. The subsurface structures are summarized below:
• Underground utility lines have been identified in the vicinity of the former UST locations. Usually, utilities are
buried two to four ft bls (MAA, 2021a).
• Sanitary sewer pipes (and/or the trench in which they are situated) located beneath East Davis Street may have
intersected the water table in the past. The elevation (relative to the Site benchmark) of the bottom of the sewer
pipe is approximately 80 ft (MAA, 2021a).
• LNAPL and impacted groundwater have historically been observed in the basement of the Willowbrook Hosiery
building.
• Previous vapor monitoring of the basement for the Bateman residence did not reveal evidence of petroleum
vapors (MAA, 2021a).
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
3.8 Initial Abatement and Remediation Activities
On November 6, 1997, a release of regular unleaded gasoline was discovered from an impact valve air pressure
gauge on an underground line feeding a dispenser island located at the Site’s north end. The volume of the release is
unknown. The leak was repaired, and subsequent assessments revealed the presence of LNAPL on the water table.
A CSA was conducted at the Site, as well as LNAPL recovery. Thirty Aggressive Fluid/Vapor Recovery (AFVR)
events were conducted, which removed approximately 1,525 gallons of LNAPL from the water table. The North
Carolina Department of Environment Natural Resources (NCDENR), Division of Waste Management (DWM)
classified the Site as “intermediate” based on the presence of petroleum-fuel-related compounds in groundwater at
concentrations exceeding the GCLs.
The September 6, 2000 Corrective Action Plan ([CAP] MAA, 2000) suggested the implementation of the SVE/GW
system. The SVE/GW system was installed in 2001, but shortly after installation, LNAPL and vapors were discovered
in the Willowbrook Hosiery building, located at 423 Tucket Street, which is downgradient of the known extent of the
release. An emergency VR system consisting of vertical wells placed along the Willowbrook Hosiery building’s
foundation and connected to a blower was installed and successfully removed vapors from the building.
The SVE/GW system was permanently shut down on November 30, 2004 due to Session Law 2004-124; however,
the VR system at the Willowbrook Hosiery property continued to operate. WilcoHess renovated the Site in 2005. The
renovation consisted of removing and replacing the USTs, product line, and dispensers, razing Site buildings, and
constructing a new building. The renovation also involved abandoning former remediation and monitoring wells and
removing the former remediation system. With the lowering of the Trust Fund “funding bar” in 2008, the NCDEQ
directed the renewal of assessment and remediation activities at the Site.
During assessment activities, LNAPL was not found at the Site, but three off-site monitoring wells (MW-21, MW-23,
and MW-24) exhibited LNAPL. The monitoring wells are located on the adjacent and surrounding properties
northwest of the Site (Figure 2). After LNAPL was detected in the monitoring wells, passive skimming devices (such
as absorbent socks) were installed to recover the LNAPL. Manual LNAPL recovery activities were then conducted
from February 2009 through December 2009. The Free Product Recovery Report dated January 25, 2010 (MAA,
2010) documented the results of the LNAPL recovery activities and recommended the evaluation of more aggressive
active LNAPL recovery methods. Based on the evaluation, three subsequent MMPE events were conducted at the
Site from June 2012 to August 2013.
Based on historical LNAPL recovery results and discussions between MAA and NCDEQ, it was determined that
additional MMPE events would be conducted at the Site on a quarterly basis. Four additional MMPE events were
conducted at the Site from April 2014 to January 2015. While performing the additional MMPE events, the VR system
at the Willowbrook Hosiery building and the absorbent socks were inspected twice a month. The additional MMPE
events recovered approximately 21,791 gallons of product/water mix, with an estimated 277 gallons of gasoline
removed as vapor. LNAPL was not detected in any of the monitoring wells over the reporting period (MAA, 2021b).
Based on the MMPE events’ effectiveness and a historical assessment data review, a NTCP was approved by
NCDEQ to implement a full-scale DPE system at the Site. Construction of the system was initiated on September 17,
2020. The construction involved the installation of six extraction wells (DPE-01 through DPE-06), followed by
trenching, conduit placement, installation of well boxes at each extraction well, pouring of a concrete pad for the DPE
system enclosure, completion of a manifold connection point adjacent to the concrete pad, and a connection to the
City of Burlington sanitary sewer. On February 17, 2021, a DPE treatment system enclosed in a mobile trailer unit
(MTU) was transported to the Site and placed on the concrete pad. An electric meter was installed, and the electric
line was energized by Duke Power the week of March 8, 2021. Well construction details for all wells installed at the
Site are summarized in Table 3. Locations of the DPE wells, trenching, and MTU are illustrated in Figure 2.
Operation of the DPE system began in March 2021 and extended through September 2021 when it was intentionally
shutdown for reporting and sampling purposes. During that initial operating period, a total of 187,966 gallons
(approximately 1,033 gallons per day) of water were extracted, and an estimated 710 gallons of petroleum were
removed as vapor. Groundwater sampling and gauging activities were performed on October 4, 2021 and no LNAPL
was detected in any of the monitoring wells. The second operational period for the DPE system began when it was
restarted on March 17, 2022.
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4 Groundwater Monitoring
This section discusses the activities of, and results from, the most recent groundwater monitoring event which was
performed on November 8, 2022. A well inventory log and daily activity logs from the event are included as Appendix
B.
4.1 Groundwater Gauging
AECOM personnel performed a groundwater monitoring event on November 8, 2022. The monitoring event objective
was to gauge and sample 17 monitoring wells; however, only 11 monitoring wells (MW-6R, MW-15, MW-19, MW-21,
MW-23, MW-29, MW-30, MW-31, MWWB-1, MWWB-2, and MWWB-3) were able to be located and gauged.
Monitoring well MW-10R was located but closed with a PVC cap that was unable to be removed and monitoring wells
MW-16, MW-24, MW-25, MW-26, and VE-3 were not located.
The monitoring wells were opened and allowed to stabilize under atmospheric pressure prior to being gauged with an
electronic oil/water interface probe. The average groundwater depth was approximately 12 ft and ranged from 5.45 ft
(monitoring well MWWB-1) to 16.04 ft (monitoring well MW-6R). The hydraulic gradient from monitoring well MW-6R
to monitoring well MWWB-1 was approximately 0.018 feet-per-foot (ft/ft) in November 2022. A groundwater elevation
contour map was generated based on the November 8, 2022 gauging event and is provided as Figure 4.
Measurable LNAPL was detected in monitoring well MW-19 at a thickness of 0.02 ft. The interface probe indicated
the presence of product at monitoring wells MW-29 and MW-31 but did not indicate the presence of water in both
cases so a depth to water (DTW) measurement could not be collected. Without the DTW measurement for monitoring
wells MW-29 and MW-31, an LNAPL thickness could not be determined, nor could the presence of LNAPL be
confirmed. It should be noted that LNAPL has never been detected in either monitoring well, historically, and LNAPL
indication during the event was likely due to malfunctioning equipment. The historical LNAPL thickness and
groundwater elevation data which include the most recent event are summarized in Table 4.
In addition to groundwater gauging and sampling, AECOM personnel visited the Willowbrook Hosiery basement to
collect readings using a photoionization detector (PID). The Willowbrook Hosiery basement is occupied by a fabric
washing and drying company. Chemical drums used in the on-site operations were observed in the basement. Poor
housekeeping practices including spilled materials were observed during the visit. However, AECOM personnel did
not observe any detections when collecting PID readings within the breathing space.
4.2 Groundwater Sampling Methods
During the November 8, 2022 groundwater monitoring event, eight monitoring wells were sampled including
monitoring wells MW-6R, MW-15, MW-21, MW-23, MW-30, MWWB-1, MWWB-2, and MWWB-3. Monitoring well MW-
19 was not sampled due to the presence of measurable LNAPL and monitoring wells MW-29 and MW-31 were not
sampled due to the potential presence of LNAPL.
Prior to sample collection, AECOM personnel used disposable bailers to purge three well volumes. Samples were
then collected using a clean, disposable bailer. Collected samples were labeled, sealed, and placed on ice in coolers
for transportation under chain-of custody protocol to Pace Analytical (Pace), located at 4915 Waters Edge Dr Suite
180, Raleigh, NC 27606, for analysis of volatile organic compounds (VOCs) using the SM 6200B Method. The daily
activity logs (Appendix B) document the monitoring well purge volumes and sample collection times.
4.3 Groundwater Analytical Results
The laboratory analytical report and chain-of-custody for groundwater samples collected during the November 8,
2022 groundwater monitoring event are provided in Appendix C.
Monitoring well MW-21 was the only monitoring well sampled that exhibited a CoC concentration exceeding the GCL.
Several of the sampled monitoring wells exhibited CoC concentrations above the 2L Standard. Details of the
analytical CoC exceedances are summarized below:
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Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
• Benzene exceeded the 2L Standard in seven of the eight monitoring wells which included monitoring wells MW-
6R, MW-15, MW-21, MW-23, MW-30, MWWB-1, and MWWB-3. Benzene also exceeded the GCL in monitoring
well MW-21. The estimated benzene isoconcentration contours are illustrated in Figure 5. Note that monitoring
well MW-19 was not sampled due to the presence of measurable LNAPL (0.02 ft).
• Toluene exceeded the 2L Standard in one monitoring well, MW-21.
• Ethylbenzene exceeded the 2L Standard in two of the eight monitoring wells which included monitoring wells
MW-21 and MW-23.
• Total xylenes exceeded the 2L Standard in three of the eight monitoring wells which included monitoring wells
MW-6R, MW-21, and MW-23.
• N-butylbenzene exceeded the 2L Standard in two of the eight monitoring wells which included monitoring wells
MW-21 and MW-23.
• Diisopropyl ether (DIPE) exceeded the 2L Standard in three of the eight monitoring wells which included
monitoring wells MW-15, MW-21, and MW-30.
• Isopropylbenzene (cumene) exceeded the 2L Standard in three of the eight monitoring wells which included
monitoring wells MW-6R, MW-21, and MW-23.
• Methyl tert-butyl ether (MTBE) exceeded the 2L Standard in four of the eight monitoring wells which included
monitoring wells MW-15, MW-21, MW-30, and MWWB-3.
• Naphthalene exceeded the 2L Standard in seven of the eight monitoring wells which included monitoring wells
MW-6R, MW-15, MW-21, MW-23, MW-30, MWWB-1, and MWWB-3.
• N-propylbenzene exceeded the 2L Standard in four of the eight monitoring wells which included monitoring wells
MW-6R, MW-15, MW-21, and MW-23.
• 1,2,4-trimethylbenzene exceeded the 2L Standard in three of the eight monitoring wells which included
monitoring wells MW-6R, MW-21, and MW-23.
• 1,3,5-trimethylbenzene exceeded the 2L Standard in one monitoring well, MW-21.
A summary of the analytical results from the November 8, 2022 groundwater monitoring event is provided in Table 5.
The historical analytical results for the Site are provided in Table 6.
5-1
Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
5 Corrective Action
5.1 Description
A full-scale DPE system was constructed at the Site between September 2020 and March 2021. The DPE system
uses a high-powered vacuum pump to collect impacted groundwater and soil vapor for treatment and discharge. The
DPE system consists of six extraction wells connected to a mobile treatment unit (MTU) through three manifolds. The
extraction wells (DPE-01 through DPE-06) are located along the residential apartment complex west of the Site, and
the MTU is located in a fenced area behind the store (Figure 2). The MTU contains a vacuum pump, a water/vapor
separator tank, two transfer pumps, an oil/water separator, a low-profile diffuser-type air stripper, bag filters, and an
active carbon filtration system. The DPE system discharges treated liquid to the publicly owned treatment works
(POTW) under a wastewater discharge permit obtained from the City of Burlington. The wastewater discharge permit
was renewed on June 15, 2022 and now has a new expiration date of June 16, 2027. Appendix D provides the DPE
Piping and Trenching Layout map, DPE MTU Layout, DPE P&ID, and the wastewater discharge permit.
5.2 Objectives
The DPE system was implemented to reduce groundwater CoC concentrations and remove LNAPL at the Site and
nearby properties to ultimately progress the Site towards risk-based closure. Historically, benzene has been the CoC
that repeatedly exceeded the GCL.
5.3 Operation and Maintenance
Routine inspections of, and necessary maintenance on, the DPE system were conducted bi-weekly. The routine
inspections included the following:
• Inspect the DPE system and MTU conditions.
• Record applied vacuum at DPE banks and wells.
• Record air flow at the DPE air stack and flow meter reading for the treated liquid discharge to the POTW.
• Record DPE equipment data (e.g., operating hours, temperature, airflow, etc.).
• Remote system response and alert monitoring.
• Regular maintenance (e.g., changing oil, replacing bag filters and carbon filter media, inspecting pumps and
liquid level controls, etc.).
• Collection of air stack samples and treated liquid discharge samples.

Monitoring data collected during routine inspections was recorded on system inspection forms and then transferred to
an operation and maintenance (O&M) table log for performance tracking purposes. The O&M table log and a copy of
the inspection form are provided in Appendix E.
The operational data is summarized below:
• The operational period for the DPE system began on March 17, 2022 and ended on September 14, 2022 (181
days).
• The DPE system operated for a total of 3,985.2 hours resulting in a runtime efficiency of 92 %.
• The DPE blower operated at an average vacuum of 12.7 inches of mercury (in-Hg).
• The DPE blower operated at an average flowrate of 68 standard cubic feet-per-minute (scfm).
• The total volume of groundwater recovered and treated by the DPE system was 120,603 gallons.
• The DPE system averaged an effective pump rate of 726.3 gpd, or 0.50 gallons-per-min (gpm).
5.4 Monitoring and Performance
As stated earlier, the second operating period began on March 17, 2022 and extended through September 14, 2022.
Air stack samples were collected on a monthly basis resulting in a total of seven air stack samples collected during
the operating period. The samples were collected from a sample port located on the piping influent to the DPE
vacuum pump. All collected samples were shipped under chain-of-custody control to Pace. The Air stack samples
were analyzed for VOCs by Method TO-15 or Method M18-Mod A summary of the analytical results for the air stack
5-2
Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
sampling during the operating period is provided in Table 7. The laboratory analytical reports and chain-of-custody
records for the air stack effluent samples are included in Appendix C.
Treated liquid discharge samples were collected on a quarterly basis. A total of three treated liquid discharge samples
were collected during the operating period which were analyzed for mercury by Method 245.1, metals by Method
200.8, and VOCs by Method 624.1. The samples were collected from a sample port located on the effluent piping
near the flow totalizer and then shipped under chain-of-custody control to Pace. The previously mentioned
wastewater discharge permit (Appendix D) defines the treated liquid discharge sampling quarters. The third
discharge sampling event did not occur within the third quarter as defined by the permit. Therefore, a fourth discharge
sample was collected on October 10, 2022 to satisfy the quarterly reporting permit requirements. The discharge
sample was collected after the system shutdown and was analyzed for pesticides by United States Environmental
Protection Agency (EPA) 608.3, diesel and oil range organics by EPA 8015C, gas range organics by EPA
5030B/8015C, cadmium by EPA 200.7, mercury by EPA 245.1, metals by EPA 6010D, semi volatile pollutants by EPA
625.1, and volatile organics acrolein by EPA 624.1. A summary of the analytical results for the treated liquid discharge
sampling during the operating period is provided in Table 8. The laboratory analytical reports and chain-of-custody
records for the treated liquid discharge samples are included in Appendix C.

Contaminant mass removed as vapor during the operational period was calculated based on assumptions and inputs
which are defined in Table 7. The calculations provide an estimate of the contaminant mass removed based on the
following considerations:
• Airflow rates were measured at the air stack using a handheld anemometer.
• The makeup air valve was not adjusted during air stack sampling in order to capture the most representative
sample of influent concentrations during typical operation.
• Airflow rates and analytical samples collected from the air stack are instantaneous measurements which are
used to average the variable nature over extended periods of time during system operation.
Based on the contaminant mass removal calculations performed using the assumptions and inputs defined in Table 7
and the considerations above, a total of 320.39 gallons of petroleum were removed as vapor. The 320.39 gallons
exhibits a decrease in total mass removal when compared to the initial operating period which resulted in 710 gallons
of petroleum removed as vapor (MAA, 2021a). The decrease could be due to a combination of several factors such
as differences in operational methods, contaminant mass reduction by the DPE system operation, or differences in
airflow measurement and sampling techniques. One similar trend between the initial operating period and the recent
operating period is that the mass removal efficiency increased as the DPE system continued to operate. For example,
the DPE system removed petroleum at an estimated 0.97 gpd during the first month of the operating period and an
estimated 4.01 gpd during the last month of the operating period. The increase in removal efficiency overtime
appears to be mainly due to increasing influent concentrations which may be due to influence from the system
drawing contaminant mass to the extraction wells from the surrounding formation. Based on these increasing trends,
the stoppage of DPE system operation after six months occurred when the system was most effective during both
operating periods.

Contaminant mass removed as liquid could not be estimated because influent samples were not collected during the
operating period. However, a total of 120,603 gallons of petroleum impacted groundwater was recovered and treated
by the DPE system during the operating period. The total volume of recovered groundwater exhibits a decrease when
compared to the initial operating period which resulted in 187,966 gallons (MAA, 2021a) even though the DPE
system had a higher runtime efficiency (92% versus 82%) during the recent operating period. This may be due to
differences in operational methods. For example, the makeup air valve was adjusted several times during the recent
operating period to reduce the vacuum applied to the DPE wells. Although, no LNAPL was recovered by the DPE
system during the operating period, measurable LNAPL was detected in monitoring well MW-19. No LNAPL was
observed in any of the monitoring wells during the groundwater monitoring event performed after the initial operating
period on October 4, 2021 (MAA, 2021b). This may further suggest that contaminant mass in the surrounding
formation is being mobilized by the DPE system toward the extraction wells.
6-1
Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
6 Conclusions and Recommendations
The activities conducted during the second DPE system operating period (March 2022 through September 2022) are
summarized as follows:
• AECOM personnel conducted groundwater gauging activities for 11 monitoring wells and groundwater sampling
activities for eight monitoring wells.
• DPE system O&M was conducted on a routine and as-needed basis to maintain system operation.
• Air stack samples and treated liquid discharge samples were collected from the DPE system on a routine basis.
Based on the observations and results from the second DPE system operating period that are detailed in this report,
AECOM concludes the following:
• Several CoCs were detected in groundwater at concentrations exceeding the 2L Standards.
• Benzene was detected in monitoring well MW-21 at a concentration exceeding the GCL.
• Measurable LNAPL was present in monitoring well MW-19 at a thickness of 0.02 ft.
• The DPE system operated with a runtime efficiency of 92%.
• The DPE system recovered and treated 120,603 gallons of petroleum impacted groundwater at an average
effective pump rate of 726.3 gpd.
• Mass removal calculations estimated 320.39 gallons of petroleum were removed as vapor by the DPE system.
• Mass removal efficiency of the DPE system appears to increase overtime through continuous operation.
• The DPE system may be mobilizing contaminant mass towards the extraction wells from the surrounding
formation.
Based on these conclusions, AECOM, on behalf of Speedway recommends the following:
• Continue operating the DPE system. Extend the operational period from six months to 12 months in order to
further evaluate the increasing trends of mass removal efficiency over time.
• Perform semi-annual groundwater sampling while the DPE system is operating in order to evaluate the effects
of the system on localized groundwater elevations (e.g., radius of influence, groundwater drawdown, and cones
of depression) and groundwater CoC concentrations. The first event should occur after six months of operation
and the second event should occur after 12 months of operation.
• Continue to perform monthly air stack sampling of the DPE system.
• Continue to perform quarterly sampling of the DPE system treated liquid discharge.
• Collect influent liquid samples during the quarterly discharge sampling in order to further evaluate and monitor
mass removal as liquid and air stripper/active carbon treatment efficiency.
• Generate and submit a CAPR after 12 months of operation summarizing the results and conclusions after
implementation of the above recommendations.

7-1
Speedway 6958 Burlington, NC Corrective Action Performance Report January 2023
7 References
City of Burlington, Planning Dept., 2022. Burlington Zoning Viewer - Public,
https://regisnc.maps.arcgis.com/apps/webappviewer/index.html?id=d8169997319149c6a44da62941577d42,
accessed November 22, 2022.
MAA,1998. Report of Environmental Services, Comprehensive Site Assessment. Speedway Store No. 6958. 653
East Webb Avenue, Burlington, North Carolina, 27217. Incident No. 19272. October 21, 1998.
MAA, 2000. Corrective Action Plan. Speedway Store No. 6958. 653 East Webb Avenue, Burlington, North Carolina,
27217. Incident No. 19272. September 6, 2000.
MAA, 2010. Free Product Recovery Report. Speedway Store No. 6958. 653 East Webb Avenue, Burlington, North
Carolina, 27217. Incident No. 19272. January 25, 2010.
MAA, 2017. New Technology Cleanup Plan, Speedway Store No. 6958. 653 East Webb Avenue, Burlington, North
Carolina, 27217. Incident No. 19272. April 21, 2017.
MAA, 2021a. Corrective Action Performance Report (Initial). Speedway Store No. 6958. 653 East Webb Avenue,
Burlington, North Carolina, 27217. Incident No. 19272. December 7, 2021.
MAA, 2021b. Groundwater Monitoring Report. Speedway Store No. 6958. 653 East Webb Avenue, Burlington, North
Carolina, 27217. Incident No. 19272. December 7, 2021.
MAA, 2022. Site Check Report. Speedway Store No. 6958. 653 East Webb Avenue, Burlington, North Carolina,
27217. Incident No. 48221. February 4, 2022.
NCDEQ Division of Water Resources, 2021. Local Water Supply Planning,
https://www.ncwater.org/WUDC/app/LWSP/report.php?pwsid=02-01-010&year=2021, accessed November
21, 2022.
NCDEQ, 2021a. Guidelines for Assessment and Corrective Action for UST Releases. Effective January 19, 2021.
NCDEQ, 2021b. Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases.
Effective January 19, 2021.
NCDEQ, 2021c. SWAP 2.0,
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=26f4e2b3140f4e58825e48781ccebf5e,
accessed November 22, 2022.
NCDEQ, 2022a. Incident Management Database,
https://deq.nc.gov/about/divisions/waste-management/science-data-and-reports/gis-maps/underground-
storage-tank-incidents-map, accessed November 22, 2022.
NCDEQ, 2022b. Ground Water Management Branch Map Interface,
https://www.ncwater.org/GWMS/openlayers/ol.php?entrance=home_page&menulist=bl, accessed November
21, 2022.
Session Law 2004-124, 2004. House Bill 1414, ratified July 17, 2004, signed by Governor Easley July 20, 2004.

AECOM
FIGURES

2,0002,000
N
SITE LOCATION
FIGURE 1Site Location Map
Source: Topo USGS 7.5 Minute Topographic MapQuadrangle: Burlington, NC
Copyright: 2019 National Geographic Society
DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:File: C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington.dwg Layout: Site Location Map Date: 15 Dec, 2022 Xrefs:00
SCALE IN FEET:
NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.
60686627I. DUMITRUDECEMBER 2022 M. LINK
Speedway LLC.
Speedway Store #6958
653 East Webb Avenue
Burlington, North Carolina
SCALE IN FEET:6060060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington.dwg, 12/15/2022 7:59 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUDECEMBER 2022M. LINKFIGURE 2Speedway LLC.Speedway Store #6958653 East Webb AvenueBurlington, North CarolinaSite Features MapMonitoring Well Location (Willowbrook)Vertical Extent WellLEGENDFenceProduct DispenserUnderground Storage TankMonitoring Well Location15,000-Gal. RUL Gasoline8,000-Gal. PUL Gasoline12,000-Gal. Diesel10,000-Gal. KeroseneApproximate Site Property BoundaryApproximate Property BoundaryBuilding FootprintDual-Phase Extraction WellDPE Piping Trench
© 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS SCALE IN FEET:350350060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington.dwg, 12/15/2022 8:00 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUDECEMBER 2022M. LINKFIGURE 3Speedway LLC.Speedway Store #6958653 East Webb AvenueBurlington, North CarolinaZoning MapLEGENDApproximate Site Property BoundaryApproximate Property BoundarySurface WaterMedium Density ResidentialHigh Density ResidentialOffice InstitutionalGeneral BusinessGeneral Business - Limited UseConditional BusinessConditional IndustrialLight IndustrialHeavy Industrial
SCALE IN FEET:6060060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington Analytical.dwg, 12/15/2022 8:19 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUDECEMBER 2022M. LINKFIGURE 4Speedway LLC.Speedway Store #6958653 East Webb AvenueBurlington, North CarolinaGroundwater ElevationContour MapNovember 8, 2022Monitoring Well Location (Willowbrook)Vertical Extent WellLEGENDApproximate Site Property BoundaryFenceProduct DispenserUnderground Storage TankMonitoring Well Location15,000-Gal. RUL Gasoline8,000-Gal. PUL Gasoline12,000-Gal. Diesel10,000-Gal. Kerosene11/8/22 LNAPL LocationsStatic Water Elevation (Ft)Not GaugedStatic Water Elevation Contour (Ft)Dashed Where InferredApproximate GroundwaterFlow DirectionNot ApplicableApproximate Property BoundaryBuilding FootprintDual-Phase Extraction WellDPE Piping Trench
SCALE IN FEET:6060060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington Analytical.dwg, 12/15/2022 8:14 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUDECEMBER 2022M. LINKFIGURE 5Speedway LLC.Speedway Store #6958653 East Webb AvenueBurlington, North CarolinaEstimated BenzeneIsoconcentration MapNovember 8, 2022Monitoring Well Location (Willowbrook)Former LNAPL LocationsVertical Extent WellLEGENDApproximate Site Property BoundaryFenceProduct DispenserUnderground Storage TankMonitoring Well Location15,000-Gal. RUL Gasoline11/8/22 LNAPL LocationsBenzene Concentration (µg/L)8,000-Gal. PUL Gasoline12,000-Gal. Diesel10,000-Gal. KeroseneNot DetectedNot SampledEstimated Benzene ConcentrationContour (NC 2L Standard = 1.0 μg/L)Estimated Benzene ConcentrationContour (GCL = 5,000 μg/L)Approximate Property BoundaryBuilding FootprintContour (10,000 μg/L)Estimated Benzene ConcentrationDual-Phase Extraction WellDPE Piping Trench

AECOM
TABLES

Table 1
Site History - UST Owner/Operator and Other Responsible Party Information
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
UST ID Number A1, A2, A3, A4 Facility ID Number 0-004038
City State Zip Telephone Number
Springfield OH 45501 [phone]
Incident number 19272; Open
Andrew McMillan 2005 - Present
Name of UST Owner Date of Operation
Current UST Owner Address
PO Box 1500
Name of UST Operator Date of Operation
Speedway, LLC 2005 - Present
Page 1 of 1
Table 2
Site History - UST System and Other Release Information
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
UST ID
Number Product Stored Capacity
(gallons)Construction Details Associated Piping
and Pumps Date Installed Current Status
Was release
associated with
UST System?
A1
Regular
Unleaded
Gasoline
15,000 Steel (Fiberglass
Coated) Double Wall
Fiberglass (Single
Wall)9/1/2005 Active No
A2
Premium
Unleaded
Gasoline
8,000 Steel (Fiberglass
Coated) Double Wall
Fiberglass (Single
Wall)9/1/2005 Active No
A3 Diesel 12,000 Steel (Fiberglass
Coated) Double Wall
Fiberglass (Single
Wall)9/1/2005 Active No
A4 Kerosone 10,000 Steel (Fiberglass
Coated) Double Wall
Fiberglass (Single
Wall)9/1/2005 Active No
Page 1 of 1
Table 3
Monitoring and Recovery Well Construction Summary
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
MW-1* 11/10/1997 4 28 8 – 28
MW-2* 12/11/1997 4 18 8 – 18
MW-3* 12/11/1997 4 18 8 – 18
MW-4* 12/11/1997 4 20 10 – 20
MW-5* 12/11/1997 4 20 10 – 20
MW-6* 12/11/1997 4 21 11 – 21
MW-7* 1/9/1998 4 20 10 – 20
MW-8* 1/9/1998 4 23.5 13.5 – 23.5
MW-9* 4/29/1998 2 18 8 – 18
MW-10* 4/29/1998 2 17 7 – 17
MW-11D* 4/29&30/98 2 60 55 - 60
MW-12* 4/29/1998 2 18 8 – 18
MW-13* 4/29/1998 2 18 8 – 18
MW-14* 4/29/1998 2 18 8 – 18
MW-15 7/27/1998 2 18 8 – 18
MW-16 7/27/1998 2 18 8 – 18
MW-17* 7/27/1998 2 18 8 – 18
MW-18 8/21/1998 2 18 8 – 18
MW-19 3/9/2000 2 18 8 – 18
MW-20 3/31/2003 2 19 4 – 19
MW-21 4/1/2003 2 21 6 – 21
MW-22 4/1/2003 2 19 4 – 19
MW-23 4/1/2003 2 19 5 – 20
MW-24 4/2/2003 2 20 5 – 20
MW-25 3/6/2004 2 13 3 - 13
MW-26 3/6/2004 2 12.5 2.5 - 12.5
MW-27 4/2/2004 2 14 4 - 14
MW-28 4/2/2004 2 20 5 – 20
MW-29 4/16/2009 2 22 7 - 22
MW-30 4/27/2010 2 20 5 – 20
VE-1* 3/23/1999 4 20 5 – 20
VE-2* 3/23/1999 4 20 5 – 20
VE-3 3/23/1999 4 20 5 – 20
VE-4* 3/23/1999 4 20 5 – 20
VE-5* 3/24/1999 4 20 5 – 20
VE-6* 3/24/1999 4 20 5 – 20
VE-7* 3/24/1999 4 20 5 – 20
MWWB-1 12/18/2001 2 18 3 – 18
MWWB-2 12/18/2001 2 20 5 – 20
MWWB-3 12/18/2001 2 20 5 – 20
MWWB-4 12/18/2001 2 20 5 – 20
MW-2R 4/15/2008 2 22 7 – 22
MW-6R 4/15/2008 2 22 7 – 22
MW-10R 4/15/2008 2 22 7 – 22
MW-13R 4/15/2008 2 22 7 – 22
MW-31 2/6/2018 2 19 9 – 19
Well ID Date Installed
Diameter
(inches)
Total Well Depth
(feet bls)
Screened Interval
(feet bls)
Monitoring Wells
Page 1 of 2
Table 3
Monitoring and Recovery Well Construction Summary
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
DPE-1 9/17/2020 4 17 7 - 17
DPE-2 9/17/2020 4 17 7 - 17
DPE-3 9/17/2020 4 17 7 - 17
DPE-4 9/17/2020 4 17 7 - 17
DPE-5 9/17/2020 4 17 7 - 17
DPE-6 9/17/2020 4 17 7 - 17
Notes:
Monitoring and Recovery Well Construction Data were obtained from the December 7, 2021
Groundwater Monitoring Report.
* Removal during site redevelopment activities in 2005
bls - below land surface
Well ID Date Installed
Diameter
(inches)
Total Well Depth
(feet bls)
Screened Interval
(feet bls)
Extraction Wells
Page 2 of 2
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
4/2/1998 4.5 11.94 88.04
5/5/1998 3.94 11.95 87.62
7/29/1998 1.26 13.07 84.54
3/15/2000 1.09 12.71 84.78
12/10/01 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
11/11/2002 NM NM NM
2/26/2003 NM NM NM
5/28/2003 0.90 9.45 87.9
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 13.75 83.94
11/18/2004 NM NM NM
4/2/1998 0 7.4 88.13
5/5/1998 NM NM NM
7/29/1998 0 11.08 84.45
3/15/2000 0 11.15 84.38
12/10/2001 0 16.23 79.3
5/14/2002 0 14.72 80.81
8/29/2002 0 17.41 78.12
11/11/2002 0 13.69 81.84
2/26/2003 0 11.33 84.2
5/15/2003 0 9.67 85.86
8/14/2003 0 7.36 88.17
11/5/2003 0 10.08 86.45
5/5/2004 0 11.69 84.84
11/18/2004 0 11.4 85.13
4/29/2008 0 12.59 83.25
4/21/2009 0 11.15 84.69
4/27/2010 0 10.69 85.15
4/18/2011 0 12.17 83.67
4/10/2012 0 12.59 83.25
4/16/2013 0 11.86 83.98
4/28/2014 0 9.08 86.76
4/9/2015 0 11.94 83.9
1/6/2016 0 9.37 86.47
11/8/2022 NM NM NM
95.844/15/2008MW-2R
Groundwater
Elevation** (ft)
95.53
96.53
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)
Well destroyed during construction activities in 2005
Well ID Date Installed
96.69
97.69
Well destroyed during construction activities in 2005
11/10/1997MW-1
12/11/1997MW-2
Page 1 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
4/2/1998 0 7.84 88.1
5/5/1998 NM NM NM
7/29/1998 0 11.5 84.44
3/15/2000 0 11.36 84.58
12/10/2001 0 16.19 79.75
5/14/2002 0 14.88 81.06
8/29/2002 0 17.46 78.48
11/11/2002 0 14.43 81.51
2/26/2003 0 12.11 83.83
5/15/2003 0 10.02 85.92
8/14/2003 0 7.76 88.18
11/5/2003 0 10.46 85.48
5/5/2004 0 12.08 83.86
11/18/2004 0 12.22 83.72
10/4/2021 0 12.88 86.62
11/8/2022
4/2/1998 3.37 12.91 86.18
5/5/1998 2.6 12.77 85.76
7/29/1998 1.09 14.89 82.54
3/15/2000 0.59 13.8 83.26
12/10/2001 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
11/11/2002 NM NM NM
2/26/2003 NM NM NM
5/28/2003 0.30 10.78 86.07
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 17.03 79.6
11/18/2004 NM NM NM
4/2/1998 0 9.13 87.71
5/5/1998 NM NM NM
7/29/1998 0 12.15 84.69
3/15/2000 0 12.23 84.61
12/10/2001 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
11/11/2002 NM NM NM
2/26/2003 NM NM NM
99.5VE-3 3/23/1999
Well destroyed during construction activities in 2005
MW-4 12/11/1997
Well could not be located - not measured
96.63
Well destroyed during construction activities in 2005
12/11/1997MW-3 95.94
96.8412/11/1997MW-5
Page 2 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
5/28/2003 0.01 8.55 88.3
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 14.15 82.69
11/18/2004 NM NM NM
4/2/1998 2.9 14.32 84.49
5/5/1998 2.71 14.63 84.04
7/29/1998 1.41 16.82 80.9
3/15/2000 2.05 16.97 81.22
12/10/2001 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
11/11/2002 NM NM NM
2/26/2003 NM NM NM
5/28/2003 0 11.84 84.85
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 16.92 79.77
11/18/2004 NM NM NM
4/29/2008 0 14.85 81.56
4/21/2009 0 13.3 83.11
4/27/2010 0 12.61 83.8
4/18/2011 0 14.46 81.95
4/10/2012 0 14.51 81.9
4/16/2013 0 13.73 82.68
4/28/2014 0 11.23 85.18
4/10/2015 0 13.21 83.2
1/6/2016 0 11.41 85
8/21/2019 0 12.73 83.68
1/15/2021 0 9.93 86.48
10/4/2021 0 13.25 83.16
11/8/2022 0 16.04 80.37
4/2/1998 0 9.39 87.29
5/5/1998 NM NM NM
7/29/1998 NM NM NM
3/15/2000 0.58 12.93 84.17
12/10/2001 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
96.69
Well destroyed during construction activities in 2005
MW-6 12/11/1997
Well destroyed during construction activities in 2005
96.41MW-6R 4/15/2008
MW-7 1/9/1998 96.68
MW-5 12/11/1997 96.84
Page 3 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
11/11/2002 NM NM NM
2/26/2003 NM NM NM
5/28/2003 0 9.3 87.38
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 16.85 79.83
11/18/2004 NM NM NM
4/2/1998 0.03 11.37 85.74
5/5/1998 0.02 12.06 85.04
7/29/1998 0.24 15.3 81.97
3/15/2000 0.57 14.55 82.96
12/10/2001 NM NM NM
5/14/2002 NM NM NM
8/29/2002 NM NM NM
11/11/2002 NM NM NM
2/26/2003 NM NM NM
5/28/2003 0.02 11.42 85.68
8/14/2003 NM NM NM
11/5/2003 NM NM NM
5/5/2004 0 21.29 75.8
11/18/2004 NM NM NM
5/5/1998 0.56 11.11 82.63
7/29/1998 1.25 14.76 79.48
3/15/2000 NM NM NM
12/10/2001 NM NM NM
5/14/2002 0.02 14.1 79.24
8/29/2002 DRY DRY DRY
11/11/2002 0 16.13 77.2
2/26/2003 0 13.74 79.59
5/15/2003 0 11.94 81.39
8/14/2003 0 13.1 80.23
11/5/2003 0 12.59 80.74
5/5/2004 0 14.03 79.3
11/18/2004 0 14.07 79.26
7/29/1998 0 11.99 81.39
3/15/2000 0 11.02 82.36
12/10/2001 0 15.82 77.56
5/14/2002 0 15.66 77.72
8/29/2002 DRY DRY DRY
97.09
Well destroyed during construction activities in 2005
4/29/1998MW-9 93.33
Well destroyed during construction activities in 2005
Well destroyed during construction activities in 2005
MW-8 1/9/1998
MW-7 1/9/1998 96.68
4/29/1998MW-10 93.38
Page 4 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
11/11/2002 DRY DRY DRY
2/26/2003 0 13.74 79.64
5/15/2003 0 10.04 83.34
8/15/2003 0 12.81 80.57
11/5/2003 0 10.89 82.49
5/5/2004 0 14.24 79.14
11/18/2004 0 12.35 81.03
4/29/2008 0 13.81 81.3
4/21/2009 0 12.22 82.89
4/27/2010 0 12.12 82.99
4/18/2011 0 13.27 81.84
4/10/2012 0 13.63 81.48
4/16/2013 0 12.92 82.19
4/28/2014 0 10.71 84.4
4/9/2015 0 12.9 82.21
1/6/2016 0 10.85 84.26
8/21/2019 0 13.1 82.01
1/15/2021 0 10.49 84.62
10/4/2021 0 13.45 81.66
11/8/2022
7/29/1998 0 14 83.07
3/15/2000 0 13.58 83.49
12/10/2001 0 18.35 78.72
5/14/2002 NM NM NM
8/29/2002 0 19.67 77.4
11/11/2002 0 17.57 79.5
2/26/2003 0 15.3 81.77
5/15/2003 0 12.36 84.71
8/14/2003 0 12.71 84.36
11/5/2003 0 12.83 84.24
5/5/2004 0 14.68 82.39
11/18/2004 0 14.43 82.64
7/29/1998 0 14.01 82.97
3/15/2000 0 13.56 83.42
12/10/2001 0 18.04 78.94
5/14/2002 0 17.82 79.16
8/29/2002 DRY DRY DRY
11/11/2002 DRY DRY DRY
2/26/2003 DRY DRY DRY
Well destroyed during construction activities in 2005
MW-10R 4/15/2008
95.11
Well is capped - not measured
Well destroyed during construction activities in 2005
MW-11D 4/29&30/1998 97.07
4/29/1998MW-10 93.38
96.984/29/1998MW-12
Page 5 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
5/15/2003 0 11.85 85.13
8/14/2003 0 17.3 79.68
11/5/2003 0 12.64 84.34
5/5/2004 0 15.25 81.73
11/18/2004 0 15.91 81.07
7/29/1998 0 13.53 81.95
3/15/2000 0 12.72 82.76
12/10/2001 0 17.27 78.21
5/14/2002 0 16.19 79.29
8/29/2002 DRY DRY DRY
11/11/2002 0 15.7 79.78
2/26/2003 0 13.43 82.05
5/15/2003 0 11.59 83.89
8/14/2003 0 11 84.48
11/5/2003 0 12.13 83.35
5/5/2004 0 13.67 81.81
11/18/2004 0 13.52 81.96
4/29/2008 0 12.4 83.48
4/21/2009 0 11.81 84.07
4/27/2010 0 11.85 84.03
4/18/2011 0 12.95 82.93
4/10/2012 0 13.39 82.49
4/16/2013 0 12.68 83.2
4/28/2014 0 10.43 85.45
4/10/2015 0 12.86 83.02
1/6/2016 0 10.6 85.28
11/8/2022 NM NM NM
7/29/1998 0 12.19 84.45
3/15/2000 0 12.12 84.52
12/10/2001 0 17.05 79.59
5/14/2002 0 15.62 81.02
8/29/2002 DRY DRY DRY
11/11/2002 0 14.94 81.7
2/26/2003 0 12.59 84.05
5/15/2003 0 10.63 86.01
8/14/2003 0 9.15 87.49
11/5/2003 0 11.03 85.61
5/5/2004 0 12.77 83.87
11/18/2004 0 12.35 84.29
Well destroyed during construction activities in 2005
MW-12 4/29/1998 96.98
95.884/15/2008MW-13R
MW-14 4/29/1998 96.64
Well destroyed during construction activities in 2005
MW-13 4/29/1998 95.48
Page 6 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
7/29/1998 0 11.48 77.34
3/15/2000 0 9.6 79.22
12/10/2001 1.49 14.9 75.01
5/14/2002 0.11 12.6 76.3
8/29/2002 0.95 16.16 73.35
11/11/2002 0.05 11.47 77.39
2/26/2003 0 9.04 79.78
5/15/2003 0 8.79 80.03
8/14/2003 0 12.09 76.73
11/5/2003 0 9.55 79.27
5/5/2004 0 10.77 78.05
11/18/2004 0 13.32 75.5
4/29/2008 0 8.84 79.98
4/21/2009 0 8.43 80.39
4/27/2010 0 9.11 79.71
4/18/2011 0 9.64 79.18
4/10/2012 0 10.05 78.77
4/16/2013 0 9.5 79.32
4/28/2014 0 7.48 81.34
4/9/2015 0 9.41 79.41
1/6/2016 0 7.88 80.94
8/21/2019 0 10.93 77.89
1/15/2021 0 7.02 81.8
10/4/2021 0 10.62 78.2
11/8/2022 0 14.91 73.91
7/29/1998 0 9.78 77.27
3/15/2000 0 8.76 78.29
12/10/2001 0 12.28 74.77
5/14/2002 0 10.83 76.22
8/29/2002 0 14.33 72.72
11/11/2002 0 9.94 77.11
2/26/2003 0 7.44 79.61
5/15/2003 0 7.01 80.04
8/14/2003 0 6.51 80.54
11/5/2003 0 7.99 79.06
5/5/2004 0 7.73 79.24
11/18/2004 0 8.14 78.83
4/29/2008 0 4.71 82.26
4/21/2009 0 2.71 84.26
4/27/2010 0 5.39 81.58
87.05
MW-15 7/27/1998
88.82
86.97
7/27/1998MW-16
Well destroyed during construction activities in 2005
Page 7 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
4/18/2011 0 3.77 83.2
4/10/2012 0 4.02 82.95
4/16/2013 0 3.91 83.06
4/28/2014 0 3.87 83.1
4/9/2015 0 5.39 81.58
1/6/2016 0 2.14 84.83
8/21/2019 0 9.18 77.79
1/15/2021 0 1.92 85.05
10/4/2021 0 8.91 78.06
11/8/2022
7/29/1998 0 13.86 77.97
3/15/2000 0.33 12.57 79.5
12/10/2001 NM NM NM
5/14/2002 0.02 12.62 79.22
8/29/2002 DRY DRY DRY
11/11/2002 0 15.21 76.62
2/26/2003 0 13.1 78.73
5/15/2003 0 11.76 80.07
8/15/2003 0 12.72 79.11
11/5/2003 0 12.42 79.41
5/5/2004 0 13.31 78.52
11/18/2004 0 13.53 78.3
3/15/2000 0 10.68 84.88
12/10/2001 0 15.69 79.87
5/14/2002 0 14.33 81.23
8/29/2002 0 17.1 78.46
11/11/2002 0 13.45 82.11
2/26/2003 0 11.28 84.28
5/15/2003 0 9.05 86.51
8/14/2003 0 7.53 88.03
11/5/2003 0 9.56 86
5/5/2004 0 11.28 84.28
11/18/2004 0 11.06 84.5
4/29/2008 0 11.73 83.83
4/21/2009 0 10.23 85.33
4/27/2010 0 9.6 85.96
4/18/2011 0 11.22 84.34
4/10/2012 0 11.6 83.96
4/16/2013 0 10.83 84.73
4/28/2014 0 8.05 87.51
Well could not be located - not measured
Well destroyed during construction activities in 2005
91.837/27/1998MW-17
MW-16 7/27/1998
86.97
MW-18 8/21/1998 95.56
Page 8 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
4/10/2015 0 10.81 84.75
1/6/2016 0 8.52 87.04
11/8/2022 NS NS NS
3/15/2000 0 11.11 78.99
12/10/2001 0 15.06 75.04
5/14/2002 0 13.76 76.34
8/29/2002 0 16.85 73.25
11/11/2002 0 12.98 77.12
2/26/2003 0 10.84 79.26
5/15/2003 0 10.17 79.93
8/14/2003 0 10.19 79.91
11/5/2003 0 10.99 79.11
5/5/2004 0 11.82 78.28
11/18/2004 0 11.77 78.33
4/29/2008 0 11.31 78.79
4/21/2009 0 10.31 79.79
4/27/2010 0 10.61 79.49
4/18/2011 0 11.34 78.76
4/10/2012 0 11.57 78.53
4/16/2013 0 11.02 79.08
4/28/2014 0.28 9.61 80.69
1/6/2016 0 9.73 80.37
8/21/2019 0 12.04 78.06
1/15/2021 0 8.8 81.3
10/4/2021 0 11.82 78.28
11/8/2022 0.02 13.63 76.48
4/4/2003 0 5.94 80.08
5/15/2003 0 6.7 79.32
8/14/2003 0 6.15 79.87
11/5/2003 0 7.32 78.7
5/5/2004 0 8.05 77.97
11/18/2004 0 7.91 78.11
4/4/2003 0 9.21 80.1
5/15/2003 0 9.82 79.49
8/14/2003 0 9.36 79.95
11/5/2003 0 10.39 78.92
5/5/2004 0 11.1 78.21
11/18/2004 0 11.02 78.29
MW-19 3/9/2000
90.1
Well covered by concrete slab
86.023/31/2003MW-20
89.314/1/2003MW-21
8/21/1998MW-18 95.56
Page 9 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
4/29/2008 0.08 10.79 78.58
4/21/2009
4/27/2010 0.02 10.36 78.96
4/18/2011 0.47 10.81 78.84
4/10/2012 0.07 11.06 78.3
4/16/2013 0.04 10.63 78.71
4/29/2014 0 9.03 80.28
4/9/2015 0 10.85 78.46
1/6/2016 0 9.2 80.11
8/21/2019 0 11.58 77.73
1/15/2021 0 8.33 80.98
10/4/2021 0 11.31 78
11/8/2022 0 13.07 76.24
4/4/2003 0 7.38 82.28
5/15/2003 0 8.53 81.13
8/14/2003 0 7.83 81.83
11/5/2003 0 9.07 80.59
5/5/2004 0 10.38 79.28
11/18/2004 0 10 79.66
4/29/2008 0 6.51 83.15
4/21/2009 0 8.46 81.2
4/27/2010 0 8.84 80.82
4/18/2011 0 9.41 80.25
4/10/2012 0 9.91 79.75
4/16/2013 0 9.29 80.37
4/28/2014 0 7.14 82.52
4/9/2015 0 9.48 80.18
1/6/2016 0 7.09 82.57
11/8/2022 NM NM NM
4/4/2003 0 6.04 79.93
5/15/2003 0 7.06 78.91
8/14/2003 0 6.05 79.92
11/5/2003 0 7.86 78.11
5/5/2004 0 8.24 77.73
11/18/2004 0 8.28 77.69
4/29/2008 0.18 8.48 77.62
4/21/2009
4/27/2010 0 7.49 78.48
4/18/2011 0 8.31 77.66
4/10/2012 0.65 8.79 77.65
Free Product Absorbent Socks Currently in Well
89.664/1/2003MW-22
Free Product Absorbent Socks Currently in Well
MW-21 4/1/2003
89.31
85.974/1/2003MW-23
Page 10 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
4/16/2013 0 7.81 78.16
4/28/2014 0 6.21 79.76
4/9/2015 0 8.1 77.87
1/6/2016 0 6.67 79.3
8/21/2019 0 9.21 76.76
1/15/2021 0 6.35 79.62
10/4/2021 0 8.81 77.16
11/8/2022 0 10.66 75.31
4/4/2003 0 7.63 79.89
5/15/2003 0 8.24 79.28
8/14/2003 0 7.49 80.03
11/5/2003 0 8.86 78.66
5/5/2004 0 9.47 78.05
11/18/2004 0 9.37 78.15
4/29/2008 0.19 9.29 78.37
4/21/2009
4/27/2010 0 8.64 78.88
4/18/2011 0 9.2 78.32
4/10/2012 0.36 9.69 78.09
4/16/2013 0 9.01 78.51
4/28/2014 0 7.41 80.11
4/9/2015 0 9.26 78.26
1/6/2016 0 7.67 79.85
8/21/2019 0 9.95 77.57
1/15/2021 0 6.79 80.73
10/4/2021 0 9.64 77.88
11/8/2022
5/5/2004 0 8.45 76.7
11/18/2004 0 8.13 77.02
4/30/2008 0 4.11 81.04
4/21/2009 0 7.13 78.02
4/27/2010 0 7.87 77.28
4/18/2011 0 8.32 76.83
4/10/2012 0 8.57 76.58
4/16/2013 0 8.12 77.03
4/29/2014 0 6.7 78.45
4/9/2015 0 8.4 76.75
1/6/2016 0 6.67 78.48
8/21/2019 0 9.49 75.66
1/15/2021 0 6.12 79.03
Well could not be located - not measured
4/2/2003MW-24
Free Product Absorbent Socks Currently in Well
87.52
MW-23 4/1/2003
85.97
MW-25 3/6/2004 85.15
Page 11 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
10/4/2021 0 9.34 75.81
11/8/2022
5/5/2004 0 3.2 75.36
11/18/2004 0 3.15 75.41
4/30/2008 0 2.84 75.72
4/21/2009 0 2.4 76.16
4/27/2010 0 3 75.56
4/18/2011 0 3.18 75.38
4/10/2012 0 3.37 75.19
4/16/2013 0 3.14 75.42
4/29/2014 0 2.2 76.36
4/9/2015 0 3.38 75.18
1/6/2016 0 2.16 76.4
8/21/2019 0 4.11 74.45
1/15/2021 0 1.53 77.03
10/4/2021 0 3.94 74.62
11/8/2022
5/5/2004 0 9.83 78.05
11/18/2004 0 9.75 78.13
4/30/2008 0 9.47 78.41
4/22/2009 0 8.63 79.25
4/27/2010 0 8.94 78.94
4/18/2011 0 9.56 78.32
4/10/2012 0 9.81 78.08
4/16/2013 0 9.36 78.53
4/29/2014 0 7.82 80.07
4/9/2015 0 9.61 78.28
1/6/2016 0 8.01 79.88
8/22/2019 0 10.34 77.55
5/5/2004 0 11.52 77.09
11/18/2004 0 11.47 77.14
4/30/2008 0 11.11 77.5
4/21/2009 0 10.2 78.41
4/27/2010 0 10.73 77.88
4/18/2011 0 11.33 77.28
4/10/2012 0 11.56 77.05
4/16/2013 0 11.11 77.5
4/28/2014 0 9.5 79.11
4/9/2015 0 11.36 77.25
MW-28 4/2/2004
Well could not be located - not measured
88.61
Monitoring well no longer accessible/property owner denied access
MW-27 4/2/2004
78.56
Well could not be located - not measured
3/6/2004MW-26
MW-25 3/6/2004
85.15
87.88
87.89
Page 12 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
1/6/2016 0 9.67 78.94
11/8/2022 NM NM NM
4/21/2009 0 12.54 79.93
4/27/2010 0 12.97 79.5
4/18/2011 0 13.68 78.79
4/10/2012 0 13.86 78.61
4/16/2013 0 13.4 79.07
4/28/2014 0 11.75 80.72
4/9/2015 0 13.61 78.86
1/6/2016 0 12.03 80.44
8/21/2019 0 14.34 78.13
1/15/2021 0 11.11 81.36
10/4/2021 0 14.09 78.38
11/8/2022
4/27/2010 0 11.14 79.09
4/18/2011 0 11.71 78.52
4/10/2012 0 11.91 78.32
4/16/2013 0 11.49 78.74
4/29/2014 0 9.94 80.29
4/9/2015 0 11.72 78.51
1/6/2016 0 10.13 80.1
8/21/2019 0 12.44 77.79
1/15/2021 0 9.29 80.94
10/4/2021 0 12.21 78.02
11/8/2022 0 13.98 76.25
8/21/2019 0 13.61 82.78
1/15/2021 0 12.03 84.36
10/4/2021 0 15.14 81.25
11/8/2022
12/10/2001 0 6 73.02
5/14/2002 0 5.01 74.01
8/29/2002 0 7.34 71.68
11/11/2002 0 4.51 74.51
2/26/2003 0 3.25 75.77
5/15/2003 0 3.43 75.59
8/15/2003 0 2.69 76.33
11/5/2003 0 3.62 75.4
5/5/2004 0 3.66 75.36
Depth to Water and LNAPL Thickness not determined***
Depth to Water and LNAPL Thickness not determined***
90.23MW-30 4/27/2010
92.474/16/2009MW-29
MW-31 2/6/2018
96.39
88.614/20/2004
MWWB-1 12/18/2001 79.02
MW-28
Page 13 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
11/18/2004 0 3.86 75.16
4/29/2008 0 3.83 75.19
4/21/2009 0 3.46 75.56
4/27/2010 0 4.02 75
4/18/2011 0 4.11 74.91
4/11/2012 0 4.35 74.67
4/16/2013 0 4.06 74.96
4/29/2014 0 3.46 75.56
4/9/2015 0 4.34 74.68
1/7/2016 0 3.96 75.06
8/22/2019 0 4.63 74.39
1/15/2021 0 3.31 75.71
10/4/2021 0 4.49 74.53
11/8/2022 0 5.45 73.57
12/10/2001 0 10.41 74.66
5/14/2002 0 9.31 75.76
8/29/2002 0 11.83 73.24
11/11/2002 0 8.64 76.43
2/26/2003 0 6.64 78.43
5/15/2003 0 6.64 78.43
8/15/2003 0 5.88 79.19
11/5/2003 0 7.04 78.03
5/5/2004 0 7.28 77.79
11/18/2004 0 7.37 77.7
4/29/2008 0 7.09 77.98
4/22/2009 0 6.62 78.45
4/27/2010 0 7.21 77.86
4/18/2011 0 7.69 77.38
4/10/2012 0 7.59 77.48
4/16/2013 0 7.3 77.77
4/29/2014 0 6.07 79
4/9/2015 0 7.51 77.56
1/7/2016 0 6.02 79.05
8/21/2019 0 8.19 76.88
1/15/2021 0 5.54 79.53
10/4/2021 0 7.99 77.08
11/8/2022 0 9.45 75.62
12/10/2001 0 9.97 73.32
5/14/2002 0 8.81 74.48MWWB-3 12/18/2001 83.29
85.07MWWB-2 12/18/2001
79.0212/18/2001MWWB-1
Page 14 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
8/29/2002 0 11.33 71.96
11/11/2002 0 8.17 75.12
2/26/2003 0 6.48 76.81
5/15/2003 0 6.51 76.78
8/15/2003 0 5.67 77.62
11/5/2003 0 7 76.29
5/5/2004 0 7.46 75.83
11/18/2004 0 7.31 75.98
4/29/2008 0 7.03 76.26
4/22/2009 0 6.71 76.58
4/27/2010 0 7.07 76.22
4/18/2011 0 7.44 75.85
4/10/2012 0 7.56 75.73
4/16/2013 0 7.26 76.03
4/29/2014 0 6.21 77.08
4/9/2015 0 7.53 75.76
1/6/2016 0 6.27 77.02
8/21/2019 0 8.16 75.13
1/15/2021 0 6.68 76.61
10/4/2021 0 7.96 75.33
11/8/2022 0 9.22 74.07
12/10/2001 0 10.63 73.64
5/14/2002 0 9.29 74.98
8/29/2002 0 12.41 71.86
11/11/2002 0 8.7 75.57
2/26/2003 0 6.7 77.57
5/15/2003 0 6.65 77.62
8/15/2003 0 5.76 78.51
11/5/2003 0 7.27 77
5/5/2004 0 7.93 76.34
11/18/2004 0 7.55 76.72
4/29/2008 0 6.96 77.31
4/22/2009 0 6.61 77.66
4/27/2010 0 7.08 77.19
4/18/2011 0 7.42 76.85
4/10/2012 0 7.76 76.51
4/16/2013 0 7.27 77
4/29/2014 0 5.91 78.36
4/9/2015 0 7.55 76.72
1/6/2016 0 6.08 78.19
12/18/2001MWWB-4 84.27
MWWB-3 12/18/2001
83.29
Page 15 of 16
Table 4
Historical LNAPL Thickness and Groundwater Elevation Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Groundwater
Elevation** (ft)
Date Water
Level Measured
Top of Casing
Elevation*
LNAPL
Thickness (ft)
Depth to Water
from TOC (ft)Well ID Date Installed
11/8/2022 84.27 NM NM NM
TOC = Top of well casing
ft = Feet
***Water not detected by oil/water interface probe
Historical Free Product Thickness and Groundwater Elevation Data were obtained from the December 7, 2021 Groundwater
Monitoring Report. November 8, 2022 elevation data was colleccted by AECOM.
All elevations based on relative elevation to SW concrete pedestal of the Wilco sign - Assumed datum 100.00 feet
NM = Elevation not surveyed
**Groundwater elevation adjusted for free product
LNAPL = Light Non-Aqueous Phase Liquid
Notes:
*Top of casing elevation based on assumed datum
MW-16 manhole was replaced and re-surveyed in May 2004
12/18/2001MWWB-4
Page 16 of 16
Table 5
November 2022 Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
1 600 600 500 70 70 70 70 20 6 70 400 400
5,000 260,000 84,500 85,500 6,900 8,500 70,000 25,000 20,000 6,000 30,000 28,500 25,000
MW-6R 11/8/22 6.5 ND 407 723 50.7 ND ND 81.9 12.7 558 190 1,030 58.6
MW-15 11/8/22 2,230 ND 581 313 ND ND 229 ND 16,500 259 144 280 107
MW-21 11/8/22 14,200 3,170 2,140 7,770 97.6 ND 120 102 79.7 621 285 1,980 562
MW-23 11/8/22 1,350 301.0 2,300 1,143.1 107 ND ND 131 ND 738 356 1,030 160
MW-30 11/8/22 2,360 103 311 198.2 21.0 ND 98.7 20.1 507 118 48.2 167 41.8
MWWB-1 11/8/22 147 10.8 71.3 77.3 ND ND ND 3.5 ND 10.9 7.5 32.3 1.4
MWWB-2 11/8/22 ND ND 1.6 ND ND 0.53 0.71 1.6 0.77 ND 1.9 ND ND
MWWB-3 11/8/22 97.4 7.1 78.3 16.8 12.4 ND 18.0 18.2 32.5 28.3 45.5 20.2 5.4
Notes:
DIPE
GCL = North Carolina Gross Contaminant Levels
Isopropylbenzene
(Cumene)MTBE Naphthalene n-
Propylbenzene
1,2,4-
Trimethylbenzene
1,3,5-
Trimethylbenzene
Well ID Date
Sampled
Constituents of Concern
Benzene Toluene Ethylbenzene
Total
Xylenes
n-
Butylbenzene
sec-
Butylbenzene
2L Standard (µg/L)
GCL (µg/L)
Analytical Method: SM 6200B
µg/L = micrograms per liter
2L Standard = 15A NCAC 02L .0202 Groundwater Standard
Bold = values exceed 2L Standard
Red = values exceed GCL
ND = Not detected at or above laboratory reporting limit
MTBE = Methyl tert-butyl ether
DIPE = Diisopropyl ether
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
4/2/98 FP FP FP FP FP FP FP FP FP FP
5/5/98 FP FP FP FP FP FP FP FP FP FP
7/29/98 FP FP FP FP FP FP FP FP FP FP
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 NS NS NS NS NS NS NS NS NS NS
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
4/2/98 ND ND ND ND ND ND NR NR NR ND
5/5/98 NS NS NS NS NS NS NS NS NS NS
7/29/98 ND ND ND ND ND ND ND ND ND ND
3/15/00 ND ND ND ND ND ND NR NR NR NR
12/11/01 ND ND ND ND ND ND ND ND ND ND
5/14/02 ND ND ND ND ND ND ND ND ND ND
8/29/02 ND ND ND ND ND ND ND ND ND 14.6
11/11/02 ND ND ND ND ND ND ND ND ND ND
2/26/03 ND ND ND ND ND ND ND ND ND 5.0
5/15/03 ND ND ND ND ND ND ND ND ND ND
8/14/03 ND ND ND ND ND ND NR NR NR NR
11/5/03 ND ND ND ND ND ND NR NR NR NR
5/5/04 ND ND ND ND ND ND NR NR NR NR
11/18/04 ND ND ND ND ND ND NR NR NR NR
4/30/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 ND ND ND ND ND ND NR NR NR NR
4/27/10 ND ND ND ND ND ND NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 ND ND ND ND 0.483J ND NR NR NR NR
4/16/13 ND ND ND ND 2.5J ND NR NR NR NR
4/28/14 ND ND ND ND ND ND NR NR NR NR
4/9/15 ND 102.0 ND ND 4.0 1.6 NR NR NR NR
1/6/16 ND ND ND ND ND ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
4/2/98 6.3 ND ND ND 37.0 16.0 NR NR NR ND
5/5/98 NS NS NS NS NS NS NS NS NS NS
7/29/98 20.0 2.5 4.5 5.1 52.0 25.0 200.0 202.0 61.0 ND
3/15/00 160.0 31.0 57.0 89.0 59.0 36.0 NR NR NR NR
12/11/01 270.0 8.0 46.0 37.0 220.0 83.0 1,200.0 190.0 ND 24.4
5/14/02 4.0 ND 3.0 ND 2.0 1.0 120.0 ND ND 31.9
8/29/02 15.0 1.0 15.0 8.0 17.0 12.0 ND ND ND 587.0
11/11/02 1.0 1.0 2.0 ND 10.0 4.0 ND ND ND 12.2
2/26/03 1.3 320.0 5.5 8.9 9.4 10.0 300.0 ND ND 17.0
5/15/03 ND 870.0 ND ND ND ND 1,100.0 450.0 ND 134.0
8/14/03 ND 51.0 ND ND ND ND NR NR NR NR
11/5/03 0.25J 6.7 0.68J ND 16.0 8.0 NR NR NR NR
5/5/04 0.487J ND ND ND 35.9 22.3 NR NR NR NR
11/18/04 ND 1,090.0 ND ND 62J ND NR NR NR NR
4/30/08 8.3 1.3 9.3 39.5 ND ND NR NR NR NR
4/21/09 19.9 4.9 24.3 77.7 ND ND NR NR NR NR
4/27/10 24.4 3.6 53.3 108.5 32.9 5.6 NR NR NR NR
4/18/11
4/10/12 47.6 69.3 616.0 2,740.0 1,240.0 53.0 NR NR NR NR
4/16/13 65.0 59.0 890.0 3,700.0 2,200.0 25J NR NR NR NR
4/28/14 49.0 85.0 1,700.0 6,800.0 280 L ND NR NR NR NR
4/9/15 53 J 100 J 1,200.0 5,000.0 ND (<37)ND NR NR NR NR
1/6/16 19.7 J 32.4 J 439.0 1,903.0 129.0 ND NR NR NR NR
8/21/19 ND 121.0 1,120.0 5,100.0 ND ND NR NR NR NR
1/15/21 14.1 J 464.0 3,350.0 15,690.0 248.0 ND NR NR NR NR
10/4/21 30.7 J 384.0 2,880.0 11,940.0 1,060.0 ND NR NR NR NR
11/8/22
4/2/98 FP FP FP FP FP FP FP FP FP FP
5/5/98 FP FP FP FP FP FP FP FP FP FP
7/29/98 FP FP FP FP FP FP FP FP FP FP
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
C5-C8 Aliphatics C9-C12
Aliphatics
C9-C10
Aromatics LeadContaminant of Concern
GCL (µg/L)
Benzene Toluene Ethylbenzene Total Xylenes MTBE DIPE
Well destroyed during construction activities
MW-3
Well destroyed during construction activities
2L Standard (µg/L)
Well destroyed during construction activities
MW-2
MW-1
MW-2R
VE-3
Well could not be located - no sample collected
MW-4
Well could not be located - no sample collected
Page 1 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
8/29/02 NS NS NS NS NS NS NS NS NS NS
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
4/2/98 2,100.0 1,400.0 330.0 2,000.0 900.0 380.0 NR NR NR ND
5/5/98 NS NS NS NS NS NS NS NS NS NS
7/29/98 2,200.0 530.0 150.0 820.0 790.0 260.0 9,600.0 9,050.0 2,880.0 5.3
3/15/00 2,000.0 1,300.0 240.0 1,720.0 690.0 93.0 NR NR NR NR
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 NS NS NS NS NS NS NS NS NS NS
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
4/2/98 FP FP FP FP FP FP FP FP FP FP
5/5/98 FP FP FP FP FP FP FP FP FP FP
7/29/98 FP FP FP FP FP FP FP FP FP FP
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 NS NS NS NS NS NS NS NS NS NS
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
4/30/08 6,600.0 ND 848 J 9,380 J 50,000.0 650 J NR NR NR NR
4/21/09 6,440.0 ND ND 5,170 J 42,900.0 ND NR NR NR NR
4/27/10 5,540.0 ND 1,330.0 7640J 29,800.0 ND NR NR NR NR
4/18/11 5,210.0 ND 424.0 3599J 16,700.0 360J NR NR NR NR
4/10/12 3,450.0 ND 390.0 3,765J 10,200.0 157 J NR NR NR NR
4/16/13 1,800.0 66.0 540.0 4,700.0 7,700.0 56 J NR NR NR NR
4/28/14 620.0 ND 750.0 6,000.0 2,300.0 ND NR NR NR NR
4/10/15 140.0 56 J 430.0 2,800.0 890.0 ND NR NR NR NR
1/6/16 51.9 48.9 449.0 2,868 J 294.0 12.0 NR NR NR NR
8/21/19 4.96J 11.5 407.0 1,278.0 ND ND NR NR NR NR
1/15/21 2.41 J ND 404.0 1,132.0 ND ND NR NR NR NR
10/4/21 2.87 J ND 570.0 1,419.01 J ND ND NR NR NR NR
11/8/22 6.5 ND 407.0 723.0 12.7 ND NR NR NR NR
4/2/98 3,700.0 13,000.0 840.0 4,300.0 18,000.0 270.0 NR NR NR ND
5/5/98 NS NS NS NS NS NS NS NS NS NS
7/29/98 14,000.0 19,000.0 1,900.0 11,000.0 94,000.0 1,300.0 109,000.0 26,300.0 8,810.0 ND
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 NS NS NS NS NS NS NS NS NS NS
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
4/2/98 FP FP FP FP FP FP FP FP FP FP
5/5/98 FP FP FP FP FP FP FP FP FP FP
7/29/98 FP FP FP FP FP FP FP FP FP FP
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 NS NS NS NS NS NS NS NS NS NS
Total Xylenes MTBE
Well destroyed during construction activities
MW-7
Well destroyed during construction activities
MW-6
MW-6R
GCL (µg/L)
Benzene Toluene Ethylbenzene
MW-4
MW-8
DIPE C5-C8 Aliphatics
C9-C12
Aliphatics
C9-C10
Aromatics Lead
2L Standard (µg/L)
Well destroyed during construction activities
MW-5
Well destroyed during construction activities
Contaminant of Concern
Page 2 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
11/11/02 NS NS NS NS NS NS NS NS NS NS
2/26/03 NS NS NS NS NS NS NS NS NS NS
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 NS NS NS NS NS NS NS NS NS NS
11/5/03 NS NS NS NS NS NS NS NS NS NS
5/5/04 NS NS NS NS NS NS NS NS NS NS
11/18/04 NS NS NS NS NS NS NS NS NS NS
5/5/98 FP FP FP FP FP FP FP FP FP FP
7/29/98 FP FP FP FP FP FP FP FP FP FP
3/15/00 NS NS NS NS NS NS NS NS NS NS
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 FP FP FP FP FP FP FP FP FP FP
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 12,000.0 22,000.0 2,200.0 15,400.0 5,000.0 ND 41,000.0 29,000.0 ND 25.1
2/26/03 690.0 4,400.0 1,300.0 13,300.0 2,000.0 46.0 8,800.0 19,000.0 4,900.0 37.8
5/15/03 1,100.0 640.0 230.0 2,970.0 13,000.0 180.0 9,100.0 4,900.0 ND 5.6
8/14/03 790.0 430.0 140.0 3,700.0 3,300.0 69.0 NR NR NR NR
11/5/03 5,900.0 J 220 J 200 3,390.0 38,000.0 460J NR NR NR NR
5/5/04 4,000.0 J 262 596.0 3,662.0 23,200.0 465J NR NR NR NR
11/18/04 2,360.0 ND J 314 1,690.0 20,300.0 321J NR NR NR NR
5/5/98 ND ND ND ND 7.3 ND NR NR NR ND
7/29/98 ND ND ND ND 2.7 ND ND ND ND ND
3/15/00 ND ND ND ND ND ND NR NR NR NR
12/11/01 1.0 4.0 2.0 12.0 20.0 4.0 ND ND ND ND
5/14/02 ND ND ND ND 270.0 46.0 160.0 ND ND ND
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
2/26/03 13.0 160.0 400.0 620.0 ND ND 2,100.0 1,500.0 300.0 ND
5/16/03 10.0 33.0 250.0 204.0 ND ND 1,600.0 800.0 ND ND
8/15/03 5.1 10.0 87.0 36.0 ND ND NR NR NR NR
11/5/03 ND ND 5.6 ND 240.0 26.0 NR NR NR NR
5/5/04 J 0.936 ND ND J 1.06 236.0 34.9 NR NR NR NR
11/18/04 11.2 ND ND ND 393.0 27.9 NR NR NR NR
4/30/08 ND ND 0.449 J ND 16.5 0.801 J NR NR NR NR
4/21/09 ND ND 0.372 J 0.662 J 12.4 ND NR NR NR NR
4/27/10 ND ND ND ND 23.9 ND NR NR NR NR
4/18/11 ND ND ND ND 14.4 ND NR NR NR NR
4/10/12 ND ND ND ND 18.4 ND NR NR NR NR
4/16/13 ND ND ND ND 20.0 ND NR NR NR NR
4/28/14 ND ND ND ND 19.0 ND NR NR NR NR
4/9/15 ND ND ND ND 11.0 1.6 NR NR NR NR
8/21/19 ND ND ND ND 3.7 ND NR NR NR NR
1/15/21 ND ND ND ND 1.4 ND NR NR NR NR
10/4/21 ND ND ND ND 1.5 ND NR NR NR NR
11/8/22
5/5/98 8.2 20.0 2.7 14.0 ND ND NR NR NR 11.0
7/29/98 120.0 260.0 17.0 94.0 62.0 4.1 774.0 236.0 62.5 ND
3/15/00 ND ND ND ND ND ND NR NR NR NR
12/11/01 ND ND ND ND ND ND ND ND ND ND
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 ND ND ND ND ND ND ND ND ND ND
11/11/02 ND ND ND ND ND ND ND ND ND ND
2/26/03 ND ND ND ND ND ND ND ND ND ND
5/16/03 ND ND ND ND ND ND ND ND ND ND
8/14/03 ND ND ND ND ND ND NR NR NR NR
11/5/03 ND ND ND ND ND ND NR NR NR NR
5/5/04 ND ND ND ND ND ND NR NR NR NR
11/18/04 ND ND ND ND ND ND NR NR NR NR
5/5/98 16,000.0 15,000.0 2,500.0 9,500.0 ND 750.0 NR NR NR 0.19
7/29/98 14,000.0 14,000.0 2,200.0 8,500.0 ND 1,900.0 36,300.0 20,300.0 5,078.0 44.0
3/15/00 6,300.0 3,800.0 2,200.0 7,500.0 ND 1,300.0 NR NR NR NR
12/10/01 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
2/26/03 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
5/16/03 10.0 2.8 5.5 37.0 ND 13.0 320.0 450.0 120.0 5.9
8/14/03 3.8 2.8 10.0 32.0 ND 5.8 NR NR NR NR
11/5/03 10.0 4.8 10.0 41.0 ND 20.0 NR NR NR NR
5/5/04 5.4 J 0.572 2.9 19.0 0.465J 11.0 NR NR NR NR
MW-8
Benzene Toluene Ethylbenzene Total Xylenes
Well destroyed during construction activities
MW-10
MTBE DIPE C5-C8 Aliphatics
C9-C12
Aliphatics
C9-C10
Aromatics Lead
2L Standard (µg/L)
Contaminant of Concern
GCL (µg/L)
MW-10R
Well is capped - no cample collected
Well destroyed during construction activities
MW-11D
Well destroyed during construction activities
Well destroyed during construction activities
MW-9
MW-12
Page 3 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
11/18/04 J 0.925 J 0.373 ND J 1.43 ND 3.4 NR NR NR NR
5/5/98 ND ND ND ND ND ND NR NR NR ND
7/29/98 ND ND ND ND ND ND ND ND ND ND
3/15/00 ND ND ND ND ND ND NR NR NR NR
12/11/01 ND ND ND ND ND ND ND ND ND ND
5/14/02 ND ND ND ND ND ND ND ND ND ND
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 ND ND ND ND ND ND ND ND ND ND
2/26/03 ND ND ND ND ND ND ND ND ND ND
5/16/03 ND ND ND ND ND ND ND ND ND ND
8/14/03 ND ND ND ND ND ND NR NR NR NR
11/5/03 ND ND ND ND ND ND NR NR NR NR
5/5/04 ND ND ND ND ND ND NR NR NR NR
11/18/04 ND ND ND ND ND ND NR NR NR NR
4/30/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 ND ND ND ND ND ND NR NR NR NR
4/27/10 ND ND ND ND ND ND NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 ND ND ND ND ND ND NR NR NR NR
4/16/13 ND ND ND ND ND ND NR NR NR NR
4/28/14 ND ND 0.17 J ND ND ND NR NR NR NR
4/10/15 ND ND 0.50 J ND ND ND NR NR NR NR
1/6/16 ND ND ND ND ND ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
5/5/98 ND ND ND ND ND ND NR NR NR ND
7/29/98 ND ND ND ND 1.4 ND ND ND ND ND
3/15/00 ND ND ND ND ND ND NR NR NR NR
12/11/01 ND ND ND ND ND ND ND ND ND ND
5/14/02 ND ND ND ND ND ND ND ND ND ND
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 ND ND ND ND ND ND ND ND ND ND
2/26/03 ND ND ND ND ND ND ND ND ND ND
5/15/03 NS NS NS NS NS NS NS NS NS NS
8/14/03 ND ND ND ND 2.3 ND NR NR NR NR
11/5/03 ND ND ND ND J 1.2 ND NR NR NR NR
5/5/04 ND ND ND ND J 1.35 ND NR NR NR NR
11/18/04 ND ND ND ND 3.4 ND NR NR NR NR
4/2/98 NS NS NS NS NS NS NS NS NS NS
5/5/98 NS NS NS NS NS NS NS NS NS NS
7/29/98 1.5 1.0 1.5 11.9 ND 4.0 270.0 87.9 89.0 ND
3/15/00 3,900.0 13,000.0 2,300.0 13,400.0 ND ND NR NR NR NR
12/10/01 FP FP FP FP FP FP FP FP FP FP
5/14/02 FP FP FP FP FP FP FP FP FP FP
8/29/02 FP FP FP FP FP FP FP FP FP FP
11/11/02 FP FP FP FP FP FP FP FP FP FP
2/26/03 6,300.0 14,000.0 2,900.0 21,100.0 53.0 75.0 22,000.0 24,000.0 4,700.0 14.3
5/16/03 3,400.0 5,400.0 1,400.0 8,300.0 72.0 110.0 10,000.0 12,000.0 1,900.0 5.5
8/14/03 11,000.0 5,900.0 1,700.0 11,000.0 ND ND NR NR NR NR
11/5/03 4,500.0 2,000.0 780.0 4,900.0 ND J 50 NR NR NR NR
5/5/04 8,860.0 2,460.0 961.0 6,080.0 ND 207J NR NR NR NR
11/18/04 9,580.0 2,050.0 845.0 5,540.0 ND 554.0 NR NR NR NR
4/29/08 301.0 30.1 299.0 876.0 ND 30.0 NR NR NR NR
4/21/09 254.0 9.20 J 237.0 541.0 ND 27.4 NR NR NR NR
4/27/10 313.0 10.9 175.0 313.4 17.0 13.5 NR NR NR NR
4/18/11 395.0 26.7 384.0 810.0 ND ND NR NR NR NR
4/10/12 123.0 4.24J 160.0 314.4 ND ND NR NR NR NR
4/16/13 120.0 6.1 160.0 320.0 ND 3.2J NR NR NR NR
4/28/14 97.0 5.5 J 99.0 170.0 ND ND NR NR NR NR
4/9/15 83.0 7.4 130.0 190.0 ND 2.5 NR NR NR NR
1/6/16 29.3 ND 79.8 103.4 ND ND NR NR NR NR
8/21/19 3.1 1.5 33.5 41.7 ND ND NR NR NR NR
1/15/21 23.3 3.5 61.1 55.3 ND ND NR NR NR NR
10/4/21 3.02 J ND 29.4 25.37 J ND ND NR NR NR NR
11/8/22 2,230.0 ND 581.0 313.0 16,500.0 229.0 NR NR NR NR
7/29/98 ND ND ND ND ND ND ND ND ND ND
3/15/00 40.0 6.0 31.0 8.0 ND ND NR NR NR NR
12/11/01 ND ND 1.0 ND ND ND ND ND ND ND
5/14/02 ND ND ND ND ND ND ND ND ND ND
8/29/02 ND 12.0 7.0 47.0 ND ND ND ND ND 17.3
11/11/02 ND ND 2.0 7.0 ND ND ND ND ND 5.0
C9-C12
Aliphatics
C9-C10
AromaticsMTBE DIPE C5-C8 Aliphatics Lead
2L Standard (µg/L)
GCL (µg/L)
Contaminant of Concern Benzene Toluene Ethylbenzene Total Xylenes
MW-13R
Well destroyed during construction activities
MW-14
Well destroyed during construction activitiesMW-12
Well destroyed during construction activities
MW-13
MW-15
MW-16
Page 4 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
2/26/03 ND ND 1.7 ND ND ND ND ND ND ND
5/16/03 ND ND ND ND ND ND ND ND ND 13.2
8/14/03 ND ND ND ND ND ND NR NR NR NR
11/5/03 ND ND ND ND ND ND NR NR NR NR
5/5/04 ND ND ND ND ND ND NR NR NR NR
11/18/04 ND ND ND ND ND ND NR NR NR NR
4/29/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 ND ND ND ND ND ND NR NR NR NR
4/27/10 ND ND ND ND ND ND NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 ND ND ND ND ND ND NR NR NR NR
4/16/13 ND ND ND ND ND ND NR NR NR NR
4/28/14 ND ND ND ND ND ND NR NR NR NR
4/9/15 ND ND ND ND ND ND NR NR NR NR
1/6/16 ND 4.65 J ND ND ND ND NR NR NR NR
8/21/19 ND ND ND ND ND ND NR NR NR NR
1/15/21 ND ND ND ND ND ND NR NR NR NR
10/4/21 ND ND ND ND ND ND NR NR NR NR
11/8/22
7/29/98 27,000.0 15,000.0 2,100.0 8,400.0 67,000.0 4,300.0 120,000.0 30,500.0 7,160.0 17.0
3/15/00 FP FP FP FP FP FP FP FP FP FP
12/10/01 NS NS NS NS NS NS NS NS NS NS
5/14/02 NS NS NS NS NS NS NS NS NS NS
8/29/02 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
11/11/02 14,000.0 27,000.0 2,600.0 17,500.0 4,100.0 ND 68,000.0 47,000.0 6,800.0 15.8
2/26/03 3,200.0 11,000.0 1,800.0 13,900.0 4,400.0 190.0 18,000.0 22,000.0 4,400.0 9.6
5/15/03 250.0 1,300.0 460.0 4,200.0 470.0 ND 4,300.0 9,500.0 2,000.0 5.3
8/15/03 120.0 640.0 480.0 4,900.0 1,200.0 ND NR NR NR NR
11/5/03 560.0 720.0 360.0 4,000.0 12,000.0 160J NR NR NR NR
5/5/04 4,320.0 1,340.0 J 519 5,030.0 63,800.0 589J NR NR NR NR
11/18/04 6,180.0 988J ND 6,290.0 48,100.0 1,030J NR NR NR NR
8/21/98 570.0 2,500.0 490.0 2,870.0 ND ND 9,300.0 13,000.0 2,900.0 79.0
3/15/00 1,000.0 460.0 370.0 1,670.0 ND 54.0 NR NR NR NR
12/11/01 560.0 330.0 320.0 1,290.0 33.0 ND 3,900.0 1,900.0 460.0 78.1
5/14/02 16.0 7.0 2.0 29.0 14.0 8.0 480.0 120.0 ND ND
8/29/02 ND ND ND ND 8.0 4.0 ND ND ND 30.8
11/11/02 1.0 ND ND ND 12.0 3.0 ND ND ND 30.2
2/26/03 ND ND ND ND 15.0 3.3 ND ND ND 11.5
5/16/03 13.0 2.5 2.4 32.7 8.4 3.4 ND 150.0 ND ND
8/14/03 3.9 ND 1.3 5.5 19.0 4.2 NR NR NR NR
11/5/03 1.9 ND 1.2 ND 13.0 2.7 NR NR NR NR
5/5/04 ND ND ND ND 11.5 3.2 NR NR NR NR
11/18/04 ND ND ND ND 22.2 2.6 NR NR NR NR
4/29/08 ND ND ND ND 4.6 0.684 J NR NR NR NR
4/21/09 ND ND ND ND 6.0 0.595 J NR NR NR NR
4/27/10 ND ND ND ND 3.6 ND NR NR NR NR
4/18/11 ND ND ND ND 3.9 ND NR NR NR NR
4/10/12 ND ND ND ND 4.1 ND NR NR NR NR
4/16/13 ND ND ND ND 7.4 ND NR NR NR NR
4/28/14 ND ND ND ND 9.5 ND NR NR NR NR
4/10/15 ND ND ND ND 4.5 ND NR NR NR NR
1/6/16 ND ND ND ND 0.982 J ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
3/15/00 24,000.0 22,000.0 2,300.0 10,700.0 77,000.0 2,700.0 NR NR NR NR
12/11/01 30,000.0 25,000.0 3,700.0 16,600.0 68,000.0 2,800.0 ND ND ND ND
5/14/02 1,800.0 1,900.0 120.0 3,900.0 3,100.0 170.0 7,300.0 5,300.0 1,000.0 ND
8/29/02 5,000.0 1,400.0 530.0 2,950.0 8,800.0 750.0 11,000.0 950.0 ND ND
11/11/02 9,400.0 4,300.0 880.0 2,800.0 21,000.0 1,200.0 40,000.0 9,800.0 ND 7.0
2/26/03 15,000.0 8,100.0 730.0 5,400.0 33,000.0 1,600.0 50,000.0 9,800.0 1,400.0 7.2
5/16/03 7,700.0 6,400.0 630.0 4,400.0 17,000.0 720.0 33,000.0 23,000.0 ND ND
8/14/03 4,700.0 3,500.0 640.0 4,100.0 4,300.0 270.0 NR NR NR NR
11/5/03 8,800.0 4,900.0 810.0 4,400.0 13,000.0 830.0 NR NR NR NR
5/5/04 16,000.0 9,610.0 1,210.0 5,840.0 18,900.0 1,270.0 NR NR NR NR
11/18/04 19,000.0 8,430.0 1,270.0 5,460.0 49,600.0 1,710.0 NR NR NR NR
4/29/08 23,000.0 10,300.0 2,180.0 8,120 J 36,300.0 2,030.0 NR NR NR NR
4/21/09 18,400.0 10,900.0 1,860.0 7,910 J 23,100.0 1,480 J NR NR NR NR
4/27/10 18,000.0 11,600.0 1,970.0 9,580.0 16,300.0 1,010.0 NR NR NR NR
4/18/11 22,600.0 6,170.0 2,320.0 9,130.0 27,500.0 1,650.0 NR NR NR NR
4/10/12 22,900.0 3,890.0 1,990.0 6,120.0 28,000.0 1,070.0 NR NR NR NR
4/16/13 21,000.0 8,100.0 2,700.0 11,000.0 20,000.0 1,000.0 NR NR NR NR
4/28/14 FP FP FP FP FP FP FP FP FP FP
4/9/15 13,000.0 8,300.0 1,400.0 7,000.0 24,000.0 860.0 NR NR NR NR
C5-C8 Aliphatics C9-C12
Aliphatics
C9-C10
AromaticsDIPE
Well destroyed during construction activities
MW-17
Contaminant of Concern Benzene Toluene Ethylbenzene Total Xylenes MTBE Lead
2L Standard (µg/L)
GCL (µg/L)
MW-16
MW-19
MW-18
Well could not be located - no sample collected
Page 5 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
1/6/16 7,280.0 6,480.0 1,330.0 8,040.0 1,880.0 204.0 NR NR NR NR
8/21/19 14,400.0 3,100.0 1,950.0 9,790.0 5,700.0 356.0 NR NR NR NR
1/15/21 16,900.0 1,270.0 2,520.0 9,840.0 10,100.0 648.0 NR NR NR NR
10/4/21 18,100.0 1,390.0 2,330.0 8,230.0 15,900.0 764.0 NR NR NR NR
11/8/22 FP FP FP FP FP FP FP FP FP FP
4/4/03 5,700.0 8,500.0 1,200.0 5,700.0 ND ND 6,300.0 2,500.0 240.0 ND
5/15/03 12,000.0 13,000.0 910.0 6,500.0 ND 790.0 34,000.0 15,000.0 ND 9.6
8/14/03 18,000.0 13,000.0 1,000.0 5,600.0 ND 550.0 NR NR NR NR
11/5/03 12,000.0 6,600.0 720.0 2,530.0 ND 450J NR NR NR NR
5/5/04 16,600.0 8,880.0 1,150.0 3,490.0 ND 406J NR NR NR NR
11/18/04 12,600.0 3,410.0 587.0 1,324J ND 500.0 NR NR NR NR
4/4/03 11,000.0 15,000.0 2,000.0 9,200.0 ND ND 16,000.0 7,800.0 980.0 7.6
5/15/03 16,000.0 17,000.0 1,800.0 7,900.0 120.0 1,300.0 49,000.0 17,000.0 ND 26.4
8/14/03 20,000.0 19,000.0 2,200.0 9,800.0 ND 930.0 NR NR NR NR
11/5/03 18,000.0 18,000.0 J 1,500 7,100.0 ND J 780 NR NR NR NR
5/5/04 23,500.0 22,000.0 2,460.0 11,190.0 ND 1,290.0 NR NR NR NR
11/18/04 20,000.0 15,500.0 1,620.0 6,820.0 ND 1,250.0 NR NR NR NR
4/29/08 FP FP FP FP FP FP FP FP FP FP
4/21/09 FP FP FP FP FP FP FP FP FP FP
4/27/10 FP FP FP FP FP FP FP FP FP FP
4/18/11 16,400.0 18,700.0 2,810.0 13,590.0 371J 690.0 NR NR NR NR
4/10/12 FP FP FP FP FP FP FP FP FP FP
4/16/13 FP FP FP FP FP FP FP FP FP FP
4/28/14 7,700.0 4,900.0 2,100.0 12,000.0 ND 210.0 NR NR NR NR
4/9/15 11,000.0 5,600.0 1,400.0 7,200.0 180 J 350.0 NR NR NR NR
1/6/16 11,300.0 6,380.0 1,620.0 8,200.0 238.0 297.0 NR NR NR NR
8/21/19 14,800.0 7,030.0 2,230.0 8,780.0 155.0 194.0 NR NR NR NR
1/15/21 14,900.0 6,720.0 3,020.0 11,820.0 269.0 247.0 NR NR NR NR
10/4/21 9,660.0 3,760.0 2,050.0 7,860.0 81.8 J 113.0 NR NR NR NR
11/8/22 14,200.0 3,170.0 2,140.0 7,770.0 79.7 120.0 NR NR NR NR
4/4/03 ND ND ND ND ND ND ND ND ND ND
5/16/03 ND ND ND ND ND ND ND ND ND 12.4
8/14/03 ND ND ND ND ND ND NR NR NR NR
11/5/03 ND ND ND ND ND ND NR NR NR NR
5/5/04 ND ND ND ND ND ND NR NR NR NR
11/18/04 ND ND ND ND ND ND NR NR NR NR
4/29/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 ND ND ND ND ND ND NR NR NR NR
4/27/10 ND ND ND ND ND ND NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 ND ND ND ND ND ND NR NR NR NR
4/16/13 ND ND ND ND ND ND NR NR NR NR
4/28/14 ND ND ND ND ND ND NR NR NR NR
4/9/15 ND ND ND ND ND ND NR NR NR NR
1/6/16 ND ND ND ND ND ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
4/4/03 12,000.0 12,000.0 1,700.0 8,100.0 ND ND 10,000.0 3,900.0 480.0 ND
5/15/03 16,000.0 13,000.0 1,400.0 4,800.0 ND 46.0 45,000.0 20,000.0 ND ND
8/14/03 20,000.0 8,700.0 1,700.0 7,500.0 ND 1,100.0 NR NR NR NR
11/5/03 16,000.0 3,800.0 1,300.0 5,000.0 ND 810.0 NR NR NR NR
5/5/04 18,100.0 3,540.0 1,350.0 3,076.0 ND ND NR NR NR NR
11/18/04 15,700.0 2,410.0 1,430.0 2,648.0 ND 664.0 NR NR NR NR
4/29/08 FP FP FP FP FP FP FP FP FP FP
4/21/09 FP FP FP FP FP FP FP FP FP FP
4/27/10 6,330.0 1,140.0 1,350.0 3,475.0 ND 228.0 NR NR NR NR
4/18/11 6,790.0 1,960.0 2,170.0 6,312.0 ND 317.0 NR NR NR NR
4/10/12 FP FP FP FP FP FP FP FP FP FP
4/16/13 7,000.0 1,300.0 2,400.0 5,900.0 ND 95J NR NR NR NR
4/28/14 4,900.0 700.0 1,800.0 3,300.0 ND ND NR NR NR NR
4/9/15 4,600.0 610.0 1,700.0 3,100.0 ND 38.0 NR NR NR NR
1/6/16 4,950.0 475.0 1,630.0 2,215.0 ND 42.1 NR NR NR NR
8/21/19 3,460.0 448.0 2,350.0 1,846.0 ND ND NR NR NR NR
1/15/21 2,170.0 339.0 2,360.0 1,461.0 ND ND NR NR NR NR
10/4/21 2,200.0 526.0 3,180.0 1,495.0 ND ND NR NR NR NR
11/8/22 1,350.0 301.0 2,300.0 1,143.1 ND ND NR NR NR NR
4/4/03 10,000.0 6,600.0 890.0 3,400.0 ND 940.0 11,000.0 3,300.0 390.0 36.0
5/15/03 25,000.0 37,000.0 2,300.0 8,800.0 ND ND 74,000.0 26,000.0 ND 879.0
8/14/03 27,000.0 43,000.0 3,300.0 11,000.0 ND ND NR NR NR NR
11/6/03 21,000.0 27,000.0 1,900J 8,200.0 ND ND NR NR NR NR
5/5/04 24,200.0 27,700.0 1,890J 7,950.0 ND ND NR NR NR NR
C5-C8 AliphaticsEthylbenzene Total Xylenes MTBE DIPE
MW-24
2L Standard (µg/L)
GCL (µg/L)
Well covered by concrete slab
MW-20
MW-19
MW-21
MW-22
MW-23
C9-C12
Aliphatics
C9-C10
Aromatics LeadContaminant of Concern Benzene Toluene
Page 6 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
11/18/04 20,500.0 28,500.0 2,130.0 9,500.0 ND J 530 NR NR NR NR
4/29/08 FP FP FP FP FP FP FP FP FP FP
4/21/09 FP FP FP FP FP FP FP FP FP FP
4/27/10 FP FP FP FP FP FP FP FP FP FP
4/18/11 16,000.0 32,700.0 3,380.0 16,230.0 ND ND NR NR NR NR
4/10/12 FP FP FP FP FP FP FP FP FP FP
4/16/13 14,000.0 31,000.0 4,100.0 19,100.0 ND 90J NR NR NR NR
4/28/14 7,900.0 9,500.0 2,000.0 9,200.0 ND 170.0 NR NR NR NR
4/9/15 6,300.0 8,600.0 2,500.0 14,000.0 ND 98.0 NR NR NR NR
1/6/16 9,010.0 8,340.0 2,280.0 11,190.0 27.5 216.0 NR NR NR NR
8/21/19 7,990.0 7,230.0 2,990.0 14,100.0 ND 52.8 NR NR NR NR
1/15/21 4,850.0 4,800.0 2,800.0 13,180.0 ND 38.3 J NR NR NR NR
10/4/21 4,610.0 2,530.0 2,470.0 11,370.0 ND ND NR NR NR NR
11/8/22
5/5/04 930.0 394.0 152.0 2,832.0 ND 88.4 3,400.0 3,300.0 570.0 0.0
11/19/04 141.0 32.4 10.3 734.0 ND ND NR NR NR NR
4/30/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 2.8 0.559 J 2.1 3.08J ND ND NR NR NR NR
4/27/10 10.6 ND 3.5 1.9J 1.49J 3.1 NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 0.241J ND ND ND 3.2 6.3 NR NR NR NR
4/16/13 ND ND ND ND 2.8 J 2.3J NR NR NR NR
4/29/14 ND ND ND ND ND ND NR NR NR NR
4/9/15 0.34 J ND ND ND 2.4 1.2 NR NR NR NR
1/6/16 ND ND ND ND ND ND NR NR NR NR
8/21/19 ND ND ND ND 2.5 0.55J NR NR NR NR
1/15/21 ND ND ND ND ND ND NR NR NR NR
10/4/21 ND ND ND ND ND ND NR NR NR NR
11/8/22
5/5/04 16.0 ND ND ND 0.719J J 0.585 ND ND ND 6.5
11/19/04 5.3 ND ND ND 2.9 1.4 NR NR NR NR
4/30/08 ND ND ND ND 12.2 5.1 NR NR NR NR
4/21/09 ND ND ND ND 20.6 6.6 NR NR NR NR
4/27/10 ND ND ND ND 32.3 9.6 NR NR NR NR
4/18/11 ND ND ND ND 14.1 3.6 NR NR NR NR
4/10/12 ND ND ND ND 23.4 6.7 NR NR NR NR
4/16/13 ND ND ND ND 30.0 3.9J NR NR NR NR
4/29/14 ND ND ND ND 48.0 3.2 NR NR NR NR
4/9/15 ND ND ND ND 22.0 2.6 NR NR NR NR
1/6/16 ND ND ND ND 12.1 3.4 NR NR NR NR
8/21/19 ND ND ND ND 183.0 8.2 NR NR NR NR
1/15/21 ND ND ND ND 37.5 2.1 NR NR NR NR
10/4/21 ND ND ND ND 108.0 3.4 NR NR NR NR
11/8/22
5/5/04 29,000.0 30,800.0 2,110.0 10,360.0 2,860.0 1,790.0 150,000.0 31,000.0 ND 130.0
11/18/04 29,800.0 31,800.0 2,270.0 11,440.0 8,170.0 2,200.0 NR NR NR NR
4/30/08 29,400.0 35,200.0 2,650.0 13,190.0 1,770.0 1,420.0 NR NR NR NR
4/22/09 28,800.0 35,000.0 2,850.0 15,630.0 3,000.0 2,610.0 NR NR NR NR
4/27/10 23,000.0 27,100.0 3,340.0 16,240.0 3,280.0 1270J NR NR NR NR
4/18/11 13,100.0 15,100.0 1,850.0 18,410.0 1,460.0 1,560.0 NR NR NR NR
4/10/12 15,800.0 19,600.0 2,160.0 15,970.0 570J 783J NR NR NR NR
4/16/13 18,000.0 19,000.0 2,500.0 17,000.0 2,200.0 910.0 NR NR NR NR
4/29/14 13,000.0 14,000.0 2,100.0 14,000.0 1,300.0 580.0 NR NR NR NR
4/9/15 8,600.0 10,000.0 1,800.0 11,000.0 1,000.0 440.0 NR NR NR NR
1/6/16 112,000.0 115,000.0 22,200.0 132,600.0 11,500.0 4,780.0 NR NR NR NR
8/21/19 8,550.0 4,390.0 1,550.0 9,040.0 1,570.0 391.0 NR NR NR NR
5/5/04 9.2 1.5 6.4 13.7 7.5 ND 1,100.0 230.0 140.0 9.6
11/18/04 6.9 ND 2.0 ND ND ND NR NR NR NR
4/30/08 ND ND ND ND ND ND NR NR NR NR
4/21/09 ND ND ND ND ND ND NR NR NR NR
4/27/10 0.758J ND 0.372J ND ND ND NR NR NR NR
4/18/11 0.759J ND ND ND ND ND NR NR NR NR
4/10/12 ND ND ND ND ND ND NR NR NR NR
4/16/13 ND ND ND ND ND ND NR NR NR NR
4/28/14 ND ND 0.33 J ND ND ND NR NR NR NR
4/9/15 ND ND ND ND ND ND NR NR NR NR
1/6/16 ND ND ND ND ND ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
4/21/09 22.7 ND 13.1 285.0 ND ND NR NR NR NR
4/27/10 24.6 3.3 5.6 47.8 ND ND NR NR NR NR
Monitoring well no longer accessible/property owner denied access
MW-27
Contaminant of Concern
MW-28
MW-29
Well could not be located - no sample collected
DIPE C5-C8 Aliphatics
C9-C12
Aliphatics
C9-C10
Aromatics LeadEthylbenzene Total Xylenes MTBE
MW-25
Well could not be located - no sample collected
MW-26
Well could not be located - no sample collected
2L Standard (µg/L)
GCL (µg/L)
MW-24
Benzene Toluene
Page 7 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
4/18/11 25.5 6.2 3.4 16.6 ND ND NR NR NR NR
4/10/12 ND 6.1 2.3 10.9 ND ND NR NR NR NR
4/16/13 ND ND 2.1 8.5 ND ND NR NR NR NR
4/28/14 ND ND 1.0 3.5 ND ND NR NR NR NR
4/9/15 ND ND 0.43 J 1.6 J ND ND NR NR NR NR
1/6/16 ND ND ND 1.05 J ND ND NR NR NR NR
8/21/19 ND ND ND ND ND ND NR NR NR NR
1/15/21 ND 0.394 J ND ND ND ND NR NR NR NR
10/4/21 ND 0.374 J ND ND ND ND NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
4/27/10 17,900.0 5,230.0 2,410.0 8,310.0 ND ND NR NR NR NR
4/18/11 4,890.0 4,070.0 1,250.0 5,130.0 205J 370.0 NR NR NR NR
4/10/12 11,000.0 3,420.0 1,480.0 4,970.0 NDa 431.0 NR NR NR NR
4/16/13 8,300.0 2,000.0 1,300.0 3,800.0 200J 320J NR NR NR NR
4/29/14 4,100.0 930.0 880.0 2,300.0 300.0 180.0 NR NR NR NR
4/9/15 2,400.0 420.0 500.0 1,200.0 180.0 140.0 NR NR NR NR
1/6/16 2,130.0 197.0 368.0 825.0 162.0 158.0 NR NR NR NR
8/21/19 15,100.0 665.0 934.0 1,556.0 118.0 177.0 NR NR NR NR
1/15/21 6,570.0 195.0 725.0 846.0 210.0 142.0 NR NR NR NR
10/4/21 2,780.0 194.0 485.0 357.9 J 574.0 136.0 NR NR NR NR
11/8/22 2,360.0 103.0 311.0 198.2 507.0 98.7 NR NR NR NR
8/21/19 1,360.0 1,270.0 4,620.0 16,010.0 1,180.0 ND NR NR NR NR
1/15/21 684.0 795.0 5,030.0 15,080.0 1,970.0 ND NR NR NR NR
10/4/21 529.0 510.0 4,550.0 12,960.0 1,560.0 29.0 J NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
12/21/01 150.0 250.0 53.0 232.0 ND ND NR NR NR NR
5/14/02 290.0 33.0 ND 69.0 ND ND 540.0 120.0 ND ND
8/29/02 110.0 45.0 23.0 28.0 ND ND 290.0 ND ND 15.7
11/11/02 210.0 75.0 26.0 55.0 ND ND 360.0 100.0 ND 6.8
2/27/03 390.0 99.0 32.0 122.0 ND ND 730.0 260.0 ND ND
5/15/03 360.0 220.0 64.0 140.0 ND ND 850.0 410.0 ND ND
8/15/03 460.0 300.0 76.0 215.0 ND ND NR NR NR NR
11/6/03 540.0 210.0 60.0 143.0 ND ND NR NR NR NR
5/6/04 938.0 556.0 164.0 397.0 ND ND NR NR NR NR
11/19/04 978.0 298.0 130.0 209.9 ND J 16.3 NR NR NR NR
4/30/08 379.0 112.0 64.6 74.5 J ND ND NR NR NR NR
4/21/09 759.0 293.0 144.0 248.0 ND ND NR NR NR NR
4/27/10 347.0 128.0 74.7 117.2 ND ND NR NR NR NR
4/18/11 3,140.0 3,290.0 788.0 2,314.0 ND 57.8 NR NR NR NR
4/11/12 355.0 127.0 113.0 121.1 ND ND NR NR NR NR
4/18/13 380.0 210.0 170.0 210.0 ND ND NR NR NR NR
4/29/14 320.0 210.0 160.0 240.0 ND ND NR NR NR NR
4/9/15 190.0 41.0 80.0 81.0 ND 0.38 J NR NR NR NR
1/7/16 180.0 112.0 86.6 132.2 ND ND NR NR NR NR
8/22/19 330.0 42.5 146.0 153.8 ND 0.743J NR NR NR NR
1/15/21 151.0 79.7 66.2 107.0 ND ND NR NR NR NR
10/4/21 175.0 18.4 95.6 62.7 ND 0.450 J NR NR NR NR
11/8/22 147.0 10.8 71.3 77.3 ND ND NR NR NR NR
12/21/01 23.0 140.0 35.0 172.0 ND 10.0 NR NR NR NR
5/14/02 36.0 30.0 2.0 146.0 5.0 15.0 180.0 180.0 ND ND
8/29/02 ND ND ND ND 3.0 16.0 ND ND ND ND
11/11/02 26.0 12.0 11.0 37.0 8.0 22.0 ND ND ND ND
2/27/03 18.0 4.9 19.0 23.2 14.0 21.0 ND ND ND ND
5/15/03 24.0 4.7 25.0 22.9 11.0 11.0 ND ND ND ND
8/15/03 34.0 6.2 28.0 44.0 14.0 22.0 NR NR NR NR
11/6/03 14.0 2.6 17.0 9.7 4.2 6.9 NR NR NR NR
5/6/04 11.5 1.6 22.1 15.6 2.1 5.9 NR NR NR NR
11/19/04 5.9 3.1 9.5 12.3 1.51J 7.2 NR NR NR NR
4/30/08 9.4 0.334J 18.9 3.7 2.6 7.5 NR NR NR NR
4/22/09 10.4 1.1 28.2 22.55 J ND 7.7 NR NR NR NR
4/27/10 3.0 ND 2.3 ND ND 2.1 NR NR NR NR
4/18/11 ND ND ND ND 1.88J 0.876J NR NR NR NR
4/10/12 1.4 ND 1.8 0.746J 1.81J 5.6 NR NR NR NR
4/18/13 0.56 ND 1.3 3.1 2.3J 3.4J NR NR NR NR
4/29/14 0.98 0.18J 3.0 6.3 ND ND NR NR NR NR
4/9/15 2.7 ND 2.5 3.6 0.97J 1.3 NR NR NR NR
1/7/16 0.334J ND 1.7 2.582J 1.4 1.4 NR NR NR NR
8/21/19 ND ND 1.7 1.66J 1.3 1.3 NR NR NR NR
1/15/21 0.577J ND 68.0 10.855J 0.206J 0.265J NR NR NR NR
10/4/21 0.164J ND 2.6 0.846J 0.556J ND NR NR NR NR
11/8/22 ND ND 1.6 ND 0.8 0.7 NR NR NR NR
Contaminant of Concern Lead
2L Standard (µg/L)
GCL (µg/L)
MW-29
MW-30
MW-31
MWWB-1
C5-C8 Aliphatics C9-C12
Aliphatics
C9-C10
Aromatics
MWWB-2
Benzene Toluene Ethylbenzene Total Xylenes MTBE DIPE
Page 8 of 9
Table 6
Historical Groundwater Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Well ID Date Sampled
1 600 600 500 20 70 420 4,200 210 15
5,000 260,000 84,500 85,500 20,000 70,000 NL NL NL 15,000
12/21/01 1,400.0 2,300.0 410.0 2,060.0 ND ND NR NR NR NR
5/14/02 1,800.0 1,100.0 320.0 1,420.0 ND ND 4,500.0 1,800.0 370.0 ND
8/29/02 1,500.0 2,600.0 550.0 2,200.0 ND ND 4,900.0 2,700.0 490.0 20.1
11/11/02 290.0 340.0 120.0 380.0 ND ND 1,100.0 660.0 100.0 ND
2/27/03 180.0 130.0 81.0 205.0 ND 19.0 630.0 400.0 ND ND
5/15/03 330.0 120.0 84.0 191.0 ND 19.0 1,400.0 570.0 ND ND
8/15/03 220.0 120.0 68.0 155.0 ND 30.0 NR NR NR NR
11/6/03 370.0 130.0 83.0 176.0 ND 34.0 NR NR NR NR
5/6/04 290.0 101.0 93.2 171.6 ND 31.2 NR NR NR NR
11/19/04 689.0 199.0 147.0 285.0 ND 72.5 NR NR NR NR
4/30/08 256.0 15.1 37.0 49.2 ND 20.4 NR NR NR NR
4/22/09 246.0 21.9 44.9 60.35J ND 28.5 NR NR NR NR
4/27/10 337.0 78.2 52.8 56.2 ND 6.64J NR NR NR NR
4/18/11 1,390.0 416.0 323.0 395.4J 46.8J 41.9J NR NR NR NR
4/10/12 165.0 9.0 32.6 29.5 ND 6.70J NR NR NR NR
4/16/13 210.0 50.0 66.0 83.0 4.3J 7.0 NR NR NR NR
4/29/14 150.0 34.0 38.0 64.0 5.1 L 6.4 NR NR NR NR
4/9/15 130.0 25.0 24.0 37.0 ND 7.8 NR NR NR NR
1/6/16 120.0 45.4 20.9 61.5 ND 7.7 NR NR NR NR
8/21/19 136.0 7.9 34.3 27.7 14.5 10.2 NR NR NR NR
1/15/21 121.0 8.7 42.4 33.3 24.5 15.3 NR NR NR NR
10/4/21 92.8 3.7 27.3 20.420J 31.2 19.7 NR NR NR NR
11/8/22 97.4 7.1 78.3 16.8 32.5 18.0 NR NR NR NR
12/21/01 310.0 6.0 16.0 25.0 ND 170.0 NR NR NR NR
5/14/02 64.0 13.0 4.0 56.0 ND 43.0 290.0 100.0 ND ND
8/29/02 480.0 ND ND ND ND 170.0 220.0 ND ND ND
11/11/02 4.0 ND ND ND ND 4.0 ND ND ND ND
2/27/03 290.0 54.0 21.0 ND ND 22.0 320.0 100.0 ND ND
5/15/03 620.0 81.0 ND ND ND 36.0 1,300.0 210.0 ND ND
8/15/03 24.0 2.4 2.6 ND ND 2.0 NR NR NR NR
11/6/03 1,400.0 19J 15J ND ND 110.0 NR NR NR NR
5/6/04 962.0 31.0 13.3J ND ND 88.0 NR NR NR NR
11/19/04 104.0 2.94J 3.86J 3.97J ND 15.9 NR NR NR NR
4/30/08 10.5 1.4 0.742J 2.624 J ND 3.8 NR NR NR NR
4/22/09 22.0 3.4 7.6 6.2 ND 6.9 NR NR NR NR
4/27/10 32.9 2.7 4.2 3.0J 1.65J 10.8 NR NR NR NR
4/18/11 ND ND ND ND ND ND NR NR NR NR
4/10/12 5.1 0.546J 2.6 0.537J ND 3.8 NR NR NR NR
4/16/13 0.89 ND ND ND ND 1.4J NR NR NR NR
4/29/14 1.8 0.90 1.2 1.3J ND 0.89 NR NR NR NR
4/9/15 0.64J ND ND ND 0.50J 2.4 NR NR NR NR
1/6/16 0.718J ND ND ND ND 0.436J NR NR NR NR
11/8/22 NS NS NS NS NS NS NS NS NS NS
2L Standard = 15A NCAC 02L .0202 Groundwater Standard NL = not listed
GCL = North Carolina Gross Contaminant Levels NR = laboratory analysis not requested
Bold = values exceed 2L Standard NS = not sampled
Red = values exceed GCL FP = well not sampled due to the presence of LNAPL
ug/L = micrograms per liter J = estimated value
NDa = not detected at or above laboratory PQL and laboratory PQL exceeds the 2L Standard ND = not detected at or above laboratory PQL
Historical Groundwater Analytical Results were obtained from the December 7, 2021 Groundwater Monitoring Report. Analytical
results for the November 8, 2022 were collected by AECOM.
MTBE = Methyl tert-butyl ether
DIPE = Diisopropyl ether
EthylbenzeneContaminant of Concern Benzene Toluene
L = laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the high side.
MWWB-3
C9-C10
Aromatics Lead
2L Standard (µg/L)
GCL (µg/L)
Notes:
MWWB-4
Total Xylenes MTBE DIPE C5-C8 Aliphatics
C9-C12
Aliphatics
Page 9 of 9
Table 7
Summary of Air Stack Analytical Results and Mass Removal Calculations
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
Benzene Mw = 78.10 Toluene Mw = 92.10 Ethylbenzene Mw = 106 Total Xylenes Mw = 106
ug/m3 ppmv Md ug/m3 ppmv Md ug/m3 ppmv Md ug/m3 ppmv Md
03/24/22 17 25 68 23,600 7.39 0.14 2,580 0.69 0.02 4,140 0.96 0.03 12,560 2.90 0.08
04/26/22 13 25 70 32,900 10.31 0.21 12,700 3.37 0.08 7,540 1.74 0.05 41,100 9.49 0.26
05/27/22 13 25 72 32,900 10.31 0.21 11,000 2.92 0.07 5,550 1.28 0.04 26,860 6.20 0.17
Air Stack 06/13/22 9 60 90 13,400 4.20 0.11 8,060 2.14 0.07 3,230 0.75 0.03 20,730 4.79 0.17
07/18/22 11 50 60 35,800 11.22 0.19 32,200 8.56 0.17 10,200 2.35 0.06 90,800 20.96 0.49
08/15/22 11 40 56 77,000 24.13 0.39 57,300 15.22 0.29 14,100 3.25 0.07 170,800 39.43 0.86
09/14/22 14 20 60 101,000 31.64 0.55 80,200 21.31 0.43 19,000 4.39 0.10 252,200 58.22 1.36
03/24/22 28,571.5 0.26 2.63 0.43
04/26/22 29,368.4 0.59 5.94 0.97
05/27/22 30,104.4 0.49 4.95 0.81
Air Stack 06/13/22 30,484.0 0.37 3.68 0.60
07/18/22 31,137.8 0.91 9.13 1.50
08/15/22 31,676.1 1.61 16.10 2.64
09/14/22 32,394.9 2.44 24.45 4.01
Notes and Assumptions:
Airflow rate not recorded during the 3/24/22 inspection. Average operation period airflow rate used for calculation purposes.Mw = Average molecular weight Q = Flow rate (scfm)
fpm to acfm conversion calculated using 2-inch diameter pipe.Mv = Molar volume of air at standard laboratory temperature (24.47 at 25oC)acfm = actual cubic feet per minute
acfm to scfm conversion calculated using vacuum, average air temperature of 62oF, and an altitude of 633 feet.P = Standard atmospheric pressure (2116.8 lbs/ft2)scfm = Standard cubic feet per minute
Md = Mass of contaminant discharged (lbs/day) = (ppmv)(Mw)(P/RT)(Q)(1440 min/day)(10-6)R = Universal gas constant (1,545 ft-lb/mole-oR)lbs = Pounds
Gasoline Md = (BTEX Md)(10), assumes BTEX makes up 10% of one pound of gasoline T = Standard temperature at which results are to be reported (536oR)gal = Gallons
Gasoline Gd = Volume of gasoline (gal/day) = (Gasoline Md)*(1 gal of gas/6.1 lbs)ug/L = micrograms per liter oR = Degrees Rankine
ppmv = parts per million volume = (ug/m3)(1 mg/1000 ug)(Mv/Mw)ug/m3 = micrograms per cubic meter ft = Feet
BTEX = Benzene, toluene, ethylbenzene, xylenes PID = Photoionization Detector in-Hg = inches of mercury
32.34
24.88
9.55
40.79
59.20
209.94 320.39
169.66
Blower Vacuum
(in-Hg)
Make-up Air
Valve Position
(% open)
Runtime, Total
(hours)BTEX Md
Total Gallons of Gasoline
Recovered
2.90
60.12
69.67
110.46
Cummulative Gallons of
Gasoline Recovered
2.90
35.25
Gasoline Gd
Location Date
Airflow Rate
(scfm)
Location Date Gasoline Md
Page 1 of 1
Table 8
Summary of Liquid Discharge Flow Data and Analytical Results
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number: 0-004038
3/17/2022 3/24/2022 4/13/2022 4/14/2022 4/26/2022 5/10/2022 5/31/2022 6/3/2022 6/13/2022 6/16/2022 7/5/2022 7/13/2022 7/18/2022 8/2/2022 8/15/2022 8/31/2022 9/14/2022 10/10/2022
--7 20 1 12 14 21 3 10 3 19 8 5 15 13 16 14 26
1,423,171 1,438,152 1,455,878 1,456,170 1,465,850 1,474,680 1,488,250 1,489,720 1,491,560 1,491,881 1,492,282 1,492,662 1,496,439 1,503,074 1,508,169 1,522,223 1,543,774 1,543,774
-- 14,981 17,726 292 9,680 8,830 13,570 1,470 1,840 321 401 380 3,777 6,635 5,095 14,054 21,551 0
-- YES ---- YES ------ YES ---------------- YES
Parameter Permit Limit
Flow (GPD) 10,000 -- 2,140 886 292 807 631 646 490 184 107 21 48 755 442 392 878 1,539 NO FLOW
Flow (GPM) 10 -- 1.49 0.62 0.20 0.56 0.44 0.45 0.34 0.13 0.07 0.01 0.03 0.52 0.31 0.27 0.61 1.07 NO FLOW
Lead (μg/L) 400 -- 6.74 ---- 8.52 ------ 1.26 J ----------------20
BTEX (μg/L) 5,000 -- ND ---- ND ------ ND ---------------- ND
TPH (μg/L) 10,000 -- NA ---- NA ------ NA ---------------- ND
TTO (μg/L) 2130 -- NA ---- NA ------ NA ---------------- ND
TTO = total toxic organics as defined by EPA "Priority Pollutant List"
Average Flow and Analytical Results
Discharge Flow Data
ND = below laboratory method detection limit
Date
Days Between Visits
J = identification of the analyte is acceptable; reported value is an estimate
Water Meter Reading (gal)
Gallons Between Visits
Sample Collected
GPD = gallons per day
GPM = gallons per minute
gal - gallons
μg/L = micrograms per liter
BTEX = benzene, toluene, ethylbenzene, and xylenes
Notes:
NA = not analyzed
TPH = total petroleum hydrocarbons
Page 1 of 1

AECOM
Appendix A – Adjacent Parcel Data
© 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS SCALE IN FEET:8080060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\20221122\6958 Burlington.dwg, 11/23/2022 2:13 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUNOVEMBER 2022M. LINKSpeedway LLC.Speedway Store #6958653 East Webb AvenueBurlington, North CarolinaADJACENT PARCEL MAPLEGENDSubject Property BoundaryAdjacent Property BoundaryBuilding
Map ID Tax Parcel No. Property Address Owner Name Owner Address
1 8875217376
635 E Webb Ave
Burlington, NC 27217 Davis St United Methodist Church 606 E Davis St
Burlington, NC 27215
2 8875215338
606 E Davis St
Burlington, NC 27215 Davis St United Methodist Church 606 E Davis St
Burlington, NC 27215
3 8875216515
605 E Webb Ave
Burlington, NC 27217 Donnell Renee Mechelle 605 E Webb Ave
Burlington, NC27217
4 8875215291
616 E Davis Street
Burlington, NC 27215 Bateman Danny L 616 E Davis Street
Burlington, NC 27215
5 8875216126
620 E Davis Street
Burlington, NC 27215 Whitt Real Estate LLC PO Box 1233
Mebane, NC 27302
6 8875216013
600 E Davis Street
Burlington, NC 27215 Elder John F Trustee For PO Box 2377
Burlington, NC 27216
7 8875216056
117 Tucker St
Burlington, NC 27215 Elder John F Trustee For PO Box 2377
Burlington, NC 27216
8 8875217121
115 Tucker St
Burlington, NC 27215 Good News Real Estate Invest 115 Tucker St
Burlington, NC 27215
9 8875217196
111 Tucker St
Burlington, NC 27215 Newton robert Grant 111 Tucker St
Burlington, NC 27215
Appendix A
Adjacent Parcel Data
Speedway Store No. 6958
653 East Webb Avenue, Burlington, NC 27217
Incident Number: 19272 Facility Number : 0-004038
Page 1 of 1

AECOM
Appendix B – Groundwater Monitoring Event Documentation
Site Monitoring Well Inventory Worksheet
CLIENT:PROJECT NAME:PROJECT LOCATION:PROJECT NO.:INVENTORY DATE:PERSONNEL:
Pad Condition
Manhole Conditions
(bolts/seals on undersideof cover/secured)
Locking Cap
(y/n)Well Identification Tag(legible info.)
Sheen or Odor SurroundingWells/Surface Water
Introduced Into Well
GENERAL COMMENTS
CommentsWell I.D.
Well
Depth
(feet)
Well
Diameter
(inches)
Well IntegrityDepth to
Water
(feet)

Speedway Speedway 6958
Burlington, NC
November 8, 2022
Carter Paradis & Angie Sastoque Ardila
60686627
Page____ of ____
Field Personnel:
Date:Project Number:
Daily Objective:
Daily Activity Log
Project Manager:
Project Name:Client:

Page____ of ____
Field Personnel:
Date:Project Number:
Daily Objective:
Daily Activity Log
Project Manager:
Project Name:Client:

AECOM
Appendix C – Laboratory Analytical Reports
#=CL#
December 06, 2022
LIMS USE: FR - MARIANNE LINK
LIMS OBJECT ID: 92636177
92636177
Project:
Pace Project No.:
RE:
Marianne Link
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
46865-6958 BURLINGTON NC
Dear Marianne Link:
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 46
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 46
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92636177001 MWWB-1 SM 6200B 69 PASI-CSAS
92636177002 MWWB-2 SM 6200B 69 PASI-CSAS
92636177003 MWWB-3 SM 6200B 69 PASI-CCL
92636177004 MW-6R SM 6200B 69 PASI-CCL
92636177005 MW-15 SM 6200B 69 PASI-CCL
92636177006 MW-21 SM 6200B 69 PASI-CCL
92636177007 MW-23 SM 6200B 69 PASI-CCL
92636177008 MW-30 SM 6200B 69 PASI-CCL
92636177009 TRIP BLANK SM 6200B 69 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-1 Lab ID: 92636177001 Collected: 11/08/22 13:35 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/14/22 21:08 75-85-4100 1
tert-Amylmethyl ether ND ug/L 11/14/22 21:08 994-05-810.0 1
Benzene 147 ug/L 11/14/22 21:08 71-43-20.50 1
Bromobenzene ND ug/L 11/14/22 21:08 108-86-10.50 1
Bromochloromethane ND ug/L 11/14/22 21:08 74-97-50.50 1
Bromodichloromethane ND ug/L 11/14/22 21:08 75-27-40.50 1
Bromoform ND ug/L 11/14/22 21:08 75-25-20.50 1
Bromomethane ND ug/L 11/14/22 21:08 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/14/22 21:08 75-65-050.0 1
n-Butylbenzene ND ug/L 11/14/22 21:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/14/22 21:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/14/22 21:08 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/14/22 21:08 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/14/22 21:08 56-23-50.50 1
Chlorobenzene ND ug/L 11/14/22 21:08 108-90-70.50 1
Chloroethane ND ug/L 11/14/22 21:08 75-00-31.0 1
Chloroform ND ug/L 11/14/22 21:08 67-66-30.50 1
Chloromethane ND ug/L 11/14/22 21:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/14/22 21:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/14/22 21:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/14/22 21:08 96-12-81.0 1
Dibromochloromethane ND ug/L 11/14/22 21:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/14/22 21:08 106-93-40.50 1
Dibromomethane ND ug/L 11/14/22 21:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/14/22 21:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/14/22 21:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/14/22 21:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/14/22 21:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/14/22 21:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/14/22 21:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/14/22 21:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/14/22 21:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/14/22 21:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/14/22 21:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/14/22 21:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/14/22 21:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/14/22 21:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/14/22 21:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/14/22 21:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/14/22 21:08 108-20-30.50 1
Ethanol ND ug/L 11/14/22 21:08 64-17-5200 1
Ethylbenzene 71.3 ug/L 11/14/22 21:08 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/14/22 21:08 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/14/22 21:08 87-68-32.0 1
Isopropylbenzene (Cumene)3.5 ug/L 11/14/22 21:08 98-82-80.50 1
Methylene Chloride ND ug/L 11/14/22 21:08 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-1 Lab ID: 92636177001 Collected: 11/08/22 13:35 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/14/22 21:08 1634-04-40.50 1
Naphthalene 10.9 ug/L 11/14/22 21:08 91-20-32.0 1
n-Propylbenzene 7.5 ug/L 11/14/22 21:08 103-65-10.50 1
Styrene ND ug/L 11/14/22 21:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/14/22 21:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/14/22 21:08 79-34-50.50 1
Tetrachloroethene ND ug/L 11/14/22 21:08 127-18-40.50 1
Toluene 10.8 ug/L 11/14/22 21:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/14/22 21:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/14/22 21:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/14/22 21:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/14/22 21:08 79-00-50.50 1
Trichloroethene ND ug/L 11/14/22 21:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/14/22 21:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/14/22 21:08 96-18-40.50 1
1,2,4-Trimethylbenzene 32.3 ug/L 11/14/22 21:08 95-63-60.50 1
1,3,5-Trimethylbenzene 1.4 ug/L 11/14/22 21:08 108-67-80.50 1
Vinyl chloride ND ug/L 11/14/22 21:08 75-01-41.0 1
m&p-Xylene 76.3 ug/L 11/14/22 21:08 179601-23-11.0 1
o-Xylene 1.0 ug/L 11/14/22 21:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/14/22 21:08 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %11/14/22 21:08 460-00-470-130 1
Toluene-d8 (S)99 %11/14/22 21:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-2 Lab ID: 92636177002 Collected: 11/08/22 11:02 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/14/22 21:26 75-85-4100 1
tert-Amylmethyl ether ND ug/L 11/14/22 21:26 994-05-810.0 1
Benzene ND ug/L 11/14/22 21:26 71-43-20.50 1
Bromobenzene ND ug/L 11/14/22 21:26 108-86-10.50 1
Bromochloromethane ND ug/L 11/14/22 21:26 74-97-50.50 1
Bromodichloromethane ND ug/L 11/14/22 21:26 75-27-40.50 1
Bromoform ND ug/L 11/14/22 21:26 75-25-20.50 1
Bromomethane ND ug/L 11/14/22 21:26 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/14/22 21:26 75-65-050.0 1
n-Butylbenzene ND ug/L 11/14/22 21:26 104-51-80.50 1
sec-Butylbenzene 0.53 ug/L 11/14/22 21:26 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/14/22 21:26 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/14/22 21:26 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/14/22 21:26 56-23-50.50 1
Chlorobenzene ND ug/L 11/14/22 21:26 108-90-70.50 1
Chloroethane ND ug/L 11/14/22 21:26 75-00-31.0 1
Chloroform ND ug/L 11/14/22 21:26 67-66-30.50 1
Chloromethane ND ug/L 11/14/22 21:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/14/22 21:26 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/14/22 21:26 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/14/22 21:26 96-12-81.0 1
Dibromochloromethane ND ug/L 11/14/22 21:26 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/14/22 21:26 106-93-40.50 1
Dibromomethane ND ug/L 11/14/22 21:26 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/14/22 21:26 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/14/22 21:26 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/14/22 21:26 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/14/22 21:26 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/14/22 21:26 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/14/22 21:26 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/14/22 21:26 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/14/22 21:26 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/14/22 21:26 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/14/22 21:26 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/14/22 21:26 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/14/22 21:26 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/14/22 21:26 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/14/22 21:26 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/14/22 21:26 10061-02-60.50 1
Diisopropyl ether 0.71 ug/L 11/14/22 21:26 108-20-30.50 1
Ethanol ND ug/L 11/14/22 21:26 64-17-5200 1
Ethylbenzene 1.6 ug/L 11/14/22 21:26 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/14/22 21:26 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/14/22 21:26 87-68-32.0 1
Isopropylbenzene (Cumene)1.6 ug/L 11/14/22 21:26 98-82-80.50 1
Methylene Chloride ND ug/L 11/14/22 21:26 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-2 Lab ID: 92636177002 Collected: 11/08/22 11:02 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 0.77 ug/L 11/14/22 21:26 1634-04-40.50 1
Naphthalene ND ug/L 11/14/22 21:26 91-20-32.0 1
n-Propylbenzene 1.9 ug/L 11/14/22 21:26 103-65-10.50 1
Styrene ND ug/L 11/14/22 21:26 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/14/22 21:26 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/14/22 21:26 79-34-50.50 1
Tetrachloroethene ND ug/L 11/14/22 21:26 127-18-40.50 1
Toluene ND ug/L 11/14/22 21:26 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/14/22 21:26 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/14/22 21:26 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/14/22 21:26 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/14/22 21:26 79-00-50.50 1
Trichloroethene ND ug/L 11/14/22 21:26 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/14/22 21:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/14/22 21:26 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/14/22 21:26 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/14/22 21:26 108-67-80.50 1
Vinyl chloride ND ug/L 11/14/22 21:26 75-01-41.0 1
m&p-Xylene ND ug/L 11/14/22 21:26 179601-23-11.0 1
o-Xylene ND ug/L 11/14/22 21:26 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/14/22 21:26 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %11/14/22 21:26 460-00-470-130 1
Toluene-d8 (S)102 %11/14/22 21:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-3 Lab ID: 92636177003 Collected: 11/08/22 11:20 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/16/22 06:04 75-85-4100 1
tert-Amylmethyl ether ND ug/L 11/16/22 06:04 994-05-810.0 1
Benzene 97.4 ug/L 11/16/22 06:04 71-43-20.50 1
Bromobenzene ND ug/L 11/16/22 06:04 108-86-10.50 1
Bromochloromethane ND ug/L 11/16/22 06:04 74-97-50.50 1
Bromodichloromethane ND ug/L 11/16/22 06:04 75-27-40.50 1
Bromoform ND ug/L 11/16/22 06:04 75-25-20.50 1
Bromomethane ND ug/L 11/16/22 06:04 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/16/22 06:04 75-65-050.0 1
n-Butylbenzene 12.4 ug/L 11/16/22 06:04 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/16/22 06:04 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/16/22 06:04 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/16/22 06:04 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/16/22 06:04 56-23-50.50 1
Chlorobenzene ND ug/L 11/16/22 06:04 108-90-70.50 1
Chloroethane ND ug/L 11/16/22 06:04 75-00-31.0 1
Chloroform ND ug/L 11/16/22 06:04 67-66-30.50 1
Chloromethane ND ug/L 11/16/22 06:04 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/16/22 06:04 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/16/22 06:04 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/16/22 06:04 96-12-81.0 1
Dibromochloromethane ND ug/L 11/16/22 06:04 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/16/22 06:04 106-93-40.50 1
Dibromomethane ND ug/L 11/16/22 06:04 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/16/22 06:04 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/16/22 06:04 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/16/22 06:04 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/16/22 06:04 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/16/22 06:04 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/16/22 06:04 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/16/22 06:04 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/16/22 06:04 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/16/22 06:04 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/16/22 06:04 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/16/22 06:04 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/16/22 06:04 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/16/22 06:04 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/16/22 06:04 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/16/22 06:04 10061-02-60.50 1
Diisopropyl ether 18.0 ug/L 11/16/22 06:04 108-20-30.50 1
Ethanol ND ug/L 11/16/22 06:04 64-17-5200 1
Ethylbenzene 78.3 ug/L 11/16/22 06:04 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/16/22 06:04 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/16/22 06:04 87-68-32.0 1
Isopropylbenzene (Cumene)18.2 ug/L 11/16/22 06:04 98-82-80.50 1
Methylene Chloride ND ug/L 11/16/22 06:04 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MWWB-3 Lab ID: 92636177003 Collected: 11/08/22 11:20 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 32.5 ug/L 11/16/22 06:04 1634-04-40.50 1
Naphthalene 28.3 ug/L 11/16/22 06:04 91-20-32.0 1
n-Propylbenzene 45.5 ug/L 11/16/22 06:04 103-65-10.50 1
Styrene ND ug/L 11/16/22 06:04 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/16/22 06:04 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/16/22 06:04 79-34-50.50 1
Tetrachloroethene ND ug/L 11/16/22 06:04 127-18-40.50 1
Toluene 7.1 ug/L 11/16/22 06:04 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/16/22 06:04 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/16/22 06:04 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/16/22 06:04 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/16/22 06:04 79-00-50.50 1
Trichloroethene ND ug/L 11/16/22 06:04 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/16/22 06:04 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/16/22 06:04 96-18-40.50 1
1,2,4-Trimethylbenzene 20.2 ug/L 11/16/22 06:04 95-63-60.50 1
1,3,5-Trimethylbenzene 5.4 ug/L 11/16/22 06:04 108-67-80.50 1
Vinyl chloride ND ug/L 11/16/22 06:04 75-01-41.0 1
m&p-Xylene 15.6 ug/L 11/16/22 06:04 179601-23-11.0 1
o-Xylene 1.2 ug/L 11/16/22 06:04 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %11/16/22 06:04 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/16/22 06:04 460-00-470-130 1
Toluene-d8 (S)96 %11/16/22 06:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-6R Lab ID: 92636177004 Collected: 11/09/22 09:15 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/16/22 11:49 75-85-41000 10
tert-Amylmethyl ether ND ug/L 11/16/22 11:49 994-05-8100 10
Benzene 6.5 ug/L 11/16/22 11:49 71-43-25.0 10
Bromobenzene ND ug/L 11/16/22 11:49 108-86-15.0 10
Bromochloromethane ND ug/L 11/16/22 11:49 74-97-55.0 10
Bromodichloromethane ND ug/L 11/16/22 11:49 75-27-45.0 10
Bromoform ND ug/L 11/16/22 11:49 75-25-25.0 10
Bromomethane ND ug/L 11/16/22 11:49 74-83-950.0 10
tert-Butyl Alcohol ND ug/L 11/16/22 11:49 75-65-0500 10
n-Butylbenzene 50.7 ug/L 11/16/22 11:49 104-51-85.0 10
sec-Butylbenzene ND ug/L 11/16/22 11:49 135-98-85.0 10
tert-Butylbenzene ND ug/L 11/16/22 11:49 98-06-65.0 10
tert-Butyl Formate ND ug/L 11/16/22 11:49 762-75-4500 10
Carbon tetrachloride ND ug/L 11/16/22 11:49 56-23-55.0 10
Chlorobenzene ND ug/L 11/16/22 11:49 108-90-75.0 10
Chloroethane ND ug/L 11/16/22 11:49 75-00-310.0 10
Chloroform ND ug/L 11/16/22 11:49 67-66-35.0 10
Chloromethane ND ug/L 11/16/22 11:49 74-87-310.0 10
2-Chlorotoluene ND ug/L 11/16/22 11:49 95-49-85.0 10
4-Chlorotoluene ND ug/L 11/16/22 11:49 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 11/16/22 11:49 96-12-810.0 10
Dibromochloromethane ND ug/L 11/16/22 11:49 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 11/16/22 11:49 106-93-45.0 10
Dibromomethane ND ug/L 11/16/22 11:49 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 11/16/22 11:49 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 11/16/22 11:49 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 11/16/22 11:49 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 11/16/22 11:49 75-71-85.0 10
1,1-Dichloroethane ND ug/L 11/16/22 11:49 75-34-35.0 10
1,2-Dichloroethane ND ug/L 11/16/22 11:49 107-06-25.0 10
1,1-Dichloroethene ND ug/L 11/16/22 11:49 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 11/16/22 11:49 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 11/16/22 11:49 156-60-55.0 10
1,2-Dichloropropane ND ug/L 11/16/22 11:49 78-87-55.0 10
1,3-Dichloropropane ND ug/L 11/16/22 11:49 142-28-95.0 10
2,2-Dichloropropane ND ug/L 11/16/22 11:49 594-20-75.0 10
1,1-Dichloropropene ND ug/L 11/16/22 11:49 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 11/16/22 11:49 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 11/16/22 11:49 10061-02-65.0 10
Diisopropyl ether ND ug/L 11/16/22 11:49 108-20-35.0 10
Ethanol ND ug/L 11/16/22 11:49 64-17-52000 10
Ethylbenzene 407 ug/L 11/16/22 11:49 100-41-45.0 10
Ethyl-tert-butyl ether ND ug/L 11/16/22 11:49 637-92-3100 10
Hexachloro-1,3-butadiene ND ug/L 11/16/22 11:49 87-68-320.0 10
Isopropylbenzene (Cumene)81.9 ug/L 11/16/22 11:49 98-82-85.0 10
Methylene Chloride ND ug/L 11/16/22 11:49 75-09-220.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-6R Lab ID: 92636177004 Collected: 11/09/22 09:15 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 12.7 ug/L 11/16/22 11:49 1634-04-45.0 10
Naphthalene 558 ug/L 11/16/22 11:49 91-20-320.0 10
n-Propylbenzene 190 ug/L 11/16/22 11:49 103-65-15.0 10
Styrene ND ug/L 11/16/22 11:49 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 11/16/22 11:49 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 11/16/22 11:49 79-34-55.0 10
Tetrachloroethene ND ug/L 11/16/22 11:49 127-18-45.0 10
Toluene ND ug/L 11/16/22 11:49 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 11/16/22 11:49 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 11/16/22 11:49 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 11/16/22 11:49 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 11/16/22 11:49 79-00-55.0 10
Trichloroethene ND ug/L 11/16/22 11:49 79-01-65.0 10
Trichlorofluoromethane ND ug/L 11/16/22 11:49 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 11/16/22 11:49 96-18-45.0 10
1,2,4-Trimethylbenzene 1030 ug/L 11/16/22 11:49 95-63-65.0 10
1,3,5-Trimethylbenzene 58.6 ug/L 11/16/22 11:49 108-67-85.0 10
Vinyl chloride ND ug/L 11/16/22 11:49 75-01-410.0 10
m&p-Xylene 723 ug/L 11/16/22 11:49 179601-23-110.0 10
o-Xylene ND ug/L 11/16/22 11:49 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/16/22 11:49 17060-07-070-130 10
4-Bromofluorobenzene (S)95 %11/16/22 11:49 460-00-470-130 10
Toluene-d8 (S)100 %11/16/22 11:49 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-15 Lab ID: 92636177005 Collected: 11/09/22 08:57 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/17/22 00:04 75-85-412500 125
tert-Amylmethyl ether ND ug/L 11/17/22 00:04 994-05-81250 125
Benzene 2230 ug/L 11/17/22 00:04 71-43-262.5 125
Bromobenzene ND ug/L 11/17/22 00:04 108-86-162.5 125
Bromochloromethane ND ug/L 11/17/22 00:04 74-97-562.5 125
Bromodichloromethane ND ug/L 11/17/22 00:04 75-27-462.5 125
Bromoform ND ug/L 11/17/22 00:04 75-25-262.5 125
Bromomethane ND ug/L 11/17/22 00:04 74-83-9625 125
tert-Butyl Alcohol ND ug/L 11/17/22 00:04 75-65-06250 125
n-Butylbenzene ND ug/L 11/17/22 00:04 104-51-862.5 125
sec-Butylbenzene ND ug/L 11/17/22 00:04 135-98-862.5 125
tert-Butylbenzene ND ug/L 11/17/22 00:04 98-06-662.5 125
tert-Butyl Formate ND ug/L 11/17/22 00:04 762-75-46250 125
Carbon tetrachloride ND ug/L 11/17/22 00:04 56-23-562.5 125
Chlorobenzene ND ug/L 11/17/22 00:04 108-90-762.5 125
Chloroethane ND ug/L 11/17/22 00:04 75-00-3 M1125 125
Chloroform ND ug/L 11/17/22 00:04 67-66-362.5 125
Chloromethane ND ug/L 11/17/22 00:04 74-87-3 M1125 125
2-Chlorotoluene ND ug/L 11/17/22 00:04 95-49-862.5 125
4-Chlorotoluene ND ug/L 11/17/22 00:04 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 11/17/22 00:04 96-12-8125 125
Dibromochloromethane ND ug/L 11/17/22 00:04 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 11/17/22 00:04 106-93-462.5 125
Dibromomethane ND ug/L 11/17/22 00:04 74-95-3 M162.5 125
1,2-Dichlorobenzene ND ug/L 11/17/22 00:04 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 11/17/22 00:04 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 11/17/22 00:04 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 11/17/22 00:04 75-71-8 M162.5 125
1,1-Dichloroethane ND ug/L 11/17/22 00:04 75-34-362.5 125
1,2-Dichloroethane ND ug/L 11/17/22 00:04 107-06-262.5 125
1,1-Dichloroethene ND ug/L 11/17/22 00:04 75-35-4 M162.5 125
cis-1,2-Dichloroethene ND ug/L 11/17/22 00:04 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 11/17/22 00:04 156-60-5 M162.5 125
1,2-Dichloropropane ND ug/L 11/17/22 00:04 78-87-562.5 125
1,3-Dichloropropane ND ug/L 11/17/22 00:04 142-28-962.5 125
2,2-Dichloropropane ND ug/L 11/17/22 00:04 594-20-762.5 125
1,1-Dichloropropene ND ug/L 11/17/22 00:04 563-58-6 M162.5 125
cis-1,3-Dichloropropene ND ug/L 11/17/22 00:04 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 11/17/22 00:04 10061-02-662.5 125
Diisopropyl ether 229 ug/L 11/17/22 00:04 108-20-362.5 125
Ethanol ND ug/L 11/17/22 00:04 64-17-525000 125
Ethylbenzene 581 ug/L 11/17/22 00:04 100-41-462.5 125
Ethyl-tert-butyl ether ND ug/L 11/17/22 00:04 637-92-31250 125
Hexachloro-1,3-butadiene ND ug/L 11/17/22 00:04 87-68-3250 125
Isopropylbenzene (Cumene)ND ug/L 11/17/22 00:04 98-82-862.5 125
Methylene Chloride ND ug/L 11/17/22 00:04 75-09-2250 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-15 Lab ID: 92636177005 Collected: 11/09/22 08:57 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 16500 ug/L 11/17/22 00:04 1634-04-4 M162.5 125
Naphthalene 259 ug/L 11/17/22 00:04 91-20-3 M1250 125
n-Propylbenzene 144 ug/L 11/17/22 00:04 103-65-162.5 125
Styrene ND ug/L 11/17/22 00:04 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 11/17/22 00:04 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 11/17/22 00:04 79-34-562.5 125
Tetrachloroethene ND ug/L 11/17/22 00:04 127-18-462.5 125
Toluene ND ug/L 11/17/22 00:04 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 11/17/22 00:04 87-61-6250 125
1,2,4-Trichlorobenzene ND ug/L 11/17/22 00:04 120-82-1250 125
1,1,1-Trichloroethane ND ug/L 11/17/22 00:04 71-55-6 M162.5 125
1,1,2-Trichloroethane ND ug/L 11/17/22 00:04 79-00-562.5 125
Trichloroethene ND ug/L 11/17/22 00:04 79-01-6 M162.5 125
Trichlorofluoromethane ND ug/L 11/17/22 00:04 75-69-4125 125
1,2,3-Trichloropropane ND ug/L 11/17/22 00:04 96-18-462.5 125
1,2,4-Trimethylbenzene 280 ug/L 11/17/22 00:04 95-63-662.5 125
1,3,5-Trimethylbenzene 107 ug/L 11/17/22 00:04 108-67-862.5 125
Vinyl chloride ND ug/L 11/17/22 00:04 75-01-4 M1125 125
m&p-Xylene 313 ug/L 11/17/22 00:04 179601-23-1125 125
o-Xylene ND ug/L 11/17/22 00:04 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/17/22 00:04 17060-07-070-130 125
4-Bromofluorobenzene (S)98 %11/17/22 00:04 460-00-470-130 125
Toluene-d8 (S)101 %11/17/22 00:04 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-21 Lab ID: 92636177006 Collected: 11/08/22 13:00 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/16/22 11:31 75-85-412500 125
tert-Amylmethyl ether ND ug/L 11/16/22 11:31 994-05-81250 125
Benzene 14200 ug/L 11/16/22 11:31 71-43-262.5 125
Bromobenzene ND ug/L 11/16/22 11:31 108-86-162.5 125
Bromochloromethane ND ug/L 11/16/22 11:31 74-97-562.5 125
Bromodichloromethane ND ug/L 11/16/22 11:31 75-27-462.5 125
Bromoform ND ug/L 11/16/22 11:31 75-25-262.5 125
Bromomethane ND ug/L 11/16/22 11:31 74-83-9625 125
tert-Butyl Alcohol ND ug/L 11/16/22 11:31 75-65-06250 125
n-Butylbenzene 97.6 ug/L 11/16/22 11:31 104-51-862.5 125
sec-Butylbenzene ND ug/L 11/16/22 11:31 135-98-862.5 125
tert-Butylbenzene ND ug/L 11/16/22 11:31 98-06-662.5 125
tert-Butyl Formate ND ug/L 11/16/22 11:31 762-75-46250 125
Carbon tetrachloride ND ug/L 11/16/22 11:31 56-23-562.5 125
Chlorobenzene ND ug/L 11/16/22 11:31 108-90-762.5 125
Chloroethane ND ug/L 11/16/22 11:31 75-00-3125 125
Chloroform ND ug/L 11/16/22 11:31 67-66-362.5 125
Chloromethane ND ug/L 11/16/22 11:31 74-87-3125 125
2-Chlorotoluene ND ug/L 11/16/22 11:31 95-49-862.5 125
4-Chlorotoluene ND ug/L 11/16/22 11:31 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 11/16/22 11:31 96-12-8125 125
Dibromochloromethane ND ug/L 11/16/22 11:31 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 11/16/22 11:31 106-93-462.5 125
Dibromomethane ND ug/L 11/16/22 11:31 74-95-362.5 125
1,2-Dichlorobenzene ND ug/L 11/16/22 11:31 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 11/16/22 11:31 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 11/16/22 11:31 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 11/16/22 11:31 75-71-862.5 125
1,1-Dichloroethane ND ug/L 11/16/22 11:31 75-34-362.5 125
1,2-Dichloroethane ND ug/L 11/16/22 11:31 107-06-262.5 125
1,1-Dichloroethene ND ug/L 11/16/22 11:31 75-35-462.5 125
cis-1,2-Dichloroethene ND ug/L 11/16/22 11:31 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 11/16/22 11:31 156-60-562.5 125
1,2-Dichloropropane ND ug/L 11/16/22 11:31 78-87-562.5 125
1,3-Dichloropropane ND ug/L 11/16/22 11:31 142-28-962.5 125
2,2-Dichloropropane ND ug/L 11/16/22 11:31 594-20-762.5 125
1,1-Dichloropropene ND ug/L 11/16/22 11:31 563-58-662.5 125
cis-1,3-Dichloropropene ND ug/L 11/16/22 11:31 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 11/16/22 11:31 10061-02-662.5 125
Diisopropyl ether 120 ug/L 11/16/22 11:31 108-20-362.5 125
Ethanol ND ug/L 11/16/22 11:31 64-17-525000 125
Ethylbenzene 2140 ug/L 11/16/22 11:31 100-41-462.5 125
Ethyl-tert-butyl ether ND ug/L 11/16/22 11:31 637-92-31250 125
Hexachloro-1,3-butadiene ND ug/L 11/16/22 11:31 87-68-3250 125
Isopropylbenzene (Cumene)102 ug/L 11/16/22 11:31 98-82-862.5 125
Methylene Chloride ND ug/L 11/16/22 11:31 75-09-2250 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-21 Lab ID: 92636177006 Collected: 11/08/22 13:00 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 79.7 ug/L 11/16/22 11:31 1634-04-462.5 125
Naphthalene 621 ug/L 11/16/22 11:31 91-20-3250 125
n-Propylbenzene 285 ug/L 11/16/22 11:31 103-65-162.5 125
Styrene ND ug/L 11/16/22 11:31 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 11/16/22 11:31 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 11/16/22 11:31 79-34-562.5 125
Tetrachloroethene ND ug/L 11/16/22 11:31 127-18-462.5 125
Toluene 3170 ug/L 11/16/22 11:31 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 11/16/22 11:31 87-61-6250 125
1,2,4-Trichlorobenzene ND ug/L 11/16/22 11:31 120-82-1250 125
1,1,1-Trichloroethane ND ug/L 11/16/22 11:31 71-55-662.5 125
1,1,2-Trichloroethane ND ug/L 11/16/22 11:31 79-00-562.5 125
Trichloroethene ND ug/L 11/16/22 11:31 79-01-662.5 125
Trichlorofluoromethane ND ug/L 11/16/22 11:31 75-69-4125 125
1,2,3-Trichloropropane ND ug/L 11/16/22 11:31 96-18-462.5 125
1,2,4-Trimethylbenzene 1980 ug/L 11/16/22 11:31 95-63-662.5 125
1,3,5-Trimethylbenzene 562 ug/L 11/16/22 11:31 108-67-862.5 125
Vinyl chloride ND ug/L 11/16/22 11:31 75-01-4125 125
m&p-Xylene 5600 ug/L 11/16/22 11:31 179601-23-1125 125
o-Xylene 2170 ug/L 11/16/22 11:31 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/16/22 11:31 17060-07-070-130 125
4-Bromofluorobenzene (S)98 %11/16/22 11:31 460-00-470-130 125
Toluene-d8 (S)100 %11/16/22 11:31 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-23 Lab ID: 92636177007 Collected: 11/09/22 08:45 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/16/22 10:37 75-85-42000 20
tert-Amylmethyl ether ND ug/L 11/16/22 10:37 994-05-8200 20
Benzene 1350 ug/L 11/16/22 10:37 71-43-210.0 20
Bromobenzene ND ug/L 11/16/22 10:37 108-86-110.0 20
Bromochloromethane ND ug/L 11/16/22 10:37 74-97-510.0 20
Bromodichloromethane ND ug/L 11/16/22 10:37 75-27-410.0 20
Bromoform ND ug/L 11/16/22 10:37 75-25-210.0 20
Bromomethane ND ug/L 11/16/22 10:37 74-83-9100 20
tert-Butyl Alcohol ND ug/L 11/16/22 10:37 75-65-01000 20
n-Butylbenzene 107 ug/L 11/16/22 10:37 104-51-810.0 20
sec-Butylbenzene ND ug/L 11/16/22 10:37 135-98-810.0 20
tert-Butylbenzene ND ug/L 11/16/22 10:37 98-06-610.0 20
tert-Butyl Formate ND ug/L 11/16/22 10:37 762-75-41000 20
Carbon tetrachloride ND ug/L 11/16/22 10:37 56-23-510.0 20
Chlorobenzene ND ug/L 11/16/22 10:37 108-90-710.0 20
Chloroethane ND ug/L 11/16/22 10:37 75-00-320.0 20
Chloroform ND ug/L 11/16/22 10:37 67-66-310.0 20
Chloromethane ND ug/L 11/16/22 10:37 74-87-320.0 20
2-Chlorotoluene ND ug/L 11/16/22 10:37 95-49-810.0 20
4-Chlorotoluene ND ug/L 11/16/22 10:37 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 11/16/22 10:37 96-12-820.0 20
Dibromochloromethane ND ug/L 11/16/22 10:37 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 11/16/22 10:37 106-93-410.0 20
Dibromomethane ND ug/L 11/16/22 10:37 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 11/16/22 10:37 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 11/16/22 10:37 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 11/16/22 10:37 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 11/16/22 10:37 75-71-810.0 20
1,1-Dichloroethane ND ug/L 11/16/22 10:37 75-34-310.0 20
1,2-Dichloroethane ND ug/L 11/16/22 10:37 107-06-210.0 20
1,1-Dichloroethene ND ug/L 11/16/22 10:37 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 11/16/22 10:37 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 11/16/22 10:37 156-60-510.0 20
1,2-Dichloropropane ND ug/L 11/16/22 10:37 78-87-510.0 20
1,3-Dichloropropane ND ug/L 11/16/22 10:37 142-28-910.0 20
2,2-Dichloropropane ND ug/L 11/16/22 10:37 594-20-710.0 20
1,1-Dichloropropene ND ug/L 11/16/22 10:37 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 11/16/22 10:37 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 11/16/22 10:37 10061-02-610.0 20
Diisopropyl ether ND ug/L 11/16/22 10:37 108-20-310.0 20
Ethanol ND ug/L 11/16/22 10:37 64-17-54000 20
Ethylbenzene 2300 ug/L 11/16/22 10:37 100-41-410.0 20
Ethyl-tert-butyl ether ND ug/L 11/16/22 10:37 637-92-3200 20
Hexachloro-1,3-butadiene ND ug/L 11/16/22 10:37 87-68-340.0 20
Isopropylbenzene (Cumene)131 ug/L 11/16/22 10:37 98-82-810.0 20
Methylene Chloride ND ug/L 11/16/22 10:37 75-09-240.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-23 Lab ID: 92636177007 Collected: 11/09/22 08:45 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/16/22 10:37 1634-04-410.0 20
Naphthalene 738 ug/L 11/16/22 10:37 91-20-340.0 20
n-Propylbenzene 356 ug/L 11/16/22 10:37 103-65-110.0 20
Styrene ND ug/L 11/16/22 10:37 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 11/16/22 10:37 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 11/16/22 10:37 79-34-510.0 20
Tetrachloroethene ND ug/L 11/16/22 10:37 127-18-410.0 20
Toluene 301 ug/L 11/16/22 10:37 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 11/16/22 10:37 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 11/16/22 10:37 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 11/16/22 10:37 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 11/16/22 10:37 79-00-510.0 20
Trichloroethene ND ug/L 11/16/22 10:37 79-01-610.0 20
Trichlorofluoromethane ND ug/L 11/16/22 10:37 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 11/16/22 10:37 96-18-410.0 20
1,2,4-Trimethylbenzene 1030 ug/L 11/16/22 10:37 95-63-610.0 20
1,3,5-Trimethylbenzene 160 ug/L 11/16/22 10:37 108-67-810.0 20
Vinyl chloride ND ug/L 11/16/22 10:37 75-01-420.0 20
m&p-Xylene 1060 ug/L 11/16/22 10:37 179601-23-120.0 20
o-Xylene 83.1 ug/L 11/16/22 10:37 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/16/22 10:37 17060-07-070-130 20
4-Bromofluorobenzene (S)97 %11/16/22 10:37 460-00-470-130 20
Toluene-d8 (S)99 %11/16/22 10:37 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-30 Lab ID: 92636177008 Collected: 11/08/22 13:10 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/16/22 23:46 75-85-42000 20
tert-Amylmethyl ether ND ug/L 11/16/22 23:46 994-05-8200 20
Benzene 2360 ug/L 11/16/22 23:46 71-43-210.0 20
Bromobenzene ND ug/L 11/16/22 23:46 108-86-110.0 20
Bromochloromethane ND ug/L 11/16/22 23:46 74-97-510.0 20
Bromodichloromethane ND ug/L 11/16/22 23:46 75-27-410.0 20
Bromoform ND ug/L 11/16/22 23:46 75-25-210.0 20
Bromomethane ND ug/L 11/16/22 23:46 74-83-9100 20
tert-Butyl Alcohol ND ug/L 11/16/22 23:46 75-65-01000 20
n-Butylbenzene 21.0 ug/L 11/16/22 23:46 104-51-810.0 20
sec-Butylbenzene ND ug/L 11/16/22 23:46 135-98-810.0 20
tert-Butylbenzene ND ug/L 11/16/22 23:46 98-06-610.0 20
tert-Butyl Formate ND ug/L 11/16/22 23:46 762-75-41000 20
Carbon tetrachloride ND ug/L 11/16/22 23:46 56-23-510.0 20
Chlorobenzene ND ug/L 11/16/22 23:46 108-90-710.0 20
Chloroethane ND ug/L 11/16/22 23:46 75-00-320.0 20
Chloroform ND ug/L 11/16/22 23:46 67-66-310.0 20
Chloromethane ND ug/L 11/16/22 23:46 74-87-320.0 20
2-Chlorotoluene ND ug/L 11/16/22 23:46 95-49-810.0 20
4-Chlorotoluene ND ug/L 11/16/22 23:46 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 11/16/22 23:46 96-12-820.0 20
Dibromochloromethane ND ug/L 11/16/22 23:46 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 11/16/22 23:46 106-93-410.0 20
Dibromomethane ND ug/L 11/16/22 23:46 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 11/16/22 23:46 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 11/16/22 23:46 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 11/16/22 23:46 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 11/16/22 23:46 75-71-810.0 20
1,1-Dichloroethane ND ug/L 11/16/22 23:46 75-34-310.0 20
1,2-Dichloroethane ND ug/L 11/16/22 23:46 107-06-210.0 20
1,1-Dichloroethene ND ug/L 11/16/22 23:46 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 11/16/22 23:46 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 11/16/22 23:46 156-60-510.0 20
1,2-Dichloropropane ND ug/L 11/16/22 23:46 78-87-510.0 20
1,3-Dichloropropane ND ug/L 11/16/22 23:46 142-28-910.0 20
2,2-Dichloropropane ND ug/L 11/16/22 23:46 594-20-710.0 20
1,1-Dichloropropene ND ug/L 11/16/22 23:46 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 11/16/22 23:46 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 11/16/22 23:46 10061-02-610.0 20
Diisopropyl ether 98.7 ug/L 11/16/22 23:46 108-20-310.0 20
Ethanol ND ug/L 11/16/22 23:46 64-17-54000 20
Ethylbenzene 311 ug/L 11/16/22 23:46 100-41-410.0 20
Ethyl-tert-butyl ether ND ug/L 11/16/22 23:46 637-92-3200 20
Hexachloro-1,3-butadiene ND ug/L 11/16/22 23:46 87-68-340.0 20
Isopropylbenzene (Cumene)20.1 ug/L 11/16/22 23:46 98-82-810.0 20
Methylene Chloride ND ug/L 11/16/22 23:46 75-09-240.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: MW-30 Lab ID: 92636177008 Collected: 11/08/22 13:10 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 507 ug/L 11/16/22 23:46 1634-04-410.0 20
Naphthalene 118 ug/L 11/16/22 23:46 91-20-340.0 20
n-Propylbenzene 48.2 ug/L 11/16/22 23:46 103-65-110.0 20
Styrene ND ug/L 11/16/22 23:46 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 11/16/22 23:46 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 11/16/22 23:46 79-34-510.0 20
Tetrachloroethene ND ug/L 11/16/22 23:46 127-18-410.0 20
Toluene 103 ug/L 11/16/22 23:46 108-88-310.0 20
1,2,3-Trichlorobenzene ND ug/L 11/16/22 23:46 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 11/16/22 23:46 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 11/16/22 23:46 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 11/16/22 23:46 79-00-510.0 20
Trichloroethene ND ug/L 11/16/22 23:46 79-01-610.0 20
Trichlorofluoromethane ND ug/L 11/16/22 23:46 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 11/16/22 23:46 96-18-410.0 20
1,2,4-Trimethylbenzene 167 ug/L 11/16/22 23:46 95-63-610.0 20
1,3,5-Trimethylbenzene 41.8 ug/L 11/16/22 23:46 108-67-810.0 20
Vinyl chloride ND ug/L 11/16/22 23:46 75-01-420.0 20
m&p-Xylene 181 ug/L 11/16/22 23:46 179601-23-120.0 20
o-Xylene 17.2 ug/L 11/16/22 23:46 95-47-610.0 20
Surrogates
1,2-Dichloroethane-d4 (S)100 %11/16/22 23:46 17060-07-070-130 20
4-Bromofluorobenzene (S)97 %11/16/22 23:46 460-00-470-130 20
Toluene-d8 (S)98 %11/16/22 23:46 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: TRIP BLANK Lab ID: 92636177009 Collected: 11/08/22 00:00 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 11/14/22 18:16 75-85-4100 1
tert-Amylmethyl ether ND ug/L 11/14/22 18:16 994-05-810.0 1
Benzene ND ug/L 11/14/22 18:16 71-43-20.50 1
Bromobenzene ND ug/L 11/14/22 18:16 108-86-10.50 1
Bromochloromethane ND ug/L 11/14/22 18:16 74-97-50.50 1
Bromodichloromethane ND ug/L 11/14/22 18:16 75-27-40.50 1
Bromoform ND ug/L 11/14/22 18:16 75-25-20.50 1
Bromomethane ND ug/L 11/14/22 18:16 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 11/14/22 18:16 75-65-050.0 1
n-Butylbenzene ND ug/L 11/14/22 18:16 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/14/22 18:16 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/14/22 18:16 98-06-60.50 1
tert-Butyl Formate ND ug/L 11/14/22 18:16 762-75-450.0 1
Carbon tetrachloride ND ug/L 11/14/22 18:16 56-23-50.50 1
Chlorobenzene ND ug/L 11/14/22 18:16 108-90-70.50 1
Chloroethane ND ug/L 11/14/22 18:16 75-00-31.0 1
Chloroform ND ug/L 11/14/22 18:16 67-66-30.50 1
Chloromethane ND ug/L 11/14/22 18:16 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/14/22 18:16 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/14/22 18:16 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/14/22 18:16 96-12-81.0 1
Dibromochloromethane ND ug/L 11/14/22 18:16 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/14/22 18:16 106-93-40.50 1
Dibromomethane ND ug/L 11/14/22 18:16 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/14/22 18:16 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/14/22 18:16 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/14/22 18:16 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/14/22 18:16 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/14/22 18:16 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/14/22 18:16 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/14/22 18:16 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/14/22 18:16 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/14/22 18:16 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/14/22 18:16 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/14/22 18:16 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/14/22 18:16 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/14/22 18:16 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/14/22 18:16 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/14/22 18:16 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/14/22 18:16 108-20-30.50 1
Ethanol ND ug/L 11/14/22 18:16 64-17-5200 1
Ethylbenzene ND ug/L 11/14/22 18:16 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 11/14/22 18:16 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 11/14/22 18:16 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/14/22 18:16 98-82-80.50 1
Methylene Chloride ND ug/L 11/14/22 18:16 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Sample: TRIP BLANK Lab ID: 92636177009 Collected: 11/08/22 00:00 Received: 11/10/22 09:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 11/14/22 18:16 1634-04-40.50 1
Naphthalene ND ug/L 11/14/22 18:16 91-20-32.0 1
n-Propylbenzene ND ug/L 11/14/22 18:16 103-65-10.50 1
Styrene ND ug/L 11/14/22 18:16 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/14/22 18:16 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/14/22 18:16 79-34-50.50 1
Tetrachloroethene ND ug/L 11/14/22 18:16 127-18-40.50 1
Toluene ND ug/L 11/14/22 18:16 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/14/22 18:16 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/14/22 18:16 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/14/22 18:16 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/14/22 18:16 79-00-50.50 1
Trichloroethene ND ug/L 11/14/22 18:16 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/14/22 18:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/14/22 18:16 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/14/22 18:16 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/14/22 18:16 108-67-80.50 1
Vinyl chloride ND ug/L 11/14/22 18:16 75-01-41.0 1
m&p-Xylene ND ug/L 11/14/22 18:16 179601-23-11.0 1
o-Xylene ND ug/L 11/14/22 18:16 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/14/22 18:16 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %11/14/22 18:16 460-00-470-130 1
Toluene-d8 (S)106 %11/14/22 18:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
736786
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92636177009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3834449
Associated Lab Samples:92636177009
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/14/22 16:46
1,1,1-Trichloroethane ug/L ND 0.50 11/14/22 16:46
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/14/22 16:46
1,1,2-Trichloroethane ug/L ND 0.50 11/14/22 16:46
1,1-Dichloroethane ug/L ND 0.50 11/14/22 16:46
1,1-Dichloroethene ug/L ND 0.50 11/14/22 16:46
1,1-Dichloropropene ug/L ND 0.50 11/14/22 16:46
1,2,3-Trichlorobenzene ug/L ND 2.0 11/14/22 16:46
1,2,3-Trichloropropane ug/L ND 0.50 11/14/22 16:46
1,2,4-Trichlorobenzene ug/L ND 2.0 11/14/22 16:46
1,2,4-Trimethylbenzene ug/L ND 0.50 11/14/22 16:46
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/14/22 16:46
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/14/22 16:46
1,2-Dichlorobenzene ug/L ND 0.50 11/14/22 16:46
1,2-Dichloroethane ug/L ND 0.50 11/14/22 16:46
1,2-Dichloropropane ug/L ND 0.50 11/14/22 16:46
1,3,5-Trimethylbenzene ug/L ND 0.50 11/14/22 16:46
1,3-Dichlorobenzene ug/L ND 0.50 11/14/22 16:46
1,3-Dichloropropane ug/L ND 0.50 11/14/22 16:46
1,4-Dichlorobenzene ug/L ND 0.50 11/14/22 16:46
2,2-Dichloropropane ug/L ND 0.50 11/14/22 16:46
2-Chlorotoluene ug/L ND 0.50 11/14/22 16:46
4-Chlorotoluene ug/L ND 0.50 11/14/22 16:46
Benzene ug/L ND 0.50 11/14/22 16:46
Bromobenzene ug/L ND 0.50 11/14/22 16:46
Bromochloromethane ug/L ND 0.50 11/14/22 16:46
Bromodichloromethane ug/L ND 0.50 11/14/22 16:46
Bromoform ug/L ND 0.50 11/14/22 16:46
Bromomethane ug/L ND 5.0 11/14/22 16:46
Carbon tetrachloride ug/L ND 0.50 11/14/22 16:46
Chlorobenzene ug/L ND 0.50 11/14/22 16:46
Chloroethane ug/L ND 1.0 11/14/22 16:46
Chloroform ug/L ND 0.50 11/14/22 16:46
Chloromethane ug/L ND 1.0 11/14/22 16:46
cis-1,2-Dichloroethene ug/L ND 0.50 11/14/22 16:46
cis-1,3-Dichloropropene ug/L ND 0.50 11/14/22 16:46
Dibromochloromethane ug/L ND 0.50 11/14/22 16:46
Dibromomethane ug/L ND 0.50 11/14/22 16:46
Dichlorodifluoromethane ug/L ND 0.50 11/14/22 16:46
Diisopropyl ether ug/L ND 0.50 11/14/22 16:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3834449
Associated Lab Samples:92636177009
Matrix: Water
Analyzed
Ethanol ug/L ND 200 11/14/22 16:46
Ethyl-tert-butyl ether ug/L ND 10.0 11/14/22 16:46
Ethylbenzene ug/L ND 0.50 11/14/22 16:46
Hexachloro-1,3-butadiene ug/L ND 2.0 11/14/22 16:46
Isopropylbenzene (Cumene)ug/L ND 0.50 11/14/22 16:46
m&p-Xylene ug/L ND 1.0 11/14/22 16:46
Methyl-tert-butyl ether ug/L ND 0.50 11/14/22 16:46
Methylene Chloride ug/L ND 2.0 11/14/22 16:46
n-Butylbenzene ug/L ND 0.50 11/14/22 16:46
n-Propylbenzene ug/L ND 0.50 11/14/22 16:46
Naphthalene ug/L ND 2.0 11/14/22 16:46
o-Xylene ug/L ND 0.50 11/14/22 16:46
sec-Butylbenzene ug/L ND 0.50 11/14/22 16:46
Styrene ug/L ND 0.50 11/14/22 16:46
tert-Amyl Alcohol ug/L ND 100 11/14/22 16:46
tert-Amylmethyl ether ug/L ND 10.0 11/14/22 16:46
tert-Butyl Alcohol ug/L ND 50.0 11/14/22 16:46
tert-Butyl Formate ug/L ND 50.0 11/14/22 16:46
tert-Butylbenzene ug/L ND 0.50 11/14/22 16:46
Tetrachloroethene ug/L ND 0.50 11/14/22 16:46
Toluene ug/L ND 0.50 11/14/22 16:46
trans-1,2-Dichloroethene ug/L ND 0.50 11/14/22 16:46
trans-1,3-Dichloropropene ug/L ND 0.50 11/14/22 16:46
Trichloroethene ug/L ND 0.50 11/14/22 16:46
Trichlorofluoromethane ug/L ND 1.0 11/14/22 16:46
Vinyl chloride ug/L ND 1.0 11/14/22 16:46
1,2-Dichloroethane-d4 (S)%91 70-130 11/14/22 16:46
4-Bromofluorobenzene (S)%101 70-130 11/14/22 16:46
Toluene-d8 (S)%107 70-130 11/14/22 16:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834450LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 43.450 87 60-140
1,1,1-Trichloroethane ug/L 38.750 77 60-140
1,1,2,2-Tetrachloroethane ug/L 43.050 86 60-140
1,1,2-Trichloroethane ug/L 44.950 90 60-140
1,1-Dichloroethane ug/L 38.750 77 60-140
1,1-Dichloroethene ug/L 35.450 71 60-140
1,1-Dichloropropene ug/L 35.050 70 60-140
1,2,3-Trichlorobenzene ug/L 45.950 92 60-140
1,2,3-Trichloropropane ug/L 41.650 83 60-140
1,2,4-Trichlorobenzene ug/L 45.450 91 60-140
1,2,4-Trimethylbenzene ug/L 42.250 84 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834450LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 39.250 78 60-140
1,2-Dibromoethane (EDB)ug/L 39.350 79 60-140
1,2-Dichlorobenzene ug/L 42.350 85 60-140
1,2-Dichloroethane ug/L 40.850 82 60-140
1,2-Dichloropropane ug/L 39.450 79 60-140
1,3,5-Trimethylbenzene ug/L 42.650 85 60-140
1,3-Dichlorobenzene ug/L 40.850 82 60-140
1,3-Dichloropropane ug/L 44.250 88 60-140
1,4-Dichlorobenzene ug/L 41.150 82 60-140
2,2-Dichloropropane ug/L 38.650 77 60-140
2-Chlorotoluene ug/L 41.050 82 60-140
4-Chlorotoluene ug/L 41.750 83 60-140
Benzene ug/L 38.150 76 60-140
Bromobenzene ug/L 41.850 84 60-140
Bromochloromethane ug/L 42.750 85 60-140
Bromodichloromethane ug/L 42.350 85 60-140
Bromoform ug/L 41.150 82 60-140
Bromomethane ug/L 33.450 67 60-140
Carbon tetrachloride ug/L 37.250 74 60-140
Chlorobenzene ug/L 40.350 81 60-140
Chloroethane ug/L 35.750 71 60-140
Chloroform ug/L 38.950 78 60-140
Chloromethane ug/L 36.850 74 60-140
cis-1,2-Dichloroethene ug/L 40.050 80 60-140
cis-1,3-Dichloropropene ug/L 38.450 77 60-140
Dibromochloromethane ug/L 44.850 90 60-140
Dibromomethane ug/L 41.150 82 60-140
Dichlorodifluoromethane ug/L 32.650 65 60-140
Diisopropyl ether ug/L 34.950 70 60-140
Ethanol ug/L 17102000 86 60-140
Ethyl-tert-butyl ether ug/L 67.5100 67 60-140
Ethylbenzene ug/L 40.550 81 60-140
Hexachloro-1,3-butadiene ug/L 41.550 83 60-140
Isopropylbenzene (Cumene)ug/L 40.050 80 60-140
m&p-Xylene ug/L 79.8100 80 60-140
Methyl-tert-butyl ether ug/L 34.550 69 60-140
Methylene Chloride ug/L 42.950 86 60-140
n-Butylbenzene ug/L 44.150 88 60-140
n-Propylbenzene ug/L 40.950 82 60-140
Naphthalene ug/L 48.650 97 60-140
o-Xylene ug/L 41.250 82 60-140
sec-Butylbenzene ug/L 41.650 83 60-140
Styrene ug/L 43.450 87 60-140
tert-Amyl Alcohol ug/L 7131000 71 60-140
tert-Amylmethyl ether ug/L 83.6100 84 60-140
tert-Butyl Alcohol ug/L 320500 64 60-140
tert-Butyl Formate ug/L 293400 73 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834450LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 35.650 71 60-140
Tetrachloroethene ug/L 38.950 78 60-140
Toluene ug/L 38.050 76 60-140
trans-1,2-Dichloroethene ug/L 38.850 78 60-140
trans-1,3-Dichloropropene ug/L 38.850 78 60-140
Trichloroethene ug/L 41.050 82 60-140
Trichlorofluoromethane ug/L 30.650 61 60-140
Vinyl chloride ug/L 37.950 76 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3834451MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92634373014
3834452
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L H1250010660-140104 22500ND2650 2610
1,1,1-Trichloroethane ug/L H1250011160-140113 22500ND2770 2820
1,1,2,2-Tetrachloroethane ug/L H1250010960-140113 42500ND2730 2840
1,1,2-Trichloroethane ug/L H1250010960-140110 12500ND2730 2760
1,1-Dichloroethane ug/L H1250012260-140123 02500ND3060 3070
1,1-Dichloroethene ug/L H1250012560-140126 02500ND3130 3140
1,1-Dichloropropene ug/L H1250010960-140108 02500ND2720 2710
1,2,3-Trichlorobenzene ug/L H1250010260-140106 42500ND2550 2650
1,2,3-Trichloropropane ug/L H1250010460-140107 32500ND2600 2680
1,2,4-Trichlorobenzene ug/L H1250010360-140106 32500ND2570 2650
1,2,4-Trimethylbenzene ug/L H1250011060-140124 5250037506500 6850
1,2-Dibromo-3-chloropropane ug/L H125009260-14092 02500ND2300 2300
1,2-Dibromoethane (EDB)ug/L H125009960-140101 22500ND2460 2520
1,2-Dichlorobenzene ug/L H1250010660-140104 32500ND2660 2590
1,2-Dichloroethane ug/L H1250011060-140109 12500ND2760 2730
1,2-Dichloropropane ug/L H1250011160-140112 12500ND2760 2800
1,3,5-Trimethylbenzene ug/L H1250011260-140116 325009413730 3830
1,3-Dichlorobenzene ug/L H1250010260-140103 12500ND2550 2570
1,3-Dichloropropane ug/L H1250011260-140112 02500ND2790 2790
1,4-Dichlorobenzene ug/L H1250010360-140102 12500ND2570 2540
2,2-Dichloropropane ug/L H1250010060-140101 12500ND2500 2520
2-Chlorotoluene ug/L H125009760-14096 02500ND2420 2410
4-Chlorotoluene ug/L H1250010860-140107 02500ND2700 2690
Benzene ug/L H1250012260-140121 0250036206670 6640
Bromobenzene ug/L H1250010460-140106 12500ND2610 2650
Bromochloromethane ug/L H1250012560-140125 02500ND3130 3120
Bromodichloromethane ug/L H1250010160-140104 32500ND2520 2590
Bromoform ug/L H125008960-14091 32500ND2220 2290
Bromomethane ug/L H125006860-14090 282500ND1710 2260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3834451MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92634373014
3834452
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L H125009760-140100 32500ND2430 2510
Chlorobenzene ug/L H1250010560-140106 02500ND2630 2640
Chloroethane ug/L H1,M1250014360-140145 22500ND3580 3630
Chloroform ug/L H1250011260-140110 22500ND2810 2760
Chloromethane ug/L H1250013060-140132 22500ND3240 3310
cis-1,2-Dichloroethene ug/L H1250012260-140124 22500ND3050 3100
cis-1,3-Dichloropropene ug/L H125009560-14096 12500ND2370 2390
Dibromochloromethane ug/L H1250010360-140103 02500ND2590 2590
Dibromomethane ug/L H1250010460-140108 42500ND2590 2700
Dichlorodifluoromethane ug/L H1250010060-14099 02500ND2490 2480
Diisopropyl ether ug/L H1250010960-140106 22500ND2710 2660
Ethanol ug/L H110000012160-140126 4100000ND121000 126000
Ethyl-tert-butyl ether ug/L H150009360-14094 15000ND4640 4680
Ethylbenzene ug/L H1250011160-140113 1250023205100 5150
Hexachloro-1,3-butadiene ug/L H125009660-140100 42500ND2400 2490
Isopropylbenzene (Cumene) ug/L H1250010460-140107 325001462740 2820
m&p-Xylene ug/L H1500010560-140114 35000901014300 14700
Methyl-tert-butyl ether ug/L H1250010660-140104 22500ND2650 2590
Methylene Chloride ug/L H1250012360-140128 42500ND3070 3200
n-Butylbenzene ug/L H1250011860-140122 32500ND2950 3040
n-Propylbenzene ug/L H1250010760-140109 125005053190 3240
Naphthalene ug/L H1250011060-140119 5250015804330 4570
o-Xylene ug/L H1250011060-140118 3250046807430 7630
sec-Butylbenzene ug/L H1250010960-140113 32500ND2720 2820
Styrene ug/L H1250011160-140113 22500ND2780 2820
tert-Amyl Alcohol ug/L H1500008460-14084 050000ND42000 42000
tert-Amylmethyl ether ug/L H1500010760-140109 25000ND5360 5440
tert-Butyl Alcohol ug/L H1250008760-14084 325000ND21600 21000
tert-Butyl Formate ug/L H1200009660-14098 220000ND19200 19600
tert-Butylbenzene ug/L H125009360-14093 02500ND2320 2320
Tetrachloroethene ug/L H1250010160-140105 42500ND2530 2630
Toluene ug/L H1,M125005860-14057 025002010021500 21500
trans-1,2-Dichloroethene ug/L H1250012560-140125 02500ND3110 3120
trans-1,3-Dichloropropene ug/L H125008960-14092 32500ND2230 2300
Trichloroethene ug/L H1250011260-140113 12500ND2790 2820
Trichlorofluoromethane ug/L H1250010660-140107 12500ND2640 2680
Vinyl chloride ug/L H1,M1250013860-140144 42500ND3440 3590
1,2-Dichloroethane-d4 (S)%94 70-13093
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
736788
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92636177001, 92636177002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3834455
Associated Lab Samples:92636177001, 92636177002
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/14/22 11:50
1,1,1-Trichloroethane ug/L ND 0.50 11/14/22 11:50
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/14/22 11:50
1,1,2-Trichloroethane ug/L ND 0.50 11/14/22 11:50
1,1-Dichloroethane ug/L ND 0.50 11/14/22 11:50
1,1-Dichloroethene ug/L ND 0.50 11/14/22 11:50
1,1-Dichloropropene ug/L ND 0.50 11/14/22 11:50
1,2,3-Trichlorobenzene ug/L ND 2.0 11/14/22 11:50
1,2,3-Trichloropropane ug/L ND 0.50 11/14/22 11:50
1,2,4-Trichlorobenzene ug/L ND 2.0 11/14/22 11:50
1,2,4-Trimethylbenzene ug/L ND 0.50 11/14/22 11:50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/14/22 11:50
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/14/22 11:50
1,2-Dichlorobenzene ug/L ND 0.50 11/14/22 11:50
1,2-Dichloroethane ug/L ND 0.50 11/14/22 11:50
1,2-Dichloropropane ug/L ND 0.50 11/14/22 11:50
1,3,5-Trimethylbenzene ug/L ND 0.50 11/14/22 11:50
1,3-Dichlorobenzene ug/L ND 0.50 11/14/22 11:50
1,3-Dichloropropane ug/L ND 0.50 11/14/22 11:50
1,4-Dichlorobenzene ug/L ND 0.50 11/14/22 11:50
2,2-Dichloropropane ug/L ND 0.50 11/14/22 11:50
2-Chlorotoluene ug/L ND 0.50 11/14/22 11:50
4-Chlorotoluene ug/L ND 0.50 11/14/22 11:50
Benzene ug/L ND 0.50 11/14/22 11:50
Bromobenzene ug/L ND 0.50 11/14/22 11:50
Bromochloromethane ug/L ND 0.50 11/14/22 11:50
Bromodichloromethane ug/L ND 0.50 11/14/22 11:50
Bromoform ug/L ND 0.50 11/14/22 11:50
Bromomethane ug/L ND 5.0 11/14/22 11:50
Carbon tetrachloride ug/L ND 0.50 11/14/22 11:50
Chlorobenzene ug/L ND 0.50 11/14/22 11:50
Chloroethane ug/L ND 1.0 11/14/22 11:50
Chloroform ug/L ND 0.50 11/14/22 11:50
Chloromethane ug/L ND 1.0 11/14/22 11:50
cis-1,2-Dichloroethene ug/L ND 0.50 11/14/22 11:50
cis-1,3-Dichloropropene ug/L ND 0.50 11/14/22 11:50
Dibromochloromethane ug/L ND 0.50 11/14/22 11:50
Dibromomethane ug/L ND 0.50 11/14/22 11:50
Dichlorodifluoromethane ug/L ND 0.50 11/14/22 11:50
Diisopropyl ether ug/L ND 0.50 11/14/22 11:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3834455
Associated Lab Samples:92636177001, 92636177002
Matrix: Water
Analyzed
Ethanol ug/L ND 200 11/14/22 11:50
Ethyl-tert-butyl ether ug/L ND 10.0 11/14/22 11:50
Ethylbenzene ug/L ND 0.50 11/14/22 11:50
Hexachloro-1,3-butadiene ug/L ND 2.0 11/14/22 11:50
Isopropylbenzene (Cumene)ug/L ND 0.50 11/14/22 11:50
m&p-Xylene ug/L ND 1.0 11/14/22 11:50
Methyl-tert-butyl ether ug/L ND 0.50 11/14/22 11:50
Methylene Chloride ug/L ND 2.0 11/14/22 11:50
n-Butylbenzene ug/L ND 0.50 11/14/22 11:50
n-Propylbenzene ug/L ND 0.50 11/14/22 11:50
Naphthalene ug/L ND 2.0 11/14/22 11:50
o-Xylene ug/L ND 0.50 11/14/22 11:50
sec-Butylbenzene ug/L ND 0.50 11/14/22 11:50
Styrene ug/L ND 0.50 11/14/22 11:50
tert-Amyl Alcohol ug/L ND 100 11/14/22 11:50
tert-Amylmethyl ether ug/L ND 10.0 11/14/22 11:50
tert-Butyl Alcohol ug/L ND 50.0 11/14/22 11:50
tert-Butyl Formate ug/L ND 50.0 11/14/22 11:50
tert-Butylbenzene ug/L ND 0.50 11/14/22 11:50
Tetrachloroethene ug/L ND 0.50 11/14/22 11:50
Toluene ug/L ND 0.50 11/14/22 11:50
trans-1,2-Dichloroethene ug/L ND 0.50 11/14/22 11:50
trans-1,3-Dichloropropene ug/L ND 0.50 11/14/22 11:50
Trichloroethene ug/L ND 0.50 11/14/22 11:50
Trichlorofluoromethane ug/L ND 1.0 11/14/22 11:50
Vinyl chloride ug/L ND 1.0 11/14/22 11:50
1,2-Dichloroethane-d4 (S)%101 70-130 11/14/22 11:50
4-Bromofluorobenzene (S)%101 70-130 11/14/22 11:50
Toluene-d8 (S)%103 70-130 11/14/22 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834456LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 60-140
1,1,1-Trichloroethane ug/L 51.650 103 60-140
1,1,2,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,2-Trichloroethane ug/L 52.250 104 60-140
1,1-Dichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethene ug/L 52.650 105 60-140
1,1-Dichloropropene ug/L 57.850 116 60-140
1,2,3-Trichlorobenzene ug/L 49.950 100 60-140
1,2,3-Trichloropropane ug/L 45.150 90 60-140
1,2,4-Trichlorobenzene ug/L 49.450 99 60-140
1,2,4-Trimethylbenzene ug/L 48.250 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834456LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 47.450 95 60-140
1,2-Dibromoethane (EDB)ug/L 52.250 104 60-140
1,2-Dichlorobenzene ug/L 49.350 99 60-140
1,2-Dichloroethane ug/L 49.950 100 60-140
1,2-Dichloropropane ug/L 50.950 102 60-140
1,3,5-Trimethylbenzene ug/L 51.050 102 60-140
1,3-Dichlorobenzene ug/L 50.550 101 60-140
1,3-Dichloropropane ug/L 50.250 100 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 53.850 108 60-140
2-Chlorotoluene ug/L 45.350 91 60-140
4-Chlorotoluene ug/L 45.350 91 60-140
Benzene ug/L 48.750 97 60-140
Bromobenzene ug/L 49.250 98 60-140
Bromochloromethane ug/L 54.950 110 60-140
Bromodichloromethane ug/L 52.150 104 60-140
Bromoform ug/L 54.550 109 60-140
Bromomethane ug/L 48.750 97 60-140
Carbon tetrachloride ug/L 53.150 106 60-140
Chlorobenzene ug/L 50.250 100 60-140
Chloroethane ug/L 47.450 95 60-140
Chloroform ug/L 50.350 101 60-140
Chloromethane ug/L 55.250 110 60-140
cis-1,2-Dichloroethene ug/L 51.450 103 60-140
cis-1,3-Dichloropropene ug/L 52.750 105 60-140
Dibromochloromethane ug/L 54.150 108 60-140
Dibromomethane ug/L 51.050 102 60-140
Dichlorodifluoromethane ug/L 51.650 103 60-140
Diisopropyl ether ug/L 51.450 103 60-140
Ethanol ug/L 19102000 96 60-140
Ethyl-tert-butyl ether ug/L 99.3100 99 60-140
Ethylbenzene ug/L 49.950 100 60-140
Hexachloro-1,3-butadiene ug/L 53.350 107 60-140
Isopropylbenzene (Cumene)ug/L 50.250 100 60-140
m&p-Xylene ug/L 100100 100 60-140
Methyl-tert-butyl ether ug/L 51.350 103 60-140
Methylene Chloride ug/L 50.550 101 60-140
n-Butylbenzene ug/L 52.750 105 60-140
n-Propylbenzene ug/L 50.150 100 60-140
Naphthalene ug/L 49.450 99 60-140
o-Xylene ug/L 50.650 101 60-140
sec-Butylbenzene ug/L 49.150 98 60-140
Styrene ug/L 52.850 106 60-140
tert-Amyl Alcohol ug/L 9481000 95 60-140
tert-Amylmethyl ether ug/L 101100 101 60-140
tert-Butyl Alcohol ug/L 481500 96 60-140
tert-Butyl Formate ug/L 412400 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3834456LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 42.750 85 60-140
Tetrachloroethene ug/L 53.250 106 60-140
Toluene ug/L 50.550 101 60-140
trans-1,2-Dichloroethene ug/L 52.850 106 60-140
trans-1,3-Dichloropropene ug/L 52.850 106 60-140
Trichloroethene ug/L 53.850 108 60-140
Trichlorofluoromethane ug/L 48.150 96 60-140
Vinyl chloride ug/L 57.250 114 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3834783MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636136001
3834784
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 118 60-140114 420ND23.6 22.7
1,1,1-Trichloroethane ug/L 20 112 60-140113 120ND22.5 22.7
1,1,2,2-Tetrachloroethane ug/L 20 116 60-140109 620ND23.1 21.8
1,1,2-Trichloroethane ug/L 20 116 60-140115 120ND23.2 22.9
1,1-Dichloroethane ug/L 20 103 60-140104 220ND20.5 20.8
1,1-Dichloroethene ug/L 20 105 60-140103 220ND21.0 20.6
1,1-Dichloropropene ug/L 20 123 60-140125 120ND24.7 25.0
1,2,3-Trichlorobenzene ug/L 20 126 60-140112 1220ND25.2 22.5
1,2,3-Trichloropropane ug/L 20 100 60-140110 1020ND20.1 22.1
1,2,4-Trichlorobenzene ug/L 20 120 60-140109 1020ND24.1 21.7
1,2,4-Trimethylbenzene ug/L 20 114 60-140109 420ND22.7 21.8
1,2-Dibromo-3-chloropropane ug/L 20 112 60-140103 920ND22.5 20.5
1,2-Dibromoethane (EDB)ug/L 20 113 60-140112 120ND22.5 22.4
1,2-Dichlorobenzene ug/L 20 115 60-140107 720ND23.0 21.5
1,2-Dichloroethane ug/L 20 106 60-140108 220ND21.1 21.6
1,2-Dichloropropane ug/L 20 109 60-140110 020ND21.8 21.9
1,3,5-Trimethylbenzene ug/L 20 121 60-140115 520ND24.3 23.0
1,3-Dichlorobenzene ug/L 20 115 60-140110 420ND22.9 22.1
1,3-Dichloropropane ug/L 20 110 60-140110 020ND22.0 22.0
1,4-Dichlorobenzene ug/L 20 113 60-140108 420ND22.5 21.7
2,2-Dichloropropane ug/L 20 116 60-140118 220ND23.2 23.7
2-Chlorotoluene ug/L 20 114 60-140100 1320ND22.9 20.1
4-Chlorotoluene ug/L 20 114 60-140100 1320ND22.9 20.1
Benzene ug/L 20 102 60-140100 220ND20.5 20.1
Bromobenzene ug/L 20 111 60-140109 220ND22.2 21.7
Bromochloromethane ug/L 20 116 60-140116 020ND23.2 23.2
Bromodichloromethane ug/L 20 114 60-140115 120ND22.8 23.0
Bromoform ug/L 20 117 60-140112 420ND23.4 22.4
Bromomethane ug/L 20 118 60-140108 920ND23.7 21.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3834783MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636136001
3834784
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 20 115 60-140115 020ND22.9 22.9
Chlorobenzene ug/L 20 114 60-140112 220ND22.9 22.4
Chloroethane ug/L 20 112 60-140113 120ND22.3 22.6
Chloroform ug/L 20 114 60-140112 120ND22.8 22.5
Chloromethane ug/L 20 106 60-140104 220ND21.3 20.9
cis-1,2-Dichloroethene ug/L 20 110 60-140112 220ND22.0 22.3
cis-1,3-Dichloropropene ug/L 20 117 60-140115 220ND23.4 23.0
Dibromochloromethane ug/L 20 115 60-140113 220ND23.1 22.6
Dibromomethane ug/L 20 111 60-140107 420ND22.2 21.4
Dichlorodifluoromethane ug/L 20 109 60-140105 320ND21.7 21.0
Diisopropyl ether ug/L 20 102 60-140103 120ND20.7 20.9
Ethanol ug/L 800 119 60-140110 8800ND956 879
Ethyl-tert-butyl ether ug/L 40 99 60-140101 240ND39.4 40.2
Ethylbenzene ug/L 20 117 60-140114 320ND23.5 22.8
Hexachloro-1,3-butadiene ug/L 20 140 60-140128 920ND27.9 25.6
Isopropylbenzene (Cumene) ug/L 20 118 60-140115 320ND23.7 23.0
m&p-Xylene ug/L 40 117 60-140116 140ND46.9 46.3
Methyl-tert-butyl ether ug/L 20 108 60-140112 3204.5 26.2 26.9
Methylene Chloride ug/L 20 97 60-14096 120ND19.4 19.2
n-Butylbenzene ug/L 20 127 60-140120 620ND25.4 24.0
n-Propylbenzene ug/L 20 119 60-140113 420ND23.7 22.7
Naphthalene ug/L 20 121 60-140107 1220ND24.1 21.4
o-Xylene ug/L 20 116 60-140116 020ND23.2 23.2
sec-Butylbenzene ug/L 20 123 60-140116 620ND24.6 23.3
Styrene ug/L 20 113 60-140115 120ND22.7 23.0
tert-Amyl Alcohol ug/L 400 108 60-140103 4400ND430 412
tert-Amylmethyl ether ug/L 40 103 60-140103 040ND41.1 41.2
tert-Butyl Alcohol ug/L 200 115 60-140116 0200ND230 231
tert-Butyl Formate ug/L 160 81 60-14074 10160ND130 118
tert-Butylbenzene ug/L 20 104 60-14098 620ND20.8 19.7
Tetrachloroethene ug/L 20 116 60-140115 120ND23.2 23.0
Toluene ug/L 20 113 60-140111 220ND22.7 22.2
trans-1,2-Dichloroethene ug/L 20 109 60-140109 020ND21.8 21.8
trans-1,3-Dichloropropene ug/L 20 117 60-140113 320ND23.4 22.6
Trichloroethene ug/L 20 120 60-140115 420ND24.0 23.0
Trichlorofluoromethane ug/L 20 102 60-140103 020ND20.4 20.5
Vinyl chloride ug/L 20 111 60-140107 320ND22.1 21.5
1,2-Dichloroethane-d4 (S)%98 70-130102
4-Bromofluorobenzene (S)%102 70-130104
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
737275
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92636177003, 92636177004, 92636177006, 92636177007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3837123
Associated Lab Samples:92636177003, 92636177004, 92636177006, 92636177007
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/16/22 02:26
1,1,1-Trichloroethane ug/L ND 0.50 11/16/22 02:26
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/16/22 02:26
1,1,2-Trichloroethane ug/L ND 0.50 11/16/22 02:26
1,1-Dichloroethane ug/L ND 0.50 11/16/22 02:26
1,1-Dichloroethene ug/L ND 0.50 11/16/22 02:26
1,1-Dichloropropene ug/L ND 0.50 11/16/22 02:26
1,2,3-Trichlorobenzene ug/L ND 2.0 11/16/22 02:26
1,2,3-Trichloropropane ug/L ND 0.50 11/16/22 02:26
1,2,4-Trichlorobenzene ug/L ND 2.0 11/16/22 02:26
1,2,4-Trimethylbenzene ug/L ND 0.50 11/16/22 02:26
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/16/22 02:26
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/16/22 02:26
1,2-Dichlorobenzene ug/L ND 0.50 11/16/22 02:26
1,2-Dichloroethane ug/L ND 0.50 11/16/22 02:26
1,2-Dichloropropane ug/L ND 0.50 11/16/22 02:26
1,3,5-Trimethylbenzene ug/L ND 0.50 11/16/22 02:26
1,3-Dichlorobenzene ug/L ND 0.50 11/16/22 02:26
1,3-Dichloropropane ug/L ND 0.50 11/16/22 02:26
1,4-Dichlorobenzene ug/L ND 0.50 11/16/22 02:26
2,2-Dichloropropane ug/L ND 0.50 11/16/22 02:26
2-Chlorotoluene ug/L ND 0.50 11/16/22 02:26
4-Chlorotoluene ug/L ND 0.50 11/16/22 02:26
Benzene ug/L ND 0.50 11/16/22 02:26
Bromobenzene ug/L ND 0.50 11/16/22 02:26
Bromochloromethane ug/L ND 0.50 11/16/22 02:26
Bromodichloromethane ug/L ND 0.50 11/16/22 02:26
Bromoform ug/L ND 0.50 11/16/22 02:26
Bromomethane ug/L ND 5.0 11/16/22 02:26
Carbon tetrachloride ug/L ND 0.50 11/16/22 02:26
Chlorobenzene ug/L ND 0.50 11/16/22 02:26
Chloroethane ug/L ND 1.0 11/16/22 02:26
Chloroform ug/L ND 0.50 11/16/22 02:26
Chloromethane ug/L ND 1.0 11/16/22 02:26
cis-1,2-Dichloroethene ug/L ND 0.50 11/16/22 02:26
cis-1,3-Dichloropropene ug/L ND 0.50 11/16/22 02:26
Dibromochloromethane ug/L ND 0.50 11/16/22 02:26
Dibromomethane ug/L ND 0.50 11/16/22 02:26
Dichlorodifluoromethane ug/L ND 0.50 11/16/22 02:26
Diisopropyl ether ug/L ND 0.50 11/16/22 02:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3837123
Associated Lab Samples:92636177003, 92636177004, 92636177006, 92636177007
Matrix: Water
Analyzed
Ethanol ug/L ND 200 11/16/22 02:26
Ethyl-tert-butyl ether ug/L ND 10.0 11/16/22 02:26
Ethylbenzene ug/L ND 0.50 11/16/22 02:26
Hexachloro-1,3-butadiene ug/L ND 2.0 11/16/22 02:26
Isopropylbenzene (Cumene)ug/L ND 0.50 11/16/22 02:26
m&p-Xylene ug/L ND 1.0 11/16/22 02:26
Methyl-tert-butyl ether ug/L ND 0.50 11/16/22 02:26
Methylene Chloride ug/L ND 2.0 11/16/22 02:26
n-Butylbenzene ug/L ND 0.50 11/16/22 02:26
n-Propylbenzene ug/L ND 0.50 11/16/22 02:26
Naphthalene ug/L ND 2.0 11/16/22 02:26
o-Xylene ug/L ND 0.50 11/16/22 02:26
sec-Butylbenzene ug/L ND 0.50 11/16/22 02:26
Styrene ug/L ND 0.50 11/16/22 02:26
tert-Amyl Alcohol ug/L ND 100 11/16/22 02:26
tert-Amylmethyl ether ug/L ND 10.0 11/16/22 02:26
tert-Butyl Alcohol ug/L ND 50.0 11/16/22 02:26
tert-Butyl Formate ug/L ND 50.0 11/16/22 02:26
tert-Butylbenzene ug/L ND 0.50 11/16/22 02:26
Tetrachloroethene ug/L ND 0.50 11/16/22 02:26
Toluene ug/L ND 0.50 11/16/22 02:26
trans-1,2-Dichloroethene ug/L ND 0.50 11/16/22 02:26
trans-1,3-Dichloropropene ug/L ND 0.50 11/16/22 02:26
Trichloroethene ug/L ND 0.50 11/16/22 02:26
Trichlorofluoromethane ug/L ND 1.0 11/16/22 02:26
Vinyl chloride ug/L ND 1.0 11/16/22 02:26
1,2-Dichloroethane-d4 (S)%99 70-130 11/16/22 02:26
4-Bromofluorobenzene (S)%98 70-130 11/16/22 02:26
Toluene-d8 (S)%100 70-130 11/16/22 02:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3837124LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 60-140
1,1,1-Trichloroethane ug/L 47.750 95 60-140
1,1,2,2-Tetrachloroethane ug/L 48.250 96 60-140
1,1,2-Trichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethane ug/L 45.650 91 60-140
1,1-Dichloroethene ug/L 48.650 97 60-140
1,1-Dichloropropene ug/L 49.950 100 60-140
1,2,3-Trichlorobenzene ug/L 50.750 101 60-140
1,2,3-Trichloropropane ug/L 46.950 94 60-140
1,2,4-Trichlorobenzene ug/L 48.750 97 60-140
1,2,4-Trimethylbenzene ug/L 47.350 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3837124LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 48.650 97 60-140
1,2-Dibromoethane (EDB)ug/L 49.650 99 60-140
1,2-Dichlorobenzene ug/L 48.150 96 60-140
1,2-Dichloroethane ug/L 47.750 95 60-140
1,2-Dichloropropane ug/L 50.250 100 60-140
1,3,5-Trimethylbenzene ug/L 46.450 93 60-140
1,3-Dichlorobenzene ug/L 47.750 95 60-140
1,3-Dichloropropane ug/L 47.750 95 60-140
1,4-Dichlorobenzene ug/L 45.550 91 60-140
2,2-Dichloropropane ug/L 44.050 88 60-140
2-Chlorotoluene ug/L 44.750 89 60-140
4-Chlorotoluene ug/L 45.650 91 60-140
Benzene ug/L 46.650 93 60-140
Bromobenzene ug/L 47.350 95 60-140
Bromochloromethane ug/L 49.250 98 60-140
Bromodichloromethane ug/L 49.850 100 60-140
Bromoform ug/L 51.250 102 60-140
Bromomethane ug/L 49.050 98 60-140
Carbon tetrachloride ug/L 46.150 92 60-140
Chlorobenzene ug/L 48.150 96 60-140
Chloroethane ug/L 49.950 100 60-140
Chloroform ug/L 44.450 89 60-140
Chloromethane ug/L 52.950 106 60-140
cis-1,2-Dichloroethene ug/L 45.850 92 60-140
cis-1,3-Dichloropropene ug/L 48.950 98 60-140
Dibromochloromethane ug/L 49.650 99 60-140
Dibromomethane ug/L 52.650 105 60-140
Dichlorodifluoromethane ug/L 54.850 110 60-140
Diisopropyl ether ug/L 45.350 91 60-140
Ethanol ug/L 15502000 78 60-140
Ethyl-tert-butyl ether ug/L 90.5100 90 60-140
Ethylbenzene ug/L 46.150 92 60-140
Hexachloro-1,3-butadiene ug/L 45.550 91 60-140
Isopropylbenzene (Cumene)ug/L 46.550 93 60-140
m&p-Xylene ug/L 93.2100 93 60-140
Methyl-tert-butyl ether ug/L 48.550 97 60-140
Methylene Chloride ug/L 48.950 98 60-140
n-Butylbenzene ug/L 45.950 92 60-140
n-Propylbenzene ug/L 44.150 88 60-140
Naphthalene ug/L 52.250 104 60-140
o-Xylene ug/L 47.950 96 60-140
sec-Butylbenzene ug/L 44.350 89 60-140
Styrene ug/L 49.350 99 60-140
tert-Amyl Alcohol ug/L 8921000 89 60-140
tert-Amylmethyl ether ug/L 97.3100 97 60-140
tert-Butyl Alcohol ug/L 438500 88 60-140
tert-Butyl Formate ug/L 374400 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3837124LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 39.150 78 60-140
Tetrachloroethene ug/L 47.250 94 60-140
Toluene ug/L 46.450 93 60-140
trans-1,2-Dichloroethene ug/L 47.150 94 60-140
trans-1,3-Dichloropropene ug/L 49.250 98 60-140
Trichloroethene ug/L 50.950 102 60-140
Trichlorofluoromethane ug/L 43.550 87 60-140
Vinyl chloride ug/L 49.350 99 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3837125MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636177006
3837126
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 112 60-140111 12500ND2800 2770
1,1,1-Trichloroethane ug/L 2500 103 60-140102 02500ND2570 2560
1,1,2,2-Tetrachloroethane ug/L 2500 107 60-140109 22500ND2670 2720
1,1,2-Trichloroethane ug/L 2500 110 60-140108 22500ND2740 2690
1,1-Dichloroethane ug/L 2500 96 60-14094 12500ND2390 2350
1,1-Dichloroethene ug/L 2500 98 60-14096 22500ND2440 2390
1,1-Dichloropropene ug/L 2500 106 60-140105 12500ND2660 2620
1,2,3-Trichlorobenzene ug/L 2500 116 60-140115 12500ND2900 2870
1,2,3-Trichloropropane ug/L 2500 104 60-140111 72500ND2590 2780
1,2,4-Trichlorobenzene ug/L 2500 113 60-140108 52500ND2830 2700
1,2,4-Trimethylbenzene ug/L 2500 110 60-140112 1250019804730 4780
1,2-Dibromo-3-chloropropane ug/L 2500 104 60-140106 22500ND2600 2660
1,2-Dibromoethane (EDB)ug/L 2500 109 60-140109 02500ND2740 2730
1,2-Dichlorobenzene ug/L 2500 109 60-140109 02500ND2730 2730
1,2-Dichloroethane ug/L 2500 104 60-140104 02500ND2610 2610
1,2-Dichloropropane ug/L 2500 109 60-140108 12500ND2720 2690
1,3,5-Trimethylbenzene ug/L 2500 107 60-140106 125005623250 3220
1,3-Dichlorobenzene ug/L 2500 108 60-140106 12500ND2700 2660
1,3-Dichloropropane ug/L 2500 106 60-140107 22500ND2640 2680
1,4-Dichlorobenzene ug/L 2500 104 60-140102 22500ND2610 2560
2,2-Dichloropropane ug/L 2500 82 60-14081 12500ND2040 2030
2-Chlorotoluene ug/L 2500 113 60-140112 12500ND2830 2790
4-Chlorotoluene ug/L 2500 105 60-140101 42500ND2620 2520
Benzene ug/L 2500 82 60-14071 225001420016300 16000
Bromobenzene ug/L 2500 107 60-140107 12500ND2680 2670
Bromochloromethane ug/L 2500 103 60-140102 12500ND2580 2550
Bromodichloromethane ug/L 2500 107 60-140107 02500ND2690 2690
Bromoform ug/L 2500 105 60-140106 12500ND2630 2660
Bromomethane ug/L 2500 99 60-14096 32500ND2480 2400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3837125MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636177006
3837126
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 2500 101 60-14098 32500ND2540 2450
Chlorobenzene ug/L 2500 108 60-140109 12500ND2710 2720
Chloroethane ug/L 2500 103 60-140103 12500ND2580 2560
Chloroform ug/L 2500 94 60-14098 42500ND2340 2450
Chloromethane ug/L 2500 97 60-14095 22500ND2430 2380
cis-1,2-Dichloroethene ug/L 2500 96 60-14095 12500ND2400 2380
cis-1,3-Dichloropropene ug/L 2500 104 60-140103 12500ND2600 2580
Dibromochloromethane ug/L 2500 106 60-140108 12500ND2660 2690
Dibromomethane ug/L 2500 112 60-140111 12500ND2800 2770
Dichlorodifluoromethane ug/L 2500 85 60-14083 22500ND2140 2080
Diisopropyl ether ug/L 2500 95 60-14096 025001202500 2510
Ethanol ug/L 100000 87 60-14089 2100000ND87200 89100
Ethyl-tert-butyl ether ug/L 5000 94 60-14094 05000ND4700 4720
Ethylbenzene ug/L 2500 107 60-140107 0250021404820 4810
Hexachloro-1,3-butadiene ug/L 2500 108 60-140107 12500ND2700 2670
Isopropylbenzene (Cumene) ug/L 2500 107 60-140108 025001022790 2790
m&p-Xylene ug/L 5000 107 60-140106 05000560010900 10900
Methyl-tert-butyl ether ug/L 2500 100 60-14099 1250079.7 2580 2560
Methylene Chloride ug/L 2500 101 60-140100 12500ND2520 2500
n-Butylbenzene ug/L 2500 106 60-140102 3250097.6 2740 2650
n-Propylbenzene ug/L 2500 103 60-140100 325002852850 2770
Naphthalene ug/L 2500 120 60-140123 225006213620 3700
o-Xylene ug/L 2500 107 60-140110 1250021704850 4910
sec-Butylbenzene ug/L 2500 107 60-140104 32500ND2680 2600
Styrene ug/L 2500 112 60-140109 22500ND2790 2730
tert-Amyl Alcohol ug/L 50000 102 60-140100 250000ND51100 49800
tert-Amylmethyl ether ug/L 5000 103 60-140102 05000ND5130 5110
tert-Butyl Alcohol ug/L 25000 96 60-14095 125000ND24000 23800
tert-Butyl Formate ug/L 20000 99 60-14099 020000ND19700 19700
tert-Butylbenzene ug/L 2500 93 60-14092 22500ND2340 2290
Tetrachloroethene ug/L 2500 107 60-140106 12500ND2690 2650
Toluene ug/L 2500 101 60-14097 2250031705680 5580
trans-1,2-Dichloroethene ug/L 2500 97 60-14096 12500ND2420 2390
trans-1,3-Dichloropropene ug/L 2500 103 60-140104 12500ND2580 2590
Trichloroethene ug/L 2500 110 60-140109 12500ND2740 2720
Trichlorofluoromethane ug/L 2500 89 60-14087 22500ND2220 2180
Vinyl chloride ug/L 2500 90 60-14088 22500ND2250 2210
1,2-Dichloroethane-d4 (S)%98 70-13097
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
737556
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92636177005, 92636177008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3838437
Associated Lab Samples:92636177005, 92636177008
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/16/22 19:14
1,1,1-Trichloroethane ug/L ND 0.50 11/16/22 19:14
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/16/22 19:14
1,1,2-Trichloroethane ug/L ND 0.50 11/16/22 19:14
1,1-Dichloroethane ug/L ND 0.50 11/16/22 19:14
1,1-Dichloroethene ug/L ND 0.50 11/16/22 19:14
1,1-Dichloropropene ug/L ND 0.50 11/16/22 19:14
1,2,3-Trichlorobenzene ug/L ND 2.0 11/16/22 19:14
1,2,3-Trichloropropane ug/L ND 0.50 11/16/22 19:14
1,2,4-Trichlorobenzene ug/L ND 2.0 11/16/22 19:14
1,2,4-Trimethylbenzene ug/L ND 0.50 11/16/22 19:14
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/16/22 19:14
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/16/22 19:14
1,2-Dichlorobenzene ug/L ND 0.50 11/16/22 19:14
1,2-Dichloroethane ug/L ND 0.50 11/16/22 19:14
1,2-Dichloropropane ug/L ND 0.50 11/16/22 19:14
1,3,5-Trimethylbenzene ug/L ND 0.50 11/16/22 19:14
1,3-Dichlorobenzene ug/L ND 0.50 11/16/22 19:14
1,3-Dichloropropane ug/L ND 0.50 11/16/22 19:14
1,4-Dichlorobenzene ug/L ND 0.50 11/16/22 19:14
2,2-Dichloropropane ug/L ND 0.50 11/16/22 19:14
2-Chlorotoluene ug/L ND 0.50 11/16/22 19:14
4-Chlorotoluene ug/L ND 0.50 11/16/22 19:14
Benzene ug/L ND 0.50 11/16/22 19:14
Bromobenzene ug/L ND 0.50 11/16/22 19:14
Bromochloromethane ug/L ND 0.50 11/16/22 19:14
Bromodichloromethane ug/L ND 0.50 11/16/22 19:14
Bromoform ug/L ND 0.50 11/16/22 19:14
Bromomethane ug/L ND 5.0 11/16/22 19:14
Carbon tetrachloride ug/L ND 0.50 11/16/22 19:14
Chlorobenzene ug/L ND 0.50 11/16/22 19:14
Chloroethane ug/L ND 1.0 11/16/22 19:14
Chloroform ug/L ND 0.50 11/16/22 19:14
Chloromethane ug/L ND 1.0 11/16/22 19:14
cis-1,2-Dichloroethene ug/L ND 0.50 11/16/22 19:14
cis-1,3-Dichloropropene ug/L ND 0.50 11/16/22 19:14
Dibromochloromethane ug/L ND 0.50 11/16/22 19:14
Dibromomethane ug/L ND 0.50 11/16/22 19:14
Dichlorodifluoromethane ug/L ND 0.50 11/16/22 19:14
Diisopropyl ether ug/L ND 0.50 11/16/22 19:14
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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Page 37 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3838437
Associated Lab Samples:92636177005, 92636177008
Matrix: Water
Analyzed
Ethanol ug/L ND 200 11/16/22 19:14
Ethyl-tert-butyl ether ug/L ND 10.0 11/16/22 19:14
Ethylbenzene ug/L ND 0.50 11/16/22 19:14
Hexachloro-1,3-butadiene ug/L ND 2.0 11/16/22 19:14
Isopropylbenzene (Cumene)ug/L ND 0.50 11/16/22 19:14
m&p-Xylene ug/L ND 1.0 11/16/22 19:14
Methyl-tert-butyl ether ug/L ND 0.50 11/16/22 19:14
Methylene Chloride ug/L ND 2.0 11/16/22 19:14
n-Butylbenzene ug/L ND 0.50 11/16/22 19:14
n-Propylbenzene ug/L ND 0.50 11/16/22 19:14
Naphthalene ug/L ND 2.0 11/16/22 19:14
o-Xylene ug/L ND 0.50 11/16/22 19:14
sec-Butylbenzene ug/L ND 0.50 11/16/22 19:14
Styrene ug/L ND 0.50 11/16/22 19:14
tert-Amyl Alcohol ug/L ND 100 11/16/22 19:14
tert-Amylmethyl ether ug/L ND 10.0 11/16/22 19:14
tert-Butyl Alcohol ug/L ND 50.0 11/16/22 19:14
tert-Butyl Formate ug/L ND 50.0 11/16/22 19:14
tert-Butylbenzene ug/L ND 0.50 11/16/22 19:14
Tetrachloroethene ug/L ND 0.50 11/16/22 19:14
Toluene ug/L ND 0.50 11/16/22 19:14
trans-1,2-Dichloroethene ug/L ND 0.50 11/16/22 19:14
trans-1,3-Dichloropropene ug/L ND 0.50 11/16/22 19:14
Trichloroethene ug/L ND 0.50 11/16/22 19:14
Trichlorofluoromethane ug/L ND 1.0 11/16/22 19:14
Vinyl chloride ug/L ND 1.0 11/16/22 19:14
1,2-Dichloroethane-d4 (S)%98 70-130 11/16/22 19:14
4-Bromofluorobenzene (S)%98 70-130 11/16/22 19:14
Toluene-d8 (S)%100 70-130 11/16/22 19:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3838438LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.150 106 60-140
1,1,1-Trichloroethane ug/L 49.450 99 60-140
1,1,2,2-Tetrachloroethane ug/L 51.550 103 60-140
1,1,2-Trichloroethane ug/L 51.650 103 60-140
1,1-Dichloroethane ug/L 47.250 94 60-140
1,1-Dichloroethene ug/L 51.250 102 60-140
1,1-Dichloropropene ug/L 52.950 106 60-140
1,2,3-Trichlorobenzene ug/L 53.550 107 60-140
1,2,3-Trichloropropane ug/L 52.750 105 60-140
1,2,4-Trichlorobenzene ug/L 51.650 103 60-140
1,2,4-Trimethylbenzene ug/L 51.450 103 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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Page 38 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3838438LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 51.650 103 60-140
1,2-Dibromoethane (EDB)ug/L 53.650 107 60-140
1,2-Dichlorobenzene ug/L 51.450 103 60-140
1,2-Dichloroethane ug/L 49.550 99 60-140
1,2-Dichloropropane ug/L 52.350 105 60-140
1,3,5-Trimethylbenzene ug/L 50.050 100 60-140
1,3-Dichlorobenzene ug/L 51.150 102 60-140
1,3-Dichloropropane ug/L 51.150 102 60-140
1,4-Dichlorobenzene ug/L 49.450 99 60-140
2,2-Dichloropropane ug/L 49.550 99 60-140
2-Chlorotoluene ug/L 47.950 96 60-140
4-Chlorotoluene ug/L 49.050 98 60-140
Benzene ug/L 48.750 97 60-140
Bromobenzene ug/L 50.750 101 60-140
Bromochloromethane ug/L 51.150 102 60-140
Bromodichloromethane ug/L 52.150 104 60-140
Bromoform ug/L 55.050 110 60-140
Bromomethane ug/L 47.550 95 60-140
Carbon tetrachloride ug/L 48.250 96 60-140
Chlorobenzene ug/L 50.650 101 60-140
Chloroethane ug/L 52.450 105 60-140
Chloroform ug/L 46.750 93 60-140
Chloromethane ug/L 51.850 104 60-140
cis-1,2-Dichloroethene ug/L 47.950 96 60-140
cis-1,3-Dichloropropene ug/L 51.450 103 60-140
Dibromochloromethane ug/L 52.650 105 60-140
Dibromomethane ug/L 54.750 109 60-140
Dichlorodifluoromethane ug/L 56.550 113 60-140
Diisopropyl ether ug/L 48.250 96 60-140
Ethanol ug/L 16502000 83 60-140
Ethyl-tert-butyl ether ug/L 94.9100 95 60-140
Ethylbenzene ug/L 49.650 99 60-140
Hexachloro-1,3-butadiene ug/L 50.650 101 60-140
Isopropylbenzene (Cumene)ug/L 49.650 99 60-140
m&p-Xylene ug/L 99.5100 100 60-140
Methyl-tert-butyl ether ug/L 51.550 103 60-140
Methylene Chloride ug/L 49.350 99 60-140
n-Butylbenzene ug/L 50.250 100 60-140
n-Propylbenzene ug/L 48.050 96 60-140
Naphthalene ug/L 55.150 110 60-140
o-Xylene ug/L 50.450 101 60-140
sec-Butylbenzene ug/L 48.650 97 60-140
Styrene ug/L 52.350 105 60-140
tert-Amyl Alcohol ug/L 9731000 97 60-140
tert-Amylmethyl ether ug/L 104100 104 60-140
tert-Butyl Alcohol ug/L 462500 92 60-140
tert-Butyl Formate ug/L 398400 99 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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Huntersville, NC 28078
[phone]
Page 39 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3838438LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 42.650 85 60-140
Tetrachloroethene ug/L 52.250 104 60-140
Toluene ug/L 48.250 96 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 52.050 104 60-140
Trichloroethene ug/L 53.350 107 60-140
Trichlorofluoromethane ug/L 45.950 92 60-140
Vinyl chloride ug/L 52.750 105 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3838439MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636177005
3838440
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 132 60-140137 32500ND3310 3420
1,1,1-Trichloroethane ug/L M1250014260-140140 12500ND3540 3500
1,1,2,2-Tetrachloroethane ug/L 2500 128 60-140131 22500ND3210 3270
1,1,2-Trichloroethane ug/L 2500 130 60-140133 22500ND3240 3330
1,1-Dichloroethane ug/L 2500 138 60-140132 42500ND3440 3310
1,1-Dichloroethene ug/L M1250014760-140147 02500ND3680 3670
1,1-Dichloropropene ug/L M1250014860-140148 02500ND3700 3690
1,2,3-Trichlorobenzene ug/L 2500 123 60-140137 112500ND3070 3420
1,2,3-Trichloropropane ug/L 2500 129 60-140127 22500ND3220 3170
1,2,4-Trichlorobenzene ug/L 2500 124 60-140128 42500ND3100 3210
1,2,4-Trimethylbenzene ug/L 2500 127 60-140130 225002803470 3530
1,2-Dibromo-3-chloropropane ug/L 2500 122 60-140128 52500ND3060 3210
1,2-Dibromoethane (EDB)ug/L 2500 133 60-140137 32500ND3330 3430
1,2-Dichlorobenzene ug/L 2500 128 60-140131 32500ND3190 3280
1,2-Dichloroethane ug/L 2500 138 60-140136 22500ND3450 3390
1,2-Dichloropropane ug/L 2500 139 60-140138 12500ND3480 3450
1,3,5-Trimethylbenzene ug/L 2500 126 60-140128 125001073260 3300
1,3-Dichlorobenzene ug/L 2500 125 60-140128 22500ND3140 3210
1,3-Dichloropropane ug/L 2500 130 60-140133 22500ND3260 3330
1,4-Dichlorobenzene ug/L 2500 123 60-140123 02500ND3070 3070
2,2-Dichloropropane ug/L 2500 128 60-140127 12500ND3190 3170
2-Chlorotoluene ug/L 2500 125 60-140125 12500ND3120 3130
4-Chlorotoluene ug/L 2500 123 60-140124 02500ND3080 3090
Benzene ug/L 2500 133 60-140131 1250022305560 5500
Bromobenzene ug/L 2500 130 60-140129 12500ND3250 3220
Bromochloromethane ug/L 2500 137 60-140138 12500ND3420 3450
Bromodichloromethane ug/L 2500 135 60-140133 22500ND3380 3320
Bromoform ug/L 2500 126 60-140132 42500ND3160 3290
Bromomethane ug/L 2500 116 60-140121 42500ND2900 3020
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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[phone]
Page 40 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3838439MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92636177005
3838440
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 2500 129 60-140131 12500ND3230 3270
Chlorobenzene ug/L 2500 130 60-140133 22500ND3250 3330
Chloroethane ug/L M1250016860-140165 12500ND4190 4140
Chloroform ug/L 2500 125 60-140123 22500ND3130 3080
Chloromethane ug/L M1250015160-140147 32500ND3780 3680
cis-1,2-Dichloroethene ug/L 2500 136 60-140128 62500ND3410 3200
cis-1,3-Dichloropropene ug/L 2500 130 60-140132 22500ND3240 3300
Dibromochloromethane ug/L 2500 129 60-140134 32500ND3230 3340
Dibromomethane ug/L M1250013860-140142 32500ND3440 3550
Dichlorodifluoromethane ug/L M1250016760-140165 12500ND4170 4130
Diisopropyl ether ug/L 2500 134 60-140131 325002293580 3490
Ethanol ug/L 100000 110 60-140109 1100000ND110000 109000
Ethyl-tert-butyl ether ug/L 5000 128 60-140126 15000ND6390 6310
Ethylbenzene ug/L 2500 129 60-140131 125005813810 3850
Hexachloro-1,3-butadiene ug/L 2500 121 60-140127 42500ND3030 3160
Isopropylbenzene (Cumene) ug/L 2500 126 60-140130 32500ND3210 3300
m&p-Xylene ug/L 5000 128 60-140131 250003136730 6850
Methyl-tert-butyl ether ug/L M1250021160-140189 325001650021800 21200
Methylene Chloride ug/L 2500 137 60-140128 72500ND3420 3190
n-Butylbenzene ug/L 2500 122 60-140125 22500ND3120 3190
n-Propylbenzene ug/L 2500 123 60-140122 125001443220 3200
Naphthalene ug/L M1250012760-140141 1025002593430 3790
o-Xylene ug/L 2500 129 60-140132 22500ND3230 3300
sec-Butylbenzene ug/L 2500 125 60-140126 12500ND3120 3150
Styrene ug/L 2500 130 60-140134 32500ND3250 3350
tert-Amyl Alcohol ug/L 50000 119 60-140124 450000ND59700 62100
tert-Amylmethyl ether ug/L 5000 128 60-140131 25000ND7390 7550
tert-Butyl Alcohol ug/L 25000 128 60-140130 125000ND32000 32400
tert-Butyl Formate ug/L 20000 129 60-140129 020000ND25700 25800
tert-Butylbenzene ug/L 2500 110 60-140110 02500ND2740 2750
Tetrachloroethene ug/L 2500 130 60-140133 32500ND3240 3330
Toluene ug/L 2500 128 60-140129 12500ND3230 3260
trans-1,2-Dichloroethene ug/L M1250014460-140138 42500ND3590 3460
trans-1,3-Dichloropropene ug/L 2500 128 60-140129 12500ND3190 3230
Trichloroethene ug/L M1250013960-140141 12500ND3480 3520
Trichlorofluoromethane ug/L 2500 137 60-140137 02500ND3420 3410
Vinyl chloride ug/L M1250015160-140149 12500ND3770 3740
1,2-Dichloroethane-d4 (S)%102 70-130100
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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[phone]
Page 41 of 46
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/06/2022 11:27 AM
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Page 42 of 46
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92636177
46865-6958 BURLINGTON NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92636177001 736788MWWB-1 SM 6200B
92636177002 736788MWWB-2 SM 6200B
92636177003 737275MWWB-3 SM 6200B
92636177004 737275MW-6R SM 6200B
92636177005 737556MW-15 SM 6200B
92636177006 737275MW-21 SM 6200B
92636177007 737275MW-23 SM 6200B
92636177008 737556MW-30 SM 6200B
92636177009 736786TRIP BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
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Page 43 of 46
Page 44 of 46
Page 45 of 46
Page 46 of 46
ANALYTICAL REPORT
March 29, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1475124
Samples Received:03/25/2022
Project Number:R0583.84
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
March 29, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/29/22 12:04 1 of 14
March 31, 2022
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/31/22 09:58 1 of 14
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
AIR STACK L1475124-01 5
Qc: Quality Control Summary 7
Volatile Organic Compounds (MS) by Method TO-15 7
Gl: Glossary of Terms 12
Al: Accreditations & Locations 13
Sc: Sample Chain of Custody 14
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/29/22 12:04 2 of 14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/31/22 09:58 2 of 14
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
AIR STACK L1475124-01 Air Gary A Fischer 03/24/22 07:30 03/25/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG1838974 80 03/28/22 01:33 03/28/22 01:33 MBF Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method TO-15 WG1839631 400 03/29/22 07:29 03/29/22 07:29 MBF Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/29/22 12:04 3 of 14
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Mid-Atlantic - Speedway NC R0583.84 L1475124 03/31/22 09:58 3 of 14
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
Sample Delivery Group (SDG) Narrative
Sample received in tedlar bag.
Lab Sample ID Project Sample ID Method
L1475124-01 AIR STACK TO-15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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T. Alan Harvill
Project Manager
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SAMPLE RESULTS - 01
L1475124
AIR STACK
Collected date/time: 03/24/22 07:30
Volatile Organic Compounds (MS) by Method TO-15
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 100 238 218 518 80 WG1838974
Allyl chloride 107-05-1 76.53 16.0 50.1 ND ND 80 WG1838974
Benzene 71-43-2 78.10 16.0 51.1 7380 23600 80 WG1838974
Benzyl Chloride 100-44-7 127 16.0 83.1 ND ND 80 WG1838974
Bromodichloromethane 75-27-4 164 16.0 107 ND ND 80 WG1838974
Bromoform 75-25-2 253 48.0 497 ND ND 80 WG1838974
Bromomethane 74-83-9 94.90 16.0 62.1 ND ND 80 WG1838974
1,3-Butadiene 106-99-0 54.10 160 354 ND ND 80 WG1838974
Carbon disulfide 75-15-0 76.10 16.0 49.8 ND ND 80 WG1838974
Carbon tetrachloride 56-23-5 154 16.0 101 ND ND 80 WG1838974
Chlorobenzene 108-90-7 113 16.0 73.9 ND ND 80 WG1838974
Chloroethane 75-00-3 64.50 16.0 42.2 ND ND 80 WG1838974
Chloroform 67-66-3 119 16.0 77.9 ND ND 80 WG1838974
Chloromethane 74-87-3 50.50 16.0 33.0 ND ND 80 WG1838974
2-Chlorotoluene 95-49-8 126 16.0 82.5 ND ND 80 WG1838974
Cyclohexane 110-82-7 84.20 16.0 55.1 3630 12500 80 WG1838974
Dibromochloromethane 124-48-1 208 16.0 136 ND ND 80 WG1838974
1,2-Dibromoethane 106-93-4 188 16.0 123 ND ND 80 WG1838974
1,2-Dichlorobenzene 95-50-1 147 16.0 96.2 ND ND 80 WG1838974
1,3-Dichlorobenzene 541-73-1 147 16.0 96.2 ND ND 80 WG1838974
1,4-Dichlorobenzene 106-46-7 147 16.0 96.2 ND ND 80 WG1838974
1,2-Dichloroethane 107-06-2 99 16.0 64.8 ND ND 80 WG1838974
1,1-Dichloroethane 75-34-3 98 16.0 64.1 ND ND 80 WG1838974
1,1-Dichloroethene 75-35-4 96.90 16.0 63.4 ND ND 80 WG1838974
cis-1,2-Dichloroethene 156-59-2 96.90 16.0 63.4 ND ND 80 WG1838974
trans-1,2-Dichloroethene 156-60-5 96.90 16.0 63.4 ND ND 80 WG1838974
1,2-Dichloropropane 78-87-5 113 16.0 73.9 ND ND 80 WG1838974
cis-1,3-Dichloropropene 10061-01-5 111 16.0 72.6 ND ND 80 WG1838974
trans-1,3-Dichloropropene 10061-02-6 111 16.0 72.6 ND ND 80 WG1838974
1,4-Dioxane 123-91-1 88.10 16.0 57.7 ND ND 80 WG1838974
Ethanol 64-17-5 46.10 100 189 351 662 80 WG1838974
Ethylbenzene 100-41-4 106 16.0 69.4 956 4140 80 WG1838974
4-Ethyltoluene 622-96-8 120 16.0 78.5 364 1790 80 WG1838974
Trichlorofluoromethane 75-69-4 137.40 16.0 89.9 ND ND 80 WG1838974
Dichlorodifluoromethane 75-71-8 120.92 16.0 79.1 ND ND 80 WG1838974
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 16.0 123 ND ND 80 WG1838974
1,2-Dichlorotetrafluoroethane 76-14-2 171 16.0 112 ND ND 80 WG1838974
Heptane 142-82-5 100 16.0 65.4 4040 16500 80 WG1838974
Hexachloro-1,3-butadiene 87-68-3 261 50.4 538 ND ND 80 WG1838974
n-Hexane 110-54-3 86.20 252 888 20600 72600 400 WG1839631
Isopropylbenzene 98-82-8 120.20 16.0 78.7 39.4 194 80 WG1838974
Methylene Chloride 75-09-2 84.90 16.0 55.6 ND ND 80 WG1838974
Methyl Butyl Ketone 591-78-6 100 100 409 ND ND 80 WG1838974
2-Butanone (MEK)78-93-3 72.10 100 295 ND ND 80 WG1838974
4-Methyl-2-pentanone (MIBK) 108-10-1 100.10 100 409 ND ND 80 WG1838974
Methyl methacrylate 80-62-6 100.12 16.0 65.5 ND ND 80 WG1838974
MTBE 1634-04-4 88.10 16.0 57.7 746 2690 80 WG1838974
Naphthalene 91-20-3 128 50.4 264 ND ND 80 WG1838974
2-Propanol 67-63-0 60.10 100 246 4520 11100 80 WG1838974
Propene 115-07-1 42.10 100 172 ND ND 80 WG1838974
Styrene 100-42-5 104 16.0 68.1 ND ND 80 WG1838974
1,1,2,2-Tetrachloroethane 79-34-5 168 16.0 110 ND ND 80 WG1838974
Tetrachloroethylene 127-18-4 166 16.0 109 ND ND 80 WG1838974
Tetrahydrofuran 109-99-9 72.10 16.0 47.2 ND ND 80 WG1838974
Toluene 108-88-3 92.10 40.0 151 685 2580 80 WG1838974
1,2,4-Trichlorobenzene 120-82-1 181 50.4 373 ND ND 80 WG1838974
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1475124
AIR STACK
Collected date/time: 03/24/22 07:30
Volatile Organic Compounds (MS) by Method TO-15
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
1,1,1-Trichloroethane 71-55-6 133 16.0 87.0 ND ND 80 WG1838974
1,1,2-Trichloroethane 79-00-5 133 16.0 87.0 ND ND 80 WG1838974
Trichloroethylene 79-01-6 131 16.0 85.7 ND ND 80 WG1838974
1,2,4-Trimethylbenzene 95-63-6 120 16.0 78.5 308 1510 80 WG1838974
1,3,5-Trimethylbenzene 108-67-8 120 16.0 78.5 172 844 80 WG1838974
2,2,4-Trimethylpentane 540-84-1 114.22 80.0 374 9500 44400 400 WG1839631
Vinyl chloride 75-01-4 62.50 16.0 40.9 ND ND 80 WG1838974
Vinyl Bromide 593-60-2 106.95 16.0 70.0 ND ND 80 WG1838974
Vinyl acetate 108-05-4 86.10 16.0 56.3 ND ND 80 WG1838974
m&p-Xylene 1330-20-7 106 32.0 139 2150 9320 80 WG1838974
o-Xylene 95-47-6 106 16.0 69.4 747 3240 80 WG1838974
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 95.9 WG1838974
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 100 WG1839631
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838974
Volatile Organic Compounds (MS) by Method TO-15 L1475124-01
Method Blank (MB)
(MB) R3774579-3 03/27/22 11:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Acetone U 0.584 1.25
Allyl Chloride U 0.114 0.200
Benzene U 0.0715 0.200
Benzyl Chloride U 0.0598 0.200
Bromodichloromethane U 0.0702 0.200
Bromoform U 0.0732 0.600
Bromomethane U 0.0982 0.200
1,3-Butadiene U 0.104 2.00
Carbon disulfide U 0.102 0.200
Carbon tetrachloride 0.0836 J 0.0732 0.200
Chlorobenzene U 0.0832 0.200
Chloroethane U 0.0996 0.200
Chloroform U 0.0717 0.200
Chloromethane U 0.103 0.200
2-Chlorotoluene U 0.0828 0.200
Cyclohexane U 0.0753 0.200
Dibromochloromethane U 0.0727 0.200
1,2-Dibromoethane U 0.0721 0.200
1,2-Dichlorobenzene U 0.128 0.200
1,3-Dichlorobenzene U 0.182 0.200
1,4-Dichlorobenzene U 0.0557 0.200
1,2-Dichloroethane U 0.0700 0.200
1,1-Dichloroethane U 0.0723 0.200
1,1-Dichloroethene U 0.0762 0.200
cis-1,2-Dichloroethene U 0.0784 0.200
trans-1,2-Dichloroethene U 0.0673 0.200
1,2-Dichloropropane U 0.0760 0.200
cis-1,3-Dichloropropene U 0.0689 0.200
trans-1,3-Dichloropropene U 0.0728 0.200
1,4-Dioxane U 0.0833 0.200
Ethanol U 0.265 1.25
Ethylbenzene U 0.0835 0.200
4-Ethyltoluene U 0.0783 0.200
Trichlorofluoromethane U 0.0819 0.200
Dichlorodifluoromethane U 0.137 0.200
1,1,2-Trichlorotrifluoroethane U 0.0793 0.200
1,2-Dichlorotetrafluoroethane U 0.0890 0.200
Heptane U 0.104 0.200
Hexachloro-1,3-butadiene U 0.105 0.630
Isopropylbenzene U 0.0777 0.200
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838974
Volatile Organic Compounds (MS) by Method TO-15 L1475124-01
Method Blank (MB)
(MB) R3774579-3 03/27/22 11:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Methylene Chloride U 0.0979 0.200
Methyl Butyl Ketone U 0.133 1.25
2-Butanone (MEK)U 0.0814 1.25
4-Methyl-2-pentanone (MIBK) U 0.0765 1.25
Methyl Methacrylate U 0.0876 0.200
MTBE U 0.0647 0.200
Naphthalene U 0.350 0.630
2-Propanol U 0.264 1.25
Propene 0.292 J 0.0932 1.25
Styrene U 0.0788 0.200
1,1,2,2-Tetrachloroethane U 0.0743 0.200
Tetrachloroethylene U 0.0814 0.200
Tetrahydrofuran U 0.0734 0.200
Toluene U 0.0870 0.500
1,2,4-Trichlorobenzene U 0.148 0.630
1,1,1-Trichloroethane U 0.0736 0.200
1,1,2-Trichloroethane U 0.0775 0.200
Trichloroethylene U 0.0680 0.200
1,2,4-Trimethylbenzene U 0.0764 0.200
1,3,5-Trimethylbenzene U 0.0779 0.200
Vinyl chloride U 0.0949 0.200
Vinyl Bromide U 0.0852 0.200
Vinyl acetate U 0.116 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
(S) 1,4-Bromofluorobenzene 94.3 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3774579-1 03/27/22 09:45 • (LCSD) R3774579-2 03/27/22 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Acetone 3.75 4.01 4.05 107 108 70.0-130 0.993 25
Allyl Chloride 3.75 3.99 3.97 106 106 70.0-130 0.503 25
Benzene 3.75 4.00 4.00 107 107 70.0-130 0.000 25
Benzyl Chloride 3.75 4.47 4.45 119 119 70.0-152 0.448 25
Bromodichloromethane 3.75 3.90 3.95 104 105 70.0-130 1.27 25
Bromoform 3.75 3.98 3.99 106 106 70.0-130 0.251 25
Bromomethane 3.75 3.99 4.01 106 107 70.0-130 0.500 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838974
Volatile Organic Compounds (MS) by Method TO-15 L1475124-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3774579-1 03/27/22 09:45 • (LCSD) R3774579-2 03/27/22 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
1,3-Butadiene 3.75 4.09 4.07 109 109 70.0-130 0.490 25
Carbon disulfide 3.75 4.00 4.01 107 107 70.0-130 0.250 25
Carbon tetrachloride 3.75 3.95 3.98 105 106 70.0-130 0.757 25
Chlorobenzene 3.75 3.89 3.95 104 105 70.0-130 1.53 25
Chloroethane 3.75 4.16 4.15 111 111 70.0-130 0.241 25
Chloroform 3.75 3.94 3.97 105 106 70.0-130 0.759 25
Chloromethane 3.75 4.21 4.21 112 112 70.0-130 0.000 25
2-Chlorotoluene 3.75 4.10 4.11 109 110 70.0-130 0.244 25
Cyclohexane 3.75 4.05 4.03 108 107 70.0-130 0.495 25
Dibromochloromethane 3.75 3.86 3.93 103 105 70.0-130 1.80 25
1,2-Dibromoethane 3.75 3.91 3.95 104 105 70.0-130 1.02 25
1,2-Dichlorobenzene 3.75 4.10 4.13 109 110 70.0-130 0.729 25
1,3-Dichlorobenzene 3.75 4.26 4.30 114 115 70.0-130 0.935 25
1,4-Dichlorobenzene 3.75 4.45 4.48 119 119 70.0-130 0.672 25
1,2-Dichloroethane 3.75 3.88 3.90 103 104 70.0-130 0.514 25
1,1-Dichloroethane 3.75 4.11 4.14 110 110 70.0-130 0.727 25
1,1-Dichloroethene 3.75 4.07 4.09 109 109 70.0-130 0.490 25
cis-1,2-Dichloroethene 3.75 4.02 4.04 107 108 70.0-130 0.496 25
trans-1,2-Dichloroethene 3.75 3.97 4.03 106 107 70.0-130 1.50 25
1,2-Dichloropropane 3.75 4.01 4.06 107 108 70.0-130 1.24 25
cis-1,3-Dichloropropene 3.75 3.91 3.95 104 105 70.0-130 1.02 25
trans-1,3-Dichloropropene 3.75 3.99 4.01 106 107 70.0-130 0.500 25
1,4-Dioxane 3.75 3.81 3.90 102 104 70.0-140 2.33 25
Ethanol 3.75 3.56 3.74 94.9 99.7 55.0-148 4.93 25
Ethylbenzene 3.75 4.09 4.13 109 110 70.0-130 0.973 25
4-Ethyltoluene 3.75 4.05 4.08 108 109 70.0-130 0.738 25
Trichlorofluoromethane 3.75 3.90 3.96 104 106 70.0-130 1.53 25
Dichlorodifluoromethane 3.75 4.01 4.09 107 109 64.0-139 1.98 25
1,1,2-Trichlorotrifluoroethane 3.75 3.96 3.99 106 106 70.0-130 0.755 25
1,2-Dichlorotetrafluoroethane 3.75 4.07 4.09 109 109 70.0-130 0.490 25
Heptane 3.75 4.01 4.18 107 111 70.0-130 4.15 25
Hexachloro-1,3-butadiene 3.75 3.86 3.88 103 103 70.0-151 0.517 25
Isopropylbenzene 3.75 3.94 3.97 105 106 70.0-130 0.759 25
Methylene Chloride 3.75 4.08 4.16 109 111 70.0-130 1.94 25
Methyl Butyl Ketone 3.75 4.35 4.40 116 117 70.0-149 1.14 25
Methyl Ethyl Ketone 3.75 4.13 4.15 110 111 70.0-130 0.483 25
4-Methyl-2-pentanone (MIBK) 3.75 4.22 4.25 113 113 70.0-139 0.708 25
Methyl Methacrylate 3.75 3.98 4.05 106 108 70.0-130 1.74 25
MTBE 3.75 4.00 4.05 107 108 70.0-130 1.24 25
Naphthalene 3.75 4.78 4.83 127 129 70.0-159 1.04 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838974
Volatile Organic Compounds (MS) by Method TO-15 L1475124-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3774579-1 03/27/22 09:45 • (LCSD) R3774579-2 03/27/22 10:27
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
2-Propanol 3.75 3.99 4.08 106 109 70.0-139 2.23 25
Propene 3.75 4.07 4.14 109 110 64.0-144 1.71 25
Styrene 3.75 4.08 4.12 109 110 70.0-130 0.976 25
1,1,2,2-Tetrachloroethane 3.75 3.99 4.03 106 107 70.0-130 0.998 25
Tetrachloroethylene 3.75 3.75 3.77 100 101 70.0-130 0.532 25
Tetrahydrofuran 3.75 4.20 4.25 112 113 70.0-137 1.18 25
Toluene 3.75 3.87 3.90 103 104 70.0-130 0.772 25
1,2,4-Trichlorobenzene 3.75 4.93 4.95 131 132 70.0-160 0.405 25
1,1,1-Trichloroethane 3.75 3.92 3.98 105 106 70.0-130 1.52 25
1,1,2-Trichloroethane 3.75 3.87 3.84 103 102 70.0-130 0.778 25
Trichloroethylene 3.75 3.79 3.83 101 102 70.0-130 1.05 25
1,2,4-Trimethylbenzene 3.75 4.02 4.02 107 107 70.0-130 0.000 25
1,3,5-Trimethylbenzene 3.75 4.08 4.09 109 109 70.0-130 0.245 25
Vinyl chloride 3.75 4.06 4.16 108 111 70.0-130 2.43 25
Vinyl Bromide 3.75 3.93 3.97 105 106 70.0-130 1.01 25
Vinyl acetate 3.75 4.30 4.23 115 113 70.0-130 1.64 25
m&p-Xylene 7.50 8.01 8.06 107 107 70.0-130 0.622 25
o-Xylene 3.75 3.96 3.96 106 106 70.0-130 0.000 25
(S) 1,4-Bromofluorobenzene 96.0 95.9 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1839631
Volatile Organic Compounds (MS) by Method TO-15 L1475124-01
Method Blank (MB)
(MB) R3775009-3 03/29/22 01:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
n-Hexane U 0.206 0.630
2,2,4-Trimethylpentane U 0.133 0.200
(S) 1,4-Bromofluorobenzene 97.8 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3775009-1 03/28/22 23:55 • (LCSD) R3775009-2 03/29/22 00:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
n-Hexane 3.75 3.78 3.73 101 99.5 70.0-130 1.33 25
2,2,4-Trimethylpentane 3.75 3.74 3.73 99.7 99.5 70.0-130 0.268 25
(S) 1,4-Bromofluorobenzene 99.2 99.4 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
April 03, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1475438
Samples Received:03/25/2022
Project Number:R0583.91
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
April 03, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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April 04, 2022
T. Alan Harvill
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SPENT CARBON L1475438-01 5
EFFLUENT L1475438-02 6
Qc: Quality Control Summary 7
Wet Chemistry by Method 1010B/ASTM D8175-18 7
Mercury by Method 245.1 8
Metals (ICPMS) by Method 200.8 9
Volatile Organic Compounds (GC/MS) by Method 624.1 11
Volatile Organic Compounds (GC/MS) by Method 8260D 14
Gl: Glossary of Terms 16
Al: Accreditations & Locations 17
Sc: Sample Chain of Custody 18
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SPENT CARBON L1475438-01 GW Gary A. Fischer 03/24/22 06:45 03/25/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Preparation by Method 1311 WG1838926 1 03/29/22 09:43 03/29/22 09:43 JWS Mt. Juliet, TN
Wet Chemistry by Method 1010B/ASTM D8175-18 WG1839105 1 03/28/22 01:00 03/28/22 01:00 WOS Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1840472 1 03/30/22 17:02 03/30/22 17:02 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
EFFLUENT L1475438-02 WW Gary A. Fischer 03/24/22 07:10 03/25/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 245.1 WG1841064 1 03/31/22 09:47 04/03/22 11:21 MRW Mt. Juliet, TN
Metals (ICPMS) by Method 200.8 WG1838743 1 03/28/22 23:55 03/29/22 11:58 JPD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1840993 1 03/31/22 03:52 03/31/22 03:52 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1841211 1 03/31/22 14:27 03/31/22 14:27 ACG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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T. Alan Harvill
Project Manager
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SAMPLE RESULTS - 01
L1475438
SPENT CARBON
Collected date/time: 03/24/22 06:45
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP ZHE Extraction -3/29/2022 9:43:14 AM WG1838926
Wet Chemistry by Method 1010B/ASTM D8175-18
Result Qualifier Dilution Analysis Batch
Analyte deg F date / time
Flashpoint DNF at 170 1 03/28/2022 01:00 WG1839105
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Benzene ND 0.0500 0.50 1 03/30/2022 17:02 WG1840472
Carbon tetrachloride ND 0.0500 0.50 1 03/30/2022 17:02 WG1840472
Chlorobenzene ND 0.0500 100 1 03/30/2022 17:02 WG1840472
Chloroform ND 0.250 6 1 03/30/2022 17:02 WG1840472
1,2-Dichloroethane ND 0.0500 0.50 1 03/30/2022 17:02 WG1840472
1,1-Dichloroethene ND 0.0500 0.70 1 03/30/2022 17:02 WG1840472
2-Butanone (MEK)ND 0.500 200 1 03/30/2022 17:02 WG1840472
Tetrachloroethene ND 0.0500 0.70 1 03/30/2022 17:02 WG1840472
Trichloroethene ND 0.0500 0.50 1 03/30/2022 17:02 WG1840472
Vinyl chloride ND 0.0500 0.20 1 03/30/2022 17:02 WG1840472
(S) Toluene-d8 112 80.0-120 03/30/2022 17:02 WG1840472
(S) 4-Bromofluorobenzene 89.6 77.0-126 03/30/2022 17:02 WG1840472
(S) 1,2-Dichloroethane-d4 106 70.0-130 03/30/2022 17:02 WG1840472
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1475438
EFFLUENT
Collected date/time: 03/24/22 07:10
Mercury by Method 245.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.100 0.200 1 04/03/2022 11:21 WG1841064
Metals (ICPMS) by Method 200.8
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic 1.24 B 0.195 1.00 1 03/29/2022 11:58 WG1838743
Barium 18.4 0.476 5.00 1 03/29/2022 11:58 WG1838743
Cadmium U 0.160 1.00 1 03/29/2022 11:58 WG1838743
Chromium U 5.60 20.0 1 03/29/2022 11:58 WG1838743
Lead 6.74 0.513 2.00 1 03/29/2022 11:58 WG1838743
Selenium U 0.437 2.00 1 03/29/2022 11:58 WG1838743
Silver U 0.144 1.00 1 03/29/2022 11:58 WG1838743
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acrolein U 2.54 50.0 1 03/31/2022 14:27 WG1841211
Acrylonitrile U 0.671 10.0 1 03/31/2022 03:52 WG1840993
Benzene U 0.0941 1.00 1 03/31/2022 03:52 WG1840993
Bromodichloromethane U 0.136 1.00 1 03/31/2022 03:52 WG1840993
Bromoform U 0.129 1.00 1 03/31/2022 03:52 WG1840993
Bromomethane U 0.605 5.00 1 03/31/2022 03:52 WG1840993
Carbon tetrachloride U 0.128 1.00 1 03/31/2022 03:52 WG1840993
Chlorobenzene U 0.116 1.00 1 03/31/2022 03:52 WG1840993
Chlorodibromomethane U 0.140 1.00 1 03/31/2022 03:52 WG1840993
Chloroethane U 0.192 5.00 1 03/31/2022 03:52 WG1840993
2-Chloroethyl vinyl ether U 0.575 50.0 1 03/31/2022 03:52 WG1840993
Chloroform U 0.111 5.00 1 03/31/2022 03:52 WG1840993
Chloromethane U 0.960 2.50 1 03/31/2022 03:52 WG1840993
1,2-Dichlorobenzene U 0.107 1.00 1 03/31/2022 03:52 WG1840993
1,3-Dichlorobenzene U 0.110 1.00 1 03/31/2022 03:52 WG1840993
1,4-Dichlorobenzene U 0.120 1.00 1 03/31/2022 03:52 WG1840993
1,1-Dichloroethane U 0.100 1.00 1 03/31/2022 03:52 WG1840993
1,2-Dichloroethane U 0.0819 1.00 1 03/31/2022 03:52 WG1840993
1,1-Dichloroethene U 0.188 1.00 1 03/31/2022 03:52 WG1840993
trans-1,2-Dichloroethene U 0.149 1.00 1 03/31/2022 03:52 WG1840993
1,2-Dichloropropane U 0.149 1.00 1 03/31/2022 03:52 WG1840993
cis-1,3-Dichloropropene U 0.111 1.00 1 03/31/2022 03:52 WG1840993
trans-1,3-Dichloropropene U 0.118 1.00 1 03/31/2022 03:52 WG1840993
Ethylbenzene U 0.137 1.00 1 03/31/2022 03:52 WG1840993
Methylene Chloride U 0.430 5.00 1 03/31/2022 03:52 WG1840993
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 03/31/2022 03:52 WG1840993
Tetrachloroethene U 0.300 1.00 1 03/31/2022 03:52 WG1840993
Toluene U 0.278 1.00 1 03/31/2022 03:52 WG1840993
1,1,1-Trichloroethane U 0.149 1.00 1 03/31/2022 03:52 WG1840993
1,1,2-Trichloroethane U 0.158 1.00 1 03/31/2022 03:52 WG1840993
Trichloroethene U 0.190 1.00 1 03/31/2022 03:52 WG1840993
Vinyl chloride U 0.234 1.00 1 03/31/2022 03:52 WG1840993
(S) Toluene-d8 110 80.0-120 03/31/2022 03:52 WG1840993
(S) Toluene-d8 104 80.0-120 03/31/2022 14:27 WG1841211
(S) 4-Bromofluorobenzene 102 80.0-120 03/31/2022 03:52 WG1840993
(S) 4-Bromofluorobenzene 104 80.0-120 03/31/2022 14:27 WG1841211
(S) 1,2-Dichloroethane-d4 87.9 70.0-130 03/31/2022 03:52 WG1840993
(S) 1,2-Dichloroethane-d4 106 70.0-130 03/31/2022 14:27 WG1841211
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1839105
Wet Chemistry by Method 1010B/ASTM D8175-18 L1475438-01
L1475033-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1475033-01 03/28/22 01:00 • (DUP) R3774866-3 03/28/22 01:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte deg F deg F %%
Flashpoint 150 154 1 2.64 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3774866-1 03/28/22 01:00 • (LCSD) R3774866-2 03/28/22 01:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F %%%%%
Flashpoint 126 124 128 98.1 101 96.0-104 3.19 10
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1841064
Mercury by Method 245.1 L1475438-02
Method Blank (MB)
(MB) R3776984-1 04/03/22 11:12
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.100 0.200
Laboratory Control Sample (LCS)
(LCS) R3776984-2 04/03/22 11:14
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Mercury 3.00 3.31 110 85.0-115
L1476584-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1476584-01 04/03/22 11:15 • (MS) R3776984-3 04/03/22 11:17 • (MSD) R3776984-4 04/03/22 11:19
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.66 3.45 122 115 1 70.0-130 5.89 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838743
Metals (ICPMS) by Method 200.8 L1475438-02
Method Blank (MB)
(MB) R3775102-1 03/29/22 10:25
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic 0.213 J 0.195 1.00
Barium U 0.476 5.00
Cadmium U 0.160 1.00
Chromium U 5.60 20.0
Lead U 0.513 2.00
Selenium U 0.437 2.00
Silver U 0.144 1.00
Laboratory Control Sample (LCS)
(LCS) R3775102-2 03/29/22 10:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Arsenic 50.0 48.8 97.6 85.0-115
Barium 50.0 44.3 88.6 85.0-115
Cadmium 50.0 50.0 99.9 85.0-115
Chromium 50.0 51.3 103 85.0-115
Lead 50.0 50.1 100 85.0-115
Selenium 50.0 47.2 94.4 85.0-115
Silver 50.0 49.1 98.2 85.0-115
L1474782-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1474782-01 03/29/22 10:32 • (MS) R3775102-4 03/29/22 10:39 • (MSD) R3775102-5 03/29/22 10:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 0.293 47.2 45.8 93.8 91.0 1 70.0-130 2.92 20
Barium 50.0 33.1 79.7 74.9 93.2 83.6 1 70.0-130 6.22 20
Cadmium 50.0 U 49.7 50.9 99.3 102 1 70.0-130 2.47 20
Chromium 50.0 U 49.7 48.5 99.3 97.1 1 70.0-130 2.33 20
Lead 50.0 U 47.4 47.4 94.8 94.7 1 70.0-130 0.0444 20
Selenium 50.0 U 46.1 47.6 92.2 95.1 1 70.0-130 3.13 20
Silver 50.0 U 50.3 49.2 101 98.5 1 70.0-130 2.05 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1838743
Metals (ICPMS) by Method 200.8 L1475438-02
L1475618-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1475618-01 03/29/22 10:46 • (MS) R3775102-6 03/29/22 10:49 • (MSD) R3775102-7 03/29/22 10:52
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 0.540 45.3 49.1 89.4 97.1 1 70.0-130 8.15 20
Barium 50.0 39.7 85.2 88.1 91.1 96.9 1 70.0-130 3.39 20
Cadmium 50.0 U 50.1 51.4 100 103 1 70.0-130 2.53 20
Chromium 50.0 6.57 51.7 55.6 90.2 98.1 1 70.0-130 7.36 20
Lead 50.0 U 48.1 48.0 96.2 95.9 1 70.0-130 0.290 20
Selenium 50.0 3.12 51.2 52.4 96.1 98.5 1 70.0-130 2.28 20
Silver 50.0 U 47.5 49.6 95.1 99.3 1 70.0-130 4.33 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1840993
Volatile Organic Compounds (GC/MS) by Method 624.1 L1475438-02
Method Blank (MB)
(MB) R3776000-3 03/30/22 21:58
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
2-Chloroethyl vinyl ether U 0.575 50.0
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
Ethylbenzene U 0.137 1.00
Methylene Chloride U 0.430 5.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Vinyl chloride U 0.234 1.00
(S) Toluene-d8 110 80.0-120
(S) 4-Bromofluorobenzene 101 80.0-120
(S) 1,2-Dichloroethane-d4 87.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1840993
Volatile Organic Compounds (GC/MS) by Method 624.1 L1475438-02
Laboratory Control Sample (LCS)
(LCS) R3776000-1 03/30/22 20:24
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acrylonitrile 25.0 22.5 90.0 60.0-140
Benzene 5.00 4.84 96.8 65.0-135
Bromodichloromethane 5.00 4.15 83.0 65.0-135
Bromoform 5.00 3.83 76.6 70.0-130
Bromomethane 5.00 3.87 77.4 15.0-185
Carbon tetrachloride 5.00 4.61 92.2 70.0-130
Chlorobenzene 5.00 5.12 102 65.0-135
Chlorodibromomethane 5.00 4.41 88.2 70.0-135
Chloroethane 5.00 5.29 106 40.0-160
2-Chloroethyl vinyl ether 25.0 24.2 96.8 0.100-225
Chloroform 5.00 4.68 93.6 70.0-135
Chloromethane 5.00 4.12 82.4 0.100-205
1,2-Dichlorobenzene 5.00 5.23 105 65.0-135
1,3-Dichlorobenzene 5.00 5.18 104 70.0-130
1,4-Dichlorobenzene 5.00 5.31 106 65.0-135
1,1-Dichloroethane 5.00 4.52 90.4 70.0-130
1,2-Dichloroethane 5.00 4.52 90.4 70.0-130
1,1-Dichloroethene 5.00 4.97 99.4 50.0-150
trans-1,2-Dichloroethene 5.00 5.21 104 70.0-130
1,2-Dichloropropane 5.00 4.93 98.6 35.0-165
cis-1,3-Dichloropropene 5.00 4.45 89.0 25.0-175
trans-1,3-Dichloropropene 5.00 4.48 89.6 50.0-150
Ethylbenzene 5.00 5.01 100 60.0-140
Methylene Chloride 5.00 4.77 95.4 60.0-140
1,1,2,2-Tetrachloroethane 5.00 5.31 106 60.0-140
Tetrachloroethene 5.00 5.10 102 70.0-130
Toluene 5.00 5.05 101 70.0-130
1,1,1-Trichloroethane 5.00 4.71 94.2 70.0-130
1,1,2-Trichloroethane 5.00 4.97 99.4 70.0-130
Trichloroethene 5.00 4.86 97.2 65.0-135
Vinyl chloride 5.00 4.33 86.6 5.00-195
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 101 80.0-120
(S) 1,2-Dichloroethane-d4 88.6 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1841211
Volatile Organic Compounds (GC/MS) by Method 624.1 L1475438-02
Method Blank (MB)
(MB) R3776215-3 03/31/22 12:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acrolein U 2.54 50.0
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 107 80.0-120
(S) 1,2-Dichloroethane-d4 107 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3776215-1 03/31/22 11:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acrolein 25.0 26.2 105 60.0-140
(S) Toluene-d8 104 80.0-120
(S) 4-Bromofluorobenzene 106 80.0-120
(S) 1,2-Dichloroethane-d4 108 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1840472
Volatile Organic Compounds (GC/MS) by Method 8260D L1475438-01
Method Blank (MB)
(MB) R3775992-3 03/30/22 10:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Benzene U 0.0167 0.0500
Carbon tetrachloride U 0.0167 0.0500
Chlorobenzene U 0.0167 0.0500
Chloroform U 0.0833 0.250
1,2-Dichloroethane U 0.0167 0.0500
1,1-Dichloroethene U 0.0167 0.0500
2-Butanone (MEK)U 0.167 0.500
Tetrachloroethene U 0.0167 0.0500
Trichloroethene U 0.0167 0.0500
Vinyl chloride U 0.0167 0.0500
(S) Toluene-d8 114 80.0-120
(S) 4-Bromofluorobenzene 93.1 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3775992-1 03/30/22 08:05 • (LCSD) R3775992-2 03/30/22 09:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Benzene 0.250 0.241 0.252 96.4 101 70.0-123 4.46 20
Carbon tetrachloride 0.250 0.225 0.243 90.0 97.2 68.0-126 7.69 20
Chlorobenzene 0.250 0.269 0.281 108 112 80.0-121 4.36 20
Chloroform 0.250 0.228 0.252 91.2 101 73.0-120 10.0 20
1,2-Dichloroethane 0.250 0.244 0.259 97.6 104 70.0-128 5.96 20
1,1-Dichloroethene 0.250 0.250 0.273 100 109 71.0-124 8.80 20
2-Butanone (MEK)1.25 1.15 1.26 92.0 101 44.0-160 9.13 20
Tetrachloroethene 0.250 0.235 0.248 94.0 99.2 72.0-132 5.38 20
Trichloroethene 0.250 0.245 0.245 98.0 98.0 78.0-124 0.000 20
Vinyl chloride 0.250 0.277 0.315 111 126 67.0-131 12.8 20
(S) Toluene-d8 112 111 80.0-120
(S) 4-Bromofluorobenzene 89.9 88.6 77.0-126
(S) 1,2-Dichloroethane-d4 103 101 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1840472
Volatile Organic Compounds (GC/MS) by Method 8260D L1475438-01
L1475514-08 Original Sample (OS) • Matrix Spike (MS)
(OS) L1475514-08 03/30/22 17:23 • (MS) R3775992-4 03/30/22 18:50
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/l mg/l mg/l %%
Benzene 0.250 ND 0.270 108 1 17.0-158
Carbon tetrachloride 0.250 ND 0.272 109 1 23.0-159
Chlorobenzene 0.250 ND 0.307 123 1 33.0-152
Chloroform 0.250 ND 0.270 108 1 29.0-154
1,2-Dichloroethane 0.250 ND 0.271 108 1 29.0-151
1,1-Dichloroethene 0.250 ND 0.266 106 1 11.0-160
2-Butanone (MEK)1.25 ND 1.40 112 1 10.0-160
Tetrachloroethene 0.250 ND 0.273 109 1 10.0-160
Trichloroethene 0.250 ND 0.284 114 1 10.0-160
Vinyl chloride 0.250 ND 0.306 122 1 10.0-160
(S) Toluene-d8 111 80.0-120
(S) 4-Bromofluorobenzene 91.6 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
L1475529-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1475529-01 03/30/22 17:45 • (MS) R3775992-6 03/30/22 19:12 • (MSD) R3775992-7 03/30/22 19:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Benzene 0.250 ND 0.303 0.344 121 138 1 17.0-158 12.7 27
Carbon tetrachloride 0.250 ND 0.303 0.340 121 136 1 23.0-159 11.5 28
Chlorobenzene 0.250 ND 0.334 0.366 134 146 1 33.0-152 9.14 27
Chloroform 0.250 ND 0.304 0.326 122 130 1 29.0-154 6.98 28
1,2-Dichloroethane 0.250 ND 0.298 0.323 119 129 1 29.0-151 8.05 27
1,1-Dichloroethene 0.250 ND 0.308 0.362 123 145 1 11.0-160 16.1 29
2-Butanone (MEK)1.25 ND 1.68 1.91 134 153 1 10.0-160 12.8 32
Tetrachloroethene 0.250 ND 0.280 0.317 112 127 1 10.0-160 12.4 27
Trichloroethene 0.250 ND 0.296 0.340 118 136 1 10.0-160 13.8 25
Vinyl chloride 0.250 ND 0.340 0.386 136 154 1 10.0-160 12.7 27
(S) Toluene-d8 111 110 80.0-120
(S) 4-Bromofluorobenzene 82.6 81.9 77.0-126
(S) 1,2-Dichloroethane-d4 105 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
April 28, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1486557
Samples Received:04/27/2022
Project Number:R0583.0C
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
April 28, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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April 28, 2022
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
AIR STACK L1486557-01 5
Qc: Quality Control Summary 7
Volatile Organic Compounds (MS) by Method TO-15 7
Gl: Glossary of Terms 11
Al: Accreditations & Locations 12
Sc: Sample Chain of Custody 13
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
AIR STACK L1486557-01 Air Gary A. Fischer 04/26/22 12:30 04/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method TO-15 WG1855045 2000 04/28/22 00:48 04/28/22 00:48 CEP Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
Sample Delivery Group (SDG) Narrative
Sample received in tedlar bag.
Lab Sample ID Project Sample ID Method
L1486557-01 AIR STACK TO-15
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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T. Alan Harvill
Project Manager
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SAMPLE RESULTS - 01
L1486557
AIR STACK
Collected date/time: 04/26/22 12:30
Volatile Organic Compounds (MS) by Method TO-15
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Acetone 67-64-1 58.10 2500 5940 ND ND 2000 WG1855045
Allyl chloride 107-05-1 76.53 400 1250 ND ND 2000 WG1855045
Benzene 71-43-2 78.10 400 1280 10300 32900 2000 WG1855045
Benzyl Chloride 100-44-7 127 400 2080 ND ND 2000 WG1855045
Bromodichloromethane 75-27-4 164 400 2680 ND ND 2000 WG1855045
Bromoform 75-25-2 253 1200 12400 ND ND 2000 WG1855045
Bromomethane 74-83-9 94.90 400 1550 ND ND 2000 WG1855045
1,3-Butadiene 106-99-0 54.10 4000 8850 ND ND 2000 WG1855045
Carbon disulfide 75-15-0 76.10 400 1240 ND ND 2000 WG1855045
Carbon tetrachloride 56-23-5 154 400 2520 ND ND 2000 WG1855045
Chlorobenzene 108-90-7 113 400 1850 ND ND 2000 WG1855045
Chloroethane 75-00-3 64.50 400 1060 ND ND 2000 WG1855045
Chloroform 67-66-3 119 400 1950 ND ND 2000 WG1855045
Chloromethane 74-87-3 50.50 400 826 ND ND 2000 WG1855045
2-Chlorotoluene 95-49-8 126 400 2060 ND ND 2000 WG1855045
Cyclohexane 110-82-7 84.20 400 1380 8500 29300 2000 WG1855045
Dibromochloromethane 124-48-1 208 400 3400 ND ND 2000 WG1855045
1,2-Dibromoethane 106-93-4 188 400 3080 ND ND 2000 WG1855045
1,2-Dichlorobenzene 95-50-1 147 400 2400 ND ND 2000 WG1855045
1,3-Dichlorobenzene 541-73-1 147 400 2400 ND ND 2000 WG1855045
1,4-Dichlorobenzene 106-46-7 147 400 2400 ND ND J4 2000 WG1855045
1,2-Dichloroethane 107-06-2 99 400 1620 ND ND 2000 WG1855045
1,1-Dichloroethane 75-34-3 98 400 1600 ND ND 2000 WG1855045
1,1-Dichloroethene 75-35-4 96.90 400 1590 ND ND 2000 WG1855045
cis-1,2-Dichloroethene 156-59-2 96.90 400 1590 ND ND 2000 WG1855045
trans-1,2-Dichloroethene 156-60-5 96.90 400 1590 ND ND 2000 WG1855045
1,2-Dichloropropane 78-87-5 113 400 1850 ND ND 2000 WG1855045
cis-1,3-Dichloropropene 10061-01-5 111 400 1820 ND ND 2000 WG1855045
trans-1,3-Dichloropropene 10061-02-6 111 400 1820 ND ND 2000 WG1855045
1,4-Dioxane 123-91-1 88.10 400 1440 ND ND 2000 WG1855045
Ethanol 64-17-5 46.10 2500 4710 ND ND 2000 WG1855045
Ethylbenzene 100-41-4 106 400 1730 1740 7540 2000 WG1855045
4-Ethyltoluene 622-96-8 120 400 1960 1280 6280 2000 WG1855045
Trichlorofluoromethane 75-69-4 137.40 400 2250 ND ND 2000 WG1855045
Dichlorodifluoromethane 75-71-8 120.92 400 1980 ND ND 2000 WG1855045
1,1,2-Trichlorotrifluoroethane 76-13-1 187.40 400 3070 ND ND 2000 WG1855045
1,2-Dichlorotetrafluoroethane 76-14-2 171 400 2800 ND ND 2000 WG1855045
Heptane 142-82-5 100 400 1640 11400 46600 2000 WG1855045
Hexachloro-1,3-butadiene 87-68-3 261 1260 13500 ND ND 2000 WG1855045
n-Hexane 110-54-3 86.20 1260 4440 35600 126000 2000 WG1855045
Isopropylbenzene 98-82-8 120.20 400 1970 ND ND 2000 WG1855045
Methylene Chloride 75-09-2 84.90 400 1390 ND ND 2000 WG1855045
Methyl Butyl Ketone 591-78-6 100 2500 10200 ND ND 2000 WG1855045
2-Butanone (MEK)78-93-3 72.10 2500 7370 ND ND 2000 WG1855045
4-Methyl-2-pentanone (MIBK) 108-10-1 100.10 2500 10200 ND ND 2000 WG1855045
Methyl methacrylate 80-62-6 100.12 400 1640 ND ND 2000 WG1855045
MTBE 1634-04-4 88.10 400 1440 882 3180 2000 WG1855045
Naphthalene 91-20-3 128 1260 6600 ND ND 2000 WG1855045
2-Propanol 67-63-0 60.10 2500 6150 7580 18600 2000 WG1855045
Propene 115-07-1 42.10 2500 4300 ND ND 2000 WG1855045
Styrene 100-42-5 104 400 1700 ND ND 2000 WG1855045
1,1,2,2-Tetrachloroethane 79-34-5 168 400 2750 ND ND 2000 WG1855045
Tetrachloroethylene 127-18-4 166 400 2720 ND ND 2000 WG1855045
Tetrahydrofuran 109-99-9 72.10 400 1180 ND ND 2000 WG1855045
Toluene 108-88-3 92.10 1000 3770 3360 12700 2000 WG1855045
1,2,4-Trichlorobenzene 120-82-1 181 1260 9330 ND ND 2000 WG1855045
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1486557
AIR STACK
Collected date/time: 04/26/22 12:30
Volatile Organic Compounds (MS) by Method TO-15
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
1,1,1-Trichloroethane 71-55-6 133 400 2180 ND ND 2000 WG1855045
1,1,2-Trichloroethane 79-00-5 133 400 2180 ND ND 2000 WG1855045
Trichloroethylene 79-01-6 131 400 2140 ND ND 2000 WG1855045
1,2,4-Trimethylbenzene 95-63-6 120 400 1960 795 3900 2000 WG1855045
1,3,5-Trimethylbenzene 108-67-8 120 400 1960 650 3190 2000 WG1855045
2,2,4-Trimethylpentane 540-84-1 114.22 400 1870 22400 105000 2000 WG1855045
Vinyl chloride 75-01-4 62.50 400 1020 ND ND 2000 WG1855045
Vinyl Bromide 593-60-2 106.95 400 1750 ND ND 2000 WG1855045
Vinyl acetate 108-05-4 86.10 400 1410 ND ND 2000 WG1855045
m&p-Xylene 1330-20-7 106 800 3470 6990 30300 2000 WG1855045
o-Xylene 95-47-6 106 400 1730 2500 10800 2000 WG1855045
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 93.5 WG1855045
Sample Narrative:
L1486557-01 WG1855045: Non-target compounds too high to run at a lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1855045
Volatile Organic Compounds (MS) by Method TO-15 L1486557-01
Method Blank (MB)
(MB) R3785694-3 04/27/22 10:23
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Acetone U 0.584 1.25
Allyl Chloride U 0.114 0.200
Benzene U 0.0715 0.200
Benzyl Chloride U 0.0598 0.200
Bromodichloromethane U 0.0702 0.200
Bromoform U 0.0732 0.600
Bromomethane U 0.0982 0.200
1,3-Butadiene U 0.104 2.00
Carbon disulfide U 0.102 0.200
Carbon tetrachloride U 0.0732 0.200
Chlorobenzene U 0.0832 0.200
Chloroethane U 0.0996 0.200
Chloroform U 0.0717 0.200
Chloromethane U 0.103 0.200
2-Chlorotoluene U 0.0828 0.200
Cyclohexane U 0.0753 0.200
Dibromochloromethane U 0.0727 0.200
1,2-Dibromoethane U 0.0721 0.200
1,2-Dichlorobenzene U 0.128 0.200
1,3-Dichlorobenzene U 0.182 0.200
1,4-Dichlorobenzene U 0.0557 0.200
1,2-Dichloroethane U 0.0700 0.200
1,1-Dichloroethane U 0.0723 0.200
1,1-Dichloroethene U 0.0762 0.200
cis-1,2-Dichloroethene U 0.0784 0.200
trans-1,2-Dichloroethene U 0.0673 0.200
1,2-Dichloropropane U 0.0760 0.200
cis-1,3-Dichloropropene U 0.0689 0.200
trans-1,3-Dichloropropene U 0.0728 0.200
1,4-Dioxane U 0.0833 0.200
Ethanol U 0.265 1.25
Ethylbenzene U 0.0835 0.200
4-Ethyltoluene U 0.0783 0.200
Trichlorofluoromethane U 0.0819 0.200
Dichlorodifluoromethane U 0.137 0.200
1,1,2-Trichlorotrifluoroethane U 0.0793 0.200
1,2-Dichlorotetrafluoroethane U 0.0890 0.200
Heptane U 0.104 0.200
Hexachloro-1,3-butadiene U 0.105 0.630
n-Hexane U 0.206 0.630
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1855045
Volatile Organic Compounds (MS) by Method TO-15 L1486557-01
Method Blank (MB)
(MB) R3785694-3 04/27/22 10:23
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Isopropylbenzene U 0.0777 0.200
Methylene Chloride U 0.0979 0.200
Methyl Butyl Ketone U 0.133 1.25
2-Butanone (MEK)U 0.0814 1.25
4-Methyl-2-pentanone (MIBK) U 0.0765 1.25
Methyl Methacrylate U 0.0876 0.200
MTBE U 0.0647 0.200
Naphthalene U 0.350 0.630
2-Propanol U 0.264 1.25
Propene 0.296 J 0.0932 1.25
Styrene U 0.0788 0.200
1,1,2,2-Tetrachloroethane U 0.0743 0.200
Tetrachloroethylene U 0.0814 0.200
Tetrahydrofuran U 0.0734 0.200
Toluene U 0.0870 0.500
1,2,4-Trichlorobenzene U 0.148 0.630
1,1,1-Trichloroethane U 0.0736 0.200
1,1,2-Trichloroethane U 0.0775 0.200
Trichloroethylene U 0.0680 0.200
1,2,4-Trimethylbenzene U 0.0764 0.200
1,3,5-Trimethylbenzene U 0.0779 0.200
2,2,4-Trimethylpentane U 0.133 0.200
Vinyl chloride U 0.0949 0.200
Vinyl Bromide U 0.0852 0.200
Vinyl acetate U 0.116 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
(S) 1,4-Bromofluorobenzene 93.0 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3785694-1 04/27/22 09:02 • (LCSD) R3785694-2 04/27/22 09:43
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Acetone 3.75 4.43 4.40 118 117 70.0-130 0.679 25
Allyl Chloride 3.75 4.51 4.39 120 117 70.0-130 2.70 25
Benzene 3.75 4.50 4.37 120 117 70.0-130 2.93 25
Benzyl Chloride 3.75 3.81 3.74 102 99.7 70.0-152 1.85 25
Bromodichloromethane 3.75 4.48 4.37 119 117 70.0-130 2.49 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1855045
Volatile Organic Compounds (MS) by Method TO-15 L1486557-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3785694-1 04/27/22 09:02 • (LCSD) R3785694-2 04/27/22 09:43
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Bromoform 3.75 4.50 4.37 120 117 70.0-130 2.93 25
Bromomethane 3.75 4.28 4.25 114 113 70.0-130 0.703 25
1,3-Butadiene 3.75 4.32 4.26 115 114 70.0-130 1.40 25
Carbon disulfide 3.75 4.48 4.37 119 117 70.0-130 2.49 25
Carbon tetrachloride 3.75 4.44 4.36 118 116 70.0-130 1.82 25
Chlorobenzene 3.75 4.59 4.47 122 119 70.0-130 2.65 25
Chloroethane 3.75 4.34 4.31 116 115 70.0-130 0.694 25
Chloroform 3.75 4.42 4.34 118 116 70.0-130 1.83 25
Chloromethane 3.75 4.40 4.32 117 115 70.0-130 1.83 25
2-Chlorotoluene 3.75 4.73 4.62 126 123 70.0-130 2.35 25
Cyclohexane 3.75 4.50 4.45 120 119 70.0-130 1.12 25
Dibromochloromethane 3.75 4.50 4.42 120 118 70.0-130 1.79 25
1,2-Dibromoethane 3.75 4.54 4.46 121 119 70.0-130 1.78 25
1,2-Dichlorobenzene 3.75 4.66 4.56 124 122 70.0-130 2.17 25
1,3-Dichlorobenzene 3.75 4.83 4.68 129 125 70.0-130 3.15 25
1,4-Dichlorobenzene 3.75 4.98 4.86 133 130 70.0-130 J4 2.44 25
1,2-Dichloroethane 3.75 4.49 4.40 120 117 70.0-130 2.02 25
1,1-Dichloroethane 3.75 4.50 4.42 120 118 70.0-130 1.79 25
1,1-Dichloroethene 3.75 4.50 4.40 120 117 70.0-130 2.25 25
cis-1,2-Dichloroethene 3.75 4.53 4.40 121 117 70.0-130 2.91 25
trans-1,2-Dichloroethene 3.75 4.52 4.36 121 116 70.0-130 3.60 25
1,2-Dichloropropane 3.75 4.52 4.42 121 118 70.0-130 2.24 25
cis-1,3-Dichloropropene 3.75 4.45 4.36 119 116 70.0-130 2.04 25
trans-1,3-Dichloropropene 3.75 4.49 4.42 120 118 70.0-130 1.57 25
1,4-Dioxane 3.75 4.24 4.15 113 111 70.0-140 2.15 25
Ethanol 3.75 4.16 4.20 111 112 55.0-148 0.957 25
Ethylbenzene 3.75 4.70 4.57 125 122 70.0-130 2.80 25
4-Ethyltoluene 3.75 4.73 4.60 126 123 70.0-130 2.79 25
Trichlorofluoromethane 3.75 4.46 4.35 119 116 70.0-130 2.50 25
Dichlorodifluoromethane 3.75 4.28 4.15 114 111 64.0-139 3.08 25
1,1,2-Trichlorotrifluoroethane 3.75 4.48 4.37 119 117 70.0-130 2.49 25
1,2-Dichlorotetrafluoroethane 3.75 4.47 4.39 119 117 70.0-130 1.81 25
Heptane 3.75 4.52 4.43 121 118 70.0-130 2.01 25
Hexachloro-1,3-butadiene 3.75 4.50 4.40 120 117 70.0-151 2.25 25
n-Hexane 3.75 4.50 4.43 120 118 70.0-130 1.57 25
Isopropylbenzene 3.75 4.62 4.50 123 120 70.0-130 2.63 25
Methylene Chloride 3.75 4.24 4.17 113 111 70.0-130 1.66 25
Methyl Butyl Ketone 3.75 4.55 4.49 121 120 70.0-149 1.33 25
Methyl Ethyl Ketone 3.75 4.60 4.50 123 120 70.0-130 2.20 25
4-Methyl-2-pentanone (MIBK) 3.75 4.67 4.58 125 122 70.0-139 1.95 25
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1855045
Volatile Organic Compounds (MS) by Method TO-15 L1486557-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3785694-1 04/27/22 09:02 • (LCSD) R3785694-2 04/27/22 09:43
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Methyl Methacrylate 3.75 4.60 4.49 123 120 70.0-130 2.42 25
MTBE 3.75 4.50 4.38 120 117 70.0-130 2.70 25
Naphthalene 3.75 4.21 4.17 112 111 70.0-159 0.955 25
2-Propanol 3.75 4.40 4.35 117 116 70.0-139 1.14 25
Propene 3.75 4.09 3.96 109 106 64.0-144 3.23 25
Styrene 3.75 4.68 4.57 125 122 70.0-130 2.38 25
1,1,2,2-Tetrachloroethane 3.75 4.55 4.40 121 117 70.0-130 3.35 25
Tetrachloroethylene 3.75 4.44 4.35 118 116 70.0-130 2.05 25
Tetrahydrofuran 3.75 4.50 4.43 120 118 70.0-137 1.57 25
Toluene 3.75 4.54 4.44 121 118 70.0-130 2.23 25
1,2,4-Trichlorobenzene 3.75 4.41 4.42 118 118 70.0-160 0.227 25
1,1,1-Trichloroethane 3.75 4.45 4.35 119 116 70.0-130 2.27 25
1,1,2-Trichloroethane 3.75 4.47 4.36 119 116 70.0-130 2.49 25
Trichloroethylene 3.75 4.42 4.33 118 115 70.0-130 2.06 25
1,2,4-Trimethylbenzene 3.75 4.72 4.58 126 122 70.0-130 3.01 25
1,3,5-Trimethylbenzene 3.75 4.64 4.60 124 123 70.0-130 0.866 25
2,2,4-Trimethylpentane 3.75 4.58 4.47 122 119 70.0-130 2.43 25
Vinyl chloride 3.75 4.44 4.40 118 117 70.0-130 0.905 25
Vinyl Bromide 3.75 4.44 4.33 118 115 70.0-130 2.51 25
Vinyl acetate 3.75 3.90 3.89 104 104 70.0-130 0.257 25
m&p-Xylene 7.50 9.38 9.15 125 122 70.0-130 2.48 25
o-Xylene 3.75 4.54 4.43 121 118 70.0-130 2.45 25
(S) 1,4-Bromofluorobenzene 98.1 97.1 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
May 10, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1487021
Samples Received:04/27/2022
Project Number:R0593.93
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
May 10, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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May 13, 2022
T. Alan Harvill
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
EFFLUENT L1487021-01 5
Qc: Quality Control Summary 6
Mercury by Method 245.1 6
Metals (ICPMS) by Method 200.8 7
Volatile Organic Compounds (GC/MS) by Method 624.1 9
Gl: Glossary of Terms 11
Al: Accreditations & Locations 12
Sc: Sample Chain of Custody 13
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
EFFLUENT L1487021-01 WW Gary A. Fischer 04/26/22 12:10 04/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 245.1 WG1857957 1 05/09/22 09:12 05/10/22 13:52 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 200.8 WG1857203 1 05/02/22 22:41 05/03/22 15:16 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1856030 1 04/28/22 22:27 04/28/22 22:27 BMB Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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T. Alan Harvill
Project Manager
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SAMPLE RESULTS - 01
L1487021
EFFLUENT
Collected date/time: 04/26/22 12:10
Mercury by Method 245.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.100 0.200 1 05/10/2022 13:52 WG1857957
Metals (ICPMS) by Method 200.8
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic 0.368 J 0.195 1.00 1 05/03/2022 15:16 WG1857203
Barium 11.3 0.476 5.00 1 05/03/2022 15:16 WG1857203
Cadmium U 0.160 1.00 1 05/03/2022 15:16 WG1857203
Chromium U 5.60 20.0 1 05/03/2022 15:16 WG1857203
Lead 8.52 0.513 2.00 1 05/03/2022 15:16 WG1857203
Selenium U 0.437 2.00 1 05/03/2022 15:16 WG1857203
Silver U 0.144 1.00 1 05/03/2022 15:16 WG1857203
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acrolein U 2.54 50.0 1 04/28/2022 22:27 WG1856030
Acrylonitrile U 0.671 10.0 1 04/28/2022 22:27 WG1856030
Benzene U 0.0941 1.00 1 04/28/2022 22:27 WG1856030
Bromodichloromethane U 0.136 1.00 1 04/28/2022 22:27 WG1856030
Bromoform U 0.129 1.00 1 04/28/2022 22:27 WG1856030
Bromomethane U 0.605 5.00 1 04/28/2022 22:27 WG1856030
Carbon tetrachloride U 0.128 1.00 1 04/28/2022 22:27 WG1856030
Chlorobenzene U 0.116 1.00 1 04/28/2022 22:27 WG1856030
Chlorodibromomethane U 0.140 1.00 1 04/28/2022 22:27 WG1856030
Chloroethane U 0.192 5.00 1 04/28/2022 22:27 WG1856030
2-Chloroethyl vinyl ether U 0.575 50.0 1 04/28/2022 22:27 WG1856030
Chloroform U 0.111 5.00 1 04/28/2022 22:27 WG1856030
Chloromethane U 0.960 2.50 1 04/28/2022 22:27 WG1856030
1,2-Dichlorobenzene U 0.107 1.00 1 04/28/2022 22:27 WG1856030
1,3-Dichlorobenzene U 0.110 1.00 1 04/28/2022 22:27 WG1856030
1,4-Dichlorobenzene U 0.120 1.00 1 04/28/2022 22:27 WG1856030
1,1-Dichloroethane U 0.100 1.00 1 04/28/2022 22:27 WG1856030
1,2-Dichloroethane U 0.0819 1.00 1 04/28/2022 22:27 WG1856030
1,1-Dichloroethene U 0.188 1.00 1 04/28/2022 22:27 WG1856030
trans-1,2-Dichloroethene U 0.149 1.00 1 04/28/2022 22:27 WG1856030
1,2-Dichloropropane U 0.149 1.00 1 04/28/2022 22:27 WG1856030
cis-1,3-Dichloropropene U 0.111 1.00 1 04/28/2022 22:27 WG1856030
trans-1,3-Dichloropropene U 0.118 1.00 1 04/28/2022 22:27 WG1856030
Ethylbenzene U 0.137 1.00 1 04/28/2022 22:27 WG1856030
Methylene Chloride U 0.430 5.00 1 04/28/2022 22:27 WG1856030
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 04/28/2022 22:27 WG1856030
Tetrachloroethene U 0.300 1.00 1 04/28/2022 22:27 WG1856030
Toluene U 0.278 1.00 1 04/28/2022 22:27 WG1856030
1,1,1-Trichloroethane U 0.149 1.00 1 04/28/2022 22:27 WG1856030
1,1,2-Trichloroethane U 0.158 1.00 1 04/28/2022 22:27 WG1856030
Trichloroethene U 0.190 1.00 1 04/28/2022 22:27 WG1856030
Vinyl chloride U 0.234 1.00 1 04/28/2022 22:27 WG1856030
(S) Toluene-d8 115 80.0-120 04/28/2022 22:27 WG1856030
(S) 4-Bromofluorobenzene 117 80.0-120 04/28/2022 22:27 WG1856030
(S) 1,2-Dichloroethane-d4 102 70.0-130 04/28/2022 22:27 WG1856030
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1857957
Mercury by Method 245.1 L1487021-01
Method Blank (MB)
(MB) R3790215-1 05/10/22 13:41
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.100 0.200
Laboratory Control Sample (LCS)
(LCS) R3790215-2 05/10/22 13:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Mercury 3.00 3.25 108 85.0-115
L1486189-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1486189-01 05/10/22 13:45 • (MS) R3790215-3 05/10/22 13:48 • (MSD) R3790215-4 05/10/22 13:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.29 3.28 110 109 1 70.0-130 0.304 20
L1487021-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487021-01 05/10/22 13:52 • (MS) R3790215-5 05/10/22 13:59 • (MSD) R3790215-6 05/10/22 14:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.20 3.12 107 104 1 70.0-130 2.53 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1857203
Metals (ICPMS) by Method 200.8 L1487021-01
Method Blank (MB)
(MB) R3787678-1 05/03/22 14:27
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 0.195 1.00
Barium U 0.476 5.00
Cadmium U 0.160 1.00
Chromium U 5.60 20.0
Lead U 0.513 2.00
Selenium U 0.437 2.00
Silver U 0.144 1.00
Laboratory Control Sample (LCS)
(LCS) R3787678-2 05/03/22 14:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Arsenic 50.0 46.3 92.5 85.0-115
Barium 50.0 47.3 94.6 85.0-115
Cadmium 50.0 50.0 100 85.0-115
Chromium 50.0 47.6 95.3 85.0-115
Lead 50.0 48.0 96.0 85.0-115
Selenium 50.0 42.8 85.7 85.0-115
Silver 50.0 49.2 98.4 85.0-115
L1484390-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1484390-01 05/03/22 14:33 • (MS) R3787678-4 05/03/22 14:40 • (MSD) R3787678-5 05/03/22 14:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 0.301 44.6 47.4 88.6 94.2 1 70.0-130 6.09 20
Barium 50.0 27.1 70.8 73.6 87.4 93.0 1 70.0-130 3.85 20
Cadmium 50.0 U 49.0 50.2 98.1 100 1 70.0-130 2.30 20
Chromium 50.0 U 46.0 49.7 91.9 99.5 1 70.0-130 7.90 20
Lead 50.0 U 46.6 46.7 93.2 93.3 1 70.0-130 0.127 20
Selenium 50.0 U 45.5 45.7 91.0 91.5 1 70.0-130 0.511 20
Silver 50.0 U 47.3 48.4 94.6 96.8 1 70.0-130 2.20 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1857203
Metals (ICPMS) by Method 200.8 L1487021-01
L1486634-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1486634-01 05/03/22 14:47 • (MS) R3787678-6 05/03/22 14:50 • (MSD) R3787678-7 05/03/22 14:53
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 0.370 46.6 44.6 92.4 88.5 1 70.0-130 4.34 20
Barium 50.0 17.2 64.3 64.6 94.1 94.8 1 70.0-130 0.553 20
Cadmium 50.0 U 49.1 47.6 98.3 95.3 1 70.0-130 3.10 20
Chromium 50.0 U 48.4 47.4 96.8 94.9 1 70.0-130 2.05 20
Lead 50.0 U 45.9 46.8 91.9 93.6 1 70.0-130 1.91 20
Selenium 50.0 U 45.2 44.4 90.5 88.9 1 70.0-130 1.78 20
Silver 50.0 U 46.6 46.0 93.3 92.1 1 70.0-130 1.32 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1856030
Volatile Organic Compounds (GC/MS) by Method 624.1 L1487021-01
Method Blank (MB)
(MB) R3786278-3 04/28/22 18:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
2-Chloroethyl vinyl ether U 0.575 50.0
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
Ethylbenzene U 0.137 1.00
Methylene Chloride U 0.430 5.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Vinyl chloride U 0.234 1.00
(S) Toluene-d8 114 80.0-120
(S) 4-Bromofluorobenzene 111 80.0-120
(S) 1,2-Dichloroethane-d4 94.5 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1856030
Volatile Organic Compounds (GC/MS) by Method 624.1 L1487021-01
Laboratory Control Sample (LCS)
(LCS) R3786278-1 04/28/22 17:46
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acrolein 25.0 29.2 117 60.0-140
Acrylonitrile 25.0 25.4 102 60.0-140
Benzene 5.00 5.55 111 65.0-135
Bromodichloromethane 5.00 5.38 108 65.0-135
Bromoform 5.00 4.52 90.4 70.0-130
Bromomethane 5.00 5.69 114 15.0-185
Carbon tetrachloride 5.00 5.11 102 70.0-130
Chlorobenzene 5.00 5.07 101 65.0-135
Chlorodibromomethane 5.00 4.99 99.8 70.0-135
Chloroethane 5.00 4.69 93.8 40.0-160
2-Chloroethyl vinyl ether 25.0 23.2 92.8 0.100-225
Chloroform 5.00 5.44 109 70.0-135
Chloromethane 5.00 4.49 89.8 0.100-205
1,2-Dichlorobenzene 5.00 5.15 103 65.0-135
1,3-Dichlorobenzene 5.00 4.62 92.4 70.0-130
1,4-Dichlorobenzene 5.00 4.92 98.4 65.0-135
1,1-Dichloroethane 5.00 5.73 115 70.0-130
1,2-Dichloroethane 5.00 5.44 109 70.0-130
1,1-Dichloroethene 5.00 5.50 110 50.0-150
trans-1,2-Dichloroethene 5.00 5.60 112 70.0-130
1,2-Dichloropropane 5.00 5.35 107 35.0-165
cis-1,3-Dichloropropene 5.00 5.12 102 25.0-175
trans-1,3-Dichloropropene 5.00 4.68 93.6 50.0-150
Ethylbenzene 5.00 5.04 101 60.0-140
Methylene Chloride 5.00 6.46 129 60.0-140
1,1,2,2-Tetrachloroethane 5.00 6.31 126 60.0-140
Tetrachloroethene 5.00 4.93 98.6 70.0-130
Toluene 5.00 5.28 106 70.0-130
1,1,1-Trichloroethane 5.00 5.49 110 70.0-130
1,1,2-Trichloroethane 5.00 5.35 107 70.0-130
Trichloroethene 5.00 5.12 102 65.0-135
Vinyl chloride 5.00 4.88 97.6 5.00-195
(S) Toluene-d8 101 80.0-120
(S) 4-Bromofluorobenzene 92.3 80.0-120
(S) 1,2-Dichloroethane-d4 97.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
June 02, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1499584
Samples Received:05/31/2022
Project Number:R0583.84
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
June 02, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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June 03, 2022
T. Alan Harvill
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
AIR STACK L1499584-01 5
Qc: Quality Control Summary 6
Volatile Organic Compounds (MS) by Method M18-Mod 6
Gl: Glossary of Terms 7
Al: Accreditations & Locations 8
Sc: Sample Chain of Custody 9
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
AIR STACK L1499584-01 Air Gary A Fischer 05/27/22 06:45 05/31/22 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method M18-Mod WG1872569 2000 06/02/22 01:17 06/02/22 01:17 DAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1499584
AIR STACK
Collected date/time: 05/27/22 06:45
Volatile Organic Compounds (MS) by Method M18-Mod
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Benzene 71-43-2 78.10 400 1280 10300 32900 T8 2000 WG1872569
Toluene 108-88-3 92.10 1000 3770 2910 11000 T8 2000 WG1872569
Ethylbenzene 100-41-4 106 400 1730 1280 5550 T8 2000 WG1872569
m&p-Xylene 1330-20-7 106 800 3470 4480 19400 T8 2000 WG1872569
o-Xylene 95-47-6 106 400 1730 1720 7460 T8 2000 WG1872569
Methyl tert-butyl ether 1634-04-4 88.10 400 1440 ND ND T8 2000 WG1872569
TPH (GC/MS) Low Fraction 8006-61-9 101 400000 1650000 495000 2040000 T8 2000 WG1872569
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 87.8 WG1872569
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1872569
Volatile Organic Compounds (MS) by Method M18-Mod L1499584-01
Method Blank (MB)
(MB) R3798428-3 06/01/22 10:24
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Benzene U 0.0715 0.200
Toluene U 0.0870 0.500
Ethylbenzene U 0.0835 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
MTBE U 0.0647 0.200
TPH (GC/MS) Low Fraction U 39.7 200
(S) 1,4-Bromofluorobenzene 86.7 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3798428-1 06/01/22 08:58 • (LCSD) R3798428-2 06/01/22 09:42
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Benzene 3.75 4.19 4.23 112 113 70.0-130 0.950 25
Toluene 3.75 4.14 4.07 110 109 70.0-130 1.71 25
Ethylbenzene 3.75 4.04 4.01 108 107 70.0-130 0.745 25
m&p-Xylene 7.50 8.47 8.23 113 110 70.0-130 2.87 25
o-Xylene 3.75 4.08 3.95 109 105 70.0-130 3.24 25
MTBE 3.75 4.13 4.08 110 109 70.0-130 1.22 25
TPH (GC/MS) Low Fraction 203 226 220 111 108 70.0-130 2.69 25
(S) 1,4-Bromofluorobenzene 87.1 87.5 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
T8 Sample(s) received past/too close to holding time expiration.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
July 04, 2022
Mid-Atlantic - Speedway NC
Sample Delivery Group:L1504501
Samples Received:06/14/2022
Project Number:R0583
Description:Speedway #6958
Report To:Mr. Jim Young
409 Rogers View Court
Raleigh, NC 27610
Entire Report Reviewed By:
July 04, 2022
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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July 04, 2022
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
EFFLUENT L1504501-01 5
AIR STACK L1504501-02 6
Qc: Quality Control Summary 7
Mercury by Method 245.1 7
Metals (ICPMS) by Method 200.8 8
Volatile Organic Compounds (MS) by Method M18-Mod 10
Volatile Organic Compounds (GC/MS) by Method 624.1 12
Gl: Glossary of Terms 14
Al: Accreditations & Locations 15
Sc: Sample Chain of Custody 16
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
EFFLUENT L1504501-01 WW Gary Fischer 06/13/22 09:25 06/14/22 12:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 245.1 WG1881166 1 06/30/22 10:55 07/03/22 11:39 MRW Mt. Juliet, TN
Metals (ICPMS) by Method 200.8 WG1884444 1 06/24/22 09:39 06/27/22 15:23 LD Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1 WG1883724 1 06/22/22 23:06 06/22/22 23:06 FKG Mt. Juliet, TN
Collected by Collected date/time Received date/time
AIR STACK L1504501-02 Air Gary Fischer 06/13/22 09:45 06/14/22 12:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method M18-Mod WG1879678 80 06/15/22 20:38 06/15/22 20:38 FKG Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method M18-Mod WG1880536 400 06/16/22 17:17 06/16/22 17:17 CEP Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1504501
EFFLUENT
Collected date/time: 06/13/22 09:25
Mercury by Method 245.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.100 0.200 1 07/03/2022 11:39 WG1881166
Metals (ICPMS) by Method 200.8
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic 0.616 J 0.195 1.00 1 06/27/2022 15:23 WG1884444
Barium 13.2 0.476 5.00 1 06/27/2022 15:23 WG1884444
Cadmium U 0.160 1.00 1 06/27/2022 15:23 WG1884444
Chromium U J4 5.60 20.0 1 06/27/2022 15:23 WG1884444
Lead 1.26 J 0.513 2.00 1 06/27/2022 15:23 WG1884444
Selenium U 0.437 2.00 1 06/27/2022 15:23 WG1884444
Silver U 0.144 1.00 1 06/27/2022 15:23 WG1884444
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acrolein U 2.54 50.0 1 06/22/2022 23:06 WG1883724
Acrylonitrile U 0.671 10.0 1 06/22/2022 23:06 WG1883724
Benzene U 0.0941 1.00 1 06/22/2022 23:06 WG1883724
Bromodichloromethane U 0.136 1.00 1 06/22/2022 23:06 WG1883724
Bromoform U 0.129 1.00 1 06/22/2022 23:06 WG1883724
Bromomethane U 0.605 5.00 1 06/22/2022 23:06 WG1883724
Carbon tetrachloride U 0.128 1.00 1 06/22/2022 23:06 WG1883724
Chlorobenzene U 0.116 1.00 1 06/22/2022 23:06 WG1883724
Chlorodibromomethane U 0.140 1.00 1 06/22/2022 23:06 WG1883724
Chloroethane U 0.192 5.00 1 06/22/2022 23:06 WG1883724
2-Chloroethyl vinyl ether U 0.575 50.0 1 06/22/2022 23:06 WG1883724
Chloroform U 0.111 5.00 1 06/22/2022 23:06 WG1883724
Chloromethane U 0.960 2.50 1 06/22/2022 23:06 WG1883724
1,2-Dichlorobenzene U 0.107 1.00 1 06/22/2022 23:06 WG1883724
1,3-Dichlorobenzene U 0.110 1.00 1 06/22/2022 23:06 WG1883724
1,4-Dichlorobenzene U 0.120 1.00 1 06/22/2022 23:06 WG1883724
1,1-Dichloroethane U 0.100 1.00 1 06/22/2022 23:06 WG1883724
1,2-Dichloroethane U 0.0819 1.00 1 06/22/2022 23:06 WG1883724
1,1-Dichloroethene U 0.188 1.00 1 06/22/2022 23:06 WG1883724
trans-1,2-Dichloroethene U 0.149 1.00 1 06/22/2022 23:06 WG1883724
1,2-Dichloropropane U 0.149 1.00 1 06/22/2022 23:06 WG1883724
cis-1,3-Dichloropropene U 0.111 1.00 1 06/22/2022 23:06 WG1883724
trans-1,3-Dichloropropene U 0.118 1.00 1 06/22/2022 23:06 WG1883724
Ethylbenzene U 0.137 1.00 1 06/22/2022 23:06 WG1883724
Methylene Chloride U 0.430 5.00 1 06/22/2022 23:06 WG1883724
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 06/22/2022 23:06 WG1883724
Tetrachloroethene U 0.300 1.00 1 06/22/2022 23:06 WG1883724
Toluene U 0.278 1.00 1 06/22/2022 23:06 WG1883724
1,1,1-Trichloroethane U 0.149 1.00 1 06/22/2022 23:06 WG1883724
1,1,2-Trichloroethane U 0.158 1.00 1 06/22/2022 23:06 WG1883724
Trichloroethene U 0.190 1.00 1 06/22/2022 23:06 WG1883724
Vinyl chloride U 0.234 1.00 1 06/22/2022 23:06 WG1883724
(S) Toluene-d8 103 80.0-120 06/22/2022 23:06 WG1883724
(S) 4-Bromofluorobenzene 95.4 80.0-120 06/22/2022 23:06 WG1883724
(S) 1,2-Dichloroethane-d4 97.9 70.0-130 06/22/2022 23:06 WG1883724
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1504501
AIR STACK
Collected date/time: 06/13/22 09:45
Volatile Organic Compounds (MS) by Method M18-Mod
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Benzene 71-43-2 78.10 16.0 51.1 4200 13400 80 WG1879678
Toluene 108-88-3 92.10 40.0 151 2140 8060 80 WG1879678
Ethylbenzene 100-41-4 106 16.0 69.4 745 3230 80 WG1879678
m&p-Xylene 1330-20-7 106 32.0 139 3320 14400 80 WG1879678
o-Xylene 95-47-6 106 16.0 69.4 1460 6330 80 WG1879678
Methyl tert-butyl ether 1634-04-4 88.10 16.0 57.7 ND ND 80 WG1879678
TPH (GC/MS) Low Fraction 8006-61-9 101 80000 330000 530000 2190000 400 WG1880536
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 102 WG1879678
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 94.2 WG1880536
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1881166
Mercury by Method 245.1 L1504501-01
Method Blank (MB)
(MB) R3810448-6 07/03/22 13:05
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.100 0.200
Laboratory Control Sample (LCS)
(LCS) R3810448-1 07/03/22 11:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Mercury 3.00 3.18 106 85.0-115
L1502824-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1502824-01 07/03/22 11:09 • (MS) R3810448-2 07/03/22 11:11 • (MSD) R3810448-3 07/03/22 11:13
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.20 3.05 107 102 1 70.0-130 4.65 20
L1505254-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1505254-06 07/03/22 11:15 • (MS) R3810448-4 07/03/22 11:21 • (MSD) R3810448-5 07/03/22 11:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.19 3.19 106 106 1 70.0-130 0.144 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1884444
Metals (ICPMS) by Method 200.8 L1504501-01
Method Blank (MB)
(MB) R3808081-1 06/27/22 13:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 0.195 1.00
Barium U 0.476 5.00
Cadmium U 0.160 1.00
Chromium U 5.60 20.0
Lead U 0.513 2.00
Selenium U 0.437 2.00
Silver U 0.144 1.00
Laboratory Control Sample (LCS)
(LCS) R3808081-2 06/27/22 13:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Arsenic 50.0 45.9 91.7 85.0-115
Barium 50.0 46.9 93.9 85.0-115
Cadmium 50.0 52.6 105 85.0-115
Chromium 50.0 102 203 85.0-115 J4
Lead 50.0 46.2 92.3 85.0-115
Selenium 50.0 51.3 103 85.0-115
Silver 50.0 48.9 97.8 85.0-115
L1503512-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1503512-01 06/27/22 14:00 • (MS) R3808081-4 06/27/22 14:07 • (MSD) R3808081-5 06/27/22 14:10
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 6.91 54.4 52.9 95.0 91.9 10 70.0-130 2.95 20
Barium 50.0 U 51.8 54.6 104 109 10 70.0-130 5.35 20
Cadmium 50.0 3.32 56.3 54.8 106 103 10 70.0-130 2.70 20
Chromium 50.0 1220 1100 1060 0.000 0.000 10 70.0-130 V V 4.32 20
Lead 50.0 U 50.8 49.7 102 99.3 10 70.0-130 2.37 20
Selenium 50.0 U 54.6 51.6 109 103 10 70.0-130 5.58 20
Silver 50.0 1.52 49.5 49.0 95.9 95.0 10 70.0-130 0.983 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1884444
Metals (ICPMS) by Method 200.8 L1504501-01
L1504994-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1504994-01 06/27/22 14:14 • (MS) R3808081-6 06/27/22 14:17 • (MSD) R3808081-7 06/27/22 14:20
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 1.86 47.8 46.6 91.9 89.4 1 70.0-130 2.67 20
Barium 50.0 45.8 92.4 92.1 93.3 92.6 1 70.0-130 0.386 20
Cadmium 50.0 U 51.5 51.4 103 103 1 70.0-130 0.264 20
Chromium 50.0 U 48.8 47.5 97.6 94.9 1 70.0-130 2.78 20
Lead 50.0 0.669 48.5 47.0 95.7 92.7 1 70.0-130 3.08 20
Selenium 50.0 1.23 52.2 50.9 102 99.3 1 70.0-130 2.51 20
Silver 50.0 U 48.9 48.1 97.7 96.2 1 70.0-130 1.60 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1879678
Volatile Organic Compounds (MS) by Method M18-Mod L1504501-02
Method Blank (MB)
(MB) R3803433-3 06/15/22 10:27
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Benzene U 0.0715 0.200
Toluene U 0.0870 0.500
Ethylbenzene U 0.0835 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
MTBE U 0.0647 0.200
(S) 1,4-Bromofluorobenzene 93.0 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3803433-1 06/15/22 09:21 • (LCSD) R3803433-2 06/15/22 09:54
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Benzene 3.75 4.67 4.82 125 129 70.0-130 3.16 25
Toluene 3.75 4.66 4.79 124 128 70.0-130 2.75 25
Ethylbenzene 3.75 4.69 4.88 125 130 70.0-130 3.97 25
m&p-Xylene 7.50 9.33 9.70 124 129 70.0-130 3.89 25
o-Xylene 3.75 4.55 4.69 121 125 70.0-130 3.03 25
MTBE 3.75 4.71 4.79 126 128 70.0-130 1.68 25
(S) 1,4-Bromofluorobenzene 95.6 96.4 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1880536
Volatile Organic Compounds (MS) by Method M18-Mod L1504501-02
Method Blank (MB)
(MB) R3803894-3 06/16/22 11:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
TPH (GC/MS) Low Fraction U 39.7 200
(S) 1,4-Bromofluorobenzene 92.9 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3803894-1 06/16/22 10:47 • (LCSD) R3803894-2 06/16/22 11:19
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
TPH (GC/MS) Low Fraction 203 197 199 97.0 98.0 70.0-130 1.01 25
(S) 1,4-Bromofluorobenzene 95.3 94.6 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1883724
Volatile Organic Compounds (GC/MS) by Method 624.1 L1504501-01
Method Blank (MB)
(MB) R3806610-3 06/22/22 22:32
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
2-Chloroethyl vinyl ether U 0.575 50.0
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
Ethylbenzene U 0.137 1.00
Methylene Chloride U 0.430 5.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Vinyl chloride U 0.234 1.00
(S) Toluene-d8 104 80.0-120
(S) 4-Bromofluorobenzene 94.4 80.0-120
(S) 1,2-Dichloroethane-d4 95.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1883724
Volatile Organic Compounds (GC/MS) by Method 624.1 L1504501-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3806610-1 06/22/22 21:29 • (LCSD) R3806610-2 06/22/22 21:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acrolein 25.0 25.2 27.5 101 110 60.0-140 8.73 20
Acrylonitrile 25.0 21.9 23.0 87.6 92.0 60.0-140 4.90 20
Benzene 5.00 4.88 4.91 97.6 98.2 65.0-135 0.613 20
Bromodichloromethane 5.00 4.55 4.34 91.0 86.8 65.0-135 4.72 20
Bromoform 5.00 3.84 3.80 76.8 76.0 70.0-130 1.05 20
Bromomethane 5.00 5.02 5.29 100 106 15.0-185 5.24 20
Carbon tetrachloride 5.00 4.28 4.40 85.6 88.0 70.0-130 2.76 20
Chlorobenzene 5.00 4.51 4.64 90.2 92.8 65.0-135 2.84 20
Chlorodibromomethane 5.00 3.93 4.19 78.6 83.8 70.0-135 6.40 20
Chloroethane 5.00 3.86 3.87 77.2 77.4 40.0-160 0.259 20
2-Chloroethyl vinyl ether 25.0 20.6 20.1 82.4 80.4 0.100-225 2.46 20
Chloroform 5.00 5.16 4.96 103 99.2 70.0-135 3.95 20
Chloromethane 5.00 4.54 4.67 90.8 93.4 0.100-205 2.82 20
1,2-Dichlorobenzene 5.00 4.63 4.73 92.6 94.6 65.0-135 2.14 20
1,3-Dichlorobenzene 5.00 4.54 4.60 90.8 92.0 70.0-130 1.31 20
1,4-Dichlorobenzene 5.00 4.59 4.49 91.8 89.8 65.0-135 2.20 20
1,1-Dichloroethane 5.00 4.63 4.70 92.6 94.0 70.0-130 1.50 20
1,2-Dichloroethane 5.00 4.62 4.50 92.4 90.0 70.0-130 2.63 20
1,1-Dichloroethene 5.00 5.08 5.48 102 110 50.0-150 7.58 20
trans-1,2-Dichloroethene 5.00 5.34 5.15 107 103 70.0-130 3.62 20
1,2-Dichloropropane 5.00 4.59 4.52 91.8 90.4 35.0-165 1.54 20
cis-1,3-Dichloropropene 5.00 4.24 4.36 84.8 87.2 25.0-175 2.79 20
trans-1,3-Dichloropropene 5.00 4.34 4.48 86.8 89.6 50.0-150 3.17 20
Ethylbenzene 5.00 4.33 4.55 86.6 91.0 60.0-140 4.95 20
Methylene Chloride 5.00 5.34 5.39 107 108 60.0-140 0.932 20
1,1,2,2-Tetrachloroethane 5.00 4.92 4.87 98.4 97.4 60.0-140 1.02 20
Tetrachloroethene 5.00 4.76 4.75 95.2 95.0 70.0-130 0.210 20
Toluene 5.00 4.78 4.88 95.6 97.6 70.0-130 2.07 20
1,1,1-Trichloroethane 5.00 4.87 4.94 97.4 98.8 70.0-130 1.43 20
1,1,2-Trichloroethane 5.00 4.65 4.87 93.0 97.4 70.0-130 4.62 20
Trichloroethene 5.00 4.59 4.90 91.8 98.0 65.0-135 6.53 20
Vinyl chloride 5.00 3.93 4.15 78.6 83.0 5.00-195 5.45 20
(S) Toluene-d8 104 104 80.0-120
(S) 4-Bromofluorobenzene 99.6 101 80.0-120
(S) 1,2-Dichloroethane-d4 98.4 95.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
V The sample concentration is too high to evaluate accurate spike recoveries.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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#=CL#
July 27, 2022
LIMS USE: FR - MARIANNE LINK
LIMS OBJECT ID: 92616976
92616976
Project:
Pace Project No.:
RE:
Marianne Link
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
Transfeer Speedway Site-6958 B
Dear Marianne Link:
Enclosed are the analytical results for sample(s) received by the laboratory on July 19, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 8
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 8
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92616976001 Air Stack Method 18 Air MeOH & EtOH 8 PANCEP
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 8
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
Sample: Air Stack Lab ID: 92616976001 Collected: 07/18/22 12:00 Received: 07/19/22 10:15 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 35800 ug/m3 07/20/22 00:10 71-43-207/20/22 00:101280 2000
Toluene 32200 ug/m3 07/20/22 00:10 108-88-307/20/22 00:103770 2000
Ethylbenzene 10200 ug/m3 07/20/22 00:10 100-41-407/20/22 00:101730 2000
m&p-Xylene 68500 ug/m3 07/20/22 00:10 179601-23-107/20/22 00:103470 2000
o-Xylene 22300 ug/m3 07/20/22 00:10 95-47-607/20/22 00:101730 2000
Methyl-tert-butyl ether ND ug/m3 07/20/22 00:10 1634-04-407/20/22 00:101440 2000
Gasoline Range Organics 4790000 ug/m3 07/20/22 00:10 8006-61-907/20/22 00:101650000 2000
Surrogates
1,4-Dichlorobenzene-d4 (IS)82.7 %07/20/22 00:10 3855-82-107/20/22 00:1060.0-140 2000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/27/2022 02:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 8
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1897337
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92616976001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3816982-3
Associated Lab Samples:92616976001
Matrix: Air
Analyzed
Benzene ppbv ND 0.200 07/19/22 10:05
Toluene ppbv ND 0.500 07/19/22 10:05
Ethylbenzene ppbv ND 0.200 07/19/22 10:05
m&p-Xylene ppbv ND 0.400 07/19/22 10:05
o-Xylene ppbv ND 0.200 07/19/22 10:05
Methyl-tert-butyl ether ppbv ND 0.200 07/19/22 10:05
Gasoline Range Organics ppbv ND 200 07/19/22 10:05
1,4-Dichlorobenzene-d4 (IS)%84.7 60.0-140 07/19/22 10:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3816982-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3816982-2
Benzene ppbv 3.733.75 99.5 70.0-1301023.81 2.12 25
Toluene ppbv 3.863.75 103 70.0-1301053.92 1.54 25
Ethylbenzene ppbv 3.993.75 106 70.0-1301094.09 2.48 25
m&p-Xylene ppbv 7.977.50 106 70.0-1301088.13 1.99 25
o-Xylene ppbv 3.903.75 104 70.0-1301063.97 1.78 25
Methyl-tert-butyl ether ppbv 3.733.75 99.5 70.0-1301003.76 0.801 25
Gasoline Range Organics ppbv 204203 100 70.0-130103209 2.42 25
1,4-Dichlorobenzene-d4 (IS)%87.9 60.0-14088.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/27/2022 02:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 8
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92616976001
Volatile Organic Compounds (MS) by Method M18-Mod - Non-target compounds too high to run at a lower dilution.[1]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/27/2022 02:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 8
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92616976
Transfeer Speedway Site-6958 B
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92616976001 1897337 1897337Air Stack M18-Mod Method 18 Air MeOH &EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/27/2022 02:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 8
Page 8 of 8
ANALYTICAL REPORT
August 22, 2022
AECOM - Speedway
Sample Delivery Group:L1525449
Samples Received:08/16/2022
Project Number:60686627
Description:Speedway #6958
Report To:Marianne Link
5438 Wade Park Blvd
Suite 200
Raleigh, NC 27607
Entire Report Reviewed By:
August 22, 2022
[Preliminary Report]
Marty Edwards III
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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August 22, 2022
Marty Edwards III
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
AIR STACK L1525449-01 5
Qc: Quality Control Summary 6
Volatile Organic Compounds (MS) by Method M18-Mod 6
Gl: Glossary of Terms 7
Al: Accreditations & Locations 8
Sc: Sample Chain of Custody 9
1 Cp
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3Ss
4Cn
5Sr
6Qc
7Gl
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
AIR STACK L1525449-01 Air Jerry Maciejewski 08/15/22 11:30 08/16/22 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method M18-Mod WG1911574 2000 08/16/22 19:53 08/16/22 19:53 CEP Mt. Juliet, TN
1 Cp
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3Ss
4Cn
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Marty Edwards III
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Marty Edwards III
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1525449
AIR STACK
Collected date/time: 08/15/22 11:30
Volatile Organic Compounds (MS) by Method M18-Mod
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Benzene 71-43-2 78.10 400 1280 24100 77000 2000 WG1911574
Toluene 108-88-3 92.10 1000 3770 15200 57300 2000 WG1911574
Ethylbenzene 100-41-4 106 400 1730 3260 14100 2000 WG1911574
m&p-Xylene 1330-20-7 106 800 3470 29900 130000 2000 WG1911574
o-Xylene 95-47-6 106 400 1730 9400 40800 2000 WG1911574
Methyl tert-butyl ether 1634-04-4 88.10 400 1440 ND ND 2000 WG1911574
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 90.6 WG1911574
Sample Narrative:
L1525449-01 WG1911574: Non-target compounds too high to run at a lower dilution.
1 Cp
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3Ss
4Cn
5Sr
6Qc
7Gl
8Al
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QUALITY CONTROL SUMMARYWG1911574
Volatile Organic Compounds (MS) by Method M18-Mod L1525449-01
Method Blank (MB)
(MB) R3827141-3 08/16/22 11:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Benzene U 0.0715 0.200
Toluene U 0.0870 0.500
Ethylbenzene U 0.0835 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
MTBE U 0.0647 0.200
(S) 1,4-Bromofluorobenzene 88.8 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3827141-1 08/16/22 09:12 • (LCSD) R3827141-2 08/16/22 09:57
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Benzene 3.75 4.18 4.20 111 112 70.0-130 0.477 25
Toluene 3.75 4.09 4.10 109 109 70.0-130 0.244 25
Ethylbenzene 3.75 4.28 4.28 114 114 70.0-130 0.000 25
m&p-Xylene 7.50 8.59 8.67 115 116 70.0-130 0.927 25
o-Xylene 3.75 4.11 4.14 110 110 70.0-130 0.727 25
MTBE 3.75 4.31 4.32 115 115 70.0-130 0.232 25
(S) 1,4-Bromofluorobenzene 95.5 94.9 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
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ANALYTICAL REPORT
September 19, 2022
AECOM - Speedway
Sample Delivery Group:L1535946
Samples Received:09/15/2022
Project Number:60686627
Description:Speedway #6958 Burlington, NC
Report To:Marianne Link
5438 Wade Park Blvd
Suite 200
Raleigh, NC 27607
Entire Report Reviewed By:
September 19, 2022
[Preliminary Report]
Marty Edwards III
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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September 20, 2022
Marty Edwards III
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
AIR STACK L1535946-01 5
Qc: Quality Control Summary 6
Volatile Organic Compounds (MS) by Method M18-Mod 6
Gl: Glossary of Terms 8
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
1 Cp
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3Ss
4Cn
5Sr
6Qc
7Gl
8Al
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
AIR STACK L1535946-01 Air Jerry Maciejewski 09/14/22 09:00 09/15/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (MS) by Method M18-Mod WG1927061 400 09/15/22 23:22 09/15/22 23:22 SDS Mt. Juliet, TN
Volatile Organic Compounds (MS) by Method M18-Mod WG1927483 4000 09/16/22 15:38 09/16/22 15:38 DAH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Marty Edwards III
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Marty Edwards III
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1535946
AIR STACK
Collected date/time: 09/14/22 09:00
Volatile Organic Compounds (MS) by Method M18-Mod
CAS # Mol. Wt. RDL1 RDL2 Result Result Qualifier Dilution Batch
Analyte ppbv ug/m3 ppbv ug/m3
Benzene 71-43-2 78.10 80.0 256 31600 101000 400 WG1927061
Toluene 108-88-3 92.10 200 753 21300 80200 400 WG1927061
Ethylbenzene 100-41-4 106 80.0 347 4380 19000 400 WG1927061
m&p-Xylene 1330-20-7 106 160 694 40300 175000 400 WG1927061
o-Xylene 95-47-6 106 80.0 347 17800 77200 400 WG1927061
Methyl tert-butyl ether 1634-04-4 88.10 80.0 288 ND ND 400 WG1927061
TPH (GC/MS) Low Fraction 8006-61-9 101 800000 3300000 3900000 16100000 4000 WG1927483
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 101 WG1927061
(S) 1,4-Bromofluorobenzene 460-00-4 175 60.0-140 102 WG1927483
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1927061
Volatile Organic Compounds (MS) by Method M18-Mod L1535946-01
Method Blank (MB)
(MB) R3837925-3 09/15/22 13:38
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
Benzene U 0.0715 0.200
Toluene U 0.0870 0.500
Ethylbenzene U 0.0835 0.200
m&p-Xylene U 0.135 0.400
o-Xylene U 0.0828 0.200
MTBE U 0.0647 0.200
(S) 1,4-Bromofluorobenzene 96.1 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3837925-1 09/15/22 12:39 • (LCSD) R3837925-2 09/15/22 13:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
Benzene 3.75 3.88 3.86 103 103 70.0-130 0.517 25
Toluene 3.75 4.02 4.00 107 107 70.0-130 0.499 25
Ethylbenzene 3.75 4.17 4.16 111 111 70.0-130 0.240 25
m&p-Xylene 7.50 9.13 9.10 122 121 70.0-130 0.329 25
o-Xylene 3.75 4.45 4.46 119 119 70.0-130 0.224 25
MTBE 3.75 3.96 3.94 106 105 70.0-130 0.506 25
(S) 1,4-Bromofluorobenzene 102 101 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1927483
Volatile Organic Compounds (MS) by Method M18-Mod L1535946-01
Method Blank (MB)
(MB) R3838038-3 09/16/22 10:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ppbv ppbv ppbv
TPH (GC/MS) Low Fraction U 39.7 200
(S) 1,4-Bromofluorobenzene 103 60.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3838038-1 09/16/22 08:44 • (LCSD) R3838038-2 09/16/22 09:26
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ppbv ppbv ppbv %%%%%
TPH (GC/MS) Low Fraction 203 218 199 107 98.0 70.0-130 9.11 25
(S) 1,4-Bromofluorobenzene 102 102 60.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Speedway 60686627 L1535946 09/19/22 17:06 9 of 10
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Speedway 60686627 L1535946 09/20/22 13:26 9 of 10
#=CL#
October 20, 2022
LIMS USE: FR - MARIANNE LINK
LIMS OBJECT ID: 92630529
92630529
Project:
Pace Project No.:
RE:
Marianne Link
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
7-Eleven 6958 Burlington
Dear Marianne Link:
Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
Report Revision 1: On 10/18/22, Total Xylenes was added and reported.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92630529001 EFFLUENT EPA 608.3 30 PASI-CSEM
EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CAP2
EPA 5030B/8015C 2 PASI-CTEG
EPA 200.7 1 PASI-GAKH
EPA 245.1 1 PASI-GAVB
EPA 6010D 11 PASI-GAKH
EPA 625.1 62 PASI-CPKS
EPA 624.1 36 PASI-CSAS
SM 4500-CN-E-2011 1 PASI-AANM
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Sample: EFFLUENT Lab ID: 92630529001 Collected: 10/10/22 16:00 Received: 10/11/22 09:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services - Charlotte
608 PCB Pest RVE
Aldrin ND mg/L 10/13/22 17:28 309-00-210/12/22 12:080.000042 1
alpha-BHC ND mg/L 10/13/22 17:28 319-84-610/12/22 12:080.000042 1
beta-BHC ND mg/L 10/13/22 17:28 319-85-710/12/22 12:080.000042 1
delta-BHC ND mg/L 10/13/22 17:28 319-86-810/12/22 12:080.000042 1
gamma-BHC (Lindane)ND mg/L 10/13/22 17:28 58-89-910/12/22 12:080.000042 1
Chlordane (Technical)ND mg/L 10/13/22 17:28 57-74-910/12/22 12:080.00042 1
alpha-Chlordane ND mg/L 10/13/22 17:28 5103-71-910/12/22 12:080.000042 1
gamma-Chlordane ND mg/L 10/13/22 17:28 5103-74-210/12/22 12:080.000042 1
4,4'-DDD ND mg/L 10/13/22 17:28 72-54-810/12/22 12:080.000042 1
4,4'-DDE ND mg/L 10/13/22 17:28 72-55-910/12/22 12:080.000042 1
4,4'-DDT ND mg/L 10/13/22 17:28 50-29-310/12/22 12:080.000042 1
Dieldrin ND mg/L 10/13/22 17:28 60-57-110/12/22 12:080.000042 1
Endosulfan I ND mg/L 10/13/22 17:28 959-98-810/12/22 12:080.000042 1
Endosulfan II ND mg/L 10/13/22 17:28 33213-65-910/12/22 12:080.000042 1
Endosulfan sulfate ND mg/L 10/13/22 17:28 1031-07-810/12/22 12:080.000042 1
Endrin ND mg/L 10/13/22 17:28 72-20-810/12/22 12:080.000042 1
Endrin aldehyde ND mg/L 10/13/22 17:28 7421-93-410/12/22 12:080.000042 1
Heptachlor ND mg/L 10/13/22 17:28 76-44-810/12/22 12:080.000042 1
Heptachlor epoxide ND mg/L 10/13/22 17:28 1024-57-310/12/22 12:080.000042 1
PCB-1016 (Aroclor 1016)ND mg/L 10/13/22 17:28 12674-11-210/12/22 12:080.00042 1
PCB-1221 (Aroclor 1221)ND mg/L 10/13/22 17:28 11104-28-210/12/22 12:080.00042 1
PCB-1232 (Aroclor 1232)ND mg/L 10/13/22 17:28 11141-16-510/12/22 12:080.00042 1
PCB-1242 (Aroclor 1242)ND mg/L 10/13/22 17:28 53469-21-910/12/22 12:080.00042 1
PCB-1248 (Aroclor 1248)ND mg/L 10/13/22 17:28 12672-29-610/12/22 12:080.00042 1
PCB-1254 (Aroclor 1254)ND mg/L 10/13/22 17:28 11097-69-110/12/22 12:080.00042 1
PCB-1260 (Aroclor 1260)ND mg/L 10/13/22 17:28 11096-82-510/12/22 12:080.00042 1
PCB, Total ND mg/L 10/13/22 17:28 1336-36-310/12/22 12:080.00042 1
Toxaphene ND mg/L 10/13/22 17:28 8001-35-210/12/22 12:080.00042 1
Surrogates
Tetrachloro-m-xylene (S)45 %10/13/22 17:28 877-09-810/12/22 12:0810-154 1
Decachlorobiphenyl (S)139 %10/13/22 17:28 2051-24-310/12/22 12:0810-184 1
Analytical Method: EPA 8015C Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Diesel Low Volume
Diesel Range Organics(C10-C28)ND mg/L 10/12/22 23:0410/12/22 12:030.50 1
Surrogates
n-Pentacosane (S)106 %10/12/22 23:04 629-99-210/12/22 12:0341-183 1
Analytical Method: EPA 8015C Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8015 Oil Range Low Volume
Oil Range Organics (C28-C40)ND mg/L 10/12/22 23:0410/12/22 12:032.0 1
Surrogates
n-Pentacosane (S)72 %10/12/22 23:04 629-99-210/12/22 12:0341-183 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Sample: EFFLUENT Lab ID: 92630529001 Collected: 10/10/22 16:00 Received: 10/11/22 09:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 5030B/8015C
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/L 10/12/22 16:020.080 1
Surrogates
4-Bromofluorobenzene (S)96 %10/12/22 16:02 460-00-470-130 1
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services - Peachtree Corners, GA
200.7 MET ICP
Cadmium ND mg/L 10/13/22 16:14 7440-43-910/13/22 11:500.010 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Pace Analytical Services - Peachtree Corners, GA
245.1 Mercury
Mercury ND mg/L 10/13/22 14:35 7439-97-610/13/22 08:000.00020 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Antimony ND mg/L 10/13/22 21:31 7440-36-010/13/22 15:140.050 1
Arsenic ND mg/L 10/13/22 21:31 7440-38-210/13/22 15:140.030 1
Beryllium ND mg/L 10/13/22 21:31 7440-41-710/13/22 15:140.010 1
Chromium ND mg/L 10/13/22 21:31 7440-47-310/13/22 15:140.010 1
Copper ND mg/L 10/13/22 21:31 7440-50-810/13/22 15:140.020 1
Lead 0.020 mg/L 10/13/22 21:31 7439-92-110/13/22 15:140.020 1
Nickel ND mg/L 10/13/22 21:31 7440-02-010/13/22 15:140.020 1
Selenium ND mg/L 10/13/22 21:31 7782-49-210/13/22 15:140.040 1
Silver ND mg/L 10/13/22 21:31 7440-22-410/13/22 15:140.010 1
Thallium ND mg/L 10/13/22 21:31 7440-28-010/13/22 15:140.20 1
Zinc ND mg/L 10/13/22 21:31 7440-66-610/13/22 15:140.020 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND mg/L 10/13/22 00:50 83-32-910/11/22 18:170.0042 1
Acenaphthylene ND mg/L 10/13/22 00:50 208-96-810/11/22 18:170.0042 1
Anthracene ND mg/L 10/13/22 00:50 120-12-710/11/22 18:170.0042 1
Benzo(a)anthracene ND mg/L 10/13/22 00:50 56-55-310/11/22 18:170.0042 1
Benzo(a)pyrene ND mg/L 10/13/22 00:50 50-32-810/11/22 18:170.0042 1
Benzo(b)fluoranthene ND mg/L 10/13/22 00:50 205-99-210/11/22 18:170.0042 1
Benzo(g,h,i)perylene ND mg/L 10/13/22 00:50 191-24-210/11/22 18:170.0042 1
Benzo(k)fluoranthene ND mg/L 10/13/22 00:50 207-08-910/11/22 18:170.0042 1
4-Bromophenylphenyl ether ND mg/L 10/13/22 00:50 101-55-310/11/22 18:170.0042 1
Butylbenzylphthalate ND mg/L 10/13/22 00:50 85-68-710/11/22 18:170.0042 1
4-Chloro-3-methylphenol ND mg/L 10/13/22 00:50 59-50-710/11/22 18:170.0042 1
bis(2-Chloroethoxy)methane ND mg/L 10/13/22 00:50 111-91-110/11/22 18:170.0083 1
bis(2-Chloroethyl) ether ND mg/L 10/13/22 00:50 111-44-410/11/22 18:170.0042 1
2-Chloronaphthalene ND mg/L 10/13/22 00:50 91-58-710/11/22 18:170.0042 1
2-Chlorophenol ND mg/L 10/13/22 00:50 95-57-810/11/22 18:170.0042 1
4-Chlorophenylphenyl ether ND mg/L 10/13/22 00:50 7005-72-310/11/22 18:170.0042 1
Chrysene ND mg/L 10/13/22 00:50 218-01-910/11/22 18:170.0042 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Sample: EFFLUENT Lab ID: 92630529001 Collected: 10/10/22 16:00 Received: 10/11/22 09:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Dibenz(a,h)anthracene ND mg/L 10/13/22 00:50 53-70-310/11/22 18:170.0042 1
1,2-Dichlorobenzene ND mg/L 10/13/22 00:50 95-50-110/11/22 18:170.0042 1
1,3-Dichlorobenzene ND mg/L 10/13/22 00:50 541-73-110/11/22 18:170.0042 1
1,4-Dichlorobenzene ND mg/L 10/13/22 00:50 106-46-710/11/22 18:170.0042 1
3,3'-Dichlorobenzidine ND mg/L 10/13/22 00:50 91-94-110/11/22 18:170.0083 1
2,4-Dichlorophenol ND mg/L 10/13/22 00:50 120-83-210/11/22 18:170.0042 1
Diethylphthalate ND mg/L 10/13/22 00:50 84-66-2 L110/11/22 18:170.0042 1
2,4-Dimethylphenol ND mg/L 10/13/22 00:50 105-67-9 L110/11/22 18:170.0083 1
Dimethylphthalate ND mg/L 10/13/22 00:50 131-11-3 L110/11/22 18:170.0042 1
Di-n-butylphthalate ND mg/L 10/13/22 00:50 84-74-2 L110/11/22 18:170.0042 1
4,6-Dinitro-2-methylphenol ND mg/L 10/13/22 00:50 534-52-110/11/22 18:170.0083 1
2,4-Dinitrophenol ND mg/L 10/13/22 00:50 51-28-510/11/22 18:170.042 1
2,4-Dinitrotoluene ND mg/L 10/13/22 00:50 121-14-210/11/22 18:170.0042 1
2,6-Dinitrotoluene ND mg/L 10/13/22 00:50 606-20-210/11/22 18:170.0042 1
Di-n-octylphthalate ND mg/L 10/13/22 00:50 117-84-0 L110/11/22 18:170.0042 1
1,2-Diphenylhydrazine ND mg/L 10/13/22 00:50 122-66-710/11/22 18:170.0042 1
bis(2-Ethylhexyl)phthalate ND mg/L 10/13/22 00:50 117-81-710/11/22 18:170.0042 1
Fluoranthene ND mg/L 10/13/22 00:50 206-44-010/11/22 18:170.0042 1
Fluorene ND mg/L 10/13/22 00:50 86-73-710/11/22 18:170.0042 1
Hexachloro-1,3-butadiene ND mg/L 10/13/22 00:50 87-68-310/11/22 18:170.0042 1
Hexachlorobenzene ND mg/L 10/13/22 00:50 118-74-110/11/22 18:170.0042 1
Hexachlorocyclopentadiene ND mg/L 10/13/22 00:50 77-47-410/11/22 18:170.0083 1
Hexachloroethane ND mg/L 10/13/22 00:50 67-72-1 L210/11/22 18:170.0042 1
Indeno(1,2,3-cd)pyrene ND mg/L 10/13/22 00:50 193-39-510/11/22 18:170.0042 1
Isophorone ND mg/L 10/13/22 00:50 78-59-110/11/22 18:170.0083 1
Naphthalene ND mg/L 10/13/22 00:50 91-20-310/11/22 18:170.0042 1
Nitrobenzene ND mg/L 10/13/22 00:50 98-95-310/11/22 18:170.0042 1
2-Nitrophenol ND mg/L 10/13/22 00:50 88-75-510/11/22 18:170.0042 1
4-Nitrophenol ND mg/L 10/13/22 00:50 100-02-710/11/22 18:170.0083 1
N-Nitrosodimethylamine ND mg/L 10/13/22 00:50 62-75-910/11/22 18:170.0042 1
N-Nitroso-di-n-propylamine ND mg/L 10/13/22 00:50 621-64-710/11/22 18:170.0042 1
N-Nitrosodiphenylamine ND mg/L 10/13/22 00:50 86-30-610/11/22 18:170.0083 1
2,2'-Oxybis(1-chloropropane)ND mg/L 10/13/22 00:50 108-60-110/11/22 18:170.0042 1
Pentachlorophenol ND mg/L 10/13/22 00:50 87-86-510/11/22 18:170.0083 1
Phenanthrene ND mg/L 10/13/22 00:50 85-01-8 L110/11/22 18:170.0042 1
Phenol ND mg/L 10/13/22 00:50 108-95-210/11/22 18:170.0042 1
Pyrene ND mg/L 10/13/22 00:50 129-00-010/11/22 18:170.0042 1
1,2,4-Trichlorobenzene ND mg/L 10/13/22 00:50 120-82-110/11/22 18:170.0042 1
2,4,6-Trichlorophenol ND mg/L 10/13/22 00:50 88-06-210/11/22 18:170.0083 1
Surrogates
Nitrobenzene-d5 (S)46 %10/13/22 00:50 4165-60-010/11/22 18:1710-120 1
2-Fluorobiphenyl (S)15 %10/13/22 00:50 321-60-810/11/22 18:1715-120 1
Terphenyl-d14 (S)138 %10/13/22 00:50 1718-51-0 S310/11/22 18:1711-131 1
Phenol-d6 (S)22 %10/13/22 00:50 13127-88-310/11/22 18:1710-120 1
2-Fluorophenol (S)21 %10/13/22 00:50 367-12-410/11/22 18:1710-120 1
2,4,6-Tribromophenol (S)55 %10/13/22 00:50 118-79-610/11/22 18:1710-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Sample: EFFLUENT Lab ID: 92630529001 Collected: 10/10/22 16:00 Received: 10/11/22 09:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
624 Volatile Organics Acrolein
Acrolein ND mg/L 10/12/22 18:59 107-02-80.0050 1
Acrylonitrile ND mg/L 10/12/22 18:59 107-13-10.0050 1
Benzene ND mg/L 10/12/22 18:59 71-43-20.0010 1
Bromodichloromethane ND mg/L 10/12/22 18:59 75-27-40.0020 1
Bromoform ND mg/L 10/12/22 18:59 75-25-20.0020 1
Bromomethane ND mg/L 10/12/22 18:59 74-83-90.0020 1
Carbon tetrachloride ND mg/L 10/12/22 18:59 56-23-50.0020 1
Chlorobenzene ND mg/L 10/12/22 18:59 108-90-70.0020 1
Chloroethane ND mg/L 10/12/22 18:59 75-00-30.0020 1
2-Chloroethylvinyl ether ND mg/L 10/12/22 18:59 110-75-80.0050 1
Chloroform ND mg/L 10/12/22 18:59 67-66-30.0020 1
Chloromethane ND mg/L 10/12/22 18:59 74-87-30.0020 1
Dibromochloromethane ND mg/L 10/12/22 18:59 124-48-10.0020 1
1,1-Dichloroethane ND mg/L 10/12/22 18:59 75-34-30.0020 1
1,2-Dichloroethane ND mg/L 10/12/22 18:59 107-06-20.0020 1
1,1-Dichloroethene ND mg/L 10/12/22 18:59 75-35-40.0020 1
trans-1,2-Dichloroethene ND mg/L 10/12/22 18:59 156-60-50.0020 1
1,2-Dichloropropane ND mg/L 10/12/22 18:59 78-87-50.0020 1
cis-1,3-Dichloropropene ND mg/L 10/12/22 18:59 10061-01-50.0020 1
trans-1,3-Dichloropropene ND mg/L 10/12/22 18:59 10061-02-60.0020 1
Ethylbenzene ND mg/L 10/12/22 18:59 100-41-40.0010 1
Methylene Chloride ND mg/L 10/12/22 18:59 75-09-2 L10.0020 1
Naphthalene ND mg/L 10/12/22 18:59 91-20-30.0050 1
1,1,2,2-Tetrachloroethane ND mg/L 10/12/22 18:59 79-34-50.0020 1
Tetrachloroethene ND mg/L 10/12/22 18:59 127-18-40.0020 1
Toluene ND mg/L 10/12/22 18:59 108-88-30.0010 1
1,1,1-Trichloroethane ND mg/L 10/12/22 18:59 71-55-60.0020 1
1,1,2-Trichloroethane ND mg/L 10/12/22 18:59 79-00-50.0020 1
Trichloroethene ND mg/L 10/12/22 18:59 79-01-60.0020 1
Vinyl chloride ND mg/L 10/12/22 18:59 75-01-40.0020 1
Xylene (Total)ND ug/L 10/12/22 18:59 1330-20-73.0 1
m&p-Xylene ND ug/L 10/12/22 18:59 179601-23-15.0 1
o-Xylene ND ug/L 10/12/22 18:59 95-47-65.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/12/22 18:59 460-00-470-130 1
Toluene-d8 (S)107 %10/12/22 18:59 2037-26-570-130 1
1,2-Dichloroethane-d4 (S)90 %10/12/22 18:59 17060-07-070-130 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide ND mg/L 10/12/22 20:10 57-12-510/12/22 17:060.0080 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729734
EPA 5030B/8015C
EPA 5030B/8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799862
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Gas Range Organics (C6-C10)mg/L ND 0.080 10/12/22 15:34
4-Bromofluorobenzene (S)%93 70-130 10/12/22 15:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799863LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/L 0.991 99 70-130
4-Bromofluorobenzene (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799864MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630641001
3799865
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Gas Range Organics (C6-C10) mg/L 1 99 63-13097 21ND1.0 0.98
4-Bromofluorobenzene (S)%96 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729971
EPA 200.7
EPA 200.7
200.7 Metals Total
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3800917
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Cadmium mg/L ND 0.010 10/13/22 15:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3800918LABORATORY CONTROL SAMPLE:
LCSSpike
Cadmium mg/L 1.01 104 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3800919MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629474001
3800920
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cadmium mg/L 1 105 70-130108 21ND1.1 1.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3800921MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630488003
3800922
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cadmium mg/L 1 107 70-130106 11ND1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729698
EPA 245.1
EPA 245.1
245.1 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799623
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Mercury mg/L ND 0.00020 10/13/22 10:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799624LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.00230.0025 92 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799625MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629342002
3799626
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L 0.0025 87 70-13086 10.0025ND 0.0022 0.0022
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799627MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629652001
3799628
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L 0.0025 84 70-13085 10.0025ND 0.0022 0.0022
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730072
EPA 3010A
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3801632
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Antimony mg/L ND 0.050 10/13/22 20:19
Arsenic mg/L ND 0.030 10/13/22 20:19
Beryllium mg/L ND 0.010 10/13/22 20:19
Chromium mg/L ND 0.010 10/13/22 20:19
Copper mg/L ND 0.020 10/13/22 20:19
Lead mg/L ND 0.020 10/13/22 20:19
Nickel mg/L ND 0.020 10/13/22 20:19
Selenium mg/L ND 0.040 10/13/22 20:19
Silver mg/L ND 0.010 10/13/22 20:19
Thallium mg/L ND 0.20 10/13/22 20:19
Zinc mg/L ND 0.020 10/13/22 20:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3801633LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/L 1.01 104 80-120
Arsenic mg/L 1.11 105 80-120
Beryllium mg/L 1.11 109 80-120
Chromium mg/L 1.11 107 80-120
Copper mg/L 1.11 108 80-120
Lead mg/L 1.11 105 80-120
Nickel mg/L 1.11 106 80-120
Selenium mg/L 1.11 107 80-120
Silver mg/L 1.01 104 80-120
Thallium mg/L 1.01 103 80-120
Zinc mg/L 1.01 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3801634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630198001
3801635
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony mg/L 1 102 75-12599 31ND1.0 0.99
Arsenic mg/L 1 105 75-125101 41ND1.1 1.0
Beryllium mg/L 1 109 75-125108 01ND1.1 1.1
Chromium mg/L 1 107 75-125105 11ND1.1 1.1
Copper mg/L 1 109 75-125108 11ND1.1 1.1
Lead mg/L 1 107 75-125105 21ND1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3801634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630198001
3801635
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nickel mg/L 1 107 75-125105 21ND1.1 1.1
Selenium mg/L 1 106 75-125105 11ND1.1 1.0
Silver mg/L 1 102 75-125100 21ND1.0 1.0
Thallium mg/L 1 104 75-125103 21ND1.0 1.0
Zinc mg/L 1 104 75-125101 2162.5
ug/L
1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729751
EPA 624.1
EPA 624.1
624 MSV with Acrolein
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799949
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
1,1,1-Trichloroethane mg/L ND 0.0020 10/12/22 12:41
1,1,2,2-Tetrachloroethane mg/L ND 0.0020 10/12/22 12:41
1,1,2-Trichloroethane mg/L ND 0.0020 10/12/22 12:41
1,1-Dichloroethane mg/L ND 0.0020 10/12/22 12:41
1,1-Dichloroethene mg/L ND 0.0020 10/12/22 12:41
1,2-Dichloroethane mg/L ND 0.0020 10/12/22 12:41
1,2-Dichloropropane mg/L ND 0.0020 10/12/22 12:41
2-Chloroethylvinyl ether mg/L ND 0.0050 10/12/22 12:41
Acrolein mg/L ND 0.0050 10/12/22 12:41
Acrylonitrile mg/L ND 0.0050 10/12/22 12:41
Benzene mg/L ND 0.0010 10/12/22 12:41
Bromodichloromethane mg/L ND 0.0020 10/12/22 12:41
Bromoform mg/L ND 0.0020 10/12/22 12:41
Bromomethane mg/L ND 0.0020 10/12/22 12:41
Carbon tetrachloride mg/L ND 0.0020 10/12/22 12:41
Chlorobenzene mg/L ND 0.0020 10/12/22 12:41
Chloroethane mg/L ND 0.0020 10/12/22 12:41
Chloroform mg/L ND 0.0020 10/12/22 12:41
Chloromethane mg/L ND 0.0020 10/12/22 12:41
cis-1,3-Dichloropropene mg/L ND 0.0020 10/12/22 12:41
Dibromochloromethane mg/L ND 0.0020 10/12/22 12:41
Ethylbenzene mg/L ND 0.0010 10/12/22 12:41
m&p-Xylene ug/L ND 5.0 10/12/22 12:41
Methylene Chloride mg/L 0.0054 0.0020 10/12/22 12:41
Naphthalene mg/L ND 0.0050 10/12/22 12:41
o-Xylene ug/L ND 5.0 10/12/22 12:41
Tetrachloroethene mg/L ND 0.0020 10/12/22 12:41
Toluene mg/L ND 0.0010 10/12/22 12:41
trans-1,2-Dichloroethene mg/L ND 0.0020 10/12/22 12:41
trans-1,3-Dichloropropene mg/L ND 0.0020 10/12/22 12:41
Trichloroethene mg/L ND 0.0020 10/12/22 12:41
Vinyl chloride mg/L ND 0.0020 10/12/22 12:41
Xylene (Total)ug/L ND 3.0 10/12/22 12:41
1,2-Dichloroethane-d4 (S)%91 70-130 10/12/22 12:41
4-Bromofluorobenzene (S)%105 70-130 10/12/22 12:41
Toluene-d8 (S)%107 70-130 10/12/22 12:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799950LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane mg/L 0.0200.02 98 70-130
1,1,2,2-Tetrachloroethane mg/L 0.0180.02 91 70-130
1,1,2-Trichloroethane mg/L 0.0200.02 102 70-130
1,1-Dichloroethane mg/L 0.0190.02 97 70-130
1,1-Dichloroethene mg/L 0.0190.02 97 70-130
1,2-Dichloroethane mg/L 0.0200.02 98 70-130
1,2-Dichloropropane mg/L 0.0210.02 103 70-130
2-Chloroethylvinyl ether mg/L 0.0420.04 105 63-130
Acrolein mg/L 0.0750.1 75 60-140
Acrylonitrile mg/L 0.0970.1 97 70-130
Benzene mg/L 0.0190.02 95 70-130
Bromodichloromethane mg/L 0.0200.02 100 70-130
Bromoform mg/L 0.0170.02 87 70-130
Bromomethane mg/L 0.0190.02 97 45-151
Carbon tetrachloride mg/L 0.0190.02 97 70-130
Chlorobenzene mg/L 0.0190.02 94 70-130
Chloroethane mg/L 0.0210.02 106 40-152
Chloroform mg/L 0.0190.02 97 70-130
Chloromethane mg/L 0.0220.02 110 58-130
cis-1,3-Dichloropropene mg/L 0.0200.02 100 70-130
Dibromochloromethane mg/L 0.0180.02 91 70-130
Ethylbenzene mg/L 0.0190.02 95 70-130
Methylene Chloride mg/L 0.057 L10.02 284 66-130
Naphthalene mg/L 0.0200.02 102 70-130
Tetrachloroethene mg/L 0.0180.02 91 70-130
Toluene mg/L 0.0200.02 98 70-130
trans-1,2-Dichloroethene mg/L 0.0200.02 100 70-130
trans-1,3-Dichloropropene mg/L 0.0200.02 100 70-130
Trichloroethene mg/L 0.0210.02 103 70-130
Vinyl chloride mg/L 0.0210.02 106 62-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630306001
3799952
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1-Trichloroethane mg/L 0.02 109 70-150108 10.02ND 0.022 0.022
1,1,2,2-Tetrachloroethane mg/L 0.02 110 69-142108 20.02ND 0.022 0.022
1,1,2-Trichloroethane mg/L 0.02 115 70-138112 20.02ND 0.023 0.022
1,1-Dichloroethane mg/L 0.02 109 70-150107 20.02ND 0.022 0.021
1,1-Dichloroethene mg/L 0.02 113 70-156110 20.02ND 0.023 0.022
1,2-Dichloroethane mg/L 0.02 109 69-143106 30.02ND 0.022 0.021
1,2-Dichloropropane mg/L 0.02 114 70-156114 00.02ND 0.023 0.023
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630306001
3799952
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Chloroethylvinyl ether mg/L 0.04 126 10-200123 20.04ND 0.050 0.049
Acrolein mg/L P50.1 1 40-16000.1ND ND ND
Acrylonitrile mg/L 0.1 115 69-147111 40.1ND 0.12 0.11
Benzene mg/L 0.02 107 70-142106 10.02ND 0.021 0.021
Bromodichloromethane mg/L 0.02 111 70-139109 20.02ND 0.022 0.022
Bromoform mg/L 0.02 110 64-140108 20.02ND 0.022 0.022
Bromomethane mg/L 0.02 89 28-19290 10.02ND 0.018 0.018
Carbon tetrachloride mg/L 0.02 108 70-140108 00.02ND 0.022 0.022
Chlorobenzene mg/L 0.02 115 70-141112 20.02ND 0.023 0.022
Chloroethane mg/L 0.02 110 58-191107 20.02ND 0.022 0.021
Chloroform mg/L 0.02 107 70-138104 30.02ND 0.021 0.021
Chloromethane mg/L 0.02 115 43-162115 00.02ND 0.023 0.023
cis-1,3-Dichloropropene mg/L 0.02 108 68-151108 10.02ND 0.022 0.022
Dibromochloromethane mg/L 0.02 113 70-144112 10.02ND 0.023 0.022
Ethylbenzene mg/L 0.02 114 70-143110 40.02ND 0.023 0.022
Methylene Chloride mg/L 0.02 102 70-144100 20.02ND 0.020 0.020
Naphthalene mg/L 0.02 133 62-149114 150.02ND 0.027 0.023
Tetrachloroethene mg/L 0.02 110 70-143109 10.02ND 0.022 0.022
Toluene mg/L 0.02 105 69-144105 00.02ND 0.021 0.021
trans-1,2-Dichloroethene mg/L 0.02 112 70-151110 20.02ND 0.022 0.022
trans-1,3-Dichloropropene mg/L 0.02 110 70-139108 10.02ND 0.022 0.022
Trichloroethene mg/L 0.02 116 70-142115 10.02ND 0.023 0.023
Vinyl chloride mg/L 0.02 116 61-162116 00.02ND 0.023 0.023
1,2-Dichloroethane-d4 (S)%95 70-13094
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%96 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729632
EPA 608.3
EPA 608.3
608 PCB Pest Red Vol
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799262
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
4,4'-DDD mg/L ND 0.000050 10/13/22 21:03
4,4'-DDE mg/L ND 0.000050 10/13/22 21:03
4,4'-DDT mg/L ND 0.000050 10/13/22 21:03
Aldrin mg/L ND 0.000050 10/13/22 21:03
alpha-BHC mg/L ND 0.000050 10/13/22 21:03
alpha-Chlordane mg/L ND 0.000050 10/13/22 21:03
beta-BHC mg/L ND 0.000050 10/13/22 21:03
Chlordane (Technical)mg/L ND 0.00050 10/13/22 21:03
delta-BHC mg/L ND 0.000050 10/13/22 21:03
Dieldrin mg/L ND 0.000050 10/13/22 21:03
Endosulfan I mg/L ND 0.000050 10/13/22 21:03
Endosulfan II mg/L ND 0.000050 10/13/22 21:03
Endosulfan sulfate mg/L ND 0.000050 10/13/22 21:03
Endrin mg/L ND 0.000050 10/13/22 21:03
Endrin aldehyde mg/L ND 0.000050 10/13/22 21:03
gamma-BHC (Lindane)mg/L ND 0.000050 10/13/22 21:03
gamma-Chlordane mg/L ND 0.000050 10/13/22 21:03
Heptachlor mg/L ND 0.000050 10/13/22 21:03
Heptachlor epoxide mg/L ND 0.000050 10/13/22 21:03
PCB-1016 (Aroclor 1016)mg/L ND 0.00050 10/13/22 21:03
PCB-1221 (Aroclor 1221)mg/L ND 0.00050 10/13/22 21:03
PCB-1232 (Aroclor 1232)mg/L ND 0.00050 10/13/22 21:03
PCB-1242 (Aroclor 1242)mg/L ND 0.00050 10/13/22 21:03
PCB-1248 (Aroclor 1248)mg/L ND 0.00050 10/13/22 21:03
PCB-1254 (Aroclor 1254)mg/L ND 0.00050 10/13/22 21:03
PCB-1260 (Aroclor 1260)mg/L ND 0.00050 10/13/22 21:03
Toxaphene mg/L ND 0.00050 10/13/22 21:03
Decachlorobiphenyl (S)%117 10-184 10/13/22 21:03
Tetrachloro-m-xylene (S)%55 10-154 10/13/22 21:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799263LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD mg/L 0.000260.00025 103 50-141
4,4'-DDE mg/L 0.000230.00025 91 43-145
4,4'-DDT mg/L 0.000270.00025 108 25-160
Aldrin mg/L 0.000190.00025 74 42-137
alpha-BHC mg/L 0.000230.00025 93 37-140
alpha-Chlordane mg/L 0.000260.00025 104 45-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799263LABORATORY CONTROL SAMPLE:
LCSSpike
beta-BHC mg/L 0.000270.00025 109 54-147
delta-BHC mg/L 0.000270.00025 110 42-140
Dieldrin mg/L 0.000230.00025 91 42-146
Endosulfan I mg/L 0.000260.00025 104 45-153
Endosulfan II mg/L 0.000270.00025 107 45-176
Endosulfan sulfate mg/L 0.000300.00025 119 48-144
Endrin mg/L 0.000260.00025 103 46-147
Endrin aldehyde mg/L 0.000210.00025 86 35-168
gamma-BHC (Lindane)mg/L 0.000250.00025 102 38-140
gamma-Chlordane mg/L 0.000250.00025 102 45-140
Heptachlor mg/L 0.000230.00025 90 34-140
Heptachlor epoxide mg/L 0.000250.00025 102 43-142
Decachlorobiphenyl (S)%123 10-184
Tetrachloro-m-xylene (S)%56 10-154
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799264LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)mg/L 0.00400.005 81 50-140
PCB-1260 (Aroclor 1260)mg/L 0.00430.005 86 42-140
Decachlorobiphenyl (S)%114 10-184
Tetrachloro-m-xylene (S)%43 10-154
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799265MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629593001
3799266
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4,4'-DDD mg/L 0.00042 60 31-14154 120.00042<0.000014 0.00025 0.00022
4,4'-DDE mg/L 0.00042 59 30-14553 100.00042<0.0000
20 0.00024 0.00022
4,4'-DDT mg/L 0.00042 93 25-16086 90.00042<0.0000
22 0.00039 0.00036
Aldrin mg/L 0.00042 97 42-14082 170.00042<0.0000
12 0.00041 0.00034
alpha-BHC mg/L 0.00042 74 37-14072 30.00042<0.0000
10 0.00031 0.00030
alpha-Chlordane mg/L 0.00042 76 45-14069 100.00042<0.000011 0.00032 0.00029
beta-BHC mg/L 0.00042 93 17-14789 40.00042<0.0000
41 0.00039 0.00037
delta-BHC mg/L 0.00042 74 19-14070 70.00042<0.0000
12 0.00031 0.00029
Dieldrin mg/L 0.00042 81 36-14668 190.00042<0.0000
12 0.00034 0.00028
Endosulfan I mg/L M10.00042 321 45-153280 140.00042<0.0000
14 0.0013 0.0012
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799265MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629593001
3799266
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Endosulfan II mg/L 0.00042 150 10-202142 60.00042<0.0000
13 0.00063 0.00059
Endosulfan sulfate mg/L 0.00042 104 26-14495 90.00042<0.0000
12 0.00043 0.00040
Endrin mg/L 0.00042 67 30-14761 90.00042<0.0000
15 0.00028 0.00025
Endrin aldehyde mg/L 0.00042 62 10-19860 40.00042<0.0000
14
0.00026 0.00025
gamma-BHC (Lindane)mg/L 0.00042 73 32-14070 40.00042<0.0000
10 0.00031 0.00029
gamma-Chlordane mg/L 0.00042 83 45-14077 80.00042<0.0000
19 0.00035 0.00032
Heptachlor mg/L 0.00042 74 34-14068 80.00042<0.0000
16 0.00031 0.00028
Heptachlor epoxide mg/L 0.00042 70 37-14264 80.00042<0.0000
24 0.00029 0.00027
Decachlorobiphenyl (S)%99 10-18476
Tetrachloro-m-xylene (S)%44 10-15433
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799267MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630529001
3799268
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)mg/L 0.0083 52 50-14072 320.0083ND 0.0044 0.0060
PCB-1260 (Aroclor 1260)mg/L 0.0083 70 42-14076 80.0083ND 0.0058 0.0063
Decachlorobiphenyl (S)%91 10-184101
Tetrachloro-m-xylene (S)%21 10-15444
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729455
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3798630
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene mg/L ND 0.0050 10/12/22 10:45
1,2-Dichlorobenzene mg/L ND 0.0050 10/12/22 10:45
1,2-Diphenylhydrazine mg/L ND 0.0050 10/12/22 10:45
1,3-Dichlorobenzene mg/L ND 0.0050 10/12/22 10:45
1,4-Dichlorobenzene mg/L ND 0.0050 10/12/22 10:45
2,2'-Oxybis(1-chloropropane)mg/L ND 0.0050 10/12/22 10:45
2,4,6-Trichlorophenol mg/L ND 0.010 10/12/22 10:45
2,4-Dichlorophenol mg/L ND 0.0050 10/12/22 10:45
2,4-Dimethylphenol mg/L ND 0.010 10/12/22 10:45
2,4-Dinitrophenol mg/L ND 0.050 10/12/22 10:45
2,4-Dinitrotoluene mg/L ND 0.0050 10/12/22 10:45
2,6-Dinitrotoluene mg/L ND 0.0050 10/12/22 10:45
2-Chloronaphthalene mg/L ND 0.0050 10/12/22 10:45
2-Chlorophenol mg/L ND 0.0050 10/12/22 10:45
2-Nitrophenol mg/L ND 0.0050 10/12/22 10:45
3,3'-Dichlorobenzidine mg/L ND 0.010 10/12/22 10:45
4,6-Dinitro-2-methylphenol mg/L ND 0.010 10/12/22 10:45
4-Bromophenylphenyl ether mg/L ND 0.0050 10/12/22 10:45
4-Chloro-3-methylphenol mg/L ND 0.0050 10/12/22 10:45
4-Chlorophenylphenyl ether mg/L ND 0.0050 10/12/22 10:45
4-Nitrophenol mg/L ND 0.010 10/12/22 10:45
Acenaphthene mg/L ND 0.0050 10/12/22 10:45
Acenaphthylene mg/L ND 0.0050 10/12/22 10:45
Anthracene mg/L ND 0.0050 10/12/22 10:45
Benzo(a)anthracene mg/L ND 0.0050 10/12/22 10:45
Benzo(a)pyrene mg/L ND 0.0050 10/12/22 10:45
Benzo(b)fluoranthene mg/L ND 0.0050 10/12/22 10:45
Benzo(g,h,i)perylene mg/L ND 0.0050 10/12/22 10:45
Benzo(k)fluoranthene mg/L ND 0.0050 10/12/22 10:45
bis(2-Chloroethoxy)methane mg/L ND 0.010 10/12/22 10:45
bis(2-Chloroethyl) ether mg/L ND 0.0050 10/12/22 10:45
bis(2-Ethylhexyl)phthalate mg/L ND 0.0050 10/12/22 10:45
Butylbenzylphthalate mg/L ND 0.0050 10/12/22 10:45
Chrysene mg/L ND 0.0050 10/12/22 10:45
Di-n-butylphthalate mg/L ND 0.0050 10/12/22 10:45
Di-n-octylphthalate mg/L ND 0.0050 10/12/22 10:45
Dibenz(a,h)anthracene mg/L ND 0.0050 10/12/22 10:45
Diethylphthalate mg/L ND 0.0050 10/12/22 10:45
Dimethylphthalate mg/L ND 0.0050 10/12/22 10:45
Fluoranthene mg/L ND 0.0050 10/12/22 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3798630
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Fluorene mg/L ND 0.0050 10/12/22 10:45
Hexachloro-1,3-butadiene mg/L ND 0.0050 10/12/22 10:45
Hexachlorobenzene mg/L ND 0.0050 10/12/22 10:45
Hexachlorocyclopentadiene mg/L ND 0.010 10/12/22 10:45
Hexachloroethane mg/L ND 0.0050 10/12/22 10:45
Indeno(1,2,3-cd)pyrene mg/L ND 0.0050 10/12/22 10:45
Isophorone mg/L ND 0.010 10/12/22 10:45
N-Nitroso-di-n-propylamine mg/L ND 0.0050 10/12/22 10:45
N-Nitrosodimethylamine mg/L ND 0.0050 10/12/22 10:45
N-Nitrosodiphenylamine mg/L ND 0.010 10/12/22 10:45
Naphthalene mg/L ND 0.0050 10/12/22 10:45
Nitrobenzene mg/L ND 0.0050 10/12/22 10:45
Pentachlorophenol mg/L ND 0.010 10/12/22 10:45
Phenanthrene mg/L ND 0.0050 10/12/22 10:45
Phenol mg/L ND 0.0050 10/12/22 10:45
Pyrene mg/L ND 0.0050 10/12/22 10:45
2,4,6-Tribromophenol (S)%136 10-137 10/12/22 10:45
2-Fluorobiphenyl (S)%90 15-120 10/12/22 10:45
2-Fluorophenol (S)%88 10-120 10/12/22 10:45
Nitrobenzene-d5 (S)%114 10-120 10/12/22 10:45
Phenol-d6 (S)%69 10-120 10/12/22 10:45
Terphenyl-d14 (S)%135 11-131 S310/12/22 10:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3798631LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/L 0.0340.05 67 44-142
1,2-Dichlorobenzene mg/L 0.0220.05 45 32-129
1,2-Diphenylhydrazine mg/L 0.0640.05 128 25-150
1,3-Dichlorobenzene mg/L 0.0190.05 37 1-172
1,4-Dichlorobenzene mg/L 0.0210.05 41 20-124
2,2'-Oxybis(1-chloropropane)mg/L 0.0450.05 89 36-166
2,4,6-Trichlorophenol mg/L 0.0570.05 114 37-144
2,4-Dichlorophenol mg/L 0.0520.05 105 1-191
2,4-Dimethylphenol mg/L 0.072 L10.05 144 32-119
2,4-Dinitrophenol mg/L 0.370.25 150 1-181
2,4-Dinitrotoluene mg/L 0.0670.05 134 39-139
2,6-Dinitrotoluene mg/L 0.0630.05 127 50-158
2-Chloronaphthalene mg/L 0.0520.05 104 60-118
2-Chlorophenol mg/L 0.0480.05 97 23-134
2-Nitrophenol mg/L 0.0580.05 115 29-182
3,3'-Dichlorobenzidine mg/L 0.120.1 124 1-262
4,6-Dinitro-2-methylphenol mg/L 0.160.1 155 1-181
4-Bromophenylphenyl ether mg/L 0.0550.05 111 53-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3798631LABORATORY CONTROL SAMPLE:
LCSSpike
4-Chloro-3-methylphenol mg/L 0.110.1 110 22-147
4-Chlorophenylphenyl ether mg/L 0.0520.05 104 25-158
4-Nitrophenol mg/L 0.190.25 76 1-132
Acenaphthene mg/L 0.0530.05 106 47-145
Acenaphthylene mg/L 0.0530.05 106 33-145
Anthracene mg/L 0.0560.05 112 1-166
Benzo(a)anthracene mg/L 0.0600.05 120 33-143
Benzo(a)pyrene mg/L 0.0580.05 115 17-163
Benzo(b)fluoranthene mg/L 0.0590.05 117 24-159
Benzo(g,h,i)perylene mg/L 0.0640.05 128 1-219
Benzo(k)fluoranthene mg/L 0.0560.05 112 11-162
bis(2-Chloroethoxy)methane mg/L 0.0500.05 101 33-184
bis(2-Chloroethyl) ether mg/L 0.0480.05 96 12-158
bis(2-Ethylhexyl)phthalate mg/L 0.0700.05 141 8-158
Butylbenzylphthalate mg/L 0.0700.05 139 1-152
Chrysene mg/L 0.0590.05 118 17-168
Di-n-butylphthalate mg/L 0.070 L10.05 140 1-118
Di-n-octylphthalate mg/L 0.078 L10.05 156 4-146
Dibenz(a,h)anthracene mg/L 0.0630.05 127 1-227
Diethylphthalate mg/L 0.060 L10.05 121 1-114
Dimethylphthalate mg/L 0.059 L10.05 119 1-112
Fluoranthene mg/L 0.0650.05 131 26-137
Fluorene mg/L 0.0560.05 111 59-121
Hexachloro-1,3-butadiene mg/L 0.0260.05 52 24-116
Hexachlorobenzene mg/L 0.0560.05 112 1-152
Hexachlorocyclopentadiene mg/L 0.0410.05 83 25-150
Hexachloroethane mg/L 0.017 L20.05 35 40-113
Indeno(1,2,3-cd)pyrene mg/L 0.0640.05 128 1-171
Isophorone mg/L 0.0540.05 109 21-196
N-Nitroso-di-n-propylamine mg/L 0.0570.05 114 1-230
N-Nitrosodimethylamine mg/L 0.0500.05 100 25-150
N-Nitrosodiphenylamine mg/L 0.0590.05 118 25-150
Naphthalene mg/L 0.0390.05 78 21-133
Nitrobenzene mg/L 0.0530.05 107 35-180
Pentachlorophenol mg/L 0.130.1 128 14-176
Phenanthrene mg/L 0.060 L10.05 121 54-120
Phenol mg/L 0.0370.05 73 5-112
Pyrene mg/L 0.0530.05 106 52-115
2,4,6-Tribromophenol (S)%S0143 10-137
2-Fluorobiphenyl (S)%95 15-120
2-Fluorophenol (S)%90 10-120
Nitrobenzene-d5 (S)%113 10-120
Phenol-d6 (S)%74 10-120
Terphenyl-d14 (S)%126 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3798632MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35751307003
3798633
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/L 0.05 47 44-142450.058.6U
ug/L .024J .022J
1,2-Dichlorobenzene mg/L M10.05 32 32-129300.059.0U
ug/L .016J .015J
1,2-Diphenylhydrazine mg/L 0.05 90 25-15088 20.058.0U
ug/L 0.045 0.044
1,3-Dichlorobenzene mg/L 0.05 27 1-172250.058.0U
ug/L
.014J .012J
1,4-Dichlorobenzene mg/L 0.05 29 20-124280.058.4U
ug/L .015J .014J
2,2'-Oxybis(1-chloropropane) mg/L 0.05 51 36-166490.055.8U
ug/L 0.026 ND
2,4,6-Trichlorophenol mg/L 0.05 75 37-144700.057.8U
ug/L .038J .035J
2,4-Dichlorophenol mg/L 0.05 59 1-19159 10.057.0U
ug/L 0.029 0.030
2,4-Dimethylphenol mg/L 0.05 85 32-119880.058.5Uug/L .043J .044J
2,4-Dinitrophenol mg/L 0.25 15 1-181100.25130U
ug/L ND ND
2,4-Dinitrotoluene mg/L 0.05 92 39-13988 50.058.1U
ug/L 0.046 0.044
2,6-Dinitrotoluene mg/L 0.05 86 50-15882 50.058.6U
ug/L 0.043 0.041
2-Chloronaphthalene mg/L 0.05 67 60-11862 80.058.6U
ug/L 0.034 0.031
2-Chlorophenol mg/L 0.05 56 23-134500.056.0Uug/L 0.028 ND
2-Nitrophenol mg/L 0.05 61 29-18258 50.057.0U
ug/L 0.030 0.029
3,3'-Dichlorobenzidine mg/L 0.1 64 1-26261 40.140.6U
ug/L 0.064 0.061
4,6-Dinitro-2-methylphenol mg/L 0.1 49 1-181440.138.9U
ug/L .049J .044J
4-Bromophenylphenyl ether mg/L 0.05 79 53-12776 40.058.8U
ug/L 0.040 0.038
4-Chloro-3-methylphenol mg/L 0.1 80 22-14776 50.116.7Uug/L 0.080 0.076
4-Chlorophenylphenyl ether mg/L 0.05 77 25-15877 10.0510.0U
ug/L 0.038 0.039
4-Nitrophenol mg/L 0.25 46 1-13241 120.2533.0U
ug/L 0.12 0.10
Acenaphthene mg/L 0.05 73 47-14573 00.0510.0U
ug/L 0.037 0.037
Acenaphthylene mg/L 0.05 69 33-14569 10.059.8U
ug/L 0.034 0.035
Anthracene mg/L 0.05 81 1-16680 10.0511.6Uug/L 0.040 0.040
Benzo(a)anthracene mg/L 0.05 92 33-14386 70.0513.4U
ug/L 0.046 0.043
Benzo(a)pyrene mg/L 0.05 83 17-16379 50.0513.9U
ug/L 0.041 0.039
Benzo(b)fluoranthene mg/L 0.05 85 24-15979 70.0513.0U
ug/L 0.043 0.039
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3798632MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35751307003
3798633
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzo(g,h,i)perylene mg/L 0.05 100 1-219100 00.0514.2U
ug/L 0.050 0.050
Benzo(k)fluoranthene mg/L 0.05 80 11-16280 00.0513.6U
ug/L 0.040 0.040
bis(2-Chloroethoxy)methane mg/L 0.05 53 33-184530.059.1U
ug/L .027J .027J
bis(2-Chloroethyl) ether mg/L 0.05 50 12-158490.059.6U
ug/L
ND ND
bis(2-Ethylhexyl)phthalate mg/L 0.05 112 8-158104 70.0518.6U
ug/L 0.056 0.052
Butylbenzylphthalate mg/L 0.05 111 1-152105 60.0515.7U
ug/L 0.055 0.052
Chrysene mg/L 0.05 93 17-16886 70.0513.8U
ug/L 0.047 0.043
Di-n-butylphthalate mg/L 0.05 107 1-118104 30.0511.0U
ug/L 0.053 0.052
Di-n-octylphthalate mg/L 0.05 112 4-146104 70.0519.6Uug/L 0.056 0.052
Dibenz(a,h)anthracene mg/L 0.05 94 1-22788 70.0514.8U
ug/L 0.047 0.044
Diethylphthalate mg/L 0.05 100 1-11496 50.0510.2U
ug/L 0.050 0.048
Dimethylphthalate mg/L 0.05 82 1-11280 30.0510.6U
ug/L 0.041 0.040
Fluoranthene mg/L 0.05 94 26-13795 10.0511.0U
ug/L 0.047 0.047
Fluorene mg/L 0.05 83 59-12179 50.0510.4Uug/L 0.042 0.039
Hexachloro-1,3-butadiene mg/L 0.05 38 24-116380.058.8U
ug/L .019J .019J
Hexachlorobenzene mg/L 0.05 84 1-15285 10.0510.8U
ug/L 0.042 0.042
Hexachlorocyclopentadiene mg/L 0.05 44 25-150350.058.0U
ug/L .022J .018J
Hexachloroethane mg/L M00.05 26 40-113240.056.9U
ug/L .013J .012J
Indeno(1,2,3-cd)pyrene mg/L 0.05 94 1-17193 20.0514.4Uug/L 0.047 0.046
Isophorone mg/L 0.05 58 21-196580.058.3U
ug/L .029J .029J
N-Nitroso-di-n-propylamine mg/L 0.05 60 1-23058 40.056.6U
ug/L 0.030 0.029
N-Nitrosodimethylamine mg/L 0.05 49 25-150490.059.4U
ug/L ND .024J
N-Nitrosodiphenylamine mg/L 0.05 82 25-150830.0515.0U
ug/L .041J .041J
Naphthalene mg/L 0.05 51 21-13351 00.0510.4Uug/L 0.026 0.026
Nitrobenzene mg/L 0.05 59 35-18062 50.059.4U
ug/L 0.030 0.031
Pentachlorophenol mg/L 0.1 79 14-17677 20.118.8U
ug/L 0.079 0.077
Phenanthrene mg/L 0.05 88 54-12086 20.0510.0U
ug/L 0.044 0.043
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3798632MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35751307003
3798633
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol mg/L 0.05 49 5-112460.056.8U
ug/L ND .023J
Pyrene mg/L 0.05 88 52-11579 100.0511.0U
ug/L 0.044 0.039
2,4,6-Tribromophenol (S)%90 10-13792
2-Fluorobiphenyl (S)%59 15-12058
2-Fluorophenol (S)%43 10-12040
Nitrobenzene-d5 (S)%D36110-12059
Phenol-d6 (S)%38 10-12037
Terphenyl-d14 (S)%95 11-13188
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729578
EPA 3511
EPA 8015C
8015 Diesel Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799069
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Diesel Range Organics(C10-C28)mg/L ND 0.50 10/12/22 21:44
n-Pentacosane (S)%103 41-183 10/12/22 21:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799070LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/L 9.310 93 70-130
n-Pentacosane (S)%104 41-183
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799071MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630143001
3799072
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Diesel Range Organics(C10-
C28)mg/L 10 95 30-14495 0100.23J 9.7 9.8
n-Pentacosane (S)%107 41-183108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729579
EPA 3511
EPA 8015C
8015 Oil Range Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799073
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Oil Range Organics (C28-C40)mg/L ND 2.0 10/12/22 21:44
n-Pentacosane (S)%70 41-183 10/12/22 21:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799074LABORATORY CONTROL SAMPLE:
LCSSpike
Oil Range Organics (C28-C40)mg/L 11.112.5 89 69-144
n-Pentacosane (S)%96 41-183
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3799075MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92630529001
3799076
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Oil Range Organics (C28-C40) mg/L 25 88 10-18590 225ND22.3 22.8
n-Pentacosane (S)%94 41-18396
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729520
SM 4500-CN-E-2011
SM 4500-CN-E-2011
4500CNE Cyanide, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92630529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3798918
Associated Lab Samples:92630529001
Matrix: Water
Analyzed
Cyanide mg/L ND 0.0080 10/12/22 19:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3798919LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.100.1 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3798920MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92628907002
3798921
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cyanide mg/L M1,R10.1 52 80-12060 130.1ND 0.057 0.065
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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9800 Kincey Ave. Suite 100
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Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92630529
7-Eleven 6958 Burlington
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92630529001 729632 729885EFFLUENTEPA 608.3 EPA 608.3
92630529001 729578 729756EFFLUENTEPA 3511 EPA 8015C
92630529001 729579 729757EFFLUENTEPA 3511 EPA 8015C
92630529001 729734EFFLUENTEPA 5030B/8015C
92630529001 729971 730057EFFLUENTEPA 200.7 EPA 200.7
92630529001 729698 729940EFFLUENTEPA 245.1 EPA 245.1
92630529001 730072 730140EFFLUENTEPA 3010A EPA 6010D
92630529001 729455 729630EFFLUENTEPA 625.1 EPA 625.1
92630529001 729751EFFLUENTEPA 624.1
92630529001 729520 729837EFFLUENTSM 4500-CN-E-2011 SM 4500-CN-E-2011
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/20/2022 08:59 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32

AECOM
Appendix D – DPE System Drawings and Wastewater Permit
SCALE IN FEET:3030060686627DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:NOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.C:\Confidential\AECOM\7-Eleven\Sites Folders\North Carolina\6958 Burlington\6958 Burlington.dwg, 9/15/2022 5:55 PM, Dumitru, Ionut, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUSEPTEMBER 2022M. LINKSpeedway LLC. FIGURE 4Speedway Store #6958 653 East Webb Avenue Burlington, North CarolinaPIPING AND TRENCHINGLAYOUT MAP

AECOM
Appendix E – System O&M Tracking and Inspection Form

Operation and Maintenance Table LogSpeedway Store No. 6958653 East Webb Avenue, Burlington, NC 27217Incident Number: 19272 Facility Number: 0-004038
Planned O&M Visits:Mid-March Late March Early April Other 1 Late April Early May Late May Other 2 Early June 3 Other 4 Late June Other 5 Early July Other 6 Late July Early August Late August Other 7 Early SeptemberDate:3/17/2022 3/24/2022 4/13/2022 4/14/2022 4/26/2022 5/10/2022 5/27/2022 5/31/2022 6/2/2022 6/3/2022 6/13/2022 6/16/2022 7/5/2022 7/13/2022 7/18/2022 8/2/2022 8/15/2022 8/31/2022 9/14/2022Arrival Time:13:14 6:30 13:23 5:55 12:02 11:03 6:20 13:16 12:27 10:08 9:16 9:26 12:45 12;30 10:00 8:30 9:00 7:15 7:40Technician:Young Fischer Moore Fischer Fischer Fischer Fischer Fischer Fischer Young Fischer Young Maciejewski Maciejewski Maciejewski Maciejewski Maciejewski Maciejewski MaciejewskiDeparture Time:16:15 15:30 12:40 12:15 12:00 8:40 9:30Read MetersRun Time, Total (Hours)28409.7 28571.5 29057.3 29073.9 29368.4 297027 30104.4 30207.4 302412 30244.8 30484 30556 31016 31016 31137.8 31445.7 31676.1 32058 32394.9Time Flow Meter Read 5:14:33 PM 11:28:40 AM 5:23:12 PM 9:58:06 AM 4:15:12 PM 3:04:47 6:20 AM 1:16 PM 12:27 PM 10:13 AM 9:16 AM 9:30 AM 3:00 PM 12:24 PM 10:30 AM 9:25 AM 7:40 8:11
DPE Flow Rate (FPM)--4410 --4128 --5345Inlet Filter Status Good? (Yes/No)Yes Yes Yes Yes Yes Yes Yes --------
Lube (Yes/No)Yes No No No No No No No No No No
Valves Closed? (Yes/No)Yes No --No No ------------Temperature (°F)140 195 180 175 195 170 185 200 165 180 185 185 200 185 --200Blower Vacuum Pressure (in Hg)24 17 12 13 11 13 13 13 9 10.5 9 11 11 11 12 14
Makeup Air Valve Status? (Open/Closed)Closed 25% Open 25% Open 25% Open 25% Open 25% Open 40% Closed 40% Closed 50% closed 60% closed 60% closed 60% closed 80% closed
Oil Level Good? (Yes/No)Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes YesOil Changed? (Yes/No)No No No No Yes No No No No No No
VaporVapor Flow Rate (FPM)5800 6000 --4410 --4128 --5345Odor(None/Faint/Moderate/Strong)Moderate Moderate --Moderate Moderate Moderate Moderate Moderate
Air Sample Collected? (Yes/No)No Yes Yes No Yes No Yes No Yes No Yes No Yes
Water Fluid
Appearance (Clear/Murky/Other)Murky Murky Murky Murky Murky Good Good Good Good --Good
High Level Cutoff Working? (Yes/No)Yes --No/Tested --Tested ------
High Level Switches Tested and Cleaned? (Yes/No)Yes --Diagnosed Yes/Operating Yes/Replaced OWS ------
Water Sample Collected? (Yes/No)No Yes Yes No No No Yes No No No No No No
Bag Filter Status? (Good/Replaced)Replaced Good Replaced Good Replaced Replaced Good Replaced Good Replaced Good
AST Product Level None None None None None None None None None None None
pH ------------High Level Cutoff Working? (Yes/No)Yes --No/Tested Yes --Tested ------
General System ObservationsCondition of Remediation System Trenches Good Good --Good --Good --Good
Pavement Condition Good Good --Good --Good --GoodHigh Level Cut Off Working? (Yes/No)Yes --No/Tested --Tested ------
Condition of Remediation System Vaults --Good --Good --Good
Telemetry System Tested, Operating Normally? (Yes/No)Tested/Diagnosed Yes --Yes Yes Yes
System DataDPE-1 Vacuum (in Hg)8 9.5 10 10 10 13
DPE-3 Vacuum (in Hg)7 9 9 9 9.5 11.5DPE-4 Vacuum (in Hg)4 6.5 7 7 7.5 8.5
KO Tank Vacuum (in Hg)16 12 11 10 13 9 13 13 12.5 8.5 11 8 10 10 10 11.5 13Blower Vacuum (in Hg)17 13 10 13 10 13 13 13 9 9 11 11 11 12 14OWS Pump Pressure (PSI)8 30 32 35 25 20 22 42 42 42 42 42 42 42
AS Pump Pressure (PSI)70 78 78 --30 22 28 0 Broken Gauge Broken Gauge Needs Replacing Broken Gauge Broken Gauge --AS Blower Pressure (PSIG)--20 0.35 0.4 0.4 --0.4 0.4 0.4
GAC #1 Pressure (PSI)30 28 30 30 28 28 26 22 18 18 18 18 20 22GAC #2 Pressure (PSI)28 20 29 28 27 28 28 18 10 8 8 9 8 8Blue Filter Pressure (PSI)18 18 18 18 20 22
GPM 1.8 1.8 1.7 1.7 1 ------7.2 --6.5Water Meter Reading (cf)1423171 1438152 1455878 145617 146585 147468 1484236 148825.7 1489383 1489726 1491569 1491881 1492282 1492662 1496439 1503074 1508169 1522223 1543774
Air Flow Rate (FPM)5800 6000 6000 --4410 --4128 5345Air Flow Rate (acfm)126.54 130.90 130.90 96.21 90.06 116.61
Air Flow Rate (scfm) 8 70 72 90 60 56 60
DPE-1DPE-2DPE-3DPE-4DPE-5DPE-6Notes:8scfm is calculated at the website below using the acfm reading, blower vacuum, 62 degree F, and 633 feet of altitude.https://www.falmouthproducts.com/catoxflowconversion.html
4 Floor Sump Alarm. Issue resolved.5 Mid-Atlantic reviewed system with AECOM.6 System repairs and restart.7 System Maintenance
The system is scheduled to operate mid-March through mid-September per the PATA.1 Bag Filter Replacement2 Modem Reset3 System was down due to water getting on the floor. Water was drained and system was restarted.
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