WA-88914_93109_CA_RPTS_20190528_LSA ADDENDUM

May 28, 2019

Mr. Jared M. Edwards, Hydrogeologist
Washington Regional Office - DEQ
Division of Waste Management
UST Section
943 Washington Square Mall
Washington, NC 27889

Subject: SUPPLEMENTAL ASSESSMENT REPORT
PETROLEUM RELEASE ASSESSMENT
DUKE ENERGY H.F. LEE PLANT
1677 OLD SMITHFIELD ROAD
GOLDSBORO, NORTH CAROLINA
MID-ATLANTIC JOB NO. 000R2470.13
Dear Mr. Edwards:

On behalf of Duke Energy, Mid-Atlantic Associates, Inc. submits the enclosed
Supplemental Assessment Report for the above-referenced site. This report is being
submitted in response to a Notice of Regulatory Requirements issued by the Department
of Environmental Quality dated February 28, 2019. If you have any questions, please do
not hesitate to contact me at [phone].

Sincerely,

MID-ATLANTIC ASSOCIATES, INC.
Daniel Nielsen, PE
Principal Engineer

Enclosure: Supplemental Assessment Report
CC: Hank Lyon, Duke Energy (via email)

SUPPLEMENTAL ASSESSMENT REPORT
DUKE ENERGY H.F. LEE PLANT
1677 OLD SMITHFIELD ROAD
GOLDSBORO, WAYNE COUNTY, NORTH CAROLINA
INCIDENT NO.: 93109

Risk Classification: Not Assigned
Land Use: Not Assigned

Latitude: 35o22’42.31’’ N
Longitude: 78o05’20.86’’ W

Date Discovered: June 17, 2011 (AOC 1)
Estimated Quantity of Release: Unknown
Cause/Source of Release: Former underground fuel lines and tank systems

Prepared For:

Duke Energy
C/O Mr. Hank Lyon, LG
Duke Energy Remediation
1451 Military Cutoff Road, ERO
Wilmington, North Carolina 28403

Prepared By:

Mid-Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610

May 28, 2018

TABLE OF CONTENTS

1.0 GENERAL INFORMATION .................................................................................... 1
2.0 SUMMARY OF FIELD ACTIVITIES ....................................................................... 1
3.0 LABORATORY ANALYTICAL RESULTS ............................................................. 2
4.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS ................................. 3

DRAWINGS

Drawing 1.1 Topographic Site Map
Drawing 2.1 Monitoring Well and Soil Sample Location Map

TABLES

Table 2.1 Depth to Groundwater
Table 3.1 Summary of Chemical Constituents Detected in Groundwater

APPENDICES

Appendix A Groundwater Sampling Procedures
Appendix B Laboratory Analytical Reports and Chain-of-Custody Records

1.0 GENERAL INFORMATION

The subject site is located on the Duke Energy Progress, Inc. (Duke) H.F. Lee plant site at
1677 Old Smithfield Road in Goldsboro, North Carolina (Drawing 1.1). Prior to and during
plant decommissioning activities five Areas of Concern (AOC) associated with petroleum
releases were identified at the subject site. Duke notified the North Carolina Department of
Environmental Quality (NCDEQ), then the Department of Environment and Natural
Resources (NCDENR), Underground Storage Tank (UST) Section of these releases and it
was determined, for safety reasons, that they would be addressed once demolition
activities were complete. It was also decided that these releases would be addressed
under the facility’s current incident number (93109) as they are associated with a common
petroleum fuel storage and transfer system.

In 2017 the majority of plant decommissioning activities were completed such that
assessment activities could be conducted safely. A site-wide Phase I Limited Site
Assessment was conducted to address all five AOCs. These activities were described in a
Phase I Limited Site Assessment (LSA) report dated September 1, 2017. Upon review of
the Phase I LSA report, NCDEQ issued a Notice of Regulatory Requirements (NORR)
dated February 28, 2019. This report is intended to address the supplemental assessment
activities outlined in the February 28, 2019 NORR.

The opinions included herein are based on our experience and the information obtained
during the study. This report is based on limited observations made on the dates noted
using the procedures described herein. If additional information becomes available, we
request the opportunity to review the information, reassess the potential environmental
concerns and modify our conclusions and recommendations, if appropriate.

2.0 SUMMARY OF FIELD ACTIVITIES

The February 28, 2019 NORR outlined the supplemental assessment activities as follows:

Collect one groundwater sample from monitoring wells MW-104, MW-201 and
MW-501 (Drawing 2.1). Test the collected groundwater samples by EPA
Methods 8260 and 8270 as well as MADEP VPH and EPH.

Collect one soil sample from a depth just above the water table at locations adjacent
to monitoring wells MW-104, MW-201 and MW-501. Test each soil sample by EPA
Method 8260, EPA Method 8270, MADEP VPH and EPH.

On April 29, 2019 Mid-Atlantic personnel mobilized to the subject site to collect the
groundwater and soil samples outlined above. Each monitoring well was gauged for the
presence of free phase petroleum product with an oil water interface probe capable of
detecting oil thickness to 0.01 feet. Free phase product was not detected in any of the
wells. The depth to groundwater at each location was then recorded (Table 2.1). This table
Supplemental Assessment Report May 28, 2019
Duke Energy H.F. Lee Plant Page 2
Goldsboro, North Carolina

also includes previous depth-to-groundwater measurements (1/30/2017 and 3/17/2017). A
comparison of the 2017 data to the 2019 data shows the water table was 2 to 3 feet higher
in 2019. Each well was purged and samples were collected in accordance with the
procedures outlined in Appendix A.

Mid-Atlantic was successful using a hand auger to collect the soil sample adjacent to MW-
501 at a depth just above the water table (approximately 4 feet below land surface (bls)).
However, repeated attempts to collect soil samples adjacent to MW-104 and MW-201 were
unsuccessful. At location MW-104, where the water table was approximately 12.5 feet bls,
auguring could not advance beyond 4.5 feet bls. This area was previously filled with gravel
and the gravel fill would immediately fill the borehole each time the auger was removed.
Three separate attempts to advance the boring were attempted and each was
unsuccessful. At location MW-201, where the depth to the water table as approximately 7
feet, three hand auger attempts were thwarted at approximately 2.5 feet bls. A very hard
packed gravel layer was encountered at this depth. Attempts were made to break the hard
pack with a digger bar, but these attempts also proved fruitless.

3.0 LABORATORY ANALYTICAL RESULTS

The laboratory analytical report and chains-of-custody record for the soil and
groundwater samples collected at the site are provided in Appendix B. As described
above, one soil sample was analyzed. The sample had one detection for acetone at
0.0088J mg/kg. This concentration is below the lowest Maximum Soil Contaminant
Concentrations (MSCC). It is also likely that acetone is a laboratory artifact.

The groundwater test results are summarized in Table 3.1. This table also includes the
results from the sampling conducted during the Phase I LSA (January 30, 2017 sample
collection date). A comparison of the April 29, 2019 sample date data to the January 30,
2017 sample date data shows a general decline in contaminant concentrations at each
of the three wells sampled. During the April 2019 sample event, two compounds,
tetrachloroethylene and 1-methylnaphthalene were detected at concentrations above
North Carolina Groundwater Quality Standards (NCGQS) in the sample collected from
MW-104. In the sample collected from MW-201 the concentration of 1-
methylnaphthalene (estimated) and C9-C18 Aliphatics exceeded the NCGQS. There
were no detections in the sample collected from MW-501. The concentrations of
detected compounds recorded during this sampling event did not exceed Gross
Contamination Levels (GCL) or the North Carolina Surface Water Quality Standards
(NCSWQS) by a factor of ten.

Supplemental Assessment Report May 28, 2019
Duke Energy H.F. Lee Plant Page 3
Goldsboro, North Carolina

4.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS

The results of this Supplemental Assessment are summarized as follows:

 Due to site conditions, only one of the three planned soil samples could be
collected;

 Petroleum-related compounds were not detected above laboratory detection
limits in the one soil analyzed during this assessment;
 Groundwater elevations were approximately 2 to 3 feet higher in April 2019 in
comparison to January and March 2017;

 Free product was not detected in the site monitoring wells;

 Tetrachloroethylene and the 1-methylnaphthalene were detected in excess of the
NCGQS in the groundwater sample collected from monitoring well MW-104.
These detected concentrations were below GCLs and below ten times the
NCSWQS;

 Both 1-methylnaphthalene and the aliphatic carbon chain C9-C18 were detected
in the groundwater sample collected from the monitoring well MW-201 at a
concentration exceeding the NCGQS, but below the GCLs and below ten times
the NCSWQS; and

 Compounds were not detected above laboratory detection limits in the
groundwater sample collected from MW-501.

Based on the results of our assessment, Mid-Atlantic concludes the following:

 Human exposure to released petroleum, petroleum vapors and petroleum-impacted
groundwater at the subject site is unlikely; and

 Based on the results of this investigation, and in accordance with 15A NCAC
02L.0506 (2)(a), it appears the site should be classified as “low risk” and the land
use should be classified as “industrial”. The DWM UST Section will assign risk and
land use classifications.

Mid-Atlantic recommends the following:

 Submit this report to NCDEQ to determine if risk-based site closure is appropriate
for this site.

DRAWINGS
´
TOPOGRAPHIC SITE MAPDUKE ENERGY H.F. LEE PLANT1677 OLD SMITHFIELD ROADGOLDSBORO, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO:
REFERENCES:SCALE:
WAYNE
LENOIR
JOHNSTON
DUPLIN
GREENE
SAMPSON
PITTWILSON
JONES
§¨¦I95
AREA SHOWNWITHIN WAYNE COUNTY
MAY 2019
000R2470.13
01-R24700.13-11.1
1. NORTHWEST & SOUTHWEST GOLDSBORO, NC DIGITAL RASTER GRAPHICS, USGS. SCANNED FROM1:24,000-SCALE NORTHWEST & SOUTHWEST GOLDSBORO, NC TOPOGRAPHIC MAPS, PUBLISHED 2013, USGS.2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS, BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.3. PROPERTY BOUNDARY DATA FROM WAYNE COUNTY GIS.
CONTOUR INTERVAL = 5 FEET
0 3,000 6,000Feet
SITE - GENERAL RELEASE AREA
1:36,000
Legend
PROPERTY BOUNDARY
EBA
!A
!A
!A
!.
!.!.
!.
!.
!.
!.
0 100 200Feet
LEGEND
!.SOIL BORING LOCATION
!A MONITORING WELL LOCATION
´
MONITORING WELL AND SOIL SAMPLE LOCATION MAPDUKE ENERGY PROGRESS, INC. - LEE PLANT1199 BLACK JACK CHURCH ROADGOLDSBORO, NORTH CAROLINA
DRAWN BY:DATE:
ENG. CHECK:
JOB NO:
APPROVAL:
DRAFTCHECK:GIS NO:
DWG NO: 2.1
MAY 2019
000R2470.13
01G-R2470.13-2
REFERENCES: JUNE 2013 PROPERTY BOUNDARY DATA FROM WAYNE CO. GIS. 2013 AERIAL PHOTOGRAPHS FROM NC ONEMAP. MID-ATLANTIC FIELD NOTES.
MW-104
EBA
MW-501
MW-201
THREE ATTEMPTS TOCOLLECT SOIL SAMPLEFAILED DUE TO AUGER REFUSAL
THREE ATTEMPTS TOCOLLECT SOIL SAMPLEFAILED DUE TO CAVE-IN
MW-501 (4')

TABLES
WELL ID
DEPTH TO
WATER FROM TOC
(1/31/2017)
DEPTH TO
WATER FROM TOC
(3/17/2017)
DEPTH TO
WATER FROM TOC
(4/29/2019)
MW-104 18.59 18.89 15.79
MW-201 12.74 13.19 10.50
MW-501 9.37 9.65 7.40
TABLE 2.1
DEPTH TO GROUNDWATER
DUKE ENERGY H.F. LEE PLANT
GOLDSBORO, NORTH CAROLINA
MID-ATLANTIC JOB NO. 000R2470.13
Date Sampled1/31/2017 4/29/2019 1/31/2017 4/29/2019 1/30/2017 4/29/2019Acetone -- 19 -- 7.7 -- -- 6,000 6,000,000 NEBenzene2.10.99 -- 0.27J -- --15,000 11.9n-Butylbenzene 8.7 2.6 1 -- -- -- 70 6,900 NEsec-Butylbenzene 15 5 4.3 1.2 3.4 -- 70 8,500 NEtert-Butylbenzene 1.6 1.5 -- -- -- -- 70 15,000 NEEthylbenzene 1.4 0.26J -- -- 2.3 -- 600 84,500 NEIsopropylbenzene (Cumene) 12 6.3 2.6 0.87 2 -- 70 25,000 NE4-Isopropyltoluene 5.9 1.3 -- -- 2 -- 25 11,700 NENaphthalene110 --3.5 --31-- 6 6,000 NEn-Propylbenzene 16 4.5 2.9 0.27J 2.7 -- 70 30,000 NE1,2,4-Trimethylbenzene 13 0.67 -- -- 11 -- 400 28,500 NE1,3,5-Trimethylbenzene 4.5 1.6 -- -- 7.7 -- 400 25,000 NETetrachloroethylene --0.84-- -- -- -- 0.7 700 7m,p-Xylenes 6 1.1 -- -- 1.4 -- 500 85,500 NEo-Xylene 1.3 0.65 -- -- 0.96 -- 500 85,500 NEAcenaphthene 9 J 24 -- -- -- -- 80 2120 NEFluorene 12 11J 4.1 J -- 4.2 J -- 300 990 NENaphthalene24 ---- --13-- 6 6,000 NE1-Methylnaphthalene120 42 11 6.2J 31-- 1 1,000 NE2-Methylnaphthalene14015 6.1 J --39-- 30 12,500 NEPhenanthrene 15 8.7J 4.2 J -- 6 J -- 200 410 NEC9-C10 Aromatics 600 260 260 11J 340 -- 10,200 NE NEC11-C22 Aromatics 2700 440 1800 940 420 -- 10,200 NE NEC5-C8 Aliphatics 38 J 11J 16 -- 20 J -- 400 NE NEC9-C12 Aliphatics 220 270 110 23J 140 -- 700 NE NEC9-C18 Aliphatics28003801900 150026 J -- 700 NE NEC19-C36 Aliphatics 810 120J 690 350J -- -- NE NE NENotes:Analytical results present in micrograms per liter (ug/L). -- = below laboratory practical quantitation limitsResults in bold exceed their NCGQSJ = Detected but below the Reporting Limit; therefore, result is an estimated concentration.NE = Not establishedSemi-volatile Organic Compounds - EPA METHOD 8270MADEP VPH & EPHTABLE 3.1SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN GROUNDWATERDUKE ENERGY H.F. LEE PLANT1677 OLD SMITHFIELD ROADGOLDSBORO, NORTH CAROLINAMID-ATLANTIC JOB NO. 000R2470.13Volatile Organic Compounds - EPA METHOD 8260North Carolina Groundwater Quality Standards(September 2014)North Carolina GrossContamination LevelsFor Groundwater (September 2014)MW-104 MW-201 MW-50110X the NC Surface Water Quality Standards(September 22, 2017)

APPENDIX A

GROUNDWATER SAMPLING PROCEDURES
Groundwater Sampling Procedures

I. Sample Collection

A. Monitoring Wells

Prior to sample collection, each well is purged of three to five standing well volumes or to
dryness to remove stagnant water from the well and well bore in an effort to collect
samples that are representative of the water quality in the formation surrounding each
well. Purging is performed either with a new, polyethylene bailer dedicated to each well, or
with a decontaminated pump. Samples are retrieved from the monitoring well using the
dedicated bailer. New nylon string is used on each dedicated bailer, and new nitrile
sampling gloves are donned prior to purging and sampling of each well.

B. Geoprobe “Screen Point Sampler”

The screen point sampler is a “grab” sampling device that is driven into the saturated zone
and a surrounding metal sheath is retracted, exposing a screen. Groundwater entering the
screen is then drawn to land surface through disposable tubing that is placed through the
hollow push rods. The sample is collected from the tubing into the appropriate sampling
glassware.

C. Water-Supply Wells

Water samples are typically collected from the available spigot that is nearest to the well.
The water is allowed to run at a high flow from the spigot for approximately 10 to 15
minutes to allow the water in the delivery lines to be purged. The sample flow is then
reduced and the samples are collected directly into pre-labeled containers as described
below. New nitrile sampling gloves are donned prior to sampling of each well.

D. Treatment System Influent/Effluent

Samples are typically collected from the influent or effluent of pump-and-treat groundwater
remediation systems using designated sampling ports in the influent and effluent water
transport lines. The water is typically allowed to run for several seconds to clear potential
debris in the sampling port. The sample is then collected directly into sampling containers
as described below. New nitrile sampling gloves are donned prior to sample collection.

II. Preparation for Laboratory Analysis

Groundwater samples are decanted directly into laboratory-prepared, pre-labeled, sampling
containers, packed in ice, and shipped to a certified laboratory under chain-of-custody control.
Laboratory analyses performed on the samples are specified on the chain-of-custody.

APPENDIX B

LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY
RECORD

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
5/14/19 11:52
Mid-Atlantic Associates, Inc. - Raleigh
Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: Duke Energy (Lee Plant)
Project No.: J19050361
Lab Submittal Date: 05/01/2019
Prism Work Order: 9050052
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SE Surrogate recovery outside the QC limits due to emulsion.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 49
Sample Receipt Summary
05/14/2019
Prism Work Order: 9050052
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
9050052-01 04/29/19 11:10MW-104 05/01/19 11:55Water
9050052-02 04/29/19 13:10MW-201 05/01/19 11:55Water
9050052-03 04/29/19 9:40MW-501 05/01/19 11:55Water
9050052-04 04/29/19 9:25MW-501 (4’)05/01/19 11:55Solid
Samples were received in good condition at 1.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 49
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 9050052
05/14/2019
Summary of Detections
380 ug/L9050052-01 MW-104 C9-C18 Aliphatics MADEP EPH
120 J ug/L9050052-01 MW-104 C19-C36 Aliphatics MADEP EPH
440 ug/L9050052-01 MW-104 C11-C22 Aromatics MADEP EPH
42 ug/L9050052-01 MW-104 1-Methylnaphthalene 8270D
15 ug/L9050052-01 MW-104 2-Methylnaphthalene 8270D
24 ug/L9050052-01 MW-104 Acenaphthene 8270D
11 J ug/L9050052-01 MW-104 Fluorene 8270D
8.7 J ug/L9050052-01 MW-104 Phenanthrene 8270D
0.67 ug/L9050052-01 MW-104 1,2,4-Trimethylbenzene 8260B
1.6 ug/L9050052-01 MW-104 1,3,5-Trimethylbenzene 8260B
1.3 ug/L9050052-01 MW-104 4-Isopropyltoluene 8260B
19 ug/L9050052-01 MW-104 Acetone 8260B
0.99 ug/L9050052-01 MW-104 Benzene 8260B
0.26 J ug/L9050052-01 MW-104 Ethylbenzene 8260B
6.3 ug/L9050052-01 MW-104 Isopropylbenzene (Cumene)8260B
1.1 ug/L9050052-01 MW-104 m,p-Xylenes 8260B
2.6 ug/L9050052-01 MW-104 n-Butylbenzene 8260B
4.5 ug/L9050052-01 MW-104 n-Propylbenzene 8260B
0.65 ug/L9050052-01 MW-104 o-Xylene 8260B
5.0 ug/L9050052-01 MW-104 sec-Butylbenzene 8260B
1.5 ug/L9050052-01 MW-104 tert-Butylbenzene 8260B
0.84 ug/L9050052-01 MW-104 Tetrachloroethylene 8260B
1.7 ug/L9050052-01 MW-104 Xylenes, total 8260B
11 J ug/L9050052-01 MW-104 C5-C8 Aliphatics MADEP VPH
270 ug/L9050052-01 MW-104 C9-C12 Aliphatics MADEP VPH
260 ug/L9050052-01 MW-104 C9-C10 Aromatics MADEP VPH
1500 ug/L9050052-02 MW-201 C9-C18 Aliphatics MADEP EPH
350 J ug/L9050052-02 MW-201 C19-C36 Aliphatics MADEP EPH
940 ug/L9050052-02 MW-201 C11-C22 Aromatics MADEP EPH
6.2 J ug/L9050052-02 MW-201 1-Methylnaphthalene 8270D
7.7 ug/L9050052-02 MW-201 Acetone 8260B
0.27 J ug/L9050052-02 MW-201 Benzene 8260B
0.87 ug/L9050052-02 MW-201 Isopropylbenzene (Cumene)8260B
0.27 J ug/L9050052-02 MW-201 n-Propylbenzene 8260B
1.2 ug/L9050052-02 MW-201 sec-Butylbenzene 8260B
23 J ug/L9050052-02 MW-201 C9-C12 Aliphatics MADEP VPH
11 J ug/L9050052-02 MW-201 C9-C10 Aromatics MADEP VPH
0.0088 J mg/kg dry9050052-04 MW-501 (4’)Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-104
Prism Sample ID: 9050052-01
Prism Work Order: 9050052
Time Collected: 04/29/19 11:10
Time Submitted: 05/01/19 11:55
J19050361
Extractable Petroleum Hydrocarbons by GC/FID
380 MADEP EPH P9E006713605/10/19 16:09 BGBug/L 24C9-C18 Aliphatics
120 MADEP EPH P9E006715105/10/19 16:09 BGBJug/L 120C19-C36 Aliphatics
440 MADEP EPH P9E006712605/10/19 16:09 BGBug/L 82C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14014 %1-Chlorooctadecane SE
40-14020 %o-Terphenyl SE
40-140103 %2-Fluorobiphenyl
40-140123 %2-Bromonaphthalene
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.01,2,4-Trichlorobenzene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.41,2-Dichlorobenzene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.91,3-Dichlorobenzene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.11,4-Dichlorobenzene
42 8270D P9E00681105/6/19 16:55 JMVug/L 3.61-Methylnaphthalene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 3.62,4,5-Trichlorophenol
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.52,4,6-Trichlorophenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.92,4-Dimethylphenol
BRL 8270D P9E00681505/6/19 16:55 JMVug/L 122,4-Dinitrophenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.22,4-Dinitrotoluene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 3.92,6-Dinitrotoluene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.72-Chloronaphthalene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.72-Chlorophenol
15 8270D P9E00681105/6/19 16:55 JMVug/L 4.22-Methylnaphthalene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.42-Methylphenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.12-Nitroaniline
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.62-Nitrophenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.93,3’-Dichlorobenzidine
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.53/4-Methylphenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.83-Nitroaniline
BRL 8270D P9E00681505/6/19 16:55 JMVug/L 114,6-Dinitro-2-methylphenol
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.44-Bromophenyl phenyl ether
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.94-Chloro-3-methylphenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.54-Chloroaniline
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.74-Chlorophenyl phenyl ether
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.14-Nitroaniline
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.64-Nitrophenol
24 8270D P9E00681205/6/19 16:55 JMVug/L 4.3Acenaphthene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.4Acenaphthylene
BRL 8270D P9E00681505/6/19 16:55 JMVug/L 12Aniline
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.6Anthracene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-104
Prism Sample ID: 9050052-01
Prism Work Order: 9050052
Time Collected: 04/29/19 11:10
Time Submitted: 05/01/19 11:55
J19050361
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.2Azobenzene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.2Benzo(a)anthracene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.5Benzo(a)pyrene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.5Benzo(b)fluoranthene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.6Benzo(g,h,i)perylene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.6Benzo(k)fluoranthene
BRL 8270D P9E006811005/6/19 16:55 JMVug/L 19Benzoic Acid
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.5Benzyl alcohol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.8bis(2-Chloroethoxy)methane
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.6Bis(2-Chloroethyl)ether
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.8Bis(2-chloroisopropyl)ether
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.7Bis(2-Ethylhexyl)phthalate
BRL 8270D P9E00681105/6/19 16:55 JMVug/LBromochloroacetonitrile
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.9Butyl benzyl phthalate
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.3Chrysene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 5.7Dibenzo(a,h)anthracene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.2Dibenzofuran
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.2Diethyl phthalate
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.1Dimethyl phthalate
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.3Di-n-butyl phthalate
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.5Di-n-octyl phthalate
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.0Fluoranthene
11 8270D P9E00681205/6/19 16:55 JMVJug/L 5.0Fluorene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 3.9Hexachlorobenzene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.5Hexachlorobutadiene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 7.3Hexachlorocyclopentadiene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.7Hexachloroethane
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 2.6Indeno(1,2,3-cd)pyrene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.1Isophorone
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 4.1Naphthalene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.8Nitrobenzene
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 3.3N-Nitroso-di-n-propylamine
BRL 8270D P9E00681205/6/19 16:55 JMVug/L 4.4N-Nitrosodiphenylamine
BRL 8270D P9E00681505/6/19 16:55 JMVug/L 11Pentachlorophenol
8.7 8270D P9E00681205/6/19 16:55 JMVJug/L 3.9Phenanthrene
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 1.4Phenol
BRL 8270D P9E00681105/6/19 16:55 JMVug/L 3.5Pyrene
Surrogate Recovery Control Limits
43-14052 %2,4,6-Tribromophenol
44-11950 %2-Fluorobiphenyl
19-11945 %2-Fluorophenol
44-12045 %Nitrobenzene-d5
11-5232 %Phenol-d5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-104
Prism Sample ID: 9050052-01
Prism Work Order: 9050052
Time Collected: 04/29/19 11:10
Time Submitted: 05/01/19 11:55
J19050361
50-13451 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P9E009812.0 5/6/19 20:17 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.131,2,4-Trichlorobenzene
0.67 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P9E009812.0 5/6/19 20:17 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.111,2-Dichloropropane
1.6 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P9E009812.0 5/6/19 20:17 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0504-Chlorotoluene
1.3 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.0894-Isopropyltoluene
19 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.31Acetone
BRL 8260B P9E00981205/6/19 20:17 KDMug/L 0.20Acrolein
BRL 8260B P9E00981205/6/19 20:17 KDMug/L 0.20Acrylonitrile
0.99 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.048Benzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.057Bromobenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.14Bromochloromethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.062Bromodichloromethane
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.040Bromoform
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.18Bromomethane
BRL 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.075Carbon disulfide
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.062Chlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.22Chloroethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.076Chloroform
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.079Chloromethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.079cis-1,3-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-104
Prism Sample ID: 9050052-01
Prism Work Order: 9050052
Time Collected: 04/29/19 11:10
Time Submitted: 05/01/19 11:55
J19050361
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.081Dibromochloromethane
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.065Dibromomethane
BRL 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.11Dichlorodifluoromethane
0.26 8260B P9E009810.50 5/6/19 20:17 KDMJug/L 0.061Ethylbenzene
BRL 8260B P9E009812.0 5/6/19 20:17 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.050Isopropyl Ether
6.3 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.054Isopropylbenzene (Cumene)
1.1 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.12m,p-Xylenes
BRL 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P9E009815.0 5/6/19 20:17 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.083Methylene Chloride
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.19Naphthalene
2.6 8260B P9E009811.0 5/6/19 20:17 KDMug/L 0.076n-Butylbenzene
4.5 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.087n-Propylbenzene
0.65 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.044o-Xylene
5.0 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.047Styrene
1.5 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.088tert-Butylbenzene
0.84 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.044Toluene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.078Trichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P9E009812.0 5/6/19 20:17 KDMug/L 0.060Vinyl acetate
BRL 8260B P9E009810.50 5/6/19 20:17 KDMug/L 0.097Vinyl chloride
1.7 8260B P9E009811.5 5/6/19 20:17 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124105 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-12398 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
11 MADEP VPH P9E00791505/6/19 12:29 TBLJug/L 4.0C5-C8 Aliphatics
270 MADEP VPH P9E00791505/6/19 12:29 TBLug/L 3.9C9-C12 Aliphatics
260 MADEP VPH P9E00791505/6/19 12:29 TBLug/L 4.2C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130120 %2,5-Dibromotoluene (PID)
70-130117 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-201
Prism Sample ID: 9050052-02
Prism Work Order: 9050052
Time Collected: 04/29/19 13:10
Time Submitted: 05/01/19 11:55
J19050361
Extractable Petroleum Hydrocarbons by GC/FID
1500 MADEP EPH P9E006713705/10/19 16:45 BGBug/L 25C9-C18 Aliphatics
350 MADEP EPH P9E006715305/10/19 16:45 BGBJug/L 130C19-C36 Aliphatics
940 MADEP EPH P9E006712705/10/19 16:45 BGBug/L 85C11-C22 Aromatics
Surrogate Recovery Control Limits
40-140106 %1-Chlorooctadecane
40-140115 %o-Terphenyl
40-140110 %2-Fluorobiphenyl
40-140127 %2-Bromonaphthalene
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.01,2,4-Trichlorobenzene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.41,2-Dichlorobenzene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.91,3-Dichlorobenzene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.11,4-Dichlorobenzene
6.2 8270D P9E00681105/6/19 17:17 JMVJug/L 3.61-Methylnaphthalene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 3.62,4,5-Trichlorophenol
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.52,4,6-Trichlorophenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.92,4-Dimethylphenol
BRL 8270D P9E00681505/6/19 17:17 JMVug/L 122,4-Dinitrophenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.22,4-Dinitrotoluene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 3.92,6-Dinitrotoluene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.72-Chloronaphthalene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.72-Chlorophenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.22-Methylnaphthalene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.42-Methylphenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.12-Nitroaniline
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.62-Nitrophenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.93,3’-Dichlorobenzidine
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.53/4-Methylphenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.83-Nitroaniline
BRL 8270D P9E00681505/6/19 17:17 JMVug/L 114,6-Dinitro-2-methylphenol
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.44-Bromophenyl phenyl ether
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.94-Chloro-3-methylphenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.54-Chloroaniline
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.74-Chlorophenyl phenyl ether
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.14-Nitroaniline
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.64-Nitrophenol
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.3Acenaphthene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.4Acenaphthylene
BRL 8270D P9E00681505/6/19 17:17 JMVug/L 12Aniline
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.6Anthracene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-201
Prism Sample ID: 9050052-02
Prism Work Order: 9050052
Time Collected: 04/29/19 13:10
Time Submitted: 05/01/19 11:55
J19050361
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.2Azobenzene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.2Benzo(a)anthracene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.5Benzo(a)pyrene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.5Benzo(b)fluoranthene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.6Benzo(g,h,i)perylene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.6Benzo(k)fluoranthene
BRL 8270D P9E006811005/6/19 17:17 JMVug/L 19Benzoic Acid
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.5Benzyl alcohol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.8bis(2-Chloroethoxy)methane
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.6Bis(2-Chloroethyl)ether
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.8Bis(2-chloroisopropyl)ether
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.7Bis(2-Ethylhexyl)phthalate
BRL 8270D P9E00681105/6/19 17:17 JMVug/LBromochloroacetonitrile
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.9Butyl benzyl phthalate
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.3Chrysene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 5.7Dibenzo(a,h)anthracene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.2Dibenzofuran
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.2Diethyl phthalate
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.1Dimethyl phthalate
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.3Di-n-butyl phthalate
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.5Di-n-octyl phthalate
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.0Fluoranthene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 5.0Fluorene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 3.9Hexachlorobenzene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.5Hexachlorobutadiene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 7.3Hexachlorocyclopentadiene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.7Hexachloroethane
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 2.6Indeno(1,2,3-cd)pyrene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.1Isophorone
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 4.1Naphthalene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.8Nitrobenzene
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 3.3N-Nitroso-di-n-propylamine
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 4.4N-Nitrosodiphenylamine
BRL 8270D P9E00681505/6/19 17:17 JMVug/L 11Pentachlorophenol
BRL 8270D P9E00681205/6/19 17:17 JMVug/L 3.9Phenanthrene
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 1.4Phenol
BRL 8270D P9E00681105/6/19 17:17 JMVug/L 3.5Pyrene
Surrogate Recovery Control Limits
43-140112 %2,4,6-Tribromophenol
44-119100 %2-Fluorobiphenyl
19-11967 %2-Fluorophenol
44-12095 %Nitrobenzene-d5
11-5244 %Phenol-d5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-201
Prism Sample ID: 9050052-02
Prism Work Order: 9050052
Time Collected: 04/29/19 13:10
Time Submitted: 05/01/19 11:55
J19050361
50-134104 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P9E009812.0 5/6/19 20:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P9E009812.0 5/6/19 20:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P9E009812.0 5/6/19 20:51 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.0894-Isopropyltoluene
7.7 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.31Acetone
BRL 8260B P9E00981205/6/19 20:51 KDMug/L 0.20Acrolein
BRL 8260B P9E00981205/6/19 20:51 KDMug/L 0.20Acrylonitrile
0.27 8260B P9E009810.50 5/6/19 20:51 KDMJug/L 0.048Benzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.057Bromobenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.14Bromochloromethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.062Bromodichloromethane
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.040Bromoform
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.18Bromomethane
BRL 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.075Carbon disulfide
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.062Chlorobenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.22Chloroethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.076Chloroform
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.079Chloromethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.079cis-1,3-Dichloropropylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-201
Prism Sample ID: 9050052-02
Prism Work Order: 9050052
Time Collected: 04/29/19 13:10
Time Submitted: 05/01/19 11:55
J19050361
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.081Dibromochloromethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.065Dibromomethane
BRL 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.061Ethylbenzene
BRL 8260B P9E009812.0 5/6/19 20:51 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.050Isopropyl Ether
0.87 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.12m,p-Xylenes
BRL 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P9E009815.0 5/6/19 20:51 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.083Methylene Chloride
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.19Naphthalene
BRL 8260B P9E009811.0 5/6/19 20:51 KDMug/L 0.076n-Butylbenzene
0.27 8260B P9E009810.50 5/6/19 20:51 KDMJug/L 0.087n-Propylbenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.044o-Xylene
1.2 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.047Styrene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.044Toluene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.078Trichloroethylene
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P9E009812.0 5/6/19 20:51 KDMug/L 0.060Vinyl acetate
BRL 8260B P9E009810.50 5/6/19 20:51 KDMug/L 0.097Vinyl chloride
BRL 8260B P9E009811.5 5/6/19 20:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124104 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123102 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P9E00441505/3/19 21:38 TBLug/L 4.0C5-C8 Aliphatics
23 MADEP VPH P9E00441505/3/19 21:38 TBLJug/L 3.9C9-C12 Aliphatics
11 MADEP VPH P9E00441505/3/19 21:38 TBLJug/L 4.2C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130120 %2,5-Dibromotoluene (PID)
70-130116 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-501
Prism Sample ID: 9050052-03
Prism Work Order: 9050052
Time Collected: 04/29/19 09:40
Time Submitted: 05/01/19 11:55
J19050361
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P9E006713805/10/19 17:21 BGBug/L 25C9-C18 Aliphatics
BRL MADEP EPH P9E006715405/10/19 17:21 BGBug/L 130C19-C36 Aliphatics
BRL MADEP EPH P9E006712705/10/19 17:21 BGBug/L 86C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14054 %1-Chlorooctadecane
40-14077 %o-Terphenyl
40-14090 %2-Fluorobiphenyl
40-140116 %2-Bromonaphthalene
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.01,2,4-Trichlorobenzene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.41,2-Dichlorobenzene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.91,3-Dichlorobenzene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.11,4-Dichlorobenzene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.61-Methylnaphthalene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 3.62,4,5-Trichlorophenol
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.52,4,6-Trichlorophenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.92,4-Dimethylphenol
BRL 8270D P9E00681505/6/19 17:39 JMVug/L 122,4-Dinitrophenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.22,4-Dinitrotoluene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 3.92,6-Dinitrotoluene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.72-Chloronaphthalene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.72-Chlorophenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.22-Methylnaphthalene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.42-Methylphenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.12-Nitroaniline
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.62-Nitrophenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.93,3’-Dichlorobenzidine
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.53/4-Methylphenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.83-Nitroaniline
BRL 8270D P9E00681505/6/19 17:39 JMVug/L 114,6-Dinitro-2-methylphenol
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.44-Bromophenyl phenyl ether
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.94-Chloro-3-methylphenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.54-Chloroaniline
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.74-Chlorophenyl phenyl ether
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.14-Nitroaniline
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.64-Nitrophenol
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.3Acenaphthene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.4Acenaphthylene
BRL 8270D P9E00681505/6/19 17:39 JMVug/L 12Aniline
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.6Anthracene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.2Azobenzene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-501
Prism Sample ID: 9050052-03
Prism Work Order: 9050052
Time Collected: 04/29/19 09:40
Time Submitted: 05/01/19 11:55
J19050361
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.2Benzo(a)anthracene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.5Benzo(a)pyrene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.5Benzo(b)fluoranthene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.6Benzo(g,h,i)perylene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.6Benzo(k)fluoranthene
BRL 8270D P9E006811005/6/19 17:39 JMVug/L 19Benzoic Acid
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.5Benzyl alcohol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.8bis(2-Chloroethoxy)methane
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.6Bis(2-Chloroethyl)ether
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.8Bis(2-chloroisopropyl)ether
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.7Bis(2-Ethylhexyl)phthalate
BRL 8270D P9E00681105/6/19 17:39 JMVug/LBromochloroacetonitrile
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.9Butyl benzyl phthalate
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.3Chrysene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 5.7Dibenzo(a,h)anthracene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.2Dibenzofuran
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.2Diethyl phthalate
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.1Dimethyl phthalate
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.3Di-n-butyl phthalate
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.5Di-n-octyl phthalate
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.0Fluoranthene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 5.0Fluorene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 3.9Hexachlorobenzene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.5Hexachlorobutadiene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 7.3Hexachlorocyclopentadiene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.7Hexachloroethane
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 2.6Indeno(1,2,3-cd)pyrene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.1Isophorone
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 4.1Naphthalene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.8Nitrobenzene
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 3.3N-Nitroso-di-n-propylamine
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 4.4N-Nitrosodiphenylamine
BRL 8270D P9E00681505/6/19 17:39 JMVug/L 11Pentachlorophenol
BRL 8270D P9E00681205/6/19 17:39 JMVug/L 3.9Phenanthrene
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 1.4Phenol
BRL 8270D P9E00681105/6/19 17:39 JMVug/L 3.5Pyrene
Surrogate Recovery Control Limits
43-14090 %2,4,6-Tribromophenol
44-11989 %2-Fluorobiphenyl
19-11956 %2-Fluorophenol
44-12089 %Nitrobenzene-d5
11-5237 %Phenol-d5
50-13496 %Terphenyl-d14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-501
Prism Sample ID: 9050052-03
Prism Work Order: 9050052
Time Collected: 04/29/19 09:40
Time Submitted: 05/01/19 11:55
J19050361
Volatile Organic Compounds by GC/MS
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P9E009812.0 5/6/19 21:24 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P9E009812.0 5/6/19 21:24 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P9E009812.0 5/6/19 21:24 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.31Acetone
BRL 8260B P9E00981205/6/19 21:24 KDMug/L 0.20Acrolein
BRL 8260B P9E00981205/6/19 21:24 KDMug/L 0.20Acrylonitrile
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.048Benzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.057Bromobenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.14Bromochloromethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.062Bromodichloromethane
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.040Bromoform
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.18Bromomethane
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.075Carbon disulfide
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.062Chlorobenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.22Chloroethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.076Chloroform
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.079Chloromethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Water
Client Sample ID: MW-501
Prism Sample ID: 9050052-03
Prism Work Order: 9050052
Time Collected: 04/29/19 09:40
Time Submitted: 05/01/19 11:55
J19050361
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.065Dibromomethane
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.061Ethylbenzene
BRL 8260B P9E009812.0 5/6/19 21:24 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.050Isopropyl Ether
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.12m,p-Xylenes
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P9E009815.0 5/6/19 21:24 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.083Methylene Chloride
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.19Naphthalene
BRL 8260B P9E009811.0 5/6/19 21:24 KDMug/L 0.076n-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.087n-Propylbenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.044o-Xylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.047Styrene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.044Toluene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.078Trichloroethylene
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P9E009812.0 5/6/19 21:24 KDMug/L 0.060Vinyl acetate
BRL 8260B P9E009810.50 5/6/19 21:24 KDMug/L 0.097Vinyl chloride
BRL 8260B P9E009811.5 5/6/19 21:24 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124102 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-123102 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P9E00441505/3/19 21:09 TBLug/L 4.0C5-C8 Aliphatics
BRL MADEP VPH P9E00441505/3/19 21:09 TBLug/L 3.9C9-C12 Aliphatics
BRL MADEP VPH P9E00441505/3/19 21:09 TBLug/L 4.2C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130123 %2,5-Dibromotoluene (PID)
70-130121 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Solid
Client Sample ID: MW-501 (4’)
Prism Sample ID: 9050052-04
Prism Work Order: 9050052
Time Collected: 04/29/19 09:25
Time Submitted: 05/01/19 11:55
J19050361
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P9E00421295/10/19 17:58 BGBmg/kg dry 1.4C9-C18 Aliphatics
BRL MADEP EPH P9E00421295/10/19 17:58 BGBmg/kg dry 4.9C19-C36 Aliphatics
BRL MADEP EPH P9E00421295/10/19 17:58 BGBmg/kg dry 7.9C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14082 %1-Chlorooctadecane
40-14096 %o-Terphenyl
40-14093 %2-Fluorobiphenyl
40-140121 %2-Bromonaphthalene
General Chemistry Parameters
83.5 *SM2540 G P9E014710.100 5/9/19 9:20 KBS% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.141,2,4-Trichlorobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.131,2-Dichlorobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.121,3-Dichlorobenzene
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.121,4-Dichlorobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.171-Methylnaphthalene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.172,4,5-Trichlorophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.192,4,6-Trichlorophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.152,4-Dichlorophenol
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.162,4-Dimethylphenol
BRL 8270D P9E007011.8 5/3/19 19:21 JMVmg/kg dry 0.462,4-Dinitrophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.212,4-Dinitrotoluene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.202,6-Dinitrotoluene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.192-Chloronaphthalene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.152-Chlorophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.152-Methylnaphthalene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.152-Methylphenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.132-Nitrophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.163,3’-Dichlorobenzidine
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.173/4-Methylphenol
BRL 8270D P9E007011.8 5/3/19 19:21 JMVmg/kg dry 0.444,6-Dinitro-2-methylphenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.194-Bromophenyl phenyl ether
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.154-Chloro-3-methylphenol
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.0964-Chloroaniline
BRL 8270D P9E007011.2 5/3/19 19:21 JMVmg/kg dry 0.244-Chlorophenyl phenyl ether
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.204-Nitrophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.19Acenaphthene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.21Acenaphthylene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.21Anthracene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Azobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Benzo(a)anthracene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Solid
Client Sample ID: MW-501 (4’)
Prism Sample ID: 9050052-04
Prism Work Order: 9050052
Time Collected: 04/29/19 09:25
Time Submitted: 05/01/19 11:55
J19050361
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18Benzo(a)pyrene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18Benzo(b)fluoranthene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.15Benzo(g,h,i)perylene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Benzo(k)fluoranthene
BRL 8270D P9E007012.4 5/3/19 19:21 JMVmg/kg dry 0.66Benzoic Acid
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.15Benzyl alcohol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.15bis(2-Chloroethoxy)methane
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.14Bis(2-chloroisopropyl)ether
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18Bis(2-Ethylhexyl)phthalate
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.14Butyl benzyl phthalate
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Chrysene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.23Dibenzo(a,h)anthracene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.21Dibenzofuran
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.20Diethyl phthalate
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.19Dimethyl phthalate
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.20Di-n-butyl phthalate
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.20Di-n-octyl phthalate
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.20Fluoranthene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.24Fluorene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Hexachlorobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18Hexachlorobutadiene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.27Hexachlorocyclopentadiene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.12Hexachloroethane
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.14Indeno(1,2,3-cd)pyrene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.17Isophorone
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.16Naphthalene
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.17Nitrobenzene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18N-Nitroso-di-n-propylamine
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.22N-Nitrosodiphenylamine
BRL 8270D P9E007011.2 5/3/19 19:21 JMVmg/kg dry 0.50Pentachlorophenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.20Phenanthrene
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.13Phenol
BRL 8270D P9E007010.79 5/3/19 19:21 JMVmg/kg dry 0.18Pyrene
BRL 8270D P9E007010.39 5/3/19 19:21 JMVmg/kg dry 0.075Pyridine
Surrogate Recovery Control Limits
39-13292 %2,4,6-Tribromophenol
44-11590 %2-Fluorobiphenyl
35-11587 %2-Fluorophenol
37-12282 %Nitrobenzene-d5
34-12185 %Phenol-d5
54-12792 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Solid
Client Sample ID: MW-501 (4’)
Prism Sample ID: 9050052-04
Prism Work Order: 9050052
Time Collected: 04/29/19 09:25
Time Submitted: 05/01/19 11:55
J19050361
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000481,1,1,2-Tetrachloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000571,1,1-Trichloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000281,1,2,2-Tetrachloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000421,1,2-Trichloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000701,1-Dichloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000721,1-Dichloroethylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000601,1-Dichloropropylene
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.000561,2,3-Trichlorobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000441,2,3-Trichloropropane
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.000371,2,4-Trichlorobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000411,2,4-Trimethylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000351,2-Dibromoethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000441,2-Dichlorobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000461,2-Dichloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000591,2-Dichloropropane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000491,3,5-Trimethylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000491,3-Dichlorobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000491,4-Dichlorobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000492,2-Dichloropropane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000522-Chlorotoluene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000444-Chlorotoluene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.000984-Isopropyltoluene
0.0088 8260B P9E006510.016 5/2/19 18:00 JLBJmg/kg dry 0.0010Acetone
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00061Benzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00054Bromobenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00064Bromochloromethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00030Bromoform
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.0019Bromomethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00077Carbon Tetrachloride
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00061Chlorobenzene
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.00074Chloroethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00048Chloroform
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.0012Chloromethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00061cis-1,2-Dichloroethylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00038cis-1,3-Dichloropropylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.0011Dichlorodifluoromethane
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00059Ethylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00057Isopropyl Ether
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00045Isopropylbenzene (Cumene)
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.0010m,p-Xylenes
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 49
Laboratory Report
05/14/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
409 Rogers View Court Project No.:
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Sample Matrix: Solid
Client Sample ID: MW-501 (4’)
Prism Sample ID: 9050052-04
Prism Work Order: 9050052
Time Collected: 04/29/19 09:25
Time Submitted: 05/01/19 11:55
J19050361
BRL 8260B P9E006510.016 5/2/19 18:00 JLBmg/kg dry 0.00027Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9E006510.016 5/2/19 18:00 JLBmg/kg dry 0.00091Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P9E006510.016 5/2/19 18:00 JLBmg/kg dry 0.00032Methyl Isobutyl Ketone
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00063Methylene Chloride
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00055Methyl-tert-Butyl Ether
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.00039Naphthalene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00037n-Butylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00057n-Propylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00042o-Xylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00042sec-Butylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00038Styrene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00046tert-Butylbenzene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00071Tetrachloroethylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00062Toluene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00075trans-1,2-Dichloroethylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P9E006510.0039 5/2/19 18:00 JLBmg/kg dry 0.00076Trichloroethylene
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.0011Trichlorofluoromethane
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.00042Vinyl acetate
BRL 8260B P9E006510.0078 5/2/19 18:00 JLBmg/kg dry 0.00077Vinyl chloride
BRL 8260B P9E006510.012 5/2/19 18:00 JLBmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130112 %4-Bromofluorobenzene
84-123110 %Dibromofluoromethane
76-129109 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID RLM
BRL MADEP VPH P9E00691003.9 5/3/19 15:01 TBLmg/kg dry 0.76C5-C8 Aliphatics
BRL MADEP VPH P9E00691003.9 5/3/19 15:01 TBLmg/kg dry 0.34C9-C12 Aliphatics
BRL MADEP VPH P9E00691003.9 5/3/19 15:01 TBLmg/kg dry 0.36C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130140 %2,5-Dibromotoluene (PID)SR
70-130137 %2,5-Dibromotoluene (FID)SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0065 - 5035
Blank (P9E0065-BLK1)Prepared & Analyzed: 05/02/19
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0050
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0065 - 5035
Blank (P9E0065-BLK1)Prepared & Analyzed: 05/02/19
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl acetate mg/kg wetBRL0.010
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10954.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10452.2
ug/L 50.00 76-129Surrogate: Toluene-d8 10954.5
LCS (P9E0065-BS1)Prepared & Analyzed: 05/02/19
1,1,1,2-Tetrachloroethane mg/kg wet0.0488 0.0050 0.05000 72-11598
1,1,1-Trichloroethane mg/kg wet0.0418 0.0050 0.05000 67-13184
1,1,2,2-Tetrachloroethane mg/kg wet0.0577 0.0050 0.05000 56-126115
1,1,2-Trichloroethane mg/kg wet0.0460 0.0050 0.05000 70-13392
1,1-Dichloroethane mg/kg wet0.0426 0.0050 0.05000 74-12785
1,1-Dichloroethylene mg/kg wet0.0477 0.0050 0.05000 67-14995
1,1-Dichloropropylene mg/kg wet0.0432 0.0050 0.05000 71-13086
1,2,3-Trichlorobenzene mg/kg wet0.0574 0.010 0.05000 68-130115
1,2,3-Trichloropropane mg/kg wet0.0586 0.0050 0.05000 60-137117
1,2,4-Trichlorobenzene mg/kg wet0.0568 0.010 0.05000 66-125114
1,2,4-Trimethylbenzene mg/kg wet0.0589 0.0050 0.05000 69-129118
1,2-Dibromoethane mg/kg wet0.0460 0.0050 0.05000 70-13292
1,2-Dichlorobenzene mg/kg wet0.0561 0.0050 0.05000 72-123112
1,2-Dichloroethane mg/kg wet0.0416 0.0050 0.05000 68-12883
1,2-Dichloropropane mg/kg wet0.0451 0.0050 0.05000 73-13090
1,3,5-Trimethylbenzene mg/kg wet0.0589 0.0050 0.05000 69-128118
1,3-Dichlorobenzene mg/kg wet0.0564 0.0050 0.05000 71-120113
1,3-Dichloropropane mg/kg wet0.0462 0.0050 0.05000 75-12492
1,4-Dichlorobenzene mg/kg wet0.0564 0.0050 0.05000 71-123113
2,2-Dichloropropane mg/kg wet0.0430 0.0050 0.05000 50-14286
2-Chlorotoluene mg/kg wet0.0571 0.0050 0.05000 67-124114
4-Chlorotoluene mg/kg wet0.0572 0.0050 0.05000 71-126114
4-Isopropyltoluene mg/kg wet0.0589 0.0050 0.05000 68-129118
Acetone mg/kg wet0.151 0.020 0.1000 29-198151
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0065 - 5035
LCS (P9E0065-BS1)Prepared & Analyzed: 05/02/19
Benzene mg/kg wet0.0422 0.0050 0.05000 74-12784
Bromobenzene mg/kg wet0.0575 0.0050 0.05000 73-125115
Bromochloromethane mg/kg wet0.0418 0.0050 0.05000 72-13484
Bromodichloromethane mg/kg wet0.0420 0.0050 0.05000 75-12284
Bromoform mg/kg wet0.0452 0.0050 0.05000 66-13590
Bromomethane mg/kg wet0.0471 0.010 0.05000 20-18094
Carbon Tetrachloride mg/kg wet0.0433 0.0050 0.05000 64-14387
Chlorobenzene mg/kg wet0.0448 0.0050 0.05000 74-11890
Chloroethane mg/kg wet0.0616 0.010 0.05000 33-149123
Chloroform mg/kg wet0.0453 0.0050 0.05000 73-12791
Chloromethane mg/kg wet0.0417 0.010 0.05000 45-14383
cis-1,2-Dichloroethylene mg/kg wet0.0425 0.0050 0.05000 76-13485
cis-1,3-Dichloropropylene mg/kg wet0.0439 0.0050 0.05000 71-12588
Dibromochloromethane mg/kg wet0.0446 0.0050 0.05000 73-12289
Dichlorodifluoromethane mg/kg wet0.0397 0.010 0.05000 26-14679
Ethylbenzene mg/kg wet0.0465 0.0050 0.05000 74-12893
Isopropyl Ether mg/kg wet0.0401 0.0050 0.05000 59-15980
Isopropylbenzene (Cumene)mg/kg wet0.0594 0.0050 0.05000 68-126119
m,p-Xylenes mg/kg wet0.0932 0.010 0.1000 75-12493
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0530 0.020 0.05000 61-157106
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0588 0.020 0.05000 63-149118
Methyl Isobutyl Ketone mg/kg wet0.0439 0.020 0.05000 57-16288
Methylene Chloride mg/kg wet0.0435 0.0050 0.05000 74-12987
Methyl-tert-Butyl Ether mg/kg wet0.0425 0.0050 0.05000 70-13085
Naphthalene mg/kg wet0.0557 0.010 0.05000 57-157111
n-Butylbenzene mg/kg wet0.0605 0.0050 0.05000 65-135121
n-Propylbenzene mg/kg wet0.0586 0.0050 0.05000 67-130117
o-Xylene mg/kg wet0.0466 0.0050 0.05000 74-12693
sec-Butylbenzene mg/kg wet0.0592 0.0050 0.05000 66-131118
Styrene mg/kg wet0.0454 0.0050 0.05000 77-12191
tert-Butylbenzene mg/kg wet0.0589 0.0050 0.05000 67-132118
Tetrachloroethylene mg/kg wet0.0435 0.0050 0.05000 68-13087
Toluene mg/kg wet0.0470 0.0050 0.05000 71-12994
trans-1,2-Dichloroethylene mg/kg wet0.0422 0.0050 0.05000 73-13284
trans-1,3-Dichloropropylene mg/kg wet0.0437 0.0050 0.05000 68-12387
Trichloroethylene mg/kg wet0.0423 0.0050 0.05000 75-13385
Trichlorofluoromethane mg/kg wet0.0409 0.010 0.05000 44-14682
Vinyl acetate mg/kg wet0.0445 0.010 0.05000 85-16189
Vinyl chloride mg/kg wet0.0398 0.010 0.05000 48-14780
Xylenes, total mg/kg wet0.140 0.015 0.1500 74-12693
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10753.5
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10251.2
ug/L 50.00 76-129Surrogate: Toluene-d8 10954.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0065 - 5035
LCS Dup (P9E0065-BSD1)Prepared & Analyzed: 05/02/19
1,1,1,2-Tetrachloroethane mg/kg wet0.0444 0.0050 0.05000 2072-11589 9
1,1,1-Trichloroethane mg/kg wet0.0375 0.0050 0.05000 2067-13175 11
1,1,2,2-Tetrachloroethane mg/kg wet0.0550 0.0050 0.05000 2056-126110 5
1,1,2-Trichloroethane mg/kg wet0.0421 0.0050 0.05000 2070-13384 9
1,1-Dichloroethane mg/kg wet0.0387 0.0050 0.05000 2074-12777 10
1,1-Dichloroethylene mg/kg wet0.0412 0.0050 0.05000 2067-14982 15
1,1-Dichloropropylene mg/kg wet0.0383 0.0050 0.05000 2071-13077 12
1,2,3-Trichlorobenzene mg/kg wet0.0523 0.010 0.05000 2068-130105 9
1,2,3-Trichloropropane mg/kg wet0.0555 0.0050 0.05000 2060-137111 5
1,2,4-Trichlorobenzene mg/kg wet0.0518 0.010 0.05000 2066-125104 9
1,2,4-Trimethylbenzene mg/kg wet0.0533 0.0050 0.05000 2069-129107 10
1,2-Dibromoethane mg/kg wet0.0423 0.0050 0.05000 2070-13285 8
1,2-Dichlorobenzene mg/kg wet0.0520 0.0050 0.05000 2072-123104 8
1,2-Dichloroethane mg/kg wet0.0378 0.0050 0.05000 2068-12876 9
1,2-Dichloropropane mg/kg wet0.0407 0.0050 0.05000 2073-13081 10
1,3,5-Trimethylbenzene mg/kg wet0.0538 0.0050 0.05000 2069-128108 9
1,3-Dichlorobenzene mg/kg wet0.0511 0.0050 0.05000 2071-120102 10
1,3-Dichloropropane mg/kg wet0.0432 0.0050 0.05000 2075-12486 7
1,4-Dichlorobenzene mg/kg wet0.0515 0.0050 0.05000 2071-123103 9
2,2-Dichloropropane mg/kg wet0.0386 0.0050 0.05000 2050-14277 11
2-Chlorotoluene mg/kg wet0.0520 0.0050 0.05000 2067-124104 9
4-Chlorotoluene mg/kg wet0.0520 0.0050 0.05000 2071-126104 9
4-Isopropyltoluene mg/kg wet0.0532 0.0050 0.05000 2068-129106 10
Acetone mg/kg wet0.110 0.020 0.1000 20 D29-198110 31
Benzene mg/kg wet0.0380 0.0050 0.05000 2074-12776 10
Bromobenzene mg/kg wet0.0530 0.0050 0.05000 2073-125106 8
Bromochloromethane mg/kg wet0.0387 0.0050 0.05000 2072-13477 8
Bromodichloromethane mg/kg wet0.0381 0.0050 0.05000 2075-12276 10
Bromoform mg/kg wet0.0424 0.0050 0.05000 2066-13585 6
Bromomethane mg/kg wet0.0433 0.010 0.05000 2020-18087 8
Carbon Tetrachloride mg/kg wet0.0380 0.0050 0.05000 2064-14376 13
Chlorobenzene mg/kg wet0.0406 0.0050 0.05000 2074-11881 10
Chloroethane mg/kg wet0.0542 0.010 0.05000 2033-149108 13
Chloroform mg/kg wet0.0406 0.0050 0.05000 2073-12781 11
Chloromethane mg/kg wet0.0373 0.010 0.05000 2045-14375 11
cis-1,2-Dichloroethylene mg/kg wet0.0382 0.0050 0.05000 2076-13476 11
cis-1,3-Dichloropropylene mg/kg wet0.0399 0.0050 0.05000 2071-12580 10
Dibromochloromethane mg/kg wet0.0413 0.0050 0.05000 2073-12283 8
Dichlorodifluoromethane mg/kg wet0.0350 0.010 0.05000 2026-14670 12
Ethylbenzene mg/kg wet0.0420 0.0050 0.05000 2074-12884 10
Isopropyl Ether mg/kg wet0.0367 0.0050 0.05000 2059-15973 9
Isopropylbenzene (Cumene)mg/kg wet0.0536 0.0050 0.05000 2068-126107 10
m,p-Xylenes mg/kg wet0.0845 0.010 0.1000 2075-12485 10
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0470 0.020 0.05000 2061-15794 12
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0481 0.020 0.05000 2063-14996 20
Methyl Isobutyl Ketone mg/kg wet0.0414 0.020 0.05000 2057-16283 6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0065 - 5035
LCS Dup (P9E0065-BSD1)Prepared & Analyzed: 05/02/19
Methylene Chloride mg/kg wet0.0390 0.0050 0.05000 2074-12978 11
Methyl-tert-Butyl Ether mg/kg wet0.0384 0.0050 0.05000 2070-13077 10
Naphthalene mg/kg wet0.0528 0.010 0.05000 2057-157106 5
n-Butylbenzene mg/kg wet0.0540 0.0050 0.05000 2065-135108 11
n-Propylbenzene mg/kg wet0.0532 0.0050 0.05000 2067-130106 10
o-Xylene mg/kg wet0.0420 0.0050 0.05000 2074-12684 10
sec-Butylbenzene mg/kg wet0.0539 0.0050 0.05000 2066-131108 9
Styrene mg/kg wet0.0416 0.0050 0.05000 2077-12183 9
tert-Butylbenzene mg/kg wet0.0532 0.0050 0.05000 2067-132106 10
Tetrachloroethylene mg/kg wet0.0386 0.0050 0.05000 2068-13077 12
Toluene mg/kg wet0.0416 0.0050 0.05000 2071-12983 12
trans-1,2-Dichloroethylene mg/kg wet0.0372 0.0050 0.05000 2073-13274 13
trans-1,3-Dichloropropylene mg/kg wet0.0401 0.0050 0.05000 2068-12380 8
Trichloroethylene mg/kg wet0.0372 0.0050 0.05000 20 L275-13374 13
Trichlorofluoromethane mg/kg wet0.0357 0.010 0.05000 2044-14671 14
Vinyl acetate mg/kg wet0.0428 0.010 0.05000 2085-16186 4
Vinyl chloride mg/kg wet0.0350 0.010 0.05000 2048-14770 13
Xylenes, total mg/kg wet0.126 0.015 0.1500 2074-12684 10
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10954.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 76-129Surrogate: Toluene-d8 10954.4
Batch P9E0098 - 5030B
Blank (P9E0098-BLK1)Prepared & Analyzed: 05/06/19
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0098 - 5030B
Blank (P9E0098-BLK1)Prepared & Analyzed: 05/06/19
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL5.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0098 - 5030B
Blank (P9E0098-BLK1)Prepared & Analyzed: 05/06/19
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.7
ug/L 50.00 77-123Surrogate: Toluene-d8 10150.5
LCS (P9E0098-BS1)Prepared & Analyzed: 05/06/19
1,1,1,2-Tetrachloroethane ug/L21.6 0.50 20.00 79-134108
1,1,1-Trichloroethane ug/L20.2 0.50 20.00 75-136101
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 62-127107
1,1,2-Trichloroethane ug/L20.2 0.50 20.00 70-140101
1,1-Dichloroethane ug/L20.9 0.50 20.00 78-130104
1,1-Dichloroethylene ug/L18.0 0.50 20.00 70-15490
1,1-Dichloropropylene ug/L19.3 0.50 20.00 71-13697
1,2,3-Trichlorobenzene ug/L20.3 2.0 20.00 58-144101
1,2,3-Trichloropropane ug/L20.7 1.0 20.00 71-127104
1,2,4-Trichlorobenzene ug/L20.0 1.0 20.00 66-139100
1,2,4-Trimethylbenzene ug/L21.8 0.50 20.00 75-133109
1,2-Dibromo-3-chloropropane ug/L20.4 2.0 20.00 63-134102
1,2-Dibromoethane ug/L20.4 0.50 20.00 77-135102
1,2-Dichlorobenzene ug/L20.9 0.50 20.00 78-128104
1,2-Dichloroethane ug/L20.5 0.50 20.00 68-131103
1,2-Dichloropropane ug/L19.9 0.50 20.00 77-130100
1,3,5-Trimethylbenzene ug/L21.6 0.50 20.00 75-131108
1,3-Dichlorobenzene ug/L20.5 0.50 20.00 77-125102
1,3-Dichloropropane ug/L21.7 0.50 20.00 76-132109
1,4-Dichlorobenzene ug/L20.8 0.50 20.00 75-126104
2,2-Dichloropropane ug/L20.9 2.0 20.00 29-149104
2-Chlorotoluene ug/L20.6 0.50 20.00 74-126103
4-Chlorotoluene ug/L20.8 0.50 20.00 78-129104
4-Isopropyltoluene ug/L19.1 0.50 20.00 69-13296
Acetone ug/L55.1 5.0 40.00 40-166138
Acrolein ug/L38.2 20 40.00 70-13095
Acrylonitrile ug/L38.5 20 40.00 81-12796
Benzene ug/L21.0 0.50 20.00 77-128105
Bromobenzene ug/L20.4 0.50 20.00 78-129102
Bromochloromethane ug/L20.2 0.50 20.00 78-135101
Bromodichloromethane ug/L20.5 0.50 20.00 76-138102
Bromoform ug/L22.0 1.0 20.00 71-135110
Bromomethane ug/L16.4 1.0 20.00 41-16882
Carbon disulfide ug/L20.2 5.0 20.00 59-135101
Carbon Tetrachloride ug/L19.7 0.50 20.00 72-14299
Chlorobenzene ug/L20.8 0.50 20.00 78-119104
Chloroethane ug/L20.1 0.50 20.00 57-142100
Chloroform ug/L20.8 0.50 20.00 77-130104
Chloromethane ug/L20.8 0.50 20.00 47-145104
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 76-141104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0098 - 5030B
LCS (P9E0098-BS1)Prepared & Analyzed: 05/06/19
cis-1,3-Dichloropropylene ug/L21.5 0.50 20.00 65-140108
Dibromochloromethane ug/L21.4 0.50 20.00 75-134107
Dibromomethane ug/L21.4 0.50 20.00 76-138107
Dichlorodifluoromethane ug/L16.6 5.0 20.00 28-16383
Ethylbenzene ug/L21.7 0.50 20.00 80-127108
Hexachlorobutadiene ug/L19.6 2.0 20.00 61-13498
Isopropyl Ether ug/L19.2 0.50 20.00 60-15496
Isopropylbenzene (Cumene)ug/L19.6 0.50 20.00 70-13098
m,p-Xylenes ug/L43.4 1.0 40.00 77-133108
Methyl Butyl Ketone (2-Hexanone)ug/L23.8 5.0 20.00 64-137119
Methyl Ethyl Ketone (2-Butanone)ug/L27.0 5.0 20.00 LH71-134135
Methyl Isobutyl Ketone ug/L22.3 5.0 20.00 69-134112
Methylene Chloride ug/L20.4 1.0 20.00 73-131102
Methyl-tert-Butyl Ether ug/L21.2 0.50 20.00 68-135106
Naphthalene ug/L20.6 1.0 20.00 64-136103
n-Butylbenzene ug/L18.6 1.0 20.00 68-13493
n-Propylbenzene ug/L21.0 0.50 20.00 72-132105
o-Xylene ug/L21.8 0.50 20.00 78-128109
sec-Butylbenzene ug/L18.8 0.50 20.00 71-13194
Styrene ug/L19.1 0.50 20.00 78-12995
tert-Butylbenzene ug/L18.7 0.50 20.00 70-13293
Tetrachloroethylene ug/L18.8 0.50 20.00 80-12994
Toluene ug/L21.7 0.50 20.00 76-131108
trans-1,2-Dichloroethylene ug/L20.4 0.50 20.00 76-135102
trans-1,3-Dichloropropylene ug/L23.5 0.50 20.00 67-140117
Trichloroethylene ug/L20.4 0.50 20.00 77-133102
Trichlorofluoromethane ug/L16.5 0.50 20.00 62-14883
Vinyl acetate ug/L20.0 2.0 20.00 34-167100
Vinyl chloride ug/L16.7 0.50 20.00 57-14184
Xylenes, total ug/L65.2 1.5 60.00 77-133109
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9849.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9949.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0098 - 5030B
LCS Dup (P9E0098-BSD1)Prepared & Analyzed: 05/06/19
1,1,1,2-Tetrachloroethane ug/L21.8 0.50 20.00 2079-134109 1
1,1,1-Trichloroethane ug/L21.4 0.50 20.00 2075-136107 6
1,1,2,2-Tetrachloroethane ug/L22.1 0.50 20.00 2062-127110 4
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 2070-140103 2
1,1-Dichloroethane ug/L20.9 0.50 20.00 2078-130105 0.2
1,1-Dichloroethylene ug/L18.1 0.50 20.00 2070-15490 0.3
1,1-Dichloropropylene ug/L18.8 0.50 20.00 2071-13694 3
1,2,3-Trichlorobenzene ug/L19.8 2.0 20.00 2058-14499 2
1,2,3-Trichloropropane ug/L20.1 1.0 20.00 2071-127100 3
1,2,4-Trichlorobenzene ug/L20.4 1.0 20.00 2066-139102 2
1,2,4-Trimethylbenzene ug/L21.7 0.50 20.00 2075-133109 0.4
1,2-Dibromo-3-chloropropane ug/L20.2 2.0 20.00 2063-134101 1
1,2-Dibromoethane ug/L21.6 0.50 20.00 2077-135108 6
1,2-Dichlorobenzene ug/L21.6 0.50 20.00 2078-128108 4
1,2-Dichloroethane ug/L21.3 0.50 20.00 2068-131106 4
1,2-Dichloropropane ug/L20.1 0.50 20.00 2077-130100 0.9
1,3,5-Trimethylbenzene ug/L21.6 0.50 20.00 2075-131108 0.05
1,3-Dichlorobenzene ug/L20.8 0.50 20.00 2077-125104 1
1,3-Dichloropropane ug/L21.4 0.50 20.00 2076-132107 1
1,4-Dichlorobenzene ug/L20.6 0.50 20.00 2075-126103 0.5
2,2-Dichloropropane ug/L21.2 2.0 20.00 2029-149106 1
2-Chlorotoluene ug/L20.6 0.50 20.00 2074-126103 0.2
4-Chlorotoluene ug/L20.7 0.50 20.00 2078-129104 0.5
4-Isopropyltoluene ug/L18.8 0.50 20.00 2069-13294 2
Acetone ug/L56.5 5.0 40.00 2040-166141 3
Acrolein ug/L40.1 20 40.00 2070-130100 5
Acrylonitrile ug/L39.3 20 40.00 2081-12798 2
Benzene ug/L21.0 0.50 20.00 2077-128105 0.2
Bromobenzene ug/L20.8 0.50 20.00 2078-129104 2
Bromochloromethane ug/L20.4 0.50 20.00 2078-135102 1
Bromodichloromethane ug/L20.8 0.50 20.00 2076-138104 1
Bromoform ug/L21.4 1.0 20.00 2071-135107 3
Bromomethane ug/L18.0 1.0 20.00 2041-16890 10
Carbon disulfide ug/L20.2 5.0 20.00 2059-135101 0.5
Carbon Tetrachloride ug/L19.9 0.50 20.00 2072-14299 0.8
Chlorobenzene ug/L20.2 0.50 20.00 2078-119101 3
Chloroethane ug/L20.7 0.50 20.00 2057-142103 3
Chloroform ug/L20.2 0.50 20.00 2077-130101 3
Chloromethane ug/L20.2 0.50 20.00 2047-145101 3
cis-1,2-Dichloroethylene ug/L20.9 0.50 20.00 2076-141105 0.5
cis-1,3-Dichloropropylene ug/L21.7 0.50 20.00 2065-140108 0.6
Dibromochloromethane ug/L21.6 0.50 20.00 2075-134108 0.7
Dibromomethane ug/L21.6 0.50 20.00 2076-138108 1
Dichlorodifluoromethane ug/L15.1 5.0 20.00 2028-16375 9
Ethylbenzene ug/L21.5 0.50 20.00 2080-127107 1
Hexachlorobutadiene ug/L19.0 2.0 20.00 2061-13495 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9E0098 - 5030B
LCS Dup (P9E0098-BSD1)Prepared & Analyzed: 05/06/19
Isopropyl Ether ug/L19.9 0.50 20.00 2060-15499 3
Isopropylbenzene (Cumene)ug/L19.4 0.50 20.00 2070-13097 0.6
m,p-Xylenes ug/L43.2 1.0 40.00 2077-133108 0.5
Methyl Butyl Ketone (2-Hexanone)ug/L22.9 5.0 20.00 2064-137115 4
Methyl Ethyl Ketone (2-Butanone)ug/L27.3 5.0 20.00 20 LH71-134137 1
Methyl Isobutyl Ketone ug/L22.4 5.0 20.00 2069-134112 0.4
Methylene Chloride ug/L20.7 1.0 20.00 2073-131104 2
Methyl-tert-Butyl Ether ug/L22.1 0.50 20.00 2068-135111 4
Naphthalene ug/L21.5 1.0 20.00 2064-136107 4
n-Butylbenzene ug/L18.1 1.0 20.00 2068-13491 2
n-Propylbenzene ug/L20.9 0.50 20.00 2072-132105 0.4
o-Xylene ug/L21.3 0.50 20.00 2078-128107 2
sec-Butylbenzene ug/L18.8 0.50 20.00 2071-13194 0.2
Styrene ug/L18.6 0.50 20.00 2078-12993 2
tert-Butylbenzene ug/L19.1 0.50 20.00 2070-13295 2
Tetrachloroethylene ug/L18.7 0.50 20.00 2080-12993 0.6
Toluene ug/L21.6 0.50 20.00 2076-131108 0.5
trans-1,2-Dichloroethylene ug/L20.4 0.50 20.00 2076-135102 0
trans-1,3-Dichloropropylene ug/L22.9 0.50 20.00 2067-140114 3
Trichloroethylene ug/L20.0 0.50 20.00 2077-133100 2
Trichlorofluoromethane ug/L16.2 0.50 20.00 2062-14881 2
Vinyl acetate ug/L20.7 2.0 20.00 2034-167103 3
Vinyl chloride ug/L16.7 0.50 20.00 2057-14184 0.06
Xylenes, total ug/L64.5 1.5 60.00 2077-133107 1
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10351.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9849.0
ug/L 50.00 77-123Surrogate: Toluene-d8 9949.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
Blank (P9E0068-BLK1)Prepared: 05/03/19 Analyzed: 05/06/19
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL20
2,4,6-Trichlorophenol ug/LBRL20
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL50
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL20
2-Chloronaphthalene ug/LBRL20
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3’-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL50
4-Bromophenyl phenyl ether ug/LBRL20
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL20
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
Acenaphthene ug/LBRL20
Acenaphthylene ug/LBRL20
Aniline ug/LBRL50
Anthracene ug/LBRL20
Azobenzene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
Blank (P9E0068-BLK1)Prepared: 05/03/19 Analyzed: 05/06/19
Dibenzo(a,h)anthracene ug/LBRL20
Dibenzofuran ug/LBRL20
Diethyl phthalate ug/LBRL20
Dimethyl phthalate ug/LBRL20
Di-n-butyl phthalate ug/LBRL20
Di-n-octyl phthalate ug/LBRL10
Fluoranthene ug/LBRL20
Fluorene ug/LBRL20
Hexachlorobenzene ug/LBRL20
Hexachlorobutadiene ug/LBRL20
Hexachlorocyclopentadiene ug/LBRL20
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL20
N-Nitrosodiphenylamine ug/LBRL20
Pentachlorophenol ug/LBRL50
Phenanthrene ug/LBRL20
Phenol ug/LBRL10
Pyrene ug/LBRL10
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 106106
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 9848.8
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6666.5
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 10050.2
ug/L 100.0 11-52Surrogate: Phenol-d5 4141.2
ug/L 50.00 50-134Surrogate: Terphenyl-d14 11356.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
LCS (P9E0068-BS1)Prepared: 05/03/19 Analyzed: 05/06/19
1,2,4-Trichlorobenzene ug/L29.7 10 50.00 29-12659
1,2-Dichlorobenzene ug/L29.9 10 50.00 32-11160
1,3-Dichlorobenzene ug/L28.2 10 50.00 28-11056
1,4-Dichlorobenzene ug/L28.6 10 50.00 29-11257
1-Methylnaphthalene ug/L38.5 10 50.00 41-11977
2,4,5-Trichlorophenol ug/L51.5 20 50.00 53-123103
2,4,6-Trichlorophenol ug/L51.6 20 50.00 50-125103
2,4-Dichlorophenol ug/L42.2 10 50.00 47-12184
2,4-Dimethylphenol ug/L50.3 10 50.00 31-124101
2,4-Dinitrophenol ug/L31.8 50 50.00 J23-14364
2,4-Dinitrotoluene ug/L52.6 10 50.00 57-128105
2,6-Dinitrotoluene ug/L52.7 20 50.00 57-124105
2-Chloronaphthalene ug/L44.4 20 50.00 40-11689
2-Chlorophenol ug/L45.1 10 50.00 38-11790
2-Methylnaphthalene ug/L36.1 10 50.00 40-12172
2-Methylphenol ug/L45.8 10 50.00 30-11792
2-Nitroaniline ug/L49.3 10 50.00 55-12799
2-Nitrophenol ug/L41.0 10 50.00 47-12382
3,3’-Dichlorobenzidine ug/L58.8 10 50.00 27-129118
3/4-Methylphenol ug/L36.7 10 50.00 29-11073
3-Nitroaniline ug/L50.1 10 50.00 41-128100
4,6-Dinitro-2-methylphenol ug/L42.2 50 50.00 J44-13784
4-Bromophenyl phenyl ether ug/L50.5 20 50.00 55-124101
4-Chloro-3-methylphenol ug/L45.6 10 50.00 52-11991
4-Chloroaniline ug/L46.0 10 50.00 33-11792
4-Chlorophenyl phenyl ether ug/L51.1 20 50.00 53-121102
4-Nitroaniline ug/L50.6 10 50.00 45-135101
4-Nitrophenol ug/L22.1 10 50.00 10-7744
Acenaphthene ug/L50.2 20 50.00 47-122100
Acenaphthylene ug/L48.0 20 50.00 41-13096
Aniline ug/L54.8 50 50.00 12-197110
Anthracene ug/L55.4 20 50.00 57-123111
Azobenzene ug/L52.9 10 50.00 61-116106
Benzo(a)anthracene ug/L54.7 10 50.00 58-125109
Benzo(a)pyrene ug/L52.9 10 50.00 54-128106
Benzo(b)fluoranthene ug/L53.2 10 50.00 53-131106
Benzo(g,h,i)perylene ug/L54.6 10 50.00 50-134109
Benzo(k)fluoranthene ug/L51.8 10 50.00 57-129104
Benzoic Acid ug/LBRL100 50.00 L10-125
Benzyl alcohol ug/L38.0 10 50.00 31-11276
bis(2-Chloroethoxy)methane ug/L42.7 10 50.00 48-12085
Bis(2-Chloroethyl)ether ug/L42.0 10 50.00 43-11884
Bis(2-chloroisopropyl)ether ug/L43.2 10 50.00 37-13086
Bis(2-Ethylhexyl)phthalate ug/L56.6 10 50.00 55-135113
Butyl benzyl phthalate ug/L55.4 10 50.00 53-134111
Chrysene ug/L54.8 10 50.00 59-123110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
LCS (P9E0068-BS1)Prepared: 05/03/19 Analyzed: 05/06/19
Dibenzo(a,h)anthracene ug/L54.4 20 50.00 51-134109
Dibenzofuran ug/L49.5 20 50.00 53-11899
Diethyl phthalate ug/L53.8 20 50.00 56-125108
Dimethyl phthalate ug/L52.1 20 50.00 45-127104
Di-n-butyl phthalate ug/L54.0 20 50.00 59-127108
Di-n-octyl phthalate ug/L53.6 10 50.00 51-140107
Fluoranthene ug/L53.8 20 50.00 57-128108
Fluorene ug/L53.0 20 50.00 52-124106
Hexachlorobenzene ug/L49.7 20 50.00 53-12599
Hexachlorobutadiene ug/L27.7 20 50.00 22-12455
Hexachlorocyclopentadiene ug/L24.4 20 50.00 32-11749
Hexachloroethane ug/L26.2 10 50.00 21-11552
Indeno(1,2,3-cd)pyrene ug/L53.2 10 50.00 52-134106
Isophorone ug/L43.6 10 50.00 42-12487
Naphthalene ug/L34.2 10 50.00 40-12168
Nitrobenzene ug/L40.2 10 50.00 45-12180
N-Nitroso-di-n-propylamine ug/L47.7 20 50.00 49-11995
N-Nitrosodiphenylamine ug/L63.4 20 50.00 L151-123127
Pentachlorophenol ug/L50.4 50 50.00 35-138101
Phenanthrene ug/L54.1 20 50.00 59-120108
Phenol ug/L20.4 10 50.00 12-5841
Pyrene ug/L55.2 10 50.00 57-126110
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 108108
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 9346.4
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6059.6
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8241.0
ug/L 100.0 11-52Surrogate: Phenol-d5 3939.1
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10854.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
LCS Dup (P9E0068-BSD1)Prepared: 05/03/19 Analyzed: 05/06/19
1,2,4-Trichlorobenzene ug/L30.2 10 50.00 2029-12660 2
1,2-Dichlorobenzene ug/L31.9 10 50.00 2032-11164 6
1,3-Dichlorobenzene ug/L29.9 10 50.00 2028-11060 6
1,4-Dichlorobenzene ug/L30.8 10 50.00 2029-11262 8
1-Methylnaphthalene ug/L36.6 10 50.00 2041-11973 5
2,4,5-Trichlorophenol ug/L50.1 20 50.00 2053-123100 3
2,4,6-Trichlorophenol ug/L50.2 20 50.00 2050-125100 3
2,4-Dichlorophenol ug/L42.1 10 50.00 2047-12184 0.2
2,4-Dimethylphenol ug/L51.7 10 50.00 2031-124103 3
2,4-Dinitrophenol ug/L36.1 50 50.00 20 J23-14372 13
2,4-Dinitrotoluene ug/L50.7 10 50.00 2057-128101 4
2,6-Dinitrotoluene ug/L50.8 20 50.00 2057-124102 4
2-Chloronaphthalene ug/L42.2 20 50.00 2040-11684 5
2-Chlorophenol ug/L46.5 10 50.00 2038-11793 3
2-Methylnaphthalene ug/L34.7 10 50.00 2040-12169 4
2-Methylphenol ug/L46.4 10 50.00 2030-11793 1
2-Nitroaniline ug/L48.4 10 50.00 2055-12797 2
2-Nitrophenol ug/L41.5 10 50.00 2047-12383 1
3,3’-Dichlorobenzidine ug/L55.0 10 50.00 2027-129110 7
3/4-Methylphenol ug/L36.7 10 50.00 2029-11073 0.1
3-Nitroaniline ug/L48.5 10 50.00 2041-12897 3
4,6-Dinitro-2-methylphenol ug/L41.3 50 50.00 20 J44-13783 2
4-Bromophenyl phenyl ether ug/L48.1 20 50.00 2055-12496 5
4-Chloro-3-methylphenol ug/L44.1 10 50.00 2052-11988 4
4-Chloroaniline ug/L45.0 10 50.00 2033-11790 2
4-Chlorophenyl phenyl ether ug/L48.8 20 50.00 2053-12198 4
4-Nitroaniline ug/L49.4 10 50.00 2045-13599 2
4-Nitrophenol ug/L21.7 10 50.00 2010-7743 2
Acenaphthene ug/L47.2 20 50.00 2047-12294 6
Acenaphthylene ug/L46.6 20 50.00 2041-13093 3
Aniline ug/L56.5 50 50.00 2012-197113 3
Anthracene ug/L52.6 20 50.00 2057-123105 5
Azobenzene ug/L49.6 10 50.00 2061-11699 7
Benzo(a)anthracene ug/L50.7 10 50.00 2058-125101 8
Benzo(a)pyrene ug/L49.8 10 50.00 2054-128100 6
Benzo(b)fluoranthene ug/L50.0 10 50.00 2053-131100 6
Benzo(g,h,i)perylene ug/L50.8 10 50.00 2050-134102 7
Benzo(k)fluoranthene ug/L48.8 10 50.00 2057-12998 6
Benzoic Acid ug/LBRL100 50.00 20 L10-125
Benzyl alcohol ug/L38.2 10 50.00 2031-11276 0.8
bis(2-Chloroethoxy)methane ug/L43.0 10 50.00 2048-12086 0.7
Bis(2-Chloroethyl)ether ug/L44.8 10 50.00 2043-11890 6
Bis(2-chloroisopropyl)ether ug/L43.9 10 50.00 2037-13088 2
Bis(2-Ethylhexyl)phthalate ug/L52.2 10 50.00 2055-135104 8
Butyl benzyl phthalate ug/L51.8 10 50.00 2053-134104 7
Chrysene ug/L50.8 10 50.00 2059-123102 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0068 - 3510C MS
LCS Dup (P9E0068-BSD1)Prepared: 05/03/19 Analyzed: 05/06/19
Dibenzo(a,h)anthracene ug/L50.8 20 50.00 2051-134102 7
Dibenzofuran ug/L47.2 20 50.00 2053-11894 5
Diethyl phthalate ug/L51.8 20 50.00 2056-125104 4
Dimethyl phthalate ug/L50.3 20 50.00 2045-127101 3
Di-n-butyl phthalate ug/L51.2 20 50.00 2059-127102 5
Di-n-octyl phthalate ug/L49.6 10 50.00 2051-14099 8
Fluoranthene ug/L50.5 20 50.00 2057-128101 6
Fluorene ug/L51.3 20 50.00 2052-124103 3
Hexachlorobenzene ug/L47.3 20 50.00 2053-12595 5
Hexachlorobutadiene ug/L28.9 20 50.00 2022-12458 4
Hexachlorocyclopentadiene ug/L24.3 20 50.00 2032-11749 0.7
Hexachloroethane ug/L27.7 10 50.00 2021-11555 6
Indeno(1,2,3-cd)pyrene ug/L61.5 10 50.00 2052-134123 14
Isophorone ug/L42.6 10 50.00 2042-12485 2
Naphthalene ug/L34.0 10 50.00 2040-12168 0.6
Nitrobenzene ug/L41.2 10 50.00 2045-12182 2
N-Nitroso-di-n-propylamine ug/L47.0 20 50.00 2049-11994 2
N-Nitrosodiphenylamine ug/L60.2 20 50.00 2051-123120 5
Pentachlorophenol ug/L50.9 50 50.00 2035-138102 0.8
Phenanthrene ug/L50.7 20 50.00 2059-120101 7
Phenol ug/L20.3 10 50.00 2012-5841 0.3
Pyrene ug/L52.0 10 50.00 2057-126104 6
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 103103
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8442.0
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6059.7
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8140.6
ug/L 100.0 11-52Surrogate: Phenol-d5 3938.5
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9849.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0070 - 3546
Blank (P9E0070-BLK1)Prepared & Analyzed: 05/03/19
1,2,4-Trichlorobenzene mg/kg wetBRL0.66
1,2-Dichlorobenzene mg/kg wetBRL0.66
1,3-Dichlorobenzene mg/kg wetBRL0.66
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.66
2,4,5-Trichlorophenol mg/kg wetBRL0.66
2,4,6-Trichlorophenol mg/kg wetBRL0.66
2,4-Dichlorophenol mg/kg wetBRL0.66
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL1.5
2,4-Dinitrotoluene mg/kg wetBRL0.66
2,6-Dinitrotoluene mg/kg wetBRL0.66
2-Chloronaphthalene mg/kg wetBRL0.66
2-Chlorophenol mg/kg wetBRL0.66
2-Methylnaphthalene mg/kg wetBRL0.66
2-Methylphenol mg/kg wetBRL0.66
2-Nitrophenol mg/kg wetBRL0.66
3,3’-Dichlorobenzidine mg/kg wetBRL0.66
3/4-Methylphenol mg/kg wetBRL0.66
4,6-Dinitro-2-methylphenol mg/kg wetBRL1.5
4-Bromophenyl phenyl ether mg/kg wetBRL0.66
4-Chloro-3-methylphenol mg/kg wetBRL0.66
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL1.0
4-Nitrophenol mg/kg wetBRL0.66
Acenaphthene mg/kg wetBRL0.66
Acenaphthylene mg/kg wetBRL0.66
Anthracene mg/kg wetBRL0.66
Azobenzene mg/kg wetBRL0.66
Benzo(a)anthracene mg/kg wetBRL0.66
Benzo(a)pyrene mg/kg wetBRL0.66
Benzo(b)fluoranthene mg/kg wetBRL0.66
Benzo(g,h,i)perylene mg/kg wetBRL0.66
Benzo(k)fluoranthene mg/kg wetBRL0.66
Benzoic Acid mg/kg wetBRL2.0
Benzyl alcohol mg/kg wetBRL0.66
bis(2-Chloroethoxy)methane mg/kg wetBRL0.66
Bis(2-Chloroethyl)ether mg/kg wetBRL0.66
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.66
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.66
Dibenzo(a,h)anthracene mg/kg wetBRL0.66
Dibenzofuran mg/kg wetBRL0.66
Diethyl phthalate mg/kg wetBRL0.66
Dimethyl phthalate mg/kg wetBRL0.66
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0070 - 3546
Blank (P9E0070-BLK1)Prepared & Analyzed: 05/03/19
Di-n-butyl phthalate mg/kg wetBRL0.66
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.66
Fluorene mg/kg wetBRL0.66
Hexachlorobenzene mg/kg wetBRL0.66
Hexachlorobutadiene mg/kg wetBRL0.66
Hexachlorocyclopentadiene mg/kg wetBRL0.66
Hexachloroethane mg/kg wetBRL0.66
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66
Isophorone mg/kg wetBRL0.66
Naphthalene mg/kg wetBRL0.66
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.66
N-Nitrosodiphenylamine mg/kg wetBRL0.66
Pentachlorophenol mg/kg wetBRL1.0
Phenanthrene mg/kg wetBRL0.66
Phenol mg/kg wetBRL0.66
Pyrene mg/kg wetBRL0.66
Pyridine mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 903.00
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 891.49
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 923.06
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 831.38
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 892.98
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 941.57
LCS (P9E0070-BS1)Prepared & Analyzed: 05/03/19
1,2,4-Trichlorobenzene mg/kg wet1.17 0.66 1.667 34-11870
1,2-Dichlorobenzene mg/kg wet1.22 0.66 1.667 33-11773
1,3-Dichlorobenzene mg/kg wet1.18 0.66 1.667 30-11571
1,4-Dichlorobenzene mg/kg wet1.20 0.33 1.667 31-11572
1-Methylnaphthalene mg/kg wet1.29 0.66 1.667 40-11978
2,4,5-Trichlorophenol mg/kg wet1.47 0.66 1.667 62-12488
2,4,6-Trichlorophenol mg/kg wet1.53 0.66 1.667 39-12692
2,4-Dichlorophenol mg/kg wet1.27 0.66 1.667 40-12276
2,4-Dimethylphenol mg/kg wet1.68 0.33 1.667 30-127101
2,4-Dinitrophenol mg/kg wet0.837 1.5 1.667 J27-12950
2,4-Dinitrotoluene mg/kg wet1.50 0.66 1.667 48-12690
2,6-Dinitrotoluene mg/kg wet1.53 0.66 1.667 46-12492
2-Chloronaphthalene mg/kg wet1.45 0.66 1.667 41-11487
2-Chlorophenol mg/kg wet1.45 0.66 1.667 34-12187
2-Methylnaphthalene mg/kg wet1.24 0.66 1.667 38-12275
2-Methylphenol mg/kg wet1.61 0.66 1.667 32-12297
2-Nitrophenol mg/kg wet1.19 0.66 1.667 36-12371
3,3’-Dichlorobenzidine mg/kg wet1.57 0.66 1.667 22-12194
3/4-Methylphenol mg/kg wet1.36 0.66 1.667 34-11982
4,6-Dinitro-2-methylphenol mg/kg wet1.06 1.5 1.667 J29-13263
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0070 - 3546
LCS (P9E0070-BS1)Prepared & Analyzed: 05/03/19
4-Bromophenyl phenyl ether mg/kg wet1.49 0.66 1.667 46-12490
4-Chloro-3-methylphenol mg/kg wet1.34 0.66 1.667 45-12280
4-Chloroaniline mg/kg wet1.29 0.33 1.667 17-10678
4-Chlorophenyl phenyl ether mg/kg wet1.51 1.0 1.667 45-12191
4-Nitrophenol mg/kg wet1.54 0.66 1.667 30-13293
Acenaphthene mg/kg wet1.51 0.66 1.667 40-12391
Acenaphthylene mg/kg wet1.46 0.66 1.667 32-13288
Anthracene mg/kg wet1.61 0.66 1.667 47-12397
Azobenzene mg/kg wet1.51 0.66 1.667 39-12590
Benzo(a)anthracene mg/kg wet1.55 0.66 1.667 49-12693
Benzo(a)pyrene mg/kg wet1.48 0.66 1.667 45-12989
Benzo(b)fluoranthene mg/kg wet1.44 0.66 1.667 45-13286
Benzo(g,h,i)perylene mg/kg wet1.52 0.66 1.667 43-13491
Benzo(k)fluoranthene mg/kg wet1.52 0.66 1.667 47-13291
Benzoic Acid mg/kg wet0.820 2.0 1.667 J10-8349
Benzyl alcohol mg/kg wet1.18 0.66 1.667 29-12271
bis(2-Chloroethoxy)methane mg/kg wet1.26 0.66 1.667 36-12176
Bis(2-Chloroethyl)ether mg/kg wet1.12 0.66 1.667 31-12067
Bis(2-chloroisopropyl)ether mg/kg wet1.31 0.33 1.667 33-13178
Bis(2-Ethylhexyl)phthalate mg/kg wet1.56 0.66 1.667 51-13393
Butyl benzyl phthalate mg/kg wet1.50 0.33 1.667 48-13290
Chrysene mg/kg wet1.52 0.66 1.667 50-12491
Dibenzo(a,h)anthracene mg/kg wet1.51 0.66 1.667 45-13490
Dibenzofuran mg/kg wet1.47 0.66 1.667 44-12088
Diethyl phthalate mg/kg wet1.52 0.66 1.667 50-12491
Dimethyl phthalate mg/kg wet1.50 0.66 1.667 48-12490
Di-n-butyl phthalate mg/kg wet1.51 0.66 1.667 51-12891
Di-n-octyl phthalate mg/kg wet1.47 0.33 1.667 45-14088
Fluoranthene mg/kg wet1.51 0.66 1.667 50-12790
Fluorene mg/kg wet1.58 0.66 1.667 43-12595
Hexachlorobenzene mg/kg wet1.41 0.66 1.667 45-12285
Hexachlorobutadiene mg/kg wet1.24 0.66 1.667 32-12374
Hexachlorocyclopentadiene mg/kg wet1.02 0.66 1.667 32-11761
Hexachloroethane mg/kg wet1.15 0.66 1.667 28-11769
Indeno(1,2,3-cd)pyrene mg/kg wet1.44 0.66 1.667 45-13387
Isophorone mg/kg wet1.23 0.66 1.667 30-12274
Naphthalene mg/kg wet1.21 0.66 1.667 35-12372
Nitrobenzene mg/kg wet1.18 0.33 1.667 34-12271
N-Nitroso-di-n-propylamine mg/kg wet1.34 0.66 1.667 36-12080
N-Nitrosodiphenylamine mg/kg wet1.81 0.66 1.667 38-127109
Pentachlorophenol mg/kg wet1.44 1.0 1.667 25-13386
Phenanthrene mg/kg wet1.56 0.66 1.667 50-12194
Phenol mg/kg wet1.59 0.66 1.667 34-12195
Pyrene mg/kg wet1.55 0.66 1.667 47-12793
Pyridine mg/kg wet0.832 0.33 1.667 10-6050
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 933.10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0070 - 3546
LCS (P9E0070-BS1)Prepared & Analyzed: 05/03/19
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 891.49
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 882.95
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 721.19
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 852.82
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 961.60
LCS Dup (P9E0070-BSD1)Prepared & Analyzed: 05/03/19
1,2,4-Trichlorobenzene mg/kg wet1.00 0.66 1.667 2034-11860 16
1,2-Dichlorobenzene mg/kg wet0.962 0.66 1.667 20 D33-11758 24
1,3-Dichlorobenzene mg/kg wet0.913 0.66 1.667 20 D30-11555 26
1,4-Dichlorobenzene mg/kg wet0.929 0.33 1.667 20 D31-11556 26
1-Methylnaphthalene mg/kg wet1.17 0.66 1.667 2040-11970 10
2,4,5-Trichlorophenol mg/kg wet1.42 0.66 1.667 2062-12485 3
2,4,6-Trichlorophenol mg/kg wet1.40 0.66 1.667 2039-12684 9
2,4-Dichlorophenol mg/kg wet1.18 0.66 1.667 2040-12271 8
2,4-Dimethylphenol mg/kg wet1.52 0.33 1.667 2030-12791 10
2,4-Dinitrophenol mg/kg wet0.805 1.5 1.667 20 J27-12948 4
2,4-Dinitrotoluene mg/kg wet1.43 0.66 1.667 2048-12686 5
2,6-Dinitrotoluene mg/kg wet1.47 0.66 1.667 2046-12488 4
2-Chloronaphthalene mg/kg wet1.33 0.66 1.667 2041-11480 9
2-Chlorophenol mg/kg wet1.20 0.66 1.667 2034-12172 19
2-Methylnaphthalene mg/kg wet1.13 0.66 1.667 2038-12268 9
2-Methylphenol mg/kg wet1.38 0.66 1.667 2032-12283 16
2-Nitrophenol mg/kg wet1.05 0.66 1.667 2036-12363 13
3,3’-Dichlorobenzidine mg/kg wet1.50 0.66 1.667 2022-12190 4
3/4-Methylphenol mg/kg wet1.21 0.66 1.667 2034-11972 12
4,6-Dinitro-2-methylphenol mg/kg wet1.08 1.5 1.667 20 J29-13265 3
4-Bromophenyl phenyl ether mg/kg wet1.41 0.66 1.667 2046-12484 6
4-Chloro-3-methylphenol mg/kg wet1.26 0.66 1.667 2045-12275 6
4-Chloroaniline mg/kg wet1.19 0.33 1.667 2017-10672 8
4-Chlorophenyl phenyl ether mg/kg wet1.45 1.0 1.667 2045-12187 4
4-Nitrophenol mg/kg wet1.56 0.66 1.667 2030-13293 0.9
Acenaphthene mg/kg wet1.42 0.66 1.667 2040-12385 6
Acenaphthylene mg/kg wet1.38 0.66 1.667 2032-13283 6
Anthracene mg/kg wet1.55 0.66 1.667 2047-12393 4
Azobenzene mg/kg wet1.43 0.66 1.667 2039-12586 5
Benzo(a)anthracene mg/kg wet1.46 0.66 1.667 2049-12688 6
Benzo(a)pyrene mg/kg wet1.38 0.66 1.667 2045-12983 7
Benzo(b)fluoranthene mg/kg wet1.39 0.66 1.667 2045-13284 3
Benzo(g,h,i)perylene mg/kg wet1.44 0.66 1.667 2043-13486 6
Benzo(k)fluoranthene mg/kg wet1.44 0.66 1.667 2047-13287 5
Benzoic Acid mg/kg wet0.702 2.0 1.667 20 J10-8342 15
Benzyl alcohol mg/kg wet1.03 0.66 1.667 2029-12262 13
bis(2-Chloroethoxy)methane mg/kg wet1.11 0.66 1.667 2036-12166 13
Bis(2-Chloroethyl)ether mg/kg wet0.923 0.66 1.667 2031-12055 20
Bis(2-chloroisopropyl)ether mg/kg wet1.05 0.33 1.667 20 D33-13163 22
Bis(2-Ethylhexyl)phthalate mg/kg wet1.51 0.66 1.667 2051-13390 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9E0070 - 3546
LCS Dup (P9E0070-BSD1)Prepared & Analyzed: 05/03/19
Butyl benzyl phthalate mg/kg wet1.43 0.33 1.667 2048-13286 4
Chrysene mg/kg wet1.48 0.66 1.667 2050-12489 3
Dibenzo(a,h)anthracene mg/kg wet1.45 0.66 1.667 2045-13487 4
Dibenzofuran mg/kg wet1.41 0.66 1.667 2044-12084 4
Diethyl phthalate mg/kg wet1.47 0.66 1.667 2050-12488 3
Dimethyl phthalate mg/kg wet1.44 0.66 1.667 2048-12487 4
Di-n-butyl phthalate mg/kg wet1.48 0.66 1.667 2051-12889 2
Di-n-octyl phthalate mg/kg wet1.40 0.33 1.667 2045-14084 5
Fluoranthene mg/kg wet1.48 0.66 1.667 2050-12789 1
Fluorene mg/kg wet1.50 0.66 1.667 2043-12590 5
Hexachlorobenzene mg/kg wet1.37 0.66 1.667 2045-12282 3
Hexachlorobutadiene mg/kg wet1.00 0.66 1.667 20 D32-12360 21
Hexachlorocyclopentadiene mg/kg wet0.896 0.66 1.667 2032-11754 13
Hexachloroethane mg/kg wet0.883 0.66 1.667 20 D28-11753 26
Indeno(1,2,3-cd)pyrene mg/kg wet1.43 0.66 1.667 2045-13386 0.9
Isophorone mg/kg wet1.12 0.66 1.667 2030-12267 9
Naphthalene mg/kg wet1.04 0.66 1.667 2035-12362 15
Nitrobenzene mg/kg wet1.00 0.33 1.667 2034-12260 16
N-Nitroso-di-n-propylamine mg/kg wet1.17 0.66 1.667 2036-12070 14
N-Nitrosodiphenylamine mg/kg wet1.74 0.66 1.667 2038-127104 4
Pentachlorophenol mg/kg wet1.51 1.0 1.667 2025-13391 5
Phenanthrene mg/kg wet1.49 0.66 1.667 2050-12189 5
Phenol mg/kg wet1.19 0.66 1.667 20 D34-12172 28
Pyrene mg/kg wet1.48 0.66 1.667 2047-12789 5
Pyridine mg/kg wet0.647 0.33 1.667 20 D10-6039 25
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 913.02
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 801.34
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 692.32
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 611.01
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 722.39
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 851.41
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P9E0044 - MADEP VPH (W)
Blank (P9E0044-BLK1)Prepared: 05/02/19 Analyzed: 05/03/19
C5-C8 Aliphatics ug/LBRL50
C9-C12 Aliphatics ug/LBRL50
C9-C10 Aromatics ug/LBRL50
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)122122
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)120120
LCS (P9E0044-BS1)Prepared: 05/02/19 Analyzed: 05/03/19
C5-C8 Aliphatics ug/L32950 300.0 70-130110
C9-C10 Aromatics ug/L110 50 100.0 70-130110
C9-C12 Aliphatic ug/L34850 300.0 70-130116
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)108108
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)110110
LCS Dup (P9E0044-BSD1)Prepared: 05/02/19 Analyzed: 05/03/19
C5-C8 Aliphatics ug/L30850 300.0 5070-130103 7
C9-C10 Aromatics ug/L10750 100.0 5070-130107 2
C9-C12 Aliphatic ug/L33150 300.0 5070-130110 5
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)107107
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)108108
Batch P9E0069 - MADEP VPH (S)
Blank (P9E0069-BLK1)Prepared & Analyzed: 05/03/19
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11911900
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11611600
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P9E0069 - MADEP VPH (S)
LCS (P9E0069-BS1)Prepared & Analyzed: 05/03/19
C5-C8 Aliphatics mg/kg wet35.2 5.0 32.00 70-130110
C9-C10 Aromatics mg/kg wet11.9 5.0 10.67 70-130112
C9-C12 Aliphatic mg/kg wet39.3 5.0 32.00 70-130123
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11411400
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11411400
LCS Dup (P9E0069-BSD1)Prepared & Analyzed: 05/03/19
C5-C8 Aliphatics mg/kg wet34.0 5.0 32.00 5070-130106 3
C9-C10 Aromatics mg/kg wet11.6 5.0 10.67 5070-130108 3
C9-C12 Aliphatic mg/kg wet37.6 5.0 32.00 5070-130118 4
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11111100
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11111100
Batch P9E0079 - MADEP VPH (W)
Blank (P9E0079-BLK1)Prepared & Analyzed: 05/06/19
C5-C8 Aliphatics ug/LBRL50
C9-C12 Aliphatics ug/LBRL50
C9-C10 Aromatics ug/LBRL50
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)125125
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)123123
LCS (P9E0079-BS1)Prepared & Analyzed: 05/06/19
C5-C8 Aliphatics ug/L29850 300.0 70-13099
C9-C10 Aromatics ug/L110 50 100.0 70-130110
C9-C12 Aliphatic ug/L36550 300.0 70-130122
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)115115
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)113113
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P9E0079 - MADEP VPH (W)
LCS Dup (P9E0079-BSD1)Prepared & Analyzed: 05/06/19
C5-C8 Aliphatics ug/L29650 300.0 5070-13099 0.7
C9-C10 Aromatics ug/L10850 100.0 5070-130108 2
C9-C12 Aliphatic ug/L36850 300.0 5070-130123 0.9
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (PID)114114
ug/L 100.0 70-130Surrogate: 2,5-Dibromotoluene (FID)114114
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P9E0042 - 3546
Blank (P9E0042-BLK1)Prepared: 05/02/19 Analyzed: 05/03/19
C9-C18 Aliphatics mg/kg wetBRL25
C19-C36 Aliphatics mg/kg wetBRL25
C11-C22 Aromatics mg/kg wetBRL25
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 821.64
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 981.95
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 873.48
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1134.51
LCS (P9E0042-BS1)Prepared: 05/02/19 Analyzed: 05/03/19
C9-C18 Aliphatics mg/kg wet50.9 25 60.00 40-14085
C19-C36 Aliphatics mg/kg wet93.8 25 80.00 40-140117
C11-C22 Aromatics mg/kg wet17625 170.0 40-140103
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 921.84
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 961.93
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 923.70
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1134.53
LCS Dup (P9E0042-BSD1)Prepared: 05/02/19 Analyzed: 05/03/19
C9-C18 Aliphatics mg/kg wet56.8 25 60.00 5040-14095 11
C19-C36 Aliphatics mg/kg wet10225 80.00 5040-140127 8
C11-C22 Aromatics mg/kg wet20625 170.0 5040-140121 16
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 901.80
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 1072.13
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 963.85
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 1194.76
Batch P9E0067 - MADEP EPH (W)
Blank (P9E0067-BLK1)Prepared: 05/03/19 Analyzed: 05/07/19
C9-C18 Aliphatics ug/LBRL350
C19-C36 Aliphatics ug/LBRL500
C11-C22 Aromatics ug/LBRL250
ug/L 20.00 40-140Surrogate: 1-Chlorooctadecane 6312.6
ug/L 20.00 40-140Surrogate: o-Terphenyl 8116.3
ug/L 40.00 40-140Surrogate: 2-Fluorobiphenyl 9738.7
ug/L 40.00 40-140Surrogate: 2-Bromonaphthalene 12148.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P9E0067 - MADEP EPH (W)
LCS (P9E0067-BS1)Prepared: 05/03/19 Analyzed: 05/07/19
C9-C18 Aliphatics ug/L274 350 600.0 J40-14046
C19-C36 Aliphatics ug/L651 500 800.0 40-14081
C11-C22 Aromatics ug/L1300250 1700 40-14076
ug/L 20.00 40-140Surrogate: 1-Chlorooctadecane 7414.9
ug/L 20.00 40-140Surrogate: o-Terphenyl 8817.6
ug/L 40.00 40-140Surrogate: 2-Fluorobiphenyl 9738.8
ug/L 40.00 40-140Surrogate: 2-Bromonaphthalene 13152.3
LCS Dup (P9E0067-BSD1)Prepared: 05/03/19 Analyzed: 05/07/19
C9-C18 Aliphatics ug/L266 350 600.0 50 J40-14044 3
C19-C36 Aliphatics ug/L597 500 800.0 5040-14075 9
C11-C22 Aromatics ug/L1370250 1700 5040-14081 5
ug/L 20.00 40-140Surrogate: 1-Chlorooctadecane 6913.8
ug/L 20.00 40-140Surrogate: o-Terphenyl 9118.1
ug/L 40.00 40-140Surrogate: 2-Fluorobiphenyl 10040.2
ug/L 40.00 40-140Surrogate: 2-Bromonaphthalene 13554.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 49
5/14/19
Level II QC Report
409 Rogers View Court Project No: J19050361
Project: Duke Energy (Lee Plant)Mid-Atlantic Associates, Inc. - Raleigh
Raleigh, NC 27610
Attn: Dan Nielsen
Prism Work Order: 9050052
Time Submitted: 5/1/2019 11:55:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P9E0147 - NO PREP
Duplicate (P9E0147-DUP2)Prepared: 05/08/19 Analyzed: 05/09/19 Source: 9050052-04
% Solids % by Weight83.1 0.100 83.5 200.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 49
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P9E00429050052-04 05/02/19 11:4010.33 2g mL
Prep Method: MADEP EPH (W)
Lab Number Batch Date/TimeInitialFinal
P9E00679050052-01 05/03/19 9:209802mL mL
P9E00679050052-02 05/03/19 9:209402mL mL
P9E00679050052-03 05/03/19 9:209302mL mL
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P9E00689050052-01 05/03/19 9:261000 1mL mL
P9E00689050052-02 05/03/19 9:261000 1mL mL
P9E00689050052-03 05/03/19 9:261000 1mL mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P9E00709050052-04 05/03/19 10:5530.02 1g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P9E00989050052-01 05/06/19 11:5110 10mL mL
P9E00989050052-02 05/06/19 11:5110 10mL mL
P9E00989050052-03 05/06/19 11:5110 10mL mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P9E00659050052-04 05/02/19 10:007.67 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P9E00699050052-04 05/03/19 12:1623.29 16g mL
Prep Method: MADEP VPH (W)
Lab Number Batch Date/TimeInitialFinal
P9E00799050052-01 05/06/19 11:4044 44mL mL
P9E00449050052-02 05/03/19 10:0144 44mL mL
P9E00449050052-03 05/03/19 10:0144 44mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 49
Page 48 of 49
Page 49 of 49