WS-3727_12188_CA_RPTS_20230307_LetRpt

Terraquest Environmental Consultants, P.C.
100 East Ruffin Street, Mebane, North Carolina 27302
Telephone [phone] ·Facsimile [phone]
www.terraquestpc.com

March 7, 2023

Linda Estkowski VIA EMAIL
NCDWM-UST Section
Winston-Salem Regional Office
585 Waughtown Street
Winston-Salem, NC 27107

Re: Letter Report (ePATA 12188-035 groundwater sampling)
Jonesville Amoco-B
428 North Bridge Street
Jonesville, Yadkin County, NC
NCDWM-UST Incident No. 12188
Terraquest Project No. 02209

Dear Ms. Estkowski:

On behalf of the responsible party, Beroth Oil Company, Inc., Terraquest Environmental
Consultants, P.C. hereby submits this Letter Report to document groundwater sampling efforts
conducted for the Jonesville Amoco B release incident. The site’s location, vicinity, and layout
are provided on the enclosed Figures 1, 2, and 3. Work was pre-approved on 12188-035 and -
035A. This letter report is submitted in lieu of the Corrective Action Design Report as there are
outstanding issues to resolve prior to the completion of that report at this time.

Terraquest personnel sampled monitoring wells MW5, MW17, MW20, MW24, MW25, MW27,
and MW30 as prescribed by the NCDWM-UST. Monitoring wells MW1, MW6, MW18, MW19,
MW26, MW29, and RW2 were gauged for free product thickness. The depth to water
measurements presented in Table 1 were collected prior to purging the sampled wells and used
to create the potentiometric surface map presented as Figure 4. Table 1 also contains measured
free product thicknesses. Four wells had product at thicknesses as great as 1.92 feet.

Each of the sampled wells was purged of three well volumes prior to sample collection. The
disposable purging bailer was used by field personnel donning new, disposable, nitrile gloves to
retrieve a sample that was placed into laboratory-prepared containers, labeled, and packed on
ice pending shipment to an NC-certified laboratory. Chain of custody documentation was
maintained throughout the process. Samples were analyzed by method 6200B.

As shown on the enclosed Table 2, Figure 5, and lab analytical report, the analytical results
revealed the presence of petroleum-type compounds in all samples. In addition to the gauged
free product, lab results indicated Gross Contamination Level violations were reported for
Page 2 of 2
Jonesville Amoco B (12188)
Letter Report (ePATA 12188-035 groundwater sampling)
3/7/23

Terraquest Environmental Consultants, P.C.
100 East Ruffin Street, Mebane, North Carolina 27302
Telephone [phone] ·Facsimile [phone]
www.terraquestpc.com
monitoring well MW20, 2L Standard violations for monitoring wells MW24, MW25, MW27, and
MW30. The full analytical report is enclosed.

Terraquest recommends corrective actions, including free product recovery, at this release
incident. The completion of a Corrective Action Design Report for the CAP Feasibility Study
approved dual-phase extraction is currently on hold pending NCDEQ review of air emissions
regulations and the necessity of an oxidizer to treat emissions.

Please call me at [phone] with any questions you may have. Thank you.

Sincerely,

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C.

Ryan D. Kerins Michael J. Brown, P.G.
Project Manager President

Enclosures
cc: Kevin Beroth, Beroth Oil Company, Inc.
ENVIRONMENTAL CONSULTANTS, P.C.
ENVIRONMENTAL CONSULTANTS, P.C.
ENVIRONMENTAL CONSULTANTS, P.C.
Table 1
Date: 3/7/23 Facility ID No. 0-005098
Well ID Date Installed
Date Water
Level Measured
Well Casing
Depth (ft.
BGS)
Screened Interval
(x to y ft. BGS)
Bottom of
Well (ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing (ft.)
Free
Product
Thickness
(ft.)
Groundwater
Elevation (ft.)Comments
MW1 2/9/1994 2/1/23 15 15-30 30 99.26 20.03 0.86 79.86 Type II Well
MW2 4/13/1994 Type II Well
MW3 4/13/1994 Type II Well
MW4 4/13/1994 Type II Well
MW5 4/14/1994 2/1/23 15 15-30 30 97.76 21.65 0 76.11 Type II Well
MW6 4/14/1994 2/1/23 20 20-35 35 99.22 18.30 0 80.92 Type II Well
MW7 4/14/1994 -18 18-33 33 99.16 ---Type II Well
MW8 4/18/1994 -18 18-34 34 101.38 ---Type II Well
MW9 8/1/1994 -18 18-31 31 103.36 ---Type II Well
MW10 8/1/1994 -18 18-32 32 102.26 ---Type II Well
MW11 8/1/1994 -25 25-40 39 96.06 ---Type II Well
MW12 8/1/1994 -37 37-47 47 97.68 ---Type II Well
MW13 11/10/1994 -OC: 51 IC: 56 56-61 61 97.52 ---Type III Well
MW14 12/1/2011 -15 15-35 35 99.34 ---Type II Well
MW15 12/1/2011 -15 15-35 35 100.26 ---Type II Well
MW16 12/1/2011 -15 15-35 35 100.38 ---Type II Well
MW17 12/1/2011 2/1/23 15 15-35 35 98.12 21.28 0 76.84 Type II Well
MW18 12/1/2011 2/1/23 15 15-35 35 97.90 18.36 0 79.54 Type II Well
MW19 12/1/2011 2/1/23 15 15-35 35 100.06 20.62 0.24 79.62 Type II Well
MW20 12/1/2011 2/1/23 15 15-35 35 99.10 18.72 0 80.38 Type II Well
MW21 7/16/2012 -15 15-35 35 99.68 ---Type II Well
MW22 7/16/2012 -15 15-35 35 97.14 ---Type II Well
MW23 7/16/2012 -15 15-35 35 97.63 ---Type II Well
MW24 7/16/2012 2/1/23 15 15-35 35 98.13 18.20 0 79.93 Type II Well
MW25 12/10/2012 2/1/23 15 15-35 35 98.61 20.86 0 77.75 Type II Well
MW26 12/10/2012 2/1/23 15 15-35 35 99.32 23.49 1.92 77.23 Type II Well
MW27 12/10/2012 2/1/23 15 15-35 35 98.87 22.80 0 76.07 Type II Well
MW28 12/10/2012 Type II Well
MW29 6/2/2014 2/1/23 15 15-25 25 98.16 18.35 0.15 79.92 Type II Well
MW30 6/2/2014 2/1/23 15 15-25 25 98.53 18.79 0 79.74 Type II Well
MW"2"11/11/2008 -15 15-30 30 101.38 ---Type II Well
MW"3"11/11/2008 -15 15-25 25 100.82 ---Type II Well
MW"4"11/11/2008 -15 15-25 25 100.74 ---Type II Well
SVE1 11/20/2012 -5 5-25 25 98.44 ---SVE Well
SVE2 11/20/2012 -5 5-25 25 98.26 ---SVE Well
SVE3 3/1/2022 -15 15-25 25 99.94 ---SVE Well
AS1 11/20/2012 -40 40-45 45 98.49 ---1" Air Sparge Well
RW1 12/10/2012 -10 10-45 45 99.14 ---4" Type II Well
RW2 3/1/2022 2/1/23 10 10-35 35 98.90 19.25 0 79.65 4" Type II Well
Notes:
1. All units in feet.
2. - Indicates no detection of free product found in the well.
3. NA - Not Applicable
4. The groundwater elevation for monitoring wells with free product was adjusted using the following formula:
[top of casing elevation - depth to water] + [free product thickness x 0.7305].
5. "OC" - Outter Casing "IC" - Inner Casing
DESTROYED
DESTROYED
DESTROYED
PILOT TESTING WELLS
MONITORING WELL CONSTRUCTION INFORMATION
Incident Name: Jonesville Amoco-B Incident No.: 12188
DESTROYED
Table 2
Date: 3/7/23
6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200BWell ID
Date
Collected
MW1 2/1/23MW52/1/23 0.712 J 0.986 J 1.03 9.34 J < 0.220 < 0.200 < 10.0 < 2.60 < 0.760 < 0.700 < 0.530 5.43 < 0.690 < 4.90 4.77 1.65MW172/1/23 0.475 J < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 10.0 < 2.60 < 0.760 < 0.700 < 0.530 < 3.00 < 0.690 < 4.90 < 0.820 < 0.560MW192/1/23MW202/1/23 12,000 31,300 2,450 13,500 14,800 78 J 2,740 J 743 J < 152 < 140 < 106 1,170 236 23,500 2,390 669
MW24 2/1/23 704 1,510 1,220 3,790 134 2.18 J < 100 < 26.0 37.5 10.5 66.9 614 223 < 49.0 1,640 442
MW25 2/1/23 1.17 < 0.410 < 0.500 3.39 J < 0.220 < 0.200 < 10.0 < 2.60 < 0.760 1.08 2.27 < 3.00 < 0.690 < 4.90 13.3 < 0.560
MW26 2/1/23
MW27 2/1/23 1,020 199 1,200 3,600 77.5 < 4.00 < 200 < 52.0 23.1 < 14.0 64.5 652 110 < 98.0 1,140 387MW292/1/23MW302/1/23 132 1,330 661 3,430 < 4.40 < 4.00 < 200 < 52.0 27.2 < 14.0 39.7 454 123 < 98.0 1,110 302160060050020706,000 4,000 70 70 70 6 70 10 400 4005,000 260,000 84,500 85,500 20,000 70,000 6,000,000 4,000,000 6,900 8,500 25,000 6,000 30,000 10,000 28,500 25,000Notes:
1. All results in µg/l.
2. Bold denotes a detection.
3. Shading denotes a 2L Standard violation.
4. Italics denotes a GCL violation. 5. "J" - Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.MTBEIPE0.86 feet of free product
0.24 feet of free product
1.92 feet of free product
0.15 feet of free product sec-Butylbenzene 2L Standard
SUMMARY OF GROUNDWATER SAMPLING RESULTSIncident Name: Jonesville Amoco-B Incident No. 12188
Analytical MethodContaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesGCLs t-Butyl alcohol1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneNaphthalene n-PropylbenzeneAcetone2-Butanone (MEK)n-Butylbenzene
ANALYTICAL REPORT
PREPARED FOR
Attn: Ryan Kerins
Terraquest Environmental Consultants, PC
100 E. Ruffin Street
Mebane, North Carolina 27302
Generated 2/13/2023 3:26:59 PM
JOB DESCRIPTION
Jonesville Amoco B
JOB NUMBER
400-232732-1
See page two for job notes and contact information.
Pensacola FL 32514
3355 McLemore Drive
Eurofins Pensacola
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Eurofins Pensacola
Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and relate
only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without written
approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on this page, or
the telephone number at the bottom of the page. Eurofins Environment Testing Southeast LLC, Pensacola Certifications and
Approvals: Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida (E81010), Illinois (200041), Iowa (367), Kansas
(E-10253), Kentucky UST (53), Louisiana (30748), Maryland (233), Massachusetts (M-FL094), Michigan (9912), New
Hampshire (250510), New Jersey (FL006), North Carolina (314), Oklahoma (9810), Pennsylvania (68-00467), Rhode Island
(LAO00307), South Carolina (96026), Tennessee (TN02907), Texas (T104704286-10-2), Virginia (00008), Washington
(C2043), West Virginia (136), USDA Foreign Soil Permit (P330-08-00006).
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
2/13/2023 3:26:59 PM
Authorized for release by
Chad Bechtold, Project Manager
[e-mail]
[phone]
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Table of Contents
Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Laboratory Job ID: 400-232732-1
Page 3 of 44 Eurofins Pensacola2/13/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
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Case Narrative
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Job ID: 400-232732-1
Laboratory: Eurofins Pensacola
Narrative
Job Narrative
400-232732-1
Receipt
The samples were received on 2/6/2023 8:51 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.4°C
GC/MS VOA
Method SM6200_B: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW20
(400-232732-3). Elevated reporting limits (RLs) are provided.
Method SM6200_B: The matrix spike / matrix spike duplicate (MS/MSD) precision for analytical batch 400-611700 was outside control
limits. Sample matrix interference is suspected.
Method SM6200_B: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW27
(400-232732-6) and MW30 (400-232732-7). Elevated reporting limits (RLs) are provided.
Method SM6200_B: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW24
(400-232732-4). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins PensacolaPage 4 of 44 2/13/2023
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Detection Summary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Client Sample ID: MW5 Lab Sample ID: 400-232732-1
1,2,4-Trimethylbenzene
RL
1.00 ug/L
MDL
0.820
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.77 SM6200-B
1,3,5-Trimethylbenzene 1.00 ug/L0.560 Total/NA11.65 SM6200-B
Benzene 1.00 ug/L0.130 Total/NA10.712 J SM6200-B
Ethylbenzene 1.00 ug/L0.500 Total/NA11.03 SM6200-B
m-Xylene & p-Xylene 5.00 ug/L0.630 Total/NA16.72 SM6200-B
Naphthalene 5.00 ug/L3.00 Total/NA15.43 SM6200-B
o-Xylene 5.00 ug/L0.600 Total/NA12.61 J SM6200-B
Toluene 1.00 ug/L0.410 Total/NA10.986 J SM6200-B
Xylenes, Total 10.0 ug/L1.60 Total/NA19.34 J SM6200-B
Client Sample ID: MW17 Lab Sample ID: 400-232732-2
Benzene
RL
1.00 ug/L
MDL
0.130
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.475 SM6200-B
Client Sample ID: MW20 Lab Sample ID: 400-232732-3
1,2,4-Trimethylbenzene
RL
200 ug/L
MDL
164
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA2002390SM6200-B
1,3,5-Trimethylbenzene 200 ug/L112 Total/NA200669SM6200-B
2-Butanone (MEK)5000 ug/L520 Total/NA200743JSM6200-B
Acetone 5000 ug/L2000 Total/NA2002740JSM6200-B
Benzene 200 ug/L26.0 Total/NA20012000SM6200-B
Diisopropyl ether 200 ug/L40.0 Total/NA20078.0 J SM6200-B
Ethylbenzene 200 ug/L100 Total/NA2002450SM6200-B
Methyl tert-butyl ether 200 ug/L44.0 Total/NA20014800SM6200-B
m-Xylene & p-Xylene 1000 ug/L126 Total/NA2008660SM6200-B
Naphthalene 1000 ug/L600 Total/NA2001170SM6200-B
N-Propylbenzene 200 ug/L138 Total/NA200236SM6200-B
o-Xylene 1000 ug/L120 Total/NA2004810SM6200-B
Toluene 200 ug/L82.0 Total/NA20031300SM6200-B
Xylenes, Total 2000 ug/L320 Total/NA20013500SM6200-B
t-Butyl alcohol 2000 ug/L980 Total/NA20023500SM6200-B
Client Sample ID: MW24 Lab Sample ID: 400-232732-4
1,2,4-Trimethylbenzene
RL
10.0 ug/L
MDL
8.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA101640SM6200-B
1,3,5-Trimethylbenzene 10.0 ug/L5.60 Total/NA10442SM6200-B
Benzene 10.0 ug/L1.30 Total/NA10704SM6200-B
Diisopropyl ether 10.0 ug/L2.00 Total/NA102.18 J SM6200-B
Ethylbenzene 10.0 ug/L5.00 Total/NA101220SM6200-B
Isopropylbenzene 10.0 ug/L5.30 Total/NA1066.9 SM6200-B
Methyl tert-butyl ether 10.0 ug/L2.20 Total/NA10134SM6200-B
Naphthalene 50.0 ug/L30.0 Total/NA10614SM6200-B
n-Butylbenzene 10.0 ug/L7.60 Total/NA1037.5 SM6200-B
N-Propylbenzene 10.0 ug/L6.90 Total/NA10223SM6200-B
sec-Butylbenzene 10.0 ug/L7.00 Total/NA1010.5 SM6200-B
Toluene 10.0 ug/L4.10 Total/NA101510SM6200-B
m-Xylene & p-Xylene - DL 100 ug/L12.6 Total/NA203110SM6200-B
o-Xylene - DL 100 ug/L12.0 Total/NA20677SM6200-B
Xylenes, Total - DL 200 ug/L32.0 Total/NA203790SM6200-B
Eurofins Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Client Sample ID: MW25 Lab Sample ID: 400-232732-5
1,2,4-Trimethylbenzene
RL
1.00 ug/L
MDL
0.820
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA113.3 SM6200-B
Benzene 1.00 ug/L0.130 Total/NA11.17 SM6200-B
Isopropylbenzene 1.00 ug/L0.530 Total/NA12.27 SM6200-B
m-Xylene & p-Xylene 5.00 ug/L0.630 Total/NA13.39 J SM6200-B
sec-Butylbenzene 1.00 ug/L0.700 Total/NA11.08 SM6200-B
Xylenes, Total 10.0 ug/L1.60 Total/NA13.39 J SM6200-B
Client Sample ID: MW27 Lab Sample ID: 400-232732-6
1,2,4-Trimethylbenzene
RL
20.0 ug/L
MDL
16.4
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA201140SM6200-B
1,3,5-Trimethylbenzene 20.0 ug/L11.2 Total/NA20387SM6200-B
Benzene 20.0 ug/L2.60 Total/NA201020SM6200-B
Ethylbenzene 20.0 ug/L10.0 Total/NA201200SM6200-B
Isopropylbenzene 20.0 ug/L10.6 Total/NA2064.5 SM6200-B
Methyl tert-butyl ether 20.0 ug/L4.40 Total/NA2077.5 SM6200-B
m-Xylene & p-Xylene 100 ug/L12.6 Total/NA202840SM6200-B
Naphthalene 100 ug/L60.0 Total/NA20652SM6200-B
n-Butylbenzene 20.0 ug/L15.2 Total/NA2023.1 SM6200-B
N-Propylbenzene 20.0 ug/L13.8 Total/NA20110SM6200-B
o-Xylene 100 ug/L12.0 Total/NA20762SM6200-B
Toluene 20.0 ug/L8.20 Total/NA20199SM6200-B
Xylenes, Total 200 ug/L32.0 Total/NA203600SM6200-B
Client Sample ID: MW30 Lab Sample ID: 400-232732-7
1,2,4-Trimethylbenzene
RL
20.0 ug/L
MDL
16.4
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA201110SM6200-B
1,3,5-Trimethylbenzene 20.0 ug/L11.2 Total/NA20302SM6200-B
Benzene 20.0 ug/L2.60 Total/NA20132SM6200-B
Ethylbenzene 20.0 ug/L10.0 Total/NA20661SM6200-B
Isopropylbenzene 20.0 ug/L10.6 Total/NA2039.7 SM6200-B
m-Xylene & p-Xylene 100 ug/L12.6 Total/NA202360SM6200-B
Naphthalene 100 ug/L60.0 Total/NA20454SM6200-B
n-Butylbenzene 20.0 ug/L15.2 Total/NA2027.2 SM6200-B
N-Propylbenzene 20.0 ug/L13.8 Total/NA20123SM6200-B
o-Xylene 100 ug/L12.0 Total/NA201070SM6200-B
Toluene 20.0 ug/L8.20 Total/NA201330SM6200-B
Xylenes, Total 200 ug/L32.0 Total/NA203430SM6200-B
Eurofins Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Lab Sample ID Client Sample ID Matrix Collected Received
400-232732-1 MW5 Water 02/01/23 14:28 02/06/23 08:51
400-232732-2 MW17 Water 02/01/23 13:39 02/06/23 08:51
400-232732-3 MW20 Water 02/01/23 13:28 02/06/23 08:51
400-232732-4 MW24 Water 02/01/23 13:19 02/06/23 08:51
400-232732-5 MW25 Water 02/01/23 14:14 02/06/23 08:51
400-232732-6 MW27 Water 02/01/23 14:01 02/06/23 08:51
400-232732-7 MW30 Water 02/01/23 13:52 02/06/23 08:51
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-1Client Sample ID: MW5
Matrix: WaterDate Collected: 02/01/23 14:28
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 02/09/23 10:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 02/09/23 10:14 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 02/09/23 10:14 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 02/09/23 10:14 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 02/09/23 10:14 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 02/09/23 10:14 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 02/09/23 10:14 14.771,2,4-Trimethylbenzene
1.00 0.230 ug/L 02/09/23 10:14 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 02/09/23 10:14 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 02/09/23 10:14 11.651,3,5-Trimethylbenzene
1.00 0.540 ug/L 02/09/23 10:14 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 10:14 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 02/09/23 10:14 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 10:14 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 02/09/23 10:14 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 02/09/23 10:14 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 02/09/23 10:14 11.40 U2-Hexanone
1.00 0.560 ug/L 02/09/23 10:14 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 02/09/23 10:14 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 02/09/23 10:14 110.0 UAcetone
1.00 0.130 ug/L 02/09/23 10:14 10.712 JBenzene
1.00 0.540 ug/L 02/09/23 10:14 10.540 UBromobenzene
1.00 0.210 ug/L 02/09/23 10:14 10.210 UBromochloromethane
1.00 0.500 ug/L 02/09/23 10:14 10.500 UBromodichloromethane
5.00 0.250 ug/L 02/09/23 10:14 10.250 UBromoform
1.00 0.980 ug/L 02/09/23 10:14 10.980 UBromomethane
1.00 0.190 ug/L 02/09/23 10:14 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 02/09/23 10:14 10.150 UChlorobenzene
1.00 0.760 ug/L 02/09/23 10:14 10.760 UChloroethane
1.00 1.00 ug/L 02/09/23 10:14 11.00 UChloroform
1.00 0.320 ug/L 02/09/23 10:14 10.320 UChloromethane
1.00 0.200 ug/L 02/09/23 10:14 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 02/09/23 10:14 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 02/09/23 10:14 10.240 UDibromochloromethane
1.00 0.850 ug/L 02/09/23 10:14 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 02/09/23 10:14 10.200 UDiisopropyl ether
100 24.0 ug/L 02/09/23 10:14 124.0 UEthanol
1.00 0.500 ug/L 02/09/23 10:14 11.03Ethylbenzene
1.00 0.530 ug/L 02/09/23 10:14 10.530 UIsopropylbenzene
1.00 0.220 ug/L 02/09/23 10:14 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 02/09/23 10:14 13.00 UMethylene Chloride
5.00 0.630 ug/L 02/09/23 10:14 16.72m-Xylene & p-Xylene
5.00 3.00 ug/L 02/09/23 10:14 15.43Naphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-1Client Sample ID: MW5
Matrix: WaterDate Collected: 02/01/23 14:28
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U F2 1.00 0.760 ug/L 02/09/23 10:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 02/09/23 10:14 10.690 UN-Propylbenzene
5.00 0.600 ug/L 02/09/23 10:14 12.61 Jo-Xylene
1.00 0.710 ug/L 02/09/23 10:14 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 02/09/23 10:14 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 02/09/23 10:14 11.00 UStyrene
1.00 0.630 ug/L 02/09/23 10:14 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 02/09/23 10:14 10.900 UTetrachloroethene
1.00 0.410 ug/L 02/09/23 10:14 10.986 JToluene
1.00 0.500 ug/L 02/09/23 10:14 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 02/09/23 10:14 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 02/09/23 10:14 10.150 UTrichloroethene
1.00 0.520 ug/L 02/09/23 10:14 10.520 UTrichlorofluoromethane
25.0 0.930 ug/L 02/09/23 10:14 10.930 UVinyl acetate
1.00 0.500 ug/L 02/09/23 10:14 10.500 UVinyl chloride
10.0 1.60 ug/L 02/09/23 10:14 19.34 JXylenes, Total
10.0 4.90 ug/L 02/09/23 10:14 14.90 Ut-Butyl alcohol
4-Bromofluorobenzene 99 72-119 02/09/23 10:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 97 02/09/23 10:14 175-126
Toluene-d8 (Surr)96 02/09/23 10:14 164-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-2Client Sample ID: MW17
Matrix: WaterDate Collected: 02/01/23 13:39
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 02/09/23 17:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 02/09/23 17:37 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 02/09/23 17:37 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 02/09/23 17:37 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 02/09/23 17:37 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 02/09/23 17:37 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 02/09/23 17:37 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 02/09/23 17:37 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 02/09/23 17:37 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 02/09/23 17:37 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 02/09/23 17:37 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 17:37 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 02/09/23 17:37 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 17:37 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 02/09/23 17:37 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 02/09/23 17:37 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 02/09/23 17:37 11.40 U2-Hexanone
1.00 0.560 ug/L 02/09/23 17:37 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 02/09/23 17:37 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 02/09/23 17:37 110.0 UAcetone
1.00 0.130 ug/L 02/09/23 17:37 10.475 JBenzene
1.00 0.540 ug/L 02/09/23 17:37 10.540 UBromobenzene
1.00 0.210 ug/L 02/09/23 17:37 10.210 UBromochloromethane
1.00 0.500 ug/L 02/09/23 17:37 10.500 UBromodichloromethane
5.00 0.250 ug/L 02/09/23 17:37 10.250 UBromoform
1.00 0.980 ug/L 02/09/23 17:37 10.980 UBromomethane
1.00 0.190 ug/L 02/09/23 17:37 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 02/09/23 17:37 10.150 UChlorobenzene
1.00 0.760 ug/L 02/09/23 17:37 10.760 UChloroethane
1.00 1.00 ug/L 02/09/23 17:37 11.00 UChloroform
1.00 0.320 ug/L 02/09/23 17:37 10.320 UChloromethane
1.00 0.200 ug/L 02/09/23 17:37 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 02/09/23 17:37 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 02/09/23 17:37 10.240 UDibromochloromethane
1.00 0.850 ug/L 02/09/23 17:37 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 02/09/23 17:37 10.200 UDiisopropyl ether
100 24.0 ug/L 02/09/23 17:37 124.0 UEthanol
1.00 0.500 ug/L 02/09/23 17:37 10.500 UEthylbenzene
1.00 0.530 ug/L 02/09/23 17:37 10.530 UIsopropylbenzene
1.00 0.220 ug/L 02/09/23 17:37 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 02/09/23 17:37 13.00 UMethylene Chloride
5.00 0.630 ug/L 02/09/23 17:37 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 02/09/23 17:37 13.00 UNaphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-2Client Sample ID: MW17
Matrix: WaterDate Collected: 02/01/23 13:39
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 02/09/23 17:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 02/09/23 17:37 10.690 UN-Propylbenzene
5.00 0.600 ug/L 02/09/23 17:37 10.600 Uo-Xylene
1.00 0.710 ug/L 02/09/23 17:37 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 02/09/23 17:37 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 02/09/23 17:37 11.00 UStyrene
1.00 0.630 ug/L 02/09/23 17:37 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 02/09/23 17:37 10.900 UTetrachloroethene
1.00 0.410 ug/L 02/09/23 17:37 10.410 UToluene
1.00 0.500 ug/L 02/09/23 17:37 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 02/09/23 17:37 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 02/09/23 17:37 10.150 UTrichloroethene
1.00 0.520 ug/L 02/09/23 17:37 10.520 UTrichlorofluoromethane
25.0 0.930 ug/L 02/09/23 17:37 10.930 UVinyl acetate
1.00 0.500 ug/L 02/09/23 17:37 10.500 UVinyl chloride
10.0 1.60 ug/L 02/09/23 17:37 11.60 UXylenes, Total
10.0 4.90 ug/L 02/09/23 17:37 14.90 Ut-Butyl alcohol
4-Bromofluorobenzene 100 72-119 02/09/23 17:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 97 02/09/23 17:37 175-126
Toluene-d8 (Surr)95 02/09/23 17:37 164-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-3Client Sample ID: MW20
Matrix: WaterDate Collected: 02/01/23 13:28
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
32.0 U 200 32.0 ug/L 02/08/23 18:18 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
200 36.0 ug/L 02/08/23 18:18 20036.0 U1,1,1-Trichloroethane
200 100 ug/L 02/08/23 18:18 200100U1,1,2,2-Tetrachloroethane
1000 42.0 ug/L 02/08/23 18:18 20042.0 U1,1,2-Trichloroethane
200 100 ug/L 02/08/23 18:18 200100U1,1-Dichloroethane
200 100 ug/L 02/08/23 18:18 200100U1,1-Dichloroethene
200 100 ug/L 02/08/23 18:18 200100U1,1-Dichloropropene
200 180 ug/L 02/08/23 18:18 200180U1,2,3-Trichlorobenzene
1000 168 ug/L 02/08/23 18:18 200168U1,2,3-Trichloropropane
200 164 ug/L 02/08/23 18:18 200164U1,2,4-Trichlorobenzene
200 164 ug/L 02/08/23 18:18 20023901,2,4-Trimethylbenzene
200 46.0 ug/L 02/08/23 18:18 20046.0 U1,2-Dibromoethane (EDB)
200 100 ug/L 02/08/23 18:18 200100U1,2-Dichlorobenzene
200 38.0 ug/L 02/08/23 18:18 20038.0 U1,2-Dichloroethane
200 100 ug/L 02/08/23 18:18 200100U1,2-Dichloropropane
200 112 ug/L 02/08/23 18:18 2006691,3,5-Trimethylbenzene
200 108 ug/L 02/08/23 18:18 200108U1,3-Dichlorobenzene
200 100 ug/L 02/08/23 18:18 200100U1,3-Dichloropropane
200 128 ug/L 02/08/23 18:18 200128U1,4-Dichlorobenzene
200 100 ug/L 02/08/23 18:18 200100U2,2-Dichloropropane
5000 520 ug/L 02/08/23 18:18 200743J2-Butanone (MEK)
200 114 ug/L 02/08/23 18:18 200114U2-Chlorotoluene
5000 280 ug/L 02/08/23 18:18 200280U2-Hexanone
200 112 ug/L 02/08/23 18:18 200112U4-Chlorotoluene
5000 360 ug/L 02/08/23 18:18 200360U4-Methyl-2-pentanone (MIBK)
5000 2000 ug/L 02/08/23 18:18 2002740JAcetone
200 26.0 ug/L 02/08/23 18:18 20012000Benzene
200 108 ug/L 02/08/23 18:18 200108UBromobenzene
200 42.0 ug/L 02/08/23 18:18 20042.0 UBromochloromethane
200 100 ug/L 02/08/23 18:18 200100UBromodichloromethane
1000 50.0 ug/L 02/08/23 18:18 20050.0 UBromoform
200 196 ug/L 02/08/23 18:18 200196UBromomethane
200 38.0 ug/L 02/08/23 18:18 20038.0 UCarbon tetrachloride
200 30.0 ug/L 02/08/23 18:18 20030.0 UChlorobenzene
200 152 ug/L 02/08/23 18:18 200152UChloroethane
200 200 ug/L 02/08/23 18:18 200200UChloroform
200 64.0 ug/L 02/08/23 18:18 20064.0 UChloromethane
200 40.0 ug/L 02/08/23 18:18 20040.0 Ucis-1,2-Dichloroethene
1000 100 ug/L 02/08/23 18:18 200100Ucis-1,3-Dichloropropene
200 48.0 ug/L 02/08/23 18:18 20048.0 UDibromochloromethane
200 170 ug/L 02/08/23 18:18 200170UDichlorodifluoromethane
200 40.0 ug/L 02/08/23 18:18 20078.0 JDiisopropyl ether
20000 4800 ug/L 02/08/23 18:18 2004800UEthanol
200 100 ug/L 02/08/23 18:18 2002450Ethylbenzene
200 106 ug/L 02/08/23 18:18 200106UIsopropylbenzene
200 44.0 ug/L 02/08/23 18:18 20014800Methyl tert-butyl ether
1000 600 ug/L 02/08/23 18:18 200600UMethylene Chloride
1000 126 ug/L 02/08/23 18:18 2008660m-Xylene & p-Xylene
1000 600 ug/L 02/08/23 18:18 2001170Naphthalene
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-3Client Sample ID: MW20
Matrix: WaterDate Collected: 02/01/23 13:28
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
152 U 200 152 ug/L 02/08/23 18:18 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
200 138 ug/L 02/08/23 18:18 200236N-Propylbenzene
1000 120 ug/L 02/08/23 18:18 2004810o-Xylene
200 142 ug/L 02/08/23 18:18 200142Up-Cymene (p-Isopropyltoluene)
200 140 ug/L 02/08/23 18:18 200140Usec-Butylbenzene
200 200 ug/L 02/08/23 18:18 200200UStyrene
200 126 ug/L 02/08/23 18:18 200126Utert-Butylbenzene
200 180 ug/L 02/08/23 18:18 200180UTetrachloroethene
200 82.0 ug/L 02/08/23 18:18 20031300Toluene
200 100 ug/L 02/08/23 18:18 200100Utrans-1,2-Dichloroethene
1000 40.0 ug/L 02/08/23 18:18 20040.0 Utrans-1,3-Dichloropropene
200 30.0 ug/L 02/08/23 18:18 20030.0 UTrichloroethene
200 104 ug/L 02/08/23 18:18 200104UTrichlorofluoromethane
5000 186 ug/L 02/08/23 18:18 200186UVinyl acetate
200 100 ug/L 02/08/23 18:18 200100UVinyl chloride
2000 320 ug/L 02/08/23 18:18 20013500Xylenes, Total
2000 980 ug/L 02/08/23 18:18 20023500t-Butyl alcohol
4-Bromofluorobenzene 97 72-119 02/08/23 18:18 200
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 99 02/08/23 18:18 20075-126
Toluene-d8 (Surr)95 02/08/23 18:18 20064-132
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-4Client Sample ID: MW24
Matrix: WaterDate Collected: 02/01/23 13:19
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1.60 U 10.0 1.60 ug/L 02/11/23 10:38 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
10.0 1.80 ug/L 02/11/23 10:38 101.80 U1,1,1-Trichloroethane
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,1,2,2-Tetrachloroethane
50.0 2.10 ug/L 02/11/23 10:38 102.10 U1,1,2-Trichloroethane
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,1-Dichloroethane
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,1-Dichloroethene
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,1-Dichloropropene
10.0 9.00 ug/L 02/11/23 10:38 109.00 U1,2,3-Trichlorobenzene
50.0 8.40 ug/L 02/11/23 10:38 108.40 U1,2,3-Trichloropropane
10.0 8.20 ug/L 02/11/23 10:38 108.20 U1,2,4-Trichlorobenzene
10.0 8.20 ug/L 02/11/23 10:38 1016401,2,4-Trimethylbenzene
10.0 2.30 ug/L 02/11/23 10:38 102.30 U1,2-Dibromoethane (EDB)
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,2-Dichlorobenzene
10.0 1.90 ug/L 02/11/23 10:38 101.90 U1,2-Dichloroethane
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,2-Dichloropropane
10.0 5.60 ug/L 02/11/23 10:38 104421,3,5-Trimethylbenzene
10.0 5.40 ug/L 02/11/23 10:38 105.40 U1,3-Dichlorobenzene
10.0 5.00 ug/L 02/11/23 10:38 105.00 U1,3-Dichloropropane
10.0 6.40 ug/L 02/11/23 10:38 106.40 U1,4-Dichlorobenzene
10.0 5.00 ug/L 02/11/23 10:38 105.00 U2,2-Dichloropropane
250 26.0 ug/L 02/11/23 10:38 1026.0 U2-Butanone (MEK)
10.0 5.70 ug/L 02/11/23 10:38 105.70 U2-Chlorotoluene
250 14.0 ug/L 02/11/23 10:38 1014.0 U2-Hexanone
10.0 5.60 ug/L 02/11/23 10:38 105.60 U4-Chlorotoluene
250 18.0 ug/L 02/11/23 10:38 1018.0 U4-Methyl-2-pentanone (MIBK)
250 100 ug/L 02/11/23 10:38 10100UAcetone
10.0 1.30 ug/L 02/11/23 10:38 10704Benzene
10.0 5.40 ug/L 02/11/23 10:38 105.40 UBromobenzene
10.0 2.10 ug/L 02/11/23 10:38 102.10 UBromochloromethane
10.0 5.00 ug/L 02/11/23 10:38 105.00 UBromodichloromethane
50.0 2.50 ug/L 02/11/23 10:38 102.50 UBromoform
10.0 9.80 ug/L 02/11/23 10:38 109.80 UBromomethane
10.0 1.90 ug/L 02/11/23 10:38 101.90 UCarbon tetrachloride
10.0 1.50 ug/L 02/11/23 10:38 101.50 UChlorobenzene
10.0 7.60 ug/L 02/11/23 10:38 107.60 UChloroethane
10.0 10.0 ug/L 02/11/23 10:38 1010.0 UChloroform
10.0 3.20 ug/L 02/11/23 10:38 103.20 UChloromethane
10.0 2.00 ug/L 02/11/23 10:38 102.00 Ucis-1,2-Dichloroethene
50.0 5.00 ug/L 02/11/23 10:38 105.00 Ucis-1,3-Dichloropropene
10.0 2.40 ug/L 02/11/23 10:38 102.40 UDibromochloromethane
10.0 8.50 ug/L 02/11/23 10:38 108.50 UDichlorodifluoromethane
10.0 2.00 ug/L 02/11/23 10:38 102.18 JDiisopropyl ether
1000 240 ug/L 02/11/23 10:38 10240UEthanol
10.0 5.00 ug/L 02/11/23 10:38 101220Ethylbenzene
10.0 5.30 ug/L 02/11/23 10:38 1066.9Isopropylbenzene
10.0 2.20 ug/L 02/11/23 10:38 10134Methyl tert-butyl ether
50.0 30.0 ug/L 02/11/23 10:38 1030.0 UMethylene Chloride
50.0 30.0 ug/L 02/11/23 10:38 10614Naphthalene
10.0 7.60 ug/L 02/11/23 10:38 1037.5n-Butylbenzene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-4Client Sample ID: MW24
Matrix: WaterDate Collected: 02/01/23 13:19
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
223 10.0 6.90 ug/L 02/11/23 10:38 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
N-Propylbenzene
10.0 7.10 ug/L 02/11/23 10:38 107.10 Up-Cymene (p-Isopropyltoluene)
10.0 7.00 ug/L 02/11/23 10:38 1010.5sec-Butylbenzene
10.0 10.0 ug/L 02/11/23 10:38 1010.0 UStyrene
10.0 6.30 ug/L 02/11/23 10:38 106.30 Utert-Butylbenzene
10.0 9.00 ug/L 02/11/23 10:38 109.00 UTetrachloroethene
10.0 4.10 ug/L 02/11/23 10:38 101510Toluene
10.0 5.00 ug/L 02/11/23 10:38 105.00 Utrans-1,2-Dichloroethene
50.0 2.00 ug/L 02/11/23 10:38 102.00 Utrans-1,3-Dichloropropene
10.0 1.50 ug/L 02/11/23 10:38 101.50 UTrichloroethene
10.0 5.20 ug/L 02/11/23 10:38 105.20 UTrichlorofluoromethane
250 9.30 ug/L 02/11/23 10:38 109.30 UVinyl acetate
10.0 5.00 ug/L 02/11/23 10:38 105.00 UVinyl chloride
100 49.0 ug/L 02/11/23 10:38 1049.0 Ut-Butyl alcohol
4-Bromofluorobenzene 97 72-119 02/11/23 10:38 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 98 02/11/23 10:38 1075-126
Toluene-d8 (Surr)92 02/11/23 10:38 1064-132
Method: SM6200-B - Volatile Organic Compounds - DL
RL MDL
3110 100 12.6 ug/L 02/11/23 17:45 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
m-Xylene & p-Xylene
100 12.0 ug/L 02/11/23 17:45 20677o-Xylene
200 32.0 ug/L 02/11/23 17:45 203790Xylenes, Total
4-Bromofluorobenzene 96 72-119 02/11/23 17:45 20
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 100 02/11/23 17:45 2075-126
Toluene-d8 (Surr)93 02/11/23 17:45 2064-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-5Client Sample ID: MW25
Matrix: WaterDate Collected: 02/01/23 14:14
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 02/09/23 18:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 02/09/23 18:02 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 02/09/23 18:02 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 02/09/23 18:02 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 02/09/23 18:02 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 02/09/23 18:02 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 02/09/23 18:02 113.31,2,4-Trimethylbenzene
1.00 0.230 ug/L 02/09/23 18:02 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 02/09/23 18:02 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 02/09/23 18:02 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 02/09/23 18:02 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 18:02 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 02/09/23 18:02 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 02/09/23 18:02 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 02/09/23 18:02 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 02/09/23 18:02 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 02/09/23 18:02 11.40 U2-Hexanone
1.00 0.560 ug/L 02/09/23 18:02 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 02/09/23 18:02 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 02/09/23 18:02 110.0 UAcetone
1.00 0.130 ug/L 02/09/23 18:02 11.17Benzene
1.00 0.540 ug/L 02/09/23 18:02 10.540 UBromobenzene
1.00 0.210 ug/L 02/09/23 18:02 10.210 UBromochloromethane
1.00 0.500 ug/L 02/09/23 18:02 10.500 UBromodichloromethane
5.00 0.250 ug/L 02/09/23 18:02 10.250 UBromoform
1.00 0.980 ug/L 02/09/23 18:02 10.980 UBromomethane
1.00 0.190 ug/L 02/09/23 18:02 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 02/09/23 18:02 10.150 UChlorobenzene
1.00 0.760 ug/L 02/09/23 18:02 10.760 UChloroethane
1.00 1.00 ug/L 02/09/23 18:02 11.00 UChloroform
1.00 0.320 ug/L 02/09/23 18:02 10.320 UChloromethane
1.00 0.200 ug/L 02/09/23 18:02 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 02/09/23 18:02 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 02/09/23 18:02 10.240 UDibromochloromethane
1.00 0.850 ug/L 02/09/23 18:02 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 02/09/23 18:02 10.200 UDiisopropyl ether
100 24.0 ug/L 02/09/23 18:02 124.0 UEthanol
1.00 0.500 ug/L 02/09/23 18:02 10.500 UEthylbenzene
1.00 0.530 ug/L 02/09/23 18:02 12.27Isopropylbenzene
1.00 0.220 ug/L 02/09/23 18:02 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 02/09/23 18:02 13.00 UMethylene Chloride
5.00 0.630 ug/L 02/09/23 18:02 13.39 Jm-Xylene & p-Xylene
5.00 3.00 ug/L 02/09/23 18:02 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-5Client Sample ID: MW25
Matrix: WaterDate Collected: 02/01/23 14:14
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 02/09/23 18:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 02/09/23 18:02 10.690 UN-Propylbenzene
5.00 0.600 ug/L 02/09/23 18:02 10.600 Uo-Xylene
1.00 0.710 ug/L 02/09/23 18:02 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 02/09/23 18:02 11.08sec-Butylbenzene
1.00 1.00 ug/L 02/09/23 18:02 11.00 UStyrene
1.00 0.630 ug/L 02/09/23 18:02 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 02/09/23 18:02 10.900 UTetrachloroethene
1.00 0.410 ug/L 02/09/23 18:02 10.410 UToluene
1.00 0.500 ug/L 02/09/23 18:02 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 02/09/23 18:02 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 02/09/23 18:02 10.150 UTrichloroethene
1.00 0.520 ug/L 02/09/23 18:02 10.520 UTrichlorofluoromethane
25.0 0.930 ug/L 02/09/23 18:02 10.930 UVinyl acetate
1.00 0.500 ug/L 02/09/23 18:02 10.500 UVinyl chloride
10.0 1.60 ug/L 02/09/23 18:02 13.39 JXylenes, Total
10.0 4.90 ug/L 02/09/23 18:02 14.90 Ut-Butyl alcohol
4-Bromofluorobenzene 100 72-119 02/09/23 18:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 98 02/09/23 18:02 175-126
Toluene-d8 (Surr)94 02/09/23 18:02 164-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-6Client Sample ID: MW27
Matrix: WaterDate Collected: 02/01/23 14:01
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
3.20 U 20.0 3.20 ug/L 02/09/23 18:27 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
20.0 3.60 ug/L 02/09/23 18:27 203.60 U1,1,1-Trichloroethane
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,1,2,2-Tetrachloroethane
100 4.20 ug/L 02/09/23 18:27 204.20 U1,1,2-Trichloroethane
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,1-Dichloroethane
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,1-Dichloroethene
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,1-Dichloropropene
20.0 18.0 ug/L 02/09/23 18:27 2018.0 U1,2,3-Trichlorobenzene
100 16.8 ug/L 02/09/23 18:27 2016.8 U1,2,3-Trichloropropane
20.0 16.4 ug/L 02/09/23 18:27 2016.4 U1,2,4-Trichlorobenzene
20.0 16.4 ug/L 02/09/23 18:27 2011401,2,4-Trimethylbenzene
20.0 4.60 ug/L 02/09/23 18:27 204.60 U1,2-Dibromoethane (EDB)
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,2-Dichlorobenzene
20.0 3.80 ug/L 02/09/23 18:27 203.80 U1,2-Dichloroethane
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,2-Dichloropropane
20.0 11.2 ug/L 02/09/23 18:27 203871,3,5-Trimethylbenzene
20.0 10.8 ug/L 02/09/23 18:27 2010.8 U1,3-Dichlorobenzene
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U1,3-Dichloropropane
20.0 12.8 ug/L 02/09/23 18:27 2012.8 U1,4-Dichlorobenzene
20.0 10.0 ug/L 02/09/23 18:27 2010.0 U2,2-Dichloropropane
500 52.0 ug/L 02/09/23 18:27 2052.0 U2-Butanone (MEK)
20.0 11.4 ug/L 02/09/23 18:27 2011.4 U2-Chlorotoluene
500 28.0 ug/L 02/09/23 18:27 2028.0 U2-Hexanone
20.0 11.2 ug/L 02/09/23 18:27 2011.2 U4-Chlorotoluene
500 36.0 ug/L 02/09/23 18:27 2036.0 U4-Methyl-2-pentanone (MIBK)
500 200 ug/L 02/09/23 18:27 20200UAcetone
20.0 2.60 ug/L 02/09/23 18:27 201020Benzene
20.0 10.8 ug/L 02/09/23 18:27 2010.8 UBromobenzene
20.0 4.20 ug/L 02/09/23 18:27 204.20 UBromochloromethane
20.0 10.0 ug/L 02/09/23 18:27 2010.0 UBromodichloromethane
100 5.00 ug/L 02/09/23 18:27 205.00 UBromoform
20.0 19.6 ug/L 02/09/23 18:27 2019.6 UBromomethane
20.0 3.80 ug/L 02/09/23 18:27 203.80 UCarbon tetrachloride
20.0 3.00 ug/L 02/09/23 18:27 203.00 UChlorobenzene
20.0 15.2 ug/L 02/09/23 18:27 2015.2 UChloroethane
20.0 20.0 ug/L 02/09/23 18:27 2020.0 UChloroform
20.0 6.40 ug/L 02/09/23 18:27 206.40 UChloromethane
20.0 4.00 ug/L 02/09/23 18:27 204.00 Ucis-1,2-Dichloroethene
100 10.0 ug/L 02/09/23 18:27 2010.0 Ucis-1,3-Dichloropropene
20.0 4.80 ug/L 02/09/23 18:27 204.80 UDibromochloromethane
20.0 17.0 ug/L 02/09/23 18:27 2017.0 UDichlorodifluoromethane
20.0 4.00 ug/L 02/09/23 18:27 204.00 UDiisopropyl ether
2000 480 ug/L 02/09/23 18:27 20480UEthanol
20.0 10.0 ug/L 02/09/23 18:27 201200Ethylbenzene
20.0 10.6 ug/L 02/09/23 18:27 2064.5Isopropylbenzene
20.0 4.40 ug/L 02/09/23 18:27 2077.5Methyl tert-butyl ether
100 60.0 ug/L 02/09/23 18:27 2060.0 UMethylene Chloride
100 12.6 ug/L 02/09/23 18:27 202840m-Xylene & p-Xylene
100 60.0 ug/L 02/09/23 18:27 20652Naphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-6Client Sample ID: MW27
Matrix: WaterDate Collected: 02/01/23 14:01
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
23.1 20.0 15.2 ug/L 02/09/23 18:27 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
20.0 13.8 ug/L 02/09/23 18:27 20110N-Propylbenzene
100 12.0 ug/L 02/09/23 18:27 20762o-Xylene
20.0 14.2 ug/L 02/09/23 18:27 2014.2 Up-Cymene (p-Isopropyltoluene)
20.0 14.0 ug/L 02/09/23 18:27 2014.0 Usec-Butylbenzene
20.0 20.0 ug/L 02/09/23 18:27 2020.0 UStyrene
20.0 12.6 ug/L 02/09/23 18:27 2012.6 Utert-Butylbenzene
20.0 18.0 ug/L 02/09/23 18:27 2018.0 UTetrachloroethene
20.0 8.20 ug/L 02/09/23 18:27 20199Toluene
20.0 10.0 ug/L 02/09/23 18:27 2010.0 Utrans-1,2-Dichloroethene
100 4.00 ug/L 02/09/23 18:27 204.00 Utrans-1,3-Dichloropropene
20.0 3.00 ug/L 02/09/23 18:27 203.00 UTrichloroethene
20.0 10.4 ug/L 02/09/23 18:27 2010.4 UTrichlorofluoromethane
500 18.6 ug/L 02/09/23 18:27 2018.6 UVinyl acetate
20.0 10.0 ug/L 02/09/23 18:27 2010.0 UVinyl chloride
200 32.0 ug/L 02/09/23 18:27 203600Xylenes, Total
200 98.0 ug/L 02/09/23 18:27 2098.0 Ut-Butyl alcohol
4-Bromofluorobenzene 98 72-119 02/09/23 18:27 20
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 100 02/09/23 18:27 2075-126
Toluene-d8 (Surr)95 02/09/23 18:27 2064-132
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-7Client Sample ID: MW30
Matrix: WaterDate Collected: 02/01/23 13:52
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds
RL MDL
3.20 U 20.0 3.20 ug/L 02/09/23 18:51 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
20.0 3.60 ug/L 02/09/23 18:51 203.60 U1,1,1-Trichloroethane
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,1,2,2-Tetrachloroethane
100 4.20 ug/L 02/09/23 18:51 204.20 U1,1,2-Trichloroethane
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,1-Dichloroethane
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,1-Dichloroethene
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,1-Dichloropropene
20.0 18.0 ug/L 02/09/23 18:51 2018.0 U1,2,3-Trichlorobenzene
100 16.8 ug/L 02/09/23 18:51 2016.8 U1,2,3-Trichloropropane
20.0 16.4 ug/L 02/09/23 18:51 2016.4 U1,2,4-Trichlorobenzene
20.0 16.4 ug/L 02/09/23 18:51 2011101,2,4-Trimethylbenzene
20.0 4.60 ug/L 02/09/23 18:51 204.60 U1,2-Dibromoethane (EDB)
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,2-Dichlorobenzene
20.0 3.80 ug/L 02/09/23 18:51 203.80 U1,2-Dichloroethane
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,2-Dichloropropane
20.0 11.2 ug/L 02/09/23 18:51 203021,3,5-Trimethylbenzene
20.0 10.8 ug/L 02/09/23 18:51 2010.8 U1,3-Dichlorobenzene
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U1,3-Dichloropropane
20.0 12.8 ug/L 02/09/23 18:51 2012.8 U1,4-Dichlorobenzene
20.0 10.0 ug/L 02/09/23 18:51 2010.0 U2,2-Dichloropropane
500 52.0 ug/L 02/09/23 18:51 2052.0 U2-Butanone (MEK)
20.0 11.4 ug/L 02/09/23 18:51 2011.4 U2-Chlorotoluene
500 28.0 ug/L 02/09/23 18:51 2028.0 U2-Hexanone
20.0 11.2 ug/L 02/09/23 18:51 2011.2 U4-Chlorotoluene
500 36.0 ug/L 02/09/23 18:51 2036.0 U4-Methyl-2-pentanone (MIBK)
500 200 ug/L 02/09/23 18:51 20200UAcetone
20.0 2.60 ug/L 02/09/23 18:51 20132Benzene
20.0 10.8 ug/L 02/09/23 18:51 2010.8 UBromobenzene
20.0 4.20 ug/L 02/09/23 18:51 204.20 UBromochloromethane
20.0 10.0 ug/L 02/09/23 18:51 2010.0 UBromodichloromethane
100 5.00 ug/L 02/09/23 18:51 205.00 UBromoform
20.0 19.6 ug/L 02/09/23 18:51 2019.6 UBromomethane
20.0 3.80 ug/L 02/09/23 18:51 203.80 UCarbon tetrachloride
20.0 3.00 ug/L 02/09/23 18:51 203.00 UChlorobenzene
20.0 15.2 ug/L 02/09/23 18:51 2015.2 UChloroethane
20.0 20.0 ug/L 02/09/23 18:51 2020.0 UChloroform
20.0 6.40 ug/L 02/09/23 18:51 206.40 UChloromethane
20.0 4.00 ug/L 02/09/23 18:51 204.00 Ucis-1,2-Dichloroethene
100 10.0 ug/L 02/09/23 18:51 2010.0 Ucis-1,3-Dichloropropene
20.0 4.80 ug/L 02/09/23 18:51 204.80 UDibromochloromethane
20.0 17.0 ug/L 02/09/23 18:51 2017.0 UDichlorodifluoromethane
20.0 4.00 ug/L 02/09/23 18:51 204.00 UDiisopropyl ether
2000 480 ug/L 02/09/23 18:51 20480UEthanol
20.0 10.0 ug/L 02/09/23 18:51 20661Ethylbenzene
20.0 10.6 ug/L 02/09/23 18:51 2039.7Isopropylbenzene
20.0 4.40 ug/L 02/09/23 18:51 204.40 UMethyl tert-butyl ether
100 60.0 ug/L 02/09/23 18:51 2060.0 UMethylene Chloride
100 12.6 ug/L 02/09/23 18:51 202360m-Xylene & p-Xylene
100 60.0 ug/L 02/09/23 18:51 20454Naphthalene
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Client Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Lab Sample ID: 400-232732-7Client Sample ID: MW30
Matrix: WaterDate Collected: 02/01/23 13:52
Date Received: 02/06/23 08:51
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
27.2 20.0 15.2 ug/L 02/09/23 18:51 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
20.0 13.8 ug/L 02/09/23 18:51 20123N-Propylbenzene
100 12.0 ug/L 02/09/23 18:51 201070o-Xylene
20.0 14.2 ug/L 02/09/23 18:51 2014.2 Up-Cymene (p-Isopropyltoluene)
20.0 14.0 ug/L 02/09/23 18:51 2014.0 Usec-Butylbenzene
20.0 20.0 ug/L 02/09/23 18:51 2020.0 UStyrene
20.0 12.6 ug/L 02/09/23 18:51 2012.6 Utert-Butylbenzene
20.0 18.0 ug/L 02/09/23 18:51 2018.0 UTetrachloroethene
20.0 8.20 ug/L 02/09/23 18:51 201330Toluene
20.0 10.0 ug/L 02/09/23 18:51 2010.0 Utrans-1,2-Dichloroethene
100 4.00 ug/L 02/09/23 18:51 204.00 Utrans-1,3-Dichloropropene
20.0 3.00 ug/L 02/09/23 18:51 203.00 UTrichloroethene
20.0 10.4 ug/L 02/09/23 18:51 2010.4 UTrichlorofluoromethane
500 18.6 ug/L 02/09/23 18:51 2018.6 UVinyl acetate
20.0 10.0 ug/L 02/09/23 18:51 2010.0 UVinyl chloride
200 32.0 ug/L 02/09/23 18:51 203430Xylenes, Total
200 98.0 ug/L 02/09/23 18:51 2098.0 Ut-Butyl alcohol
4-Bromofluorobenzene 97 72-119 02/09/23 18:51 20
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 98 02/09/23 18:51 2075-126
Toluene-d8 (Surr)95 02/09/23 18:51 2064-132
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Definitions/Glossary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Surrogate Summary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (72-119)(75-126)(64-132)
BFB DBFM TOL
99 97 96400-232732-1
Percent Surrogate Recovery (Acceptance Limits)
MW5
96 99 97400-232732-1 MS MW5
98 99 96400-232732-1 MSD MW5
100 97 95400-232732-2 MW17
97 99 95400-232732-3 MW20
97 98 92400-232732-4 MW24
96 100 93400-232732-4 - DL MW24
100 98 94400-232732-5 MW25
98 100 95400-232732-6 MW27
97 98 95400-232732-7 MW30
98 99 96LCS 400-611533/1003 Lab Control Sample
99 97 96LCS 400-611700/1003 Lab Control Sample
96 99 93LCS 400-612025/1002 Lab Control Sample
101 98 96MB 400-611533/5 Method Blank
100 97 95MB 400-611700/5 Method Blank
99 99 94MB 400-612025/4 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Eurofins Pensacola
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QC Association Summary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
GC/MS VOA
Analysis Batch: 611533
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232732-3 MW20 Total/NA
Water SM6200-BMB 400-611533/5 Method Blank Total/NA
Water SM6200-BLCS 400-611533/1003 Lab Control Sample Total/NA
Analysis Batch: 611700
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232732-1 MW5 Total/NA
Water SM6200-B400-232732-2 MW17 Total/NA
Water SM6200-B400-232732-5 MW25 Total/NA
Water SM6200-B400-232732-6 MW27 Total/NA
Water SM6200-B400-232732-7 MW30 Total/NA
Water SM6200-BMB 400-611700/5 Method Blank Total/NA
Water SM6200-BLCS 400-611700/1003 Lab Control Sample Total/NA
Water SM6200-B400-232732-1 MS MW5 Total/NA
Water SM6200-B400-232732-1 MSD MW5 Total/NA
Analysis Batch: 612025
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232732-4 MW24 Total/NA
Water SM6200-B400-232732-4 - DL MW24 Total/NA
Water SM6200-BMB 400-612025/4 Method Blank Total/NA
Water SM6200-BLCS 400-612025/1002 Lab Control Sample Total/NA
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 400-611533/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611533
RL MDL
1,1,1,2-Tetrachloroethane 0.160 U 1.00 0.160 ug/L 02/08/23 09:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.180 U 0.1801.00 ug/L 02/08/23 09:16 11,1,1-Trichloroethane
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,1,2,2-Tetrachloroethane
0.210 U 0.2105.00 ug/L 02/08/23 09:16 11,1,2-Trichloroethane
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,1-Dichloroethane
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,1-Dichloroethene
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,1-Dichloropropene
0.900 U 0.9001.00 ug/L 02/08/23 09:16 11,2,3-Trichlorobenzene
0.840 U 0.8405.00 ug/L 02/08/23 09:16 11,2,3-Trichloropropane
0.820 U 0.8201.00 ug/L 02/08/23 09:16 11,2,4-Trichlorobenzene
0.820 U 0.8201.00 ug/L 02/08/23 09:16 11,2,4-Trimethylbenzene
0.230 U 0.2301.00 ug/L 02/08/23 09:16 11,2-Dibromoethane (EDB)
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,2-Dichlorobenzene
0.190 U 0.1901.00 ug/L 02/08/23 09:16 11,2-Dichloroethane
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,2-Dichloropropane
0.560 U 0.5601.00 ug/L 02/08/23 09:16 11,3,5-Trimethylbenzene
0.540 U 0.5401.00 ug/L 02/08/23 09:16 11,3-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/08/23 09:16 11,3-Dichloropropane
0.640 U 0.6401.00 ug/L 02/08/23 09:16 11,4-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/08/23 09:16 12,2-Dichloropropane
2.60 U 2.6025.0 ug/L 02/08/23 09:16 12-Butanone (MEK)
0.570 U 0.5701.00 ug/L 02/08/23 09:16 12-Chlorotoluene
1.40 U 1.4025.0 ug/L 02/08/23 09:16 12-Hexanone
0.560 U 0.5601.00 ug/L 02/08/23 09:16 14-Chlorotoluene
1.80 U 1.8025.0 ug/L 02/08/23 09:16 14-Methyl-2-pentanone (MIBK)
10.0 U 10.025.0 ug/L 02/08/23 09:16 1Acetone
0.130 U 0.1301.00 ug/L 02/08/23 09:16 1Benzene
0.540 U 0.5401.00 ug/L 02/08/23 09:16 1Bromobenzene
0.210 U 0.2101.00 ug/L 02/08/23 09:16 1Bromochloromethane
0.500 U 0.5001.00 ug/L 02/08/23 09:16 1Bromodichloromethane
0.250 U 0.2505.00 ug/L 02/08/23 09:16 1Bromoform
0.980 U 0.9801.00 ug/L 02/08/23 09:16 1Bromomethane
0.190 U 0.1901.00 ug/L 02/08/23 09:16 1Carbon tetrachloride
0.150 U 0.1501.00 ug/L 02/08/23 09:16 1Chlorobenzene
0.760 U 0.7601.00 ug/L 02/08/23 09:16 1Chloroethane
1.00 U 1.001.00 ug/L 02/08/23 09:16 1Chloroform
0.320 U 0.3201.00 ug/L 02/08/23 09:16 1Chloromethane
0.200 U 0.2001.00 ug/L 02/08/23 09:16 1cis-1,2-Dichloroethene
0.500 U 0.5005.00 ug/L 02/08/23 09:16 1cis-1,3-Dichloropropene
0.240 U 0.2401.00 ug/L 02/08/23 09:16 1Dibromochloromethane
0.850 U 0.8501.00 ug/L 02/08/23 09:16 1Dichlorodifluoromethane
0.200 U 0.2001.00 ug/L 02/08/23 09:16 1Diisopropyl ether
24.0 U 24.0100 ug/L 02/08/23 09:16 1Ethanol
0.500 U 0.5001.00 ug/L 02/08/23 09:16 1Ethylbenzene
0.530 U 0.5301.00 ug/L 02/08/23 09:16 1Isopropylbenzene
0.220 U 0.2201.00 ug/L 02/08/23 09:16 1Methyl tert-butyl ether
3.00 U 3.005.00 ug/L 02/08/23 09:16 1Methylene Chloride
0.630 U 0.6305.00 ug/L 02/08/23 09:16 1m-Xylene & p-Xylene
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-611533/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611533
RL MDL
Naphthalene 3.00 U 5.00 3.00 ug/L 02/08/23 09:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.760 U 0.7601.00 ug/L 02/08/23 09:16 1n-Butylbenzene
0.690 U 0.6901.00 ug/L 02/08/23 09:16 1N-Propylbenzene
0.600 U 0.6005.00 ug/L 02/08/23 09:16 1o-Xylene
0.710 U 0.7101.00 ug/L 02/08/23 09:16 1p-Cymene (p-Isopropyltoluene)
0.700 U 0.7001.00 ug/L 02/08/23 09:16 1sec-Butylbenzene
1.00 U 1.001.00 ug/L 02/08/23 09:16 1Styrene
0.630 U 0.6301.00 ug/L 02/08/23 09:16 1tert-Butylbenzene
0.900 U 0.9001.00 ug/L 02/08/23 09:16 1Tetrachloroethene
0.410 U 0.4101.00 ug/L 02/08/23 09:16 1Toluene
0.500 U 0.5001.00 ug/L 02/08/23 09:16 1trans-1,2-Dichloroethene
0.200 U 0.2005.00 ug/L 02/08/23 09:16 1trans-1,3-Dichloropropene
0.150 U 0.1501.00 ug/L 02/08/23 09:16 1Trichloroethene
0.520 U 0.5201.00 ug/L 02/08/23 09:16 1Trichlorofluoromethane
0.930 U 0.93025.0 ug/L 02/08/23 09:16 1Vinyl acetate
0.500 U 0.5001.00 ug/L 02/08/23 09:16 1Vinyl chloride
1.60 U 1.6010.0 ug/L 02/08/23 09:16 1Xylenes, Total
4.90 U 4.9010.0 ug/L 02/08/23 09:16 1t-Butyl alcohol
4-Bromofluorobenzene 101 72-119 02/08/23 09:16 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 02/08/23 09:16 1Dibromofluoromethane75-126
96 02/08/23 09:16 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611533/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611533
1,1,1,2-Tetrachloroethane 50.0 42.21 ug/L 84 67 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 40.03 ug/L 80 68 -130
1,1,2,2-Tetrachloroethane 50.0 43.99 ug/L 88 70 -131
1,1,2-Trichloroethane 50.0 43.07 ug/L 86 70 -130
1,1-Dichloroethane 50.0 43.53 ug/L 87 70 -130
1,1-Dichloroethene 50.0 43.65 ug/L 87 63 -134
1,1-Dichloropropene 50.0 42.64 ug/L 85 70 -130
1,2,3-Trichlorobenzene 50.0 48.51 ug/L 97 60 -138
1,2,3-Trichloropropane 50.0 42.60 ug/L 85 70 -130
1,2,4-Trichlorobenzene 50.0 46.68 ug/L 93 60 -140
1,2,4-Trimethylbenzene 50.0 41.42 ug/L 83 70 -130
1,2-Dibromoethane (EDB)50.0 44.85 ug/L 90 70 -130
1,2-Dichlorobenzene 50.0 42.98 ug/L 86 67 -130
1,2-Dichloroethane 50.0 39.89 ug/L 80 69 -130
1,2-Dichloropropane 50.0 44.10 ug/L 88 70 -130
1,3,5-Trimethylbenzene 50.0 40.38 ug/L 81 69 -130
1,3-Dichlorobenzene 50.0 42.88 ug/L 86 70 -130
1,3-Dichloropropane 50.0 44.52 ug/L 89 70 -130
1,4-Dichlorobenzene 50.0 42.70 ug/L 85 70 -130
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611533/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611533
2,2-Dichloropropane 50.0 43.24 ug/L 86 52 -135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Butanone (MEK)200 171.2 ug/L 86 61 -145
2-Chlorotoluene 50.0 40.37 ug/L 81 70 -130
2-Hexanone 200 171.1 ug/L 86 65 -137
4-Chlorotoluene 50.0 39.43 ug/L 79 70 -130
4-Methyl-2-pentanone (MIBK)200 182.1 ug/L 91 69 -138
Acetone 200 155.2 ug/L 78 43 -160
Benzene 50.0 43.86 ug/L 88 70 -130
Bromobenzene 50.0 41.64 ug/L 83 70 -132
Bromochloromethane 50.0 45.69 ug/L 91 70 -130
Bromodichloromethane 50.0 42.76 ug/L 86 67 -133
Bromoform 50.0 43.98 ug/L 88 57 -140
Bromomethane 50.0 45.11 ug/L 90 10 -160
Carbon tetrachloride 50.0 40.27 ug/L 81 61 -137
Chlorobenzene 50.0 42.41 ug/L 85 70 -130
Chloroethane 50.0 38.27 ug/L 77 55 -141
Chloroform 50.0 42.27 ug/L 85 69 -130
Chloromethane 50.0 36.20 ug/L 72 58 -137
cis-1,2-Dichloroethene 50.0 41.91 ug/L 84 68 -130
cis-1,3-Dichloropropene 50.0 45.18 ug/L 90 69 -132
Dibromochloromethane 50.0 42.61 ug/L 85 67 -135
Dichlorodifluoromethane 50.0 36.92 ug/L 74 41 -146
Diisopropyl ether 50.0 42.66 ug/L 85 64 -132
Ethanol 2000 966.8 ug/L 48 20 -160
Ethylbenzene 50.0 40.36 ug/L 81 70 -130
Isopropylbenzene 50.0 40.11 ug/L 80 70 -130
Methyl tert-butyl ether 50.0 45.12 ug/L 90 66 -130
Methylene Chloride 50.0 45.09 ug/L 90 66 -135
m-Xylene & p-Xylene 50.0 40.46 ug/L 81 70 -130
Naphthalene 50.0 54.20 ug/L 108 47 -149
n-Butylbenzene 50.0 40.48 ug/L 81 67 -130
N-Propylbenzene 50.0 40.68 ug/L 81 70 -130
o-Xylene 50.0 40.58 ug/L 81 70 -130
p-Cymene (p-Isopropyltoluene)50.0 40.23 ug/L 80 65 -130
sec-Butylbenzene 50.0 40.00 ug/L 80 66 -130
Styrene 50.0 41.18 ug/L 82 70 -130
tert-Butylbenzene 50.0 43.64 ug/L 87 64 -139
Tetrachloroethene 50.0 43.93 ug/L 88 65 -130
Toluene 50.0 41.47 ug/L 83 70 -130
trans-1,2-Dichloroethene 50.0 41.89 ug/L 84 70 -130
trans-1,3-Dichloropropene 50.0 42.35 ug/L 85 63 -130
Trichloroethene 50.0 44.60 ug/L 89 70 -130
Trichlorofluoromethane 50.0 41.96 ug/L 84 65 -138
Vinyl acetate 100 88.26 ug/L 88 26 -160
Vinyl chloride 50.0 42.23 ug/L 84 59 -136
Xylenes, Total 100 81.04 ug/L 81 70 -130
t-Butyl alcohol 500 326.5 ug/L 65 46 -143
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611533/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611533
4-Bromofluorobenzene 72 -119
Surrogate
98
LCS LCS
Qualifier Limits%Recovery
99Dibromofluoromethane 75 -126
96Toluene-d8 (Surr)64 -132
Client Sample ID: Method BlankLab Sample ID: MB 400-611700/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
RL MDL
1,1,1,2-Tetrachloroethane 0.160 U 1.00 0.160 ug/L 02/09/23 09:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.180 U 0.1801.00 ug/L 02/09/23 09:49 11,1,1-Trichloroethane
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,1,2,2-Tetrachloroethane
0.210 U 0.2105.00 ug/L 02/09/23 09:49 11,1,2-Trichloroethane
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,1-Dichloroethane
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,1-Dichloroethene
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,1-Dichloropropene
0.900 U 0.9001.00 ug/L 02/09/23 09:49 11,2,3-Trichlorobenzene
0.840 U 0.8405.00 ug/L 02/09/23 09:49 11,2,3-Trichloropropane
0.820 U 0.8201.00 ug/L 02/09/23 09:49 11,2,4-Trichlorobenzene
0.820 U 0.8201.00 ug/L 02/09/23 09:49 11,2,4-Trimethylbenzene
0.230 U 0.2301.00 ug/L 02/09/23 09:49 11,2-Dibromoethane (EDB)
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,2-Dichlorobenzene
0.190 U 0.1901.00 ug/L 02/09/23 09:49 11,2-Dichloroethane
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,2-Dichloropropane
0.560 U 0.5601.00 ug/L 02/09/23 09:49 11,3,5-Trimethylbenzene
0.540 U 0.5401.00 ug/L 02/09/23 09:49 11,3-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/09/23 09:49 11,3-Dichloropropane
0.640 U 0.6401.00 ug/L 02/09/23 09:49 11,4-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/09/23 09:49 12,2-Dichloropropane
2.60 U 2.6025.0 ug/L 02/09/23 09:49 12-Butanone (MEK)
0.570 U 0.5701.00 ug/L 02/09/23 09:49 12-Chlorotoluene
1.40 U 1.4025.0 ug/L 02/09/23 09:49 12-Hexanone
0.560 U 0.5601.00 ug/L 02/09/23 09:49 14-Chlorotoluene
1.80 U 1.8025.0 ug/L 02/09/23 09:49 14-Methyl-2-pentanone (MIBK)
10.0 U 10.025.0 ug/L 02/09/23 09:49 1Acetone
0.130 U 0.1301.00 ug/L 02/09/23 09:49 1Benzene
0.540 U 0.5401.00 ug/L 02/09/23 09:49 1Bromobenzene
0.210 U 0.2101.00 ug/L 02/09/23 09:49 1Bromochloromethane
0.500 U 0.5001.00 ug/L 02/09/23 09:49 1Bromodichloromethane
0.250 U 0.2505.00 ug/L 02/09/23 09:49 1Bromoform
0.980 U 0.9801.00 ug/L 02/09/23 09:49 1Bromomethane
0.190 U 0.1901.00 ug/L 02/09/23 09:49 1Carbon tetrachloride
0.150 U 0.1501.00 ug/L 02/09/23 09:49 1Chlorobenzene
0.760 U 0.7601.00 ug/L 02/09/23 09:49 1Chloroethane
1.00 U 1.001.00 ug/L 02/09/23 09:49 1Chloroform
0.320 U 0.3201.00 ug/L 02/09/23 09:49 1Chloromethane
0.200 U 0.2001.00 ug/L 02/09/23 09:49 1cis-1,2-Dichloroethene
0.500 U 0.5005.00 ug/L 02/09/23 09:49 1cis-1,3-Dichloropropene
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-611700/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
RL MDL
Dibromochloromethane 0.240 U 1.00 0.240 ug/L 02/09/23 09:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.850 U 0.8501.00 ug/L 02/09/23 09:49 1Dichlorodifluoromethane
0.200 U 0.2001.00 ug/L 02/09/23 09:49 1Diisopropyl ether
24.0 U 24.0100 ug/L 02/09/23 09:49 1Ethanol
0.500 U 0.5001.00 ug/L 02/09/23 09:49 1Ethylbenzene
0.530 U 0.5301.00 ug/L 02/09/23 09:49 1Isopropylbenzene
0.220 U 0.2201.00 ug/L 02/09/23 09:49 1Methyl tert-butyl ether
3.00 U 3.005.00 ug/L 02/09/23 09:49 1Methylene Chloride
0.630 U 0.6305.00 ug/L 02/09/23 09:49 1m-Xylene & p-Xylene
3.00 U 3.005.00 ug/L 02/09/23 09:49 1Naphthalene
0.760 U 0.7601.00 ug/L 02/09/23 09:49 1n-Butylbenzene
0.690 U 0.6901.00 ug/L 02/09/23 09:49 1N-Propylbenzene
0.600 U 0.6005.00 ug/L 02/09/23 09:49 1o-Xylene
0.710 U 0.7101.00 ug/L 02/09/23 09:49 1p-Cymene (p-Isopropyltoluene)
0.700 U 0.7001.00 ug/L 02/09/23 09:49 1sec-Butylbenzene
1.00 U 1.001.00 ug/L 02/09/23 09:49 1Styrene
0.630 U 0.6301.00 ug/L 02/09/23 09:49 1tert-Butylbenzene
0.900 U 0.9001.00 ug/L 02/09/23 09:49 1Tetrachloroethene
0.410 U 0.4101.00 ug/L 02/09/23 09:49 1Toluene
0.500 U 0.5001.00 ug/L 02/09/23 09:49 1trans-1,2-Dichloroethene
0.200 U 0.2005.00 ug/L 02/09/23 09:49 1trans-1,3-Dichloropropene
0.150 U 0.1501.00 ug/L 02/09/23 09:49 1Trichloroethene
0.520 U 0.5201.00 ug/L 02/09/23 09:49 1Trichlorofluoromethane
0.930 U 0.93025.0 ug/L 02/09/23 09:49 1Vinyl acetate
0.500 U 0.5001.00 ug/L 02/09/23 09:49 1Vinyl chloride
1.60 U 1.6010.0 ug/L 02/09/23 09:49 1Xylenes, Total
4.90 U 4.9010.0 ug/L 02/09/23 09:49 1t-Butyl alcohol
4-Bromofluorobenzene 100 72-119 02/09/23 09:49 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
97 02/09/23 09:49 1Dibromofluoromethane75-126
95 02/09/23 09:49 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611700/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
1,1,1,2-Tetrachloroethane 50.0 42.26 ug/L 85 67 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 39.90 ug/L 80 68 -130
1,1,2,2-Tetrachloroethane 50.0 41.68 ug/L 83 70 -131
1,1,2-Trichloroethane 50.0 41.90 ug/L 84 70 -130
1,1-Dichloroethane 50.0 42.43 ug/L 85 70 -130
1,1-Dichloroethene 50.0 43.20 ug/L 86 63 -134
1,1-Dichloropropene 50.0 43.23 ug/L 86 70 -130
1,2,3-Trichlorobenzene 50.0 51.31 ug/L 103 60 -138
1,2,3-Trichloropropane 50.0 39.87 ug/L 80 70 -130
1,2,4-Trichlorobenzene 50.0 50.53 ug/L 101 60 -140
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611700/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
1,2,4-Trimethylbenzene 50.0 43.75 ug/L 87 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dibromoethane (EDB)50.0 42.88 ug/L 86 70 -130
1,2-Dichlorobenzene 50.0 44.99 ug/L 90 67 -130
1,2-Dichloroethane 50.0 39.52 ug/L 79 69 -130
1,2-Dichloropropane 50.0 42.60 ug/L 85 70 -130
1,3,5-Trimethylbenzene 50.0 42.54 ug/L 85 69 -130
1,3-Dichlorobenzene 50.0 45.36 ug/L 91 70 -130
1,3-Dichloropropane 50.0 43.01 ug/L 86 70 -130
1,4-Dichlorobenzene 50.0 45.33 ug/L 91 70 -130
2,2-Dichloropropane 50.0 43.06 ug/L 86 52 -135
2-Butanone (MEK)200 149.1 ug/L 75 61 -145
2-Chlorotoluene 50.0 43.15 ug/L 86 70 -130
2-Hexanone 200 152.9 ug/L 76 65 -137
4-Chlorotoluene 50.0 41.78 ug/L 84 70 -130
4-Methyl-2-pentanone (MIBK)200 169.1 ug/L 85 69 -138
Acetone 200 133.9 ug/L 67 43 -160
Benzene 50.0 43.72 ug/L 87 70 -130
Bromobenzene 50.0 43.49 ug/L 87 70 -132
Bromochloromethane 50.0 44.73 ug/L 89 70 -130
Bromodichloromethane 50.0 42.49 ug/L 85 67 -133
Bromoform 50.0 42.58 ug/L 85 57 -140
Bromomethane 50.0 57.10 ug/L 114 10 -160
Carbon tetrachloride 50.0 40.63 ug/L 81 61 -137
Chlorobenzene 50.0 42.50 ug/L 85 70 -130
Chloroethane 50.0 47.12 ug/L 94 55 -141
Chloroform 50.0 41.11 ug/L 82 69 -130
Chloromethane 50.0 45.82 ug/L 92 58 -137
cis-1,2-Dichloroethene 50.0 40.67 ug/L 81 68 -130
cis-1,3-Dichloropropene 50.0 45.03 ug/L 90 69 -132
Dibromochloromethane 50.0 41.61 ug/L 83 67 -135
Dichlorodifluoromethane 50.0 44.23 ug/L 88 41 -146
Diisopropyl ether 50.0 50.19 ug/L 100 64 -132
Ethanol 2000 813.5 ug/L 41 20 -160
Ethylbenzene 50.0 41.27 ug/L 83 70 -130
Isopropylbenzene 50.0 41.17 ug/L 82 70 -130
Methyl tert-butyl ether 50.0 44.32 ug/L 89 66 -130
Methylene Chloride 50.0 44.10 ug/L 88 66 -135
m-Xylene & p-Xylene 50.0 41.11 ug/L 82 70 -130
Naphthalene 50.0 52.94 ug/L 106 47 -149
n-Butylbenzene 50.0 46.10 ug/L 92 67 -130
N-Propylbenzene 50.0 43.02 ug/L 86 70 -130
o-Xylene 50.0 41.37 ug/L 83 70 -130
p-Cymene (p-Isopropyltoluene)50.0 43.58 ug/L 87 65 -130
sec-Butylbenzene 50.0 42.45 ug/L 85 66 -130
Styrene 50.0 41.91 ug/L 84 70 -130
tert-Butylbenzene 50.0 46.05 ug/L 92 64 -139
Tetrachloroethene 50.0 44.02 ug/L 88 65 -130
Toluene 50.0 41.75 ug/L 84 70 -130
trans-1,2-Dichloroethene 50.0 44.04 ug/L 88 70 -130
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-611700/1003
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
trans-1,3-Dichloropropene 50.0 41.81 ug/L 84 63 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Trichloroethene 50.0 44.45 ug/L 89 70 -130
Trichlorofluoromethane 50.0 49.88 ug/L 100 65 -138
Vinyl acetate 100 107.1 ug/L 107 26 -160
Vinyl chloride 50.0 50.34 ug/L 101 59 -136
Xylenes, Total 100 82.49 ug/L 82 70 -130
t-Butyl alcohol 500 264.0 ug/L 53 46 -143
4-Bromofluorobenzene 72 -119
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
97Dibromofluoromethane 75 -126
96Toluene-d8 (Surr)64 -132
Client Sample ID: MW5Lab Sample ID: 400-232732-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
1,1,1,2-Tetrachloroethane 0.160 U 50.0 36.17 ug/L 72 59 -137
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,1-Trichloroethane 0.180 U 50.0 36.13 ug/L 72 57 -142
1,1,2,2-Tetrachloroethane 0.500 U 50.0 36.35 ug/L 73 66 -135
1,1,2-Trichloroethane 0.210 U 50.0 37.09 ug/L 74 66 -131
1,1-Dichloroethane 0.500 U 50.0 38.16 ug/L 76 61 -144
1,1-Dichloroethene 0.500 U 50.0 39.45 ug/L 79 54 -147
1,1-Dichloropropene 0.500 U 50.0 37.04 ug/L 74 65 -136
1,2,3-Trichlorobenzene 0.900 U 50.0 40.04 ug/L 80 43 -145
1,2,3-Trichloropropane 0.840 U 50.0 35.58 ug/L 71 65 -133
1,2,4-Trichlorobenzene 0.820 U 50.0 38.20 ug/L 76 39 -148
1,2,4-Trimethylbenzene 4.77 50.0 35.76 ug/L 62 50 -139
1,2-Dibromoethane (EDB)0.230 U 50.0 37.59 ug/L 75 64 -132
1,2-Dichlorobenzene 0.500 U 50.0 34.10 ug/L 68 52 -137
1,2-Dichloroethane 0.190 U 50.0 34.92 ug/L 70 60 -141
1,2-Dichloropropane 0.500 U 50.0 37.81 ug/L 76 66 -137
1,3,5-Trimethylbenzene 1.65 50.0 32.06 ug/L 61 52 -135
1,3-Dichlorobenzene 0.540 U 50.0 33.39 ug/L 67 54 -135
1,3-Dichloropropane 0.500 U 50.0 37.80 ug/L 76 66 -133
1,4-Dichlorobenzene 0.640 U 50.0 32.90 ug/L 66 53 -135
2,2-Dichloropropane 0.500 U 50.0 38.44 ug/L 77 42 -144
2-Butanone (MEK)2.60 U 200 146.9 ug/L 73 55 -150
2-Chlorotoluene 0.570 U 50.0 31.09 ug/L 62 53 -134
2-Hexanone 1.40 U 200 143.5 ug/L 72 65 -140
4-Chlorotoluene 0.560 U 50.0 30.42 ug/L 61 54 -133
4-Methyl-2-pentanone (MIBK)1.80 U 200 157.8 ug/L 79 63 -146
Acetone 10.0 U 200 124.8 ug/L 62 43 -150
Benzene 0.712 J 50.0 39.36 ug/L 77 56 -142
Bromobenzene 0.540 U 50.0 33.79 ug/L 68 59 -136
Bromochloromethane 0.210 U 50.0 39.81 ug/L 80 64 -140
Bromodichloromethane 0.500 U 50.0 35.69 ug/L 71 59 -143
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: MW5Lab Sample ID: 400-232732-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
Bromoform 0.250 U 50.0 35.72 ug/L 71 50 -140
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Bromomethane 0.980 U 50.0 53.07 ug/L 106 10 -150
Carbon tetrachloride 0.190 U 50.0 36.10 ug/L 72 55 -145
Chlorobenzene 0.150 U 50.0 34.44 ug/L 69 64 -130
Chloroethane 0.760 U 50.0 43.14 ug/L 86 50 -150
Chloroform 1.00 U 50.0 37.10 ug/L 74 60 -141
Chloromethane 0.320 U 50.0 40.25 ug/L 80 49 -148
cis-1,2-Dichloroethene 0.200 U 50.0 36.80 ug/L 74 59 -143
cis-1,3-Dichloropropene 0.500 U 50.0 38.78 ug/L 78 57 -140
Dibromochloromethane 0.240 U 50.0 36.30 ug/L 73 56 -143
Dichlorodifluoromethane 0.850 U 50.0 41.21 ug/L 82 16 -150
Diisopropyl ether 0.200 U 50.0 43.12 ug/L 86 60 -144
Ethanol 24.0 U 2000 784.6 ug/L 39 10 -150
Ethylbenzene 1.03 50.0 33.22 ug/L 64 58 -131
Isopropylbenzene 0.530 U 50.0 31.39 ug/L 63 56 -133
Methyl tert-butyl ether 0.220 U 50.0 39.11 ug/L 78 59 -137
Methylene Chloride 3.00 U 50.0 40.74 ug/L 81 60 -146
m-Xylene & p-Xylene 6.72 50.0 38.49 ug/L 64 57 -130
Naphthalene 5.43 50.0 52.23 ug/L 94 25 -150
n-Butylbenzene 0.760 U F2 50.0 29.86 ug/L 60 41 -142
N-Propylbenzene 0.690 U 50.0 30.98 ug/L 62 51 -138
o-Xylene 2.61 J 50.0 35.20 ug/L 65 61 -130
p-Cymene (p-Isopropyltoluene)0.710 U 50.0 29.36 ug/L 59 48 -139
sec-Butylbenzene 0.700 U 50.0 29.55 ug/L 59 50 -138
Styrene 1.00 U 50.0 32.93 ug/L 66 58 -131
tert-Butylbenzene 0.630 U 50.0 33.56 ug/L 67 54 -146
Tetrachloroethene 0.900 U 50.0 34.73 ug/L 69 52 -133
Toluene 0.986 J 50.0 35.51 ug/L 69 65 -130
trans-1,2-Dichloroethene 0.500 U 50.0 36.34 ug/L 73 61 -143
trans-1,3-Dichloropropene 0.200 U 50.0 35.66 ug/L 71 53 -133
Trichloroethene 0.150 U 50.0 38.65 ug/L 77 64 -136
Trichlorofluoromethane 0.520 U 50.0 43.97 ug/L 88 54 -150
Vinyl acetate 0.930 U 100 100.2 ug/L 100 26 -150
Vinyl chloride 0.500 U 50.0 46.10 ug/L 92 46 -150
Xylenes, Total 9.34 J 100 73.69 ug/L 64 59 -130
t-Butyl alcohol 4.90 U 500 317.3 ug/L 63 31 -150
4-Bromofluorobenzene 72 -119
Surrogate
96
MS MS
Qualifier Limits%Recovery
99Dibromofluoromethane 75 -126
97Toluene-d8 (Surr)64 -132
Client Sample ID: MW5Lab Sample ID: 400-232732-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
1,1,1,2-Tetrachloroethane 0.160 U 50.0 40.49 ug/L 81 59 -137 11 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: MW5Lab Sample ID: 400-232732-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
1,1,1-Trichloroethane 0.180 U 50.0 39.06 ug/L 78 57 -142 8 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 0.500 U 50.0 41.57 ug/L 83 66 -135 13 30
1,1,2-Trichloroethane 0.210 U 50.0 41.91 ug/L 84 66 -131 12 30
1,1-Dichloroethane 0.500 U 50.0 41.69 ug/L 83 61 -144 9 30
1,1-Dichloroethene 0.500 U 50.0 43.54 ug/L 87 54 -147 10 30
1,1-Dichloropropene 0.500 U 50.0 41.21 ug/L 82 65 -136 11 30
1,2,3-Trichlorobenzene 0.900 U 50.0 49.96 ug/L 100 43 -145 22 30
1,2,3-Trichloropropane 0.840 U 50.0 41.42 ug/L 83 65 -133 15 30
1,2,4-Trichlorobenzene 0.820 U 50.0 46.91 ug/L 94 39 -148 20 30
1,2,4-Trimethylbenzene 4.77 50.0 45.32 ug/L 81 50 -139 24 30
1,2-Dibromoethane (EDB)0.230 U 50.0 42.73 ug/L 85 64 -132 13 30
1,2-Dichlorobenzene 0.500 U 50.0 41.84 ug/L 84 52 -137 20 30
1,2-Dichloroethane 0.190 U 50.0 38.38 ug/L 77 60 -141 9 30
1,2-Dichloropropane 0.500 U 50.0 42.12 ug/L 84 66 -137 11 30
1,3,5-Trimethylbenzene 1.65 50.0 41.41 ug/L 80 52 -135 25 30
1,3-Dichlorobenzene 0.540 U 50.0 42.00 ug/L 84 54 -135 23 30
1,3-Dichloropropane 0.500 U 50.0 42.23 ug/L 84 66 -133 11 30
1,4-Dichlorobenzene 0.640 U 50.0 41.84 ug/L 84 53 -135 24 30
2,2-Dichloropropane 0.500 U 50.0 40.46 ug/L 81 42 -144 5 31
2-Butanone (MEK)2.60 U 200 162.6 ug/L 81 55 -150 10 30
2-Chlorotoluene 0.570 U 50.0 38.99 ug/L 78 53 -134 23 30
2-Hexanone 1.40 U 200 161.9 ug/L 81 65 -140 12 30
4-Chlorotoluene 0.560 U 50.0 38.96 ug/L 78 54 -133 25 30
4-Methyl-2-pentanone (MIBK)1.80 U 200 180.4 ug/L 90 63 -146 13 30
Acetone 10.0 U 200 134.2 ug/L 67 43 -150 7 30
Benzene 0.712 J 50.0 43.28 ug/L 85 56 -142 10 30
Bromobenzene 0.540 U 50.0 40.41 ug/L 81 59 -136 18 30
Bromochloromethane 0.210 U 50.0 44.26 ug/L 89 64 -140 11 30
Bromodichloromethane 0.500 U 50.0 40.65 ug/L 81 59 -143 13 30
Bromoform 0.250 U 50.0 41.75 ug/L 83 50 -140 16 30
Bromomethane 0.980 U 50.0 48.23 ug/L 96 10 -150 10 50
Carbon tetrachloride 0.190 U 50.0 39.31 ug/L 79 55 -145 9 30
Chlorobenzene 0.150 U 50.0 40.66 ug/L 81 64 -130 17 30
Chloroethane 0.760 U 50.0 38.50 ug/L 77 50 -150 11 30
Chloroform 1.00 U 50.0 40.47 ug/L 81 60 -141 9 30
Chloromethane 0.320 U 50.0 38.10 ug/L 76 49 -148 5 31
cis-1,2-Dichloroethene 0.200 U 50.0 40.46 ug/L 81 59 -143 9 30
cis-1,3-Dichloropropene 0.500 U 50.0 43.70 ug/L 87 57 -140 12 30
Dibromochloromethane 0.240 U 50.0 40.80 ug/L 82 56 -143 12 30
Dichlorodifluoromethane 0.850 U 50.0 32.83 ug/L 66 16 -150 23 31
Diisopropyl ether 0.200 U 50.0 45.50 ug/L 91 60 -144 5 30
Ethanol 24.0 U 2000 754.7 ug/L 38 10 -150 4 40
Ethylbenzene 1.03 50.0 39.80 ug/L 78 58 -131 18 30
Isopropylbenzene 0.530 U 50.0 39.15 ug/L 78 56 -133 22 30
Methyl tert-butyl ether 0.220 U 50.0 42.94 ug/L 86 59 -137 9 30
Methylene Chloride 3.00 U 50.0 43.55 ug/L 87 60 -146 7 32
m-Xylene & p-Xylene 6.72 50.0 46.33 ug/L 79 57 -130 18 30
Naphthalene 5.43 50.0 60.48 ug/L 110 25 -150 15 30
n-Butylbenzene 0.760 U F2 50.0 41.39 F2 ug/L 83 41 -142 32 31
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: MW5Lab Sample ID: 400-232732-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 611700
N-Propylbenzene 0.690 U 50.0 40.22 ug/L 80 51 -138 26 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
o-Xylene 2.61 J 50.0 42.17 ug/L 79 61 -130 18 30
p-Cymene (p-Isopropyltoluene)0.710 U 50.0 39.88 ug/L 80 48 -139 30 30
sec-Butylbenzene 0.700 U 50.0 39.66 ug/L 79 50 -138 29 30
Styrene 1.00 U 50.0 40.18 ug/L 80 58 -131 20 30
tert-Butylbenzene 0.630 U 50.0 43.60 ug/L 87 54 -146 26 30
Tetrachloroethene 0.900 U 50.0 40.40 ug/L 81 52 -133 15 30
Toluene 0.986 J 50.0 41.26 ug/L 81 65 -130 15 30
trans-1,2-Dichloroethene 0.500 U 50.0 40.86 ug/L 82 61 -143 12 30
trans-1,3-Dichloropropene 0.200 U 50.0 40.36 ug/L 81 53 -133 12 30
Trichloroethene 0.150 U 50.0 42.84 ug/L 86 64 -136 10 30
Trichlorofluoromethane 0.520 U 50.0 41.89 ug/L 84 54 -150 5 30
Vinyl acetate 0.930 U 100 94.09 ug/L 94 26 -150 6 33
Vinyl chloride 0.500 U 50.0 44.34 ug/L 89 46 -150 4 30
Xylenes, Total 9.34 J 100 88.50 ug/L 79 59 -130 18 30
t-Butyl alcohol 4.90 U 500 349.2 ug/L 70 31 -150 10 42
4-Bromofluorobenzene 72 -119
Surrogate
98
MSD MSD
Qualifier Limits%Recovery
99Dibromofluoromethane 75 -126
96Toluene-d8 (Surr)64 -132
Client Sample ID: Method BlankLab Sample ID: MB 400-612025/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612025
RL MDL
1,1,1,2-Tetrachloroethane 0.160 U 1.00 0.160 ug/L 02/11/23 07:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.180 U 0.1801.00 ug/L 02/11/23 07:54 11,1,1-Trichloroethane
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,1,2,2-Tetrachloroethane
0.210 U 0.2105.00 ug/L 02/11/23 07:54 11,1,2-Trichloroethane
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,1-Dichloroethane
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,1-Dichloroethene
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,1-Dichloropropene
0.900 U 0.9001.00 ug/L 02/11/23 07:54 11,2,3-Trichlorobenzene
0.840 U 0.8405.00 ug/L 02/11/23 07:54 11,2,3-Trichloropropane
0.820 U 0.8201.00 ug/L 02/11/23 07:54 11,2,4-Trichlorobenzene
0.820 U 0.8201.00 ug/L 02/11/23 07:54 11,2,4-Trimethylbenzene
0.230 U 0.2301.00 ug/L 02/11/23 07:54 11,2-Dibromoethane (EDB)
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,2-Dichlorobenzene
0.190 U 0.1901.00 ug/L 02/11/23 07:54 11,2-Dichloroethane
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,2-Dichloropropane
0.560 U 0.5601.00 ug/L 02/11/23 07:54 11,3,5-Trimethylbenzene
0.540 U 0.5401.00 ug/L 02/11/23 07:54 11,3-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/11/23 07:54 11,3-Dichloropropane
0.640 U 0.6401.00 ug/L 02/11/23 07:54 11,4-Dichlorobenzene
0.500 U 0.5001.00 ug/L 02/11/23 07:54 12,2-Dichloropropane
2.60 U 2.6025.0 ug/L 02/11/23 07:54 12-Butanone (MEK)
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-612025/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612025
RL MDL
2-Chlorotoluene 0.570 U 1.00 0.570 ug/L 02/11/23 07:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.40 U 1.4025.0 ug/L 02/11/23 07:54 12-Hexanone
0.560 U 0.5601.00 ug/L 02/11/23 07:54 14-Chlorotoluene
1.80 U 1.8025.0 ug/L 02/11/23 07:54 14-Methyl-2-pentanone (MIBK)
10.0 U 10.025.0 ug/L 02/11/23 07:54 1Acetone
0.130 U 0.1301.00 ug/L 02/11/23 07:54 1Benzene
0.540 U 0.5401.00 ug/L 02/11/23 07:54 1Bromobenzene
0.210 U 0.2101.00 ug/L 02/11/23 07:54 1Bromochloromethane
0.500 U 0.5001.00 ug/L 02/11/23 07:54 1Bromodichloromethane
0.250 U 0.2505.00 ug/L 02/11/23 07:54 1Bromoform
0.980 U 0.9801.00 ug/L 02/11/23 07:54 1Bromomethane
0.190 U 0.1901.00 ug/L 02/11/23 07:54 1Carbon tetrachloride
0.150 U 0.1501.00 ug/L 02/11/23 07:54 1Chlorobenzene
0.760 U 0.7601.00 ug/L 02/11/23 07:54 1Chloroethane
1.00 U 1.001.00 ug/L 02/11/23 07:54 1Chloroform
0.320 U 0.3201.00 ug/L 02/11/23 07:54 1Chloromethane
0.200 U 0.2001.00 ug/L 02/11/23 07:54 1cis-1,2-Dichloroethene
0.500 U 0.5005.00 ug/L 02/11/23 07:54 1cis-1,3-Dichloropropene
0.240 U 0.2401.00 ug/L 02/11/23 07:54 1Dibromochloromethane
0.850 U 0.8501.00 ug/L 02/11/23 07:54 1Dichlorodifluoromethane
0.200 U 0.2001.00 ug/L 02/11/23 07:54 1Diisopropyl ether
24.0 U 24.0100 ug/L 02/11/23 07:54 1Ethanol
0.500 U 0.5001.00 ug/L 02/11/23 07:54 1Ethylbenzene
0.530 U 0.5301.00 ug/L 02/11/23 07:54 1Isopropylbenzene
0.220 U 0.2201.00 ug/L 02/11/23 07:54 1Methyl tert-butyl ether
3.00 U 3.005.00 ug/L 02/11/23 07:54 1Methylene Chloride
0.630 U 0.6305.00 ug/L 02/11/23 07:54 1m-Xylene & p-Xylene
3.00 U 3.005.00 ug/L 02/11/23 07:54 1Naphthalene
0.760 U 0.7601.00 ug/L 02/11/23 07:54 1n-Butylbenzene
0.690 U 0.6901.00 ug/L 02/11/23 07:54 1N-Propylbenzene
0.600 U 0.6005.00 ug/L 02/11/23 07:54 1o-Xylene
0.710 U 0.7101.00 ug/L 02/11/23 07:54 1p-Cymene (p-Isopropyltoluene)
0.700 U 0.7001.00 ug/L 02/11/23 07:54 1sec-Butylbenzene
1.00 U 1.001.00 ug/L 02/11/23 07:54 1Styrene
0.630 U 0.6301.00 ug/L 02/11/23 07:54 1tert-Butylbenzene
0.900 U 0.9001.00 ug/L 02/11/23 07:54 1Tetrachloroethene
0.410 U 0.4101.00 ug/L 02/11/23 07:54 1Toluene
0.500 U 0.5001.00 ug/L 02/11/23 07:54 1trans-1,2-Dichloroethene
0.200 U 0.2005.00 ug/L 02/11/23 07:54 1trans-1,3-Dichloropropene
0.150 U 0.1501.00 ug/L 02/11/23 07:54 1Trichloroethene
0.520 U 0.5201.00 ug/L 02/11/23 07:54 1Trichlorofluoromethane
0.930 U 0.93025.0 ug/L 02/11/23 07:54 1Vinyl acetate
0.500 U 0.5001.00 ug/L 02/11/23 07:54 1Vinyl chloride
1.60 U 1.6010.0 ug/L 02/11/23 07:54 1Xylenes, Total
4.90 U 4.9010.0 ug/L 02/11/23 07:54 1t-Butyl alcohol
4-Bromofluorobenzene 99 72-119 02/11/23 07:54 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-612025/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612025
Dibromofluoromethane 99 75-126 02/11/23 07:54 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 02/11/23 07:54 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-612025/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612025
1,1,1,2-Tetrachloroethane 50.0 44.60 ug/L 89 67 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 41.96 ug/L 84 68 -130
1,1,2,2-Tetrachloroethane 50.0 45.57 ug/L 91 70 -131
1,1,2-Trichloroethane 50.0 45.13 ug/L 90 70 -130
1,1-Dichloroethane 50.0 45.58 ug/L 91 70 -130
1,1-Dichloroethene 50.0 47.06 ug/L 94 63 -134
1,1-Dichloropropene 50.0 45.54 ug/L 91 70 -130
1,2,3-Trichlorobenzene 50.0 56.59 ug/L 113 60 -138
1,2,3-Trichloropropane 50.0 43.41 ug/L 87 70 -130
1,2,4-Trichlorobenzene 50.0 54.14 ug/L 108 60 -140
1,2,4-Trimethylbenzene 50.0 44.64 ug/L 89 70 -130
1,2-Dibromoethane (EDB)50.0 47.37 ug/L 95 70 -130
1,2-Dichlorobenzene 50.0 47.02 ug/L 94 67 -130
1,2-Dichloroethane 50.0 43.35 ug/L 87 69 -130
1,2-Dichloropropane 50.0 46.69 ug/L 93 70 -130
1,3,5-Trimethylbenzene 50.0 42.63 ug/L 85 69 -130
1,3-Dichlorobenzene 50.0 46.09 ug/L 92 70 -130
1,3-Dichloropropane 50.0 47.07 ug/L 94 70 -130
1,4-Dichlorobenzene 50.0 45.96 ug/L 92 70 -130
2,2-Dichloropropane 50.0 45.05 ug/L 90 52 -135
2-Butanone (MEK)200 185.2 ug/L 93 61 -145
2-Chlorotoluene 50.0 42.66 ug/L 85 70 -130
2-Hexanone 200 174.5 ug/L 87 65 -137
4-Chlorotoluene 50.0 42.24 ug/L 84 70 -130
4-Methyl-2-pentanone (MIBK)200 194.2 ug/L 97 69 -138
Acetone 200 181.8 ug/L 91 43 -160
Benzene 50.0 46.57 ug/L 93 70 -130
Bromobenzene 50.0 44.47 ug/L 89 70 -132
Bromochloromethane 50.0 48.99 ug/L 98 70 -130
Bromodichloromethane 50.0 45.46 ug/L 91 67 -133
Bromoform 50.0 45.50 ug/L 91 57 -140
Bromomethane 50.0 46.38 ug/L 93 10 -160
Carbon tetrachloride 50.0 42.51 ug/L 85 61 -137
Chlorobenzene 50.0 44.91 ug/L 90 70 -130
Chloroethane 50.0 40.73 ug/L 81 55 -141
Chloroform 50.0 44.56 ug/L 89 69 -130
Chloromethane 50.0 39.03 ug/L 78 58 -137
cis-1,2-Dichloroethene 50.0 44.14 ug/L 88 68 -130
cis-1,3-Dichloropropene 50.0 49.28 ug/L 99 69 -132
Dibromochloromethane 50.0 44.88 ug/L 90 67 -135
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-612025/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 612025
Dichlorodifluoromethane 50.0 38.31 ug/L 77 41 -146
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Diisopropyl ether 50.0 47.00 ug/L 94 64 -132
Ethanol 2000 1206 ug/L 60 20 -160
Ethylbenzene 50.0 42.79 ug/L 86 70 -130
Isopropylbenzene 50.0 42.48 ug/L 85 70 -130
Methyl tert-butyl ether 50.0 47.64 ug/L 95 66 -130
Methylene Chloride 50.0 47.61 ug/L 95 66 -135
m-Xylene & p-Xylene 50.0 42.96 ug/L 86 70 -130
Naphthalene 50.0 60.97 ug/L 122 47 -149
n-Butylbenzene 50.0 44.04 ug/L 88 67 -130
N-Propylbenzene 50.0 43.24 ug/L 86 70 -130
o-Xylene 50.0 42.52 ug/L 85 70 -130
p-Cymene (p-Isopropyltoluene)50.0 43.83 ug/L 88 65 -130
sec-Butylbenzene 50.0 42.55 ug/L 85 66 -130
Styrene 50.0 43.64 ug/L 87 70 -130
tert-Butylbenzene 50.0 45.72 ug/L 91 64 -139
Tetrachloroethene 50.0 44.95 ug/L 90 65 -130
Toluene 50.0 42.95 ug/L 86 70 -130
trans-1,2-Dichloroethene 50.0 44.67 ug/L 89 70 -130
trans-1,3-Dichloropropene 50.0 44.55 ug/L 89 63 -130
Trichloroethene 50.0 46.90 ug/L 94 70 -130
Trichlorofluoromethane 50.0 42.41 ug/L 85 65 -138
Vinyl acetate 100 98.55 ug/L 99 26 -160
Vinyl chloride 50.0 45.29 ug/L 91 59 -136
Xylenes, Total 100 85.48 ug/L 85 70 -130
t-Butyl alcohol 500 392.1 ug/L 78 46 -143
4-Bromofluorobenzene 72 -119
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
99Dibromofluoromethane 75 -126
93Toluene-d8 (Surr)64 -132
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Client Sample ID: MW5 Lab Sample ID: 400-232732-1
Matrix: WaterDate Collected: 02/01/23 14:28
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 10:141 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW17 Lab Sample ID: 400-232732-2
Matrix: WaterDate Collected: 02/01/23 13:39
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 17:371 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW20 Lab Sample ID: 400-232732-3
Matrix: WaterDate Collected: 02/01/23 13:28
Date Received: 02/06/23 08:51
Analysis SM6200-B WPD02/08/23 18:18200 EET PEN611533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW24 Lab Sample ID: 400-232732-4
Matrix: WaterDate Collected: 02/01/23 13:19
Date Received: 02/06/23 08:51
Analysis SM6200-B WPD02/11/23 10:3810 EET PEN612025
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis SM6200-B DL 20 612025 02/11/23 17:45 WPD EET PENTotal/NA 5 mL 5 mL
Client Sample ID: MW25 Lab Sample ID: 400-232732-5
Matrix: WaterDate Collected: 02/01/23 14:14
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 18:021 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW27 Lab Sample ID: 400-232732-6
Matrix: WaterDate Collected: 02/01/23 14:01
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 18:2720 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW30 Lab Sample ID: 400-232732-7
Matrix: WaterDate Collected: 02/01/23 13:52
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 18:5120 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Client Sample ID: Method Blank Lab Sample ID: MB 400-611533/5
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD02/08/23 09:161 EET PEN611533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-611700/5
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP02/09/23 09:491 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-612025/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD02/11/23 07:541 EET PEN612025
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-611533/1003
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD02/08/23 08:251 EET PEN611533
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-611700/1003
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP02/09/23 08:471 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-612025/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B WPD02/11/23 07:101 EET PEN612025
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW5 Lab Sample ID: 400-232732-1 MS
Matrix: WaterDate Collected: 02/01/23 14:28
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 11:031 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Client Sample ID: MW5 Lab Sample ID: 400-232732-1 MSD
Matrix: WaterDate Collected: 02/01/23 14:28
Date Received: 02/06/23 08:51
Analysis SM6200-B BEP02/09/23 11:281 EET PEN611700
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins Pensacola
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Method Summary
Job ID: 400-232732-1Client: Terraquest Environmental Consultants, PC
Project/Site: Jonesville Amoco B
Method Method Description LaboratoryProtocol
SMSM6200-B Volatile Organic Compounds EET PEN
SW8465030BPurge and Trap EET PEN
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins Pensacola
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Accreditation/Certification Summary
Client: Terraquest Environmental Consultants, PC Job ID: 400-232732-1
Project/Site: Jonesville Amoco B
Laboratory: Eurofins Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 314 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
SM6200-B Water 2-Butanone (MEK)
SM6200-B Water 2-Hexanone
SM6200-B Water 4-Methyl-2-pentanone (MIBK)
SM6200-B Water Acetone
SM6200-B Water t-Butyl alcohol
SM6200-B Water Vinyl acetate
Eurofins Pensacola
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Login Sample Receipt Checklist
Client: Terraquest Environmental Consultants, PC Job Number: 400-232732-1
Login Number: 232732
Question Answer Comment
Creator: Perez, Trina M
List Source: Eurofins Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.1.4°C IR-8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pensacola
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