WS-2805_6783_CA_RMR_20151203

Analytical Report 519903
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Hollar's Grocery
02-DEC-15
02001
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 41 Final 1.001

Page 2 of 41 Final 1.001
Table of Contents
Cover Page 1
Cover Letter 3
Sample ID Cross Reference 4
Explanation of Qualifiers (Flags) 5
Hits Summary 6
Certificate of Analysis (Detailed Report) 10
Summary of Quality control 28
Blank Summary 34
Chain of Custody 39
Sample Receipt Conformance Report 41
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 519903
Hollar's Grocery
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 519903. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 519903 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
02-DEC-15
Chad Bechtold
Page 3 of 41 Final 1.001
Sample Cross Reference 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
Sample Id
MWA
MWB/RW4
MWN
MWT
VERW1
VERW2/RW3
RW5
RW7
SWN
11-18-15 13:48
11-18-15 13:42
11-18-15 13:10
11-18-15 13:03
11-18-15 13:37
11-18-15 13:18
11-18-15 13:29
11-18-15 12:44
11-18-15 12:50
Date Collected Lab Sample Id
519903-001
519903-002
519903-003
519903-004
519903-005
519903-006
519903-007
519903-008
519903-009

Sample DepthMatrix
W
W
W
W
W
W
W
W
W
Page 4 of 41 Final 1.001
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 5 of 41 Final 1.001
Hits Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42
11.20.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.18.15 13.48
11.18.15 13.42
Date Collected :
Date Collected :
519903-001
519903-002
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MWA
MWB/RW4
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
Prep Method:
11.25.15 23.40
11.25.15 23.40
11.27.15 11.24
Date Prep:
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
4-Isopropyltoluene
Isopropylbenzene
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Toluene
Acetone
Benzene
Methyl tert-butyl ether (MTBE)
sec-Butylbenzene
Isopropyl ether
Parameter
Parameter
Parameter
Result
Result
Result
J
D
Flag
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
10
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
95-63-6
108-67-8
99-87-6
98-82-8
91-20-3
104-51-8
103-65-1
135-98-8
108-88-3
67-64-1
71-43-2
1634-04-4
135-98-8
108-20-3
18.2
7.76
0.230
0.780
9.84
2.68
4.25
0.680
31.3
106
0.560
38.4
1.52
288
982275
982275
982275
Seq Number
Seq Number
Seq Number
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.27.15 20.03
Analysis Date
Analysis Date
Analysis Date
Page 6 of 41 Final 1.001
Hits Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42
11.20.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.18.15 13.10
11.18.15 13.03
Date Collected :
Date Collected :
519903-003
519903-004
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MWN
MWT
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
Prep Method:
11.25.15 23.40
11.27.15 11.24
11.25.15 23.40
Date Prep:
Date Prep:
Date Prep:
1,2-Dichloroethane
Benzene
Isopropylbenzene
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
o-Xylene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Methyl tert-butyl ether (MTBE)
Parameter
Parameter
Parameter
Result
Result
Result
J
J
J
D
D
Flag
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
Units
1
1
1
1
1
1
1
1
50
50
1
Dil
Dil
Dil
Cas Number
Cas Number
Cas Number
107-06-2
71-43-2
98-82-8
91-20-3
104-51-8
103-65-1
135-98-8
95-47-6
108-20-3
1634-04-4
1634-04-4
73.0
72.6
5.61
8.10
0.310
0.160
0.450
0.620
1330
305
4.02
982275
982275
982275
Seq Number
Seq Number
Seq Number
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.27.15 20.32
11.27.15 20.32
11.26.15 09.33
Analysis Date
Analysis Date
Analysis Date
Page 7 of 41 Final 1.001
Hits Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received :
% Moisture :
11.18.15 13.37 Date Collected : 519903-005Lab Sample Id :
Ground WaterMatrix : VERW1Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.25.15 23.40
11.30.15 06.34
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
4-Isopropyltoluene
Acetone
Benzene
Ethylbenzene
Isopropylbenzene
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Toluene
m,p-Xylenes
o-Xylene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Parameter
Parameter
Result
Result
J
J
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
50
50
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
99-87-6
67-64-1
71-43-2
100-41-4
98-82-8
91-20-3
104-51-8
103-65-1
135-98-8
108-88-3
179601-23-1
95-47-6
108-20-3
1634-04-4
22.7
3.11
0.240
115
75.7
68.9
4.15
14.8
0.800
7.98
0.780
2.24
10.7
2.37
1450
1000
982275
982275
Seq Number
Seq Number
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.30.15 12.38
11.30.15 12.38
Analysis Date
Analysis Date
Page 8 of 41 Final 1.001
Hits Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42
11.20.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.18.15 13.18
11.18.15 12.44
Date Collected :
Date Collected :
519903-006
519903-008
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
VERW2/RW3
RW7
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.27.15 11.24
11.27.15 11.24
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
4-Isopropyltoluene
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Toluene
m,p-Xylenes
2-Butanone (MEK)
4-Isopropyltoluene
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
J
J
X
J
J
J
J
J
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
10
1
10
1
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
99-87-6
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
108-88-3
179601-23-1
78-93-3
99-87-6
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
104-51-8
103-65-1
135-98-8
108-88-3
179601-23-1
95-47-6
0.230
0.200
0.520
0.750
1.90
4.65
5.03
3.05
7.96
1.60
2.07
5.04
0.210
0.130
0.420
0.410
26.6
1.04
183
44.5
355
24.0
32.8
77.1
2.41
9.17
2.43
12.9
4.76
2.77
982291
982291
Seq Number
Seq Number
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 20.59
11.27.15 20.59
11.27.15 21.28
11.27.15 20.59
11.27.15 21.28
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
Analysis Date
Analysis Date
Page 9 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.48 Date Collected:519903-001Lab Sample Id:
Ground WaterMatrix: MWASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
18.2
U
U
U
U
7.76
U
U
U
U
U
U
U
U
0.230
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
Analysis Date
% Moisture:
Page 10 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.48 Date Collected:519903-001Lab Sample Id:
Ground WaterMatrix: MWASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
0.780
U
U
9.84
2.68
4.25
0.680
U
U
U
31.3
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
110
103
110
11.26.15 07.59
11.26.15 07.59
11.26.15 07.59
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 11 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.42 Date Collected:519903-002Lab Sample Id:
Ground WaterMatrix: MWB/RW4Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
106
0.560
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
Analysis Date
% Moisture:
Page 12 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.42 Date Collected:519903-002Lab Sample Id:
Ground WaterMatrix: MWB/RW4Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
5.00
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
288
U
38.4
U
U
U
U
1.52
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.27.15 20.03
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
104
108
105
11.26.15 08.30
11.26.15 08.30
11.26.15 08.30
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 13 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.10 Date Collected:519903-003Lab Sample Id:
Ground WaterMatrix: MWNSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
73.0
U
U
U
U
U
U
U
U
U
U
U
U
U
72.6
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
Analysis Date
% Moisture:
Page 14 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.10 Date Collected:519903-003Lab Sample Id:
Ground WaterMatrix: MWNSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
4.60
0.0980
8.45
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
D
D
U
J
J
J
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
25.0
0.500
25.0
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
50
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
1330
5.61
305
U
8.10
0.310
0.160
0.450
U
U
U
U
U
U
U
U
U
U
U
0.620
982275Seq Number:
RL MDL
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.27.15 20.32
11.26.15 09.01
11.27.15 20.32
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
100
103
109
11.26.15 09.01
11.26.15 09.01
11.26.15 09.01
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 15 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.03 Date Collected:519903-004Lab Sample Id:
Ground WaterMatrix: MWTSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
Analysis Date
% Moisture:
Page 16 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.03 Date Collected:519903-004Lab Sample Id:
Ground WaterMatrix: MWTSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
4.02
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
108
106
108
11.26.15 09.33
11.26.15 09.33
11.26.15 09.33
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 17 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.37 Date Collected:519903-005Lab Sample Id:
Ground WaterMatrix: VERW1Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
22.7
U
U
U
U
3.11
U
U
U
U
U
U
U
U
0.240
U
115
75.7
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
Analysis Date
% Moisture:
Page 18 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.37 Date Collected:519903-005Lab Sample Id:
Ground WaterMatrix: VERW1Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
4.60
0.0980
8.45
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
D
D
U
J
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
25.0
0.500
25.0
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
50
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
68.9
1450
4.15
1000
U
14.8
0.800
7.98
0.780
U
U
U
2.24
U
U
U
U
U
U
10.7
2.37
982275Seq Number:
RL MDL
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.30.15 12.38
11.26.15 10.04
11.30.15 12.38
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
101
105
107
11.26.15 10.04
11.26.15 10.04
11.26.15 10.04
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 19 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.18 Date Collected:519903-006Lab Sample Id:
Ground WaterMatrix: VERW2/RW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
0.230
U
U
U
U
0.200
U
U
U
U
U
U
U
U
0.520
U
U
0.750
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
RL MDL
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
Analysis Date
% Moisture:
Page 20 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.18 Date Collected:519903-006Lab Sample Id:
Ground WaterMatrix: VERW2/RW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
X
J
J
J
U
J
U
U
U
U
U
U
J
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
1.90
4.65
5.03
3.05
U
7.96
1.60
2.07
5.04
0.210
0.130
U
0.420
U
U
U
U
U
U
0.410
U
982291Seq Number:
RL MDL
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
101
103
110
11.27.15 18.09
11.27.15 18.09
11.27.15 18.09
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 21 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.29 Date Collected:519903-007Lab Sample Id:
Ground WaterMatrix: RW5Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
Analysis Date
% Moisture:
Page 22 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 13.29 Date Collected:519903-007Lab Sample Id:
Ground WaterMatrix: RW5Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23.40 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
RL MDL
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
101
104
108
11.26.15 11.06
11.26.15 11.06
11.26.15 11.06
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 23 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 12.44 Date Collected:519903-008Lab Sample Id:
Ground WaterMatrix: RW7Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
1.19
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
5.00
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
26.6
U
U
U
1.04
U
U
183
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
RL MDL
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 21.28
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
Analysis Date
% Moisture:
Page 24 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 12.44 Date Collected:519903-008Lab Sample Id:
Ground WaterMatrix: RW7Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
5.00
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
44.5
355
24.0
32.8
U
77.1
2.41
9.17
2.43
U
U
U
12.9
U
U
U
U
U
U
4.76
2.77
982291Seq Number:
RL MDL
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 21.28
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
102
104
107
11.27.15 20.59
11.27.15 20.59
11.27.15 20.59
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 25 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 12.50 Date Collected:519903-009Lab Sample Id:
Ground WaterMatrix: SWNSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
RL MDL
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
Analysis Date
% Moisture:
Page 26 of 41 Final 1.001
Certificate of Analytical Results 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
11.20.15 09.42 Date Received:
11.18.15 12.50 Date Collected:519903-009Lab Sample Id:
Ground WaterMatrix: SWNSample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11.24 Date Prep:
ZHOTech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
RL MDL
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
105
104
110
11.27.15 21.54
11.27.15 21.54
11.27.15 21.54
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 27 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
701439-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.25.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
3
3
0
2
2
6
11
3
5
3
6
2
2
0
3
6
4
0
5
6
5
7
4
4
9
3
0
2
4
0
4
1
5
5
3
4
0
1
1
4
1
5
6
6
2
7
2
16
4
9
8
7
982275Seq Number:
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
111
98
107
113
93
94
99
122
107
118
107
115
110
100
96
106
109
112
108
86
97
104
127
104
107
111
94
98
108
116
104
126
89
97
105
118
100
99
79
96
102
67
99
107
101
105
104
98
112
105
104
102
LCSD
Result
27.7
24.5
26.7
28.2
23.3
23.5
24.8
30.5
26.8
29.5
26.8
28.7
27.5
25.0
24.1
26.5
27.3
28.0
27.1
21.5
48.4
25.9
63.5
26.0
26.7
55.3
47.2
24.6
27.0
29.1
26.0
31.4
22.2
24.3
26.3
29.6
24.9
24.8
19.7
24.0
25.6
16.8
993
26.7
25.3
26.3
51.9
24.5
28.1
26.3
25.9
25.6
LCS
%Rec
108
95
107
115
92
88
89
118
102
114
101
112
108
100
94
100
104
112
103
81
92
96
122
100
98
108
95
96
104
116
100
127
85
93
102
114
99
98
78
92
101
71
94
100
99
98
106
115
108
96
95
95
26.9
23.8
26.8
28.8
22.9
22.1
22.3
29.6
25.6
28.5
25.3
28.1
27.0
25.0
23.5
25.0
26.1
27.9
25.7
20.3
45.9
24.1
61.1
25.0
24.4
53.8
47.3
24.0
26.0
29.1
25.1
31.7
21.2
23.2
25.5
28.4
24.8
24.5
19.6
23.0
25.3
17.7
937
25.1
24.8
24.4
52.9
28.8
27.0
24.0
23.8
23.8
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
701439-1-BKSLCS Sample Id:701439-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 28 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
701439-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.25.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
4
10
8
4
6
2
6
5
3
1
6
6
982275Seq Number:
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
110
107
105
105
97
115
100
86
106
87
109
108
LCSD
Result
27.6
26.7
26.3
26.2
24.3
28.7
25.0
21.6
26.5
21.8
54.3
27.1
LCS
%Rec
106
96
97
100
91
112
94
82
102
86
102
102
26.6
24.1
24.3
25.1
22.8
28.0
23.6
20.6
25.6
21.5
50.9
25.5
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
701439-1-BKSLCS Sample Id:701439-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
11.26.15 00:43
11.26.15 00:43
11.26.15 00:43
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
106
101
110
LCS
%Rec
105
100
110
MB
%Rec
104
106
107
%
%
%
UnitsLCS
Flag
MB
Flag
Page 29 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
701458-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.27.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
2
11
7
0
3
2
1
10
11
7
2
2
3
0
3
2
3
1
2
3
8
2
1
3
1
2
1
3
3
14
1
8
3
0
1
1
5
18
0
1
1
7
1
1
1
3
1
7
4
3
3
3
982291Seq Number:
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
106
97
104
102
92
94
95
122
86
119
108
105
109
96
94
108
110
103
108
105
91
103
107
107
108
101
99
96
106
99
100
119
88
96
102
109
111
86
92
98
102
71
92
103
100
105
100
109
112
108
106
105
LCSD
Result
26.4
24.3
25.9
25.4
23.1
23.6
23.7
30.4
21.5
29.7
27.0
26.3
27.2
24.1
23.6
26.9
27.4
25.7
26.9
26.2
45.4
25.7
53.7
26.7
27.0
50.3
49.6
23.9
26.6
24.7
24.9
29.7
22.0
23.9
25.4
27.3
27.7
21.5
23.0
24.5
25.4
17.8
924
25.8
24.9
26.2
50.2
27.3
28.1
27.1
26.6
26.2
LCS
%Rec
108
108
97
101
95
96
96
110
96
110
106
103
106
96
98
105
106
102
106
108
99
100
106
103
106
98
98
99
103
114
101
110
91
95
101
108
106
103
92
99
100
76
94
104
101
101
100
118
108
106
103
102
26.9
27.1
24.2
25.3
23.7
24.1
24.0
27.5
24.0
27.6
26.4
25.7
26.4
24.0
24.4
26.3
26.5
25.4
26.4
27.1
49.4
25.1
53.2
25.8
26.6
49.1
49.0
24.7
25.7
28.4
25.2
27.4
22.7
23.8
25.2
27.1
26.4
25.7
23.0
24.8
25.1
19.1
937
26.1
25.2
25.3
49.8
29.4
27.1
26.4
25.8
25.4
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
701458-1-BKSLCS Sample Id:701458-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 30 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
701458-1-BLK
701555-1-BLK
MB Sample Id:
MB Sample Id:
Water
Water
Matrix:
Matrix:
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method:
Analytical Method:
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.27.15
11.30.15
Date Prep:
Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Parameter
Parameter
%RPD
%RPD
Flag
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
RPD
Limit
1
3
0
3
6
4
2
1
7
1
1
1
3
2
982291
982462
Seq Number:
Seq Number:
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.30.15 08:00
11.30.15 08:00
Analysis
Date
Analysis
Date
Limits
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
77-125
53-149
LCSD
%Rec
LCSD
%Rec
108
106
100
100
96
108
97
87
99
87
104
104
105
106
LCSD
Result
LCSD
Result
26.9
26.6
25.1
25.0
24.0
26.9
24.2
21.7
24.8
21.8
52.0
26.0
26.3
53.2
LCS
%Rec
LCS
%Rec
106
103
101
103
102
103
99
88
92
88
105
105
108
104
26.6
25.8
25.2
25.7
25.5
25.8
24.8
22.0
23.1
22.0
52.6
26.3
27.1
52.2
Spike
Amount
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
25.0
50.0
MB
Result
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
<0.0920
<0.169
701458-1-BKS
701555-1-BKS
LCS Sample Id:
LCS Sample Id:
701458-1-BSD
701555-1-BSD
LCSD Sample Id:
LCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
LCS
Result
LCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate
Surrogate
LCSD
Flag
LCSD
Flag
11.27.15 13:15
11.27.15 13:15
11.27.15 13:15
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
Analysis
Date
Analysis
Date
Limits
Limits
65-126
86-111
83-116
65-126
86-111
83-116
LCSD
%Rec
LCSD
%Rec
98
105
106
98
102
102
LCS
%Rec
LCS
%Rec
102
100
108
95
100
104
MB
%Rec
MB
%Rec
102
104
106
98
102
101
%
%
%
%
%
%
Units
Units
LCS
Flag
LCS
Flag
MB
Flag
MB
Flag
Page 31 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
519903-006Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.27.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
1
2
0
1
0
4
3
7
1
4
0
0
3
3
5
1
1
1
3
1
3
6
4
1
11
2
3
4
13
2
1
0
9
1
1
11
7
8
0
6
1
6
2
1
4
3
2
4
3
2
3
982291Seq Number:
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
106
94
106
114
91
92
95
120
98
114
96
110
106
103
96
93
103
111
100
90
110
95
131
96
100
117
100
95
99
96
104
117
84
101
100
115
106
94
75
95
101
70
101
100
100
95
104
95
143
99
96
94
MSD
Result
26.5
23.5
26.6
28.5
22.8
23.0
23.7
30.1
24.6
28.5
24.2
27.6
26.5
25.8
24.1
23.5
25.8
27.8
25.1
22.6
54.9
23.7
65.3
24.0
25.5
58.7
50.1
24.5
24.7
23.9
26.0
29.2
21.0
25.3
25.0
28.8
26.6
23.5
18.7
23.7
25.3
17.5
1010
27.0
29.7
28.7
55.2
23.8
43.7
26.4
26.1
28.6
MS
%Rec
106
93
105
114
90
92
99
117
105
112
99
110
106
100
100
98
104
110
101
88
111
98
123
100
101
105
99
98
103
108
106
118
84
93
101
114
96
101
69
95
108
70
107
103
99
99
101
93
135
103
99
98
26.5
23.3
26.2
28.6
22.6
22.9
24.7
29.3
26.3
28.1
25.1
27.6
26.5
25.1
24.9
24.7
26.0
27.6
25.3
21.9
55.5
24.4
61.7
24.9
25.7
52.5
49.3
25.2
25.8
27.1
26.5
29.6
21.1
23.2
25.3
28.5
23.9
25.2
17.3
23.7
26.9
17.4
1070
27.6
29.5
29.8
53.7
23.3
41.8
27.3
26.7
29.6
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
0.230
<0.180
<0.0940
<0.0900
<0.122
0.200
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
0.520
<0.253
<0.352
0.750
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
1.90
4.65
5.03
3.05
<0.190
7.96
1.60
2.07
5.04
519903-006 SMS Sample Id:519903-006 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 32 of 41 Final 1.001
QC Summary 519903
Terraquest Environmental Consultants, P.C.
Hollar's Grocery
519903-006
520193-004
Parent Sample Id:
Parent Sample Id:
Ground Water
Ground Water
Matrix:
Matrix:
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method:
Analytical Method:
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.27.15
11.30.15
Date Prep:
Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Parameter
Parameter
%RPD
%RPD
Flag
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
RPD
Limit
4
2
9
3
1
1
4
4
2
2
3
1
3
2
982291
982462
Seq Number:
Seq Number:
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.30.15 19:04
11.30.15 19:04
Analysis
Date
Analysis
Date
Limits
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
77-125
51-155
MSD
%Rec
MSD
%Rec
92
100
94
98
92
109
95
85
93
83
100
102
97
102
MSD
Result
MSD
Result
23.2
25.1
23.5
24.8
23.0
27.2
23.7
21.3
23.3
20.7
50.5
25.5
24.3
50.8
MS
%Rec
MS
%Rec
96
101
103
101
91
110
98
89
95
84
103
103
100
103
24.1
25.5
25.8
25.6
22.8
27.4
24.6
22.2
23.7
21.1
52.1
25.7
25.0
51.7
Spike
Amount
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
25.0
50.0
Parent
Result
Parent
Result
0.210
0.130
<0.0540
0.420
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
0.410
<0.122
<0.0920
<0.169
519903-006 S
520193-004 S
MS Sample Id:
MS Sample Id:
519903-006 SD
520193-004 SD
MSD Sample Id:
MSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
MS
Result
MS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate
Surrogate
MSD
Flag
MSD
Flag
11.27.15 22:25
11.27.15 22:25
11.27.15 22:25
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
Analysis
Date
Analysis
Date
Limits
Limits
65-126
86-111
83-116
65-126
86-111
83-116
MSD
%Rec
MSD
%Rec
105
99
109
100
100
104
MS
%Rec
MS
%Rec
109
98
106
102
100
104
%
%
%
%
%
%
Units
Units
MS
Flag
MS
Flag
Page 33 of 41 Final 1.001
Blank Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
701439-1-BLKLab Sample Id:
WATERMatrix: 701439-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23:40Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
MDLRL
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
Analysis
Date
Page 34 of 41 Final 1.001
Blank Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
701439-1-BLKLab Sample Id:
WATERMatrix: 701439-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.25.15 23:40Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982275Seq Number:
MDLRL
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
11.26.15 02:47
Analysis
Date
Page 35 of 41 Final 1.001
Blank Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
701458-1-BLKLab Sample Id:
WATERMatrix: 701458-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11:24Date Prep:
ZHOTech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
MDLRL
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
Analysis
Date
Page 36 of 41 Final 1.001
Blank Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
701458-1-BLKLab Sample Id:
WATERMatrix: 701458-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.27.15 11:24Date Prep:
ZHOTech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982291Seq Number:
MDLRL
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
11.27.15 14:35
Analysis
Date
Page 37 of 41 Final 1.001
Blank Summary 519903
Terraquest Environmental Consultants, P.C., Mebane, NC
Hollar's Grocery
701555-1-BLKLab Sample Id:
WATERMatrix: 701555-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06:34Date Prep:
MWETech:
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Parameter
0.0920
0.169
Result
U
U
0.500
0.500
Flag
ug/L
ug/L
Units
1
1
DilCas Number
108-20-3
1634-04-4
U
U
982462Seq Number:
MDLRL
11.30.15 09:19
11.30.15 09:19
Analysis
Date
Page 38 of 41 Final 1.001
Page 39 of 41 Final 1.001
Page 40 of 41 Final 1.001
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
519903Work Order #:
11/20/2015 09:42:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Chad Bechtold
11/20/2015
11/23/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
N/A
N/A

#1 *Temperature of cooler(s)?1.5
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:
Comments
Dario Lagunas
Temperature Measuring device used : #61
Page 41 of 41 Final 1.001