WA-29026_48218_CA_RPTS_20220517_LSA

An Equal Opportunity Employer

May 17, 2022

Ms. Sylvia Hunneke
NCDEQ, UST Section
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Phase I LSA Report
Speedway #8654
5068 NC Highway 33 East
Greenville, Pitt County, NC
Incident Number: 38440
GRI Project Number: 3389

Dear Ms. Hunneke,

Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do
not hesitate to contact Nicole Long with Geological Resources, Inc. at 704-845-4010.

Sincerely,
Speedway, LLC.

Chuck Chiara
Manager, Environmental Services

Enclosure

Speedway LLC

Speedway Office
P.O. Box 1500
Springfield, OH 45501
Telephone [phone]

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Phase I Limited Site Assessment Report
Speedway #8654
5068 NC Highway 33 East
Greenville, Pitt County
North Carolina
Facility ID Number: 0-036281
Incident Number: 48218
GRI Project Number: 3389

Prepared for:

Charles Chiara
Speedway, LLC
500 Speedway Drive
Enon, Ohio 45323

May 17, 2022

Nicole Long
Senior Account Project Manager
Eric Eubanks, G.I.T.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
i
EXECUTIVE SUMMARY
The Speedway #8654 site is located at 5068 NC Highway 33 East in Greenville, Pitt County, North Carolina.
The property operates as a petroleum retail facility and convenience store. The site is covered by concrete
and grass. There are one 12,000-gallon gasoline, two 6,000-gallon gasoline, and one 6,000-gallon diesel
USTs currently in use at the site with eight associated dispenser islands. The surrounding properties are
residential, agricultural, and commercial.

On September 29, 2021, during triennial hydrostatic testing activities, one non-passing spill bucket was
reported for the 6,000-gallon diesel UST. GRI conducted a site check at the subject site on December 2,
2021. One soil sample (DSL-2’) was collected approximately 2 feet BGS beneath the non-passing spill
bucket. The RALs were below the TPH-GRO and TPH-DRO concentrations. No free product was noted at
the site. The non-passing spill bucket was replaced and received passing compliance testing results on
December 2, 2021. Site Check results identified a release at the site and an LSA was required.

An updated receptor survey was conducted on April 26, 2022. One water supply well was identified within
a 1,500-foot radius of the site. The water supply well is within a 500-foot radius of the site but is in
disrepair and is not usable. The residence is connected to public water. Public water is available to the
subject site and to all surrounding properties. An unnamed creek was identified along the western
boundary of the property.

On April 25, 2022, one Type II monitoring well (MW-3) was installed in the vicinity of the non-passing
diesel UST spill bucket. A soil sample (MW-3-2’) was collected approximately 2 feet BGS during the
installation of monitoring well MW-3. All contaminant concentrations reported in soil sample MW-3-2’
were below the applicable standards.

On April 25, 2022, a ground water sample was collected from MW-3. The MAC was below the
concentration of lead reported in the ground water sample collected from MW-3. All reported
contaminant concentrations were below the GCLs and ten times the 2B Standards. No free product was
observed at the site.

Based on the lack of observed water supply wells within 1,500 feet of the source area and all reported
contaminant concentrations being below the GCLs, the site risk classification should be Low. The MAC for
lead was below the concentration reported in the ground water sample collected from MW-3; however,
it is interpreted that the concentration of lead is naturally occurring. Therefore, the incident should be
granted an NFA and closed under the existing NRP.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
ii
SITE INFORMATION
1. Site Identification
 Speedway #8654 (Facility ID 0-036281)
 Incident Number 48218 – Risk Classification Pending
 Location of Source Area: 5068 NC Highway 33 East
Greenville, NC 27858
Pitt County (Figure 1)
35.5834070°N, 77.2867350°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST/AST Owner
Speedway, LLC (Table 1)
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069

UST/AST Operator
Speedway, LLC
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069

Property Owner
Williams Family Heirs, LLC
539 South Main Street
Findlay, Ohio 45840
Email Unknown
Phone No. Unknown

Property Occupant
Speedway, LLC
500 Speedway Drive
Enon, OH 45323
[e-mail]
919-516-8069
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Pace Analytical
12065 Lebanon Road
Mt. Juliet, TN 37122
State Certification No. 375
615-758-5858
3. Information about Release
 Release was discovered on December 2, 2021
 An unknown amount of product was released from the UST System via a non-passing spill bucket
 One 12,000-gallon gasoline UST, two 6,000-gallon gasoline USTs, and one 6,000-gallon diesel UST are in
use at the site

Certification:

I, John M. Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................7
6. LIMITATIONS ........................................................................................................................8

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Soil Quality Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Pitt County Property Cards
Appendix B: Well Construction Record and Subsurface Log
Appendix C: State Correspondence
Appendix D: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? YES

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? NO

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? YES

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? NO
If YES, describe.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
2
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility for the foreseeable future.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
3
7. What is the zoning status of the property?
According to the Village of Simpson Official Zoning Map, the site is zoned GB (General Business
District).

8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and is
likely remain a convenience store for the foreseeable future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 5076 NC Highway 33 East, located approximately 40 feet east of
the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

A baseball field is located at 5273 NC Highway 33 East, approximately 2,700 feet east-northeast
of the source area at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Village of Simpson Official Zoning Map, the surrounding areas are zoned
Agricultural-Residential (AR), Neighborhood-Residential (NR), Single Family Residential (SFR) and
General Business (GB).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, agricultural, and residential. Land use
information has been included as Table 3. A zoning map has been included as Figure 3B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
An updated receptor survey was conducted on April 26, 2022. One non-potable water supply well
(WSW-1) was identified within a 1,500-foot radius of the site. The water supply well is
approximately 460’ southeast of the site but is in disrepair and is not usable. A Site Location Map

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
4
is provided as Figure 1 and a Site Vicinity Map showing property boundaries for the site and
surrounding properties has been included as Figure 3A. Water supply well information has been
provided in Table 4.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by Eastern Pines Water Corporation.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
A drainage creek borders the western property boundary of the site. The creek flows north into
the Tar River.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On April 29, 2022, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is in the Coastal Plain Physiographic Region. Surficial soils at the site overlie the confining
unit of the Yorktown Formation.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along NC Highway 33 East and several underground utility
lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property cards for the adjacent property owners are attached as Appendix A.
3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the surficial soils at the site overlie the Yorktown
Formation. The Yorktown Formation soils are described as fossiliferous clays with varying amount of fine-
grained bluish-gray sands with concentrated lenses of shell material. The depth to ground water during
the April 2022 LSA activities was approximately 2.64 feet below the top of well casing. The well

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
5
construction record and subsurface log are included as Appendix B. A Site Map is included as Figure 2.
Well construction and gauging information is presented in Table 6. A photograph of the newly installed
monitoring well is shown below:

4. SITE INVESTIGATION
On September 29, 2021, one non-passing spill bucket was reported for the 6,000-gallon diesel UST, and
on December 2, 2021, GRI conducted a site check at the subject site. One soil sample (DSL-2’) was
collected approximately 2 feet BGS beneath the non-passing spill bucket. The RALs were below the TPH-
GRO and TPH-DRO concentrations. Based on these results, an LSA was recommended in the Site Check
report.

In accordance with the NORR dated March 17, 2021, one monitoring well (MW-3) was installed by a North
Carolina licensed well contractor on April 25, 2022, to assess the identified release at the site. MW-3 was
installed to a total depth of 12 feet BGS with a 10-foot screened interval set to bracket the water table at
the time of installation. Monitoring well MW-3 was installed adjacent to the spill bucket of the 6,000-
gallon diesel UST. A copy of the NORR has been included in Appendix C.

Monitoring well MW-3 was gauged on April 26, 2022. The depth to ground water was approximately 2.64
feet below TOC. Gauging data from the April 2022 LSA activities is included in Table 6. A summary of the
current gauging data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
6
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-3 2 - 12 12 NM 2.64 NM

1. Soil Sampling:
Soil sample DSL-2’ was collected on December 2, 2021, during Site Check activities, and submitted for
laboratory analyses of TPH-GRO and TPH-DRO by EPA Method 8015D. The RALs were below the
concentrations of GRO and DRO reported in the soil sample. No free product was noted at the site.

On April 25, 2022, one soil sample (MW-3-2’) was collected at approximately 2 feet BGS during the
installation of MW-3. The soil sample was submitted for analyses of VOCs by EPA Method 8260,
SVOCs by EPA Method 8270D, and VPH/EPH by the MADEP Method.

All contaminant concentrations reported in soil sample MW-3-2’ were below the applicable
standards. A Soil Quality Map has been included as Figure 4. A summary of the soil sample analytical
results is presented in Table 7. A copy of the laboratory analytical report from the April 2022 soil
sampling event has been included in Appendix D. A copy of the current soil sampling data collected
during the LSA activities is shown below:
Sample ID Sample Depth (ft-BGS) Benzene Toluene Ethylbenzene Total Xylenes MTBE Naphthalene Soil to Water MCC (mg/kg) 0.0072 5.4 8 6 0.085 0.2
Residential SCLs (mg/kg) 12 1,250 60.3 3,120 156 5.5
MW-3-2’ 2 <0.00113 <0.00563 0.00519 0.0601 <0.00113 0.0215

2. Ground Water Sampling:
On April 26, 2022, MW-3 was gauged, purged, and sampled as required by NCDEQ. The ground water
sample was submitted for analysis of VOCs by EPA Method 6200B, SVOCs by EPA Method 625.1, EDB
by EPA Method 504.1, total lead by EPA Method 6010 and VPH/EPH by the MADEP Method. The MAC
was below the concentration of lead reported in the ground water sample collected from MW-3. All
contaminant concentrations were below the GCLs and ten times the 2B Standards. No free product
was observed at the site. A Ground Water Quality Map is included as Figure 5. A summary of the
ground water analytical data is included in Table 8. A copy of the laboratory analytical report is
included in Appendix D. A summary of the current ground water sampling data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
7
Contaminant of
Concern
 Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Lead Well
ID
MAC (µg/l) 1 600 600 500 20 6 15
10 x 2B Standard (µg/l) 510 110 1,300 6,700 15,000 120 NE
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000 15,000
MW-3 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 29.8

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. The samples were transported to a North Carolina
certified laboratory for analysis. A laboratory supplied trip blank was included in the sample cooler.
No detectable concentrations of requested method constituents were reported in the trip blank.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of agricultural, residential, and commercial properties.
 An updated receptor survey was conducted on April 26, 2022. One water supply well was
identified within a 1,500-foot radius of the site. The water supply well is within a 500-foot radius
of the site but is in disrepair and is not usable. Public water is available to the subject site and to
all surrounding properties.
 An unnamed creek was identified on the western boundary of the property.
 On April 25, 2022, one monitoring well was installed adjacent to 6,000-gallon diesel UST spill
bucket to a depth of 12 feet BGS and completed with a 10-foot screened interval.
 Soil sample MW-3-2’ was collected at approximately 2 feet BGS during the installation of MW-3.
All contaminant concentrations reported in soil sample MW-3-2’ were below the applicable
standards.
 On April 26, 2022, a ground water sample was collected from MW-3. The MAC was below the
concentration of lead reported in the ground water sample collected from MW-3. All contaminant
concentrations were below the GCLs and ten times the 2B Standards. No free product was
observed at the site.
 Based on the lack of observed water supply wells within 1,500 feet of the source area and all
reported contaminant concentrations being below the GCLs and ten times the 2B Standards, the
site risk classification should be Low. The MAC for lead was below the concentration reported in
the ground water sample collected from MW-3; however, it is interpreted that the concentration
of lead is naturally occurring. Therefore, the incident should be granted an NFA and closed under
the existing NRP.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: May 17, 2022 Speedway #8654
Project Manager: Nicole Long GRI Project No. 3389
8
6. LIMITATIONS
This report has been prepared for the exclusive use of Speedway, LLC. for specific application to the
referenced site in Pitt County, North Carolina. The assessment was conducted based on the scope of work
and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
Copyright (C) 2009 MyTopo, 2006-2018 TomTom
077.3000000° W
077.3000000° W
077.2833333° W
077.2833333° W
077.2666666° W
077.2666666° W35.6000000° N35.6000000° N35.5833333° N35.5833333° N35.5666666° N35.5666666° NSCALE 1:24000
0 1000 2000 3000 4000 5000
FEET
Declination
MN 9.98° W
MN Figure 1
Site Location Map
Speedway #8654
5068 NC Highway 33 East, Greenville
Pitt County, NC
Incident No. N/A
GRI Project No. 3389
Date: 10/29/18
Scale: 1 inch = 2,000 ft.Copyright (C) 2009 MyTopo
Location: 035.5834070° N 077.2867350° W
"J
SITE
5607905710
5607921010
5607816455
5607819284
5607913964
5607924140
5607912597
5607916941
5607914566WSW-1
NC 33
BRITTBLACK JACK-SIMPSON
C I R C L E STONE GATEEDGEBROOKVALLEYWAY
AMY ALTON VILLAGEJETHRO MILLSVINEYARDMCDONALDGARDEN GROVE
HIGH PLACE
M A R B L E
GIL
M
A
N
MILLBROOK
FIGURE 3A: SITE VICINITY MAPSPEEDWAY #8654 (FORMER WILCO HESS#1872)5068 NC HIGHWAY 33 EASTGREENVILLE, PITT COUNTYNORTH CAROLINAINCIDENT NO. 48218GRI NO. 3389
PREPARED BY:GEOLOGICAL RESOURCES, INC.APRIL 21, 2022
³
0 300150Feet1 inch = 325 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS500-FOOT RADIUS
LEGEND
"J Water Supply Well
Unnamed Creek
Greenville_Street_Centerlines
Pitt_County_Roads
Well Owner and Adjacent Properties
nc_pitt_parcels_poly
Land Use Code1
"J
SITE
WSW-1
NC 33
BRITTBLACK JACK-SIMPSON
STONE GATEC IR C L E
VALLEYWAY EDGEBROOKAMY ALTON VILLAGEVINEYARDJETHRO MILLSGARDEN GROVE
HIGH PLACE
M A R B L E
MCDONALDGIL
M
A
N
FIGURE 3B: ZONING MAPSPEEDWAY #8654 (FORMER WILCO HESS#1872)5068 NC HIGHWAY 33 EASTGREENVILLE, PITT COUNTYNORTH CAROLINAINCIDENT NO. 48218GRI NO. 3389
PREPARED BY:GEOLOGICAL RESOURCES, INC.APRIL 21, 2022
³
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS500-FOOT RADIUS
LEGEND
"J Water Supply Well
Unnamed Creek
Greenville_Street_Centerlines
Pitt_County_Roads
ZONING - GB
ZONING - AR
ZONING - SFR
ZONING - NR
nc_pitt_parcels_poly

TABLES
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
3602 Highway 264 East, Greenville, NC 27834 1-252-752-4366
5446 University Parkway, Winston-Salem, NC 27105-1366 1-800-642-0945
0-036281
Trade Oil Company 08/01/2001 - 06/01/2005
500 Speedway Drive, Enon, Ohio 45323 1-937-591-1283
0-036281
WilcoHess, LLC.06/01/2005 - 01/01/2016
TABLE 1
UST OWNER/OPERATOR INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Address Telephone Number
Name of Owner or Operator Dates of Ownership / Operation
0-036281
Speedway, LLC.01/01/2016 - Current
Address Telephone Number
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
Name of Owner or Operator Dates of Ownership / Operation
Page 1 of 1
Date: 01/19/22
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline NA 12,000 8/1/2001 Single Wall
Steel/FR 8' x 32'Other Current No
2 Gasoline NA 6,000 8/1/2001 Single Wall
Steel/FR 8' x 16'Other Current No
3 Gasoline NA 6,000 8/1/2001 Single Wall
Steel/FR 8' x 16'Other Current No
4 Diesel NA 6,000 8/1/2001 Single Wall
Steel/FR 8' x 16'Other Current Yes
UST
ID
No.
TABLE 2
UST SYSTEM INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Facility ID #: 0-036281
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 05/10/22 Facility ID # : 0-036281
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a GB General Business
District n/a n/a
n/a SFR Single Family Residential n/a n/a
n/a AR Agricultural-Residential n/a n/a
n/a NR Neighborhood-
Residential n/a n/a
Note:
• Properties are keyed to Figure 3A.
TABLE 3
LAND USE INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Page 1 of 1
Facility ID # : 0-036281
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
WSW-1 14268 Brown, Annie M. and Ebron, Tonya
S.P.O. Box 27 Simpson, NC 27879 376 Black Jack Simpson Road Inactive Non-Potable
Inactive Yes Yes ~450 SE
Receptor
ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
1 n/a Down ~225 W
Notes:
• Receptors are shown on Figure 3A.
• n/a: not applicable.
Unnamed Creek Runs along the western portion of the site in a culvert and continues north
of the site into the Tar River n/a Drainage
Description Location Contact/Phone Number Usage
Unknown
TABLE 4
RECEPTOR INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Date: 09/11/15
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
Page 1 of 1
Date: 03/29/19 Facility ID #: 0-036281
PIN Number Property Owner Name Property Owner Address
5607912597 (site)Williams Family Heirs, LLC 539 South Main Street
Findlay, OH 45840
5607816455 Speight, Maxine A.4761 NC Hwy 33 E Suite A
Greenville, NC 27858
5607905710 Brown, Annie M. and Ebron, Tonya
S.P.O. Box 27 Simpson, NC 27879
5607914566 Trade Land Company, LLC 3675 Marine Drive Greenville, NC
27834
5607819284 Trade Land Company, LLC 3675 Marine Drive Greenville, NC
27834
5607913964 Randolph, Benedict Boswell Jr. and
Randolph, Karina Robles 5063 NC 33 E Greenville, NC 27858
5607924140 Randolph, Benedict Boswell Jr. and
Randolph, Karina Robles 5063 NC 33 E Greenville, NC 27858
5607921010 Rodgers, Eugene L. and Rodgers,
Melanie G.
209 Edgebrook Dr. Greenville, NC
27858
5607916941 Wagoner, Keith R. and Wagoner,
Victoria A.
254 Brown Farm Dr. Greenville, NC
27858
Note:
• Properties are keyed to Figure 3A.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Page 1 of 1
Date: 05/2/22 Facility ID #: 0-036281
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
MW-1 01/21/14 01/21/14 2 2 - 12 12 NM 2.03 ---NM Abandoned
MW-2 06/17/19 06/17/19 2 2 - 12 12 NM 2.40 ---NM Abandoned
MW-3 04/25/22 04/26/22 2 2 - 12 12 NM 2.64 ---NM
Notes:
• ft BGS : feet below ground surface.
• NM: Not measured.
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
SPEEDWAY #8654 (INCIDENT NO. 48218)
Page 1 of 1
Date: 05/09/22
Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)Gasoline-Range TPHDiesel-Range TPHBenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthalene1-Methylnaphthalene2-MethylnaphthaleneUnadjusted C9-C18 AliphaticsUnadjusted C19-C36 AliphaticsC11-C22 AromaticsC5-C8 AliphaticsC9-C12 AliphaticsUnadjusted C9-C10 Aromatics50 100 NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0072 5.4 8 6 0.085 0.2 0.054 1.5 540 NE 31 68 540 31
NE NE 12 1,250 60.3 3,120 156 5.5 22.8 62.5 1,560 31,200 469 625 1,560 469
MW-1 (2')01/21/14 2 NR NR 0.0488 0.0105 0.0271 0.159 <0.065 0.0038 J NR <0.018 <5.7 <5.7 <8.5 <2.3 <2.3 <2.3
SB-1 3'10/10/18 3 13.3 NR 0.00834 0.0110 0.0552 0.322 NR NR NR NR NR NR NR NR NR NR
SB-2 3'10/10/18 3 28.9 NR 0.358 0.537 0.353 2.39 NR NR NR NR NR NR NR NR NR NR
SB-3 3'10/10/18 3 8.69 NR 0.917 0.243 0.289 1.03 NR NR NR NR NR NR NR NR NR NR
DSL-2'12/02/21 2 963 891 NR NR NR NR NR NR NR NR NR NR NR NR NR NR
MW-3-2'04/25/22 2 NR NR <0.00113 <0.00563 0.00519 0.0601 <0.00113 0.0215 <0.0352 <0.0352 <6.88 <6.88 <6.88 <5.58 <5.58 <5.58
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• J: Estimated Value
• B: Indicates analyte found in associated method blank
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• Concentrations in bold face type indicate the RALs or soil to water MCCs were below the reported concentrations.
• Concentrations in italic type indicate that Residential SCLs were below the reported concentrations.
• NE: Not Established
• NR: Not Requested.
Facility ID #: 0-036281
TABLE 7
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
SPEEDWAY #8654 (INCIDENT NO. 48218)
Analytical Method 5030/ 8015D/ UVF EPA Method 8260B MADEP EPH MADEP VPH
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
EPA Method 8270D
Page 1 of 1
Date: 05/10/22 Facility ID #: 0-036281
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 1 30 0.02 15 700 10,000 200 400 700 200
510 110 1,300 6,700 15,000 120 8 850 1.0 NE 1,800 (S)2,100 (S)40,000 (S)1,250 (S)1,800 (S)40,000 (S)
5,000 260,000 80,000 50,000 20,000 6,000 1,000 12,000 50 15,000 NE NE NE NE NE NE
MW-1 01/21/14 1.4 0.55 1.4 8.9 <0.10 0.12 J NR <0.53 <0.0094 263 <100 109 J <150 <35 <35 <35
MW-2 06/17/19 540 112 156 530 <1.00 9.24 NR NR NR NR NR NR NR NR NR NR
MW-3 04/26/22 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <0.0216 29.8 <100 <100 <100 <100 <100 <100
10/10/18 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 NR NR NR NR NR NR NR NR NR NR
06/17/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 NR NR NR NR NR NR NR NR NR NR
04/25/22 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Results in italics indicate the GCLs were below the reported concentrations.
• J: Estimated value.
• NE: Not established.
• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not reported.
GCL (μg/l)
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.Unadjusted C9-C18 AliphaticsUnadjusted C19-C36 AliphaticsC11-C22 AromaticsLeadTrip Blank
MAC (μg/l)
10 x 2B Standard (µg/l)Naphthalene1-Methylnaphthalene2-MethylnaphthaleneTABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SPEEDWAY #8654 (INCIDENT NO. 48218)
Analytical Method
EPA 6200B MADEP VPH
Contaminant of Concern
BenzeneTolueneEthylbenzeneXylenesMTBEC5-C8 AliphaticsC9-C12 AliphaticsUnadjusted C9-C10 AromaticsEDBEPA 625.1 MADEP EPH
Page 1 of 1

APPENDICES

APPENDIX A
Pitt County Property Cards

APPENDIX B
Well Construction Record and Subsurface Log
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #8654
Address 5068 NC Highway 33 East Greenville, NC 27858
Boring Number MW-3 Date Drilled
Sample Method Grab Drilling Method Direct Push Technology
Completion Details0-0.5' grout, 0.5-1' bentonite, 1-12' sand; flush-mount, 2" Inner Casing, 0-2' riser, 2-12' screen
Driller Matthew Steele Log By Eric Eubanks
Lab Sample PID Depth
Depth Sample Interval(ft)ppm (feet)
0 0.0 - 0.5 Mulch/topsoil
0.5 - 6 Backfill
1
2 MW-3-2'
3
4
5
MW-3
6 GW 6 - 12 Direct Push; no recovery
Sample
7
8

9
10
11

12 Total depth = 12'
13
14

15
04/25/22
LITHOLOGY

APPENDIX C
State Correspondence
Site Name City / County /Pitt Incident #48218
Resp Pty Name / Contact Incident Mgr Region WAS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #0
Consultant / Project Mgr /Nicole M Long
Telephone / Fax Number /Task Authorization Number:1 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:Unk (Low)RRA Date:3/29/2022
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
2.600 1 /Sct1:Mob y $350.00 y $350.00 $350.00 /
3.397 1 /T.I.I.Mob y $100.00 y $100.00 $100.00 /
2.600 2A 12 /Sct1:DrFt y $50.00 y $600.00 $600.00 /
3.118 2A 12 /T.I.I. Ft y $5.00 y $60.00 $60.00 /
2.600 2A 12 /Sct1:SpvFt y $12.50 y $150.00 $150.00 /
2.600 #409 1 /8260+y $84.00 y $84.00 $84.00 /
2.600 #410 1 /8720BNA y $187.00 y $187.00 $187.00 /
2.600 #421 1 /VPH-S y $58.00 y $58.00 $58.00 /
2.600 #422 1 /EPH-S y $100.00 y $100.00 $100.00 /
2.600 #240 1 /6200++y $94.00 y $94.00 $94.00 /
2.600 #280 1 /504.1 y $45.00 y $45.00 $45.00 /
2.600 #330 1 /Pb y $14.00 y $14.00 $14.00 /
2.600 #301 1 /625BNA+y $208.00 y $208.00 $208.00 /
2.600 #341 1 /VPH-GW y $56.00 y $56.00 $56.00 /
2.600 #342 1 /EPH-GW y $100.00 y $100.00 $100.00 /
2.600 #272 1 /TrpBnlk y $66.00 y $66.00 $66.00 /
2.600 S/H 1 /Ship 0 $60.00 0 $60.00 $0.00 /
2.600 1 /Sct3:Othr y $2,300.00 y $2,300.00 $2,300.00 /
12.055 1 /T.I.I.Mob y $50.00 y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed3
TOTAL:$4,682.00 $4,622.00 TOTAL:
Total Standard Costs (Not Third Party)$4,682.00 $4,622.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:3/24/22 by:(PM)(Reserved for RO)
RO Review:4/4/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 4/21/2022
CO Review:4/20/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 8/1/2020
DIRECTED COSTS
Greenville
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Speedway 8654
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed,incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order"in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain within the Statute of Limitations.All ePATAs submitted within a claim are closed with that
claim,and may not be re-used in a separate submittal, even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
JME
TC
(Initials)
NML
Proposed
Units / Type
(Consultant)
JME for ABE
ActiveFALSE*
22-079 April 2022
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
NO
[e-mail]
Speedway, LLC
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
* Two prior releases confirmed onsite: 38440 (2013) closed via NRP NFA in 2014 and 38752 (2019) closed under existing Receptor Survey & NRP in 2019. ##
These releases must be incorporated into any eligibility determination for this new release. ##
SCH detected soils above TPH Action at spill bucket that failed hydrostatic testing (GRO=963 mg/kg & DRO=891 mg/kg). No GW sample collected in SCH.
Approved for LSA-equivalent event at site with prior confirmed releases, with costs as documented on SOW Trust Fund Claim Secondary Form C.1 based on >5
years since 2014 receptor survey and lack of GW sample in source area of this new confirmed release.
Lab sample shipping and handling included in Section 3: Other / Miscellaneous Costs, not as a line-item in Section 2 -Part B.

APPENDIX D
Laboratory Analytical Report
ANALYTICAL REPORT
May 09, 2022
Geological Resources- NC Speedway
Sample Delivery Group:L1487337
Samples Received:04/27/2022
Project Number:3386
Description:Speedway 8654
Site:8654
Report To:Ms. Nicole Long
113 West Firetower Rd
Ste G
Winterville, NC 28590
Entire Report Reviewed By:
May 09, 2022
[Preliminary Report]
Christl M Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 1 of 43
May 09, 2022
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 1 of 43
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TRIP BLANK L1487337-01 5
MW-3-2 L1487337-02 7
MW-3 L1487337-03 10
Qc: Quality Control Summary 14
Total Solids by Method 2540 G-2011 14
Metals (ICP) by Method 6010D 15
Volatile Petroleum Hydrocarbons by Method MADEPV 16
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 19
Volatile Organic Compounds (GC/MS) by Method 8260D 23
EDB / DBCP by Method 504.1 26
TPH by Method MADEPE 27
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 30
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 35
Gl: Glossary of Terms 41
Al: Accreditations & Locations 42
Sc: Sample Chain of Custody 43
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 2 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 2 of 43
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TRIP BLANK L1487337-01 GW Ethan Rogerson 04/26/22 14:30 04/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1856165 1 04/28/22 23:36 04/28/22 23:36 JAH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3-2 L1487337-02 Solid Ethan Rogerson 04/26/22 15:40 04/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1856225 1 04/29/22 18:54 04/29/22 19:04 KDW Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1857266 1 04/26/22 15:40 05/02/22 15:14 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1857901 1.01 04/26/22 15:40 05/04/22 09:20 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1858005 1 05/03/22 05:55 05/04/22 19:29 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1858005 1 05/03/22 05:55 05/05/22 01:01 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1859393 1 05/06/22 04:50 05/07/22 00:36 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1487337-03 GW Ethan Rogerson 04/26/22 14:45 04/27/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1857161 1 05/03/22 16:05 05/03/22 22:22 CCE Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1856767 1 04/30/22 09:39 04/30/22 09:39 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1856165 1 04/29/22 05:11 04/29/22 05:11 JAH Mt. Juliet, TN
EDB / DBCP by Method 504.1 WG1857459 1.08 05/03/22 07:40 05/03/22 21:37 HLA Mt. Juliet, TN
TPH by Method MADEPE WG1857535 1 05/02/22 05:16 05/03/22 13:36 JN Mt. Juliet, TN
TPH by Method MADEPE WG1857535 1 05/02/22 05:16 05/04/22 15:25 JN Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1857249 1 05/03/22 02:33 05/03/22 15:26 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 3 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 3 of 43
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Christl M Wagner
Project Manager
Project Narrative
Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH
Methods.

Sample Delivery Group (SDG) Narrative
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.
Lab Sample ID Project Sample ID Method
L1487337-03 MW-3 MADEPE
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 4 of 43
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 4 of 43
SAMPLE RESULTS - 01
L1487337
TRIP BLANK
Collected date/time: 04/26/22 14:30
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,1,1-Trichloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,1,2,2-Tetrachloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,1,2-Trichloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,1-Dichloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,1-Dichloroethene ND 1.00 1 04/28/2022 23:36 WG1856165
1,1-Dichloropropene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2,3-Trichlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2,3-Trichloropropane ND 2.50 1 04/28/2022 23:36 WG1856165
1,2,3-Trimethylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2,4-Trichlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2,4-Trimethylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2-Dibromo-3-Chloropropane ND 5.00 1 04/28/2022 23:36 WG1856165
1,2-Dibromoethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,2-Dichlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,2-Dichloroethane ND 1.00 1 04/28/2022 23:36 WG1856165
1,2-Dichloropropane ND 1.00 1 04/28/2022 23:36 WG1856165
1,3,5-Trimethylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,3-Dichlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
1,3-Dichloropropane ND 1.00 1 04/28/2022 23:36 WG1856165
1,4-Dichlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
2,2-Dichloropropane ND 1.00 1 04/28/2022 23:36 WG1856165
Benzene ND 1.00 1 04/28/2022 23:36 WG1856165
Bromobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
Bromochloromethane ND 1.00 1 04/28/2022 23:36 WG1856165
Bromodichloromethane ND 1.00 1 04/28/2022 23:36 WG1856165
Bromoform ND 1.00 1 04/28/2022 23:36 WG1856165
Carbon tetrachloride ND 1.00 1 04/28/2022 23:36 WG1856165
Chlorobenzene ND 1.00 1 04/28/2022 23:36 WG1856165
Chloroethane ND 5.00 1 04/28/2022 23:36 WG1856165
Chloroform ND 5.00 1 04/28/2022 23:36 WG1856165
Chlorodibromomethane ND 1.00 1 04/28/2022 23:36 WG1856165
Dichlorodifluoromethane ND 5.00 1 04/28/2022 23:36 WG1856165
Di-isopropyl ether ND 1.00 1 04/28/2022 23:36 WG1856165
Ethylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
Hexachloro-1,3-butadiene ND 1.00 1 04/28/2022 23:36 WG1856165
Isopropylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
Bromomethane ND 5.00 1 04/28/2022 23:36 WG1856165
Chloromethane ND 2.50 1 04/28/2022 23:36 WG1856165
Methyl tert-butyl ether ND 1.00 1 04/28/2022 23:36 WG1856165
Dibromomethane ND 1.00 1 04/28/2022 23:36 WG1856165
Methylene Chloride ND 5.00 1 04/28/2022 23:36 WG1856165
Naphthalene ND 5.00 1 04/28/2022 23:36 WG1856165
Styrene ND 1.00 1 04/28/2022 23:36 WG1856165
Tetrachloroethene ND 1.00 1 04/28/2022 23:36 WG1856165
Toluene ND 1.00 1 04/28/2022 23:36 WG1856165
Trichloroethene ND 1.00 1 04/28/2022 23:36 WG1856165
Trichlorofluoromethane ND 5.00 1 04/28/2022 23:36 WG1856165
Vinyl chloride ND 1.00 1 04/28/2022 23:36 WG1856165
Total Xylenes ND 3.00 1 04/28/2022 23:36 WG1856165
cis-1,2-Dichloroethene ND 1.00 1 04/28/2022 23:36 WG1856165
cis-1,3-Dichloropropene ND 1.00 1 04/28/2022 23:36 WG1856165
n-Butylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
n-Propylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
2-Chlorotoluene ND 1.00 1 04/28/2022 23:36 WG1856165
p-Isopropyltoluene ND 1.00 1 04/28/2022 23:36 WG1856165
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 5 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 5 of 43
SAMPLE RESULTS - 01
L1487337
TRIP BLANK
Collected date/time: 04/26/22 14:30
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorotoluene ND 1.00 1 04/28/2022 23:36 WG1856165
sec-Butylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
tert-Butylbenzene ND 1.00 1 04/28/2022 23:36 WG1856165
trans-1,2-Dichloroethene ND 1.00 1 04/28/2022 23:36 WG1856165
trans-1,3-Dichloropropene ND 1.00 1 04/28/2022 23:36 WG1856165
(S) Toluene-d8 110 80.0-120 04/28/2022 23:36 WG1856165
(S) 4-Bromofluorobenzene 104 77.0-126 04/28/2022 23:36 WG1856165
(S) 1,2-Dichloroethane-d4 99.1 70.0-130 04/28/2022 23:36 WG1856165
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 6 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 6 of 43
SAMPLE RESULTS - 02
L1487337
MW-3-2
Collected date/time: 04/26/22 15:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.5 1 04/29/2022 19:04 WG1856225
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 5.58 1 05/02/2022 15:14 WG1857266
Unadjusted C9-C12 Aliphatics ND 5.58 1 05/02/2022 15:14 WG1857266
Unadjusted C9-C10 Aromatics ND 5.58 1 05/02/2022 15:14 WG1857266
Adjusted C5-C8 Aliphatics ND 5.58 1 05/02/2022 15:14 WG1857266
Adjusted C9-C12 Aliphatics ND 5.58 1 05/02/2022 15:14 WG1857266
Total VPH ND 11.2 1 05/02/2022 15:14 WG1857266
Total Purgeable Hydrocarbons C5-C12 ND 11.2 1 05/02/2022 15:14 WG1857266
(S) 2,5-Dibromotoluene(FID)96.1 70.0-130 05/02/2022 15:14 WG1857266
(S) 2,5-Dibromotoluene(PID)75.7 70.0-130 05/02/2022 15:14 WG1857266
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,2,3-Trichlorobenzene ND C3 0.0141 1.01 05/04/2022 09:20 WG1857901
1,1,1-Trichloroethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,1,2,2-Tetrachloroethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,1,2-Trichloroethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,1-Dichloroethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,1-Dichloroethene ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,2,4-Trichlorobenzene ND 0.0141 1.01 05/04/2022 09:20 WG1857901
1,2,4-Trimethylbenzene 0.0607 0.00563 1.01 05/04/2022 09:20 WG1857901
1,2-Dibromo-3-Chloropropane ND 0.0282 1.01 05/04/2022 09:20 WG1857901
1,2-Dibromoethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,2-Dichlorobenzene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
1,2-Dichloroethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
1,2-Dichloropropane ND 0.00563 1.01 05/04/2022 09:20 WG1857901
1,3,5-Trimethylbenzene 0.0168 0.00563 1.01 05/04/2022 09:20 WG1857901
1,3-Dichlorobenzene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
1,4-Dichlorobenzene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
4-Methyl-2-pentanone (MIBK)ND 0.0282 1.01 05/04/2022 09:20 WG1857901
Acetone ND 0.0563 1.01 05/04/2022 09:20 WG1857901
Benzene ND 0.00113 1.01 05/04/2022 09:20 WG1857901
Bromodichloromethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Bromoform ND 0.0282 1.01 05/04/2022 09:20 WG1857901
Carbon tetrachloride ND 0.00563 1.01 05/04/2022 09:20 WG1857901
Chlorobenzene ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Chloroethane ND C3 0.00563 1.01 05/04/2022 09:20 WG1857901
Chloroform ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Chlorodibromomethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Ethylbenzene 0.00519 0.00282 1.01 05/04/2022 09:20 WG1857901
Isopropylbenzene ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Bromomethane ND 0.0141 1.01 05/04/2022 09:20 WG1857901
Chloromethane ND 0.0141 1.01 05/04/2022 09:20 WG1857901
2-Butanone (MEK)ND 0.113 1.01 05/04/2022 09:20 WG1857901
Methyl tert-butyl ether ND 0.00113 1.01 05/04/2022 09:20 WG1857901
Methylene Chloride ND 0.0282 1.01 05/04/2022 09:20 WG1857901
Naphthalene 0.0215 C3 0.0141 1.01 05/04/2022 09:20 WG1857901
Styrene ND 0.0141 1.01 05/04/2022 09:20 WG1857901
Tetrachloroethene 0.00501 0.00282 1.01 05/04/2022 09:20 WG1857901
Toluene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 7 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 7 of 43
SAMPLE RESULTS - 02
L1487337
MW-3-2
Collected date/time: 04/26/22 15:40
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Xylenes, Total 0.0601 0.00732 1.01 05/04/2022 09:20 WG1857901
Trichloroethene ND 0.00113 1.01 05/04/2022 09:20 WG1857901
Trichlorofluoromethane ND 0.00282 1.01 05/04/2022 09:20 WG1857901
Vinyl chloride ND C3 0.00282 1.01 05/04/2022 09:20 WG1857901
cis-1,2-Dichloroethene ND 0.00282 1.01 05/04/2022 09:20 WG1857901
cis-1,3-Dichloropropene ND 0.00282 1.01 05/04/2022 09:20 WG1857901
n-Butylbenzene ND C3 0.0141 1.01 05/04/2022 09:20 WG1857901
n-Propylbenzene 0.00584 0.00563 1.01 05/04/2022 09:20 WG1857901
sec-Butylbenzene ND 0.0141 1.01 05/04/2022 09:20 WG1857901
trans-1,2-Dichloroethene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
trans-1,3-Dichloropropene ND 0.00563 1.01 05/04/2022 09:20 WG1857901
Bromobenzene ND 0.0141 1.01 05/04/2022 09:20 WG1857901
(S) Toluene-d8 109 75.0-131 05/04/2022 09:20 WG1857901
(S) 4-Bromofluorobenzene 91.8 67.0-138 05/04/2022 09:20 WG1857901
(S) 1,2-Dichloroethane-d4 103 70.0-130 05/04/2022 09:20 WG1857901
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics ND 6.88 1 05/04/2022 19:29 WG1858005
Unadjusted C19-C36 Aliphatics ND 6.88 1 05/04/2022 19:29 WG1858005
Unadjusted C11-C22 Aromatics ND 6.88 1 05/05/2022 01:01 WG1858005
Unadjusted Total Petroleum
Hydrocarbons ND 6.88 1 05/05/2022 01:01 WG1858005
Adjusted C11-C22 Aromatics ND 6.88 1 05/05/2022 01:01 WG1858005
Adjusted Total Petroleum Hydrocarbons ND 6.88 1 05/05/2022 01:01 WG1858005
(S) o-Terphenyl 59.4 40.0-140 05/05/2022 01:01 WG1858005
(S) 1-Chloro-octadecane 50.8 40.0-140 05/04/2022 19:29 WG1858005
(S) 2-Fluorobiphenyl 79.3 40.0-140 05/05/2022 01:01 WG1858005
(S) 2-Bromonaphthalene 76.1 40.0-140 05/05/2022 01:01 WG1858005
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0352 1 05/07/2022 00:36 WG1859393
Acenaphthylene ND 0.0352 1 05/07/2022 00:36 WG1859393
Anthracene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzo(a)anthracene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzo(b)fluoranthene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzo(k)fluoranthene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzo(g,h,i)perylene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzo(a)pyrene ND 0.0352 1 05/07/2022 00:36 WG1859393
Bis(2-chlorethoxy)methane ND 0.352 1 05/07/2022 00:36 WG1859393
Bis(2-chloroethyl)ether ND 0.352 1 05/07/2022 00:36 WG1859393
2,2-Oxybis(1-Chloropropane)ND 0.352 1 05/07/2022 00:36 WG1859393
4-Bromophenyl-phenylether ND 0.352 1 05/07/2022 00:36 WG1859393
4-Chloroaniline ND 0.352 1 05/07/2022 00:36 WG1859393
2-Chloronaphthalene ND 0.0352 1 05/07/2022 00:36 WG1859393
4-Chlorophenyl-phenylether ND 0.352 1 05/07/2022 00:36 WG1859393
Chrysene ND 0.0352 1 05/07/2022 00:36 WG1859393
Dibenz(a,h)anthracene ND 0.0352 1 05/07/2022 00:36 WG1859393
Dibenzofuran ND 0.352 1 05/07/2022 00:36 WG1859393
1,4-Dichlorobenzene ND 0.352 1 05/07/2022 00:36 WG1859393
3,3-Dichlorobenzidine ND 0.352 1 05/07/2022 00:36 WG1859393
2,4-Dinitrotoluene ND 0.352 1 05/07/2022 00:36 WG1859393
2,6-Dinitrotoluene ND 0.352 1 05/07/2022 00:36 WG1859393
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 8 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 8 of 43
SAMPLE RESULTS - 02
L1487337
MW-3-2
Collected date/time: 04/26/22 15:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Fluoranthene ND 0.0352 1 05/07/2022 00:36 WG1859393
Fluorene ND 0.0352 1 05/07/2022 00:36 WG1859393
Hexachlorobenzene ND 0.352 1 05/07/2022 00:36 WG1859393
Hexachloro-1,3-butadiene ND 0.352 1 05/07/2022 00:36 WG1859393
Hexachlorocyclopentadiene ND 0.352 1 05/07/2022 00:36 WG1859393
Hexachloroethane ND 0.352 1 05/07/2022 00:36 WG1859393
Indeno(1,2,3-cd)pyrene ND 0.0352 1 05/07/2022 00:36 WG1859393
Isophorone ND 0.352 1 05/07/2022 00:36 WG1859393
1-Methylnaphthalene ND 0.0352 1 05/07/2022 00:36 WG1859393
2-Methylnaphthalene ND 0.0352 1 05/07/2022 00:36 WG1859393
Naphthalene ND 0.0352 1 05/07/2022 00:36 WG1859393
Nitrobenzene ND 0.352 1 05/07/2022 00:36 WG1859393
n-Nitrosodiphenylamine ND 0.352 1 05/07/2022 00:36 WG1859393
n-Nitrosodi-n-propylamine ND 0.352 1 05/07/2022 00:36 WG1859393
Phenanthrene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzylbutyl phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Bis(2-ethylhexyl)phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Di-n-butyl phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Diethyl phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Dimethyl phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Di-n-octyl phthalate ND 0.352 1 05/07/2022 00:36 WG1859393
Pyrene ND 0.0352 1 05/07/2022 00:36 WG1859393
Benzoic acid ND 1.77 1 05/07/2022 00:36 WG1859393
4-Chloro-3-methylphenol ND 0.352 1 05/07/2022 00:36 WG1859393
2-Chlorophenol ND 0.352 1 05/07/2022 00:36 WG1859393
2-Methylphenol ND 0.352 1 05/07/2022 00:36 WG1859393
3&4-Methyl Phenol ND 0.352 1 05/07/2022 00:36 WG1859393
2,4-Dichlorophenol ND 0.352 1 05/07/2022 00:36 WG1859393
2,4-Dimethylphenol ND 0.352 1 05/07/2022 00:36 WG1859393
4,6-Dinitro-2-methylphenol ND 0.352 1 05/07/2022 00:36 WG1859393
2,4-Dinitrophenol ND 0.352 1 05/07/2022 00:36 WG1859393
2-Nitrophenol ND 0.352 1 05/07/2022 00:36 WG1859393
4-Nitrophenol ND 0.352 1 05/07/2022 00:36 WG1859393
Pentachlorophenol ND 0.352 1 05/07/2022 00:36 WG1859393
Phenol ND 0.352 1 05/07/2022 00:36 WG1859393
Pyridine ND 0.352 1 05/07/2022 00:36 WG1859393
2,4,5-Trichlorophenol ND 0.352 1 05/07/2022 00:36 WG1859393
2,4,6-Trichlorophenol ND 0.352 1 05/07/2022 00:36 WG1859393
(S) 2-Fluorophenol 56.2 12.0-120 05/07/2022 00:36 WG1859393
(S) Phenol-d5 52.9 10.0-120 05/07/2022 00:36 WG1859393
(S) Nitrobenzene-d5 53.7 10.0-122 05/07/2022 00:36 WG1859393
(S) 2-Fluorobiphenyl 54.3 15.0-120 05/07/2022 00:36 WG1859393
(S) 2,4,6-Tribromophenol 62.3 10.0-127 05/07/2022 00:36 WG1859393
(S) p-Terphenyl-d14 49.7 10.0-120 05/07/2022 00:36 WG1859393
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 9 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 9 of 43
SAMPLE RESULTS - 03
L1487337
MW-3
Collected date/time: 04/26/22 14:45
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead 29.8 6.00 1 05/03/2022 22:22 WG1857161
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 04/30/2022 09:39 WG1856767
Unadjusted C9-C12 Aliphatics ND 100 1 04/30/2022 09:39 WG1856767
Unadjusted C9-C10 Aromatics ND 100 1 04/30/2022 09:39 WG1856767
Adjusted C5-C8 Aliphatics ND 100 1 04/30/2022 09:39 WG1856767
Adjusted C9-C12 Aliphatics ND 100 1 04/30/2022 09:39 WG1856767
Total VPH ND 200 1 04/30/2022 09:39 WG1856767
Total Purgeable Hydrocarbons C5-C12 ND 200 1 04/30/2022 09:39 WG1856767
(S) 2,5-Dibromotoluene(FID)103 70.0-130 04/30/2022 09:39 WG1856767
(S) 2,5-Dibromotoluene(PID)85.1 70.0-130 04/30/2022 09:39 WG1856767
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,1,1-Trichloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,1,2,2-Tetrachloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,1,2-Trichloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,1-Dichloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,1-Dichloroethene ND 1.00 1 04/29/2022 05:11 WG1856165
1,1-Dichloropropene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2,3-Trichlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2,3-Trichloropropane ND 2.50 1 04/29/2022 05:11 WG1856165
1,2,3-Trimethylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2,4-Trichlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2,4-Trimethylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2-Dibromo-3-Chloropropane ND 5.00 1 04/29/2022 05:11 WG1856165
1,2-Dibromoethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,2-Dichlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,2-Dichloroethane ND 1.00 1 04/29/2022 05:11 WG1856165
1,2-Dichloropropane ND 1.00 1 04/29/2022 05:11 WG1856165
1,3,5-Trimethylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,3-Dichlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
1,3-Dichloropropane ND 1.00 1 04/29/2022 05:11 WG1856165
1,4-Dichlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
2,2-Dichloropropane ND 1.00 1 04/29/2022 05:11 WG1856165
Benzene ND 1.00 1 04/29/2022 05:11 WG1856165
Bromobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
Bromochloromethane ND 1.00 1 04/29/2022 05:11 WG1856165
Bromodichloromethane ND 1.00 1 04/29/2022 05:11 WG1856165
Bromoform ND 1.00 1 04/29/2022 05:11 WG1856165
Carbon tetrachloride ND 1.00 1 04/29/2022 05:11 WG1856165
Chlorobenzene ND 1.00 1 04/29/2022 05:11 WG1856165
Chloroethane ND 5.00 1 04/29/2022 05:11 WG1856165
Chloroform ND 5.00 1 04/29/2022 05:11 WG1856165
Chlorodibromomethane ND 1.00 1 04/29/2022 05:11 WG1856165
Dichlorodifluoromethane ND 5.00 1 04/29/2022 05:11 WG1856165
Di-isopropyl ether ND 1.00 1 04/29/2022 05:11 WG1856165
Ethanol ND 100 1 04/29/2022 05:11 WG1856165
Ethylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
Hexachloro-1,3-butadiene ND 1.00 1 04/29/2022 05:11 WG1856165
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 10 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 10 of 43
SAMPLE RESULTS - 03
L1487337
MW-3
Collected date/time: 04/26/22 14:45
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isopropylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
Bromomethane ND 5.00 1 04/29/2022 05:11 WG1856165
Chloromethane ND 2.50 1 04/29/2022 05:11 WG1856165
Methyl tert-butyl ether ND 1.00 1 04/29/2022 05:11 WG1856165
Dibromomethane ND 1.00 1 04/29/2022 05:11 WG1856165
Methylene Chloride ND 5.00 1 04/29/2022 05:11 WG1856165
Naphthalene ND 5.00 1 04/29/2022 05:11 WG1856165
Styrene ND 1.00 1 04/29/2022 05:11 WG1856165
Tetrachloroethene ND 1.00 1 04/29/2022 05:11 WG1856165
Toluene ND 1.00 1 04/29/2022 05:11 WG1856165
Trichloroethene ND 1.00 1 04/29/2022 05:11 WG1856165
Trichlorofluoromethane ND 5.00 1 04/29/2022 05:11 WG1856165
Vinyl chloride ND 1.00 1 04/29/2022 05:11 WG1856165
Total Xylenes ND 3.00 1 04/29/2022 05:11 WG1856165
cis-1,2-Dichloroethene ND 1.00 1 04/29/2022 05:11 WG1856165
cis-1,3-Dichloropropene ND 1.00 1 04/29/2022 05:11 WG1856165
n-Butylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
n-Propylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
2-Chlorotoluene ND 1.00 1 04/29/2022 05:11 WG1856165
p-Isopropyltoluene ND 1.00 1 04/29/2022 05:11 WG1856165
4-Chlorotoluene ND 1.00 1 04/29/2022 05:11 WG1856165
sec-Butylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
tert-Butylbenzene ND 1.00 1 04/29/2022 05:11 WG1856165
trans-1,2-Dichloroethene ND 1.00 1 04/29/2022 05:11 WG1856165
trans-1,3-Dichloropropene ND 1.00 1 04/29/2022 05:11 WG1856165
Ethyl tert-butyl ether ND 1.00 1 04/29/2022 05:11 WG1856165
t-Amyl Alcohol ND 50.0 1 04/29/2022 05:11 WG1856165
tert-Butyl alcohol ND 5.00 1 04/29/2022 05:11 WG1856165
tert-Amyl Methyl Ether ND 1.00 1 04/29/2022 05:11 WG1856165
Tert-Amyl Ethyl Ether ND 1.00 1 04/29/2022 05:11 WG1856165
tert-Butyl Formate ND 20.0 1 04/29/2022 05:11 WG1856165
(S) Toluene-d8 108 80.0-120 04/29/2022 05:11 WG1856165
(S) 1,2-Dichloroethane-d4 98.0 70.0-130 04/29/2022 05:11 WG1856165
(S) 4-Bromofluorobenzene 104 77.0-126 04/29/2022 05:11 WG1856165
EDB / DBCP by Method 504.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide ND 0.0216 1.08 05/03/2022 21:37 WG1857459
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND J3 100 1 05/03/2022 13:36 WG1857535
Unadjusted C19-C36 Aliphatics ND 100 1 05/03/2022 13:36 WG1857535
Unadjusted C11-C22 Aromatics ND 100 1 05/04/2022 15:25 WG1857535
Unadjusted Total Petroleum
Hydrocarbons ND 100 1 05/04/2022 15:25 WG1857535
Adjusted C11-C22 Aromatics ND 100 1 05/04/2022 15:25 WG1857535
Adjusted Total Petroleum Hydrocarbons ND 100 1 05/04/2022 15:25 WG1857535
(S) o-Terphenyl 61.3 40.0-140 05/04/2022 15:25 WG1857535
(S) 1-Chloro-octadecane 45.9 40.0-140 05/03/2022 13:36 WG1857535
(S) 2-Fluorobiphenyl 84.6 40.0-140 05/04/2022 15:25 WG1857535
(S) 2-Bromonaphthalene 81.6 40.0-140 05/04/2022 15:25 WG1857535
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 11 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 11 of 43
SAMPLE RESULTS - 03
L1487337
MW-3
Collected date/time: 04/26/22 14:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1-Methylnaphthalene ND 1.00 1 05/03/2022 15:26 WG1857249
2,4,6-Trichlorophenol ND 10.0 1 05/03/2022 15:26 WG1857249
2,4-Dichlorophenol ND 10.0 1 05/03/2022 15:26 WG1857249
2,4-Dimethylphenol ND 10.0 1 05/03/2022 15:26 WG1857249
2,4-Dinitrophenol ND 10.0 1 05/03/2022 15:26 WG1857249
2,4-Dinitrotoluene ND 10.0 1 05/03/2022 15:26 WG1857249
2,6-Dinitrotoluene ND 10.0 1 05/03/2022 15:26 WG1857249
2-Chloronaphthalene ND J4 1.00 1 05/03/2022 15:26 WG1857249
2-Chlorophenol ND 10.0 1 05/03/2022 15:26 WG1857249
2-Methylnaphthalene ND 1.00 1 05/03/2022 15:26 WG1857249
2-Methylphenol ND 10.0 1 05/03/2022 15:26 WG1857249
2-Nitrophenol ND 10.0 1 05/03/2022 15:26 WG1857249
3,3-Dichlorobenzidine ND 10.0 1 05/03/2022 15:26 WG1857249
3&4-Methyl Phenol ND 10.0 1 05/03/2022 15:26 WG1857249
4,6-Dinitro-2-methylphenol ND 10.0 1 05/03/2022 15:26 WG1857249
4-Bromophenyl-phenylether ND 10.0 1 05/03/2022 15:26 WG1857249
4-Chloro-3-methylphenol ND 10.0 1 05/03/2022 15:26 WG1857249
4-Chloroaniline ND 10.0 1 05/03/2022 15:26 WG1857249
4-Chlorophenyl-phenylether ND 10.0 1 05/03/2022 15:26 WG1857249
4-Nitrophenol ND 10.0 1 05/03/2022 15:26 WG1857249
Acenaphthene ND 1.00 1 05/03/2022 15:26 WG1857249
Acenaphthylene ND 1.00 1 05/03/2022 15:26 WG1857249
Anthracene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzo(a)anthracene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzo(a)pyrene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzo(b)fluoranthene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzo(g,h,i)perylene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzo(k)fluoranthene ND 1.00 1 05/03/2022 15:26 WG1857249
Benzoic acid ND J4 50.0 1 05/03/2022 15:26 WG1857249
Bis(2-chlorethoxy)methane ND 10.0 1 05/03/2022 15:26 WG1857249
2,2-Oxybis(1-Chloropropane)ND 10.0 1 05/03/2022 15:26 WG1857249
Bis(2-ethylhexyl)phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Benzylbutyl phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Chrysene ND 1.00 1 05/03/2022 15:26 WG1857249
Di-n-butyl phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Di-n-octyl phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Dibenz(a,h)anthracene ND 1.00 1 05/03/2022 15:26 WG1857249
Dibenzofuran ND 10.0 1 05/03/2022 15:26 WG1857249
Diethyl phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Dimethyl phthalate ND 3.00 1 05/03/2022 15:26 WG1857249
Fluoranthene ND 1.00 1 05/03/2022 15:26 WG1857249
Fluorene ND 1.00 1 05/03/2022 15:26 WG1857249
Hexachlorobenzene ND 1.00 1 05/03/2022 15:26 WG1857249
Hexachloro-1,3-butadiene ND 10.0 1 05/03/2022 15:26 WG1857249
Hexachlorocyclopentadiene ND 10.0 1 05/03/2022 15:26 WG1857249
Hexachloroethane ND 10.0 1 05/03/2022 15:26 WG1857249
Indeno(1,2,3-cd)pyrene ND 1.00 1 05/03/2022 15:26 WG1857249
Isophorone ND 10.0 1 05/03/2022 15:26 WG1857249
n-Nitrosodi-n-propylamine ND 10.0 1 05/03/2022 15:26 WG1857249
n-Nitrosodiphenylamine ND 10.0 1 05/03/2022 15:26 WG1857249
Naphthalene ND 1.00 1 05/03/2022 15:26 WG1857249
Nitrobenzene ND 10.0 1 05/03/2022 15:26 WG1857249
Pentachlorophenol ND 10.0 1 05/03/2022 15:26 WG1857249
Phenanthrene ND 1.00 1 05/03/2022 15:26 WG1857249
Phenol ND 10.0 1 05/03/2022 15:26 WG1857249
Pyrene ND 1.00 1 05/03/2022 15:26 WG1857249
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 12 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 12 of 43
SAMPLE RESULTS - 03
L1487337
MW-3
Collected date/time: 04/26/22 14:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
(S) 2-Fluorophenol 20.7 10.0-120 05/03/2022 15:26 WG1857249
(S) Phenol-d5 14.0 8.00-424 05/03/2022 15:26 WG1857249
(S) Nitrobenzene-d5 67.1 15.0-314 05/03/2022 15:26 WG1857249
(S) 2-Fluorobiphenyl 48.5 22.0-127 05/03/2022 15:26 WG1857249
(S) 2,4,6-Tribromophenol 53.4 10.0-153 05/03/2022 15:26 WG1857249
(S) p-Terphenyl-d14 24.1 J2 29.0-141 05/03/2022 15:26 WG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier RDL Dilution Analysis Batch CAS #RT
Analyte ug/l ug/l date / time
Unknown-04 70.9 J N 0.000 1 05/03/2022 15:26 WG1857249 109773-69-5 14.53
Unknown-03 15.0 J N 0.000 1 05/03/2022 15:26 WG1857249 017455-13-9 14.48
Unknown-01 6.13 J N 0.000 1 05/03/2022 15:26 WG1857249 000622-80-0 3.86
Unknown-02 4.89 J N 0.000 1 05/03/2022 15:26 WG1857249 033100-27-5 14.31
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 13 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 13 of 43
QUALITY CONTROL SUMMARYWG1856225
Total Solids by Method 2540 G-2011 L1487337-02
Method Blank (MB)
(MB) R3786694-1 04/29/22 19:04
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1487353-06 Original Sample (OS) • Duplicate (DUP)
(OS) L1487353-06 04/29/22 19:04 • (DUP) R3786694-3 04/29/22 19:04
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 84.7 79.0 1 6.92 10
Laboratory Control Sample (LCS)
(LCS) R3786694-2 04/29/22 19:04
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 14 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 14 of 43
QUALITY CONTROL SUMMARYWG1857161
Metals (ICP) by Method 6010D L1487337-03
Method Blank (MB)
(MB) R3787772-1 05/03/22 21:26
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead U 2.99 6.00
Laboratory Control Sample (LCS)
(LCS) R3787772-2 05/03/22 21:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Lead 1000 976 97.6 80.0-120
L1486746-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1486746-02 05/03/22 21:31 • (MS) R3787772-4 05/03/22 21:37 • (MSD) R3787772-5 05/03/22 21:39
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Lead 1000 ND 955 989 95.5 98.9 1 75.0-125 3.51 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 15 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 15 of 43
QUALITY CONTROL SUMMARYWG1856767
Volatile Petroleum Hydrocarbons by Method MADEPV L1487337-03
Method Blank (MB)
(MB) R3787435-3 04/30/22 04:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Adjusted C5-C8 Aliphatics U 33.3 100
Adjusted C9-C12 Aliphatics U 33.3 100
Total VPH U 66.7 200
Total Purgeable Hydrocarbons
C5-C12 U 66.7 200
(S) 2,5-Dibromotoluene(FID)101 70.0-130
(S) 2,5-Dibromotoluene(PID)84.7 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787435-1 04/30/22 02:29 • (LCSD) R3787435-2 04/30/22 03:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1210 1260 101 105 70.0-130 4.05 50
Unadjusted C9-C12 Aliphatics 1400 1460 1410 104 101 70.0-130 3.48 50
Unadjusted C9-C10 Aromatics 200 180 168 90.0 84.0 70.0-130 6.90 50
Total VPH 2800 2850 2840 102 101 70.0-130 0.351 50
Total Purgeable Hydrocarbons
C5-C12 2800 2890 2880 103 103 70.0-130 0.347 50
(S) 2,5-Dibromotoluene(FID) 101 104 70.0-130
(S) 2,5-Dibromotoluene(PID) 84.0 89.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 16 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 16 of 43
QUALITY CONTROL SUMMARYWG1857266
Volatile Petroleum Hydrocarbons by Method MADEPV L1487337-02
Method Blank (MB)
(MB) R3787692-3 05/02/22 09:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics U 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Adjusted C5-C8 Aliphatics U 1.67 5.00
Adjusted C9-C12 Aliphatics U 1.67 5.00
Total VPH U 3.34 10.0
Total Purgeable Hydrocarbons
C5-C12 3.85 J 3.34 10.0
(S) 2,5-Dibromotoluene(FID)97.1 70.0-130
(S) 2,5-Dibromotoluene(PID)79.0 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787692-1 05/02/22 07:07 • (LCSD) R3787692-2 05/02/22 07:41
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 60.0 67.5 68.8 113 115 70.0-130 1.91 50
Unadjusted C9-C12 Aliphatics 70.0 70.8 70.4 101 101 70.0-130 0.567 50
Unadjusted C9-C10 Aromatics 10.0 8.39 8.18 83.9 81.8 70.0-130 2.53 50
Total VPH 140 147 147 105 105 70.0-130 0.000 50
Total Purgeable Hydrocarbons
C5-C12 140 148 149 106 106 70.0-130 0.673 50
(S) 2,5-Dibromotoluene(FID) 102 106 70.0-130
(S) 2,5-Dibromotoluene(PID) 86.4 88.8 70.0-130
L1487412-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487412-10 05/02/22 17:26 • (MS) R3787692-4 05/02/22 22:55 • (MSD) R3787692-5 05/02/22 23:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 47.4 ND 80.6 77.7 116 112 1 70.0-130 3.64 50
Unadjusted C9-C12 Aliphatics 55.3 ND 83.6 78.3 107 100 1 70.0-130 6.62 50
Unadjusted C9-C10 Aromatics 7.90 ND 10.2 9.78 93.7 90.1 1 70.0-130 3.86 50
Total VPH 111 ND 174 166 110 104 1 70.0-130 4.84 50
Total Purgeable Hydrocarbons C5-C12 111 ND 176 166 110 104 1 70.0-130 5.62 50
(S) 2,5-Dibromotoluene(FID) 102 100 70.0-130
(S) 2,5-Dibromotoluene(PID) 81.3 81.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 17 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 17 of 43
QUALITY CONTROL SUMMARYWG1857266
Volatile Petroleum Hydrocarbons by Method MADEPV L1487337-02
L1487447-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487447-01 05/02/22 09:53 • (MS) R3787692-6 05/03/22 00:01 • (MSD) R3787692-7 05/03/22 00:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 72.6 ND 78.2 84.5 108 116 1.08 70.0-130 7.71 50
Unadjusted C9-C12 Aliphatics 84.7 ND 86.8 99.6 103 118 1.08 70.0-130 13.7 50
Unadjusted C9-C10 Aromatics 12.1 ND 10.3 11.3 84.9 93.5 1.08 70.0-130 9.65 50
Total VPH 169 ND 175 195 100 112 1.08 70.0-130 10.9 50
Total Purgeable Hydrocarbons
C5-C12 169 ND 178 198 100 112 1.08 70.0-130 10.7 50
(S) 2,5-Dibromotoluene(FID) 102 99.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 82.6 79.6 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 18 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 18 of 43
QUALITY CONTROL SUMMARYWG1856165
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1487337-01,03
Method Blank (MB)
(MB) R3786814-3 04/28/22 22:40
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2-Trichloroethane U 0.158 1.00
1,1-Dichloropropene U 0.142 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,3-Trimethylbenzene U 0.104 1.00
1,2,4-Trimethylbenzene U 0.322 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichloropropane U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromochloromethane U 0.128 1.00
Bromoform U 0.129 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Dichlorodifluoromethane U 0.374 5.00
Di-isopropyl ether U 0.105 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Bromomethane U 0.605 5.00
Chloromethane U 0.960 2.50
Dibromomethane U 0.122 1.00
Naphthalene U 1.00 5.00
Styrene U 0.118 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
Vinyl chloride U 0.234 1.00
n-Butylbenzene U 0.157 1.00
n-Propylbenzene U 0.0993 1.00
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
trans-1,2-Dichloroethene U 0.149 1.00
trans-1,3-Dichloropropene U 0.118 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
1,1-Dichloroethane U 0.100 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 19 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 19 of 43
QUALITY CONTROL SUMMARYWG1856165
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1487337-01,03
Method Blank (MB)
(MB) R3786814-3 04/28/22 22:40
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1,1-Dichloroethene U 0.188 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,2-Dichloroethane U 0.0819 1.00
1,2-Dichloropropane U 0.149 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
1,3-Dichlorobenzene U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Bromodichloromethane U 0.136 1.00
Carbon tetrachloride U 0.128 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Ethanol U 42.0 100
Ethylbenzene U 0.137 1.00
Isopropylbenzene U 0.105 1.00
Methyl tert-butyl ether U 0.101 1.00
Methylene Chloride U 0.430 5.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
Xylenes, Total U 0.174 3.00
cis-1,2-Dichloroethene U 0.126 1.00
cis-1,3-Dichloropropene U 0.111 1.00
p-Isopropyltoluene U 0.120 1.00
Ethyl tert-butyl ether U 0.101 1.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl alcohol U 4.06 5.00
tert-Amyl Methyl Ether U 0.195 1.00
Tert-Amyl Ethyl Ether U 0.401 1.00
tert-Butyl formate U 4.51 20.0
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 98.4 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3786814-1 04/28/22 21:37
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1,1,2-Tetrachloroethane 5.00 4.88 97.6 75.0-125
1,1,2-Trichloroethane 5.00 5.03 101 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 20 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 20 of 43
QUALITY CONTROL SUMMARYWG1856165
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1487337-01,03
Laboratory Control Sample (LCS)
(LCS) R3786814-1 04/28/22 21:37
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,1-Dichloropropene 5.00 4.93 98.6 74.0-126
1,2,3-Trichlorobenzene 5.00 5.09 102 50.0-138
1,2,3-Trichloropropane 5.00 5.13 103 73.0-130
1,2,3-Trimethylbenzene 5.00 4.89 97.8 77.0-120
1,2,4-Trimethylbenzene 5.00 4.91 98.2 76.0-121
1,2-Dibromo-3-Chloropropane 5.00 3.97 79.4 58.0-134
1,2-Dibromoethane 5.00 5.25 105 80.0-122
1,2-Dichlorobenzene 5.00 5.25 105 79.0-121
1,3-Dichloropropane 5.00 5.08 102 80.0-120
1,4-Dichlorobenzene 5.00 5.19 104 79.0-120
Benzene 5.00 5.02 100 70.0-123
Bromobenzene 5.00 4.84 96.8 73.0-121
Bromochloromethane 5.00 5.15 103 76.0-122
Bromoform 5.00 4.20 84.0 68.0-132
Chlorobenzene 5.00 5.05 101 80.0-121
Chlorodibromomethane 5.00 4.58 91.6 77.0-125
Dichlorodifluoromethane 5.00 3.40 68.0 51.0-149
Di-isopropyl ether 5.00 4.71 94.2 58.0-138
Hexachloro-1,3-butadiene 5.00 5.12 102 54.0-138
Bromomethane 5.00 3.65 73.0 10.0-160
Chloromethane 5.00 4.17 83.4 41.0-142
Dibromomethane 5.00 4.93 98.6 80.0-120
Naphthalene 5.00 4.01 80.2 54.0-135
Styrene 5.00 4.92 98.4 73.0-130
Trichloroethene 5.00 5.40 108 78.0-124
Trichlorofluoromethane 5.00 5.06 101 59.0-147
Vinyl chloride 5.00 4.48 89.6 67.0-131
n-Butylbenzene 5.00 4.47 89.4 73.0-125
n-Propylbenzene 5.00 5.35 107 77.0-124
2-Chlorotoluene 5.00 5.11 102 76.0-123
4-Chlorotoluene 5.00 5.12 102 75.0-122
sec-Butylbenzene 5.00 5.29 106 75.0-125
tert-Butylbenzene 5.00 5.13 103 76.0-124
trans-1,2-Dichloroethene 5.00 4.73 94.6 73.0-120
trans-1,3-Dichloropropene 5.00 4.92 98.4 78.0-124
1,1,1-Trichloroethane 5.00 5.19 104 73.0-124
1,1,2,2-Tetrachloroethane 5.00 4.76 95.2 65.0-130
1,1-Dichloroethane 5.00 5.02 100 70.0-126
1,1-Dichloroethene 5.00 4.74 94.8 71.0-124
1,2,4-Trichlorobenzene 5.00 3.98 79.6 57.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 21 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 21 of 43
QUALITY CONTROL SUMMARYWG1856165
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1487337-01,03
Laboratory Control Sample (LCS)
(LCS) R3786814-1 04/28/22 21:37
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1,2-Dichloroethane 5.00 4.73 94.6 70.0-128
1,2-Dichloropropane 5.00 5.19 104 77.0-125
1,3,5-Trimethylbenzene 5.00 5.30 106 76.0-122
1,3-Dichlorobenzene 5.00 5.09 102 79.0-120
2,2-Dichloropropane 5.00 4.80 96.0 58.0-130
Bromodichloromethane 5.00 4.43 88.6 75.0-120
Carbon tetrachloride 5.00 5.07 101 68.0-126
Chloroethane 5.00 4.20 84.0 47.0-150
Chloroform 5.00 4.83 96.6 73.0-120
ethanol 250 251 100 10.0-160
Ethylbenzene 5.00 5.34 107 79.0-123
Isopropylbenzene 5.00 5.10 102 76.0-127
Methyl tert-butyl ether 5.00 4.63 92.6 68.0-125
Methylene Chloride 5.00 5.37 107 67.0-120
Tetrachloroethene 5.00 5.44 109 72.0-132
Toluene 5.00 5.19 104 79.0-120
Xylenes, Total 15.0 15.8 105 79.0-123
cis-1,2-Dichloroethene 5.00 4.81 96.2 73.0-120
cis-1,3-Dichloropropene 5.00 4.76 95.2 80.0-123
p-Isopropyltoluene 5.00 5.34 107 76.0-125
Ethyl tert-butyl ether 5.00 4.94 98.8 63.0-138
t-Amyl Alcohol 25.0 23.1 92.4 50.0-160
tert-Butyl alcohol 25.0 23.4 93.6 27.0-160
tert-Amyl Methyl Ether 5.00 4.72 94.4 66.0-125
Tert-Amyl Ethyl Ether 5.00 4.97 99.4 70.0-130
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 103 77.0-126
(S) 1,2-Dichloroethane-d4 99.8 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3786814-2 04/28/22 21:58
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl Formate 100 97.3 97.3 10.0-160
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 104 77.0-126
(S) 1,2-Dichloroethane-d4 103 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 22 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 22 of 43
QUALITY CONTROL SUMMARYWG1857901
Volatile Organic Compounds (GC/MS) by Method 8260D L1487337-02
Method Blank (MB)
(MB) R3787966-3 05/04/22 03:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,1-Dichloroethene U 0.000606 0.00250
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
1,2-Dichlorobenzene U 0.000425 0.00500
1,2-Dichloroethane U 0.000649 0.00250
1,2-Dichloropropane U 0.00142 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
1,3-Dichlorobenzene 0.000600 J 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Acetone U 0.0365 0.0500
Benzene U 0.000467 0.00100
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chlorodibromomethane U 0.000612 0.00250
Ethylbenzene U 0.000737 0.00250
Isopropylbenzene U 0.000425 0.00250
Bromomethane U 0.00197 0.0125
Chloromethane U 0.00435 0.0125
2-Butanone (MEK)U 0.0635 0.100
Methyl tert-butyl ether U 0.000350 0.00100
Methylene Chloride U 0.00664 0.0250
Naphthalene U 0.00488 0.0125
Styrene U 0.000229 0.0125
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
Xylenes, Total U 0.000880 0.00650
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 23 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 23 of 43
QUALITY CONTROL SUMMARYWG1857901
Volatile Organic Compounds (GC/MS) by Method 8260D L1487337-02
Method Blank (MB)
(MB) R3787966-3 05/04/22 03:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Vinyl chloride U 0.00116 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
cis-1,3-Dichloropropene U 0.000757 0.00250
n-Butylbenzene U 0.00525 0.0125
n-Propylbenzene U 0.000950 0.00500
sec-Butylbenzene U 0.00288 0.0125
trans-1,2-Dichloroethene U 0.00104 0.00500
trans-1,3-Dichloropropene U 0.00114 0.00500
Bromobenzene U 0.000900 0.0125
(S) Toluene-d8 106 75.0-131
(S) 4-Bromofluorobenzene 86.9 67.0-138
(S) 1,2-Dichloroethane-d4 100 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787966-1 05/04/22 02:15 • (LCSD) R3787966-2 05/04/22 02:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
1,2,3-Trichlorobenzene 0.125 0.0863 0.0889 69.0 71.1 59.0-139 2.97 20
1,1,1-Trichloroethane 0.125 0.119 0.120 95.2 96.0 69.0-126 0.837 20
1,1,2,2-Tetrachloroethane 0.125 0.116 0.110 92.8 88.0 68.0-128 5.31 20
1,1,2-Trichloroethane 0.125 0.118 0.120 94.4 96.0 78.0-123 1.68 20
1,1-Dichloroethane 0.125 0.109 0.111 87.2 88.8 70.0-127 1.82 20
1,1-Dichloroethene 0.125 0.108 0.108 86.4 86.4 65.0-131 0.000 20
1,2,4-Trichlorobenzene 0.125 0.108 0.125 86.4 100 62.0-137 14.6 20
1,2,4-Trimethylbenzene 0.125 0.109 0.106 87.2 84.8 70.0-126 2.79 20
1,2-Dibromo-3-Chloropropane 0.125 0.101 0.0953 80.8 76.2 59.0-130 5.81 20
1,2-Dibromoethane 0.125 0.120 0.118 96.0 94.4 74.0-128 1.68 20
1,2-Dichlorobenzene 0.125 0.114 0.122 91.2 97.6 76.0-124 6.78 20
1,2-Dichloroethane 0.125 0.109 0.115 87.2 92.0 65.0-131 5.36 20
1,2-Dichloropropane 0.125 0.101 0.102 80.8 81.6 74.0-125 0.985 20
1,3,5-Trimethylbenzene 0.125 0.103 0.0974 82.4 77.9 73.0-127 5.59 20
1,3-Dichlorobenzene 0.125 0.117 0.123 93.6 98.4 76.0-125 5.00 20
1,4-Dichlorobenzene 0.125 0.108 0.113 86.4 90.4 77.0-121 4.52 20
4-Methyl-2-pentanone (MIBK)0.625 0.648 0.666 104 107 56.0-143 2.74 20
Acetone 0.625 0.689 0.824 110 132 10.0-160 17.8 31
Benzene 0.125 0.105 0.110 84.0 88.0 70.0-123 4.65 20
Bromodichloromethane 0.125 0.121 0.121 96.8 96.8 73.0-121 0.000 20
Bromoform 0.125 0.117 0.121 93.6 96.8 64.0-132 3.36 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 24 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 24 of 43
QUALITY CONTROL SUMMARYWG1857901
Volatile Organic Compounds (GC/MS) by Method 8260D L1487337-02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787966-1 05/04/22 02:15 • (LCSD) R3787966-2 05/04/22 02:35
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.125 0.102 0.109 81.6 87.2 66.0-128 6.64 20
Chlorobenzene 0.125 0.120 0.117 96.0 93.6 76.0-128 2.53 20
Chloroethane 0.125 0.0951 0.0911 76.1 72.9 61.0-134 4.30 20
Chloroform 0.125 0.120 0.124 96.0 99.2 72.0-123 3.28 20
Chlorodibromomethane 0.125 0.121 0.127 96.8 102 74.0-127 4.84 20
Ethylbenzene 0.125 0.118 0.119 94.4 95.2 74.0-126 0.844 20
Isopropylbenzene 0.125 0.114 0.117 91.2 93.6 72.0-127 2.60 20
Bromomethane 0.125 0.130 0.129 104 103 56.0-147 0.772 20
Chloromethane 0.125 0.103 0.102 82.4 81.6 51.0-138 0.976 20
2-Butanone (MEK)0.625 0.627 0.626 100 100 30.0-160 0.160 24
Methyl tert-butyl ether 0.125 0.110 0.113 88.0 90.4 66.0-132 2.69 20
Methylene Chloride 0.125 0.111 0.118 88.8 94.4 68.0-123 6.11 20
Naphthalene 0.125 0.0752 0.0839 60.2 67.1 59.0-130 10.9 20
Styrene 0.125 0.113 0.120 90.4 96.0 72.0-127 6.01 20
Tetrachloroethene 0.125 0.136 0.127 109 102 70.0-136 6.84 20
Toluene 0.125 0.112 0.109 89.6 87.2 75.0-121 2.71 20
Xylenes, Total 0.375 0.344 0.354 91.7 94.4 72.0-127 2.87 20
Trichloroethene 0.125 0.125 0.122 100 97.6 76.0-126 2.43 20
Trichlorofluoromethane 0.125 0.111 0.114 88.8 91.2 61.0-142 2.67 20
Vinyl chloride 0.125 0.0932 0.0914 74.6 73.1 63.0-134 1.95 20
cis-1,2-Dichloroethene 0.125 0.117 0.116 93.6 92.8 73.0-125 0.858 20
cis-1,3-Dichloropropene 0.125 0.112 0.108 89.6 86.4 76.0-127 3.64 20
n-Butylbenzene 0.125 0.0954 0.104 76.3 83.2 68.0-135 8.63 20
n-Propylbenzene 0.125 0.115 0.109 92.0 87.2 74.0-126 5.36 20
sec-Butylbenzene 0.125 0.102 0.0975 81.6 78.0 74.0-130 4.51 20
trans-1,2-Dichloroethene 0.125 0.120 0.119 96.0 95.2 71.0-125 0.837 20
trans-1,3-Dichloropropene 0.125 0.114 0.107 91.2 85.6 73.0-127 6.33 20
Bromobenzene 0.125 0.121 0.119 96.8 95.2 73.0-121 1.67 20
(S) Toluene-d8 98.6 94.9 75.0-131
(S) 4-Bromofluorobenzene 93.0 97.6 67.0-138
(S) 1,2-Dichloroethane-d4 106 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 25 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 25 of 43
QUALITY CONTROL SUMMARYWG1857459
EDB / DBCP by Method 504.1 L1487337-03
Method Blank (MB)
(MB) R3788157-1 05/03/22 17:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ethylene Dibromide U 0.00536 0.0200
L1487046-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1487046-01 05/03/22 18:24 • (DUP) R3788157-3 05/03/22 18:12
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Ethylene Dibromide ND ND 1.15 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3788157-4 05/03/22 20:25 • (LCSD) R3788157-5 05/03/22 23:01
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ethylene Dibromide 0.250 0.309 0.305 124 122 70.0-130 1.30 20
L1486786-05 Original Sample (OS) • Matrix Spike (MS)
(OS) L1486786-05 05/03/22 18:00 • (MS) R3788157-2 05/03/22 17:47
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ethylene Dibromide 0.113 ND 0.115 102 1.13 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 26 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 26 of 43
QUALITY CONTROL SUMMARYWG1857535
TPH by Method MADEPE L1487337-03
Method Blank (MB)
(MB) R3787761-1 05/03/22 04:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 33.0 33.0 100
Unadjusted C19-C36 Aliphatics 35.0 J 33.0 100
(S) 1-Chloro-octadecane 62.4 40.0-140
Method Blank (MB)
(MB) R3787761-4 05/03/22 06:17
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.0 100
(S) o-Terphenyl 75.5 40.0-140
(S) 2-Fluorobiphenyl 80.7 40.0-140
(S) 2-Bromonaphthalene 82.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787761-2 05/03/22 05:10 • (LCSD) R3787761-3 05/03/22 05:43
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 422 323 70.3 53.8 40.0-140 J3 26.6 25
Unadjusted C19-C36 Aliphatics 800 582 549 72.8 68.6 40.0-140 5.84 25
(S) 1-Chloro-octadecane 68.3 63.2 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3787761-5 05/03/22 06:50 • (LCSD) R3787761-6 05/03/22 07:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1070 893 62.9 52.5 40.0-140 18.0 25
(S) o-Terphenyl 79.1 68.1 40.0-140
(S) 2-Fluorobiphenyl 85.8 86.8 40.0-140
(S) 2-Bromonaphthalene 88.6 89.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 27 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 27 of 43
QUALITY CONTROL SUMMARYWG1858005
TPH by Method MADEPE L1487337-02
Method Blank (MB)
(MB) R3788405-1 05/04/22 09:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) 1-Chloro-octadecane 51.1 40.0-140
Method Blank (MB)
(MB) R3788405-4 05/04/22 10:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) o-Terphenyl 63.7 40.0-140
(S) 2-Fluorobiphenyl 76.7 40.0-140
(S) 2-Bromonaphthalene 73.9 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3788405-2 05/04/22 09:52 • (LCSD) R3788405-3 05/04/22 10:14
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 23.8 25.8 59.6 64.7 40.0-140 8.06 25
Unadjusted C19-C36 Aliphatics 53.2 35.0 39.2 65.8 73.7 40.0-140 11.3 25
(S) 1-Chloro-octadecane 51.3 58.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3788405-5 05/04/22 10:59 • (LCSD) R3788405-6 05/04/22 11:21
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 82.6 87.7 73.1 77.6 40.0-140 5.99 25
(S) o-Terphenyl 66.5 69.7 40.0-140
(S) 2-Fluorobiphenyl 75.9 80.6 40.0-140
(S) 2-Bromonaphthalene 73.1 77.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 28 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 28 of 43
QUALITY CONTROL SUMMARYWG1858005
TPH by Method MADEPE L1487337-02
L1486494-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1486494-01 05/04/22 12:50 • (MS) R3788405-9 05/04/22 13:12 • (MSD) R3788405-10 05/04/22 13:34
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 138 ND 94.3 98.2 63.4 66.8 1 40.0-140 4.07 50
(S) o-Terphenyl 55.6 58.1 40.0-140
(S) 2-Fluorobiphenyl 83.3 79.7 40.0-140
(S) 2-Bromonaphthalene 79.5 76.1 40.0-140
L1486494-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1486494-01 05/06/22 01:38 • (MS) R3788405-7 05/04/22 12:05 • (MSD) R3788405-8 05/04/22 12:28
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 48.9 17.6 41.2 43.2 48.1 52.8 1 40.0-140 4.93 50
Unadjusted C9-C18 Aliphatics 48.9 17.6 41.2 45.2 48.1 56.8 1 40.0-140 9.36 50
Unadjusted C19-C36 Aliphatics 65.2 ND 41.3 36.7 63.3 56.8 1 40.0-140 11.6 50
Unadjusted C19-C36 Aliphatics 65.2 ND 41.3 38.9 63.3 60.2 1 40.0-140 5.80 50
(S) 1-Chloro-octadecane 47.7 45.6 40.0-140
(S) 1-Chloro-octadecane 47.7 49.2 40.0-140
L1486494-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1486494-01 05/06/22 01:38 • (MS) R3788405-11 05/06/22 02:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Unadjusted C9-C18 Aliphatics 48.9 17.6 44.0 53.9 1 40.0-140
Unadjusted C19-C36 Aliphatics 65.2 ND 44.2 67.9 1 40.0-140
(S) 1-Chloro-octadecane 52.4 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 29 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 29 of 43
QUALITY CONTROL SUMMARYWG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1487337-03
Method Blank (MB)
(MB) R3788080-2 05/03/22 11:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
1-Methylnaphthalene U 0.0790 1.00
2,4,6-Trichlorophenol U 0.100 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
2,4-Dinitrophenol U 5.93 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
2-Chloronaphthalene U 0.0648 1.00
2-Chlorophenol U 0.133 10.0
2-Methylnaphthalene U 0.117 1.00
2-Methylphenol U 0.0929 10.0
2-Nitrophenol U 0.117 10.0
3,3-Dichlorobenzidine U 0.212 10.0
3&4-Methyl Phenol U 0.168 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
4-Chloro-3-methylphenol U 0.131 10.0
4-Chloroaniline U 0.234 10.0
4-Chlorophenyl-phenylether U 0.0926 10.0
4-Nitrophenol U 0.143 10.0
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzo(a)anthracene U 0.199 1.00
Benzo(a)pyrene U 0.0381 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzoic Acid U 1.70 50.0
Bis(2-chlorethoxy)methane U 0.116 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Benzylbutyl phthalate U 0.765 3.00
Chrysene U 0.130 1.00
Di-n-butyl phthalate U 0.453 3.00
Di-n-octyl phthalate U 0.932 3.00
Dibenz(a,h)anthracene U 0.0644 1.00
Dibenzofuran U 0.0970 10.0
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 30 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 30 of 43
QUALITY CONTROL SUMMARYWG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1487337-03
Method Blank (MB)
(MB) R3788080-2 05/03/22 11:44
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
n-Nitrosodiphenylamine U 2.37 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
Pentachlorophenol U 0.313 10.0
Phenanthrene U 0.112 1.00
Phenol U 4.33 10.0
Pyrene U 0.107 1.00
(S) 2-Fluorophenol 29.4 10.0-120
(S) Phenol-d5 17.1 8.00-424
(S) Nitrobenzene-d5 55.6 15.0-314
(S) 2-Fluorobiphenyl 53.7 22.0-127
(S) 2,4,6-Tribromophenol 53.0 10.0-153
(S) p-Terphenyl-d14 50.0 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3788080-1 05/03/22 11:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
1-Methylnaphthalene 50.0 26.9 53.8 33.0-120
2,4,6-Trichlorophenol 50.0 28.6 57.2 37.0-144
2,4-Dichlorophenol 50.0 24.2 48.4 39.0-135
2,4-Dimethylphenol 50.0 25.0 50.0 32.0-120
2,4-Dinitrophenol 50.0 28.8 57.6 1.00-191
2,4-Dinitrotoluene 50.0 33.9 67.8 39.0-139
2,6-Dinitrotoluene 50.0 30.9 61.8 50.0-158
2-Chloronaphthalene 50.0 29.3 58.6 60.0-120 J4
2-Chlorophenol 50.0 27.2 54.4 23.0-134
2-Methylnaphthalene 50.0 26.8 53.6 35.0-120
2-Methylphenol 50.0 23.1 46.2 26.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 31 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 31 of 43
QUALITY CONTROL SUMMARYWG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1487337-03
Laboratory Control Sample (LCS)
(LCS) R3788080-1 05/03/22 11:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2-Nitrophenol 50.0 28.6 57.2 29.0-182
3,3-Dichlorobenzidine 100 60.4 60.4 1.00-262
3&4-Methyl Phenol 50.0 23.6 47.2 27.0-120
4,6-Dinitro-2-methylphenol 50.0 36.2 72.4 1.00-181
4-Bromophenyl-phenylether 50.0 31.5 63.0 53.0-127
4-Chloro-3-methylphenol 50.0 25.4 50.8 22.0-147
4-Chloroaniline 50.0 26.1 52.2 23.0-120
4-Chlorophenyl-phenylether 50.0 30.2 60.4 25.0-158
4-Nitrophenol 50.0 10.9 21.8 1.00-132
Acenaphthene 50.0 30.5 61.0 47.0-145
Acenaphthylene 50.0 31.2 62.4 33.0-145
Anthracene 50.0 28.6 57.2 27.0-133
Benzo(a)anthracene 50.0 29.7 59.4 33.0-143
Benzo(a)pyrene 50.0 29.4 58.8 17.0-163
Benzo(b)fluoranthene 50.0 28.5 57.0 24.0-159
Benzo(g,h,i)perylene 50.0 30.0 60.0 1.00-219
Benzo(k)fluoranthene 50.0 29.9 59.8 11.0-162
Benzoic Acid 100 6.55 6.55 10.0-120 J4
Bis(2-chlorethoxy)methane 50.0 29.6 59.2 1.00-219
2,2-Oxybis(1-Chloropropane)50.0 31.2 62.4 36.0-166
Bis(2-ethylhexyl)phthalate 50.0 27.8 55.6 8.00-158
Benzylbutyl phthalate 50.0 27.8 55.6 1.00-152
Chrysene 50.0 29.8 59.6 17.0-168
Di-n-butyl phthalate 50.0 32.1 64.2 1.00-120
Di-n-octyl phthalate 50.0 26.5 53.0 4.00-146
Dibenz(a,h)anthracene 50.0 30.2 60.4 1.00-227
Dibenzofuran 50.0 31.3 62.6 42.0-120
Diethyl phthalate 50.0 33.2 66.4 1.00-120
Dimethyl phthalate 50.0 31.2 62.4 1.00-120
Fluoranthene 50.0 29.7 59.4 26.0-137
Fluorene 50.0 29.6 59.2 59.0-121
Hexachlorobenzene 50.0 32.8 65.6 1.00-152
Hexachloro-1,3-butadiene 50.0 23.6 47.2 24.0-120
Hexachlorocyclopentadiene 50.0 14.2 28.4 10.0-120
Hexachloroethane 50.0 31.3 62.6 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 28.9 57.8 1.00-171
Isophorone 50.0 28.1 56.2 21.0-196
n-Nitrosodi-n-propylamine 50.0 34.3 68.6 1.00-230
n-Nitrosodiphenylamine 50.0 27.3 54.6 44.0-120
Naphthalene 50.0 27.0 54.0 21.0-133
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 32 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 32 of 43
QUALITY CONTROL SUMMARYWG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1487337-03
Laboratory Control Sample (LCS)
(LCS) R3788080-1 05/03/22 11:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Nitrobenzene 50.0 30.2 60.4 35.0-180
Pentachlorophenol 50.0 31.7 63.4 14.0-176
Phenanthrene 50.0 29.6 59.2 54.0-120
Phenol 50.0 10.3 20.6 5.00-120
Pyrene 50.0 26.4 52.8 52.0-120
(S) 2-Fluorophenol 31.6 10.0-120
(S) Phenol-d5 19.3 8.00-424
(S) Nitrobenzene-d5 54.6 15.0-314
(S) 2-Fluorobiphenyl 57.5 22.0-127
(S) 2,4,6-Tribromophenol 63.0 10.0-153
(S) p-Terphenyl-d14 51.4 29.0-141
L1487729-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487729-01 05/03/22 17:59 • (MS) R3788080-3 05/03/22 18:21 • (MSD) R3788080-4 05/03/22 18:42
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
1-Methylnaphthalene 50.0 ND 24.8 22.7 49.6 45.4 1 33.0-120 8.84 23
2,4,6-Trichlorophenol 50.0 ND 24.8 22.6 49.6 45.2 1 37.0-144 9.28 58
2,4-Dichlorophenol 50.0 ND 21.7 19.3 43.4 38.6 1 39.0-135 J6 11.7 50
2,4-Dimethylphenol 50.0 ND 24.4 21.5 48.0 42.2 1 32.0-120 12.6 58
2,4-Dinitrophenol 50.0 ND 29.3 20.3 58.6 40.6 1 1.00-191 36.3 132
2,4-Dinitrotoluene 50.0 ND 31.7 30.0 63.4 60.0 1 39.0-139 5.51 42
2,6-Dinitrotoluene 50.0 ND 29.5 27.0 59.0 54.0 1 50.0-158 8.85 48
2-Chloronaphthalene 50.0 ND 26.2 24.5 52.4 49.0 1 60.0-120 J6 J6 6.71 24
2-Chlorophenol 50.0 ND 24.3 21.6 48.6 43.2 1 23.0-134 11.8 61
2-Methylnaphthalene 50.0 ND 24.2 22.6 48.4 45.2 1 13.0-142 6.84 29
2-Methylphenol 50.0 ND 22.0 19.3 44.0 38.6 1 14.0-120 13.1 29
2-Nitrophenol 50.0 ND 25.1 22.2 50.2 44.4 1 29.0-182 12.3 55
3,3-Dichlorobenzidine 100 ND 20.8 24.4 20.8 24.4 1 1.00-262 15.9 108
3&4-Methyl Phenol 50.0 ND 22.1 20.0 42.0 37.8 1 13.0-124 9.98 26
4,6-Dinitro-2-methylphenol 50.0 ND 31.4 24.8 62.8 49.6 1 1.00-181 23.5 203
4-Bromophenyl-phenylether 50.0 ND 30.5 28.7 61.0 57.4 1 53.0-127 6.08 43
4-Chloro-3-methylphenol 50.0 ND 24.4 22.3 48.8 44.6 1 22.0-147 8.99 73
4-Chloroaniline 50.0 ND 21.8 20.9 43.6 41.8 1 10.0-137 4.22 33
4-Chlorophenyl-phenylether 50.0 ND 27.5 25.2 55.0 50.4 1 25.0-158 8.73 61
4-Nitrophenol 50.0 ND 11.4 ND 22.8 18.9 1 1.00-132 18.6 131
Acenaphthene 50.0 ND 27.9 25.8 55.8 51.6 1 47.0-145 7.82 48
Acenaphthylene 50.0 ND 28.3 26.4 56.6 52.8 1 33.0-145 6.95 74
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 33 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 33 of 43
QUALITY CONTROL SUMMARYWG1857249
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1487337-03
L1487729-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487729-01 05/03/22 17:59 • (MS) R3788080-3 05/03/22 18:21 • (MSD) R3788080-4 05/03/22 18:42
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Anthracene 50.0 ND 27.3 25.7 54.6 51.4 1 27.0-133 6.04 66
Benzo(a)anthracene 50.0 ND 28.2 26.4 56.4 52.8 1 33.0-143 6.59 53
Benzo(a)pyrene 50.0 ND 28.9 27.2 57.8 54.4 1 17.0-163 6.06 72
Benzo(b)fluoranthene 50.0 ND 27.8 26.4 55.6 52.8 1 24.0-159 5.17 71
Benzo(g,h,i)perylene 50.0 ND 27.1 25.3 54.2 50.6 1 1.00-219 6.87 97
Benzo(k)fluoranthene 50.0 ND 27.5 26.8 55.0 53.6 1 11.0-162 2.58 63
Benzoic Acid 100 ND ND ND 24.4 14.5 1 10.0-120 J3 50.9 40
Bis(2-chlorethoxy)methane 50.0 ND 26.7 24.2 53.4 48.4 1 33.0-184 9.82 54
2,2-Oxybis(1-Chloropropane)50.0 ND 28.4 25.7 56.8 51.4 1 36.0-166 9.98 76
Bis(2-ethylhexyl)phthalate 50.0 ND 28.4 27.0 56.8 54.0 1 8.00-158 5.05 82
Benzylbutyl phthalate 50.0 ND 29.0 27.3 58.0 54.6 1 1.00-152 6.04 60
Chrysene 50.0 ND 28.2 26.3 56.4 52.6 1 17.0-168 6.97 87
Di-n-butyl phthalate 50.0 ND 31.1 29.6 62.2 59.2 1 1.00-120 4.94 47
Di-n-octyl phthalate 50.0 ND 27.7 26.0 55.4 52.0 1 4.00-146 6.33 69
Dibenz(a,h)anthracene 50.0 ND 27.3 25.5 54.6 51.0 1 1.00-227 6.82 126
Dibenzofuran 50.0 ND 28.2 26.3 56.4 52.6 1 17.0-150 6.97 27
Diethyl phthalate 50.0 ND 30.3 28.6 60.6 57.2 1 1.00-120 5.77 100
Dimethyl phthalate 50.0 ND 28.6 26.7 57.2 53.4 1 1.00-120 6.87 183
Fluoranthene 50.0 ND 28.7 27.0 57.4 54.0 1 26.0-137 6.10 66
Fluorene 50.0 ND 27.2 25.5 54.4 51.0 1 59.0-121 J6 J6 6.45 38
Hexachlorobenzene 50.0 ND 29.6 27.9 59.2 55.8 1 1.00-152 5.91 55
Hexachloro-1,3-butadiene 50.0 ND 21.3 19.3 42.6 38.6 1 24.0-120 9.85 62
Hexachlorocyclopentadiene 50.0 ND 15.8 14.3 31.6 28.6 1 10.0-146 9.97 34
Hexachloroethane 50.0 ND 27.9 24.7 55.8 49.4 1 40.0-120 12.2 52
Indeno(1,2,3-cd)pyrene 50.0 ND 27.2 25.4 54.4 50.8 1 1.00-171 6.84 99
Isophorone 50.0 ND 26.0 24.1 52.0 48.2 1 21.0-196 7.58 93
n-Nitrosodi-n-propylamine 50.0 ND 32.0 29.7 64.0 59.4 1 1.00-230 7.46 87
n-Nitrosodiphenylamine 50.0 ND 26.8 25.0 53.6 50.0 1 16.0-160 6.95 28
Naphthalene 50.0 ND 24.0 22.1 48.0 44.2 1 21.0-133 8.24 65
Nitrobenzene 50.0 ND 26.8 24.7 53.6 49.4 1 35.0-180 8.16 62
Pentachlorophenol 50.0 ND 30.6 24.8 61.2 49.6 1 14.0-176 20.9 86
Phenanthrene 50.0 ND 27.4 26.1 54.8 52.2 1 54.0-120 J6 4.86 39
Phenol 50.0 ND ND ND 18.8 16.7 1 5.00-120 11.6 64
Pyrene 50.0 ND 26.4 25.0 52.8 50.0 1 52.0-120 J6 5.45 49
(S) 2-Fluorophenol 29.2 24.5 10.0-120
(S) Phenol-d5 18.6 16.1 8.00-424
(S) Nitrobenzene-d5 51.2 44.8 15.0-314
(S) 2-Fluorobiphenyl 52.1 47.9 22.0-127
(S) 2,4,6-Tribromophenol 56.0 53.5 10.0-153
(S) p-Terphenyl-d14 53.1 49.3 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 34 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 34 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
Method Blank (MB)
(MB) R3789566-2 05/06/22 16:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
4-Chloroaniline U 0.0120 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
Dibenzofuran U 0.0109 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
1-Methylnaphthalene U 0.00426 0.0333
2-Methylnaphthalene U 0.00432 0.0333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 35 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 35 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
Method Blank (MB)
(MB) R3789566-2 05/06/22 16:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
Benzoic Acid U 0.118 1.67
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2-Methylphenol U 0.0100 0.333
3&4-Methyl Phenol U 0.0104 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
Pyridine U 0.0220 0.333
2,4,5-Trichlorophenol U 0.0113 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 68.8 12.0-120
(S) Phenol-d5 65.8 10.0-120
(S) Nitrobenzene-d5 64.9 10.0-122
(S) 2-Fluorobiphenyl 65.2 15.0-120
(S) 2,4,6-Tribromophenol 65.3 10.0-127
(S) p-Terphenyl-d14 60.4 10.0-120
Laboratory Control Sample (LCS)
(LCS) R3789566-1 05/06/22 15:48
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.451 67.7 38.0-120
Acenaphthylene 0.666 0.496 74.5 40.0-120
Anthracene 0.666 0.496 74.5 42.0-120
Benzo(a)anthracene 0.666 0.501 75.2 44.0-120
Benzo(b)fluoranthene 0.666 0.448 67.3 43.0-120
Benzo(k)fluoranthene 0.666 0.459 68.9 44.0-120
Benzo(g,h,i)perylene 0.666 0.480 72.1 43.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 36 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 36 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
Laboratory Control Sample (LCS)
(LCS) R3789566-1 05/06/22 15:48
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Benzo(a)pyrene 0.666 0.540 81.1 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.387 58.1 20.0-120
Bis(2-chloroethyl)ether 0.666 0.486 73.0 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.414 62.2 23.0-120
4-Bromophenyl-phenylether 0.666 0.468 70.3 40.0-120
4-Chloroaniline 0.666 0.363 54.5 18.0-120
2-Chloronaphthalene 0.666 0.458 68.8 35.0-120
4-Chlorophenyl-phenylether 0.666 0.475 71.3 40.0-120
Chrysene 0.666 0.460 69.1 43.0-120
Dibenz(a,h)anthracene 0.666 0.491 73.7 44.0-120
Dibenzofuran 0.666 0.475 71.3 44.0-120
1,4-Dichlorobenzene 0.666 0.413 62.0 31.0-120
3,3-Dichlorobenzidine 1.33 1.02 76.7 28.0-120
2,4-Dinitrotoluene 0.666 0.565 84.8 45.0-120
2,6-Dinitrotoluene 0.666 0.515 77.3 42.0-120
Fluoranthene 0.666 0.497 74.6 44.0-120
Fluorene 0.666 0.477 71.6 41.0-120
Hexachlorobenzene 0.666 0.437 65.6 39.0-120
Hexachloro-1,3-butadiene 0.666 0.371 55.7 15.0-120
Hexachlorocyclopentadiene 0.666 0.418 62.8 15.0-120
Hexachloroethane 0.666 0.422 63.4 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.511 76.7 45.0-120
Isophorone 0.666 0.395 59.3 23.0-120
1-Methylnaphthalene 0.666 0.384 57.7 34.0-120
2-Methylnaphthalene 0.666 0.383 57.5 34.0-120
Naphthalene 0.666 0.370 55.6 18.0-120
Nitrobenzene 0.666 0.405 60.8 17.0-120
n-Nitrosodiphenylamine 0.666 0.466 70.0 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.477 71.6 26.0-120
Phenanthrene 0.666 0.452 67.9 42.0-120
Benzylbutyl phthalate 0.666 0.455 68.3 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.455 68.3 41.0-120
Di-n-butyl phthalate 0.666 0.491 73.7 43.0-120
Diethyl phthalate 0.666 0.502 75.4 43.0-120
Dimethyl phthalate 0.666 0.488 73.3 43.0-120
Di-n-octyl phthalate 0.666 0.463 69.5 40.0-120
Pyrene 0.666 0.403 60.5 41.0-120
Benzoic Acid 1.33 0.351 26.4 10.0-120
4-Chloro-3-methylphenol 0.666 0.427 64.1 28.0-120
2-Chlorophenol 0.666 0.465 69.8 28.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 37 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 37 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
Laboratory Control Sample (LCS)
(LCS) R3789566-1 05/06/22 15:48
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Methylphenol 0.666 0.475 71.3 35.0-120
3&4-Methyl Phenol 0.666 0.533 80.0 42.0-120
2,4-Dichlorophenol 0.666 0.418 62.8 25.0-120
2,4-Dimethylphenol 0.666 0.414 62.2 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.513 77.0 16.0-120
2,4-Dinitrophenol 0.666 0.419 62.9 10.0-120
2-Nitrophenol 0.666 0.459 68.9 20.0-120
4-Nitrophenol 0.666 0.670 101 27.0-120
Pentachlorophenol 0.666 0.467 70.1 29.0-120
Phenol 0.666 0.462 69.4 28.0-120
Pyridine 0.666 0.252 37.8 10.0-120
2,4,5-Trichlorophenol 0.666 0.519 77.9 38.0-120
2,4,6-Trichlorophenol 0.666 0.509 76.4 37.0-120
(S) 2-Fluorophenol 70.1 12.0-120
(S) Phenol-d5 67.4 10.0-120
(S) Nitrobenzene-d5 58.9 10.0-122
(S) 2-Fluorobiphenyl 67.3 15.0-120
(S) 2,4,6-Tribromophenol 74.0 10.0-127
(S) p-Terphenyl-d14 59.8 10.0-120
L1487440-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487440-03 05/06/22 22:47 • (MS) R3789566-3 05/06/22 23:09 • (MSD) R3789566-4 05/06/22 23:30
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Acenaphthene 0.648 ND 0.456 0.496 50.2 55.0 1 18.0-120 8.32 32
Acenaphthylene 0.648 ND 0.505 0.546 56.2 61.2 1 25.0-120 7.79 32
Anthracene 0.648 ND 0.533 0.556 56.2 59.2 1 22.0-120 4.27 29
Benzo(a)anthracene 0.648 0.168 0.557 0.605 44.0 49.7 1 25.0-120 8.23 29
Benzo(b)fluoranthene 0.648 0.206 0.508 0.546 34.1 38.7 1 19.0-122 7.25 31
Benzo(k)fluoranthene 0.648 0.0728 0.468 0.504 44.7 49.0 1 23.0-120 7.30 30
Benzo(g,h,i)perylene 0.648 0.0975 0.481 0.490 43.3 44.7 1 10.0-120 1.97 33
Benzo(a)pyrene 0.648 0.162 0.591 0.616 48.5 51.6 1 24.0-120 4.07 30
Bis(2-chlorethoxy)methane 0.648 ND ND ND 44.4 48.6 1 10.0-120 8.32 34
Bis(2-chloroethyl)ether 0.648 ND 0.462 0.504 52.2 57.3 1 10.0-120 8.77 40
2,2-Oxybis(1-Chloropropane)0.648 ND ND ND 45.2 50.0 1 10.0-120 9.43 40
4-Bromophenyl-phenylether 0.648 ND 0.505 0.546 57.1 62.1 1 27.0-120 7.79 30
4-Chloroaniline 0.648 ND ND ND 40.3 41.9 1 10.0-120 3.39 36
2-Chloronaphthalene 0.648 ND 0.466 0.490 52.6 55.7 1 20.0-120 5.14 32
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 38 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 38 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
L1487440-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487440-03 05/06/22 22:47 • (MS) R3789566-3 05/06/22 23:09 • (MSD) R3789566-4 05/06/22 23:30
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
4-Chlorophenyl-phenylether 0.648 ND 0.482 0.541 54.5 61.5 1 24.0-120 11.5 29
Chrysene 0.648 0.169 0.511 0.556 38.6 43.9 1 21.0-120 8.45 29
Dibenz(a,h)anthracene 0.648 ND 0.496 0.520 53.1 56.2 1 10.0-120 4.84 32
Dibenzofuran 0.648 ND 0.486 0.527 52.2 57.2 1 24.0-120 8.09 30
1,4-Dichlorobenzene 0.648 ND ND ND 45.8 50.0 1 10.0-120 8.08 39
3,3-Dichlorobenzidine 1.30 ND 0.886 0.840 49.9 47.7 1 10.0-120 5.38 34
2,4-Dinitrotoluene 0.648 ND 0.578 0.646 65.3 73.4 1 30.0-120 11.2 31
2,6-Dinitrotoluene 0.648 ND 0.524 0.584 59.3 66.5 1 25.0-120 10.8 31
Fluoranthene 0.648 0.330 0.599 0.620 30.4 32.9 1 18.0-126 3.36 32
Fluorene 0.648 ND 0.485 0.526 53.7 58.7 1 25.0-120 8.11 30
Hexachlorobenzene 0.648 ND 0.466 0.511 52.6 58.1 1 27.0-120 9.23 28
Hexachloro-1,3-butadiene 0.648 ND ND ND 43.4 45.7 1 10.0-120 4.52 38
Hexachlorocyclopentadiene 0.648 ND ND ND 30.7 35.6 1 10.0-120 14.0 40
Hexachloroethane 0.648 ND ND ND 44.3 48.9 1 10.0-120 9.30 40
Indeno(1,2,3-cd)pyrene 0.648 0.120 0.557 0.571 49.4 51.3 1 10.0-120 2.42 32
Isophorone 0.648 ND ND ND 45.2 48.6 1 13.0-120 6.60 34
1-Methylnaphthalene 0.648 0.0679 0.416 0.438 39.4 42.1 1 10.0-120 5.11 36
2-Methylnaphthalene 0.648 0.0837 0.422 0.434 38.2 39.9 1 10.0-120 2.87 37
Naphthalene 0.648 0.0571 0.396 0.414 38.3 40.6 1 10.0-120 4.38 35
Nitrobenzene 0.648 ND ND ND 46.3 48.9 1 10.0-120 4.88 36
n-Nitrosodiphenylamine 0.648 ND ND ND 49.1 50.3 1 17.0-120 1.87 29
n-Nitrosodi-n-propylamine 0.648 ND 0.472 0.518 53.4 58.9 1 10.0-120 9.10 37
Phenanthrene 0.648 0.180 0.522 0.549 38.6 41.9 1 17.0-120 5.10 31
Benzylbutyl phthalate 0.648 ND 0.519 0.593 58.6 67.4 1 23.0-120 13.3 30
Bis(2-ethylhexyl)phthalate 0.648 ND 0.497 0.578 56.2 65.7 1 17.0-126 15.0 30
Di-n-butyl phthalate 0.648 ND 0.560 0.605 63.3 68.8 1 30.0-120 7.74 29
Diethyl phthalate 0.648 ND 0.522 0.575 59.0 65.4 1 26.0-120 9.71 28
Dimethyl phthalate 0.648 ND 0.500 0.561 56.5 63.8 1 25.0-120 11.6 29
Di-n-octyl phthalate 0.648 ND 0.549 0.612 62.0 69.6 1 21.0-123 10.8 29
Pyrene 0.648 0.202 0.466 0.507 29.8 34.6 1 16.0-121 8.43 32
Benzoic Acid 1.30 ND ND ND 50.2 46.2 1 10.0-152 8.01 40
4-Chloro-3-methylphenol 0.648 ND ND 0.472 50.2 53.7 1 15.0-120 6.26 30
2-Chlorophenol 0.648 ND ND 0.457 50.3 52.0 1 15.0-120 2.72 37
2-Methylphenol 0.648 ND ND ND 50.8 48.9 1 11.0-120 4.35 40
3&4-Methyl Phenol 0.648 ND 0.489 0.474 55.2 53.9 1 12.0-123 3.12 38
2,4-Dichlorophenol 0.648 ND ND ND 48.3 50.2 1 20.0-120 3.14 31
2,4-Dimethylphenol 0.648 ND ND ND 38.1 36.2 1 10.0-120 5.83 33
4,6-Dinitro-2-methylphenol 0.648 ND 0.606 0.627 68.5 71.3 1 10.0-120 3.32 39
2,4-Dinitrophenol 0.648 ND 0.624 0.625 70.5 71.1 1 10.0-121 0.219 40
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 39 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 39 of 43
QUALITY CONTROL SUMMARYWG1859393
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1487337-02
L1487440-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1487440-03 05/06/22 22:47 • (MS) R3789566-3 05/06/22 23:09 • (MSD) R3789566-4 05/06/22 23:30
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
2-Nitrophenol 0.648 ND 0.487 0.515 55.1 58.5 1 12.0-120 5.45 39
4-Nitrophenol 0.648 ND 0.729 0.763 82.4 86.8 1 10.0-137 4.57 32
Pentachlorophenol 0.648 ND 0.520 0.571 58.8 64.9 1 10.0-160 9.26 31
Phenol 0.648 ND ND 0.462 50.0 52.5 1 12.0-120 4.23 38
Pyridine 0.648 ND ND ND 36.0 39.9 1 10.0-120 9.80 40
2,4,5-Trichlorophenol 0.648 ND 0.545 0.608 61.6 69.1 1 20.0-120 10.9 30
2,4,6-Trichlorophenol 0.648 ND 0.489 0.530 55.2 60.2 1 19.0-120 8.04 32
(S) 2-Fluorophenol 51.9 57.3 12.0-120
(S) Phenol-d5 50.9 55.4 10.0-120
(S) Nitrobenzene-d5 44.4 49.7 10.0-122
(S) 2-Fluorobiphenyl 52.2 57.5 15.0-120
(S) 2,4,6-Tribromophenol 61.7 68.2 10.0-127
(S) p-Terphenyl-d14 49.1 58.4 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 40 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 40 of 43
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RT Retention Time.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low. Method sensitivity check is acceptable.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual concentration present in the sample.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 41 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 41 of 43

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 11:00 42 of 43
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 3386 L1487337 05/09/22 12:18 42 of 43