The URL can be used to link to this page

Home My WebLink AboutWA-92955_96655_CA_LAB_20211228The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC. Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Report of Analysis NCDEQ-DWM-UST Section 943 Washington SQ Mall Washington,NC 27889 Attention:Jared Edwards Project Name:Tighe Property Lot Number:WL14026 Date Completed:12/28/2021 01/06/2022 10:52 PM Approved and released by: Project Manager II:Cathy S.Dover Page 1 of 22 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com Case Narrative NCDEQ-DWM-UST Section Lot Number:WL14026 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample.All results listed in this report relate only to the samples that are contained within this report. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace") Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI scope of accreditation: Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,Boron,Calcium, Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320 B-2011,Fecal Coliform SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011, Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2-dichloroethane)EPA 524.2,Solid Chemical Material:TOC Walkley-Black. Where applicable,all soil sample results (including LOQ and DL if requested)are corrected for dry weight unless flagged with a "W"qualifier. TPH-GRO 8015C Insufficient sample volume was provided to perform matrix spike/matrix spike duplicate (MS/MSD)for analytical batch 25726.An LCS/LCSD was run in lieu of an MS/MSD. Sample WL14026-003 (Trip)had an air bubble >6mm in the sample vial. TPH-DRO 8015C Insufficient sample volume was provided to perform matrix spike/matrix spike duplicate (MS/MSD)for prep batch 25778.An LCS/LCSD was run in lieu of an MS/MSD. Samples WL14026-001 (SS-1)and WL14026-002 (SS-2)required a 100x dilution which affected the surrogate recovery. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Page 2 of 22 PACE ANALYTICAL SERVICES, LLC Sample Summary NCDEQ-DWM-UST Section Lot Number: WL14026 Project Name: Tighe Property Project Number: Sample Number Sample ID Matrix Date Sampled Date Received 001 12/10/2021 1031SS-1 Solid 12/14/2021 002 12/10/2021 1037SS-2 Solid 12/14/2021 003 12/10/2021TripAqueous 12/14/2021 (3 samples) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 3 of 22 PACE ANALYTICAL SERVICES, LLC Detection Summary NCDEQ-DWM-UST Section Lot Number: WL14026 Project Name: Tighe Property Project Number: Sample Sample ID Matrix Parameter Method Result Q Units Page 001 SS-1 Solid TPH-DRO 8015C 41000 Q mg/Kg 5 001 SS-1 Solid TPH-GRO 8015C 11000 mg/Kg 6 002 SS-2 Solid TPH-DRO 8015C 93000 Q mg/Kg 7 002 SS-2 Solid TPH-GRO 8015C 8100 mg/Kg 8 (4 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 4 of 22 TPH - DRO Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: NCDEQ-DWM-UST Section SS-1 WL14026-001 12/10/2021 1031 12/14/2021 Solid % Solids:84.0 12/15/2021 0111Project Name: Tighe Property Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 100 12/28/2021 1323 NCM 12/15/2021 2249 25778 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run TPH-DRO 8015C 41000 Q 1mg/Kg800 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl N 242 55-120 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failureW = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 5 of 22 TPH - GRO Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: NCDEQ-DWM-UST Section SS-1 WL14026-001 12/10/2021 1031 12/14/2021 Solid % Solids:84.0 12/15/2021 0111Project Name: Tighe Property Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 10 12/15/2021 2005 ECB 25726 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run TPH-GRO 8015C 11000 1mg/Kg220 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 93 23-179 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failureW = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 6 of 22 TPH - DRO Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: NCDEQ-DWM-UST Section SS-2 WL14026-002 12/10/2021 1037 12/14/2021 Solid % Solids:70.1 12/15/2021 0111Project Name: Tighe Property Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 100 12/28/2021 1332 NCM 12/15/2021 2249 25778 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run TPH-DRO 8015C 93000 Q 1mg/Kg950 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl N 271 55-120 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failureW = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 7 of 22 TPH - GRO Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: NCDEQ-DWM-UST Section SS-2 WL14026-002 12/10/2021 1037 12/14/2021 Solid % Solids:70.1 12/15/2021 0111Project Name: Tighe Property Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 5 12/15/2021 2030 ECB 25726 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run TPH-GRO 8015C 8100 1mg/Kg190 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 78 23-179 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failureW = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 8 of 22 TPH - GRO Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: NCDEQ-DWM-UST Section Trip WL14026-003 12/10/2021 12/14/2021 Aqueous Project Name: Tighe Property Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 12/21/2021 1732 ECB 26371 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run TPH-GRO 8015C ND 1mg/L0.10 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 113 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failureW = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 9 of 22 QC Summary QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 10 of 22 TPH - DRO - MB Batch:Prep Method: Prep Date: Sample ID:WQ25778-001 25778 3550C 12/15/2021 2249Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ Units Analysis DateDil TPH-DRO ND 12/23/2021 11406.7 mg/Kg1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 95 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 11 of 22 TPH - DRO - LCS Batch:Prep Method: Prep Date: Sample ID:WQ25778-002 25778 3550C 12/15/2021 2249Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/Kg)(mg/Kg) TPH-DRO 88 12/23/2021 11501068370-1301 Surrogate Q % Rec Acceptance Limit o - Terphenyl 99 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 12 of 22 TPH - DRO - LCSD Batch:Prep Method: Prep Date: Sample ID:WQ25778-003 25778 3550C 12/15/2021 2249Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/Kg)(mg/Kg) TPH-DRO 87 12/23/2021 11591058370-1300.82 201 Surrogate Q % Rec Acceptance Limit o - Terphenyl 94 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 13 of 22 TPH - GRO - MB Batch:Prep Method: Sample ID:WQ25726-001 25726 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ Units Analysis DateDil TPH-GRO ND 12/15/2021 16085.0 mg/Kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 123 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 14 of 22 TPH - GRO - LCS Batch:Prep Method: Sample ID:WQ25726-002 25726 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/Kg)(mg/Kg) TPH-GRO 59 12/15/2021 15181185070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 116 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 15 of 22 TPH - GRO - LCSD Batch:Prep Method: Sample ID:WQ25726-003 25726 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/Kg)(mg/Kg) TPH-GRO 59 12/15/2021 15431175070-1300.51 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 112 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 16 of 22 TPH - GRO - MB Batch:Prep Method: Sample ID:WQ26371-001 26371 5030B Analytical Method:8015C Matrix:Aqueous Parameter Result Q LOQ Units Analysis DateDil TPH-GRO ND 12/21/2021 15040.10 mg/L1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 111 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 17 of 22 TPH - GRO - LCS Batch:Prep Method: Sample ID:WQ26371-002 26371 5030B Analytical Method:8015C Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/L)(mg/L) TPH-GRO 1.2 12/21/2021 14141151.0 70-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 102 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 18 of 22 TPH - GRO - LCSD Batch:Prep Method: Sample ID:WQ26371-003 26371 5030B Analytical Method:8015C Matrix:Aqueous Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/L)(mg/L) TPH-GRO 1.1 12/21/2021 14391091.0 70-1305.4 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 98 70-130 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria* = RSD is out of criteria QC Data for Lot Number: WL14026 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 19 of 22 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 20 of 22 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 21 of 22 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 22 of 22