WI-28993_48187_CA_LSA_20230217

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
February 17, 2023

Mr. Clark Wipfield
NCDEQ-UST Section
Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405

Re: Limited Site Assessment Report
Home race Mart #1
7824 Seven Springs Highway
Nakina, Columbus County
North Carolina
Facility ID Number: 00-0-0000034121
Incident Number: 48187
GRI Project Number: 5836

Dear Mr. Wipfield,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Ethan Rogerson at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Sanjeev Sethi; K&S, LLC, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Limited Site Assessment Report
Home Race Mart #1
7824 Seven Springs Highway
Nakina, Columbus County
North Carolina
Facility ID Number: 00-0-0000034121
Incident Number: 48187
GRI Project Number: 5836

Prepared for:

Sanjeev Sethi
K&S, LLC
7824 Seven Creeks Highway
Nakina, NC 28455

February 17, 2023

Ethan Rogerson, GIT
Project Manager
William Regenthal, P.G.
Report Editor

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
i
EXECUTIVE SUMMARY
The Home Race Mart #1 site is located at 7824 Seven Springs Highway in Nakina, Columbus County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered
by concrete, asphalt and grass. There are one 12,000-gallon compartmentalized gasoline (8,000-gallon
and 4,000-gallon compartments), one 6,000-gallon diesel and one 2,000-gallon off-road diesel USTs
currently in use at the site with six associated dispenser islands.

On October 21, 2021, two soil sample (SS-PREM-2' and SS-ORDSL-2’) were collected at the 4,000-gallon
gasoline and 2,000-gallon off-road diesel spill buckets, respectively. Concentrations of TPH-GRO and TPH-
DRO that exceeded the RALs were reported in soil sample SS-ORDSL-2’. No free product was noted at the
site. Site Check results identified a release at the site and a LSA was required.

On November 21, 2022, a receptor survey was conducted. Three potable water supply wells and five non-
potable water supply wells were identified within a 1,500-foot radius of the site. One non-potable water
supply well was identified within a 250-foot radius of the site. Public water is available to the subject site
and the surrounding properties. No surface water bodies were identified within a 500-foot radius of the
site.

On November 21, 2022, one monitoring well (MW-1) was installed directly adjacent to the diesel UST
basin. During the installation of MW-1, soil sample (MW-1 (5’)) was collected at 5 feet BGS and submitted
for laboratory analyses of VOCs using EPA Method 8260B, semi-VOCs using EPA Method 8270B and
VPH/EPH by the MADEP Methods. All reported contaminant concentrations were less than the Soil-to-
Water MCCs.

On November 21, 2022, a ground water sample was collected from MW-1. The ground water sample was
submitted for laboratory analyses of VOCs by EPA Method 602, semi-VOCs using EPA Method 625 + 10
highest tentatively identified compounds, EDB by EPA Method 504.1, lead by 6010C and MADEP VPH/EPH.
A concentration of lead that exceeded the MACs was reported in the ground water sample collected from
MW-1. All contaminant concentrations were less than the GCLs.

On January 30, 2023, water samples were collected from potable water supply wells WSW-5 and WSW-6.
The water supply well samples were submitted for laboratory analyses of VOCs by EPA Method 602, semi-
VOCs by EPA Method 625+ 10 highest tentatively identified compounds, EDB by EPA Method 504.1, lead
by 6010C and MADEP VPH/EPH. All contaminant concentrations were less than the MACs and GCLs.

Based on these results no further assessment is warranted. The concentration of lead is not associated
with the diesel spill bucket release and incident 48187 should be closed.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836

ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS .........................................................................................................................................
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................7
6. LIMITATIONS ........................................................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Soil Quality Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Soil Sample Analytical Results
Table 7: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Columbus County Property Cards
Appendix B: Well Construction Record and Subsurface Log
Appendix C: Laboratory Reports – Soil and Ground Water Samples

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? YES

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
YES

An inactive, non-potable water supply well (WSW-1) is located approximately 90 feet to the
southeast of the release.

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? YES

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
2
10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? NO
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
3
The site is expected to remain in operation as an active convenience store and petroleum retail
facility in the near future.
7. What is the zoning status of the property?
According to the Columbus County Zoning Map, the site is zoned GU (General Use).

8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store in the near future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 7888 7 creeks Highway located approximately 80 feet southwest
of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Nakina Baptist Church is located at 7883 7 Creeks Highway approximately 200 feet east of the
source area at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Columbus County Zoning Map, the surrounding areas are zoned GU (General
Use).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, public/institutional and residential.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on November 21, 2022. Three potable water supply wells
(WSW-5, WSW-6 and WSW-8) and five non-potable water supply wells (WSW-1, WSW-2, WSW-
3, WSW-4 and WSW-7) were identified within a 1,500-foot radius of the site. One inactive, non-
potable water supply well (WSW-1) was identified within a 250-foot radius of the site. Public

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
4
water is available to the subject site and the surrounding properties. Water Supply Well Owner
Information is included as Table 3. A Site Location Map is provided as Figure 1 and a Site Vicinity
Map showing property boundaries for the site and surrounding properties has been included as
Figure 2.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
7 Creeks Highway. Public water is supplied by the Columbus County Water Department.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
One creek (Sand Pitt Branch) identified approximately 1,000 feet to the south/southeast of the
site.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On December 13, 2022, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is located in the Coastal Plain Physiographic Region. The surficial aquifer in the vicinity of
the site is underlain by the Peedee confining unit and the Peedee aquifer, respectively.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along 7 Creeks Highway and several underground utility lines
were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
4. Property boundaries are shown on Figure 2. Property cards for the adjacent property owners
are attached as Appendix A.
3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Waccamaw Formation.
The Waccamaw Formation consists of bluish-gray to tan, loosely consolidated fossiliferous sand with silt

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
5
and clay. The formation straddles the Pleistocene-Pliocene boundary.

On November 21, 2022, one monitoring well (MW-1) was installed directly adjacent to the diesel UST
basin. The soil sample collected during the well installation was a brown silty clay mix. The depth to
ground water during the November gauging event was 4.06 feet below the top of well casing. Copies of
the well construction record and subsurface log are included as Appendix B. A Site Map showing the
location of MW-1 is included as Figure 3. Well construction and gauging information is presented in Table
5. A photo of MW-1 is shown below:

4. SITE INVESTIGATION
On October 21, 2021, GRI performed a site check that included collecting soil samples at the 4,000-gallon
gasoline compartment and 2,000-gallon off-road diesel spill buckets, respectively. Soil samples SS-PREM-
2' and SS-ORDSL-2’ were each collected at depths of approximately 2 feet bgs. The concentrations of GRO
and DRO reported in soil sample SS-ORDSL-2' exceeded the RALs.

On November 21, 2022, a receptor survey was conducted. Three potable water supply wells and five non-
potable water supply wells were identified within a 1,500-foot radius of the site. One non-potable water
supply well was identified within a 250-foot radius of the site. Public water is available to the subject site
and the surrounding properties. No surface water bodies were identified within a 500-foot radius of the
site.

During the installation of MW-1, one soil sample (MW-1 (5’)) was collected at 5 feet BGS and submitted

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
6
for laboratory analyses of VOCs using EPA Method 8260B semi-VOCs using EPA Method 8270B and
VPH/EPH by the MADEP Methods.

On November 21, 2022, a ground water sample was collected from MW-1. The ground water sample was
submitted for laboratory analyses of VOCs by EPA Method 602, semi-VOCs by EPA Method 625 + 10
highest tentatively identified compounds, EDB by EPA Method 504.1, lead by 6010C and MADEP VPH/EPH.

On January 30, 2023, water samples were collected from potable water supply wells WSW-5 and WSW-6.
The water supply well sample was submitted for laboratory analyses of VOCs by EPA Method 602, semi-
VOCs by EPA Method 625 + 10 highest tentatively identified compounds, EDB by EPA Method 504.1, lead
by 6010C and MADEP VPH/EPH.

1. Soil Sampling:
All reported contaminant concentrations were less than the Soil-to-Water MCCs and Residential SCLs. A
Soil Quality Map has been included as Figure 4. A summary of the soil sample analytical results is
presented in Table 6. A copy of the laboratory report from the November 2022 soil sampling event has
been included in Appendix C. A summary of the current soil sampling data collected during the LSA
activities is shown below: Sample ID Sample Depth (ft-BGS) Benzene Toluene Ethylbenzene Total Xylenes Soil to Water MCC (mg/kg) 0.0072 5.4 8.0 6.0
Residential SCLs (mg/kg) 12 1,250 60.3 3,120
MW-1 (5') 5 <0.0011 <0.0091 <0.00091 <0.0019

2. Ground Water & Water Supply Well Sampling:
A concentration of lead that exceeded the MAC was reported in soil sample MW-1. All the reported
contaminant concentrations were less than the GCLs. No free product was observed at the site. All
contaminant concentrations were less than the MACs and GCLs in water supply well samples collected
from WSW-5 and WSW-6 in January 2023. A Ground Water Quality Map has been included as Figure 5.
A summary of the ground water analytical data has been included in Table 7. Copies of the laboratory
reports have been included in Appendix C. A summary of the current ground water sampling data is
shown below:
Contaminant of
Concern
 Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
WSW-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
WSW-5 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
7

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the
monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples were
logged using proper chain-of-custody procedures. The samples were transported to a North Carolina
certified laboratory for analysis. A laboratory supplied trip blank was included in the sample cooler. No
detectable concentrations of requested method constituents were reported in the trip blank.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, residential, office and public/institutional properties.
 November 21, 2022, a receptor survey was conducted on. Four potable water supply wells and
four non-potable water supply wells were identified within a 1,500-foot radius of the site. One
potable water supply well was identified within a 250-foot radius of the site. Public water is
available to the subject site and the surrounding properties. No surface water bodies were
identified within a 500-foot radius of the site.
 On November 21, 2022, one monitoring well (MW-1) was installed directly adjacent to the diesel
UST basin. During the installation of MW-1, one soil sample (MW-1 (5’)) was collected at 5 feet
BGS. All reported contaminant concentrations were less than the Soil-to-Water MCCs.
 On November 21, 2022, a ground water sample was collected from MW-1. A concentration of
lead that exceeded the MACs was reported in the ground water sample collected from MW-1. All
contaminant concentrations were less than the GCLs.
 On January 30, 2023, water samples were collected from potable water supply wells WSW-5 and
WSW-6. All reported contaminant concentrations were less than the MACs and GCLs.
 Based on these results no further assessment is warranted. The concentration of lead is not
associated with the diesel spill bucket release and incident 48187 should be closed.

6. LIMITATIONS
This report has been prepared for the exclusive use of K&S, LLC for specific application to the referenced
site in Columbus County, North Carolina. The assessment was conducted based on the scope of work and
level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our findings
have been developed in accordance with generally accepted standards of geology and hydrogeology
practices in the State of North Carolina, available information and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: February 17, 2023 Home Race Mart #1
Project Manager: Ethan Rogerson, GIT GRI Project No. 5836
8
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site Location Home Race Mart #17824 7 Creeks HighwayNakina, North CarolinaColumbus CountyIncident No. N/AGRI Project No. 5836500 M2000 FTDate: 11/20/2021Location: 34.134276° N -78.668266° W Dad
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"J
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SITE
1103.00-19-0876.000
1103.00-09-1554.000
1104.00-00-6001.000
1104.00-00-4354.000
1104.00-01-0160.000
1103.00-09-8436.000
1
1
0
3.0
0
-0
9-2
9
4
0.
0
0
01104.00-00-2736.0000194.00-90-9656.000
1103.00-09-3962.000
1104.00-00-2162.000
1103.00-09-4729.000
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
M M R A Y R D
S
E
V
E
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FIGURE 2: SITE VICINITY MAPHOME RACE MARKET #17824 SEVEN SPRINGS HIGHWAYNAKINA, COLUMBUS COUNTYNORTH CAROLINAINCIDENT NO. 48187GRI NO. 5836
PREPARED BY:GEOLOGICAL RESOURCES, INC.NOVEMBER 11, 2022
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
1,000-FOOT RADIUS
LEGEND
"J Water Supply Well
streets
Drainage Ditch
ncrivers
Well Owners and Adjacent Properties
Columbis County NC Parcels

TABLES
UST ID Number 1-3 and 1B Facility ID Number
Owner or Operator?
Owner
UST ID Number 2 and 3 Facility ID Number
Owner or Operator?
Owner
UST ID Number 2 and 3 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1 and 1B Facility ID Number
Owner or Operator?
OwnerHome Run Food Mart, Inc.08/01/1993 - 10/08/2010
Address Telephone Number
Unknown Unknown
Name of Owner or Operator Dates of Ownership / Operation
Unknown Unknown
00-0-0000034121
Name of Owner or Operator Dates of Ownership / Operation
Home Run Food Mart, Inc.04/03/2002 - 10/08/2010
Address Telephone Number
Unknown Unknown
00-0-0000034121
Address Telephone Number
K & S, LLC 01/03/2017 - Current
Address Telephone Number
7824 Seven Creeks Highway, Nakina, NC 28455 910-234-0453
00-0-0000034121
Name of Owner or Operator Dates of Ownership / Operation
Nikki and Vicky, Inc.10/08/2010 - 01/03/2017
TABLE 1
UST OWNER/OPERATOR INFORMATION
HOME RACE #1 (INCIDENT NO. PENDING)
00-0-0000034121
Name of Owner or Operator Dates of Ownership / Operation
Page 1 of 1
Date: 11/12/21
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 8,000 Single Wall FRP Current No
1B Gasoline 4,000 Single Wall FRP Current No
3 Diesel 2,000 4/3/2002 Single Wall
Steel/FRP Unknown Other Current No
2 Diesel 6,000 4/3/2002 Single Wall
Steel/FRP Unknown Double Wall FRP Current Yes
UnknownSingle Wall
Steel/FRP12/1/1993
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
HOME RACE #1 (INCIDENT NO. PENDING)
Facility ID #: 00-0-0000034121
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Page 1 of 1
Facility ID # :00-0-0000034121
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
WSW-1 1103.00-09-4729.000 Griffith, Heather & Monica Jimenez -
Elder
8420 Shire Court
Mechanicsville, VA 23111
7906 Seven Creeks Highway
Nakina, NC 28455 Inactive Non-Potable Yes No ~90 SE
WSW-2 1103.00-09-6687.000 Bost, Damien Draper 7953 Seven Creeks Highway
Nakina, NC 28455
7953 Seven Creeks Highway
Nakina, NC 28455 Unknown Non-Potable Yes Yes ~350 SE
WSW-3 1103.00-09-8436.000 Butler, Royce & Doris Post Office Box 70
Nakina, NC 28455
7987 Seven Creeks Highway
Nakina, NC 28455 Unknown Non-Potable Yes Yes ~660 SE
WSW-4 1104.00-00-2736.000 Ray, Claudette Saxon Post Office Box 99
Nakina, NC 28455
7731 Seven Creeks Highway
Nakina, NC 28455 Active Non-Potable Yes Yes ~850 N
WSW-5 1104.00-00-6001.000 Nakina Baptist Church Inc Post Office Box 120
Nakina, NC 28455
7983 Seven Creeks Highway
Nakina, NC 28455 Active Potable Yes No ~415 E
WSW-6 1104.00-00-5222.000 Columbus County Memorial
Veterans of Foreign Wars Post #8073
Post Office Box 912
Loris, SC 29569
4604 Ervin T Richardson
Nakina, NC 28455 Active Potable Yes No ~400 NE
WSW-7 1104.00-00-1924.000 Mcdowell, Chares T & Regina S Post Office Box 59
Nakina, NC 28455
7691 Seven Creeks Highway
Nakina, NC 28455 Unknown Non-Potable Yes Unknown ~1,200 N
WSW-8 0194.00-90-9656.000 Williamson, Ryan K 1180 Ervin T Richardson Road
Nakina, NC 28455
7722 Seven Creeks Highway
Nakina, NC 28455 Active Potable Yes Unknown ~880 N
Notes:
• Receptors are shown on Figure 3.
• n/a: not applicable.
Unknown
Unknown
Unknown
TABLE 3
RECEPTOR INFORMATION
HOME RACE MART #1 (INCIDENT NO. 48187)
Date: 02/07/23
Well Construction Details
(Depth, Screened Interval,
Type of Well, ect.)
Unknown
Unknown
Unknown
Unknown
Unknown
Page 1 of 1
Date: 11/22/2022 Facility ID # :00-0-0000034121
Parcel Number Owner Name Mailing Address
1104.00-00-2162.000(Site)
1104.00-00-2102.000
1103.00-09-2940.000
1103.00-09-3962.000
1103.00-09-1554.000 Cardona Gabriel Bugarin 67 M M Ray Road
Nakina, NC 28455
1103.00-09-4729.000 Griffith Heather & Monica Jimenez-
Elder
8420 Shire Court
Mechanicsville, VA 23111
1104.00-00-6001.00
1104.00-00-4354.000
1104.00-00-1314.000 Michael Ray & John G Richardson 2265 Ervin T Richardson Road
Nakina, NC 28455
Note:
• Properties are keyed to Figure 2.
Nakina Baptist Church Inc Post Office Box 120
Nakina, NC 28455
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
HOME RACE MART #1 (INCIDENT NO. 48187)
K & S FOOD MART LLC 7824 Seven Creeks Highway
Nakina, NC 28455
Page 1 of 1
Date: 11/22/2022
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
MW-1 11/21/2022 11/21/22 12 2-12 12 NM 4.06 ---NM
Notes:
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HOME RACE MART #1 (INCIDENT NO. 48187)
Facility ID # :00-0-0000034121
• Well depths based on field measuurements.
• NA: Information not available
• NM : Not measured.
• ft BGS : feet below ground surface.
• Elevations not available.
Page 1 of 1
Date: 12/9/22 Facility ID #: 00-0-0000034121
5030/
8015D
3550/
8015C
Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)Gasoline-Range TPHDiesel-Range TPHBenzeneTolueneEthylbenzeneTotal XylenesAcenaphtheneAcenaphthyleneAnthraceneC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsC9-C18 AliphaticsC19-C36 AliphaticsC11-C12 Aromatics50 100 NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0072 5.4 8.0 6.0 8.1 20 640 68 540 31 540 NE 31
NE NE 12 1,250 60.3 3,120 930 930 4,600 625 1,560 469 1,560 31,200 469
SS-ORDSL-2 10/21/2021 2 176 3,250 NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-PREM-2 10/21/2021 2 8.67 NR NR NR NR NR NR NR NR NR NR NR NR NR NR
MW-1 (5')11/21/22 5 NR NR <0.0011 <0.0091 <0.00091 <0.0019 <0.023 <0.021 <0.024 <3.2 <3.2 <3.2 <3.2 <3.2 8.47 J
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the
laboratory report
• Concentrations in bold face type indicate the reported
concentrations exceeded the soil-to-water MCCs.
• Concentrations in italic type indicate the reported
concentrations exceeded the residential SCLs.
• NE: Not Established
• NR: Not Requested.
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
TABLE 6
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
Analytical Method 
RAL (mg/kg)
EPA Method 8260B MADEP VPH MADEP EPHEPA Method 8270B
HOME RACE #1 (INCIDENT NO. 48187)
Page 1 of 1
Facility ID # :00-0-0000034121
EPA 504.1 EPA 625.1 SW846
6010D
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.02 6,000 70 400 700 200 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 50 NE 26,100 NE NE NE NE NE NE
MW-1 11/21/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.0092 4.8 248 <50 <50 <20 <48 <48 <76
WSW-5 01/30/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR <1.0 <5.0 <50 <50 <20 <50 <50 <80
WSW-6 01/30/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR <0.98 <5.0 <50 <50 <20 <49 <49 <78
11/21/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR
01/30/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR
Notes:
• Concentrations in bold face type indicate the reported concentrations exceeded the MACs.
• Concentrations in italics indicate the reported concentrations exceeded the GCLs.
• J: Estimated value.
• E: Reported value exceeded the calibration range.
• Results reported in µg/l (micrograms per liter)
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• < : Less than the method detection limit specified in the laboratory report.
• FP: Free Product.TolueneEthylbenzeneXylenesMTBEC11-C22 AromaticsC9-C12 AliphaticsC9-C10 AromaticsC9-C18 AliphaticsC5-C8 AliphaticsC19-C36 AliphaticsTrip Blank
MADEP EPH
• NR: Not Requested.
TABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HOME RACE MART #1 (INCIDENT NO. 48187)
Date: 02/15/2023
Analytical Method

Contaminant of Concern
BenzeneMACs (μg/l)
GCL (μg/l)NaphthaleneSM 6200B MADEP VPH Diethyl PhthalateLead1,2-Dibromoethane(EDB)Page 1 of 1

APPENDICES

APPENDIX A
Columbus County Property Cards
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-1554.000 007080 000002 210581
6561 03 L 12 104 56800 61700 1 JOHN WARD 007080 000003 210582
3-01164 007080 000004 210583
CARDONA GABRIEL BUGARIN 03 37 04 01 01 01 007080 000005 210584
67 M M RAY RD 1223 4352020 10000 67 M M RAY RD 007080 000006 210585
28455 PPD 11-1590 007080 000007 210586
NAKINA NC NF -- CR -- 007080 000008 210587
CARTRETTE/DWG REMOD - FUNC DEPRE CHG 007080 000009 210588
AC CORR FOR'21//STG BN OFF FOR'20-R A 17 007080 000010 210589
B 17 007080 000011 210590
1940 A 1967 007080 000014 210591
02 PIER/P 007080 000016 210592
03 WD.FR. BASE 1448 73.26 007080 000018 210593
01 WD.FR. BASE 1448 73.26 106080 +5+-----24----+ 007080 000020 210594
01-1STY : : : 007080 000021 210595
07 ASBEST BASE 8 B 8 007080 000022 210596
+5: +-+ 007080 000023 210597
01 WD.FR. BASE 1 : : 007080 000024 210598
17 : : 007080 000025 210599
01 COMP. F SCR P 176 4316 3 : 007080 000026 210600
03 GABEL 17 2 : 007080 000027 210601
BASE F SCR P 40 1311 : : 007080 000028 210602
: : 007080 000029 210603
01 S.WOOD BASE : 3 007080 000030 210604
: 6 007080 000031 210605
03 AVG. BASE +---16--+ : 007080 000032 210606
: : 007080 000033 210607
03 AVG BASE : : 007080 000034 210608
: : 007080 000035 210609
03 AVG. BASE 2 50 : 007080 000036 210610
0 +------26-----+ 007080 000037 210611
5 : : : 007080 000038 210612
104901 : 8 A : 007080 000039 210613
D+- 85 89166 +---16--+----22----+ 007080 000040 210614
01 NONE 6805- 58/25/ 61079 007080 000042 210615
01 NONE XF UD FACT 007080 000043 210616
28087 .00 28100 007080 000044 210617
DIRT FACT 007080 000051 210618
B S 1.000 2.40 2.40 3800 9120 007080 000052 210619
OPN 7.300 1.30 1.30 2100 19929 007080 000053 210620
WD 1.120 1.30 1.30 575 837 007080 000054 210621
U/R .900 1.30 1.30 3200 3744 007080 000055 210622
10.320 33630 007080 000058 210623
50000 33600 007080 000061 210624
2/25/2020 007080 000062 210625
YES 28100 007080 000063 210626
61700 11/28/22 007080 000066 210627
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-2940.000 005336 000002 755594
95037 03 L 12 104 6300 6500 1 K & S LLC 005336 000003 755595
3-04644 005336 000004 755596
K & S FOOD MART LLC 13 00 02 01 01 01 005336 000005 755597
7824 SEVEN CREEKS HWY 1227 4512020 7888 SEVEN CREEKS HWY 005336 000006 755598
28455 00-0000 005336 000007 755599
NAKINA NC NF -- CR -- 005336 000008 755600
BKDWN CORR FOR'21 005336 000009 755601
/ / 005336 000042 755602
XF UD FACT 005336 000043 755603
.00 005336 000044 755604
DIRT FACT 005336 000051 755605
B S 1.000 1.70 1.70 3800 6460 005336 000052 755606
1.000 6460 005336 000058 755607
6500 005336 000061 755608
5/08/2020 005336 000062 755609
NO - 005336 000063 755610
6500 11/28/22 005336 000066 755611
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-3962.000 005335 000002 755573
91094 03 L 12 102 44100 51100 1 K & S LLC 005335 000003 755574
3-04644 005335 000004 755575
K & S FOOD MART LLC 13 00 04 01 00 01 005335 000005 755576
7824 SEVEN CREEKS HWY 1227 4512020 NEAR 7888 SEVEN CREEKS HWY 005335 000006 755577
28455 00-0000 005335 000007 755578
NAKINA NC NF -- CR -- 005335 000008 755579
SEE 855/91(DESC)//CNP-SER FR #7419 FOR'06 005335 000009 755580
/ / 005335 000042 755581
XF UD FACT 005335 000043 755582
.00 005335 000044 755583
4 CNP-SER 1 MTL 24X24 576 3000 005335 000049 755584
4 CNP-SER 1 28X82 22962037 02 5 44430 005335 000050 755585
DIRT FACT 005335 000051 755586
U/R .390 3.00 3.00 3200 3744 005335 000055 755587
.390 3744 005335 000058 755588
47400 005335 000059 755589
3700 005335 000061 755590
5/08/2020 005335 000062 755591
NO - 47400 005335 000063 755592
51100 11/28/22 005335 000066 755593
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-4729.000 009330 000002 573525
7328 03 L 12 101 4600 5100 1 EDDIE LONG 009330 000003 573526
3-05473 009330 000004 573527
GRIFFITH HEATHER & 13 00 04 01 00 01 009330 000005 573528
MONICA JIMENEZ-ELDER 1204 9972019 1600 7906 SEVEN CREEKS HWY 009330 000006 573529
8420 SHIRE COURT 23111 PPD 11-1590 009330 000007 573530
MECHANICSVILLE VA NF -- CR -- 009330 000008 573531
WHITEVILLE OIL CO. 009330 000009 573532
AC CORR FOR'11//AC CORR FOR'07 009330 000010 573533
MTL SHLT ADDED FOR'20 009330 000011 573534
/ / 009330 000042 573535
XF UD FACT 009330 000043 573536
.00 009330 000044 573537
47 P BN/SD 1 MTL 20X40 800 427 19 5 3240 009330 000049 573538
DIRT FACT 009330 000051 573539
U/R .200 3.00 3.00 3200 1920 009330 000055 573540
.200 1920 009330 000058 573541
3200 009330 000059 573542
8000 1900 009330 000061 573543
6/07/2019 009330 000062 573544
YES 3200 009330 000063 573545
5100 11/28/22 009330 000066 573546
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-1314.000 00761} 000002 129523
89481 03 L 12 106 78000 87100 1 LOT#B//MICHAEL RICHARDSON ETAL 00761} 000003 129524
3-02070 00761} 000004 129525
RICHARDSON MICHAEL RAY & JOHN G 03 37 04 01 01 01 00761} 000005 129526
2265 ERVIN T RICHARDSON RD 971 5672009 7792 SEVEN CREEKS HWY 00761} 000006 129527
28455 P 00-0000 00761} 000007 129528
NAKINA NC NF -- CR -- 00761} 000008 129529
AUDIT-HSE FOR'18 00761} 000009 129530
A 05 00761} 000010 129531
B 06 00761} 000011 129532
C 10 00761} 000012 129533
D 15 00761} 000013 129534
1977 G 1984 E 19 00761} 000014 129535
F 42 00761} 000015 129536
04 PER.FT 00761} 000016 129537
03 WD.FR. BASE 1352 80.11 00761} 000018 129538
01 WD.FR. BASE 1352 80.11 108308 +---16--+-8-+ 00761} 000020 129539
06 WD/LOG 01-1STY : 8 : 00761} 000021 129540
01 BRICK BASE : :D : 00761} 000022 129541
: +-8-+ 00761} 000023 129542
01 WD.FR. BASE 1 2 : +---14-+ 00761} 000024 129543
5 3 1 : : 00761} 000025 129544
01 COMP. CARPORT 488 9974 : 5 1 1 00761} 000026 129545
03 GABEL 6 : A : 0 F 0 00761} 000027 129546
BASE COV P 60 1655 +6-+------------51----------+ 00761} 000028 129547
10 6 C: : 00761} 000029 129548
02 H.WOOD BASE E BR P 36 2076 +-6: : 00761} 000030 129549
15 : : : 00761} 000031 129550
03 AVG. BASE FR STG 64 2195 : : : 00761} 000032 129551
19 : 50 : 00761} 000033 129552
03 AVG BASE H SCR P 210 5000 2 +7-+ 3 00761} 000034 129553
42 0 : 2 00761} 000035 129554
03 AVG. BASE SHLT POLE 140 1068 : 1 : 00761} 000036 129555
: E 0 : 00761} 000037 129556
7 1150 +--14-+------28-----+ : 00761} 000038 129557
142880 6 B 6 : 00761} 000039 129558
C-05 95 135736 +--10+---16--+ 00761} 000040 129559
07 P.H/AC 6354 42/ / 5 60946 00761} 000042 129560
104 1ST.SG 5100 XF UD FACT 00761} 000043 129561
74790 .00 74800 00761} 000044 129562
28 STG BN 1 1/S 26X30 780 300 00761} 000049 129563
10 GAR-FR 1 FR 20X20 400 400 00761} 000050 129564
DIRT FACT 00761} 000051 129565
B S 1.000 2.40 2.40 3800 9120 00761} 000052 129566
U/R .390 2.00 2.00 3200 2496 00761} 000055 129567
1.390 11616 00761} 000058 129568
700 00761} 000059 129569
11600 00761} 000061 129570
10/13/2009 00761} 000062 129571
NO - 75500 00761} 000063 129572
87100 11/28/22 00761} 000066 129573
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-2102.000 005337 000002 755612
99369 03 L 12 105 600 600 1 K & S LLC 005337 000003 755613
3-04644 005337 000004 755614
K & S FOOD MART LLC 14 00 04 01 00 01 005337 000005 755615
7824 SEVEN CREEKS HWY 1227 4512020 M M RAY RD 005337 000006 755616
28455 00-0000 005337 000007 755617
NAKINA NC NF -- CR -- 005337 000008 755618
SEE 426/227(DESC) 005337 000009 755619
/ / 005337 000042 755620
XF UD FACT 005337 000043 755621
.00 005337 000044 755622
DIRT FACT 005337 000051 755623
U/R .060 3.00 3.00 3200 576 005337 000055 755624
.060 576 005337 000058 755625
600 005337 000061 755626
5/08/2020 005337 000062 755627
NO - 005337 000063 755628
600 11/28/22 005337 000066 755629
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-2162.000 005334 000002 755524
7419 03 L 12 105 167500 182800 1 K & S LLC 005334 000003 755525
3-04644 005334 000004 755526
K & S FOOD MART LLC 04 41 04 01 01 01 005334 000005 755527
7824 SEVEN CREEKS HWY 1227 4512020 7842 SEVEN CREEKS HWY 005334 000006 755528
28455 PPD 11-1590 005334 000007 755529
NAKINA NC NF -- CR -- 005334 000008 755530
DBA: HR MART//REMOD'02--CNP-SER FR#7419 FOR'06 +--------------60-------------+ 005334 000009 755531
SEE SURVEY 22/51'02//AC CORR FOR'06 : : A 04 005334 000010 755532
GRD,OCCUP,SFT & AWNING CORR FOR'18 : : B 04 005334 000011 755533
SEE 426/227(DESC) : : C 06 005334 000012 755534
: : 005334 000013 755535
1975 A 1980 : : 005334 000014 755536
: : 005334 000015 755537
03 SLAB : : 005334 000016 755538
: : 005334 000017 755539
02 SLAB BASE 4500 61.65 : : 005334 000018 755540
: : 005334 000019 755541
04 STL/FP BASE 4500 61.65 277425 : : 005334 000020 755542
03 CO.BLK 01-1STY : : 005334 000021 755543
02 STONE BASE : : 005334 000022 755544
7 : 005334 000023 755545
03 STL.TR BASE 1 5 7 005334 000024 755546
4 +4: 5 005334 000025 755547
02 BLT-UP CNP/AWN 280 3743 : : : 005334 000026 755548
01 FLAT 4 : : : 005334 000027 755549
BASE CNP/AWN 60 861 1 : : 005334 000028 755550
08 H.TILE 6 5 B : 005334 000029 755551
06 CONC. BASE COV P 140 3233 + : : 005334 000030 755552
+--10: : 005334 000031 755553
03 AVG. BASE : : : 005334 000032 755554
1 : : 005334 000033 755555
03 AVG BASE 4 : : 005334 000034 755556
: C : : 005334 000035 755557
03 AVG. BASE +---4: : 005334 000036 755558
: : 50 : 005334 000037 755559
3 1875 1 +--------------60-------------+ 005334 000038 755560
324577 0 A 4 005334 000039 755561
C+- 100 324577 +---------------64--------------+ 005334 000040 755562
07 P.H/AC 37440 45/ / 146060 005334 000042 755563
01 NONE XF UD FACT 005334 000043 755564
178517 .00 178500 005334 000044 755565
DIRT FACT 005334 000051 755566
B S .380 3.00 3.00 3800 4332 005334 000052 755567
.380 4332 005334 000058 755568
4300 005334 000061 755569
5/08/2020 005334 000062 755570
NO - 178500 005334 000063 755571
182800 11/28/22 005334 000066 755572
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-4354.000 00274N 000002 976115
8418 03 L 12 13 11800 12200 1 COURTNEY HEATH 00274N 000003 976116
3-01352 00274N 000004 976117
NAKINA BAPTIST CHURCH INC 13 00 04 01 00 01 00274N 000005 976118
7883 SEVEN CREEKS HWY 790 6562004 5000 7843 SEVEN CREEKS HWY 00274N 000006 976119
PO BOX 120 28455 PPD 11-1590 00274N 000007 976120
NAKINA NC NF -- CR -- 00274N 000008 976121
AC CORR BY 76/90'05 00274N 000009 976122
1943HSE TO #90404'06 00274N 000010 976123
/ / 00274N 000042 976124
XF UD FACT 00274N 000043 976125
.00 00274N 000044 976126
23 SHED 1 300 0 00274N 000049 976127
DIRT FACT 00274N 000051 976128
U/R 1.910 2.00 2.00 3200 12224 00274N 000055 976129
1.910 12224 00274N 000058 976130
25000 12200 00274N 000061 976131
8/27/2004 00274N 000062 976132
NO - K 00274N 000063 976133
12200 11/28/22 00274N 000066 976134
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-6001.000 00274M 000002 976135
61110 03 L 12 26 439100 464100 1 2@ WARD 00274M 000003 976136
3-01352 00274M 000004 976137
NAKINA BAPTIST CHURCH INC 07 10 04 01 01 01 00274M 000005 976138
7883 SEVEN CREEKS HWY 797 7882004 7883 SEVEN CREEKS HWY 00274M 000006 976139
PO BOX 120 28455 PPD 11-1590 00274M 000007 976140
NAKINA NC NF -- CR -- 00274M 000008 976141
1930 BLDG OFF/1985 BLDG ADDED(REVAL) 00274M 000009 976142
#61109 COM/HERE;AC CORR'05 A 05 00274M 000010 976143
CARPORT ADDED FOR'14 B 06 00274M 000011 976144
1985 A 00274M 000014 976145
03 SLAB 00274M 000016 976146
+------39----+ 00274M 000017 976147
02 SLAB BASE 5218 85.46 : : 00274M 000018 976148
: : 00274M 000019 976149
01 WD.FR. BASE 5218 85.46 445930 : : 00274M 000020 976150
01-1STY : : 00274M 000021 976151
01 BRICK BASE : : 00274M 000022 976152
5 5 00274M 000023 976153
01 WD.FR. BASE 1 0 0 00274M 000024 976154
5 : : 00274M 000025 976155
01 COMP. CARPORT 806 14991 : : 00274M 000026 976156
03 GABEL 6 : : 00274M 000027 976157
BASE COV P 112 2586 +---26--+ : : 00274M 000028 976158
05 CARPET : +-----36----+ +-11 00274M 000029 976159
04 VINYL BASE : : : 00274M 000030 976160
: : : 00274M 000031 976161
03 AVG. BASE 3 : : 00274M 000032 976162
1 3 : 00274M 000033 976163
03 AVG BASE : 8 3 00274M 000034 976164
: A : 8 00274M 000035 976165
03 AVG. BASE +---26--: : 00274M 000036 976166
: 50 : 00274M 000037 976167
+-------------86------------+ 00274M 000038 976168
463506 8 B 8 00274M 000039 976169
C+10 110 509857 +-14+ 00274M 000040 976170
01 NONE 39/ / 198844 00274M 000042 976171
01 NONE XF UD FACT 00274M 000043 976172
311013 .00 311000 00274M 000044 976173
DIRT FACT 00274M 000051 976174
B S 1.000 2.40 2.40 3800 9120 00274M 000052 976175
U/R 1.090 1.80 1.80 3200 6278 00274M 000055 976176
2.090 15398 00274M 000058 976177
15400 00274M 000061 976178
11/06/2004 00274M 000062 976179
NO - 311000 00274M 000063 976180
326400 11/28/22 00274M 000066 976181
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-6001.000 00274L 000002 976182
61110 03 L 12 26 439100 464100 2 2@ WARD 00274L 000003 976183
3-01352 00274L 000004 976184
NAKINA BAPTIST CHURCH INC 07 52 04 01 00 01 00274L 000005 976185
7883 SEVEN CREEKS HWY 797 7882004 7883 SEVEN CREEKS HWY 00274L 000006 976186
PO BOX 120 28455 00-0000 00274L 000007 976187
NAKINA NC NF -- CR -- 00274L 000008 976188
FELLOWSHIP HALL 100%'02 00274L 000009 976189
A 06 00274L 000010 976190
+-------46-----+ 00274L 000012 976191
: : 00274L 000013 976192
2002 G : : 00274L 000014 976193
: : 00274L 000015 976194
03 SLAB : : 00274L 000016 976195
: : 00274L 000017 976196
02 SLAB BASE 4224 30.55 : : 00274L 000018 976197
: : 00274L 000019 976198
01 WD.FR. BASE 4224 30.55 129043 : : 00274L 000020 976199
01-1STY : : 00274L 000021 976200
01 BRICK BASE 7 7 00274L 000022 976201
6 6 00274L 000023 976202
01 WD.FR. BASE 2 24 : : 00274L 000024 976203
6 : : 00274L 000025 976204
01 COMP. COV P 280 5379 : : 00274L 000026 976205
03 GABEL : : 00274L 000027 976206
BASE : : 00274L 000028 976207
06 CONC. : : 00274L 000029 976208
05 CARPET BASE : : 00274L 000030 976209
50 : 00274L 000031 976210
03 AVG. BASE +9-+ +9-+ 00274L 000032 976211
: : 00274L 000033 976212
03 AVG BASE : : 00274L 000034 976213
2 2 00274L 000035 976214
03 AVG. BASE 6 6 00274L 000036 976215
: : 00274L 000037 976216
4 2500 +---28---+ 00274L 000038 976217
172065 1 A 1 00274L 000039 976218
C+- 100 172065 0----28--0 00274L 000040 976219
07 P.H/AC 35143 20/ / 34413 00274L 000042 976220
01 NONE XF UD FACT 00274L 000043 976221
137652 .00 137700 00274L 000044 976222
DIRT FACT 00274L 000051 976223
B S 00274L 000052 976224
U/R 00274L 000055 976225
11/04/2002 00274L 000062 976226
NO - 137700 00274L 000063 976227
137700 11/28/22 00274L 000066 976228
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-6001.000 00274K 000002 976229
61110 03 L 12 26 439100 464100 2 2@ WARD 00274K 000003 976230
LEES 00274K 000004 976231
NAKINA BAPTIST CHURCH INC 00274K 000005 976232
7883 SEVEN CREEKS HWY 797 00274K 000006 976233
PO BOX 120 28455 0000000 00274K 000007 976234
SUMMARY CARD 00274K 000012 976235
15400 00274K 000062 976236
NO - 448700 00274K 000063 976237
448700 00274K 000064 976238
464100 00274K 000066 976239
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-6687.000 003862 000002 115078
102688 03 L 12 31 69200 1 003862 000003 115079
3-00965 003862 000004 115080
BOST DAMIEN DRAPER 03 37 04 01 01 01 003862 000005 115081
7953 SEVEN CREEKS HWY 1272 5862021 27000 7953 SEVEN CREEKS HWY 003862 000006 115082
28455 PPD 11-1590 003862 000007 115083
NAKINA NC NF -- CR -- 003862 000008 115084
'77HSE FR #8231 C/HERE FOR'22 003862 000009 115085
A 05 003862 000010 115086
B 06 003862 000011 115087
C 21 003862 000012 115088
1977 G 1984 003862 000014 115089
04 PER.FT 003862 000016 115090
03 WD.FR. BASE 1026 89.01 003862 000018 115091
01 WD.FR. BASE 1026 89.01 91324 003862 000020 115092
01-1STY 003862 000021 115093
01 BRICK BASE 003862 000022 115094
01 WD.FR. BASE 1 003862 000024 115095
5 003862 000025 115096
01 COMP. CARPORT 308 6673 003862 000026 115097
03 GABEL 6 003862 000027 115098
BASE COV P 54 1490 003862 000028 115099
21 003862 000029 115100
01 S.WOOD BASE BR STG 40 1558 +-----------48----------+-8-+ 003862 000030 115101
: 50 :C 5 003862 000031 115102
03 AVG. BASE : +6-+-8-+ 003862 000032 115103
: : : 003862 000033 115104
03 AVG BASE : : : 003862 000034 115105
2 1 : 003862 000035 115106
03 AVG. BASE 5 7 2 003862 000036 115107
: : 2 003862 000037 115108
7 1150 : +---18---+ : 003862 000038 115109
107017 : : B : A : 003862 000039 115110
C+- 100 107017 +-----24----+---18---+---14-+ 003862 000040 115111
07 P.H/AC 4822 42/ / 44947 003862 000042 115112
01 NONE XF UD FACT 003862 000043 115113
62070 .00 62100 003862 000044 115114
DIRT FACT 003862 000051 115115
B S .690 2.70 2.70 3800 7079 003862 000052 115116
.690 7079 003862 000058 115117
135000 7100 003862 000061 115118
11/01/2021 003862 000062 115119
YES 62100 003862 000063 115120
69200 11/28/22 003862 000066 115121
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1103.00-09-8436.000 006266 000002 186854
6503 03 L 12 30 111400 125000 1 006266 000003 186855
3-02260 006266 000004 186856
BUTLER ROYCE & DORIS 03 37 04 01 01 01 006266 000005 186857
PO BOX 70 830 768 7987 SEVEN CREEKS HWY 006266 000006 186858
28455 PPD 11-1590 006266 000007 186859
NAKINA NC NF -- CR -- 006266 000008 186860
CHIM CORR FOR'19-R//SEE 233/578;244/218 006266 000009 186861
A 05 006266 000010 186862
B 06 006266 000011 186863
C 06 006266 000012 186864
D 26 006266 000013 186865
1967 G 1984 006266 000014 186866
04 PER.FT 006266 000016 186867
03 WD.FR. BASE 2088 76.40 006266 000018 186868
01 WD.FR. BASE 2088 76.40 159523 006266 000020 186869
01-1STY 006266 000021 186870
01 BRICK BASE 006266 000022 186871
01 WD.FR. BASE 1 006266 000024 186872
5 006266 000025 186873
01 COMP. CARPORT 696 13514 006266 000026 186874
03 GABEL 6 006266 000027 186875
BASE COV P 48 1324 +-12+ 006266 000028 186876
6 +6+ : 1 006266 000029 186877
02 H.WOOD BASE COV P 24 701 C4 : 1 D 4 006266 000030 186878
26 +-----------72----4-----+---24--+ 006266 000031 186879
03 AVG. BASE SLAB/PAT 168 636 : : : 006266 000032 186880
: : : 006266 000033 186881
03 AVG BASE 2 : : 006266 000034 186882
9 2 2 006266 000035 186883
03 AVG. BASE : 9 9 006266 000036 186884
: 50 : A : 006266 000037 186885
11 3450 +-----------72----------+---24--+ 006266 000038 186886
199161 4 B 4 006266 000039 186887
C+- 100 199161 +-12+ 006266 000040 186888
07 P.H/AC 9813 42/ / 83648 006266 000042 186889
204 1ST.SG 10200 XF UD FACT 006266 000043 186890
115513 .00 115500 006266 000044 186891
23 SHED 1 FR 16X18 288 400 006266 000049 186892
DIRT FACT 006266 000051 186893
B S 1.000 2.40 2.40 3800 9120 006266 000052 186894
1.000 9120 006266 000058 186895
400 006266 000059 186896
9100 006266 000061 186897
NO - 115900 006266 000063 186898
125000 11/28/22 006266 000066 186899
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-5222.000 009238 000002 274912
62028 03 L 12 14 9400 10600 1 WACCAMAW MEMORIAL VERERANS 009238 000003 274913
3-04173 009238 000004 274914
COLUMBUS COUNTY MEMORIAL VETERANS 07 52 04 01 01 01 009238 000005 274915
OF FOREIGN WARS POST #8073 1209 6362019 4604 ERVIN T RICHARDSON RD 009238 000006 274916
PO BOX 912 29569 PPD 11-1590 009238 000007 274917
LORIS SC NF -- CR -- 009238 000008 274918
WHITE//NAME CORR'02(POST 6066(VFW) 009238 000009 274919
1978 F 009238 000014 274920
03 SLAB 009238 000016 274921
03 WD.FR. BASE 1440 28.33 009238 000018 274922
01 WD.FR. BASE 1440 28.33 40795 009238 000020 274923
01-1STY +-------30-----+ 009238 000021 274924
09 COR.MT BASE : : 009238 000022 274925
: : 009238 000023 274926
01 WD.FR. BASE 1 : : 009238 000024 274927
: : 009238 000025 274928
01 COMP. : : 009238 000026 274929
03 GABEL : : 009238 000027 274930
BASE : : 009238 000028 274931
: : 009238 000029 274932
06 CONC. BASE 4 : 009238 000030 274933
8 4 009238 000031 274934
03 AVG. BASE : 8 009238 000032 274935
: : 009238 000033 274936
03 AVG BASE : : 009238 000034 274937
: : 009238 000035 274938
03 AVG. BASE : : 009238 000036 274939
: : 009238 000037 274940
4 2500 : : 009238 000038 274941
43294 : 50 : 009238 000039 274942
E+- 65 28141 +------30------+ 009238 000040 274943
01 NONE 70/ / 19699 009238 000042 274944
01 NONE XF UD FACT 009238 000043 274945
8442 .00 8400 009238 000044 274946
DIRT FACT 009238 000051 274947
B S .190 3.00 3.00 3800 2166 009238 000052 274948
.190 2166 009238 000058 274949
2200 009238 000061 274950
8/21/2019 009238 000062 274951
NO - 8400 009238 000063 274952
10600 11/28/22 009238 000066 274953
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-2736.000 00833M 000002 108563
7613 03 L 12 10 40500 44600 1 (LIFE ESTATE)/POST OFFICE TRACT/W RAY 00833M 000003 108564
3-03736 00833M 000004 108565
RAY CLAUDETTE SAXON 04 32 04 01 01 01 00833M 000005 108566
PO BOX 99 1036 3532012 7731 SEVEN CREEKS HWY 00833M 000006 108567
28455 PPD 11-1590 00833M 000007 108568
NAKINA NC NF -- CR -- 00833M 000008 108569
POST OFFICE/ COND CHG 00833M 000009 108570
SEE 1036/361 (LIFE);1159/238 A 04 00833M 000010 108571
1969 A 1974 00833M 000014 108572
02 PIER/P 00833M 000016 108573
03 WD.FR. BASE 988 77.99 00833M 000018 108574
02 MASON. BASE 988 77.99 77054 00833M 000020 108575
03 CO.BLK 01-1STY 00833M 000021 108576
01 BRICK BASE +--12-+ 00833M 000022 108577
: 8 00833M 000023 108578
01 WD.FR. BASE 1 8 A : 00833M 000024 108579
4 +------26----+ 00833M 000025 108580
01 COMP. CNP/AWN 96 1378 : : 00833M 000026 108581
03 GABEL : : 00833M 000027 108582
BASE : : 00833M 000028 108583
: : 00833M 000029 108584
06 CONC. BASE : : 00833M 000030 108585
: : 00833M 000031 108586
03 AVG. BASE 3 : 00833M 000032 108587
8 3 00833M 000033 108588
03 AVG BASE : 8 00833M 000034 108589
: : 00833M 000035 108590
03 AVG. BASE : : 00833M 000036 108591
: : 00833M 000037 108592
4 2500 : : 00833M 000038 108593
89152 : 50 : 00833M 000039 108594
D+- 85 75779 +-----26-----+ 00833M 000040 108595
07 P.H/AC 8220 52/ / 39405 00833M 000042 108596
01 NONE XF UD FACT 00833M 000043 108597
36374 .00 36400 00833M 000044 108598
DIRT FACT 00833M 000051 108599
B S .900 2.40 2.40 3800 8208 00833M 000052 108600
.900 8208 00833M 000058 108601
8200 00833M 000061 108602
6/01/2012 00833M 000062 108603
NO - 36400 00833M 000063 108604
44600 11/28/22 00833M 000066 108605
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
1104.00-00-1924.000 009712 000002 884016
7460 03 L 12 9 110300 133100 1 JOSEPH FLOYD 009712 000003 884017
3-15720 009712 000004 884018
MCDOWELL CHARLES T & REGINA S 03 37 04 01 01 01 009712 000005 884019
PO BOX 59 322 4091980 50 7691 SEVEN CREEKS HWY 009712 000006 884020
28455 PPD 11-1590 009712 000007 884021
NAKINA NC NF -- CR -- 009712 000008 884022
SHACKLEFORD**DOG**GARAGE ENC INTO 1/S PART OF DWG 009712 000009 884023
COND CHG A 06 009712 000010 884024
NAME CORR BY 322/409;AC CORR BY 43/84 FOR'09 009712 000011 884025
1980 A 1987 009712 000014 884026
04 PER.FT 009712 000016 884027
03 WD.FR. BASE 1740 75.66 009712 000018 884028
01 WD.FR. BASE 2301 75.66 174093 009712 000020 884029
02-1.5STY 009712 000021 884030
01 BRICK BASE 009712 000022 884031
01 WD.FR. BASE 1 009712 000024 884032
6 009712 000025 884033
01 COMP. COV P 220 4496 +----20---+ 009712 000026 884034
03 GABEL : : 009712 000027 884035
BASE +----22----+ 1 009712 000028 884036
08 H.TILE : 6 A 1 009712 000029 884037
01 S.WOOD BASE : +----20---+--------36-------+ 009712 000030 884038
: : : 009712 000031 884039
03 AVG. BASE 2 : : 009712 000032 884040
2 1 : 009712 000033 884041
03 AVG BASE : 6 : 009712 000034 884042
: 50 : 2 009712 000035 884043
03 AVG. BASE +----------42--------: 6 009712 000036 884044
: : 009712 000037 884045
8 1725 : : 009712 000038 884046
185414 : 90 : 009712 000039 884047
C+10 110 203955 +--------36-------+ 009712 000040 884048
05 FHA 39/ /10 91984 009712 000042 884049
104 1ST.SG 5100 XF UD FACT 009712 000043 884050
111971 .00 112000 009712 000044 884051
29 STG UTY 1 BR 13X24 312 1000 009712 000049 884052
5 CARPORT 1 SFR 24X30 7201019 21 7330 009712 000050 884053
DIRT FACT 009712 000051 884054
B S 1.000 2.40 2.40 3800 9120 009712 000052 884055
OPN .880 2.00 2.00 2100 3696 009712 000053 884056
1.880 12816 009712 000058 884057
8300 009712 000059 884058
12800 009712 000061 884059
3/01/1980 009712 000062 884060
NO - 120300 009712 000063 884061
133100 11/28/22 009712 000066 884062
COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS
MAP ACCESS TOPO LND IMP SHAPE
RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP
LISTED DATE BUILDING
APPR DATE ZONED % COMPLETE
ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS
VALUE DESCRIPTION VALUE
FOUNDATION ATTIC
FLOORING SYSTEM BASE OF AREA
STRUCTURAL FRM BASE S/F
EXTERIOR WALLS STORY
C/D
ROOF FRAMING WALL HEIGHT
ROOF COVER ATTACHMENTS
ROOF DESIGN
FLOOR COVER
INTERIOR FINISH
CAB/MILL WORK
ELECTRICAL
PLUMBING
FIXTURES
PERIMETER MULT
SPRINKLER
SYSTEM
GRADE
HEAT/COOL DEPR P/F/E
FIREPLACE TOTAL
VALUE
BASEMENT NEIGHBORHOOD
INFLUENCE
SUMMARY OF OTHER IMPROVEMENTS
LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE
SALES INFORMATION
AMOUNT:
DATE:
QUAL SALE:
TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS
TOTAL VALUE LAND
TOTAL VALUE BUILDINGS
TOTAL VALUE
LAND DESCRIPTION CALCULATIONS
FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE
CLASS ACRES SIZE FAC NET %RATE LAND VALUE
TOTAL
ACRES TOTAL LAND VALUE
LAND USE VALUATIONS AND TOTALS
CLASS # ACRES RATE LAND VALUE
BUILDING SITE
TOTAL ACRES
TOTAL USE
VALUE LAND
TOTAL USE
VALUE BUILDINGS
TOTAL USE VALUE
0194.00-90-9656.000 00482N 000002 512129
7771 03 L 12 108 151700 164700 1 CLYDE WILLIAMSON 00482N 000003 512130
3-00231 00482N 000004 512131
WILLIAMSON RYAN K 03 33 04 01 01 01 00482N 000005 512132
1180 ERVIN T RICHARDSON RD 875 1252006 7722 SEVEN CREEKS HWY 00482N 000006 512133
28455 PPD 11-1590 00482N 000007 512134
NAKINA NC NF -- CR -- 00482N 000008 512135
35X33 AREA IS RETAIL * THE REST IS A RESTURANT 00482N 000009 512136
SEE 875/127(ETAL);993/607 ETALS REMVED FOR'11 A 06 00482N 000010 512137
B 09 00482N 000011 512138
1989 A 1996 00482N 000014 512139
03 SLAB 00482N 000016 512140
02 SLAB BASE 3073 61.51 +-------33------+ 00482N 000018 512141
: 6 00482N 000019 512142
01 WD.FR. BASE 3073 61.51 189020 : +----18--+------28-----+ 00482N 000020 512143
01-1STY : : : 00482N 000021 512144
06 WD/LOG BASE : 1 1 00482N 000022 512145
: 2 A 2 00482N 000023 512146
01 WD.FR. BASE 1 3 +------28-----+ 00482N 000024 512147
6 5 : 00482N 000025 512148
01 COMP. COV P 336 6043 : : 00482N 000026 512149
03 GABEL 9 : : 00482N 000027 512150
BASE E GL P 35 1948 : : 00482N 000028 512151
06 CONC. : 50 : 00482N 000029 512152
05 CARPET BASE +-------33------+ : 00482N 000030 512153
: 3 00482N 000031 512154
03 AVG. BASE : 7 00482N 000032 512155
: : 00482N 000033 512156
03 AVG BASE 2 : 00482N 000034 512157
0 : 00482N 000035 512158
03 AVG. BASE : : 00482N 000036 512159
: : 00482N 000037 512160
6 3750 +----------46----------+ 00482N 000038 512161
226328 5 B5 00482N 000039 512162
C+- 100 226328 +-7+ 00482N 000040 512163
07 P.H/AC 25567 30/ / 67898 00482N 000042 512164
01 NONE XF UD FACT 00482N 000043 512165
158430 .00 158400 00482N 000044 512166
DIRT FACT 00482N 000051 512167
B S .610 2.70 2.70 3800 6258 00482N 000052 512168
.610 6258 00482N 000058 512169
6300 00482N 000061 512170
9/23/2010 00482N 000062 512171
NO - 158400 00482N 000063 512172
164700 12/12/22 00482N 000066 512173

APPENDIX B
Well Construction Record and Subsurface Log
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Sam Bowers
3220 A
Geological Resources, Inc.
4
11/21/22 MW-1
Home Race Mart #1 00-0-0000034121
7824 Seven Springs Highway, Nakina, NC
Columbus 1104.00-00-2162.000
34.134276 78.668266
4
4
1
12
4.06
6
Solid flight auger
0 2 2 sch 40 PVC
2 12 2 0.010 sch 40 PVC
0 0.5 Grout
0.5 1 Bentonite
1 12 Sand
0 0.4 Asphalt
0.4 2 Brown silt
2 7 Brown clay
7 10 Gray fine sand
10 12 Tan fine sand
11/29/2022
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Home Race Mart #1
Address 7824 Seven Springs Highway, Nakina, NC
Boring Number MW-1 Date Drilled
Sample Method Grab Drilling Method Solid flight auger
Completion Details Well installed at completion to a total depth of 12 feet with a 10 foot screened interval
Driller Sam Bowers Log By J. Brooks
Lab Sample OVADepthSampleInterval(ft)ppm LITHOLOGY
0 - 0.4'; Asphalt
0
2
4

6
8
10

12
14

16

18
20

22

24
26

28

30
32
34

36

38

40

11/21/22
0.4' - 2'; Brown silt (dry)
2' - 7'; Brown clay (moist)

7' - 10'; Gray fine sand (moist)
10' - 12'; Tan fine sand (wet)
Well set at 12'

APPENDIX C
Laboratory Reports – Soil and Ground Water Samples
12/08/22
Technical Report for
GRI (Geological Resources Inc.)
Home Race 1; 7824 Seven Circle Rd, Nakina, NC
5836
SGS Job Number: FC801
Sampling Date: 11/21/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Ethan Rogerson
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 12/08/22
e-Hardcopy 2.0
Automated Report
79
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 79
FC801
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FC801-1: TRIP BLANK ...............................................................................................6
3.2: FC801-2: MW-1 (5') .....................................................................................................8
3.3: FC801-3: MW-1 ............................................................................................................14
Section 4: Misc. Forms ............................................................................................................22
4.1: Chain of Custody ...........................................................................................................23
Section 5: MS Volatiles - QC Data Summaries .....................................................................25
5.1: Method Blank Summary ................................................................................................26
5.2: Blank Spike Summary ...................................................................................................30
5.3: Matrix Spike Summary ..................................................................................................34
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................37
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................39
6.1: Method Blank Summary ................................................................................................40
6.2: Blank Spike Summary ...................................................................................................44
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................48
Section 7: GC Volatiles - QC Data Summaries .....................................................................50
7.1: Method Blank Summary ................................................................................................51
7.2: Blank Spike Summary ...................................................................................................52
7.3: Duplicate Summary .......................................................................................................53
Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................54
8.1: Method Blank Summary ................................................................................................55
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................57
8.3: Duplicate Summary .......................................................................................................60
Section 9: Metals Analysis - QC Data Summaries ................................................................61
9.1: Prep QC MP41544: Pb ..................................................................................................62
Section 10: Misc. Forms (SGS Scott, LA) ..............................................................................68
10.1: Chain of Custody .........................................................................................................69
Section 11: GC Volatiles - QC Data (SGS Scott, LA) ...........................................................73
11.1: Method Blank Summary ..............................................................................................74
11.2: Blank Spike/Blank Spike Duplicate Summary ............................................................76
11.3: Duplicate Summary .....................................................................................................78 12345678910112 of 79
FC801
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FC801
Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Project No: 5836
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC801-1 11/21/22 13:53 JB 11/23/22 AQ Trip Blank Water TRIP BLANK
FC801-2 11/21/22 14:27 JB 11/23/22 SO Soil MW-1 (5')
FC801-3 11/21/22 15:04 JB 11/23/22 AQ Ground Water MW-1
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 79
FC8011
Summary of Hits Page 1 of 1
Job Number:FC801
Account:GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Collected:11/21/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC801-1 TRIP BLANK
No hits reported in this sample.
FC801-2 MW-1 (5')
C11-C22 Aromatics (Unadj.)8.47 J 13 5.1 mg/kg MADEP EPH REV 2.1
FC801-3 MW-1
Diethyl Phthalate 4.8 4.8 0.95 ug/l EPA 625.1
Naphthalene a 0.71 J 5.0 0.41 ug/l MADEP VPH REV 2.1
m,p-Xylene a 0.62 J 10 0.40 ug/l MADEP VPH REV 2.1
o-Xylene a 0.30 J 5.0 0.18 ug/l MADEP VPH REV 2.1
Lead 248 5.0 ug/l SW846 6010D
(a) Analysis performed at SGS Scott, LA.
4 of 79
FC8012
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 79
FC8013
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC801-1 Date Sampled:11/21/22
Matrix:AQ - Trip Blank Water Date Received:11/23/22
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0236099.D 1 12/05/22 13:44 SS n/a n/a VA3311
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 79
FC80133.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FC801-1 Date Sampled:11/21/22
Matrix:AQ - Trip Blank Water Date Received:11/23/22
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 79
FC80133.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:SW846 8260D Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2B20415.D 1 11/28/22 16:51 DB n/a n/a V2B862
Run #2
Initial Weight Final Volume
Run #1 7.10 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 0.18 0.091 mg/kg
71-43-2 Benzene ND 0.0045 0.0011 mg/kg
75-27-4 Bromodichloromethane ND 0.0045 0.00091 mg/kg
75-25-2 Bromoform ND 0.0045 0.00091 mg/kg
78-93-3 2-Butanone (MEK)ND 0.023 0.0066 mg/kg
104-51-8 n-Butylbenzene ND 0.0045 0.00091 mg/kg
75-15-0 Carbon Disulfide ND 0.0045 0.00091 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0045 0.00092 mg/kg
108-90-7 Chlorobenzene ND 0.0045 0.00091 mg/kg
75-00-3 Chloroethane ND 0.0045 0.0018 mg/kg
67-66-3 Chloroform ND 0.0045 0.0012 mg/kg
110-82-7 Cyclohexane ND 0.0045 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0045 0.00091 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0045 0.0017 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0045 0.00091 mg/kg
75-71-8 Dichlorodifluoromethane a ND 0.0045 0.0018 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0045 0.00091 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0045 0.00091 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0045 0.0010 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0045 0.0016 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0045 0.00091 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0045 0.00091 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0045 0.0012 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0045 0.00091 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0045 0.00091 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0045 0.00091 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0045 0.00091 mg/kg
100-41-4 Ethylbenzene ND 0.0045 0.00091 mg/kg
591-78-6 2-Hexanone ND 0.023 0.0068 mg/kg
98-82-8 Isopropylbenzene ND 0.0045 0.00091 mg/kg
79-20-9 Methyl Acetate ND 0.023 0.0081 mg/kg
74-83-9 Methyl Bromide a ND 0.0045 0.0018 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:SW846 8260D Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0045 0.0018 mg/kg
108-87-2 Methylcyclohexane ND 0.0045 0.0015 mg/kg
75-09-2 Methylene Chloride ND 0.018 0.010 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.023 0.0068 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0045 0.00091 mg/kg
91-20-3 Naphthalene ND 0.0045 0.0018 mg/kg
103-65-1 n-Propylbenzene ND 0.0045 0.00091 mg/kg
100-42-5 Styrene ND 0.0045 0.00091 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0045 0.00091 mg/kg
127-18-4 Tetrachloroethylene ND 0.0045 0.0012 mg/kg
108-88-3 Toluene ND 0.018 0.0091 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0045 0.00091 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0045 0.00091 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0045 0.00091 mg/kg
79-01-6 Trichloroethylene ND 0.0045 0.00091 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0045 0.0018 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0045 0.00091 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0045 0.00091 mg/kg
75-01-4 Vinyl Chloride ND 0.0045 0.00091 mg/kg
1330-20-7 Xylene (total)ND 0.014 0.0019 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%75-124%
17060-07-0 1,2-Dichloroethane-D4 89%72-135%
2037-26-5 Toluene-D8 102%75-126%
460-00-4 4-Bromofluorobenzene 109%71-133%
(a) Associated CCV outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:SW846 8270E SW846 3550C Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F16818.D 1 11/28/22 14:50 KA 11/28/22 07:30 OP94242 S6F630
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.1 0.21 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.21 0.024 mg/kg
95-57-8 2-Chlorophenol ND 0.21 0.026 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.21 0.025 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.21 0.057 mg/kg
51-28-5 2,4-Dinitrophenol a ND 1.1 0.21 mg/kg
534-52-1 4,6-Dinitro-o-cresol a ND 0.43 0.086 mg/kg
95-48-7 2-Methylphenol ND 0.21 0.026 mg/kg
3&4-Methylphenol ND 0.21 0.035 mg/kg
88-75-5 2-Nitrophenol a ND 0.21 0.023 mg/kg
100-02-7 4-Nitrophenol ND 1.1 0.21 mg/kg
87-86-5 Pentachlorophenol ND 1.1 0.21 mg/kg
108-95-2 Phenol ND 0.21 0.021 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.21 0.025 mg/kg
83-32-9 Acenaphthene ND 0.21 0.023 mg/kg
208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg
120-12-7 Anthracene ND 0.21 0.024 mg/kg
56-55-3 Benzo(a)anthracene ND 0.21 0.021 mg/kg
50-32-8 Benzo(a)pyrene ND 0.21 0.025 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.21 0.023 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.21 0.022 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.21 0.028 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.022 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.21 0.043 mg/kg
106-47-8 4-Chloroaniline ND 0.21 0.054 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.025 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.21 0.027 mg/kg
91-58-7 2-Chloronaphthalene ND 0.21 0.021 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.021 mg/kg
218-01-9 Chrysene ND 0.21 0.022 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.027 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:SW846 8270E SW846 3550C Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.051 mg/kg
84-66-2 Diethyl Phthalate ND 0.43 0.043 mg/kg
131-11-3 Dimethyl Phthalate ND 0.21 0.043 mg/kg
117-84-0 Di-n-octyl Phthalate a ND 0.21 0.043 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.43 0.086 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.21 0.021 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.21 0.028 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.43 0.043 mg/kg
206-44-0 Fluoranthene ND 0.21 0.021 mg/kg
86-73-7 Fluorene ND 0.21 0.023 mg/kg
118-74-1 Hexachlorobenzene ND 0.21 0.022 mg/kg
87-68-3 Hexachlorobutadiene ND 0.21 0.022 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.21 0.043 mg/kg
67-72-1 Hexachloroethane ND 0.21 0.025 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.21 0.026 mg/kg
78-59-1 Isophorone ND 0.21 0.021 mg/kg
90-12-0 1-Methylnaphthalene ND 0.21 0.021 mg/kg
91-57-6 2-Methylnaphthalene ND 0.21 0.021 mg/kg
91-20-3 Naphthalene ND 0.21 0.021 mg/kg
98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.21 0.021 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.21 0.023 mg/kg
85-01-8 Phenanthrene ND 0.21 0.021 mg/kg
129-00-0 Pyrene ND 0.21 0.025 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 82%40-102%
4165-62-2 Phenol-d5 90%41-100%
118-79-6 2,4,6-Tribromophenol 67%42-108%
4165-60-0 Nitrobenzene-d5 84%40-105%
321-60-8 2-Fluorobiphenyl 76%43-107%
1718-51-0 Terphenyl-d14 85%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:MADEP VPH REV 2.1 Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE039494.D 1 12/02/22 17:24 ALA n/a n/a L:GLE2325
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.5 g 5.0 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.32 0.0088 mg/kg
100-41-4 Ethylbenzene ND 0.32 0.0091 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.32 0.0090 mg/kg
91-20-3 Naphthalene ND 0.32 0.024 mg/kg
108-88-3 Toluene ND 0.32 0.0081 mg/kg
m,p-Xylene ND 0.64 0.023 mg/kg
95-47-6 o-Xylene ND 0.32 0.011 mg/kg
C5- C8 Aliphatics (Unadj.)ND 6.4 3.2 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.4 3.2 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.4 3.2 mg/kg
C5- C8 Aliphatics ND 6.4 3.2 mg/kg
C9- C12 Aliphatics ND 6.4 3.2 mg/kg
C9- C10 Aromatics ND 6.4 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 94%70-130%
615-59-8 2,5-Dibromotoluene 79%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1 (5')
Lab Sample ID:FC801-2 Date Sampled:11/21/22
Matrix:SO - Soil Date Received:11/23/22
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:77.8
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN040658.D 1 11/29/22 16:45 AF 11/28/22 07:00 OP94241 GNN1873
Run #2
Initial Weight Final Volume
Run #1 20.3 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.25 0.13 mg/kg
208-96-8 Acenaphthylene ND 0.25 0.13 mg/kg
120-12-7 Anthracene ND 0.25 0.13 mg/kg
56-55-3 Benzo(a)anthracene ND 0.25 0.13 mg/kg
50-32-8 Benzo(a)pyrene ND 0.25 0.13 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.25 0.13 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.25 0.13 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.25 0.13 mg/kg
218-01-9 Chrysene ND 0.25 0.13 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.25 0.13 mg/kg
206-44-0 Fluoranthene ND 0.25 0.13 mg/kg
86-73-7 Fluorene ND 0.25 0.13 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.25 0.13 mg/kg
91-57-6 2-Methylnaphthalene ND 0.25 0.13 mg/kg
91-20-3 Naphthalene ND 0.25 0.13 mg/kg
85-01-8 Phenanthrene ND 0.25 0.13 mg/kg
129-00-0 Pyrene ND 0.25 0.13 mg/kg
C11-C22 Aromatics (Unadj.)8.47 13 5.1 mg/kg J
C9-C18 Aliphatics ND 13 3.2 mg/kg
C19-C36 Aliphatics ND 13 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 76%40-140%
580-13-2 2-Bromonaphthalene 95%40-140%
84-15-1 o-Terphenyl 87%40-140%
321-60-8 2-Fluorobiphenyl 91%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 79
FC80133.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0236112.D 1 12/05/22 19:10 SS n/a n/a VA3311
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Vials combined due to high silt.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F16815.D 1 11/28/22 13:32 KA 11/28/22 06:15 OP94245 S6F630
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol a ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol a ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol b ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate c ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether c ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane) cND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate 4.8 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate b ND 4.8 0.95 ug/l
121-14-2 2,4-Dinitrotoluene ND 4.8 0.77 ug/l
606-20-2 2,6-Dinitrotoluene ND 4.8 0.68 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone c ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 44%14-67%
4165-62-2 Phenol-d5 33%10-50%
118-79-6 2,4,6-Tribromophenol 64%33-118%
4165-60-0 Nitrobenzene-d5 77%42-108%
321-60-8 2-Fluorobiphenyl 67%40-106%
1718-51-0 Terphenyl-d14 72%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
(b) Associated BS and CCV outside of control limits high, sample was ND.
(c) Associated BS outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:EPA 504.1 SW846 8011 Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CC086640.D 1 12/05/22 17:21 AF 12/02/22 13:20 OP94349 GCC2239
Run #2 a CC086694.D 1 12/07/22 00:53 AF 12/02/22 13:20 OP94349 GCC2241
Initial Volume Final Volume
Run #1 38.2 ml 2.0 ml
Run #2 38.2 ml 2.0 ml
CAS No.Compound Result RL MDL Units Q
106-93-4 1,2-Dibromoethane ND 0.018 0.0092 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 64%81%63-137%
(a) Sample reanalyzed beyond hold time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE039452.D 1 11/30/22 22:15 ALA n/a n/a L:GLE2324
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene ND 5.0 0.17 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 0.71 5.0 0.41 ug/l J
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene 0.62 10 0.40 ug/l J
95-47-6 o-Xylene 0.30 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 110%70-130%
615-59-8 2,5-Dibromotoluene 112%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN040664.D 1 11/29/22 19:41 AF 11/29/22 06:00 OP94268 GNN1873
Run #2
Initial Volume Final Volume
Run #1 1050 ml 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 3.8 1.9 ug/l
208-96-8 Acenaphthylene ND 3.8 1.9 ug/l
120-12-7 Anthracene ND 3.8 1.9 ug/l
56-55-3 Benzo(a)anthracene ND 3.8 1.9 ug/l
50-32-8 Benzo(a)pyrene ND 3.8 1.9 ug/l
205-99-2 Benzo(b)fluoranthene ND 3.8 1.9 ug/l
191-24-2 Benzo(g,h,i)perylene ND 3.8 1.9 ug/l
207-08-9 Benzo(k)fluoranthene ND 3.8 1.9 ug/l
218-01-9 Chrysene ND 3.8 1.9 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 3.8 1.9 ug/l
206-44-0 Fluoranthene ND 3.8 1.9 ug/l
86-73-7 Fluorene ND 3.8 1.9 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 3.8 1.9 ug/l
91-57-6 2-Methylnaphthalene ND 3.8 1.9 ug/l
91-20-3 Naphthalene ND 3.8 1.9 ug/l
85-01-8 Phenanthrene ND 3.8 1.9 ug/l
129-00-0 Pyrene ND 3.8 1.9 ug/l
C11-C22 Aromatics (Unadj.)ND 190 76 ug/l
C9-C18 Aliphatics ND 190 48 ug/l
C19-C36 Aliphatics ND 190 48 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 75%40-140%
580-13-2 2-Bromonaphthalene 106%40-140%
84-15-1 o-Terphenyl 94%40-140%
321-60-8 2-Fluorobiphenyl 102%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 79
FC80133.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FC801-3 Date Sampled:11/21/22
Matrix:AQ - Ground Water Date Received:11/23/22
Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 248 5.0 ug/l 1 12/02/22 12/05/22 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA19074
(2) Prep QC Batch: MP41544
RL = Reporting Limit
21 of 79
FC80133.3
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
22 of 79
FC8014
FC801: Chain of Custody
Page 1 of 2
23 of 79
FC80144.1
Job Number:FC801 Client:GRI
Date / Time Received:11/23/2022 9:30:00 AM Delivery Method:FEDEX
Project:HOME RACE MART #1
Airbill #'s:1009 6379 9533
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments FROZEN @ 11/23/22 // 1045.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (0.8);
Cooler 1: (1.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.6; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SAMUELM Date:Date:11/23/2022 9:30:00 A
FC801: Chain of Custody
Page 2 of 2
24 of 79
FC80144.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
25 of 79
FC8015
Method Blank Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3311-MB A0236097.D 1 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
26 of 79
FC80155.1.1
Method Blank Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3311-MB A0236097.D 1 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
27 of 79
FC80155.1.1
Method Blank Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B862-MB 2B20406.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
110-82-7 Cyclohexane ND 5.0 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.9 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
79-20-9 Methyl Acetate ND 25 8.9 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.7 ug/kg
75-09-2 Methylene Chloride 20.1 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
28 of 79
FC80155.1.2
Method Blank Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B862-MB 2B20406.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene 13.1 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 93%75-124%
17060-07-0 1,2-Dichloroethane-D4 88%72-135%
2037-26-5 Toluene-D8 101%75-126%
460-00-4 4-Bromofluorobenzene 106%71-133%
29 of 79
FC80155.1.2
Blank Spike Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3311-BS a A0236095.D 1 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 9.6 96 70-130
74-97-5 Bromochloromethane 10 9.9 99 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.7 97 70-130
104-51-8 n-Butylbenzene 10 10.1 101 70-130
135-98-8 sec-Butylbenzene 10 11.1 111 70-130
98-06-6 tert-Butylbenzene 10 10.9 109 70-130
56-23-5 Carbon Tetrachloride 10 10.3 103 70-130
108-90-7 Chlorobenzene 10 10.2 102 70-130
75-00-3 Chloroethane 10 10.1 101 60-140
67-66-3 Chloroform 10 9.9 99 70-130
95-49-8 o-Chlorotoluene 10 10.5 105 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.1 91 70-130
106-93-4 1,2-Dibromoethane 10 10.1 101 70-130
75-71-8 Dichlorodifluoromethane 10 7.6 76 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.6 106 70-130
106-46-7 1,4-Dichlorobenzene 10 10.1 101 70-130
75-34-3 1,1-Dichloroethane 10 10.5 105 70-130
107-06-2 1,2-Dichloroethane 10 9.7 97 70-130
75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.7 97 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.5 105 70-130
108-20-3 Di-Isopropyl Ether 10 10.1 101 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 10.4 104 70-130
98-82-8 Isopropylbenzene 10 10.5 105 70-130
* = Outside of Control Limits.
30 of 79
FC80155.2.1
Blank Spike Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3311-BS a A0236095.D 1 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.7 107 70-130
74-83-9 Methyl Bromide 10 9.4 94 60-140
74-87-3 Methyl Chloride 10 9.5 95 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 9.4 94 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130
91-20-3 Naphthalene 10 9.9 99 70-130
103-65-1 n-Propylbenzene 10 10.9 109 70-130
100-42-5 Styrene 10 10 100 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.1 101 70-130
127-18-4 Tetrachloroethylene 10 10.8 108 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130
79-00-5 1,1,2-Trichloroethane 10 10.1 101 70-130
79-01-6 Trichloroethylene 10 10.1 101 70-130
75-69-4 Trichlorofluoromethane 10 10.2 102 60-140
96-18-4 1,2,3-Trichloropropane 10 9.6 96 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.4 104 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130
75-01-4 Vinyl Chloride 10 9.7 97 60-140
m,p-Xylene 20 21.2 106 70-130
95-47-6 o-Xylene 10 10.7 107 70-130
1330-20-7 Xylene (total)30 31.9 106 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) No MSD available for this run.
* = Outside of Control Limits.
31 of 79
FC80155.2.1
Blank Spike Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B862-BS 2B20404.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 276 110 61-152
71-43-2 Benzene 50 52.5 105 76-126
75-27-4 Bromodichloromethane 50 52.2 104 74-130
75-25-2 Bromoform 50 51.2 102 76-127
78-93-3 2-Butanone (MEK)250 285 114 75-137
104-51-8 n-Butylbenzene 50 45.4 91 71-128
75-15-0 Carbon Disulfide 50 46.4 93 72-122
56-23-5 Carbon Tetrachloride 50 50.7 101 78-133
108-90-7 Chlorobenzene 50 50.4 101 81-129
75-00-3 Chloroethane 50 46.9 94 68-133
67-66-3 Chloroform 50 52.2 104 72-123
110-82-7 Cyclohexane 50 49.2 98 73-126
124-48-1 Dibromochloromethane 50 51.8 104 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 44.4 89 70-137
106-93-4 1,2-Dibromoethane 50 51.6 103 77-126
75-71-8 Dichlorodifluoromethane 50 53.2 106 68-168
95-50-1 1,2-Dichlorobenzene 50 48.6 97 80-129
541-73-1 1,3-Dichlorobenzene 50 49.2 98 81-129
106-46-7 1,4-Dichlorobenzene 50 47.2 94 76-130
75-34-3 1,1-Dichloroethane 50 51.0 102 73-125
107-06-2 1,2-Dichloroethane 50 48.3 97 74-128
75-35-4 1,1-Dichloroethylene 50 46.1 92 81-136
156-59-2 cis-1,2-Dichloroethylene 50 55.8 112 74-126
156-60-5 trans-1,2-Dichloroethylene 50 46.1 92 70-127
78-87-5 1,2-Dichloropropane 50 49.9 100 74-125
10061-01-5 cis-1,3-Dichloropropene 50 52.7 105 80-123
10061-02-6 trans-1,3-Dichloropropene 50 50.7 101 75-131
100-41-4 Ethylbenzene 50 48.3 97 77-123
591-78-6 2-Hexanone 250 260 104 72-133
98-82-8 Isopropylbenzene 50 51.6 103 80-136
79-20-9 Methyl Acetate 250 241 96 67-137
74-83-9 Methyl Bromide 50 61.2 122 65-139
74-87-3 Methyl Chloride 50 47.5 95 71-144
108-87-2 Methylcyclohexane 50 51.9 104 75-128
75-09-2 Methylene Chloride 50 53.0 106 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 261 104 76-132
* = Outside of Control Limits.
32 of 79
FC80155.2.2
Blank Spike Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B862-BS 2B20404.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 54.2 108 77-120
91-20-3 Naphthalene 50 50.6 101 79-129
103-65-1 n-Propylbenzene 50 46.2 92 80-135
100-42-5 Styrene 50 53.0 106 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 47.1 94 71-126
127-18-4 Tetrachloroethylene 50 51.3 103 79-130
108-88-3 Toluene 50 49.5 99 76-124
120-82-1 1,2,4-Trichlorobenzene 50 50.9 102 78-130
71-55-6 1,1,1-Trichloroethane 50 52.3 105 70-129
79-00-5 1,1,2-Trichloroethane 50 50.1 100 74-124
79-01-6 Trichloroethylene 50 51.0 102 75-128
75-69-4 Trichlorofluoromethane 50 52.9 106 73-145
95-63-6 1,2,4-Trimethylbenzene 50 46.8 94 74-123
108-67-8 1,3,5-Trimethylbenzene 50 45.9 92 73-122
75-01-4 Vinyl Chloride 50 55.0 110 76-141
1330-20-7 Xylene (total)150 150 100 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 88%72-135%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 101%71-133%
* = Outside of Control Limits.
33 of 79
FC80155.2.2
Matrix Spike Summary Page 1 of 3
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC893-1MS A0236110.D 50 12/05/22 SS n/a n/a VA3311
FC893-1 a A0236119.D 50 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
FC893-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 203 500 821 124 70-130
108-86-1 Bromobenzene ND 500 572 114 70-130
74-97-5 Bromochloromethane ND 500 600 120 70-130
75-27-4 Bromodichloromethane ND 500 616 123 70-130
75-25-2 Bromoform ND 500 567 113 70-130
104-51-8 n-Butylbenzene 6.4 J 500 588 116 70-130
135-98-8 sec-Butylbenzene ND 500 648 130 70-130
98-06-6 tert-Butylbenzene ND 500 642 128 70-130
56-23-5 Carbon Tetrachloride ND 500 565 113 70-130
108-90-7 Chlorobenzene ND 500 611 122 70-130
75-00-3 Chloroethane ND 500 683 137 60-140
67-66-3 Chloroform ND 500 595 119 70-130
95-49-8 o-Chlorotoluene ND 500 646 129 70-130
106-43-4 p-Chlorotoluene ND 500 624 125 70-130
124-48-1 Dibromochloromethane ND 500 552 110 70-130
96-12-8 1,2-Dibromo-3-chloropropane ND 500 581 116 70-130
106-93-4 1,2-Dibromoethane ND 500 605 121 70-130
75-71-8 Dichlorodifluoromethane ND 500 501 100 60-140
95-50-1 1,2-Dichlorobenzene ND 500 595 119 70-130
541-73-1 1,3-Dichlorobenzene ND 500 619 124 70-130
106-46-7 1,4-Dichlorobenzene ND 500 587 117 70-130
75-34-3 1,1-Dichloroethane ND 500 621 124 70-130
107-06-2 1,2-Dichloroethane ND 500 598 120 70-130
75-35-4 1,1-Dichloroethylene ND 500 647 129 70-130
156-59-2 cis-1,2-Dichloroethylene ND 500 609 122 70-130
156-60-5 trans-1,2-Dichloroethylene ND 500 613 123 70-130
78-87-5 1,2-Dichloropropane ND 500 582 116 70-130
142-28-9 1,3-Dichloropropane ND 500 557 111 70-130
594-20-7 2,2-Dichloropropane ND 500 568 114 70-130
563-58-6 1,1-Dichloropropene ND 500 611 122 70-130
10061-01-5 cis-1,3-Dichloropropene ND 500 576 115 70-130
10061-02-6 trans-1,3-Dichloropropene ND 500 631 126 70-130
108-20-3 Di-Isopropyl Ether 14.0 J 500 640 125 70-130
100-41-4 Ethylbenzene 288 500 925 127 70-130
87-68-3 Hexachlorobutadiene ND 500 598 120 70-130
98-82-8 Isopropylbenzene 19.4 J 500 636 123 70-130
* = Outside of Control Limits.
34 of 79
FC80155.3.1
Matrix Spike Summary Page 2 of 3
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC893-1MS A0236110.D 50 12/05/22 SS n/a n/a VA3311
FC893-1 a A0236119.D 50 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
FC893-1 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene ND 500 620 124 70-130
74-83-9 Methyl Bromide ND 500 730 146*60-140
74-87-3 Methyl Chloride ND 500 635 127 60-140
74-95-3 Methylene Bromide ND 500 576 115 70-130
75-09-2 Methylene Chloride 123 500 648 105 70-130
1634-04-4 Methyl Tert Butyl Ether 37.7 500 652 123 70-130
91-20-3 Naphthalene 251 500 865 123 70-130
103-65-1 n-Propylbenzene 60.0 500 700 128 70-130
100-42-5 Styrene ND 500 600 120 70-130
630-20-6 1,1,1,2-Tetrachloroethane ND 500 590 118 70-130
79-34-5 1,1,2,2-Tetrachloroethane ND 500 609 122 70-130
127-18-4 Tetrachloroethylene ND 500 621 124 70-130
108-88-3 Toluene 1490 500 2170 136* b 70-130
87-61-6 1,2,3-Trichlorobenzene ND 500 602 120 70-130
120-82-1 1,2,4-Trichlorobenzene ND 500 610 122 70-130
71-55-6 1,1,1-Trichloroethane ND 500 614 123 70-130
79-00-5 1,1,2-Trichloroethane ND 500 608 122 70-130
79-01-6 Trichloroethylene ND 500 616 123 70-130
75-69-4 Trichlorofluoromethane ND 500 725 145*60-140
96-18-4 1,2,3-Trichloropropane ND 500 585 117 70-130
95-63-6 1,2,4-Trimethylbenzene 787 500 1410 125 70-130
108-67-8 1,3,5-Trimethylbenzene 159 500 760 120 70-130
75-01-4 Vinyl Chloride ND 500 662 132 60-140
m,p-Xylene 1320 1000 2670 135*70-130
95-47-6 o-Xylene 827 500 1500 135*70-130
1330-20-7 Xylene (total)2150 1500 4170 135*70-130
CAS No.Surrogate Recoveries MS FC893-1 Limits
1868-53-7 Dibromofluoromethane 100%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%99%70-130%
2037-26-5 Toluene-D8 100%100%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
(a) QC SAMPLE. rr50x, possible co. Sample was analyzed beyond the 12 hour analysis window.
* = Outside of Control Limits.
35 of 79
FC80155.3.1
Matrix Spike Summary Page 3 of 3
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC893-1MS A0236110.D 50 12/05/22 SS n/a n/a VA3311
FC893-1 a A0236119.D 50 12/05/22 SS n/a n/a VA3311
The QC reported here applies to the following samples:Method: SM 6200B
FC801-1, FC801-3
(b) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
36 of 79
FC80155.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC800-1MS 2B20419.D 1 11/28/22 DB n/a n/a V2B862
FC800-1MSD 2B20420.D 1 11/28/22 DB n/a n/a V2B862
FC800-1 2B20413.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
FC800-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 131 J 347 478 100 327 455 99 5 61-152/27
71-43-2 Benzene ND 69.3 68.8 99 65.4 63.0 96 9 76-126/26
75-27-4 Bromodichloromethane ND 69.3 65.0 94 65.4 60.2 92 8 74-130/25
75-25-2 Bromoform ND 69.3 50.9 73*65.4 49.2 75*3 76-127/26
78-93-3 2-Butanone (MEK)22.0 347 417 114 327 383 110 9 75-137/25
104-51-8 n-Butylbenzene ND 69.3 46.3 67*65.4 43.1 66*7 71-128/35
75-15-0 Carbon Disulfide 1.7 J 69.3 55.0 77 65.4 50.7 75 8 72-122/29
56-23-5 Carbon Tetrachloride ND 69.3 61.5 89 65.4 57.6 88 7 78-133/29
108-90-7 Chlorobenzene ND 69.3 57.9 84 65.4 53.1 81 9 81-129/29
75-00-3 Chloroethane ND 69.3 63.4 91 65.4 53.7 82 17 68-133/29
67-66-3 Chloroform ND 69.3 71.1 103 65.4 65.2 100 9 72-123/26
110-82-7 Cyclohexane ND 69.3 65.2 94 65.4 59.9 92 8 73-126/32
124-48-1 Dibromochloromethane ND 69.3 62.2 90 65.4 57.0 87 9 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 69.3 50.2 72 65.4 47.6 73 5 70-137/29
106-93-4 1,2-Dibromoethane ND 69.3 66.4 96 65.4 60.5 93 9 77-126/26
75-71-8 Dichlorodifluoromethane ND 69.3 71.9 104 65.4 63.7 97 12 68-168/29
95-50-1 1,2-Dichlorobenzene ND 69.3 51.6 74*65.4 47.9 73*7 80-129/32
541-73-1 1,3-Dichlorobenzene ND 69.3 51.6 74*65.4 46.7 71*10 81-129/33
106-46-7 1,4-Dichlorobenzene ND 69.3 48.0 69*65.4 44.3 68*8 76-130/32
75-34-3 1,1-Dichloroethane ND 69.3 69.2 100 65.4 63.8 98 8 73-125/27
107-06-2 1,2-Dichloroethane ND 69.3 65.6 95 65.4 60.9 93 7 74-128/23
75-35-4 1,1-Dichloroethylene ND 69.3 59.2 85 65.4 54.9 84 8 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 69.3 73.0 105 65.4 66.7 102 9 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 69.3 59.2 85 65.4 54.9 84 8 70-127/27
78-87-5 1,2-Dichloropropane ND 69.3 66.8 96 65.4 61.2 94 9 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND 69.3 63.4 91 65.4 58.8 90 8 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 69.3 61.0 88 65.4 55.1 84 10 75-131/28
100-41-4 Ethylbenzene ND 69.3 57.0 82 65.4 52.5 80 8 77-123/31
591-78-6 2-Hexanone ND 347 345 100 327 325 99 6 72-133/26
98-82-8 Isopropylbenzene ND 69.3 59.8 86 65.4 54.3 83 10 80-136/32
79-20-9 Methyl Acetate 55.3 347 278 64*327 251 60*10 67-137/30
74-83-9 Methyl Bromide ND 69.3 56.7 82 65.4 30.2 46*61*65-139/31
74-87-3 Methyl Chloride ND 69.3 65.5 95 65.4 58.8 90 11 71-144/27
108-87-2 Methylcyclohexane ND 69.3 65.9 95 65.4 60.2 92 9 75-128/31
75-09-2 Methylene Chloride ND 69.3 82.5 119 65.4 79.0 121 4 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 347 362 104 327 338 103 7 76-132/26
* = Outside of Control Limits.
37 of 79
FC80155.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC800-1MS 2B20419.D 1 11/28/22 DB n/a n/a V2B862
FC800-1MSD 2B20420.D 1 11/28/22 DB n/a n/a V2B862
FC800-1 2B20413.D 1 11/28/22 DB n/a n/a V2B862
The QC reported here applies to the following samples:Method: SW846 8260D
FC801-2
FC800-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND 69.3 72.8 105 65.4 67.5 103 8 77-120/24
91-20-3 Naphthalene ND 69.3 22.5 32*65.4 20.8 32*8 79-129/33
103-65-1 n-Propylbenzene ND 69.3 61.0 88 65.4 56.6 87 7 80-135/33
100-42-5 Styrene ND 69.3 36.0 52*65.4 30.9 47*15 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND 69.3 71.4 103 65.4 66.4 102 7 71-126/30
127-18-4 Tetrachloroethylene ND 69.3 61.9 89 65.4 57.7 88 7 79-130/31
108-88-3 Toluene 9.4 J 69.3 63.3 78 65.4 58.6 75*8 76-124/30
120-82-1 1,2,4-Trichlorobenzene ND 69.3 29.7 43*65.4 27.6 42*7 78-130/34
71-55-6 1,1,1-Trichloroethane ND 69.3 68.5 99 65.4 63.3 97 8 70-129/27
79-00-5 1,1,2-Trichloroethane ND 69.3 67.9 98 65.4 62.7 96 8 74-124/28
79-01-6 Trichloroethylene ND 69.3 64.2 93 65.4 58.7 90 9 75-128/27
75-69-4 Trichlorofluoromethane ND 69.3 28.4 41*65.4 28.6 44*1 73-145/31
95-63-6 1,2,4-Trimethylbenzene ND 69.3 57.5 83 65.4 53.4 82 7 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 69.3 59.1 85 65.4 54.1 83 9 73-122/33
75-01-4 Vinyl Chloride ND 69.3 73.0 105 65.4 68.5 105 6 76-141/27
1330-20-7 Xylene (total)ND 208 170 82 196 157 80 8 80-129/30
CAS No.Surrogate Recoveries MS MSD FC800-1 Limits
1868-53-7 Dibromofluoromethane 105%104%113%75-124%
17060-07-0 1,2-Dichloroethane-D4 88%87%100%72-135%
2037-26-5 Toluene-D8 98%99%142%* a 75-126%
460-00-4 4-Bromofluorobenzene 140%*120%155%* a 71-133%
(a) Outside control limits.
* = Outside of Control Limits.
38 of 79
FC80155.4.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
39 of 79
FC8016
Method Blank Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94245-MB 6F16814.D 1 11/28/22 KA 11/28/22 OP94245 S6F630
The QC reported here applies to the following samples:Method: EPA 625.1
FC801-3
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
40 of 79
FC80166.1.1
Method Blank Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94245-MB 6F16814.D 1 11/28/22 KA 11/28/22 OP94245 S6F630
The QC reported here applies to the following samples:Method: EPA 625.1
FC801-3
CAS No.Compound Result RL MDL Units Q
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 44%14-67%
4165-62-2 Phenol-d5 31%10-50%
118-79-6 2,4,6-Tribromophenol 67%33-118%
4165-60-0 Nitrobenzene-d5 91%42-108%
321-60-8 2-Fluorobiphenyl 77%40-106%
1718-51-0 Terphenyl-d14 87%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
41 of 79
FC80166.1.1
Method Blank Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-MB 6F16817.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
42 of 79
FC80166.1.2
Method Blank Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-MB 6F16817.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 83%40-102%
4165-62-2 Phenol-d5 90%41-100%
118-79-6 2,4,6-Tribromophenol 66%42-108%
4165-60-0 Nitrobenzene-d5 86%40-105%
321-60-8 2-Fluorobiphenyl 79%43-107%
1718-51-0 Terphenyl-d14 90%45-119%
43 of 79
FC80166.1.2
Blank Spike Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94245-BS a 6F16813.D 1 11/28/22 KA 11/28/22 OP94245 S6F630
The QC reported here applies to the following samples:Method: EPA 625.1
FC801-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 29.9 30 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 43.5 87 54-103
95-57-8 2-Chlorophenol 50 40.6 81 52-98
120-83-2 2,4-Dichlorophenol 50 42.9 86 53-103
105-67-9 2,4-Dimethylphenol 50 37.4 75 43-90
51-28-5 2,4-Dinitrophenol 100 94.9 95 44-112
534-52-1 4,6-Dinitro-o-cresol 100 102 102 66-121
95-48-7 2-Methylphenol 50 36.0 72 43-90
3&4-Methylphenol 100 67.0 67 36-88
88-75-5 2-Nitrophenol 50 55.3 111*53-102
100-02-7 4-Nitrophenol 100 36.8 37 18-62
87-86-5 Pentachlorophenol 100 76.5 77 61-115
108-95-2 Phenol 50 21.4 43 19-56
88-06-2 2,4,6-Trichlorophenol 50 44.7 89 59-107
83-32-9 Acenaphthene 50 44.2 88 61-107
208-96-8 Acenaphthylene 50 48.2 96 60-104
120-12-7 Anthracene 50 46.3 93 65-108
56-55-3 Benzo(a)anthracene 50 46.5 93 66-111
50-32-8 Benzo(a)pyrene 50 45.7 91 62-107
205-99-2 Benzo(b)fluoranthene 50 45.9 92 65-114
191-24-2 Benzo(g,h,i)perylene 50 49.1 98 66-116
207-08-9 Benzo(k)fluoranthene 50 50.3 101 65-114
101-55-3 4-Bromophenyl Phenyl Ether 50 43.0 86 65-109
85-68-7 Butyl Benzyl Phthalate 50 57.1 114*65-112
106-47-8 4-Chloroaniline 50 40.9 82 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 50.3 101 51-102
111-44-4 bis(2-Chloroethyl)ether 50 50.3 101*53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 56.9 114*45-106
91-58-7 2-Chloronaphthalene 50 44.0 88 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 42.7 85 62-105
218-01-9 Chrysene 50 48.5 97 66-111
53-70-3 Dibenzo(a,h)anthracene 50 45.3 91 66-119
132-64-9 Dibenzofuran 50 43.7 87 61-106
91-94-1 3,3'-Dichlorobenzidine 50 45.9 92 46-117
84-66-2 Diethyl Phthalate 50 48.3 97 64-108
131-11-3 Dimethyl Phthalate 50 46.2 92 63-106
* = Outside of Control Limits.
44 of 79
FC80166.2.1
Blank Spike Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94245-BS a 6F16813.D 1 11/28/22 KA 11/28/22 OP94245 S6F630
The QC reported here applies to the following samples:Method: EPA 625.1
FC801-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
84-74-2 Di-n-butyl Phthalate 50 52.9 106 65-107
117-84-0 Di-n-octyl Phthalate 50 61.2 122*62-118
121-14-2 2,4-Dinitrotoluene 50 53.6 107 61-110
606-20-2 2,6-Dinitrotoluene 50 49.4 99 63-108
117-81-7 bis(2-Ethylhexyl)phthalate 50 57.3 115 61-117
206-44-0 Fluoranthene 50 44.2 88 63-106
86-73-7 Fluorene 50 46.4 93 62-108
118-74-1 Hexachlorobenzene 50 38.5 77 63-108
87-68-3 Hexachlorobutadiene 50 37.9 76 42-102
77-47-4 Hexachlorocyclopentadiene 50 39.2 78 39-102
67-72-1 Hexachloroethane 50 44.1 88 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 45.2 90 64-119
78-59-1 Isophorone 50 48.7 97*43-87
90-12-0 1-Methylnaphthalene 50 46.0 92 53-102
91-57-6 2-Methylnaphthalene 50 45.3 91 51-102
91-20-3 Naphthalene 50 44.8 90 47-100
98-95-3 Nitrobenzene 50 50.7 101 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 50.2 100 52-104
86-30-6 N-Nitrosodiphenylamine 50 44.6 89 64-108
85-01-8 Phenanthrene 50 46.8 94 66-110
129-00-0 Pyrene 50 50.1 100 64-113
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 44%14-67%
4165-62-2 Phenol-d5 33%10-50%
118-79-6 2,4,6-Tribromophenol 68%33-118%
4165-60-0 Nitrobenzene-d5 93%42-108%
321-60-8 2-Fluorobiphenyl 80%40-106%
1718-51-0 Terphenyl-d14 86%39-121%
(a) Insufficient sample for MS/MSD.
* = Outside of Control Limits.
45 of 79
FC80166.2.1
Blank Spike Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-BS 6F16816.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 2820 85 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1470 88 52-108
95-57-8 2-Chlorophenol 1670 1320 79 48-104
120-83-2 2,4-Dichlorophenol 1670 1370 82 51-105
105-67-9 2,4-Dimethylphenol 1670 1200 72 43-96
51-28-5 2,4-Dinitrophenol 3330 3090 93 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3320 100 64-121
95-48-7 2-Methylphenol 1670 1340 80 46-107
3&4-Methylphenol 3330 2820 85 44-111
88-75-5 2-Nitrophenol 1670 1610 97 49-104
100-02-7 4-Nitrophenol 3330 2770 83 56-116
87-86-5 Pentachlorophenol 3330 2470 74 61-114
108-95-2 Phenol 1670 1540 92 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1420 85 56-109
83-32-9 Acenaphthene 1670 1330 80 56-109
208-96-8 Acenaphthylene 1670 1460 88 56-106
120-12-7 Anthracene 1670 1450 87 61-110
56-55-3 Benzo(a)anthracene 1670 1480 89 66-111
50-32-8 Benzo(a)pyrene 1670 1430 86 59-104
205-99-2 Benzo(b)fluoranthene 1670 1450 87 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1560 94 67-113
207-08-9 Benzo(k)fluoranthene 1670 1590 95 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1350 81 62-110
85-68-7 Butyl benzyl phthalate 1670 1790 107 65-113
106-47-8 4-Chloroaniline 1670 1130 68 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1430 86 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1340 80 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 1510 91 40-110
91-58-7 2-Chloronaphthalene 1670 1310 79 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1300 78 58-106
218-01-9 Chrysene 1670 1510 91 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1520 91 68-115
132-64-9 Dibenzofuran 1670 1310 79 57-108
91-94-1 3,3'-Dichlorobenzidine 1670 1190 71 36-114
84-66-2 Diethyl Phthalate 1670 1460 88 61-109
131-11-3 Dimethyl Phthalate 1670 1420 85 59-108
* = Outside of Control Limits.
46 of 79
FC80166.2.2
Blank Spike Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-BS 6F16816.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1920 115 64-119
84-74-2 Di-n-butyl Phthalate 1670 1660 100 63-108
121-14-2 2,4-Dinitrotoluene 1670 1640 98 59-109
606-20-2 2,6-Dinitrotoluene 1670 1510 91 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1790 107 64-115
206-44-0 Fluoranthene 1670 1390 83 60-108
86-73-7 Fluorene 1670 1420 85 58-109
118-74-1 Hexachlorobenzene 1670 1190 71 59-111
87-68-3 Hexachlorobutadiene 1670 1060 64 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1140 68 49-110
67-72-1 Hexachloroethane 1670 1180 71 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1440 86 66-116
78-59-1 Isophorone 1670 1400 84 42-89
90-12-0 1-Methylnaphthalene 1670 1320 79 49-106
91-57-6 2-Methylnaphthalene 1670 1280 77 47-106
91-20-3 Naphthalene 1670 1270 76 44-104
98-95-3 Nitrobenzene 1670 1420 85 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1350 81 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1410 85 62-110
85-01-8 Phenanthrene 1670 1460 88 63-111
129-00-0 Pyrene 1670 1580 95 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 70%40-102%
4165-62-2 Phenol-d5 79%41-100%
118-79-6 2,4,6-Tribromophenol 64%42-108%
4165-60-0 Nitrobenzene-d5 76%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 78%45-119%
* = Outside of Control Limits.
47 of 79
FC80166.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-MS 6F16823.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
OP94242-MSD 6F16824.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
FC819-3 6F16821.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
FC819-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 3830 3020 79 3810 2870 75 5 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 1910 1620 85 1910 1500 79 8 52-108/21
95-57-8 2-Chlorophenol ND 1910 1510 79 1910 1380 72 9 48-104/26
120-83-2 2,4-Dichlorophenol ND 1910 1530 80 1910 1400 73 9 51-105/27
105-67-9 2,4-Dimethylphenol ND 1910 1340 70 1910 1240 65 8 43-96/23
51-28-5 2,4-Dinitrophenol ND 3830 3440 90 3810 3250 85 6 40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 3830 3690 96 3810 3470 91 6 64-121/29
95-48-7 2-Methylphenol ND 1910 1530 80 1910 1400 73 9 46-107/24
3&4-Methylphenol ND 3830 3130 82 3810 2900 76 8 44-111/24
88-75-5 2-Nitrophenol ND 1910 1860 97 1910 1680 88 10 49-104/27
100-02-7 4-Nitrophenol ND 3830 3080 80 3810 2860 75 7 56-116/23
87-86-5 Pentachlorophenol ND 3830 2750 72 3810 2550 67 8 61-114/23
108-95-2 Phenol ND 1910 1740 91 1910 1590 83 9 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 1910 1640 86 1910 1470 77 11 56-109/25
83-32-9 Acenaphthene ND 1910 1520 79 1910 1390 73 9 56-109/23
208-96-8 Acenaphthylene ND 1910 1680 88 1910 1510 79 11 56-106/23
120-12-7 Anthracene ND 1910 1590 83 1910 1460 77 9 61-110/21
56-55-3 Benzo(a)anthracene ND 1910 1620 85 1910 1490 78 8 66-111/23
50-32-8 Benzo(a)pyrene ND 1910 1580 83 1910 1450 76 9 59-104/23
205-99-2 Benzo(b)fluoranthene ND 1910 1590 83 1910 1470 77 8 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1910 1780 93 1910 1600 84 11 67-113/21
207-08-9 Benzo(k)fluoranthene ND 1910 1690 88 1910 1550 81 9 67-114/22
101-55-3 4-Bromophenyl phenyl ether ND 1910 1500 78 1910 1350 71 11 62-110/21
85-68-7 Butyl benzyl phthalate ND 1910 1980 103 1910 1840 96 7 65-113/20
106-47-8 4-Chloroaniline ND 1910 1200 63 1910 1160 61 3 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1910 1640 86 1910 1500 79 9 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1910 1560 82 1910 1420 74 9 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1910 1760 92 1910 1590 83 10 40-110/25
91-58-7 2-Chloronaphthalene ND 1910 1540 80 1910 1390 73 10 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 1910 1480 77 1910 1320 69 11 58-106/21
218-01-9 Chrysene ND 1910 1670 87 1910 1520 80 9 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1910 1700 89 1910 1540 81 10 68-115/23
132-64-9 Dibenzofuran ND 1910 1500 78 1910 1380 72 8 57-108/22
91-94-1 3,3'-Dichlorobenzidine ND 1910 1370 72 1910 1350 71 1 36-114/28
84-66-2 Diethyl Phthalate ND 1910 1630 85 1910 1500 79 8 61-109/20
131-11-3 Dimethyl Phthalate ND 1910 1580 83 1910 1440 76 9 59-108/20
* = Outside of Control Limits.
48 of 79
FC80166.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94242-MS 6F16823.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
OP94242-MSD 6F16824.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
FC819-3 6F16821.D 1 11/28/22 KA 11/28/22 OP94242 S6F630
The QC reported here applies to the following samples:Method: SW846 8270E
FC801-2
FC819-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
117-84-0 Di-n-octyl Phthalate ND 1910 2110 110 1910 1980 104 6 64-119/21
84-74-2 Di-n-butyl Phthalate ND 1910 1820 95 1910 1670 88 9 63-108/19
121-14-2 2,4-Dinitrotoluene ND 1910 1800 94 1910 1640 86 9 59-109/20
606-20-2 2,6-Dinitrotoluene ND 1910 1700 89 1910 1520 80 11 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 1910 1990 104 1910 1870 98 6 64-115/23
206-44-0 Fluoranthene ND 1910 1520 79 1910 1390 73 9 60-108/25
86-73-7 Fluorene ND 1910 1620 85 1910 1450 76 11 58-109/21
118-74-1 Hexachlorobenzene ND 1910 1330 70 1910 1200 63 10 59-111/21
87-68-3 Hexachlorobutadiene ND 1910 1230 64 1910 1110 58 10 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1910 1340 70 1910 1200 63 11 49-110/31
67-72-1 Hexachloroethane ND 1910 1410 74 1910 1270 67 10 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1910 1620 85 1910 1480 78 9 66-116/22
78-59-1 Isophorone ND 1910 1590 83 1910 1450 76 9 42-89/22
90-12-0 1-Methylnaphthalene ND 1910 1500 78 1910 1370 72 9 49-106/26
91-57-6 2-Methylnaphthalene ND 1910 1490 78 1910 1370 72 8 47-106/27
91-20-3 Naphthalene ND 1910 1470 77 1910 1340 70 9 44-104/27
98-95-3 Nitrobenzene ND 1910 1620 85 1910 1480 78 9 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1910 1550 81 1910 1420 74 9 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1910 1580 83 1910 1430 75 10 62-110/21
85-01-8 Phenanthrene ND 1910 1630 85 1910 1490 78 9 63-111/22
129-00-0 Pyrene ND 1910 1760 92 1910 1620 85 8 65-115/25
CAS No.Surrogate Recoveries MS MSD FC819-3 Limits
367-12-4 2-Fluorophenol 72%67%79%40-102%
4165-62-2 Phenol-d5 79%74%86%41-100%
118-79-6 2,4,6-Tribromophenol 63%59%65%42-108%
4165-60-0 Nitrobenzene-d5 78%72%84%40-105%
321-60-8 2-Fluorobiphenyl 73%67%76%43-107%
1718-51-0 Terphenyl-d14 77%73%83%45-119%
* = Outside of Control Limits.
49 of 79
FC80166.3.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
50 of 79
FC8017
Method Blank Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94349-MB CC086691.D 1 12/06/22 AF 12/02/22 OP94349 GCC2241
The QC reported here applies to the following samples:Method: EPA 504.1
FC801-3
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 110%63-137%
51 of 79
FC80177.1.1
Blank Spike Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94349-BS CC086692.D 1 12/07/22 AF 12/02/22 OP94349 GCC2241
The QC reported here applies to the following samples:Method: EPA 504.1
FC801-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 102%63-137%
* = Outside of Control Limits.
52 of 79
FC80177.2.1
Duplicate Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94349-DUP CC086693.D 1 12/07/22 AF 12/02/22 OP94349 GCC2241
FC801-3 a CC086694.D 1 12/07/22 AF 12/02/22 OP94349 GCC2241
The QC reported here applies to the following samples:Method: EPA 504.1
FC801-3
FC801-3 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
CAS No.Surrogate Recoveries DUP FC801-3 Limits
460-00-4 4-Bromofluorobenzene 76%81%63-137%
(a) Sample reanalyzed beyond hold time.
* = Outside of Control Limits.
53 of 79
FC80177.3.1
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 8
54 of 79
FC8018
Method Blank Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94241-MB NN040684.D 1 12/01/22 AF 11/28/22 OP94241 GNN1875
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-2
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 4000 ug/kg
C9-C18 Aliphatics ND 10000 2500 ug/kg
C19-C36 Aliphatics ND 10000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 64%40-140%
580-13-2 2-Bromonaphthalene 131%40-140%
84-15-1 o-Terphenyl 96%40-140%
321-60-8 2-Fluorobiphenyl 126%40-140%
55 of 79
FC80188.1.1
Method Blank Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94268-MB NN040661.D 1 11/29/22 AF 11/29/22 OP94268 GNN1873
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-3
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics 50.1 200 50 ug/l J
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 78%40-140%
580-13-2 2-Bromonaphthalene 127%40-140%
84-15-1 o-Terphenyl 97%40-140%
321-60-8 2-Fluorobiphenyl 123%40-140%
56 of 79
FC80188.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94241-BS NN040652.D 1 11/29/22 AF 11/28/22 OP94241 GNN1873
OP94241-BSD NN040653.D 1 11/29/22 AF 11/28/22 OP94241 GNN1873
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-2
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 4830 97 3670 73 27 40-140/30
208-96-8 Acenaphthylene 5000 4220 84 3280 66 25 40-140/30
120-12-7 Anthracene 5000 4970 99 3770 75 27 40-140/30
56-55-3 Benzo(a)anthracene 5000 5820 116 4390 88 28 40-140/30
50-32-8 Benzo(a)pyrene 5000 5510 110 4210 84 27 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 5390 108 4070 81 28 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 5080 102 3840 77 28 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 5090 102 3840 77 28 40-140/30
218-01-9 Chrysene 5000 5470 109 4110 82 28 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 5500 110 4150 83 28 40-140/30
206-44-0 Fluoranthene 5000 5240 105 3940 79 28 40-140/30
86-73-7 Fluorene 5000 4860 97 3670 73 28 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 5040 101 3830 77 27 40-140/30
91-57-6 2-Methylnaphthalene 5000 4380 88 3310 66 28 40-140/30
91-20-3 Naphthalene 5000 4030 81 3070 61 27 40-140/30
85-01-8 Phenanthrene 5000 4970 99 3740 75 28 40-140/30
129-00-0 Pyrene 5000 5450 109 4110 82 28 40-140/30
C11-C22 Aromatics (Unadj.)85000 89500 105 67900 80 27 40-140/30
C9-C18 Aliphatics 30000 20000 67 19100 64 5 40-140/30
C19-C36 Aliphatics 40000 33900 85 33100 83 2 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 74%71%40-140%
580-13-2 2-Bromonaphthalene 100%81%40-140%
84-15-1 o-Terphenyl 91%69%40-140%
321-60-8 2-Fluorobiphenyl 97%79%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP94241-BS 2-Methylnaphthalene 4380 ND 0.0%5.0
OP94241-BS Naphthalene 4030 ND 0.0%5.0
OP94241-BSD 2-Methylnaphthalene 3310 ND 0.0%5.0
OP94241-BSD Naphthalene 3070 ND 0.0%5.0
* = Outside of Control Limits.
57 of 79
FC80188.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94268-BS a NN040662.D 1 11/29/22 AF 11/29/22 OP94268 GNN1873
OP94268-BSD NN040663.D 1 11/29/22 AF 11/29/22 OP94268 GNN1873
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
83-32-9 Acenaphthene 100 59.9 60 96.3 96 47*40-140/30
208-96-8 Acenaphthylene 100 53.2 53 85.6 86 47*40-140/30
120-12-7 Anthracene 100 64.8 65 101 101 44*40-140/30
56-55-3 Benzo(a)anthracene 100 76.6 77 118 118 43*40-140/30
50-32-8 Benzo(a)pyrene 100 73.0 73 112 112 42*40-140/30
205-99-2 Benzo(b)fluoranthene 100 70.7 71 109 109 43*40-140/30
191-24-2 Benzo(g,h,i)perylene 100 66.5 67 103 103 43*40-140/30
207-08-9 Benzo(k)fluoranthene 100 67.0 67 103 103 42*40-140/30
218-01-9 Chrysene 100 72.0 72 111 111 43*40-140/30
53-70-3 Dibenzo(a,h)anthracene 100 71.7 72 111 111 43*40-140/30
206-44-0 Fluoranthene 100 69.0 69 106 106 42*40-140/30
86-73-7 Fluorene 100 61.0 61 97.0 97 46*40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 100 66.1 66 102 102 43*40-140/30
91-57-6 2-Methylnaphthalene 100 52.1 52 85.3 85 48*40-140/30
91-20-3 Naphthalene 100 47.5 48 77.2 77 48*40-140/30
85-01-8 Phenanthrene 100 64.3 64 100 100 43*40-140/30
129-00-0 Pyrene 100 71.7 72 111 111 43*40-140/30
C11-C22 Aromatics (Unadj.)1700 1160 68 1800 106 43*40-140/30
C9-C18 Aliphatics 600 340 57 376 63 10 40-140/30
C19-C36 Aliphatics 800 668 84 704 88 5 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 75%80%40-140%
580-13-2 2-Bromonaphthalene 69%104%40-140%
84-15-1 o-Terphenyl 63%98%40-140%
321-60-8 2-Fluorobiphenyl 66%100%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP94268-BS 2-Methylnaphthalene 52.1 ND 0.0%5.0
OP94268-BS Naphthalene 47.5 ND 0.0%5.0
OP94268-BSD 2-Methylnaphthalene 85.3 ND 0.0%5.0
OP94268-BSD Naphthalene 77.2 ND 0.0%5.0
* = Outside of Control Limits.
58 of 79
FC80188.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94268-BS a NN040662.D 1 11/29/22 AF 11/29/22 OP94268 GNN1873
OP94268-BSD NN040663.D 1 11/29/22 AF 11/29/22 OP94268 GNN1873
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-3
(a) Insufficient sample for batch duplicate.
* = Outside of Control Limits.
59 of 79
FC80188.2.2
Duplicate Summary Page 1 of 1
Job Number:FC801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP94241-DUP NN040654.D 1 11/29/22 AF 11/28/22 OP94241 GNN1873
FC761-1 NN040655.D 1 11/29/22 AF 11/28/22 OP94241 GNN1873
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC801-2
FC761-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 a
208-96-8 Acenaphthylene ND ND nc 30 a
120-12-7 Anthracene ND ND nc 30 a
56-55-3 Benzo(a)anthracene ND ND nc 30 a
50-32-8 Benzo(a)pyrene ND ND nc 30 a
205-99-2 Benzo(b)fluoranthene ND ND nc 30 a
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a
207-08-9 Benzo(k)fluoranthene ND ND nc 30 a
218-01-9 Chrysene ND ND nc 30 a
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a
206-44-0 Fluoranthene ND ND nc 30 a
86-73-7 Fluorene ND ND nc 30 a
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a
91-57-6 2-Methylnaphthalene ND ND nc 30 a
91-20-3 Naphthalene ND ND nc 30 a
85-01-8 Phenanthrene ND ND nc 30 a
129-00-0 Pyrene ND ND nc 30 a
C11-C22 Aromatics (Unadj.)5010 J ND 200*30 a
C9-C18 Aliphatics ND ND nc 30 a
C19-C36 Aliphatics ND ND nc 30 a
CAS No.Surrogate Recoveries DUP FC761-1 Limits
3386-33-2 1-Chlorooctadecane 69%74%40-140%
580-13-2 2-Bromonaphthalene 95%100%40-140%
84-15-1 o-Terphenyl 83%87%40-140%
321-60-8 2-Fluorobiphenyl 93%98%40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
60 of 79
FC80188.3.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 9
61 of 79
FC8019
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22
MB
Metal RL IDL MDL raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3
Barium 200 .5 1
Beryllium 4.0 .1 .2
Boron 100 5 10
Cadmium 5.0 .1 .2
Calcium 1000 50 50
Chromium 10 .5 1
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 15 17
Lead 5.0 1 1.1 -0.50 <5.0
Magnesium 5000 35 35
Manganese 15 .25 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 100 200
Selenium 10 2 2.9
Silver 10 .5 .7
Sodium 10000 250 500
Strontium 10 .25 .5
Thallium 10 1 1.4
Tin 50 .5 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
62 of 79
FC80199.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22 12/02/22
FC719-9F QC FC719-9F Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic
Barium anr
Beryllium
Boron
Cadmium
Calcium anr
Chromium
Cobalt
Copper
Iron anr
Lead 0.0 0.0 NC 0-20 0.0 470 500 94.0 80-120
Magnesium anr
Manganese anr
Molybdenum
Nickel
Potassium anr
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
63 of 79
FC80199.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22
FC719-9F Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium anr
Beryllium
Boron
Cadmium
Calcium anr
Chromium
Cobalt
Copper
Iron anr
Lead 0.0 469 500 93.8 0.2 20
Magnesium anr
Manganese anr
Molybdenum
Nickel
Potassium anr
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
64 of 79
FC80199.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic
Barium anr
Beryllium
Boron
Cadmium
Calcium anr
Chromium
Cobalt
Copper
Iron anr
Lead 475 500 95.0 80-120
Magnesium anr
Manganese anr
Molybdenum
Nickel
Potassium anr
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
65 of 79
FC80199.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22
FC719-9F QC
Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium anr
Beryllium
Boron
Cadmium
Calcium anr
Chromium
Cobalt
Copper
Iron anr
Lead 0.00 0.00 NC 0-10
Magnesium anr
Manganese anr
Molybdenum
Nickel
Potassium anr
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
66 of 79
FC80199.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FC801
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41544 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 12/02/22
Sample Final FC719-9F PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 9.8 10 42 0.2 2.5 50 84.0 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41544: FC801-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
67 of 79
FC80199.1.5
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Scott, LA)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 10
68 of 79
FC80110
FC801-1 HCL
Bot tfl
1fl]ililililuililililiiltiililuill]iltiiltifli
CHAIN OF CUSTODY
SGS North America lnc. - Orlando
4()5 Vlnoland Road, Sulte C.15 Orlando, F132811
TEL. 40742S6700 Frtxt 1O7{.2$O7O7
Page'l ol 2FC801-1
Bot# 1
VR-3
FC801-2
Bot# 3
R-33
I\Iat.ix Codes
LAB USE ONL'
SO Sor
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VR-3
lnlormatlon
R-33 e Race 1 7824 Seven Ci,cle Rd \akrna NC
APPT.EC By (sos Plrll / D.r.
FC801
FC801-2
Bot #o
MeOH
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Orlando FL
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& Rlsn T/A data availabe vra Labmk
Sam lo Custo must bs documentod bolow each lamo !am
R.rriqui.h.d by s.mFl.r:
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C Enl Pu.chase Order I
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11t21t22 227 00PM JB 2 XMW-1 (5)
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CommorcE|A = R€suts on,
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FC801: Chain of Custody
Page 1 of 4
SGS Scott, LA
69 of 79
FC8011010.1
oRIGIN tD:oFLh [phone]SANPLE RECEIVINGSGS NORTH EIERICA INC4405 VTNELANO ROADSTE 15ORLANDO, FL 32811UNITEO STATES U6
SHIP DATE: 28NOV22ACTL]6T; 7.OO LB IIANcAo: o3ss7s9/cAFE36l6
BILL SENDER
3E
IO SAMPLE RECEIVING
SGS NORTH AMERICA INC.
109 COMM]SSION BLYD
LAFAYETTE LA 70508
(807) 23r-a775
ilrilil]ilffir1ililllll[Ir[]IliltIIIlill[FedExErp
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FC801: Chain of Custody
Page 2 of 4
70 of 79
FC8011010.1
Job Number:FC801 Client:SGS FL
Date / Time Received:11/29/2022 9:30:00 AM Delivery Method:
Project:SGS
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR001;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (5.6/5.6);
SGS Sample Receipt Summary
FC801: Chain of Custody
Page 3 of 4
71 of 79
FC8011010.1
Page 2 of 2
Problem Resolution
CSR:Response Date:
Response:
Job Number:FC801
FC801: Chain of Custody
Page 4 of 4
72 of 79
FC8011010.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
(SGS Scott, LA)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 11
73 of 79
FC80111
Method Blank Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2324-MB1 LE039449.D 1 11/30/22 MB n/a n/a GLE2324
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene 0.26 5.0 0.17 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 1.8 5.0 0.41 ug/l J
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene 0.98 10 0.40 ug/l J
95-47-6 o-Xylene 0.53 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 105%70-130%
615-59-8 2,5-Dibromotoluene 106%70-130%
74 of 79
FC8011111.1.1
Method Blank Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2325-MB1 LE039485.D 1 12/02/22 MB n/a n/a GLE2325
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 250 6.9 ug/kg
100-41-4 Ethylbenzene ND 250 7.2 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 250 7.1 ug/kg
91-20-3 Naphthalene 72.6 250 18 ug/kg J
108-88-3 Toluene ND 250 6.3 ug/kg
m,p-Xylene 35.0 500 18 ug/kg J
95-47-6 o-Xylene ND 250 8.3 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C10 Aromatics (Unadj.)ND 5000 2500 ug/kg
C5- C8 Aliphatics ND 5000 2500 ug/kg
C9- C12 Aliphatics ND 5000 2500 ug/kg
C9- C10 Aromatics ND 5000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 114%70-130%
615-59-8 2,5-Dibromotoluene 98%70-130%
75 of 79
FC8011111.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2324-BS1 LE039447.D 1 11/30/22 MB n/a n/a GLE2324
GLE2324-BSD1 LE039448.D 1 11/30/22 MB n/a n/a GLE2324
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 40 43.3 108 42.8 107 1 70-130/25
100-41-4 Ethylbenzene 40 41.5 104 41.2 103 1 70-130/25
1634-04-4 Methyl Tert Butyl Ether 40 43.1 108 42.5 106 1 70-130/25
91-20-3 Naphthalene 40 42.3 106 41.3 103 2 70-130/25
108-88-3 Toluene 40 41.9 105 41.6 104 1 70-130/25
m,p-Xylene 80 85.9 107 85.1 106 1 70-130/25
95-47-6 o-Xylene 40 42.8 107 42.3 106 1 70-130/25
C5- C8 Aliphatics (Unadj.)120 135 112 133 111 1 70-130/25
C9- C12 Aliphatics (Unadj.)120 122 102 118 98 3 70-130/25
C9- C10 Aromatics (Unadj.)40 42.3 106 41.8 105 1 70-130/25
C5- C8 Aliphatics 232 228 2 70-130/25
C9- C12 Aliphatics 253 248 2 70-130/25
C9- C10 Aromatics 40 42.3 106 41.8 105 1 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 110%109%70-130%
615-59-8 2,5-Dibromotoluene 112%112%70-130%
* = Outside of Control Limits.
76 of 79
FC8011111.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2325-BS1 LE039483.D 1 12/02/22 MB n/a n/a GLE2325
GLE2325-BSD1 LE039484.D 1 12/02/22 MB n/a n/a GLE2325
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-2
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 2000 1810 91 1840 92 2 70-130/25
100-41-4 Ethylbenzene 2000 1930 97 1950 98 1 70-130/25
1634-04-4 Methyl Tert Butyl Ether 2000 1860 93 1870 94 1 70-130/25
91-20-3 Naphthalene 2000 2050 103 2010 101 2 70-130/25
108-88-3 Toluene 2000 1880 94 1900 95 1 70-130/25
m,p-Xylene 4000 3880 97 3920 98 1 70-130/25
95-47-6 o-Xylene 2000 1930 97 1960 98 2 70-130/25
C5- C8 Aliphatics (Unadj.)6000 6260 104 6220 104 1 70-130/25
C9- C12 Aliphatics (Unadj.)6000 6430 107 6290 105 2 70-130/25
C9- C10 Aromatics (Unadj.)2000 1910 96 1940 97 2 70-130/25
C5- C8 Aliphatics 11000 10800 2 70-130/25
C9- C12 Aliphatics 14100 14000 1 70-130/25
C9- C10 Aromatics 2000 1910 96 1940 97 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 115%115%70-130%
615-59-8 2,5-Dibromotoluene 100%99%70-130%
* = Outside of Control Limits.
77 of 79
FC8011111.2.2
Duplicate Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC681-1DUP LE039451.D 500 11/30/22 MB n/a n/a GLE2324
FC681-1 LE039450.D 500 11/30/22 MB n/a n/a GLE2324
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-3
FC681-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 10800 10900 1 50
100-41-4 Ethylbenzene 2000 J 1990 J 1 50
1634-04-4 Methyl Tert Butyl Ether 86800 90300 4 50
91-20-3 Naphthalene 1180 J 1110 J 6 50
108-88-3 Toluene 3640 3710 2 50
m,p-Xylene 7960 7930 0 50
95-47-6 o-Xylene 3200 3110 3 50
C5- C8 Aliphatics (Unadj.)109000 111000 2 50
C9- C12 Aliphatics (Unadj.)39500 J 38700 J 2 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FC681-1 Limits
615-59-8 2,5-Dibromotoluene 112%103%70-130%
615-59-8 2,5-Dibromotoluene 114%105%70-130%
* = Outside of Control Limits.
78 of 79
FC8011111.3.1
Duplicate Summary Page 1 of 1
Job Number:FC801
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC691-1DUP LE039487.D 1 12/02/22 MB n/a n/a GLE2325
FC691-1 LE039486.D 1 12/02/22 MB n/a n/a GLE2325
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC801-2
FC691-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FC691-1 Limits
615-59-8 2,5-Dibromotoluene 52%* a 56%* a 70-130%
615-59-8 2,5-Dibromotoluene 43%* a 47%* a 70-130%
(a) Outside control limits due to matrix interference. Confirmed by duplicate analysis.
* = Outside of Control Limits.
79 of 79
FC8011111.3.2
02/09/23
Technical Report for
GRI (Geological Resources Inc.)
Home Race 1; 7824 Seven Circle Rd, Nakina, NC
5836
SGS Job Number: FC2288
Sampling Date: 01/30/23
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Ethan Rogerson
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 02/09/23
e-Hardcopy 2.0
Automated Report
54
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1 of 54
FC2288
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FC2288-1: TRIP BLANK .............................................................................................6
3.2: FC2288-2: WSW-5 .......................................................................................................7
3.3: FC2288-3: WSW-6 .......................................................................................................14
Section 4: Misc. Forms ............................................................................................................21
4.1: Chain of Custody ...........................................................................................................22
Section 5: MS Volatiles - QC Data Summaries .....................................................................24
5.1: Method Blank Summary ................................................................................................25
5.2: Blank Spike Summary ...................................................................................................26
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................27
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................28
6.1: Method Blank Summary ................................................................................................29
6.2: Blank Spike Summary ...................................................................................................31
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................33
Section 7: GC/LC Semi-volatiles - QC Data Summaries .....................................................35
7.1: Method Blank Summary ................................................................................................36
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................38
7.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................39
Section 8: Metals Analysis - QC Data Summaries ................................................................40
8.1: Prep QC MP41783: Pb ..................................................................................................41
Section 9: Misc. Forms (SGS Scott, LA) ................................................................................47
9.1: Chain of Custody ...........................................................................................................48
Section 10: GC Volatiles - QC Data (SGS Scott, LA) ...........................................................51
10.1: Method Blank Summary ..............................................................................................52
10.2: Blank Spike/Blank Spike Duplicate Summary ............................................................53
10.3: Duplicate Summary .....................................................................................................54 123456789102 of 54
FC2288
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FC2288
Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Project No: 5836
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FC2288-1 01/30/23 08:59 JB 01/31/23 AQ Trip Blank Water TRIP BLANK
FC2288-2 01/30/23 09:27 JB 01/31/23 AQ Ground Water WSW-5
FC2288-3 01/30/23 09:56 JB 01/31/23 AQ Ground Water WSW-6
3 of 54
FC22881
Summary of Hits Page 1 of 1
Job Number:FC2288
Account:GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Collected:01/30/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC2288-1 TRIP BLANK
No hits reported in this sample.
FC2288-2 WSW-5
Ethylbenzene a 0.21 J 5.0 0.17 ug/l MADEP VPH REV 2.1
Naphthalene a 1.2 J 5.0 0.41 ug/l MADEP VPH REV 2.1
m,p-Xylene a 0.68 J 10 0.40 ug/l MADEP VPH REV 2.1
o-Xylene a 0.38 J 5.0 0.18 ug/l MADEP VPH REV 2.1
FC2288-3 WSW-6
Naphthalene a 1.2 J 5.0 0.41 ug/l MADEP VPH REV 2.1
m,p-Xylene a 0.52 J 10 0.40 ug/l MADEP VPH REV 2.1
o-Xylene a 0.27 J 5.0 0.18 ug/l MADEP VPH REV 2.1
(a) Analysis performed at SGS Scott, LA.
4 of 54
FC22882
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 54
FC22883
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TRIP BLANK
Lab Sample ID:FC2288-1 Date Sampled:01/30/23
Matrix:AQ - Trip Blank Water Date Received:01/31/23
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E111132.D 1 02/01/23 12:56 TD n/a n/a VE2648
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 110%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 54
FC228833.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E111133.D 1 02/01/23 13:19 TD n/a n/a VE2648
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 110%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X086144.D 1 02/03/23 12:21 KA 02/03/23 05:30 OP95288 SX3414
Run #2
Initial Volume Final Volume
Run #1 1000 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene a ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene a ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane a ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate a ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
84-74-2 Di-n-butyl Phthalate a ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate b ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone a ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene a ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 28%14-67%
4165-62-2 Phenol-d5 17%10-50%
118-79-6 2,4,6-Tribromophenol 64%33-118%
4165-60-0 Nitrobenzene-d5 77%42-108%
321-60-8 2-Fluorobiphenyl 72%40-106%
1718-51-0 Terphenyl-d14 81%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
(a) Associated BS outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
(b) Associated BS and CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE040441.D 1 02/07/23 23:00 ALA n/a n/a L:GLE2368
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene 0.21 5.0 0.17 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 1.2 5.0 0.41 ug/l J
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene 0.68 10 0.40 ug/l J
95-47-6 o-Xylene 0.38 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 112%70-130%
615-59-8 2,5-Dibromotoluene 113%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN041304.D 1 02/04/23 00:03 AF 02/01/23 07:55 OP95250 GNN1899
Run #2
Initial Volume Final Volume
Run #1 1000 ml 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 45%40-140%
580-13-2 2-Bromonaphthalene 82%40-140%
84-15-1 o-Terphenyl 70%40-140%
321-60-8 2-Fluorobiphenyl 79%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-5
Lab Sample ID:FC2288-2 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <5.0 5.0 ug/l 1 02/01/23 02/02/23 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA19195
(2) Prep QC Batch: MP41783
RL = Reporting Limit
13 of 54
FC228833.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:SM 6200B Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E111134.D 1 02/01/23 13:42 TD n/a n/a VE2648
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 110%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X086145.D 1 02/03/23 12:48 KA 02/03/23 05:30 OP95288 SX3414
Run #2
Initial Volume Final Volume
Run #1 1020 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 49 9.8 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.9 0.58 ug/l
95-57-8 2-Chlorophenol ND 4.9 0.62 ug/l
120-83-2 2,4-Dichlorophenol ND 4.9 0.82 ug/l
105-67-9 2,4-Dimethylphenol ND 4.9 0.72 ug/l
51-28-5 2,4-Dinitrophenol ND 25 4.9 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.8 2.0 ug/l
95-48-7 2-Methylphenol ND 4.9 0.55 ug/l
3&4-Methylphenol ND 4.9 0.96 ug/l
88-75-5 2-Nitrophenol ND 4.9 0.84 ug/l
100-02-7 4-Nitrophenol ND 25 4.9 ug/l
87-86-5 Pentachlorophenol ND 25 4.9 ug/l
108-95-2 Phenol ND 4.9 0.49 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.9 0.74 ug/l
83-32-9 Acenaphthene ND 4.9 0.61 ug/l
208-96-8 Acenaphthylene ND 4.9 0.63 ug/l
120-12-7 Anthracene ND 4.9 0.78 ug/l
56-55-3 Benzo(a)anthracene ND 4.9 0.75 ug/l
50-32-8 Benzo(a)pyrene a ND 4.9 0.77 ug/l
205-99-2 Benzo(b)fluoranthene a ND 4.9 0.76 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.9 0.81 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.9 0.84 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.9 0.83 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.9 0.98 ug/l
106-47-8 4-Chloroaniline ND 4.9 0.62 ug/l
111-91-1 bis(2-Chloroethoxy)methane a ND 4.9 0.79 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.9 0.72 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.9 0.74 ug/l
91-58-7 2-Chloronaphthalene ND 4.9 0.49 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.9 0.53 ug/l
218-01-9 Chrysene ND 4.9 0.83 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.9 0.79 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 4.9 0.59 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.9 0.63 ug/l
84-66-2 Diethyl Phthalate a ND 4.9 0.98 ug/l
131-11-3 Dimethyl Phthalate ND 4.9 0.98 ug/l
84-74-2 Di-n-butyl Phthalate a ND 4.9 0.98 ug/l
117-84-0 Di-n-octyl Phthalate b ND 4.9 0.98 ug/l
121-14-2 2,4-Dinitrotoluene ND 4.9 0.80 ug/l
606-20-2 2,6-Dinitrotoluene ND 4.9 0.70 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.9 0.98 ug/l
206-44-0 Fluoranthene ND 4.9 0.54 ug/l
86-73-7 Fluorene ND 4.9 0.69 ug/l
118-74-1 Hexachlorobenzene ND 4.9 0.68 ug/l
87-68-3 Hexachlorobutadiene ND 4.9 0.49 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.9 1.8 ug/l
67-72-1 Hexachloroethane ND 4.9 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.9 0.70 ug/l
78-59-1 Isophorone a ND 4.9 0.76 ug/l
90-12-0 1-Methylnaphthalene ND 4.9 0.51 ug/l
91-57-6 2-Methylnaphthalene ND 4.9 0.59 ug/l
91-20-3 Naphthalene ND 4.9 0.49 ug/l
98-95-3 Nitrobenzene a ND 4.9 0.91 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.9 0.66 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.9 0.79 ug/l
85-01-8 Phenanthrene ND 4.9 0.85 ug/l
129-00-0 Pyrene ND 4.9 0.67 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 23%14-67%
4165-62-2 Phenol-d5 14%10-50%
118-79-6 2,4,6-Tribromophenol 58%33-118%
4165-60-0 Nitrobenzene-d5 67%42-108%
321-60-8 2-Fluorobiphenyl 65%40-106%
1718-51-0 Terphenyl-d14 72%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
(a) Associated BS outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
(b) Associated BS and CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE040442.D 1 02/07/23 23:32 ALA n/a n/a L:GLE2368
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene ND 5.0 0.17 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 1.2 5.0 0.41 ug/l J
108-88-3 Toluene ND 5.0 0.15 ug/l
m,p-Xylene 0.52 10 0.40 ug/l J
95-47-6 o-Xylene 0.27 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 115%70-130%
615-59-8 2,5-Dibromotoluene 116%70-130%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN041305.D 1 02/04/23 00:32 AF 02/01/23 07:55 OP95250 GNN1899
Run #2
Initial Volume Final Volume
Run #1 1020 ml 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 3.9 2.0 ug/l
208-96-8 Acenaphthylene ND 3.9 2.0 ug/l
120-12-7 Anthracene ND 3.9 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 3.9 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 3.9 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 3.9 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 3.9 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 3.9 2.0 ug/l
218-01-9 Chrysene ND 3.9 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 3.9 2.0 ug/l
206-44-0 Fluoranthene ND 3.9 2.0 ug/l
86-73-7 Fluorene ND 3.9 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 3.9 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 3.9 2.0 ug/l
91-20-3 Naphthalene ND 3.9 2.0 ug/l
85-01-8 Phenanthrene ND 3.9 2.0 ug/l
129-00-0 Pyrene ND 3.9 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 78 ug/l
C9-C18 Aliphatics ND 200 49 ug/l
C19-C36 Aliphatics ND 200 49 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 44%40-140%
580-13-2 2-Bromonaphthalene 80%40-140%
84-15-1 o-Terphenyl 68%40-140%
321-60-8 2-Fluorobiphenyl 77%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 54
FC228833.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:WSW-6
Lab Sample ID:FC2288-3 Date Sampled:01/30/23
Matrix:AQ - Ground Water Date Received:01/31/23
Percent Solids:n/a
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <5.0 5.0 ug/l 1 02/01/23 02/02/23 LM SW846 6010D 1 SW846 3010A 2
(1) Instrument QC Batch: MA19195
(2) Prep QC Batch: MP41783
RL = Reporting Limit
20 of 54
FC228833.3
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
21 of 54
FC22884
FC2288: Chain of Custody
Page 1 of 2
22 of 54
FC228844.1
Job Number:FC2288 Client:GEOLOGICAL RESOURCES INC.
Date / Time Received:1/31/2023 10:30:00 AM Delivery Method:FEDEX
Project:HOME RACE MART #1
Airbill #'s:1009 6379 5641
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.6);
Cooler 1: (1.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:ZANEB Date:Date:1/31/2023 10:30:00 A
FC2288: Chain of Custody
Page 2 of 2
23 of 54
FC228844.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
24 of 54
FC22885
Method Blank Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2648-MB E111131.D 1 02/01/23 TD n/a n/a VE2648
The QC reported here applies to the following samples:Method: SM 6200B
FC2288-1, FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 108%70-130%
25 of 54
FC228855.1.1
Blank Spike Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2648-BS E111129.D 1 02/01/23 TD n/a n/a VE2648
The QC reported here applies to the following samples:Method: SM 6200B
FC2288-1, FC2288-2, FC2288-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.9 99 70-130
108-90-7 Chlorobenzene 10 9.2 92 70-130
95-50-1 1,2-Dichlorobenzene 10 8.9 89 70-130
541-73-1 1,3-Dichlorobenzene 10 9.1 91 70-130
106-46-7 1,4-Dichlorobenzene 10 8.7 87 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
100-41-4 Ethylbenzene 10 9.5 95 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.6 96 70-130
91-20-3 Naphthalene 10 9.2 92 70-130
108-88-3 Toluene 10 9.1 91 70-130
1330-20-7 Xylene (total)30 28.6 95 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
* = Outside of Control Limits.
26 of 54
FC228855.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FC2288-2MS E111135.D 1 02/01/23 TD n/a n/a VE2648
FC2288-2MSD E111136.D 1 02/01/23 TD n/a n/a VE2648
FC2288-2 E111133.D 1 02/01/23 TD n/a n/a VE2648
The QC reported here applies to the following samples:Method: SM 6200B
FC2288-1, FC2288-2, FC2288-3
FC2288-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.7 117 10 11.1 111 5 70-130/20
108-90-7 Chlorobenzene ND 10 10.5 105 10 10 100 5 70-130/20
95-50-1 1,2-Dichlorobenzene ND 10 9.8 98 10 9.6 96 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 10.2 102 10 9.7 97 5 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.7 97 10 9.4 94 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 12.2 122 10 11.9 119 2 70-130/20
100-41-4 Ethylbenzene ND 10 11.1 111 10 10.5 105 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.5 105 10 10.4 104 1 70-130/20
91-20-3 Naphthalene ND 10 9.7 97 10 9.8 98 1 70-130/20
108-88-3 Toluene ND 10 10.4 104 10 9.9 99 5 70-130/20
1330-20-7 Xylene (total)ND 30 33.3 111 30 31.6 105 5 70-130/20
CAS No.Surrogate Recoveries MS MSD FC2288-2 Limits
1868-53-7 Dibromofluoromethane 104%104%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%110%107%70-130%
2037-26-5 Toluene-D8 96%97%101%70-130%
460-00-4 4-Bromofluorobenzene 103%104%110%70-130%
* = Outside of Control Limits.
27 of 54
FC228855.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
28 of 54
FC22886
Method Blank Summary Page 1 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-MB X086143.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
29 of 54
FC228866.1.1
Method Blank Summary Page 2 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-MB X086143.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 32%14-67%
4165-62-2 Phenol-d5 20%10-50%
118-79-6 2,4,6-Tribromophenol 62%33-118%
4165-60-0 Nitrobenzene-d5 72%42-108%
321-60-8 2-Fluorobiphenyl 70%40-106%
1718-51-0 Terphenyl-d14 77%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
30 of 54
FC228866.1.1
Blank Spike Summary Page 1 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-BS X086142.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 36.5 37 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 46.5 93 54-103
95-57-8 2-Chlorophenol 50 38.4 77 52-98
120-83-2 2,4-Dichlorophenol 50 44.4 89 53-103
105-67-9 2,4-Dimethylphenol 50 36.0 72 43-90
51-28-5 2,4-Dinitrophenol 100 82.6 83 44-112
534-52-1 4,6-Dinitro-o-cresol 100 93.0 93 66-121
95-48-7 2-Methylphenol 50 33.0 66 43-90
3&4-Methylphenol 100 60.3 60 36-88
88-75-5 2-Nitrophenol 50 47.0 94 53-102
100-02-7 4-Nitrophenol 100 36.7 37 18-62
87-86-5 Pentachlorophenol 100 82.5 83 61-115
108-95-2 Phenol 50 18.6 37 19-56
88-06-2 2,4,6-Trichlorophenol 50 43.0 86 59-107
83-32-9 Acenaphthene 50 46.3 93 61-107
208-96-8 Acenaphthylene 50 52.0 104 60-104
120-12-7 Anthracene 50 46.3 93 65-108
56-55-3 Benzo(a)anthracene 50 48.1 96 66-111
50-32-8 Benzo(a)pyrene 50 54.8 110*62-107
205-99-2 Benzo(b)fluoranthene 50 59.3 119*65-114
191-24-2 Benzo(g,h,i)perylene 50 55.9 112 66-116
207-08-9 Benzo(k)fluoranthene 50 57.0 114 65-114
101-55-3 4-Bromophenyl Phenyl Ether 50 48.2 96 65-109
85-68-7 Butyl Benzyl Phthalate 50 56.2 112 65-112
106-47-8 4-Chloroaniline 50 45.3 91 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 53.5 107*51-102
111-44-4 bis(2-Chloroethyl)ether 50 48.8 98 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 51.8 104 45-106
91-58-7 2-Chloronaphthalene 50 47.1 94 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 44.7 89 62-105
218-01-9 Chrysene 50 49.0 98 66-111
53-70-3 Dibenzo(a,h)anthracene 50 58.8 118 66-119
132-64-9 Dibenzofuran 50 46.5 93 61-106
91-94-1 3,3'-Dichlorobenzidine 50 48.8 98 46-117
84-66-2 Diethyl Phthalate 50 54.3 109*64-108
131-11-3 Dimethyl Phthalate 50 50.6 101 63-106
* = Outside of Control Limits.
31 of 54
FC228866.2.1
Blank Spike Summary Page 2 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-BS X086142.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
84-74-2 Di-n-butyl Phthalate 50 58.6 117*65-107
117-84-0 Di-n-octyl Phthalate 50 64.2 128*62-118
121-14-2 2,4-Dinitrotoluene 50 51.0 102 61-110
606-20-2 2,6-Dinitrotoluene 50 48.4 97 63-108
117-81-7 bis(2-Ethylhexyl)phthalate 50 55.3 111 61-117
206-44-0 Fluoranthene 50 48.5 97 63-106
86-73-7 Fluorene 50 48.4 97 62-108
118-74-1 Hexachlorobenzene 50 46.1 92 63-108
87-68-3 Hexachlorobutadiene 50 41.0 82 42-102
77-47-4 Hexachlorocyclopentadiene 50 43.0 86 39-102
67-72-1 Hexachloroethane 50 42.6 85 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 51.5 103 64-119
78-59-1 Isophorone 50 51.6 103*43-87
90-12-0 1-Methylnaphthalene 50 48.3 97 53-102
91-57-6 2-Methylnaphthalene 50 47.2 94 51-102
91-20-3 Naphthalene 50 45.8 92 47-100
98-95-3 Nitrobenzene 50 52.7 105*50-104
621-64-7 N-Nitrosodi-n-propylamine 50 50.9 102 52-104
86-30-6 N-Nitrosodiphenylamine 50 52.1 104 64-108
85-01-8 Phenanthrene 50 48.8 98 66-110
129-00-0 Pyrene 50 49.6 99 64-113
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 44%14-67%
4165-62-2 Phenol-d5 32%10-50%
118-79-6 2,4,6-Tribromophenol 81%33-118%
4165-60-0 Nitrobenzene-d5 98%42-108%
321-60-8 2-Fluorobiphenyl 84%40-106%
1718-51-0 Terphenyl-d14 84%39-121%
* = Outside of Control Limits.
32 of 54
FC228866.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-MS X086147.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
OP95288-MSD X086148.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
FC2307-1 X086146.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
FC2307-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
65-85-0 Benzoic Acid ND 196 98.9 50 196 89.4 46 10 10-69/39
59-50-7 4-Chloro-3-methyl Phenol ND 98 91.2 93 98 90.8 93 0 54-103/23
95-57-8 2-Chlorophenol ND 98 68.6 70 98 65.2 67 5 52-98/25
120-83-2 2,4-Dichlorophenol ND 98 72.9 74 98 72.8 74 0 53-103/26
105-67-9 2,4-Dimethylphenol 29.6 98 99.9 72 98 99.8 72 0 43-90/27
51-28-5 2,4-Dinitrophenol ND 196 166 85 196 170 87 2 44-112/25
534-52-1 4,6-Dinitro-o-cresol ND 196 160 82 196 163 83 2 66-121/23
95-48-7 2-Methylphenol 5.0 98 80.9 77 98 76.8 73 5 43-90/28
3&4-Methylphenol ND 196 142 72 196 133 68 7 36-88/28
88-75-5 2-Nitrophenol ND 98 76.4 78 98 75.7 77 1 53-102/29
100-02-7 4-Nitrophenol ND 196 126 64*196 121 62 4 18-62/33
87-86-5 Pentachlorophenol ND 196 172 88 196 172 88 0 61-115/26
108-95-2 Phenol ND 98 44.6 45 98 39.8 41 11 19-56/35
88-06-2 2,4,6-Trichlorophenol ND 98 74.5 76 98 75.7 77 2 59-107/23
83-32-9 Acenaphthene ND 98 74.7 76 98 73.6 75 1 61-107/22
208-96-8 Acenaphthylene ND 98 82.8 84 98 81.3 83 2 60-104/22
120-12-7 Anthracene ND 98 73.5 75 98 73.1 75 1 65-108/20
56-55-3 Benzo(a)anthracene ND 98 79.2 81 98 79.0 81 0 66-111/22
50-32-8 Benzo(a)pyrene ND 98 86.8 89 98 91.2 93 5 62-107/23
205-99-2 Benzo(b)fluoranthene ND 98 94.5 96 98 94.7 97 0 65-114/23
191-24-2 Benzo(g,h,i)perylene ND 98 84.9 87 98 86.5 88 2 66-116/23
207-08-9 Benzo(k)fluoranthene ND 98 89.5 91 98 89.3 91 0 65-114/24
101-55-3 4-Bromophenyl Phenyl Ether ND 98 76.6 78 98 77.7 79 1 65-109/23
85-68-7 Butyl Benzyl Phthalate ND 98 98.0 100 98 97.8 100 0 65-112/24
106-47-8 4-Chloroaniline ND 98 56.0 57 98 47.2 48*17 49-105/27
111-91-1 bis(2-Chloroethoxy)methane ND 98 82.8 84 98 80.9 83 2 51-102/28
111-44-4 bis(2-Chloroethyl)ether 1.2 J 98 82.5 83 98 78.0 78 6 53-100/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 98 83.7 85 98 80.8 82 4 45-106/26
91-58-7 2-Chloronaphthalene ND 98 76.2 78 98 73.4 75 4 57-103/23
7005-72-3 4-Chlorophenyl Phenyl Ether ND 98 73.7 75 98 72.1 74 2 62-105/20
218-01-9 Chrysene ND 98 77.3 79 98 79.0 81 2 66-111/22
53-70-3 Dibenzo(a,h)anthracene ND 98 90.0 92 98 90.2 92 0 66-119/24
132-64-9 Dibenzofuran ND 98 77.4 79 98 76.1 78 2 61-106/21
91-94-1 3,3'-Dichlorobenzidine ND 98 3.7 4*98 2.9 3*24 46-117/29
84-66-2 Diethyl Phthalate ND 98 88.5 90 98 87.8 90 1 64-108/21
131-11-3 Dimethyl Phthalate ND 98 80.4 82 98 79.5 81 1 63-106/22
* = Outside of Control Limits.
33 of 54
FC228866.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95288-MS X086147.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
OP95288-MSD X086148.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
FC2307-1 X086146.D 1 02/03/23 KA 02/03/23 OP95288 SX3414
The QC reported here applies to the following samples:Method: EPA 625.1
FC2288-2, FC2288-3
FC2307-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
84-74-2 Di-n-butyl Phthalate ND 98 96.5 98 98 96.8 99 0 65-107/21
117-84-0 Di-n-octyl Phthalate ND 98 120 122*98 121 123*1 62-118/24
121-14-2 2,4-Dinitrotoluene ND 98 83.2 85 98 83.3 85 0 61-110/21
606-20-2 2,6-Dinitrotoluene ND 98 76.9 78 98 77.9 79 1 63-108/21
117-81-7 bis(2-Ethylhexyl)phthalate ND 98 98.3 100 98 98.1 100 0 61-117/23
206-44-0 Fluoranthene ND 98 79.2 81 98 78.7 80 1 63-106/21
86-73-7 Fluorene ND 98 80.8 82 98 77.9 79 4 62-108/20
118-74-1 Hexachlorobenzene ND 98 75.1 77 98 73.5 75 2 63-108/22
87-68-3 Hexachlorobutadiene ND 98 63.9 65 98 62.1 63 3 42-102/28
77-47-4 Hexachlorocyclopentadiene ND 98 65.8 67 98 65.3 67 1 39-102/29
67-72-1 Hexachloroethane ND 98 73.8 75 98 71.1 73 4 42-100/29
193-39-5 Indeno(1,2,3-cd)pyrene ND 98 86.7 88 98 89.7 91 3 64-119/24
78-59-1 Isophorone ND 98 78.9 80 98 77.2 79 2 43-87/25
90-12-0 1-Methylnaphthalene ND 98 76.1 78 98 73.7 75 3 53-102/27
91-57-6 2-Methylnaphthalene ND 98 76.1 78 98 73.6 75 3 51-102/26
91-20-3 Naphthalene 4.7 J 98 76.6 73 98 74.3 71 3 47-100/29
98-95-3 Nitrobenzene ND 98 79.5 81 98 78.2 80 2 50-104/28
621-64-7 N-Nitrosodi-n-propylamine ND 98 86.5 88 98 82.7 84 4 52-104/25
86-30-6 N-Nitrosodiphenylamine ND 98 84.0 86 98 84.1 86 0 64-108/23
85-01-8 Phenanthrene ND 98 78.9 80 98 78.6 80 0 66-110/21
129-00-0 Pyrene ND 98 81.2 83 98 81.1 83 0 64-113/23
CAS No.Surrogate Recoveries MS MSD FC2307-1 Limits
367-12-4 2-Fluorophenol 46%43%29%14-67%
4165-62-2 Phenol-d5 42%37%24%10-50%
118-79-6 2,4,6-Tribromophenol 71%72%67%33-118%
4165-60-0 Nitrobenzene-d5 77%74%75%42-108%
321-60-8 2-Fluorobiphenyl 68%67%64%40-106%
1718-51-0 Terphenyl-d14 70%68%59%39-121%
* = Outside of Control Limits.
34 of 54
FC228866.3.1
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
35 of 54
FC22887
Method Blank Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95250-MB NN041292.D 1 02/03/23 AF 02/01/23 OP95250 GNN1899
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 41%40-140%
580-13-2 2-Bromonaphthalene 82%40-140%
84-15-1 o-Terphenyl 70%40-140%
321-60-8 2-Fluorobiphenyl 80%40-140%
36 of 54
FC228877.1.1
Method Blank Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95250-MB NN041324.D 1 02/06/23 AF 02/01/23 OP95250 GNN1900
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics 111 200 50 ug/l J
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 59%40-140%
580-13-2 2-Bromonaphthalene 85%40-140%
84-15-1 o-Terphenyl 73%40-140%
321-60-8 2-Fluorobiphenyl 83%40-140%
37 of 54
FC228877.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95250-BS NN041293.D 1 02/03/23 AF 02/01/23 OP95250 GNN1899
OP95250-BSD NN041294.D 1 02/03/23 AF 02/01/23 OP95250 GNN1899
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC2288-2, FC2288-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
83-32-9 Acenaphthene 100 77.9 78 82.9 83 6 40-140/30
208-96-8 Acenaphthylene 100 74.3 74 79.2 79 6 40-140/30
120-12-7 Anthracene 100 80.1 80 82.7 83 3 40-140/30
56-55-3 Benzo(a)anthracene 100 94.4 94 96.6 97 2 40-140/30
50-32-8 Benzo(a)pyrene 100 89.7 90 92.5 93 3 40-140/30
205-99-2 Benzo(b)fluoranthene 100 87.9 88 89.7 90 2 40-140/30
191-24-2 Benzo(g,h,i)perylene 100 78.1 78 80.9 81 4 40-140/30
207-08-9 Benzo(k)fluoranthene 100 82.5 83 84.5 85 2 40-140/30
218-01-9 Chrysene 100 89.0 89 90.9 91 2 40-140/30
53-70-3 Dibenzo(a,h)anthracene 100 78.5 79 81.9 82 4 40-140/30
206-44-0 Fluoranthene 100 86.3 86 87.9 88 2 40-140/30
86-73-7 Fluorene 100 78.8 79 82.6 83 5 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 100 76.2 76 79.1 79 4 40-140/30
91-57-6 2-Methylnaphthalene 100 67.1 67 70.8 71 5 40-140/30
91-20-3 Naphthalene 100 62.9 63 65.2 65 4 40-140/30
85-01-8 Phenanthrene 100 81.1 81 83.5 84 3 40-140/30
129-00-0 Pyrene 100 89.5 90 91.2 91 2 40-140/30
C11-C22 Aromatics (Unadj.)1700 1410 83 1460 86 3 40-140/30
C9-C18 Aliphatics 600 369 62 365 61 1 40-140/30
C19-C36 Aliphatics 800 626 78 595 74 5 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 47%44%40-140%
580-13-2 2-Bromonaphthalene 76%84%40-140%
84-15-1 o-Terphenyl 73%75%40-140%
321-60-8 2-Fluorobiphenyl 75%82%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP95250-BS 2-Methylnaphthalene 67.1 ND 0.0%5.0
OP95250-BS Naphthalene 62.9 ND 0.0%5.0
OP95250-BSD 2-Methylnaphthalene 70.8 ND 0.0%5.0
OP95250-BSD Naphthalene 65.2 ND 0.0%5.0
* = Outside of Control Limits.
38 of 54
FC228877.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FC2288
Account:GRINCC GRI (Geological Resources Inc.)
Project:Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP95250-MS NN041349.D 1 02/07/23 AF 02/01/23 OP95250 GNN1900
OP95250-MSD NN041296.D 1 02/03/23 AF 02/01/23 OP95250 GNN1899
FC2186-1 NN041297.D 1 02/03/23 AF 02/01/23 OP95250 GNN1899
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FC2288-2, FC2288-3
FC2186-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
83-32-9 Acenaphthene ND 196 107 55 196 152 78 20 40-140/50
208-96-8 Acenaphthylene ND 196 103 53 196 145 74 21 40-140/50
120-12-7 Anthracene 3.0 J 196 107 53 196 156 78 24 40-140/50
56-55-3 Benzo(a)anthracene ND 196 116 59 196 172 88 26 40-140/50
50-32-8 Benzo(a)pyrene ND 196 109 56 196 161 82 28 40-140/50
205-99-2 Benzo(b)fluoranthene ND 196 105 54 196 155 79 26 40-140/50
191-24-2 Benzo(g,h,i)perylene ND 196 93.2 48 196 137 70 28 40-140/50
207-08-9 Benzo(k)fluoranthene ND 196 101 52 196 149 76 27 40-140/50
218-01-9 Chrysene ND 196 109 56 196 163 83 26 40-140/50
53-70-3 Dibenzo(a,h)anthracene ND 196 94.5 48 196 144 73 31 40-140/50
206-44-0 Fluoranthene ND 196 107 55 196 158 81 25 40-140/50
86-73-7 Fluorene ND 196 105 54 196 152 78 22 40-140/50
193-39-5 Indeno(1,2,3-cd)pyrene ND 196 91.3 47 196 135 69 29 40-140/50
91-57-6 2-Methylnaphthalene ND 196 94.4 48 196 131 67 18 40-140/50
91-20-3 Naphthalene ND 196 87.4 45 196 121 62 18 40-140/50
85-01-8 Phenanthrene ND 196 104 53 196 152 78 24 40-140/50
129-00-0 Pyrene ND 196 111 57 196 163 83 25 40-140/50
C11-C22 Aromatics (Unadj.)ND 3330 1820 55 3330 2640 79 24 40-140/50
C9-C18 Aliphatics 183 J 1180 680 42 1180 839 56 15 40-140/50
C19-C36 Aliphatics ND 1570 930 59 1570 1140 73 23 40-140/50
CAS No.Surrogate Recoveries MS MSD FC2186-1 Limits
3386-33-2 1-Chlorooctadecane 41%48%31%* a 40-140%
580-13-2 2-Bromonaphthalene 78%78%101%40-140%
84-15-1 o-Terphenyl 47%69%50%40-140%
321-60-8 2-Fluorobiphenyl 77%76%96%40-140%
(a) Outside control limits.
* = Outside of Control Limits.
39 of 54
FC228877.3.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 8
40 of 54
FC22888
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23
MB
Metal RL IDL MDL raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3
Barium 200 .5 1
Beryllium 4.0 .1 .2
Boron 100 5 10
Cadmium 5.0 .1 .2
Calcium 1000 50 50
Chromium 10 .5 1
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 15 17
Lead 5.0 1 1.1 -0.10 <5.0
Lithium 10 .5 1.3
Magnesium 5000 35 35
Manganese 15 .25 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 100 200
Selenium 10 2 2.9
Silver 10 .5 .7
Sodium 10000 250 500
Strontium 10 .25 .5
Thallium 10 1 1.4
Tin 50 .5 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
41 of 54
FC228888.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23 02/01/23
FC2288-2 QC FC2288-2 Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum anr
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Boron
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 1.4 1.5 6.9 0-20 1.4 508 500 101.3 80-120
Lithium
Magnesium anr
Manganese anr
Molybdenum anr
Nickel anr
Potassium anr
Selenium anr
Silver anr
Sodium anr
Strontium
Thallium anr
Tin anr
Titanium
Vanadium anr
Zinc anr
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
42 of 54
FC228888.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23
FC2288-2 Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum anr
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Boron
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 1.4 495 500 98.7 2.6 20
Lithium
Magnesium anr
Manganese anr
Molybdenum anr
Nickel anr
Potassium anr
Selenium anr
Silver anr
Sodium anr
Strontium
Thallium anr
Tin anr
Titanium
Vanadium anr
Zinc anr
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
43 of 54
FC228888.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum anr
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Boron
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 511 500 102.2 80-120
Lithium
Magnesium anr
Manganese anr
Molybdenum anr
Nickel anr
Potassium anr
Selenium anr
Silver anr
Sodium anr
Strontium
Thallium anr
Tin anr
Titanium
Vanadium anr
Zinc anr
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
44 of 54
FC228888.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23
FC2288-2 QC
Metal Original SDL 1:5 %DIF Limits
Aluminum anr
Antimony anr
Arsenic anr
Barium anr
Beryllium anr
Boron
Cadmium anr
Calcium anr
Chromium anr
Cobalt anr
Copper anr
Iron anr
Lead 1.40 0.00 100.0(a) 0-10
Lithium
Magnesium anr
Manganese anr
Molybdenum anr
Nickel anr
Potassium anr
Selenium anr
Silver anr
Sodium anr
Strontium
Thallium anr
Tin anr
Titanium
Vanadium anr
Zinc anr
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
45 of 54
FC228888.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FC2288
Account: GRINCC - GRI (Geological Resources Inc.)
Project: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
QC Batch ID: MP41783 Methods: SW846 6010D
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 02/01/23
Sample Final FC2288-2 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 9.8 10 1.4 1.372 47.7 0.2 2.5 50 92.7 80-120
Lithium
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP41783: FC2288-2, FC2288-3
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
46 of 54
FC228888.1.5
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Scott, LA)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 9
47 of 54
FC22889
Page 1 ol 2
I
?
SGS
CHAIN OF CUSTODY
SGS North America lnc. - Orlando
4405 Vinoland Road, Suito C"15 Orlando, F|32811
TEL. 407-{216700 Ft\X: 107425-0707
Send to LA Lab
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FC22A8
Cliant / Repo(ing lnformation Projsct lnformation R€quested Analysis ( s€e TEST COOE she€t)
SGS North Americ. lnc.Home Race 1i 7824 Seven Circi€ Rd Nakina, NC
4405 vinoland Rd, Suit€ C"15 ailli.g rntom.tion ( , ditr.E(t ttu6 R.p..t to)
328't1OrlandoFL
ProlectConla.r
m!n..moh.mh.de.c..com
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FC2288: Chain of Custody
Page 1 of 3
SGS Scott, LA
48 of 54
FC228899.1
=tsHX"SI3€3JYI/6SZBS80 iOV3NUH a-l 00 02 :13lr.L3u€z8l-lI0 :l1UO dIHSsr 31souoa slu-l3Nrd Eoi}3NI YSlU3ltU l]tUON S5S9NIAT3J3U 3'1dI,JUSo0Z9-S?l (1.0t) C'180:0I ]119I]rL-,,'+I-r sn-vl.i7 aB0sor#0[{u]^0 ,tIlu0ludgoer 9099 rElg qF?unn:nl nlJ- nHtrutG4H:l:tu4E-e,u.Bl8090r v'l lllrlvJv'IFC2288: Chain of Custody
Page 2 of 3
49 of 54
FC228899.1
SGS Sample Receipt Summary
Job Number:FC2288 Client:SGS
Date / Time Received:2/6/2023 10:40:00 AM Delivery Method:FED EX
Project:HOME RACE 1
4. No. Coolers:1
Airbill #'s:6134 6605 7206
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR002;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (4.2/4); IR002
FC2288: Chain of Custody
Page 3 of 3
50 of 54
FC228899.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
(SGS Scott, LA)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 10
51 of 54
FC228810
Method Blank Summary Page 1 of 1
Job Number:FC2288
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2368-MB1 LE040440.D 1 02/07/23 MB n/a n/a GLE2368
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC2288-2, FC2288-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 0.14 ug/l
100-41-4 Ethylbenzene 0.34 5.0 0.17 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 5.0 0.14 ug/l
91-20-3 Naphthalene 2.1 5.0 0.41 ug/l J
108-88-3 Toluene 0.19 5.0 0.15 ug/l J
m,p-Xylene 1.2 10 0.40 ug/l J
95-47-6 o-Xylene 0.61 5.0 0.18 ug/l J
C5- C8 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 50 ug/l
C9- C10 Aromatics (Unadj.)ND 100 20 ug/l
C5- C8 Aliphatics ND 100 50 ug/l
C9- C12 Aliphatics ND 100 50 ug/l
C9- C10 Aromatics ND 100 20 ug/l
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 115%70-130%
615-59-8 2,5-Dibromotoluene 116%70-130%
52 of 54
FC22881010.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FC2288
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2368-BS1 LE040438.D 1 02/07/23 MB n/a n/a GLE2368
GLE2368-BSD1 LE040439.D 1 02/07/23 MB n/a n/a GLE2368
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC2288-2, FC2288-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 40 44.7 112 46.2 116 3 70-130/25
100-41-4 Ethylbenzene 40 44.1 110 45.4 114 3 70-130/25
1634-04-4 Methyl Tert Butyl Ether 40 42.9 107 43.8 110 2 70-130/25
91-20-3 Naphthalene 40 49.0 123 49.8 125 2 70-130/25
108-88-3 Toluene 40 44.6 112 46.1 115 3 70-130/25
m,p-Xylene 80 88.4 111 90.7 113 3 70-130/25
95-47-6 o-Xylene 40 44.5 111 45.7 114 3 70-130/25
C5- C8 Aliphatics (Unadj.)120 143 120 148 123 3 70-130/25
C9- C12 Aliphatics (Unadj.)120 115 96 115 96 0 70-130/25
C9- C10 Aromatics (Unadj.)40 43.1 108 43.9 110 2 70-130/25
C5- C8 Aliphatics 242 250 3 70-130/25
C9- C12 Aliphatics 189 191 1 70-130/25
C9- C10 Aromatics 40 43.1 108 43.9 110 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 113%116%70-130%
615-59-8 2,5-Dibromotoluene 114%118%70-130%
* = Outside of Control Limits.
53 of 54
FC22881010.2.1
Duplicate Summary Page 1 of 1
Job Number:FC2288
Account:ALSE SGS Orlando, FL
Project:GRINCC: Home Race 1; 7824 Seven Circle Rd, Nakina, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA87631-2DUP LE040445.D 1 02/08/23 MB n/a n/a GLE2368
LA87631-2 LE040444.D 1 02/08/23 MB n/a n/a GLE2368
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FC2288-2, FC2288-3
LA87631-2 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene 0.76 J 0.70 J 8 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP LA87631-2 Limits
615-59-8 2,5-Dibromotoluene 113%113%70-130%
615-59-8 2,5-Dibromotoluene 113%114%70-130%
* = Outside of Control Limits.
54 of 54
FC22881010.3.1