WA-92993_96847_CA_RPTS_20220919_LSI

Revised Limited Site Investigation
Report
Bayer Property
407 West Main Street
Havelock, Craven County, NC
September 19, 2022
Terracon Project No. 72227070

Prepared for:
Cathy Bayer
Havelock, North Carolina

Prepared by:
Terracon Consultants, Inc.
Winterville, North Carolina

Terracon Consultants, Inc. 314 Beacon Drive, Winterville, NC 28590
P [252] 353 1600 F [252] 353 0002 terracon.com

September 19, 2022

Cathy Bayer
PO Box 436
Havelock, NC 28532

Attn: Ms. Cathy Bayer
P: [phone]
E: [e-mail]

Re: Revised Limited Site Investigation Report
Bayer Property
407 West Main Street
Havelock, Craven County, North Carolina
Terracon Project No. 72227070

Dear Ms. Bayer:

At your request, Terracon Consultants, Inc. (Terracon) has completed a Limited Site
Investigation (LSI) at the above-referenced property. This investigation was performed in
general accordance with Terracon’s Proposal No. P72227070 dated July 19, 2022.

If you have any questions or comments pertaining to the material presented herein, please
contact Allen McColl by telephone at [phone] or by email at
[e-mail].

Sincerely,
Terracon Consultants, Inc.

Allen McColl Carl F. Bonner, PE
Project Scientist Principal / Office Manager
Environmental Services

Reviewed by: George K. Flores, PE

Attachments

TABLE OF CONTENTS

1.0 INTRODUCTION ...................................................................................................... 1
1.1 Standard of Care ...................................................................................................... 3
1.2 Additional Scope Limitations ..................................................................................... 3
1.3 Reliance.................................................................................................................... 4
2.0 LIMITED SITE INVESTIGATION TASKS ................................................................. 4
2.1 Preliminary Assessment Tasks ................................................................................. 4
2.2 Field Services ........................................................................................................... 4
2.3 Boring Information .................................................................................................... 5
2.4 Groundwater Sample Collection ............................................................................... 5
3.0 LABORATORY ANALYTICAL RESULTS ............................................................... 6
3.1 Laboratory Analytical Program .................................................................................. 6
3.2 Soil Analytical Results ............................................................................................... 6
3.3 Groundwater Analytical Results ................................................................................ 7
4.0 DISCUSSION ........................................................................................................... 7
5.0 GENERAL COMMENTS .......................................................................................... 8

LIST OF APPENDICES

Appendix A Exhibit 1 – Topographic Vicinity Map
Exhibit 2 – Site Diagram
Exhibit 3 – Boring Location Diagram
Appendix B Tables
Appendix C Boring Logs
Appendix D Laboratory Analytical Reports

Responsive ■ Resourceful ■ Reliable 1

REVISED LIMITED SITE INVESTIGATION
BAYER PROPERTY
407 WEST MAIN STREET
HAVELOCK, CRAVEN COUNTY, NC

Project No. 72227070

September 19, 2022

1.0 INTRODUCTION

Terracon Consultants, Inc. (Terracon) has completed a Limited Site Investigation (LSI) of the
Bayer Property located at 407 West Main Street in Havelock, Craven County, North Carolina
(site). Based on information provided by the client and/or the Craven County GIS website, we
further understand the following: the site is listed under Parcel Identification Number 6-053-
020; the site totals approximately 0.81 acres; and the site is currently unoccupied and
recently utilized as a used car sales lot (Tim Newton Auto Sales).

We further that the site was formerly an automobile dealership over 60 years ago that
potentially performed automotive repair services and automotive body shop and painting
operations.

The site contains two buildings: One building contains an office and service bays that is a “L”
shaped building and the second building could be a former automotive paint/body shop.

Terracon performed an LSI at the site in April 2011 (Terracon Project Number 72117018,
report dated April 26, 2011). The 2011 LSI was requested by the current property owner in
order to evaluate soil and/or groundwater contamination associated with the site due to
concerns regarding “back door dumping” of automotive chemicals on the eastern and
southern sides of the “L” shaped former automotive repair shop.

In April 2011, six borings were advanced on the eastern and southern sides of the “L” shaped
building with three soil samples and two groundwater samples collected from these borings
based on field screening findings. Of the samples collected, boring SB-6/GW-2, that was
advanced in a stained soil area near the southwestern corner of the “L” shaped building, was
analyzed to contain soil above the North Carolina Department of Environmental Quality
(NCDEQ) Total Petroleum Hydrocarbon (TPH) Action Level for Gasoline Range Organics
(GRO) and Diesel Range Organics (DRO). The groundwater sample collected from boring
SB-6/GW-2 was also analyzed to contain naphthalene above NCDEQ’s 2L Groundwater
Quality Standards.

With permission from Ms. Bayer, Terracon notified NCDEQ about the soil and groundwater
contamination exceedances identified in 2011.

Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 2

After review of the 2011 LSI, NCDEQ opened a regulatory incident (Inc # 93124) and
requested that the contaminated soil in the area of SB-6/GW-2 be removed, a permanent
groundwater monitoring well be installed and sampled in the area of SB-6/GW-2 after over-
excavation of soils and backfilling had been conducted; and a receptor survey be performed.

The Initial Abatement Actions and Limited Site Assessment activities requested by NCDEQ
occurred between November 2011 and January 2012. During these activities, approximately
42 tons of contaminated soil were removed from the site; confirmation soil samples were
collected from the excavation pit; the pit was backfilled with offsite soil; one permanent
groundwater monitoring well (MW-1) was installed and a groundwater sample was collected
from this well; and a receptor survey was performed.

Based on the confirmation soil samples, contaminated soils above NCDEQ’s Soil-to-Water
Maximum Soil Contaminant Concentrations (MSCCs) remained in the source area.
Specifically, confirmation soil samples SW-1 (collected from the southwestern excavation pit
sidewall), SW-4 (collected from the northwestern excavation pit sidewall) and the basin soil
sample (collected from the base of the excavation pit) contained target contaminants above
NCDEQ’s Soil-to-Water MSCCs, but not above NCDEQ’s established Residential or
Industrial/Commercial MSCCs. Additional contaminated soil could not be readily removed
due to the shallow groundwater level and the risk of undermining the repair shop building,
fencing and a power pole with guy wires in the area of the excavation.

The groundwater sample collected from MW-1 during Initial Abatement Actions and Limited
Site Assessment activities was analyzed to be below the laboratory reporting limits and
NCDEQ’s 2L Groundwater Quality Standards.

Receptors of concern were not identified in the area of the site.

Based on the findings of the Initial Abatement Action and Limited Site Assessment services,
NCDEQ issued a “Notice of No Further Action” (NFA) for the incident on March 26, 2012.

Based on several phone conversations between Terracon personnel and Ms. Bayer in June
and July 2022, we understand that she is planning to sell the site to an interested party and
that prior to the property transaction, Ms. Bayer would like to demonstrate that the residual
soil contamination is attenuating and that contaminated soil or groundwater is not located
under the slab of the “L” shaped building, adjacent to the 2011 soil abatement area.

Terracon conducted a cursory site visit on June 30, 2022 to look inside the bay areas of the
“L” shaped building and to observe the current site status in the area where the contaminated
soil was removed. During this site visit, Terracon observed a concrete patch in the concrete
slab of one of the service bays inside the “L” shaped building that would potentially indicate
an underground hydraulic vehicle lift was formerly utilized onsite. Terracon also observed a
large floor drain in the northernmost bay. No other markings or patches were observed
Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 3

inside the repair bays that would suggest other underground lifts or floor drains have
historically been utilized inside this building. lonely aboveground lifts are currently utilized in
this building.

During the June 2022 site visit, Terracon also observed a disconnected/open drain pipe near
the southwestern corner of the site that appears to be potentially connected to the interior
floor drain. The excavation area of 2011 is located approximately 25 feet northeast of this
open drain and it is thought that the interior floor drain mentioned above is connected to the
open piping.

Based on discussions with Ms. Bayer and findings during the June 2022 site visit, Terracon
proposed the scope of services as discussed in Section 2.0 of this report.

The location of the site is illustrated on Exhibit 1 in Appendix A, Topographic Vicinity
Map. The general layout of the site and adjoining property identifications are illustrated on
the Site Diagram, Exhibit 2 in Appendix A. Exhibits 2 and 3 also indicate other pertinent
info for the site such as the location of the 2011 excavation area and location of the existing
monitoring well on the site. Boring locations are shown in the Boring Location Diagram,
Exhibit 3 in Appendix A. Analytical data tables are located in Appendix B. Boring Logs
are presented in Appendix C. The laboratory analytical report and chain-of-custody are
presented in Appendix D.

1.1 Standard of Care

Terracon’s services were performed in a manner consistent with generally accepted practices
of the profession undertaken in similar studies in the same geographical area during the
same time period. Terracon makes no warranties, either express or implied, regarding the
findings, conclusions or recommendations. Please note that Terracon does not warrant the
work of laboratories, regulatory agencies or other third parties supplying information used in
the preparation of the report. These LSI services were performed in accordance with the
scope of work agreed with you, our client, as reflected in our proposal and were not restricted
by ASTM E1903-19.

1.2 Additional Scope Limitations

Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope
of work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, nondetectable or not present during these services, and we
cannot represent that the site contains no hazardous substances, toxic materials, petroleum
products, or other latent conditions beyond those identified during this LSI. Subsurface
conditions may vary from those encountered at specific borings or wells or during other
Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 4

surveys, tests, assessments, investigations or exploratory services; the data, interpretations,
findings, and our recommendations are based solely upon data obtained at the time and
within the scope of these services.

1.3 Reliance

This report has been prepared for the exclusive use of Cathy Bayer and any authorization for
use or reliance by any other party is prohibited without the express written authorization of
Ms. Bayer and Terracon. Any unauthorized distribution or reuse is at the client’s sole risk.
Notwithstanding the foregoing, reliance by authorized parties will be subject to the terms,
conditions and limitations stated in the proposal, LSI report, and Terracon’s terms and
conditions as presented in our Agreement for Services. The limitation of liability defined in out
Agreement for Services is the aggregate limit of Terracon’s liability to the client and all relying
parties unless otherwise agreed in writing.

2.0 LIMITED SITE INVESTIGATION TASKS

2.1 Preliminary Assessment Tasks

Prior to drilling activities occurring, underground utilities assigned to public entities were
identified and marked by North Carolina 811 service contractors in the planned drilling areas.
Efforts were also made by Terracon personnel to identify private underground utilities using
ground penetrating radar (GPR) and other underground utility clearing devices prior to drilling
activities commencing.

2.2 Field Services

Drilling services were performed on August 18, 2022 by Environmental Hydrogeological
Consultants, Inc. (EHC, Inc.) using direct-push technology (DPT) drilling equipment under the
supervision of a Terracon environmental professional. Borings were advanced to a depth of
approximately 6 to 8 feet below ground surface (bgs) at the specific locations noted below:

◼ B–1: advanced inside the building near the interior floor drain of the garage area.
◼ B-2: advanced inside the building near the former underground lift of the garage area.
◼ B-3: advanced at the open drain pipe near the southwestern property corner.
◼ B-4, B-5 and B-6: advanced around three sides of the perimeter of the former paint/body
shop (northwestern, southwestern and southeastern). Sampling and/or field screening
along a portion of the northeastern side of this building was performed during the 2011
LSI.
◼ B-7 and B-8: advanced in the general areas where residual soil contamination remained
in pit sidewalls after the 2011 excavation activities.

Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 5

One soil sample was collected from each of these eight boring locations and sent to a
laboratory for analysis of target contaminants.

Based on field screening readings and/or in assumed down-gradient areas of the site,
groundwater samples were also collected from borings B-2, B-3 and B-5 though temporary
monitoring wells installed by EHC.

During the 2022 LSI services, Terracon also collected a groundwater sample from existing
monitoring well MW-1.

A Boring Location Diagram (Exhibit 3) indicating the general site layout and
boring/temporary well locations is included in Appendix A. Exhibits 2 and 3 also show the
location of existing monitoring well MW-1.

2.3 Boring Information

Soil samples were collected continuously using four-foot core barrel samplers and observed
to document soil lithology, color, moisture content and sensory evidence of impairment. A
disposable clear plastic liner in the sampling tube was changed between each boring interval
and location. Drilling equipment was cleaned using a high-pressure washer prior to beginning
the project and before beginning each boring.

Soils encountered during drilling activities consisted predominantly of silty and clayey sand
and clays.

Apparent petroleum odors were noted in soil cores obtained during the drilling in boring B-3.

Groundwater was encountered during drilling at approximately 4.5 feet bgs and was recorded
at 4.35 feet below the top of casing of established monitoring well MW-1.

The collected soil samples were field-screened for volatile organic vapors (VOVs) using
typical field-screening equipment (MiniRAE 3000 photoionization detector [PID]). Boring logs
indicating depths of each boring, soil types encountered during drilling activities and PID
readings at approximately 2-foot intervals are located in Appendix C. One soil sample from
each boring was collected for laboratory analysis from borings B-1 through B-8, from depths
of between 2 to 4 feet bgs. Soil samples selected for laboratory analysis were based on field
screen readings and/or were collected just above the perceived groundwater saturation zone.

2.4 Groundwater Sample Collection

Soil borings B-2, B-3 and B-5 were converted to temporary groundwater monitoring wells to
facilitate the collection of groundwater samples for laboratory analysis. Well construction
consisted of one-inch diameter polyvinyl chloride (PVC) well screen with solid riser pipe.
Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 6

Terracon also sampled existing monitoring well MW-1.

Prior to groundwater sample collection, each temporary well and permanent monitoring well
MW-1 were purged using a low-flow peristaltic pump and dedicated tubing. Approximately 3
well volumes were purged from monitoring well MW-1 and each temporary well prior to
sample collection. Disposable gloves were used and changed at each sample location.
Groundwater samples were collected into laboratory prepared containers and placed into an
iced cooler along with the soil samples.

Apparent petroleum odors were noted in groundwater sample B-3 GW during the purge of
this temporary well. Petroleum odors were not noted during the purging or sampling of the
other two temporary wells or established monitoring well MW-1.

Following sample collection, temporary well materials were removed and the borings were
backfilled using hydrated bentonite pellets to within one foot of land surface then topped with
sand backfill and the surface was restored (to the extent practicable) to its previous
appearance. The borings advanced inside the garage area were capped with concrete to the
slab surface.

3.0 LABORATORY ANALYTICAL RESULTS

3.1 Laboratory Analytical Program

The sample cooler containing the soil and groundwater samples and completed chain-of-
custody form was relinquished to Pace Analytical, Inc., an analytical laboratory in
Huntersville, NC for standard laboratory reporting schedule. Soil samples B-1 Soil through B-
8 Soil were analyzed for volatile organic compounds (VOCs) by U.S. Environmental
Protection Agency (EPA) Method 8260 and Polycyclic Aromatic Hydrocarbons (PAHs) using
EPA Method 8270. Groundwater samples MW-1, B-2 GW, B-3 GW and B-5 GW were
analyzed for VOCs by EPA Method 8260 and PAHs by EPA Method 8270.

3.2 Soil Analytical Results

p-Isopropyltoluene, naphthalene and 2-methylnaphthalene were detected in soil sample B-3
Soil above NCDEQ’s Soil-to-Water Maximum Soil Contamination Concentrations (MSCCs).
Methylene chloride and 2-methylnaphthalene with a “J” flags were also detected in soil
sample B-3 Soil above NCDEQ’s Soil-to-Water MSCCs. According to Pace Analytical, the
“J” flag associated with these results indicates the constituent was detected above the
laboratory adjusted detection limit, but below the laboratory adjusted reporting limit. Other
target contaminants analyzed for soil sample B-3 Soil were reported to be below the
laboratory method detection limits.

Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 7

Benzo(a)pyrene (with a “J” flag) was detected in soil sample B-5 Soil above NCDEQ’s Soil-
to-Water MSCCs.

Total xylenes were detected in soil sample B-8 Soil above NCDEQ’s Soil-to-Water MSCCs.

In soil samples B-1 Soil, B-2 Soil, B-4 Soil, B-6 Soil and B-7 Soil, target contaminants were
reported to be below the laboratory method detection limits.

None of the analytical results for the soil samples analyzed for this project were above
NCDEQ’s Residential MSCCs or Industrial/Commercial MSCCs.

A summary of soil analytical results are provided in Table 1 included in Appendix B. The
laboratory analytical report is provided in Appendix D.

3.3 Groundwater Analytical Results

In groundwater sample B-3 GW, benzene, naphthalene, 1-methylnapthalene, 2-
methylnapthalene were analyzed above the NCDEQ 2L Groundwater Quality Standards (2L
Standards) established for these constituents. In addition, 1,2,3-Trichloropropane was
analyzed in sample B-3 GW with a “J” flag qualifier and this estimated value is above
NCDEQ’s 2L Standards.

In groundwater samples MW-1, B-2 GW and B-5 GW, target contaminants were reported to
be below the laboratory method detection limits.

Table 2 in Appendix B provides a summary of groundwater analytical results. The laboratory
report is provided in Appendix D.

4.0 DISCUSSION

This investigation was performed in general accordance with Terracon’s Proposal No.
P72227070, dated July 19, 2022. The scope of work was designed to investigate the
potential for soil and groundwater impairment at the site as a result of the historical usage of
the site as an automotive repair shop and automotive body/painting shop and to investigate
further in the open drain areas of the site and in areas where residual soil contamination was
left during the 2011 soil excavation activities.

VOCs and PAHs were detected in soil sample B-3 Soil (advanced near the outdoor open and
disconnected drain piping area) at concentrations above NCDEQ Soil-to-Water MSCCs, but
below NCDEQ Residential and Industrial/Commercial MSCCs.

A PAH (benzo(a)pyrene) was also detected in soil sample B-5 Soil (advanced on the
southwestern side of the former body/paint shop) above NCDEQ’s Soil-to-Water MSCCs.
Revised Limited Site Investigation Report
Bayer Property ■ Havelock, NC
September 19, 2022 ■ Terracon Project No. 72227070

Responsive ■ Resourceful ■ Reliable 8

Total xylenes were detected in soil sample B-8 Soil (advanced on the southwestern side of
the 2011 excavation pit) above NCDEQ’s Soil-to-Water MSCCs.

None of the target contaminants were analyzed above NCDEQ’s Residential or
Industrial/Commercial MSCCs.

VOCs and PAHs were detected in groundwater sample B-3 GW at a concentration above
NCDEQ’s 2L Standards, but below established Gross Contamination Levels (GCLs).

The soil impacts on the site are potentially from the historic use of the site as an automotive
repair shop and/or body/paint shop. It appears that potentially a release to the interior floor
drain and the exterior drain piping being “open” and disconnected contributed to the release.
Based on the findings of this LSI, Terracon recommends the owner of the property notify the
NCDEQ of a release. A copy of this report should also be forwarded to the NCDEQ
Washington Regional Office for their review and comment.

5.0 GENERAL COMMENTS

The analysis and opinions expressed in this report are based upon data obtained from the
soil borings/temporary monitoring wells installed at the indicated location and from any other
information discussed in this report. This report does not reflect any variations in subsurface
chemistry, stratigraphy, of geohydrology which may occur between borings or across the site.
Actual subsurface conditions may vary and may not become evident without further
exploration.

This report is prepared for the exclusive use of our client for specific application to the project
discussed and has been prepared in accordance with generally accepted environmental
engineering practices. No warranties, express or implied, are intended or made.

Appendix A
Exhibits

SITE
7.5 MINUTE SERIES (TOPOGRAPHIC)
Drawn By:
Checked By:
Approved By:
Project Mngr:
File No.
Date:
Scale:
Project No.
Consulting Engineers and Scientists
EXHIBITTOPOGRAPHIC VICINITY MAP
1
LIMITED SITE INVESTIGATION
BAYER PROPERTY
407 W. MAIN ST.
HAVELOCK, NC
KAM
RLW
MRF/KAM
KAM
72227070
AS SHOWN
LSI72227070-1
SEPT. 2022 314 Beacon Drive Winterville, NC 28590
[phone] [phone]
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSES
LEGEND
SUBJECT SITE
Drawn By:
Checked By:
Approved By:
Project Mngr:
File No.
Date:
Scale:
Project No.
Consulting Engineers and Scientists
EXHIBITSITE DIAGRAM
2
LIMITED SITE INVESTIGATION
BAYER PROPERTY
407 W. MAIN ST.
HAVELOCK, NC
KAM
RLW
MRF/KAM
KAM
72227070
AS SHOWN
LSI72227070-2
SEPT. 2022 314 Beacon Drive Winterville, NC 28590
[phone] [phone]
AIR COMPRESSOR
GROUNDWATER MONITORING WELL LOCATION
MW-1
MINI STORAGESUBWAYLA ROSA RESTAURANTCANOPYOFFICEG
A
R
A
G
E

A
R
E
A
S
H
O
P
GRASSED
ASPHALT
ASPHALT
GRASSED
G
R
A
S
S
E
D
SE
R
V
I
C
E

R
O
A
D
W
E
S
T

M
A
I
N

S
T
R
E
E
T
Approximate Scale
0
(Feet)
60
MOBILE
HOME PARK
STRIP
MALL
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X XXXXXXXXXXXXXXXXX
X
CHAIN LINK FENCEXXX
LIMITS OF
SOIL EXCAVATION
(2011)
OPEN DRAIN
PIPING
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSES
LEGEND
SUBJECT SITE
Drawn By:
Checked By:
Approved By:
Project Mngr:
File No.
Date:
Scale:
Project No.
Consulting Engineers and Scientists
BORING LOCATION DIAGRAM EXHIBIT
3
LIMITED SITE INVESTIGATION
BAYER PROPERTY
407 W. MAIN ST.
HAVELOCK, NC
KAM
RLW
MRF/KAM
KAM
72227070
AS SHOWN
LSI72227070-3
SEPT. 2022 314 Beacon Drive Winterville, NC 28590
[phone] [phone]
AIR COMPRESSOR
GROUNDWATER MONITORING WELL LOCATION
MW-1
MINI STORAGE
SUBWAY
CANOPY
OFFICEGARAGE AREA
SHOP
GRASSED
ASPHALT
GRASSED
GRASSED
Approximate Scale
0
(Feet)
30
MOBILE
HOME PARKXXXXXXXXXXXXXXXXX
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X XXXXXXXXXXXXXXXXXXXXXXXXCHAIN LINK FENCEXXX
LIMITS OF
SOIL EXCAVATION
(2011)
B-1
B-8
B-4
B-7
BORING LOCATION
T POLE-MOUNTED TRANSFORMER
T
INTERIOR
FLOOR DRAIN
POTENTIAL FORMER
IN-GROUND
HYDRAULIC LIFTB-2
OPEN DRAIN
PIPING B-3
B-5
B-6

Appendix B
Tables

Table 1
Limited Site Investigation
Summary of Soil Analytical Results
Bayer Property
Havelock, Craven County, NC
Terracon Project No. 72227070

Page 1 of 1

Analytical Method 8260 (VOCs) 8270 (PAHs)
Contaminant of Concern -> Benzene 2-Butanone (MEK) sec-Butylbenzene Ethylbenzene Isopropylbenzene (Cumene) p-Isopropyltoluene (aka p-Cymene) Methylene Chloride Naphthalene n-Propylbenzene Tetrachloroethylene (aka perchloroethylene (PCE) Toluene Trichloroethylene (TCE) 1,2,4 - Trimethylbenzene Xylene (Total) Benzo(a)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Soil Sample
ID
Date
Collected
Depth
(in Feet) Below
Land Surface
B-1 Soil 8/18/2022 2 - 4 <0.0025 <0.0306 <0.0028 <0.003 <0.0022 <0.0031 <0.0175 <0.0034 <0.0023 <0.002 0.0149 0.0038J <0.0017 0.0068J <0.0128 <0.0130 <0.0148 <0.0126
B-2 Soil 8/18/2022 2 - 4 <0.0024 <0.029 <0.0027 <0.0028 <0.0021 <0.003 <0.0165 <0.0032 <0.0021 <0.0019 0.0062 <0.0016 <0.0017 <0.0069J <0.126 <0.128 <0.146 <0.124
B-3 Soil 8/18/2022 2 - 4 0.011J 0.101J <0.0132 0.289 0.216 1.57 0.0412J 2.49 <0.0047 <0.0042 0.11 <0.0034 3.76 1.37 <1.35 3.68J 5.01 1.42J
B-4 Soil 8/18/2022 2 - 4 <0.0034 <0.0408 <0.0037 <0.004 <0.0029 <0.0042 <0.0233 <0.0045 <0.003 <0.0027 0.0051J <0.0022 <0.0023 0.0073J <0.141 <0.144 <0.163 <0.139
B-5 Soil 8/18/2022 2 - 4 <0.0028 <0.0341 <0.0031 <0.0033 <0.0024 <0.0035 <0.0195 <0.0037 <0.0025 <0.0022 <0.002 <0.0018 <0.0019 <0.004 0.145J <0.135 <0.154 <0.131
B-6 Soil 8/18/2022 2 - 4 <0.0024 <0.0286 <0.0026 <0.0028 <0.002 <0.0029 <0.0163 <0.0031 <0.0021 <0.0019 <0.0017 <0.0015 <0.0016 0.0059J <0.125 <0.132 <0.150 <0.128
B-7 Soil 8/18/2022 2 - 4 <0.0028 <0.034 <0.0031 <0.0033 <0.0024 <0.0035 <0.0194 <0.0037 <0.0025 <0.0022 <0.002 <0.0018 <0.0059 <0.004 <0.138 <0.140 <0.160 <0.135
B-8 Soil 8/18/2022 2 - 4 <0.0046 0.128J 0.472 0.0223 0.155 <0.0114 <0.0458 0.149 0.168 <0.0056 <0.0033 <0.003 <0.0031 90.9 <1.33 <1.33 <1.51 <1.28
Soil to Water MSCCs (mg/kg) 0.0072 16 2.2 8 1.3 0.12 0.023 0.2 1.4 0.005 5.4 0.017 6.6 6 0.084 0.0054 1.5 0.2
Residential MSCCs (mg/kg) 12 9,380 1,560 60.3 1,560 1,560 93.8 5.5 1,560 93.8 1,250 7.82 156 3,120 0.66 22.8 62.5 5.5
Industrial/Commercial MSCCs (mg/kg) 59.4 140,000 23,300 297 23,300 23,300 1,400 27 23,300 1,400 18,600 71 2,330 46,700 3.2 112 934 27

Soil Analytical results in milligrams per kilogram (mg/kg)

Soil samples B-1 Soil through B-8 Soil were collected from borings advanced by the Geoprobe unit.

Each soil sample was collected just above the observed groundwater table or at the highest field screening reading just above the observed groundwater table.

Maximum Soil Contamination Concentrations (MSCCs) in this table are sourced from the North Carolina Department of Environmental Quality (NCDEQ) Comprehensive Tables for Corrective Action Guidance for Petroleum and Hazardous
Substance UST Releases and Petroleum Non-UST Releases using the March 7, 2022 version of this document.

Constituents shaded are equal to or above at least the NCDEQ Soil to Water MSCCs, if applicable. Constituents in red font and shaded are above NCDEQ’s Residential MSCCs, if applicable. Constituents in blue font and shaded are above
NCDEQ’s Industrial/Commercial MSCCs, if applicable.

Results with the “<” symbol are below the laboratory method detection limits.

Where “J” flags are noted behind lab data, the lab provided an estimated concentration of a target contaminant above the adjusted method detection limit and below the adjusted reporting limit.

Table 2
Limited Site Investigation
Summary of Groundwater Analytical Results
Bayer Property
Havelock, Craven County, NC
Terracon Project No. 72227070

Page 1 of 1

Analytical Method 8260 (VOCs) 8270 (PAHs)
Contaminant of Concern -> Acetone Benzene 1,2-Dichlorobenzene cis-1,2-Dichloroethene Ethylbenzene p-Isopropyltoluene (aka p-cymene) Naphthalene Tetrachloroethylene (aka perchloroethylene (PCE) Toluene Trichloroethylene (TCE) 1,2,3-Trichloropropane Xylenes (Total) 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Sample ID Date
Collected
MW-1 8/18/2022 <5.1 <0.34 <0.32 <0.38 <0.3 <0.41 <0.64 <0.29 <0.48 <0.38 <0.26 <0.34 <3.7 <3.4 <3.2
B-2 GW 8/18/2022 <5.1 <0.34 <0.32 <0.38 <0.3 <0.41 <0.64 <0.29 <0.48 <0.38 <0.26 <0.34 <44.2 <41.3 <37.8
B-3 GW 8/18/2022 10J 3 7.7 1 11.9 11 74.1 <0.29 22.4 0.93J 0.86J 77.3 37.4 54.4 41
B-5 GW 8/18/2022 <5.1 <0.34 <0.34 <0.38 <0.3 <0.41 <0.64 <0.29 <0.48 <0.38 <0.26 <0.34 <3.7 <3.4 <3.2
NC 2L Groundwater Quality
Standards (µg/l) 6,000 1 20 70 600 25 6 0.7 600 3 0.005 500 1 30 6
Gross Contamination Levels
for Groundwater (µg/l) 6,000,000 5,000 20,000 70,000 80,000 11,700 6,000 700 260,000 3,000 NE 50,000 1,000 12,000 6,000

Groundwater sample indicated as MW-1 was collected from an existing permanent monitoring installed on the site in 2011 as part of a stained soil investigation. Groundwater samples B-2 GW, B-3 GW, B-5 GW were collected from temporary
groundwater monitoring wells installed and abandoned on August 18, 2022 as part of the current LSI activities.
Quantities are reported in µg/l (parts per billion).
Results with the “<” symbol are below the laboratory method detection limits.
Bolded constituents are above the laboratory method detection limits.
Shaded constituents are above NCDEQ’s 2L Groundwater Quality Standards.
Constituents in the table in red are above Gross Contamination Levels for Groundwater, if applicable.
Multiple constituents analyzed below the laboratory’s method detection limits in the groundwater samples are not listed in the above table.
Where “J” flags are noted behind lab data, the lab provided an estimated concentration of a target contaminant above the adjusted method detection limit and below the adjusted reporting limit.
NE = a level is not currently established by NCDEQ.

Appendix C
Boring Logs

POORLY GRADED SAND WITH SILT (SP-SM), brown, orange, gray and light tan
SILTY SAND (SM), orange
Boring Terminated at 8 Feet
6.0
8.0
0.0
0.0
0.0
0.0
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-1
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
POORLY GRADED SAND WITH SILT (SP-SM), brown
Boring Terminated at 8 Feet
4.0
8.0
0.0
0.0
Noreturn
Noreturn
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-2
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
SILTY SAND (SM), dark gray
Boring Terminated at 8 Feet
4.0
8.0
14.3
55.3
Noreturn
Noreturn
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-3
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
SILTY SAND (SM), dark gray to gray
Boring Terminated at 8 Feet
4.0
8.0
0.0
0.0
Noreturn
Noreturn
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-4
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
POORLY GRADED SAND WITH SILT (SP-SM), brown and orange
SILTY SAND (SM), tannish brown and gray to dark gray
CLAYEY SAND (SC), light gray and orange
Boring Terminated at 8 Feet
2.0
6.0
8.0
0.0
0.0
0.0
0.0
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-5
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
POORLY GRADED SAND WITH SILT (SP-SM), orange, gray and light tan
SILTY CLAYEY SAND (SC), orange and light gray
Boring Terminated at 8 Feet
6.0
8.0
0.0
0.0
0.0
0.0
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-6
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
POORLY GRADED SAND WITH SILT (SP-SM), brown and orange
Boring Terminated at 8 Feet
4.0
8.0
1.8
15.6
Noreturn
Noreturn
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-7
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
POORLY GRADED SAND WITH SILT (SP-SM), brown
SILTY SAND (SM), dark gray
Boring Terminated at 8 Feet
2.0
4.0
8.0
0.0
104
Noreturn
Noreturn
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 9/2/22DEPTH (Ft.)1
2
3
4
5
6
7
8 WATER LEVELOBSERVATIONSLOCATION
Latitude: 34.8888° Longitude: -75.9208°GRAPHIC LOGDEPTH PIDReadings 407 W. Main Street
Havelock, NC, NC
SITE:
Page 1 of 1
Advancement Method:
Abandonment Method:Boring backfilled with bentonite and sand upon completion,and capped with asphalt patch.
Notes:
Project No.: 72227070
Drill Rig: Geoprobe
Boring Started: 08-18-2022
BORING LOG NO. B-8
Cathy BayerCLIENT:PO Box 436; Havelock, NC
Driller: EHC, Inc.
Boring Completed: 08-18-2022
PROJECT: Bayer Property
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE

Appendix D
Laboratory Analytical Reports

#=CL#
September 01, 2022
LIMS USE: FR - ALLEN MCCOLL
LIMS OBJECT ID: 92621510
92621510
Project:
Pace Project No.:
RE:
Mr. Allen McColl
Terracon
314 Beacon Drive
Winterville, NC 28590
BAYER PROPERTY 72227070
Dear Mr. McColl:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
A revised report is being issued on 9/1/22 to include J flags per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 76
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 76
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Lab ID Sample ID Matrix Date Collected Date Received
92621510001 B-1 SOIL Solid 08/18/22 10:59 08/19/22 09:50
92621510002 B-2 SOIL Solid 08/18/22 10:45 08/19/22 09:50
92621510003 B-3 SOIL Solid 08/18/22 12:22 08/19/22 09:50
92621510004 B-4 SOIL Solid 08/18/22 13:05 08/19/22 09:50
92621510005 B-5 SOIL Solid 08/18/22 13:35 08/19/22 09:50
92621510006 B-6 SOIL Solid 08/18/22 13:22 08/19/22 09:50
92621510007 B-7 SOIL Solid 08/18/22 12:06 08/19/22 09:50
92621510008 B-8 SOIL Solid 08/18/22 11:56 08/19/22 09:50
92621510009 MW-1 Water 08/18/22 11:15 08/19/22 09:50
92621510010 B-2 GW Water 08/18/22 11:38 08/19/22 09:50
92621510011 B-3 GW Water 08/18/22 12:55 08/19/22 09:50
92621510012 B-5 GW Water 08/18/22 13:55 08/19/22 09:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 76
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92621510001 B-1 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510002 B-2 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510003 B-3 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510004 B-4 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510005 B-5 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510006 B-6 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510007 B-7 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510008 B-8 SOIL EPA 8270E 21 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92621510009 MW-1 EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CGAW
92621510010 B-2 GW EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CGAW
92621510011 B-3 GW EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CGAW
92621510012 B-5 GW EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-1 SOIL Lab ID:92621510001 Collected:08/18/22 10:59 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 17:48 83-32-908/20/22 03:053711301
Acenaphthylene ND ug/kg 08/23/22 17:48 208-96-808/20/22 03:053711301
Anthracene ND ug/kg 08/23/22 17:48 120-12-708/20/22 03:053711211
Benzo(a)anthracene ND ug/kg 08/23/22 17:48 56-55-308/20/22 03:053711241
Benzo(a)pyrene ND ug/kg 08/23/22 17:48 50-32-808/20/22 03:053711281
Benzo(b)fluoranthene ND ug/kg 08/23/22 17:48 205-99-208/20/22 03:053711241
Benzo(g,h,i)perylene ND ug/kg 08/23/22 17:48 191-24-208/20/22 03:053711441
Benzo(k)fluoranthene ND ug/kg 08/23/22 17:48 207-08-908/20/22 03:053711301
Chrysene ND ug/kg 08/23/22 17:48 218-01-908/20/22 03:053711351
Dibenz(a,h)anthracene ND ug/kg 08/23/22 17:48 53-70-308/20/22 03:053711431
Fluoranthene ND ug/kg 08/23/22 17:48 206-44-008/20/22 03:053711271
Fluorene ND ug/kg 08/23/22 17:48 86-73-708/20/22 03:053711301
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 17:48 193-39-508/20/22 03:053711461
1-Methylnaphthalene ND ug/kg 08/23/22 17:48 90-12-008/20/22 03:053711301
2-Methylnaphthalene ND ug/kg 08/23/22 17:48 91-57-608/20/22 03:053711481
Naphthalene ND ug/kg 08/23/22 17:48 91-20-308/20/22 03:053711261
Phenanthrene ND ug/kg 08/23/22 17:48 85-01-808/20/22 03:053711211
Pyrene ND ug/kg 08/23/22 17:48 129-00-008/20/22 03:053711511
Surrogates
Nitrobenzene-d5 (S)61 %08/23/22 17:48 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)63 %08/23/22 17:48 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)71 %08/23/22 17:48 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 20:10 67-64-108/19/22 15:4912840.9 1
Benzene ND ug/kg 08/19/22 20:10 71-43-208/19/22 15:496.4 2.5 1
Bromobenzene ND ug/kg 08/19/22 20:10 108-86-108/19/22 15:496.4 2.1 1
Bromochloromethane ND ug/kg 08/19/22 20:10 74-97-508/19/22 15:496.4 1.9 1
Bromodichloromethane ND ug/kg 08/19/22 20:10 75-27-408/19/22 15:496.4 2.5 1
Bromoform ND ug/kg 08/19/22 20:10 75-25-208/19/22 15:496.4 2.2 1
Bromomethane ND ug/kg 08/19/22 20:10 74-83-908/19/22 15:4912.8 10.1 1
2-Butanone (MEK)ND ug/kg 08/19/22 20:10 78-93-308/19/22 15:4912830.6 1
n-Butylbenzene ND ug/kg 08/19/22 20:10 104-51-808/19/22 15:496.4 3.0 1
sec-Butylbenzene ND ug/kg 08/19/22 20:10 135-98-808/19/22 15:496.4 2.8 1
tert-Butylbenzene ND ug/kg 08/19/22 20:10 98-06-608/19/22 15:496.4 2.3 1
Carbon tetrachloride ND ug/kg 08/19/22 20:10 56-23-508/19/22 15:496.4 2.4 1
Chlorobenzene ND ug/kg 08/19/22 20:10 108-90-708/19/22 15:496.4 1.2 1
Chloroethane ND ug/kg 08/19/22 20:10 75-00-308/19/22 15:4912.8 4.9 1
Chloroform ND ug/kg 08/19/22 20:10 67-66-308/19/22 15:496.4 3.9 1
Chloromethane ND ug/kg 08/19/22 20:10 74-87-308/19/22 15:4912.8 5.4 1
2-Chlorotoluene ND ug/kg 08/19/22 20:10 95-49-808/19/22 15:496.4 2.3 1
4-Chlorotoluene ND ug/kg 08/19/22 20:10 106-43-408/19/22 15:496.4 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 20:10 96-12-8 M108/19/22 15:496.4 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-1 SOIL Lab ID:92621510001 Collected:08/18/22 10:59 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 20:10 124-48-108/19/22 15:496.4 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 20:10 106-93-408/19/22 15:496.4 2.8 1
Dibromomethane ND ug/kg 08/19/22 20:10 74-95-308/19/22 15:496.4 1.4 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 20:10 95-50-108/19/22 15:496.4 2.3 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 20:10 541-73-108/19/22 15:496.4 2.0 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 20:10 106-46-708/19/22 15:496.4 1.7 1
Dichlorodifluoromethane ND ug/kg 08/19/22 20:10 75-71-8 IH08/19/22 15:4912.8 2.8 1
1,1-Dichloroethane ND ug/kg 08/19/22 20:10 75-34-308/19/22 15:496.4 2.6 1
1,2-Dichloroethane ND ug/kg 08/19/22 20:10 107-06-208/19/22 15:496.4 4.2 1
1,1-Dichloroethene ND ug/kg 08/19/22 20:10 75-35-408/19/22 15:496.4 2.6 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 20:10 156-59-208/19/22 15:496.4 2.2 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 20:10 156-60-508/19/22 15:496.4 2.2 1
1,2-Dichloropropane ND ug/kg 08/19/22 20:10 78-87-508/19/22 15:496.4 1.9 1
1,3-Dichloropropane ND ug/kg 08/19/22 20:10 142-28-908/19/22 15:496.4 2.0 1
2,2-Dichloropropane ND ug/kg 08/19/22 20:10 594-20-708/19/22 15:496.4 2.1 1
1,1-Dichloropropene ND ug/kg 08/19/22 20:10 563-58-608/19/22 15:496.4 3.1 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 20:10 10061-01-508/19/22 15:496.4 1.7 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 20:10 10061-02-608/19/22 15:496.4 2.2 1
Diisopropyl ether ND ug/kg 08/19/22 20:10 108-20-308/19/22 15:496.4 1.7 1
Ethylbenzene ND ug/kg 08/19/22 20:10 100-41-408/19/22 15:496.4 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 20:10 87-68-308/19/22 15:4912.8 10.4 1
2-Hexanone ND ug/kg 08/19/22 20:10 591-78-608/19/22 15:4963.8 6.1 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 20:10 98-82-808/19/22 15:496.4 2.2 1
p-Isopropyltoluene ND ug/kg 08/19/22 20:10 99-87-608/19/22 15:496.4 3.1 1
Methylene Chloride ND ug/kg 08/19/22 20:10 75-09-208/19/22 15:4925.5 17.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 20:10 108-10-108/19/22 15:4963.8 6.1 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 20:10 1634-04-408/19/22 15:496.4 2.4 1
Naphthalene ND ug/kg 08/19/22 20:10 91-20-3 M108/19/22 15:496.4 3.4 1
n-Propylbenzene ND ug/kg 08/19/22 20:10 103-65-108/19/22 15:496.4 2.3 1
Styrene ND ug/kg 08/19/22 20:10 100-42-508/19/22 15:496.4 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 20:10 630-20-608/19/22 15:496.4 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 20:10 79-34-508/19/22 15:496.4 1.7 1
Tetrachloroethene ND ug/kg 08/19/22 20:10 127-18-408/19/22 15:496.4 2.0 1
Toluene 14.9 ug/kg 08/19/22 20:10 108-88-308/19/22 15:496.4 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 20:10 87-61-6 M108/19/22 15:496.4 5.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 20:10 120-82-1 M108/19/22 15:496.4 5.4 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 20:10 71-55-608/19/22 15:496.4 3.3 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 20:10 79-00-508/19/22 15:496.4 2.1 1
Trichloroethene 3.8J ug/kg 08/19/22 20:10 79-01-608/19/22 15:496.4 1.6 1
Trichlorofluoromethane ND ug/kg 08/19/22 20:10 75-69-408/19/22 15:496.4 3.5 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 20:10 96-18-408/19/22 15:496.4 3.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 20:10 95-63-608/19/22 15:496.4 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 20:10 108-67-808/19/22 15:496.4 2.1 1
Vinyl acetate ND ug/kg 08/19/22 20:10 108-05-408/19/22 15:4963.8 4.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-1 SOIL Lab ID:92621510001 Collected:08/18/22 10:59 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 20:10 75-01-408/19/22 15:4912.8 3.2 1
Xylene (Total)6.8J ug/kg 08/19/22 20:10 1330-20-708/19/22 15:4912.8 3.6 1
m&p-Xylene ND ug/kg 08/19/22 20:10 179601-23-108/19/22 15:4912.8 4.4 1
o-Xylene 6.8 ug/kg 08/19/22 20:10 95-47-608/19/22 15:496.4 2.8 1
Surrogates
Toluene-d8 (S)100 %08/19/22 20:10 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)101 %08/19/22 20:10 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)101 %08/19/22 20:10 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.0 %08/22/22 15:40 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-2 SOIL Lab ID:92621510002 Collected:08/18/22 10:45 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 18:16 83-32-908/20/22 03:053651281
Acenaphthylene ND ug/kg 08/23/22 18:16 208-96-808/20/22 03:053651281
Anthracene ND ug/kg 08/23/22 18:16 120-12-708/20/22 03:053651191
Benzo(a)anthracene ND ug/kg 08/23/22 18:16 56-55-308/20/22 03:053651221
Benzo(a)pyrene ND ug/kg 08/23/22 18:16 50-32-808/20/22 03:053651261
Benzo(b)fluoranthene ND ug/kg 08/23/22 18:16 205-99-208/20/22 03:053651221
Benzo(g,h,i)perylene ND ug/kg 08/23/22 18:16 191-24-208/20/22 03:053651421
Benzo(k)fluoranthene ND ug/kg 08/23/22 18:16 207-08-908/20/22 03:053651281
Chrysene ND ug/kg 08/23/22 18:16 218-01-908/20/22 03:053651331
Dibenz(a,h)anthracene ND ug/kg 08/23/22 18:16 53-70-308/20/22 03:053651401
Fluoranthene ND ug/kg 08/23/22 18:16 206-44-008/20/22 03:053651251
Fluorene ND ug/kg 08/23/22 18:16 86-73-708/20/22 03:053651281
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 18:16 193-39-508/20/22 03:053651441
1-Methylnaphthalene ND ug/kg 08/23/22 18:16 90-12-008/20/22 03:053651281
2-Methylnaphthalene ND ug/kg 08/23/22 18:16 91-57-608/20/22 03:053651461
Naphthalene ND ug/kg 08/23/22 18:16 91-20-308/20/22 03:053651241
Phenanthrene ND ug/kg 08/23/22 18:16 85-01-808/20/22 03:053651191
Pyrene ND ug/kg 08/23/22 18:16 129-00-008/20/22 03:053651481
Surrogates
Nitrobenzene-d5 (S)59 %08/23/22 18:16 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)60 %08/23/22 18:16 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)66 %08/23/22 18:16 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 20:27 67-64-108/19/22 15:4912138.7 1
Benzene ND ug/kg 08/19/22 20:27 71-43-208/19/22 15:496.0 2.4 1
Bromobenzene ND ug/kg 08/19/22 20:27 108-86-108/19/22 15:496.0 2.0 1
Bromochloromethane ND ug/kg 08/19/22 20:27 74-97-508/19/22 15:496.0 1.8 1
Bromodichloromethane ND ug/kg 08/19/22 20:27 75-27-408/19/22 15:496.0 2.3 1
Bromoform ND ug/kg 08/19/22 20:27 75-25-208/19/22 15:496.0 2.1 1
Bromomethane ND ug/kg 08/19/22 20:27 74-83-908/19/22 15:4912.1 9.5 1
2-Butanone (MEK)ND ug/kg 08/19/22 20:27 78-93-308/19/22 15:4912129.0 1
n-Butylbenzene ND ug/kg 08/19/22 20:27 104-51-808/19/22 15:496.0 2.8 1
sec-Butylbenzene ND ug/kg 08/19/22 20:27 135-98-808/19/22 15:496.0 2.7 1
tert-Butylbenzene ND ug/kg 08/19/22 20:27 98-06-608/19/22 15:496.0 2.1 1
Carbon tetrachloride ND ug/kg 08/19/22 20:27 56-23-508/19/22 15:496.0 2.3 1
Chlorobenzene ND ug/kg 08/19/22 20:27 108-90-708/19/22 15:496.0 1.2 1
Chloroethane ND ug/kg 08/19/22 20:27 75-00-308/19/22 15:4912.1 4.7 1
Chloroform ND ug/kg 08/19/22 20:27 67-66-308/19/22 15:496.0 3.7 1
Chloromethane ND ug/kg 08/19/22 20:27 74-87-308/19/22 15:4912.1 5.1 1
2-Chlorotoluene ND ug/kg 08/19/22 20:27 95-49-808/19/22 15:496.0 2.1 1
4-Chlorotoluene ND ug/kg 08/19/22 20:27 106-43-408/19/22 15:496.0 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 20:27 96-12-808/19/22 15:496.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-2 SOIL Lab ID:92621510002 Collected:08/18/22 10:45 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 20:27 124-48-108/19/22 15:496.0 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 20:27 106-93-408/19/22 15:496.0 2.7 1
Dibromomethane ND ug/kg 08/19/22 20:27 74-95-308/19/22 15:496.0 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 20:27 95-50-108/19/22 15:496.0 2.2 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 20:27 541-73-108/19/22 15:496.0 1.9 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 20:27 106-46-708/19/22 15:496.0 1.6 1
Dichlorodifluoromethane ND ug/kg 08/19/22 20:27 75-71-8 IH08/19/22 15:4912.1 2.6 1
1,1-Dichloroethane ND ug/kg 08/19/22 20:27 75-34-308/19/22 15:496.0 2.5 1
1,2-Dichloroethane ND ug/kg 08/19/22 20:27 107-06-208/19/22 15:496.0 4.0 1
1,1-Dichloroethene ND ug/kg 08/19/22 20:27 75-35-408/19/22 15:496.0 2.5 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 20:27 156-59-208/19/22 15:496.0 2.1 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 20:27 156-60-508/19/22 15:496.0 2.1 1
1,2-Dichloropropane ND ug/kg 08/19/22 20:27 78-87-508/19/22 15:496.0 1.8 1
1,3-Dichloropropane ND ug/kg 08/19/22 20:27 142-28-908/19/22 15:496.0 1.9 1
2,2-Dichloropropane ND ug/kg 08/19/22 20:27 594-20-708/19/22 15:496.0 2.0 1
1,1-Dichloropropene ND ug/kg 08/19/22 20:27 563-58-608/19/22 15:496.0 2.9 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 20:27 10061-01-508/19/22 15:496.0 1.6 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 20:27 10061-02-608/19/22 15:496.0 2.1 1
Diisopropyl ether ND ug/kg 08/19/22 20:27 108-20-308/19/22 15:496.0 1.6 1
Ethylbenzene ND ug/kg 08/19/22 20:27 100-41-408/19/22 15:496.0 2.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 20:27 87-68-308/19/22 15:4912.1 9.9 1
2-Hexanone ND ug/kg 08/19/22 20:27 591-78-608/19/22 15:4960.3 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 20:27 98-82-808/19/22 15:496.0 2.1 1
p-Isopropyltoluene ND ug/kg 08/19/22 20:27 99-87-608/19/22 15:496.0 3.0 1
Methylene Chloride ND ug/kg 08/19/22 20:27 75-09-208/19/22 15:4924.1 16.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 20:27 108-10-108/19/22 15:4960.3 5.8 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 20:27 1634-04-408/19/22 15:496.0 2.3 1
Naphthalene ND ug/kg 08/19/22 20:27 91-20-308/19/22 15:496.0 3.2 1
n-Propylbenzene ND ug/kg 08/19/22 20:27 103-65-108/19/22 15:496.0 2.1 1
Styrene ND ug/kg 08/19/22 20:27 100-42-508/19/22 15:496.0 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 20:27 630-20-608/19/22 15:496.0 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 20:27 79-34-508/19/22 15:496.0 1.6 1
Tetrachloroethene ND ug/kg 08/19/22 20:27 127-18-408/19/22 15:496.0 1.9 1
Toluene 6.2 ug/kg 08/19/22 20:27 108-88-308/19/22 15:496.0 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 20:27 87-61-608/19/22 15:496.0 4.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 20:27 120-82-108/19/22 15:496.0 5.1 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 20:27 71-55-608/19/22 15:496.0 3.1 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 20:27 79-00-508/19/22 15:496.0 2.0 1
Trichloroethene ND ug/kg 08/19/22 20:27 79-01-608/19/22 15:496.0 1.6 1
Trichlorofluoromethane ND ug/kg 08/19/22 20:27 75-69-408/19/22 15:496.0 3.3 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 20:27 96-18-408/19/22 15:496.0 3.1 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 20:27 95-63-608/19/22 15:496.0 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 20:27 108-67-808/19/22 15:496.0 2.0 1
Vinyl acetate ND ug/kg 08/19/22 20:27 108-05-408/19/22 15:4960.3 4.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-2 SOIL Lab ID:92621510002 Collected:08/18/22 10:45 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 20:27 75-01-408/19/22 15:4912.1 3.1 1
Xylene (Total)6.9J ug/kg 08/19/22 20:27 1330-20-708/19/22 15:4912.1 3.4 1
m&p-Xylene ND ug/kg 08/19/22 20:27 179601-23-108/19/22 15:4912.1 4.1 1
o-Xylene 6.9 ug/kg 08/19/22 20:27 95-47-608/19/22 15:496.0 2.7 1
Surrogates
Toluene-d8 (S)101 %08/19/22 20:27 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)101 %08/19/22 20:27 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)99 %08/19/22 20:27 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.9 %08/22/22 15:40 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-3 SOIL Lab ID:92621510003 Collected:08/18/22 12:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/24/22 10:52 83-32-908/20/22 03:053910137010
Acenaphthylene ND ug/kg 08/24/22 10:52 208-96-808/20/22 03:053910137010
Anthracene ND ug/kg 08/24/22 10:52 120-12-708/20/22 03:053910128010
Benzo(a)anthracene ND ug/kg 08/24/22 10:52 56-55-308/20/22 03:053910130010
Benzo(a)pyrene ND ug/kg 08/24/22 10:52 50-32-808/20/22 03:053910135010
Benzo(b)fluoranthene ND ug/kg 08/24/22 10:52 205-99-208/20/22 03:053910130010
Benzo(g,h,i)perylene ND ug/kg 08/24/22 10:52 191-24-208/20/22 03:053910151010
Benzo(k)fluoranthene ND ug/kg 08/24/22 10:52 207-08-908/20/22 03:053910137010
Chrysene ND ug/kg 08/24/22 10:52 218-01-908/20/22 03:053910142010
Dibenz(a,h)anthracene ND ug/kg 08/24/22 10:52 53-70-308/20/22 03:053910150010
Fluoranthene ND ug/kg 08/24/22 10:52 206-44-008/20/22 03:053910134010
Fluorene ND ug/kg 08/24/22 10:52 86-73-708/20/22 03:053910137010
Indeno(1,2,3-cd)pyrene ND ug/kg 08/24/22 10:52 193-39-508/20/22 03:053910154010
1-Methylnaphthalene 3680J ug/kg 08/24/22 10:52 90-12-008/20/22 03:053910137010
2-Methylnaphthalene 5010 ug/kg 08/24/22 10:52 91-57-608/20/22 03:053910156010
Naphthalene 1420J ug/kg 08/24/22 10:52 91-20-308/20/22 03:053910133010
Phenanthrene ND ug/kg 08/24/22 10:52 85-01-808/20/22 03:053910128010
Pyrene ND ug/kg 08/24/22 10:52 129-00-008/20/22 03:053910159010
Surrogates
Nitrobenzene-d5 (S)0 %08/24/22 10:52 4165-60-0 D3,S408/20/22 03:0521-130 10
2-Fluorobiphenyl (S)0 %08/24/22 10:52 321-60-8 S408/20/22 03:0519-130 10
Terphenyl-d14 (S)0 %08/24/22 10:52 1718-51-0 S408/20/22 03:0515-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/22/22 21:44 67-64-108/22/22 12:5326484.7 2
Benzene 11.0J ug/kg 08/22/22 21:44 71-43-208/22/22 12:5313.2 5.2 2
Bromobenzene ND ug/kg 08/22/22 21:44 108-86-108/22/22 12:5313.2 4.3 2
Bromochloromethane ND ug/kg 08/22/22 21:44 74-97-508/22/22 12:5313.2 3.9 2
Bromodichloromethane ND ug/kg 08/22/22 21:44 75-27-408/22/22 12:5313.2 5.1 2
Bromoform ND ug/kg 08/22/22 21:44 75-25-208/22/22 12:5313.2 4.6 2
Bromomethane ND ug/kg 08/22/22 21:44 74-83-908/22/22 12:5326.4 20.8 2
2-Butanone (MEK)101J ug/kg 08/22/22 21:44 78-93-308/22/22 12:5326463.3 2
n-Butylbenzene ND ug/kg 08/22/22 21:44 104-51-808/22/22 12:5313.2 6.2 2
sec-Butylbenzene ND ug/kg 08/22/22 21:44 135-98-808/22/22 12:5313.2 5.8 2
tert-Butylbenzene ND ug/kg 08/22/22 21:44 98-06-608/22/22 12:5313.2 4.7 2
Carbon tetrachloride ND ug/kg 08/22/22 21:44 56-23-508/22/22 12:5313.2 4.9 2
Chlorobenzene ND ug/kg 08/22/22 21:44 108-90-708/22/22 12:5313.2 2.5 2
Chloroethane ND ug/kg 08/22/22 21:44 75-00-308/22/22 12:5326.4 10.2 2
Chloroform ND ug/kg 08/22/22 21:44 67-66-308/22/22 12:5313.2 8.0 2
Chloromethane ND ug/kg 08/22/22 21:44 74-87-308/22/22 12:5326.4 11.1 2
2-Chlorotoluene ND ug/kg 08/22/22 21:44 95-49-808/22/22 12:5313.2 4.7 2
4-Chlorotoluene ND ug/kg 08/22/22 21:44 106-43-408/22/22 12:5313.2 2.3 2
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/22 21:44 96-12-808/22/22 12:5313.2 5.1 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-3 SOIL Lab ID:92621510003 Collected:08/18/22 12:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/22/22 21:44 124-48-108/22/22 12:5313.2 7.4 2
1,2-Dibromoethane (EDB)ND ug/kg 08/22/22 21:44 106-93-408/22/22 12:5313.2 5.8 2
Dibromomethane ND ug/kg 08/22/22 21:44 74-95-308/22/22 12:5313.2 2.8 2
1,2-Dichlorobenzene ND ug/kg 08/22/22 21:44 95-50-108/22/22 12:5313.2 4.7 2
1,3-Dichlorobenzene ND ug/kg 08/22/22 21:44 541-73-108/22/22 12:5313.2 4.1 2
1,4-Dichlorobenzene ND ug/kg 08/22/22 21:44 106-46-708/22/22 12:5313.2 3.4 2
Dichlorodifluoromethane ND ug/kg 08/22/22 21:44 75-71-8 IH,L1,
v1
08/22/22 12:5326.4 5.7 2
1,1-Dichloroethane ND ug/kg 08/22/22 21:44 75-34-308/22/22 12:5313.2 5.4 2
1,2-Dichloroethane ND ug/kg 08/22/22 21:44 107-06-208/22/22 12:5313.2 8.7 2
1,1-Dichloroethene ND ug/kg 08/22/22 21:44 75-35-408/22/22 12:5313.2 5.4 2
cis-1,2-Dichloroethene ND ug/kg 08/22/22 21:44 156-59-208/22/22 12:5313.2 4.5 2
trans-1,2-Dichloroethene ND ug/kg 08/22/22 21:44 156-60-508/22/22 12:5313.2 4.6 2
1,2-Dichloropropane ND ug/kg 08/22/22 21:44 78-87-508/22/22 12:5313.2 4.0 2
1,3-Dichloropropane ND ug/kg 08/22/22 21:44 142-28-908/22/22 12:5313.2 4.1 2
2,2-Dichloropropane ND ug/kg 08/22/22 21:44 594-20-708/22/22 12:5313.2 4.3 2
1,1-Dichloropropene ND ug/kg 08/22/22 21:44 563-58-608/22/22 12:5313.2 6.3 2
cis-1,3-Dichloropropene ND ug/kg 08/22/22 21:44 10061-01-508/22/22 12:5313.2 3.6 2
trans-1,3-Dichloropropene ND ug/kg 08/22/22 21:44 10061-02-608/22/22 12:5313.2 4.5 2
Diisopropyl ether ND ug/kg 08/22/22 21:44 108-20-308/22/22 12:5313.2 3.6 2
Ethylbenzene 289 ug/kg 08/22/22 21:44 100-41-408/22/22 12:5313.2 6.1 2
Hexachloro-1,3-butadiene ND ug/kg 08/22/22 21:44 87-68-308/22/22 12:5326.4 21.6 2
2-Hexanone ND ug/kg 08/22/22 21:44 591-78-608/22/22 12:5313212.7 2
Isopropylbenzene (Cumene)216 ug/kg 08/22/22 21:44 98-82-808/22/22 12:5313.2 4.5 2
p-Isopropyltoluene 1570 ug/kg 08/22/22 21:44 99-87-608/22/22 12:5313.2 6.5 2
Methylene Chloride 41.2J ug/kg 08/22/22 21:44 75-09-208/22/22 12:5352.8 36.1 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/22 21:44 108-10-108/22/22 12:5313212.7 2
Methyl-tert-butyl ether ND ug/kg 08/22/22 21:44 1634-04-408/22/22 12:5313.2 4.9 2
Naphthalene 2490 ug/kg 08/22/22 21:44 91-20-308/22/22 12:5313.2 6.9 2
n-Propylbenzene ND ug/kg 08/22/22 21:44 103-65-108/22/22 12:5313.2 4.7 2
Styrene ND ug/kg 08/22/22 21:44 100-42-508/22/22 12:5313.2 3.5 2
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/22 21:44 630-20-608/22/22 12:5313.2 5.1 2
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/22 21:44 79-34-508/22/22 12:5313.2 3.5 2
Tetrachloroethene ND ug/kg 08/22/22 21:44 127-18-408/22/22 12:5313.2 4.2 2
Toluene 110 ug/kg 08/22/22 21:44 108-88-308/22/22 12:5313.2 3.7 2
1,2,3-Trichlorobenzene ND ug/kg 08/22/22 21:44 87-61-608/22/22 12:5313.2 10.7 2
1,2,4-Trichlorobenzene ND ug/kg 08/22/22 21:44 120-82-108/22/22 12:5313.2 11.1 2
1,1,1-Trichloroethane ND ug/kg 08/22/22 21:44 71-55-608/22/22 12:5313.2 6.9 2
1,1,2-Trichloroethane ND ug/kg 08/22/22 21:44 79-00-508/22/22 12:5313.2 4.4 2
Trichloroethene ND ug/kg 08/22/22 21:44 79-01-608/22/22 12:5313.2 3.4 2
Trichlorofluoromethane ND ug/kg 08/22/22 21:44 75-69-408/22/22 12:5313.2 7.3 2
1,2,3-Trichloropropane ND ug/kg 08/22/22 21:44 96-18-408/22/22 12:5313.2 6.7 2
1,2,4-Trimethylbenzene 3760 ug/kg 08/22/22 21:44 95-63-608/22/22 12:5313.2 3.6 2
1,3,5-Trimethylbenzene ND ug/kg 08/22/22 21:44 108-67-808/22/22 12:5313.2 4.4 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-3 SOIL Lab ID:92621510003 Collected:08/18/22 12:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl acetate ND ug/kg 08/22/22 21:44 108-05-408/22/22 12:531329.6 2
Vinyl chloride ND ug/kg 08/22/22 21:44 75-01-408/22/22 12:5326.4 6.7 2
Xylene (Total)1370 ug/kg 08/22/22 21:44 1330-20-708/22/22 12:5326.4 7.5 2
m&p-Xylene 629 ug/kg 08/22/22 21:44 179601-23-108/22/22 12:5326.4 9.0 2
o-Xylene 737 ug/kg 08/22/22 21:44 95-47-608/22/22 12:5313.2 5.8 2
Surrogates
Toluene-d8 (S)99 %08/22/22 21:44 2037-26-508/22/22 12:5370-130 2
4-Bromofluorobenzene (S)133 %08/22/22 21:44 460-00-4 S208/22/22 12:5370-130 2
1,2-Dichloroethane-d4 (S)99 %08/22/22 21:44 17060-07-008/22/22 12:5370-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.3 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-4 SOIL Lab ID:92621510004 Collected:08/18/22 13:05 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 19:12 83-32-908/20/22 03:054091441
Acenaphthylene ND ug/kg 08/23/22 19:12 208-96-808/20/22 03:054091441
Anthracene ND ug/kg 08/23/22 19:12 120-12-708/20/22 03:054091341
Benzo(a)anthracene ND ug/kg 08/23/22 19:12 56-55-308/20/22 03:054091361
Benzo(a)pyrene ND ug/kg 08/23/22 19:12 50-32-808/20/22 03:054091411
Benzo(b)fluoranthene ND ug/kg 08/23/22 19:12 205-99-208/20/22 03:054091361
Benzo(g,h,i)perylene ND ug/kg 08/23/22 19:12 191-24-208/20/22 03:054091591
Benzo(k)fluoranthene ND ug/kg 08/23/22 19:12 207-08-908/20/22 03:054091441
Chrysene ND ug/kg 08/23/22 19:12 218-01-908/20/22 03:054091491
Dibenz(a,h)anthracene ND ug/kg 08/23/22 19:12 53-70-308/20/22 03:054091571
Fluoranthene ND ug/kg 08/23/22 19:12 206-44-008/20/22 03:054091401
Fluorene ND ug/kg 08/23/22 19:12 86-73-708/20/22 03:054091441
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 19:12 193-39-508/20/22 03:054091611
1-Methylnaphthalene ND ug/kg 08/23/22 19:12 90-12-008/20/22 03:054091441
2-Methylnaphthalene ND ug/kg 08/23/22 19:12 91-57-608/20/22 03:054091631
Naphthalene ND ug/kg 08/23/22 19:12 91-20-308/20/22 03:054091391
Phenanthrene ND ug/kg 08/23/22 19:12 85-01-808/20/22 03:054091341
Pyrene ND ug/kg 08/23/22 19:12 129-00-008/20/22 03:054091661
Surrogates
Nitrobenzene-d5 (S)59 %08/23/22 19:12 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)41 %08/23/22 19:12 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)37 %08/23/22 19:12 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 21:03 67-64-108/19/22 15:4917054.6 1
Benzene ND ug/kg 08/19/22 21:03 71-43-208/19/22 15:498.5 3.4 1
Bromobenzene ND ug/kg 08/19/22 21:03 108-86-108/19/22 15:498.5 2.8 1
Bromochloromethane ND ug/kg 08/19/22 21:03 74-97-508/19/22 15:498.5 2.5 1
Bromodichloromethane ND ug/kg 08/19/22 21:03 75-27-408/19/22 15:498.5 3.3 1
Bromoform ND ug/kg 08/19/22 21:03 75-25-208/19/22 15:498.5 3.0 1
Bromomethane ND ug/kg 08/19/22 21:03 74-83-908/19/22 15:4917.0 13.4 1
2-Butanone (MEK)ND ug/kg 08/19/22 21:03 78-93-308/19/22 15:4917040.8 1
n-Butylbenzene ND ug/kg 08/19/22 21:03 104-51-808/19/22 15:498.5 4.0 1
sec-Butylbenzene ND ug/kg 08/19/22 21:03 135-98-808/19/22 15:498.5 3.7 1
tert-Butylbenzene ND ug/kg 08/19/22 21:03 98-06-608/19/22 15:498.5 3.0 1
Carbon tetrachloride ND ug/kg 08/19/22 21:03 56-23-508/19/22 15:498.5 3.2 1
Chlorobenzene ND ug/kg 08/19/22 21:03 108-90-708/19/22 15:498.5 1.6 1
Chloroethane ND ug/kg 08/19/22 21:03 75-00-308/19/22 15:4917.0 6.6 1
Chloroform ND ug/kg 08/19/22 21:03 67-66-308/19/22 15:498.5 5.2 1
Chloromethane ND ug/kg 08/19/22 21:03 74-87-308/19/22 15:4917.0 7.1 1
2-Chlorotoluene ND ug/kg 08/19/22 21:03 95-49-808/19/22 15:498.5 3.0 1
4-Chlorotoluene ND ug/kg 08/19/22 21:03 106-43-408/19/22 15:498.5 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 21:03 96-12-808/19/22 15:498.5 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-4 SOIL Lab ID:92621510004 Collected:08/18/22 13:05 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 21:03 124-48-108/19/22 15:498.5 4.8 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 21:03 106-93-408/19/22 15:498.5 3.7 1
Dibromomethane ND ug/kg 08/19/22 21:03 74-95-308/19/22 15:498.5 1.8 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 21:03 95-50-108/19/22 15:498.5 3.1 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 21:03 541-73-108/19/22 15:498.5 2.6 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 21:03 106-46-708/19/22 15:498.5 2.2 1
Dichlorodifluoromethane ND ug/kg 08/19/22 21:03 75-71-8 IH08/19/22 15:4917.0 3.7 1
1,1-Dichloroethane ND ug/kg 08/19/22 21:03 75-34-308/19/22 15:498.5 3.5 1
1,2-Dichloroethane ND ug/kg 08/19/22 21:03 107-06-208/19/22 15:498.5 5.6 1
1,1-Dichloroethene ND ug/kg 08/19/22 21:03 75-35-408/19/22 15:498.5 3.5 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 21:03 156-59-208/19/22 15:498.5 2.9 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 21:03 156-60-508/19/22 15:498.5 3.0 1
1,2-Dichloropropane ND ug/kg 08/19/22 21:03 78-87-508/19/22 15:498.5 2.6 1
1,3-Dichloropropane ND ug/kg 08/19/22 21:03 142-28-908/19/22 15:498.5 2.7 1
2,2-Dichloropropane ND ug/kg 08/19/22 21:03 594-20-708/19/22 15:498.5 2.8 1
1,1-Dichloropropene ND ug/kg 08/19/22 21:03 563-58-608/19/22 15:498.5 4.1 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 21:03 10061-01-508/19/22 15:498.5 2.3 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 21:03 10061-02-608/19/22 15:498.5 2.9 1
Diisopropyl ether ND ug/kg 08/19/22 21:03 108-20-308/19/22 15:498.5 2.3 1
Ethylbenzene ND ug/kg 08/19/22 21:03 100-41-408/19/22 15:498.5 4.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 21:03 87-68-308/19/22 15:4917.0 13.9 1
2-Hexanone ND ug/kg 08/19/22 21:03 591-78-608/19/22 15:4985.1 8.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 21:03 98-82-808/19/22 15:498.5 2.9 1
p-Isopropyltoluene ND ug/kg 08/19/22 21:03 99-87-608/19/22 15:498.5 4.2 1
Methylene Chloride ND ug/kg 08/19/22 21:03 75-09-208/19/22 15:4934.0 23.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 21:03 108-10-108/19/22 15:4985.1 8.2 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 21:03 1634-04-408/19/22 15:498.5 3.2 1
Naphthalene ND ug/kg 08/19/22 21:03 91-20-308/19/22 15:498.5 4.5 1
n-Propylbenzene ND ug/kg 08/19/22 21:03 103-65-108/19/22 15:498.5 3.0 1
Styrene ND ug/kg 08/19/22 21:03 100-42-508/19/22 15:498.5 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 21:03 630-20-608/19/22 15:498.5 3.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 21:03 79-34-508/19/22 15:498.5 2.2 1
Tetrachloroethene ND ug/kg 08/19/22 21:03 127-18-408/19/22 15:498.5 2.7 1
Toluene 5.1J ug/kg 08/19/22 21:03 108-88-308/19/22 15:498.5 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 21:03 87-61-608/19/22 15:498.5 6.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 21:03 120-82-108/19/22 15:498.5 7.1 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 21:03 71-55-608/19/22 15:498.5 4.4 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 21:03 79-00-508/19/22 15:498.5 2.8 1
Trichloroethene ND ug/kg 08/19/22 21:03 79-01-608/19/22 15:498.5 2.2 1
Trichlorofluoromethane ND ug/kg 08/19/22 21:03 75-69-408/19/22 15:498.5 4.7 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 21:03 96-18-408/19/22 15:498.5 4.3 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 21:03 95-63-608/19/22 15:498.5 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 21:03 108-67-808/19/22 15:498.5 2.9 1
Vinyl acetate ND ug/kg 08/19/22 21:03 108-05-408/19/22 15:4985.1 6.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-4 SOIL Lab ID:92621510004 Collected:08/18/22 13:05 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 21:03 75-01-408/19/22 15:4917.0 4.3 1
Xylene (Total)ND ug/kg 08/19/22 21:03 1330-20-708/19/22 15:4917.0 4.8 1
m&p-Xylene ND ug/kg 08/19/22 21:03 179601-23-108/19/22 15:4917.0 5.8 1
o-Xylene 7.3J ug/kg 08/19/22 21:03 95-47-608/19/22 15:498.5 3.8 1
Surrogates
Toluene-d8 (S)100 %08/19/22 21:03 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)100 %08/19/22 21:03 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)99 %08/19/22 21:03 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.0 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-5 SOIL Lab ID:92621510005 Collected:08/18/22 13:35 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 19:40 83-32-908/20/22 03:053851351
Acenaphthylene ND ug/kg 08/23/22 19:40 208-96-808/20/22 03:053851351
Anthracene ND ug/kg 08/23/22 19:40 120-12-708/20/22 03:053851261
Benzo(a)anthracene ND ug/kg 08/23/22 19:40 56-55-308/20/22 03:053851281
Benzo(a)pyrene 145J ug/kg 08/23/22 19:40 50-32-808/20/22 03:053851331
Benzo(b)fluoranthene ND ug/kg 08/23/22 19:40 205-99-208/20/22 03:053851281
Benzo(g,h,i)perylene ND ug/kg 08/23/22 19:40 191-24-208/20/22 03:053851501
Benzo(k)fluoranthene ND ug/kg 08/23/22 19:40 207-08-908/20/22 03:053851351
Chrysene ND ug/kg 08/23/22 19:40 218-01-908/20/22 03:053851401
Dibenz(a,h)anthracene ND ug/kg 08/23/22 19:40 53-70-308/20/22 03:053851481
Fluoranthene ND ug/kg 08/23/22 19:40 206-44-008/20/22 03:053851321
Fluorene ND ug/kg 08/23/22 19:40 86-73-708/20/22 03:053851351
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 19:40 193-39-508/20/22 03:053851521
1-Methylnaphthalene ND ug/kg 08/23/22 19:40 90-12-008/20/22 03:053851351
2-Methylnaphthalene ND ug/kg 08/23/22 19:40 91-57-608/20/22 03:053851541
Naphthalene ND ug/kg 08/23/22 19:40 91-20-308/20/22 03:053851311
Phenanthrene ND ug/kg 08/23/22 19:40 85-01-808/20/22 03:053851261
Pyrene ND ug/kg 08/23/22 19:40 129-00-008/20/22 03:053851571
Surrogates
Nitrobenzene-d5 (S)74 %08/23/22 19:40 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)64 %08/23/22 19:40 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)60 %08/23/22 19:40 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 21:20 67-64-108/19/22 15:4914245.6 1
Benzene ND ug/kg 08/19/22 21:20 71-43-208/19/22 15:497.1 2.8 1
Bromobenzene ND ug/kg 08/19/22 21:20 108-86-108/19/22 15:497.1 2.3 1
Bromochloromethane ND ug/kg 08/19/22 21:20 74-97-508/19/22 15:497.1 2.1 1
Bromodichloromethane ND ug/kg 08/19/22 21:20 75-27-408/19/22 15:497.1 2.7 1
Bromoform ND ug/kg 08/19/22 21:20 75-25-208/19/22 15:497.1 2.5 1
Bromomethane ND ug/kg 08/19/22 21:20 74-83-908/19/22 15:4914.2 11.2 1
2-Butanone (MEK)ND ug/kg 08/19/22 21:20 78-93-308/19/22 15:4914234.1 1
n-Butylbenzene ND ug/kg 08/19/22 21:20 104-51-808/19/22 15:497.1 3.4 1
sec-Butylbenzene ND ug/kg 08/19/22 21:20 135-98-808/19/22 15:497.1 3.1 1
tert-Butylbenzene ND ug/kg 08/19/22 21:20 98-06-608/19/22 15:497.1 2.5 1
Carbon tetrachloride ND ug/kg 08/19/22 21:20 56-23-508/19/22 15:497.1 2.7 1
Chlorobenzene ND ug/kg 08/19/22 21:20 108-90-708/19/22 15:497.1 1.4 1
Chloroethane ND ug/kg 08/19/22 21:20 75-00-308/19/22 15:4914.2 5.5 1
Chloroform ND ug/kg 08/19/22 21:20 67-66-308/19/22 15:497.1 4.3 1
Chloromethane ND ug/kg 08/19/22 21:20 74-87-308/19/22 15:4914.2 6.0 1
2-Chlorotoluene ND ug/kg 08/19/22 21:20 95-49-808/19/22 15:497.1 2.5 1
4-Chlorotoluene ND ug/kg 08/19/22 21:20 106-43-408/19/22 15:497.1 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 21:20 96-12-808/19/22 15:497.1 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-5 SOIL Lab ID:92621510005 Collected:08/18/22 13:35 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 21:20 124-48-108/19/22 15:497.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 21:20 106-93-408/19/22 15:497.1 3.1 1
Dibromomethane ND ug/kg 08/19/22 21:20 74-95-308/19/22 15:497.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 21:20 95-50-108/19/22 15:497.1 2.6 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 21:20 541-73-108/19/22 15:497.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 21:20 106-46-708/19/22 15:497.1 1.8 1
Dichlorodifluoromethane ND ug/kg 08/19/22 21:20 75-71-8 IH08/19/22 15:4914.2 3.1 1
1,1-Dichloroethane ND ug/kg 08/19/22 21:20 75-34-308/19/22 15:497.1 2.9 1
1,2-Dichloroethane ND ug/kg 08/19/22 21:20 107-06-208/19/22 15:497.1 4.7 1
1,1-Dichloroethene ND ug/kg 08/19/22 21:20 75-35-408/19/22 15:497.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 21:20 156-59-208/19/22 15:497.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 21:20 156-60-508/19/22 15:497.1 2.5 1
1,2-Dichloropropane ND ug/kg 08/19/22 21:20 78-87-508/19/22 15:497.1 2.1 1
1,3-Dichloropropane ND ug/kg 08/19/22 21:20 142-28-908/19/22 15:497.1 2.2 1
2,2-Dichloropropane ND ug/kg 08/19/22 21:20 594-20-708/19/22 15:497.1 2.3 1
1,1-Dichloropropene ND ug/kg 08/19/22 21:20 563-58-608/19/22 15:497.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 21:20 10061-01-508/19/22 15:497.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 21:20 10061-02-608/19/22 15:497.1 2.4 1
Diisopropyl ether ND ug/kg 08/19/22 21:20 108-20-308/19/22 15:497.1 1.9 1
Ethylbenzene ND ug/kg 08/19/22 21:20 100-41-408/19/22 15:497.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 21:20 87-68-308/19/22 15:4914.2 11.6 1
2-Hexanone ND ug/kg 08/19/22 21:20 591-78-608/19/22 15:4971.0 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 21:20 98-82-808/19/22 15:497.1 2.4 1
p-Isopropyltoluene ND ug/kg 08/19/22 21:20 99-87-608/19/22 15:497.1 3.5 1
Methylene Chloride ND ug/kg 08/19/22 21:20 75-09-208/19/22 15:4928.4 19.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 21:20 108-10-108/19/22 15:4971.0 6.8 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 21:20 1634-04-408/19/22 15:497.1 2.7 1
Naphthalene ND ug/kg 08/19/22 21:20 91-20-308/19/22 15:497.1 3.7 1
n-Propylbenzene ND ug/kg 08/19/22 21:20 103-65-108/19/22 15:497.1 2.5 1
Styrene ND ug/kg 08/19/22 21:20 100-42-508/19/22 15:497.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 21:20 630-20-608/19/22 15:497.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 21:20 79-34-508/19/22 15:497.1 1.9 1
Tetrachloroethene ND ug/kg 08/19/22 21:20 127-18-408/19/22 15:497.1 2.2 1
Toluene ND ug/kg 08/19/22 21:20 108-88-308/19/22 15:497.1 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 21:20 87-61-608/19/22 15:497.1 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 21:20 120-82-108/19/22 15:497.1 6.0 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 21:20 71-55-608/19/22 15:497.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 21:20 79-00-508/19/22 15:497.1 2.4 1
Trichloroethene ND ug/kg 08/19/22 21:20 79-01-608/19/22 15:497.1 1.8 1
Trichlorofluoromethane ND ug/kg 08/19/22 21:20 75-69-408/19/22 15:497.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 21:20 96-18-408/19/22 15:497.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 21:20 95-63-608/19/22 15:497.1 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 21:20 108-67-808/19/22 15:497.1 2.4 1
Vinyl acetate ND ug/kg 08/19/22 21:20 108-05-408/19/22 15:4971.0 5.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-5 SOIL Lab ID:92621510005 Collected:08/18/22 13:35 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 21:20 75-01-408/19/22 15:4914.2 3.6 1
Xylene (Total)ND ug/kg 08/19/22 21:20 1330-20-708/19/22 15:4914.2 4.0 1
m&p-Xylene ND ug/kg 08/19/22 21:20 179601-23-108/19/22 15:4914.2 4.9 1
o-Xylene ND ug/kg 08/19/22 21:20 95-47-608/19/22 15:497.1 3.1 1
Surrogates
Toluene-d8 (S)100 %08/19/22 21:20 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)100 %08/19/22 21:20 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)98 %08/19/22 21:20 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.5 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-6 SOIL Lab ID:92621510006 Collected:08/18/22 13:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 20:08 83-32-908/20/22 03:053761321
Acenaphthylene ND ug/kg 08/23/22 20:08 208-96-808/20/22 03:053761321
Anthracene ND ug/kg 08/23/22 20:08 120-12-708/20/22 03:053761231
Benzo(a)anthracene ND ug/kg 08/23/22 20:08 56-55-308/20/22 03:053761251
Benzo(a)pyrene ND ug/kg 08/23/22 20:08 50-32-808/20/22 03:053761301
Benzo(b)fluoranthene ND ug/kg 08/23/22 20:08 205-99-208/20/22 03:053761251
Benzo(g,h,i)perylene ND ug/kg 08/23/22 20:08 191-24-208/20/22 03:053761461
Benzo(k)fluoranthene ND ug/kg 08/23/22 20:08 207-08-908/20/22 03:053761321
Chrysene ND ug/kg 08/23/22 20:08 218-01-908/20/22 03:053761371
Dibenz(a,h)anthracene ND ug/kg 08/23/22 20:08 53-70-308/20/22 03:053761451
Fluoranthene ND ug/kg 08/23/22 20:08 206-44-008/20/22 03:053761291
Fluorene ND ug/kg 08/23/22 20:08 86-73-708/20/22 03:053761321
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 20:08 193-39-508/20/22 03:053761481
1-Methylnaphthalene ND ug/kg 08/23/22 20:08 90-12-008/20/22 03:053761321
2-Methylnaphthalene ND ug/kg 08/23/22 20:08 91-57-608/20/22 03:053761501
Naphthalene ND ug/kg 08/23/22 20:08 91-20-308/20/22 03:053761281
Phenanthrene ND ug/kg 08/23/22 20:08 85-01-808/20/22 03:053761231
Pyrene ND ug/kg 08/23/22 20:08 129-00-008/20/22 03:053761531
Surrogates
Nitrobenzene-d5 (S)72 %08/23/22 20:08 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)69 %08/23/22 20:08 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)60 %08/23/22 20:08 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 21:38 67-64-108/19/22 15:4911938.3 1
Benzene ND ug/kg 08/19/22 21:38 71-43-208/19/22 15:496.0 2.4 1
Bromobenzene ND ug/kg 08/19/22 21:38 108-86-108/19/22 15:496.0 1.9 1
Bromochloromethane ND ug/kg 08/19/22 21:38 74-97-508/19/22 15:496.0 1.8 1
Bromodichloromethane ND ug/kg 08/19/22 21:38 75-27-408/19/22 15:496.0 2.3 1
Bromoform ND ug/kg 08/19/22 21:38 75-25-208/19/22 15:496.0 2.1 1
Bromomethane ND ug/kg 08/19/22 21:38 74-83-908/19/22 15:4911.9 9.4 1
2-Butanone (MEK)ND ug/kg 08/19/22 21:38 78-93-308/19/22 15:4911928.6 1
n-Butylbenzene ND ug/kg 08/19/22 21:38 104-51-808/19/22 15:496.0 2.8 1
sec-Butylbenzene ND ug/kg 08/19/22 21:38 135-98-808/19/22 15:496.0 2.6 1
tert-Butylbenzene ND ug/kg 08/19/22 21:38 98-06-608/19/22 15:496.0 2.1 1
Carbon tetrachloride ND ug/kg 08/19/22 21:38 56-23-508/19/22 15:496.0 2.2 1
Chlorobenzene ND ug/kg 08/19/22 21:38 108-90-708/19/22 15:496.0 1.1 1
Chloroethane ND ug/kg 08/19/22 21:38 75-00-308/19/22 15:4911.9 4.6 1
Chloroform ND ug/kg 08/19/22 21:38 67-66-308/19/22 15:496.0 3.6 1
Chloromethane ND ug/kg 08/19/22 21:38 74-87-308/19/22 15:4911.9 5.0 1
2-Chlorotoluene ND ug/kg 08/19/22 21:38 95-49-808/19/22 15:496.0 2.1 1
4-Chlorotoluene ND ug/kg 08/19/22 21:38 106-43-408/19/22 15:496.0 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 21:38 96-12-808/19/22 15:496.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-6 SOIL Lab ID:92621510006 Collected:08/18/22 13:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 21:38 124-48-108/19/22 15:496.0 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 21:38 106-93-408/19/22 15:496.0 2.6 1
Dibromomethane ND ug/kg 08/19/22 21:38 74-95-308/19/22 15:496.0 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 21:38 95-50-108/19/22 15:496.0 2.1 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 21:38 541-73-108/19/22 15:496.0 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 21:38 106-46-708/19/22 15:496.0 1.6 1
Dichlorodifluoromethane ND ug/kg 08/19/22 21:38 75-71-8 IH08/19/22 15:4911.9 2.6 1
1,1-Dichloroethane ND ug/kg 08/19/22 21:38 75-34-308/19/22 15:496.0 2.5 1
1,2-Dichloroethane ND ug/kg 08/19/22 21:38 107-06-208/19/22 15:496.0 3.9 1
1,1-Dichloroethene ND ug/kg 08/19/22 21:38 75-35-408/19/22 15:496.0 2.5 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 21:38 156-59-208/19/22 15:496.0 2.0 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 21:38 156-60-508/19/22 15:496.0 2.1 1
1,2-Dichloropropane ND ug/kg 08/19/22 21:38 78-87-508/19/22 15:496.0 1.8 1
1,3-Dichloropropane ND ug/kg 08/19/22 21:38 142-28-908/19/22 15:496.0 1.9 1
2,2-Dichloropropane ND ug/kg 08/19/22 21:38 594-20-708/19/22 15:496.0 1.9 1
1,1-Dichloropropene ND ug/kg 08/19/22 21:38 563-58-608/19/22 15:496.0 2.9 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 21:38 10061-01-508/19/22 15:496.0 1.6 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 21:38 10061-02-608/19/22 15:496.0 2.1 1
Diisopropyl ether ND ug/kg 08/19/22 21:38 108-20-308/19/22 15:496.0 1.6 1
Ethylbenzene ND ug/kg 08/19/22 21:38 100-41-408/19/22 15:496.0 2.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 21:38 87-68-308/19/22 15:4911.9 9.8 1
2-Hexanone ND ug/kg 08/19/22 21:38 591-78-608/19/22 15:4959.7 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 21:38 98-82-808/19/22 15:496.0 2.0 1
p-Isopropyltoluene ND ug/kg 08/19/22 21:38 99-87-608/19/22 15:496.0 2.9 1
Methylene Chloride ND ug/kg 08/19/22 21:38 75-09-208/19/22 15:4923.9 16.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 21:38 108-10-108/19/22 15:4959.7 5.8 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 21:38 1634-04-408/19/22 15:496.0 2.2 1
Naphthalene ND ug/kg 08/19/22 21:38 91-20-308/19/22 15:496.0 3.1 1
n-Propylbenzene ND ug/kg 08/19/22 21:38 103-65-108/19/22 15:496.0 2.1 1
Styrene ND ug/kg 08/19/22 21:38 100-42-508/19/22 15:496.0 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 21:38 630-20-608/19/22 15:496.0 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 21:38 79-34-508/19/22 15:496.0 1.6 1
Tetrachloroethene ND ug/kg 08/19/22 21:38 127-18-408/19/22 15:496.0 1.9 1
Toluene ND ug/kg 08/19/22 21:38 108-88-308/19/22 15:496.0 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 21:38 87-61-608/19/22 15:496.0 4.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 21:38 120-82-108/19/22 15:496.0 5.0 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 21:38 71-55-608/19/22 15:496.0 3.1 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 21:38 79-00-508/19/22 15:496.0 2.0 1
Trichloroethene ND ug/kg 08/19/22 21:38 79-01-608/19/22 15:496.0 1.5 1
Trichlorofluoromethane ND ug/kg 08/19/22 21:38 75-69-408/19/22 15:496.0 3.3 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 21:38 96-18-408/19/22 15:496.0 3.0 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 21:38 95-63-608/19/22 15:496.0 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 21:38 108-67-808/19/22 15:496.0 2.0 1
Vinyl acetate ND ug/kg 08/19/22 21:38 108-05-408/19/22 15:4959.7 4.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-6 SOIL Lab ID:92621510006 Collected:08/18/22 13:22 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 21:38 75-01-408/19/22 15:4911.9 3.0 1
Xylene (Total)ND ug/kg 08/19/22 21:38 1330-20-708/19/22 15:4911.9 3.4 1
m&p-Xylene ND ug/kg 08/19/22 21:38 179601-23-108/19/22 15:4911.9 4.1 1
o-Xylene 5.9J ug/kg 08/19/22 21:38 95-47-608/19/22 15:496.0 2.6 1
Surrogates
Toluene-d8 (S)99 %08/19/22 21:38 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)100 %08/19/22 21:38 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)100 %08/19/22 21:38 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.8 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-7 SOIL Lab ID:92621510007 Collected:08/18/22 12:06 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/23/22 20:36 83-32-908/20/22 03:053991401
Acenaphthylene ND ug/kg 08/23/22 20:36 208-96-808/20/22 03:053991401
Anthracene ND ug/kg 08/23/22 20:36 120-12-708/20/22 03:053991311
Benzo(a)anthracene ND ug/kg 08/23/22 20:36 56-55-308/20/22 03:053991331
Benzo(a)pyrene ND ug/kg 08/23/22 20:36 50-32-808/20/22 03:053991381
Benzo(b)fluoranthene ND ug/kg 08/23/22 20:36 205-99-208/20/22 03:053991331
Benzo(g,h,i)perylene ND ug/kg 08/23/22 20:36 191-24-208/20/22 03:053991551
Benzo(k)fluoranthene ND ug/kg 08/23/22 20:36 207-08-908/20/22 03:053991401
Chrysene ND ug/kg 08/23/22 20:36 218-01-908/20/22 03:053991451
Dibenz(a,h)anthracene ND ug/kg 08/23/22 20:36 53-70-308/20/22 03:053991541
Fluoranthene ND ug/kg 08/23/22 20:36 206-44-008/20/22 03:053991371
Fluorene ND ug/kg 08/23/22 20:36 86-73-708/20/22 03:053991401
Indeno(1,2,3-cd)pyrene ND ug/kg 08/23/22 20:36 193-39-508/20/22 03:053991571
1-Methylnaphthalene ND ug/kg 08/23/22 20:36 90-12-008/20/22 03:053991401
2-Methylnaphthalene ND ug/kg 08/23/22 20:36 91-57-608/20/22 03:053991601
Naphthalene ND ug/kg 08/23/22 20:36 91-20-308/20/22 03:053991351
Phenanthrene ND ug/kg 08/23/22 20:36 85-01-808/20/22 03:053991311
Pyrene ND ug/kg 08/23/22 20:36 129-00-008/20/22 03:053991621
Surrogates
Nitrobenzene-d5 (S)61 %08/23/22 20:36 4165-60-008/20/22 03:0521-130 1
2-Fluorobiphenyl (S)67 %08/23/22 20:36 321-60-808/20/22 03:0519-130 1
Terphenyl-d14 (S)55 %08/23/22 20:36 1718-51-008/20/22 03:0515-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/19/22 23:42 67-64-108/19/22 15:4914245.5 1
Benzene ND ug/kg 08/19/22 23:42 71-43-208/19/22 15:497.1 2.8 1
Bromobenzene ND ug/kg 08/19/22 23:42 108-86-108/19/22 15:497.1 2.3 1
Bromochloromethane ND ug/kg 08/19/22 23:42 74-97-508/19/22 15:497.1 2.1 1
Bromodichloromethane ND ug/kg 08/19/22 23:42 75-27-408/19/22 15:497.1 2.7 1
Bromoform ND ug/kg 08/19/22 23:42 75-25-208/19/22 15:497.1 2.5 1
Bromomethane ND ug/kg 08/19/22 23:42 74-83-908/19/22 15:4914.2 11.2 1
2-Butanone (MEK)ND ug/kg 08/19/22 23:42 78-93-308/19/22 15:4914234.0 1
n-Butylbenzene ND ug/kg 08/19/22 23:42 104-51-808/19/22 15:497.1 3.3 1
sec-Butylbenzene ND ug/kg 08/19/22 23:42 135-98-808/19/22 15:497.1 3.1 1
tert-Butylbenzene ND ug/kg 08/19/22 23:42 98-06-608/19/22 15:497.1 2.5 1
Carbon tetrachloride ND ug/kg 08/19/22 23:42 56-23-508/19/22 15:497.1 2.6 1
Chlorobenzene ND ug/kg 08/19/22 23:42 108-90-708/19/22 15:497.1 1.4 1
Chloroethane ND ug/kg 08/19/22 23:42 75-00-308/19/22 15:4914.2 5.5 1
Chloroform ND ug/kg 08/19/22 23:42 67-66-308/19/22 15:497.1 4.3 1
Chloromethane ND ug/kg 08/19/22 23:42 74-87-308/19/22 15:4914.2 5.9 1
2-Chlorotoluene ND ug/kg 08/19/22 23:42 95-49-808/19/22 15:497.1 2.5 1
4-Chlorotoluene ND ug/kg 08/19/22 23:42 106-43-408/19/22 15:497.1 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/19/22 23:42 96-12-808/19/22 15:497.1 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-7 SOIL Lab ID:92621510007 Collected:08/18/22 12:06 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/19/22 23:42 124-48-108/19/22 15:497.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/19/22 23:42 106-93-408/19/22 15:497.1 3.1 1
Dibromomethane ND ug/kg 08/19/22 23:42 74-95-308/19/22 15:497.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 08/19/22 23:42 95-50-108/19/22 15:497.1 2.5 1
1,3-Dichlorobenzene ND ug/kg 08/19/22 23:42 541-73-108/19/22 15:497.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 08/19/22 23:42 106-46-708/19/22 15:497.1 1.8 1
Dichlorodifluoromethane ND ug/kg 08/19/22 23:42 75-71-8 IH08/19/22 15:4914.2 3.1 1
1,1-Dichloroethane ND ug/kg 08/19/22 23:42 75-34-308/19/22 15:497.1 2.9 1
1,2-Dichloroethane ND ug/kg 08/19/22 23:42 107-06-208/19/22 15:497.1 4.7 1
1,1-Dichloroethene ND ug/kg 08/19/22 23:42 75-35-408/19/22 15:497.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 08/19/22 23:42 156-59-208/19/22 15:497.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 08/19/22 23:42 156-60-508/19/22 15:497.1 2.5 1
1,2-Dichloropropane ND ug/kg 08/19/22 23:42 78-87-508/19/22 15:497.1 2.1 1
1,3-Dichloropropane ND ug/kg 08/19/22 23:42 142-28-908/19/22 15:497.1 2.2 1
2,2-Dichloropropane ND ug/kg 08/19/22 23:42 594-20-708/19/22 15:497.1 2.3 1
1,1-Dichloropropene ND ug/kg 08/19/22 23:42 563-58-608/19/22 15:497.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 08/19/22 23:42 10061-01-508/19/22 15:497.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 08/19/22 23:42 10061-02-608/19/22 15:497.1 2.4 1
Diisopropyl ether ND ug/kg 08/19/22 23:42 108-20-308/19/22 15:497.1 1.9 1
Ethylbenzene ND ug/kg 08/19/22 23:42 100-41-408/19/22 15:497.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/19/22 23:42 87-68-308/19/22 15:4914.2 11.6 1
2-Hexanone ND ug/kg 08/19/22 23:42 591-78-608/19/22 15:4970.8 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 08/19/22 23:42 98-82-808/19/22 15:497.1 2.4 1
p-Isopropyltoluene ND ug/kg 08/19/22 23:42 99-87-608/19/22 15:497.1 3.5 1
Methylene Chloride ND ug/kg 08/19/22 23:42 75-09-208/19/22 15:4928.3 19.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/19/22 23:42 108-10-108/19/22 15:4970.8 6.8 1
Methyl-tert-butyl ether ND ug/kg 08/19/22 23:42 1634-04-408/19/22 15:497.1 2.6 1
Naphthalene ND ug/kg 08/19/22 23:42 91-20-308/19/22 15:497.1 3.7 1
n-Propylbenzene ND ug/kg 08/19/22 23:42 103-65-108/19/22 15:497.1 2.5 1
Styrene ND ug/kg 08/19/22 23:42 100-42-508/19/22 15:497.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/19/22 23:42 630-20-608/19/22 15:497.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/19/22 23:42 79-34-508/19/22 15:497.1 1.9 1
Tetrachloroethene ND ug/kg 08/19/22 23:42 127-18-408/19/22 15:497.1 2.2 1
Toluene ND ug/kg 08/19/22 23:42 108-88-308/19/22 15:497.1 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 08/19/22 23:42 87-61-608/19/22 15:497.1 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 08/19/22 23:42 120-82-108/19/22 15:497.1 5.9 1
1,1,1-Trichloroethane ND ug/kg 08/19/22 23:42 71-55-608/19/22 15:497.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 08/19/22 23:42 79-00-508/19/22 15:497.1 2.4 1
Trichloroethene ND ug/kg 08/19/22 23:42 79-01-608/19/22 15:497.1 1.8 1
Trichlorofluoromethane ND ug/kg 08/19/22 23:42 75-69-408/19/22 15:497.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 08/19/22 23:42 96-18-408/19/22 15:497.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/19/22 23:42 95-63-608/19/22 15:497.1 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 08/19/22 23:42 108-67-808/19/22 15:497.1 2.4 1
Vinyl acetate ND ug/kg 08/19/22 23:42 108-05-408/19/22 15:4970.8 5.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-7 SOIL Lab ID:92621510007 Collected:08/18/22 12:06 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND ug/kg 08/19/22 23:42 75-01-408/19/22 15:4914.2 3.6 1
Xylene (Total)ND ug/kg 08/19/22 23:42 1330-20-708/19/22 15:4914.2 4.0 1
m&p-Xylene ND ug/kg 08/19/22 23:42 179601-23-108/19/22 15:4914.2 4.8 1
o-Xylene ND ug/kg 08/19/22 23:42 95-47-608/19/22 15:497.1 3.1 1
Surrogates
Toluene-d8 (S)100 %08/19/22 23:42 2037-26-508/19/22 15:4970-130 1
4-Bromofluorobenzene (S)101 %08/19/22 23:42 460-00-408/19/22 15:4970-130 1
1,2-Dichloroethane-d4 (S)98 %08/19/22 23:42 17060-07-008/19/22 15:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.1 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-8 SOIL Lab ID:92621510008 Collected:08/18/22 11:56 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV PAH Microwave
Acenaphthene ND ug/kg 08/30/22 10:54 83-32-908/29/22 15:533770133010
Acenaphthylene ND ug/kg 08/30/22 10:54 208-96-808/29/22 15:533770133010
Anthracene ND ug/kg 08/30/22 10:54 120-12-708/29/22 15:533770123010
Benzo(a)anthracene ND ug/kg 08/30/22 10:54 56-55-308/29/22 15:533770126010
Benzo(a)pyrene ND ug/kg 08/30/22 10:54 50-32-808/29/22 15:533770130010
Benzo(b)fluoranthene ND ug/kg 08/30/22 10:54 205-99-208/29/22 15:533770126010
Benzo(g,h,i)perylene ND ug/kg 08/30/22 10:54 191-24-208/29/22 15:533770146010
Benzo(k)fluoranthene ND ug/kg 08/30/22 10:54 207-08-908/29/22 15:533770133010
Chrysene ND ug/kg 08/30/22 10:54 218-01-908/29/22 15:533770137010
Dibenz(a,h)anthracene ND ug/kg 08/30/22 10:54 53-70-308/29/22 15:533770145010
Fluoranthene ND ug/kg 08/30/22 10:54 206-44-008/29/22 15:533770129010
Fluorene ND ug/kg 08/30/22 10:54 86-73-708/29/22 15:533770133010
Indeno(1,2,3-cd)pyrene ND ug/kg 08/30/22 10:54 193-39-508/29/22 15:533770149010
1-Methylnaphthalene ND ug/kg 08/30/22 10:54 90-12-008/29/22 15:533770133010
2-Methylnaphthalene ND ug/kg 08/30/22 10:54 91-57-608/29/22 15:533770151010
Naphthalene ND ug/kg 08/30/22 10:54 91-20-308/29/22 15:533770128010
Phenanthrene ND ug/kg 08/30/22 10:54 85-01-808/29/22 15:533770123010
Pyrene ND ug/kg 08/30/22 10:54 129-00-008/29/22 15:533770153010
Surrogates
Nitrobenzene-d5 (S)0 %08/30/22 10:54 4165-60-0 D3,S408/29/22 15:5321-130 10
2-Fluorobiphenyl (S)0 %08/30/22 10:54 321-60-8 S408/29/22 15:5319-130 10
Terphenyl-d14 (S)0 %08/30/22 10:54 1718-51-0 S408/29/22 15:5315-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/22/22 22:02 67-64-108/22/22 12:5322973.5 2
Benzene ND ug/kg 08/22/22 22:02 71-43-208/22/22 12:5311.4 4.6 2
Bromobenzene ND ug/kg 08/22/22 22:02 108-86-108/22/22 12:5311.4 3.7 2
Bromochloromethane ND ug/kg 08/22/22 22:02 74-97-508/22/22 12:5311.4 3.4 2
Bromodichloromethane ND ug/kg 08/22/22 22:02 75-27-408/22/22 12:5311.4 4.4 2
Bromoform ND ug/kg 08/22/22 22:02 75-25-208/22/22 12:5311.4 4.0 2
Bromomethane ND ug/kg 08/22/22 22:02 74-83-908/22/22 12:5322.9 18.1 2
2-Butanone (MEK)128J ug/kg 08/22/22 22:02 78-93-308/22/22 12:5322955.0 2
n-Butylbenzene ND ug/kg 08/22/22 22:02 104-51-808/22/22 12:5311.4 5.4 2
sec-Butylbenzene 472 ug/kg 08/22/22 22:02 135-98-808/22/22 12:5311.4 5.0 2
tert-Butylbenzene ND ug/kg 08/22/22 22:02 98-06-608/22/22 12:5311.4 4.1 2
Carbon tetrachloride ND ug/kg 08/22/22 22:02 56-23-508/22/22 12:5311.4 4.3 2
Chlorobenzene ND ug/kg 08/22/22 22:02 108-90-708/22/22 12:5311.4 2.2 2
Chloroethane ND ug/kg 08/22/22 22:02 75-00-308/22/22 12:5322.9 8.8 2
Chloroform ND ug/kg 08/22/22 22:02 67-66-308/22/22 12:5311.4 7.0 2
Chloromethane ND ug/kg 08/22/22 22:02 74-87-308/22/22 12:5322.9 9.6 2
2-Chlorotoluene ND ug/kg 08/22/22 22:02 95-49-808/22/22 12:5311.4 4.1 2
4-Chlorotoluene ND ug/kg 08/22/22 22:02 106-43-408/22/22 12:5311.4 2.0 2
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/22 22:02 96-12-808/22/22 12:5311.4 4.4 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-8 SOIL Lab ID:92621510008 Collected:08/18/22 11:56 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Dibromochloromethane ND ug/kg 08/22/22 22:02 124-48-108/22/22 12:5311.4 6.4 2
1,2-Dibromoethane (EDB)ND ug/kg 08/22/22 22:02 106-93-408/22/22 12:5311.4 5.0 2
Dibromomethane ND ug/kg 08/22/22 22:02 74-95-308/22/22 12:5311.4 2.5 2
1,2-Dichlorobenzene ND ug/kg 08/22/22 22:02 95-50-108/22/22 12:5311.4 4.1 2
1,3-Dichlorobenzene ND ug/kg 08/22/22 22:02 541-73-108/22/22 12:5311.4 3.5 2
1,4-Dichlorobenzene ND ug/kg 08/22/22 22:02 106-46-708/22/22 12:5311.4 3.0 2
Dichlorodifluoromethane ND ug/kg 08/22/22 22:02 75-71-8 IH,L1,
v1
08/22/22 12:5322.9 5.0 2
1,1-Dichloroethane ND ug/kg 08/22/22 22:02 75-34-308/22/22 12:5311.4 4.7 2
1,2-Dichloroethane ND ug/kg 08/22/22 22:02 107-06-208/22/22 12:5311.4 7.6 2
1,1-Dichloroethene ND ug/kg 08/22/22 22:02 75-35-408/22/22 12:5311.4 4.7 2
cis-1,2-Dichloroethene ND ug/kg 08/22/22 22:02 156-59-208/22/22 12:5311.4 3.9 2
trans-1,2-Dichloroethene ND ug/kg 08/22/22 22:02 156-60-508/22/22 12:5311.4 4.0 2
1,2-Dichloropropane ND ug/kg 08/22/22 22:02 78-87-508/22/22 12:5311.4 3.4 2
1,3-Dichloropropane ND ug/kg 08/22/22 22:02 142-28-908/22/22 12:5311.4 3.6 2
2,2-Dichloropropane ND ug/kg 08/22/22 22:02 594-20-708/22/22 12:5311.4 3.7 2
1,1-Dichloropropene ND ug/kg 08/22/22 22:02 563-58-608/22/22 12:5311.4 5.5 2
cis-1,3-Dichloropropene ND ug/kg 08/22/22 22:02 10061-01-508/22/22 12:5311.4 3.1 2
trans-1,3-Dichloropropene ND ug/kg 08/22/22 22:02 10061-02-608/22/22 12:5311.4 3.9 2
Diisopropyl ether ND ug/kg 08/22/22 22:02 108-20-308/22/22 12:5311.4 3.1 2
Ethylbenzene 22.3 ug/kg 08/22/22 22:02 100-41-408/22/22 12:5311.4 5.3 2
Hexachloro-1,3-butadiene ND ug/kg 08/22/22 22:02 87-68-308/22/22 12:5322.9 18.7 2
2-Hexanone ND ug/kg 08/22/22 22:02 591-78-608/22/22 12:5311411.0 2
Isopropylbenzene (Cumene)155 ug/kg 08/22/22 22:02 98-82-808/22/22 12:5311.4 3.9 2
p-Isopropyltoluene ND ug/kg 08/22/22 22:02 99-87-608/22/22 12:5311.4 5.6 2
Methylene Chloride ND ug/kg 08/22/22 22:02 75-09-208/22/22 12:5345.8 31.4 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/22 22:02 108-10-108/22/22 12:5311411.0 2
Methyl-tert-butyl ether ND ug/kg 08/22/22 22:02 1634-04-408/22/22 12:5311.4 4.3 2
Naphthalene 149 ug/kg 08/22/22 22:02 91-20-308/22/22 12:5311.4 6.0 2
n-Propylbenzene 168 ug/kg 08/22/22 22:02 103-65-108/22/22 12:5311.4 4.1 2
Styrene ND ug/kg 08/22/22 22:02 100-42-508/22/22 12:5311.4 3.0 2
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/22 22:02 630-20-608/22/22 12:5311.4 4.4 2
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/22 22:02 79-34-508/22/22 12:5311.4 3.0 2
Tetrachloroethene ND ug/kg 08/22/22 22:02 127-18-408/22/22 12:5311.4 3.6 2
Toluene ND ug/kg 08/22/22 22:02 108-88-308/22/22 12:5311.4 3.3 2
1,2,3-Trichlorobenzene ND ug/kg 08/22/22 22:02 87-61-608/22/22 12:5311.4 9.3 2
1,2,4-Trichlorobenzene ND ug/kg 08/22/22 22:02 120-82-108/22/22 12:5311.4 9.6 2
1,1,1-Trichloroethane ND ug/kg 08/22/22 22:02 71-55-608/22/22 12:5311.4 6.0 2
1,1,2-Trichloroethane ND ug/kg 08/22/22 22:02 79-00-508/22/22 12:5311.4 3.8 2
Trichloroethene ND ug/kg 08/22/22 22:02 79-01-608/22/22 12:5311.4 3.0 2
Trichlorofluoromethane ND ug/kg 08/22/22 22:02 75-69-408/22/22 12:5311.4 6.3 2
1,2,3-Trichloropropane ND ug/kg 08/22/22 22:02 96-18-408/22/22 12:5311.4 5.8 2
1,2,4-Trimethylbenzene ND ug/kg 08/22/22 22:02 95-63-608/22/22 12:5311.4 3.1 2
1,3,5-Trimethylbenzene ND ug/kg 08/22/22 22:02 108-67-808/22/22 12:5311.4 3.8 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-8 SOIL Lab ID:92621510008 Collected:08/18/22 11:56 Received:08/19/22 09:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl acetate ND ug/kg 08/22/22 22:02 108-05-408/22/22 12:531148.3 2
Vinyl chloride ND ug/kg 08/22/22 22:02 75-01-408/22/22 12:5322.9 5.8 2
Xylene (Total)90.9 ug/kg 08/22/22 22:02 1330-20-708/22/22 12:5322.9 6.5 2
m&p-Xylene 56.7 ug/kg 08/22/22 22:02 179601-23-108/22/22 12:5322.9 7.8 2
o-Xylene 34.2 ug/kg 08/22/22 22:02 95-47-608/22/22 12:5311.4 5.1 2
Surrogates
Toluene-d8 (S)99 %08/22/22 22:02 2037-26-508/22/22 12:5370-130 2
4-Bromofluorobenzene (S)143 %08/22/22 22:02 460-00-4 S208/22/22 12:5370-130 2
1,2-Dichloroethane-d4 (S)92 %08/22/22 22:02 17060-07-008/22/22 12:5370-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.9 %08/22/22 15:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:MW-1 Lab ID:92621510009 Collected:08/18/22 11:15 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 08/24/22 20:50 83-32-908/24/22 17:0510.0 3.2 1
Acenaphthylene ND ug/L 08/24/22 20:50 208-96-808/24/22 17:0510.0 3.9 1
Anthracene ND ug/L 08/24/22 20:50 120-12-708/24/22 17:0510.0 3.9 1
Benzo(a)anthracene ND ug/L 08/24/22 20:50 56-55-308/24/22 17:0510.0 4.0 1
Benzo(a)pyrene ND ug/L 08/24/22 20:50 50-32-808/24/22 17:0510.0 3.6 1
Benzo(b)fluoranthene ND ug/L 08/24/22 20:50 205-99-208/24/22 17:0510.0 3.9 1
Benzo(g,h,i)perylene ND ug/L 08/24/22 20:50 191-24-208/24/22 17:0510.0 3.7 1
Benzo(k)fluoranthene ND ug/L 08/24/22 20:50 207-08-908/24/22 17:0510.0 3.6 1
Chrysene ND ug/L 08/24/22 20:50 218-01-908/24/22 17:0510.0 3.4 1
Dibenz(a,h)anthracene ND ug/L 08/24/22 20:50 53-70-308/24/22 17:0510.0 4.3 1
Fluoranthene ND ug/L 08/24/22 20:50 206-44-008/24/22 17:0510.0 3.4 1
Fluorene ND ug/L 08/24/22 20:50 86-73-708/24/22 17:0510.0 3.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/22 20:50 193-39-508/24/22 17:0510.0 4.0 1
1-Methylnaphthalene ND ug/L 08/24/22 20:50 90-12-008/24/22 17:0510.0 3.7 1
2-Methylnaphthalene ND ug/L 08/24/22 20:50 91-57-608/24/22 17:0510.0 3.4 1
Naphthalene ND ug/L 08/24/22 20:50 91-20-308/24/22 17:0510.0 3.2 1
Phenanthrene ND ug/L 08/24/22 20:50 85-01-808/24/22 17:0510.0 3.4 1
Pyrene ND ug/L 08/24/22 20:50 129-00-008/24/22 17:0510.0 3.8 1
Surrogates
Nitrobenzene-d5 (S)83 %08/24/22 20:50 4165-60-008/24/22 17:0542-147 1
2-Fluorobiphenyl (S)83 %08/24/22 20:50 321-60-808/24/22 17:0558-131 1
Terphenyl-d14 (S)61 %08/24/22 20:50 1718-51-008/24/22 17:0555-151 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/23/22 18:03 67-64-125.0 5.1 1
Benzene ND ug/L 08/23/22 18:03 71-43-21.0 0.34 1
Bromobenzene ND ug/L 08/23/22 18:03 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 08/23/22 18:03 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 08/23/22 18:03 75-27-41.0 0.31 1
Bromoform ND ug/L 08/23/22 18:03 75-25-21.0 0.34 1
Bromomethane ND ug/L 08/23/22 18:03 74-83-9 IH,IK2.0 1.7 1
2-Butanone (MEK)ND ug/L 08/23/22 18:03 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 08/23/22 18:03 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 08/23/22 18:03 108-90-71.0 0.28 1
Chloroethane ND ug/L 08/23/22 18:03 75-00-31.0 0.65 1
Chloroform ND ug/L 08/23/22 18:03 67-66-31.0 0.43 1
Chloromethane ND ug/L 08/23/22 18:03 74-87-3 v21.0 0.54 1
2-Chlorotoluene ND ug/L 08/23/22 18:03 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 08/23/22 18:03 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/22 18:03 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 08/23/22 18:03 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 08/23/22 18:03 106-93-41.0 0.27 1
Dibromomethane ND ug/L 08/23/22 18:03 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 08/23/22 18:03 95-50-11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:MW-1 Lab ID:92621510009 Collected:08/18/22 11:15 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,3-Dichlorobenzene ND ug/L 08/23/22 18:03 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 08/23/22 18:03 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/23/22 18:03 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 08/23/22 18:03 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 08/23/22 18:03 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 08/23/22 18:03 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 08/23/22 18:03 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 08/23/22 18:03 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 08/23/22 18:03 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 08/23/22 18:03 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/22 18:03 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 08/23/22 18:03 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 08/23/22 18:03 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 08/23/22 18:03 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 08/23/22 18:03 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 08/23/22 18:03 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/23/22 18:03 87-68-32.0 1.5 1
2-Hexanone ND ug/L 08/23/22 18:03 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 08/23/22 18:03 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 08/23/22 18:03 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/22 18:03 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 08/23/22 18:03 1634-04-41.0 0.42 1
Naphthalene ND ug/L 08/23/22 18:03 91-20-31.0 0.64 1
Styrene ND ug/L 08/23/22 18:03 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/22 18:03 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/22 18:03 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/23/22 18:03 127-18-41.0 0.29 1
Toluene ND ug/L 08/23/22 18:03 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 08/23/22 18:03 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 08/23/22 18:03 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 08/23/22 18:03 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 08/23/22 18:03 79-00-51.0 0.32 1
Trichloroethene ND ug/L 08/23/22 18:03 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 08/23/22 18:03 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 08/23/22 18:03 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 08/23/22 18:03 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 08/23/22 18:03 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 08/23/22 18:03 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 08/23/22 18:03 179601-23-12.0 0.71 1
o-Xylene ND ug/L 08/23/22 18:03 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)101 %08/23/22 18:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %08/23/22 18:03 17060-07-070-130 1
Toluene-d8 (S)98 %08/23/22 18:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-2 GW Lab ID:92621510010 Collected:08/18/22 11:38 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 08/24/22 21:15 83-32-908/24/22 17:0512039.0 1
Acenaphthylene ND ug/L 08/24/22 21:15 208-96-808/24/22 17:0512046.3 1
Anthracene ND ug/L 08/24/22 21:15 120-12-708/24/22 17:0512046.9 1
Benzo(a)anthracene ND ug/L 08/24/22 21:15 56-55-308/24/22 17:0512048.4 1
Benzo(a)pyrene ND ug/L 08/24/22 21:15 50-32-808/24/22 17:0512043.4 1
Benzo(b)fluoranthene ND ug/L 08/24/22 21:15 205-99-208/24/22 17:0512047.2 1
Benzo(g,h,i)perylene ND ug/L 08/24/22 21:15 191-24-208/24/22 17:0512044.9 1
Benzo(k)fluoranthene ND ug/L 08/24/22 21:15 207-08-908/24/22 17:0512043.8 1
Chrysene ND ug/L 08/24/22 21:15 218-01-908/24/22 17:0512040.8 1
Dibenz(a,h)anthracene ND ug/L 08/24/22 21:15 53-70-308/24/22 17:0512052.1 1
Fluoranthene ND ug/L 08/24/22 21:15 206-44-008/24/22 17:0512040.3 1
Fluorene ND ug/L 08/24/22 21:15 86-73-708/24/22 17:0512038.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/22 21:15 193-39-508/24/22 17:0512048.6 1
1-Methylnaphthalene ND ug/L 08/24/22 21:15 90-12-008/24/22 17:0512044.2 1
2-Methylnaphthalene ND ug/L 08/24/22 21:15 91-57-608/24/22 17:0512041.3 1
Naphthalene ND ug/L 08/24/22 21:15 91-20-308/24/22 17:0512037.8 1
Phenanthrene ND ug/L 08/24/22 21:15 85-01-808/24/22 17:0512040.8 1
Pyrene ND ug/L 08/24/22 21:15 129-00-008/24/22 17:0512046.2 1
Surrogates
Nitrobenzene-d5 (S)69 %08/24/22 21:15 4165-60-0 P308/24/22 17:0542-147 1
2-Fluorobiphenyl (S)63 %08/24/22 21:15 321-60-808/24/22 17:0558-131 1
Terphenyl-d14 (S)11 %08/24/22 21:15 1718-51-0 S008/24/22 17:0555-151 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/23/22 18:40 67-64-125.0 5.1 1
Benzene ND ug/L 08/23/22 18:40 71-43-21.0 0.34 1
Bromobenzene ND ug/L 08/23/22 18:40 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 08/23/22 18:40 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 08/23/22 18:40 75-27-41.0 0.31 1
Bromoform ND ug/L 08/23/22 18:40 75-25-21.0 0.34 1
Bromomethane ND ug/L 08/23/22 18:40 74-83-9 IH,IK2.0 1.7 1
2-Butanone (MEK)ND ug/L 08/23/22 18:40 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 08/23/22 18:40 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 08/23/22 18:40 108-90-71.0 0.28 1
Chloroethane ND ug/L 08/23/22 18:40 75-00-31.0 0.65 1
Chloroform ND ug/L 08/23/22 18:40 67-66-31.0 0.43 1
Chloromethane ND ug/L 08/23/22 18:40 74-87-3 v21.0 0.54 1
2-Chlorotoluene ND ug/L 08/23/22 18:40 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 08/23/22 18:40 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/22 18:40 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 08/23/22 18:40 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 08/23/22 18:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 08/23/22 18:40 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 08/23/22 18:40 95-50-11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-2 GW Lab ID:92621510010 Collected:08/18/22 11:38 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,3-Dichlorobenzene ND ug/L 08/23/22 18:40 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 08/23/22 18:40 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/23/22 18:40 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 08/23/22 18:40 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 08/23/22 18:40 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 08/23/22 18:40 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 08/23/22 18:40 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 08/23/22 18:40 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 08/23/22 18:40 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 08/23/22 18:40 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/22 18:40 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 08/23/22 18:40 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 08/23/22 18:40 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 08/23/22 18:40 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 08/23/22 18:40 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 08/23/22 18:40 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/23/22 18:40 87-68-32.0 1.5 1
2-Hexanone ND ug/L 08/23/22 18:40 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 08/23/22 18:40 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 08/23/22 18:40 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/22 18:40 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 08/23/22 18:40 1634-04-41.0 0.42 1
Naphthalene ND ug/L 08/23/22 18:40 91-20-31.0 0.64 1
Styrene ND ug/L 08/23/22 18:40 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/22 18:40 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/22 18:40 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/23/22 18:40 127-18-41.0 0.29 1
Toluene ND ug/L 08/23/22 18:40 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 08/23/22 18:40 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 08/23/22 18:40 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 08/23/22 18:40 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 08/23/22 18:40 79-00-51.0 0.32 1
Trichloroethene ND ug/L 08/23/22 18:40 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 08/23/22 18:40 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 08/23/22 18:40 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 08/23/22 18:40 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 08/23/22 18:40 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 08/23/22 18:40 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 08/23/22 18:40 179601-23-12.0 0.71 1
o-Xylene ND ug/L 08/23/22 18:40 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)106 %08/23/22 18:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %08/23/22 18:40 17060-07-070-130 1
Toluene-d8 (S)99 %08/23/22 18:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-3 GW Lab ID:92621510011 Collected:08/18/22 12:55 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 08/24/22 21:41 83-32-908/24/22 17:0520.0 6.5 1
Acenaphthylene ND ug/L 08/24/22 21:41 208-96-808/24/22 17:0520.0 7.7 1
Anthracene ND ug/L 08/24/22 21:41 120-12-708/24/22 17:0520.0 7.8 1
Benzo(a)anthracene ND ug/L 08/24/22 21:41 56-55-308/24/22 17:0520.0 8.1 1
Benzo(a)pyrene ND ug/L 08/24/22 21:41 50-32-808/24/22 17:0520.0 7.2 1
Benzo(b)fluoranthene ND ug/L 08/24/22 21:41 205-99-208/24/22 17:0520.0 7.9 1
Benzo(g,h,i)perylene ND ug/L 08/24/22 21:41 191-24-208/24/22 17:0520.0 7.5 1
Benzo(k)fluoranthene ND ug/L 08/24/22 21:41 207-08-908/24/22 17:0520.0 7.3 1
Chrysene ND ug/L 08/24/22 21:41 218-01-908/24/22 17:0520.0 6.8 1
Dibenz(a,h)anthracene ND ug/L 08/24/22 21:41 53-70-308/24/22 17:0520.0 8.7 1
Fluoranthene ND ug/L 08/24/22 21:41 206-44-008/24/22 17:0520.0 6.7 1
Fluorene ND ug/L 08/24/22 21:41 86-73-708/24/22 17:0520.0 6.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/22 21:41 193-39-508/24/22 17:0520.0 8.1 1
1-Methylnaphthalene 37.4 ug/L 08/24/22 21:41 90-12-0 P308/24/22 17:0520.0 7.4 1
2-Methylnaphthalene 54.4 ug/L 08/24/22 21:41 91-57-608/24/22 17:0520.0 6.9 1
Naphthalene 41.0 ug/L 08/24/22 21:41 91-20-308/24/22 17:0520.0 6.3 1
Phenanthrene ND ug/L 08/24/22 21:41 85-01-808/24/22 17:0520.0 6.8 1
Pyrene ND ug/L 08/24/22 21:41 129-00-008/24/22 17:0520.0 7.7 1
Surrogates
Nitrobenzene-d5 (S)68 %08/24/22 21:41 4165-60-008/24/22 17:0542-147 1
2-Fluorobiphenyl (S)83 %08/24/22 21:41 321-60-808/24/22 17:0558-131 1
Terphenyl-d14 (S)69 %08/24/22 21:41 1718-51-008/24/22 17:0555-151 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 10.0J ug/L 08/23/22 18:58 67-64-125.0 5.1 1
Benzene 3.0 ug/L 08/23/22 18:58 71-43-21.0 0.34 1
Bromobenzene ND ug/L 08/23/22 18:58 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 08/23/22 18:58 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 08/23/22 18:58 75-27-41.0 0.31 1
Bromoform ND ug/L 08/23/22 18:58 75-25-21.0 0.34 1
Bromomethane ND ug/L 08/23/22 18:58 74-83-9 IH,IK2.0 1.7 1
2-Butanone (MEK)ND ug/L 08/23/22 18:58 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 08/23/22 18:58 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 08/23/22 18:58 108-90-71.0 0.28 1
Chloroethane ND ug/L 08/23/22 18:58 75-00-31.0 0.65 1
Chloroform ND ug/L 08/23/22 18:58 67-66-31.0 0.43 1
Chloromethane ND ug/L 08/23/22 18:58 74-87-3 v21.0 0.54 1
2-Chlorotoluene ND ug/L 08/23/22 18:58 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 08/23/22 18:58 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 08/23/22 18:58 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 08/23/22 18:58 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 08/23/22 18:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 08/23/22 18:58 74-95-31.0 0.39 1
1,2-Dichlorobenzene 7.7 ug/L 08/23/22 18:58 95-50-11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-3 GW Lab ID:92621510011 Collected:08/18/22 12:55 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,3-Dichlorobenzene ND ug/L 08/23/22 18:58 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 08/23/22 18:58 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/23/22 18:58 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 08/23/22 18:58 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 08/23/22 18:58 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 08/23/22 18:58 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 1.0 ug/L 08/23/22 18:58 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 08/23/22 18:58 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 08/23/22 18:58 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 08/23/22 18:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/23/22 18:58 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 08/23/22 18:58 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 08/23/22 18:58 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 08/23/22 18:58 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 08/23/22 18:58 108-20-31.0 0.31 1
Ethylbenzene 11.9 ug/L 08/23/22 18:58 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/23/22 18:58 87-68-32.0 1.5 1
2-Hexanone ND ug/L 08/23/22 18:58 591-78-65.0 0.48 1
p-Isopropyltoluene 11.0 ug/L 08/23/22 18:58 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 08/23/22 18:58 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/23/22 18:58 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 08/23/22 18:58 1634-04-41.0 0.42 1
Naphthalene 74.1 ug/L 08/23/22 18:58 91-20-31.0 0.64 1
Styrene ND ug/L 08/23/22 18:58 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 08/23/22 18:58 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 08/23/22 18:58 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/23/22 18:58 127-18-41.0 0.29 1
Toluene 22.4 ug/L 08/23/22 18:58 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 08/23/22 18:58 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 08/23/22 18:58 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 08/23/22 18:58 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 08/23/22 18:58 79-00-51.0 0.32 1
Trichloroethene 0.93J ug/L 08/23/22 18:58 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 08/23/22 18:58 75-69-41.0 0.30 1
1,2,3-Trichloropropane 0.86J ug/L 08/23/22 18:58 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 08/23/22 18:58 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 08/23/22 18:58 75-01-41.0 0.39 1
Xylene (Total)77.3 ug/L 08/23/22 18:58 1330-20-71.0 0.34 1
m&p-Xylene 44.5 ug/L 08/23/22 18:58 179601-23-12.0 0.71 1
o-Xylene 32.8 ug/L 08/23/22 18:58 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)106 %08/23/22 18:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %08/23/22 18:58 17060-07-070-130 1
Toluene-d8 (S)102 %08/23/22 18:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-5 GW Lab ID:92621510012 Collected:08/18/22 13:55 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 08/24/22 22:07 83-32-908/24/22 17:0510.0 3.2 1
Acenaphthylene ND ug/L 08/24/22 22:07 208-96-808/24/22 17:0510.0 3.9 1
Anthracene ND ug/L 08/24/22 22:07 120-12-708/24/22 17:0510.0 3.9 1
Benzo(a)anthracene ND ug/L 08/24/22 22:07 56-55-308/24/22 17:0510.0 4.0 1
Benzo(a)pyrene ND ug/L 08/24/22 22:07 50-32-808/24/22 17:0510.0 3.6 1
Benzo(b)fluoranthene ND ug/L 08/24/22 22:07 205-99-208/24/22 17:0510.0 3.9 1
Benzo(g,h,i)perylene ND ug/L 08/24/22 22:07 191-24-208/24/22 17:0510.0 3.7 1
Benzo(k)fluoranthene ND ug/L 08/24/22 22:07 207-08-908/24/22 17:0510.0 3.6 1
Chrysene ND ug/L 08/24/22 22:07 218-01-908/24/22 17:0510.0 3.4 1
Dibenz(a,h)anthracene ND ug/L 08/24/22 22:07 53-70-308/24/22 17:0510.0 4.3 1
Fluoranthene ND ug/L 08/24/22 22:07 206-44-008/24/22 17:0510.0 3.4 1
Fluorene ND ug/L 08/24/22 22:07 86-73-708/24/22 17:0510.0 3.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/22 22:07 193-39-508/24/22 17:0510.0 4.0 1
1-Methylnaphthalene ND ug/L 08/24/22 22:07 90-12-008/24/22 17:0510.0 3.7 1
2-Methylnaphthalene ND ug/L 08/24/22 22:07 91-57-608/24/22 17:0510.0 3.4 1
Naphthalene ND ug/L 08/24/22 22:07 91-20-308/24/22 17:0510.0 3.2 1
Phenanthrene ND ug/L 08/24/22 22:07 85-01-808/24/22 17:0510.0 3.4 1
Pyrene ND ug/L 08/24/22 22:07 129-00-008/24/22 17:0510.0 3.8 1
Surrogates
Nitrobenzene-d5 (S)86 %08/24/22 22:07 4165-60-008/24/22 17:0542-147 1
2-Fluorobiphenyl (S)86 %08/24/22 22:07 321-60-808/24/22 17:0558-131 1
Terphenyl-d14 (S)66 %08/24/22 22:07 1718-51-008/24/22 17:0555-151 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/22 13:12 67-64-125.0 5.1 1
Benzene ND ug/L 08/25/22 13:12 71-43-21.0 0.34 1
Bromobenzene ND ug/L 08/25/22 13:12 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 08/25/22 13:12 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 08/25/22 13:12 75-27-41.0 0.31 1
Bromoform ND ug/L 08/25/22 13:12 75-25-21.0 0.34 1
Bromomethane ND ug/L 08/25/22 13:12 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 08/25/22 13:12 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 08/25/22 13:12 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 08/25/22 13:12 108-90-71.0 0.28 1
Chloroethane ND ug/L 08/25/22 13:12 75-00-31.0 0.65 1
Chloroform ND ug/L 08/25/22 13:12 67-66-31.0 0.43 1
Chloromethane ND ug/L 08/25/22 13:12 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 08/25/22 13:12 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 08/25/22 13:12 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/22 13:12 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 08/25/22 13:12 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/22 13:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 08/25/22 13:12 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 08/25/22 13:12 95-50-11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 76
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Sample:B-5 GW Lab ID:92621510012 Collected:08/18/22 13:55 Received:08/19/22 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,3-Dichlorobenzene ND ug/L 08/25/22 13:12 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 08/25/22 13:12 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 08/25/22 13:12 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 08/25/22 13:12 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 08/25/22 13:12 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 08/25/22 13:12 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 08/25/22 13:12 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 08/25/22 13:12 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 08/25/22 13:12 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 08/25/22 13:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 08/25/22 13:12 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 08/25/22 13:12 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 08/25/22 13:12 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 08/25/22 13:12 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 08/25/22 13:12 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 08/25/22 13:12 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 08/25/22 13:12 87-68-32.0 1.5 1
2-Hexanone ND ug/L 08/25/22 13:12 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 08/25/22 13:12 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 08/25/22 13:12 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/22 13:12 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 08/25/22 13:12 1634-04-41.0 0.42 1
Naphthalene ND ug/L 08/25/22 13:12 91-20-3 v11.0 0.64 1
Styrene ND ug/L 08/25/22 13:12 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/22 13:12 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/22 13:12 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/25/22 13:12 127-18-41.0 0.29 1
Toluene ND ug/L 08/25/22 13:12 108-88-31.0 0.48 1
1,2,3-Trichlorobenzene ND ug/L 08/25/22 13:12 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 08/25/22 13:12 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 08/25/22 13:12 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 08/25/22 13:12 79-00-51.0 0.32 1
Trichloroethene ND ug/L 08/25/22 13:12 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 08/25/22 13:12 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 08/25/22 13:12 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 08/25/22 13:12 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 08/25/22 13:12 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 08/25/22 13:12 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 08/25/22 13:12 179601-23-12.0 0.71 1
o-Xylene ND ug/L 08/25/22 13:12 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)99 %08/25/22 13:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %08/25/22 13:12 17060-07-070-130 1
Toluene-d8 (S)99 %08/25/22 13:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718484
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510001, 92621510002, 92621510004, 92621510005, 92621510006, 92621510007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3745387
Associated Lab Samples:92621510001, 92621510002, 92621510004, 92621510005, 92621510006, 92621510007
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/19/22 16:371.9
1,1,1-Trichloroethane ug/kg ND 5.0 08/19/22 16:372.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/19/22 16:371.3
1,1,2-Trichloroethane ug/kg ND 5.0 08/19/22 16:371.7
1,1-Dichloroethane ug/kg ND 5.0 08/19/22 16:372.1
1,1-Dichloroethene ug/kg ND 5.0 08/19/22 16:372.1
1,1-Dichloropropene ug/kg ND 5.0 08/19/22 16:372.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/19/22 16:374.0
1,2,3-Trichloropropane ug/kg ND 5.0 08/19/22 16:372.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/19/22 16:374.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/19/22 16:371.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/19/22 16:371.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/19/22 16:372.2
1,2-Dichlorobenzene ug/kg ND 5.0 08/19/22 16:371.8
1,2-Dichloroethane ug/kg ND 5.0 08/19/22 16:373.3
1,2-Dichloropropane ug/kg ND 5.0 08/19/22 16:371.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/19/22 16:371.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/19/22 16:371.6
1,3-Dichloropropane ug/kg ND 5.0 08/19/22 16:371.6
1,4-Dichlorobenzene ug/kg ND 5.0 08/19/22 16:371.3
2,2-Dichloropropane ug/kg ND 5.0 08/19/22 16:371.6
2-Butanone (MEK)ug/kg ND 100 08/19/22 16:3724.0
2-Chlorotoluene ug/kg ND 5.0 08/19/22 16:371.8
2-Hexanone ug/kg ND 50.0 08/19/22 16:374.8
4-Chlorotoluene ug/kg ND 5.0 08/19/22 16:370.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/19/22 16:374.8
Acetone ug/kg ND 100 08/19/22 16:3732.1
Benzene ug/kg ND 5.0 08/19/22 16:372.0
Bromobenzene ug/kg ND 5.0 08/19/22 16:371.6
Bromochloromethane ug/kg ND 5.0 08/19/22 16:371.5
Bromodichloromethane ug/kg ND 5.0 08/19/22 16:371.9
Bromoform ug/kg ND 5.0 08/19/22 16:371.8
Bromomethane ug/kg ND 10.0 08/19/22 16:377.9
Carbon tetrachloride ug/kg ND 5.0 08/19/22 16:371.9
Chlorobenzene ug/kg ND 5.0 08/19/22 16:370.96
Chloroethane ug/kg ND 10.0 08/19/22 16:373.9
Chloroform ug/kg ND 5.0 08/19/22 16:373.0
Chloromethane ug/kg ND 10.0 08/19/22 16:374.2
cis-1,2-Dichloroethene ug/kg ND 5.0 08/19/22 16:371.7
cis-1,3-Dichloropropene ug/kg ND 5.0 08/19/22 16:371.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3745387
Associated Lab Samples:92621510001, 92621510002, 92621510004, 92621510005, 92621510006, 92621510007
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 08/19/22 16:372.8
Dibromomethane ug/kg ND 5.0 08/19/22 16:371.1
Dichlorodifluoromethane ug/kg ND 10.0 IH08/19/22 16:372.2
Diisopropyl ether ug/kg ND 5.0 08/19/22 16:371.4
Ethylbenzene ug/kg ND 5.0 08/19/22 16:372.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/19/22 16:378.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/19/22 16:371.7
m&p-Xylene ug/kg ND 10.0 08/19/22 16:373.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/19/22 16:371.9
Methylene Chloride ug/kg ND 20.0 08/19/22 16:3713.7
n-Butylbenzene ug/kg ND 5.0 08/19/22 16:372.4
n-Propylbenzene ug/kg ND 5.0 08/19/22 16:371.8
Naphthalene ug/kg ND 5.0 08/19/22 16:372.6
o-Xylene ug/kg ND 5.0 08/19/22 16:372.2
p-Isopropyltoluene ug/kg ND 5.0 08/19/22 16:372.5
sec-Butylbenzene ug/kg ND 5.0 08/19/22 16:372.2
Styrene ug/kg ND 5.0 08/19/22 16:371.3
tert-Butylbenzene ug/kg ND 5.0 08/19/22 16:371.8
Tetrachloroethene ug/kg ND 5.0 08/19/22 16:371.6
Toluene ug/kg ND 5.0 08/19/22 16:371.4
trans-1,2-Dichloroethene ug/kg ND 5.0 08/19/22 16:371.8
trans-1,3-Dichloropropene ug/kg ND 5.0 08/19/22 16:371.7
Trichloroethene ug/kg ND 5.0 08/19/22 16:371.3
Trichlorofluoromethane ug/kg ND 5.0 08/19/22 16:372.8
Vinyl acetate ug/kg ND 50.0 08/19/22 16:373.6
Vinyl chloride ug/kg ND 10.0 08/19/22 16:372.5
Xylene (Total)ug/kg ND 10.0 08/19/22 16:372.8
1,2-Dichloroethane-d4 (S)%103 70-130 08/19/22 16:37
4-Bromofluorobenzene (S)%100 70-130 08/19/22 16:37
Toluene-d8 (S)%100 70-130 08/19/22 16:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745388LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12901250 103 70-130
1,1,1-Trichloroethane ug/kg 12101250 97 70-130
1,1,2,2-Tetrachloroethane ug/kg 11801250 94 70-130
1,1,2-Trichloroethane ug/kg 12001250 96 70-130
1,1-Dichloroethane ug/kg 11901250 95 70-130
1,1-Dichloroethene ug/kg 13001250 104 70-130
1,1-Dichloropropene ug/kg 12401250 99 70-130
1,2,3-Trichlorobenzene ug/kg 12101250 97 70-130
1,2,3-Trichloropropane ug/kg 11501250 92 70-130
1,2,4-Trichlorobenzene ug/kg 11801250 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745388LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12601250 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 10701250 86 67-130
1,2-Dibromoethane (EDB)ug/kg 12501250 100 70-130
1,2-Dichlorobenzene ug/kg 12101250 97 70-130
1,2-Dichloroethane ug/kg 11701250 94 70-130
1,2-Dichloropropane ug/kg 12201250 98 70-130
1,3,5-Trimethylbenzene ug/kg 13001250 104 70-130
1,3-Dichlorobenzene ug/kg 12201250 98 70-130
1,3-Dichloropropane ug/kg 12301250 98 70-130
1,4-Dichlorobenzene ug/kg 11701250 93 70-130
2,2-Dichloropropane ug/kg 10501250 84 67-130
2-Butanone (MEK)ug/kg 22102500 88 66-130
2-Chlorotoluene ug/kg 12501250 100 70-130
2-Hexanone ug/kg 25902500 104 70-130
4-Chlorotoluene ug/kg 12401250 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24902500 100 70-130
Acetone ug/kg 22202500 89 67-130
Benzene ug/kg 11801250 94 70-130
Bromobenzene ug/kg 12301250 98 70-130
Bromochloromethane ug/kg 12301250 98 70-130
Bromodichloromethane ug/kg 12401250 99 70-130
Bromoform ug/kg 12301250 99 70-130
Bromomethane ug/kg 11801250 94 53-175
Carbon tetrachloride ug/kg 12901250 103 70-130
Chlorobenzene ug/kg 12401250 99 70-130
Chloroethane ug/kg 12701250 102 70-135
Chloroform ug/kg 10801250 87 70-130
Chloromethane ug/kg 13601250 109 64-130
cis-1,2-Dichloroethene ug/kg 12201250 97 70-130
cis-1,3-Dichloropropene ug/kg 12601250 100 70-130
Dibromochloromethane ug/kg 12501250 100 70-130
Dibromomethane ug/kg 12201250 98 70-130
Dichlorodifluoromethane ug/kg 1640 IH125013163-145
Diisopropyl ether ug/kg 12601250 101 68-130
Ethylbenzene ug/kg 11601250 93 70-130
Hexachloro-1,3-butadiene ug/kg 11101250 89 70-130
Isopropylbenzene (Cumene)ug/kg 12401250 99 70-130
m&p-Xylene ug/kg 24902500 99 70-130
Methyl-tert-butyl ether ug/kg 12701250 102 70-130
Methylene Chloride ug/kg 11401250 92 67-130
n-Butylbenzene ug/kg 12401250 99 70-130
n-Propylbenzene ug/kg 12301250 99 70-130
Naphthalene ug/kg 12401250 99 70-130
o-Xylene ug/kg 12901250 103 70-130
p-Isopropyltoluene ug/kg 12801250 103 70-130
sec-Butylbenzene ug/kg 12601250 100 70-130
Styrene ug/kg 13001250 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745388LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12201250 98 64-130
Tetrachloroethene ug/kg 11401250 92 70-130
Toluene ug/kg 12001250 96 70-130
trans-1,2-Dichloroethene ug/kg 12501250 100 70-130
trans-1,3-Dichloropropene ug/kg 12501250 100 70-130
Trichloroethene ug/kg 12201250 98 70-130
Trichlorofluoromethane ug/kg 12601250 101 70-130
Vinyl acetate ug/kg 23902500 95 70-134
Vinyl chloride ug/kg 12701250 102 68-130
Xylene (Total)ug/kg 37703750 101 70-130
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3745389MATRIX SPIKE SAMPLE:
MSSpike
Result
92621510001
1,1,1,2-Tetrachloroethane ug/kg 398575 69 58-140ND
1,1,1-Trichloroethane ug/kg 419575 73 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 343575 60 52-139ND
1,1,2-Trichloroethane ug/kg 379575 66 56-140ND
1,1-Dichloroethane ug/kg 387575 67 58-145ND
1,1-Dichloroethene ug/kg 422575 73 57-158ND
1,1-Dichloropropene ug/kg 433575 75 58-151ND
1,2,3-Trichlorobenzene ug/kg 139 M15752448-149ND
1,2,3-Trichloropropane ug/kg 337575 59 54-132ND
1,2,4-Trichlorobenzene ug/kg 257 M15754551-151ND
1,2,4-Trimethylbenzene ug/kg 408575 71 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 241 M15754244-134ND
1,2-Dibromoethane (EDB)ug/kg 377575 66 60-138ND
1,2-Dichlorobenzene ug/kg 398575 69 59-147ND
1,2-Dichloroethane ug/kg 387575 67 57-139ND
1,2-Dichloropropane ug/kg 410575 71 62-145ND
1,3,5-Trimethylbenzene ug/kg 419575 73 47-159ND
1,3-Dichlorobenzene ug/kg 397575 69 58-144ND
1,3-Dichloropropane ug/kg 388575 67 60-142ND
1,4-Dichlorobenzene ug/kg 382575 66 57-143ND
2,2-Dichloropropane ug/kg 373575 65 37-144ND
2-Butanone (MEK)ug/kg 6391150 55 28-146ND
2-Chlorotoluene ug/kg 404575 70 55-158ND
2-Hexanone ug/kg 6741150 58 44-141ND
4-Chlorotoluene ug/kg 404575 70 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 6901150 60 50-138ND
Acetone ug/kg 5781150 50 20-136ND
Benzene ug/kg 405575 70 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3745389MATRIX SPIKE SAMPLE:
MSSpike
Result
92621510001
Bromobenzene ug/kg 391575 68 59-145ND
Bromochloromethane ug/kg 381575 66 57-143ND
Bromodichloromethane ug/kg 374575 65 53-133ND
Bromoform ug/kg 330575 57 48-133ND
Bromomethane ug/kg 375575 65 10-167ND
Carbon tetrachloride ug/kg 436575 76 57-147ND
Chlorobenzene ug/kg 412575 72 61-144ND
Chloroethane ug/kg 271575 47 10-153ND
Chloroform ug/kg 347575 60 58-141ND
Chloromethane ug/kg 502575 87 54-165ND
cis-1,2-Dichloroethene ug/kg 399575 69 59-144ND
cis-1,3-Dichloropropene ug/kg 397575 69 56-137ND
Dibromochloromethane ug/kg 356575 62 53-139ND
Dibromomethane ug/kg 373575 65 60-136ND
Dichlorodifluoromethane ug/kg 609 IH57510649-177ND
Diisopropyl ether ug/kg 407575 71 53-136ND
Ethylbenzene ug/kg 389575 68 53-150ND
Hexachloro-1,3-butadiene ug/kg 371575 64 42-186ND
Isopropylbenzene (Cumene)ug/kg 415575 72 62-154ND
m&p-Xylene ug/kg 8261150 72 49-156ND
Methyl-tert-butyl ether ug/kg 385575 67 54-133ND
Methylene Chloride ug/kg 314575 55 50-153ND
n-Butylbenzene ug/kg 405575 70 44-174ND
n-Propylbenzene ug/kg 394575 68 52-157ND
Naphthalene ug/kg 154 M15752737-150ND
o-Xylene ug/kg 431575 74 54-1506.8
p-Isopropyltoluene ug/kg 424575 74 50-164ND
sec-Butylbenzene ug/kg 431575 75 58-161ND
Styrene ug/kg 404575 70 60-148ND
tert-Butylbenzene ug/kg 421575 73 44-151ND
Tetrachloroethene ug/kg 361575 63 53-151ND
Toluene ug/kg 407575 68 52-14814.9
trans-1,2-Dichloroethene ug/kg 414575 72 60-148ND
trans-1,3-Dichloropropene ug/kg 382575 66 55-133ND
Trichloroethene ug/kg 422575 73 60-1483.8J
Trichlorofluoromethane ug/kg 274575 48 10-154ND
Vinyl acetate ug/kg 7031150 61 50-149ND
Vinyl chloride ug/kg 529575 92 57-157ND
Xylene (Total)ug/kg 12601730 72 52-1536.8J
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621510002
3745390SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621510002
3745390SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 6.5 6 306.9
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 4.4J 306.2
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 6.5J 306.9J
1,2-Dichloroethane-d4 (S)%10199
4-Bromofluorobenzene (S)%98101
Toluene-d8 (S)%99101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718519
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510003, 92621510008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3745569
Associated Lab Samples:92621510003, 92621510008
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/22/22 13:451.9
1,1,1-Trichloroethane ug/kg ND 5.0 08/22/22 13:452.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/22/22 13:451.3
1,1,2-Trichloroethane ug/kg ND 5.0 08/22/22 13:451.7
1,1-Dichloroethane ug/kg ND 5.0 08/22/22 13:452.1
1,1-Dichloroethene ug/kg ND 5.0 08/22/22 13:452.1
1,1-Dichloropropene ug/kg ND 5.0 08/22/22 13:452.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/22/22 13:454.0
1,2,3-Trichloropropane ug/kg ND 5.0 08/22/22 13:452.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/22/22 13:454.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/22/22 13:451.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/22/22 13:451.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/22/22 13:452.2
1,2-Dichlorobenzene ug/kg ND 5.0 08/22/22 13:451.8
1,2-Dichloroethane ug/kg ND 5.0 08/22/22 13:453.3
1,2-Dichloropropane ug/kg ND 5.0 08/22/22 13:451.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/22/22 13:451.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/22/22 13:451.6
1,3-Dichloropropane ug/kg ND 5.0 08/22/22 13:451.6
1,4-Dichlorobenzene ug/kg ND 5.0 08/22/22 13:451.3
2,2-Dichloropropane ug/kg ND 5.0 08/22/22 13:451.6
2-Butanone (MEK)ug/kg ND 100 08/22/22 13:4524.0
2-Chlorotoluene ug/kg ND 5.0 08/22/22 13:451.8
2-Hexanone ug/kg ND 50.0 08/22/22 13:454.8
4-Chlorotoluene ug/kg ND 5.0 08/22/22 13:450.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/22/22 13:454.8
Acetone ug/kg ND 100 08/22/22 13:4532.1
Benzene ug/kg ND 5.0 08/22/22 13:452.0
Bromobenzene ug/kg ND 5.0 08/22/22 13:451.6
Bromochloromethane ug/kg ND 5.0 08/22/22 13:451.5
Bromodichloromethane ug/kg ND 5.0 08/22/22 13:451.9
Bromoform ug/kg ND 5.0 08/22/22 13:451.8
Bromomethane ug/kg ND 10.0 08/22/22 13:457.9
Carbon tetrachloride ug/kg ND 5.0 08/22/22 13:451.9
Chlorobenzene ug/kg ND 5.0 08/22/22 13:450.96
Chloroethane ug/kg ND 10.0 08/22/22 13:453.9
Chloroform ug/kg ND 5.0 08/22/22 13:453.0
Chloromethane ug/kg ND 10.0 08/22/22 13:454.2
cis-1,2-Dichloroethene ug/kg ND 5.0 08/22/22 13:451.7
cis-1,3-Dichloropropene ug/kg ND 5.0 08/22/22 13:451.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3745569
Associated Lab Samples:92621510003, 92621510008
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 08/22/22 13:452.8
Dibromomethane ug/kg ND 5.0 08/22/22 13:451.1
Dichlorodifluoromethane ug/kg ND 10.0 IH,v108/22/22 13:452.2
Diisopropyl ether ug/kg ND 5.0 08/22/22 13:451.4
Ethylbenzene ug/kg ND 5.0 08/22/22 13:452.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/22/22 13:458.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/22/22 13:451.7
m&p-Xylene ug/kg ND 10.0 08/22/22 13:453.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/22/22 13:451.9
Methylene Chloride ug/kg ND 20.0 08/22/22 13:4513.7
n-Butylbenzene ug/kg ND 5.0 08/22/22 13:452.4
n-Propylbenzene ug/kg ND 5.0 08/22/22 13:451.8
Naphthalene ug/kg ND 5.0 08/22/22 13:452.6
o-Xylene ug/kg ND 5.0 08/22/22 13:452.2
p-Isopropyltoluene ug/kg ND 5.0 08/22/22 13:452.5
sec-Butylbenzene ug/kg ND 5.0 08/22/22 13:452.2
Styrene ug/kg ND 5.0 08/22/22 13:451.3
tert-Butylbenzene ug/kg ND 5.0 08/22/22 13:451.8
Tetrachloroethene ug/kg ND 5.0 08/22/22 13:451.6
Toluene ug/kg ND 5.0 08/22/22 13:451.4
trans-1,2-Dichloroethene ug/kg ND 5.0 08/22/22 13:451.8
trans-1,3-Dichloropropene ug/kg ND 5.0 08/22/22 13:451.7
Trichloroethene ug/kg ND 5.0 08/22/22 13:451.3
Trichlorofluoromethane ug/kg ND 5.0 08/22/22 13:452.8
Vinyl acetate ug/kg ND 50.0 08/22/22 13:453.6
Vinyl chloride ug/kg ND 10.0 08/22/22 13:452.5
Xylene (Total)ug/kg ND 10.0 08/22/22 13:452.8
1,2-Dichloroethane-d4 (S)%109 70-130 08/22/22 13:45
4-Bromofluorobenzene (S)%103 70-130 08/22/22 13:45
Toluene-d8 (S)%100 70-130 08/22/22 13:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745570LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13701250 110 70-130
1,1,1-Trichloroethane ug/kg 13401250 108 70-130
1,1,2,2-Tetrachloroethane ug/kg 12201250 98 70-130
1,1,2-Trichloroethane ug/kg 12701250 102 70-130
1,1-Dichloroethane ug/kg 13001250 104 70-130
1,1-Dichloroethene ug/kg 14601250 117 70-130
1,1-Dichloropropene ug/kg 13901250 111 70-130
1,2,3-Trichlorobenzene ug/kg 12501250 100 70-130
1,2,3-Trichloropropane ug/kg 12201250 98 70-130
1,2,4-Trichlorobenzene ug/kg 12401250 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745570LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13301250 106 70-130
1,2-Dibromo-3-chloropropane ug/kg 11201250 90 67-130
1,2-Dibromoethane (EDB)ug/kg 13001250 104 70-130
1,2-Dichlorobenzene ug/kg 12501250 100 70-130
1,2-Dichloroethane ug/kg 12701250 102 70-130
1,2-Dichloropropane ug/kg 13201250 106 70-130
1,3,5-Trimethylbenzene ug/kg 13601250 109 70-130
1,3-Dichlorobenzene ug/kg 12501250 100 70-130
1,3-Dichloropropane ug/kg 12701250 102 70-130
1,4-Dichlorobenzene ug/kg 12701250 101 70-130
2,2-Dichloropropane ug/kg 13201250 106 67-130
2-Butanone (MEK)ug/kg 23002500 92 66-130
2-Chlorotoluene ug/kg 13301250 106 70-130
2-Hexanone ug/kg 25102500 101 70-130
4-Chlorotoluene ug/kg 13101250 105 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 25702500 103 70-130
Acetone ug/kg 23002500 92 67-130
Benzene ug/kg 12701250 101 70-130
Bromobenzene ug/kg 12601250 101 70-130
Bromochloromethane ug/kg 13001250 104 70-130
Bromodichloromethane ug/kg 13601250 109 70-130
Bromoform ug/kg 13701250 109 70-130
Bromomethane ug/kg 13201250 106 53-175
Carbon tetrachloride ug/kg 14301250 114 70-130
Chlorobenzene ug/kg 13001250 104 70-130
Chloroethane ug/kg 13601250 109 70-135
Chloroform ug/kg 11801250 94 70-130
Chloromethane ug/kg 14801250 118 64-130
cis-1,2-Dichloroethene ug/kg 13301250 107 70-130
cis-1,3-Dichloropropene ug/kg 14001250 112 70-130
Dibromochloromethane ug/kg 13701250 109 70-130
Dibromomethane ug/kg 12801250 103 70-130
Dichlorodifluoromethane ug/kg 1950 IH,L1,v1125015663-145
Diisopropyl ether ug/kg 13601250 109 68-130
Ethylbenzene ug/kg 12501250 100 70-130
Hexachloro-1,3-butadiene ug/kg 12301250 99 70-130
Isopropylbenzene (Cumene)ug/kg 13001250 104 70-130
m&p-Xylene ug/kg 26702500 107 70-130
Methyl-tert-butyl ether ug/kg 12901250 103 70-130
Methylene Chloride ug/kg 12101250 97 67-130
n-Butylbenzene ug/kg 13301250 106 70-130
n-Propylbenzene ug/kg 13201250 105 70-130
Naphthalene ug/kg 12501250 100 70-130
o-Xylene ug/kg 13601250 109 70-130
p-Isopropyltoluene ug/kg 13601250 108 70-130
sec-Butylbenzene ug/kg 13201250 106 70-130
Styrene ug/kg 13801250 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745570LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12901250 103 64-130
Tetrachloroethene ug/kg 11501250 92 70-130
Toluene ug/kg 13101250 104 70-130
trans-1,2-Dichloroethene ug/kg 13801250 110 70-130
trans-1,3-Dichloropropene ug/kg 14101250 113 70-130
Trichloroethene ug/kg 13401250 107 70-130
Trichlorofluoromethane ug/kg 14201250 114 70-130
Vinyl acetate ug/kg 25102500 101 70-134
Vinyl chloride ug/kg 13701250 110 68-130
Xylene (Total)ug/kg 40303750 107 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3745571MATRIX SPIKE SAMPLE:
MSSpike
Result
92621514007
1,1,1,2-Tetrachloroethane ug/kg 580625 93 58-140ND
1,1,1-Trichloroethane ug/kg 616625 99 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 492625 79 52-139ND
1,1,2-Trichloroethane ug/kg 572625 92 56-140ND
1,1-Dichloroethane ug/kg 565625 90 58-145ND
1,1-Dichloroethene ug/kg 651625 104 57-158ND
1,1-Dichloropropene ug/kg 655625 105 58-151ND
1,2,3-Trichlorobenzene ug/kg 252 M16254048-149ND
1,2,3-Trichloropropane ug/kg 436625 70 54-132ND
1,2,4-Trichlorobenzene ug/kg 424625 68 51-151ND
1,2,4-Trimethylbenzene ug/kg 628625 100 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 350625 56 44-134ND
1,2-Dibromoethane (EDB)ug/kg 553625 88 60-138ND
1,2-Dichlorobenzene ug/kg 620625 99 59-147ND
1,2-Dichloroethane ug/kg 552625 88 57-139ND
1,2-Dichloropropane ug/kg 594625 95 62-145ND
1,3,5-Trimethylbenzene ug/kg 651625 104 47-159ND
1,3-Dichlorobenzene ug/kg 613625 98 58-144ND
1,3-Dichloropropane ug/kg 550625 88 60-142ND
1,4-Dichlorobenzene ug/kg 609625 98 57-143ND
2,2-Dichloropropane ug/kg 316625 51 37-144ND
2-Butanone (MEK)ug/kg 8231250 65 28-146ND
2-Chlorotoluene ug/kg 607625 97 55-158ND
2-Hexanone ug/kg 8481250 68 44-141ND
4-Chlorotoluene ug/kg 611625 98 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 9291250 74 50-138ND
Acetone ug/kg 8411250 67 20-136ND
Benzene ug/kg 609625 97 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3745571MATRIX SPIKE SAMPLE:
MSSpike
Result
92621514007
Bromobenzene ug/kg 622625 99 59-145ND
Bromochloromethane ug/kg 588625 94 57-143ND
Bromodichloromethane ug/kg 537625 86 53-133ND
Bromoform ug/kg 451625 72 48-133ND
Bromomethane ug/kg 684625 109 10-167ND
Carbon tetrachloride ug/kg 633625 101 57-147ND
Chlorobenzene ug/kg 627625 100 61-144ND
Chloroethane ug/kg 470625 75 10-153ND
Chloroform ug/kg 526625 84 58-141ND
Chloromethane ug/kg 643625 103 54-165ND
cis-1,2-Dichloroethene ug/kg 586625 94 59-144ND
cis-1,3-Dichloropropene ug/kg 513625 82 56-137ND
Dibromochloromethane ug/kg 500625 80 53-139ND
Dibromomethane ug/kg 608625 97 60-136ND
Dichlorodifluoromethane ug/kg 892 IH,v162514349-177ND
Diisopropyl ether ug/kg 552625 88 53-136ND
Ethylbenzene ug/kg 586625 94 53-150ND
Hexachloro-1,3-butadiene ug/kg 593625 95 42-186ND
Isopropylbenzene (Cumene)ug/kg 632625 101 62-154ND
m&p-Xylene ug/kg 12601250 100 49-156ND
Methyl-tert-butyl ether ug/kg 565625 90 54-133ND
Methylene Chloride ug/kg 450625 72 50-153ND
n-Butylbenzene ug/kg 602625 96 44-174ND
n-Propylbenzene ug/kg 601625 96 52-157ND
Naphthalene ug/kg 264625 42 37-150ND
o-Xylene ug/kg 639625 102 54-150ND
p-Isopropyltoluene ug/kg 662625 106 50-164ND
sec-Butylbenzene ug/kg 652625 104 58-161ND
Styrene ug/kg 619625 99 60-148ND
tert-Butylbenzene ug/kg 641625 103 44-151ND
Tetrachloroethene ug/kg 590625 94 53-151ND
Toluene ug/kg 639625 102 52-148ND
trans-1,2-Dichloroethene ug/kg 600625 96 60-148ND
trans-1,3-Dichloropropene ug/kg 500625 80 55-133ND
Trichloroethene ug/kg 690625 110 60-148ND
Trichlorofluoromethane ug/kg 462625 74 10-154ND
Vinyl acetate ug/kg 8801250 70 50-149ND
Vinyl chloride ug/kg 758625 121 57-157ND
Xylene (Total)ug/kg 18901870 101 52-153ND
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621514008
3745572SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH,v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621514008
3745572SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 308.8
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 308.8J
1,2-Dichloroethane-d4 (S)%9695
4-Bromofluorobenzene (S)%9796
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
719094
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510009, 92621510010, 92621510011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3748233
Associated Lab Samples:92621510009, 92621510010, 92621510011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/23/22 13:420.31
1,1,1-Trichloroethane ug/L ND 1.0 08/23/22 13:420.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/23/22 13:420.22
1,1,2-Trichloroethane ug/L ND 1.0 08/23/22 13:420.32
1,1-Dichloroethane ug/L ND 1.0 08/23/22 13:420.37
1,1-Dichloroethene ug/L ND 1.0 08/23/22 13:420.35
1,1-Dichloropropene ug/L ND 1.0 08/23/22 13:420.43
1,2,3-Trichlorobenzene ug/L ND 1.0 08/23/22 13:420.81
1,2,3-Trichloropropane ug/L ND 1.0 08/23/22 13:420.26
1,2,4-Trichlorobenzene ug/L ND 1.0 08/23/22 13:420.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/23/22 13:420.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/23/22 13:420.27
1,2-Dichlorobenzene ug/L ND 1.0 08/23/22 13:420.34
1,2-Dichloroethane ug/L ND 1.0 08/23/22 13:420.32
1,2-Dichloropropane ug/L ND 1.0 08/23/22 13:420.36
1,3-Dichlorobenzene ug/L ND 1.0 08/23/22 13:420.34
1,3-Dichloropropane ug/L ND 1.0 08/23/22 13:420.28
1,4-Dichlorobenzene ug/L ND 1.0 08/23/22 13:420.33
2,2-Dichloropropane ug/L ND 1.0 08/23/22 13:420.39
2-Butanone (MEK)ug/L ND 5.0 08/23/22 13:424.0
2-Chlorotoluene ug/L ND 1.0 08/23/22 13:420.32
2-Hexanone ug/L ND 5.0 08/23/22 13:420.48
4-Chlorotoluene ug/L ND 1.0 08/23/22 13:420.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/23/22 13:422.7
Acetone ug/L ND 25.0 08/23/22 13:425.1
Benzene ug/L ND 1.0 08/23/22 13:420.34
Bromobenzene ug/L ND 1.0 08/23/22 13:420.29
Bromochloromethane ug/L ND 1.0 08/23/22 13:420.47
Bromodichloromethane ug/L ND 1.0 08/23/22 13:420.31
Bromoform ug/L ND 1.0 08/23/22 13:420.34
Bromomethane ug/L ND 2.0 IH,IK08/23/22 13:421.7
Carbon tetrachloride ug/L ND 1.0 08/23/22 13:420.33
Chlorobenzene ug/L ND 1.0 08/23/22 13:420.28
Chloroethane ug/L ND 1.0 08/23/22 13:420.65
Chloroform ug/L ND 1.0 08/23/22 13:420.43
Chloromethane ug/L ND 1.0 v208/23/22 13:420.54
cis-1,2-Dichloroethene ug/L ND 1.0 08/23/22 13:420.38
cis-1,3-Dichloropropene ug/L ND 1.0 08/23/22 13:420.36
Dibromochloromethane ug/L ND 1.0 08/23/22 13:420.36
Dibromomethane ug/L ND 1.0 08/23/22 13:420.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3748233
Associated Lab Samples:92621510009, 92621510010, 92621510011
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 08/23/22 13:420.35
Diisopropyl ether ug/L ND 1.0 08/23/22 13:420.31
Ethylbenzene ug/L ND 1.0 08/23/22 13:420.30
Hexachloro-1,3-butadiene ug/L ND 2.0 08/23/22 13:421.5
m&p-Xylene ug/L ND 2.0 08/23/22 13:420.71
Methyl-tert-butyl ether ug/L ND 1.0 08/23/22 13:420.42
Methylene Chloride ug/L ND 5.0 08/23/22 13:422.0
Naphthalene ug/L ND 1.0 08/23/22 13:420.64
o-Xylene ug/L ND 1.0 08/23/22 13:420.34
p-Isopropyltoluene ug/L ND 1.0 08/23/22 13:420.41
Styrene ug/L ND 1.0 08/23/22 13:420.29
Tetrachloroethene ug/L ND 1.0 08/23/22 13:420.29
Toluene ug/L ND 1.0 08/23/22 13:420.48
trans-1,2-Dichloroethene ug/L ND 1.0 08/23/22 13:420.40
trans-1,3-Dichloropropene ug/L ND 1.0 08/23/22 13:420.36
Trichloroethene ug/L ND 1.0 08/23/22 13:420.38
Trichlorofluoromethane ug/L ND 1.0 08/23/22 13:420.30
Vinyl acetate ug/L ND 2.0 08/23/22 13:421.3
Vinyl chloride ug/L ND 1.0 08/23/22 13:420.39
Xylene (Total)ug/L ND 1.0 08/23/22 13:420.34
1,2-Dichloroethane-d4 (S)%109 70-130 08/23/22 13:42
4-Bromofluorobenzene (S)%105 70-130 08/23/22 13:42
Toluene-d8 (S)%101 70-130 08/23/22 13:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3748234LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.050 108 70-130
1,1,1-Trichloroethane ug/L 52.850 106 70-130
1,1,2,2-Tetrachloroethane ug/L 47.150 94 70-130
1,1,2-Trichloroethane ug/L 49.650 99 70-130
1,1-Dichloroethane ug/L 48.050 96 70-130
1,1-Dichloroethene ug/L 52.050 104 70-132
1,1-Dichloropropene ug/L 51.850 104 70-131
1,2,3-Trichlorobenzene ug/L 50.350 101 70-134
1,2,3-Trichloropropane ug/L 49.450 99 70-130
1,2,4-Trichlorobenzene ug/L 51.550 103 70-130
1,2-Dibromo-3-chloropropane ug/L 48.750 97 70-132
1,2-Dibromoethane (EDB)ug/L 51.150 102 70-130
1,2-Dichlorobenzene ug/L 50.550 101 70-130
1,2-Dichloroethane ug/L 54.250 108 70-130
1,2-Dichloropropane ug/L 49.950 100 70-130
1,3-Dichlorobenzene ug/L 50.450 101 70-130
1,3-Dichloropropane ug/L 49.750 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3748234LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 49.650 99 70-130
2,2-Dichloropropane ug/L 53.350 107 70-130
2-Butanone (MEK)ug/L 87.8100 88 70-133
2-Chlorotoluene ug/L 49.850 100 70-130
2-Hexanone ug/L 98.6100 99 70-130
4-Chlorotoluene ug/L 50.050 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 98.8100 99 70-130
Acetone ug/L 88.1100 88 70-144
Benzene ug/L 46.350 93 70-130
Bromobenzene ug/L 48.250 96 70-130
Bromochloromethane ug/L 49.550 99 70-130
Bromodichloromethane ug/L 56.150 112 70-130
Bromoform ug/L 53.550 107 70-131
Bromomethane ug/L 61.3 IH,IK5012330-177
Carbon tetrachloride ug/L 57.250 114 70-130
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 47.850 96 46-131
Chloroform ug/L 47.450 95 70-130
Chloromethane ug/L 40.5 v3508149-130
cis-1,2-Dichloroethene ug/L 51.750 103 70-130
cis-1,3-Dichloropropene ug/L 51.350 103 70-130
Dibromochloromethane ug/L 54.250 108 70-130
Dibromomethane ug/L 52.850 106 70-130
Dichlorodifluoromethane ug/L 47.850 96 52-134
Diisopropyl ether ug/L 51.150 102 70-131
Ethylbenzene ug/L 51.150 102 70-130
Hexachloro-1,3-butadiene ug/L 53.650 107 70-131
m&p-Xylene ug/L 105100 105 70-130
Methyl-tert-butyl ether ug/L 49.850 100 70-130
Methylene Chloride ug/L 40.350 81 68-130
Naphthalene ug/L 50.650 101 70-133
o-Xylene ug/L 50.750 101 70-130
p-Isopropyltoluene ug/L 51.550 103 70-130
Styrene ug/L 51.450 103 70-130
Tetrachloroethene ug/L 48.250 96 70-130
Toluene ug/L 46.650 93 70-130
trans-1,2-Dichloroethene ug/L 50.750 101 70-130
trans-1,3-Dichloropropene ug/L 53.250 106 70-130
Trichloroethene ug/L 49.750 99 70-130
Trichlorofluoromethane ug/L 50.450 101 61-130
Vinyl acetate ug/L 105100 105 70-140
Vinyl chloride ug/L 46.250 92 59-142
Xylene (Total)ug/L 155150 104 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3748236MATRIX SPIKE SAMPLE:
MSSpike
Result
92621510010
1,1,1,2-Tetrachloroethane ug/L 25.320 126 70-135ND
1,1,1-Trichloroethane ug/L 25.620 128 70-148ND
1,1,2,2-Tetrachloroethane ug/L 21.920 109 70-131ND
1,1,2-Trichloroethane ug/L 21.720 108 70-136ND
1,1-Dichloroethane ug/L 22.620 113 70-147ND
1,1-Dichloroethene ug/L 25.620 128 70-158ND
1,1-Dichloropropene ug/L 23.920 120 70-149ND
1,2,3-Trichlorobenzene ug/L 20.720 104 68-140ND
1,2,3-Trichloropropane ug/L 22.020 110 67-137ND
1,2,4-Trichlorobenzene ug/L 20.920 104 70-139ND
1,2-Dibromo-3-chloropropane ug/L 22.020 110 69-136ND
1,2-Dibromoethane (EDB)ug/L 22.420 112 70-137ND
1,2-Dichlorobenzene ug/L 22.220 111 70-133ND
1,2-Dichloroethane ug/L 25.620 128 67-138ND
1,2-Dichloropropane ug/L 23.320 116 70-138ND
1,3-Dichlorobenzene ug/L 22.520 113 70-133ND
1,3-Dichloropropane ug/L 22.420 112 70-136ND
1,4-Dichlorobenzene ug/L 21.520 108 70-133ND
2,2-Dichloropropane ug/L 24.720 124 52-155ND
2-Butanone (MEK)ug/L 41.540 104 61-147ND
2-Chlorotoluene ug/L 22.220 111 70-141ND
2-Hexanone ug/L 46.440 116 67-139ND
4-Chlorotoluene ug/L 22.420 112 70-135ND
4-Methyl-2-pentanone (MIBK)ug/L 45.840 115 67-136ND
Acetone ug/L 41.840 105 55-159ND
Benzene ug/L 21.620 108 67-150ND
Bromobenzene ug/L 22.020 110 70-134ND
Bromochloromethane ug/L 23.020 115 70-146ND
Bromodichloromethane ug/L 25.420 127 70-138ND
Bromoform ug/L 23.920 119 57-138ND
Bromomethane ug/L 19.7 IH,IK209910-200ND
Carbon tetrachloride ug/L 28.120 141 70-147ND
Chlorobenzene ug/L 22.820 114 70-137ND
Chloroethane ug/L 23.220 116 51-166ND
Chloroform ug/L 21.820 109 70-144ND
Chloromethane ug/L 19.4 v3209724-161ND
cis-1,2-Dichloroethene ug/L 24.020 120 67-148ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-142ND
Dibromochloromethane ug/L 24.120 120 68-138ND
Dibromomethane ug/L 24.920 125 70-134ND
Dichlorodifluoromethane ug/L 22.920 114 43-155ND
Diisopropyl ether ug/L 23.120 116 65-146ND
Ethylbenzene ug/L 23.320 116 68-143ND
Hexachloro-1,3-butadiene ug/L 22.520 113 62-151ND
m&p-Xylene ug/L 48.640 122 53-157ND
Methyl-tert-butyl ether ug/L 21.920 110 59-156ND
Methylene Chloride ug/L 15.320 76 64-148ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3748236MATRIX SPIKE SAMPLE:
MSSpike
Result
92621510010
Naphthalene ug/L 21.120 106 57-150ND
o-Xylene ug/L 23.020 115 68-143ND
p-Isopropyltoluene ug/L 22.220 111 70-141ND
Styrene ug/L 23.420 117 70-136ND
Tetrachloroethene ug/L 22.320 111 70-139ND
Toluene ug/L 21.620 108 47-157ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-149ND
trans-1,3-Dichloropropene ug/L 24.120 121 70-138ND
Trichloroethene ug/L 23.320 116 70-149ND
Trichlorofluoromethane ug/L 24.520 123 61-154ND
Vinyl acetate ug/L 46.240 115 48-156ND
Vinyl chloride ug/L 22.320 111 55-172ND
Xylene (Total)ug/L 71.760 119 66-145ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621510009
3748235SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621510009
3748235SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND IH,IK30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND v230ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%111111
4-Bromofluorobenzene (S)%103101
Toluene-d8 (S)%10098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
719554
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3750130
Associated Lab Samples:92621510012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/25/22 12:370.31
1,1,1-Trichloroethane ug/L ND 1.0 08/25/22 12:370.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/25/22 12:370.22
1,1,2-Trichloroethane ug/L ND 1.0 08/25/22 12:370.32
1,1-Dichloroethane ug/L ND 1.0 08/25/22 12:370.37
1,1-Dichloroethene ug/L ND 1.0 08/25/22 12:370.35
1,1-Dichloropropene ug/L ND 1.0 08/25/22 12:370.43
1,2,3-Trichlorobenzene ug/L ND 1.0 08/25/22 12:370.81
1,2,3-Trichloropropane ug/L ND 1.0 08/25/22 12:370.26
1,2,4-Trichlorobenzene ug/L ND 1.0 08/25/22 12:370.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/25/22 12:370.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/25/22 12:370.27
1,2-Dichlorobenzene ug/L ND 1.0 08/25/22 12:370.34
1,2-Dichloroethane ug/L ND 1.0 08/25/22 12:370.32
1,2-Dichloropropane ug/L ND 1.0 08/25/22 12:370.36
1,3-Dichlorobenzene ug/L ND 1.0 08/25/22 12:370.34
1,3-Dichloropropane ug/L ND 1.0 08/25/22 12:370.28
1,4-Dichlorobenzene ug/L ND 1.0 08/25/22 12:370.33
2,2-Dichloropropane ug/L ND 1.0 08/25/22 12:370.39
2-Butanone (MEK)ug/L ND 5.0 08/25/22 12:374.0
2-Chlorotoluene ug/L ND 1.0 08/25/22 12:370.32
2-Hexanone ug/L ND 5.0 08/25/22 12:370.48
4-Chlorotoluene ug/L ND 1.0 08/25/22 12:370.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/25/22 12:372.7
Acetone ug/L ND 25.0 08/25/22 12:375.1
Benzene ug/L ND 1.0 08/25/22 12:370.34
Bromobenzene ug/L ND 1.0 08/25/22 12:370.29
Bromochloromethane ug/L ND 1.0 08/25/22 12:370.47
Bromodichloromethane ug/L ND 1.0 08/25/22 12:370.31
Bromoform ug/L ND 1.0 08/25/22 12:370.34
Bromomethane ug/L ND 2.0 v208/25/22 12:371.7
Carbon tetrachloride ug/L ND 1.0 08/25/22 12:370.33
Chlorobenzene ug/L ND 1.0 08/25/22 12:370.28
Chloroethane ug/L ND 1.0 08/25/22 12:370.65
Chloroform ug/L ND 1.0 08/25/22 12:370.43
Chloromethane ug/L ND 1.0 08/25/22 12:370.54
cis-1,2-Dichloroethene ug/L ND 1.0 08/25/22 12:370.38
cis-1,3-Dichloropropene ug/L ND 1.0 08/25/22 12:370.36
Dibromochloromethane ug/L ND 1.0 08/25/22 12:370.36
Dibromomethane ug/L ND 1.0 08/25/22 12:370.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3750130
Associated Lab Samples:92621510012
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 08/25/22 12:370.35
Diisopropyl ether ug/L ND 1.0 08/25/22 12:370.31
Ethylbenzene ug/L ND 1.0 08/25/22 12:370.30
Hexachloro-1,3-butadiene ug/L ND 2.0 08/25/22 12:371.5
m&p-Xylene ug/L ND 2.0 08/25/22 12:370.71
Methyl-tert-butyl ether ug/L ND 1.0 08/25/22 12:370.42
Methylene Chloride ug/L ND 5.0 08/25/22 12:372.0
Naphthalene ug/L ND 1.0 v108/25/22 12:370.64
o-Xylene ug/L ND 1.0 08/25/22 12:370.34
p-Isopropyltoluene ug/L ND 1.0 08/25/22 12:370.41
Styrene ug/L ND 1.0 08/25/22 12:370.29
Tetrachloroethene ug/L ND 1.0 08/25/22 12:370.29
Toluene ug/L ND 1.0 08/25/22 12:370.48
trans-1,2-Dichloroethene ug/L ND 1.0 08/25/22 12:370.40
trans-1,3-Dichloropropene ug/L ND 1.0 08/25/22 12:370.36
Trichloroethene ug/L ND 1.0 08/25/22 12:370.38
Trichlorofluoromethane ug/L ND 1.0 08/25/22 12:370.30
Vinyl acetate ug/L ND 2.0 08/25/22 12:371.3
Vinyl chloride ug/L ND 1.0 08/25/22 12:370.39
Xylene (Total)ug/L ND 1.0 08/25/22 12:370.34
1,2-Dichloroethane-d4 (S)%100 70-130 08/25/22 12:37
4-Bromofluorobenzene (S)%98 70-130 08/25/22 12:37
Toluene-d8 (S)%100 70-130 08/25/22 12:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3750131LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.150 112 70-130
1,1,1-Trichloroethane ug/L 46.050 92 70-130
1,1,2,2-Tetrachloroethane ug/L 52.650 105 70-130
1,1,2-Trichloroethane ug/L 50.950 102 70-130
1,1-Dichloroethane ug/L 43.350 87 70-130
1,1-Dichloroethene ug/L 43.650 87 70-132
1,1-Dichloropropene ug/L 50.850 102 70-131
1,2,3-Trichlorobenzene ug/L 58.950 118 70-134
1,2,3-Trichloropropane ug/L 51.850 104 70-130
1,2,4-Trichlorobenzene ug/L 58.550 117 70-130
1,2-Dibromo-3-chloropropane ug/L 58.050 116 70-132
1,2-Dibromoethane (EDB)ug/L 54.650 109 70-130
1,2-Dichlorobenzene ug/L 56.650 113 70-130
1,2-Dichloroethane ug/L 43.950 88 70-130
1,2-Dichloropropane ug/L 50.750 101 70-130
1,3-Dichlorobenzene ug/L 56.350 113 70-130
1,3-Dichloropropane ug/L 55.150 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3750131LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 55.550 111 70-130
2,2-Dichloropropane ug/L 47.450 95 70-130
2-Butanone (MEK)ug/L 88.9100 89 70-133
2-Chlorotoluene ug/L 56.450 113 70-130
2-Hexanone ug/L 114100 114 70-130
4-Chlorotoluene ug/L 56.250 112 70-130
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-130
Acetone ug/L 83.2100 83 70-144
Benzene ug/L 47.350 95 70-130
Bromobenzene ug/L 55.750 111 70-130
Bromochloromethane ug/L 45.850 92 70-130
Bromodichloromethane ug/L 50.950 102 70-130
Bromoform ug/L 56.550 113 70-131
Bromomethane ug/L 35.2 v3507030-177
Carbon tetrachloride ug/L 48.950 98 70-130
Chlorobenzene ug/L 52.750 105 70-130
Chloroethane ug/L 48.050 96 46-131
Chloroform ug/L 45.850 92 70-130
Chloromethane ug/L 45.050 90 49-130
cis-1,2-Dichloroethene ug/L 43.550 87 70-130
cis-1,3-Dichloropropene ug/L 54.050 108 70-130
Dibromochloromethane ug/L 56.850 114 70-130
Dibromomethane ug/L 48.150 96 70-130
Dichlorodifluoromethane ug/L 47.650 95 52-134
Diisopropyl ether ug/L 47.650 95 70-131
Ethylbenzene ug/L 53.050 106 70-130
Hexachloro-1,3-butadiene ug/L 57.650 115 70-131
m&p-Xylene ug/L 107100 107 70-130
Methyl-tert-butyl ether ug/L 47.150 94 70-130
Methylene Chloride ug/L 41.650 83 68-130
Naphthalene ug/L 60.8 v15012270-133
o-Xylene ug/L 53.150 106 70-130
p-Isopropyltoluene ug/L 59.750 119 70-130
Styrene ug/L 54.050 108 70-130
Tetrachloroethene ug/L 53.050 106 70-130
Toluene ug/L 46.650 93 70-130
trans-1,2-Dichloroethene ug/L 45.250 90 70-130
trans-1,3-Dichloropropene ug/L 53.850 108 70-130
Trichloroethene ug/L 51.850 104 70-130
Trichlorofluoromethane ug/L 41.650 83 61-130
Vinyl acetate ug/L 91.4100 91 70-140
Vinyl chloride ug/L 47.650 95 59-142
Xylene (Total)ug/L 160150 106 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3750132MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92622251004
3750133
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 70-135114 7 3020ND21.4 22.8
1,1,1-Trichloroethane ug/L 20 94 70-148101 7 3020ND19.4 20.8
1,1,2,2-Tetrachloroethane ug/L 20 106 70-131111 4 3020ND21.3 22.2
1,1,2-Trichloroethane ug/L 20 97 70-136103 7 3020ND19.4 20.7
1,1-Dichloroethane ug/L M120470-14727 3 3020134135140
1,1-Dichloroethene ug/L M1,v320-18 70-1586 3 3020147143148
1,1-Dichloropropene ug/L 20 101 70-149105 4 3020ND20.2 21.0
1,2,3-Trichlorobenzene ug/L 20 129 68-140133 3 3020ND25.8 26.5
1,2,3-Trichloropropane ug/L 20 104 67-137109 5 3020ND20.8 21.8
1,2,4-Trichlorobenzene ug/L 20 130 70-139131 1 3020ND25.9 26.3
1,2-Dibromo-3-
chloropropane ug/L 20 111 69-136118 6 3020ND22.2 23.6
1,2-Dibromoethane (EDB)ug/L 20 108 70-137112 4 3020ND21.6 22.5
1,2-Dichlorobenzene ug/L 20 118 70-133126 6 3020ND23.7 25.1
1,2-Dichloroethane ug/L 20 86 67-13892 7 3020ND17.2 18.4
1,2-Dichloropropane ug/L 20 100 70-138108 7 3020ND20.0 21.5
1,3-Dichlorobenzene ug/L 20 121 70-133126 4 3020ND24.2 25.2
1,3-Dichloropropane ug/L 20 107 70-136112 5 3020ND21.4 22.4
1,4-Dichlorobenzene ug/L 20 119 70-133128 7 3020ND23.8 25.6
2,2-Dichloropropane ug/L 20 99 52-155107 8 3020ND19.8 21.3
2-Butanone (MEK)ug/L 40 83 61-14784 1 3040ND33.1 33.5
2-Chlorotoluene ug/L 20 118 70-141126 7 3020ND23.6 25.2
2-Hexanone ug/L 40 114 67-139115 1 3040ND45.5 45.9
4-Chlorotoluene ug/L 20 119 70-135127 6 3020ND23.7 25.3
4-Methyl-2-pentanone
(MIBK)ug/L 40 97 67-136100 3 3040ND39.0 40.1
Acetone ug/L v3408755-15990 3 3040ND34.9 36.1
Benzene ug/L 20 95 67-15099 5 3020ND19.0 19.9
Bromobenzene ug/L 20 115 70-134121 5 3020ND23.0 24.2
Bromochloromethane ug/L 20 94 70-146101 7 3020ND18.9 20.2
Bromodichloromethane ug/L 20 96 70-138104 8 3020ND19.2 20.8
Bromoform ug/L 20 106 57-138111 5 3020ND21.1 22.3
Bromomethane ug/L v3207810-20079 2 3020ND15.5 15.9
Carbon tetrachloride ug/L 20 100 70-147108 8 3020ND20.0 21.6
Chlorobenzene ug/L 20 110 70-137122 10 3020ND22.1 24.3
Chloroethane ug/L 20 101 51-166109 8 3020ND20.2 21.9
Chloroform ug/L 20 93 70-144100 7 3020ND18.7 20.0
Chloromethane ug/L v32010024-161107 7 3020ND20.0 21.5
cis-1,2-Dichloroethene ug/L 20 86 67-14894 7 30206.4 23.6 25.3
cis-1,3-Dichloropropene ug/L 20 98 70-142104 6 3020ND19.6 20.8
Dibromochloromethane ug/L 20 104 68-138112 7 3020ND20.9 22.4
Dibromomethane ug/L 20 101 70-134108 7 3020ND20.2 21.6
Dichlorodifluoromethane ug/L 20 97 43-155107 9 3020ND19.4 21.3
Diisopropyl ether ug/L 20 88 65-14694 7 3020ND17.5 18.9
Ethylbenzene ug/L 20 113 68-143121 7 3020ND22.6 24.3
Hexachloro-1,3-butadiene ug/L 20 133 62-151139 4 3020ND26.7 27.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3750132MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92622251004
3750133
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 115 53-157122 6 3040ND46.0 48.9
Methyl-tert-butyl ether ug/L 20 86 59-15692 6 3020ND17.2 18.3
Methylene Chloride ug/L 20 77 64-14885 9 3020ND15.5 16.9
Naphthalene ug/L 20 133 57-150133 0 3020ND26.5 26.6
o-Xylene ug/L 20 112 68-143120 7 3020ND22.4 24.0
p-Isopropyltoluene ug/L 20 135 70-141139 2 3020ND27.0 27.7
Styrene ug/L 20 112 70-136120 7 3020ND22.4 24.1
Tetrachloroethene ug/L 20 114 70-139120 6 3020ND22.7 24.1
Toluene ug/L 20 97 47-157105 7 3020ND19.5 20.9
trans-1,2-Dichloroethene ug/L 20 94 70-149102 8 3020ND18.8 20.5
trans-1,3-Dichloropropene ug/L 20 98 70-138104 6 3020ND19.6 20.7
Trichloroethene ug/L 20 110 70-149119 5 302017.2 39.1 41.1
Trichlorofluoromethane ug/L 20 85 61-15491 7 3020ND17.0 18.2
Vinyl acetate ug/L 40 81 48-15687 6 3040ND32.6 34.6
Vinyl chloride ug/L 20 101 55-172110 7 3020ND20.9 22.6
Xylene (Total)ug/L 60 114 66-145122 6 3060ND68.5 72.9
1,2-Dichloroethane-d4 (S)%90 70-13089
4-Bromofluorobenzene (S)%95 70-13096
Toluene-d8 (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718547
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave PAH
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510001, 92621510002, 92621510003, 92621510004, 92621510005, 92621510006, 92621510007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3745668
Associated Lab Samples:92621510001, 92621510002, 92621510003, 92621510004, 92621510005, 92621510006, 92621510007
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 325 08/23/22 09:53114
2-Methylnaphthalene ug/kg ND 325 08/23/22 09:53130
Acenaphthene ug/kg ND 325 08/23/22 09:53114
Acenaphthylene ug/kg ND 325 08/23/22 09:53114
Anthracene ug/kg ND 325 08/23/22 09:53106
Benzo(a)anthracene ug/kg ND 325 08/23/22 09:53108
Benzo(a)pyrene ug/kg ND 325 08/23/22 09:53112
Benzo(b)fluoranthene ug/kg ND 325 08/23/22 09:53108
Benzo(g,h,i)perylene ug/kg ND 325 08/23/22 09:53126
Benzo(k)fluoranthene ug/kg ND 325 08/23/22 09:53114
Chrysene ug/kg ND 325 08/23/22 09:53118
Dibenz(a,h)anthracene ug/kg ND 325 08/23/22 09:53125
Fluoranthene ug/kg ND 325 08/23/22 09:53111
Fluorene ug/kg ND 325 08/23/22 09:53114
Indeno(1,2,3-cd)pyrene ug/kg ND 325 08/23/22 09:53128
Naphthalene ug/kg ND 325 08/23/22 09:53110
Phenanthrene ug/kg ND 325 08/23/22 09:53106
Pyrene ug/kg ND 325 08/23/22 09:53132
2-Fluorobiphenyl (S)%37 19-130 08/23/22 09:53
Nitrobenzene-d5 (S)%37 21-130 08/23/22 09:53
Terphenyl-d14 (S)%78 15-130 08/23/22 09:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745669LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 11501670 69 54-130
2-Methylnaphthalene ug/kg 11101670 67 57-130
Acenaphthene ug/kg 12201670 73 56-130
Acenaphthylene ug/kg 13601670 82 58-130
Anthracene ug/kg 11101670 67 60-130
Benzo(a)anthracene ug/kg 11901670 72 59-130
Benzo(a)pyrene ug/kg 15101670 90 57-130
Benzo(b)fluoranthene ug/kg 14901670 89 54-130
Benzo(g,h,i)perylene ug/kg 15901670 95 59-130
Benzo(k)fluoranthene ug/kg 13501670 81 54-130
Chrysene ug/kg 13001670 78 57-130
Dibenz(a,h)anthracene ug/kg 15301670 92 60-130
Fluoranthene ug/kg 13101670 79 57-130
Fluorene ug/kg 12301670 74 56-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3745669LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/kg 15701670 94 61-130
Naphthalene ug/kg 11101670 66 56-130
Phenanthrene ug/kg 12501670 75 60-130
Pyrene ug/kg 12701670 76 61-130
2-Fluorobiphenyl (S)%73 19-130
Nitrobenzene-d5 (S)%66 21-130
Terphenyl-d14 (S)%76 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3745670MATRIX SPIKE SAMPLE:
MSSpike
Result
92621173001
1-Methylnaphthalene ug/kg 14202050 69 30-130ND
2-Methylnaphthalene ug/kg 13602050 66 29-130ND
Acenaphthene ug/kg 15002050 73 29-130ND
Acenaphthylene ug/kg 17202050 83 31-130ND
Anthracene ug/kg 15302050 74 33-130ND
Benzo(a)anthracene ug/kg 16302050 79 32-130ND
Benzo(a)pyrene ug/kg 20102050 98 32-130ND
Benzo(b)fluoranthene ug/kg 19802050 96 33-130ND
Benzo(g,h,i)perylene ug/kg 20602050 100 28-130ND
Benzo(k)fluoranthene ug/kg 18202050 89 31-130ND
Chrysene ug/kg 17702050 86 30-130ND
Dibenz(a,h)anthracene ug/kg 20402050 99 27-130ND
Fluoranthene ug/kg 17902050 87 26-130ND
Fluorene ug/kg 16002050 78 31-130ND
Indeno(1,2,3-cd)pyrene ug/kg 20702050 101 28-130ND
Naphthalene ug/kg 13002050 63 30-130ND
Phenanthrene ug/kg 16902050 82 34-130ND
Pyrene ug/kg 16902050 82 31-130ND
2-Fluorobiphenyl (S)%68 19-130
Nitrobenzene-d5 (S)%60 21-130
Terphenyl-d14 (S)%80 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621173002
3745671SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621173002
3745671SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%7533
Nitrobenzene-d5 (S)%7435
Terphenyl-d14 (S)%8775
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
720229
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave PAH
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3753313
Associated Lab Samples:92621510008
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 330 08/30/22 09:31116
2-Methylnaphthalene ug/kg ND 330 08/30/22 09:31132
Acenaphthene ug/kg ND 330 08/30/22 09:31116
Acenaphthylene ug/kg ND 330 08/30/22 09:31116
Anthracene ug/kg ND 330 08/30/22 09:31108
Benzo(a)anthracene ug/kg ND 330 08/30/22 09:31110
Benzo(a)pyrene ug/kg ND 330 08/30/22 09:31114
Benzo(b)fluoranthene ug/kg ND 330 08/30/22 09:31110
Benzo(g,h,i)perylene ug/kg ND 330 08/30/22 09:31128
Benzo(k)fluoranthene ug/kg ND 330 08/30/22 09:31116
Chrysene ug/kg ND 330 08/30/22 09:31120
Dibenz(a,h)anthracene ug/kg ND 330 08/30/22 09:31127
Fluoranthene ug/kg ND 330 08/30/22 09:31113
Fluorene ug/kg ND 330 08/30/22 09:31116
Indeno(1,2,3-cd)pyrene ug/kg ND 330 08/30/22 09:31130
Naphthalene ug/kg ND 330 08/30/22 09:31112
Phenanthrene ug/kg ND 330 08/30/22 09:31108
Pyrene ug/kg ND 330 08/30/22 09:31134
2-Fluorobiphenyl (S)%49 19-130 08/30/22 09:31
Nitrobenzene-d5 (S)%55 21-130 08/30/22 09:31
Terphenyl-d14 (S)%52 15-130 08/30/22 09:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3753314LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 12301670 74 54-130
2-Methylnaphthalene ug/kg 12001670 72 57-130
Acenaphthene ug/kg 12401670 74 56-130
Acenaphthylene ug/kg 14001670 84 58-130
Anthracene ug/kg 11101670 67 60-130
Benzo(a)anthracene ug/kg 11901670 71 59-130
Benzo(a)pyrene ug/kg 15301670 92 57-130
Benzo(b)fluoranthene ug/kg 16501670 99 54-130
Benzo(g,h,i)perylene ug/kg 15701670 94 59-130
Benzo(k)fluoranthene ug/kg 14201670 85 54-130
Chrysene ug/kg 13101670 79 57-130
Dibenz(a,h)anthracene ug/kg 15301670 92 60-130
Fluoranthene ug/kg 12501670 75 57-130
Fluorene ug/kg 12401670 74 56-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3753314LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/kg 15501670 93 61-130
Naphthalene ug/kg 11901670 72 56-130
Phenanthrene ug/kg 12301670 74 60-130
Pyrene ug/kg 13001670 78 61-130
2-Fluorobiphenyl (S)%69 19-130
Nitrobenzene-d5 (S)%71 21-130
Terphenyl-d14 (S)%70 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92622672002
3753957SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%0 S40
Nitrobenzene-d5 (S)%0 D3,S40
Terphenyl-d14 (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718954
EPA 3511
EPA 8270E
8270E PAH Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510009, 92621510010, 92621510011, 92621510012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3747361
Associated Lab Samples:92621510009, 92621510010, 92621510011, 92621510012
Matrix:Water
AnalyzedMDL
1-Methylnaphthalene ug/L ND 10.0 08/23/22 17:363.7
2-Methylnaphthalene ug/L ND 10.0 08/23/22 17:363.4
Acenaphthene ug/L ND 10.0 08/23/22 17:363.2
Acenaphthylene ug/L ND 10.0 08/23/22 17:363.9
Anthracene ug/L ND 10.0 08/23/22 17:363.9
Benzo(a)anthracene ug/L ND 10.0 08/23/22 17:364.0
Benzo(a)pyrene ug/L ND 10.0 08/23/22 17:363.6
Benzo(b)fluoranthene ug/L ND 10.0 08/23/22 17:363.9
Benzo(g,h,i)perylene ug/L ND 10.0 08/23/22 17:363.7
Benzo(k)fluoranthene ug/L ND 10.0 08/23/22 17:363.6
Chrysene ug/L ND 10.0 08/23/22 17:363.4
Dibenz(a,h)anthracene ug/L ND 10.0 08/23/22 17:364.3
Fluoranthene ug/L ND 10.0 08/23/22 17:363.4
Fluorene ug/L ND 10.0 08/23/22 17:363.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/23/22 17:364.0
Naphthalene ug/L ND 10.0 08/23/22 17:363.2
Phenanthrene ug/L ND 10.0 08/23/22 17:363.4
Pyrene ug/L ND 10.0 08/23/22 17:363.8
2-Fluorobiphenyl (S)%87 58-131 08/23/22 17:36
Nitrobenzene-d5 (S)%103 42-147 08/23/22 17:36
Terphenyl-d14 (S)%88 55-151 08/23/22 17:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3747362LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 61.362.5 98 70-130
2-Methylnaphthalene ug/L 58.162.5 93 70-130
Acenaphthene ug/L 61.862.5 99 70-130
Acenaphthylene ug/L 63.262.5 101 70-130
Anthracene ug/L 58.562.5 94 70-130
Benzo(a)anthracene ug/L 63.262.5 101 70-130
Benzo(a)pyrene ug/L 74.262.5 119 70-130
Benzo(b)fluoranthene ug/L 72.762.5 116 70-130
Benzo(g,h,i)perylene ug/L 69.862.5 112 70-130
Benzo(k)fluoranthene ug/L 75.662.5 121 70-130
Chrysene ug/L 62.562.5 100 70-130
Dibenz(a,h)anthracene ug/L 69.162.5 111 70-130
Fluoranthene ug/L 63.162.5 101 70-130
Fluorene ug/L 62.562.5 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3747362LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/L 70.262.5 112 70-130
Naphthalene ug/L 56.962.5 91 70-130
Phenanthrene ug/L 62.662.5 100 70-130
Pyrene ug/L 68.062.5 109 70-130
2-Fluorobiphenyl (S)%104 58-131
Nitrobenzene-d5 (S)%108 42-147
Terphenyl-d14 (S)%104 55-151
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3748114MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92621235004
3748115
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1-Methylnaphthalene ug/L 125 93 59-15291 3 30125ND116113
2-Methylnaphthalene ug/L 125 90 49-15990 0 30125ND113113
Acenaphthene ug/L 125 94 61-15093 1 30125ND117116
Acenaphthylene ug/L 125 94 62-15493 1 30125ND117116
Anthracene ug/L 125 84 58-15782 2 30125ND105103
Benzo(a)anthracene ug/L 125 93 52-159101 7 30125ND117126
Benzo(a)pyrene ug/L 125 106 55-157107 2 30125ND132134
Benzo(b)fluoranthene ug/L 125 107 54-153104 2 30125ND134131
Benzo(g,h,i)perylene ug/L 125 102 55-164104 2 30125ND128130
Benzo(k)fluoranthene ug/L 125 112 56-162112 1 30125ND140140
Chrysene ug/L 125 92 53-16593 1 30125ND115117
Dibenz(a,h)anthracene ug/L 125 101 53-162105 4 30125ND126132
Fluoranthene ug/L 125 91 55-15991 0 30125ND114114
Fluorene ug/L 125 94 61-15294 0 30125ND117117
Indeno(1,2,3-cd)pyrene ug/L 125 111 54-160111 0 30125ND139139
Naphthalene ug/L 125 88 51-16088 0 30125ND110111
Phenanthrene ug/L 125 92 60-15594 2 30125ND116118
Pyrene ug/L 125 96 56-159104 7 30125ND121130
2-Fluorobiphenyl (S)%87 58-13188
Nitrobenzene-d5 (S)%89 42-14788
Terphenyl-d14 (S)%81 55-15177
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718782
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510001, 92621510002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621086006
3746810SAMPLE DUPLICATE:
Percent Moisture %14.8 N222514.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621510002
3746811SAMPLE DUPLICATE:
Percent Moisture %10.2 N23259.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 76
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
718799
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92621510003, 92621510004, 92621510005, 92621510006, 92621510007, 92621510008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92620531001
3746847SAMPLE DUPLICATE:
Percent Moisture %14.4 N232514.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92621521001
3746848SAMPLE DUPLICATE:
Percent Moisture %9.9 N292510.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 76
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 76
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 76
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92621510
BAYER PROPERTY 72227070
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92621510001 718547 718950B-1 SOIL EPA 3546 EPA 8270E
92621510002 718547 718950B-2 SOIL EPA 3546 EPA 8270E
92621510003 718547 718950B-3 SOIL EPA 3546 EPA 8270E
92621510004 718547 718950B-4 SOIL EPA 3546 EPA 8270E
92621510005 718547 718950B-5 SOIL EPA 3546 EPA 8270E
92621510006 718547 718950B-6 SOIL EPA 3546 EPA 8270E
92621510007 718547 718950B-7 SOIL EPA 3546 EPA 8270E
92621510008 720229 720304B-8 SOIL EPA 3546 EPA 8270E
92621510009 718954 719114MW-1 EPA 3511 EPA 8270E
92621510010 718954 719114B-2 GW EPA 3511 EPA 8270E
92621510011 718954 719114B-3 GW EPA 3511 EPA 8270E
92621510012 718954 719114B-5 GW EPA 3511 EPA 8270E
92621510001 718484 718702B-1 SOIL EPA 5035A/5030B EPA 8260D
92621510002 718484 718702B-2 SOIL EPA 5035A/5030B EPA 8260D
92621510003 718519 718733B-3 SOIL EPA 5035A/5030B EPA 8260D
92621510004 718484 718702B-4 SOIL EPA 5035A/5030B EPA 8260D
92621510005 718484 718702B-5 SOIL EPA 5035A/5030B EPA 8260D
92621510006 718484 718702B-6 SOIL EPA 5035A/5030B EPA 8260D
92621510007 718484 718702B-7 SOIL EPA 5035A/5030B EPA 8260D
92621510008 718519 718733B-8 SOIL EPA 5035A/5030B EPA 8260D
92621510009 719094MW-1 EPA 8260D
92621510010 719094B-2 GW EPA 8260D
92621510011 719094B-3 GW EPA 8260D
92621510012 719554B-5 GW EPA 8260D
92621510001 718782B-1 SOIL SW-846
92621510002 718782B-2 SOIL SW-846
92621510003 718799B-3 SOIL SW-846
92621510004 718799B-4 SOIL SW-846
92621510005 718799B-5 SOIL SW-846
92621510006 718799B-6 SOIL SW-846
92621510007 718799B-7 SOIL SW-846
92621510008 718799B-8 SOIL SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/01/2022 12:49 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 76
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