WA-29401_48553_CA_CLO_20220531

TANK CLOSURE REPORT
Farm Tank and Residential Tank
3201 Charles Boulevard and Northern Adjoining Property
Greenville, Pitt County, North Carolina
May 23, 2022
Terracon Project No. 72227042

Prepared for:
Ms. Patricia Bowen
Arapahoe, North Carolina

Prepared by:
Terracon Consultants, Inc.
Winterville, North Carolina

Table of Contents
A. SITE INFORMATION ...................................................................................................................... 1
B. EXECUTIVE SUMMARY ................................................................................................................. 2
C. SITE HISTORY AND CHARACTERIZATION ............................................................................. 4
C.1 Site Setting ............................................................................................................................................... 4
C.2 Release Summary ..................................................................................................................................... 4
C.3 Previous Investigations and Tank Information ......................................................................................... 5
C.4 Water Supply Wells .................................................................................................................................. 5
C.5 Surface Water .......................................................................................................................................... 5
C.6 Land Use Information ............................................................................................................................... 6
C.7 Initial Abatement, Assessment Activities and Corrective Actions Summary ............................................. 6
C.8 Site Geology and Hydrogeology ............................................................................................................... 6
D. TANK CLOSURE AND INITIAL RESPONSE AND ................................................................ 7
ABATEMENT ACTION ........................................................................................................................... 7
D.1 UST Closure Preparations/Procedures ......................................................................................................... 7
D.2 Excavation of Contaminated Soil .................................................................................................................. 8
D.3 Sampling Activities ................................................................................................................................... 8
D.3.1 Free Product Evaluation ............................................................................................................................... 9
D.3.2 Soil Sampling Activities................................................................................................................................. 9
D.3.3 Groundwater Sampling Activities ................................................................................................................. 9
D.3.4 Analytical Results ....................................................................................................................................... 10
E. CONCLUSIONS AND RECOMMENDATIONS .............................................................. 10
EXHIBITS
Exhibit 1: Topographic Vicinity Map
Exhibit 2: Site Diagram
Exhibit 3: Tank Location Diagram
Exhibit 4: Soil Sample Location Diagram
Exhibit 5: Groundwater Sample Location Diagram

TABLES
Table 1: UST System Information
Table 2: Summary of Soil Analytical Results
Table 3: Summary of Groundwater Analytical Results

APPENDIX
Appendix A: Supporting Documents
Appendix B: Laboratory Analytical Results and Chain of Custody Forms
Appendix C: Photographs
Tank Closure Report
Farm Tank and Residential Tank
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TANK CLOSURE REPORT
A. SITE INFORMATION
NCDEQ Incident No: Not Currently Assigned
Facility ID: Not Applicable – Unregulated/Unregistered Tanks
Site Name: Farm Tank and Residential Tank
Site Location: 3201 Charles Boulevard and Northern Adjoining Property
Greenville, Pitt County, North Carolina
Latitude: Residential Tank = N 35.57244; Farm Tank = N 35.57256
Longitude: Residential Tank = W -77.35198; Farm Tank = W -77.35218
UST Owner/Operator: Unknown – Potentially Deceased
Current Property Owner: Residential Tank = Sony Huynh & Quynh Chan Phan, 3201 Charles
Boulevard, Greenville, NC 27858
Farm Tank = John Taft and Patricia Bowen, et al, 1607 Beaumont Drive,
Greenville, NC 27858

Current Property
Occupant: The site of the Residential Tank is currently developed with a residence.
The site of the Farm Tank is currently a large undeveloped agricultural field
and wooded lot.

Consultant: Terracon Consultants, Inc. (Contact: Allen McColl)
314 Beacon Drive
Winterville, North Carolina 28590
[phone]

Laboratory: Pace Analytical (NCDEQ No. 5342)
9800 Kincey Avenue
Huntersville, North Carolina 28028
704-875-9092

Release Information: Release Date: Unknown, discovered in May 2018 during sampling for tank
closure for both the Residential Tank and Farm Tank
Estimated Quantity: Unknown
Cause of Release: Underground Storage Tank
Currently Active Tanks: None known.
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Pumps or product lines were not observed to be associated with the Farm Tank during its removal. A short
length (3 feet or less) of copper return and supply lines was observed associated with the Residential tank.
These copper lines were removed during the removal of the Residential Tank.

Groundwater was encountered in each tank basin after the tanks were removed.

Terracon field screened overburden soils removed to facilitate the removal of each tank using a
Photoionization Detector (PID). Field screening did not suggest elevated contamination readings above
0.0 parts per million on the PID meter and no petroleum odors were noted in the overburden soils. After
the tanks were removed and confirmation soil samples were collected, Terracon directed our tank removal
subcontractor to utilize the overburden soils as backfill for each tank pit. No contaminated soil was removed
from the site for disposal.

On April 18, 2018, since groundwater was encountered in each tank basin, Terracon collected eight
confirmation soil samples from the sidewalls of each tank pit (4 from each tank). The four sidewall soil
samples collected from the Residential Tank were designated by Terracon as HT-SW-1, HT-SW-2, HT-
SW-3 and HT-SW-4. The four sidewall soil samples collected from the Farm Tank were designated by
Terracon as FT-SW-1, FT-SW-2, FT-SW-3 and FT-SW-4.

The eight confirmation soil samples were sent to Pace Analytical, Inc. to be analyzed for VOCs using EPA
Method 8260, semi-volatile organic compounds (SVOCs) using EPA Method 8270 and Massachusetts
Department of Environmental Protection (MADEP) Volatile Petroleum Hydrocarbons (VPH) and Extractable
Petroleum Hydrocarbons (EPH).

In one of the sidewall confirmation soil samples collected from the Farm Tank (FT-SW-4), benzo(a)pyrene
was analyzed to be above NCDEQ’s established Residential Maximum Soil Contaminant Concentrations
(MSCCs), but below Industrial/Commercial MSCCs established by the NCDEQ. In addition,
benzo(a)anthracene and benzo(b)fluoranthene in FT-SW-4 were analyzed to be above NCDEQ’s Soil-to-
Water MSCCs, but below the NCDEQ established Residential and Industrial/Commercial MSCCs. Target
contaminants in the other confirmation soil samples collected from the Farm Tank pit were below the
laboratory reporting limits.

Target contaminants in the confirmation soil samples collected from the Residential Tank pit were below
NCDEQ’s established MSCCs or were below the laboratory reporting limits.

Terracon returned to the site on April 25, 2018 with a licensed driller to collect a groundwater sample from
temporary monitoring wells installed in each tank basin. The groundwater sample and temporary well at
the Farm Tank was called FT-GW by Terracon. The groundwater sample and temporary well at the
Residential Tank was called HT-GW by Terracon. After the wells were adequately developed, Terracon
collected a groundwater samples from FT-GW and HT-GW on April 25, 2018. The groundwater samples
were analyzed for VOCs using EPA Method 602, SVOCs using EPA Method 625 and MADEP VPH/EPH
as required by NCDEQ for diesel or heating oil tank groundwater sampling assessments.

The groundwater sample collected from the Residential Tank (HT-GW) was analyzed to contain
naphthalene and MADEP C9-C22 aromatics above NCDEQ’s 2L Groundwater Quality Standards (2L
Standards), but below Gross Contamination Levels (GCLs) established by NCDEQ. The other target
contaminants in HT-GW were analyzed to be below the 2L Standard or below the laboratory reporting limits.
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The target contaminants in the groundwater sample collected from the Farm Tank (FT-GW) were analyzed
to be below the laboratory reporting limits.
C. SITE HISTORY AND CHARACTERIZATION
The purpose of this scope of work was to perform tank closure services for the Farm Tank and Residential
Tank property (the site) that is located at 3201 Charles Boulevard and on the northern adjoining property
in Greenville, Pitt County, North Carolina (Exhibit 1). Terracon completed this report to summarize the
findings of tank closure activities performed at the site on April 18 and April 25, 2018.

This Tank Closure Report was prepared in general accordance with the 15A NCAC 2L .0115 regulations
and the NCDEQ Underground Storage Tank (UST) Section Guidelines for Site Checks, Tank Closure and
Initial Response and Abatement for UST Releases, that were in effect in 2018, under the supervision of Mr.
Carl F. Bonner, PE, a North Carolina registered Professional Engineer (NC Registration No. 16252).

C.1 Site Setting
Site 1, the location of the Residential Tank, is comprised of approximately 2.3 acres that is currently
developed with a residence with a few barns and/or storage buildings. Based on information from the Pitt
County Online Parcel Information System (OPIS) Website, Site 1 is currently Parcel Number 19664.

Site 2, the location of the Farm Tank, is comprised of approximately 58 acres that is currently an
undeveloped large agricultural field with some woodland on the eastern side of the tract. Based on
information from the Pitt County OPIS Website, Site 2 is currently Parcel Number 09010. Site 2 adjoins
Site 1 to the north.

Adjoining properties nearest the former USTs are residential, undeveloped or commercial as depicted in
Exhibit 2.

C.2 Release Summary
On-site Releases
Based on our review of the NCDEQ online Waste Management Site Locator Tool that includes regulatory
database information, prior release incidents have not been reported for either property containing the
tanks. The two properties also do not appear on the UST database.

Off-site Releases
Agrivest Heating Oil Tank, is a reported tank leaking incident (NCDEQ Incident # 47889) that occurred on
the western former residential property across Charles Boulevard.

Based on information from NCDEQ’s online file repository we understand the following about this incident:
a 200-gallon heating oil tank was found behind the former residence during demolition activities; a
confirmation soil sample was analyzed to be below NCDEQ’s Soil-to-Water MSCC; a groundwater sample
indicated contamination above NCDEQ’s 2L Standards; the incident at this facility achieved closure with a
“No Further Action Notice” in August 2021 after a “Notice of Residual Petroleum” for groundwater use
restrictions at this facility were recorded at the Pitt County Register of Deeds Office; the former heating oil
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tank at this facility would be located approximately 300 feet west of the closest point of the site.

Additional reported incidents are not listed on the adjoining properties to the site.

C.3 Previous Investigations and Tank Information
Prior to the current tank closure activities, previous reported environmental investigations do not appear to
have occurred at either site.

As part of a potential property transaction in 2018, Terracon was contracted by the potential buyer of the
property to remove two underground storage tank (USTs) from the two above described properties. Both
the Farm Tank and Residential Tank were approximately 250-gallons each and were removed from the
properties on April 18, 2018. Neither property is listed on the UST database and neither property appears
to be associated with prior incidents. Both tanks appear to be undocumented and/or unregistered tanks.
The Farm Tank was reportedly used for the storage of diesel fuel for fueling tractors working in the fields
around the site area. The Residential Tank was formerly used for heating oil storage. The dates of usage
for either tank is unknown.

Pumps or product lines were not observed to be associated with the Farm Tank during its removal. A short
length (3 feet or less) of copper return and supply lines was observed associated with the Residential tank.
These copper lines were removed during the removal of the Residential Tank.

Please see Table 1 for summary of UST System Information for each of the two tanks.

C.4 Water Supply Wells
Terracon is not aware of receptor surveys that have been performed for the site or in the site area.

Water supply wells are not located on the property containing the Farm Tank.

Water supply wells are not located on the property containing the Residential Tank.

Municipal water is utilized on the site and municipal water is available to properties in the site area.

A receptor survey does not appear to have been conducted for the Agrivest Heating Oil Tank leaking
incident (NCDEQ Incident # 47889) that occurred on the western adjoining property discussed in Section
C.2 of this report.

C.5 Surface Water
Surface water was not observed on the sites. Meeting House Branch is located along the eastern property
line of Site 2. This water body appears to be the closest depicted surface water and is located
approximately 2,000 feet east from both former USTs. Surface waters are depicted on the USGS
Topographic map excerpt presented as Exhibit 1.

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C.6 Land Use Information
Adjoining properties nearest the former USTs are residential, undeveloped or commercial as depicted in
Exhibit 2.

C.7 Initial Abatement, Assessment Activities and Corrective Actions Summary
The initial abatement measures performed at the site on April 18, 2018 included uncovering the tanks,
purging the remaining contents of the USTs and the removal of the two USTs.
Confirmation soil samples and a groundwater sample were collected after the tank was removed. The
sampling data is further discussed in Section D.3 of this report.
C.8 Site Geology and Hydrogeology
The following resources were reviewed to evaluate site-specific geological and hydrogeological
characteristics.
Greenville Southeast Quadrangle, North Carolina, USGS 7.5-minute series topographic map, dated
1998 (Exhibit 1).
Geologic Map of North Carolina, dated 1985.
The Geology of the Carolinas, Carolina Geological Society Fiftieth Anniversary Volume, edited by J.
Wright Horton, Jr., and Victor A. Zullo, The University of Tennessee Press, dated 1991.
Soil Survey of Pitt County, North Carolina, US Department of Agriculture, Natural Resources
Conservation Service, Issued November 1974.

The site is in the Coastal Plain Region. The Coastal Plain is generally a higher, denser area of rich, sandy
soil. The Coastal Plain Region was developed on loose, unconsolidated and flat layers of sediment, caused
by sea level changes and erosion of the mountains. Most parts of the Coastal Plain Region consist of well
to moderately well-drained loamy soils.

The site is underlain by a sequence of marine sediments of the Tertiary age known as the Yorktown and
Duplin Formation, undivided (Tpy). The Yorktown and Duplin Formations consists of sand, clay, gravel and
peat deposited in marine fluvial, eolian and lacustrine environments.

Information obtained from the Soil Survey for Pitt County, depicts soils on the sites with several different
soil types. In the area where the two tanks are located, the soil type is Norfolk sandy loam, 0 to 1 percent
slopes (NrA). NrA soil types are well-drained soils on broad, smooth divides in the uplands; infiltration is
moderate; runoff is slow; and the seasonal high-water table is around 5 feet below land surface.

In the site area, groundwater generally is obtained from the Black Creek Aquifer. The Black Creek Aquifer
is lagoonal to marine consisting of thinly laminated clay interlayered with sand. Sediments in the subsurface
are highly organic and sediments are typically from the Black Creek and Middendorf formations. On
average, the Black Creek aquifer consists of nearly 60 percent sand. The hydraulic conductivity ranges
from 15 to 50 feet/day and averages 28 feet/day. Recharge occurs mainly by the downward percolation
from the overlying aquifers. Discharge is typically into streams where there are channels cut into it or its
overlying confining unit.
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In Greenville, NC, the potable water supply is mainly provided by Greenville Utilities Commission (GUC).
GUC utilizes water from the Tar River and three deep wells for the municipal water supply to the site area.

The depth to the water table is not consistent and is dependent upon several factors that include the amount
of rainfall, permeability of the soil, and the influences of groundwater pumping. Groundwater typically flows
in directions parallel to the ground surface and under the influence of gravity, migrates to discharge points
such as surface water features, the toes of slopes or natural springs.

Fluctuations in the depth of the water table can be expected depending on variations in precipitation,
surface water run-off and other factors. Normally, the highest levels of the water table occur in late winter
and spring and the lowest levels occur in the late summer and fall. Groundwater was encountered in each
tank pit after the tanks were removed on April 18, 2018. On April 25, 2018 when the temporary wells were
installed in each tank pit, groundwater was encountered at approximately 3.5 feet below land surface.

D. TANK CLOSURE AND INITIAL RESPONSE AND
ABATEMENT ACTION
Terracon was initially contracted by a prospective buyer of the two sites in 2018 to perform the tank closure
activities. Terracon contracted with Environmental Hydrogeological Consultants, Inc. (EHC, Inc.) to perform
the tank pumping and cleaning, tank removals and temporary monitoring well installations that occurred in
April 2018. In early May 2018, the prospective buyer reportedly backed out of the purchase of the properties
and requested that Terracon not move forward with completing the tank closure report and indicated that
they would not pay Terracon to complete the tank closure report.
In May 2022, Terracon was contacted by one of the current property owners where the Farm Tank was
located to complete the tank closure report. This same property owner formerly owned the site where the
Residential Tank was located. Sometime between May 2018 and currently, the property where the
Residential Tank was located was purchased by another entity.
Please see the following sections for additional discussions about tank closure and confirmation sampling
activities. Photo-documentation of site activities is provided in Appendix C.
D.1 UST Closure Preparations/Procedures
Prior to UST closure services, the City of Greenville Fire Inspections Department was contacted, and a tank
removal permit was obtained from this agency. A representative of the City of Greenville Fire Inspections
Department was onsite to observe the tank removal activities.
Terracon and EHC, Inc. personnel initially mobilized to the site on April 18, 2018 to perform the tank closure
activities.
Terracon produced a Health and Safety Plan (HASP) prior to beginning tank closure services. The HASP
was discussed with EHC, Inc. personnel prior to beginning site work.
Approximately 250 gallons total of residual liquids were removed from the two tanks on April 18, 2018 just
prior to the two tanks being removed. The residual fluid was transported by EHC, Inc. to their facility in Red
Springs, NC for holding prior to disposal. The non-hazardous waste disposal manifests for the fluids is
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included in Appendix A of this report.

Overburden soils were removed from on top of and beside the two UST to facilitate removal of the tanks.
Once uncovered, it was discovered that each tank was approximately 250 gallons in capacity. The Farm
Tank was utilized for the storage of fuel to fuel tractors working in the fields around the site. The Residential
tank was utilized for the storage of heating oil to fuel heaters at the residence. Each tank was buried
approximately 1 foot below land surface.
During the removal of the overburden soils for the tanks, no petroleum odors were noted. Terracon also
field screened the overburden soils with a MiniREA 3000 photo-ionization detector (PID). The field
screening did not indicate PID readings above 0.0 parts per million (ppm) in the overburden soils. Based
upon the lack of discernable odor and measurable PID detections, the excavated soil was deemed
uncontaminated and suitable for reuse as backfill. The soil was stockpiled onsite beside each tank basin
and later reused to backfill a portion of the tank pit after the tanks were removed.
During the excavation of the overburden soils or after each tank was removed, groundwater was
encountered at approximately 4 feet below land surface in each tank pit.
The USTs were hauled offsite for disposal at a permitted facility. A copy of the tank disposal documentation
provided by EHC, Inc. is included in Appendix A.
A short length (3 feet or less) of copper dual supply/return lines extended from the Residential Tank to the back
of the residence at the site.

A dispenser pump or product lines were not found to be associated with the Farm Tank. Potentially, the former
dispenser pump for the Farm Tank was situated on top of this formerly buried tank.

After the tanks were removed, each tank pit was backfilled with overburden and offsite soil on April 18, 2018.

Please see the attached Exhibits 2 and 3 for diagrams indicating the former tank locations, the onsite
building location, property boundaries and adjacent property identifications.
D.2 Excavation of Contaminated Soil
At the issuance of this report, no contaminated soil has been removed from the site for offsite disposal.
D.3 Sampling Activities
On April 18, 2018, since groundwater was encountered in each tank basin, Terracon collected eight
confirmation soil samples from the sidewalls of the tank pits (4 at each tank). The four sidewall soil samples
collected from the Residential Tank were designated by Terracon as HT-SW-1, HT-SW-2, HT-SW-3 and
HT-SW-4. The four sidewall soil samples collected from the Farm Tank were designated by Terracon as
FT-SW-1, FT-SW-2, FT-SW-3 and FT-SW-4. Soil sample locations are provided in Exhibit 4. The soil
sampling is further discussed in Sections D.3.2 and D.3.4 of this report.

Terracon returned to the site on April 25, 2018 with a licensed driller to collect a groundwater sample from
temporary monitoring wells installed in each tank basin. The groundwater sample and temporary well at
the Farm Tank was called FT-GW by Terracon. The groundwater sample and temporary well at the
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Residential Tank was called HT-GW by Terracon. After the wells were adequately developed, Terracon
collected a groundwater samples from FT-GW and HT-GW on April 25, 2018. Groundwater sample
locations are provided in Exhibit 5. The groundwater sampling is further discussed in Section D.3.1 and
D.3.4 of this report.

D.3.1 Free Product Evaluation
Free product was not observed entering the pit during the tank removal activities nor was free product noted
in the temporary monitoring wells installed for the tank closure activities.

D.3.2 Soil Sampling Activities
Due to groundwater being encountered in the excavation, only sidewall samples were collected from the
tank pits. The confirmation soil samples from the sidewalls were collected at approximately 2.5 feet to 3
feet bls.
The confirmation soil samples from each tank pit were collected by a gloved hand from the bucket of a track
hoe used to remove the tanks. Gloves were changed prior to each sample collection point.
The soil samples were packaged and placed in a cooler for delivery to Pace Analytical Services, Inc. (Pace)
in Huntersville, North Carolina for analysis. The eight confirmation soil samples were sent to Pace
Analytical, Inc. to be analyzed for VOCs using EPA Method 8260, SVOCs using EPA Method 8270 and
MADEP VPH and EPH. The approximate locations of the soil samples are shown in Exhibit 4.
D.3.3 Groundwater Sampling Activities
Due to groundwater being encountered in each tank pit, Terracon mobilized back to the site on April 25,
2018 with a North Carolina Licensed Drilling Firm, EHC, Inc. to supervise the installation of one temporary
groundwater monitoring well in each tank pit (two total temporary wells). A Geoprobe unit was used to
install the temporary monitoring well in each former tank pit.

The temporary monitoring well and the groundwater sample collected at the Farm Tank pit was referred to
by Terracon as “FT-GW.” The temporary monitoring well and the groundwater sample collected at the
Residential Tank pit was referred to by Terracon as “HT-GW.” During the drilling for the advancement of
both temporary monitoring wells, groundwater was encountered at approximately 3.5 feet below land
surface in each well. Temporary well casing and riser piping for FT-GW was subsequently installed to a
depth of approximately 12 feet below land surface and included 10 feet of 1-inch diameter 0.010-inch
machine slotted PVC well screen with 2 feet of PVC riser to the surface. Temporary well casing and riser
piping for HT-GW was subsequently installed to a depth of approximately 16 feet below land surface and
included 15 feet of 1-inch diameter 0.010-inch machine slotted PVC well screen with 1 foot of PVC riser to
the surface.

Following well installations, FT-GW and HT-GW were developed by pumping using a low flow peristaltic
pump until the purge water was substantially free of suspended sediment. Following development of the
two wells, a groundwater sample was collected from each well. The groundwater samples were placed in
laboratory provided containers and delivered to Pace Analytical Services, Inc., in Huntersville, North
Carolina for analysis of VOCs using EPA Method 602, SVOCs using EPA Method 625 and MADEP
VPH/EPH as required by NCDEQ for diesel or heating oil tank groundwater sampling assessments.
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The approximate locations of the temporary wells are shown on Exhibit 5.

Boring logs for each temporary well are included in Appendix A.

D.3.4 Analytical Results
Soil Analytical Results

In one of the sidewall confirmation soil samples collected from the Farm Tank (FT-SW-4), benzo(a)pyrene
(at 1.76 mg/kg) was analyzed to be above NCDEQ’s established Residential Maximum Soil Contamination
Concentrations (MSCCs) (of 0.66 mg/kg), but below Industrial/Commercial MSCCs (3.2 mg/kg) established
by the NCDEQ. In addition, benzo(a)anthracene (at 1.27 mg/kg) and benzo(b)fluoranthene (1.67 mg/kg)
in FT-SW-4 were analyzed to be above NCDEQ’s Soil-to-Water MSCCs (0.17 mg/kg and 0.6 mg/kg
respectively), but below the NCDEQ established Residential (6.6 mg/kg for both constituents) and
Industrial/Commercial MSCCs (32 mg/kg for both of constituents).

Target contaminants in the other confirmation soil samples collected from the Farm Tank pit were below
the laboratory reporting limits.

Target contaminants in the confirmation soil samples collected from the Residential Tank pit were below
NCDEQ’s established MSCCs or were below the laboratory reporting limits.

The soil analytical results are summarized in Table 2 and the laboratory analytical reports are provided in
Appendix B.

Groundwater Analytical Results

The groundwater sample collected from the Residential Tank (HT-GW) was analyzed to contain
naphthalene (at 8.6 µg/l (VOCs) and 7.6 µg/l (SVOCs)) and MADEP C9-C22 aromatics (at 409.6 µg/l)
above NCDEQ’s 2L Groundwater Quality Standards (2L Standards), but below Gross Contamination Levels
(GCLs) established by NCDEQ. The established 2L Standard for naphthalene is 6 µg/l and for C9-C22
aromatics is 200 µg/l. The other target contaminants in HT-GW were analyzed to be below the 2L Standard
or below the laboratory reporting limits.

The groundwater sample collected from the Farm Tank (FT-GW) was below the laboratory reporting limits for
all analytes.

The groundwater analytical results are summarized in Table 3 and the laboratory analytical report is
provided in Appendix B.
E. CONCLUSIONS AND RECOMMENDATIONS
Based on information obtained during the completion of the Tank Closure activities performed in April 2018,
Terracon provides the following findings:

One 250-gallon residential heating oil tank (Residential Tank) and one 250-gallon diesel tank (Farm
Tank) were removed at two adjoining properties on April 18, 2018.
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Groundwater was encountered in each tank basin during tank removal activities.
Four sidewall confirmation soil samples (eight total) were collected at each tank pit on April 18, 2018.
In one of the sidewall confirmation soil samples collected from the Farm Tank (FT-SW-4),
benzo(a)pyrene was analyzed to be above NCDEQ’s established Residential MSCCs, but below
Industrial/Commercial MSCCs established by the NCDEQ. In addition, benzo(a)anthracene and
benzo(b)fluoranthene in FT-SW-4 were analyzed to be above NCDEQ’s Soil-to-Water MSCCs, but
below the NCDEQ established Residential and Industrial/Commercial MSCCs.
Target contaminants in the other confirmation soil samples collected from the Farm Tank pit were below
the laboratory reporting limits.
Target contaminants in the confirmation soil samples collected from the Residential Tank pit were below
NCDEQ’s established MSCCs or were below the laboratory reporting limits.
Due to groundwater being encountered in the tank pits during tank removal activities, a groundwater
sample was collected at each tank pit through temporary monitoring wells installed by a North Carolina
licensed driller.
The groundwater sample collected from the Residential Tank (HT-GW) was analyzed to contain
naphthalene and MADEP C9-C22 aromatics above NCDEQ’s 2L Standards, but below GCLs
established by NCDEQ. The other target contaminants in HT-GW were analyzed to be below the 2L
Standard or below the laboratory reporting limits.
The groundwater sample collected from the Farm Tank (FT-GW) was analyzed to be below the
laboratory reporting limits.
Analytical results indicate a release to soils at the farm tank with no impacts to ground water.
Based on detections in groundwater above the 2L standards and no soil impacts above the laboratory
detection limits in the residential tank, a release appears to have occurred from the bottom of the tank.
Water supply wells are not located on the property containing the Farm Tank.
Water supply wells are not located on the property containing the Residential Tank.
The site is situated in the city limits of Greenville, NC where municipal water is available and utilized for
drinking water purposes.
Since water supply wells are not located on either tract where the Farm Tank or Residential Tank were located
and based on the results of closure activities described herein, Terracon recommends that the incident be
closed out with the recording of “Notice of Residual Petroleum” at both properties. Land use restrictions should
be considered for the property formerly containing the Farm Tank. Groundwater use restrictions should be
considered for the property formerly containing the Residential Tank.

EXHIBITS
SITE 17.5 MINUTE SERIES (TOPOGRAPHIC)Drawn By:Checked By:Approved By:Project Mngr:File No.Date:Scale:Project No.Consulting Engineers and ScientistsEXHIBITTOPOGRAPHIC VICINITY MAP1TANK CLOSURE REPORTFARM TANK AND RESIDENTIAL TANK3201 CHARLES BOULEVARDGREENVILLE, NCKAMRLWKAM/MRFKAM72227042AS SHOWN72227042-1MAY 2022314 Beacon DriveWinterville, NC 28590(252) 353-1600(252) 353-0002*INDICATES WHICH MAP SITE IS LOCATED ONSITE 2
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSESLEGENDSITEDrawn By:Checked By:Approved By:Project Mngr:File No.Date:Scale:Project No.Consulting Engineers and ScientistsEXHIBITSITE DIAGRAM2TANK CLOSURE REPORTFARM TANK AND RESIDENTIAL TANK3201 CHARLES BOULEVARDGREENVILLE, NCKAMRLWKAM/MRFKAM72227042AS SHOWN72227042-2MAY 2022314 Beacon DriveWinterville, NC 28590(252) 353-1600(252) 353-0002RRESIDENCEUSTUNDERGROUND STORAGE TANKREAST F
IRE
TOWER
ROADSMYTHEWYCK DRIVE TURNBURY DRIVESOUTH CHARLES BOULEVARDEXCHANGE DR
IVE
TARA COURTFOODLION, A.J.MCMURPHY'S, BAMBOOGARDEN, KIDS-GO-ROUND,TIMELESS TREASURESSELECT BANK& TRUSTGRACECHURCHWOODLANDFIELDTHE LANDINGAPARTMENTSRESIDENTIALPITT COUNTYFARM BUREAURE/MAXPREFERREDREALTYEAST CAROLINACARPETS & INTERIORSCAROLINA EASTFAMILY MEDICINESDS RESTAURANT GROUP(PIZZA
HUT MANAGEMENT)STORAGEBUILDINGSDILAPIDATEDBARNUSTApproximate Scale0(Feet)300USTPECANTREESSITE 1SITE 2FORMER RESIDENCE(CURRENTLY UNDEVELOPED)
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSESLEGENDSITEDrawn By:Checked By:Approved By:Project Mngr:File No.Date:Scale:Project No.Consulting Engineers and ScientistsEXHIBITTANK LOCATION DIAGRAM3TANK CLOSURE REPORTFARM TANK AND RESIDENTIAL TANK3201 CHARLES BOULEVARDGREENVILLE, NCKAMRLWKAM/MRFKAM72227042AS SHOWN72227042-3MAY 2022314 Beacon DriveWinterville, NC 28590(252) 353-1600(252) 353-0002RESIDENCERRSOUTH CHARLES BOULEVARDDILAPIDATEDBARNApproximate Scale0(Feet)60PECANTREESDIRT
DR
IVE
DI
R
T

D
R
I
V
E
FORMER FARMTANKSTORAGE SHEDSSSFORMERRESIDENTIAL TANKFIELDSITE 2SITE 1
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSESLEGENDSITEDrawn By:Checked By:Approved By:Project Mngr:File No.Date:Scale:Project No.Consulting Engineers and ScientistsEXHIBITSOIL SAMPLE LOCATION DIAGRAM4TANK CLOSURE REPORTFARM TANK AND RESIDENTIAL TANK3201 CHARLES BOULEVARDGREENVILLE, NCKAMRLWKAM/MRFKAM72227042AS SHOWN72227042-4MAY 2022314 Beacon DriveWinterville, NC 28590(252) 353-1600(252) 353-0002RESIDENCERRSOUTH CHARLES BOULEVARDDILAPIDATEDBARNApproximate Scale0(Feet)60PECANTREESDIRT
DR
IVE
DI
R
T

D
R
I
V
E
FORMER FARMTANKSTORAGE SHEDSSSFORMERRESIDENTIAL TANKFIELDSITE 2SITE 1SOIL SAMPLE LOCATIONFT-SW-2FT-SW-3FT-SW-4FT-SW-1HT-SW-4HT-SW-1HT-SW-2HT-SW-3
THIS DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSESLEGENDSITEDrawn By:Checked By:Approved By:Project Mngr:File No.Date:Scale:Project No.Consulting Engineers and ScientistsEXHIBITGROUNDWATER SAMPLE LOCATION DIAGRAM5TANK CLOSURE REPORTFARM TANK AND RESIDENTIAL TANK3201 CHARLES BOULEVARDGREENVILLE, NCKAMRLWKAM/MRFKAM72227042AS SHOWN72227042-5MAY 2022314 Beacon DriveWinterville, NC 28590(252) 353-1600(252) 353-0002RESIDENCERRSOUTH CHARLES BOULEVARDDILAPIDATEDBARNApproximate Scale0(Feet)60PECANTREESDIRT
DR
IVE
DI
R
T

D
R
I
V
E
FORMER FARMTANKSTORAGE SHEDSSSFORMERRESIDENTIAL TANKFIELDSITE 2SITE 1TEMPORARY WELL
/ GROUNDWATER SAMPLE
LOCATIONHT-GWFT-GW

TABLES

Table 1
UST System Information
Farm Tank and Residential Tank
3201 Charles Boulevard and Northern Adjoining Property
Greenville, Pitt County, NC
Terracon Project No. 72227042

Page 1 of 1

There are currently no dispenser pumps located on either property. Remnant dispenser pump islands or dispenser pump pedestals were not observed on either
property.

UST ID Number

Current/Last
Contents

Previous
Contents

Capacity (in
gallons)

Construction
Details **

Tank
Dimensions
Description of
Associated
Piping and
Pumps

Date Tank
Installed

Status of
UST

Was release
associated with
the UST
System?
Tank 1
(Residential Tank) Heating Oil Heating Oil 250 Steel
36 inches
diameter x 64
inches long
A short length
of copper lines
from the tank to
the residence
(removed)
Unknown Removed
4/18/2018 Yes
Tank 2
(Farm Tank) Diesel Fuel Diesel Fuel 250 Steel
36 inches
diameter x 64
inches long
None found Unknown Removed
4/18/2018 Yes
Table 2
Summary of Confirmation Soil Analytical Results
Farm Tank and Residential Tank
3201 Charles Boulevard and Northern Adjoining Property
Greenville, Pitt County, NC
Terracon Project No. 72227042

Page 1 of 1

Analytical Method 8260 8270 MADEP VPH/EPH
Contaminant of Concern -> Acetone Benzene Ethylbenzene Naphthalene Toluene Xylene (Total) Acenaphthylene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chyrsene Fluoranthene Indeno(1,2,3-cd)pyrene Naphthalene Pyrene Aromatic (C9-C22) Aliphatic (C19-C36) Aliphatic (C5-C8) Aliphatic (C9-C18) Soil
Sample ID
Date
Collected
Depth
(in Feet)
Below
Land
Surface
HT-SW-1 4/18/2018 2.5 - 3 <0.0794 <0.004 <0.004 <0.004 <0.004 <0.0079 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <14 <11.6 <2.4 <14
HT-SW-2 4/18/2018 2.5 - 3 0.162 <0.0043 <0.0043 <0.0043 <0.0043 <0.0086 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <0.384 <13.8 <11.6 <2.2 <13.8
HT-SW-3 4/18/2018 2.5 - 3 <0.0902 <0.0045 <0.0045 <0.0045 <0.0045 <0.009 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <0.391 <14.1 <11.8 <2.3 <14.1
HT-SW-4 4/18/2018 2.5 - 3 <0.0825 <0.0043 <0.0043 <0.0043 <0.0043 <0.0085 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <0.390 <14 <11.7 <2.3 <14
FT-SW-1 4/18/2018 2.5 - 3 <0.102 <0.0051 <0.0051 <0.0051 <0.0051 <0.0102 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <14.8 <12.1 <2.7 <14.8
FT-SW-2 4/18/2018 2.5 - 3 <0.112 <0.0056 <0.0056 <0.0056 <0.0056 <0.0112 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <15.3 <12.8 <3 <15.3
FT-SW-3 4/18/2018 2.5 - 3 <0.105 <0.0053 <0.0053 <0.0053 <0.0053 <0.00105 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <0.39 <14.2 <11.6 <2.6 <14.2
FT-SW-4 4/18/2018 2.5 - 3 <0.101 <0.005 <0.005 <0.005 <0.005 <0.0101 1.58 1.27 1.76 1.67 1.37 0.708 1.35 1.51 1.04 <0.383 3.6 <13.9 <11.6 <2.3 <13.9
Soil to Water MSCCs (mg/kg) 24 0.0072 8 0.2 5.4 6 20 0.17 0.058 0.6 7,600 5.8 18 330 1.9 0.2 210 31 NE 68 540
Residential MSCCs (mg/kg) 14,000 12 60.3 5.5 1,250 3,120 930 6.6 0.66 6.6 469 66 663 625 6.63 5.5 469 469 31,000 939 1,500
Industrial/Commercial MSCCs
(mg/kg) 210,000 59.4 297 27 18,600 46,700 14,000 32 3.2 32 7,000 327 3,270 9,340 32.7 27 7,000 12,264 810,000 24,528 40,000

Confirmation soil samples HT-SW-1 through HT-SW-4 were collected from the sidewalls of the Residential Heating Oil Tank above the water table after this tank was removed. Confirmation soil samples FT-SW-1 through FT-SW-4 were collected from the sidewalls of the
Farm Tank above the water table after this tank was removed. Due to groundwater being encountered in the tank pits after each tank was removed, a floor soil sample was not collected from either tank basin.

Former dispenser pumps or distinctive former dispenser pump areas were not observed on the site.

Constituents in the table in red are above Residential MSCCs, if applicable. Constituents in blue are above Industrial/Commercial MSCCs, if applicable. Quantities are reported in mg/kg (parts per million).

The ”<” sign is used proceeding a number in the lab data in this table when a constituent is below the laboratory reporting limits. < = non-detect.

NE = Not Established (a corresponding reportable limit has not been established by NCDEQ for this constituent); Multiple constituents analyzed below the laboratory’s reportable limits are not listed in the above table.

See Exhibit 4 for locations of these soil samples.

Table 3
Summary of Groundwater Analytical Results
Farm Tank and Residential Tank
3201 Charles Boulevard and Northern Adjoining Property
Greenville, Pitt County, NC
Terracon Project No. 72227042

Page 1 of 1

Analytical Method 602 625 MADEP
Contaminant of Concern -> Benzene Diisopropyl ether Ethylbenzene Isopropylbenzene (cumene) MTBE Naphthalene Toluene Xylene (Total) Benzo(a)pyrene Benzo(b)fluoranthene Naphthalene C5 – C8 Aliphatics C9 – C18 Aliphatics C19 – C36 Aliphatics C9 – C22 Aromatics Sample ID Date
Collected
HT-GW 4/25/2018 <1 <1 1.1 <1 <1 8.6 <1 6 <4.9 <4.9 7.9 <50 107 <98 409.6
FT-GW 4/25/2018 <1 <1 <1 <1 <1 <2 <1 <1 <4.9 <4.9 <4.9 <50 <98 <98 <50
NC 2L Groundwater Quality
Standards (µg/l) 1 70 600 70 20 6 600 500 6 400 700 10,000 200
Gross Contamination Levels
for Groundwater (µg/l) 5,000 70,000 80,000 30,500 20,000 6,000 260,000 50,00 6,000 NE NE NE NE

Shaded constituents are above NCDEQs 2L Groundwater Quality Standards (if applicable); Concentrations are reported in µg/l (parts per billion); Constituents in the table in red are above Gross Contamination Levels for Groundwater (if applicable);
Multiple constituents analyzed below the laboratory’s reporting limits in the groundwater samples are not listed in the above table. NE = Not Established, an applicable 2L Standard or GCL has not be established by NCDEQ.
The ”<” sign is used proceeding a number in the lab data in this table when a constituent is below the laboratory reporting limits. < = non-detect.
HT = Residential Heating Oil Tank
FT = Farm Tank
The groundwater samples were collected from temporary monitoring wells installed in each tank pit after the tanks were removed and the tank pits were backfilled.
See Exhibit 5 for locations of these groundwater samples.

APPENDIX A
Supporting Documents

SILTY SAND (SM), with clay, tannish gray and black
SANDY LEAN CLAY (CL), light gray, orange and black
CLAYEY SAND (SC), light gray and orange
LEAN CLAY WITH SAND (CL), light gray and orange
CLAYEY SAND (SC), light gray and orange
Boring Terminated at 12 Feet
2.0
6.0
8.0
10.0
12.0
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL 72227042 FARM TANK GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 5/17/22DEPTH (Ft.)5
10 WATER LEVELOBSERVATIONSLOCATION
Latitude: 35.5726° Longitude: -77.3522°GRAPHIC LOGDEPTH
Beside 3201 Charles Blvd.
Greenville, NC
SITE:
Page 1 of 1
Advancement Method:Geoprobe
Abandonment Method:Temporary monitoring well installed
Notes:
Project No.: 72227042
Drill Rig:
Boring Started: 04-25-2018
BORING LOG NO. FT-GW
Ms. Patricia BowenCLIENT:
Driller: EHC, Inc.
Boring Completed: 04-25-2018
PROJECT: Farm Tank
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE
CLAYEY SAND (SC), gray and red
SILTY SAND (SM), with clay, tannish gray and black
CLAYEY SAND (SC), light gray, dark gray and orange
LEAN CLAY WITH SAND (CL), light gray and orange
SANDY LEAN CLAY (CL), light gray and orange
CLAYEY SAND (SC), light gray and orange
SILTY SAND (SM), light gray
Boring Terminated at 16 Feet
4.0
6.0
8.0
10.0
12.0
14.0
16.0
Stratification lines are approximate. In-situ, the transition may be gradual.THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. GEO SMART LOG-NO WELL 72227042 RESIDENTAL TANK GINT LOGS.GPJ TERRACON_DATATEMPLATE.GDT 5/17/22DEPTH (Ft.)5
10
15 WATER LEVELOBSERVATIONSLOCATION
Latitude: 35.5724° Longitude: -77.3520°GRAPHIC LOGDEPTH
3201 Charles Blvd.
Greenville, NC
SITE:
Page 1 of 1
Advancement Method:Geoprobe
Abandonment Method:Temporary monitoring well installed
Notes:
Project No.: 72227042
Drill Rig:
Boring Started: 04-25-2018
BORING LOG NO. HT-GW
Ms. Patricia BowenCLIENT:
Driller: EHC, Inc.
Boring Completed: 04-25-2018
PROJECT: Residental Tank
314 Beacon DrWinterville, NC
Groundwater
WATER LEVEL OBSERVATIONS SAMPLE TYPE

APPENDIX B
Laboratory Analytical Results and Chain of Custody Forms

#=CL#
May 02, 2018
LIMS USE: FR - ALLEN MCCOLL
LIMS OBJECT ID: 92381713
92381713
Project:
Pace Project No.:
RE:
Mr. Allen McColl
Terracon
314 Beacon Drive
Winterville, NC 28590
3201 Charles
Dear Mr. McColl:
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 59
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92381713
3201 Charles
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 59
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92381713
3201 Charles
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92381713001 FT-SW-1 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713002 FT-SW-2 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713003 FT-SW-3 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713004 FT-SW-4 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713005 HT-SW-1 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713006 HT-SW-2 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713007 HT-SW-3 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92381713008 HT-SW-4 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 59
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92381713
3201 Charles
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-1 Lab ID:92381713001 Collected:04/18/18 02:29 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/26/18 10:49 N204/24/18 08:0012.1 1
Aliphatic (C19-C36)ND mg/kg 04/26/18 10:49 N204/24/18 08:0012.1 1
Aromatic (C11-C22)ND mg/kg 04/26/18 10:49 N204/24/18 08:0012.1 1
Surrogates
Nonatriacontane (S)68 %04/26/18 10:49 7194-86-704/24/18 08:0040-140 1
o-Terphenyl (S)74 %04/26/18 10:49 84-15-104/24/18 08:0040-140 1
2-Fluorobiphenyl (S)63 %04/26/18 10:49 321-60-804/24/18 08:0040-140 1
2-Bromonaphthalene (S)68 %04/26/18 10:49 580-13-204/24/18 08:0040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 17:32 N204/23/18 11:542.7 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 17:32 N204/23/18 11:542.7 1
Aromatic (C09-C10)ND mg/kg 04/23/18 17:32 N204/23/18 11:542.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)112 %04/23/18 17:32 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)110 %04/23/18 17:32 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/25/18 16:09 83-32-904/21/18 14:304001
Acenaphthylene ND ug/kg 04/25/18 16:09 208-96-804/21/18 14:304001
Aniline ND ug/kg 04/25/18 16:09 62-53-304/21/18 14:304001
Anthracene ND ug/kg 04/25/18 16:09 120-12-704/21/18 14:304001
Benzo(a)anthracene ND ug/kg 04/25/18 16:09 56-55-304/21/18 14:304001
Benzo(a)pyrene ND ug/kg 04/25/18 16:09 50-32-804/21/18 14:304001
Benzo(b)fluoranthene ND ug/kg 04/25/18 16:09 205-99-204/21/18 14:304001
Benzo(g,h,i)perylene ND ug/kg 04/25/18 16:09 191-24-204/21/18 14:304001
Benzo(k)fluoranthene ND ug/kg 04/25/18 16:09 207-08-904/21/18 14:304001
Benzoic Acid ND ug/kg 04/25/18 16:09 65-85-004/21/18 14:3020001
Benzyl alcohol ND ug/kg 04/25/18 16:09 100-51-604/21/18 14:308011
4-Bromophenylphenyl ether ND ug/kg 04/25/18 16:09 101-55-304/21/18 14:304001
Butylbenzylphthalate ND ug/kg 04/25/18 16:09 85-68-704/21/18 14:304001
4-Chloro-3-methylphenol ND ug/kg 04/25/18 16:09 59-50-704/21/18 14:308011
4-Chloroaniline ND ug/kg 04/25/18 16:09 106-47-804/21/18 14:3020001
bis(2-Chloroethoxy)methane ND ug/kg 04/25/18 16:09 111-91-104/21/18 14:304001
bis(2-Chloroethyl) ether ND ug/kg 04/25/18 16:09 111-44-404/21/18 14:304001
2-Chloronaphthalene ND ug/kg 04/25/18 16:09 91-58-704/21/18 14:304001
2-Chlorophenol ND ug/kg 04/25/18 16:09 95-57-804/21/18 14:304001
4-Chlorophenylphenyl ether ND ug/kg 04/25/18 16:09 7005-72-304/21/18 14:304001
Chrysene ND ug/kg 04/25/18 16:09 218-01-904/21/18 14:304001
Dibenz(a,h)anthracene ND ug/kg 04/25/18 16:09 53-70-304/21/18 14:304001
Dibenzofuran ND ug/kg 04/25/18 16:09 132-64-904/21/18 14:304001
1,2-Dichlorobenzene ND ug/kg 04/25/18 16:09 95-50-104/21/18 14:304001
1,3-Dichlorobenzene ND ug/kg 04/25/18 16:09 541-73-104/21/18 14:304001
1,4-Dichlorobenzene ND ug/kg 04/25/18 16:09 106-46-704/21/18 14:304001
3,3'-Dichlorobenzidine ND ug/kg 04/25/18 16:09 91-94-104/21/18 14:3020001
2,4-Dichlorophenol ND ug/kg 04/25/18 16:09 120-83-204/21/18 14:304001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-1 Lab ID:92381713001 Collected:04/18/18 02:29 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/25/18 16:09 84-66-204/21/18 14:304001
2,4-Dimethylphenol ND ug/kg 04/25/18 16:09 105-67-904/21/18 14:304001
Dimethylphthalate ND ug/kg 04/25/18 16:09 131-11-304/21/18 14:304001
Di-n-butylphthalate ND ug/kg 04/25/18 16:09 84-74-204/21/18 14:304001
4,6-Dinitro-2-methylphenol ND ug/kg 04/25/18 16:09 534-52-104/21/18 14:308011
2,4-Dinitrophenol ND ug/kg 04/25/18 16:09 51-28-504/21/18 14:3020001
2,4-Dinitrotoluene ND ug/kg 04/25/18 16:09 121-14-204/21/18 14:304001
2,6-Dinitrotoluene ND ug/kg 04/25/18 16:09 606-20-204/21/18 14:304001
Di-n-octylphthalate ND ug/kg 04/25/18 16:09 117-84-004/21/18 14:304001
bis(2-Ethylhexyl)phthalate ND ug/kg 04/25/18 16:09 117-81-704/21/18 14:304001
Fluoranthene ND ug/kg 04/25/18 16:09 206-44-004/21/18 14:304001
Fluorene ND ug/kg 04/25/18 16:09 86-73-704/21/18 14:304001
Hexachloro-1,3-butadiene ND ug/kg 04/25/18 16:09 87-68-304/21/18 14:304001
Hexachlorobenzene ND ug/kg 04/25/18 16:09 118-74-104/21/18 14:304001
Hexachlorocyclopentadiene ND ug/kg 04/25/18 16:09 77-47-404/21/18 14:304001
Hexachloroethane ND ug/kg 04/25/18 16:09 67-72-104/21/18 14:304001
Indeno(1,2,3-cd)pyrene ND ug/kg 04/25/18 16:09 193-39-504/21/18 14:304001
Isophorone ND ug/kg 04/25/18 16:09 78-59-104/21/18 14:304001
1-Methylnaphthalene ND ug/kg 04/25/18 16:09 90-12-004/21/18 14:304001
2-Methylnaphthalene ND ug/kg 04/25/18 16:09 91-57-604/21/18 14:304001
2-Methylphenol(o-Cresol)ND ug/kg 04/25/18 16:09 95-48-704/21/18 14:304001
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/25/18 16:09 15831-10-404/21/18 14:304001
Naphthalene ND ug/kg 04/25/18 16:09 91-20-304/21/18 14:304001
2-Nitroaniline ND ug/kg 04/25/18 16:09 88-74-404/21/18 14:3020001
3-Nitroaniline ND ug/kg 04/25/18 16:09 99-09-204/21/18 14:3020001
4-Nitroaniline ND ug/kg 04/25/18 16:09 100-01-604/21/18 14:308011
Nitrobenzene ND ug/kg 04/25/18 16:09 98-95-304/21/18 14:304001
2-Nitrophenol ND ug/kg 04/25/18 16:09 88-75-504/21/18 14:304001
4-Nitrophenol ND ug/kg 04/25/18 16:09 100-02-704/21/18 14:3020001
N-Nitrosodimethylamine ND ug/kg 04/25/18 16:09 62-75-904/21/18 14:304001
N-Nitroso-di-n-propylamine ND ug/kg 04/25/18 16:09 621-64-704/21/18 14:304001
N-Nitrosodiphenylamine ND ug/kg 04/25/18 16:09 86-30-604/21/18 14:304001
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/25/18 16:09 108-60-104/21/18 14:304001
Pentachlorophenol ND ug/kg 04/25/18 16:09 87-86-504/21/18 14:3020001
Phenanthrene ND ug/kg 04/25/18 16:09 85-01-804/21/18 14:304001
Phenol ND ug/kg 04/25/18 16:09 108-95-204/21/18 14:304001
Pyrene ND ug/kg 04/25/18 16:09 129-00-004/21/18 14:304001
1,2,4-Trichlorobenzene ND ug/kg 04/25/18 16:09 120-82-104/21/18 14:304001
2,4,5-Trichlorophenol ND ug/kg 04/25/18 16:09 95-95-404/21/18 14:304001
2,4,6-Trichlorophenol ND ug/kg 04/25/18 16:09 88-06-204/21/18 14:304001
Surrogates
Nitrobenzene-d5 (S)62 %04/25/18 16:09 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)62 %04/25/18 16:09 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)48 %04/25/18 16:09 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)59 %04/25/18 16:09 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)60 %04/25/18 16:09 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-1 Lab ID:92381713001 Collected:04/18/18 02:29 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)61 %04/25/18 16:09 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 13:48 67-64-11021
Benzene ND ug/kg 04/24/18 13:48 71-43-25.1 1
Bromobenzene ND ug/kg 04/24/18 13:48 108-86-15.1 1
Bromochloromethane ND ug/kg 04/24/18 13:48 74-97-55.1 1
Bromodichloromethane ND ug/kg 04/24/18 13:48 75-27-45.1 1
Bromoform ND ug/kg 04/24/18 13:48 75-25-25.1 1
Bromomethane ND ug/kg 04/24/18 13:48 74-83-910.2 1
2-Butanone (MEK)ND ug/kg 04/24/18 13:48 78-93-31021
n-Butylbenzene ND ug/kg 04/24/18 13:48 104-51-85.1 1
sec-Butylbenzene ND ug/kg 04/24/18 13:48 135-98-85.1 1
tert-Butylbenzene ND ug/kg 04/24/18 13:48 98-06-65.1 1
Carbon tetrachloride ND ug/kg 04/24/18 13:48 56-23-55.1 1
Chlorobenzene ND ug/kg 04/24/18 13:48 108-90-75.1 1
Chloroethane ND ug/kg 04/24/18 13:48 75-00-310.2 1
Chloroform ND ug/kg 04/24/18 13:48 67-66-35.1 1
Chloromethane ND ug/kg 04/24/18 13:48 74-87-310.2 1
2-Chlorotoluene ND ug/kg 04/24/18 13:48 95-49-85.1 1
4-Chlorotoluene ND ug/kg 04/24/18 13:48 106-43-45.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 13:48 96-12-85.1 1
Dibromochloromethane ND ug/kg 04/24/18 13:48 124-48-15.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 13:48 106-93-45.1 1
Dibromomethane ND ug/kg 04/24/18 13:48 74-95-35.1 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 13:48 95-50-15.1 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 13:48 541-73-15.1 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 13:48 106-46-75.1 1
Dichlorodifluoromethane ND ug/kg 04/24/18 13:48 75-71-810.2 1
1,1-Dichloroethane ND ug/kg 04/24/18 13:48 75-34-35.1 1
1,2-Dichloroethane ND ug/kg 04/24/18 13:48 107-06-25.1 1
1,1-Dichloroethene ND ug/kg 04/24/18 13:48 75-35-45.1 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 13:48 156-59-25.1 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 13:48 156-60-55.1 1
1,2-Dichloropropane ND ug/kg 04/24/18 13:48 78-87-55.1 1
1,3-Dichloropropane ND ug/kg 04/24/18 13:48 142-28-95.1 1
2,2-Dichloropropane ND ug/kg 04/24/18 13:48 594-20-75.1 1
1,1-Dichloropropene ND ug/kg 04/24/18 13:48 563-58-65.1 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 13:48 10061-01-55.1 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 13:48 10061-02-65.1 1
Diisopropyl ether ND ug/kg 04/24/18 13:48 108-20-35.1 1
Ethylbenzene ND ug/kg 04/24/18 13:48 100-41-45.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 13:48 87-68-35.1 1
2-Hexanone ND ug/kg 04/24/18 13:48 591-78-650.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 13:48 98-82-85.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-1 Lab ID:92381713001 Collected:04/18/18 02:29 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 13:48 99-87-65.1 1
Methylene Chloride ND ug/kg 04/24/18 13:48 75-09-2 M120.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 13:48 108-10-150.8 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 13:48 1634-04-45.1 1
Naphthalene ND ug/kg 04/24/18 13:48 91-20-35.1 1
n-Propylbenzene ND ug/kg 04/24/18 13:48 103-65-15.1 1
Styrene ND ug/kg 04/24/18 13:48 100-42-55.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 13:48 630-20-65.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 13:48 79-34-55.1 1
Tetrachloroethene ND ug/kg 04/24/18 13:48 127-18-45.1 1
Toluene ND ug/kg 04/24/18 13:48 108-88-35.1 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 13:48 87-61-65.1 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 13:48 120-82-15.1 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 13:48 71-55-65.1 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 13:48 79-00-55.1 1
Trichloroethene ND ug/kg 04/24/18 13:48 79-01-65.1 1
Trichlorofluoromethane ND ug/kg 04/24/18 13:48 75-69-45.1 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 13:48 96-18-45.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 13:48 95-63-65.1 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 13:48 108-67-85.1 1
Vinyl acetate ND ug/kg 04/24/18 13:48 108-05-4 M150.8 1
Vinyl chloride ND ug/kg 04/24/18 13:48 75-01-410.2 1
Xylene (Total)ND ug/kg 04/24/18 13:48 1330-20-710.2 1
m&p-Xylene ND ug/kg 04/24/18 13:48 179601-23-110.2 1
o-Xylene ND ug/kg 04/24/18 13:48 95-47-65.1 1
Surrogates
Toluene-d8 (S)105 %04/24/18 13:48 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %04/24/18 13:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %04/24/18 13:48 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.3 %04/23/18 10:260.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-2 Lab ID:92381713002 Collected:04/18/18 02:32 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 05/01/18 17:12 N205/01/18 06:5512.3 1
Aliphatic (C19-C36)ND mg/kg 05/01/18 17:12 N205/01/18 06:5512.3 1
Aromatic (C11-C22)ND mg/kg 05/01/18 17:12 N205/01/18 06:5512.3 1
Surrogates
Nonatriacontane (S)74 %05/01/18 17:12 7194-86-705/01/18 06:5540-140 1
o-Terphenyl (S)47 %05/01/18 17:12 84-15-105/01/18 06:5540-140 1
2-Fluorobiphenyl (S)62 %05/01/18 17:12 321-60-805/01/18 06:5540-140 1
2-Bromonaphthalene (S)62 %05/01/18 17:12 580-13-205/01/18 06:5540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 18:00 N204/23/18 11:543.0 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 18:00 N204/23/18 11:543.0 1
Aromatic (C09-C10)ND mg/kg 04/23/18 18:00 N204/23/18 11:543.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)115 %04/23/18 18:00 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)112 %04/23/18 18:00 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/25/18 16:38 83-32-904/21/18 14:304001
Acenaphthylene ND ug/kg 04/25/18 16:38 208-96-804/21/18 14:304001
Aniline ND ug/kg 04/25/18 16:38 62-53-304/21/18 14:304001
Anthracene ND ug/kg 04/25/18 16:38 120-12-704/21/18 14:304001
Benzo(a)anthracene ND ug/kg 04/25/18 16:38 56-55-304/21/18 14:304001
Benzo(a)pyrene ND ug/kg 04/25/18 16:38 50-32-804/21/18 14:304001
Benzo(b)fluoranthene ND ug/kg 04/25/18 16:38 205-99-204/21/18 14:304001
Benzo(g,h,i)perylene ND ug/kg 04/25/18 16:38 191-24-204/21/18 14:304001
Benzo(k)fluoranthene ND ug/kg 04/25/18 16:38 207-08-904/21/18 14:304001
Benzoic Acid ND ug/kg 04/25/18 16:38 65-85-004/21/18 14:3020001
Benzyl alcohol ND ug/kg 04/25/18 16:38 100-51-604/21/18 14:308001
4-Bromophenylphenyl ether ND ug/kg 04/25/18 16:38 101-55-304/21/18 14:304001
Butylbenzylphthalate ND ug/kg 04/25/18 16:38 85-68-704/21/18 14:304001
4-Chloro-3-methylphenol ND ug/kg 04/25/18 16:38 59-50-704/21/18 14:308001
4-Chloroaniline ND ug/kg 04/25/18 16:38 106-47-804/21/18 14:3020001
bis(2-Chloroethoxy)methane ND ug/kg 04/25/18 16:38 111-91-104/21/18 14:304001
bis(2-Chloroethyl) ether ND ug/kg 04/25/18 16:38 111-44-404/21/18 14:304001
2-Chloronaphthalene ND ug/kg 04/25/18 16:38 91-58-704/21/18 14:304001
2-Chlorophenol ND ug/kg 04/25/18 16:38 95-57-804/21/18 14:304001
4-Chlorophenylphenyl ether ND ug/kg 04/25/18 16:38 7005-72-304/21/18 14:304001
Chrysene ND ug/kg 04/25/18 16:38 218-01-904/21/18 14:304001
Dibenz(a,h)anthracene ND ug/kg 04/25/18 16:38 53-70-304/21/18 14:304001
Dibenzofuran ND ug/kg 04/25/18 16:38 132-64-904/21/18 14:304001
1,2-Dichlorobenzene ND ug/kg 04/25/18 16:38 95-50-104/21/18 14:304001
1,3-Dichlorobenzene ND ug/kg 04/25/18 16:38 541-73-104/21/18 14:304001
1,4-Dichlorobenzene ND ug/kg 04/25/18 16:38 106-46-704/21/18 14:304001
3,3'-Dichlorobenzidine ND ug/kg 04/25/18 16:38 91-94-104/21/18 14:3020001
2,4-Dichlorophenol ND ug/kg 04/25/18 16:38 120-83-204/21/18 14:304001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-2 Lab ID:92381713002 Collected:04/18/18 02:32 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/25/18 16:38 84-66-204/21/18 14:304001
2,4-Dimethylphenol ND ug/kg 04/25/18 16:38 105-67-904/21/18 14:304001
Dimethylphthalate ND ug/kg 04/25/18 16:38 131-11-304/21/18 14:304001
Di-n-butylphthalate ND ug/kg 04/25/18 16:38 84-74-204/21/18 14:304001
4,6-Dinitro-2-methylphenol ND ug/kg 04/25/18 16:38 534-52-104/21/18 14:308001
2,4-Dinitrophenol ND ug/kg 04/25/18 16:38 51-28-504/21/18 14:3020001
2,4-Dinitrotoluene ND ug/kg 04/25/18 16:38 121-14-204/21/18 14:304001
2,6-Dinitrotoluene ND ug/kg 04/25/18 16:38 606-20-204/21/18 14:304001
Di-n-octylphthalate ND ug/kg 04/25/18 16:38 117-84-004/21/18 14:304001
bis(2-Ethylhexyl)phthalate ND ug/kg 04/25/18 16:38 117-81-704/21/18 14:304001
Fluoranthene ND ug/kg 04/25/18 16:38 206-44-004/21/18 14:304001
Fluorene ND ug/kg 04/25/18 16:38 86-73-704/21/18 14:304001
Hexachloro-1,3-butadiene ND ug/kg 04/25/18 16:38 87-68-304/21/18 14:304001
Hexachlorobenzene ND ug/kg 04/25/18 16:38 118-74-104/21/18 14:304001
Hexachlorocyclopentadiene ND ug/kg 04/25/18 16:38 77-47-404/21/18 14:304001
Hexachloroethane ND ug/kg 04/25/18 16:38 67-72-104/21/18 14:304001
Indeno(1,2,3-cd)pyrene ND ug/kg 04/25/18 16:38 193-39-504/21/18 14:304001
Isophorone ND ug/kg 04/25/18 16:38 78-59-104/21/18 14:304001
1-Methylnaphthalene ND ug/kg 04/25/18 16:38 90-12-004/21/18 14:304001
2-Methylnaphthalene ND ug/kg 04/25/18 16:38 91-57-604/21/18 14:304001
2-Methylphenol(o-Cresol)ND ug/kg 04/25/18 16:38 95-48-704/21/18 14:304001
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/25/18 16:38 15831-10-404/21/18 14:304001
Naphthalene ND ug/kg 04/25/18 16:38 91-20-304/21/18 14:304001
2-Nitroaniline ND ug/kg 04/25/18 16:38 88-74-404/21/18 14:3020001
3-Nitroaniline ND ug/kg 04/25/18 16:38 99-09-204/21/18 14:3020001
4-Nitroaniline ND ug/kg 04/25/18 16:38 100-01-604/21/18 14:308001
Nitrobenzene ND ug/kg 04/25/18 16:38 98-95-304/21/18 14:304001
2-Nitrophenol ND ug/kg 04/25/18 16:38 88-75-504/21/18 14:304001
4-Nitrophenol ND ug/kg 04/25/18 16:38 100-02-704/21/18 14:3020001
N-Nitrosodimethylamine ND ug/kg 04/25/18 16:38 62-75-904/21/18 14:304001
N-Nitroso-di-n-propylamine ND ug/kg 04/25/18 16:38 621-64-704/21/18 14:304001
N-Nitrosodiphenylamine ND ug/kg 04/25/18 16:38 86-30-604/21/18 14:304001
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/25/18 16:38 108-60-104/21/18 14:304001
Pentachlorophenol ND ug/kg 04/25/18 16:38 87-86-504/21/18 14:3020001
Phenanthrene ND ug/kg 04/25/18 16:38 85-01-804/21/18 14:304001
Phenol ND ug/kg 04/25/18 16:38 108-95-204/21/18 14:304001
Pyrene ND ug/kg 04/25/18 16:38 129-00-004/21/18 14:304001
1,2,4-Trichlorobenzene ND ug/kg 04/25/18 16:38 120-82-104/21/18 14:304001
2,4,5-Trichlorophenol ND ug/kg 04/25/18 16:38 95-95-404/21/18 14:304001
2,4,6-Trichlorophenol ND ug/kg 04/25/18 16:38 88-06-204/21/18 14:304001
Surrogates
Nitrobenzene-d5 (S)74 %04/25/18 16:38 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)71 %04/25/18 16:38 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)54 %04/25/18 16:38 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)67 %04/25/18 16:38 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)64 %04/25/18 16:38 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-2 Lab ID:92381713002 Collected:04/18/18 02:32 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)68 %04/25/18 16:38 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 14:08 67-64-11121
Benzene ND ug/kg 04/24/18 14:08 71-43-25.6 1
Bromobenzene ND ug/kg 04/24/18 14:08 108-86-15.6 1
Bromochloromethane ND ug/kg 04/24/18 14:08 74-97-55.6 1
Bromodichloromethane ND ug/kg 04/24/18 14:08 75-27-45.6 1
Bromoform ND ug/kg 04/24/18 14:08 75-25-25.6 1
Bromomethane ND ug/kg 04/24/18 14:08 74-83-911.2 1
2-Butanone (MEK)ND ug/kg 04/24/18 14:08 78-93-31121
n-Butylbenzene ND ug/kg 04/24/18 14:08 104-51-85.6 1
sec-Butylbenzene ND ug/kg 04/24/18 14:08 135-98-85.6 1
tert-Butylbenzene ND ug/kg 04/24/18 14:08 98-06-65.6 1
Carbon tetrachloride ND ug/kg 04/24/18 14:08 56-23-55.6 1
Chlorobenzene ND ug/kg 04/24/18 14:08 108-90-75.6 1
Chloroethane ND ug/kg 04/24/18 14:08 75-00-311.2 1
Chloroform ND ug/kg 04/24/18 14:08 67-66-35.6 1
Chloromethane ND ug/kg 04/24/18 14:08 74-87-311.2 1
2-Chlorotoluene ND ug/kg 04/24/18 14:08 95-49-85.6 1
4-Chlorotoluene ND ug/kg 04/24/18 14:08 106-43-45.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 14:08 96-12-85.6 1
Dibromochloromethane ND ug/kg 04/24/18 14:08 124-48-15.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 14:08 106-93-45.6 1
Dibromomethane ND ug/kg 04/24/18 14:08 74-95-35.6 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 14:08 95-50-15.6 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 14:08 541-73-15.6 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 14:08 106-46-75.6 1
Dichlorodifluoromethane ND ug/kg 04/24/18 14:08 75-71-811.2 1
1,1-Dichloroethane ND ug/kg 04/24/18 14:08 75-34-35.6 1
1,2-Dichloroethane ND ug/kg 04/24/18 14:08 107-06-25.6 1
1,1-Dichloroethene ND ug/kg 04/24/18 14:08 75-35-45.6 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 14:08 156-59-25.6 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 14:08 156-60-55.6 1
1,2-Dichloropropane ND ug/kg 04/24/18 14:08 78-87-55.6 1
1,3-Dichloropropane ND ug/kg 04/24/18 14:08 142-28-95.6 1
2,2-Dichloropropane ND ug/kg 04/24/18 14:08 594-20-75.6 1
1,1-Dichloropropene ND ug/kg 04/24/18 14:08 563-58-65.6 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 14:08 10061-01-55.6 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 14:08 10061-02-65.6 1
Diisopropyl ether ND ug/kg 04/24/18 14:08 108-20-35.6 1
Ethylbenzene ND ug/kg 04/24/18 14:08 100-41-45.6 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 14:08 87-68-35.6 1
2-Hexanone ND ug/kg 04/24/18 14:08 591-78-656.2 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 14:08 98-82-85.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-2 Lab ID:92381713002 Collected:04/18/18 02:32 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 14:08 99-87-65.6 1
Methylene Chloride ND ug/kg 04/24/18 14:08 75-09-222.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 14:08 108-10-156.2 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 14:08 1634-04-45.6 1
Naphthalene ND ug/kg 04/24/18 14:08 91-20-35.6 1
n-Propylbenzene ND ug/kg 04/24/18 14:08 103-65-15.6 1
Styrene ND ug/kg 04/24/18 14:08 100-42-55.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 14:08 630-20-65.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 14:08 79-34-55.6 1
Tetrachloroethene ND ug/kg 04/24/18 14:08 127-18-45.6 1
Toluene ND ug/kg 04/24/18 14:08 108-88-35.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 14:08 87-61-65.6 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 14:08 120-82-15.6 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 14:08 71-55-65.6 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 14:08 79-00-55.6 1
Trichloroethene ND ug/kg 04/24/18 14:08 79-01-65.6 1
Trichlorofluoromethane ND ug/kg 04/24/18 14:08 75-69-45.6 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 14:08 96-18-45.6 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 14:08 95-63-65.6 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 14:08 108-67-85.6 1
Vinyl acetate ND ug/kg 04/24/18 14:08 108-05-456.2 1
Vinyl chloride ND ug/kg 04/24/18 14:08 75-01-411.2 1
Xylene (Total)ND ug/kg 04/24/18 14:08 1330-20-711.2 1
m&p-Xylene ND ug/kg 04/24/18 14:08 179601-23-111.2 1
o-Xylene ND ug/kg 04/24/18 14:08 95-47-65.6 1
Surrogates
Toluene-d8 (S)104 %04/24/18 14:08 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %04/24/18 14:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %04/24/18 14:08 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %04/23/18 10:260.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-3 Lab ID:92381713003 Collected:04/18/18 02:35 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/26/18 09:54 N204/24/18 08:0011.6 1
Aliphatic (C19-C36)ND mg/kg 04/26/18 09:54 N204/24/18 08:0011.6 1
Aromatic (C11-C22)ND mg/kg 04/26/18 09:54 N204/24/18 08:0011.6 1
Surrogates
Nonatriacontane (S)56 %04/26/18 09:54 7194-86-704/24/18 08:0040-140 1
o-Terphenyl (S)48 %04/26/18 09:54 84-15-104/24/18 08:0040-140 1
2-Fluorobiphenyl (S)65 %04/26/18 09:54 321-60-804/24/18 08:0040-140 1
2-Bromonaphthalene (S)51 %04/26/18 09:54 580-13-204/24/18 08:0040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 18:28 N204/23/18 11:542.6 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 18:28 N204/23/18 11:542.6 1
Aromatic (C09-C10)ND mg/kg 04/23/18 18:28 N204/23/18 11:542.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %04/23/18 18:28 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)107 %04/23/18 18:28 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/25/18 17:07 83-32-904/21/18 14:303901
Acenaphthylene ND ug/kg 04/25/18 17:07 208-96-804/21/18 14:303901
Aniline ND ug/kg 04/25/18 17:07 62-53-304/21/18 14:303901
Anthracene ND ug/kg 04/25/18 17:07 120-12-704/21/18 14:303901
Benzo(a)anthracene ND ug/kg 04/25/18 17:07 56-55-304/21/18 14:303901
Benzo(a)pyrene ND ug/kg 04/25/18 17:07 50-32-804/21/18 14:303901
Benzo(b)fluoranthene ND ug/kg 04/25/18 17:07 205-99-204/21/18 14:303901
Benzo(g,h,i)perylene ND ug/kg 04/25/18 17:07 191-24-204/21/18 14:303901
Benzo(k)fluoranthene ND ug/kg 04/25/18 17:07 207-08-904/21/18 14:303901
Benzoic Acid ND ug/kg 04/25/18 17:07 65-85-004/21/18 14:3019501
Benzyl alcohol ND ug/kg 04/25/18 17:07 100-51-604/21/18 14:307811
4-Bromophenylphenyl ether ND ug/kg 04/25/18 17:07 101-55-304/21/18 14:303901
Butylbenzylphthalate ND ug/kg 04/25/18 17:07 85-68-704/21/18 14:303901
4-Chloro-3-methylphenol ND ug/kg 04/25/18 17:07 59-50-704/21/18 14:307811
4-Chloroaniline ND ug/kg 04/25/18 17:07 106-47-804/21/18 14:3019501
bis(2-Chloroethoxy)methane ND ug/kg 04/25/18 17:07 111-91-104/21/18 14:303901
bis(2-Chloroethyl) ether ND ug/kg 04/25/18 17:07 111-44-404/21/18 14:303901
2-Chloronaphthalene ND ug/kg 04/25/18 17:07 91-58-704/21/18 14:303901
2-Chlorophenol ND ug/kg 04/25/18 17:07 95-57-804/21/18 14:303901
4-Chlorophenylphenyl ether ND ug/kg 04/25/18 17:07 7005-72-304/21/18 14:303901
Chrysene ND ug/kg 04/25/18 17:07 218-01-904/21/18 14:303901
Dibenz(a,h)anthracene ND ug/kg 04/25/18 17:07 53-70-304/21/18 14:303901
Dibenzofuran ND ug/kg 04/25/18 17:07 132-64-904/21/18 14:303901
1,2-Dichlorobenzene ND ug/kg 04/25/18 17:07 95-50-104/21/18 14:303901
1,3-Dichlorobenzene ND ug/kg 04/25/18 17:07 541-73-104/21/18 14:303901
1,4-Dichlorobenzene ND ug/kg 04/25/18 17:07 106-46-704/21/18 14:303901
3,3'-Dichlorobenzidine ND ug/kg 04/25/18 17:07 91-94-104/21/18 14:3019501
2,4-Dichlorophenol ND ug/kg 04/25/18 17:07 120-83-204/21/18 14:303901
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-3 Lab ID:92381713003 Collected:04/18/18 02:35 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/25/18 17:07 84-66-204/21/18 14:303901
2,4-Dimethylphenol ND ug/kg 04/25/18 17:07 105-67-904/21/18 14:303901
Dimethylphthalate ND ug/kg 04/25/18 17:07 131-11-304/21/18 14:303901
Di-n-butylphthalate ND ug/kg 04/25/18 17:07 84-74-204/21/18 14:303901
4,6-Dinitro-2-methylphenol ND ug/kg 04/25/18 17:07 534-52-104/21/18 14:307811
2,4-Dinitrophenol ND ug/kg 04/25/18 17:07 51-28-504/21/18 14:3019501
2,4-Dinitrotoluene ND ug/kg 04/25/18 17:07 121-14-204/21/18 14:303901
2,6-Dinitrotoluene ND ug/kg 04/25/18 17:07 606-20-204/21/18 14:303901
Di-n-octylphthalate ND ug/kg 04/25/18 17:07 117-84-004/21/18 14:303901
bis(2-Ethylhexyl)phthalate ND ug/kg 04/25/18 17:07 117-81-704/21/18 14:303901
Fluoranthene ND ug/kg 04/25/18 17:07 206-44-004/21/18 14:303901
Fluorene ND ug/kg 04/25/18 17:07 86-73-704/21/18 14:303901
Hexachloro-1,3-butadiene ND ug/kg 04/25/18 17:07 87-68-304/21/18 14:303901
Hexachlorobenzene ND ug/kg 04/25/18 17:07 118-74-104/21/18 14:303901
Hexachlorocyclopentadiene ND ug/kg 04/25/18 17:07 77-47-404/21/18 14:303901
Hexachloroethane ND ug/kg 04/25/18 17:07 67-72-104/21/18 14:303901
Indeno(1,2,3-cd)pyrene ND ug/kg 04/25/18 17:07 193-39-504/21/18 14:303901
Isophorone ND ug/kg 04/25/18 17:07 78-59-104/21/18 14:303901
1-Methylnaphthalene ND ug/kg 04/25/18 17:07 90-12-004/21/18 14:303901
2-Methylnaphthalene ND ug/kg 04/25/18 17:07 91-57-604/21/18 14:303901
2-Methylphenol(o-Cresol)ND ug/kg 04/25/18 17:07 95-48-704/21/18 14:303901
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/25/18 17:07 15831-10-404/21/18 14:303901
Naphthalene ND ug/kg 04/25/18 17:07 91-20-304/21/18 14:303901
2-Nitroaniline ND ug/kg 04/25/18 17:07 88-74-404/21/18 14:3019501
3-Nitroaniline ND ug/kg 04/25/18 17:07 99-09-204/21/18 14:3019501
4-Nitroaniline ND ug/kg 04/25/18 17:07 100-01-604/21/18 14:307811
Nitrobenzene ND ug/kg 04/25/18 17:07 98-95-304/21/18 14:303901
2-Nitrophenol ND ug/kg 04/25/18 17:07 88-75-504/21/18 14:303901
4-Nitrophenol ND ug/kg 04/25/18 17:07 100-02-704/21/18 14:3019501
N-Nitrosodimethylamine ND ug/kg 04/25/18 17:07 62-75-904/21/18 14:303901
N-Nitroso-di-n-propylamine ND ug/kg 04/25/18 17:07 621-64-704/21/18 14:303901
N-Nitrosodiphenylamine ND ug/kg 04/25/18 17:07 86-30-604/21/18 14:303901
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/25/18 17:07 108-60-104/21/18 14:303901
Pentachlorophenol ND ug/kg 04/25/18 17:07 87-86-504/21/18 14:3019501
Phenanthrene ND ug/kg 04/25/18 17:07 85-01-804/21/18 14:303901
Phenol ND ug/kg 04/25/18 17:07 108-95-204/21/18 14:303901
Pyrene ND ug/kg 04/25/18 17:07 129-00-004/21/18 14:303901
1,2,4-Trichlorobenzene ND ug/kg 04/25/18 17:07 120-82-104/21/18 14:303901
2,4,5-Trichlorophenol ND ug/kg 04/25/18 17:07 95-95-404/21/18 14:303901
2,4,6-Trichlorophenol ND ug/kg 04/25/18 17:07 88-06-204/21/18 14:303901
Surrogates
Nitrobenzene-d5 (S)69 %04/25/18 17:07 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)71 %04/25/18 17:07 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)51 %04/25/18 17:07 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)65 %04/25/18 17:07 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)66 %04/25/18 17:07 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-3 Lab ID:92381713003 Collected:04/18/18 02:35 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)70 %04/25/18 17:07 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 14:29 67-64-11051
Benzene ND ug/kg 04/24/18 14:29 71-43-25.3 1
Bromobenzene ND ug/kg 04/24/18 14:29 108-86-15.3 1
Bromochloromethane ND ug/kg 04/24/18 14:29 74-97-55.3 1
Bromodichloromethane ND ug/kg 04/24/18 14:29 75-27-45.3 1
Bromoform ND ug/kg 04/24/18 14:29 75-25-25.3 1
Bromomethane ND ug/kg 04/24/18 14:29 74-83-910.5 1
2-Butanone (MEK)ND ug/kg 04/24/18 14:29 78-93-31051
n-Butylbenzene ND ug/kg 04/24/18 14:29 104-51-85.3 1
sec-Butylbenzene ND ug/kg 04/24/18 14:29 135-98-85.3 1
tert-Butylbenzene ND ug/kg 04/24/18 14:29 98-06-65.3 1
Carbon tetrachloride ND ug/kg 04/24/18 14:29 56-23-55.3 1
Chlorobenzene ND ug/kg 04/24/18 14:29 108-90-75.3 1
Chloroethane ND ug/kg 04/24/18 14:29 75-00-310.5 1
Chloroform ND ug/kg 04/24/18 14:29 67-66-35.3 1
Chloromethane ND ug/kg 04/24/18 14:29 74-87-310.5 1
2-Chlorotoluene ND ug/kg 04/24/18 14:29 95-49-85.3 1
4-Chlorotoluene ND ug/kg 04/24/18 14:29 106-43-45.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 14:29 96-12-85.3 1
Dibromochloromethane ND ug/kg 04/24/18 14:29 124-48-15.3 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 14:29 106-93-45.3 1
Dibromomethane ND ug/kg 04/24/18 14:29 74-95-35.3 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 14:29 95-50-15.3 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 14:29 541-73-15.3 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 14:29 106-46-75.3 1
Dichlorodifluoromethane ND ug/kg 04/24/18 14:29 75-71-810.5 1
1,1-Dichloroethane ND ug/kg 04/24/18 14:29 75-34-35.3 1
1,2-Dichloroethane ND ug/kg 04/24/18 14:29 107-06-25.3 1
1,1-Dichloroethene ND ug/kg 04/24/18 14:29 75-35-45.3 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 14:29 156-59-25.3 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 14:29 156-60-55.3 1
1,2-Dichloropropane ND ug/kg 04/24/18 14:29 78-87-55.3 1
1,3-Dichloropropane ND ug/kg 04/24/18 14:29 142-28-95.3 1
2,2-Dichloropropane ND ug/kg 04/24/18 14:29 594-20-75.3 1
1,1-Dichloropropene ND ug/kg 04/24/18 14:29 563-58-65.3 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 14:29 10061-01-55.3 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 14:29 10061-02-65.3 1
Diisopropyl ether ND ug/kg 04/24/18 14:29 108-20-35.3 1
Ethylbenzene ND ug/kg 04/24/18 14:29 100-41-45.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 14:29 87-68-35.3 1
2-Hexanone ND ug/kg 04/24/18 14:29 591-78-652.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 14:29 98-82-85.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-3 Lab ID:92381713003 Collected:04/18/18 02:35 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 14:29 99-87-65.3 1
Methylene Chloride ND ug/kg 04/24/18 14:29 75-09-221.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 14:29 108-10-152.7 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 14:29 1634-04-45.3 1
Naphthalene ND ug/kg 04/24/18 14:29 91-20-35.3 1
n-Propylbenzene ND ug/kg 04/24/18 14:29 103-65-15.3 1
Styrene ND ug/kg 04/24/18 14:29 100-42-55.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 14:29 630-20-65.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 14:29 79-34-55.3 1
Tetrachloroethene ND ug/kg 04/24/18 14:29 127-18-45.3 1
Toluene ND ug/kg 04/24/18 14:29 108-88-35.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 14:29 87-61-65.3 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 14:29 120-82-15.3 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 14:29 71-55-65.3 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 14:29 79-00-55.3 1
Trichloroethene ND ug/kg 04/24/18 14:29 79-01-65.3 1
Trichlorofluoromethane ND ug/kg 04/24/18 14:29 75-69-45.3 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 14:29 96-18-45.3 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 14:29 95-63-65.3 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 14:29 108-67-85.3 1
Vinyl acetate ND ug/kg 04/24/18 14:29 108-05-452.7 1
Vinyl chloride ND ug/kg 04/24/18 14:29 75-01-410.5 1
Xylene (Total)ND ug/kg 04/24/18 14:29 1330-20-710.5 1
m&p-Xylene ND ug/kg 04/24/18 14:29 179601-23-110.5 1
o-Xylene ND ug/kg 04/24/18 14:29 95-47-65.3 1
Surrogates
Toluene-d8 (S)105 %04/24/18 14:29 2037-26-570-130 1
4-Bromofluorobenzene (S)89 %04/24/18 14:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %04/24/18 14:29 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %04/23/18 10:260.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-4 Lab ID:92381713004 Collected:04/18/18 02:38 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 05/01/18 17:40 N205/01/18 06:5511.6 1
Aliphatic (C19-C36)ND mg/kg 05/01/18 17:40 N205/01/18 06:5511.6 1
Aromatic (C11-C22)ND mg/kg 05/01/18 17:40 1g,N205/01/18 06:5511.6 1
Surrogates
Nonatriacontane (S)42 %05/01/18 17:40 7194-86-705/01/18 06:5540-140 1
o-Terphenyl (S)34 %05/01/18 17:40 84-15-1 S005/01/18 06:5540-140 1
2-Fluorobiphenyl (S)49 %05/01/18 17:40 321-60-805/01/18 06:5540-140 1
2-Bromonaphthalene (S)48 %05/01/18 17:40 580-13-205/01/18 06:5540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 18:57 N204/23/18 11:542.3 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 18:57 N204/23/18 11:542.3 1
Aromatic (C09-C10)ND mg/kg 04/23/18 18:57 N204/23/18 11:542.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %04/23/18 18:57 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)107 %04/23/18 18:57 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/25/18 17:35 83-32-904/21/18 14:303831
Acenaphthylene 1580 ug/kg 04/25/18 17:35 208-96-804/21/18 14:303831
Aniline ND ug/kg 04/25/18 17:35 62-53-304/21/18 14:303831
Anthracene ND ug/kg 04/25/18 17:35 120-12-704/21/18 14:303831
Benzo(a)anthracene 1270 ug/kg 04/25/18 17:35 56-55-304/21/18 14:303831
Benzo(a)pyrene 1760 ug/kg 04/25/18 17:35 50-32-804/21/18 14:303831
Benzo(b)fluoranthene 1670 ug/kg 04/25/18 17:35 205-99-204/21/18 14:303831
Benzo(g,h,i)perylene 1370 ug/kg 04/25/18 17:35 191-24-204/21/18 14:303831
Benzo(k)fluoranthene 708 ug/kg 04/25/18 17:35 207-08-904/21/18 14:303831
Benzoic Acid ND ug/kg 04/25/18 17:35 65-85-004/21/18 14:3019201
Benzyl alcohol ND ug/kg 04/25/18 17:35 100-51-604/21/18 14:307661
4-Bromophenylphenyl ether ND ug/kg 04/25/18 17:35 101-55-304/21/18 14:303831
Butylbenzylphthalate ND ug/kg 04/25/18 17:35 85-68-704/21/18 14:303831
4-Chloro-3-methylphenol ND ug/kg 04/25/18 17:35 59-50-704/21/18 14:307661
4-Chloroaniline ND ug/kg 04/25/18 17:35 106-47-804/21/18 14:3019201
bis(2-Chloroethoxy)methane ND ug/kg 04/25/18 17:35 111-91-104/21/18 14:303831
bis(2-Chloroethyl) ether ND ug/kg 04/25/18 17:35 111-44-404/21/18 14:303831
2-Chloronaphthalene ND ug/kg 04/25/18 17:35 91-58-704/21/18 14:303831
2-Chlorophenol ND ug/kg 04/25/18 17:35 95-57-804/21/18 14:303831
4-Chlorophenylphenyl ether ND ug/kg 04/25/18 17:35 7005-72-304/21/18 14:303831
Chrysene 1350 ug/kg 04/25/18 17:35 218-01-904/21/18 14:303831
Dibenz(a,h)anthracene ND ug/kg 04/25/18 17:35 53-70-304/21/18 14:303831
Dibenzofuran ND ug/kg 04/25/18 17:35 132-64-904/21/18 14:303831
1,2-Dichlorobenzene ND ug/kg 04/25/18 17:35 95-50-104/21/18 14:303831
1,3-Dichlorobenzene ND ug/kg 04/25/18 17:35 541-73-104/21/18 14:303831
1,4-Dichlorobenzene ND ug/kg 04/25/18 17:35 106-46-704/21/18 14:303831
3,3'-Dichlorobenzidine ND ug/kg 04/25/18 17:35 91-94-104/21/18 14:3019201
2,4-Dichlorophenol ND ug/kg 04/25/18 17:35 120-83-204/21/18 14:303831
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-4 Lab ID:92381713004 Collected:04/18/18 02:38 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/25/18 17:35 84-66-204/21/18 14:303831
2,4-Dimethylphenol ND ug/kg 04/25/18 17:35 105-67-904/21/18 14:303831
Dimethylphthalate ND ug/kg 04/25/18 17:35 131-11-304/21/18 14:303831
Di-n-butylphthalate ND ug/kg 04/25/18 17:35 84-74-204/21/18 14:303831
4,6-Dinitro-2-methylphenol ND ug/kg 04/25/18 17:35 534-52-104/21/18 14:307661
2,4-Dinitrophenol ND ug/kg 04/25/18 17:35 51-28-504/21/18 14:3019201
2,4-Dinitrotoluene ND ug/kg 04/25/18 17:35 121-14-204/21/18 14:303831
2,6-Dinitrotoluene ND ug/kg 04/25/18 17:35 606-20-204/21/18 14:303831
Di-n-octylphthalate ND ug/kg 04/25/18 17:35 117-84-004/21/18 14:303831
bis(2-Ethylhexyl)phthalate ND ug/kg 04/25/18 17:35 117-81-704/21/18 14:303831
Fluoranthene 1510 ug/kg 04/25/18 17:35 206-44-004/21/18 14:303831
Fluorene ND ug/kg 04/25/18 17:35 86-73-704/21/18 14:303831
Hexachloro-1,3-butadiene ND ug/kg 04/25/18 17:35 87-68-304/21/18 14:303831
Hexachlorobenzene ND ug/kg 04/25/18 17:35 118-74-104/21/18 14:303831
Hexachlorocyclopentadiene ND ug/kg 04/25/18 17:35 77-47-404/21/18 14:303831
Hexachloroethane ND ug/kg 04/25/18 17:35 67-72-104/21/18 14:303831
Indeno(1,2,3-cd)pyrene 1040 ug/kg 04/25/18 17:35 193-39-504/21/18 14:303831
Isophorone ND ug/kg 04/25/18 17:35 78-59-104/21/18 14:303831
1-Methylnaphthalene ND ug/kg 04/25/18 17:35 90-12-004/21/18 14:303831
2-Methylnaphthalene ND ug/kg 04/25/18 17:35 91-57-604/21/18 14:303831
2-Methylphenol(o-Cresol)ND ug/kg 04/25/18 17:35 95-48-704/21/18 14:303831
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/25/18 17:35 15831-10-404/21/18 14:303831
Naphthalene ND ug/kg 04/25/18 17:35 91-20-304/21/18 14:303831
2-Nitroaniline ND ug/kg 04/25/18 17:35 88-74-404/21/18 14:3019201
3-Nitroaniline ND ug/kg 04/25/18 17:35 99-09-204/21/18 14:3019201
4-Nitroaniline ND ug/kg 04/25/18 17:35 100-01-604/21/18 14:307661
Nitrobenzene ND ug/kg 04/25/18 17:35 98-95-304/21/18 14:303831
2-Nitrophenol ND ug/kg 04/25/18 17:35 88-75-504/21/18 14:303831
4-Nitrophenol ND ug/kg 04/25/18 17:35 100-02-704/21/18 14:3019201
N-Nitrosodimethylamine ND ug/kg 04/25/18 17:35 62-75-904/21/18 14:303831
N-Nitroso-di-n-propylamine ND ug/kg 04/25/18 17:35 621-64-704/21/18 14:303831
N-Nitrosodiphenylamine ND ug/kg 04/25/18 17:35 86-30-604/21/18 14:303831
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/25/18 17:35 108-60-104/21/18 14:303831
Pentachlorophenol ND ug/kg 04/25/18 17:35 87-86-504/21/18 14:3019201
Phenanthrene ND ug/kg 04/25/18 17:35 85-01-804/21/18 14:303831
Phenol ND ug/kg 04/25/18 17:35 108-95-204/21/18 14:303831
Pyrene 3600 ug/kg 04/25/18 17:35 129-00-004/21/18 14:303831
1,2,4-Trichlorobenzene ND ug/kg 04/25/18 17:35 120-82-104/21/18 14:303831
2,4,5-Trichlorophenol ND ug/kg 04/25/18 17:35 95-95-404/21/18 14:303831
2,4,6-Trichlorophenol ND ug/kg 04/25/18 17:35 88-06-204/21/18 14:303831
Surrogates
Nitrobenzene-d5 (S)76 %04/25/18 17:35 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)77 %04/25/18 17:35 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)50 %04/25/18 17:35 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)73 %04/25/18 17:35 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)69 %04/25/18 17:35 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-4 Lab ID:92381713004 Collected:04/18/18 02:38 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)87 %04/25/18 17:35 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 14:49 67-64-11011
Benzene ND ug/kg 04/24/18 14:49 71-43-25.0 1
Bromobenzene ND ug/kg 04/24/18 14:49 108-86-15.0 1
Bromochloromethane ND ug/kg 04/24/18 14:49 74-97-55.0 1
Bromodichloromethane ND ug/kg 04/24/18 14:49 75-27-45.0 1
Bromoform ND ug/kg 04/24/18 14:49 75-25-25.0 1
Bromomethane ND ug/kg 04/24/18 14:49 74-83-910.1 1
2-Butanone (MEK)ND ug/kg 04/24/18 14:49 78-93-31011
n-Butylbenzene ND ug/kg 04/24/18 14:49 104-51-85.0 1
sec-Butylbenzene ND ug/kg 04/24/18 14:49 135-98-85.0 1
tert-Butylbenzene ND ug/kg 04/24/18 14:49 98-06-65.0 1
Carbon tetrachloride ND ug/kg 04/24/18 14:49 56-23-55.0 1
Chlorobenzene ND ug/kg 04/24/18 14:49 108-90-75.0 1
Chloroethane ND ug/kg 04/24/18 14:49 75-00-310.1 1
Chloroform ND ug/kg 04/24/18 14:49 67-66-35.0 1
Chloromethane ND ug/kg 04/24/18 14:49 74-87-310.1 1
2-Chlorotoluene ND ug/kg 04/24/18 14:49 95-49-85.0 1
4-Chlorotoluene ND ug/kg 04/24/18 14:49 106-43-45.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 14:49 96-12-85.0 1
Dibromochloromethane ND ug/kg 04/24/18 14:49 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 14:49 106-93-45.0 1
Dibromomethane ND ug/kg 04/24/18 14:49 74-95-35.0 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 14:49 95-50-15.0 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 14:49 541-73-15.0 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 14:49 106-46-75.0 1
Dichlorodifluoromethane ND ug/kg 04/24/18 14:49 75-71-810.1 1
1,1-Dichloroethane ND ug/kg 04/24/18 14:49 75-34-35.0 1
1,2-Dichloroethane ND ug/kg 04/24/18 14:49 107-06-25.0 1
1,1-Dichloroethene ND ug/kg 04/24/18 14:49 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 14:49 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 14:49 156-60-55.0 1
1,2-Dichloropropane ND ug/kg 04/24/18 14:49 78-87-55.0 1
1,3-Dichloropropane ND ug/kg 04/24/18 14:49 142-28-95.0 1
2,2-Dichloropropane ND ug/kg 04/24/18 14:49 594-20-75.0 1
1,1-Dichloropropene ND ug/kg 04/24/18 14:49 563-58-65.0 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 14:49 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 14:49 10061-02-65.0 1
Diisopropyl ether ND ug/kg 04/24/18 14:49 108-20-35.0 1
Ethylbenzene ND ug/kg 04/24/18 14:49 100-41-45.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 14:49 87-68-35.0 1
2-Hexanone ND ug/kg 04/24/18 14:49 591-78-650.3 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 14:49 98-82-85.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:FT-SW-4 Lab ID:92381713004 Collected:04/18/18 02:38 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 14:49 99-87-65.0 1
Methylene Chloride ND ug/kg 04/24/18 14:49 75-09-220.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 14:49 108-10-150.3 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 14:49 1634-04-45.0 1
Naphthalene ND ug/kg 04/24/18 14:49 91-20-35.0 1
n-Propylbenzene ND ug/kg 04/24/18 14:49 103-65-15.0 1
Styrene ND ug/kg 04/24/18 14:49 100-42-55.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 14:49 630-20-65.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 14:49 79-34-55.0 1
Tetrachloroethene ND ug/kg 04/24/18 14:49 127-18-45.0 1
Toluene ND ug/kg 04/24/18 14:49 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 14:49 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 14:49 120-82-15.0 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 14:49 71-55-65.0 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 14:49 79-00-55.0 1
Trichloroethene ND ug/kg 04/24/18 14:49 79-01-65.0 1
Trichlorofluoromethane ND ug/kg 04/24/18 14:49 75-69-45.0 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 14:49 96-18-45.0 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 14:49 95-63-65.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 14:49 108-67-85.0 1
Vinyl acetate ND ug/kg 04/24/18 14:49 108-05-450.3 1
Vinyl chloride ND ug/kg 04/24/18 14:49 75-01-410.1 1
Xylene (Total)ND ug/kg 04/24/18 14:49 1330-20-710.1 1
m&p-Xylene ND ug/kg 04/24/18 14:49 179601-23-110.1 1
o-Xylene ND ug/kg 04/24/18 14:49 95-47-65.0 1
Surrogates
Toluene-d8 (S)103 %04/24/18 14:49 2037-26-570-130 1
4-Bromofluorobenzene (S)86 %04/24/18 14:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)86 %04/24/18 14:49 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.3 %04/23/18 10:260.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-1 Lab ID:92381713005 Collected:04/18/18 02:55 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/26/18 09:26 N204/24/18 08:0011.6 1
Aliphatic (C19-C36)ND mg/kg 04/26/18 09:26 N204/24/18 08:0011.6 1
Aromatic (C11-C22)ND mg/kg 04/26/18 09:26 N204/24/18 08:0011.6 1
Surrogates
Nonatriacontane (S)53 %04/26/18 09:26 7194-86-704/24/18 08:0040-140 1
o-Terphenyl (S)47 %04/26/18 09:26 84-15-104/24/18 08:0040-140 1
2-Fluorobiphenyl (S)28 %04/26/18 09:26 321-60-8 S004/24/18 08:0040-140 1
2-Bromonaphthalene (S)42 %04/26/18 09:26 580-13-204/24/18 08:0040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 19:25 N204/23/18 11:542.4 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 19:25 N204/23/18 11:542.4 1
Aromatic (C09-C10)ND mg/kg 04/23/18 19:25 N204/23/18 11:542.4 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %04/23/18 19:25 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)108 %04/23/18 19:25 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/26/18 01:16 83-32-904/21/18 14:303801
Acenaphthylene ND ug/kg 04/26/18 01:16 208-96-804/21/18 14:303801
Aniline ND ug/kg 04/26/18 01:16 62-53-304/21/18 14:303801
Anthracene ND ug/kg 04/26/18 01:16 120-12-704/21/18 14:303801
Benzo(a)anthracene ND ug/kg 04/26/18 01:16 56-55-304/21/18 14:303801
Benzo(a)pyrene ND ug/kg 04/26/18 01:16 50-32-804/21/18 14:303801
Benzo(b)fluoranthene ND ug/kg 04/26/18 01:16 205-99-204/21/18 14:303801
Benzo(g,h,i)perylene ND ug/kg 04/26/18 01:16 191-24-204/21/18 14:303801
Benzo(k)fluoranthene ND ug/kg 04/26/18 01:16 207-08-904/21/18 14:303801
Benzoic Acid ND ug/kg 04/26/18 01:16 65-85-004/21/18 14:3019001
Benzyl alcohol ND ug/kg 04/26/18 01:16 100-51-604/21/18 14:307601
4-Bromophenylphenyl ether ND ug/kg 04/26/18 01:16 101-55-304/21/18 14:303801
Butylbenzylphthalate ND ug/kg 04/26/18 01:16 85-68-704/21/18 14:303801
4-Chloro-3-methylphenol ND ug/kg 04/26/18 01:16 59-50-704/21/18 14:307601
4-Chloroaniline ND ug/kg 04/26/18 01:16 106-47-804/21/18 14:3019001
bis(2-Chloroethoxy)methane ND ug/kg 04/26/18 01:16 111-91-104/21/18 14:303801
bis(2-Chloroethyl) ether ND ug/kg 04/26/18 01:16 111-44-404/21/18 14:303801
2-Chloronaphthalene ND ug/kg 04/26/18 01:16 91-58-704/21/18 14:303801
2-Chlorophenol ND ug/kg 04/26/18 01:16 95-57-804/21/18 14:303801
4-Chlorophenylphenyl ether ND ug/kg 04/26/18 01:16 7005-72-304/21/18 14:303801
Chrysene ND ug/kg 04/26/18 01:16 218-01-904/21/18 14:303801
Dibenz(a,h)anthracene ND ug/kg 04/26/18 01:16 53-70-304/21/18 14:303801
Dibenzofuran ND ug/kg 04/26/18 01:16 132-64-904/21/18 14:303801
1,2-Dichlorobenzene ND ug/kg 04/26/18 01:16 95-50-104/21/18 14:303801
1,3-Dichlorobenzene ND ug/kg 04/26/18 01:16 541-73-104/21/18 14:303801
1,4-Dichlorobenzene ND ug/kg 04/26/18 01:16 106-46-704/21/18 14:303801
3,3'-Dichlorobenzidine ND ug/kg 04/26/18 01:16 91-94-104/21/18 14:3019001
2,4-Dichlorophenol ND ug/kg 04/26/18 01:16 120-83-204/21/18 14:303801
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-1 Lab ID:92381713005 Collected:04/18/18 02:55 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/26/18 01:16 84-66-204/21/18 14:303801
2,4-Dimethylphenol ND ug/kg 04/26/18 01:16 105-67-904/21/18 14:303801
Dimethylphthalate ND ug/kg 04/26/18 01:16 131-11-304/21/18 14:303801
Di-n-butylphthalate ND ug/kg 04/26/18 01:16 84-74-204/21/18 14:303801
4,6-Dinitro-2-methylphenol ND ug/kg 04/26/18 01:16 534-52-104/21/18 14:307601
2,4-Dinitrophenol ND ug/kg 04/26/18 01:16 51-28-504/21/18 14:3019001
2,4-Dinitrotoluene ND ug/kg 04/26/18 01:16 121-14-204/21/18 14:303801
2,6-Dinitrotoluene ND ug/kg 04/26/18 01:16 606-20-204/21/18 14:303801
Di-n-octylphthalate ND ug/kg 04/26/18 01:16 117-84-004/21/18 14:303801
bis(2-Ethylhexyl)phthalate ND ug/kg 04/26/18 01:16 117-81-704/21/18 14:303801
Fluoranthene ND ug/kg 04/26/18 01:16 206-44-004/21/18 14:303801
Fluorene ND ug/kg 04/26/18 01:16 86-73-704/21/18 14:303801
Hexachloro-1,3-butadiene ND ug/kg 04/26/18 01:16 87-68-304/21/18 14:303801
Hexachlorobenzene ND ug/kg 04/26/18 01:16 118-74-104/21/18 14:303801
Hexachlorocyclopentadiene ND ug/kg 04/26/18 01:16 77-47-404/21/18 14:303801
Hexachloroethane ND ug/kg 04/26/18 01:16 67-72-104/21/18 14:303801
Indeno(1,2,3-cd)pyrene ND ug/kg 04/26/18 01:16 193-39-504/21/18 14:303801
Isophorone ND ug/kg 04/26/18 01:16 78-59-104/21/18 14:303801
1-Methylnaphthalene ND ug/kg 04/26/18 01:16 90-12-004/21/18 14:303801
2-Methylnaphthalene ND ug/kg 04/26/18 01:16 91-57-604/21/18 14:303801
2-Methylphenol(o-Cresol)ND ug/kg 04/26/18 01:16 95-48-704/21/18 14:303801
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/26/18 01:16 15831-10-404/21/18 14:303801
Naphthalene ND ug/kg 04/26/18 01:16 91-20-304/21/18 14:303801
2-Nitroaniline ND ug/kg 04/26/18 01:16 88-74-404/21/18 14:3019001
3-Nitroaniline ND ug/kg 04/26/18 01:16 99-09-204/21/18 14:3019001
4-Nitroaniline ND ug/kg 04/26/18 01:16 100-01-604/21/18 14:307601
Nitrobenzene ND ug/kg 04/26/18 01:16 98-95-304/21/18 14:303801
2-Nitrophenol ND ug/kg 04/26/18 01:16 88-75-504/21/18 14:303801
4-Nitrophenol ND ug/kg 04/26/18 01:16 100-02-704/21/18 14:3019001
N-Nitrosodimethylamine ND ug/kg 04/26/18 01:16 62-75-904/21/18 14:303801
N-Nitroso-di-n-propylamine ND ug/kg 04/26/18 01:16 621-64-704/21/18 14:303801
N-Nitrosodiphenylamine ND ug/kg 04/26/18 01:16 86-30-604/21/18 14:303801
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/26/18 01:16 108-60-104/21/18 14:303801
Pentachlorophenol ND ug/kg 04/26/18 01:16 87-86-504/21/18 14:3019001
Phenanthrene ND ug/kg 04/26/18 01:16 85-01-804/21/18 14:303801
Phenol ND ug/kg 04/26/18 01:16 108-95-204/21/18 14:303801
Pyrene ND ug/kg 04/26/18 01:16 129-00-004/21/18 14:303801
1,2,4-Trichlorobenzene ND ug/kg 04/26/18 01:16 120-82-104/21/18 14:303801
2,4,5-Trichlorophenol ND ug/kg 04/26/18 01:16 95-95-404/21/18 14:303801
2,4,6-Trichlorophenol ND ug/kg 04/26/18 01:16 88-06-204/21/18 14:303801
Surrogates
Nitrobenzene-d5 (S)80 %04/26/18 01:16 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)71 %04/26/18 01:16 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)54 %04/26/18 01:16 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)69 %04/26/18 01:16 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)70 %04/26/18 01:16 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-1 Lab ID:92381713005 Collected:04/18/18 02:55 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)78 %04/26/18 01:16 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 15:10 67-64-179.4 1
Benzene ND ug/kg 04/24/18 15:10 71-43-24.0 1
Bromobenzene ND ug/kg 04/24/18 15:10 108-86-14.0 1
Bromochloromethane ND ug/kg 04/24/18 15:10 74-97-54.0 1
Bromodichloromethane ND ug/kg 04/24/18 15:10 75-27-44.0 1
Bromoform ND ug/kg 04/24/18 15:10 75-25-24.0 1
Bromomethane ND ug/kg 04/24/18 15:10 74-83-97.9 1
2-Butanone (MEK)ND ug/kg 04/24/18 15:10 78-93-379.4 1
n-Butylbenzene ND ug/kg 04/24/18 15:10 104-51-84.0 1
sec-Butylbenzene ND ug/kg 04/24/18 15:10 135-98-84.0 1
tert-Butylbenzene ND ug/kg 04/24/18 15:10 98-06-64.0 1
Carbon tetrachloride ND ug/kg 04/24/18 15:10 56-23-54.0 1
Chlorobenzene ND ug/kg 04/24/18 15:10 108-90-74.0 1
Chloroethane ND ug/kg 04/24/18 15:10 75-00-37.9 1
Chloroform ND ug/kg 04/24/18 15:10 67-66-34.0 1
Chloromethane ND ug/kg 04/24/18 15:10 74-87-37.9 1
2-Chlorotoluene ND ug/kg 04/24/18 15:10 95-49-84.0 1
4-Chlorotoluene ND ug/kg 04/24/18 15:10 106-43-44.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 15:10 96-12-84.0 1
Dibromochloromethane ND ug/kg 04/24/18 15:10 124-48-14.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 15:10 106-93-44.0 1
Dibromomethane ND ug/kg 04/24/18 15:10 74-95-34.0 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 15:10 95-50-14.0 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 15:10 541-73-14.0 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 15:10 106-46-74.0 1
Dichlorodifluoromethane ND ug/kg 04/24/18 15:10 75-71-87.9 1
1,1-Dichloroethane ND ug/kg 04/24/18 15:10 75-34-34.0 1
1,2-Dichloroethane ND ug/kg 04/24/18 15:10 107-06-24.0 1
1,1-Dichloroethene ND ug/kg 04/24/18 15:10 75-35-44.0 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 15:10 156-59-24.0 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 15:10 156-60-54.0 1
1,2-Dichloropropane ND ug/kg 04/24/18 15:10 78-87-54.0 1
1,3-Dichloropropane ND ug/kg 04/24/18 15:10 142-28-94.0 1
2,2-Dichloropropane ND ug/kg 04/24/18 15:10 594-20-74.0 1
1,1-Dichloropropene ND ug/kg 04/24/18 15:10 563-58-64.0 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 15:10 10061-01-54.0 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 15:10 10061-02-64.0 1
Diisopropyl ether ND ug/kg 04/24/18 15:10 108-20-34.0 1
Ethylbenzene ND ug/kg 04/24/18 15:10 100-41-44.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 15:10 87-68-34.0 1
2-Hexanone ND ug/kg 04/24/18 15:10 591-78-639.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 15:10 98-82-84.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-1 Lab ID:92381713005 Collected:04/18/18 02:55 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 15:10 99-87-64.0 1
Methylene Chloride ND ug/kg 04/24/18 15:10 75-09-215.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 15:10 108-10-139.7 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 15:10 1634-04-44.0 1
Naphthalene ND ug/kg 04/24/18 15:10 91-20-34.0 1
n-Propylbenzene ND ug/kg 04/24/18 15:10 103-65-14.0 1
Styrene ND ug/kg 04/24/18 15:10 100-42-54.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 15:10 630-20-64.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 15:10 79-34-54.0 1
Tetrachloroethene ND ug/kg 04/24/18 15:10 127-18-44.0 1
Toluene ND ug/kg 04/24/18 15:10 108-88-34.0 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 15:10 87-61-64.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 15:10 120-82-14.0 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 15:10 71-55-64.0 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 15:10 79-00-54.0 1
Trichloroethene ND ug/kg 04/24/18 15:10 79-01-64.0 1
Trichlorofluoromethane ND ug/kg 04/24/18 15:10 75-69-44.0 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 15:10 96-18-44.0 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 15:10 95-63-64.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 15:10 108-67-84.0 1
Vinyl acetate ND ug/kg 04/24/18 15:10 108-05-439.7 1
Vinyl chloride ND ug/kg 04/24/18 15:10 75-01-47.9 1
Xylene (Total)ND ug/kg 04/24/18 15:10 1330-20-77.9 1
m&p-Xylene ND ug/kg 04/24/18 15:10 179601-23-17.9 1
o-Xylene ND ug/kg 04/24/18 15:10 95-47-64.0 1
Surrogates
Toluene-d8 (S)110 %04/24/18 15:10 2037-26-5 IO70-130 1
4-Bromofluorobenzene (S)100 %04/24/18 15:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)124 %04/24/18 15:10 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.4 %04/23/18 10:260.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-2 Lab ID:92381713006 Collected:04/18/18 02:58 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 05/01/18 18:08 N205/01/18 06:5511.6 1
Aliphatic (C19-C36)ND mg/kg 05/01/18 18:08 N205/01/18 06:5511.6 1
Aromatic (C11-C22)ND mg/kg 05/01/18 18:08 N205/01/18 06:5511.6 1
Surrogates
Nonatriacontane (S)106 %05/01/18 18:08 7194-86-705/01/18 06:5540-140 1
o-Terphenyl (S)142 %05/01/18 18:08 84-15-1 S305/01/18 06:5540-140 1
2-Fluorobiphenyl (S)80 %05/01/18 18:08 321-60-805/01/18 06:5540-140 1
2-Bromonaphthalene (S)79 %05/01/18 18:08 580-13-205/01/18 06:5540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 19:53 N204/23/18 11:542.2 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 19:53 N204/23/18 11:542.2 1
Aromatic (C09-C10)ND mg/kg 04/23/18 19:53 N204/23/18 11:542.2 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %04/23/18 19:53 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)107 %04/23/18 19:53 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/26/18 01:44 83-32-904/21/18 14:303841
Acenaphthylene ND ug/kg 04/26/18 01:44 208-96-804/21/18 14:303841
Aniline ND ug/kg 04/26/18 01:44 62-53-304/21/18 14:303841
Anthracene ND ug/kg 04/26/18 01:44 120-12-704/21/18 14:303841
Benzo(a)anthracene ND ug/kg 04/26/18 01:44 56-55-304/21/18 14:303841
Benzo(a)pyrene ND ug/kg 04/26/18 01:44 50-32-804/21/18 14:303841
Benzo(b)fluoranthene ND ug/kg 04/26/18 01:44 205-99-204/21/18 14:303841
Benzo(g,h,i)perylene ND ug/kg 04/26/18 01:44 191-24-204/21/18 14:303841
Benzo(k)fluoranthene ND ug/kg 04/26/18 01:44 207-08-904/21/18 14:303841
Benzoic Acid ND ug/kg 04/26/18 01:44 65-85-004/21/18 14:3019201
Benzyl alcohol ND ug/kg 04/26/18 01:44 100-51-604/21/18 14:307681
4-Bromophenylphenyl ether ND ug/kg 04/26/18 01:44 101-55-304/21/18 14:303841
Butylbenzylphthalate ND ug/kg 04/26/18 01:44 85-68-704/21/18 14:303841
4-Chloro-3-methylphenol ND ug/kg 04/26/18 01:44 59-50-704/21/18 14:307681
4-Chloroaniline ND ug/kg 04/26/18 01:44 106-47-804/21/18 14:3019201
bis(2-Chloroethoxy)methane ND ug/kg 04/26/18 01:44 111-91-104/21/18 14:303841
bis(2-Chloroethyl) ether ND ug/kg 04/26/18 01:44 111-44-404/21/18 14:303841
2-Chloronaphthalene ND ug/kg 04/26/18 01:44 91-58-704/21/18 14:303841
2-Chlorophenol ND ug/kg 04/26/18 01:44 95-57-804/21/18 14:303841
4-Chlorophenylphenyl ether ND ug/kg 04/26/18 01:44 7005-72-304/21/18 14:303841
Chrysene ND ug/kg 04/26/18 01:44 218-01-904/21/18 14:303841
Dibenz(a,h)anthracene ND ug/kg 04/26/18 01:44 53-70-304/21/18 14:303841
Dibenzofuran ND ug/kg 04/26/18 01:44 132-64-904/21/18 14:303841
1,2-Dichlorobenzene ND ug/kg 04/26/18 01:44 95-50-104/21/18 14:303841
1,3-Dichlorobenzene ND ug/kg 04/26/18 01:44 541-73-104/21/18 14:303841
1,4-Dichlorobenzene ND ug/kg 04/26/18 01:44 106-46-704/21/18 14:303841
3,3'-Dichlorobenzidine ND ug/kg 04/26/18 01:44 91-94-104/21/18 14:3019201
2,4-Dichlorophenol ND ug/kg 04/26/18 01:44 120-83-204/21/18 14:303841
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-2 Lab ID:92381713006 Collected:04/18/18 02:58 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/26/18 01:44 84-66-204/21/18 14:303841
2,4-Dimethylphenol ND ug/kg 04/26/18 01:44 105-67-904/21/18 14:303841
Dimethylphthalate ND ug/kg 04/26/18 01:44 131-11-304/21/18 14:303841
Di-n-butylphthalate ND ug/kg 04/26/18 01:44 84-74-204/21/18 14:303841
4,6-Dinitro-2-methylphenol ND ug/kg 04/26/18 01:44 534-52-104/21/18 14:307681
2,4-Dinitrophenol ND ug/kg 04/26/18 01:44 51-28-504/21/18 14:3019201
2,4-Dinitrotoluene ND ug/kg 04/26/18 01:44 121-14-204/21/18 14:303841
2,6-Dinitrotoluene ND ug/kg 04/26/18 01:44 606-20-204/21/18 14:303841
Di-n-octylphthalate ND ug/kg 04/26/18 01:44 117-84-004/21/18 14:303841
bis(2-Ethylhexyl)phthalate ND ug/kg 04/26/18 01:44 117-81-704/21/18 14:303841
Fluoranthene ND ug/kg 04/26/18 01:44 206-44-004/21/18 14:303841
Fluorene ND ug/kg 04/26/18 01:44 86-73-704/21/18 14:303841
Hexachloro-1,3-butadiene ND ug/kg 04/26/18 01:44 87-68-304/21/18 14:303841
Hexachlorobenzene ND ug/kg 04/26/18 01:44 118-74-104/21/18 14:303841
Hexachlorocyclopentadiene ND ug/kg 04/26/18 01:44 77-47-404/21/18 14:303841
Hexachloroethane ND ug/kg 04/26/18 01:44 67-72-104/21/18 14:303841
Indeno(1,2,3-cd)pyrene ND ug/kg 04/26/18 01:44 193-39-504/21/18 14:303841
Isophorone ND ug/kg 04/26/18 01:44 78-59-104/21/18 14:303841
1-Methylnaphthalene ND ug/kg 04/26/18 01:44 90-12-004/21/18 14:303841
2-Methylnaphthalene ND ug/kg 04/26/18 01:44 91-57-604/21/18 14:303841
2-Methylphenol(o-Cresol)ND ug/kg 04/26/18 01:44 95-48-704/21/18 14:303841
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/26/18 01:44 15831-10-404/21/18 14:303841
Naphthalene ND ug/kg 04/26/18 01:44 91-20-304/21/18 14:303841
2-Nitroaniline ND ug/kg 04/26/18 01:44 88-74-404/21/18 14:3019201
3-Nitroaniline ND ug/kg 04/26/18 01:44 99-09-204/21/18 14:3019201
4-Nitroaniline ND ug/kg 04/26/18 01:44 100-01-604/21/18 14:307681
Nitrobenzene ND ug/kg 04/26/18 01:44 98-95-304/21/18 14:303841
2-Nitrophenol ND ug/kg 04/26/18 01:44 88-75-504/21/18 14:303841
4-Nitrophenol ND ug/kg 04/26/18 01:44 100-02-704/21/18 14:3019201
N-Nitrosodimethylamine ND ug/kg 04/26/18 01:44 62-75-904/21/18 14:303841
N-Nitroso-di-n-propylamine ND ug/kg 04/26/18 01:44 621-64-704/21/18 14:303841
N-Nitrosodiphenylamine ND ug/kg 04/26/18 01:44 86-30-604/21/18 14:303841
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/26/18 01:44 108-60-104/21/18 14:303841
Pentachlorophenol ND ug/kg 04/26/18 01:44 87-86-504/21/18 14:3019201
Phenanthrene ND ug/kg 04/26/18 01:44 85-01-804/21/18 14:303841
Phenol ND ug/kg 04/26/18 01:44 108-95-204/21/18 14:303841
Pyrene ND ug/kg 04/26/18 01:44 129-00-004/21/18 14:303841
1,2,4-Trichlorobenzene ND ug/kg 04/26/18 01:44 120-82-104/21/18 14:303841
2,4,5-Trichlorophenol ND ug/kg 04/26/18 01:44 95-95-404/21/18 14:303841
2,4,6-Trichlorophenol ND ug/kg 04/26/18 01:44 88-06-204/21/18 14:303841
Surrogates
Nitrobenzene-d5 (S)59 %04/26/18 01:44 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)48 %04/26/18 01:44 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)37 %04/26/18 01:44 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)52 %04/26/18 01:44 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)53 %04/26/18 01:44 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-2 Lab ID:92381713006 Collected:04/18/18 02:58 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)55 %04/26/18 01:44 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 162 ug/kg 04/24/18 15:30 67-64-185.9 1
Benzene ND ug/kg 04/24/18 15:30 71-43-24.3 1
Bromobenzene ND ug/kg 04/24/18 15:30 108-86-14.3 1
Bromochloromethane ND ug/kg 04/24/18 15:30 74-97-54.3 1
Bromodichloromethane ND ug/kg 04/24/18 15:30 75-27-44.3 1
Bromoform ND ug/kg 04/24/18 15:30 75-25-24.3 1
Bromomethane ND ug/kg 04/24/18 15:30 74-83-98.6 1
2-Butanone (MEK)ND ug/kg 04/24/18 15:30 78-93-385.9 1
n-Butylbenzene ND ug/kg 04/24/18 15:30 104-51-84.3 1
sec-Butylbenzene ND ug/kg 04/24/18 15:30 135-98-84.3 1
tert-Butylbenzene ND ug/kg 04/24/18 15:30 98-06-64.3 1
Carbon tetrachloride ND ug/kg 04/24/18 15:30 56-23-54.3 1
Chlorobenzene ND ug/kg 04/24/18 15:30 108-90-74.3 1
Chloroethane ND ug/kg 04/24/18 15:30 75-00-38.6 1
Chloroform ND ug/kg 04/24/18 15:30 67-66-34.3 1
Chloromethane ND ug/kg 04/24/18 15:30 74-87-38.6 1
2-Chlorotoluene ND ug/kg 04/24/18 15:30 95-49-84.3 1
4-Chlorotoluene ND ug/kg 04/24/18 15:30 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 15:30 96-12-84.3 1
Dibromochloromethane ND ug/kg 04/24/18 15:30 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 15:30 106-93-44.3 1
Dibromomethane ND ug/kg 04/24/18 15:30 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 15:30 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 15:30 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 15:30 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 04/24/18 15:30 75-71-88.6 1
1,1-Dichloroethane ND ug/kg 04/24/18 15:30 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 04/24/18 15:30 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 04/24/18 15:30 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 15:30 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 15:30 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 04/24/18 15:30 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 04/24/18 15:30 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 04/24/18 15:30 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 04/24/18 15:30 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 15:30 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 15:30 10061-02-64.3 1
Diisopropyl ether ND ug/kg 04/24/18 15:30 108-20-34.3 1
Ethylbenzene ND ug/kg 04/24/18 15:30 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 15:30 87-68-34.3 1
2-Hexanone ND ug/kg 04/24/18 15:30 591-78-642.9 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 15:30 98-82-84.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-2 Lab ID:92381713006 Collected:04/18/18 02:58 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 15:30 99-87-64.3 1
Methylene Chloride ND ug/kg 04/24/18 15:30 75-09-217.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 15:30 108-10-142.9 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 15:30 1634-04-44.3 1
Naphthalene ND ug/kg 04/24/18 15:30 91-20-34.3 1
n-Propylbenzene ND ug/kg 04/24/18 15:30 103-65-14.3 1
Styrene ND ug/kg 04/24/18 15:30 100-42-54.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 15:30 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 15:30 79-34-54.3 1
Tetrachloroethene ND ug/kg 04/24/18 15:30 127-18-44.3 1
Toluene ND ug/kg 04/24/18 15:30 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 15:30 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 15:30 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 15:30 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 15:30 79-00-54.3 1
Trichloroethene ND ug/kg 04/24/18 15:30 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 04/24/18 15:30 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 15:30 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 15:30 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 15:30 108-67-84.3 1
Vinyl acetate ND ug/kg 04/24/18 15:30 108-05-442.9 1
Vinyl chloride ND ug/kg 04/24/18 15:30 75-01-48.6 1
Xylene (Total)ND ug/kg 04/24/18 15:30 1330-20-78.6 1
m&p-Xylene ND ug/kg 04/24/18 15:30 179601-23-18.6 1
o-Xylene ND ug/kg 04/24/18 15:30 95-47-64.3 1
Surrogates
Toluene-d8 (S)121 %04/24/18 15:30 2037-26-5 IO70-130 1
4-Bromofluorobenzene (S)102 %04/24/18 15:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)130 %04/24/18 15:30 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.7 %04/23/18 10:270.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-3 Lab ID:92381713007 Collected:04/18/18 03:02 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 05/01/18 18:36 N205/01/18 06:5511.8 1
Aliphatic (C19-C36)ND mg/kg 05/01/18 18:36 N205/01/18 06:5511.8 1
Aromatic (C11-C22)ND mg/kg 05/01/18 18:36 N205/01/18 06:5511.8 1
Surrogates
Nonatriacontane (S)74 %05/01/18 18:36 7194-86-705/01/18 06:5540-140 1
o-Terphenyl (S)83 %05/01/18 18:36 84-15-105/01/18 06:5540-140 1
2-Fluorobiphenyl (S)80 %05/01/18 18:36 321-60-805/01/18 06:5540-140 1
2-Bromonaphthalene (S)82 %05/01/18 18:36 580-13-205/01/18 06:5540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 20:22 N204/23/18 11:542.3 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 20:22 N204/23/18 11:542.3 1
Aromatic (C09-C10)ND mg/kg 04/23/18 20:22 N204/23/18 11:542.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)108 %04/23/18 20:22 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)106 %04/23/18 20:22 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/26/18 02:12 83-32-904/21/18 14:303911
Acenaphthylene ND ug/kg 04/26/18 02:12 208-96-804/21/18 14:303911
Aniline ND ug/kg 04/26/18 02:12 62-53-304/21/18 14:303911
Anthracene ND ug/kg 04/26/18 02:12 120-12-704/21/18 14:303911
Benzo(a)anthracene ND ug/kg 04/26/18 02:12 56-55-304/21/18 14:303911
Benzo(a)pyrene ND ug/kg 04/26/18 02:12 50-32-804/21/18 14:303911
Benzo(b)fluoranthene ND ug/kg 04/26/18 02:12 205-99-204/21/18 14:303911
Benzo(g,h,i)perylene ND ug/kg 04/26/18 02:12 191-24-204/21/18 14:303911
Benzo(k)fluoranthene ND ug/kg 04/26/18 02:12 207-08-904/21/18 14:303911
Benzoic Acid ND ug/kg 04/26/18 02:12 65-85-004/21/18 14:3019601
Benzyl alcohol ND ug/kg 04/26/18 02:12 100-51-604/21/18 14:307831
4-Bromophenylphenyl ether ND ug/kg 04/26/18 02:12 101-55-304/21/18 14:303911
Butylbenzylphthalate ND ug/kg 04/26/18 02:12 85-68-704/21/18 14:303911
4-Chloro-3-methylphenol ND ug/kg 04/26/18 02:12 59-50-704/21/18 14:307831
4-Chloroaniline ND ug/kg 04/26/18 02:12 106-47-804/21/18 14:3019601
bis(2-Chloroethoxy)methane ND ug/kg 04/26/18 02:12 111-91-104/21/18 14:303911
bis(2-Chloroethyl) ether ND ug/kg 04/26/18 02:12 111-44-404/21/18 14:303911
2-Chloronaphthalene ND ug/kg 04/26/18 02:12 91-58-704/21/18 14:303911
2-Chlorophenol ND ug/kg 04/26/18 02:12 95-57-804/21/18 14:303911
4-Chlorophenylphenyl ether ND ug/kg 04/26/18 02:12 7005-72-304/21/18 14:303911
Chrysene ND ug/kg 04/26/18 02:12 218-01-904/21/18 14:303911
Dibenz(a,h)anthracene ND ug/kg 04/26/18 02:12 53-70-304/21/18 14:303911
Dibenzofuran ND ug/kg 04/26/18 02:12 132-64-904/21/18 14:303911
1,2-Dichlorobenzene ND ug/kg 04/26/18 02:12 95-50-104/21/18 14:303911
1,3-Dichlorobenzene ND ug/kg 04/26/18 02:12 541-73-104/21/18 14:303911
1,4-Dichlorobenzene ND ug/kg 04/26/18 02:12 106-46-704/21/18 14:303911
3,3'-Dichlorobenzidine ND ug/kg 04/26/18 02:12 91-94-104/21/18 14:3019601
2,4-Dichlorophenol ND ug/kg 04/26/18 02:12 120-83-204/21/18 14:303911
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-3 Lab ID:92381713007 Collected:04/18/18 03:02 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/26/18 02:12 84-66-204/21/18 14:303911
2,4-Dimethylphenol ND ug/kg 04/26/18 02:12 105-67-904/21/18 14:303911
Dimethylphthalate ND ug/kg 04/26/18 02:12 131-11-304/21/18 14:303911
Di-n-butylphthalate ND ug/kg 04/26/18 02:12 84-74-204/21/18 14:303911
4,6-Dinitro-2-methylphenol ND ug/kg 04/26/18 02:12 534-52-104/21/18 14:307831
2,4-Dinitrophenol ND ug/kg 04/26/18 02:12 51-28-504/21/18 14:3019601
2,4-Dinitrotoluene ND ug/kg 04/26/18 02:12 121-14-204/21/18 14:303911
2,6-Dinitrotoluene ND ug/kg 04/26/18 02:12 606-20-204/21/18 14:303911
Di-n-octylphthalate ND ug/kg 04/26/18 02:12 117-84-004/21/18 14:303911
bis(2-Ethylhexyl)phthalate ND ug/kg 04/26/18 02:12 117-81-704/21/18 14:303911
Fluoranthene ND ug/kg 04/26/18 02:12 206-44-004/21/18 14:303911
Fluorene ND ug/kg 04/26/18 02:12 86-73-704/21/18 14:303911
Hexachloro-1,3-butadiene ND ug/kg 04/26/18 02:12 87-68-304/21/18 14:303911
Hexachlorobenzene ND ug/kg 04/26/18 02:12 118-74-104/21/18 14:303911
Hexachlorocyclopentadiene ND ug/kg 04/26/18 02:12 77-47-404/21/18 14:303911
Hexachloroethane ND ug/kg 04/26/18 02:12 67-72-104/21/18 14:303911
Indeno(1,2,3-cd)pyrene ND ug/kg 04/26/18 02:12 193-39-504/21/18 14:303911
Isophorone ND ug/kg 04/26/18 02:12 78-59-104/21/18 14:303911
1-Methylnaphthalene ND ug/kg 04/26/18 02:12 90-12-004/21/18 14:303911
2-Methylnaphthalene ND ug/kg 04/26/18 02:12 91-57-604/21/18 14:303911
2-Methylphenol(o-Cresol)ND ug/kg 04/26/18 02:12 95-48-704/21/18 14:303911
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/26/18 02:12 15831-10-404/21/18 14:303911
Naphthalene ND ug/kg 04/26/18 02:12 91-20-304/21/18 14:303911
2-Nitroaniline ND ug/kg 04/26/18 02:12 88-74-404/21/18 14:3019601
3-Nitroaniline ND ug/kg 04/26/18 02:12 99-09-204/21/18 14:3019601
4-Nitroaniline ND ug/kg 04/26/18 02:12 100-01-604/21/18 14:307831
Nitrobenzene ND ug/kg 04/26/18 02:12 98-95-304/21/18 14:303911
2-Nitrophenol ND ug/kg 04/26/18 02:12 88-75-504/21/18 14:303911
4-Nitrophenol ND ug/kg 04/26/18 02:12 100-02-704/21/18 14:3019601
N-Nitrosodimethylamine ND ug/kg 04/26/18 02:12 62-75-904/21/18 14:303911
N-Nitroso-di-n-propylamine ND ug/kg 04/26/18 02:12 621-64-704/21/18 14:303911
N-Nitrosodiphenylamine ND ug/kg 04/26/18 02:12 86-30-604/21/18 14:303911
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/26/18 02:12 108-60-104/21/18 14:303911
Pentachlorophenol ND ug/kg 04/26/18 02:12 87-86-504/21/18 14:3019601
Phenanthrene ND ug/kg 04/26/18 02:12 85-01-804/21/18 14:303911
Phenol ND ug/kg 04/26/18 02:12 108-95-204/21/18 14:303911
Pyrene ND ug/kg 04/26/18 02:12 129-00-004/21/18 14:303911
1,2,4-Trichlorobenzene ND ug/kg 04/26/18 02:12 120-82-104/21/18 14:303911
2,4,5-Trichlorophenol ND ug/kg 04/26/18 02:12 95-95-404/21/18 14:303911
2,4,6-Trichlorophenol ND ug/kg 04/26/18 02:12 88-06-204/21/18 14:303911
Surrogates
Nitrobenzene-d5 (S)60 %04/26/18 02:12 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)56 %04/26/18 02:12 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)50 %04/26/18 02:12 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)52 %04/26/18 02:12 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)50 %04/26/18 02:12 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-3 Lab ID:92381713007 Collected:04/18/18 03:02 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)62 %04/26/18 02:12 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 15:50 67-64-190.2 1
Benzene ND ug/kg 04/24/18 15:50 71-43-24.5 1
Bromobenzene ND ug/kg 04/24/18 15:50 108-86-14.5 1
Bromochloromethane ND ug/kg 04/24/18 15:50 74-97-54.5 1
Bromodichloromethane ND ug/kg 04/24/18 15:50 75-27-44.5 1
Bromoform ND ug/kg 04/24/18 15:50 75-25-24.5 1
Bromomethane ND ug/kg 04/24/18 15:50 74-83-99.0 1
2-Butanone (MEK)ND ug/kg 04/24/18 15:50 78-93-390.2 1
n-Butylbenzene ND ug/kg 04/24/18 15:50 104-51-84.5 1
sec-Butylbenzene ND ug/kg 04/24/18 15:50 135-98-84.5 1
tert-Butylbenzene ND ug/kg 04/24/18 15:50 98-06-64.5 1
Carbon tetrachloride ND ug/kg 04/24/18 15:50 56-23-54.5 1
Chlorobenzene ND ug/kg 04/24/18 15:50 108-90-74.5 1
Chloroethane ND ug/kg 04/24/18 15:50 75-00-39.0 1
Chloroform ND ug/kg 04/24/18 15:50 67-66-34.5 1
Chloromethane ND ug/kg 04/24/18 15:50 74-87-39.0 1
2-Chlorotoluene ND ug/kg 04/24/18 15:50 95-49-84.5 1
4-Chlorotoluene ND ug/kg 04/24/18 15:50 106-43-44.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 15:50 96-12-84.5 1
Dibromochloromethane ND ug/kg 04/24/18 15:50 124-48-14.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 15:50 106-93-44.5 1
Dibromomethane ND ug/kg 04/24/18 15:50 74-95-34.5 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 15:50 95-50-14.5 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 15:50 541-73-14.5 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 15:50 106-46-74.5 1
Dichlorodifluoromethane ND ug/kg 04/24/18 15:50 75-71-89.0 1
1,1-Dichloroethane ND ug/kg 04/24/18 15:50 75-34-34.5 1
1,2-Dichloroethane ND ug/kg 04/24/18 15:50 107-06-24.5 1
1,1-Dichloroethene ND ug/kg 04/24/18 15:50 75-35-44.5 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 15:50 156-59-24.5 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 15:50 156-60-54.5 1
1,2-Dichloropropane ND ug/kg 04/24/18 15:50 78-87-54.5 1
1,3-Dichloropropane ND ug/kg 04/24/18 15:50 142-28-94.5 1
2,2-Dichloropropane ND ug/kg 04/24/18 15:50 594-20-74.5 1
1,1-Dichloropropene ND ug/kg 04/24/18 15:50 563-58-64.5 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 15:50 10061-01-54.5 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 15:50 10061-02-64.5 1
Diisopropyl ether ND ug/kg 04/24/18 15:50 108-20-34.5 1
Ethylbenzene ND ug/kg 04/24/18 15:50 100-41-44.5 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 15:50 87-68-34.5 1
2-Hexanone ND ug/kg 04/24/18 15:50 591-78-645.1 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 15:50 98-82-84.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-3 Lab ID:92381713007 Collected:04/18/18 03:02 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 15:50 99-87-64.5 1
Methylene Chloride ND ug/kg 04/24/18 15:50 75-09-218.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 15:50 108-10-145.1 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 15:50 1634-04-44.5 1
Naphthalene ND ug/kg 04/24/18 15:50 91-20-34.5 1
n-Propylbenzene ND ug/kg 04/24/18 15:50 103-65-14.5 1
Styrene ND ug/kg 04/24/18 15:50 100-42-54.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 15:50 630-20-64.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 15:50 79-34-54.5 1
Tetrachloroethene ND ug/kg 04/24/18 15:50 127-18-44.5 1
Toluene ND ug/kg 04/24/18 15:50 108-88-34.5 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 15:50 87-61-64.5 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 15:50 120-82-14.5 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 15:50 71-55-64.5 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 15:50 79-00-54.5 1
Trichloroethene ND ug/kg 04/24/18 15:50 79-01-64.5 1
Trichlorofluoromethane ND ug/kg 04/24/18 15:50 75-69-44.5 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 15:50 96-18-44.5 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 15:50 95-63-64.5 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 15:50 108-67-84.5 1
Vinyl acetate ND ug/kg 04/24/18 15:50 108-05-445.1 1
Vinyl chloride ND ug/kg 04/24/18 15:50 75-01-49.0 1
Xylene (Total)ND ug/kg 04/24/18 15:50 1330-20-79.0 1
m&p-Xylene ND ug/kg 04/24/18 15:50 179601-23-19.0 1
o-Xylene ND ug/kg 04/24/18 15:50 95-47-64.5 1
Surrogates
Toluene-d8 (S)105 %04/24/18 15:50 2037-26-570-130 1
4-Bromofluorobenzene (S)94 %04/24/18 15:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %04/24/18 15:50 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.8 %04/23/18 10:270.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-4 Lab ID:92381713008 Collected:04/18/18 03:05 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 05/01/18 19:04 N205/01/18 06:5511.7 1
Aliphatic (C19-C36)ND mg/kg 05/01/18 19:04 N205/01/18 06:5511.7 1
Aromatic (C11-C22)ND mg/kg 05/01/18 19:04 N205/01/18 06:5511.7 1
Surrogates
Nonatriacontane (S)40 %05/01/18 19:04 7194-86-705/01/18 06:5540-140 1
o-Terphenyl (S)48 %05/01/18 19:04 84-15-105/01/18 06:5540-140 1
2-Fluorobiphenyl (S)73 %05/01/18 19:04 321-60-805/01/18 06:5540-140 1
2-Bromonaphthalene (S)74 %05/01/18 19:04 580-13-205/01/18 06:5540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 04/23/18 20:50 N204/23/18 11:542.3 1
Aliphatic (C09-C12)ND mg/kg 04/23/18 20:50 N204/23/18 11:542.3 1
Aromatic (C09-C10)ND mg/kg 04/23/18 20:50 N204/23/18 11:542.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)107 %04/23/18 20:50 460-00-404/23/18 11:5470-130 1
4-Bromofluorobenzene (PID) (S)106 %04/23/18 20:50 460-00-404/23/18 11:5470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 04/26/18 02:41 83-32-904/21/18 14:303901
Acenaphthylene ND ug/kg 04/26/18 02:41 208-96-804/21/18 14:303901
Aniline ND ug/kg 04/26/18 02:41 62-53-304/21/18 14:303901
Anthracene ND ug/kg 04/26/18 02:41 120-12-704/21/18 14:303901
Benzo(a)anthracene ND ug/kg 04/26/18 02:41 56-55-304/21/18 14:303901
Benzo(a)pyrene ND ug/kg 04/26/18 02:41 50-32-804/21/18 14:303901
Benzo(b)fluoranthene ND ug/kg 04/26/18 02:41 205-99-204/21/18 14:303901
Benzo(g,h,i)perylene ND ug/kg 04/26/18 02:41 191-24-204/21/18 14:303901
Benzo(k)fluoranthene ND ug/kg 04/26/18 02:41 207-08-904/21/18 14:303901
Benzoic Acid ND ug/kg 04/26/18 02:41 65-85-004/21/18 14:3019501
Benzyl alcohol ND ug/kg 04/26/18 02:41 100-51-604/21/18 14:307811
4-Bromophenylphenyl ether ND ug/kg 04/26/18 02:41 101-55-304/21/18 14:303901
Butylbenzylphthalate ND ug/kg 04/26/18 02:41 85-68-704/21/18 14:303901
4-Chloro-3-methylphenol ND ug/kg 04/26/18 02:41 59-50-704/21/18 14:307811
4-Chloroaniline ND ug/kg 04/26/18 02:41 106-47-804/21/18 14:3019501
bis(2-Chloroethoxy)methane ND ug/kg 04/26/18 02:41 111-91-104/21/18 14:303901
bis(2-Chloroethyl) ether ND ug/kg 04/26/18 02:41 111-44-404/21/18 14:303901
2-Chloronaphthalene ND ug/kg 04/26/18 02:41 91-58-704/21/18 14:303901
2-Chlorophenol ND ug/kg 04/26/18 02:41 95-57-804/21/18 14:303901
4-Chlorophenylphenyl ether ND ug/kg 04/26/18 02:41 7005-72-304/21/18 14:303901
Chrysene ND ug/kg 04/26/18 02:41 218-01-904/21/18 14:303901
Dibenz(a,h)anthracene ND ug/kg 04/26/18 02:41 53-70-304/21/18 14:303901
Dibenzofuran ND ug/kg 04/26/18 02:41 132-64-904/21/18 14:303901
1,2-Dichlorobenzene ND ug/kg 04/26/18 02:41 95-50-104/21/18 14:303901
1,3-Dichlorobenzene ND ug/kg 04/26/18 02:41 541-73-104/21/18 14:303901
1,4-Dichlorobenzene ND ug/kg 04/26/18 02:41 106-46-704/21/18 14:303901
3,3'-Dichlorobenzidine ND ug/kg 04/26/18 02:41 91-94-104/21/18 14:3019501
2,4-Dichlorophenol ND ug/kg 04/26/18 02:41 120-83-204/21/18 14:303901
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-4 Lab ID:92381713008 Collected:04/18/18 03:05 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 04/26/18 02:41 84-66-204/21/18 14:303901
2,4-Dimethylphenol ND ug/kg 04/26/18 02:41 105-67-904/21/18 14:303901
Dimethylphthalate ND ug/kg 04/26/18 02:41 131-11-304/21/18 14:303901
Di-n-butylphthalate ND ug/kg 04/26/18 02:41 84-74-204/21/18 14:303901
4,6-Dinitro-2-methylphenol ND ug/kg 04/26/18 02:41 534-52-104/21/18 14:307811
2,4-Dinitrophenol ND ug/kg 04/26/18 02:41 51-28-504/21/18 14:3019501
2,4-Dinitrotoluene ND ug/kg 04/26/18 02:41 121-14-204/21/18 14:303901
2,6-Dinitrotoluene ND ug/kg 04/26/18 02:41 606-20-204/21/18 14:303901
Di-n-octylphthalate ND ug/kg 04/26/18 02:41 117-84-004/21/18 14:303901
bis(2-Ethylhexyl)phthalate ND ug/kg 04/26/18 02:41 117-81-704/21/18 14:303901
Fluoranthene ND ug/kg 04/26/18 02:41 206-44-004/21/18 14:303901
Fluorene ND ug/kg 04/26/18 02:41 86-73-704/21/18 14:303901
Hexachloro-1,3-butadiene ND ug/kg 04/26/18 02:41 87-68-304/21/18 14:303901
Hexachlorobenzene ND ug/kg 04/26/18 02:41 118-74-104/21/18 14:303901
Hexachlorocyclopentadiene ND ug/kg 04/26/18 02:41 77-47-404/21/18 14:303901
Hexachloroethane ND ug/kg 04/26/18 02:41 67-72-104/21/18 14:303901
Indeno(1,2,3-cd)pyrene ND ug/kg 04/26/18 02:41 193-39-504/21/18 14:303901
Isophorone ND ug/kg 04/26/18 02:41 78-59-104/21/18 14:303901
1-Methylnaphthalene ND ug/kg 04/26/18 02:41 90-12-004/21/18 14:303901
2-Methylnaphthalene ND ug/kg 04/26/18 02:41 91-57-604/21/18 14:303901
2-Methylphenol(o-Cresol)ND ug/kg 04/26/18 02:41 95-48-704/21/18 14:303901
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/26/18 02:41 15831-10-404/21/18 14:303901
Naphthalene ND ug/kg 04/26/18 02:41 91-20-304/21/18 14:303901
2-Nitroaniline ND ug/kg 04/26/18 02:41 88-74-404/21/18 14:3019501
3-Nitroaniline ND ug/kg 04/26/18 02:41 99-09-204/21/18 14:3019501
4-Nitroaniline ND ug/kg 04/26/18 02:41 100-01-604/21/18 14:307811
Nitrobenzene ND ug/kg 04/26/18 02:41 98-95-304/21/18 14:303901
2-Nitrophenol ND ug/kg 04/26/18 02:41 88-75-504/21/18 14:303901
4-Nitrophenol ND ug/kg 04/26/18 02:41 100-02-704/21/18 14:3019501
N-Nitrosodimethylamine ND ug/kg 04/26/18 02:41 62-75-904/21/18 14:303901
N-Nitroso-di-n-propylamine ND ug/kg 04/26/18 02:41 621-64-704/21/18 14:303901
N-Nitrosodiphenylamine ND ug/kg 04/26/18 02:41 86-30-604/21/18 14:303901
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/26/18 02:41 108-60-104/21/18 14:303901
Pentachlorophenol ND ug/kg 04/26/18 02:41 87-86-504/21/18 14:3019501
Phenanthrene ND ug/kg 04/26/18 02:41 85-01-804/21/18 14:303901
Phenol ND ug/kg 04/26/18 02:41 108-95-204/21/18 14:303901
Pyrene ND ug/kg 04/26/18 02:41 129-00-004/21/18 14:303901
1,2,4-Trichlorobenzene ND ug/kg 04/26/18 02:41 120-82-104/21/18 14:303901
2,4,5-Trichlorophenol ND ug/kg 04/26/18 02:41 95-95-404/21/18 14:303901
2,4,6-Trichlorophenol ND ug/kg 04/26/18 02:41 88-06-204/21/18 14:303901
Surrogates
Nitrobenzene-d5 (S)56 %04/26/18 02:41 4165-60-004/21/18 14:3023-110 1
2-Fluorobiphenyl (S)51 %04/26/18 02:41 321-60-804/21/18 14:3030-110 1
Terphenyl-d14 (S)35 %04/26/18 02:41 1718-51-004/21/18 14:3028-110 1
Phenol-d6 (S)52 %04/26/18 02:41 13127-88-304/21/18 14:3022-110 1
2-Fluorophenol (S)53 %04/26/18 02:41 367-12-404/21/18 14:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-4 Lab ID:92381713008 Collected:04/18/18 03:05 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)55 %04/26/18 02:41 118-79-604/21/18 14:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 04/24/18 16:11 67-64-185.2 1
Benzene ND ug/kg 04/24/18 16:11 71-43-24.3 1
Bromobenzene ND ug/kg 04/24/18 16:11 108-86-14.3 1
Bromochloromethane ND ug/kg 04/24/18 16:11 74-97-54.3 1
Bromodichloromethane ND ug/kg 04/24/18 16:11 75-27-44.3 1
Bromoform ND ug/kg 04/24/18 16:11 75-25-24.3 1
Bromomethane ND ug/kg 04/24/18 16:11 74-83-98.5 1
2-Butanone (MEK)ND ug/kg 04/24/18 16:11 78-93-385.2 1
n-Butylbenzene ND ug/kg 04/24/18 16:11 104-51-84.3 1
sec-Butylbenzene ND ug/kg 04/24/18 16:11 135-98-84.3 1
tert-Butylbenzene ND ug/kg 04/24/18 16:11 98-06-64.3 1
Carbon tetrachloride ND ug/kg 04/24/18 16:11 56-23-54.3 1
Chlorobenzene ND ug/kg 04/24/18 16:11 108-90-74.3 1
Chloroethane ND ug/kg 04/24/18 16:11 75-00-38.5 1
Chloroform ND ug/kg 04/24/18 16:11 67-66-34.3 1
Chloromethane ND ug/kg 04/24/18 16:11 74-87-38.5 1
2-Chlorotoluene ND ug/kg 04/24/18 16:11 95-49-84.3 1
4-Chlorotoluene ND ug/kg 04/24/18 16:11 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/24/18 16:11 96-12-84.3 1
Dibromochloromethane ND ug/kg 04/24/18 16:11 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 04/24/18 16:11 106-93-44.3 1
Dibromomethane ND ug/kg 04/24/18 16:11 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 04/24/18 16:11 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 04/24/18 16:11 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 04/24/18 16:11 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 04/24/18 16:11 75-71-88.5 1
1,1-Dichloroethane ND ug/kg 04/24/18 16:11 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 04/24/18 16:11 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 04/24/18 16:11 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 04/24/18 16:11 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 04/24/18 16:11 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 04/24/18 16:11 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 04/24/18 16:11 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 04/24/18 16:11 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 04/24/18 16:11 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 04/24/18 16:11 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 04/24/18 16:11 10061-02-64.3 1
Diisopropyl ether ND ug/kg 04/24/18 16:11 108-20-34.3 1
Ethylbenzene ND ug/kg 04/24/18 16:11 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/24/18 16:11 87-68-34.3 1
2-Hexanone ND ug/kg 04/24/18 16:11 591-78-642.6 1
Isopropylbenzene (Cumene)ND ug/kg 04/24/18 16:11 98-82-84.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 59
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92381713
3201 Charles
Sample:HT-SW-4 Lab ID:92381713008 Collected:04/18/18 03:05 Received:04/20/18 09:34 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 04/24/18 16:11 99-87-64.3 1
Methylene Chloride ND ug/kg 04/24/18 16:11 75-09-217.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/24/18 16:11 108-10-142.6 1
Methyl-tert-butyl ether ND ug/kg 04/24/18 16:11 1634-04-44.3 1
Naphthalene ND ug/kg 04/24/18 16:11 91-20-34.3 1
n-Propylbenzene ND ug/kg 04/24/18 16:11 103-65-14.3 1
Styrene ND ug/kg 04/24/18 16:11 100-42-54.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/24/18 16:11 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/24/18 16:11 79-34-54.3 1
Tetrachloroethene ND ug/kg 04/24/18 16:11 127-18-44.3 1
Toluene ND ug/kg 04/24/18 16:11 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/24/18 16:11 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 04/24/18 16:11 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 04/24/18 16:11 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 04/24/18 16:11 79-00-54.3 1
Trichloroethene ND ug/kg 04/24/18 16:11 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 04/24/18 16:11 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 04/24/18 16:11 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 04/24/18 16:11 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 04/24/18 16:11 108-67-84.3 1
Vinyl acetate ND ug/kg 04/24/18 16:11 108-05-442.6 1
Vinyl chloride ND ug/kg 04/24/18 16:11 75-01-48.5 1
Xylene (Total)ND ug/kg 04/24/18 16:11 1330-20-78.5 1
m&p-Xylene ND ug/kg 04/24/18 16:11 179601-23-18.5 1
o-Xylene ND ug/kg 04/24/18 16:11 95-47-64.3 1
Surrogates
Toluene-d8 (S)105 %04/24/18 16:11 2037-26-570-130 1
4-Bromofluorobenzene (S)92 %04/24/18 16:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)81 %04/24/18 16:11 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.5 %04/23/18 10:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407472
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2260769
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N204/23/18 17:04
Aliphatic (C09-C12)mg/kg ND 2.5 N204/23/18 17:04
Aromatic (C09-C10)mg/kg ND 2.5 N204/23/18 17:04
4-Bromofluorobenzene (FID) (S)%108 70-130 04/23/18 17:04
4-Bromofluorobenzene (PID) (S)%107 70-130 04/23/18 17:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2260770LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2260771
Aliphatic (C05-C08)mg/kg 14.2 N2159570-1309514.3 1 25
Aliphatic (C09-C12)mg/kg 15.4 N21510230-13010315.4 0 25
Aromatic (C09-C10)mg/kg 5.2 N2510470-1301055.3 1 25
4-Bromofluorobenzene (FID) (S)%111 70-130108
4-Bromofluorobenzene (PID) (S)%112 70-130110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407655
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2261803
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.9 04/24/18 12:06
1,1,1-Trichloroethane ug/kg ND 4.9 04/24/18 12:06
1,1,2,2-Tetrachloroethane ug/kg ND 4.9 04/24/18 12:06
1,1,2-Trichloroethane ug/kg ND 4.9 04/24/18 12:06
1,1-Dichloroethane ug/kg ND 4.9 04/24/18 12:06
1,1-Dichloroethene ug/kg ND 4.9 04/24/18 12:06
1,1-Dichloropropene ug/kg ND 4.9 04/24/18 12:06
1,2,3-Trichlorobenzene ug/kg ND 4.9 04/24/18 12:06
1,2,3-Trichloropropane ug/kg ND 4.9 04/24/18 12:06
1,2,4-Trichlorobenzene ug/kg ND 4.9 04/24/18 12:06
1,2,4-Trimethylbenzene ug/kg ND 4.9 04/24/18 12:06
1,2-Dibromo-3-chloropropane ug/kg ND 4.9 04/24/18 12:06
1,2-Dibromoethane (EDB)ug/kg ND 4.9 04/24/18 12:06
1,2-Dichlorobenzene ug/kg ND 4.9 04/24/18 12:06
1,2-Dichloroethane ug/kg ND 4.9 04/24/18 12:06
1,2-Dichloropropane ug/kg ND 4.9 04/24/18 12:06
1,3,5-Trimethylbenzene ug/kg ND 4.9 04/24/18 12:06
1,3-Dichlorobenzene ug/kg ND 4.9 04/24/18 12:06
1,3-Dichloropropane ug/kg ND 4.9 04/24/18 12:06
1,4-Dichlorobenzene ug/kg ND 4.9 04/24/18 12:06
2,2-Dichloropropane ug/kg ND 4.9 04/24/18 12:06
2-Butanone (MEK)ug/kg ND 98.2 04/24/18 12:06
2-Chlorotoluene ug/kg ND 4.9 04/24/18 12:06
2-Hexanone ug/kg ND 49.1 04/24/18 12:06
4-Chlorotoluene ug/kg ND 4.9 04/24/18 12:06
4-Methyl-2-pentanone (MIBK)ug/kg ND 49.1 04/24/18 12:06
Acetone ug/kg ND 98.2 04/24/18 12:06
Benzene ug/kg ND 4.9 04/24/18 12:06
Bromobenzene ug/kg ND 4.9 04/24/18 12:06
Bromochloromethane ug/kg ND 4.9 04/24/18 12:06
Bromodichloromethane ug/kg ND 4.9 04/24/18 12:06
Bromoform ug/kg ND 4.9 04/24/18 12:06
Bromomethane ug/kg ND 9.8 04/24/18 12:06
Carbon tetrachloride ug/kg ND 4.9 04/24/18 12:06
Chlorobenzene ug/kg ND 4.9 04/24/18 12:06
Chloroethane ug/kg ND 9.8 04/24/18 12:06
Chloroform ug/kg ND 4.9 04/24/18 12:06
Chloromethane ug/kg ND 9.8 04/24/18 12:06
cis-1,2-Dichloroethene ug/kg ND 4.9 04/24/18 12:06
cis-1,3-Dichloropropene ug/kg ND 4.9 04/24/18 12:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
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Page 38 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2261803
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 4.9 04/24/18 12:06
Dibromomethane ug/kg ND 4.9 04/24/18 12:06
Dichlorodifluoromethane ug/kg ND 9.8 04/24/18 12:06
Diisopropyl ether ug/kg ND 4.9 04/24/18 12:06
Ethylbenzene ug/kg ND 4.9 04/24/18 12:06
Hexachloro-1,3-butadiene ug/kg ND 4.9 04/24/18 12:06
Isopropylbenzene (Cumene)ug/kg ND 4.9 04/24/18 12:06
m&p-Xylene ug/kg ND 9.8 04/24/18 12:06
Methyl-tert-butyl ether ug/kg ND 4.9 04/24/18 12:06
Methylene Chloride ug/kg ND 19.6 04/24/18 12:06
n-Butylbenzene ug/kg ND 4.9 04/24/18 12:06
n-Propylbenzene ug/kg ND 4.9 04/24/18 12:06
Naphthalene ug/kg ND 4.9 04/24/18 12:06
o-Xylene ug/kg ND 4.9 04/24/18 12:06
p-Isopropyltoluene ug/kg ND 4.9 04/24/18 12:06
sec-Butylbenzene ug/kg ND 4.9 04/24/18 12:06
Styrene ug/kg ND 4.9 04/24/18 12:06
tert-Butylbenzene ug/kg ND 4.9 04/24/18 12:06
Tetrachloroethene ug/kg ND 4.9 04/24/18 12:06
Toluene ug/kg ND 4.9 04/24/18 12:06
trans-1,2-Dichloroethene ug/kg ND 4.9 04/24/18 12:06
trans-1,3-Dichloropropene ug/kg ND 4.9 04/24/18 12:06
Trichloroethene ug/kg ND 4.9 04/24/18 12:06
Trichlorofluoromethane ug/kg ND 4.9 04/24/18 12:06
Vinyl acetate ug/kg ND 49.1 04/24/18 12:06
Vinyl chloride ug/kg ND 9.8 04/24/18 12:06
Xylene (Total)ug/kg ND 9.8 04/24/18 12:06
1,2-Dichloroethane-d4 (S)%82 70-132 04/24/18 12:06
4-Bromofluorobenzene (S)%96 70-130 04/24/18 12:06
Toluene-d8 (S)%106 70-130 04/24/18 12:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2261804LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.655.2 95 74-137
1,1,1-Trichloroethane ug/kg 44.255.2 80 67-140
1,1,2,2-Tetrachloroethane ug/kg 40.255.2 73 72-141
1,1,2-Trichloroethane ug/kg 49.155.2 89 78-138
1,1-Dichloroethane ug/kg 46.955.2 85 69-134
1,1-Dichloroethene ug/kg 46.455.2 84 67-138
1,1-Dichloropropene ug/kg 47.355.2 86 69-139
1,2,3-Trichlorobenzene ug/kg 50.755.2 92 70-146
1,2,3-Trichloropropane ug/kg 47.855.2 87 69-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2261804LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 53.055.2 96 68-148
1,2,4-Trimethylbenzene ug/kg 52.055.2 94 74-137
1,2-Dibromo-3-chloropropane ug/kg 45.155.2 82 65-140
1,2-Dibromoethane (EDB)ug/kg 50.955.2 92 77-135
1,2-Dichlorobenzene ug/kg 50.655.2 92 77-141
1,2-Dichloroethane ug/kg 43.555.2 79 65-137
1,2-Dichloropropane ug/kg 47.655.2 86 72-136
1,3,5-Trimethylbenzene ug/kg 51.955.2 94 76-133
1,3-Dichlorobenzene ug/kg 51.155.2 93 74-138
1,3-Dichloropropane ug/kg 50.955.2 92 71-139
1,4-Dichlorobenzene ug/kg 50.955.2 92 76-138
2,2-Dichloropropane ug/kg 45.955.2 83 68-137
2-Butanone (MEK)ug/kg 101J110 92 58-147
2-Chlorotoluene ug/kg 50.455.2 91 73-139
2-Hexanone ug/kg 106110 96 62-145
4-Chlorotoluene ug/kg 51.655.2 94 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 102110 92 64-149
Acetone ug/kg 126110 114 53-153
Benzene ug/kg 49.355.2 89 73-135
Bromobenzene ug/kg 51.355.2 93 75-133
Bromochloromethane ug/kg 44.355.2 80 73-134
Bromodichloromethane ug/kg 48.855.2 88 71-135
Bromoform ug/kg 45.655.2 83 66-141
Bromomethane ug/kg 45.555.2 82 53-160
Carbon tetrachloride ug/kg 47.855.2 87 60-145
Chlorobenzene ug/kg 48.755.2 88 78-130
Chloroethane ug/kg 38.955.2 71 64-149
Chloroform ug/kg 45.455.2 82 70-134
Chloromethane ug/kg 40.155.2 73 52-150
cis-1,2-Dichloroethene ug/kg 48.355.2 88 70-133
cis-1,3-Dichloropropene ug/kg 52.455.2 95 68-134
Dibromochloromethane ug/kg 50.255.2 91 71-138
Dibromomethane ug/kg 46.855.2 85 74-130
Dichlorodifluoromethane ug/kg 39.155.2 71 40-160
Diisopropyl ether ug/kg 49.655.2 90 69-141
Ethylbenzene ug/kg 49.755.2 90 75-133
Hexachloro-1,3-butadiene ug/kg 51.655.2 94 68-143
Isopropylbenzene (Cumene)ug/kg 51.655.2 93 76-143
m&p-Xylene ug/kg 101110 91 75-136
Methyl-tert-butyl ether ug/kg 46.555.2 84 68-144
Methylene Chloride ug/kg 45.155.2 82 45-154
n-Butylbenzene ug/kg 52.055.2 94 72-137
n-Propylbenzene ug/kg 51.255.2 93 76-136
Naphthalene ug/kg 47.755.2 86 68-151
o-Xylene ug/kg 51.955.2 94 76-141
p-Isopropyltoluene ug/kg 50.755.2 92 76-140
sec-Butylbenzene ug/kg 50.955.2 92 79-139
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2261804LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene ug/kg 51.055.2 92 79-137
tert-Butylbenzene ug/kg 46.455.2 84 74-143
Tetrachloroethene ug/kg 44.855.2 81 71-138
Toluene ug/kg 47.655.2 86 74-131
trans-1,2-Dichloroethene ug/kg 48.455.2 88 67-135
trans-1,3-Dichloropropene ug/kg 50.755.2 92 65-146
Trichloroethene ug/kg 58.555.2 106 67-135
Trichlorofluoromethane ug/kg 43.055.2 78 59-144
Vinyl acetate ug/kg 46.9J110 43 40-160
Vinyl chloride ug/kg 44.455.2 80 56-141
Xylene (Total)ug/kg 153166 92 76-137
1,2-Dichloroethane-d4 (S)%83 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2262223MATRIX SPIKE SAMPLE:
MSSpike
Result
92381713001
1,1,1,2-Tetrachloroethane ug/kg 27.130 90 70-130ND
1,1,1-Trichloroethane ug/kg 27.830 93 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 25.630 86 70-130ND
1,1,2-Trichloroethane ug/kg 27.630 92 70-130ND
1,1-Dichloroethane ug/kg 30.130 101 70-130ND
1,1-Dichloroethene ug/kg 29.730 99 49-180ND
1,1-Dichloropropene ug/kg 28.230 94 70-130ND
1,2,3-Trichlorobenzene ug/kg 23.830 80 70-130ND
1,2,3-Trichloropropane ug/kg 24.630 82 70-130ND
1,2,4-Trichlorobenzene ug/kg 25.030 83 70-130ND
1,2,4-Trimethylbenzene ug/kg 28.830 96 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 22.430 75 70-130ND
1,2-Dibromoethane (EDB)ug/kg 28.030 94 70-130ND
1,2-Dichlorobenzene ug/kg 27.130 91 70-130ND
1,2-Dichloroethane ug/kg 27.630 92 70-130ND
1,2-Dichloropropane ug/kg 28.830 96 70-130ND
1,3,5-Trimethylbenzene ug/kg 29.630 99 70-130ND
1,3-Dichlorobenzene ug/kg 27.930 93 70-130ND
1,3-Dichloropropane ug/kg 28.730 96 70-130ND
1,4-Dichlorobenzene ug/kg 27.930 93 70-130ND
2,2-Dichloropropane ug/kg 27.830 93 70-130ND
2-Butanone (MEK)ug/kg 55.4J59.8 93 70-130ND
2-Chlorotoluene ug/kg 29.630 99 70-130ND
2-Hexanone ug/kg 46.3J59.8 77 70-130ND
4-Chlorotoluene ug/kg 29.530 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 53.9J59.8 90 70-130ND
Acetone ug/kg 118J59.8 99 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2262223MATRIX SPIKE SAMPLE:
MSSpike
Result
92381713001
Benzene ug/kg 29.130 97 50-166ND
Bromobenzene ug/kg 29.730 99 70-130ND
Bromochloromethane ug/kg 27.930 93 70-130ND
Bromodichloromethane ug/kg 27.130 91 70-130ND
Bromoform ug/kg 23.130 77 70-130ND
Bromomethane ug/kg 28.830 96 70-130ND
Carbon tetrachloride ug/kg 28.330 95 70-130ND
Chlorobenzene ug/kg 29.530 98 43-169ND
Chloroethane ug/kg 23.830 80 70-130ND
Chloroform ug/kg 28.330 95 70-130ND
Chloromethane ug/kg 23.830 80 70-130ND
cis-1,2-Dichloroethene ug/kg 29.430 98 70-130ND
cis-1,3-Dichloropropene ug/kg 27.330 91 70-130ND
Dibromochloromethane ug/kg 23.730 79 70-130ND
Dibromomethane ug/kg 26.030 87 70-130ND
Dichlorodifluoromethane ug/kg 22.530 75 70-130ND
Diisopropyl ether ug/kg 30.130 101 70-130ND
Ethylbenzene ug/kg 29.330 98 70-130ND
Hexachloro-1,3-butadiene ug/kg 26.730 89 70-130ND
Isopropylbenzene (Cumene)ug/kg 28.730 96 70-130ND
m&p-Xylene ug/kg 58.259.8 97 70-130ND
Methyl-tert-butyl ether ug/kg 26.330 88 70-130ND
Methylene Chloride ug/kg 55.8 M13018770-130ND
n-Butylbenzene ug/kg 28.730 96 70-130ND
n-Propylbenzene ug/kg 30.730 103 70-130ND
Naphthalene ug/kg 21.930 73 70-130ND
o-Xylene ug/kg 28.530 95 70-130ND
p-Isopropyltoluene ug/kg 30.030 100 70-130ND
sec-Butylbenzene ug/kg 30.730 102 70-130ND
Styrene ug/kg 26.730 89 70-130ND
tert-Butylbenzene ug/kg 27.630 92 70-130ND
Tetrachloroethene ug/kg 25.530 85 70-130ND
Toluene ug/kg 29.930 100 52-163ND
trans-1,2-Dichloroethene ug/kg 29.030 97 70-130ND
trans-1,3-Dichloropropene ug/kg 24.730 83 70-130ND
Trichloroethene ug/kg 29.430 98 49-167ND
Trichlorofluoromethane ug/kg 27.230 91 70-130ND
Vinyl acetate ug/kg 19.7J M159.8 33 70-130ND
Vinyl chloride ug/kg 27.130 91 70-130ND
Xylene (Total)ug/kg 86.689.8 96 70-130ND
1,2-Dichloroethane-d4 (S)%89 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92381713005
2262224SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92381713005
2262224SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%92 32124
4-Bromofluorobenzene (S)%89 14100
Toluene-d8 (S)%108 4110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407350
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2260319
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 04/23/18 15:13
1,2-Dichlorobenzene ug/kg ND 330 04/23/18 15:13
1,3-Dichlorobenzene ug/kg ND 330 04/23/18 15:13
1,4-Dichlorobenzene ug/kg ND 330 04/23/18 15:13
1-Methylnaphthalene ug/kg ND 330 04/23/18 15:13
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 04/23/18 15:13
2,4,5-Trichlorophenol ug/kg ND 330 04/23/18 15:13
2,4,6-Trichlorophenol ug/kg ND 330 04/23/18 15:13
2,4-Dichlorophenol ug/kg ND 330 04/23/18 15:13
2,4-Dimethylphenol ug/kg ND 330 04/23/18 15:13
2,4-Dinitrophenol ug/kg ND 1650 04/23/18 15:13
2,4-Dinitrotoluene ug/kg ND 330 04/23/18 15:13
2,6-Dinitrotoluene ug/kg ND 330 04/23/18 15:13
2-Chloronaphthalene ug/kg ND 330 04/23/18 15:13
2-Chlorophenol ug/kg ND 330 04/23/18 15:13
2-Methylnaphthalene ug/kg ND 330 04/23/18 15:13
2-Methylphenol(o-Cresol)ug/kg ND 330 04/23/18 15:13
2-Nitroaniline ug/kg ND 1650 04/23/18 15:13
2-Nitrophenol ug/kg ND 330 04/23/18 15:13
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 04/23/18 15:13
3,3'-Dichlorobenzidine ug/kg ND 1650 04/23/18 15:13
3-Nitroaniline ug/kg ND 1650 04/23/18 15:13
4,6-Dinitro-2-methylphenol ug/kg ND 660 04/23/18 15:13
4-Bromophenylphenyl ether ug/kg ND 330 04/23/18 15:13
4-Chloro-3-methylphenol ug/kg ND 660 04/23/18 15:13
4-Chloroaniline ug/kg ND 1650 04/23/18 15:13
4-Chlorophenylphenyl ether ug/kg ND 330 04/23/18 15:13
4-Nitroaniline ug/kg ND 660 04/23/18 15:13
4-Nitrophenol ug/kg ND 1650 04/23/18 15:13
Acenaphthene ug/kg ND 330 04/23/18 15:13
Acenaphthylene ug/kg ND 330 04/23/18 15:13
Aniline ug/kg ND 330 04/23/18 15:13
Anthracene ug/kg ND 330 04/23/18 15:13
Benzo(a)anthracene ug/kg ND 330 04/23/18 15:13
Benzo(a)pyrene ug/kg ND 330 04/23/18 15:13
Benzo(b)fluoranthene ug/kg ND 330 04/23/18 15:13
Benzo(g,h,i)perylene ug/kg ND 330 04/23/18 15:13
Benzo(k)fluoranthene ug/kg ND 330 04/23/18 15:13
Benzoic Acid ug/kg ND 1650 04/23/18 15:13
Benzyl alcohol ug/kg ND 660 04/23/18 15:13
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2260319
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007,
92381713008
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane ug/kg ND 330 04/23/18 15:13
bis(2-Chloroethyl) ether ug/kg ND 330 04/23/18 15:13
bis(2-Ethylhexyl)phthalate ug/kg ND 330 04/23/18 15:13
Butylbenzylphthalate ug/kg ND 330 04/23/18 15:13
Chrysene ug/kg ND 330 04/23/18 15:13
Di-n-butylphthalate ug/kg ND 330 04/23/18 15:13
Di-n-octylphthalate ug/kg ND 330 04/23/18 15:13
Dibenz(a,h)anthracene ug/kg ND 330 04/23/18 15:13
Dibenzofuran ug/kg ND 330 04/23/18 15:13
Diethylphthalate ug/kg ND 330 04/23/18 15:13
Dimethylphthalate ug/kg ND 330 04/23/18 15:13
Fluoranthene ug/kg ND 330 04/23/18 15:13
Fluorene ug/kg ND 330 04/23/18 15:13
Hexachloro-1,3-butadiene ug/kg ND 330 04/23/18 15:13
Hexachlorobenzene ug/kg ND 330 04/23/18 15:13
Hexachlorocyclopentadiene ug/kg ND 330 04/23/18 15:13
Hexachloroethane ug/kg ND 330 04/23/18 15:13
Indeno(1,2,3-cd)pyrene ug/kg ND 330 04/23/18 15:13
Isophorone ug/kg ND 330 04/23/18 15:13
N-Nitroso-di-n-propylamine ug/kg ND 330 04/23/18 15:13
N-Nitrosodimethylamine ug/kg ND 330 04/23/18 15:13
N-Nitrosodiphenylamine ug/kg ND 330 04/23/18 15:13
Naphthalene ug/kg ND 330 04/23/18 15:13
Nitrobenzene ug/kg ND 330 04/23/18 15:13
Pentachlorophenol ug/kg ND 1650 04/23/18 15:13
Phenanthrene ug/kg ND 330 04/23/18 15:13
Phenol ug/kg ND 330 04/23/18 15:13
Pyrene ug/kg ND 330 04/23/18 15:13
2,4,6-Tribromophenol (S)%84 27-110 04/23/18 15:13
2-Fluorobiphenyl (S)%90 30-110 04/23/18 15:13
2-Fluorophenol (S)%80 13-110 04/23/18 15:13
Nitrobenzene-d5 (S)%83 23-110 04/23/18 15:13
Phenol-d6 (S)%82 22-110 04/23/18 15:13
Terphenyl-d14 (S)%72 28-110 04/23/18 15:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2260320LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13501680 81 36-120
1,2-Dichlorobenzene ug/kg 13201680 79 41-120
1,3-Dichlorobenzene ug/kg 12701680 76 66-120
1,4-Dichlorobenzene ug/kg 12901680 77 42-120
1-Methylnaphthalene ug/kg 14701680 88 40-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2260320LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 10801680 65 17-120
2,4,5-Trichlorophenol ug/kg 13601680 81 37-120
2,4,6-Trichlorophenol ug/kg 14501680 86 40-120
2,4-Dichlorophenol ug/kg 14501680 86 33-120
2,4-Dimethylphenol ug/kg 15301680 91 36-120
2,4-Dinitrophenol ug/kg 61508390 73 22-121
2,4-Dinitrotoluene ug/kg 15501680 93 60-120
2,6-Dinitrotoluene ug/kg 14701680 87 54-120
2-Chloronaphthalene ug/kg 14101680 84 41-120
2-Chlorophenol ug/kg 13501680 81 39-120
2-Methylnaphthalene ug/kg 14701680 88 26-120
2-Methylphenol(o-Cresol)ug/kg 15801680 94 41-120
2-Nitroaniline ug/kg 26703360 80 45-120
2-Nitrophenol ug/kg 13601680 81 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 14301680 85 35-120
3,3'-Dichlorobenzidine ug/kg 26103360 78 16-125
3-Nitroaniline ug/kg 30003360 89 45-120
4,6-Dinitro-2-methylphenol ug/kg 33303360 99 46-120
4-Bromophenylphenyl ether ug/kg 14801680 88 36-120
4-Chloro-3-methylphenol ug/kg 30103360 90 37-120
4-Chloroaniline ug/kg 26703360 79 35-120
4-Chlorophenylphenyl ether ug/kg 15701680 94 30-120
4-Nitroaniline ug/kg 33003360 98 48-120
4-Nitrophenol ug/kg 77108390 92 43-120
Acenaphthene ug/kg 15101680 90 46-120
Acenaphthylene ug/kg 15401680 92 46-120
Aniline ug/kg 11001680 66 33-120
Anthracene ug/kg 16701680 100 63-120
Benzo(a)anthracene ug/kg 13601680 81 61-120
Benzo(a)pyrene ug/kg 14401680 86 59-120
Benzo(b)fluoranthene ug/kg 13801680 82 55-120
Benzo(g,h,i)perylene ug/kg 14901680 89 57-120
Benzo(k)fluoranthene ug/kg 14301680 85 56-120
Benzoic Acid ug/kg 41208390 49 13-120
Benzyl alcohol ug/kg 27403360 82 34-120
bis(2-Chloroethoxy)methane ug/kg 14001680 83 21-120
bis(2-Chloroethyl) ether ug/kg 12701680 76 25-120
bis(2-Ethylhexyl)phthalate ug/kg 14101680 84 56-123
Butylbenzylphthalate ug/kg 14401680 86 57-120
Chrysene ug/kg 13201680 79 64-120
Di-n-butylphthalate ug/kg 17701680 106 58-120
Di-n-octylphthalate ug/kg 15301680 91 47-121
Dibenz(a,h)anthracene ug/kg 15001680 89 56-120
Dibenzofuran ug/kg 15101680 90 43-120
Diethylphthalate ug/kg 15401680 92 55-120
Dimethylphthalate ug/kg 14901680 89 54-120
Fluoranthene ug/kg 16901680 100 61-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 47 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2260320LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 16101680 96 51-120
Hexachloro-1,3-butadiene ug/kg 12801680 76 22-120
Hexachlorobenzene ug/kg 14401680 86 53-120
Hexachlorocyclopentadiene ug/kg 11201680 67 18-150
Hexachloroethane ug/kg 13001680 77 39-120
Indeno(1,2,3-cd)pyrene ug/kg 15301680 91 58-120
Isophorone ug/kg 12901680 77 38-120
N-Nitroso-di-n-propylamine ug/kg 15301680 91 30-120
N-Nitrosodimethylamine ug/kg 13101680 78 32-120
N-Nitrosodiphenylamine ug/kg 15501680 92 50-120
Naphthalene ug/kg 13801680 82 38-120
Nitrobenzene ug/kg 12701680 75 37-120
Pentachlorophenol ug/kg 24303360 72 10-120
Phenanthrene ug/kg 16101680 96 62-120
Phenol ug/kg 13301680 79 37-120
Pyrene ug/kg 14701680 88 63-120
2,4,6-Tribromophenol (S)%86 27-110
2-Fluorobiphenyl (S)%86 30-110
2-Fluorophenol (S)%77 13-110
Nitrobenzene-d5 (S)%78 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%64 28-110
Parameter Units
Dup
Result QualifiersRPDResult
35386978001
2260322SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND0.64U mg/kg
1,2-Dichlorobenzene ug/kg ND0.88U mg/kg
1,3-Dichlorobenzene ug/kg ND0.75U mg/kg
1,4-Dichlorobenzene ug/kg ND0.93U mg/kg
1-Methylnaphthalene ug/kg ND0.86U mg/kg
2,2'-Oxybis(1-chloropropane)ug/kg ND0.88U mg/kg
2,4,5-Trichlorophenol ug/kg ND1.0U mg/kg
2,4,6-Trichlorophenol ug/kg ND0.73U mg/kg
2,4-Dichlorophenol ug/kg ND0.72U mg/kg
2,4-Dimethylphenol ug/kg ND1.3U mg/kg
2,4-Dinitrophenol ug/kg ND0.54U mg/kg
2,4-Dinitrotoluene ug/kg ND0.62U mg/kg
2,6-Dinitrotoluene ug/kg ND0.69U mg/kg
2-Chloronaphthalene ug/kg ND0.65U mg/kg
2-Chlorophenol ug/kg ND0.90U mg/kg
2-Methylnaphthalene ug/kg ND0.71U mg/kg
2-Methylphenol(o-Cresol)ug/kg ND1.0U mg/kg
2-Nitroaniline ug/kg ND1.0U mg/kg
2-Nitrophenol ug/kg ND0.80U mg/kg
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
35386978001
2260322SAMPLE DUPLICATE:
3&4-Methylphenol(m&p Cresol)ug/kg ND1.3U mg/kg
3,3'-Dichlorobenzidine ug/kg ND0.72U mg/kg
3-Nitroaniline ug/kg ND0.90U mg/kg
4,6-Dinitro-2-methylphenol ug/kg ND0.66U mg/kg
4-Bromophenylphenyl ether ug/kg ND0.60U mg/kg
4-Chloro-3-methylphenol ug/kg ND0.68U mg/kg
4-Chloroaniline ug/kg ND0.92U mg/kg
4-Chlorophenylphenyl ether ug/kg ND0.68U mg/kg
4-Nitroaniline ug/kg ND0.93U mg/kg
4-Nitrophenol ug/kg ND0.59U mg/kg
Acenaphthene ug/kg ND0.76U mg/kg
Acenaphthylene ug/kg ND0.78U mg/kg
Aniline ug/kg ND0.89U mg/kg
Anthracene ug/kg ND0.74U mg/kg
Benzo(a)anthracene ug/kg ND0.61U mg/kg
Benzo(a)pyrene ug/kg ND0.63U mg/kg
Benzo(b)fluoranthene ug/kg ND0.57U mg/kg
Benzo(g,h,i)perylene ug/kg ND0.84U mg/kg
Benzo(k)fluoranthene ug/kg ND0.65U mg/kg
Benzoic Acid ug/kg ND0.60U mg/kg
Benzyl alcohol ug/kg ND0.66U mg/kg
bis(2-Chloroethoxy)methane ug/kg ND0.77U mg/kg
bis(2-Chloroethyl) ether ug/kg ND0.84U mg/kg
bis(2-Ethylhexyl)phthalate ug/kg ND0.90U mg/kg
Butylbenzylphthalate ug/kg ND0.70U mg/kg
Chrysene ug/kg ND0.44U mg/kg
Di-n-butylphthalate ug/kg ND0.54U mg/kg
Di-n-octylphthalate ug/kg ND0.69U mg/kg
Dibenz(a,h)anthracene ug/kg ND0.70U mg/kg
Dibenzofuran ug/kg ND0.54U mg/kg
Diethylphthalate ug/kg ND0.51U mg/kg
Dimethylphthalate ug/kg ND0.67U mg/kg
Fluoranthene ug/kg ND0.48U mg/kg
Fluorene ug/kg ND0.68U mg/kg
Hexachloro-1,3-butadiene ug/kg ND0.57U mg/kg
Hexachlorobenzene ug/kg ND0.42U mg/kg
Hexachlorocyclopentadiene ug/kg ND0.61U mg/kg
Hexachloroethane ug/kg ND0.87U mg/kg
Indeno(1,2,3-cd)pyrene ug/kg ND0.68U mg/kg
Isophorone ug/kg ND0.74U mg/kg
N-Nitroso-di-n-propylamine ug/kg ND0.63U mg/kg
N-Nitrosodimethylamine ug/kg ND1.1U mg/kg
N-Nitrosodiphenylamine ug/kg ND0.98U mg/kg
Naphthalene ug/kg ND0.81U mg/kg
Nitrobenzene ug/kg ND0.90U mg/kg
Pentachlorophenol ug/kg ND0.60U mg/kg
Phenanthrene ug/kg ND0.55U mg/kg
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
35386978001
2260322SAMPLE DUPLICATE:
Phenol ug/kg ND0.99U mg/kg
Pyrene ug/kg ND0.56U mg/kg
2,4,6-Tribromophenol (S)%0 S40
2-Fluorobiphenyl (S)%0 S40
2-Fluorophenol (S)%0 S40
Nitrobenzene-d5 (S)%0 D3,P3,S40
Phenol-d6 (S)%0 S40
Terphenyl-d14 (S)%0 S40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407588
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92381713001, 92381713003, 92381713005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2261504
Associated Lab Samples:92381713001, 92381713003, 92381713005
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10 N204/26/18 08:30
Aliphatic (C19-C36)mg/kg ND 10 N204/26/18 08:30
Aromatic (C11-C22)mg/kg 22.0 10 N204/26/18 08:30
2-Bromonaphthalene (S)%66 40-140 04/26/18 08:30
2-Fluorobiphenyl (S)%63 40-140 04/26/18 08:30
Nonatriacontane (S)%60 40-140 04/26/18 08:30
o-Terphenyl (S)%73 40-140 04/26/18 08:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2261505LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2261506
Aliphatic (C09-C18)mg/kg ND N2105940-14054ND 50
Aliphatic (C19-C36)mg/kg ND N213.4 59 40-14055ND 50
Aromatic (C11-C22)mg/kg 18.7 N228.4 66 40-1408423.9 25 50
2-Bromonaphthalene (S)%47 40-14074
2-Fluorobiphenyl (S)%62 40-14070
Nonatriacontane (S)%67 40-14062
o-Terphenyl (S)%72 40-14088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
408625
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92381713002, 92381713004, 92381713006, 92381713007, 92381713008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2267232
Associated Lab Samples:92381713002, 92381713004, 92381713006, 92381713007, 92381713008
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10 N205/01/18 14:21
Aliphatic (C19-C36)mg/kg ND 10 N205/01/18 14:21
Aromatic (C11-C22)mg/kg ND 10 N205/01/18 14:21
2-Bromonaphthalene (S)%65 40-140 05/01/18 14:21
2-Fluorobiphenyl (S)%77 40-140 05/01/18 14:21
Nonatriacontane (S)%92 40-140 05/01/18 14:21
o-Terphenyl (S)%79 40-140 05/01/18 14:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2267233LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2267234
Aliphatic (C09-C18)mg/kg ND N29.9 68 40-14072ND 50
Aliphatic (C19-C36)mg/kg ND N213.2 72 40-14074ND 50
Aromatic (C11-C22)mg/kg 19.9 N228.1 71 40-1407521.0 5 50
2-Bromonaphthalene (S)%68 40-14069
2-Fluorobiphenyl (S)%78 40-14077
Nonatriacontane (S)%112 40-14088
o-Terphenyl (S)%91 40-14087
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407237
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92381713001, 92381713002, 92381713003, 92381713004, 92381713005, 92381713006, 92381713007
Parameter Units
Dup
Result QualifiersRPDResult
92381216032
2259670SAMPLE DUPLICATE:
Percent Moisture %22.6 1519.4
Parameter Units
Dup
Result QualifiersRPDResult
92381730010
2259671SAMPLE DUPLICATE:
Percent Moisture %12.6 711.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 59
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92381713
3201 Charles
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407259
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92381713008
Parameter Units
Dup
Result QualifiersRPDResult
92381528002
2259899SAMPLE DUPLICATE:
Percent Moisture %7.4 216.0
Parameter Units
Dup
Result QualifiersRPDResult
92381763001
2259900SAMPLE DUPLICATE:
Percent Moisture %24.8 125.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 59
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92381713
3201 Charles
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was re-extracted within hold time. Results from re-extraction confirm initial analysis.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.IO
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 59
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92381713
3201 Charles
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92381713001 407588 408050FT-SW-1 MADEP EPH MADEP EPH
92381713002 408625 408833FT-SW-2 MADEP EPH MADEP EPH
92381713003 407588 408050FT-SW-3 MADEP EPH MADEP EPH
92381713004 408625 408833FT-SW-4 MADEP EPH MADEP EPH
92381713005 407588 408050HT-SW-1 MADEP EPH MADEP EPH
92381713006 408625 408833HT-SW-2 MADEP EPH MADEP EPH
92381713007 408625 408833HT-SW-3 MADEP EPH MADEP EPH
92381713008 408625 408833HT-SW-4 MADEP EPH MADEP EPH
92381713001 407472 407672FT-SW-1 MADEP VPH MADEP VPH
92381713002 407472 407672FT-SW-2 MADEP VPH MADEP VPH
92381713003 407472 407672FT-SW-3 MADEP VPH MADEP VPH
92381713004 407472 407672FT-SW-4 MADEP VPH MADEP VPH
92381713005 407472 407672HT-SW-1 MADEP VPH MADEP VPH
92381713006 407472 407672HT-SW-2 MADEP VPH MADEP VPH
92381713007 407472 407672HT-SW-3 MADEP VPH MADEP VPH
92381713008 407472 407672HT-SW-4 MADEP VPH MADEP VPH
92381713001 407350 407484FT-SW-1 EPA 3546 EPA 8270
92381713002 407350 407484FT-SW-2 EPA 3546 EPA 8270
92381713003 407350 407484FT-SW-3 EPA 3546 EPA 8270
92381713004 407350 407484FT-SW-4 EPA 3546 EPA 8270
92381713005 407350 407484HT-SW-1 EPA 3546 EPA 8270
92381713006 407350 407484HT-SW-2 EPA 3546 EPA 8270
92381713007 407350 407484HT-SW-3 EPA 3546 EPA 8270
92381713008 407350 407484HT-SW-4 EPA 3546 EPA 8270
92381713001 407655FT-SW-1 EPA 8260
92381713002 407655FT-SW-2 EPA 8260
92381713003 407655FT-SW-3 EPA 8260
92381713004 407655FT-SW-4 EPA 8260
92381713005 407655HT-SW-1 EPA 8260
92381713006 407655HT-SW-2 EPA 8260
92381713007 407655HT-SW-3 EPA 8260
92381713008 407655HT-SW-4 EPA 8260
92381713001 407237FT-SW-1 ASTM D2974-87
92381713002 407237FT-SW-2 ASTM D2974-87
92381713003 407237FT-SW-3 ASTM D2974-87
92381713004 407237FT-SW-4 ASTM D2974-87
92381713005 407237HT-SW-1 ASTM D2974-87
92381713006 407237HT-SW-2 ASTM D2974-87
92381713007 407237HT-SW-3 ASTM D2974-87
92381713008 407259HT-SW-4 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/02/2018 10:48 AM
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Page 56 of 59
Page 57 of 59
Page 58 of 59
Page 59 of 59
#=CL#
May 08, 2018
LIMS USE: FR - ALLEN MCCOLL
LIMS OBJECT ID: 92382378
92382378
Project:
Pace Project No.:
RE:
Mr. Allen McColl
Terracon
314 Beacon Drive
Winterville, NC 28590
3201 Charles Blvd
Dear Mr. McColl:
Enclosed are the analytical results for sample(s) received by the laboratory on April 26, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 25
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Page 2 of 25
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92382378001 FT-GW MADEP EPH 7 PASI-CPKS
MADEP VPH 5 PASI-CCAH
EPA 625 58 PASI-CRES
SM 6200B 16 PASI-CCAH
92382378002 HT-GW MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CCAH
EPA 625 63 PASI-CRES
SM 6200B 16 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 3 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:FT-GW Lab ID:92382378001 Collected:04/25/18 10:05 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 05/07/18 15:50 N205/06/18 23:4098.0 1
Aliphatic (C19-C36)ND ug/L 05/07/18 15:50 N205/06/18 23:4098.0 1
Aromatic (C11-C22)ND ug/L 05/07/18 15:50 N205/06/18 23:4098.0 1
Surrogates
Nonatriacontane (S)16 %05/07/18 15:50 7194-86-7 S205/06/18 23:4040-140 1
o-Terphenyl (S)20 %05/07/18 15:50 84-15-1 S205/06/18 23:4040-140 1
2-Fluorobiphenyl (S)76 %05/07/18 15:50 321-60-805/06/18 23:4040-140 1
2-Bromonaphthalene (S)77 %05/07/18 15:50 580-13-205/06/18 23:4040-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 04/30/18 16:06 N250.0 1
Aliphatic (C09-C12)ND ug/L 04/30/18 16:06 N250.0 1
Aromatic (C09-C10)ND ug/L 04/30/18 16:06 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)109 %04/30/18 16:06 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)105 %04/30/18 16:06 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 04/30/18 13:30 83-32-904/26/18 20:354.9 1
Acenaphthylene ND ug/L 04/30/18 13:30 208-96-804/26/18 20:354.9 1
Anthracene ND ug/L 04/30/18 13:30 120-12-704/26/18 20:354.9 1
Benzo(a)anthracene ND ug/L 04/30/18 13:30 56-55-304/26/18 20:354.9 1
Benzo(a)pyrene ND ug/L 04/30/18 13:30 50-32-804/26/18 20:354.9 1
Benzo(b)fluoranthene ND ug/L 04/30/18 13:30 205-99-204/26/18 20:354.9 1
Benzo(g,h,i)perylene ND ug/L 04/30/18 13:30 191-24-204/26/18 20:354.9 1
Benzo(k)fluoranthene ND ug/L 04/30/18 13:30 207-08-904/26/18 20:354.9 1
4-Bromophenylphenyl ether ND ug/L 04/30/18 13:30 101-55-304/26/18 20:354.9 1
Butylbenzylphthalate ND ug/L 04/30/18 13:30 85-68-704/26/18 20:354.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/18 13:30 59-50-704/26/18 20:354.9 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/18 13:30 111-91-104/26/18 20:359.8 1
bis(2-Chloroethyl) ether ND ug/L 04/30/18 13:30 111-44-404/26/18 20:354.9 1
2-Chloronaphthalene ND ug/L 04/30/18 13:30 91-58-704/26/18 20:354.9 1
2-Chlorophenol ND ug/L 04/30/18 13:30 95-57-804/26/18 20:354.9 1
4-Chlorophenylphenyl ether ND ug/L 04/30/18 13:30 7005-72-304/26/18 20:354.9 1
Chrysene ND ug/L 04/30/18 13:30 218-01-904/26/18 20:354.9 1
Dibenz(a,h)anthracene ND ug/L 04/30/18 13:30 53-70-304/26/18 20:354.9 1
3,3'-Dichlorobenzidine ND ug/L 04/30/18 13:30 91-94-104/26/18 20:3524.5 1
2,4-Dichlorophenol ND ug/L 04/30/18 13:30 120-83-204/26/18 20:354.9 1
Diethylphthalate ND ug/L 04/30/18 13:30 84-66-204/26/18 20:354.9 1
2,4-Dimethylphenol ND ug/L 04/30/18 13:30 105-67-904/26/18 20:359.8 1
Dimethylphthalate ND ug/L 04/30/18 13:30 131-11-304/26/18 20:354.9 1
Di-n-butylphthalate ND ug/L 04/30/18 13:30 84-74-204/26/18 20:354.9 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/18 13:30 534-52-104/26/18 20:3519.6 1
2,4-Dinitrophenol ND ug/L 04/30/18 13:30 51-28-504/26/18 20:3549.0 1
2,4-Dinitrotoluene ND ug/L 04/30/18 13:30 121-14-204/26/18 20:354.9 1
2,6-Dinitrotoluene ND ug/L 04/30/18 13:30 606-20-204/26/18 20:354.9 1
Di-n-octylphthalate ND ug/L 04/30/18 13:30 117-84-004/26/18 20:354.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Huntersville, NC 28078
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Page 4 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:FT-GW Lab ID:92382378001 Collected:04/25/18 10:05 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/18 13:30 117-81-704/26/18 20:354.9 1
Fluoranthene ND ug/L 04/30/18 13:30 206-44-004/26/18 20:354.9 1
Fluorene ND ug/L 04/30/18 13:30 86-73-704/26/18 20:354.9 1
Hexachloro-1,3-butadiene ND ug/L 04/30/18 13:30 87-68-304/26/18 20:354.9 1
Hexachlorobenzene ND ug/L 04/30/18 13:30 118-74-104/26/18 20:354.9 1
Hexachlorocyclopentadiene ND ug/L 04/30/18 13:30 77-47-404/26/18 20:359.8 1
Hexachloroethane ND ug/L 04/30/18 13:30 67-72-1 L204/26/18 20:354.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/18 13:30 193-39-504/26/18 20:354.9 1
Isophorone ND ug/L 04/30/18 13:30 78-59-104/26/18 20:359.8 1
Naphthalene ND ug/L 04/30/18 13:30 91-20-304/26/18 20:354.9 1
Nitrobenzene ND ug/L 04/30/18 13:30 98-95-304/26/18 20:354.9 1
2-Nitrophenol ND ug/L 04/30/18 13:30 88-75-504/26/18 20:354.9 1
4-Nitrophenol ND ug/L 04/30/18 13:30 100-02-704/26/18 20:3549.0 1
N-Nitrosodimethylamine ND ug/L 04/30/18 13:30 62-75-904/26/18 20:354.9 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/18 13:30 621-64-704/26/18 20:354.9 1
N-Nitrosodiphenylamine ND ug/L 04/30/18 13:30 86-30-604/26/18 20:359.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/18 13:30 108-60-104/26/18 20:354.9 1
Pentachlorophenol ND ug/L 04/30/18 13:30 87-86-504/26/18 20:359.8 1
Phenanthrene ND ug/L 04/30/18 13:30 85-01-804/26/18 20:354.9 1
Phenol ND ug/L 04/30/18 13:30 108-95-204/26/18 20:354.9 1
Pyrene ND ug/L 04/30/18 13:30 129-00-004/26/18 20:354.9 1
1,2,4-Trichlorobenzene ND ug/L 04/30/18 13:30 120-82-104/26/18 20:354.9 1
2,4,6-Trichlorophenol ND ug/L 04/30/18 13:30 88-06-204/26/18 20:359.8 1
Surrogates
Nitrobenzene-d5 (S)33 %04/30/18 13:30 4165-60-004/26/18 20:3510-120 1
2-Fluorobiphenyl (S)33 %04/30/18 13:30 321-60-804/26/18 20:3515-120 1
Terphenyl-d14 (S)243 %04/30/18 13:30 1718-51-0 S304/26/18 20:3511-131 1
Phenol-d6 (S)11 %04/30/18 13:30 13127-88-304/26/18 20:3510-120 1
2-Fluorophenol (S)16 %04/30/18 13:30 367-12-404/26/18 20:3510-120 1
2,4,6-Tribromophenol (S)63 %04/30/18 13:30 118-79-604/26/18 20:3510-137 1
Analytical Method: SM 6200B602 Volatiles by Method 6200
Benzene ND ug/L 05/03/18 05:48 71-43-21.0 1
Chlorobenzene ND ug/L 05/03/18 05:48 108-90-71.0 1
1,2-Dichlorobenzene ND ug/L 05/03/18 05:48 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/03/18 05:48 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/03/18 05:48 106-46-71.0 1
Diisopropyl ether ND ug/L 05/03/18 05:48 108-20-31.0 1
Ethylbenzene ND ug/L 05/03/18 05:48 100-41-41.0 1
Isopropylbenzene (Cumene)ND ug/L 05/03/18 05:48 98-82-81.0 1
Methyl-tert-butyl ether ND ug/L 05/03/18 05:48 1634-04-41.0 1
Naphthalene ND ug/L 05/03/18 05:48 91-20-32.0 1
Toluene ND ug/L 05/03/18 05:48 108-88-31.0 1
m&p-Xylene ND ug/L 05/03/18 05:48 179601-23-12.0 1
o-Xylene ND ug/L 05/03/18 05:48 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %05/03/18 05:48 460-00-470-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 5 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:FT-GW Lab ID:92382378001 Collected:04/25/18 10:05 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B602 Volatiles by Method 6200
Surrogates
1,2-Dichloroethane-d4 (S)93 %05/03/18 05:48 17060-07-070-130 1
Toluene-d8 (S)101 %05/03/18 05:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:HT-GW Lab ID:92382378002 Collected:04/25/18 11:31 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 05/02/18 13:50 N204/29/18 23:0398.0 1
Aliphatic (C19-C36)ND ug/L 05/02/18 13:50 N204/29/18 23:0398.0 1
Aromatic (C11-C22)348 ug/L 05/02/18 13:50 N204/29/18 23:0398.0 1
Surrogates
Nonatriacontane (S)49 %05/02/18 13:50 7194-86-704/29/18 23:0340-140 1
o-Terphenyl (S)61 %05/02/18 13:50 84-15-104/29/18 23:0340-140 1
2-Fluorobiphenyl (S)65 %05/02/18 13:50 321-60-804/29/18 23:0340-140 1
2-Bromonaphthalene (S)70 %05/02/18 13:50 580-13-204/29/18 23:0340-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 04/30/18 16:34 N250.0 1
Aliphatic (C09-C12)107 ug/L 04/30/18 16:34 N250.0 1
Aromatic (C09-C10)61.6 ug/L 04/30/18 16:34 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)110 %04/30/18 16:34 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)106 %04/30/18 16:34 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 04/30/18 13:58 83-32-904/26/18 20:354.9 1
Acenaphthylene ND ug/L 04/30/18 13:58 208-96-804/26/18 20:354.9 1
Anthracene ND ug/L 04/30/18 13:58 120-12-704/26/18 20:354.9 1
Benzo(a)anthracene ND ug/L 04/30/18 13:58 56-55-304/26/18 20:354.9 1
Benzo(a)pyrene ND ug/L 04/30/18 13:58 50-32-804/26/18 20:354.9 1
Benzo(b)fluoranthene ND ug/L 04/30/18 13:58 205-99-204/26/18 20:354.9 1
Benzo(g,h,i)perylene ND ug/L 04/30/18 13:58 191-24-204/26/18 20:354.9 1
Benzo(k)fluoranthene ND ug/L 04/30/18 13:58 207-08-904/26/18 20:354.9 1
4-Bromophenylphenyl ether ND ug/L 04/30/18 13:58 101-55-304/26/18 20:354.9 1
Butylbenzylphthalate ND ug/L 04/30/18 13:58 85-68-704/26/18 20:354.9 1
4-Chloro-3-methylphenol ND ug/L 04/30/18 13:58 59-50-704/26/18 20:354.9 1
bis(2-Chloroethoxy)methane ND ug/L 04/30/18 13:58 111-91-104/26/18 20:359.8 1
bis(2-Chloroethyl) ether ND ug/L 04/30/18 13:58 111-44-404/26/18 20:354.9 1
2-Chloronaphthalene ND ug/L 04/30/18 13:58 91-58-704/26/18 20:354.9 1
2-Chlorophenol ND ug/L 04/30/18 13:58 95-57-804/26/18 20:354.9 1
4-Chlorophenylphenyl ether ND ug/L 04/30/18 13:58 7005-72-304/26/18 20:354.9 1
Chrysene ND ug/L 04/30/18 13:58 218-01-904/26/18 20:354.9 1
Dibenz(a,h)anthracene ND ug/L 04/30/18 13:58 53-70-304/26/18 20:354.9 1
3,3'-Dichlorobenzidine ND ug/L 04/30/18 13:58 91-94-104/26/18 20:3524.5 1
2,4-Dichlorophenol ND ug/L 04/30/18 13:58 120-83-204/26/18 20:354.9 1
Diethylphthalate ND ug/L 04/30/18 13:58 84-66-204/26/18 20:354.9 1
2,4-Dimethylphenol ND ug/L 04/30/18 13:58 105-67-904/26/18 20:359.8 1
Dimethylphthalate ND ug/L 04/30/18 13:58 131-11-304/26/18 20:354.9 1
Di-n-butylphthalate ND ug/L 04/30/18 13:58 84-74-204/26/18 20:354.9 1
4,6-Dinitro-2-methylphenol ND ug/L 04/30/18 13:58 534-52-104/26/18 20:3519.6 1
2,4-Dinitrophenol ND ug/L 04/30/18 13:58 51-28-504/26/18 20:3549.0 1
2,4-Dinitrotoluene ND ug/L 04/30/18 13:58 121-14-204/26/18 20:354.9 1
2,6-Dinitrotoluene ND ug/L 04/30/18 13:58 606-20-204/26/18 20:354.9 1
Di-n-octylphthalate ND ug/L 04/30/18 13:58 117-84-004/26/18 20:354.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Huntersville, NC 28078
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Page 7 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:HT-GW Lab ID:92382378002 Collected:04/25/18 11:31 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 04/30/18 13:58 117-81-704/26/18 20:354.9 1
Fluoranthene ND ug/L 04/30/18 13:58 206-44-004/26/18 20:354.9 1
Fluorene ND ug/L 04/30/18 13:58 86-73-704/26/18 20:354.9 1
Hexachloro-1,3-butadiene ND ug/L 04/30/18 13:58 87-68-304/26/18 20:354.9 1
Hexachlorobenzene ND ug/L 04/30/18 13:58 118-74-104/26/18 20:354.9 1
Hexachlorocyclopentadiene ND ug/L 04/30/18 13:58 77-47-404/26/18 20:359.8 1
Hexachloroethane ND ug/L 04/30/18 13:58 67-72-1 L204/26/18 20:354.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/30/18 13:58 193-39-504/26/18 20:354.9 1
Isophorone ND ug/L 04/30/18 13:58 78-59-104/26/18 20:359.8 1
Naphthalene 7.9 ug/L 04/30/18 13:58 91-20-304/26/18 20:354.9 1
Nitrobenzene ND ug/L 04/30/18 13:58 98-95-304/26/18 20:354.9 1
2-Nitrophenol ND ug/L 04/30/18 13:58 88-75-504/26/18 20:354.9 1
4-Nitrophenol ND ug/L 04/30/18 13:58 100-02-704/26/18 20:3549.0 1
N-Nitrosodimethylamine ND ug/L 04/30/18 13:58 62-75-904/26/18 20:354.9 1
N-Nitroso-di-n-propylamine ND ug/L 04/30/18 13:58 621-64-704/26/18 20:354.9 1
N-Nitrosodiphenylamine ND ug/L 04/30/18 13:58 86-30-604/26/18 20:359.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/30/18 13:58 108-60-104/26/18 20:354.9 1
Pentachlorophenol ND ug/L 04/30/18 13:58 87-86-504/26/18 20:359.8 1
Phenanthrene ND ug/L 04/30/18 13:58 85-01-804/26/18 20:354.9 1
Phenol ND ug/L 04/30/18 13:58 108-95-204/26/18 20:354.9 1
Pyrene ND ug/L 04/30/18 13:58 129-00-004/26/18 20:354.9 1
1,2,4-Trichlorobenzene ND ug/L 04/30/18 13:58 120-82-104/26/18 20:354.9 1
2,4,6-Trichlorophenol ND ug/L 04/30/18 13:58 88-06-204/26/18 20:359.8 1
Surrogates
Nitrobenzene-d5 (S)42 %04/30/18 13:58 4165-60-004/26/18 20:3510-120 1
2-Fluorobiphenyl (S)38 %04/30/18 13:58 321-60-804/26/18 20:3515-120 1
Terphenyl-d14 (S)298 %04/30/18 13:58 1718-51-0 S004/26/18 20:3511-131 1
Phenol-d6 (S)14 %04/30/18 13:58 13127-88-304/26/18 20:3510-120 1
2-Fluorophenol (S)21 %04/30/18 13:58 367-12-404/26/18 20:3510-120 1
2,4,6-Tribromophenol (S)61 %04/30/18 13:58 118-79-604/26/18 20:3510-137 1
Tentatively Identified Compounds
Naphthalene, 2,7-dimethy 11.4J ug/L 04/30/18 13:58 582-16-1 N04/26/18 20:351
Naphthalene, 1,3-dimethy 11.5J ug/L 04/30/18 13:58 575-41-7 N04/26/18 20:351
Naphthalene, 2,7-dimethy 10.3J ug/L 04/30/18 13:58 582-16-1 N04/26/18 20:351
Hexadecane 8.7J ug/L 04/30/18 13:58 544-76-3 N04/26/18 20:351
Heptadecane 5.2J ug/L 04/30/18 13:58 629-78-7 N04/26/18 20:351
Analytical Method: SM 6200B602 Volatiles by Method 6200
Benzene ND ug/L 05/03/18 06:04 71-43-21.0 1
Chlorobenzene ND ug/L 05/03/18 06:04 108-90-71.0 1
1,2-Dichlorobenzene ND ug/L 05/03/18 06:04 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 05/03/18 06:04 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 05/03/18 06:04 106-46-71.0 1
Diisopropyl ether ND ug/L 05/03/18 06:04 108-20-31.0 1
Ethylbenzene 1.1 ug/L 05/03/18 06:04 100-41-41.0 1
Isopropylbenzene (Cumene)ND ug/L 05/03/18 06:04 98-82-81.0 1
Methyl-tert-butyl ether ND ug/L 05/03/18 06:04 1634-04-41.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 8 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Sample:HT-GW Lab ID:92382378002 Collected:04/25/18 11:31 Received:04/26/18 10:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B602 Volatiles by Method 6200
Naphthalene 8.6 ug/L 05/03/18 06:04 91-20-32.0 1
Toluene ND ug/L 05/03/18 06:04 108-88-31.0 1
m&p-Xylene 2.9 ug/L 05/03/18 06:04 179601-23-12.0 1
o-Xylene 3.1 ug/L 05/03/18 06:04 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %05/03/18 06:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %05/03/18 06:04 17060-07-070-130 1
Toluene-d8 (S)101 %05/03/18 06:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 9 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
408497
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92382378001, 92382378002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2266494
Associated Lab Samples:92382378001, 92382378002
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N204/30/18 15:09
Aliphatic (C09-C12)ug/L ND 50.0 N204/30/18 15:09
Aromatic (C09-C10)ug/L ND 50.0 N204/30/18 15:09
4-Bromofluorobenzene (FID) (S)%115 70-130 04/30/18 15:09
4-Bromofluorobenzene (PID) (S)%111 70-130 04/30/18 15:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2266495LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2266496
Aliphatic (C05-C08)ug/L 329 N230011070-130108324 1 25
Aliphatic (C09-C12)ug/L 334 N230011130-130112335 0 25
Aromatic (C09-C10)ug/L 112 N210011270-130111111 1 25
4-Bromofluorobenzene (FID) (S)%122 70-130121
4-Bromofluorobenzene (PID) (S)%121 70-130120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 10 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
408970
SM 6200B
SM 6200B
602 by 6200B
Associated Lab Samples:92382378001, 92382378002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2268983
Associated Lab Samples:92382378001, 92382378002
Matrix:Water
Analyzed
1,2-Dichlorobenzene ug/L ND 1.0 05/03/18 05:16
1,3-Dichlorobenzene ug/L ND 1.0 05/03/18 05:16
1,4-Dichlorobenzene ug/L ND 1.0 05/03/18 05:16
Benzene ug/L ND 1.0 05/03/18 05:16
Chlorobenzene ug/L ND 1.0 05/03/18 05:16
Diisopropyl ether ug/L ND 1.0 05/03/18 05:16
Ethylbenzene ug/L ND 1.0 05/03/18 05:16
Isopropylbenzene (Cumene)ug/L ND 1.0 05/03/18 05:16
m&p-Xylene ug/L ND 2.0 05/03/18 05:16
Methyl-tert-butyl ether ug/L ND 1.0 05/03/18 05:16
Naphthalene ug/L ND 2.0 05/03/18 05:16
o-Xylene ug/L ND 1.0 05/03/18 05:16
Toluene ug/L ND 1.0 05/03/18 05:16
1,2-Dichloroethane-d4 (S)%91 70-130 05/03/18 05:16
4-Bromofluorobenzene (S)%95 70-130 05/03/18 05:16
Toluene-d8 (S)%101 70-130 05/03/18 05:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2268984LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 44.250 88 60-140
1,3-Dichlorobenzene ug/L 43.750 87 60-140
1,4-Dichlorobenzene ug/L 42.450 85 60-140
Benzene ug/L 47.650 95 60-140
Chlorobenzene ug/L 51.450 103 60-140
Diisopropyl ether ug/L 42.650 85 60-140
Ethylbenzene ug/L 48.150 96 60-140
Isopropylbenzene (Cumene)ug/L 48.850 98 60-140
m&p-Xylene ug/L 98.4100 98 60-140
Methyl-tert-butyl ether ug/L 40.950 82 60-140
Naphthalene ug/L 42.350 85 60-140
o-Xylene ug/L 49.950 100 60-140
Toluene ug/L 50.750 101 60-140
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Huntersville, NC 28078
[phone]
Page 11 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2268985MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92382378001
2268986
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 96 60-14098 320ND19.1 19.6
1,3-Dichlorobenzene ug/L 20 96 60-14098 220ND19.1 19.6
1,4-Dichlorobenzene ug/L 20 92 60-14096 520ND18.3 19.2
Benzene ug/L 20 103 60-140107 420ND20.6 21.4
Chlorobenzene ug/L 20 112 60-140113 120ND22.5 22.7
Diisopropyl ether ug/L 20 91 60-14092 120ND18.2 18.4
Ethylbenzene ug/L 20 108 60-140109 120ND21.6 21.8
Isopropylbenzene (Cumene)ug/L 20 108 60-140108 120ND21.5 21.6
m&p-Xylene ug/L 40 109 60-140109 040ND43.8 43.7
Methyl-tert-butyl ether ug/L 20 88 60-14091 320ND17.6 18.1
Naphthalene ug/L 20 89 60-14090 020ND17.9 17.9
o-Xylene ug/L 20 107 60-140109 220ND21.4 21.7
Toluene ug/L 20 111 60-140114 320ND22.2 22.8
1,2-Dichloroethane-d4 (S)%91 70-13093
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 12 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
407970
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92382378001, 92382378002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2263603
Associated Lab Samples:92382378001, 92382378002
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 04/26/18 16:42
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 04/26/18 16:42
2,4,6-Trichlorophenol ug/L ND 10.0 04/26/18 16:42
2,4-Dichlorophenol ug/L ND 5.0 04/26/18 16:42
2,4-Dimethylphenol ug/L ND 10.0 04/26/18 16:42
2,4-Dinitrophenol ug/L ND 50.0 04/26/18 16:42
2,4-Dinitrotoluene ug/L ND 5.0 04/26/18 16:42
2,6-Dinitrotoluene ug/L ND 5.0 04/26/18 16:42
2-Chloronaphthalene ug/L ND 5.0 04/26/18 16:42
2-Chlorophenol ug/L ND 5.0 04/26/18 16:42
2-Nitrophenol ug/L ND 5.0 04/26/18 16:42
3,3'-Dichlorobenzidine ug/L ND 25.0 04/26/18 16:42
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/26/18 16:42
4-Bromophenylphenyl ether ug/L ND 5.0 04/26/18 16:42
4-Chloro-3-methylphenol ug/L ND 5.0 04/26/18 16:42
4-Chlorophenylphenyl ether ug/L ND 5.0 04/26/18 16:42
4-Nitrophenol ug/L ND 50.0 04/26/18 16:42
Acenaphthene ug/L ND 5.0 04/26/18 16:42
Acenaphthylene ug/L ND 5.0 04/26/18 16:42
Anthracene ug/L ND 5.0 04/26/18 16:42
Benzo(a)anthracene ug/L ND 5.0 04/26/18 16:42
Benzo(a)pyrene ug/L ND 5.0 04/26/18 16:42
Benzo(b)fluoranthene ug/L ND 5.0 04/26/18 16:42
Benzo(g,h,i)perylene ug/L ND 5.0 04/26/18 16:42
Benzo(k)fluoranthene ug/L ND 5.0 04/26/18 16:42
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/26/18 16:42
bis(2-Chloroethyl) ether ug/L ND 5.0 04/26/18 16:42
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/26/18 16:42
Butylbenzylphthalate ug/L ND 5.0 04/26/18 16:42
Chrysene ug/L ND 5.0 04/26/18 16:42
Di-n-butylphthalate ug/L ND 5.0 04/26/18 16:42
Di-n-octylphthalate ug/L ND 5.0 04/26/18 16:42
Dibenz(a,h)anthracene ug/L ND 5.0 04/26/18 16:42
Diethylphthalate ug/L ND 5.0 04/26/18 16:42
Dimethylphthalate ug/L ND 5.0 04/26/18 16:42
Fluoranthene ug/L ND 5.0 04/26/18 16:42
Fluorene ug/L ND 5.0 04/26/18 16:42
Hexachloro-1,3-butadiene ug/L ND 5.0 04/26/18 16:42
Hexachlorobenzene ug/L ND 5.0 04/26/18 16:42
Hexachlorocyclopentadiene ug/L ND 10.0 04/26/18 16:42
Hexachloroethane ug/L ND 5.0 04/26/18 16:42
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Huntersville, NC 28078
[phone]
Page 13 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2263603
Associated Lab Samples:92382378001, 92382378002
Matrix:Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/26/18 16:42
Isophorone ug/L ND 10.0 04/26/18 16:42
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/26/18 16:42
N-Nitrosodimethylamine ug/L ND 5.0 04/26/18 16:42
N-Nitrosodiphenylamine ug/L ND 10.0 04/26/18 16:42
Naphthalene ug/L ND 5.0 04/26/18 16:42
Nitrobenzene ug/L ND 5.0 04/26/18 16:42
Pentachlorophenol ug/L ND 10.0 04/26/18 16:42
Phenanthrene ug/L ND 5.0 04/26/18 16:42
Phenol ug/L ND 5.0 04/26/18 16:42
Pyrene ug/L ND 5.0 04/26/18 16:42
2,4,6-Tribromophenol (S)%70 10-137 04/26/18 16:42
2-Fluorobiphenyl (S)%59 15-120 04/26/18 16:42
2-Fluorophenol (S)%30 10-120 04/26/18 16:42
Nitrobenzene-d5 (S)%63 10-120 04/26/18 16:42
Phenol-d6 (S)%19 10-120 04/26/18 16:42
Terphenyl-d14 (S)%51 11-131 04/26/18 16:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2263604LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 23.250 46 44-142
2,2'-Oxybis(1-chloropropane)ug/L 27.650 55 36-166
2,4,6-Trichlorophenol ug/L 39.950 80 37-144
2,4-Dichlorophenol ug/L 39.350 79 1-191
2,4-Dimethylphenol ug/L 40.350 81 32-119
2,4-Dinitrophenol ug/L 166250 67 1-181
2,4-Dinitrotoluene ug/L 39.050 78 39-139
2,6-Dinitrotoluene ug/L 39.750 79 50-158
2-Chloronaphthalene ug/L 31.550 63 60-118
2-Chlorophenol ug/L 32.450 65 23-134
2-Nitrophenol ug/L 38.750 77 29-182
3,3'-Dichlorobenzidine ug/L 74.1100 74 1-262
4,6-Dinitro-2-methylphenol ug/L 101100 101 1-181
4-Bromophenylphenyl ether ug/L 36.150 72 53-127
4-Chloro-3-methylphenol ug/L 72.3100 72 22-147
4-Chlorophenylphenyl ether ug/L 33.550 67 25-158
4-Nitrophenol ug/L 72.3250 29 1-132
Acenaphthene ug/L 34.550 69 47-145
Acenaphthylene ug/L 34.750 69 33-145
Anthracene ug/L 38.650 77 1-166
Benzo(a)anthracene ug/L 38.850 78 33-143
Benzo(a)pyrene ug/L 37.050 74 17-163
Benzo(b)fluoranthene ug/L 37.050 74 24-159
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 14 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2263604LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(g,h,i)perylene ug/L 34.950 70 1-219
Benzo(k)fluoranthene ug/L 37.350 75 11-162
bis(2-Chloroethoxy)methane ug/L 33.150 66 33-184
bis(2-Chloroethyl) ether ug/L 33.150 66 12-158
bis(2-Ethylhexyl)phthalate ug/L 36.050 72 8-158
Butylbenzylphthalate ug/L 36.250 72 1-152
Chrysene ug/L 39.250 78 17-168
Di-n-butylphthalate ug/L 36.550 73 1-118
Di-n-octylphthalate ug/L 41.650 83 4-146
Dibenz(a,h)anthracene ug/L 36.850 74 1-227
Diethylphthalate ug/L 37.350 75 1-114
Dimethylphthalate ug/L 36.150 72 1-112
Fluoranthene ug/L 38.750 77 26-137
Fluorene ug/L 37.250 74 59-121
Hexachloro-1,3-butadiene ug/L 18.750 37 24-116
Hexachlorobenzene ug/L 39.150 78 1-152
Hexachlorocyclopentadiene ug/L 28.450 57 25-150
Hexachloroethane ug/L 15.2 L2503040-113
Indeno(1,2,3-cd)pyrene ug/L 35.650 71 1-171
Isophorone ug/L 33.550 67 21-196
N-Nitroso-di-n-propylamine ug/L 34.350 69 1-230
N-Nitrosodimethylamine ug/L 20.550 41 25-150
N-Nitrosodiphenylamine ug/L 36.950 74 25-150
Naphthalene ug/L 26.850 54 21-133
Nitrobenzene ug/L 31.250 62 35-180
Pentachlorophenol ug/L 87.6100 88 14-176
Phenanthrene ug/L 37.950 76 54-120
Phenol ug/L 14.850 30 5-112
Pyrene ug/L 40.150 80 52-115
2,4,6-Tribromophenol (S)%83 10-137
2-Fluorobiphenyl (S)%69 15-120
2-Fluorophenol (S)%35 10-120
Nitrobenzene-d5 (S)%65 10-120
Phenol-d6 (S)%25 10-120
Terphenyl-d14 (S)%52 11-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2263605MATRIX SPIKE SAMPLE:
MSSpike
Result
92382071001
1,2,4-Trichlorobenzene ug/L 30.949 63 44-142ND
2,2'-Oxybis(1-chloropropane)ug/L 27.649 56 36-166ND
2,4,6-Trichlorophenol ug/L 40.449 82 37-144ND
2,4-Dichlorophenol ug/L 42.649 87 1-191ND
2,4-Dimethylphenol ug/L 51.849 93 32-119ND
2,4-Dinitrophenol ug/L 196245 80 1-181ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
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Page 15 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2263605MATRIX SPIKE SAMPLE:
MSSpike
Result
92382071001
2,4-Dinitrotoluene ug/L 40.149 82 39-139ND
2,6-Dinitrotoluene ug/L 38.149 78 50-158ND
2-Chloronaphthalene ug/L 33.749 69 60-118ND
2-Chlorophenol ug/L 32.849 67 23-134ND
2-Nitrophenol ug/L 42.549 87 29-182ND
3,3'-Dichlorobenzidine ug/L 59.098 60 1-262ND
4,6-Dinitro-2-methylphenol ug/L 10298 104 1-181ND
4-Bromophenylphenyl ether ug/L 36.649 75 53-127ND
4-Chloro-3-methylphenol ug/L 76.898 78 22-147ND
4-Chlorophenylphenyl ether ug/L 35.249 72 25-158ND
4-Nitrophenol ug/L 73.4245 30 1-132ND
Acenaphthene ug/L 36.149 74 47-145ND
Acenaphthylene ug/L 36.349 74 33-145ND
Anthracene ug/L 39.149 80 1-166ND
Benzo(a)anthracene ug/L 37.949 77 33-143ND
Benzo(a)pyrene ug/L 37.249 76 17-163ND
Benzo(b)fluoranthene ug/L 36.849 75 24-159ND
Benzo(g,h,i)perylene ug/L 34.949 71 1-219ND
Benzo(k)fluoranthene ug/L 36.449 74 11-162ND
bis(2-Chloroethoxy)methane ug/L 36.249 74 33-184ND
bis(2-Chloroethyl) ether ug/L 32.549 66 12-158ND
bis(2-Ethylhexyl)phthalate ug/L 34.249 70 8-158ND
Butylbenzylphthalate ug/L 35.549 72 1-152ND
Chrysene ug/L 38.349 78 17-168ND
Di-n-butylphthalate ug/L 37.249 76 1-118ND
Di-n-octylphthalate ug/L 39.349 80 4-146ND
Dibenz(a,h)anthracene ug/L 36.249 74 1-227ND
Diethylphthalate ug/L 37.149 76 1-114ND
Dimethylphthalate ug/L 36.349 74 1-112ND
Fluoranthene ug/L 40.149 82 26-137ND
Fluorene ug/L 38.049 78 59-121ND
Hexachloro-1,3-butadiene ug/L 27.049 55 24-116ND
Hexachlorobenzene ug/L 37.849 77 1-152ND
Hexachlorocyclopentadiene ug/L 35.049 71 25-150ND
Hexachloroethane ug/L 36.749 75 40-113ND
Indeno(1,2,3-cd)pyrene ug/L 35.549 72 1-171ND
Isophorone ug/L 35.849 73 21-196ND
N-Nitroso-di-n-propylamine ug/L 34.649 71 1-230ND
N-Nitrosodimethylamine ug/L 23.849 49 25-150ND
N-Nitrosodiphenylamine ug/L 36.849 75 25-150ND
Naphthalene ug/L 52.349 68 21-13318.9
Nitrobenzene ug/L 35.249 72 35-180ND
Pentachlorophenol ug/L 94.598 96 14-176ND
Phenanthrene ug/L 37.549 76 54-120ND
Phenol ug/L 13.649 28 5-112ND
Pyrene ug/L 37.749 77 52-115ND
2,4,6-Tribromophenol (S)%81 10-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
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Page 16 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2263605MATRIX SPIKE SAMPLE:
MSSpike
Result
92382071001
2-Fluorobiphenyl (S)%70 15-120
2-Fluorophenol (S)%33 10-120
Nitrobenzene-d5 (S)%73 10-120
Phenol-d6 (S)%22 10-120
Terphenyl-d14 (S)%44 11-131
Parameter Units
Dup
Result QualifiersRPDResult
92382072001
2263606SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L NDND
2,2'-Oxybis(1-chloropropane)ug/L NDND
2,4,6-Trichlorophenol ug/L NDND
2,4-Dichlorophenol ug/L NDND
2,4-Dimethylphenol ug/L NDND
2,4-Dinitrophenol ug/L NDND
2,4-Dinitrotoluene ug/L NDND
2,6-Dinitrotoluene ug/L NDND
2-Chloronaphthalene ug/L NDND
2-Chlorophenol ug/L NDND
2-Nitrophenol ug/L NDND
3,3'-Dichlorobenzidine ug/L NDND
4,6-Dinitro-2-methylphenol ug/L NDND
4-Bromophenylphenyl ether ug/L NDND
4-Chloro-3-methylphenol ug/L NDND
4-Chlorophenylphenyl ether ug/L NDND
4-Nitrophenol ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
bis(2-Chloroethoxy)methane ug/L NDND
bis(2-Chloroethyl) ether ug/L NDND
bis(2-Ethylhexyl)phthalate ug/L NDND
Butylbenzylphthalate ug/L NDND
Chrysene ug/L NDND
Di-n-butylphthalate ug/L NDND
Di-n-octylphthalate ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Diethylphthalate ug/L NDND
Dimethylphthalate ug/L NDND
Fluoranthene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92382072001
2263606SAMPLE DUPLICATE:
Fluorene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Hexachlorobenzene ug/L NDND
Hexachlorocyclopentadiene ug/L NDND
Hexachloroethane ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Isophorone ug/L NDND
N-Nitroso-di-n-propylamine ug/L NDND
N-Nitrosodimethylamine ug/L NDND
N-Nitrosodiphenylamine ug/L NDND
Naphthalene ug/L NDND
Nitrobenzene ug/L NDND
Pentachlorophenol ug/L NDND
Phenanthrene ug/L NDND
Phenol ug/L NDND
Pyrene ug/L NDND
2,4,6-Tribromophenol (S)%60 865
2-Fluorobiphenyl (S)%52 053
2-Fluorophenol (S)%27 626
Nitrobenzene-d5 (S)%55 155
Phenol-d6 (S)%21 1817
Terphenyl-d14 (S)%27 4341
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
408442
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92382378002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2266217
Associated Lab Samples:92382378002
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N204/30/18 17:12
Aliphatic (C19-C36)ug/L ND 100 N204/30/18 17:12
Aromatic (C11-C22)ug/L ND 100 N204/30/18 17:12
2-Bromonaphthalene (S)%71 40-140 04/30/18 17:12
2-Fluorobiphenyl (S)%77 40-140 04/30/18 17:12
Nonatriacontane (S)%80 40-140 04/30/18 17:12
o-Terphenyl (S)%69 40-140 04/30/18 17:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2266218LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2266219
Aliphatic (C09-C18)ug/L 155 N23005240-14048143 8 50
Aliphatic (C19-C36)ug/L 224 N24005640-14054215 4 50
Aromatic (C11-C22)ug/L 519 N28506140-14059505 3 50
2-Bromonaphthalene (S)%65 40-14062
2-Fluorobiphenyl (S)%63 40-14060
Nonatriacontane (S)%72 40-14060
o-Terphenyl (S)%75 40-14071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
409551
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92382378001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2272014
Associated Lab Samples:92382378001
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N205/07/18 13:01
Aliphatic (C19-C36)ug/L ND 100 N205/07/18 13:01
Aromatic (C11-C22)ug/L ND 100 N205/07/18 13:01
2-Bromonaphthalene (S)%73 40-140 05/07/18 13:01
2-Fluorobiphenyl (S)%71 40-140 05/07/18 13:01
Nonatriacontane (S)%67 40-140 05/07/18 13:01
o-Terphenyl (S)%65 40-140 05/07/18 13:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2272015LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2272016
Aliphatic (C09-C18)ug/L 187 N23006240-14059177 6 50
Aliphatic (C19-C36)ug/L 277 N24006940-14065261 6 50
Aromatic (C11-C22)ug/L 539 N28506340-14068576 7 50
2-Bromonaphthalene (S)%59 40-14066
2-Fluorobiphenyl (S)%66 40-14070
Nonatriacontane (S)%67 40-14066
o-Terphenyl (S)%69 40-14071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 25
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92382378
3201 Charles Blvd
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 25
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92382378
3201 Charles Blvd
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92382378001 409551 409671FT-GW MADEP EPH MADEP EPH
92382378002 408442 408556HT-GW MADEP EPH MADEP EPH
92382378001 408497FT-GW MADEP VPH
92382378002 408497HT-GW MADEP VPH
92382378001 407970 408107FT-GW EPA 625 EPA 625
92382378002 407970 408107HT-GW EPA 625 EPA 625
92382378001 408970FT-GW SM 6200B
92382378002 408970HT-GW SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/08/2018 02:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 25
Page 23 of 25
Page 24 of 25
Page 25 of 25

APPENDIX C
Photographs

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 1 The contents of the Residential Tank being pumped.
Photo 2 The contents of the Farm Tank being pumped after it had been uncovered.

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 3 The Residential Tank being removed.
Photo 4 The Farm Tank being removed.

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 5 Groundwater in the tank pit of the Farm Tank after the tank was removed.
Photo 6 Groundwater in the tank pit of the Residential Tank after the tank was removed.

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 7 Looking across the area of where the Farm Tank was located (between the pecan tree and the excavator in this photo).
Photo 8 Looking across the area of where the Residential Tank was located (between the tree and house in this photo).

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 9 The Farm Tank pit after it had been backfilled.
Photo 10 The Residential Tank pit after it had been backfilled.

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 11 Temporary well FT-GW installed in the tank pit for the Farm Tank.
Photo 12 Drilling occurring for temporary well HT-GW for the Residential Tank.

Farm Tank and Residential Tank
Greenville, North Carolina
Terracon Project No. 72227042
Photos Dated: April 18, 2018 and April 25, 2018

Responsive ■ Resourceful ■ Reliable
Photo 13 Temporary well HT-GW after it had been installed in the Residential Tank pit.