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HomeMy WebLinkAboutWS-2805_6783_CA_RMR_20160610Analytical Report A6E0085 Project Hollars Grocery Project Number 02001 May 26, 2016 Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Mebane, NC 27302 Minority Women Business Enterprise Small Disadvantaged Business Enterprise 6017 Financial Drive Phone #:770.449.8800 Website:www.ftsanalytical.comNorcross, GA 30071 Minority Women Business Enterprise Small Disadvantaged Business Enterprise May 26, 2016 Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Ryan Kerins RE: Hollars Grocery We are reporting the results of the analyses performed on the samples recieved on 5/13/2016 under the project name referenced above and identified as the lab Work Order A6E0085. All results being reported under this Report apply to the samples analyzed and properly identified with a Laboratory ID number. Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontracted lab, or the complete subcontracted report attached to this report. Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reporting using all other available quality control methods. The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise agreed upon. The samples received, and described as recorded in Work Order A6E0085 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard practices, controlled/regulated substances, etc.) We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions concerning this report, please do not hesitate to contact us at any time. We will be happy to help. Mebane, NC 27302 Sincerely, Chad A. Bechtold VP of Client Services Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Samples in this Report Sample Lab ID Matrix Date Sampled Date Received MWA WaterA6E0085-01 13-May-2016 09:3012-May-2016 14:38 MWB/RW4 WaterA6E0085-02 13-May-2016 09:3012-May-2016 14:20 MWN WaterA6E0085-03 13-May-2016 09:3012-May-2016 13:55 MWQ WaterA6E0085-04 13-May-2016 09:3012-May-2016 13:45 MWT WaterA6E0085-05 13-May-2016 09:3012-May-2016 13:50 VERW1 WaterA6E0085-06 13-May-2016 09:3012-May-2016 14:34 VERW2/RW3 WaterA6E0085-07 13-May-2016 09:3012-May-2016 14:25 RW7 WaterA6E0085-08 13-May-2016 09:3012-May-2016 14:00 SWN WaterA6E0085-09 13-May-2016 09:3012-May-2016 14:45 Page 3 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Analysis Case Narrative SM6200B Batch B6E0534 The RPD of the Blank Spike, Blank Spike Duplicate was outside QC limits for Tetrachloroethene. The RPD was within limits in the Matrix Spike, Matrix Spike Duplicate therefore the data was accepted. Samples affected: A6E0085-02,03,06,07,08,09. The percent recovery of the Matrix Spike Duplicate was above QC limits for Naphthalene. The percent recovery was within limits in the Blank Spike, Blank Spike Duplicate. Samples affected: A6E0085-08. SM6200B Batch B6E0562 The percent recovery of the Blank Spike was above QC limits for cis-1,3-Dichlopropene and Naphthalene. The percent recovery of the Blank Spike Duplicate was above QC limits for Tetrachloroethylene . The percent recovery was within limits in the Matrix Spike, Matrix Spike Duplicate therefore the data was accepted. The RPD of Blank Spike and Blank Spike Duplicate was outside QC limits for Tetrachloroethylene and Vinyl Acetate . The RPD was within limits in the Matrix Spike, Matrix Spike Duplicate therefore the data was accepted. Samples affected: A6E0085-01,04,05. Page 4 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary Sample: MWA MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-01 1,2,4-Trimethylbenzene 0.500 ug/L0.103 112.2 5/20/16 16:25 95-63-6 SM 6200B 1,3,5-trimethylbenzene 0.500 ug/L0.0870 15.99 5/20/16 16:25 108-67-8 SM 6200B isopropylbenzene 0.500 ug/L0.0980 10.550 5/20/16 16:25 98-82-8 SM 6200B Sec-Butylbenzene 0.500 ug/L0.0920 10.660 5/20/16 16:25 135-98-8 SM 6200B tert-Butylbenzene 0.500 ug/L0.0890 10.730 5/20/16 16:25 98-06-6 SM 6200B Toluene 0.500 ug/L0.0570 10.630 5/20/16 16:25 108-88-3 SM 6200B Sample: MWB/RW4 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-02 Isopropyl Ether 5.00 ug/L0.0920 111.1 5/19/16 17:45 108-20-3 SM 6200B Naphthalene 2.00 ug/L0.0940 1J0.540 5/19/16 17:45 91-20-3 SM 6200B Sample: MWN MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-03 1,2-Dichloroethane 0.500 ug/L0.0900 113.5 5/19/16 19:19 107-06-2 SM 6200B Benzene 0.500 ug/L0.119 10.630 5/19/16 19:19 71-43-2 SM 6200B Isopropyl Ether 250 ug/L4.60 50J140 5/19/16 21:32 108-20-3 SM 6200B Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 175.5 5/19/16 19:19 1634-04-4 SM 6200B Sample: MWT MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-05 Isopropyl Ether 5.00 ug/L0.0920 1J2.84 5/20/16 17:28 108-20-3 SM 6200B Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 13.13 5/20/16 17:28 1634-04-4 SM 6200B Sample: VERW1 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-06 Isopropyl Ether 5.00 ug/L0.0920 127.0 5/19/16 18:48 108-20-3 SM 6200B Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 138.0 5/19/16 18:48 1634-04-4 SM 6200B Page 5 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Hits Summary (Continued) Sample: VERW2/RW3 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-07 1,2-Dichloroethane 0.500 ug/L0.0900 10.570 5/19/16 16:10 107-06-2 SM 6200B Benzene 0.500 ug/L0.119 10.670 5/19/16 16:10 71-43-2 SM 6200B Isopropyl Ether 5.00 ug/L0.0920 110.6 5/19/16 16:10 108-20-3 SM 6200B isopropylbenzene 0.500 ug/L0.0980 1J0.280 5/19/16 16:10 98-82-8 SM 6200B Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 17.16 5/19/16 16:10 1634-04-4 SM 6200B Sample: RW7 MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte Lab ID: A6E0085-08 1,3,5-trimethylbenzene 0.500 ug/L0.0870 1J0.310 5/19/16 16:42 108-67-8 SM 6200B Benzene 0.500 ug/L0.119 111.2 5/19/16 16:42 71-43-2 SM 6200B Ethylbenzene 0.500 ug/L0.0920 13.50 5/19/16 16:42 100-41-4 SM 6200B Isopropyl Ether 5.00 ug/L0.0920 1X34.8 5/19/16 16:42 108-20-3 SM 6200B isopropylbenzene 0.500 ug/L0.0980 12.87 5/19/16 16:42 98-82-8 SM 6200B Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 12.97 5/19/16 16:42 1634-04-4 SM 6200B n-Propylbenzene 1.00 ug/L0.0650 1J0.430 5/19/16 16:42 103-65-1 SM 6200B Toluene 0.500 ug/L0.0570 10.930 5/19/16 16:42 108-88-3 SM 6200B m,p-Xylenes 1.00 ug/L0.176 1J0.570 5/19/16 16:42 179601-23-1 SM 6200B o-Xylene 0.500 ug/L0.122 11.56 5/19/16 16:42 95-47-6 SM 6200B Page 6 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Page 3 of 3 Sample Results ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-01 (Water) Client Sample ID: MWA RL Dil Date Prepared Sampled: 5/12/16 14:38 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/20/16 16:255/20/16 9:36 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/20/16 16:255/20/16 9:36 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/20/16 16:255/20/16 9:36 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/20/16 16:255/20/16 9:36 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/20/16 16:255/20/16 9:36 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/20/16 16:255/20/16 9:36 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/20/16 16:255/20/16 9:36 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/20/16 16:255/20/16 9:36 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/20/16 16:255/20/16 9:36 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/20/16 16:255/20/16 9:36 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 112.2 5/20/16 16:255/20/16 9:36 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/20/16 16:255/20/16 9:36 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/20/16 16:255/20/16 9:36 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/20/16 16:255/20/16 9:36 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/20/16 16:255/20/16 9:36 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 15.99 5/20/16 16:255/20/16 9:36 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/20/16 16:255/20/16 9:36 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/20/16 16:255/20/16 9:36 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/20/16 16:255/20/16 9:36 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/20/16 16:255/20/16 9:36 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/20/16 16:255/20/16 9:36 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/20/16 16:255/20/16 9:36 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/20/16 16:255/20/16 9:36 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/20/16 16:255/20/16 9:36 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/20/16 16:255/20/16 9:36 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/20/16 16:255/20/16 9:36 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/20/16 16:255/20/16 9:36 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/20/16 16:255/20/16 9:36 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/20/16 16:255/20/16 9:36 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/20/16 16:255/20/16 9:36 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/20/16 16:255/20/16 9:36 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/20/16 16:255/20/16 9:36 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/20/16 16:255/20/16 9:36 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/20/16 16:255/20/16 9:36 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/20/16 16:255/20/16 9:36 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/20/16 16:255/20/16 9:36 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/20/16 16:255/20/16 9:36 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/20/16 16:255/20/16 9:36 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/20/16 16:255/20/16 9:36 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/20/16 16:255/20/16 9:36 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U, H 5/20/16 16:255/20/16 9:36 10061-01-5 Page 7 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-01 (Water) Client Sample ID: MWA (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:38 CAS # VOCs by NC Method 6200B (Continued) Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/20/16 16:255/20/16 9:36 75-71-8 Ethanol 50.0 ug/L3.00 13.00 U 5/20/16 16:255/20/16 9:36 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/20/16 16:255/20/16 9:36 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 10.0920 U 5/20/16 16:255/20/16 9:36 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.550 5/20/16 16:255/20/16 9:36 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 10.169 U 5/20/16 16:255/20/16 9:36 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/20/16 16:255/20/16 9:36 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U, H 5/20/16 16:255/20/16 9:36 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/20/16 16:255/20/16 9:36 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/20/16 16:255/20/16 9:36 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.660 5/20/16 16:255/20/16 9:36 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/20/16 16:255/20/16 9:36 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.730 5/20/16 16:255/20/16 9:36 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F, H 5/20/16 16:255/20/16 9:36 127-18-4 Toluene 0.500 ug/L0.0570 10.630 5/20/16 16:255/20/16 9:36 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/20/16 16:255/20/16 9:36 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/20/16 16:255/20/16 9:36 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/20/16 16:255/20/16 9:36 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/20/16 16:255/20/16 9:36 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U, F 5/20/16 16:255/20/16 9:36 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/20/16 16:255/20/16 9:36 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/20/16 16:255/20/16 9:36 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/20/16 16:255/20/16 9:36 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126106%5/20/16 16:25 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111100%5/20/16 16:25 460-00-4 Surrogate: Toluene-D8 (SUR)83-11693%5/20/16 16:25 2037-26-5 Page 8 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-02 (Water) Client Sample ID: MWB/RW4 RL Dil Date Prepared Sampled: 5/12/16 14:20 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 17:455/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 17:455/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 17:455/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 17:455/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 17:455/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 17:455/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 17:455/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 17:455/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 17:455/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 17:455/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 17:455/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 17:455/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 17:455/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/19/16 17:455/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 17:455/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/19/16 17:455/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 17:455/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 17:455/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 17:455/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 17:455/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 17:455/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 17:455/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 17:455/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 17:455/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 17:455/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 17:455/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 17:455/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/19/16 17:455/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 17:455/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 17:455/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 17:455/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 17:455/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 17:455/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 17:455/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 17:455/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 17:455/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 17:455/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 17:455/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 17:455/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 17:455/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 17:455/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 17:455/19/16 11:05 75-71-8 Page 9 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-02 (Water) Client Sample ID: MWB/RW4 (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:20 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 17:455/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 17:455/19/16 11:05 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 111.1 5/19/16 17:455/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 17:455/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 10.169 U 5/19/16 17:455/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 17:455/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.540 J 5/19/16 17:455/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 17:455/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/19/16 17:455/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 17:455/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 17:455/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 17:455/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 17:455/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/19/16 17:455/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 17:455/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 17:455/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 17:455/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 17:455/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 17:455/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 17:455/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/19/16 17:455/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/19/16 17:455/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126109%5/19/16 17:45 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111104%5/19/16 17:45 460-00-4 Surrogate: Toluene-D8 (SUR)83-11698%5/19/16 17:45 2037-26-5 Page 10 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-03 (Water) Client Sample ID: MWN RL Dil Date Prepared Sampled: 5/12/16 13:55 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 19:195/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 19:195/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 19:195/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 19:195/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 19:195/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 19:195/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 19:195/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 19:195/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 19:195/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 19:195/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 19:195/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 19:195/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 19:195/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 113.5 5/19/16 19:195/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 19:195/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/19/16 19:195/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 19:195/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 19:195/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 19:195/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 19:195/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 19:195/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 19:195/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 19:195/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 19:195/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 19:195/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 19:195/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 19:195/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 10.630 5/19/16 19:195/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 19:195/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 19:195/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 19:195/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 19:195/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 19:195/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 19:195/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 19:195/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 19:195/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 19:195/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 19:195/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 19:195/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 19:195/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 19:195/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 19:195/19/16 11:05 75-71-8 Page 11 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-03 (Water) Client Sample ID: MWN (Continued) RL Dil Date Prepared Sampled: 5/12/16 13:55 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 19:195/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 19:195/19/16 11:05 100-41-4 Isopropyl Ether 250 ug/L4.60 50140J 5/19/16 21:325/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 19:195/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 175.5 5/19/16 19:195/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 19:195/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U 5/19/16 19:195/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 19:195/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/19/16 19:195/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 19:195/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 19:195/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 19:195/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 19:195/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/19/16 19:195/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 19:195/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 19:195/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 19:195/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 19:195/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 19:195/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 19:195/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/19/16 19:195/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/19/16 19:195/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126107%5/19/16 19:19 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111104%5/19/16 19:19 460-00-4 Surrogate: Toluene-D8 (SUR)83-116101%5/19/16 19:19 2037-26-5 Page 12 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-04 (Water) Client Sample ID: MWQ RL Dil Date Prepared Sampled: 5/12/16 13:45 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/20/16 16:565/20/16 9:36 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/20/16 16:565/20/16 9:36 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/20/16 16:565/20/16 9:36 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/20/16 16:565/20/16 9:36 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/20/16 16:565/20/16 9:36 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/20/16 16:565/20/16 9:36 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/20/16 16:565/20/16 9:36 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/20/16 16:565/20/16 9:36 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/20/16 16:565/20/16 9:36 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/20/16 16:565/20/16 9:36 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/20/16 16:565/20/16 9:36 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/20/16 16:565/20/16 9:36 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/20/16 16:565/20/16 9:36 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/20/16 16:565/20/16 9:36 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/20/16 16:565/20/16 9:36 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/20/16 16:565/20/16 9:36 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/20/16 16:565/20/16 9:36 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/20/16 16:565/20/16 9:36 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/20/16 16:565/20/16 9:36 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/20/16 16:565/20/16 9:36 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/20/16 16:565/20/16 9:36 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/20/16 16:565/20/16 9:36 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/20/16 16:565/20/16 9:36 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/20/16 16:565/20/16 9:36 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/20/16 16:565/20/16 9:36 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/20/16 16:565/20/16 9:36 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/20/16 16:565/20/16 9:36 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/20/16 16:565/20/16 9:36 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/20/16 16:565/20/16 9:36 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/20/16 16:565/20/16 9:36 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/20/16 16:565/20/16 9:36 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/20/16 16:565/20/16 9:36 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/20/16 16:565/20/16 9:36 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/20/16 16:565/20/16 9:36 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/20/16 16:565/20/16 9:36 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/20/16 16:565/20/16 9:36 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/20/16 16:565/20/16 9:36 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/20/16 16:565/20/16 9:36 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/20/16 16:565/20/16 9:36 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/20/16 16:565/20/16 9:36 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U, H 5/20/16 16:565/20/16 9:36 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/20/16 16:565/20/16 9:36 75-71-8 Page 13 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-04 (Water) Client Sample ID: MWQ (Continued) RL Dil Date Prepared Sampled: 5/12/16 13:45 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/20/16 16:565/20/16 9:36 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/20/16 16:565/20/16 9:36 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 10.0920 U 5/20/16 16:565/20/16 9:36 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/20/16 16:565/20/16 9:36 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 10.169 U 5/20/16 16:565/20/16 9:36 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/20/16 16:565/20/16 9:36 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U, H 5/20/16 16:565/20/16 9:36 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/20/16 16:565/20/16 9:36 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/20/16 16:565/20/16 9:36 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/20/16 16:565/20/16 9:36 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/20/16 16:565/20/16 9:36 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/20/16 16:565/20/16 9:36 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F, H 5/20/16 16:565/20/16 9:36 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/20/16 16:565/20/16 9:36 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/20/16 16:565/20/16 9:36 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/20/16 16:565/20/16 9:36 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/20/16 16:565/20/16 9:36 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/20/16 16:565/20/16 9:36 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U, F 5/20/16 16:565/20/16 9:36 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/20/16 16:565/20/16 9:36 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/20/16 16:565/20/16 9:36 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/20/16 16:565/20/16 9:36 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126107%5/20/16 16:56 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111103%5/20/16 16:56 460-00-4 Surrogate: Toluene-D8 (SUR)83-11694%5/20/16 16:56 2037-26-5 Page 14 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-05 (Water) Client Sample ID: MWT RL Dil Date Prepared Sampled: 5/12/16 13:50 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/20/16 17:285/20/16 9:36 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/20/16 17:285/20/16 9:36 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/20/16 17:285/20/16 9:36 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/20/16 17:285/20/16 9:36 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/20/16 17:285/20/16 9:36 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/20/16 17:285/20/16 9:36 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/20/16 17:285/20/16 9:36 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/20/16 17:285/20/16 9:36 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/20/16 17:285/20/16 9:36 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/20/16 17:285/20/16 9:36 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/20/16 17:285/20/16 9:36 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/20/16 17:285/20/16 9:36 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/20/16 17:285/20/16 9:36 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/20/16 17:285/20/16 9:36 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/20/16 17:285/20/16 9:36 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/20/16 17:285/20/16 9:36 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/20/16 17:285/20/16 9:36 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/20/16 17:285/20/16 9:36 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/20/16 17:285/20/16 9:36 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/20/16 17:285/20/16 9:36 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/20/16 17:285/20/16 9:36 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/20/16 17:285/20/16 9:36 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/20/16 17:285/20/16 9:36 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/20/16 17:285/20/16 9:36 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/20/16 17:285/20/16 9:36 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/20/16 17:285/20/16 9:36 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/20/16 17:285/20/16 9:36 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/20/16 17:285/20/16 9:36 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/20/16 17:285/20/16 9:36 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/20/16 17:285/20/16 9:36 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/20/16 17:285/20/16 9:36 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/20/16 17:285/20/16 9:36 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/20/16 17:285/20/16 9:36 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/20/16 17:285/20/16 9:36 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/20/16 17:285/20/16 9:36 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/20/16 17:285/20/16 9:36 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/20/16 17:285/20/16 9:36 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/20/16 17:285/20/16 9:36 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/20/16 17:285/20/16 9:36 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/20/16 17:285/20/16 9:36 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U, H 5/20/16 17:285/20/16 9:36 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/20/16 17:285/20/16 9:36 75-71-8 Page 15 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-05 (Water) Client Sample ID: MWT (Continued) RL Dil Date Prepared Sampled: 5/12/16 13:50 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/20/16 17:285/20/16 9:36 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/20/16 17:285/20/16 9:36 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 12.84 J 5/20/16 17:285/20/16 9:36 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/20/16 17:285/20/16 9:36 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 13.13 5/20/16 17:285/20/16 9:36 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/20/16 17:285/20/16 9:36 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U, H 5/20/16 17:285/20/16 9:36 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/20/16 17:285/20/16 9:36 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/20/16 17:285/20/16 9:36 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/20/16 17:285/20/16 9:36 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/20/16 17:285/20/16 9:36 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/20/16 17:285/20/16 9:36 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F, H 5/20/16 17:285/20/16 9:36 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/20/16 17:285/20/16 9:36 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/20/16 17:285/20/16 9:36 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/20/16 17:285/20/16 9:36 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/20/16 17:285/20/16 9:36 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/20/16 17:285/20/16 9:36 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U, F 5/20/16 17:285/20/16 9:36 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/20/16 17:285/20/16 9:36 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/20/16 17:285/20/16 9:36 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/20/16 17:285/20/16 9:36 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-12696%5/20/16 17:28 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111105%5/20/16 17:28 460-00-4 Surrogate: Toluene-D8 (SUR)83-11697%5/20/16 17:28 2037-26-5 Page 16 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-06 (Water) Client Sample ID: VERW1 RL Dil Date Prepared Sampled: 5/12/16 14:34 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 18:485/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 18:485/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 18:485/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 18:485/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 18:485/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 18:485/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 18:485/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 18:485/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 18:485/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 18:485/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 18:485/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 18:485/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 18:485/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/19/16 18:485/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 18:485/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/19/16 18:485/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 18:485/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 18:485/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 18:485/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 18:485/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 18:485/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 18:485/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 18:485/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 18:485/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 18:485/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 18:485/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 18:485/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/19/16 18:485/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 18:485/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 18:485/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 18:485/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 18:485/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 18:485/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 18:485/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 18:485/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 18:485/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 18:485/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 18:485/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 18:485/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 18:485/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 18:485/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 18:485/19/16 11:05 75-71-8 Page 17 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-06 (Water) Client Sample ID: VERW1 (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:34 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 18:485/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 18:485/19/16 11:05 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 127.0 5/19/16 18:485/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 18:485/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 138.0 5/19/16 18:485/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 18:485/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U 5/19/16 18:485/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 18:485/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/19/16 18:485/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 18:485/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 18:485/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 18:485/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 18:485/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/19/16 18:485/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 18:485/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 18:485/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 18:485/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 18:485/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 18:485/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 18:485/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/19/16 18:485/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/19/16 18:485/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126110%5/19/16 18:48 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111104%5/19/16 18:48 460-00-4 Surrogate: Toluene-D8 (SUR)83-116100%5/19/16 18:48 2037-26-5 Page 18 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-07 (Water) Client Sample ID: VERW2/RW3 RL Dil Date Prepared Sampled: 5/12/16 14:25 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 16:105/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 16:105/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 16:105/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 16:105/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 16:105/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 16:105/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 16:105/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 16:105/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 16:105/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 16:105/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 16:105/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 16:105/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 16:105/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.570 5/19/16 16:105/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 16:105/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/19/16 16:105/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 16:105/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 16:105/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 16:105/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 16:105/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 16:105/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 16:105/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 16:105/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 16:105/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 16:105/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 16:105/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 16:105/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 10.670 5/19/16 16:105/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 16:105/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 16:105/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 16:105/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 16:105/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 16:105/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 16:105/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 16:105/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 16:105/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 16:105/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 16:105/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 16:105/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 16:105/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 16:105/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 16:105/19/16 11:05 75-71-8 Page 19 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-07 (Water) Client Sample ID: VERW2/RW3 (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:25 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 16:105/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 16:105/19/16 11:05 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 110.6 5/19/16 16:105/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.280 J 5/19/16 16:105/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 17.16 5/19/16 16:105/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 16:105/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U 5/19/16 16:105/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 16:105/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/19/16 16:105/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 16:105/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 16:105/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 16:105/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 16:105/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/19/16 16:105/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 16:105/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 16:105/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 16:105/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 16:105/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 16:105/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 16:105/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/19/16 16:105/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/19/16 16:105/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126109%5/19/16 16:10 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111103%5/19/16 16:10 460-00-4 Surrogate: Toluene-D8 (SUR)83-11699%5/19/16 16:10 2037-26-5 Page 20 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-08 (Water) Client Sample ID: RW7 RL Dil Date Prepared Sampled: 5/12/16 14:00 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 16:425/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 16:425/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 16:425/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 16:425/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 16:425/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 16:425/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 16:425/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 16:425/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 16:425/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 16:425/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 16:425/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 16:425/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 16:425/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/19/16 16:425/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 16:425/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.310 J 5/19/16 16:425/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 16:425/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 16:425/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 16:425/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 16:425/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 16:425/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 16:425/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 16:425/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 16:425/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 16:425/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 16:425/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 16:425/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 111.2 5/19/16 16:425/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 16:425/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 16:425/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 16:425/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 16:425/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 16:425/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 16:425/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 16:425/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 16:425/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 16:425/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 16:425/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 16:425/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 16:425/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 16:425/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 16:425/19/16 11:05 75-71-8 Page 21 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-08 (Water) Client Sample ID: RW7 (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:00 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 16:425/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 13.50 5/19/16 16:425/19/16 11:05 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 134.8 X 5/19/16 16:425/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 12.87 5/19/16 16:425/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 12.97 5/19/16 16:425/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 16:425/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 XU 5/19/16 16:425/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 16:425/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.430 J 5/19/16 16:425/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 16:425/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 16:425/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 16:425/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 16:425/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.930 5/19/16 16:425/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 16:425/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 16:425/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 16:425/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 16:425/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 16:425/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 16:425/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.570 J 5/19/16 16:425/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 11.56 5/19/16 16:425/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126109%5/19/16 16:42 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111103%5/19/16 16:42 460-00-4 Surrogate: Toluene-D8 (SUR)83-116101%5/19/16 16:42 2037-26-5 Page 22 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-09 (Water) Client Sample ID: SWN RL Dil Date Prepared Sampled: 5/12/16 14:45 CAS # VOCs by NC Method 6200B 1,1,1,2-Tetrachloroethane 1.00 ug/L0.180 10.180 U 5/19/16 17:135/19/16 11:05 630-20-6 1,1,1-Trichloroethane 0.500 ug/L0.0760 10.0760 U 5/19/16 17:135/19/16 11:05 71-55-6 1,1,2,2-Tetrachloroethane 0.500 ug/L0.0700 10.0700 U 5/19/16 17:135/19/16 11:05 79-34-5 1,1,2-Trichloroethane 0.500 ug/L0.113 10.113 U 5/19/16 17:135/19/16 11:05 79-00-5 1,1-Dichloroethane 0.500 ug/L0.121 10.121 U 5/19/16 17:135/19/16 11:05 75-34-3 1,1-Dichloroethene 0.500 ug/L0.104 10.104 U 5/19/16 17:135/19/16 11:05 75-35-4 1,1-Dichloropropene 0.500 ug/L0.0600 10.0600 U 5/19/16 17:135/19/16 11:05 563-58-6 1,2,3-Trichlorobenzene 2.00 ug/L0.118 10.118 U 5/19/16 17:135/19/16 11:05 87-61-6 1,2,3-Trichloropropane 1.00 ug/L0.138 10.138 U 5/19/16 17:135/19/16 11:05 96-18-4 1,2,4-Trichlorobenzene 1.00 ug/L0.0690 10.0690 U 5/19/16 17:135/19/16 11:05 120-82-1 1,2,4-Trimethylbenzene 0.500 ug/L0.103 10.103 U 5/19/16 17:135/19/16 11:05 95-63-6 1,2-Dibromoethane (EDB)1.00 ug/L0.180 10.180 U 5/19/16 17:135/19/16 11:05 106-93-4 1,2-Dichlorobenzene 0.500 ug/L0.0940 10.0940 U 5/19/16 17:135/19/16 11:05 95-50-1 1,2-Dichloroethane 0.500 ug/L0.0900 10.0900 U 5/19/16 17:135/19/16 11:05 107-06-2 1,2-Dichloropropane 0.500 ug/L0.122 10.122 U 5/19/16 17:135/19/16 11:05 78-87-5 1,3,5-trimethylbenzene 0.500 ug/L0.0870 10.0870 U 5/19/16 17:135/19/16 11:05 108-67-8 1,3-Dichlorobenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 17:135/19/16 11:05 541-73-1 1,3-Dichloropropane 0.500 ug/L0.133 10.133 U 5/19/16 17:135/19/16 11:05 142-28-9 1,4-Dichlorobenzene 0.500 ug/L0.0670 10.0670 U 5/19/16 17:135/19/16 11:05 106-46-7 2,2-Dichloropropane 0.200 ug/L0.0970 10.0970 U 5/19/16 17:135/19/16 11:05 590-20-7 2-Butanone (MEK)20.0 ug/L0.378 10.378 U 5/19/16 17:135/19/16 11:05 78-93-3 2-Chlorotoluene 0.200 ug/L0.0880 10.0880 U 5/19/16 17:135/19/16 11:05 95-49-8 2-Hexanone 5.00 ug/L0.352 10.352 U 5/19/16 17:135/19/16 11:05 591-78-6 4-Chlorotoluene 0.500 ug/L0.0900 10.0900 U 5/19/16 17:135/19/16 11:05 106-43-4 4-Isopropyltoluene (p-Cymene)0.500 ug/L0.0890 10.0890 U 5/19/16 17:135/19/16 11:05 99-87-6 4-Methyl-2-pentanone (MIBK)5.00 ug/L0.253 10.253 U 5/19/16 17:135/19/16 11:05 108-10-1 Acetone 5.00 ug/L0.352 10.352 U 5/19/16 17:135/19/16 11:05 67-64-1 Benzene 0.500 ug/L0.119 10.119 U 5/19/16 17:135/19/16 11:05 71-43-2 Bromobenzene 0.500 ug/L0.132 10.132 U 5/19/16 17:135/19/16 11:05 108-86-1 Bromochloromethane 0.500 ug/L0.112 10.112 U 5/19/16 17:135/19/16 11:05 74-97-5 Bromodichloromethane 0.500 ug/L0.124 10.124 U 5/19/16 17:135/19/16 11:05 75-27-4 Bromoform 2.00 ug/L0.159 10.159 U 5/19/16 17:135/19/16 11:05 75-25-2 Bromomethane 1.00 ug/L0.0970 10.0970 U 5/19/16 17:135/19/16 11:05 74-83-9 Carbon Tetrachloride 0.500 ug/L0.0990 10.0990 U 5/19/16 17:135/19/16 11:05 56-23-5 Chlorobenzene 0.500 ug/L0.105 10.105 U 5/19/16 17:135/19/16 11:05 108-90-7 Chlorodibromomethane 1.00 ug/L0.177 10.177 U 5/19/16 17:135/19/16 11:05 124-48-1 Chloroethane 0.500 ug/L0.0420 10.0420 U 5/19/16 17:135/19/16 11:05 75-00-3 Chloroform 0.500 ug/L0.172 10.172 U 5/19/16 17:135/19/16 11:05 67-66-3 Chloromethane 0.500 ug/L0.0850 10.0850 U 5/19/16 17:135/19/16 11:05 74-87-3 cis-1,2-Dichloroethene 0.500 ug/L0.114 10.114 U 5/19/16 17:135/19/16 11:05 156-59-4 cis-1,3-Dichloropropene 1.00 ug/L0.100 10.100 U 5/19/16 17:135/19/16 11:05 10061-01-5 Dichlorodifluoromethane 0.500 ug/L0.0670 10.0670 U 5/19/16 17:135/19/16 11:05 75-71-8 Page 23 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Sample Results (Continued) ResultAnalyte MDL Date AnalyzedQual Units Lab Sample ID: A6E0085-09 (Water) Client Sample ID: SWN (Continued) RL Dil Date Prepared Sampled: 5/12/16 14:45 CAS # VOCs by NC Method 6200B (Continued) Ethanol 50.0 ug/L3.00 13.00 U 5/19/16 17:135/19/16 11:05 64-17-5 Ethylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 17:135/19/16 11:05 100-41-4 Isopropyl Ether 5.00 ug/L0.0920 10.0920 U 5/19/16 17:135/19/16 11:05 108-20-3 isopropylbenzene 0.500 ug/L0.0980 10.0980 U 5/19/16 17:135/19/16 11:05 98-82-8 Methyl tert-butyl ether (MTBE)1.00 ug/L0.169 10.169 U 5/19/16 17:135/19/16 11:05 1634-04-4 Methylene Chloride 0.500 ug/L0.190 10.190 U 5/19/16 17:135/19/16 11:05 75-09-2 Naphthalene 2.00 ug/L0.0940 10.0940 U 5/19/16 17:135/19/16 11:05 91-20-3 n-Butylbenzene 2.00 ug/L0.0600 10.0600 U 5/19/16 17:135/19/16 11:05 104-51-8 n-Propylbenzene 1.00 ug/L0.0650 10.0650 U 5/19/16 17:135/19/16 11:05 103-65-1 Sec-Butylbenzene 0.500 ug/L0.0920 10.0920 U 5/19/16 17:135/19/16 11:05 135-98-8 Styrene 0.500 ug/L0.0740 10.0740 U 5/19/16 17:135/19/16 11:05 100-42-5 tert-Butylbenzene 0.500 ug/L0.0890 10.0890 U 5/19/16 17:135/19/16 11:05 98-06-6 Tetrachloroethene 0.500 ug/L0.0540 10.0540 U, F 5/19/16 17:135/19/16 11:05 127-18-4 Toluene 0.500 ug/L0.0570 10.0570 U 5/19/16 17:135/19/16 11:05 108-88-3 trans-1,2-dichloroethene 0.500 ug/L0.188 10.188 U 5/19/16 17:135/19/16 11:05 156-60-5 trans-1,3-dichloropropene 1.00 ug/L0.110 10.110 U 5/19/16 17:135/19/16 11:05 1006-10-26 Trichloroethene 0.500 ug/L0.139 10.139 U 5/19/16 17:135/19/16 11:05 79-01-6 Trichlorofluoromethane 0.500 ug/L0.0540 10.0540 U 5/19/16 17:135/19/16 11:05 75-69-4 Vinyl Acetate 1.00 ug/L0.720 10.720 U 5/19/16 17:135/19/16 11:05 108-05-4 Vinyl Chloride 0.500 ug/L0.0810 10.0810 U 5/19/16 17:135/19/16 11:05 75-01-4 m,p-Xylenes 1.00 ug/L0.176 10.176 U 5/19/16 17:135/19/16 11:05 179601-23-1 o-Xylene 0.500 ug/L0.122 10.122 U 5/19/16 17:135/19/16 11:05 95-47-6 Surrogate: 1,2-Dichloroethane-D4 (SUR)65-126111%5/19/16 17:13 10706-07-0 Surrogate: 4-Bromofluorobenzene (SUR)86-111103%5/19/16 17:13 460-00-4 Surrogate: Toluene-D8 (SUR)83-116101%5/19/16 17:13 2037-26-5 Page 24 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control VOCs by NC Method 6200B MDL Batch: B6E0534 Prepared & Analyzed: 5/19/2016Blank (B6E0534-BLK1) 1.00 ug/L0.180 U 0.1801,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 U 0.07601,1,1-Trichloroethane 0.500 ug/L0.0700 U 0.07001,1,2,2-Tetrachloroethane 0.500 ug/L0.113 U 0.1131,1,2-Trichloroethane 0.500 ug/L0.121 U 0.1211,1-Dichloroethane 0.500 ug/L0.104 U 0.1041,1-Dichloroethene 0.500 ug/L0.0600 U 0.06001,1-Dichloropropene 2.00 ug/L0.118 U 0.1181,2,3-Trichlorobenzene 1.00 ug/L0.138 U 0.1381,2,3-Trichloropropane 1.00 ug/L0.0690 U 0.06901,2,4-Trichlorobenzene 0.500 ug/L0.103 U 0.1031,2,4-Trimethylbenzene 1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB) 0.500 ug/L0.0940 U 0.09401,2-Dichlorobenzene 0.500 ug/L0.0900 U 0.09001,2-Dichloroethane 0.500 ug/L0.122 U 0.1221,2-Dichloropropane 0.500 ug/L0.0870 U 0.08701,3,5-trimethylbenzene 0.500 ug/L0.0980 U 0.09801,3-Dichlorobenzene 0.500 ug/L0.133 U 0.1331,3-Dichloropropane 0.500 ug/L0.0670 U 0.06701,4-Dichlorobenzene 0.200 ug/L0.0970 U 0.09702,2-Dichloropropane 20.0 ug/L0.378 U 0.3782-Butanone (MEK) 0.200 ug/L0.0880 U 0.08802-Chlorotoluene 5.00 ug/L0.352 U 0.3522-Hexanone 0.500 ug/L0.0900 U 0.09004-Chlorotoluene 0.500 ug/L0.0890 U 0.08904-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 U 0.2534-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 U 0.352Acetone 0.500 ug/L0.119 U 0.119Benzene 0.500 ug/L0.132 U 0.132Bromobenzene 0.500 ug/L0.112 U 0.112Bromochloromethane 0.500 ug/L0.124 U 0.124Bromodichloromethane 2.00 ug/L0.159 U 0.159Bromoform 1.00 ug/L0.0970 U 0.0970Bromomethane 0.500 ug/L0.0990 U 0.0990Carbon Tetrachloride 0.500 ug/L0.105 U 0.105Chlorobenzene 1.00 ug/L0.177 U 0.177Chlorodibromomethane 0.500 ug/L0.0420 U 0.0420Chloroethane 0.500 ug/L0.172 U 0.172Chloroform 0.500 ug/L0.0850 U 0.0850Chloromethane 0.500 ug/L0.114 U 0.114cis-1,2-Dichloroethene 1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene Page 25 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016Blank (B6E0534-BLK1) 0.500 ug/L0.0670 U 0.0670Dichlorodifluoromethane 50.0 ug/L3.00 U 3.00Ethanol 0.500 ug/L0.0920 U 0.0920Ethylbenzene 5.00 ug/L0.0920 U 0.0920Isopropyl Ether 0.500 ug/L0.0980 U 0.0980isopropylbenzene 1.00 ug/L0.169 U 0.169Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 U 0.190Methylene Chloride 2.00 ug/L0.0940 U 0.0940Naphthalene 2.00 ug/L0.0600 U 0.0600n-Butylbenzene 1.00 ug/L0.0650 U 0.0650n-Propylbenzene 0.500 ug/L0.0920 U 0.0920Sec-Butylbenzene 0.500 ug/L0.0740 U 0.0740Styrene 0.500 ug/L0.0890 U 0.0890tert-Butylbenzene 0.500 ug/L0.0540 U 0.0540Tetrachloroethene 0.500 ug/L0.0570 U 0.0570Toluene 0.500 ug/L0.188 U 0.188trans-1,2-dichloroethene 1.00 ug/L0.110 U 0.110trans-1,3-dichloropropene 0.500 ug/L0.139 U 0.139Trichloroethene 0.500 ug/L0.0540 U 0.0540Trichlorofluoromethane 1.00 ug/L0.720 U 0.720Vinyl Acetate 0.500 ug/L0.0810 U 0.0810Vinyl Chloride 1.00 ug/L0.176 U 0.176m,p-Xylenes 0.500 ug/L0.122 U 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10927.2 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)10325.8 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)10025.0 ug/L Prepared & Analyzed: 5/19/2016LCS (B6E0534-BS1) 1.00 25.0 75-127109ug/L27.3 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 62-128111ug/L27.8 0.07601,1,1-Trichloroethane 0.500 25.0 77-129106ug/L26.4 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 86-120105ug/L26.2 0.1131,1,2-Trichloroethane 0.500 25.0 82-114106ug/L26.5 0.1211,1-Dichloroethane 0.500 25.0 73-123107ug/L26.9 0.1041,1-Dichloroethene 0.500 25.0 83-125103ug/L25.8 0.06001,1-Dichloropropene 2.00 25.0 57-127100ug/L24.9 0.1181,2,3-Trichlorobenzene 1.00 25.0 79-118104ug/L25.9 0.1381,2,3-Trichloropropane 1.00 25.0 59-12599ug/L24.8 0.06901,2,4-Trichlorobenzene 0.500 25.0 84-11895ug/L23.8 0.1031,2,4-Trimethylbenzene 1.00 25.0 83-126106ug/L26.5 0.1801,2-Dibromoethane (EDB) Page 26 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016LCS (B6E0534-BS1) 0.500 25.0 83-128100ug/L25.0 0.09401,2-Dichlorobenzene 0.500 25.0 56-133109ug/L27.2 0.09001,2-Dichloroethane 0.500 25.0 85-121106ug/L26.6 0.1221,2-Dichloropropane 0.500 25.0 86-11896ug/L24.0 0.08701,3,5-trimethylbenzene 0.500 25.0 90-126101ug/L25.2 0.09801,3-Dichlorobenzene 0.500 25.0 85-121104ug/L26.0 0.1331,3-Dichloropropane 0.500 25.0 88-121100ug/L25.0 0.06701,4-Dichlorobenzene 0.200 25.0 76-126116ug/L28.9 0.09702,2-Dichloropropane 20.0 50.0 66-133104ug/L52.2 0.3782-Butanone (MEK) 0.200 25.0 80-12899ug/L24.7 0.08802-Chlorotoluene 5.00 50.0 70-130110ug/L55.0 0.3522-Hexanone 0.500 25.0 82-130101ug/L25.3 0.09004-Chlorotoluene 0.500 25.0 80-12896ug/L24.1 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 74-12999ug/L49.6 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 51-143107ug/L53.5 0.352Acetone 0.500 25.0 81-12398ug/L24.6 0.119Benzene 0.500 25.0 84-114104ug/L25.9 0.132Bromobenzene 0.500 25.0 89-127108ug/L27.1 0.112Bromochloromethane 0.500 25.0 79-129113ug/L28.2 0.124Bromodichloromethane 2.00 25.0 73-140122ug/L30.5 0.159Bromoform 1.00 25.0 53-143105ug/L26.2 0.0970Bromomethane 0.500 25.0 66-136110ug/L27.5 0.0990Carbon Tetrachloride 0.500 25.0 88-118103ug/L25.8 0.105Chlorobenzene 1.00 25.0 73-139112ug/L28.0 0.177Chlorodibromomethane 0.500 25.0 70-123115ug/L28.8 0.0420Chloroethane 0.500 25.0 72-118106ug/L26.4 0.172Chloroform 0.500 25.0 65-125102ug/L25.4 0.0850Chloromethane 0.500 25.0 85-125103ug/L25.7 0.114cis-1,2-Dichloroethene 1.00 25.0 92-126115ug/L28.9 0.100cis-1,3-Dichloropropene 0.500 25.0 48-143107ug/L26.7 0.0670Dichlorodifluoromethane 50.0 1000 61-133113ug/L11303.00Ethanol 0.500 25.0 87-123102ug/L25.4 0.0920Ethylbenzene 5.00 25.0 77-125109ug/L27.2 0.0920Isopropyl Ether 0.500 25.0 82-11599ug/L24.7 0.0980isopropylbenzene 1.00 50.0 65-125108ug/L54.2 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 75-119111ug/L27.8 0.190Methylene Chloride 2.00 25.0 52-116113ug/L28.2 0.0940Naphthalene 2.00 25.0 83-13095ug/L23.7 0.0600n-Butylbenzene 1.00 25.0 84-12297ug/L24.3 0.0650n-Propylbenzene 0.500 25.0 86-12095ug/L23.8 0.0920Sec-Butylbenzene 0.500 25.0 85-123110ug/L27.6 0.0740Styrene Page 27 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016LCS (B6E0534-BS1) 0.500 25.0 79-12695ug/L23.8 0.0890tert-Butylbenzene 0.500 25.0 64-13186ug/L21.6 0.0540Tetrachloroethene 0.500 25.0 89-116101ug/L25.4 0.0570Toluene 0.500 25.0 78-118108ug/L26.9 0.188trans-1,2-dichloroethene 1.00 25.0 86-127116ug/L29.1 0.110trans-1,3-dichloropropene 0.500 25.0 82-119105ug/L26.2 0.139Trichloroethene 0.500 25.0 46-144105ug/L26.1 0.0540Trichlorofluoromethane 1.00 25.0 58-141118ug/L29.5 0.720Vinyl Acetate 0.500 25.0 76-122111ug/L27.8 0.0810Vinyl Chloride 1.00 50.0 90-125101ug/L50.6 0.176m,p-Xylenes 0.500 25.0 86-119103ug/L25.6 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)9223.1 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)10025.0 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)10025.0 ug/L Prepared & Analyzed: 5/19/2016LCS Dup (B6E0534-BSD1) 1.00 25.0 2075-127105 4ug/L26.4 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 2062-12892 18ug/L23.1 0.07601,1,1-Trichloroethane 0.500 25.0 2077-129101 5ug/L25.1 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 2086-120105 0.3ug/L26.3 0.1131,1,2-Trichloroethane 0.500 25.0 2082-11496 10ug/L23.9 0.1211,1-Dichloroethane 0.500 25.0 2073-12394 13ug/L23.5 0.1041,1-Dichloroethene 0.500 25.0 2083-12599 4ug/L24.7 0.06001,1-Dichloropropene 2.00 25.0 2057-12797 3ug/L24.2 0.1181,2,3-Trichlorobenzene 1.00 25.0 2079-118104 0.2ug/L26.0 0.1381,2,3-Trichloropropane 1.00 25.0 2059-12597 2ug/L24.3 0.06901,2,4-Trichlorobenzene 0.500 25.0 2084-11895 0.4ug/L23.7 0.1031,2,4-Trimethylbenzene 1.00 25.0 2083-126106 0.2ug/L26.5 0.1801,2-Dibromoethane (EDB) 0.500 25.0 2083-12898 2ug/L24.4 0.09401,2-Dichlorobenzene 0.500 25.0 2056-133105 4ug/L26.2 0.09001,2-Dichloroethane 0.500 25.0 2085-121103 3ug/L25.8 0.1221,2-Dichloropropane 0.500 25.0 2086-11896 0.04ug/L24.0 0.08701,3,5-trimethylbenzene 0.500 25.0 2090-12698 3ug/L24.4 0.09801,3-Dichlorobenzene 0.500 25.0 2085-121101 3ug/L25.2 0.1331,3-Dichloropropane 0.500 25.0 2088-12197 3ug/L24.2 0.06701,4-Dichlorobenzene 0.200 25.0 2076-12699 16ug/L24.6 0.09702,2-Dichloropropane 20.0 50.0 2066-133110 6ug/L55.1 0.3782-Butanone (MEK) 0.200 25.0 2080-12896 3ug/L24.1 0.08802-Chlorotoluene 5.00 50.0 2070-130107 3ug/L53.5 0.3522-Hexanone 0.500 25.0 2082-13098 3ug/L24.6 0.09004-Chlorotoluene Page 28 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016LCS Dup (B6E0534-BSD1) 0.500 25.0 2080-12898 1ug/L24.4 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 2074-12997 2ug/L48.5 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 2051-143115 7ug/L57.5 0.352Acetone 0.500 25.0 2081-123111 12ug/L27.7 0.119Benzene 0.500 25.0 2084-11497 6ug/L24.3 0.132Bromobenzene 0.500 25.0 2089-12798 11ug/L24.4 0.112Bromochloromethane 0.500 25.0 2079-129108 4ug/L27.0 0.124Bromodichloromethane 2.00 25.0 2073-140116 5ug/L29.0 0.159Bromoform 1.00 25.0 2053-14390 15ug/L22.4 0.0970Bromomethane 0.500 25.0 2066-136103 7ug/L25.7 0.0990Carbon Tetrachloride 0.500 25.0 2088-11898 5ug/L24.5 0.105Chlorobenzene 1.00 25.0 2073-139110 2ug/L27.4 0.177Chlorodibromomethane 0.500 25.0 2070-12399 15ug/L24.7 0.0420Chloroethane 0.500 25.0 2072-11898 8ug/L24.5 0.172Chloroform 0.500 25.0 2065-12587 16ug/L21.7 0.0850Chloromethane 0.500 25.0 2085-12593 10ug/L23.3 0.114cis-1,2-Dichloroethene 1.00 25.0 2092-126111 4ug/L27.8 0.100cis-1,3-Dichloropropene 0.500 25.0 2048-14397 10ug/L24.2 0.0670Dichlorodifluoromethane 50.0 1000 2061-133101 11ug/L10103.00Ethanol 0.500 25.0 2087-12398 4ug/L24.5 0.0920Ethylbenzene 5.00 25.0 2077-125100 8ug/L25.0 0.0920Isopropyl Ether 0.500 25.0 2082-11598 0.9ug/L24.5 0.0980isopropylbenzene 1.00 50.0 2065-125101 7ug/L50.6 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 2075-11999 11ug/L24.8 0.190Methylene Chloride 2.00 25.0 2052-116101 11ug/L25.2 0.0940Naphthalene 2.00 25.0 2083-13096 0.6ug/L23.9 0.0600n-Butylbenzene 1.00 25.0 2084-12297 0.7ug/L24.2 0.0650n-Propylbenzene 0.500 25.0 2086-12099 4ug/L24.7 0.0920Sec-Butylbenzene 0.500 25.0 2085-123108 2ug/L27.0 0.0740Styrene 0.500 25.0 2079-12696 1ug/L24.1 0.0890tert-Butylbenzene 0.500 25.0 2064-131117 30ug/L29.3 X 0.0540Tetrachloroethene 0.500 25.0 2089-11696 6ug/L24.0 0.0570Toluene 0.500 25.0 2078-11897 10ug/L24.3 0.188trans-1,2-dichloroethene 1.00 25.0 2086-127108 7ug/L27.1 0.110trans-1,3-dichloropropene 0.500 25.0 2082-119101 4ug/L25.2 0.139Trichloroethene 0.500 25.0 2046-14493 12ug/L23.2 0.0540Trichlorofluoromethane 1.00 25.0 2058-141102 14ug/L25.5 0.720Vinyl Acetate 0.500 25.0 2076-12295 15ug/L23.8 0.0810Vinyl Chloride 1.00 50.0 2090-125100 0.8ug/L50.2 0.176m,p-Xylenes 0.500 25.0 2086-119101 2ug/L25.2 0.122o-Xylene Page 29 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016LCS Dup (B6E0534-BSD1) 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10927.2 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9824.6 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)10025.0 ug/L Prepared & Analyzed: 5/19/2016Source: A6E0085-08Matrix Spike (B6E0534-MS1) 1.00 25.0 ND 76-126101ug/L25.2 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 63-12888ug/L22.0 0.07601,1,1-Trichloroethane 0.500 25.0 ND 79-1233101ug/L25.4 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 82-126103ug/L25.8 0.1131,1,2-Trichloroethane 0.500 25.0 ND 77-12091ug/L22.7 0.1211,1-Dichloroethane 0.500 25.0 ND 67-12389ug/L22.2 0.1041,1-Dichloroethene 0.500 25.0 ND 76-126113ug/L28.3 0.06001,1-Dichloropropene 2.00 25.0 ND 41-13690ug/L22.6 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 77-12599ug/L24.8 0.1381,2,3-Trichloropropane 1.00 25.0 ND 41-13291ug/L22.8 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 53-14190ug/L22.4 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 82-130102ug/L25.6 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 83-12893ug/L23.2 0.09401,2-Dichlorobenzene 0.500 25.0 ND 59-134106ug/L26.6 0.09001,2-Dichloroethane 0.500 25.0 ND 79-125105ug/L26.1 0.1221,2-Dichloropropane 0.500 25.0 0.310 69-12589ug/L22.6 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 83-12693ug/L23.2 0.09801,3-Dichlorobenzene 0.500 25.0 ND 85-12499ug/L24.9 0.1331,3-Dichloropropane 0.500 25.0 ND 82-12192ug/L22.9 0.06701,4-Dichlorobenzene 0.200 25.0 ND 56-12279ug/L19.7 0.09702,2-Dichloropropane 20.0 50.0 ND 66-136111ug/L55.6 0.3782-Butanone (MEK) 0.200 25.0 ND 73-12991ug/L22.8 0.08802-Chlorotoluene 5.00 50.0 ND 63-140101ug/L50.3 0.3522-Hexanone 0.500 25.0 ND 76-12992ug/L23.0 0.09004-Chlorotoluene 0.500 25.0 ND 73-12691ug/L22.9 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 71-140100ug/L50.0 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 47-13889ug/L44.6 0.352Acetone 0.500 25.0 11.2 70-135103ug/L37.0 0.119Benzene 0.500 25.0 ND 76-12094ug/L23.4 0.132Bromobenzene 0.500 25.0 ND 83-13299ug/L24.8 0.112Bromochloromethane 0.500 25.0 ND 66-132109ug/L27.3 0.124Bromodichloromethane 2.00 25.0 ND 63-143108ug/L27.0 0.159Bromoform 1.00 25.0 ND 60-13489ug/L22.2 0.0970Bromomethane 0.500 25.0 ND 59-13989ug/L22.2 0.0990Carbon Tetrachloride 0.500 25.0 ND 74-12295ug/L23.7 0.105Chlorobenzene Page 30 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016Source: A6E0085-08Matrix Spike (B6E0534-MS1) 1.00 25.0 ND 68-140108ug/L27.0 0.177Chlorodibromomethane 0.500 25.0 ND 67-12594ug/L23.4 0.0420Chloroethane 0.500 25.0 ND 72-12094ug/L23.5 0.172Chloroform 0.500 25.0 ND 59-12884ug/L21.1 0.0850Chloromethane 0.500 25.0 ND 80-12591ug/L22.8 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 74-122110ug/L27.6 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 48-13898ug/L24.5 0.0670Dichlorodifluoromethane 50.0 1000 ND 55-14096ug/L9613.00Ethanol 0.500 25.0 3.50 70-14093ug/L26.7 0.0920Ethylbenzene 5.00 25.0 34.8 77-12581ug/L55.1 0.0920Isopropyl Ether 0.500 25.0 2.87 75-11790ug/L25.4 0.0980isopropylbenzene 1.00 50.0 2.97 51-15598ug/L51.9 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 75-11990ug/L22.5 0.190Methylene Chloride 2.00 25.0 ND 34-135130ug/L32.4 0.0940Naphthalene 2.00 25.0 ND 34-13592ug/L22.9 0.0600n-Butylbenzene 1.00 25.0 0.430 75-12591ug/L23.2 0.0650n-Propylbenzene 0.500 25.0 ND 77-12294ug/L23.6 0.0920Sec-Butylbenzene 0.500 25.0 ND 54-137102ug/L25.6 0.0740Styrene 0.500 25.0 ND 74-12491ug/L22.7 0.0890tert-Butylbenzene 0.500 25.0 ND 57-13076ug/L18.9 0.0540Tetrachloroethene 0.500 25.0 0.930 81-12593ug/L24.1 0.0570Toluene 0.500 25.0 ND 69-12292ug/L23.0 0.188trans-1,2-dichloroethene 1.00 25.0 ND 73-129107ug/L26.9 0.110trans-1,3-dichloropropene 0.500 25.0 ND 73-12498ug/L24.5 0.139Trichloroethene 0.500 25.0 ND 49-13985ug/L21.1 0.0540Trichlorofluoromethane 1.00 25.0 ND 57-13493ug/L23.3 0.720Vinyl Acetate 0.500 25.0 ND 70-12192ug/L23.0 0.0810Vinyl Chloride 1.00 50.0 0.570 65-15195ug/L48.2 0.176m,p-Xylenes 0.500 25.0 1.56 58-14896ug/L25.6 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10726.7 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.8 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9724.2 ug/L Page 31 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016Source: A6E0085-08Matrix Spike Dup (B6E0534-MSD1) 1.00 25.0 ND 2076-12697 3ug/L24.3 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 2063-12882 7ug/L20.5 0.07601,1,1-Trichloroethane 0.500 25.0 ND 2079-1233101 0.2ug/L25.3 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 2082-126103 0.8ug/L25.6 0.1131,1,2-Trichloroethane 0.500 25.0 ND 2077-12085 6ug/L21.4 0.1211,1-Dichloroethane 0.500 25.0 ND 2067-12395 6ug/L23.7 0.1041,1-Dichloroethene 0.500 25.0 ND 2076-126103 10ug/L25.7 0.06001,1-Dichloropropene 2.00 25.0 ND 2041-13696 6ug/L24.0 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 2077-125101 2ug/L25.3 0.1381,2,3-Trichloropropane 1.00 25.0 ND 2041-13295 4ug/L23.6 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 2053-14185 5ug/L21.3 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 2082-130103 0.5ug/L25.7 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 2083-12891 2ug/L22.8 0.09401,2-Dichlorobenzene 0.500 25.0 ND 2059-134104 3ug/L25.9 0.09001,2-Dichloroethane 0.500 25.0 ND 2079-125101 3ug/L25.3 0.1221,2-Dichloropropane 0.500 25.0 0.310 2069-12585 5ug/L21.5 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 2083-12689 4ug/L22.2 0.09801,3-Dichlorobenzene 0.500 25.0 ND 2085-124101 1ug/L25.2 0.1331,3-Dichloropropane 0.500 25.0 ND 2082-12188 4ug/L22.0 0.06701,4-Dichlorobenzene 0.200 25.0 ND 2056-12273 8ug/L18.3 0.09702,2-Dichloropropane 20.0 50.0 ND 2066-136105 6ug/L52.6 0.3782-Butanone (MEK) 0.200 25.0 ND 2073-12986 6ug/L21.5 0.08802-Chlorotoluene 5.00 50.0 ND 2063-140109 8ug/L54.4 0.3522-Hexanone 0.500 25.0 ND 2076-12987 5ug/L21.8 0.09004-Chlorotoluene 0.500 25.0 ND 2073-12687 5ug/L21.8 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 2071-140103 3ug/L51.4 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 2047-13890 1ug/L45.1 0.352Acetone 0.500 25.0 11.2 2070-13595 6ug/L35.1 0.119Benzene 0.500 25.0 ND 2076-12091 3ug/L22.7 0.132Bromobenzene 0.500 25.0 ND 2083-13296 4ug/L23.9 0.112Bromochloromethane 0.500 25.0 ND 2066-132104 5ug/L26.0 0.124Bromodichloromethane 2.00 25.0 ND 2063-143108 0.04ug/L27.0 0.159Bromoform 1.00 25.0 ND 2060-13483 6ug/L20.8 0.0970Bromomethane 0.500 25.0 ND 2059-13984 5ug/L21.1 0.0990Carbon Tetrachloride 0.500 25.0 ND 2074-12290 5ug/L22.6 0.105Chlorobenzene 1.00 25.0 ND 2068-140106 2ug/L26.4 0.177Chlorodibromomethane 0.500 25.0 ND 2067-12583 13ug/L20.7 0.0420Chloroethane 0.500 25.0 ND 2072-12089 5ug/L22.3 0.172Chloroform 0.500 25.0 ND 2059-12883 1ug/L20.9 0.0850Chloromethane 0.500 25.0 ND 2080-12589 2ug/L22.4 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 2074-122105 5ug/L26.1 0.100cis-1,3-Dichloropropene Page 32 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0534 (Continued) Prepared & Analyzed: 5/19/2016Source: A6E0085-08Matrix Spike Dup (B6E0534-MSD1) 0.500 25.0 ND 2048-13892 6ug/L23.0 0.0670Dichlorodifluoromethane 50.0 1000 ND 2055-140104 8ug/L10403.00Ethanol 0.500 25.0 3.50 2070-14087 5ug/L25.4 0.0920Ethylbenzene 5.00 25.0 34.8 2077-12577 2ug/L54.0 0.0920Isopropyl Ether 0.500 25.0 2.87 2075-11784 6ug/L24.0 0.0980isopropylbenzene 1.00 50.0 2.97 2051-15598 0.02ug/L51.9 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 2075-11994 4ug/L23.5 0.190Methylene Chloride 2.00 25.0 ND 2034-135145 12ug/L36.4 X 0.0940Naphthalene 2.00 25.0 ND 2034-13587 5ug/L21.8 0.0600n-Butylbenzene 1.00 25.0 0.430 2075-12585 7ug/L21.7 0.0650n-Propylbenzene 0.500 25.0 ND 2077-12288 7ug/L22.1 0.0920Sec-Butylbenzene 0.500 25.0 ND 2054-13798 4ug/L24.6 0.0740Styrene 0.500 25.0 ND 2074-12486 6ug/L21.4 0.0890tert-Butylbenzene 0.500 25.0 ND 2057-13071 7ug/L17.6 0.0540Tetrachloroethene 0.500 25.0 0.930 2081-12588 5ug/L22.8 0.0570Toluene 0.500 25.0 ND 2069-12288 4ug/L22.0 0.188trans-1,2-dichloroethene 1.00 25.0 ND 2073-129106 2ug/L26.4 0.110trans-1,3-dichloropropene 0.500 25.0 ND 2073-12491 7ug/L22.7 0.139Trichloroethene 0.500 25.0 ND 2049-13982 3ug/L20.5 0.0540Trichlorofluoromethane 1.00 25.0 ND 2057-13499 5ug/L24.6 0.720Vinyl Acetate 0.500 25.0 ND 2070-12190 3ug/L22.4 0.0810Vinyl Chloride 1.00 50.0 0.570 2065-15191 5ug/L45.9 0.176m,p-Xylenes 0.500 25.0 1.56 2058-14893 4ug/L24.7 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10426.0 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9824.5 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9724.3 ug/L Page 33 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 Prepared & Analyzed: 5/20/2016Blank (B6E0562-BLK1) 1.00 ug/L0.180 U 0.1801,1,1,2-Tetrachloroethane 0.500 ug/L0.0760 U 0.07601,1,1-Trichloroethane 0.500 ug/L0.0700 U 0.07001,1,2,2-Tetrachloroethane 0.500 ug/L0.113 U 0.1131,1,2-Trichloroethane 0.500 ug/L0.121 U 0.1211,1-Dichloroethane 0.500 ug/L0.104 U 0.1041,1-Dichloroethene 0.500 ug/L0.0600 U 0.06001,1-Dichloropropene 2.00 ug/L0.118 U 0.1181,2,3-Trichlorobenzene 1.00 ug/L0.138 U 0.1381,2,3-Trichloropropane 1.00 ug/L0.0690 U 0.06901,2,4-Trichlorobenzene 0.500 ug/L0.103 U 0.1031,2,4-Trimethylbenzene 1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB) 0.500 ug/L0.0940 U 0.09401,2-Dichlorobenzene 0.500 ug/L0.0900 U 0.09001,2-Dichloroethane 0.500 ug/L0.122 U 0.1221,2-Dichloropropane 0.500 ug/L0.0870 U 0.08701,3,5-trimethylbenzene 0.500 ug/L0.0980 U 0.09801,3-Dichlorobenzene 0.500 ug/L0.133 U 0.1331,3-Dichloropropane 0.500 ug/L0.0670 U 0.06701,4-Dichlorobenzene 0.200 ug/L0.0970 U 0.09702,2-Dichloropropane 20.0 ug/L0.378 U 0.3782-Butanone (MEK) 0.200 ug/L0.0880 U 0.08802-Chlorotoluene 5.00 ug/L0.352 U 0.3522-Hexanone 0.500 ug/L0.0900 U 0.09004-Chlorotoluene 0.500 ug/L0.0890 U 0.08904-Isopropyltoluene (p-Cymene) 5.00 ug/L0.253 U 0.2534-Methyl-2-pentanone (MIBK) 5.00 ug/L0.352 U 0.352Acetone 0.500 ug/L0.119 U 0.119Benzene 0.500 ug/L0.132 U 0.132Bromobenzene 0.500 ug/L0.112 U 0.112Bromochloromethane 0.500 ug/L0.124 U 0.124Bromodichloromethane 2.00 ug/L0.159 U 0.159Bromoform 1.00 ug/L0.0970 U 0.0970Bromomethane 0.500 ug/L0.0990 U 0.0990Carbon Tetrachloride 0.500 ug/L0.105 U 0.105Chlorobenzene 1.00 ug/L0.177 U 0.177Chlorodibromomethane 0.500 ug/L0.0420 U 0.0420Chloroethane 0.500 ug/L0.172 U 0.172Chloroform 0.500 ug/L0.0850 U 0.0850Chloromethane 0.500 ug/L0.114 U 0.114cis-1,2-Dichloroethene 1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene Page 34 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016Blank (B6E0562-BLK1) 0.500 ug/L0.0670 U 0.0670Dichlorodifluoromethane 50.0 ug/L3.00 U 3.00Ethanol 0.500 ug/L0.0920 U 0.0920Ethylbenzene 5.00 ug/L0.0920 U 0.0920Isopropyl Ether 0.500 ug/L0.0980 U 0.0980isopropylbenzene 1.00 ug/L0.169 U 0.169Methyl tert-butyl ether (MTBE) 0.500 ug/L0.190 U 0.190Methylene Chloride 2.00 ug/L0.0940 U 0.0940Naphthalene 2.00 ug/L0.0600 U 0.0600n-Butylbenzene 1.00 ug/L0.0650 U 0.0650n-Propylbenzene 0.500 ug/L0.0920 U 0.0920Sec-Butylbenzene 0.500 ug/L0.0740 U 0.0740Styrene 0.500 ug/L0.0890 U 0.0890tert-Butylbenzene 0.500 ug/L0.0540 U 0.0540Tetrachloroethene 0.500 ug/L0.0570 U 0.0570Toluene 0.500 ug/L0.188 U 0.188trans-1,2-dichloroethene 1.00 ug/L0.110 U 0.110trans-1,3-dichloropropene 0.500 ug/L0.139 U 0.139Trichloroethene 0.500 ug/L0.0540 U 0.0540Trichlorofluoromethane 1.00 ug/L0.720 U 0.720Vinyl Acetate 0.500 ug/L0.0810 U 0.0810Vinyl Chloride 1.00 ug/L0.176 U 0.176m,p-Xylenes 0.500 ug/L0.122 U 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10426.0 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)10426.0 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9523.8 ug/L Prepared & Analyzed: 5/20/2016LCS (B6E0562-BS1) 1.00 25.0 75-127117ug/L29.2 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 62-128109ug/L27.2 0.07601,1,1-Trichloroethane 0.500 25.0 77-129113ug/L28.4 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 86-120117ug/L29.2 0.1131,1,2-Trichloroethane 0.500 25.0 82-114112ug/L28.1 0.1211,1-Dichloroethane 0.500 25.0 73-123113ug/L28.3 0.1041,1-Dichloroethene 0.500 25.0 83-125114ug/L28.6 0.06001,1-Dichloropropene 2.00 25.0 57-127111ug/L27.9 0.1181,2,3-Trichlorobenzene 1.00 25.0 79-118108ug/L27.0 0.1381,2,3-Trichloropropane 1.00 25.0 59-125113ug/L28.2 0.06901,2,4-Trichlorobenzene 0.500 25.0 84-118105ug/L26.1 0.1031,2,4-Trimethylbenzene 1.00 25.0 83-126117ug/L29.3 0.1801,2-Dibromoethane (EDB) Page 35 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016LCS (B6E0562-BS1) 0.500 25.0 83-128108ug/L27.0 0.09401,2-Dichlorobenzene 0.500 25.0 56-133123ug/L30.8 0.09001,2-Dichloroethane 0.500 25.0 85-121119ug/L29.8 0.1221,2-Dichloropropane 0.500 25.0 86-118105ug/L26.4 0.08701,3,5-trimethylbenzene 0.500 25.0 90-126109ug/L27.2 0.09801,3-Dichlorobenzene 0.500 25.0 85-121114ug/L28.5 0.1331,3-Dichloropropane 0.500 25.0 88-121108ug/L27.1 0.06701,4-Dichlorobenzene 0.200 25.0 76-126118ug/L29.6 0.09702,2-Dichloropropane 20.0 50.0 66-133114ug/L57.2 0.3782-Butanone (MEK) 0.200 25.0 80-128107ug/L26.7 0.08802-Chlorotoluene 5.00 50.0 70-130121ug/L60.7 0.3522-Hexanone 0.500 25.0 82-130108ug/L27.0 0.09004-Chlorotoluene 0.500 25.0 80-128109ug/L27.3 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 74-129116ug/L57.8 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 51-143127ug/L63.7 0.352Acetone 0.500 25.0 81-123110ug/L27.4 0.119Benzene 0.500 25.0 84-114108ug/L27.0 0.132Bromobenzene 0.500 25.0 89-127118ug/L29.6 0.112Bromochloromethane 0.500 25.0 79-129124ug/L31.1 0.124Bromodichloromethane 2.00 25.0 73-140122ug/L30.4 0.159Bromoform 1.00 25.0 53-143111ug/L27.7 0.0970Bromomethane 0.500 25.0 66-136112ug/L28.0 0.0990Carbon Tetrachloride 0.500 25.0 88-118109ug/L27.2 0.105Chlorobenzene 1.00 25.0 73-139122ug/L30.4 0.177Chlorodibromomethane 0.500 25.0 70-123122ug/L30.4 0.0420Chloroethane 0.500 25.0 72-118116ug/L29.0 0.172Chloroform 0.500 25.0 65-125107ug/L26.7 0.0850Chloromethane 0.500 25.0 85-125111ug/L27.6 0.114cis-1,2-Dichloroethene 1.00 25.0 92-126128ug/L32.1 X 0.100cis-1,3-Dichloropropene 0.500 25.0 48-143115ug/L28.7 0.0670Dichlorodifluoromethane 50.0 1000 61-133114ug/L11403.00Ethanol 0.500 25.0 87-123111ug/L27.7 0.0920Ethylbenzene 5.00 25.0 77-125116ug/L29.0 0.0920Isopropyl Ether 0.500 25.0 82-115106ug/L26.6 0.0980isopropylbenzene 1.00 50.0 65-125119ug/L59.3 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 75-119119ug/L29.8 0.190Methylene Chloride 2.00 25.0 52-116123ug/L30.6 X 0.0940Naphthalene 2.00 25.0 83-130109ug/L27.4 0.0600n-Butylbenzene 1.00 25.0 84-122108ug/L27.0 0.0650n-Propylbenzene 0.500 25.0 86-120108ug/L27.0 0.0920Sec-Butylbenzene 0.500 25.0 85-123119ug/L29.8 0.0740Styrene Page 36 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016LCS (B6E0562-BS1) 0.500 25.0 79-126105ug/L26.4 0.0890tert-Butylbenzene 0.500 25.0 64-13195ug/L23.7 0.0540Tetrachloroethene 0.500 25.0 89-116105ug/L26.4 0.0570Toluene 0.500 25.0 78-118115ug/L28.6 0.188trans-1,2-dichloroethene 1.00 25.0 86-127126ug/L31.4 0.110trans-1,3-dichloropropene 0.500 25.0 82-119114ug/L28.5 0.139Trichloroethene 0.500 25.0 46-144103ug/L25.8 0.0540Trichlorofluoromethane 1.00 25.0 58-141136ug/L34.0 0.720Vinyl Acetate 0.500 25.0 76-122115ug/L28.6 0.0810Vinyl Chloride 1.00 50.0 90-125112ug/L55.8 0.176m,p-Xylenes 0.500 25.0 86-119111ug/L27.8 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10826.9 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.7 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9523.8 ug/L Prepared & Analyzed: 5/20/2016LCS Dup (B6E0562-BSD1) 1.00 25.0 2075-127111 5ug/L27.8 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 2062-128116 7ug/L29.0 0.07601,1,1-Trichloroethane 0.500 25.0 2077-129102 10ug/L25.6 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 2086-120111 5ug/L27.7 0.1131,1,2-Trichloroethane 0.500 25.0 2082-114108 4ug/L27.0 0.1211,1-Dichloroethane 0.500 25.0 2073-123107 6ug/L26.7 0.1041,1-Dichloroethene 0.500 25.0 2083-125109 5ug/L27.2 0.06001,1-Dichloropropene 2.00 25.0 2057-12798 13ug/L24.5 0.1181,2,3-Trichlorobenzene 1.00 25.0 2079-118104 4ug/L25.9 0.1381,2,3-Trichloropropane 1.00 25.0 2059-125100 12ug/L25.0 0.06901,2,4-Trichlorobenzene 0.500 25.0 2084-118100 5ug/L25.0 0.1031,2,4-Trimethylbenzene 1.00 25.0 2083-126110 7ug/L27.4 0.1801,2-Dibromoethane (EDB) 0.500 25.0 2083-128102 6ug/L25.4 0.09401,2-Dichlorobenzene 0.500 25.0 2056-133118 4ug/L29.5 0.09001,2-Dichloroethane 0.500 25.0 2085-121115 3ug/L28.8 0.1221,2-Dichloropropane 0.500 25.0 2086-11899 6ug/L24.8 0.08701,3,5-trimethylbenzene 0.500 25.0 2090-126101 7ug/L25.3 0.09801,3-Dichlorobenzene 0.500 25.0 2085-121106 8ug/L26.4 0.1331,3-Dichloropropane 0.500 25.0 2088-121101 6ug/L25.4 0.06701,4-Dichlorobenzene 0.200 25.0 2076-126112 6ug/L27.9 0.09702,2-Dichloropropane 20.0 50.0 2066-133113 0.8ug/L56.7 0.3782-Butanone (MEK) 0.200 25.0 2080-128102 4ug/L25.5 0.08802-Chlorotoluene 5.00 50.0 2070-130114 6ug/L57.2 0.3522-Hexanone 0.500 25.0 2082-130103 5ug/L25.7 0.09004-Chlorotoluene Page 37 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016LCS Dup (B6E0562-BSD1) 0.500 25.0 2080-128102 7ug/L25.5 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 2074-129114 2ug/L56.8 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 2051-143109 16ug/L54.5 0.352Acetone 0.500 25.0 2081-123123 11ug/L30.7 0.119Benzene 0.500 25.0 2084-114102 5ug/L25.5 0.132Bromobenzene 0.500 25.0 2089-127114 4ug/L28.5 0.112Bromochloromethane 0.500 25.0 2079-129121 3ug/L30.2 0.124Bromodichloromethane 2.00 25.0 2073-140114 6ug/L28.6 0.159Bromoform 1.00 25.0 2053-143102 8ug/L25.6 0.0970Bromomethane 0.500 25.0 2066-136114 2ug/L28.5 0.0990Carbon Tetrachloride 0.500 25.0 2088-118104 4ug/L26.0 0.105Chlorobenzene 1.00 25.0 2073-139112 8ug/L28.1 0.177Chlorodibromomethane 0.500 25.0 2070-123110 10ug/L27.5 0.0420Chloroethane 0.500 25.0 2072-118111 5ug/L27.7 0.172Chloroform 0.500 25.0 2065-12598 9ug/L24.4 0.0850Chloromethane 0.500 25.0 2085-125109 1ug/L27.3 0.114cis-1,2-Dichloroethene 1.00 25.0 2092-126124 3ug/L31.0 0.100cis-1,3-Dichloropropene 0.500 25.0 2048-14399 15ug/L24.6 0.0670Dichlorodifluoromethane 50.0 1000 2061-133104 9ug/L10403.00Ethanol 0.500 25.0 2087-123104 6ug/L26.1 0.0920Ethylbenzene 5.00 25.0 2077-125111 5ug/L27.7 0.0920Isopropyl Ether 0.500 25.0 2082-115101 5ug/L25.4 0.0980isopropylbenzene 1.00 50.0 2065-125114 4ug/L57.0 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 2075-119113 5ug/L28.3 0.190Methylene Chloride 2.00 25.0 2052-116103 18ug/L25.7 0.0940Naphthalene 2.00 25.0 2083-130103 7ug/L25.6 0.0600n-Butylbenzene 1.00 25.0 2084-122101 6ug/L25.3 0.0650n-Propylbenzene 0.500 25.0 2086-120102 6ug/L25.6 0.0920Sec-Butylbenzene 0.500 25.0 2085-123114 5ug/L28.4 0.0740Styrene 0.500 25.0 2079-126100 5ug/L25.1 0.0890tert-Butylbenzene 0.500 25.0 2064-131135 35ug/L33.8 X 0.0540Tetrachloroethene 0.500 25.0 2089-116101 4ug/L25.3 0.0570Toluene 0.500 25.0 2078-118110 4ug/L27.5 0.188trans-1,2-dichloroethene 1.00 25.0 2086-127112 12ug/L28.0 0.110trans-1,3-dichloropropene 0.500 25.0 2082-119115 1ug/L28.8 0.139Trichloroethene 0.500 25.0 2046-144105 2ug/L26.2 0.0540Trichlorofluoromethane 1.00 25.0 2058-141102 29ug/L25.5 X 0.720Vinyl Acetate 0.500 25.0 2076-122104 10ug/L25.9 0.0810Vinyl Chloride 1.00 50.0 2090-125106 5ug/L53.0 0.176m,p-Xylenes 0.500 25.0 2086-119105 5ug/L26.3 0.122o-Xylene Page 38 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016LCS Dup (B6E0562-BSD1) 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10827.0 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.7 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9423.4 ug/L Prepared & Analyzed: 5/20/2016Source: A6E0087-03Matrix Spike (B6E0562-MS1) 1.00 25.0 ND 76-126101ug/L25.1 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 63-128104ug/L25.9 0.07601,1,1-Trichloroethane 0.500 25.0 ND 79-123397ug/L24.2 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 82-126102ug/L25.6 0.1131,1,2-Trichloroethane 0.500 25.0 ND 77-120104ug/L26.0 0.1211,1-Dichloroethane 0.500 25.0 ND 67-123100ug/L24.9 0.1041,1-Dichloroethene 0.500 25.0 ND 76-126106ug/L26.6 0.06001,1-Dichloropropene 2.00 25.0 ND 41-13685ug/L21.2 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 77-12592ug/L23.0 0.1381,2,3-Trichloropropane 1.00 25.0 ND 41-13288ug/L21.9 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 53-14191ug/L22.6 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 82-130101ug/L25.4 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 83-12893ug/L23.3 0.09401,2-Dichlorobenzene 0.500 25.0 ND 59-134114ug/L28.4 0.09001,2-Dichloroethane 0.500 25.0 ND 79-125114ug/L28.4 0.1221,2-Dichloropropane 0.500 25.0 ND 69-12592ug/L23.1 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 83-12693ug/L23.4 0.09801,3-Dichlorobenzene 0.500 25.0 ND 85-124101ug/L25.1 0.1331,3-Dichloropropane 0.500 25.0 ND 82-12193ug/L23.3 0.06701,4-Dichlorobenzene 0.200 25.0 ND 56-122111ug/L27.7 0.09702,2-Dichloropropane 20.0 50.0 ND 66-136107ug/L53.7 0.3782-Butanone (MEK) 0.200 25.0 ND 73-12994ug/L23.5 0.08802-Chlorotoluene 5.00 50.0 ND 63-14096ug/L47.8 0.3522-Hexanone 0.500 25.0 ND 76-12997ug/L24.2 0.09004-Chlorotoluene 0.500 25.0 ND 73-12695ug/L23.7 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 71-14098ug/L49.2 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 47-13898ug/L49.0 0.352Acetone 0.500 25.0 ND 70-135117ug/L29.2 0.119Benzene 0.500 25.0 ND 76-12094ug/L23.5 0.132Bromobenzene 0.500 25.0 ND 83-132110ug/L27.4 0.112Bromochloromethane 0.500 25.0 ND 66-132115ug/L28.7 0.124Bromodichloromethane 2.00 25.0 ND 63-143102ug/L25.5 0.159Bromoform 1.00 25.0 ND 60-13495ug/L23.7 0.0970Bromomethane 0.500 25.0 ND 59-139111ug/L27.8 0.0990Carbon Tetrachloride 0.500 25.0 ND 74-12297ug/L24.3 0.105Chlorobenzene Page 39 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016Source: A6E0087-03Matrix Spike (B6E0562-MS1) 1.00 25.0 ND 68-140104ug/L26.0 0.177Chlorodibromomethane 0.500 25.0 ND 67-125103ug/L25.8 0.0420Chloroethane 0.500 25.0 ND 72-120108ug/L26.9 0.172Chloroform 0.500 25.0 ND 59-12892ug/L22.9 0.0850Chloromethane 0.500 25.0 ND 80-125106ug/L26.5 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 74-122118ug/L29.5 0.100cis-1,3-Dichloropropene 0.500 25.0 ND 48-13893ug/L23.2 0.0670Dichlorodifluoromethane 50.0 1000 ND 55-14098ug/L9823.00Ethanol 0.500 25.0 ND 70-14098ug/L24.5 0.0920Ethylbenzene 5.00 25.0 ND 77-125104ug/L26.1 0.0920Isopropyl Ether 0.500 25.0 ND 75-11794ug/L23.6 0.0980isopropylbenzene 1.00 50.0 ND 51-155104ug/L51.9 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 75-119106ug/L26.6 0.190Methylene Chloride 2.00 25.0 ND 34-13585ug/L21.1 0.0940Naphthalene 2.00 25.0 ND 34-13594ug/L23.6 0.0600n-Butylbenzene 1.00 25.0 ND 75-12595ug/L23.7 0.0650n-Propylbenzene 0.500 25.0 ND 77-12295ug/L23.6 0.0920Sec-Butylbenzene 0.500 25.0 ND 54-137106ug/L26.4 0.0740Styrene 0.500 25.0 ND 74-12493ug/L23.2 0.0890tert-Butylbenzene 0.500 25.0 ND 57-13078ug/L19.5 0.0540Tetrachloroethene 0.500 25.0 ND 81-12595ug/L23.8 0.0570Toluene 0.500 25.0 ND 69-122103ug/L25.8 0.188trans-1,2-dichloroethene 1.00 25.0 ND 73-129108ug/L26.9 0.110trans-1,3-dichloropropene 0.500 25.0 ND 73-124106ug/L26.4 0.139Trichloroethene 0.500 25.0 ND 49-13994ug/L23.6 0.0540Trichlorofluoromethane 1.00 25.0 ND 57-134121ug/L30.2 0.720Vinyl Acetate 0.500 25.0 ND 70-12198ug/L24.4 0.0810Vinyl Chloride 1.00 50.0 ND 65-15197ug/L48.5 0.176m,p-Xylenes 0.500 25.0 ND 58-14898ug/L24.6 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10626.4 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9924.7 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9323.4 ug/L Page 40 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016Source: A6E0087-03Matrix Spike Dup (B6E0562-MSD1) 1.00 25.0 ND 2076-126104 3ug/L26.0 0.1801,1,1,2-Tetrachloroethane 0.500 25.0 ND 2063-128109 5ug/L27.2 0.07601,1,1-Trichloroethane 0.500 25.0 ND 2079-1233101 5ug/L25.4 0.07001,1,2,2-Tetrachloroethane 0.500 25.0 ND 2082-126106 3ug/L26.5 0.1131,1,2-Trichloroethane 0.500 25.0 ND 2077-120106 2ug/L26.4 0.1211,1-Dichloroethane 0.500 25.0 ND 2067-123106 6ug/L26.5 0.1041,1-Dichloroethene 0.500 25.0 ND 2076-126104 3ug/L25.9 0.06001,1-Dichloropropene 2.00 25.0 ND 2041-13697 13ug/L24.3 0.1181,2,3-Trichlorobenzene 1.00 25.0 ND 2077-12598 7ug/L24.6 0.1381,2,3-Trichloropropane 1.00 25.0 ND 2041-13298 11ug/L24.4 0.06901,2,4-Trichlorobenzene 0.500 25.0 ND 2053-14193 3ug/L23.4 0.1031,2,4-Trimethylbenzene 1.00 25.0 ND 2082-130106 4ug/L26.4 0.1801,2-Dibromoethane (EDB) 0.500 25.0 ND 2083-12895 2ug/L23.7 0.09401,2-Dichlorobenzene 0.500 25.0 ND 2059-134117 3ug/L29.1 0.09001,2-Dichloroethane 0.500 25.0 ND 2079-125114 0.5ug/L28.5 0.1221,2-Dichloropropane 0.500 25.0 ND 2069-12593 0.9ug/L23.3 0.08701,3,5-trimethylbenzene 0.500 25.0 ND 2083-12695 2ug/L23.8 0.09801,3-Dichlorobenzene 0.500 25.0 ND 2085-124105 4ug/L26.2 0.1331,3-Dichloropropane 0.500 25.0 ND 2082-12195 2ug/L23.7 0.06701,4-Dichlorobenzene 0.200 25.0 ND 2056-122110 0.8ug/L27.5 0.09702,2-Dichloropropane 20.0 50.0 ND 2066-136113 5ug/L56.7 0.3782-Butanone (MEK) 0.200 25.0 ND 2073-12996 2ug/L23.9 0.08802-Chlorotoluene 5.00 50.0 ND 2063-140103 7ug/L51.3 0.3522-Hexanone 0.500 25.0 ND 2076-12997 0.5ug/L24.3 0.09004-Chlorotoluene 0.500 25.0 ND 2073-12696 1ug/L24.0 0.08904-Isopropyltoluene (p-Cymene) 5.00 50.0 ND 2071-140106 8ug/L53.1 0.2534-Methyl-2-pentanone (MIBK) 5.00 50.0 ND 2047-138102 4ug/L51.2 0.352Acetone 0.500 25.0 ND 2070-135118 1ug/L29.5 0.119Benzene 0.500 25.0 ND 2076-12096 3ug/L24.1 0.132Bromobenzene 0.500 25.0 ND 2083-132112 3ug/L28.1 0.112Bromochloromethane 0.500 25.0 ND 2066-132117 2ug/L29.2 0.124Bromodichloromethane 2.00 25.0 ND 2063-143108 6ug/L27.0 0.159Bromoform 1.00 25.0 ND 2060-134102 7ug/L25.4 0.0970Bromomethane 0.500 25.0 ND 2059-139110 1ug/L27.4 0.0990Carbon Tetrachloride 0.500 25.0 ND 2074-12299 2ug/L24.8 0.105Chlorobenzene 1.00 25.0 ND 2068-140108 4ug/L27.1 0.177Chlorodibromomethane 0.500 25.0 ND 2067-125110 6ug/L27.5 0.0420Chloroethane 0.500 25.0 ND 2072-120106 1ug/L26.6 0.172Chloroform 0.500 25.0 ND 2059-12897 5ug/L24.2 0.0850Chloromethane 0.500 25.0 ND 2080-125106 0.2ug/L26.4 0.114cis-1,2-Dichloroethene 1.00 25.0 ND 2074-122121 3ug/L30.3 0.100cis-1,3-Dichloropropene Page 41 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD LimitQual Analyte Quality Control (Continued) VOCs by NC Method 6200B (Continued) MDL Batch: B6E0562 (Continued) Prepared & Analyzed: 5/20/2016Source: A6E0087-03Matrix Spike Dup (B6E0562-MSD1) 0.500 25.0 ND 2048-13894 2ug/L23.6 0.0670Dichlorodifluoromethane 50.0 1000 ND 2055-140115 16ug/L11503.00Ethanol 0.500 25.0 ND 2070-14098 0.5ug/L24.6 0.0920Ethylbenzene 5.00 25.0 ND 2077-125108 3ug/L27.0 0.0920Isopropyl Ether 0.500 25.0 ND 2075-11795 0.9ug/L23.8 0.0980isopropylbenzene 1.00 50.0 ND 2051-155111 7ug/L55.5 0.169Methyl tert-butyl ether (MTBE) 0.500 25.0 ND 2075-119110 3ug/L27.4 0.190Methylene Chloride 2.00 25.0 ND 2034-135106 23ug/L26.6 X 0.0940Naphthalene 2.00 25.0 ND 2034-13597 2ug/L24.2 0.0600n-Butylbenzene 1.00 25.0 ND 2075-12595 0.08ug/L23.7 0.0650n-Propylbenzene 0.500 25.0 ND 2077-12296 1ug/L23.9 0.0920Sec-Butylbenzene 0.500 25.0 ND 2054-137107 1ug/L26.8 0.0740Styrene 0.500 25.0 ND 2074-12494 1ug/L23.5 0.0890tert-Butylbenzene 0.500 25.0 ND 2057-13077 1ug/L19.2 0.0540Tetrachloroethene 0.500 25.0 ND 2081-12597 1ug/L24.1 0.0570Toluene 0.500 25.0 ND 2069-122106 3ug/L26.6 0.188trans-1,2-dichloroethene 1.00 25.0 ND 2073-129111 4ug/L27.9 0.110trans-1,3-dichloropropene 0.500 25.0 ND 2073-124106 0.08ug/L26.4 0.139Trichloroethene 0.500 25.0 ND 2049-139102 8ug/L25.5 0.0540Trichlorofluoromethane 1.00 25.0 ND 2057-134125 3ug/L31.3 0.720Vinyl Acetate 0.500 25.0 ND 2070-121104 6ug/L25.9 0.0810Vinyl Chloride 1.00 50.0 ND 2065-151100 3ug/L50.2 0.176m,p-Xylenes 0.500 25.0 ND 2058-14899 0.6ug/L24.7 0.122o-Xylene 25.0 65-126Surrogate: 1,2-Dichloroethane-D4 (SUR)10726.7 ug/L 25.0 86-111Surrogate: 4-Bromofluorobenzene (SUR)9824.6 ug/L 25.0 83-116Surrogate: Toluene-D8 (SUR)9623.9 ug/L Page 42 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety. Project: Project Number: Project Manager: Reported: Terraquest Environmental Consultants-Mebane 100 E. Ruffin Street Hollars Grocery 02001 Ryan Kerins 5/26/16 9:54 MWBE SDBE NELAC DoD Accredited Mebane, NC 27302 List of Certifications for FTS Analytical Services - Atlanta CodeDescriptionNumber ExpiresFacility LANELAC04176LA CERTIFICATE 06/30/2016FTSA ANC483NC CERTIFICATE 12/31/2016FTSA KENTUKY85KENTUKY CERTIFICATE FTSA ASC98015SC CERTIFICATE 06/30/2016FTSA LFLNELACE84098FL NELAC CERTIFICATE 06/30/2016FTSL AFLNELACE87429FL NELAC CERTIFICATE 06/30/2016FTSA DODLI0-135 DoD CERTIFICATE 06/30/2016FTSA USDAP330-07-00105 USDA CERTIFICATE FTSA Notes and Definitions Item Definition RPD Failure in the BKS/BSD.F The LCS data for this analytical batch was reported above the laboratory control limits.H Dry Sample results reported on a dry weight basis. U Analyte NOT DETECTED at or above the reporting limit. A Suspected adol-condensation product. B Analyte detected in the method blank. C Confirmed by GC/MS analysis. E Concentration exceeds calibration range. K Hold Time exceeded. N Tentatively Identified Compound. P >25% difference between primary and secondary columns. S Quantitation based on single-point calibration. X General QC Failure see Case Narrative. J The target analyte was positively identified below the Reporting Limit and above the Method Detection Limit. RPD Relative Percent Difference %REC Percent Recovery Source Sample that was matrix spiked or duplicated. Page 43 of 44 The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document. No duplication of this report is allowed, except in its entirety.