WS-5268_18105_CA_MRP_20230307

GROUNDWATER MONITORING REPORT

DODSON AMOCO
306 WEST CENTER STREET
MEBANE, ALAMANCE COUNTY, NORTH CAROLINA

PREPARED FOR:
MR. MICHAEL TOMPKINS
MCLEOD OIL COMPANY, INC.
PO BOX 100
MEBANE, NORTH CAROLINA 27302

PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285

MARCH 7, 2023
PILOT PROJECT G-8098.1

SITE INFORMATION

Site Name and Location Dodson Amoco
306 West Center Street
Mebane, Alamance County, North Carolina

Incident No. 18105

Facility ID: #00-0-0000023229

Latitude and Longitude: 36.097666° N; 79.272196° W

Land Use Category: Commercial
Contacts
Owner of UST: McLeod Oil Company, Inc.
PO Box 100
Mebane, North Carolina 27302
[phone]

Primary Contact: Mr. Michael Tompkins
Midway Oil and Gas Company, Inc.
[phone]

Consultant: Pilot Geological, PLLC
PO Box 128
Kernersville, North Carolina 27285
[phone]

Laboratory: Pace Analytical
1377 South Park Drive
Kernersville, North Carolina 27284
[phone]
Laboratory I.D. # Various

Release Information: The release was discovered by others during UST removal activities in October 1997.
The estimated quantity of release is unknown. The release occurred from a former gasoline UST system
consisting of three 1,000-gallon gasoline USTs.

Table of Contents
1.0 SITE HISTORY ................................................................................................................... 1
1.1 UST Information ......................................................................................................................................... 1
2.0 SITE GEOLOGY AND HYDROGEOLOGY ............................................................................... 1
3.0 FIELD ACTIVITIES .............................................................................................................. 2
3.1 Monitoring Well and Water Supply Well Sampling ..................................................................................... 2
3.2 Water Supply Wells .................................................................................................................................... 3
3.2 Groundwater Modeling .............................................................................................................................. 3
3.3 Free Product Investigation and Recovery ................................................................................................... 3
4.0 LABORATORY ANALYTICAL RESULTS ................................................................................. 3
4.1 Groundwater Sample Analysis .................................................................................................................... 3
5.0 CONCLUSIONS ................................................................................................................. 3
6.0 RECOMMENDATIONS ....................................................................................................... 4
7.0 QUALIFICATIONS OF REPORT ........................................................................................... 4
8.0 STATEMENTS AND CERTIFICATIONS ................................................................................. 4

DRAWINGS

Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 Sample Location Map
Drawing 4 Potentiometric Surface Map
Drawing 5 Benzene Isoconcentration Map
Drawing 6 Ethylbenzene Isoconcentration Map
Drawing 7 Naphthalene Isoconcentration Map
Drawing 8 n-Butylbenzene Isoconcentration Map
Drawing 9 Isopropylbenzene Isoconcentration Map
Drawing 10 n-Propylbenzene Isoconcentration Map
Drawing 11 Tetrachloroethene Isoconcentration Map
Drawing 12 Toluene Isoconcentration Map
Drawing 13 1,2,4-Trimethylbenzene Isoconcentration Map
Drawing 14 1,3,5-Trimethylbenzene Isoconcentration Map
Drawing 15 Total Xylenes Isoconcentration Map

Table of Contents (Continued)
TABLES

Table 1 UST Information
Table 2 Monitoring Well Construction Information
Table 3 Water Supply Well Information
Table 4 Summary of Groundwater Analytical Results

APPENDICIES

Appendix A Groundwater Concentration vs. Time Graphs and Monitoring Well
Sampling Sheets
Appendix B Laboratory Data Sheets and Chain of Custody Record
Groundwater Monitoring Report
Dodson’s Amoco
Pilot Project G-8098.1
March 7, 2023

1

1.0 SITE HISTORY

Dodson Amoco is located at 306 West Center Street in Mebane, Alamance County, North Carolina
(Drawings 1 and 2). The property is currently developed with an automotive repair facility. In
October of 1997, three 1,000-gallon gasoline USTs were removed from the site and a release was
detected. Mark Creel & Associates, Inc. completed the UST closure activities and associated report.
The release was confirmed through laboratory analysis of soil samples collected during the closure
activities.

Apex Environmental, Inc. completed an LSA for the site dated March 12, 2004. The site has been
classified as an intermediate risk site based on the presence of benzene above its Gross Contaminant
Level (GCL).

Based on the intermediate risk classification of the site, the NCDEQ issued a Notice of Regulatory
Requirements (NORR) dated February 13, 2023 requiring that an additional groundwater
monitoring event be completed.

Project information is based on correspondence between NCDEQ personnel, McLeod Oil Company,
Inc. and Pilot and the previously completed activities.

1.1 UST Information

A release was identified during the previous removal of three 1,000-gallon gasoline USTs by
others in October 1997. UST information is summarized in Table 1.

2.0 SITE GEOLOGY AND HYDROGEOLOGY

The United States Geological Survey (USGS) Topographic Map, Mebane and Efland, North
Carolina Quadrangle depicts the site as an urban area (Drawing 1). The site elevation is
approximately 670 feet above mean sea level. Unamend tributaries to Haw River are located
approximately 1,670 feet southwest of the site. Based on the review of the USGS topographic
map and observations of the general area and site topography, surface run-off would be
expected to flow generally to the southwest across the site.

The subject site is located within the Piedmont Physiographic Province. The Piedmont
Physiographic Province generally consists of hills and ridges which are dissected by a system of
swales and streams. The Piedmont Physiographic Province is predominantly underlain by
metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed
directly from molten material). The topography and relief of the Piedmont Province has
developed from differential weathering of the igneous and metamorphic rock. Ridges and hills
have been developed in areas of less weathered rock. Because of the continued chemical and
physical weathering rock in the Piedmont Physiographic Province is generally covered with a
Groundwater Monitoring Report
Dodson’s Amoco
Pilot Project G-8098.1
March 7, 2023

2

mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness
and are referred to as residuum or residual soils. The residuum is typically finer grained and has
higher clay content near the surface because of the advanced weathering. Similarly, the soils
typically become coarser grained with increasing depth because of decreased weathering. As the
weathering decreases, the residual soils generally retain the overall appearance, texture and
foliations of the parent rock.

In general, groundwater movement in the Piedmont Physiographic Province is from higher to
lower elevations. As such, the presumed direction of groundwater flow is generally to the south
across the site. Based on the presumed groundwater flow direction, areas to the north are
potentially up-gradient of the site.

3.0 FIELD ACTIVITIES

The field activities were completed by Pilot on February 23, 2023. The field activities consisted
of collecting groundwater samples from existing monitoring wells MW-1 through MW-4 and DW-
1 (Drawing 3).

3.1 Monitoring Well and Water Supply Well Sampling

A groundwater sample was collected from existing monitoring wells MW-1 through MW-4 and
DW-1 using a disposable bailer and new length of nylon string. Prior to sampling, approximately
three well volumes were purged from the monitoring wells. The monitoring wells were purged
to remove silt and sediment from the groundwater and collect a representative sample of
groundwater. After the purging was completed, samples were collected in the sample containers
provided by the laboratory. Pilot personnel wore a new pair of disposable nitrile gloves during
purging and sampling. Each container was labeled and placed in a cooler containing ice to
maintain the samples at approximately 4 Celsius. The samples were then transported to Pace
Analytical (Pace) for chemical analysis. The groundwater samples collected were analyzed for
volatile organic compounds (VOCs) using Standard Method 6200B. A chain of custody was
maintained and is included in Appendix B. Isoconcentration maps for select compounds that
exceed their respective 2L Standard are included as Drawings 5 through 15, respectively. Copies
of the Monitoring Well Sampling Sheets are included in Appendix A.

The depth to the groundwater surface in monitoring wells MW-1 through MW-4 and DW-1 was
measured using a decontaminated water level indicator. The top of casing elevation for each
well was surveyed relative to an arbitrary benchmark (MW-1) with an assumed elevation of
100.00 feet above mean sea level. The previously documented monitoring well elevations were
utilized to prepare a potentiometric surface map (Drawing 4). The relative groundwater
elevations collected from each monitoring well on February 23, 2023 are provided in Table 2.
Based on data collected during the assessment activities, the groundwater flow direction appears
to be generally toward the west-southwest beneath the site.
Groundwater Monitoring Report
Dodson’s Amoco
Pilot Project G-8098.1
March 7, 2023

3

3.2 Water Supply Wells

Visual evidence of water supply wells was not previously documented within 1,500 feet of the
source area.

3.2 Groundwater Modeling

Groundwater modeling has not been completed.

3.3 Free Product Investigation and Recovery

Free product was not detected during this monitoring event.

4.0 LABORATORY ANALYTICAL RESULTS

4.1 Groundwater Sample Analysis

Laboratory analysis of the groundwater samples collected from monitoring wells MW-1, MW-2,
MW-3, MW-4 and DW-1 detected targeted compounds above their respective 2L Standards, with
benzene exceeding its GCL in MW-2. A summary of the groundwater analytical results is
presented in Table 4. Historical groundwater contaminant concentrations for select monitoring
wells are presented in the graphs in Appendix A. The laboratory data sheets are included in
Appendix B.

5.0 CONCLUSIONS

Based on the results of the groundwater sampling, Pilot concludes the following:

 Laboratory analysis of the groundwater samples collected from monitoring wells MW-1, MW-
2, MW-3, MW-4 and DW-1 detected targeted compounds above their respective 2L Standards,
with benzene exceeding its GCL in MW-2.

 The groundwater flow was calculated to be generally to the west-southwest.

 It appears that natural attenuation is occurring, and it is Pilot’s opinion that monitoring
activities should continue until the concentration of benzene decreases to below its GCL.

 The inactive UST system on the site is planned for removal in the near future.

Groundwater Monitoring Report
Dodson’s Amoco
Pilot Project G-8098.1
March 7, 2023

4

6.0 RECOMMENDATIONS

Pilot recommends that the current property owner/responsible party submit a copy of this
Groundwater Monitoring Report to the NCDEQ, UST Section for their review. A NORP will need
to be recorded prior to a property transaction occurring.

7.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during
our field activities.

8.0 STATEMENTS AND CERTIFICATIONS

1 Enter the date the monitoring report was due. Not Established Will this report be
submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

3 If applicable, will any of the proposed attenuation milestones under the schedule approved in
the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
N/A
4 Does any known or suspected source zone soil contamination or free product remain outside
of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential
new release from a separate onsite or offsite source?
YES NO

6 Certification:
I, Jason T. Ricks, a Licensed Geologist for Pilot Geological, PLLC, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.

Pilot Geological, PLLC is licensed to practice geology in North Carolina. The certification
number of the company is C-542.

DRAWINGS
SITE
USGS Topographic Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098.1
Drawing 1
USGS Topographic Map
Mebane & Efland, NC Quadrangles
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
Dodson’s Amoco
306 West Center Street
Mebane, Alamance County, NC
Pilot Project G-8098.1
Drawing 2
Google Earth
Interactive Mapping Software
Scale : 1”= 80’
LEGEND
Site BoundaryU. Former UST System
U

TABLES
UST ID
Number Owner Last Contents Previous
Contents
Capacity
(in Gallons)
Construction
Details Tank Dimensions Installation
Date Status Release
6 Gasoline Gasoline 2,000 UnknownMcLeod Oil Company
2 Gasoline Gasoline Yes1,000 Unknown Unknown
McLeod Oil Company
Table 1 - UST Information
Dodsons Amoco
Mebane, North Carolina
1 Gasoline Gasoline 1,000 Unknown Unknown 5/3/1970
Removed
9/30/1997 Yes
UnknownUnknown10/2/1997Unknown
McLeod Oil Company 5/3/1970 Removed
9/30/1997
McLeod Oil Company
McLeod Oil Company
McLeod Oil Company
UnknownUnknown10/2/1997UnknownUnknown2,000
Unknown Unknown 10/2/1997 Unknown Unknown
YesRemoved
9/30/19975/3/1970UnknownUnknown1,000GasolineGasoline
5
4
3
GasolineGasoline
Gasoline Gasoline 2,000
Monitoring Well
ID
Well Diameter
(Inches)Date Installed Elevation (TOC)
Static Water Level
(2/8/23)
Groundwater
Elevation Total Depth Screened Interval
(feet)
Sand
Interval
Bentonite
Interval
MW-1 2 1/20/2004 100.00 8.84 91.16 17 7-17 ----
MW-2 2 2/12/2004 99.30 8.86 90.44 17 7-17 ----
MW-3 2 2/12/2004 99.05 8.42 90.63 17 7-17 ----
MW-4 2 2/12/2004 100.44 8.23 92.21 17 7-17 ----
DW-1 2 2/12/2004 100.23 8.79 91.44 50 45-50 -- --
Table 2 - Monitoring Well Construction Information
Dodsons Amoco
Mebane, North Carolina
*If free product is present the groundwater elevation is calculated by (TOC Elevation - Static) + (free product thickness x 0.8581)
Well ID NumberOwner Information Property Address Well Depth (feet) Well UseApproximate Distance from the Source AreaIs the Property Connected to Municipal WaterInformation was obtained from previous reports completed by others and updated as available. Table 3 - Water Supply Well InformationDodsons AmocoMebane, North CarolinaN/A N/A N/A N/A N/A N/A N/A
3030C
Sample ID Approximate Water Level (ft. BGS)Groundwater Elevation (ft.)Date Collected Benzene1,2-Dichloroethanecis-1,2-dichloroethenetrans-1,2-DichloroetheneIsopropyl ether (IPE)EthylbenzeneMTBENaphthalenen-ButylbenzeneIsopropylbenzenen-Propylbenzenep-Isopropyltoluenesec-Butylbenzenetert-ButylbenzeneStyreneTetrachloroetheneTrichloroetheneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aliphatics8.31 91.69 1/20/2004 7,180 30.2 <10 ND <50 5,560 17,300 538 <10 121 262 22.9 <10 ND 41.7 <10 <10 30,100 1,970 506 20,520 22 49,700 32,800 7,660
8.84 91.16 2/23/2023 742 ND ND ND ND 1,100 ND 131 ND 26.3 55.0 ND ND ND ND ND ND 953 310 59.9 796.8 NA NA NA NA
8.56 90.74 2/12/2004 6,160 109 ND ND 100 2,080 4,600 572 ND 124 160 21.3 20.5 ND 1.96 <1 <1 392 1,230 291 2,114.30 34 22,900 11,700 4,790
8.86 90.44 2/23/2023 5,720 ND ND ND ND 2,950 470 737 ND 99.0 215 ND ND ND ND ND ND 328 746 ND 1,210 NA NA NA NA
8.13 90.92 2/12/2004 808 <10 <10 ND <50 4,070 <50 503 <10 <10 208 11.5 <10 ND <10 <10 <10 102 1,890 444 2,986.70 41 15,600 13,700 5,220
8.42 90.63 2/23/2023 28.9 ND ND ND ND 3,730 ND 1,090 178 265 669 ND ND ND ND ND ND 68.7 2,460 694 1,570 NA NA NA NA
8.54 91.90 2/12/2004 3.27 ND ND ND <5 185 <5 128 16.7 36 78 24.2 12.3 ND 15 <1 <1 37.8 987 312 517 24 2,420 6,560 3,430
8.23 92.21 2/23/2023 ND ND ND ND ND 40.4 ND 60.2 ND 22.7 45.8 ND ND 1.8 ND 3.7 0.77 ND 180 27.3 70.4 NA NA NA NA
8.17 92.06 2/12/2004 115 ND 8.38 ND 10 ND 57.9 ND ND ND ND ND ND ND ND 52.7 26.2 4.71 ND 1.15 5.8 10 73,600 7,890 3,900
8.79 91.44 2/23/2023 ND ND 10.6 1.8 ND ND 0.57 ND ND ND ND ND ND 1.4 ND 71.2 54.0 ND ND ND ND NA NA NA NA
1 0.4 70 100 70 600 20 6 70 70 70 25 70 70 70 0.7 3 600 400 400 500 15 400 700 200
5,000 400 70,000 100,000 70,000 80,000 20,000 6,000 5,900 30,500 26,100 11,700 8,800 14,750 70,000 700 3,000 260,000 28,500 24,100 85,500 15,000 NS NS NS
= Concentration Exceeds the 2L StandardGCL = Gross Contamination Level
NA = Not Analyzed
BQL = Below Quantitation Limits
ND = Non Detect
NS = No Standard
GCLs (ug/L)
2L Standard (ug/L)
MW-3
MW-4
MW-1
MW-2
DW-1
Table 4 - Summary of Groundwater Analytical Results
Mebane, North Carolina
Dodsons Amoco
Targeted Compounds Standard Method 6200B VPH
05,00010,00015,00020,00025,00030,00091.191.291.391.491.591.691.71/1/2004 1/1/2007 1/1/2010 1/1/2013 1/1/2016 1/1/2019 1/1/2022Concentration (ug/L)Groundwater Elevation (Feet)DateMW-1Groundwater Elevation vs. Concentration vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes
01,0002,0003,0004,0005,0006,0007,00090.490.4590.590.5590.690.6590.790.7590.81/1/2004 1/1/2007 1/1/2010 1/1/2013 1/1/2016 1/1/2019 1/1/2022Concentration (ug/L)Groundwater Elevation (Feet)DateMW-3Groundwater Elevation vs. Concentration vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes
05001,0001,5002,0002,5003,0003,5004,0004,50090.690.6590.790.7590.890.8590.990.951/1/2004 1/1/2007 1/1/2010 1/1/2013 1/1/2016 1/1/2019 1/1/2022Concentration (ug/L)Groundwater Elevation (Feet)DateMW-3Groundwater Elevation vs. Concentration vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes

APPENDIX A

APPENDIX B
#=CL#
March 07, 2023
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92653704
92653704
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
G-8098.1 Dodson's Amoco
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on February 23, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 32
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Lab ID Sample ID Matrix Date Collected Date Received
92653704001 MW-1 Water 02/23/23 10:00 02/23/23 12:45
92653704002 MW-2 Water 02/23/23 11:00 02/23/23 12:45
92653704003 MW-3 Water 02/23/23 10:40 02/23/23 12:45
92653704004 MW-4 Water 02/23/23 10:20 02/23/23 12:45
92653704005 DW-1 Water 02/23/23 09:40 02/23/23 12:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92653704001 MW-1 SM 6200B 64 PASI-CLMB
92653704002 MW-2 SM 6200B 64 PASI-CLMB
92653704003 MW-3 SM 6200B 64 PASI-CLMB
92653704004 MW-4 SM 6200B 64 PASI-CLMB
92653704005 DW-1 SM 6200B 64 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-1 Lab ID:92653704001 Collected:02/23/23 10:00 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 742 ug/L 03/01/23 08:34 71-43-25.0 10
Bromobenzene ND ug/L 03/01/23 08:34 108-86-15.0 10
Bromochloromethane ND ug/L 03/01/23 08:34 74-97-55.0 10
Bromodichloromethane ND ug/L 03/01/23 08:34 75-27-45.0 10
Bromoform ND ug/L 03/01/23 08:34 75-25-25.0 10
Bromomethane ND ug/L 03/01/23 08:34 74-83-950.0 10
n-Butylbenzene ND ug/L 03/01/23 08:34 104-51-85.0 10
sec-Butylbenzene ND ug/L 03/01/23 08:34 135-98-85.0 10
tert-Butylbenzene ND ug/L 03/01/23 08:34 98-06-65.0 10
Carbon tetrachloride ND ug/L 03/01/23 08:34 56-23-55.0 10
Chlorobenzene ND ug/L 03/01/23 08:34 108-90-75.0 10
Chloroethane ND ug/L 03/01/23 08:34 75-00-310.0 10
Chloroform ND ug/L 03/01/23 08:34 67-66-35.0 10
Chloromethane ND ug/L 03/01/23 08:34 74-87-310.0 10
2-Chlorotoluene ND ug/L 03/01/23 08:34 95-49-85.0 10
4-Chlorotoluene ND ug/L 03/01/23 08:34 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 03/01/23 08:34 96-12-810.0 10
Dibromochloromethane ND ug/L 03/01/23 08:34 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 03/01/23 08:34 106-93-45.0 10
Dibromomethane ND ug/L 03/01/23 08:34 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 03/01/23 08:34 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 03/01/23 08:34 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 03/01/23 08:34 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 03/01/23 08:34 75-71-85.0 10
1,1-Dichloroethane ND ug/L 03/01/23 08:34 75-34-35.0 10
1,2-Dichloroethane ND ug/L 03/01/23 08:34 107-06-25.0 10
1,1-Dichloroethene ND ug/L 03/01/23 08:34 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 03/01/23 08:34 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 03/01/23 08:34 156-60-55.0 10
1,2-Dichloropropane ND ug/L 03/01/23 08:34 78-87-55.0 10
1,3-Dichloropropane ND ug/L 03/01/23 08:34 142-28-95.0 10
2,2-Dichloropropane ND ug/L 03/01/23 08:34 594-20-75.0 10
1,1-Dichloropropene ND ug/L 03/01/23 08:34 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 03/01/23 08:34 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 03/01/23 08:34 10061-02-65.0 10
Diisopropyl ether ND ug/L 03/01/23 08:34 108-20-35.0 10
Ethanol ND ug/L 03/01/23 08:34 64-17-5200010
Ethylbenzene 1100 ug/L 03/01/23 08:34 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 03/01/23 08:34 87-68-320.0 10
Isopropylbenzene (Cumene)26.3 ug/L 03/01/23 08:34 98-82-85.0 10
Methylene Chloride ND ug/L 03/01/23 08:34 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 03/01/23 08:34 1634-04-45.0 10
Naphthalene 131 ug/L 03/01/23 08:34 91-20-320.0 10
n-Propylbenzene 55.0 ug/L 03/01/23 08:34 103-65-15.0 10
Styrene ND ug/L 03/01/23 08:34 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 03/01/23 08:34 630-20-65.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-1 Lab ID:92653704001 Collected:02/23/23 10:00 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 03/01/23 08:34 79-34-55.0 10
Tetrachloroethene ND ug/L 03/01/23 08:34 127-18-45.0 10
Toluene 953 ug/L 03/01/23 08:34 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 03/01/23 08:34 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 03/01/23 08:34 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 03/01/23 08:34 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 03/01/23 08:34 79-00-55.0 10
Trichloroethene ND ug/L 03/01/23 08:34 79-01-65.0 10
Trichlorofluoromethane ND ug/L 03/01/23 08:34 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 03/01/23 08:34 96-18-45.0 10
1,2,4-Trimethylbenzene 310 ug/L 03/01/23 08:34 95-63-65.0 10
1,3,5-Trimethylbenzene 59.9 ug/L 03/01/23 08:34 108-67-85.0 10
Vinyl chloride ND ug/L 03/01/23 08:34 75-01-410.0 10
m&p-Xylene 700 ug/L 03/01/23 08:34 179601-23-110.0 10
o-Xylene 96.8 ug/L 03/01/23 08:34 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)103 %03/01/23 08:34 17060-07-070-130 10
4-Bromofluorobenzene (S)99 %03/01/23 08:34 460-00-470-130 10
Toluene-d8 (S)105 %03/01/23 08:34 2037-26-570-130 10
Sample:MW-2 Lab ID:92653704002 Collected:02/23/23 11:00 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 5720 ug/L 03/01/23 08:52 71-43-225.0 50
Bromobenzene ND ug/L 03/01/23 08:52 108-86-125.0 50
Bromochloromethane ND ug/L 03/01/23 08:52 74-97-525.0 50
Bromodichloromethane ND ug/L 03/01/23 08:52 75-27-425.0 50
Bromoform ND ug/L 03/01/23 08:52 75-25-225.0 50
Bromomethane ND ug/L 03/01/23 08:52 74-83-925050
n-Butylbenzene ND ug/L 03/01/23 08:52 104-51-825.0 50
sec-Butylbenzene ND ug/L 03/01/23 08:52 135-98-825.0 50
tert-Butylbenzene ND ug/L 03/01/23 08:52 98-06-625.0 50
Carbon tetrachloride ND ug/L 03/01/23 08:52 56-23-525.0 50
Chlorobenzene ND ug/L 03/01/23 08:52 108-90-725.0 50
Chloroethane ND ug/L 03/01/23 08:52 75-00-350.0 50
Chloroform ND ug/L 03/01/23 08:52 67-66-325.0 50
Chloromethane ND ug/L 03/01/23 08:52 74-87-350.0 50
2-Chlorotoluene ND ug/L 03/01/23 08:52 95-49-825.0 50
4-Chlorotoluene ND ug/L 03/01/23 08:52 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 03/01/23 08:52 96-12-850.0 50
Dibromochloromethane ND ug/L 03/01/23 08:52 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 03/01/23 08:52 106-93-425.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-2 Lab ID:92653704002 Collected:02/23/23 11:00 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromomethane ND ug/L 03/01/23 08:52 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 03/01/23 08:52 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 03/01/23 08:52 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 03/01/23 08:52 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 03/01/23 08:52 75-71-825.0 50
1,1-Dichloroethane ND ug/L 03/01/23 08:52 75-34-325.0 50
1,2-Dichloroethane ND ug/L 03/01/23 08:52 107-06-225.0 50
1,1-Dichloroethene ND ug/L 03/01/23 08:52 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 03/01/23 08:52 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 03/01/23 08:52 156-60-525.0 50
1,2-Dichloropropane ND ug/L 03/01/23 08:52 78-87-525.0 50
1,3-Dichloropropane ND ug/L 03/01/23 08:52 142-28-925.0 50
2,2-Dichloropropane ND ug/L 03/01/23 08:52 594-20-725.0 50
1,1-Dichloropropene ND ug/L 03/01/23 08:52 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 03/01/23 08:52 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 03/01/23 08:52 10061-02-625.0 50
Diisopropyl ether ND ug/L 03/01/23 08:52 108-20-325.0 50
Ethanol ND ug/L 03/01/23 08:52 64-17-51000050
Ethylbenzene 2950 ug/L 03/01/23 08:52 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 03/01/23 08:52 87-68-310050
Isopropylbenzene (Cumene)99.0 ug/L 03/01/23 08:52 98-82-825.0 50
Methylene Chloride ND ug/L 03/01/23 08:52 75-09-210050
Methyl-tert-butyl ether 470 ug/L 03/01/23 08:52 1634-04-425.0 50
Naphthalene 737 ug/L 03/01/23 08:52 91-20-310050
n-Propylbenzene 215 ug/L 03/01/23 08:52 103-65-125.0 50
Styrene ND ug/L 03/01/23 08:52 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 03/01/23 08:52 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 03/01/23 08:52 79-34-525.0 50
Tetrachloroethene ND ug/L 03/01/23 08:52 127-18-425.0 50
Toluene 328 ug/L 03/01/23 08:52 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 03/01/23 08:52 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 03/01/23 08:52 120-82-110050
1,1,1-Trichloroethane ND ug/L 03/01/23 08:52 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 03/01/23 08:52 79-00-525.0 50
Trichloroethene ND ug/L 03/01/23 08:52 79-01-625.0 50
Trichlorofluoromethane ND ug/L 03/01/23 08:52 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 03/01/23 08:52 96-18-425.0 50
1,2,4-Trimethylbenzene 746 ug/L 03/01/23 08:52 95-63-625.0 50
1,3,5-Trimethylbenzene ND ug/L 03/01/23 08:52 108-67-825.0 50
Vinyl chloride ND ug/L 03/01/23 08:52 75-01-450.0 50
m&p-Xylene 1210 ug/L 03/01/23 08:52 179601-23-150.0 50
o-Xylene ND ug/L 03/01/23 08:52 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)103 %03/01/23 08:52 17060-07-070-130 50
4-Bromofluorobenzene (S)100 %03/01/23 08:52 460-00-470-130 50
Toluene-d8 (S)107 %03/01/23 08:52 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-3 Lab ID:92653704003 Collected:02/23/23 10:40 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 28.9 ug/L 03/02/23 18:55 71-43-225.0 50
Bromobenzene ND ug/L 03/02/23 18:55 108-86-125.0 50
Bromochloromethane ND ug/L 03/02/23 18:55 74-97-525.0 50
Bromodichloromethane ND ug/L 03/02/23 18:55 75-27-425.0 50
Bromoform ND ug/L 03/02/23 18:55 75-25-225.0 50
Bromomethane ND ug/L 03/02/23 18:55 74-83-925050
n-Butylbenzene 178 ug/L 03/02/23 18:55 104-51-825.0 50
sec-Butylbenzene ND ug/L 03/02/23 18:55 135-98-825.0 50
tert-Butylbenzene ND ug/L 03/02/23 18:55 98-06-625.0 50
Carbon tetrachloride ND ug/L 03/02/23 18:55 56-23-525.0 50
Chlorobenzene ND ug/L 03/02/23 18:55 108-90-725.0 50
Chloroethane ND ug/L 03/02/23 18:55 75-00-350.0 50
Chloroform ND ug/L 03/02/23 18:55 67-66-325.0 50
Chloromethane ND ug/L 03/02/23 18:55 74-87-350.0 50
2-Chlorotoluene ND ug/L 03/02/23 18:55 95-49-825.0 50
4-Chlorotoluene ND ug/L 03/02/23 18:55 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 03/02/23 18:55 96-12-850.0 50
Dibromochloromethane ND ug/L 03/02/23 18:55 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 03/02/23 18:55 106-93-425.0 50
Dibromomethane ND ug/L 03/02/23 18:55 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 03/02/23 18:55 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 03/02/23 18:55 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 03/02/23 18:55 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 03/02/23 18:55 75-71-825.0 50
1,1-Dichloroethane ND ug/L 03/02/23 18:55 75-34-325.0 50
1,2-Dichloroethane ND ug/L 03/02/23 18:55 107-06-225.0 50
1,1-Dichloroethene ND ug/L 03/02/23 18:55 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 03/02/23 18:55 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 03/02/23 18:55 156-60-525.0 50
1,2-Dichloropropane ND ug/L 03/02/23 18:55 78-87-525.0 50
1,3-Dichloropropane ND ug/L 03/02/23 18:55 142-28-925.0 50
2,2-Dichloropropane ND ug/L 03/02/23 18:55 594-20-725.0 50
1,1-Dichloropropene ND ug/L 03/02/23 18:55 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 03/02/23 18:55 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 03/02/23 18:55 10061-02-625.0 50
Diisopropyl ether ND ug/L 03/02/23 18:55 108-20-325.0 50
Ethanol ND ug/L 03/02/23 18:55 64-17-5 L11000050
Ethylbenzene 3730 ug/L 03/02/23 18:55 100-41-425.0 50
Hexachloro-1,3-butadiene ND ug/L 03/02/23 18:55 87-68-310050
Isopropylbenzene (Cumene)265 ug/L 03/02/23 18:55 98-82-825.0 50
Methylene Chloride ND ug/L 03/02/23 18:55 75-09-210050
Methyl-tert-butyl ether ND ug/L 03/02/23 18:55 1634-04-425.0 50
Naphthalene 1090 ug/L 03/02/23 18:55 91-20-310050
n-Propylbenzene 669 ug/L 03/02/23 18:55 103-65-125.0 50
Styrene ND ug/L 03/02/23 18:55 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 03/02/23 18:55 630-20-625.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-3 Lab ID:92653704003 Collected:02/23/23 10:40 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 03/02/23 18:55 79-34-525.0 50
Tetrachloroethene ND ug/L 03/02/23 18:55 127-18-425.0 50
Toluene 68.7 ug/L 03/02/23 18:55 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 03/02/23 18:55 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 03/02/23 18:55 120-82-110050
1,1,1-Trichloroethane ND ug/L 03/02/23 18:55 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 03/02/23 18:55 79-00-525.0 50
Trichloroethene ND ug/L 03/02/23 18:55 79-01-625.0 50
Trichlorofluoromethane ND ug/L 03/02/23 18:55 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 03/02/23 18:55 96-18-425.0 50
1,2,4-Trimethylbenzene 2460 ug/L 03/02/23 18:55 95-63-625.0 50
1,3,5-Trimethylbenzene 694 ug/L 03/02/23 18:55 108-67-825.0 50
Vinyl chloride ND ug/L 03/02/23 18:55 75-01-450.0 50
m&p-Xylene 1570 ug/L 03/02/23 18:55 179601-23-150.0 50
o-Xylene ND ug/L 03/02/23 18:55 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)99 %03/02/23 18:55 17060-07-070-130 50
4-Bromofluorobenzene (S)96 %03/02/23 18:55 460-00-470-130 50
Toluene-d8 (S)100 %03/02/23 18:55 2037-26-570-130 50
Sample:MW-4 Lab ID:92653704004 Collected:02/23/23 10:20 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/28/23 21:53 71-43-20.50 1
Bromobenzene ND ug/L 02/28/23 21:53 108-86-10.50 1
Bromochloromethane ND ug/L 02/28/23 21:53 74-97-50.50 1
Bromodichloromethane ND ug/L 02/28/23 21:53 75-27-40.50 1
Bromoform ND ug/L 02/28/23 21:53 75-25-20.50 1
Bromomethane ND ug/L 02/28/23 21:53 74-83-95.0 1
n-Butylbenzene ND ug/L 02/28/23 21:53 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/28/23 21:53 135-98-80.50 1
tert-Butylbenzene 1.8 ug/L 02/28/23 21:53 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/28/23 21:53 56-23-50.50 1
Chlorobenzene ND ug/L 02/28/23 21:53 108-90-70.50 1
Chloroethane ND ug/L 02/28/23 21:53 75-00-31.0 1
Chloroform ND ug/L 02/28/23 21:53 67-66-30.50 1
Chloromethane ND ug/L 02/28/23 21:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/28/23 21:53 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/28/23 21:53 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/23 21:53 96-12-81.0 1
Dibromochloromethane ND ug/L 02/28/23 21:53 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/23 21:53 106-93-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:MW-4 Lab ID:92653704004 Collected:02/23/23 10:20 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Dibromomethane ND ug/L 02/28/23 21:53 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/28/23 21:53 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/28/23 21:53 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/28/23 21:53 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/28/23 21:53 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/28/23 21:53 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/28/23 21:53 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/28/23 21:53 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/28/23 21:53 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/28/23 21:53 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/28/23 21:53 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/28/23 21:53 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/28/23 21:53 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/28/23 21:53 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/28/23 21:53 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/28/23 21:53 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/28/23 21:53 108-20-30.50 1
Ethanol ND ug/L 02/28/23 21:53 64-17-52001
Ethylbenzene 40.4 ug/L 02/28/23 21:53 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/28/23 21:53 87-68-32.0 1
Isopropylbenzene (Cumene)22.7 ug/L 02/28/23 21:53 98-82-80.50 1
Methylene Chloride ND ug/L 02/28/23 21:53 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/28/23 21:53 1634-04-40.50 1
Naphthalene 60.2 ug/L 02/28/23 21:53 91-20-32.0 1
n-Propylbenzene 45.8 ug/L 02/28/23 21:53 103-65-10.50 1
Styrene ND ug/L 02/28/23 21:53 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/23 21:53 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/28/23 21:53 79-34-50.50 1
Tetrachloroethene 3.7 ug/L 02/28/23 21:53 127-18-40.50 1
Toluene ND ug/L 02/28/23 21:53 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/28/23 21:53 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/28/23 21:53 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/28/23 21:53 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/28/23 21:53 79-00-50.50 1
Trichloroethene 0.77 ug/L 02/28/23 21:53 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/28/23 21:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/28/23 21:53 96-18-40.50 1
1,2,4-Trimethylbenzene 180 ug/L 02/28/23 21:53 95-63-60.50 1
1,3,5-Trimethylbenzene 27.3 ug/L 02/28/23 21:53 108-67-80.50 1
Vinyl chloride ND ug/L 02/28/23 21:53 75-01-41.0 1
m&p-Xylene 70.4 ug/L 02/28/23 21:53 179601-23-11.0 1
o-Xylene ND ug/L 02/28/23 21:53 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %02/28/23 21:53 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/28/23 21:53 460-00-470-130 1
Toluene-d8 (S)103 %02/28/23 21:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:DW-1 Lab ID:92653704005 Collected:02/23/23 09:40 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 02/28/23 21:00 71-43-20.50 1
Bromobenzene ND ug/L 02/28/23 21:00 108-86-10.50 1
Bromochloromethane ND ug/L 02/28/23 21:00 74-97-50.50 1
Bromodichloromethane ND ug/L 02/28/23 21:00 75-27-40.50 1
Bromoform ND ug/L 02/28/23 21:00 75-25-20.50 1
Bromomethane ND ug/L 02/28/23 21:00 74-83-95.0 1
n-Butylbenzene ND ug/L 02/28/23 21:00 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/28/23 21:00 135-98-80.50 1
tert-Butylbenzene 1.4 ug/L 02/28/23 21:00 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/28/23 21:00 56-23-50.50 1
Chlorobenzene ND ug/L 02/28/23 21:00 108-90-70.50 1
Chloroethane ND ug/L 02/28/23 21:00 75-00-31.0 1
Chloroform ND ug/L 02/28/23 21:00 67-66-30.50 1
Chloromethane ND ug/L 02/28/23 21:00 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/28/23 21:00 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/28/23 21:00 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/28/23 21:00 96-12-81.0 1
Dibromochloromethane ND ug/L 02/28/23 21:00 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/28/23 21:00 106-93-40.50 1
Dibromomethane ND ug/L 02/28/23 21:00 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/28/23 21:00 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/28/23 21:00 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/28/23 21:00 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/28/23 21:00 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/28/23 21:00 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/28/23 21:00 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/28/23 21:00 75-35-40.50 1
cis-1,2-Dichloroethene 10.6 ug/L 02/28/23 21:00 156-59-20.50 1
trans-1,2-Dichloroethene 1.8 ug/L 02/28/23 21:00 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/28/23 21:00 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/28/23 21:00 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/28/23 21:00 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/28/23 21:00 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/28/23 21:00 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/28/23 21:00 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/28/23 21:00 108-20-30.50 1
Ethanol ND ug/L 02/28/23 21:00 64-17-52001
Ethylbenzene ND ug/L 02/28/23 21:00 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/28/23 21:00 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/28/23 21:00 98-82-80.50 1
Methylene Chloride ND ug/L 02/28/23 21:00 75-09-22.0 1
Methyl-tert-butyl ether 0.57 ug/L 02/28/23 21:00 1634-04-40.50 1
Naphthalene ND ug/L 02/28/23 21:00 91-20-32.0 1
n-Propylbenzene ND ug/L 02/28/23 21:00 103-65-10.50 1
Styrene ND ug/L 02/28/23 21:00 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/28/23 21:00 630-20-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Sample:DW-1 Lab ID:92653704005 Collected:02/23/23 09:40 Received:02/23/23 12:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 02/28/23 21:00 79-34-50.50 1
Tetrachloroethene 71.2 ug/L 02/28/23 21:00 127-18-40.50 1
Toluene ND ug/L 02/28/23 21:00 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/28/23 21:00 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/28/23 21:00 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/28/23 21:00 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/28/23 21:00 79-00-50.50 1
Trichloroethene 54.0 ug/L 02/28/23 21:00 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/28/23 21:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/28/23 21:00 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/28/23 21:00 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/28/23 21:00 108-67-80.50 1
Vinyl chloride ND ug/L 02/28/23 21:00 75-01-41.0 1
m&p-Xylene ND ug/L 02/28/23 21:00 179601-23-11.0 1
o-Xylene ND ug/L 02/28/23 21:00 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %02/28/23 21:00 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %02/28/23 21:00 460-00-470-130 1
Toluene-d8 (S)104 %02/28/23 21:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758608
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653704004, 92653704005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940357
Associated Lab Samples:92653704004, 92653704005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/28/23 17:26
1,1,1-Trichloroethane ug/L ND 0.50 02/28/23 17:26
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/28/23 17:26
1,1,2-Trichloroethane ug/L ND 0.50 02/28/23 17:26
1,1-Dichloroethane ug/L ND 0.50 02/28/23 17:26
1,1-Dichloroethene ug/L ND 0.50 02/28/23 17:26
1,1-Dichloropropene ug/L ND 0.50 02/28/23 17:26
1,2,3-Trichlorobenzene ug/L ND 2.0 02/28/23 17:26
1,2,3-Trichloropropane ug/L ND 0.50 02/28/23 17:26
1,2,4-Trichlorobenzene ug/L ND 2.0 02/28/23 17:26
1,2,4-Trimethylbenzene ug/L ND 0.50 02/28/23 17:26
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/28/23 17:26
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/28/23 17:26
1,2-Dichlorobenzene ug/L ND 0.50 02/28/23 17:26
1,2-Dichloroethane ug/L ND 0.50 02/28/23 17:26
1,2-Dichloropropane ug/L ND 0.50 02/28/23 17:26
1,3,5-Trimethylbenzene ug/L ND 0.50 02/28/23 17:26
1,3-Dichlorobenzene ug/L ND 0.50 02/28/23 17:26
1,3-Dichloropropane ug/L ND 0.50 02/28/23 17:26
1,4-Dichlorobenzene ug/L ND 0.50 02/28/23 17:26
2,2-Dichloropropane ug/L ND 0.50 02/28/23 17:26
2-Chlorotoluene ug/L ND 0.50 02/28/23 17:26
4-Chlorotoluene ug/L ND 0.50 02/28/23 17:26
Benzene ug/L ND 0.50 02/28/23 17:26
Bromobenzene ug/L ND 0.50 02/28/23 17:26
Bromochloromethane ug/L ND 0.50 02/28/23 17:26
Bromodichloromethane ug/L ND 0.50 02/28/23 17:26
Bromoform ug/L ND 0.50 02/28/23 17:26
Bromomethane ug/L ND 5.0 02/28/23 17:26
Carbon tetrachloride ug/L ND 0.50 02/28/23 17:26
Chlorobenzene ug/L ND 0.50 02/28/23 17:26
Chloroethane ug/L ND 1.0 02/28/23 17:26
Chloroform ug/L ND 0.50 02/28/23 17:26
Chloromethane ug/L ND 1.0 02/28/23 17:26
cis-1,2-Dichloroethene ug/L ND 0.50 02/28/23 17:26
cis-1,3-Dichloropropene ug/L ND 0.50 02/28/23 17:26
Dibromochloromethane ug/L ND 0.50 02/28/23 17:26
Dibromomethane ug/L ND 0.50 02/28/23 17:26
Dichlorodifluoromethane ug/L ND 0.50 02/28/23 17:26
Diisopropyl ether ug/L ND 0.50 02/28/23 17:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940357
Associated Lab Samples:92653704004, 92653704005
Matrix:Water
Analyzed
Ethanol ug/L ND 200 02/28/23 17:26
Ethylbenzene ug/L ND 0.50 02/28/23 17:26
Hexachloro-1,3-butadiene ug/L ND 2.0 02/28/23 17:26
Isopropylbenzene (Cumene)ug/L ND 0.50 02/28/23 17:26
m&p-Xylene ug/L ND 1.0 02/28/23 17:26
Methyl-tert-butyl ether ug/L ND 0.50 02/28/23 17:26
Methylene Chloride ug/L ND 2.0 02/28/23 17:26
n-Butylbenzene ug/L ND 0.50 02/28/23 17:26
n-Propylbenzene ug/L ND 0.50 02/28/23 17:26
Naphthalene ug/L ND 2.0 02/28/23 17:26
o-Xylene ug/L ND 0.50 02/28/23 17:26
sec-Butylbenzene ug/L ND 0.50 02/28/23 17:26
Styrene ug/L ND 0.50 02/28/23 17:26
tert-Butylbenzene ug/L ND 0.50 02/28/23 17:26
Tetrachloroethene ug/L ND 0.50 02/28/23 17:26
Toluene ug/L ND 0.50 02/28/23 17:26
trans-1,2-Dichloroethene ug/L ND 0.50 02/28/23 17:26
trans-1,3-Dichloropropene ug/L ND 0.50 02/28/23 17:26
Trichloroethene ug/L ND 0.50 02/28/23 17:26
Trichlorofluoromethane ug/L ND 1.0 02/28/23 17:26
Vinyl chloride ug/L ND 1.0 02/28/23 17:26
1,2-Dichloroethane-d4 (S)%96 70-130 02/28/23 17:26
4-Bromofluorobenzene (S)%103 70-130 02/28/23 17:26
Toluene-d8 (S)%109 70-130 02/28/23 17:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940358LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.020 95 60-140
1,1,1-Trichloroethane ug/L 21.420 107 60-140
1,1,2,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,2-Trichloroethane ug/L 21.020 105 60-140
1,1-Dichloroethane ug/L 21.520 107 60-140
1,1-Dichloroethene ug/L 22.920 114 60-140
1,1-Dichloropropene ug/L 23.220 116 60-140
1,2,3-Trichlorobenzene ug/L 19.820 99 60-140
1,2,3-Trichloropropane ug/L 19.420 97 60-140
1,2,4-Trichlorobenzene ug/L 19.920 99 60-140
1,2,4-Trimethylbenzene ug/L 19.920 100 60-140
1,2-Dibromo-3-chloropropane ug/L 18.520 93 60-140
1,2-Dibromoethane (EDB)ug/L 19.620 98 60-140
1,2-Dichlorobenzene ug/L 19.820 99 60-140
1,2-Dichloroethane ug/L 22.020 110 60-140
1,2-Dichloropropane ug/L 22.020 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940358LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 20.020 100 60-140
1,3-Dichlorobenzene ug/L 19.420 97 60-140
1,3-Dichloropropane ug/L 19.620 98 60-140
1,4-Dichlorobenzene ug/L 19.220 96 60-140
2,2-Dichloropropane ug/L 21.820 109 60-140
2-Chlorotoluene ug/L 19.420 97 60-140
4-Chlorotoluene ug/L 20.120 100 60-140
Benzene ug/L 20.620 103 60-140
Bromobenzene ug/L 19.620 98 60-140
Bromochloromethane ug/L 21.420 107 60-140
Bromodichloromethane ug/L 20.420 102 60-140
Bromoform ug/L 19.120 96 60-140
Bromomethane ug/L 15.820 79 60-140
Carbon tetrachloride ug/L 20.820 104 60-140
Chlorobenzene ug/L 19.220 96 60-140
Chloroethane ug/L 22.920 114 60-140
Chloroform ug/L 21.720 109 60-140
Chloromethane ug/L 21.220 106 60-140
cis-1,2-Dichloroethene ug/L 22.020 110 60-140
cis-1,3-Dichloropropene ug/L 21.420 107 60-140
Dibromochloromethane ug/L 19.220 96 60-140
Dibromomethane ug/L 19.620 98 60-140
Dichlorodifluoromethane ug/L 15.220 76 60-140
Diisopropyl ether ug/L 22.020 110 60-140
Ethanol ug/L 1010800 127 60-140
Ethylbenzene ug/L 19.620 98 60-140
Hexachloro-1,3-butadiene ug/L 19.920 99 60-140
Isopropylbenzene (Cumene)ug/L 19.220 96 60-140
m&p-Xylene ug/L 39.540 99 60-140
Methyl-tert-butyl ether ug/L 20.220 101 60-140
Methylene Chloride ug/L 23.520 118 60-140
n-Butylbenzene ug/L 20.820 104 60-140
n-Propylbenzene ug/L 20.220 101 60-140
Naphthalene ug/L 20.020 100 60-140
o-Xylene ug/L 19.720 99 60-140
sec-Butylbenzene ug/L 20.320 102 60-140
Styrene ug/L 20.120 100 60-140
tert-Butylbenzene ug/L 16.620 83 60-140
Tetrachloroethene ug/L 18.720 93 60-140
Toluene ug/L 19.620 98 60-140
trans-1,2-Dichloroethene ug/L 22.320 111 60-140
trans-1,3-Dichloropropene ug/L 20.920 104 60-140
Trichloroethene ug/L 20.820 104 60-140
Trichlorofluoromethane ug/L 19.520 98 60-140
Vinyl chloride ug/L 19.820 99 60-140
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940358LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3940359MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653957012
3940360
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 60-140115 8 3020ND21.3 23.0
1,1,1-Trichloroethane ug/L 20 125 60-140126 1 3020ND25.0 25.2
1,1,2,2-Tetrachloroethane ug/L 20 107 60-140108 1 3020ND21.4 21.5
1,1,2-Trichloroethane ug/L 20 110 60-140115 5 3020ND21.9 23.0
1,1-Dichloroethane ug/L 20 125 60-140127 2 3020ND25.0 25.4
1,1-Dichloroethene ug/L 20 132 60-140133 1 3020ND26.5 26.7
1,1-Dichloropropene ug/L M12013760-140141 3 3020ND27.4 28.2
1,2,3-Trichlorobenzene ug/L 20 96 60-140107 10 3020ND19.2 21.4
1,2,3-Trichloropropane ug/L 20 104 60-140105 1 3020ND20.8 21.0
1,2,4-Trichlorobenzene ug/L 20 97 60-140106 9 3020ND19.4 21.1
1,2,4-Trimethylbenzene ug/L 20 104 60-140109 5 3020ND20.8 21.8
1,2-Dibromo-3-
chloropropane ug/L 20 99 60-140106 6 3020ND19.9 21.1
1,2-Dibromoethane (EDB)ug/L 20 105 60-140107 1 3020ND21.1 21.3
1,2-Dichlorobenzene ug/L 20 103 60-140107 4 3020ND20.6 21.4
1,2-Dichloroethane ug/L 20 124 60-140125 1 3020ND24.8 25.0
1,2-Dichloropropane ug/L 20 120 60-140123 3 3020ND23.9 24.7
1,3,5-Trimethylbenzene ug/L 20 108 60-140111 2 3020ND21.6 22.1
1,3-Dichlorobenzene ug/L 20 104 60-140109 4 3020ND20.9 21.7
1,3-Dichloropropane ug/L 20 109 60-140110 1 3020ND21.8 22.1
1,4-Dichlorobenzene ug/L 20 101 60-140104 3 3020ND20.2 20.8
2,2-Dichloropropane ug/L 20 126 60-140129 2 3020ND25.3 25.7
2-Chlorotoluene ug/L 20 106 60-140108 2 3020ND21.2 21.6
4-Chlorotoluene ug/L 20 108 60-140113 4 3020ND21.6 22.5
Benzene ug/L 20 119 60-140120 1 3020ND23.8 24.0
Bromobenzene ug/L 20 104 60-140106 3 3020ND20.8 21.3
Bromochloromethane ug/L 20 124 60-140123 1 3020ND24.8 24.6
Bromodichloromethane ug/L 20 116 60-140117 1 3020ND23.2 23.5
Bromoform ug/L 20 104 60-140106 2 3020ND20.8 21.2
Bromomethane ug/L 20 78 60-14087 11 3020ND15.5 17.3
Carbon tetrachloride ug/L 20 121 60-140121 0 3020ND24.3 24.2
Chlorobenzene ug/L 20 105 60-140110 5 3020ND20.9 21.9
Chloroethane ug/L 20 133 60-140136 2 3020ND26.6 27.2
Chloroform ug/L 20 124 60-140128 4 3020ND24.7 25.6
Chloromethane ug/L 20 119 60-140124 4 3020ND23.9 24.7
cis-1,2-Dichloroethene ug/L 20 126 60-140132 4 3020ND25.2 26.3
cis-1,3-Dichloropropene ug/L 20 115 60-140120 4 3020ND23.0 24.0
Dibromochloromethane ug/L 20 106 60-140107 1 3020ND21.1 21.4
Dibromomethane ug/L 20 110 60-140112 2 3020ND22.0 22.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3940359MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653957012
3940360
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 20 90 60-14090 0 3020ND18.0 18.0
Diisopropyl ether ug/L 20 121 60-140130 7 3020ND24.3 26.1
Ethanol ug/L M180013960-140150 7 30800ND11101200
Ethylbenzene ug/L 20 111 60-140113 2 3020ND22.2 22.7
Hexachloro-1,3-butadiene ug/L 20 99 60-140104 5 3020ND19.8 20.7
Isopropylbenzene
(Cumene)ug/L 20 109 60-140110 1 3020ND21.7 21.9
m&p-Xylene ug/L 40 110 60-140113 2 3040ND44.0 45.0
Methyl-tert-butyl ether ug/L 20 108 60-140116 7 3020ND21.6 23.2
Methylene Chloride ug/L 20 125 60-140126 1 3020ND24.9 25.1
n-Butylbenzene ug/L 20 109 60-140114 5 3020ND21.7 22.9
n-Propylbenzene ug/L 20 107 60-140112 4 3020ND21.5 22.4
Naphthalene ug/L 20 99 60-140110 10 3020ND19.9 22.1
o-Xylene ug/L 20 109 60-140111 2 3020ND21.7 22.1
sec-Butylbenzene ug/L 20 107 60-140114 7 3020ND21.3 22.8
Styrene ug/L 20 110 60-140111 1 3020ND21.9 22.1
tert-Butylbenzene ug/L 20 88 60-14091 3 3020ND17.7 18.2
Tetrachloroethene ug/L 20 102 60-140107 5 3020ND20.3 21.3
Toluene ug/L 20 112 60-140115 3 3020ND22.5 23.1
trans-1,2-Dichloroethene ug/L 20 132 60-140134 1 3020ND26.5 26.8
trans-1,3-Dichloropropene ug/L 20 113 60-140118 4 3020ND22.7 23.7
Trichloroethene ug/L 20 117 60-140118 1 3020ND23.3 23.6
Trichlorofluoromethane ug/L 20 115 60-140116 1 3020ND22.9 23.1
Vinyl chloride ug/L 20 120 60-140116 3 3020ND24.0 23.3
1,2-Dichloroethane-d4 (S)%101 70-130101
4-Bromofluorobenzene (S)%102 70-13098
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758609
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653704001, 92653704002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940363
Associated Lab Samples:92653704001, 92653704002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/01/23 05:36
1,1,1-Trichloroethane ug/L ND 0.50 03/01/23 05:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/01/23 05:36
1,1,2-Trichloroethane ug/L ND 0.50 03/01/23 05:36
1,1-Dichloroethane ug/L ND 0.50 03/01/23 05:36
1,1-Dichloroethene ug/L ND 0.50 03/01/23 05:36
1,1-Dichloropropene ug/L ND 0.50 03/01/23 05:36
1,2,3-Trichlorobenzene ug/L ND 2.0 03/01/23 05:36
1,2,3-Trichloropropane ug/L ND 0.50 03/01/23 05:36
1,2,4-Trichlorobenzene ug/L ND 2.0 03/01/23 05:36
1,2,4-Trimethylbenzene ug/L ND 0.50 03/01/23 05:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/01/23 05:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/01/23 05:36
1,2-Dichlorobenzene ug/L ND 0.50 03/01/23 05:36
1,2-Dichloroethane ug/L ND 0.50 03/01/23 05:36
1,2-Dichloropropane ug/L ND 0.50 03/01/23 05:36
1,3,5-Trimethylbenzene ug/L ND 0.50 03/01/23 05:36
1,3-Dichlorobenzene ug/L ND 0.50 03/01/23 05:36
1,3-Dichloropropane ug/L ND 0.50 03/01/23 05:36
1,4-Dichlorobenzene ug/L ND 0.50 03/01/23 05:36
2,2-Dichloropropane ug/L ND 0.50 03/01/23 05:36
2-Chlorotoluene ug/L ND 0.50 03/01/23 05:36
4-Chlorotoluene ug/L ND 0.50 03/01/23 05:36
Benzene ug/L ND 0.50 03/01/23 05:36
Bromobenzene ug/L ND 0.50 03/01/23 05:36
Bromochloromethane ug/L ND 0.50 03/01/23 05:36
Bromodichloromethane ug/L ND 0.50 03/01/23 05:36
Bromoform ug/L ND 0.50 03/01/23 05:36
Bromomethane ug/L ND 5.0 03/01/23 05:36
Carbon tetrachloride ug/L ND 0.50 03/01/23 05:36
Chlorobenzene ug/L ND 0.50 03/01/23 05:36
Chloroethane ug/L ND 1.0 03/01/23 05:36
Chloroform ug/L ND 0.50 03/01/23 05:36
Chloromethane ug/L ND 1.0 03/01/23 05:36
cis-1,2-Dichloroethene ug/L ND 0.50 03/01/23 05:36
cis-1,3-Dichloropropene ug/L ND 0.50 03/01/23 05:36
Dibromochloromethane ug/L ND 0.50 03/01/23 05:36
Dibromomethane ug/L ND 0.50 03/01/23 05:36
Dichlorodifluoromethane ug/L ND 0.50 03/01/23 05:36
Diisopropyl ether ug/L ND 0.50 03/01/23 05:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940363
Associated Lab Samples:92653704001, 92653704002
Matrix:Water
Analyzed
Ethanol ug/L ND 200 03/01/23 05:36
Ethylbenzene ug/L ND 0.50 03/01/23 05:36
Hexachloro-1,3-butadiene ug/L ND 2.0 03/01/23 05:36
Isopropylbenzene (Cumene)ug/L ND 0.50 03/01/23 05:36
m&p-Xylene ug/L ND 1.0 03/01/23 05:36
Methyl-tert-butyl ether ug/L ND 0.50 03/01/23 05:36
Methylene Chloride ug/L ND 2.0 03/01/23 05:36
n-Butylbenzene ug/L ND 0.50 03/01/23 05:36
n-Propylbenzene ug/L ND 0.50 03/01/23 05:36
Naphthalene ug/L ND 2.0 03/01/23 05:36
o-Xylene ug/L ND 0.50 03/01/23 05:36
sec-Butylbenzene ug/L ND 0.50 03/01/23 05:36
Styrene ug/L ND 0.50 03/01/23 05:36
tert-Butylbenzene ug/L ND 0.50 03/01/23 05:36
Tetrachloroethene ug/L ND 0.50 03/01/23 05:36
Toluene ug/L ND 0.50 03/01/23 05:36
trans-1,2-Dichloroethene ug/L ND 0.50 03/01/23 05:36
trans-1,3-Dichloropropene ug/L ND 0.50 03/01/23 05:36
Trichloroethene ug/L ND 0.50 03/01/23 05:36
Trichlorofluoromethane ug/L ND 1.0 03/01/23 05:36
Vinyl chloride ug/L ND 1.0 03/01/23 05:36
1,2-Dichloroethane-d4 (S)%94 70-130 03/01/23 05:36
4-Bromofluorobenzene (S)%105 70-130 03/01/23 05:36
Toluene-d8 (S)%108 70-130 03/01/23 05:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940364LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.820 99 60-140
1,1,1-Trichloroethane ug/L 22.320 111 60-140
1,1,2,2-Tetrachloroethane ug/L 20.320 101 60-140
1,1,2-Trichloroethane ug/L 21.520 108 60-140
1,1-Dichloroethane ug/L 22.520 113 60-140
1,1-Dichloroethene ug/L 23.420 117 60-140
1,1-Dichloropropene ug/L 24.120 121 60-140
1,2,3-Trichlorobenzene ug/L 20.120 100 60-140
1,2,3-Trichloropropane ug/L 19.520 97 60-140
1,2,4-Trichlorobenzene ug/L 19.820 99 60-140
1,2,4-Trimethylbenzene ug/L 19.920 100 60-140
1,2-Dibromo-3-chloropropane ug/L 19.620 98 60-140
1,2-Dibromoethane (EDB)ug/L 20.520 103 60-140
1,2-Dichlorobenzene ug/L 19.820 99 60-140
1,2-Dichloroethane ug/L 23.020 115 60-140
1,2-Dichloropropane ug/L 22.620 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940364LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 19.920 100 60-140
1,3-Dichlorobenzene ug/L 19.720 98 60-140
1,3-Dichloropropane ug/L 20.420 102 60-140
1,4-Dichlorobenzene ug/L 19.320 97 60-140
2,2-Dichloropropane ug/L 20.020 100 60-140
2-Chlorotoluene ug/L 20.020 100 60-140
4-Chlorotoluene ug/L 20.220 101 60-140
Benzene ug/L 21.420 107 60-140
Bromobenzene ug/L 19.420 97 60-140
Bromochloromethane ug/L 22.120 110 60-140
Bromodichloromethane ug/L 21.120 106 60-140
Bromoform ug/L 19.520 97 60-140
Bromomethane ug/L 18.320 91 60-140
Carbon tetrachloride ug/L 21.320 107 60-140
Chlorobenzene ug/L 19.220 96 60-140
Chloroethane ug/L 22.920 115 60-140
Chloroform ug/L 22.820 114 60-140
Chloromethane ug/L 22.920 114 60-140
cis-1,2-Dichloroethene ug/L 23.220 116 60-140
cis-1,3-Dichloropropene ug/L 21.520 107 60-140
Dibromochloromethane ug/L 20.120 100 60-140
Dibromomethane ug/L 20.920 105 60-140
Dichlorodifluoromethane ug/L 15.720 79 60-140
Diisopropyl ether ug/L 23.220 116 60-140
Ethanol ug/L 1100800 137 60-140
Ethylbenzene ug/L 19.820 99 60-140
Hexachloro-1,3-butadiene ug/L 19.120 96 60-140
Isopropylbenzene (Cumene)ug/L 19.520 97 60-140
m&p-Xylene ug/L 39.640 99 60-140
Methyl-tert-butyl ether ug/L 21.420 107 60-140
Methylene Chloride ug/L 24.820 124 60-140
n-Butylbenzene ug/L 20.120 101 60-140
n-Propylbenzene ug/L 19.920 99 60-140
Naphthalene ug/L 20.120 101 60-140
o-Xylene ug/L 20.120 100 60-140
sec-Butylbenzene ug/L 20.420 102 60-140
Styrene ug/L 20.020 100 60-140
tert-Butylbenzene ug/L 16.220 81 60-140
Tetrachloroethene ug/L 18.220 91 60-140
Toluene ug/L 20.720 103 60-140
trans-1,2-Dichloroethene ug/L 22.820 114 60-140
trans-1,3-Dichloropropene ug/L 21.720 109 60-140
Trichloroethene ug/L 21.120 105 60-140
Trichlorofluoromethane ug/L 20.320 101 60-140
Vinyl chloride ug/L 20.920 104 60-140
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940364LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%103 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3940365MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653957003
3940366
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 124 60-140111 11 3020ND24.7 22.2
1,1,1-Trichloroethane ug/L 20 137 60-140122 12 3020ND27.5 24.5
1,1,2,2-Tetrachloroethane ug/L 20 124 60-140108 13 3020ND24.7 21.7
1,1,2-Trichloroethane ug/L 20 127 60-140109 15 3020ND25.3 21.7
1,1-Dichloroethane ug/L 20 133 60-140118 11 3020ND26.6 23.7
1,1-Dichloroethene ug/L M12014860-140131 12 3020ND29.7 26.3
1,1-Dichloropropene ug/L M12014560-140128 13 3020ND29.1 25.6
1,2,3-Trichlorobenzene ug/L 20 107 60-14095 12 3020ND21.5 19.0
1,2,3-Trichloropropane ug/L 20 116 60-140101 14 3020ND23.2 20.2
1,2,4-Trichlorobenzene ug/L 20 106 60-14096 10 3020ND21.3 19.2
1,2,4-Trimethylbenzene ug/L 20 117 60-140104 12 3020ND23.3 20.7
1,2-Dibromo-3-
chloropropane ug/L 20 113 60-140103 9 3020ND22.6 20.6
1,2-Dibromoethane (EDB)ug/L 20 121 60-140107 12 3020ND24.2 21.3
1,2-Dichlorobenzene ug/L 20 115 60-140100 14 3020ND23.0 20.1
1,2-Dichloroethane ug/L 20 137 60-140124 10 3020ND27.4 24.8
1,2-Dichloropropane ug/L 20 134 60-140117 14 3020ND26.8 23.4
1,3,5-Trimethylbenzene ug/L 20 115 60-140101 13 3020ND23.0 20.3
1,3-Dichlorobenzene ug/L 20 113 60-140100 12 3020ND22.5 20.0
1,3-Dichloropropane ug/L 20 117 60-140104 12 3020ND23.4 20.8
1,4-Dichlorobenzene ug/L 20 111 60-14099 12 3020ND22.3 19.9
2,2-Dichloropropane ug/L 20 131 60-140117 12 3020ND26.3 23.4
2-Chlorotoluene ug/L 20 116 60-140101 14 3020ND23.3 20.2
4-Chlorotoluene ug/L 20 116 60-140104 10 3020ND23.2 20.9
Benzene ug/L 20 135 60-140120 12 3020ND27.0 24.0
Bromobenzene ug/L 20 116 60-140101 14 3020ND23.2 20.1
Bromochloromethane ug/L 20 134 60-140120 11 3020ND26.8 24.0
Bromodichloromethane ug/L 20 128 60-140112 13 3020ND25.5 22.4
Bromoform ug/L 20 120 60-140105 13 3020ND24.1 21.1
Bromomethane ug/L 20 88 60-14095 8 3020ND17.5 19.0
Carbon tetrachloride ug/L 20 135 60-140118 14 3020ND27.1 23.5
Chlorobenzene ug/L 20 118 60-140106 11 3020ND23.5 21.2
Chloroethane ug/L 20 136 60-140120 13 3020ND27.3 24.0
Chloroform ug/L 20 134 60-140118 13 3020ND26.8 23.6
Chloromethane ug/L M12015060-140135 11 3020ND30.0 27.0
cis-1,2-Dichloroethene ug/L 20 136 60-140124 10 3020ND27.3 24.7
cis-1,3-Dichloropropene ug/L 20 124 60-140110 12 3020ND24.8 22.0
Dibromochloromethane ug/L 20 121 60-140105 14 3020ND24.2 21.0
Dibromomethane ug/L 20 123 60-140109 12 30201.2 25.9 23.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3940365MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653957003
3940366
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L M12014560-140130 11 3020ND29.1 26.1
Diisopropyl ether ug/L M12014960-140127 10 302015.5 45.3 40.9
Ethanol ug/L M180017260-140148 15 30800ND13701180
Ethylbenzene ug/L 20 119 60-140106 12 3020ND23.8 21.2
Hexachloro-1,3-butadiene ug/L 20 106 60-14096 11 3020ND21.3 19.1
Isopropylbenzene
(Cumene)ug/L 20 121 60-140109 10 30201.4 25.6 23.1
m&p-Xylene ug/L 40 118 60-140106 11 3040ND47.2 42.5
Methyl-tert-butyl ether ug/L M12016760-140142 6 302054.7 88.1 83.0
Methylene Chloride ug/L M12014260-140126 12 3020ND28.3 25.1
n-Butylbenzene ug/L 20 114 60-140103 10 3020ND22.8 20.6
n-Propylbenzene ug/L 20 115 60-140101 12 30201.1 24.1 21.2
Naphthalene ug/L 20 111 60-140104 6 30201.5J 23.7 22.3
o-Xylene ug/L 20 117 60-140106 10 3020ND23.4 21.2
sec-Butylbenzene ug/L 20 116 60-140100 13 30201.3 24.4 21.4
Styrene ug/L 20 110 60-14099 11 3020ND22.1 19.8
tert-Butylbenzene ug/L 20 96 60-14084 13 3020ND19.1 16.8
Tetrachloroethene ug/L 20 113 60-140101 11 3020ND22.6 20.2
Toluene ug/L 20 121 60-140108 12 3020ND24.3 21.5
trans-1,2-Dichloroethene ug/L 20 138 60-140125 10 3020ND27.6 25.0
trans-1,3-Dichloropropene ug/L 20 123 60-140111 10 3020ND24.6 22.3
Trichloroethene ug/L 20 129 60-140111 15 3020ND25.8 22.3
Trichlorofluoromethane ug/L 20 138 60-140123 12 3020ND27.6 24.6
Vinyl chloride ug/L 20 121 60-140109 10 3020ND24.2 21.9
1,2-Dichloroethane-d4 (S)%104 70-130103
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%102 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759027
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653704003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3942654
Associated Lab Samples:92653704003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/02/23 12:05
1,1,1-Trichloroethane ug/L ND 0.50 03/02/23 12:05
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/02/23 12:05
1,1,2-Trichloroethane ug/L ND 0.50 03/02/23 12:05
1,1-Dichloroethane ug/L ND 0.50 03/02/23 12:05
1,1-Dichloroethene ug/L ND 0.50 03/02/23 12:05
1,1-Dichloropropene ug/L ND 0.50 03/02/23 12:05
1,2,3-Trichlorobenzene ug/L ND 2.0 03/02/23 12:05
1,2,3-Trichloropropane ug/L ND 0.50 03/02/23 12:05
1,2,4-Trichlorobenzene ug/L ND 2.0 03/02/23 12:05
1,2,4-Trimethylbenzene ug/L ND 0.50 03/02/23 12:05
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/02/23 12:05
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/02/23 12:05
1,2-Dichlorobenzene ug/L ND 0.50 03/02/23 12:05
1,2-Dichloroethane ug/L ND 0.50 03/02/23 12:05
1,2-Dichloropropane ug/L ND 0.50 03/02/23 12:05
1,3,5-Trimethylbenzene ug/L ND 0.50 03/02/23 12:05
1,3-Dichlorobenzene ug/L ND 0.50 03/02/23 12:05
1,3-Dichloropropane ug/L ND 0.50 03/02/23 12:05
1,4-Dichlorobenzene ug/L ND 0.50 03/02/23 12:05
2,2-Dichloropropane ug/L ND 0.50 03/02/23 12:05
2-Chlorotoluene ug/L ND 0.50 03/02/23 12:05
4-Chlorotoluene ug/L ND 0.50 03/02/23 12:05
Benzene ug/L ND 0.50 03/02/23 12:05
Bromobenzene ug/L ND 0.50 03/02/23 12:05
Bromochloromethane ug/L ND 0.50 03/02/23 12:05
Bromodichloromethane ug/L ND 0.50 03/02/23 12:05
Bromoform ug/L ND 0.50 03/02/23 12:05
Bromomethane ug/L ND 5.0 03/02/23 12:05
Carbon tetrachloride ug/L ND 0.50 03/02/23 12:05
Chlorobenzene ug/L ND 0.50 03/02/23 12:05
Chloroethane ug/L ND 1.0 03/02/23 12:05
Chloroform ug/L ND 0.50 03/02/23 12:05
Chloromethane ug/L ND 1.0 03/02/23 12:05
cis-1,2-Dichloroethene ug/L ND 0.50 03/02/23 12:05
cis-1,3-Dichloropropene ug/L ND 0.50 03/02/23 12:05
Dibromochloromethane ug/L ND 0.50 03/02/23 12:05
Dibromomethane ug/L ND 0.50 03/02/23 12:05
Dichlorodifluoromethane ug/L ND 0.50 03/02/23 12:05
Diisopropyl ether ug/L ND 0.50 03/02/23 12:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3942654
Associated Lab Samples:92653704003
Matrix:Water
Analyzed
Ethanol ug/L ND 200 03/02/23 12:05
Ethylbenzene ug/L ND 0.50 03/02/23 12:05
Hexachloro-1,3-butadiene ug/L ND 2.0 03/02/23 12:05
Isopropylbenzene (Cumene)ug/L ND 0.50 03/02/23 12:05
m&p-Xylene ug/L ND 1.0 03/02/23 12:05
Methyl-tert-butyl ether ug/L ND 0.50 03/02/23 12:05
Methylene Chloride ug/L ND 2.0 03/02/23 12:05
n-Butylbenzene ug/L ND 0.50 03/02/23 12:05
n-Propylbenzene ug/L ND 0.50 03/02/23 12:05
Naphthalene ug/L ND 2.0 03/02/23 12:05
o-Xylene ug/L ND 0.50 03/02/23 12:05
sec-Butylbenzene ug/L ND 0.50 03/02/23 12:05
Styrene ug/L ND 0.50 03/02/23 12:05
tert-Butylbenzene ug/L ND 0.50 03/02/23 12:05
Tetrachloroethene ug/L ND 0.50 03/02/23 12:05
Toluene ug/L ND 0.50 03/02/23 12:05
trans-1,2-Dichloroethene ug/L ND 0.50 03/02/23 12:05
trans-1,3-Dichloropropene ug/L ND 0.50 03/02/23 12:05
Trichloroethene ug/L ND 0.50 03/02/23 12:05
Trichlorofluoromethane ug/L ND 1.0 03/02/23 12:05
Vinyl chloride ug/L ND 1.0 03/02/23 12:05
1,2-Dichloroethane-d4 (S)%102 70-130 03/02/23 12:05
4-Bromofluorobenzene (S)%103 70-130 03/02/23 12:05
Toluene-d8 (S)%107 70-130 03/02/23 12:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3942655LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.320 107 60-140
1,1,1-Trichloroethane ug/L 23.220 116 60-140
1,1,2,2-Tetrachloroethane ug/L 21.320 107 60-140
1,1,2-Trichloroethane ug/L 21.920 109 60-140
1,1-Dichloroethane ug/L 22.620 113 60-140
1,1-Dichloroethene ug/L 24.320 121 60-140
1,1-Dichloropropene ug/L 24.920 124 60-140
1,2,3-Trichlorobenzene ug/L 20.220 101 60-140
1,2,3-Trichloropropane ug/L 21.320 106 60-140
1,2,4-Trichlorobenzene ug/L 20.520 103 60-140
1,2,4-Trimethylbenzene ug/L 20.520 103 60-140
1,2-Dibromo-3-chloropropane ug/L 19.720 98 60-140
1,2-Dibromoethane (EDB)ug/L 21.620 108 60-140
1,2-Dichlorobenzene ug/L 20.220 101 60-140
1,2-Dichloroethane ug/L 24.320 122 60-140
1,2-Dichloropropane ug/L 22.520 113 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3942655LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 20.420 102 60-140
1,3-Dichlorobenzene ug/L 20.320 102 60-140
1,3-Dichloropropane ug/L 20.520 102 60-140
1,4-Dichlorobenzene ug/L 19.720 98 60-140
2,2-Dichloropropane ug/L 23.320 116 60-140
2-Chlorotoluene ug/L 20.320 101 60-140
4-Chlorotoluene ug/L 20.820 104 60-140
Benzene ug/L 22.320 111 60-140
Bromobenzene ug/L 20.220 101 60-140
Bromochloromethane ug/L 22.520 112 60-140
Bromodichloromethane ug/L 21.720 109 60-140
Bromoform ug/L 20.520 103 60-140
Bromomethane ug/L 18.820 94 60-140
Carbon tetrachloride ug/L 22.820 114 60-140
Chlorobenzene ug/L 20.120 100 60-140
Chloroethane ug/L 21.620 108 60-140
Chloroform ug/L 22.620 113 60-140
Chloromethane ug/L 25.420 127 60-140
cis-1,2-Dichloroethene ug/L 23.620 118 60-140
cis-1,3-Dichloropropene ug/L 22.320 111 60-140
Dibromochloromethane ug/L 21.020 105 60-140
Dibromomethane ug/L 21.220 106 60-140
Dichlorodifluoromethane ug/L 23.920 119 60-140
Diisopropyl ether ug/L 23.820 119 60-140
Ethanol ug/L 1160 L180014660-140
Ethylbenzene ug/L 20.420 102 60-140
Hexachloro-1,3-butadiene ug/L 21.220 106 60-140
Isopropylbenzene (Cumene)ug/L 21.020 105 60-140
m&p-Xylene ug/L 40.740 102 60-140
Methyl-tert-butyl ether ug/L 21.220 106 60-140
Methylene Chloride ug/L 24.220 121 60-140
n-Butylbenzene ug/L 20.920 105 60-140
n-Propylbenzene ug/L 20.420 102 60-140
Naphthalene ug/L 20.420 102 60-140
o-Xylene ug/L 20.820 104 60-140
sec-Butylbenzene ug/L 20.420 102 60-140
Styrene ug/L 20.820 104 60-140
tert-Butylbenzene ug/L 16.720 83 60-140
Tetrachloroethene ug/L 20.120 101 60-140
Toluene ug/L 20.620 103 60-140
trans-1,2-Dichloroethene ug/L 23.420 117 60-140
trans-1,3-Dichloropropene ug/L 22.520 113 60-140
Trichloroethene ug/L 21.920 109 60-140
Trichlorofluoromethane ug/L 22.920 115 60-140
Vinyl chloride ug/L 19.320 97 60-140
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3942655LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3942656MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92654567006
3942657
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 122 60-140121 1 3020ND24.5 24.2
1,1,1-Trichloroethane ug/L 20 123 60-140119 3 3020ND24.6 23.8
1,1,2,2-Tetrachloroethane ug/L 20 120 60-140116 3 3020ND23.9 23.3
1,1,2-Trichloroethane ug/L 20 117 60-140114 3 3020ND23.4 22.7
1,1-Dichloroethane ug/L 20 120 60-140119 1 3020ND24.0 23.9
1,1-Dichloroethene ug/L 20 132 60-140128 3 3020ND26.3 25.5
1,1-Dichloropropene ug/L 20 123 60-140121 2 3020ND24.5 24.1
1,2,3-Trichlorobenzene ug/L 20 108 60-140107 2 3020ND21.7 21.3
1,2,3-Trichloropropane ug/L 20 120 60-140120 1 3020ND24.1 24.0
1,2,4-Trichlorobenzene ug/L 20 108 60-140102 5 3020ND21.6 20.5
1,2,4-Trimethylbenzene ug/L 20 114 60-140111 3 3020ND22.8 22.2
1,2-Dibromo-3-
chloropropane ug/L 20 114 60-140109 5 3020ND22.9 21.8
1,2-Dibromoethane (EDB)ug/L 20 121 60-140119 2 3020ND24.2 23.7
1,2-Dichlorobenzene ug/L 20 114 60-140110 4 3020ND22.8 22.0
1,2-Dichloroethane ug/L 20 129 60-140125 3 3020ND25.7 25.1
1,2-Dichloropropane ug/L 20 124 60-140119 4 3020ND24.8 23.9
1,3,5-Trimethylbenzene ug/L 20 115 60-140111 3 3020ND23.0 22.3
1,3-Dichlorobenzene ug/L 20 113 60-140108 4 3020ND22.5 21.6
1,3-Dichloropropane ug/L 20 117 60-140115 2 3020ND23.5 23.0
1,4-Dichlorobenzene ug/L 20 112 60-140104 8 3020ND22.4 20.7
2,2-Dichloropropane ug/L 20 113 60-140110 2 3020ND22.5 22.0
2-Chlorotoluene ug/L 20 114 60-140109 4 3020ND22.8 21.9
4-Chlorotoluene ug/L 20 115 60-140112 3 3020ND23.1 22.4
Benzene ug/L 20 122 60-140120 2 3020ND24.4 24.0
Bromobenzene ug/L 20 113 60-140108 5 3020ND22.6 21.6
Bromochloromethane ug/L 20 118 60-140115 2 3020ND23.5 23.1
Bromodichloromethane ug/L 20 119 60-140113 5 3020ND23.7 22.7
Bromoform ug/L 20 115 60-140116 1 3020ND22.9 23.2
Bromomethane ug/L 20 87 60-14097 11 3020ND17.3 19.3
Carbon tetrachloride ug/L 20 126 60-140122 3 3020ND25.1 24.5
Chlorobenzene ug/L 20 113 60-140113 1 3020ND22.7 22.5
Chloroethane ug/L 20 114 60-140115 1 3020ND22.8 23.0
Chloroform ug/L 20 121 60-140118 3 3020ND24.2 23.6
Chloromethane ug/L 20 136 60-140131 4 3020ND27.2 26.1
cis-1,2-Dichloroethene ug/L 20 123 60-140121 1 3020ND24.5 24.3
cis-1,3-Dichloropropene ug/L 20 114 60-140110 3 3020ND22.7 22.0
Dibromochloromethane ug/L 20 119 60-140118 1 3020ND23.8 23.5
Dibromomethane ug/L 20 116 60-140108 7 3020ND23.2 21.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3942656MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92654567006
3942657
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 20 120 60-140119 1 3020ND24.0 23.8
Diisopropyl ether ug/L 20 124 60-140120 3 3020ND24.9 24.1
Ethanol ug/L M080013260-140147 10 30800ND10601170
Ethylbenzene ug/L 20 114 60-140115 1 3020ND22.8 23.1
Hexachloro-1,3-butadiene ug/L 20 114 60-140109 4 3020ND22.7 21.8
Isopropylbenzene
(Cumene)ug/L 20 117 60-140117 0 3020ND23.4 23.5
m&p-Xylene ug/L 40 114 60-140113 1 3040ND45.6 45.1
Methyl-tert-butyl ether ug/L 20 107 60-140103 4 3020ND21.3 20.5
Methylene Chloride ug/L 20 128 60-140126 2 3020ND25.6 25.2
n-Butylbenzene ug/L 20 111 60-140112 0 3020ND22.3 22.4
n-Propylbenzene ug/L 20 115 60-140111 3 3020ND22.9 22.2
Naphthalene ug/L 20 107 60-140109 1 3020ND21.5 21.8
o-Xylene ug/L 20 115 60-140109 5 3020ND23.0 21.9
sec-Butylbenzene ug/L 20 114 60-140113 2 3020ND22.9 22.5
Styrene ug/L 20 116 60-140114 1 3020ND23.1 22.9
tert-Butylbenzene ug/L 20 95 60-14092 4 3020ND19.1 18.4
Tetrachloroethene ug/L 20 107 60-140111 4 3020ND21.3 22.1
Toluene ug/L 20 111 60-140108 3 3020ND22.2 21.6
trans-1,2-Dichloroethene ug/L 20 121 60-140118 3 3020ND24.2 23.5
trans-1,3-Dichloropropene ug/L 20 113 60-140109 3 3020ND22.5 21.8
Trichloroethene ug/L 20 116 60-140115 1 3020ND23.2 23.1
Trichlorofluoromethane ug/L 20 127 60-140123 2 3020ND25.3 24.7
Vinyl chloride ug/L 20 102 60-140102 0 3020ND20.5 20.4
1,2-Dichloroethane-d4 (S)%107 70-130110
4-Bromofluorobenzene (S)%98 70-130101
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653704
G-8098.1 Dodson's Amoco
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653704001 758609MW-1 SM 6200B
92653704002 758609MW-2 SM 6200B
92653704003 759027MW-3 SM 6200B
92653704004 758608MW-4 SM 6200B
92653704005 758608DW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/07/2023 10:24 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 32
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